The shot noise thermometer

NASA Astrophysics Data System (ADS)

Spietz, Lafe Frederick

This thesis describes the development and testing of the shot noise thermometer, or SNT, a new kind of noise thermometer based on the combined thermal and shot noise of a tunnel junction in the non-superconducting state. In the shot noise thermometer, the noise power from a tunnel junction is measured as a function of the DC voltage across the junction, and the temperature is determined from the voltage dependence of the noise. This voltage dependence follows directly from the Fermi statistics of electrons in a metal, and is independent of the gain or noise temperature of the microwave amplifiers and detector used to measure the noise. Since the shot noise thermometer requires no calibration from an external temperature standard, it is a primary thermometer. In this thesis I demonstrate the operation of the shot noise thermometer over four orders of magnitude in temperature, from the base temperature of a dilution refrigerator to room temperature. Because of its wide range and the fact that it requires no outside calibration (it is a primary thermometer), the SNT is useful as a thermometer for general use in dilution refrigerators. In addition, the shot noise thermometer has sufficient accuracy to be useful as a potential temperature standard. This thesis discusses both of these applications as well as basic physics questions about the operation of the SNT and prospects for future development of the SNT technology.

A high-resolution x-ray spectrometer for a kaon mass measurement

NASA Astrophysics Data System (ADS)

Phelan, Kevin; Suzuki, Ken; Zmeskal, Johann; Tortorella, Daniele; Bühler, Matthias; Hertrich, Theo

2017-02-01

The ASPECT consortium (Adaptable Spectrometer Enabled by Cryogenic Technology) is currently constructing a generalised cryogenic platform for cryogenic detector work which will be able to accommodate a wide range of sensors. The cryogenics system is based on a small mechanical cooler with a further adiabatic demagnetisation stage and will work with cryogenic detectors at sub-Kelvin temperatures. The commercial aim of the consortium is to produce a compact, user-friendly device with an emphasis on reliability and portability which can easily be transported for specialised on-site work, such as beam-lines or telescope facilities. The cryogenic detector platform will accommodate a specially developed cryogenic sensor, either a metallic magnetic calorimeter or a magnetic penetration-depth thermometer. The detectors will be designed to work in various temperatures regions with an emphasis on optimising the various detector resolutions for specific temperatures. One resolution target is of about 10 eV at the energies range typically created in kaonic atoms experiments (soft x-ray energies). A following step will see the introduction of continuous, high-power, sub-Kelvin cooling which will bring the cryogenic basis for a high resolution spectrometer system to the market. The scientific goal of the project will produce an experimental set-up optimised for kaon-mass measurements performing high-resolution x-ray spectroscopy on a beam-line provided foreseeably by the J-PARC (Tokai, Japan) or DAΦNE (Frascati, Italy) facilities.

Clinical accuracy of tympanic thermometer and noncontact infrared skin thermometer in pediatric practice: an alternative for axillary digital thermometer.

PubMed

Apa, Hurşit; Gözmen, Salih; Bayram, Nuri; Çatkoğlu, Asl; Devrim, Fatma; Karaarslan, Utku; Günay, İlker; Ünal, Nurettin; Devrim, İlker

2013-09-01

The aim of this study was to compare the body temperature measurements of infrared tympanic and forehead noncontact thermometers with the axillary digital thermometer. Randomly selected 50 pediatric patients who were hospitalized in Dr Behcet Uz Children's Training and Research Hospital, Pediatric Infectious Disease Unit, between March 2012 and September 2012 were included in the study. Body temperature measurements were performed using an axillary thermometer (Microlife MT 3001), a tympanic thermometer (Microlife Ear Thermometer IR 100), and a noncontact thermometer (ThermoFlash LX-26). Fifty patients participated in this study. We performed 1639 temperature readings for every method. The average difference between the mean (SD) of both axillary and tympanic temperatures was -0.20°C (0.61°C) (95% confidence interval, -1.41°C to 1.00°C). The average difference between the mean (SD) of both axillary and forehead temperatures was -0.38 (0.55°C) (95% confidence interval, -1.47°C to 0.70°C). The Bland-Altman plot showed that most of the data points were tightly clustered around the zero line of the difference between the 2 temperature readings. With the use of the axillary method as the criterion standard, positive likelihood ratios were 17.9 and 16.5 and negative likelihood ratios were 0.2 and 0.4 for tympanic and forehead measurements, respectively. The results demonstrated that the infrared tympanic thermometer could be a good option in the measurement of fever in the pediatric population. The noncontact infrared thermometer is very useful for the screening of fever in the pediatric population, but it must be used with caution because it has a high value of bias.

Optical gamma thermometer

DOEpatents

Koster, Glen Peter; Xia, Hua; Lee, Boon Kwee

2013-08-06

An optical gamma thermometer includes a metal mass having a temperature proportional to a gamma flux within a core of a nuclear reactor, and an optical fiber cable for measuring the temperature of the heated metal mass. The temperature of the heated mass may be measured by using one or more fiber grating structures and/or by using scattering techniques, such as Raman, Brillouin, and the like. The optical gamma thermometer may be used in conjunction with a conventional reactor heat balance to calibrate the local power range monitors over their useful in-service life. The optical gamma thermometer occupies much less space within the in-core instrument tube and costs much less than the conventional gamma thermometer.

[The tympanic thermometer in pediatrics as an alternative to the mercury-in-glass thermometer].

PubMed

Vertedor-Hurtado, María Victoria; Padín-López, Susana; Carreira-Pastor, María José; López-Martínez, Julia María

2009-01-01

To determine the behavior of a new and smaller model of infrared thermometer cone and to assess whether it is an appropriate alternative to determine fever in children under 14-years-old. We performed a cross-sectional, descriptive study comparing the temperatures taken with a mercury thermometer with those taken by an infrared thermometer in children under 14-years-old. The researchers followed the manufacturer's instructions for use for each thermometer. The overall sample of 400 children was divided into two age groups. Group I consisted of children aged less than 2 years and group II of 2-14-years-old. In group I the rectal mercury thermometer was placed in the rectum for 3 minutes and the tympanic thermometer was used in rectal mode and placed in the right ear. In group II, the axillary mercury thermometer was placed for 8 minutes in the right axilla and the tympanic thermometer was used in the axillary mode. To analyze intraobserver bias, 50 patients were selected from the sample and their temperatures were simultaneously taken by two nurses from the team. The intraclass correlation coefficient (ICC) was used both to measure the reliability of the tympanic thermometer and to analyze intraobserver bias. Temperature measurements with both instruments showed an ICC of 0.91 (95% confidence interval [CI], 0.88-0.94) for group I and 0.90 (95% CI, 0.87-0.92) for group II. The reproducibility of the measurements taken by the two nurses in 50 patients showed an ICC of 0.97 (95% CI, 0.95-0.98) for the tympanic thermometer. The infrared thermometer is an appropriate device for rapidly measuring temperature in the emergency department. However, the measurements taken should be confirmed by another method when clinical decisions are based on temperature values.

Development of torodial magnetic thermometry to study new phenomena associated with the superfluid transition in liquid sup 4 He

DOE Office of Scientific and Technical Information (OSTI.GOV)

Duncan, R.V.

1988-01-01

A new type of paramagnetic susceptibility thermometry called toroidal magnetic thermometry (TMT) has been developed. These TMT thermometers have a thermal resolution of five nanoKelvin near the {sup 4}He superfluid transition temperature T{lambda} = 2.172K, making TMT roughly a factor of fifty times better in resolution than conventional germanium resistance thermometry which is commercially available. The dramatic improvement in thermal resolution provided by TMT has been used to observe new phenomena associated with the superfluid transition in pure liquid {sup 4}He. Such phenomena include a component of the thermal boundary (Kapitza) resistance R{sub K} which is singular at the superfluidmore » transition temperature T{lambda}. In addition to the boundary effects described above, these TMT thermometers have been used to detect the depression of T{lambda} be a heat current Q flowing through the liquid helium. When these values of {Delta}T{lambda}(Q) were used to calculate the depression of the superfluid density {Delta}{rho}{sub s}(Q) the results agreed well with a prediction based on the theory of Ginzburg and Pitaevskii. The calibration of the TMT thermometers provide high-resolution measurements of the a.c. paramagnetic susceptibility of their magnetic salt: Copper ammonium bromide (CAB). These calibration parameters, together with power dissipation data near the CAB Curie temperature {Tc} = 1.79K, provide information on the magnetic critical behavior of this nearly ideal Heisenberg ferromagnet. Throughout the detailed description of the TMT design, aspects of the CAB magnetic critical phenomena are discussed.« less

The kelvin redefined

NASA Astrophysics Data System (ADS)

Machin, Graham

2018-02-01

On 20 May 2019 it is anticipated that the most radical revision of the International System of Units (the SI), since its inception, will come into force. From that point, all the SI units will be based on defined values of fundamental constants of nature. In this paper the redefinition of the kelvin and its implications are considered. The topic will be introduced by discussing how the wording of the new definition of the kelvin developed. The kelvin redefinition is reliant on a secure low-uncertainty value of the Boltzmann constant; its determination by different physical methods and how the final definitive value for the kelvin redefinition was arrived at is discussed. The redefined kelvin will be implemented through a document known as the mise en pratique (i.e. the ‘practical realisation’) for the definition of the kelvin (MeP-K). The development and contents of the MeP-K will be described. There follows a discussion of contemporary primary thermometry, which is the bedrock on which a secure kelvin redefinition will be founded. Finally the paper ends with a discussion of the implications of the redefinition, for traceability, and, more widely, the practice of thermometry in general.

Validation of Calculations in a Digital Thermometer Firmware

NASA Astrophysics Data System (ADS)

Batagelj, V.; Miklavec, A.; Bojkovski, J.

2014-04-01

State-of-the-art digital thermometers are arguably remarkable measurement instruments, measuring outputs from resistance thermometers and/or thermocouples. Not only that they can readily achieve measuring accuracies in the parts-per-million range, but they also incorporate sophisticated algorithms for the transformation calculation of the measured resistance or voltage to temperature. These algorithms often include high-order polynomials, exponentials and logarithms, and must be performed using both standard coefficients and particular calibration coefficients. The numerical accuracy of these calculations and the associated uncertainty component must be much better than the accuracy of the raw measurement in order to be negligible in the total measurement uncertainty. In order for the end-user to gain confidence in these calculations as well as to conform to formal requirements of ISO/IEC 17025 and other standards, a way of validation of these numerical procedures performed in the firmware of the instrument is required. A software architecture which allows a simple validation of internal measuring instrument calculations is suggested. The digital thermometer should be able to expose all its internal calculation functions to the communication interface, so the end-user can compare the results of the internal measuring instrument calculation with reference results. The method can be regarded as a variation of the black-box software validation. Validation results on a thermometer prototype with implemented validation ability show that the calculation error of basic arithmetic operations is within the expected rounding error. For conversion functions, the calculation error is at least ten times smaller than the thermometer effective resolution for the particular probe type.

A new cryogenic diode thermometer

NASA Astrophysics Data System (ADS)

Courts, S. S.; Swinehart, P. R.; Yeager, C. J.

2002-05-01

While the introduction of yet another cryogenic diode thermometer is not earth shattering, a new diode thermometer, the DT-600 series, recently introduced by Lake Shore Cryotronics, possesses three features that make it unique among commercial diode thermometers. First, these diodes have been probed at the chip level, allowing for the availability of a bare chip thermometer matching a standard curve-an important feature in situations where real estate is at a premium (IR detectors), or where in-situ calibration is difficult. Second, the thermometry industry has assumed that interchangeability should be best at low temperatures. Thus, good interchangeability at room temperatures implies a very good interchangeability at cryogenic temperature, resulting in a premium priced sensor. The DT-600 series diode thermometer is available in an interchangeability band comparable to platinum RTDs with the added advantage of interchangeability to 2 K. Third, and most important, the DT-600 series diode does not exhibit an instability in the I-V characteristic in the 8 K to 20 K temperature range that is observed in other commercial diode thermometer devices [1]. This paper presents performance characteristics for the DT-600 series diode thermometer along with a comparison of I-V curves for this device and other commercial diode thermometers exhibiting an I-V instability.

Reconnection properties in Kelvin-Helmholtz instabilities

NASA Astrophysics Data System (ADS)

Vernisse, Y.; Lavraud, B.; Eriksson, S.; Gershman, D. J.; Dorelli, J.; Pollock, C. J.; Giles, B. L.; Aunai, N.; Avanov, L. A.; Burch, J.; Chandler, M. O.; Coffey, V. N.; Dargent, J.; Ergun, R.; Farrugia, C. J.; Genot, V. N.; Graham, D.; Hasegawa, H.; Jacquey, C.; Kacem, I.; Khotyaintsev, Y. V.; Li, W.; Magnes, W.; Marchaudon, A.; Moore, T. E.; Paterson, W. R.; Penou, E.; Phan, T.; Retino, A.; Schwartz, S. J.; Saito, Y.; Sauvaud, J. A.; Schiff, C.; Torbert, R. B.; Wilder, F. D.; Yokota, S.

2017-12-01

Kelvin-Helmholtz instabilities are particular laboratories to study strong guide field reconnection processes. In particular, unlike the usual dayside magnetopause, the conditions across the magnetopause in KH vortices are quasi-symmetric, with low differences in beta and magnetic shear angle. We study these properties by means of statistical analysis of the high-resolution data of the Magnetospheric Multiscale mission. Several events of Kelvin-Helmholtz instabilities pas the terminator plane and a long lasting dayside instabilities event where used in order to produce this statistical analysis. Early results present a consistency between the data and the theory. In addition, the results emphasize the importance of the thickness of the magnetopause as a driver of magnetic reconnection in low magnetic shear events.

About thermometers and temperature

NASA Astrophysics Data System (ADS)

Baldovin, M.; Puglisi, A.; Sarracino, A.; Vulpiani, A.

2017-11-01

We discuss a class of mechanical models of thermometers and their minimal requirements to determine the temperature for systems out of the common scope of thermometry. In particular we consider: (1) anharmonic chains with long time of thermalization, such as the Fermi-Pasta-Ulam (FPU) model; (2) systems with long-range interactions where the equivalence of ensembles does not always hold; (3) systems featuring absolute negative temperatures. We show that for all the three classes of systems a mechanical thermometer model can be designed: a temporal average of a suitable mechanical observable of the thermometer is sufficient to get an estimate of the system’s temperature. Several interesting lessons are learnt from our numerical study: (1) the long thermalization times in FPU-like systems do not affect the thermometer, which is not coupled to normal modes but to a group of microscopic degrees of freedom; (2) a thermometer coupled to a long-range system measures its microcanonical temperature, even at values of the total energy where its canonical temperature would be very different; (3) a thermometer to read absolute negative temperatures must have a bounded total energy (as the system), otherwise it heavily perturbs the system changing the sign of its temperature. Our study shows that in order to also work in a correct way in ‘non standard’ cases, the proper model of thermometer must have a special functional form, e.g. the kinetic part cannot be quadratic.

A validated non-linear Kelvin-Helmholtz benchmark for numerical hydrodynamics

NASA Astrophysics Data System (ADS)

Lecoanet, D.; McCourt, M.; Quataert, E.; Burns, K. J.; Vasil, G. M.; Oishi, J. S.; Brown, B. P.; Stone, J. M.; O'Leary, R. M.

2016-02-01

The non-linear evolution of the Kelvin-Helmholtz instability is a popular test for code verification. To date, most Kelvin-Helmholtz problems discussed in the literature are ill-posed: they do not converge to any single solution with increasing resolution. This precludes comparisons among different codes and severely limits the utility of the Kelvin-Helmholtz instability as a test problem. The lack of a reference solution has led various authors to assert the accuracy of their simulations based on ad hoc proxies, e.g. the existence of small-scale structures. This paper proposes well-posed two-dimensional Kelvin-Helmholtz problems with smooth initial conditions and explicit diffusion. We show that in many cases numerical errors/noise can seed spurious small-scale structure in Kelvin-Helmholtz problems. We demonstrate convergence to a reference solution using both ATHENA, a Godunov code, and DEDALUS, a pseudo-spectral code. Problems with constant initial density throughout the domain are relatively straightforward for both codes. However, problems with an initial density jump (which are the norm in astrophysical systems) exhibit rich behaviour and are more computationally challenging. In the latter case, ATHENA simulations are prone to an instability of the inner rolled-up vortex; this instability is seeded by grid-scale errors introduced by the algorithm, and disappears as resolution increases. Both ATHENA and DEDALUS exhibit late-time chaos. Inviscid simulations are riddled with extremely vigorous secondary instabilities which induce more mixing than simulations with explicit diffusion. Our results highlight the importance of running well-posed test problems with demonstrated convergence to a reference solution. To facilitate future comparisons, we include as supplementary material the resolved, converged solutions to the Kelvin-Helmholtz problems in this paper in machine-readable form.

RuO2 Thermometer for Ultra-Low Temperatures

NASA Technical Reports Server (NTRS)

Hait, Thomas; Shirron, Peter J.; DiPirro, Michael

2009-01-01

A small, high-resolution, low-power thermometer has been developed for use in ultra-low temperatures that uses multiple RuO2 chip resistors. The use of commercially available thick-film RuO2 chip resistors for measuring cryogenic temperatures is well known due to their low cost, long-term stability, and large resistance change.

Performance of Different Light Sources for the Absolute Calibration of Radiation Thermometers

NASA Astrophysics Data System (ADS)

Martín, M. J.; Mantilla, J. M.; del Campo, D.; Hernanz, M. L.; Pons, A.; Campos, J.

2017-09-01

The evolving mise en pratique for the definition of the kelvin (MeP-K) [1, 2] will, in its forthcoming edition, encourage the realization and dissemination of the thermodynamic temperature either directly (primary thermometry) or indirectly (relative primary thermometry) via fixed points with assigned reference thermodynamic temperatures. In the last years, the Centro Español de Metrología (CEM), in collaboration with the Instituto de Óptica of Consejo Superior de Investigaciones Científicas (IO-CSIC), has developed several setups for absolute calibration of standard radiation thermometers using the radiance method to allow CEM the direct dissemination of the thermodynamic temperature and the assignment of the thermodynamic temperatures to several fixed points. Different calibration facilities based on a monochromator and/or a laser and an integrating sphere have been developed to calibrate CEM's standard radiation thermometers (KE-LP2 and KE-LP4) and filter radiometer (FIRA2). This system is based on the one described in [3] placed in IO-CSIC. Different light sources have been tried and tested for measuring absolute spectral radiance responsivity: a Xe-Hg 500 W lamp, a supercontinuum laser NKT SuperK-EXR20 and a diode laser emitting at 6473 nm with a typical maximum power of 120 mW. Their advantages and disadvantages have been studied such as sensitivity to interferences generated by the laser inside the filter, flux stability generated by the radiant sources and so forth. This paper describes the setups used, the uncertainty budgets and the results obtained for the absolute temperatures of Cu, Co-C, Pt-C and Re-C fixed points, measured with the three thermometers with central wavelengths around 650 nm.

Thermometers: Understand the Options

MedlinePlus

... the options Thermometers come in a variety of styles. Understand the different types of thermometers and how ... MA. Fever in infants and children: Pathophysiology and management. http://www.uptodate.com/home. Accessed July 23, ...

Germanium resistance thermometer calibration at superfluid helium temperatures

NASA Technical Reports Server (NTRS)

Mason, F. C.

1985-01-01

The rapid increase in resistance of high purity semi-conducting germanium with decreasing temperature in the superfluid helium range of temperatures makes this material highly adaptable as a very sensitive thermometer. Also, a germanium thermometer exhibits a highly reproducible resistance versus temperature characteristic curve upon cycling between liquid helium temperatures and room temperature. These two factors combine to make germanium thermometers ideally suited for measuring temperatures in many cryogenic studies at superfluid helium temperatures. One disadvantage, however, is the relatively high cost of calibrated germanium thermometers. In space helium cryogenic systems, many such thermometers are often required, leading to a high cost for calibrated thermometers. The construction of a thermometer calibration cryostat and probe which will allow for calibrating six germanium thermometers at one time, thus effecting substantial savings in the purchase of thermometers is considered.

Mercury Thermometer Replacements in Chemistry Laboratories

ERIC Educational Resources Information Center

Foster, Barbara L.

2005-01-01

The consequences of broken mercury-in-glass thermometers in academic laboratories results in various health and environmental hazards, which needs to be replaced, by long-stem digital thermometers and non-mercury glass thermometers. The factors that should be considered during the mercury replacement process are types of applications in the…

Gamma thermometer based reactor core liquid level detector

DOEpatents

Burns, Thomas J.

1983-01-01

A system is provided which employs a modified gamma thermometer for determining the liquid coolant level within a nuclear reactor core. The gamma thermometer which normally is employed to monitor local core heat generation rate (reactor power), is modified by thermocouple junctions and leads to obtain an unambiguous indication of the presence or absence of coolant liquid at the gamma thermometer location. A signal processor generates a signal based on the thermometer surface heat transfer coefficient by comparing the signals from the thermocouples at the thermometer location. The generated signal is a direct indication of loss of coolant due to the change in surface heat transfer when coolant liquid drops below the thermometer location. The loss of coolant indication is independent of reactor power at the thermometer location. Further, the same thermometer may still be used for the normal power monitoring function.

Sub-Kelvin resistance thermometer

NASA Technical Reports Server (NTRS)

Castles, Stephen H. (Inventor)

1992-01-01

A device capable of accurate temperature measurement down to 0.01 K of a particular object is discussed. The device is comprised of the following: a heat sink wafer; a first conducting pad bonded near one end of the heat sink wafer; a second conducting pad bonded near the other end of the heat sink wafer; and an oblong doped semiconductor crystal such as germanium. The oblong doped semiconductor crystal has a third conducting pad bonded on its bottom surface with the oblong doped semiconductor crystal bonded to the heat sink wafer by having the fourth conducting pad bonded to the first conducting pad. A wire is bonded between the second and third conducting pads. Current and voltage wires bonded to the first and second conducting pads measure the change in resistance of the oblong doped semiconductor crystal; this indicates the temperature of the object whose temperature is to be measured.

Intraoperative body temperature control: esophageal thermometer versus infrared tympanic thermometer.

PubMed

Poveda, Vanessa de Brito; Nascimento, Ariane de Souza

2016-01-01

To verify the correlation between temperature measurements performed using an infrared tympanic thermometer and an esophageal thermometer during the intraoperative period. A longitudinal study of repeated measures was performed including subjects aged 18 years or older undergoing elective oncologic surgery of the digestive system, with anesthesia duration of at least 1 hour. Temperature measurements were performed simultaneously by a calibrated esophageal thermometer and by a calibrated infrared tympanic thermometer, with laboratory reading precision of ±0.2ºC. The operating room temperature remained between 19 and 21ºC. The study included 51 patients, mostly men (51%), white (80.4%). All patients were kept warm by a forced-air heating system, for an average of 264.14 minutes (SD = 87.7). The two temperature measurements showed no different behavior over time (p = 0.2205), however, tympanic measurements were consistently 1.24°C lower (p<0.0001). The tympanic thermometer presented reliable results but reflected lower temperatures than the esophageal thermometer. Verificar a correlação entre as medidas de temperatura realizadas por meio de um termômetro timpânico por infravermelho e por um termômetro esofágico, durante o período intraoperatório. Realizou-se um estudo longitudinal, de medidas repetidas, incluindo sujeitos com idade igual ou superior a 18 anos, submetidos à cirurgia oncológica eletiva do sistema digestório, com duração da anestesia de, no mínimo, 1 hora. As medidas de temperatura eram realizadas, ao mesmo tempo, por meio de um termômetro esofágico calibrado e por termômetro timpânico por infravermelho calibrado, com precisão de leitura em laboratório de ±0,2ºC. A temperatura da sala operatória permaneceu entre 19 e 21ºC. Foram incluídos 51 pacientes, em sua maioria homens (51%), brancos (80,4%). Todos os pacientes foram aquecidos com o sistema de ar forçado aquecido, em média por 264,14 minutos (DP = 87,7). As duas

21 CFR 880.2920 - Clinical mercury thermometer.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Clinical mercury thermometer. 880.2920 Section 880.2920 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... Devices § 880.2920 Clinical mercury thermometer. (a) Identification. A clinical mercury thermometer is a...

21 CFR 880.2920 - Clinical mercury thermometer.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Clinical mercury thermometer. 880.2920 Section 880... Devices § 880.2920 Clinical mercury thermometer. (a) Identification. A clinical mercury thermometer is a... mercury. (b) Classification. Class II (special controls). The device is exempt from the premarket...

21 CFR 880.2920 - Clinical mercury thermometer.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Clinical mercury thermometer. 880.2920 Section 880... Devices § 880.2920 Clinical mercury thermometer. (a) Identification. A clinical mercury thermometer is a... mercury. (b) Classification. Class II (special controls). The device is exempt from the premarket...

21 CFR 880.2920 - Clinical mercury thermometer.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Clinical mercury thermometer. 880.2920 Section 880... Devices § 880.2920 Clinical mercury thermometer. (a) Identification. A clinical mercury thermometer is a... mercury. (b) Classification. Class II (special controls). The device is exempt from the premarket...

21 CFR 880.2920 - Clinical mercury thermometer.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Clinical mercury thermometer. 880.2920 Section 880... Devices § 880.2920 Clinical mercury thermometer. (a) Identification. A clinical mercury thermometer is a... mercury. (b) Classification. Class II (special controls). The device is exempt from the premarket...

Genetically encoded ratiometric fluorescent thermometer with wide range and rapid response

PubMed Central

Nakano, Masahiro; Arai, Yoshiyuki; Kotera, Ippei; Okabe, Kohki; Kamei, Yasuhiro; Nagai, Takeharu

2017-01-01

Temperature is a fundamental physical parameter that plays an important role in biological reactions and events. Although thermometers developed previously have been used to investigate several important phenomena, such as heterogeneous temperature distribution in a single living cell and heat generation in mitochondria, the development of a thermometer with a sensitivity over a wide temperature range and rapid response is still desired to quantify temperature change in not only homeotherms but also poikilotherms from the cellular level to in vivo. To overcome the weaknesses of the conventional thermometers, such as a limitation of applicable species and a low temporal resolution, owing to the narrow temperature range of sensitivity and the thermometry method, respectively, we developed a genetically encoded ratiometric fluorescent temperature indicator, gTEMP, by using two fluorescent proteins with different temperature sensitivities. Our thermometric method enabled a fast tracking of the temperature change with a time resolution of 50 ms. We used this method to observe the spatiotemporal temperature change between the cytoplasm and nucleus in cells, and quantified thermogenesis from the mitochondria matrix in a single living cell after stimulation with carbonyl cyanide 4-(trifluoromethoxy)phenylhydrazone, which was an uncoupler of oxidative phosphorylation. Moreover, exploiting the wide temperature range of sensitivity from 5°C to 50°C of gTEMP, we monitored the temperature in a living medaka embryo for 15 hours and showed the feasibility of in vivo thermometry in various living species. PMID:28212432

[An ear thermometer based on infrared thermopiles sensor].

PubMed

Xie, Haiyuan; Qian, Mingli

2013-09-01

According to the development of body temperature measurement mode, an ear thermometer with infrared thermopiles sensor is designed for body thermometry Compared with oral thermometer, the accuracy of ear thermometer is acceptable.

Thermometer use among Mexican immigrant mothers in California.

PubMed

Schwartz, N; Guendelman, S; English, P

1997-11-01

A community-based household survey was utilized to assess the relationship between thermometer use, home treatment and utilization of health care services. Using a cross-sectional design, the study surveyed 688 low income Mexican origin mothers of children between the ages of 8 and 16 months in San Diego County. Mothers were asked how they determine that their child has fever and how often they use a thermometer. Nearly 40% of low income Mexican mothers interviewed in San Diego county never used a thermometer for determining childhood fever. Approximately two-thirds (64.7%) relied either primarily or exclusively on embodied methods such as visual observation or touch to determine fever in their child. A multivariate logistic regression analysis determined that low education and a separated or divorced marital status decreased the odds of thermometer use, whereas regular contact with the health care system doubled the likelihood of thermometer use. Mothers who relied on embodied methods were more likely to use over-the-counter medications than those who relied on thermometers; however, no significant differences were found between groups using other methods of home treatment. Fever determination modalities can be used to screen for lack of access to care and to provide for other health care needs in a culturally appropriate manner. While clinicians' expectations may include parental experience with temperature taking, current pediatric literature questions the need for home-based thermometer use. Possible alternatives to the traditional rectal thermometer might include digital thermometers and color coded thermometer strips.

Intraseasonal to interannual variability of Kelvin wave momentum fluxes as derived from high-resolution radiosonde data

DOE PAGES

Sjoberg, Jeremiah P.; Birner, Thomas; Johnson, Richard H.

2017-07-26

Observational estimates of Kelvin wave momentum fluxes in the tropical lower stratosphere remain challenging. Here we extend a method based on linear wave theory to estimate daily time series of these momentum fluxes from high-resolution radiosonde data. Daily time series are produced for sounding sites operated by the US Department of Energy (DOE) and from the recent Dynamics of the Madden–Julian Oscillation (DYNAMO) field campaign. Our momentum flux estimates are found to be robust to different data sources and processing and in quantitative agreement with estimates from prior studies. Testing the sensitivity to vertical resolution, our estimated momentum fluxes aremore » found to be most sensitive to vertical resolution greater than 1 km, largely due to overestimation of the vertical wavelength. Climatological analysis is performed over a selected 11-year span of data from DOE Atmospheric Radiation Measurement (ARM) radiosonde sites. Analyses of this 11-year span of data reveal the expected seasonal cycle of momentum flux maxima in boreal winter and minima in boreal summer, and variability associated with the quasi-biennial oscillation of maxima during easterly phase and minima during westerly phase. Comparison between periods with active convection that is either strongly or weakly associated with the Madden–Julian Oscillation (MJO) suggests that the MJO provides a nontrivial increase in the lowermost stratospheric momentum fluxes.« less

A silicon nanowire heater and thermometer

NASA Astrophysics Data System (ADS)

Zhao, Xingyan; Dan, Yaping

2017-07-01

In the thermal conductivity measurements of thermoelectric materials, heaters and thermometers made of the same semiconducting materials under test, forming a homogeneous system, will significantly simplify fabrication and integration. In this work, we demonstrate a high-performance heater and thermometer made of single silicon nanowires (SiNWs). The SiNWs are patterned out of a silicon-on-insulator wafer by CMOS-compatible fabrication processes. The electronic properties of the nanowires are characterized by four-probe and low temperature Hall effect measurements. The I-V curves of the nanowires are linear at small voltage bias. The temperature dependence of the nanowire resistance allows the nanowire to be used as a highly sensitive thermometer. At high voltage bias, the I-V curves of the nanowire become nonlinear due to the effect of Joule heating. The temperature of the nanowire heater can be accurately monitored by the nanowire itself as a thermometer.

Examination of biogenic selenium-containing nanosystems based on polyelectrolyte complexes by atomic force, Kelvin probe force and electron microscopy methods

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sukhanova, T. E., E-mail: tat-sukhanova@mail.ru; Vylegzhanina, M. E.; Valueva, S. V.

The morphology and electrical properties of biogenic selenium-containing nanosystems based on polyelectrolyte complexes (PECs) were examined using AFM, Kelvin Probe Force and electron microscopy methods. It has been found, that prepared nanostructures significantly differed in their morphological types and parameters. In particular, multilayers capsules can be produced via varying synthesis conditions, especially, the selenium–PEC mass ratio ν. At the “special point” (ν = 0.1), filled and hollow nano- and microcapsules are formed in the system. The multilayer character of the capsules walls is visible in the phase images. Kelvin Probe Force images showed the inhomogeneity of potential distribution in capsulesmore » and outside them.« less

Infrared Thermometers

ERIC Educational Resources Information Center

Schaefers, John

2006-01-01

An infrared (IR) thermometer lab offers the opportunity to give science students a chance to measure surface temperatures, utilizing off-the-shelf technology. Potential areas of study include astronomy (exoplanets), electromagnetic spectrum, chemistry, evaporation rates, anatomy, crystal formation, and water or liquids. This article presents one…

The Fourier-Kelvin Stellar Interferometer a Low Complexity, Low Cost Space Mission for High-Resolution Astronomy and Direct Exoplanet Detection

NASA Technical Reports Server (NTRS)

Barry, R. K.; Danchi, W. C.; Deming, L. D.; Richardson, L. J.; Kuchner, M. J.; Seager, S.; Frey, B. J.; Martino, A. J.; Lee, K. A.; Zuray, M.;

Usability evaluation of the digital anger thermometer app.

PubMed

Mattson, Donald C

2017-09-01

The digital anger thermometer is a prototype for a mobile application (app) for use with adults in anger management treatment. The digital anger thermometer incorporates standards of software development in addition to anger management resources from the Substance Abuse and Mental Health Services Administration. The digital anger thermometer underwent a usability study conducted by five expert reviewers. The results indicate that it is easy to learn, efficient, and ergonomically sound. However, it does not offer support features or user-error tolerance. The digital anger thermometer prototype requires additional usability studies and comparative research in order for it to become an actual mental health app.

Assessing the appropriateness of information on childhood fever in thermometer package leaflets: a systematic audit of thermometers available in the UK.

PubMed

Hernandez, Jose; Nicholson, Brian D; Thompson, Matthew

2015-06-01

Thermometers are found in most parents' homes, but little is known about the quality and accuracy of the information they provide, nor its consistency with current guidelines for managing fever. To compare information included with commonly available thermometers with National Institute for Health and Care Excellence (NICE) guidance for management of feverish illness in children. Systematic thermometer sampling from UK retailers between February 2013 and May 2013. Information was extracted from device packaging and leaflets on details and type of thermometer, instructions for use, normal ranges, and fever thresholds cited. This was compared with key parental recommendations from the 2013 NICE guidance on feverish illness in children. Associations were explored between cost of device and level of information. There were 123 thermometers identified (ranging from £0.99 to £69.99), none of which made explicit reference to NICE guidance. Most (n = 81, 65.9%) recommended use at a body site consistent with NICE guidance, but only 17 (13.8%) defined fever using the correct threshold (≥38.0°C), and few (n = 12, 9.8%) included advice on fever management, of which four suggested actions not advised by NICE. There was no association between thermometer cost and provision of information consistent with NICE guidance. Parents and caregivers have access to a large number of thermometers, yet they lack evidence-based information about fever detection and management, and in some cases contain misleading information. This represents a missed opportunity to disseminate best practices from guidelines for management of fever in children, and thermometer manufacturers are urged to include information consistent with current guidance. © British Journal of General Practice 2015.

PREFACE: Kelvin and Ireland

NASA Astrophysics Data System (ADS)

Flood, Raymond; McCartney, Mark; Whitaker, Andrew

2009-07-01

Sir Joseph Larmor unveiling the Kelvin memorial in the Botanic Gardens, Belfast on a rainy day in 1913 Sir Joseph Larmor unveiling the Kelvin memorial in the Botanic Gardens, Belfast on a rainy day in 1913 © The Ulster Museum: Hogg collection William Thomson, later Lord Kelvin, was born in Belfast in 1824, and his family had lived near Ballynahinch in the north of Ireland, quite close to Belfast, from the seventeenth century. At the time of Kelvin's birth, James Thomson, his father, was Professor of Mathematics at the Belfast Royal Academical Institution (Inst). However, following the death of his wife in 1830, James took up a new position as Professor at the University of Glasgow, and he and his children moved there in 1832. Apart from three years studying at Cambridge, and a very brief period immediately afterwards travelling and teaching in Cambridge, Kelvin was to spend the rest of his life in Glasgow, where he occupied the Chair of Natural Philosophy (or Physics) for 53 years. The natural assumption might be that his birth in Ireland was irrelevant to Kelvin's life and work, and that the fine monument erected in his honour in Belfast's Botanic Gardens, which is pictured on the front cover of this volume, was more a demonstration of civic pride than a recognition of an aspect of Kelvin's life which was important to him. The purpose of the meeting was to demon strate that this was not the case, that, great Glaswegian as he undoubtedly became, Kelvin always delighted in the title of Irishman. The influence of his father, very much an Ulsterman, was immense, and Kelvin and his siblings were to follow his non-sectarian and reforming approach. Also important for Kelvin was his Christian upbringing, which began in Belfast, and his beliefs were to play a role of importance in his life and indeed in much of his most important work, in particular that on thermodynamics. Two of his siblings returned to Belfast and spent much of their lives there, and Kelvin was a

Time's Up, Turkey--Pop-Up Thermometers

ERIC Educational Resources Information Center

Moyer, Richard; Everett, Susan

2009-01-01

Meat thermometers can be awkward to use in terms of placement and avoidance of bones. Because of these problems, each year 30 million Thanksgiving turkeys have a built-in thermometer that pops up when the turkey is properly cooked. Turkey timers are an example of how engineering solved a common, everyday problem. The following 5E learning cycle…

Accuracy of tympanic and infrared skin thermometers in children.

PubMed

Paes, B F; Vermeulen, K; Brohet, R M; van der Ploeg, T; de Winter, J P

2010-12-01

Rectal measurement is considered a gold standard in many healthcare systems for body temperature measurement in children. Although this method has several disadvantages, an ideal alternative thermometer has not yet been introduced. However tympanic and infrared skin thermometers are potential alternatives. A prospective cohort study was performed including 100 children between 0 and 18 years of age admitted to the general paediatric ward of Spaarne Hospital in The Netherlands between January and March 2009. The objectives of this study are to evaluate the accuracy of tympanic and two types of infrared skin thermometers (Beurer and Thermofocus) compared to rectal measurement and furthermore to evaluate the influence of different variables on temperature measurements. Compared to rectal measurement (37.56°C), the mean temperatures of the tympanic (37.29°C), Beurer (36.79°C) and Thermofocus (37.30°C) thermometers differed significantly (p<0.001). Mean and SD of differences between rectal temperature and temperature measured with these alternative devices varied significantly (p<0.001). Sensitivity, specificity, positive and negative predictive values for detecting rectal fever measured with the tympanic, Beurer and Thermofocus thermometers are unacceptable, especially for the Beurer thermometer. This difference in temperature between rectal and the alternative thermometers remained after stratification on gender, age, skin colour and otoscopic abnormalities. In this study the authors demonstrated that the tympanic, Beurer and Thermofocus thermometers cannot reliably predict rectal temperature. Therefore the authors do not advise replacement of rectal measurement as the gold standard for detecting fever in children by one of these devices. When rectal measurement is not used, the infrared skin thermometers appear to perform less well than tympanic measurements.

NIST-NRC Comparison of Total Immersion Liquid-in-Glass Thermometers

NASA Astrophysics Data System (ADS)

Hill, K. D.; Gee, D. J.; Cross, C. D.; Strouse, G. F.

2009-02-01

The use of liquid-in-glass (LIG) thermometers is described in many documentary standards in the fields of environmental testing, material testing, and material transfer. Many national metrology institutes, including the National Institute of Standards and Technology (NIST) and the National Research Council of Canada (NRC), list calibration services for these thermometers among the Calibration Measurement Capabilities of Appendix C of the BIPM Key Comparison Database. NIST and NRC arranged a bilateral comparison of a set of total-immersion ASTM-type LIG thermometers to validate their uncertainty claims. Two each of ASTM thermometer types 62C through 69C were calibrated at NIST and at NRC at four temperatures distributed over the range appropriate to each thermometer, in addition to the ice point. Collectively, the thermometers span a temperature range of - 38 °C to 305 °C. In total, 160 measurements (80 pairs) comprise the comparison data set. Pair-wise differences ( T NIST- T NRC) were formed for each thermometer at each temperature. For 8 of the 80 pairs (10 %), the differences exceed the k = 2 combined uncertainties. These results support the claimed capabilities of NIST and NRC for the calibration of LIG thermometers.

Evaluation of industrial platinum resistance thermometers

NASA Technical Reports Server (NTRS)

Daryabeigi, Kamran; Dillontownes, Lawrence A.; Alderfer, David W.

1987-01-01

The calibration and stability of four surface temperature measuring industrial platinum resistance thermometers for use in the temperature range -120 C to 160 C was investigated. It was found that the calibration formulation of the International Practical Temperature Scale of 1968 provided the most accurate calibration. It was also found that all the resistance thermometers suffered from varying degrees of instability and hysteresis.

Broadband interferometric characterisation of nano-positioning stages with sub-10 pm resolution

NASA Astrophysics Data System (ADS)

Li, Zhi; Brand, Uwe; Wolff, Helmut; Koenders, Ludger; Yacoot, Andrew; Puranto, Prabowo

2017-06-01

A traceable calibration setup for investigation of the quasi-static and the dynamic performance of nano-positioning stages is detailed, which utilizes a differential plane-mirror interferometer with double-pass configuration from the National Physical Laboratory (NPL). An NPL-developed FPGA-based interferometric data acquisition and decoding system has been used to enable traceable quasi-static calibration of nano-positioning stages with high resolution. A lockin based modulation technique is further introduced to quantitatively calibrate the dynamic response of moving stages with a bandwidth up to 100 kHz and picometer resolution. First experimental results have proven that the calibration setup can achieve under nearly open-air conditions a noise floor lower than 10 pm/sqrt(Hz). A pico-positioning stage, that is used for nanoindentation with indentation depths down to a few picometers, has been characterized with this calibration setup.

Intravenous fluid temperature management by infrared thermometer.

PubMed

Lapostolle, Frédéric; Catineau, Jean; Le Toumelin, Philippe; Proust, Clément; Garrigue, Bruno; Galinski, Michel; Adnet, Frédéric

2006-03-01

The management of intravenous (IV) fluid temperature is a daily challenge in critical care, anesthesiology, and emergency medicine. Infusion of IV fluids at the right temperature partly influences clinical outcomes of critically ill patients. Nowadays, intravenous fluid temperature is poorly managed, as no suitable device is routinely available. Infrared (IR) thermometers have been recently developed for industrial, personal, or medical purposes. The aim of this study was to evaluate the accuracy of an IR thermometer in measuring temperature of warmed and cooled infusion fluids in fluid bags. This study compared temperatures simultaneously recorded by an infrared thermometer and a temperature sensor. Temperatures of warmed (41 degrees C) and cooled (4 degrees C) infusion fluids in fluid bags were recorded by 2 independent operators every minute until IV bags' temperature reached ambient temperature. The relation curve was established with 576 measures. Temperature measures performed with an IR thermometer were perfectly linear and perfectly correlated with the reference method (R(2) = 0.995, P < 10(-5)). Infrared thermometers are efficient to measure IV fluid bag temperature in the range of temperatures used in clinical practice. As these devices are easy to use and inexpensive, they could be largely used in critical care, anesthesiology, or emergency medicine.

Nanoscale temperature mapping in operating microelectronic devices

DOE PAGES

Mecklenburg, Matthew; Hubbard, William A.; White, E. R.; ...

2015-02-05

We report that modern microelectronic devices have nanoscale features that dissipate power nonuniformly, but fundamental physical limits frustrate efforts to detect the resulting temperature gradients. Contact thermometers disturb the temperature of a small system, while radiation thermometers struggle to beat the diffraction limit. Exploiting the same physics as Fahrenheit’s glass-bulb thermometer, we mapped the thermal expansion of Joule-heated, 80-nanometer-thick aluminum wires by precisely measuring changes in density. With a scanning transmission electron microscope (STEM) and electron energy loss spectroscopy (EELS), we quantified the local density via the energy of aluminum’s bulk plasmon. Rescaling density to temperature yields maps with amore » statistical precision of 3 kelvin/hertz ₋1/2, an accuracy of 10%, and nanometer-scale resolution. Lastly, many common metals and semiconductors have sufficiently sharp plasmon resonances to serve as their own thermometers.« less

Equatorial Kelvin waves: A UARS MLS view

NASA Technical Reports Server (NTRS)

Canziani, Pablo O.; Holton, James R.; Fishbein, Evan; Froidevaux, Lucien; Waters, Joe W.

1994-01-01

Data from the Microwave Limb Sounder (MLS) instrument on the Upper Atmosphere Research Satellite (UARS) are used to compare two periods of Kelvin wave activity during different stages of the equatorial quasi-biennial oscillation. The analysis is carried out using an asynoptic mapping technique. A wide bandpass filter is used to isolate the frequency bands where Kelvin waves have been identified in previous studies. Time-height and time-latitude plots of the bandpassed data are used to identify Kelvin wave activity in the temperature and ozone fields. Frequency spectra of temperature and ozone amplitudes are constructed to further analyze the latitudinal and meridional distribution of Kelvin wave activity in zonal wavenumbers 1 and 2. The characteristics identified in these plots agree well with theoretical predictions and previous observations of middle atmosphere Kelvin waves. The time-height and time-latitude plots support the existence of Kelvin waves in discrete frequency bands; the slow, fast, and ultrafast Kelvin modes are all identified in the data. The characteristics of these modes do not vary much despite different mean flow conditions in the two periods examined. For the Kelvin wave-induced perturbations in ozone, the change from a transport-dominated regime below 10 hPa to a photochemically controlled regime above 10 hPa is clearly apparent in the height dependence of the phase difference between temperature and ozone. The ratios of the ozone perturbation amplitude to the temperature perturbation amplitude for the various observed Kelvin wave modes are in agreement with model estimates and LIMS (Limb Infrared Monitor of the Stratosphere) observations in the lower half of the region sampled but appear to be too large in the upper stratosphere and lower mesosphere.

21 CFR 880.2910 - Clinical electronic thermometer.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Clinical electronic thermometer. 880.2910 Section... Monitoring Devices § 880.2910 Clinical electronic thermometer. (a) Identification. A clinical electronic... with an electronic signal amplification, conditioning, and display unit. The transducer may be in a...

21 CFR 880.2910 - Clinical electronic thermometer.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Clinical electronic thermometer. 880.2910 Section... Monitoring Devices § 880.2910 Clinical electronic thermometer. (a) Identification. A clinical electronic... with an electronic signal amplification, conditioning, and display unit. The transducer may be in a...

21 CFR 880.2910 - Clinical electronic thermometer.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Clinical electronic thermometer. 880.2910 Section... Monitoring Devices § 880.2910 Clinical electronic thermometer. (a) Identification. A clinical electronic... with an electronic signal amplification, conditioning, and display unit. The transducer may be in a...

21 CFR 880.2910 - Clinical electronic thermometer.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Clinical electronic thermometer. 880.2910 Section... Monitoring Devices § 880.2910 Clinical electronic thermometer. (a) Identification. A clinical electronic... with an electronic signal amplification, conditioning, and display unit. The transducer may be in a...

21 CFR 880.2910 - Clinical electronic thermometer.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Clinical electronic thermometer. 880.2910 Section... Monitoring Devices § 880.2910 Clinical electronic thermometer. (a) Identification. A clinical electronic... with an electronic signal amplification, conditioning, and display unit. The transducer may be in a...

Neutron monitoring systems including gamma thermometers and methods of calibrating nuclear instruments using gamma thermometers

DOEpatents

Moen, Stephan Craig; Meyers, Craig Glenn; Petzen, John Alexander; Foard, Adam Muhling

2012-08-07

A method of calibrating a nuclear instrument using a gamma thermometer may include: measuring, in the instrument, local neutron flux; generating, from the instrument, a first signal proportional to the neutron flux; measuring, in the gamma thermometer, local gamma flux; generating, from the gamma thermometer, a second signal proportional to the gamma flux; compensating the second signal; and calibrating a gain of the instrument based on the compensated second signal. Compensating the second signal may include: calculating selected yield fractions for specific groups of delayed gamma sources; calculating time constants for the specific groups; calculating a third signal that corresponds to delayed local gamma flux based on the selected yield fractions and time constants; and calculating the compensated second signal by subtracting the third signal from the second signal. The specific groups may have decay time constants greater than 5.times.10.sup.-1 seconds and less than 5.times.10.sup.5 seconds.

A Cell-Targeted Non-Cytotoxic Fluorescent Nanogel Thermometer Created with an Imidazolium-Containing Cationic Radical Initiator.

PubMed

Uchiyama, Seiichi; Tsuji, Toshikazu; Kawamoto, Kyoko; Okano, Kentaro; Fukatsu, Eiko; Noro, Takahiro; Ikado, Kumiko; Yamada, Sayuri; Shibata, Yuka; Hayashi, Teruyuki; Inada, Noriko; Kato, Masaru; Koizumi, Hideki; Tokuyama, Hidetoshi

2018-05-04

A cationic fluorescent nanogel thermometer based on thermo-responsive N-isopropylacrylamide and environment-sensitive benzothiadiazole was developed with a new azo compound bearing imidazolium rings as the first cationic radical initiator. This cationic fluorescent nanogel thermometer showed an excellent ability to enter live mammalian cells in a short incubation period (10 min), a high sensitivity to temperature variations in live cells (temperature resolution of 0.02-0.84 °C in the range 20-40 °C), and remarkable non-cytotoxicity, which permitted ordinary cell proliferation and even differentiation of primary cultured cells. © 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Lord Kelvin's atmospheric electricity measurements

NASA Astrophysics Data System (ADS)

Aplin, Karen; Harrison, R. Giles; Trainer, Matthew; Hough, James

2013-04-01

Lord Kelvin (William Thomson), one of the greatest Victorian scientists, made a substantial but little-recognised contribution to geophysics through his work on atmospheric electricity. He developed sensitive instrumentation for measuring the atmospheric electric field, including invention of a portable electrometer, which made mobile measurements possible for the first time. Kelvin's measurements of the atmospheric electric field in 1859, made during development of the portable electrometer, can be used to deduce the substantial levels of particulate pollution blown over the Scottish island of Arran from the industrial mainland. Kelvin was also testing the electrometer during the largest solar flare ever recorded, the "Carrington event" in the late summer of 1859. Subsequently, Lord Kelvin also developed a water dropper sensor, and employed photographic techniques for "incessant recording" of the atmospheric electric field, which led to the long series of measurements recorded at UK observatories for the remainder of the 19th and much of the 20th century. These data sets have been valuable in both studies of historical pollution and cosmic ray effects on atmospheric processes.

Design and characterization of a nano-Newton resolution thrust stand

NASA Astrophysics Data System (ADS)

Soni, J.; Roy, S.

2013-09-01

The paper describes the design, calibration, and characterization of a thrust stand capable of nano-Newton resolution. A low uncertainty calibration method is proposed and demonstrated. A passive eddy current based damper, which is non-contact and vacuum compatible, is employed. Signal analysis techniques are used to perform noise characterization, and potential sources are identified. Calibrated system noise floor suggests thrust measurement resolution of the order of 10 nN is feasible under laboratory conditions. Force measurement from this balance for a standard macroscale dielectric barrier discharge (DBD) plasma actuator is benchmarked with a commercial precision balance of 9.8 μN resolution and is found to be in good agreement. Published results of a microscale DBD plasma actuator force measurement and low pressure characterization of conventional plasma actuators are presented for completeness.

Germanium Resistance Thermometer For Subkelvin Temperatures

NASA Technical Reports Server (NTRS)

Castles, Stephen H.

1993-01-01

Improved germanium resistance thermometer measures temperatures as small as 0.01 K accurately. Design provides large area for electrical connections (to reduce electrical gradients and increase sensitivity to changes in temperatures) and large heat sink (to minimize resistance heating). Gold pads on top and bottom of germanium crystal distribute electrical current and flow of heat nearly uniformly across crystal. Less expensive than magnetic thermometers or superconducting quantum interference devices (SQUID's) otherwise used.

A 10 Kelvin Magnet for Space-Flight ADRs

NASA Technical Reports Server (NTRS)

Tuttle, James; Pourrahimi, Shahin; Shirron, Peter; Canavan, Edgar; DiPirro, Michael; Riall, Sara

2003-01-01

Future NASA missions will include detectors cooled by adiabatic demagnetization refrigerators (ADRs) coupled with mechanical cryocoolers. A lightweight, low-current 10 Kelvin magnet would allow the interface between these devices to be at temperatures as high as 10 Kelvin, adding flexibility to the instrument design. We report on the testing of a standard-technology Nb3Sn magnet and the development of a lightweight, low-current 10 Kelvin magnet. We also discuss the outlook for flying a 10 Kelvin magnet as part of an ADR system.

Performance and Characterization of Magnetic Penetration Thermometer Devices for X-Ray Spectroscopy

NASA Technical Reports Server (NTRS)

Porst, J. -P.; Adams, J. S.; Bandler, S. R.; Balvin, M.; Busch, S. E.; Denis, K. L.; Kelly, D.; Nagler, P.; Sadleir, J. E.; Seidel, G. M.;

Pico-Kelvin thermometry and temperature stabilization using a resonant optical cavity.

PubMed

Tan, Si; Wang, Suwen; Saraf, Shailendhar; Lipa, John A

2017-02-20

Ultra-high sensitivity temperature sensing and stable thermal control are crucial for many science experiments testing fundamental theories to high precision. Here we report the first pico-kevin scale thermometer operating at room temperature with an exceptionally low theoretical noise figure of ~70pK/Hz at 1 Hz and a high dynamic range of ~500 K. We have experimentally demonstrated a temperature sensitivity of <3.8nK/Hz at 1 Hz near room temperature, which is an order of magnitude improvement over the state of the art. We have also demonstrated an ultra-high stability thermal control system using this thermometer, achieving 3.7 nK stability at 1 s and ∼ 120 pK at 10⁴ s, which is 10-100 times more stable than the state of the art. With some upgrades to this proof-of-principle device, we can expect it to be used for very high resolution tests of special relativity and in critical point phenomena.

Comparative Study of Two InGaAs-Based Reference Radiation Thermometers

NASA Astrophysics Data System (ADS)

Nasibov, H.; Diril, A.; Pehlivan, O.; Kalemci, M.

2017-07-01

More than one decade ago, an InGaAs detector-based transfer standard infrared radiation thermometer working in the temperature range from 150 {^{circ }}\\hbox {C} to 1100 {^{circ }}\\hbox {C} was built at TUBITAK UME in the scope of collaboration with IMGC (INRIM since 2006). During this timescale, the radiation thermometer was used for the dissemination of the radiation temperature scale below the silver fixed-point temperature. Recently, a new radiation thermometer with the same design but with different spectral responsivity was constructed and employed in the laboratory. In this work, we present the comparative study of these thermometers. Furthermore, the paper describes the measurement results of the thermometer's main characteristics such as the size-of-source effect, spectral responsivity, gain ratio, and linearity. Besides, both thermometers were calibrated at the freezing temperatures of indium, tin, zinc, aluminum, and copper reference fixed-point blackbodies. The main study is focused on the impact of the spectral responsivity of thermometers on the interpolation parameters of the Sakuma-Hattori equation. Furthermore, the calibration results and the uncertainty sources are discussed in this paper.

Measurement of body temperature by use of auricular thermometers versus rectal thermometers in dogs with otitis externa.

PubMed

González, A Michelle; Mann, F A; Preziosi, Diane E; Meadows, Richard L; Wagner-Mann, Colette C

2002-08-01

To compare measurements of body temperature obtained with auricular thermometers versus rectal thermometers in dogs with otitis externa. Prospective study. 100 client-owned dogs: 50 with and 50 without clinical evidence of otitis externa. Dogs were evaluated for the presence of otitis externa on the basis of clinical signs, otoscopic examination, and cytologic evaluation of ear exudate. Auricular and rectal temperatures were obtained simultaneously in all dogs prior to and following ear examination. There was a high correlation between auricular and rectal temperatures in dogs with otitis externa both prior to and after ear manipulation. Significant differences were not detected in temperature measurements among dogs with different degrees of otitis externa. Auricular temperature readings obtained by use of an auricular thermometer in dogs with otitis externa are accurate measurements of body temperature, compared with rectal temperature measurements. Temperature measurements are reliable before and after examination of the ear canal.

Measuring Systems for Thermometer Calibration in Low-Temperature Range

NASA Astrophysics Data System (ADS)

Szmyrka-Grzebyk, A.; Lipiński, L.; Manuszkiewicz, H.; Kowal, A.; Grykałowska, A.; Jancewicz, D.

2011-12-01

The national temperature standard for the low-temperature range between 13.8033 K and 273.16 K has been established in Poland at the Institute of Low Temperature and Structure Research (INTiBS). The standard consists of sealed cells for realization of six fixed points of the International Temperature Scale of 1990 (ITS-90) in the low-temperature range, an adiabatic cryostat and Isotech water and mercury triple-point baths, capsule standard resistance thermometers (CSPRT), and AC and DC bridges with standard resistors for thermometers resistance measurements. INTiBS calibrates CSPRTs at the low-temperature fixed points with uncertainties less than 1 mK. In lower temperature range—between 2.5 K and about 25 K — rhodium-iron (RhFe) resistance thermometers are calibrated by comparison with a standard which participated in the EURAMET.T-K1.1 comparison. INTiBS offers a calibration service for industrial platinum resistance thermometers and for digital thermometers between 77 K and 273 K. These types of thermometers may be calibrated at INTiBS also in a higher temperature range up to 550°C. The Laboratory of Temperature Standard at INTiBS acquired an accreditation from the Polish Centre for Accreditation. A management system according to EN ISO/IEC 17025:2005 was established at the Laboratory and presented on EURAMET QSM Forum.

Performance of Magnetic Penetration Thermometers for X-Ray Astronomy

NASA Technical Reports Server (NTRS)

Nagler, P. C.; Adams, J. S.; Balvin, M. A.; Bandler, S. R.; Denis, K. L.; Hsieh, W. T.; Kelly, D. P.; Porst, J. P.; Sadleir, J. E.; Seidel, G. M.;

Fluorescent Nano-Probes to Image Plant Cell Walls by Super-Resolution STED Microscopy

PubMed Central

Paës, Gabriel; Habrant, Anouck; Terryn, Christine

2018-01-01

Lignocellulosic biomass is a complex network of polymers making up the cell walls of plants. It represents a feedstock of sustainable resources to be converted into fuels, chemicals, and materials. Because of its complex architecture, lignocellulose is a recalcitrant material that requires some pretreatments and several types of catalysts to be transformed efficiently. Gaining more knowledge in the architecture of plant cell walls is therefore important to understand and optimize transformation processes. For the first time, super-resolution imaging of poplar wood samples has been performed using the Stimulated Emission Depletion (STED) technique. In comparison to standard confocal images, STED reveals new details in cell wall structure, allowing the identification of secondary walls and middle lamella with fine details, while keeping open the possibility to perform topochemistry by the use of relevant fluorescent nano-probes. In particular, the deconvolution of STED images increases the signal-to-noise ratio so that images become very well defined. The obtained results show that the STED super-resolution technique can be easily implemented by using cheap commercial fluorescent rhodamine-PEG nano-probes which outline the architecture of plant cell walls due to their interaction with lignin. Moreover, the sample preparation only requires easily-prepared plant sections of a few tens of micrometers, in addition to an easily-implemented post-treatment of images. Overall, the STED super-resolution technique in combination with a variety of nano-probes can provide a new vision of plant cell wall imaging by filling in the gap between classical photon microscopy and electron microscopy. PMID:29415498

Fluorescent Nano-Probes to Image Plant Cell Walls by Super-Resolution STED Microscopy.

PubMed

Paës, Gabriel; Habrant, Anouck; Terryn, Christine

2018-02-06

Lignocellulosic biomass is a complex network of polymers making up the cell walls of plants. It represents a feedstock of sustainable resources to be converted into fuels, chemicals, and materials. Because of its complex architecture, lignocellulose is a recalcitrant material that requires some pretreatments and several types of catalysts to be transformed efficiently. Gaining more knowledge in the architecture of plant cell walls is therefore important to understand and optimize transformation processes. For the first time, super-resolution imaging of poplar wood samples has been performed using the Stimulated Emission Depletion (STED) technique. In comparison to standard confocal images, STED reveals new details in cell wall structure, allowing the identification of secondary walls and middle lamella with fine details, while keeping open the possibility to perform topochemistry by the use of relevant fluorescent nano-probes. In particular, the deconvolution of STED images increases the signal-to-noise ratio so that images become very well defined. The obtained results show that the STED super-resolution technique can be easily implemented by using cheap commercial fluorescent rhodamine-PEG nano-probes which outline the architecture of plant cell walls due to their interaction with lignin. Moreover, the sample preparation only requires easily-prepared plant sections of a few tens of micrometers, in addition to an easily-implemented post-treatment of images. Overall, the STED super-resolution technique in combination with a variety of nano-probes can provide a new vision of plant cell wall imaging by filling in the gap between classical photon microscopy and electron microscopy.

21 CFR 880.2900 - Clinical color change thermometer.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Clinical color change thermometer. 880.2900... Monitoring Devices § 880.2900 Clinical color change thermometer. (a) Identification. A clinical color change... end of a plastic or metal strip. Body heat causes a stable color change in the heat sensitive...

Galileo Chain Thermometer

ERIC Educational Resources Information Center

Ucke, C.; Schlichting, H. J.

2017-01-01

This relatively rare thermometer has a rather unusual display: lower temperatures are located at the top of the scale, higher ones at the bottom. A sphere on a chain floats in a suitable liquid, sinking at high temperatures when the density of the liquid decreases and rising in the increased density at low temperatures. With reasonable effort and…

Approaching the resolution limit of W-C nano-gaps using focused ion beam chemical vapour deposition

NASA Astrophysics Data System (ADS)

Dai, Jun; Chang, Hui; Maeda, Etsuo; Warisawa, Shin'ichi; Kometani, Reo

2018-01-01

Nano-gaps are fundamental building blocks for nanochannels, plasmonic nanostructures and superconducting Josephson junctions. We present a systematic study on the formation mechanism and resolution limit of W-C nano-gaps fabricated using focused-ion-beam chemical vapour deposition (FIB-CVD). First, the deposition size of the nanostructures is evaluated. The size averaged over 100 dots is 32 nm at FWHM. Line and space are also fabricated with the smallest size, having a spacing of only 5 nm at FWHM. Then, a model is developed to study the formation mechanism and provides the design basis for W-C nano-gaps. Both experimental and simulation results reveal that the shrinkage of W-C nano-gaps is accelerated as the Gaussian parts of the nano-wire profiles overlap. A Nano-gap with a length of 5 nm and height difference as high as 42 nm is synthesized. We believe that FIB-CVD opens avenues for novel functional nanodevices that can be potentially used for biosensing, photodetecting, or quantum computing.

Kelvin Wave Influence on the Shallow-to-Deep Transition Over the Amazon

NASA Astrophysics Data System (ADS)

Rowe, A.; Serra, Y. L.

2017-12-01

over the Central Amazon in both global and regional model simulations with differing resolution and choice of convective parameterization. This work will test the hypothesis that when the environment is strongly modified by a Kelvin wave, model shallow-to-deep transition will be better simulated than when this forcing is not present.

Observation of single-mode, Kelvin-Helmholtz instability in a supersonic flow

DOE PAGES

Wan, W. C.; Malamud, Guy; Shimony, A.; ...

2015-10-01

This manuscript reports the first observations of the Kelvin-Helmholtz instability evolving from well-characterized seed perturbations in a steady, supersonic flow. The Kelvin-Helmholtz instability occurs when two fluids move parallel to one another at different velocities, and contributes to an intermixing of fluids and transition to turbulence. It is ubiquitous in nature and engineering, including terrestrial systems such as cloud formations, astrophysical systems such as supernovae, and laboratory systems such as fusion experiments. In a supersonic flow, the growth rate of the instability is inhibited due to effects of compressibility. These effects are still not fully understood, and hold the motivationmore » for the current work. The data presented here were obtained by developing a novel experimental platform capable of sustaining a steady shockwave over a precision-machined interface for unprecedented durations. The chosen interface was a well-characterized, single-mode sine wave, allowing us to document the evolution of individual vortices at high resolution. Understanding the behavior of individual vortices is the first of two fundamental steps towards developing a comprehensive model for the Kelvin-Helmholtz instability in a compressible flow. The results of this experiment were well reproduced with 2D hydrodynamic simulations. The platform has been extended to additional experiments, which study the evolution of different hydrodynamic instabilities in steady, supersonic flows.« less

Observation of single-mode, Kelvin-Helmholtz instability in a supersonic flow

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wan, W. C.; Malamud, Guy; Shimony, A.

This manuscript reports the first observations of the Kelvin-Helmholtz instability evolving from well-characterized seed perturbations in a steady, supersonic flow. The Kelvin-Helmholtz instability occurs when two fluids move parallel to one another at different velocities, and contributes to an intermixing of fluids and transition to turbulence. It is ubiquitous in nature and engineering, including terrestrial systems such as cloud formations, astrophysical systems such as supernovae, and laboratory systems such as fusion experiments. In a supersonic flow, the growth rate of the instability is inhibited due to effects of compressibility. These effects are still not fully understood, and hold the motivationmore » for the current work. The data presented here were obtained by developing a novel experimental platform capable of sustaining a steady shockwave over a precision-machined interface for unprecedented durations. The chosen interface was a well-characterized, single-mode sine wave, allowing us to document the evolution of individual vortices at high resolution. Understanding the behavior of individual vortices is the first of two fundamental steps towards developing a comprehensive model for the Kelvin-Helmholtz instability in a compressible flow. The results of this experiment were well reproduced with 2D hydrodynamic simulations. The platform has been extended to additional experiments, which study the evolution of different hydrodynamic instabilities in steady, supersonic flows.« less

A Non-Mercury Thermometer Alternative for Use in Older Melting Point Apparatuses

ERIC Educational Resources Information Center

Ongley, Lois K.; Kern, Clayton S.; Woods, Barry W.

2008-01-01

The State of Maine seeks to eliminate most mercury use. This includes removing mercury thermometers from secondary schools and discouraging Hg use in other educational institutions. Alternatives to mercury thermometers in chemical laboratory work include non-mercury thermometers, temperature probes, and thermocouples. In organic chemistry mercury…

Polymeric spatial resolution test patterns for mass spectrometry imaging using nano-thermal analysis with atomic force microscopy

DOE PAGES

Tai, Tamin; Kertesz, Vilmos; Lin, Ming -Wei; ...

2017-05-11

As the spatial resolution of mass spectrometry imaging technologies has begun to reach into the nanometer regime, finding readily available or easily made resolution reference materials has become particularly challenging for molecular imaging purposes. This study describes the fabrication, characterization and use of vertical line array polymeric spatial resolution test patterns for nano-thermal analysis/atomic force microscopy/mass spectrometry chemical imaging.

Polymeric spatial resolution test patterns for mass spectrometry imaging using nano-thermal analysis with atomic force microscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tai, Tamin; Kertesz, Vilmos; Lin, Ming -Wei

As the spatial resolution of mass spectrometry imaging technologies has begun to reach into the nanometer regime, finding readily available or easily made resolution reference materials has become particularly challenging for molecular imaging purposes. This study describes the fabrication, characterization and use of vertical line array polymeric spatial resolution test patterns for nano-thermal analysis/atomic force microscopy/mass spectrometry chemical imaging.

A sub-Kelvin cryogen-free EPR system.

PubMed

Melhuish, Simon J; Stott, Chloe; Ariciu, Ana-Maria; Martinis, Lorenzo; McCulloch, Mark; Piccirillo, Lucio; Collison, David; Tuna, Floriana; Winpenny, Richard

2017-09-01

We present an EPR instrument built for operation at Q band below 1K. Our cryogen-free Dewar integrates with a commercial electro-magnet and bridge. A description of the cryogenic and RF systems is given, along with the adaptations to the standard EPR experiment for operation at sub-Kelvin temperatures. As a first experiment, the EPR spectra of powdered Cr 12 O 9 (OH) 3 [Formula: see text] were measured. The sub-Kelvin EPR spectra agree well with predictions, and the performance of the sub-Kelvin system at 5K is compared to that of a commercial spectrometer. Copyright © 2017 The Authors. Published by Elsevier Inc. All rights reserved.

Thermometers and thermobarometers in granitic systems

USGS Publications Warehouse

Anderson, J.L.; Barth, A.P.; Wooden, J.L.; Mazdab, F.; ,

2008-01-01

The ability to determine the thermal and barometric history during crystallization and emplacement of granitic plutons has been enhanced by several new calibrations applicable to granitic mineral assemblages. Other existing calibrations for granitic plutons have continued to be popular and fairly robust. Recent advances include the trace element thermometers Ti-in-quartz, Ti-in-zircon, and Zr-in-sphene (titanite), which need to be further evaluated on the roles of reduced activities due to lack of a saturating phase, the effect of pressure dependence (particularly for the Ti-in-zircon thermometer), and how resistive these thermometers are to subsolidus reequilibration. As zircon and sphene are also hosts to radiogenic isotopes, these minerals potentially also provide new insights into the temperature - time history of magmas. When used in conjunction with pressure-sensitive mineral equilibria in the same rocks, a complete assessment of the P-T-t (pressure-temperature-time) path is possible given that the mineralogy of plutons can reflect crystallization over a range of pressure and temperature during ascent and emplacement and that many intrusions are now seen as forming over several millions of years during the protracted history of batholith construction. Accessory mineral saturation thermometers, such as those for zircon, apatite, and allanite, provide a different and powerful perspective, specifically that of the temperature of the onset of crystallization of these minerals, which can allow an estimate of the range of temperature between the liquidus and solidus of a given pluton. In assessment of the depth of crystallization and emplacement of granitic plutons, the Al-in-hornblende remains popular for metaluminous granites when appropriately corrected for temperature. For peraluminous granites, potential new calibrations exist for the assemblages bearing garnet, biotite, plagioclase, muscovite, and quartz. Other thermometers, based on oxygen abundance, and

A compact sub-Kelvin ultrahigh vacuum scanning tunneling microscope with high energy resolution and high stability.

PubMed

Zhang, L; Miyamachi, T; Tomanić, T; Dehm, R; Wulfhekel, W

2011-10-01

We designed a scanning tunneling microscope working at sub-Kelvin temperatures in ultrahigh vacuum (UHV) in order to study the magnetic properties on the nanoscale. An entirely homebuilt three-stage cryostat is used to cool down the microscope head. The first stage is cooled with liquid nitrogen, the second stage with liquid (4)He. The third stage uses a closed-cycle Joule-Thomson refrigerator of a cooling power of 1 mW. A base temperature of 930 mK at the microscope head was achieved using expansion of (4)He, which can be reduced to ≈400 mK when using (3)He. The cryostat has a low liquid helium consumption of only 38 ml/h and standing times of up to 280 h. The fast cooling down of the samples (3 h) guarantees high sample throughput. Test experiments with a superconducting tip show a high energy resolution of 0.3 meV when performing scanning tunneling spectroscopy. The vertical stability of the tunnel junction is well below 1 pm (peak to peak) and the electric noise floor of tunneling current is about 6fA/√Hz. Atomic resolution with a tunneling current of 1 pA and 1 mV was achieved on Au(111). The lateral drift of the microscope at stable temperature is below 20 pm/h. A superconducting spilt-coil magnet allows to apply an out-of-plane magnetic field of up to 3 T at the sample surface. The flux vortices of a Nb(110) sample were clearly resolved in a map of differential conductance at 1.1 K and a magnetic field of 0.21 T. The setup is designed for in situ preparation of tip and samples under UHV condition.

Nano-Localized Thermal Analysis and Mapping of Surface and Sub-Surface Thermal Properties Using Scanning Thermal Microscopy (SThM).

PubMed

Pereira, Maria J; Amaral, Joao S; Silva, Nuno J O; Amaral, Vitor S

2016-12-01

Determining and acting on thermo-physical properties at the nanoscale is essential for understanding/managing heat distribution in micro/nanostructured materials and miniaturized devices. Adequate thermal nano-characterization techniques are required to address thermal issues compromising device performance. Scanning thermal microscopy (SThM) is a probing and acting technique based on atomic force microscopy using a nano-probe designed to act as a thermometer and resistive heater, achieving high spatial resolution. Enabling direct observation and mapping of thermal properties such as thermal conductivity, SThM is becoming a powerful tool with a critical role in several fields, from material science to device thermal management. We present an overview of the different thermal probes, followed by the contribution of SThM in three currently significant research topics. First, in thermal conductivity contrast studies of graphene monolayers deposited on different substrates, SThM proves itself a reliable technique to clarify the intriguing thermal properties of graphene, which is considered an important contributor to improve the performance of downscaled devices and materials. Second, SThM's ability to perform sub-surface imaging is highlighted by thermal conductivity contrast analysis of polymeric composites. Finally, an approach to induce and study local structural transitions in ferromagnetic shape memory alloy Ni-Mn-Ga thin films using localized nano-thermal analysis is presented.

The Kelvin and Temperature Measurements

PubMed Central

Mangum, B. W.; Furukawa, G. T.; Kreider, K. G.; Meyer, C. W.; Ripple, D. C.; Strouse, G. F.; Tew, W. L.; Moldover, M. R.; Johnson, B. Carol; Yoon, H. W.; Gibson, C. E.; Saunders, R. D.

2001-01-01

The International Temperature Scale of 1990 (ITS-90) is defined from 0.65 K upwards to the highest temperature measurable by spectral radiation thermometry, the radiation thermometry being based on the Planck radiation law. When it was developed, the ITS-90 represented thermodynamic temperatures as closely as possible. Part I of this paper describes the realization of contact thermometry up to 1234.93 K, the temperature range in which the ITS-90 is defined in terms of calibration of thermometers at 15 fixed points and vapor pressure/temperature relations which are phase equilibrium states of pure substances. The realization is accomplished by using fixed-point devices, containing samples of the highest available purity, and suitable temperature-controlled environments. All components are constructed to achieve the defining equilibrium states of the samples for the calibration of thermometers. The high quality of the temperature realization and measurements is well documented. Various research efforts are described, including research to improve the uncertainty in thermodynamic temperatures by measuring the velocity of sound in gas up to 800 K, research in applying noise thermometry techniques, and research on thermocouples. Thermometer calibration services and high-purity samples and devices suitable for “on-site” thermometer calibration that are available to the thermometry community are described. Part II of the paper describes the realization of temperature above 1234.93 K for which the ITS-90 is defined in terms of the calibration of spectroradiometers using reference blackbody sources that are at the temperature of the equilibrium liquid-solid phase transition of pure silver, gold, or copper. The realization of temperature from absolute spectral or total radiometry over the temperature range from about 60 K to 3000 K is also described. The dissemination of the temperature scale using radiation thermometry from NIST to the customer is achieved by

27 CFR 30.23 - Use of precision hydrometers and thermometers.

Code of Federal Regulations, 2010 CFR

2010-04-01

... hydrometers and thermometers. 30.23 Section 30.23 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO... Use of precision hydrometers and thermometers. Care should be exercised to obtain accurate hydrometer... entire quantity. The hydrometers should be kept clean and free of any oily substance. Immediately before...

[Application of self-developed moxibustion thermometer in experiment teaching].

PubMed

Zhang, Jing; Sun, Yan; Zhang, Yongchen; Lu, Yan

2017-04-12

In order to improve the teaching quality of moxibustion experiment, a moxibustion thermometer was self-developed to monitor the real-time and continuous data of moxibustion temperature at different time points during the experiment. After teacher's explanation and demonstration of experiment process, the students used the moxibustion thermometer to monitor the change of temperature data and extended the experiment design. In the process of experiment class, the students found the temperature of the object tested increased rapidly, arrived at the highest temperature and slowly reduced. In addition, with learned knowledge, the students were able to design the feasible experiment scheme. The self-developed moxibustion thermometer operates smoothly in actual teaching, with stable experiment data and less experiment error, which obtained satisfactory teaching effect.

DNA nanostructure-based fluorescence thermometer with silver nanoclusters.

PubMed

Bu, Congcong; Mu, Lixuan; Cao, XIngxing; Chen, Min; She, Guangwei; Shi, Wensheng

2018-04-27

Linking the fluorescent silver nanoclusters (AgNCs) and guanine-rich（G-rich）DNA chains by the thermal sensitive DNA stem-loop at teminal 5' and 3', DNA nanostructure-based fluorescence thermometers were fabricated. The variations of the temperature alter the distance between AgNCs and G-rich DNA chain, which could affect the interaction between them. As a result, the intensity of fluorescence emission from AgNCs at 636 nm can be sensitively modulated. It was found that such red emission is more sensitive to the temperature comparing with its intrinsic green emission at 543 nm, and sensitivity of -3.6%/℃ was achieved. Varying the melting temperature of the DNA stem-loop could readily adjust the response temperature range of thermometers. Novel DNA nanostructure-based fluorescence thermometers in this work could be anticipated to measure the temperature of biological system, even a single cell. © 2018 IOP Publishing Ltd.

High speed infrared radiation thermometer, system, and method

DOEpatents

Markham, James R.

2002-01-01

The high-speed radiation thermometer has an infrared measurement wavelength band that is matched to the infrared wavelength band of near-blackbody emittance of ceramic components and ceramic thermal barrier coatings used in turbine engines. It is comprised of a long wavelength infrared detector, a signal amplifier, an analog-to-digital converter, an optical system to collect radiation from the target, an optical filter, and an integral reference signal to maintain a calibrated response. A megahertz range electronic data acquisition system is connected to the radiation detector to operate on raw data obtained. Because the thermometer operates optimally at 8 to 12 .mu.m, where emittance is near-blackbody for ceramics, interferences to measurements performed in turbine engines are minimized. The method and apparatus are optimized to enable mapping of surface temperatures on fast moving ceramic elements, and the thermometer can provide microsecond response, with inherent self-diagnostic and calibration-correction features.

DNA nanostructure-based fluorescence thermometer with silver nanoclusters

NASA Astrophysics Data System (ADS)

Bu, Congcong; Mu, Lixuan; Cao, Xingxing; Chen, Min; She, Guangwei; Shi, Wensheng

2018-07-01

DNA nanostructure-based fluorescence thermometers were fabricated by linking fluorescent silver nanoclusters (AgNCs) and guanine-rich（G-rich）DNA chains via a thermally sensitive DNA stem-loop at terminals 5‧ and 3‧. Variations of temperature alter the distance between the AgNCs and G-rich DNA chain, affecting the interaction between them. As a result, the intensity of fluorescence emission from the AgNCs at 636 nm can be sensitively modulated. It was found that the intensity of such red emission is more temperature sensitive than the equivalent green emission at 543 nm; sensitivity of ‑3.6%/°C was achieved. Through variation of the melting temperature of the DNA stem-loop, the response temperature range of the thermometers could be readily adjusted. Novel DNA nanostructure-based fluorescence thermometers as described in this work are anticipated to be able to measure the temperature of biological systems at small scales—even a single cell.

Gas selectivity of SILAR grown CdS nano-bulk junction

NASA Astrophysics Data System (ADS)

Jayakrishnan, R.; Nair, Varun G.; Anand, Akhil M.; Venugopal, Meera

2018-03-01

Nano-particles of cadmium sulphide were deposited on cleaned copper substrate by an automated sequential ionic layer adsorption reaction (SILAR) system. The grown nano-bulk junction exhibits Schottky diode behavior. The response of the nano-bulk junction was investigated under oxygen and hydrogen atmospheric conditions. The gas response ratio was found to be 198% for Oxygen and 34% for Hydrogen at room temperature. An increase in the operating temperature of the nano-bulk junction resulted in a decrease in their gas response ratio. A logarithmic dependence on the oxygen partial pressure to the junction response was observed, indicating a Temkin isothermal behavior. Work function measurements using a Kelvin probe demonstrate that the exposure to an oxygen atmosphere fails to effectively separate the charges due to the built-in electric field at the interface. Based on the benefits like simple structure, ease of fabrication and response ratio the studied device is a promising candidate for gas detection applications.

Eliminating Mercury Thermometers from the Lab.

ERIC Educational Resources Information Center

Everett, T. Stephen

1997-01-01

Compares the precision, accuracy, and response of a cooking probe to a standard mercury thermometer in side-by-side heating in temperature baths, simple and fractional distillations, and melting point determination. (DDR)

Sub-diffraction nano manipulation using STED AFM.

PubMed

Chacko, Jenu Varghese; Canale, Claudio; Harke, Benjamin; Diaspro, Alberto

2013-01-01

In the last two decades, nano manipulation has been recognized as a potential tool of scientific interest especially in nanotechnology and nano-robotics. Contemporary optical microscopy (super resolution) techniques have also reached the nanometer scale resolution to visualize this and hence a combination of super resolution aided nano manipulation ineluctably gives a new perspective to the scenario. Here we demonstrate how specificity and rapid determination of structures provided by stimulated emission depletion (STED) microscope can aid another microscopic tool with capability of mechanical manoeuvring, like an atomic force microscope (AFM) to get topological information or to target nano scaled materials. We also give proof of principle on how high-resolution real time visualization can improve nano manipulation capability within a dense sample, and how STED-AFM is an optimal combination for this job. With these evidences, this article points to future precise nano dissections and maybe even to a nano-snooker game with an AFM tip and fluorospheres.

Nano-Computed Tomography: Technique and Applications.

PubMed

Kampschulte, M; Langheinirch, A C; Sender, J; Litzlbauer, H D; Althöhn, U; Schwab, J D; Alejandre-Lafont, E; Martels, G; Krombach, G A

2016-02-01

Nano-computed tomography (nano-CT) is an emerging, high-resolution cross-sectional imaging technique and represents a technical advancement of the established micro-CT technology. Based on the application of a transmission target X-ray tube, the focal spot size can be decreased down to diameters less than 400 nanometers (nm). Together with specific detectors and examination protocols, a superior spatial resolution up to 400 nm (10 % MTF) can be achieved, thereby exceeding the resolution capacity of typical micro-CT systems. The technical concept of nano-CT imaging as well as the basics of specimen preparation are demonstrated exemplarily. Characteristics of atherosclerotic plaques (intraplaque hemorrhage and calcifications) in a murine model of atherosclerosis (ApoE (-/-)/LDLR(-/-) double knockout mouse) are demonstrated in the context of superior spatial resolution in comparison to micro-CT. Furthermore, this article presents the application of nano-CT for imaging cerebral microcirculation (murine), lung structures (porcine), and trabecular microstructure (ovine) in contrast to micro-CT imaging. This review shows the potential of nano-CT as a radiological method in biomedical basic research and discusses the application of experimental, high resolution CT techniques in consideration of other high resolution cross-sectional imaging techniques. Nano-computed tomography is a high resolution CT-technology for 3D imaging at sub-micrometer resolution. The technical concept bases on a further development of the established ex-vivo-micro-CT technology. By improvement of the spatial resolution, structures at a cellular level become visible (e.g. osteocyte lacunae). © Georg Thieme Verlag KG Stuttgart · New York.

Thermal Conductivity and Liquid Crystal Thermometers.

ERIC Educational Resources Information Center

Edge, R. D., Ed.

1993-01-01

Describes using stock liquid crystal postcards as inexpensive classroom thermometers. Also suggests using these postcards as a good visual temperature indicator for classroom demonstrations such as temperature gradients. One such activity is provided. (MVL)

Size-of-source Effect in Infrared Thermometers with Direct Reading of Temperature

NASA Astrophysics Data System (ADS)

Manoi, A.; Saunders, P.

2017-07-01

The size-of-source effect (SSE) for six infrared (IR) thermometers with direct reading of temperature was measured in this work. The alternative direct method for SSE determination, where the aperture size is fixed and the measurement distance is varied, was used in this study. The experimental equivalence between the usual and the alternative direct methods is presented. The magnitudes of the SSE for different types of IR thermometers were investigated. The maxima of the SSE were found to be up to 5 %, 8 %, and 28 % for focusable, closed-focus, and open-focus thermometers, respectively. At 275°C, an SSE of 28 % corresponds to 52°C, indicating the severe effect on the accuracy of this type of IR thermometer. A method to realize the calibration conditions used by the manufacturer, in terms of aperture size and measurement distance, is discussed and validated by experimental results. This study would be of benefit to users in choosing the best IR thermometer to match their work and for calibration laboratories in selecting the technique most suitable for determining the SSE.

Novel MEMS-based thermometer with low power consumption for health-monitoring network application

NASA Astrophysics Data System (ADS)

Zhang, Y.; Ikehara, T.; Lu, J.; Kobayashi, T.; Ichiki, M.; Itoh, T.; Maeda, R.

2007-12-01

We proposed one novel MEMS-based thermometer with low power-consumption for animal/human health-monitoring network application. The novel MEMS-based thermometer was consisted of triple-beam bimorph arrays so that it could work in a continuous temperature range. Neither continuous electric supply nor A/D converter interface is required by the novel thermometer owing to the well-known deflection of bimaterials cantilever upon temperature changes. The triple-beam structure also facilitated the novel thermometer with excellent fabrication feasibility by conventional microfabrication technology. The parameters of the triple-beam bimorph arrays were determined by finite element analysis with ANSYS program. Low stress Au and Mo metal films were used as top and bottom layer, respectively. The deflection of the triple-beam bimorphs were measured on a home-made heating stage by a confocal scanning laser microscopy. The novel bimorphs had temperature responses similar to traditional single-beam bimorphs. Initial bend of the prepared triple-beam bimorphs were dominantly determined by their side beams. The sensitivity of the novel thermometer was as high as 0.1°C. Experimental results showed that the novel thermometer is attractive for network sensing applications where the power capacity is limited.

The Infrared Thermometer in School Science: Teaching Physics with Modern Technologies

ERIC Educational Resources Information Center

Girwidz, Raimund; Ireson, Gren

2011-01-01

Infrared thermometers measure temperature from a distance, using the infrared radiation emitted by all objects. These so-called non-contact thermometers make a wide variety of temperature measurement and monitoring activities accessible to school-age students. Portable hand-held sensors also enable new or simplified investigations to be carried…

Baron Kelvin of Largs: an economical engineer.

PubMed

Fara, Patricia

2007-12-01

William Thomson--honoured as Baron Kelvin of Largs--was Victorian Britain's most famous physicist, especially celebrated for laying the trans-Atlantic telegraph cable. As well as profiting financially from his many engineering projects, Kelvin introduced influential theories about energy and electromagnetism, all strongly coloured by his industrial experiences and the thrifty attitudes of Scottish Christians. Never accepting radioactivity as an additional energy source to the sun, he insisted that the Earth's life span was far too short for evolution to have taken place.

Make Your Own Digital Thermometer!

ERIC Educational Resources Information Center

Sorey, Timothy; Willard, Teri; Kim, Bom

2010-01-01

In the hands-on, guided-inquiry lesson presented in this article, high school students create, calibrate, and apply an affordable scientific-grade instrument (Lapp and Cyrus 2000). In just four class periods, they build a homemade integrated circuit (IC) digital thermometer, apply a math model to calibrate their instrument, and ask a researchable…

Kelvin wave-induced trace constituent oscillations in the equatorial stratosphere

NASA Technical Reports Server (NTRS)

Randel, William J.

1990-01-01

Kelvin wave induced oscillations in ozone (O3), water vapor (H2O), nitric acid (HNO3) and nitrogen dioxide (NO2) in the equatorial stratosphere are analyzed using Limb Infrared Monitor of the Stratosphere (LIMS) data. Power and cross-spectrum analyses reveal coherent eastward propagating zonal wave 1 and 2 constituent fluctuations, due to the influence of Kelvin waves previously documented in the LIMS data. Comparison is made between a preliminary and the archival versions of the LIMS data; significant differences are found, demonstrating the sensitivity of constituent retrievals to derived temperature profiles. Because Kelvin waves have vanishing meridional velocity, analysis of tracer transport in the meridional plane is substantially simplified. Kelvin wave vertical advection is demonstrated by coherent, in-phase temperature-tracer oscillations, co-located near regions of strong background vertical gradients.

The Kelvin-Thomson Atom. Part 2: The Many-Electron Atoms

ERIC Educational Resources Information Center

Walton, Alan J.

1977-01-01

Presents part two of a two-part article describing the Kelvin-Thomson atom. This part discusses the arrangement of electrons within the atom and examines some of the properties predicted for elements in the Kelvin-Thomson model. (SL)

The Occurrence of Tidal Hybrid Kelvin-Edge Waves in the Global Ocean

NASA Astrophysics Data System (ADS)

Kaur, H.; Buijsman, M. C.; Yankovsky, A. E.; Zhang, T.; Jeon, C. H.

2017-12-01

This study presents the analysis of hybrid Kelvin-edge waves on the continental shelves in a global ocean model. Our objective is to find areas where the transition occurs from Kelvin waves to hybrid Kelvin-edge waves. The change in continental shelf width may convert a Kelvin wave into a hybrid Kelvin-edge wave. In this process the group velocity reaches a minimum and tidal energy is radiated on and/or offshore [Zhang 2016]. We extract M2 SSH (Sea Surface Height) and velocity from the Hybrid Coordinate Ocean Model (HYCOM) and calculate barotropic energy fluxes. We analyze these three areas: the Bay of Biscay, the Amazon Shelf and North West Africa. In these three regions, the continental shelf widens in the propagation direction and the alongshore flux changes its direction towards the coast. A transect is taken at different points in these areas to compute the dispersion relations of the waves on the continental shelf. In model simulations, we change the bathymetry of the Bay of Biscay to study the behavior of the hybrid Kelvin-edge waves. BibliographyZhang, T., and A. E Yankovsky. (2016), On the nature of cross-isobath energy fluxes in topographically modified barotropic semidiurnal Kelvin waves, J. Geophys. Res. Oceans, 121, 3058-3074, doi:10.1002/2015JC011617.

Application of radio frequency based digital thermometer for real-time monitoring of dairy cattle rectal temperature

PubMed Central

Debnath, Tridib; Bera, Santanu; Deb, Suman; Pal, Prasenjit; Debbarma, Nibash; Haldar, Avijit

2017-01-01

Aim: Dairy cattle health monitoring program becomes vital for detecting the febrile conditions to prevent the outbreak of the animal diseases as well as ensuring the fitness of the animals that are directly affecting the health of the consumers. The aim of this study was to validate real-time rectal temperature (RT) data of radio frequency based digital (RFD) thermometer with RT data of mercury bulb (MB) thermometer in dairy cattle. Materials and Methods: Two experiments were conducted. In experiment I, six female Jersey crossbred cattle with a mean (±standard error of the mean) body weight of 534.83±13.90 kg at the age of 12±0.52 years were used to record RT for 2 h on empty stomach and 2 h after feeding at 0, 30, 60, 90, and 120 min using a RFD thermometer as well as a MB thermometer. In experiment II, six female Jersey crossbred cattle were further used to record RT for 2 h before exercise and 2 h after exercise at 0, 30, 60, 90, and 120 min. Two-way repeated measures analysis of variance with post hoc comparisons by Bonferroni test was done. Results: Real-time RT data recorded by RFD thermometer as well as MB thermometer did not differ (p>0.05) before and after feeding/exercise. An increase (p<0.05) in RT after feeding/exercise in experimental crossbred cattle was recorded by both RFD thermometer and MB thermometer. Conclusion: The results obtained in the present study suggest that the body temperature recordings from RFD thermometer would be acceptable and thus RFD thermometer could work well for monitoring real-time RT in cattle. PMID:29062193

Application of radio frequency based digital thermometer for real-time monitoring of dairy cattle rectal temperature.

PubMed

Debnath, Tridib; Bera, Santanu; Deb, Suman; Pal, Prasenjit; Debbarma, Nibash; Haldar, Avijit

2017-09-01

Dairy cattle health monitoring program becomes vital for detecting the febrile conditions to prevent the outbreak of the animal diseases as well as ensuring the fitness of the animals that are directly affecting the health of the consumers. The aim of this study was to validate real-time rectal temperature (RT) data of radio frequency based digital (RFD) thermometer with RT data of mercury bulb (MB) thermometer in dairy cattle. Two experiments were conducted. In experiment I, six female Jersey crossbred cattle with a mean (±standard error of the mean) body weight of 534.83±13.90 kg at the age of 12±0.52 years were used to record RT for 2 h on empty stomach and 2 h after feeding at 0, 30, 60, 90, and 120 min using a RFD thermometer as well as a MB thermometer. In experiment II, six female Jersey crossbred cattle were further used to record RT for 2 h before exercise and 2 h after exercise at 0, 30, 60, 90, and 120 min. Two-way repeated measures analysis of variance with post hoc comparisons by Bonferroni test was done. Real-time RT data recorded by RFD thermometer as well as MB thermometer did not differ (p>0.05) before and after feeding/exercise. An increase (p<0.05) in RT after feeding/exercise in experimental crossbred cattle was recorded by both RFD thermometer and MB thermometer. The results obtained in the present study suggest that the body temperature recordings from RFD thermometer would be acceptable and thus RFD thermometer could work well for monitoring real-time RT in cattle.

The aluminum-in-olivine thermometer for mantle peridotites - Experimental versus empirical calibration and potential applications

NASA Astrophysics Data System (ADS)

Bussweiler, Y.; Brey, G. P.; Pearson, D. G.; Stachel, T.; Stern, R. A.; Hardman, M. F.; Kjarsgaard, B. A.; Jackson, S. E.

2017-02-01

This study provides an experimental calibration of the empirical Al-in-olivine thermometer for mantle peridotites proposed by De Hoog et al. (2010). We report Al concentrations measured by secondary ion mass spectrometry (SIMS) in olivines produced in the original high-pressure, high-temperature, four-phase lherzolite experiments by Brey et al. (1990). These reversed experiments were used for the calibration of the two-pyroxene thermometer and Al-in-orthopyroxene barometer by Brey and Köhler (1990). The experimental conditions of the runs investigated here range from 28 to 60 kbar and 1000 to 1300 °C. Olivine compositions from this range of experiments have Al concentrations that are consistent, within analytical uncertainties, with those predicted by the empirical calibration of the Al-in-olivine thermometer for mantle peridotites. Fitting the experimental data to a thermometer equation, using the least squares method, results in the expression: This version of the Al-in-olivine thermometer appears to be applicable to garnet peridotites (lherzolites and harzburgites) well outside the range of experimental conditions investigated here. However, the thermometer is not applicable to spinel-bearing peridotites. We provide new trace element criteria to distinguish between olivine from garnet-, garnet-spinel-, and spinel-facies peridotites. The estimated accuracy of the thermometer is ± 20 °C. Thus, the thermometer could serve as a useful tool in settings where two-pyroxene thermometry cannot be applied, such as garnet harzburgites and single inclusions in diamond.

A comparison of temporal artery thermometers with internal blood monitors to measure body temperature during hemodialysis.

PubMed

Lunney, Meaghan; Tonelli, Bronwyn; Lewis, Rachel; Wiebe, Natasha; Thomas, Chandra; MacRae, Jennifer; Tonelli, Marcello

2018-06-14

Thermometers that measure core (internal) body temperature are the gold standard for monitoring temperature. Despite that most modern hemodialysis machines are equipped with an internal blood monitor that measures core body temperature, current practice is to use peripheral thermometers. A better understanding of how peripheral thermometers compare with the dialysis machine thermometer may help guide practice. The study followed a prospective cross-sectional design. Hemodialysis patients were recruited from 2 sites in Calgary, Alberta (April - June 2017). Body temperatures were obtained from peripheral (temporal artery) and dialysis machine thermometers concurrently. Paired t-tests, Bland-Altman plots, and quantile-quantile plots were used to compare measurements from the two devices and to explore potential factors affecting temperature in hemodialysis patients. The mean body temperature of 94 hemodialysis patients measured using the temporal artery thermometer (36.7 °C) was significantly different than the dialysis machine thermometer (36.4 °C); p < 0.001. The mean difference (0.27 °C) appeared to be consistent across average temperature (range: 35.8-37.3 °C). Temperature measured by the temporal artery thermometer was statistically and clinically higher than that measured by the dialysis machine thermometer. Using the dialysis machine to monitor body temperature may result in more accurate readings and is likely to reduce the purchasing and maintenance costs associated with manual temperature readings, as well as easing the workload for dialysis staff.

Estimation of the Kelvin wave contribution to the semiannual oscillation

NASA Technical Reports Server (NTRS)

Hitchman, Matthew H.; Leovy, Conway B.

1988-01-01

Daily temperature data acquired during the Limb Infrared Monitor of the Stratosphere experiment are used to study the behavior of Kelvin waves in the equatorial middle atmosphere. It is suggested that Kelvin wave packets of different zonal wave numbers propagate separately and may be forced separately. Two Kelvin wave regimes were identified during the October 1978 to May 1979 data period. Most of the properties of the observed waves are shown to be consistent with slowly-varying theory. Results suggest that gravity waves may contribute significantly to the equatorial stratopause semiannual oscillation.

THE DYNAMIC RESPONSE OF THERMOMETER-WELL ASSEMBLIES.

DTIC Science & Technology

parameter models of the thermometric system were constructed and gave acceptable agreement with the experimental results. These models can be used to predict the dynamic behavior of any similar thermometer system. (Author)

Superconducting gamma and fast-neutron spectrometers with high energy resolution

DOEpatents

Friedrich, Stephan; , Niedermayr, Thomas R.; Labov, Simon E.

2008-11-04

Superconducting Gamma-ray and fast-neutron spectrometers with very high energy resolution operated at very low temperatures are provided. The sensor consists of a bulk absorber and a superconducting thermometer weakly coupled to a cold reservoir, and determines the energy of the incident particle from the rise in temperature upon absorption. A superconducting film operated at the transition between its superconducting and its normal state is used as the thermometer, and sensor operation at reservoir temperatures around 0.1 K reduces thermal fluctuations and thus enables very high energy resolution. Depending on the choice of absorber material, the spectrometer can be configured either as a Gamma-spectrometer or as a fast-neutron spectrometer.

Blackbody for metrological control of ear thermometers

NASA Astrophysics Data System (ADS)

Cárdenas-García, D.; Méndez-Lango, E.

2013-09-01

Body temperature is an important parameter in medical practice, and most of health diagnoses are made based upon measured temperature values. Non-contact measurements are attractive to both patients and physicians, and ear thermometers (ET) are part of the set of infrared thermometers for medical applications. ETs sense the tympanic membrane temperature which best represents body temperature. They take advantage of the natural high effective emissivity cavity that is formed as radiation source. To calibrate or to check the performance of ETs, we designed a high-emissivity spherical cavity as a blackbody source which can be placed in a dry block oven. Although the blackbody cavity can have any shape, we decided to build it spherical because its effective emissivity can be easily calculated in a closed form. The cavity is made of Aluminum to take advantage of its high thermal conductivity while its inner side is covered with a black paint to increase the cavity effective emissivity. Based on paint emissivity measurements and the geometrical shape, we calculated that the cavity has an effective emissivity higher than 0.999. Blackbody temperature is measured with a calibrated contact thermometer placed inside the bottom wall of the cavity. We present the design of the cavity, the experimental setup, and results of three commercial ETs compared with this cavity.

Tympanic thermometer performance validation by use of a body-temperature fixed point blackbody

NASA Astrophysics Data System (ADS)

Machin, Graham; Simpson, Robert

2003-04-01

The use of infrared tympanic thermometers within the medical community (and more generically in the public domain) has recently grown rapidly, displacing more traditional forms of thermometry such as mercury-in-glass. Besides the obvious health concerns over mercury the increase in the use of tympanic thermometers is related to a number of factors such as their speed and relatively non-invasive method of operation. The calibration and testing of such devices is covered by a number of international standards (ASTM1, prEN2, JIS3) which specify the design of calibration blackbodies. However these calibration sources are impractical for day-to-day in-situ validation purposes. In addition several studies (e.g. Modell et al4, Craig et al5) have thrown doubt on the accuracy of tympanic thermometers in clinical use. With this in mind the NPL is developing a practical, portable and robust primary reference fixed point source for tympanic thermometer validation. The aim of this simple device is to give the clinician a rapid way of validating the performance of their tympanic thermometer, enabling the detection of mal-functioning thermometers and giving confidence in the measurement to the clinician (and patient!) at point of use. The reference fixed point operates at a temperature of 36.3 °C (97.3 °F) with a repeatability of approximately +/- 20 mK. The fixed-point design has taken into consideration the optical characteristics of tympanic thermometers enabling wide-angled field of view devices to be successfully tested. The overall uncertainty of the device is estimated to be is less than 0.1°C. The paper gives a description of the fixed point, its design and construction as well as the results to date of validation tests.

Demonstrating the Temperature Dependence of Density via Construction of a Galilean Thermometer

ERIC Educational Resources Information Center

Priest, Marie A.; Padgett, Lea W.; Padgett, Clifford W.

2011-01-01

A method for the construction of a Galilean thermometer out of common chemistry glassware is described. Students in a first-semester physical chemistry (thermodynamics) class can construct the Galilean thermometer as an investigation of the thermal expansivity of liquids and the temperature dependence of density. This is an excellent first…

Comparison of infrared thermometer with thermocouple for monitoring skin temperature.

PubMed

Matsukawa, T; Ozaki, M; Nishiyama, T; Imamura, M; Kumazawa, T

2000-02-01

To test the hypothesis that the infrared thermometer (Genius) is comparably useful with thermocouples that are routinely used for skin temperature monitoring. Prospective, controlled, not blinded study. Operating room of a university hospital. Ten healthy male volunteers. Volunteers were minimally clothed and were initially warmed by a forced air warmer until they became vasodilated at the finger and the foot for approximately 30 mins. Subsequently, they were kept in the room with no blanket. Skin temperatures were measured continuously with the Mon-a-Therm thermocouple and were also measured with the Genius thermometer just before and after the warming and subsequently every 10 mins for 70 mins. Forearm and finger-tip skin temperatures and skin-surface temperature gradients (from arm to finger and from calf to toe) measured by the Genius thermometer were compared with those measured by the Mon-a-Therm thermocouple using linear regression and Bland and Altman statistics. Forearm temperature and finger-tip temperature ranged from approximately 31 degrees to approximately 36.5 degrees C (87.8-97.7 degrees F) and approximately 22.5 degrees to approximately 36 degrees C (72.5-96.8 degrees F), respectively. Gradients (from arm to finger and from calf to toe) ranged from approximately -3 degrees to approximately 10 degrees C (26.6-50.0 degrees F) and approximately -3 degrees to approximately 11 degrees C (26.6-51.8 degrees F), respectively. Correlations between the temperatures measured by the Genius thermometer and those by the Mon-a-Therm thermocouple were similar and reliable. The correlation coefficients were as follows: 0.78 at forearm, 0.97 at finger-tip, and 0.97 at skin-surface temperature gradients. The infrared thermometer with a special probe is useful to measure the change of skin-surface temperatures and to evaluate the severity of shock in patients.

A 10 Kelvin 3 Tesla Magnet for Space Flight ADR Systems

NASA Technical Reports Server (NTRS)

Tuttle, Jim; Shirron, Peter; Canavan, Edgar; DiPirro, Michael; Riall, Sara; Pourrahimi, Shahin

2003-01-01

Many future space flight missions are expected to use adiabatic demagnetization refrigerators (ADRs) to reach detector operating temperatures well below one Kelvin. The goal is to operate each ADR with a mechanical cooler as its heat sink, thus avoiding the use of liquid cryogens. Although mechanical coolers are being developed to operate at temperatures of 6 Kelvin and below, there is a large efficiency cost associated with operating them at the bottom of their temperature range. For the multi-stage ADR system being developed at Goddard Space Flight Center, the goal is to operate with a 10 Kelvin mechanical cooler heat sink. With currently available paramagnetic materials, the highest temperature ADR stage in such a system will require a magnetic field of approximately three Tesla. Thus the goal is to develop a small, lightweight three Tesla superconducting magnet for operation at 10 Kelvin. It is important that this magnet have a low current/field ratio. Because traditional NbTi magnets do not operate safely above about six Kelvin, a magnet with a higher Tc is required. The primary focus has been on Nb3Sn magnets. Since standard Nb3Sn wire must be coated with thick insulation, wound on a magnet mandrel and then reacted, standard Nb,Sn magnets are quite heavy and require high currents Superconducting Systems developed a Nb3Sn wire which can be drawn down to small diameter, reacted, coated with thin insulation and then wound on a small diameter coil form. By using this smaller wire and operating closer to the wire s critical current, it should be possible to reduce the mass and operating current of 10 Kelvin magnets. Using this "react-then-wind" technology, Superconducting Systems has produced prototype 10 Kelvin magnets. This paper describes the development and testing of these magnets and discusses the outlook for including 10 Kelvin magnets on space-flight missions.

The use of infrared ear thermometers in pediatric and family practice offices.

PubMed

Silverman, B G; Daley, W R; Rubin, J D

1998-01-01

To describe the use of infrared (IR) ear thermometers in pediatric and family practice offices. The authors mailed a questionnaire to 350 randomly selected members of the American Academy of Pediatrics and to 355 randomly selected members of the American Academy of Family Physicians. Of respondents in clinical practice, 78% had used IR ear thermometers at least once in the past; 65% of pediatricians and 64% of family practice physicians were current users. Seventeen percent of pediatric offices and 18% of family practice offices that had used IR ear thermometers had discontinued use, most citing inaccuracy or lack of staff trust in the device. Pediatric offices were less likely than family practice offices to use the device in well neonates and sick neonates and more likely to use it in sick children. Advantages cited included rapid readings, ease of use, and accuracy. Seventy-five percent of current users reported at least one problem, including low readings and lack of staff trust. IR ear thermometers are widely used in pediatric and family practice offices. Some offices limit use of these devices to older children and adults, and most of the offices surveyed report using other devices as a check on the accuracy of IR thermometers. Statements by professional organizations that provide user guidelines and establish appropriate age cut-offs would be helpful.

Radiation Requirements and Testing of Cryogenic Thermometers for the Ilc

NASA Astrophysics Data System (ADS)

Barnett, T.; Filippov, Yu. P.; Filippova, E. Yu.; Mokhov, N. V.; Nakao, N.; Klebaner, A. L.; Korenev, S. A.; Theilacker, J. C.; Trenikhina, J.; Vaziri, K.

2008-03-01

Large quantity of cryogenic temperature sensors will be used for operation of the International Linear Collider (ILC). Most of them will be subject to high radiation doses during the accelerator lifetime. Understanding of particle energy spectra, accumulated radiation dose in thermometers and its impact on performance are vital in establishing technical specification of cryogenic thermometry for the ILC. Realistic MARS15 computer simulations were performed to understand the ILC radiation environment. Simulation results were used to establish radiation dose requirements for commercially available cryogenic thermometers. Two types of thermometers, Cernox® and TVO, were calibrated prior to irradiation using different technique. The sensors were subjected then to up to 200 kGy electron beam irradiation with kinetic energy of 5 MeV, a representative of the situation at the ILC operation. A post-irradiation behavior of the sensors was studied. The paper describes the MARS15 model, simulation results, cryogenic test set-up, irradiation tests, and cryogenic test results.

Multitip scanning bio-Kelvin probe

NASA Astrophysics Data System (ADS)

Baikie, I. D.; Smith, P. J. S.; Porterfield, D. M.; Estrup, P. J.

1999-03-01

We have developed a novel multitip scanning Kelvin probe which can measure changes in biological surface potential ΔVs to within 2 mV and, quasisimultaneously monitor displacement to <1 μm. The control and measurement subcomponents are PC based and incorporate a flexible user interface permitting software control of each individual tip, measurement, and scan parameters. We review the mode of operation and design features of the scanning bio-Kelvin probe including tip steering, signal processing, tip calibration, and novel tip tracking/dithering routines. This system uniquely offers both tip-to-sample spacing control (which is essential to avoid spurious changes in ΔVs due to variations in mean spacing) and a dithering routine to maintain tip orientation to the biological specimen, irrespective of the latter's movement. These features permit long term (>48 h) "active" tracking of the displacement and biopotentials developed along and around a plant shoot in response to an environmental stimulus, e.g., differential illumination (phototropism) or changes in orientation (gravitropism).

Modeling ramp-hold indentation measurements based on Kelvin-Voigt fractional derivative model

NASA Astrophysics Data System (ADS)

Zhang, Hongmei; zhe Zhang, Qing; Ruan, Litao; Duan, Junbo; Wan, Mingxi; Insana, Michael F.

2018-03-01

Interpretation of experimental data from micro- and nano-scale indentation testing is highly dependent on the constitutive model selected to relate measurements to mechanical properties. The Kelvin-Voigt fractional derivative model (KVFD) offers a compact set of viscoelastic features appropriate for characterizing soft biological materials. This paper provides a set of KVFD solutions for converting indentation testing data acquired for different geometries and scales into viscoelastic properties of soft materials. These solutions, which are mostly in closed-form, apply to ramp-hold relaxation, load-unload and ramp-load creep-testing protocols. We report on applications of these model solutions to macro- and nano-indentation testing of hydrogels, gastric cancer cells and ex vivo breast tissue samples using an atomic force microscope (AFM). We also applied KVFD models to clinical ultrasonic breast data using a compression plate as required for elasticity imaging. Together the results show that KVFD models fit a broad range of experimental data with a correlation coefficient typically R 2  >  0.99. For hydrogel samples, estimation of KVFD model parameters from test data using spherical indentation versus plate compression as well as ramp relaxation versus load-unload compression all agree within one standard deviation. Results from measurements made using macro- and nano-scale indentation agree in trend. For gastric cell and ex vivo breast tissue measurements, KVFD moduli are, respectively, 1/3-1/2 and 1/6 of the elasticity modulus found from the Sneddon model. In vivo breast tissue measurements yield model parameters consistent with literature results. The consistency of results found for a broad range of experimental parameters suggest the KVFD model is a reliable tool for exploring intrinsic features of the cell/tissue microenvironments.

Thermal conductivity of ultrathin nano-crystalline diamond films determined by Raman thermography assisted by silicon nanowires

NASA Astrophysics Data System (ADS)

Anaya, Julian; Rossi, Stefano; Alomari, Mohammed; Kohn, Erhard; Tóth, Lajos; Pécz, Béla; Kuball, Martin

2015-06-01

The thermal transport in polycrystalline diamond films near its nucleation region is still not well understood. Here, a steady-state technique to determine the thermal transport within the nano-crystalline diamond present at their nucleation site has been demonstrated. Taking advantage of silicon nanowires as surface temperature nano-sensors, and using Raman Thermography, the in-plane and cross-plane components of the thermal conductivity of ultra-thin diamond layers and their thermal barrier to the Si substrate were determined. Both components of the thermal conductivity of the nano-crystalline diamond were found to be well below the values of polycrystalline bulk diamond, with a cross-plane thermal conductivity larger than the in-plane thermal conductivity. Also a depth dependence of the lateral thermal conductivity through the diamond layer was determined. The results impact the design and integration of diamond for thermal management of AlGaN/GaN high power transistors and also show the usefulness of the nanowires as accurate nano-thermometers.

Silicon-based Coulomb blockade thermometer with Schottky barriers

NASA Astrophysics Data System (ADS)

Tuboltsev, V.; Savin, A.; Rogozin, V. D.; Räisänen, J.

2014-04-01

A hybrid Coulomb blockade thermometer (CBT) in form of an array of intermittent aluminum and silicon islands connected in series via tunnel junctions was fabricated on a thin silicon-on-insulator (SOI) film. Tunnel barriers in the micrometer size junctions were formed by metal-semiconductor Schottky contacts between aluminium electrodes and heavily doped silicon. Differential conductance through the array vs. bias voltage was found to exhibit characteristic features of competing thermal and charging effects enabling absolute temperature measurements over the range of ˜65 to ˜500 mK. The CBT performance implying the primary nature of the thermometer demonstrated for rather trivial architecture attempted in this work paves a route for introduction of Coulomb blockade thermometry into well-developed contemporary SOI technology.

High resolution structural characterization of giant magnetoresistance structures containing a nano-oxide layer

NASA Astrophysics Data System (ADS)

You, C. Y.; Cerezo, A.; Clifton, P. H.; Folks, L.; Carey, M. J.; Petford-Long, A. K.

2007-07-01

The microstructure and chemistry of a current-perpendicular-to-plane giant magnetoresistance structure containing a nano-oxide layer (NOL) have been studied using a combination of high resolution transmission electron microscopy and three-dimensional atom probe analysis. It was found that the morphology of the NOL changes from a planar layer to discrete particles on annealing, indicating the dominance of surface energy on the morphology evolution. Direct evidence was obtained for significant Mn diffusion from the IrMn antiferromagnetic layer and partitioning to the oxide region during annealing.

Phase locking of convectively coupled equatorial atmospheric Kelvin waves over Indian Ocean basin

NASA Astrophysics Data System (ADS)

Baranowski, Dariusz; Flatau, Maria; Flatau, Piotr; Matthews, Adrian

2015-04-01

The properties of convectively coupled Kelvin waves in the Indian Ocean and their propagation over the Maritime Continent are studied. It is shown that Kelvin waves are longitude - diurnal cycle phase locked over the Maritime Continent, Africa and the Indian Ocean. Thus, it is shown that they tend to propagate over definite areas during specific times of the day. Over the Maritime Continent, longitude-diurnal cycle phase locking is such that it agrees with mean, local diurnal cycle of convection. The strength of the longitude-diurnal cycle phase locking differs between 'non-blocked' Kelvin waves, which make successful transition over the Maritime Continent, and 'blocked' waves that terminated within it. It is shown that a specific combination of Kelvin wave phase speed and time of the day at which a wave approaches the Maritime Continent influence the chance of successful transition into the Western Pacific. Kelvin waves that maintain phase speed of 10 to 11 degrees per day over the central-eastern Indian Ocean and arrive at 90E between 9UTC and 18UTC have the highest chance of being 'non-blocked' by the Maritime Continent. The distance between the islands of Sumatra and Borneo agrees with the distance travelled by an average convectively coupled Kelvin wave in one day. This suggests that the Maritime Continent may act as a 'filter' for Kelvin waves favoring successful propagation of those waves for which propagation is in phase with the local diurnal cycle of precipitation. The AmPm index, a simple measure of local diurnal cycle for propagating disturbances, is introduced and shown to be useful metric depicting key characteristics of the convection associated with propagating Kelvin waves.

Direct imaging of defect formation in strained organic flexible electronics by Scanning Kelvin Probe Microscopy

PubMed Central

Cramer, Tobias; Travaglini, Lorenzo; Lai, Stefano; Patruno, Luca; de Miranda, Stefano; Bonfiglio, Annalisa; Cosseddu, Piero; Fraboni, Beatrice

2016-01-01

The development of new materials and devices for flexible electronics depends crucially on the understanding of how strain affects electronic material properties at the nano-scale. Scanning Kelvin-Probe Microscopy (SKPM) is a unique technique for nanoelectronic investigations as it combines non-invasive measurement of surface topography and surface electrical potential. Here we show that SKPM in non-contact mode is feasible on deformed flexible samples and allows to identify strain induced electronic defects. As an example we apply the technique to investigate the strain response of organic thin film transistors containing TIPS-pentacene patterned on polymer foils. Controlled surface strain is induced in the semiconducting layer by bending the transistor substrate. The amount of local strain is quantified by a mathematical model describing the bending mechanics. We find that the step-wise reduction of device performance at critical bending radii is caused by the formation of nano-cracks in the microcrystal morphology of the TIPS-pentacene film. The cracks are easily identified due to the abrupt variation in SKPM surface potential caused by a local increase in resistance. Importantly, the strong surface adhesion of microcrystals to the elastic dielectric allows to maintain a conductive path also after fracture thus providing the opportunity to attenuate strain effects. PMID:27910889

The Fourier-Kelvin Stellar Interferometer

NASA Astrophysics Data System (ADS)

Danchi, W. C.; Allen, R. J.; Benford, D. J.; Deming, D.; Gezari, D. Y.; Kuchner, M.; Leisawitz, D. T.; Linfield, R.; Millan-Gabet, R.; Monnier, J. D.; Mumma, M.; Mundy, L. G.; Noecker, C.; Rajagopal, J.; Seager, S.; Traub, W. A.

2003-10-01

The Fourier-Kelvin Stellar Interferometer (FKSI) is a mission concept for an imaging and nulling interferometer for the mid-infrared spectral region (5- 28 microns). FKSI is conceived as a scientific and technological pathfinder to TPF/DARWIN as well as the NASA Vision Missions SAFIR and SPECS. It will also be a high angular resolution infrared space observatory complementary to JWST. The scientific emphasis of the mission is on detection and spectroscopy of the atmospheres of Extra-solar Giant Planets (EGPs), the search for Brown Dwarfs and other low mass stellar companions, and the evolution of protostellar systems. FKSI can observe these systems from just after the collapse of the precursor molecular cloud core, through the formation of the disk surrounding the protostar, the formation of planets in the disk, and eventual dispersal of the disk material. FKSI could also play a very powerful role in the investigation of the structure of active galactic nuclei and extra-galactic star formation. We present the major results of a set of detailed design studies for the FKSI mission that were performed as a method of understanding major trade-offs pertinent to schedule, cost, and risk in preparation for submission of a Discovery proposal.

Calibration of Radiation Thermometers up to : Effective Emissivity of the Source

NASA Astrophysics Data System (ADS)

Kozlova, O.; Briaudeau, S.; Rongione, L.; Bourson, F.; Guimier, S.; Kosmalski, S.; Sadli, M.

2015-08-01

The growing demand of industry for traceable temperature measurements up to encourages improvement of calibration techniques for industrial-type radiation thermometers in this temperature range. High-temperature fixed points can be used at such high temperatures, but due to the small diameter of apertures of their cavities (3 mm), they are not adapted for the large field-of-views commonly featured by this kind of radiation thermometers. At LNE-Cnam, a Thermo Gauge furnace of 25.4 mm source aperture diameter is used as a comparison source to calibrate customers' instruments against a reference radiation thermometer calibrated according to the ITS-90 with the lowest uncertainties achievable in the Laboratory. But the furnace blackbody radiator exhibits a large temperature gradient that degrades its effective emissivity, and increases the calibration uncertainty due to the lack of information on the working spectral band of the industrial radiation thermometer. In order to estimate the corrections to apply, the temperature distribution (radial and on-axis) of the Thermo Gauge furnace blackbody radiator was characterized and the effective emissivity of the Thermo Gauge cavity was determined by three different methods. Because of this investigation, the corrections due to different fields of view and due to the different spectral bands of the reference pyrometer and the customer's pyrometer were obtained and the uncertainties on these corrections were evaluated.

Towards a practical Johnson noise thermometer for long-term measurements in harsh environments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Greenen, Adam; Pearce, Jonathan; Cruickshank, David

The impact of mechanical and chemical changes in conventional sensors such as thermocouples and resistance thermometers can be avoided by instead using temperature sensors based on fundamental thermometry. A prime example of this is Johnson noise thermometry, which is based on measurement of the fluctuations in the voltage of a resistor arising from thermal motion of charge carriers - i.e. the 'Johnson noise'. A Johnson noise thermometer never needs calibration and is insensitive to the condition of the sensor material. It is therefore ideally suited to long-term temperature measurements in harsh environments, such as nuclear reactor coolant circuits, in-pile measurements,more » nuclear waste management and storage, and severe accident monitoring. There have been a number of previous attempts to develop a Johnson noise thermometer for the nuclear industry, but none have reached commercial exploitation because of technical problems in practical implementation. The main challenge is to extract the tiny Johnson noise signal from ambient electrical noise influences, both from the internal amplification electronics, and from external electrical noise sources. Recent advances in electronics technology and digital signal processing techniques have opened up new possibilities for developing a viable, practical Johnson noise thermometer. We describe a project funded by the UK Technology Strategy Board (now Innovate UK) 'Developing the nuclear supply chain' call, currently underway, to develop a practical Johnson noise thermometer that makes use of innovative electronics for ultralow noise amplification and signal processing. The new electronics technology has the potential to help overcome the problems encountered with previous attempts at constructing a practical Johnson noise thermometer. An outline of the new developments is presented, together with an overview of the current status of the project. (authors)« less

Measurement time and statistics for a noise thermometer with a synthetic-noise reference

NASA Astrophysics Data System (ADS)

White, D. R.; Benz, S. P.; Labenski, J. R.; Nam, S. W.; Qu, J. F.; Rogalla, H.; Tew, W. L.

2008-08-01

This paper describes methods for reducing the statistical uncertainty in measurements made by noise thermometers using digital cross-correlators and, in particular, for thermometers using pseudo-random noise for the reference signal. First, a discrete-frequency expression for the correlation bandwidth for conventional noise thermometers is derived. It is shown how an alternative frequency-domain computation can be used to eliminate the spectral response of the correlator and increase the correlation bandwidth. The corresponding expressions for the uncertainty in the measurement of pseudo-random noise in the presence of uncorrelated thermal noise are then derived. The measurement uncertainty in this case is less than that for true thermal-noise measurements. For pseudo-random sources generating a frequency comb, an additional small reduction in uncertainty is possible, but at the cost of increasing the thermometer's sensitivity to non-linearity errors. A procedure is described for allocating integration times to further reduce the total uncertainty in temperature measurements. Finally, an important systematic error arising from the calculation of ratios of statistical variables is described.

Lab-based x-ray nanoCT imaging

NASA Astrophysics Data System (ADS)

Müller, Mark; Allner, Sebastian; Ferstl, Simone; Dierolf, Martin; Tuohimaa, Tomi; Pfeiffer, Franz

2017-03-01

Due to the recent development of transmission X-ray tubes with very small focal spot sizes, laboratory-based CT imaging with sub-micron resolutions is nowadays possible. We recently developed a novel X-ray nanoCT setup featuring a prototype nanofocus X-ray source and a single-photon counting detector. The system is based on mere geometrical magnification and can reach resolutions of 200 nm. To demonstrate the potential of the nanoCT system for biomedical applications we show high resolution nanoCT data of a small piece of human tooth comprising coronal dentin. The reconstructed CT data clearly visualize the dentin tubules within the tooth piece.

Real-space measurement of potential distribution in PECVD ONO electrets by Kelvin probe force microscopy.

PubMed

Emmerich, F; Thielemann, C

2016-05-20

Multilayers of silicon oxide/silicon nitride/silicon oxide (ONO) are known for their good electret properties due to deep energy traps near the material interfaces, facilitating charge storage. However, measurement of the space charge distribution in such multilayers is a challenge for conventional methods if layer thickness dimensions shrink below 1 μm. In this paper, we propose an atomic force microscope based method to determine charge distributions in ONO layers with spatial resolution below 100 nm. By applying Kelvin probe force microscopy (KPFM) on freshly cleaved, corona-charged multilayers, the surface potential is measured directly along the z-axis and across the interfaces. This new method gives insights into charge distribution and charge movement in inorganic electrets with a high spatial resolution.

27 CFR 30.22 - Hydrometers and thermometers.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 27 Alcohol, Tobacco Products and Firearms 1 2010-04-01 2010-04-01 false Hydrometers and... BUREAU, DEPARTMENT OF THE TREASURY LIQUORS GAUGING MANUAL Gauging Instruments § 30.22 Hydrometers and thermometers. The hydrometers used are graduated to read the proof of aqueous alcoholic solutions at 60 degrees...

Challenges for Super-Resolution Localization Microscopy and Biomolecular Fluorescent Nano-Probing in Cancer Research

PubMed Central

Ilić, Nataša; Pilarczyk, Götz; Lee, Jin-Ho; Logeswaran, Abiramy; Borroni, Aurora Paola; Krufczik, Matthias; Theda, Franziska; Waltrich, Nadine; Bestvater, Felix; Hildenbrand, Georg; Cremer, Christoph; Blank, Michael

2017-01-01

Understanding molecular interactions and regulatory mechanisms in tumor initiation, progression, and treatment response are key requirements towards advanced cancer diagnosis and novel treatment procedures in personalized medicine. Beyond decoding the gene expression, malfunctioning and cancer-related epigenetic pathways, investigations of the spatial receptor arrangements in membranes and genome organization in cell nuclei, on the nano-scale, contribute to elucidating complex molecular mechanisms in cells and tissues. By these means, the correlation between cell function and spatial organization of molecules or molecular complexes can be studied, with respect to carcinogenesis, tumor sensitivity or tumor resistance to anticancer therapies, like radiation or antibody treatment. Here, we present several new applications for bio-molecular nano-probes and super-resolution, laser fluorescence localization microscopy and their potential in life sciences, especially in biomedical and cancer research. By means of a tool-box of fluorescent antibodies, green fluorescent protein (GFP) tagging, or specific oligonucleotides, we present tumor relevant re-arrangements of Erb-receptors in membranes, spatial organization of Smad specific ubiquitin protein ligase 2 (Smurf2) in the cytosol, tumor cell characteristic heterochromatin organization, and molecular re-arrangements induced by radiation or antibody treatment. The main purpose of this article is to demonstrate how nano-scaled distance measurements between bio-molecules, tagged by appropriate nano-probes, can be applied to elucidate structures and conformations of molecular complexes which are characteristic of tumorigenesis and treatment responses. These applications open new avenues towards a better interpretation of the spatial organization and treatment responses of functionally relevant molecules, at the single cell level, in normal and cancer cells, offering new potentials for individualized medicine. PMID:28956810

Challenges for Super-Resolution Localization Microscopy and Biomolecular Fluorescent Nano-Probing in Cancer Research.

PubMed

Hausmann, Michael; Ilić, Nataša; Pilarczyk, Götz; Lee, Jin-Ho; Logeswaran, Abiramy; Borroni, Aurora Paola; Krufczik, Matthias; Theda, Franziska; Waltrich, Nadine; Bestvater, Felix; Hildenbrand, Georg; Cremer, Christoph; Blank, Michael

2017-09-28

Understanding molecular interactions and regulatory mechanisms in tumor initiation, progression, and treatment response are key requirements towards advanced cancer diagnosis and novel treatment procedures in personalized medicine. Beyond decoding the gene expression, malfunctioning and cancer-related epigenetic pathways, investigations of the spatial receptor arrangements in membranes and genome organization in cell nuclei, on the nano-scale, contribute to elucidating complex molecular mechanisms in cells and tissues. By these means, the correlation between cell function and spatial organization of molecules or molecular complexes can be studied, with respect to carcinogenesis, tumor sensitivity or tumor resistance to anticancer therapies, like radiation or antibody treatment. Here, we present several new applications for bio-molecular nano-probes and super-resolution, laser fluorescence localization microscopy and their potential in life sciences, especially in biomedical and cancer research. By means of a tool-box of fluorescent antibodies, green fluorescent protein (GFP) tagging, or specific oligonucleotides, we present tumor relevant re-arrangements of Erb-receptors in membranes, spatial organization of Smad specific ubiquitin protein ligase 2 (Smurf2) in the cytosol, tumor cell characteristic heterochromatin organization, and molecular re-arrangements induced by radiation or antibody treatment. The main purpose of this article is to demonstrate how nano-scaled distance measurements between bio-molecules, tagged by appropriate nano-probes, can be applied to elucidate structures and conformations of molecular complexes which are characteristic of tumorigenesis and treatment responses. These applications open new avenues towards a better interpretation of the spatial organization and treatment responses of functionally relevant molecules, at the single cell level, in normal and cancer cells, offering new potentials for individualized medicine.

Calibration and tests of commercial wireless infrared thermometers

USDA-ARS?s Scientific Manuscript database

Applications of infrared thermometers (IRTs) in large agricultural fields require wireless data transmission, and IRT target temperature should have minimal sensitivity to internal detector temperature. To meet these objectives, a prototype wireless IRT system was developed at USDA Agricultural Rese...

Observational evidence of the downstream impact on tropical rainfall from stratospheric Kelvin waves

NASA Astrophysics Data System (ADS)

Zhang, Lei; Karnauskas, Kristopher B.; Weiss, Jeffrey B.; Polvani, Lorenzo M.

2017-08-01

Analysis of one continuous decade of daily, high-vertical resolution sounding data from five proximate islands in the western equatorial Pacific region reveals eastward and downward propagating Kelvin waves in the tropical stratosphere, with a zonal wave number one structure and a period of 15 days. By defining an initiation index, we find that these waves are primarily generated over the western Pacific warm pool and South America-tropical Atlantic sector, consistent with regions of frequent deep convection. The zonal phase speed of the stratospheric Kelvin waves (SKWs) is relatively slow ( 10 m s-1) over the initiation region due to coupling with deep convection, and becomes much faster ( 30-40 m s-1) once decoupled from the downstream troposphere. SKWs have significant impacts on downstream tropical rainfall through modulation of tropopause height. The cold phase of SKWs at tropopause leads to higher tropopause heights and more convection in tropics—with opposite impacts associated with the warm phase. Downstream tropical precipitation anomalies associated with these SKWs also propagate eastward with the same speed and zonal scale as observed SKWs. Interannual variability of the amplitude of the SKWs is shown to be associated with the Quasi-Biennial oscillation (QBO); implications for predictability are discussed.

Kelvin-wave cascade in the vortex filament model

NASA Astrophysics Data System (ADS)

Baggaley, Andrew W.; Laurie, Jason

2014-01-01

The small-scale energy-transfer mechanism in zero-temperature superfluid turbulence of helium-4 is still a widely debated topic. Currently, the main hypothesis is that weakly nonlinear interacting Kelvin waves (KWs) transfer energy to sufficiently small scales such that energy is dissipated as heat via phonon excitations. Theoretically, there are at least two proposed theories for Kelvin-wave interactions. We perform the most comprehensive numerical simulation of weakly nonlinear interacting KWs to date and show, using a specially designed numerical algorithm incorporating the full Biot-Savart equation, that our results are consistent with the nonlocal six-wave KW interactions as proposed by L'vov and Nazarenko.

Development of a 300 L Calibration Bath for Oceanographic Thermometers

NASA Astrophysics Data System (ADS)

Baba, S.; Yamazawa, K.; Nakano, T.; Saito, I.; Tamba, J.; Wakimoto, T.; Katoh, K.

2017-11-01

The Japan Agency for Marine-Earth Science and Technology (JAMSTEC) has been developing a 300 L calibration bath to calibrate 24 oceanographic thermometers (OT) simultaneously and thereby reduce the calibration work load necessary to service more than 180 OT every year. This study investigated characteristics of the developed 300 L calibration bath using a SBE 3plus thermometer produced by an OT manufacturer. We also used 11 thermistor thermometers that were calibrated to be traceable to the international temperature scale of 1990 (ITS-90) within 1 mK of standard uncertainty through collaboration of JAMSTEC and NMIJ/AIST. Results show that the time stability of temperature of the developed bath was within ± 1 mK. Furthermore, the temperature uniformity was ± 1.3 mK. The expanded uncertainty (k=2) components for the characteristics of the developed 300 L calibration bath were estimated as 2.9 mK, which is much less than the value of 10 mK: the required specification for uncertainty of calibration for the OT. These results demonstrated the utility of this 300 L calibration bath as a device for use with a new calibration system.

Development of Tunneling Spectroscopy Apparatus for Kelvin and Sub-Kelvin Measurements of Superconducting Energy Gaps by Multi-disciplinary students at a Liberal Arts University

NASA Astrophysics Data System (ADS)

Eckhardt, Matt

2014-03-01

Tunneling spectroscopy is an important technique used to measure the superconducting energy gap, a feature that is at the heart of the nature of superconductivity in various materials. In this presentation, we report the progress and results in developing high-resolution tunneling spectroscopy experimental platforms in a helium three cryostat, a 3 Kelvin cryocooler and a helium dip-tester. The experimental team working in a liberal arts university is a multi-disciplinary group consisting of one physics major, chemisty majors and a biology major. Students including non-physics majors learned and implemented current-voltage measurement techniques, vacuum system engineering, built electronic boxes and amplifier circuits from scratch, built custom multi-conductor cables for thermometry and current-voltage measurements, and performed conductance measurements. We report preliminary results. Acknowledgments: We acknowledge support from National Science Foundation Grant # DMR-1206561.

Promoting Inclusive Chemistry Teaching by Developing an Accessible Thermometer for Students with Visual Disabilities

ERIC Educational Resources Information Center

Vitoriano, Felipe A.; Teles, Vânia L. G.; Rizzatti, Ivanise M.; Pesssoa de Lima, Régia C.

2016-01-01

This work discusses the construction and evaluation of a digital thermometer especially designed to be operated by people with visual disabilities. The accessibility thermometer can be used as an educational tool in practical activities in classes for sighted and visually impaired students, with the aim of helping those with special needs gain…

New blackbody standard for the evaluation and calibration of tympanic ear thermometers at the NPL, United Kingdom

NASA Astrophysics Data System (ADS)

McEvoy, Helen C.; Simpson, Robert; Machin, Graham

2004-04-01

The use of infrared tympanic thermometers for monitoring patient health is widespread. However, studies into the performance of these thermometers have questioned their accuracy and repeatability. To give users confidence in these devices, and to provide credibility in the measurements, it is necessary for them to be tested using an accredited, standard blackbody source, with a calibration traceable to the International Temperature Scale of 1990 (ITS-90). To address this need the National Physical Laboratory (NPL), UK, has recently set up a primary ear thermometer calibration (PET-C) source for the evaluation and calibration of tympanic (ear) thermometers over the range from 15 °C to 45 °C. The overall uncertainty of the PET-C source is estimated to be +/- 0.04 °C at k = 2. The PET-C source meets the requirements of the European Standard EN 12470-5: 2003 Clinical thermometers. It consists of a high emissivity blackbody cavity immersed in a bath of stirred liquid. The temperature of the blackbody is determined using an ITS-90 calibrated platinum resistance thermometer inserted close to the rear of the cavity. The temperature stability and uniformity of the PET-C source was evaluated and its performance validated. This paper provides a description of the PET-C along with the results of the validation measurements. To further confirm the performance of the PET-C source it was compared to the standard ear thermometer calibration sources of the National Metrology Institute of Japan (NMIJ), Japan and the Physikalisch-Technische Bundesanstalt (PTB), Germany. The results of this comparison will also be briefly discussed. The PET-C source extends the capability for testing ear thermometers offered by the NPL body temperature fixed-point source, described previously. An update on the progress with the commercialisation of the fixed-point source will be given.

Surface potential extraction from electrostatic and Kelvin-probe force microscopy images

NASA Astrophysics Data System (ADS)

Xu, Jie; Chen, Deyuan; Li, Wei; Xu, Jun

2018-05-01

A comprehensive comparison study of electrostatic force microscopy (EFM) and Kelvin probe force microscopy (KPFM) is conducted in this manuscript. First, it is theoretically demonstrated that for metallic or semiconductor samples, both the EFM and KPFM signals are a convolution of the sample surface potential with their respective transfer functions. Then, an equivalent point-mass model describing cantilever deflection under distributed loads is developed to reevaluate the cantilever influence on detection signals, and it is shown that the cantilever has no influence on the EFM signal, while it will affect the KPFM signal intensity but not change the resolution. Finally, EFM and KPFM experiments are carried out, and the surface potential is extracted from the EFM and KPFM images by deconvolution processing, respectively. The extracted potential intensity is well consistent with each other and the detection resolution also complies with the theoretical analysis. Our work is helpful to perform a quantitative analysis of EFM and KPFM signals, and the developed point-mass model can also be used for other cantilever beam deflection problems.

Using an Infrared Thermometer for Solar Pyranometry

ERIC Educational Resources Information Center

Fiedler, B. H.

2011-01-01

The simple hand-held infrared thermometer can be used to measure the temperature of surfaces of different reflectivity exposed to sunlight and wind. From four temperature measurements of black and white panels in windy and wind-sheltered conditions, together with the two wind speed measurements, both the flux of incident solar radiation and the…

Specific heats of lunar surface materials from 90 to 350 degrees Kelvin

USGS Publications Warehouse

Robie, R.A.; Hemingway, B.S.; Wilson, W.H.

1970-01-01

The specific heats of lunar samples 10057 and 10084 returned by the Apollo 11 mission have been measured between 90 and 350 degrees Kelvin by use of an adiabatic calorimeter. The samples are representative of type A vesicular basalt-like rocks and of finely divided lunar soil. The specific heat of these materials changes smoothly from about 0.06 calorie per gram per degree at 90 degrees Kelvin to about 0.2 calorie per gram per degree at 350 degrees Kelvin. The thermal parameter ??=(k??C)-1/2 for the lunar surface will accordingly vary by a factor of about 2 between lunar noon and midnight.

Kelvin-Helmholtz evolution in subsonic cold streams feeding galaxies

NASA Astrophysics Data System (ADS)

Angulo, Adrianna; Coffing, S.; Kuranz, C.; Drake, R. P.; Klein, S.; Trantham, M.; Malamud, G.

2017-10-01

The most prolific star formers in cosmological history lie in a regime where dense filament structures carried substantial mass into the galaxy to sustain star formation without producing a shock. However, hydrodynamic instabilities present on the filament surface limit the ability of such structures to deliver dense matter deeply enough to sustain star formation. Simulations lack the finite resolution necessary to allow fair treatment of the instabilities present at the stream boundary. Using the Omega EP laser, we simulate this mode of galaxy formation with a cold, dense, filament structure within a hotter, subsonic flow and observe the interface evolution. Machined surface perturbations stimulate the development of the Kelvin-Helmholtz (KH) instability due to the resultant shear between the two media. A spherical crystal imaging system produces high-resolution radiographs of the KH structures along the filament surface. The results from the first experiments of this kind, using a rod with single-mode, long-wavelength modulations, will be discussed. This work is funded by the U.S. Department of Energy, through the NNSA-DS and SC-OFES Joint Program in High-Energy-Density Laboratory Plasmas, Grant Number DE-NA0002956, and the National Laser User Facility Program, Grant Number DE-NA0002719, and through.

Direct probing of electron and hole trapping into nano-floating-gate in organic field-effect transistor nonvolatile memories

NASA Astrophysics Data System (ADS)

Cui, Ze-Qun; Wang, Shun; Chen, Jian-Mei; Gao, Xu; Dong, Bin; Chi, Li-Feng; Wang, Sui-Dong

2015-03-01

Electron and hole trapping into the nano-floating-gate of a pentacene-based organic field-effect transistor nonvolatile memory is directly probed by Kelvin probe force microscopy. The probing is straightforward and non-destructive. The measured surface potential change can quantitatively profile the charge trapping, and the surface characterization results are in good accord with the corresponding device behavior. Both electrons and holes can be trapped into the nano-floating-gate, with a preference of electron trapping than hole trapping. The trapped charge quantity has an approximately linear relation with the programming/erasing gate bias, indicating that the charge trapping in the device is a field-controlled process.

High resolution photolithography using arrays of polystyrene and SiO2 micro- and nano-sized spherical lenses

NASA Astrophysics Data System (ADS)

Dvoretckaia, L. N.; Mozharov, A. M.; Mukhin, I. S.

2017-11-01

Photolithography mask made of close-packed array of micro- and nano-sized spherical lenses allows to obtain the ordered structures and provides highest “optical resolution/cost” ratio between all existing photolithography and laser direct writing methods. In this letter, we present results of modeling the propagation of a plane wave falling on the array of quartz (SiO2) microspherical lenses and focusing in the image reverse photoresist layer. We present here experimental results on fabrication of ordered arrays of submicron wells and columns and substrate preparation for growth of monocrystalline nanowires on metal surface using photolithography with mask of SiO2 microspheres. Such ordered nano-sized arrays of wells and columns can be used in fabrication of further growth of monocrystalline nanowires, quantum dots and production of plasmon structures.

Development of a sapphire fiber thermometer using two wavelength bands

NASA Astrophysics Data System (ADS)

Ye, Linhua; Shen, Yonghang

1996-09-01

This paper reports the development of a sapphire ((alpha) - Al2O3) single crystal optical fiber thermometer using two wavelength bands. A thin film of precious metal or ceramic deposited onto one end of the sapphire fiber forms a mini-radiation cavity. The other end of the sapphire fiber is coupled to a low-loss silica fiber. Radiation from the small cavity is transmitted along the silica fiber into a photodetection system which consists of a lens, beam splitter, two interference filters (820 nm and 940 nm center wavelength, 30 nm bandwidth) and two silicon photocells. The temperature measurement is based on the detection of radiation from the small cavity. The sapphire fiber (0.25 - 1.0 mm diameter, 100 - 450 mm length) was grown by the laser heated pedestal growth (LHPG) methods. Transmission loss in the sapphire fiber was experimentally measured. Theoretical analysis shows the apparent emittance of the small cavity with a length to diameter (L/D) ratio greater than eight is a constant value near to one, so the small cavity can be considered as a small black-body cavity. Using the developed sapphire fiber temperature sensor, we have built a sapphire fiber thermometer based on a 8098 single-chip microcomputer system. It was calibrated at some known stable temperature point and uses the fundamental radiation law to extrapolate to other temperatures. By taking the ratio of the optical power at two wavelengths, errors due to changes in the system, such as emissivity and transmission losses, can be canceled out. The thermometer has an operating temperature range of 800 to 1900 degrees Celsius, and an accuracy of 0.2% at 1000 degrees Celsius. There are a number of applications of the thermometer both in science and industry.

Development of an Inductively Coupled Thermometer for a Cryogenic Half-Wave Plate

NASA Astrophysics Data System (ADS)

Madurowicz, Alexander; Kusaka, Akito

2017-01-01

The current state of Cosmic Microwave Background (CMB) research has focused much attention on the measurement of polarization. In an effort to modulate the CMB polarization while also minimizing photon noise due to thermal emission, we are developing a sapphire half-wave plate (HWP) cooled to 50 K rotating at 2 Hz on a superconducting magnetic levitating bearing. In order to measure the temperature of the rotor without making physical contact, we designed an inductively coupled cryogenic thermometer. The complex impedance of the circuit has a resonant peak when driven around 1 MHz. The width of this resonance is dependent on the value of the resistor, which varies with temperature and functions as a thermometer once calibrated. In this talk, we will present results from stationary measurements of this impedance and discuss the temperature accuracy of this thermometer, as well as a preliminary circuit design to measure this impedance during the HWP rotation.

Measuring Total Column Water Vapor by Pointing an Infrared Thermometer at the Sky

NASA Technical Reports Server (NTRS)

Mims, Forrest M., III; Chambers, Lin H.; Brooks, David R.

2011-01-01

A 2-year study affirms that the temperature (Tz) indicated by an inexpensive ($20 to $60) IR thermometer pointed at the cloud-free zenith sky provides an approximate indication of the total column water vapor (precipitable water or PW). PW was measured by a MICROTOPS II sun photometer. The coefficient of correlation (r2) of the PW and Tz was 0.90, and the rms difference was 3.2 mm. A comparison of the Tz data with the PW provided by a GPS site 31 km NNE yielded an r2 of 0.79, and an rms difference of 5.8 mm. An expanded study compared Tz from eight IR thermometers with PW at various times during the day and night from 17 May to 18 October 2010, mainly at the Texas site and 10 days at Hawaii's Mauna Loa Observatory (MLO). The best results of this comparison were provided by two IR thermometers models that yielded an r2 of 0.96 and an rms difference with the PW of 2.7 mm. The results of both the ongoing 2-year study and the 5-month instrument comparison show that IR thermometers can measure PW with an accuracy (rms difference/mean PW) approaching 10%, the accuracy typically ascribed to sun photometers.

Preliminary Results of a New Type of Non-Hazardous Liquid-Filled Precision Glass Thermometer

NASA Astrophysics Data System (ADS)

Miller, Charles J.; Emory, Deanne Miller

2003-09-01

Miller & Weber, Inc. has developed several liquids that, when used properly, will perform as mercury in a liquid-in-glass thermometer. These liquids are non-hazardous per OSHA standards, non-toxic per EPA standards and biodegradable. This paper discusses the research, development and testing accomplished before bringing the finished thermometers, marketed under the brand name PerformaTherm®, to market.

High-resolution droplet-based fractionation of nano-LC separations onto microarrays for MALDI-MS analysis.

PubMed

Küster, Simon K; Pabst, Martin; Jefimovs, Konstantins; Zenobi, Renato; Dittrich, Petra S

2014-05-20

We present a robust droplet-based device, which enables the fractionation of ultralow flow rate nanoflow liquid chromatography (nano-LC) eluate streams at high frequencies and high peak resolution. This is achieved by directly interfacing the separation column to a micro T-junction, where the eluate stream is compartmentalized into picoliter droplets. This immediate compartmentalization prevents peak dispersion during eluate transport and conserves the chromatographic performance. Subsequently, nanoliter eluate fractions are collected at a rate of one fraction per second on a high-density microarray to retain the separation with high temporal resolution. Chromatographic separations of up to 45 min runtime can thus be archived on a single microarray possessing 2700 sample spots. The performance of this device is demonstrated by fractionating the separation of a tryptic digest of a known protein mixture onto the microarray chip and subsequently analyzing the sample archive using matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS). Resulting peak widths are found to be significantly reduced compared to standard continuous flow spotting technologies as well as in comparison to a conventional nano-LC-electrospray ionization-mass spectrometry interface. Moreover, we demonstrate the advantage of our high-definition nanofractionation device by applying two different MALDI matrices to all collected fractions in an alternating fashion. Since the information that is obtained from a MALDI-MS measurement depends on the choice of MALDI matrix, we can extract complementary information from neighboring spots containing almost identical composition but different matrices.

21 CFR 880.2900 - Clinical color change thermometer.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Clinical color change thermometer. 880.2900 Section 880.2900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES GENERAL HOSPITAL AND PERSONAL USE DEVICES General Hospital and Personal Use...

21 CFR 880.2900 - Clinical color change thermometer.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Clinical color change thermometer. 880.2900 Section 880.2900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES GENERAL HOSPITAL AND PERSONAL USE DEVICES General Hospital and Personal Use...

21 CFR 880.2900 - Clinical color change thermometer.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Clinical color change thermometer. 880.2900 Section 880.2900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES GENERAL HOSPITAL AND PERSONAL USE DEVICES General Hospital and Personal Use...

21 CFR 880.2900 - Clinical color change thermometer.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Clinical color change thermometer. 880.2900 Section 880.2900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES GENERAL HOSPITAL AND PERSONAL USE DEVICES General Hospital and Personal Use...

Intestinal obstruction due to migration of a thermometer from bladder to abdominal cavity: a case report.

PubMed

Nie, Jing; Zhang, Bo; Duan, Yan-Chao; Hu, Yue-Hua; Gao, Xin-Ying; Gong, Jian; Cheng, Ming; Li, Yan-Qing

2014-03-07

Intraperitoneal foreign bodies such as retained surgical instruments can cause intestinal obstruction. However, intestinal obstruction due to transmural migration of foreign bodies has rarely been reported. Here, we report a case of intestinal obstruction due to a clinical thermometer which migrated from the bladder into the abdominal cavity. A 45-year-old man was admitted to our hospital with a one-year history of recurrent lower abdominal cramps. Two days before admission, the abdominal cramps aggravated. Intestinal obstruction was confirmed with upright abdominal radiography and computerized tomography scan which showed dilation of the small intestines and a thermometer in the abdominal cavity. Then laparotomy was performed. A scar was observed at the fundus of the bladder and a thermometer was adhering to the small bowels and mesentery which resulted in intestinal obstruction. Abdominal cramps were eliminated and defecation and flatus recovered soon after removal of the thermometer.

Compact and low-cost fiber optic thermometer

NASA Astrophysics Data System (ADS)

Sun, Mei H.

1997-06-01

Commercial fiberoptic thermometers have been available for a number of years. The early products were unreliable and high in price. However, the continuing effort in the development of new sensing techniques along with the breakthroughs made in many areas of optoelectronics in recent years have made the production of cost competitive and reliable systems feasible. A fluorescence decay time based system has been demonstrated to successfully meet both cost and performance requirements for various medical applications. A very critical element to the success of this low cost and compact fiberoptic thermometer is the fluorescent sensor material. The very high quantum efficiency, the operating wavelengths, and the temperature sensitivity helped significantly in simplifying the design requirements for the optics and the electronics. The one to eight channel unit contains one to eight modules of a simple optical assembly: an LED light source, a small lens, and a filter are housed in an injection molded plastic container. Both the electronics and the optics reside on a small printed circuit board of approximately 6 inches by 3 inches. This system can be packaged as a stand alone unit or embedded in original manufacturer equipment.

Elemental Identification by Combining Atomic Force Microscopy and Kelvin Probe Force Microscopy.

PubMed

Schulz, Fabian; Ritala, Juha; Krejčí, Ondrej; Seitsonen, Ari Paavo; Foster, Adam S; Liljeroth, Peter

2018-06-01

There are currently no experimental techniques that combine atomic-resolution imaging with elemental sensitivity and chemical fingerprinting on single molecules. The advent of using molecular-modified tips in noncontact atomic force microscopy (nc-AFM) has made it possible to image (planar) molecules with atomic resolution. However, the mechanisms responsible for elemental contrast with passivated tips are not fully understood. Here, we investigate elemental contrast by carrying out both nc-AFM and Kelvin probe force microscopy (KPFM) experiments on epitaxial monolayer hexagonal boron nitride (hBN) on Ir(111). The hBN overlayer is inert, and the in-plane bonds connecting nearest-neighbor boron and nitrogen atoms possess strong covalent character and a bond length of only ∼1.45 Å. Nevertheless, constant-height maps of both the frequency shift Δ f and the local contact potential difference exhibit striking sublattice asymmetry. We match the different atomic sites with the observed contrast by comparison with nc-AFM image simulations based on the density functional theory optimized hBN/Ir(111) geometry, which yields detailed information on the origin of the atomic-scale contrast.

Kelvin-Helmholtz versus Hall magnetoshear instability in astrophysical flows.

PubMed

Gómez, Daniel O; Bejarano, Cecilia; Mininni, Pablo D

2014-05-01

We study the stability of shear flows in a fully ionized plasma. Kelvin-Helmholtz is a well-known macroscopic and ideal shear-driven instability. In sufficiently low-density plasmas, also the microscopic Hall magnetoshear instability can take place. We performed three-dimensional simulations of the Hall-magnetohydrodynamic equations where these two instabilities are present, and carried out a comparative study. We find that when the shear flow is so intense that its vorticity surpasses the ion-cyclotron frequency of the plasma, the Hall magnetoshear instability is not only non-negligible, but it actually displays growth rates larger than those of the Kelvin-Helmholtz instability.

Kelvin-Helmholtz instability in a single-component atomic superfluid

NASA Astrophysics Data System (ADS)

Baggaley, A. W.; Parker, N. G.

2018-05-01

We demonstrate an experimentally feasible method for generating the classical Kelvin-Helmholtz instability in a single-component atomic Bose-Einstein condensate. By progressively reducing a potential barrier between two counterflowing channels, we seed a line of quantized vortices, which precede to form progressively larger clusters, mimicking the classical roll-up behavior of the Kelvin-Helmholtz instability. This cluster formation leads to an effective superfluid shear layer, formed through the collective motion of many quantized vortices. From this we demonstrate a straightforward method to measure the effective viscosity of a turbulent quantum fluid in a system with a moderate number of vortices, within the range of current experimental capabilities.

Erratum: SDO-AIA Observation of Kelvin-helmholtz Instability in the Solar Corona

NASA Technical Reports Server (NTRS)

Ofman, Leon; Thompson, Barbara J.

2012-01-01

The first SDOAIA observation of the KelvinHelmholtz instability in the solar corona in the 2010 April 8 event was reported by Ofman Thompson (2010, 2011). Foullon et al. (2011), which was published prior to Ofman Thompson (2011), claimed the detection of the KelvinHelmholtz instability in a later event (2010 November 3), and should have been cited in Ofman Thompson (2011).

APMP Scale Comparison with Three Radiation Thermometers and Six Fixed-Point Blackbodies

NASA Astrophysics Data System (ADS)

Yamada, Y.; Shimizu, Y.; Ishii, J.

2015-08-01

New Asia Pacific Metrology Programme (APMP) comparisons of radiation thermometry standards, APMP TS-11, and -12, have recently been initiated. These new APMP comparisons cover the temperature range from to . Three radiation thermometers with central wavelengths of 1.6 , 0.9 , and 0.65 are the transfer devices for the radiation thermometer scale comparison conducted in the so-called star configuration. In parallel, a compact fixed-point blackbody furnace that houses six types of fixed-point cells of In, Sn, Zn, Al, Ag, and Cu is circulated, again in a star-type comparison, to substantiate fixed-point calibration capabilities. Twelve APMP national metrology institutes are taking part in this endeavor, in which the National Metrology Institute of Japan acts as the pilot. In this article, the comparison scheme is described with emphasis on the features of the transfer devices, i.e., the radiation thermometers and the fixed-point blackbodies. Results of preliminary evaluations of the performance and characteristic of these instruments as well as the evaluation method of the comparison results are presented.

Exact solution for the energy spectrum of Kelvin-wave turbulence in superfluids

NASA Astrophysics Data System (ADS)

Boué, Laurent; Dasgupta, Ratul; Laurie, Jason; L'Vov, Victor; Nazarenko, Sergey; Procaccia, Itamar

2011-08-01

We study the statistical and dynamical behavior of turbulent Kelvin waves propagating on quantized vortices in superfluids and address the controversy concerning the energy spectrum that is associated with these excitations. Finding the correct energy spectrum is important because Kelvin waves play a major role in the dissipation of energy in superfluid turbulence at near-zero temperatures. In this paper, we show analytically that the solution proposed by [L’vov and Nazarenko, JETP Lett.JTPLA20021-364010.1134/S002136401008014X 91, 428 (2010)] enjoys existence, uniqueness, and regularity of the prefactor. Furthermore, we present numerical results of the dynamical equation that describes to leading order the nonlocal regime of the Kelvin-wave dynamics. We compare our findings with the analytical results from the proposed local and nonlocal theories for Kelvin-wave dynamics and show an agreement with the nonlocal predictions. Accordingly, the spectrum proposed by L’vov and Nazarenko should be used in future theories of quantum turbulence. Finally, for weaker wave forcing we observe an intermittent behavior of the wave spectrum with a fluctuating dissipative scale, which we interpreted as a finite-size effect characteristic of mesoscopic wave turbulence.

Nano-thermometers with thermo-sensitive polymer grafted USPIOs behaving as positive contrast agents in low-field MRI

NASA Astrophysics Data System (ADS)

Hannecart, Adeline; Stanicki, Dimitri; Vander Elst, Luce; Muller, Robert N.; Lecommandoux, Sébastien; Thévenot, Julie; Bonduelle, Colin; Trotier, Aurélien; Massot, Philippe; Miraux, Sylvain; Sandre, Olivier; Laurent, Sophie

2015-02-01

, also working as ``nano-thermometers''.Two commercial statistical copolymers of ethylene oxide and propylene oxide, Jeffamine® M-2005 (PEO5-st-PPO37) and M-2070 (PEO46-st-PPO13), exhibiting lower critical solution temperature (LCST) in water, were grafted onto the surface of ultra-small superparamagnetic iron oxide nanoparticles (USPIOs) using silanization and amide-bond coupling reactions. The LCSTs of the polymers in solution were measured by dynamic light scattering (DLS) and nuclear magnetic resonance (NMR). In accordance with the compositions of EO vs. PO, the transition temperature was measured to be 22 +/- 2 °C for M-2005 by both DLS and NMR, while the LCST was much higher, 52 +/- 2 °C, for M-2070 (a second transition was also detected above 80 °C by NMR in that case, ascribed to the full dehydration of chains at the molecular level). The resulting polymer-grafted USPIOs exhibit a temperature-responsive colloidal behaviour, their surface reversibly changing from hydrophilic below LCST to hydrophobic above it. This phenomenon was utilised to design thermo-sensitive contrast agents for MRI. Transverse relaxivities (r2) of the USPIO@PEO5-st-PPO37 core-shell nanoparticles were measured at 8.25, 20, 60, and 300 MHz. Nuclear magnetic resonance dispersion (NMRD) profiles, giving longitudinal relaxivities (r1) between 0.01 and 60 MHz, were acquired at temperatures ranging from 15 to 50 °C. For all tested frequencies except 300 MHz, both r1 and r2 decrease with temperature and show an inflection point at 25 °C, near the LCST. To illustrate the interest of such polymer-coated USPIOs for MRI thermometry, sample tubes were imaged on both low-field (8.25 MHz/0.194 Tesla) and high-field (300 MHz/7.05 Tesla) MRI scanners with either T1- or T2*-weighted spin echo sequences. The positive contrast on low-field MR images and the perfect linearity of the signal with a T2*-weighted sequence over the entire temperature range 15-50 °C render these LCST polymer coated USPIOs

Evaluation of Small-Sized Platinum Resistance Thermometers with ITS-90 Characteristics

NASA Astrophysics Data System (ADS)

Yamazawa, K.; Anso, K.; Widiatmo, J. V.; Tamba, J.; Arai, M.

2011-12-01

Many platinum resistance thermometers (PRTs) are applied for high precision temperature measurements in industry. Most of the applications use PRTs that follow the industrial standard of PRTs, IEC 60751. However, recently, some applications, such as measurements of the temperature distribution within equipments, require a more precise temperature scale at the 0.01 °C level. In this article the evaluation of remarkably small-sized PRTs that have temperature-resistance characteristics very close to that of standard PRTs of the International Temperature Scale of 1990 (ITS-90) is reported. Two types of the sensing element were tested, one is 1.2 mm in diameter and 10 mm long, the other is 0.8 mm and 8 mm. The resistance of the sensor is 100 Ω at the triple-point-of-water temperature. The resistance ratio at the Ga melting-point temperature of the sensing elements exceeds 1.11807. To verify the closeness of the temperature-resistance characteristics, comparison measurements up to 157 °C were employed. A pressure-controlled water heat-pipe furnace was used for the comparison measurement. Characteristics of 19 thermometers with these small-sized sensing elements were evaluated. The deviation from the temperature measured using a standard PRT used as a reference thermometer in the comparison was remarkably small, when we apply the same interpolating function for the ITS-90 sub-range to these small thermometers. Results including the stability of the PRTs and the uncertainty evaluation of the comparison measurements, and the comparison results showing the small deviation from the ITS-90 temperature-resistance characteristics are reported. The development of such a PRT might be a good solution for applications such as temperature measurements of small objects or temperature distribution measurements that need the ITS-90 temperature scale.

Cavitation and bubble dynamics: the Kelvin impulse and its applications

PubMed Central

Blake, John R.; Leppinen, David M.; Wang, Qianxi

2015-01-01

Cavitation and bubble dynamics have a wide range of practical applications in a range of disciplines, including hydraulic, mechanical and naval engineering, oil exploration, clinical medicine and sonochemistry. However, this paper focuses on how a fundamental concept, the Kelvin impulse, can provide practical insights into engineering and industrial design problems. The pathway is provided through physical insight, idealized experiments and enhancing the accuracy and interpretation of the computation. In 1966, Benjamin and Ellis made a number of important statements relating to the use of the Kelvin impulse in cavitation and bubble dynamics, one of these being ‘One should always reason in terms of the Kelvin impulse, not in terms of the fluid momentum…’. We revisit part of this paper, developing the Kelvin impulse from first principles, using it, not only as a check on advanced computations (for which it was first used!), but also to provide greater physical insights into cavitation bubble dynamics near boundaries (rigid, potential free surface, two-fluid interface, flexible surface and axisymmetric stagnation point flow) and to provide predictions on different types of bubble collapse behaviour, later compared against experiments. The paper concludes with two recent studies involving (i) the direction of the jet formation in a cavitation bubble close to a rigid boundary in the presence of high-intensity ultrasound propagated parallel to the surface and (ii) the study of a ‘paradigm bubble model’ for the collapse of a translating spherical bubble, sometimes leading to a constant velocity high-speed jet, known as the Longuet-Higgins jet. PMID:26442141

Investigation of Kelvin wave periods during Hai-Tang typhoon using Empirical Mode Decomposition

NASA Astrophysics Data System (ADS)

Kishore, P.; Jayalakshmi, J.; Lin, Pay-Liam; Velicogna, Isabella; Sutterley, Tyler C.; Ciracì, Enrico; Mohajerani, Yara; Kumar, S. Balaji

2017-11-01

Equatorial Kelvin waves (KWs) are fundamental components of the tropical climate system. In this study, we investigate Kelvin waves (KWs) during the Hai-Tang typhoon of 2005 using Empirical Mode Decomposition (EMD) of regional precipitation, zonal and meridional winds. For the analysis, we use daily precipitation datasets from the Global Precipitation Climatology Project (GPCP) and wind datasets from the European Centre for Medium-Range Weather Forecasts (ECMWF) Interim Re-analysis (ERA-Interim). As an additional measurement, we use in-situ precipitation datasets from rain-gauges over the Taiwan region. The maximum accumulated precipitation was approximately 2400 mm during the period July 17-21, 2005 over the southwestern region of Taiwan. The spectral analysis using the wind speed at 950 hPa found in the 2nd, 3rd, and 4th intrinsic mode functions (IMFs) reveals prevailing Kelvin wave periods of ∼3 days, ∼4-6 days, and ∼6-10 days, respectively. From our analysis of precipitation datasets, we found the Kelvin waves oscillated with periods between ∼8 and 20 days.

Topographic coupling of surface and internal Kelvin waves. [of ocean

NASA Technical Reports Server (NTRS)

Chao, S.-Y.

1980-01-01

An analysis is presented for computing the diffraction of barotropic Kelvin waves by a localized topographical irregularity on flat-bottom ocean with an arbitrary vertical stratification. It was shown that all baroclinic Kelvin waves will be generated downstream of the bump, with the first baroclinic mode having the largest amplitude. The Poincare waves predominate in the lowest modes, and are more directionally anisotropic. It was concluded that baroclinic Poincare waves radiating offshore from the bump topography could contribute to the internal wave field in the open ocean and provide an alternative mechanism to dissipate the barotropic tides.

Optimization of the R-SQUID noise thermometer

NASA Astrophysics Data System (ADS)

Seppä, Heikki

1986-02-01

The Josephson junction can be used to convert voltage into frequency and thus it can be used to convert voltage fluctuations generated by Johnson noise in a resistor into frequency fluctuations. As a consequence, the temperature of the resistor can be defined by measuring the variance of the frequency fluctuations. Unfortunately, the absolute determination of temperature by this approach is disturbed by several undesirable effects: a rolloff introduced by the bandwidth of the postdetection filter, additional noise caused by rf amplifiers, and a mixed noise effect caused by the nonlinearity of the Josephson junction together with rf noise in the tank circuit. Furthermore, the variance is a statistical quantity and therefore the limited number of frequency counts produces inaccuracy in a temperature measurement. In this work the total inaccuracy of the noise thermometer is analyzed and the optimal choice of the parameters is derived. A practical way to find the optimal conditions for the Josephson junction noise thermometer is discussed. The inspection shows that under the optimal conditions the total error is dependent only on the temperature under determination, the equivalent noise temperature of the preamplifier, the bias frequency of the SQUID, and the total time used for the measurement.

The Kelvin water-drop experiment

NASA Technical Reports Server (NTRS)

Shull, Robert D.

1990-01-01

This experiment was originally designed and performed by Lord Kelvin (William Thomson) in the late 1800's to demonstrate the creation of an electric potential simply by means of dividing up a body of flowing water. The objective is to demonstrate the power of electrical forces in a material as common as water and to help teach the student that even simple, well understood phenomena sometimes present unexpected results that, at first thought, defeat explanation. The experimental equipment and procedure are explained.

Electronic Thermometer Readings

NASA Technical Reports Server (NTRS)

2001-01-01

NASA Stennis' adaptive predictive algorithm for electronic thermometers uses sample readings during the initial rise in temperature and applies an algorithm that accurately and rapidly predicts the steady state temperature. The final steady state temperature of an object can be calculated based on the second-order logarithm of the temperature signals acquired by the sensor and predetermined variables from the sensor characteristics. These variables are calculated during tests of the sensor. Once the variables are determined, relatively little data acquisition and data processing time by the algorithm is required to provide a near-accurate approximation of the final temperature. This reduces the delay in the steady state response time of a temperature sensor. This advanced algorithm can be implemented in existing software or hardware with an erasable programmable read-only memory (EPROM). The capability for easy integration eliminates the expense of developing a whole new system that offers the benefits provided by NASA Stennis' technology.

Structure and mechanism of a molecular rheostat, an RNA thermometer that modulates immune evasion by Neisseria meningitidis

PubMed Central

Barnwal, Ravi Pratap; Loh, Edmund; Godin, Katherine S.; Yip, Jordan; Lavender, Hayley; Tang, Christoph M.; Varani, Gabriele

2016-01-01

Neisseria meningitidis causes bacterial meningitis and septicemia. It evades the host complement system by upregulating expression of immune evasion factors in response to changes in temperature. RNA thermometers within mRNAs control expression of bacterial immune evasion factors, including CssA, in the 5′-untranslated region of the operon for capsule biosynthesis. We dissect the molecular mechanisms of thermoregulation and report the structure of the CssA thermometer. We show that the RNA thermometer acts as a rheostat, whose stability is optimized to respond in a small temperature range around 37°C as occur within the upper airways during infection. Small increases in temperature gradually open up the structure to allow progressively increased access to the ribosome binding site. Even small changes in stability induced by mutations of imperfect base pairs, as in naturally occurring polymorphisms, shift the thermometer response outside of the desired temperature range, suggesting that its activity could be modulated by pharmacological intervention. PMID:27369378

Resistance thermometer has linear resistance-temperature coefficient at low temperatures

NASA Technical Reports Server (NTRS)

Kuzyk, W.

1966-01-01

Resistance thermometer incorporating a germanium resistance element with a platinum resistance element in a wheatstone bridge circuit has a linear temperature-resistance coefficient over a range from approximately minus 140 deg C to approximately minus 253 deg C.

Electrical and Infrared Optical Properties of Vanadium Oxide Semiconducting Thin-Film Thermometers

NASA Astrophysics Data System (ADS)

Zia, Muhammad Fakhar; Abdel-Rahman, Mohamed; Alduraibi, Mohammad; Ilahi, Bouraoui; Awad, Ehab; Majzoub, Sohaib

2017-10-01

A synthesis method has been developed for preparation of vanadium oxide thermometer thin film for microbolometer application. The structure presented is a 95-nm thin film prepared by sputter-depositing nine alternating multilayer thin films of vanadium pentoxide (V2O5) with thickness of 15 nm and vanadium with thickness of 5 nm followed by postdeposition annealing at 300°C in nitrogen (N2) and oxygen (O2) atmospheres. The resulting vanadium oxide (V x O y ) thermometer thin films exhibited temperature coefficient of resistance (TCR) of -3.55%/°C with room-temperature resistivity of 2.68 Ω cm for structures annealed in N2 atmosphere, and TCR of -3.06%/°C with room-temperature resistivity of 0.84 Ω cm for structures annealed in O2 atmosphere. Furthermore, optical measurements of N2- and O2-annealed samples were performed by Fourier-transform infrared ellipsometry to determine their dispersion curves, refractive index ( n), and extinction coefficient ( k) at wavelength from 7000 nm to 14,000 nm. The results indicate the possibility of applying the developed materials in thermometers for microbolometers.

Active control of nano dimers response using piezoelectric effect

NASA Astrophysics Data System (ADS)

Mekkawy, Ahmed A.; Ali, Tamer A.; Badawi, Ashraf H.

2016-09-01

Nano devices can be used as building blocks for Internet of Nano-Things network devices, such as sensors/actuators, transceivers, and routers. Although nano particles response can be engineered to fit in different regimes, for such a nano particle to be used as an active nano device, its properties should be dynamically controlled. This controllability is a challenge, and there are many proposed techniques to tune nanoparticle response on the spot through a sort of control signal, wither that signal is optical (for all-optical systems) or electronic (for opto-electronic systems). This will allow the use of nano particles as nano-switches or as dynamic sensors that can pick different frequencies depending on surrounding conditions or depending on a smart decisions. In this work, we propose a piezoelectric substrate as an active control mediator to control plasmonic gaps in nano dimers. This method allows for integrating nano devices with regular electronics while communicating control signals to nano devices through applying electric signals to a piezoelectric material, in order to control the gaps between nano particles in a nano cluster. We do a full numerical study to the system, analyzing the piezoelectric control resolution (minimum gap change step) and its effect on a nanodimer response as a nanoantenna. This analysis considers the dielectric functions of materials within the visible frequencies range. The effects of different parameters, such as the piezoelectric geometrical structure and materials, on the gap control resolution and the operating frequency are studied.

Boron dipyrromethene (BODIPY) functionalized carbon nano-onions for high resolution cellular imaging

NASA Astrophysics Data System (ADS)

Bartelmess, Juergen; de Luca, Elisa; Signorelli, Angelo; Baldrighi, Michele; Becce, Michele; Brescia, Rosaria; Nardone, Valentina; Parisini, Emilio; Echegoyen, Luis; Pompa, Pier Paolo; Giordani, Silvia

2014-10-01

Carbon nano-onions (CNOs) are an exciting class of carbon nanomaterials, which have recently demonstrated a facile cell-penetration capability. In the present work, highly fluorescent boron dipyrromethene (BODIPY) dyes were covalently attached to the surface of CNOs. The introduction of this new carbon nanomaterial-based imaging platform, made of CNOs and BODIPY fluorophores, allows for the exploration of synergetic effects between the two building blocks and for the elucidation of its performance in biological applications. The high fluorescence intensity exhibited by the functionalized CNOs translates into an excellent in vitro probe for the high resolution imaging of MCF-7 human breast cancer cells. It was also found that the CNOs, internalized by the cells by endocytosis, localized in the lysosomes and did not show any cytotoxic effects. The presented results highlight CNOs as excellent platforms for biological and biomedical studies due to their low toxicity, efficient cellular uptake and low fluorescence quenching of attached probes.Carbon nano-onions (CNOs) are an exciting class of carbon nanomaterials, which have recently demonstrated a facile cell-penetration capability. In the present work, highly fluorescent boron dipyrromethene (BODIPY) dyes were covalently attached to the surface of CNOs. The introduction of this new carbon nanomaterial-based imaging platform, made of CNOs and BODIPY fluorophores, allows for the exploration of synergetic effects between the two building blocks and for the elucidation of its performance in biological applications. The high fluorescence intensity exhibited by the functionalized CNOs translates into an excellent in vitro probe for the high resolution imaging of MCF-7 human breast cancer cells. It was also found that the CNOs, internalized by the cells by endocytosis, localized in the lysosomes and did not show any cytotoxic effects. The presented results highlight CNOs as excellent platforms for biological and biomedical

Facile Preparation of a Platinum Silicide Nanoparticle-Modified Tip Apex for Scanning Kelvin Probe Microscopy.

PubMed

Lin, Chun-Ting; Chen, Yu-Wei; Su, James; Wu, Chien-Ting; Hsiao, Chien-Nan; Shiao, Ming-Hua; Chang, Mao-Nan

2015-12-01

In this study, we propose an ultra-facile approach to prepare a platinum silicide nanoparticle-modified tip apex (PSM tip) used for scanning Kelvin probe microscopy (SKPM). We combined a localized fluoride-assisted galvanic replacement reaction (LFAGRR) and atmospheric microwave annealing (AMA) to deposit a single platinum silicide nanoparticle with a diameter of 32 nm on the apex of a bare silicon tip of atomic force microscopy (AFM). The total process was completed in an ambient environment in less than 3 min. The improved potential resolution in the SKPM measurement was verified. Moreover, the resolution of the topography is comparable to that of a bare silicon tip. In addition, the negative charges found on the PSM tips suggest the possibility of exploring the use of current PSM tips to sense electric fields more precisely. The ultra-fast and cost-effective preparation of the PSM tips provides a new direction for the preparation of functional tips for scanning probe microscopy.

Ratiometric near infrared luminescent thermometer based on lanthanide metal-organic frameworks

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yue, Dan; Zhang, Jun; Zhao, Dian

2016-09-15

A near infrared luminescent MOFs thermometer (Nd{sub 0.676}Yb{sub 0.324}BTC) was prepared via a simple solvothermal method using Ln{sup 3+} (Ln=Nd, Yb) ions and 1, 3, 5-benznenetricarboxylic acid (H{sub 3}BTC), and characterized by PXRD, TGA, ICP, and photoluminescence (PL) spectrum. These results indicate that the Nd{sub 0.676}Yb{sub 0.324}BTC displays high relative sensitivity and excellent repeatability in the physiological temperature range (288–323 K), and the maximum relative sensitivity is determined to be 1.187% K{sup −1} at 323 K. These NIR luminescent MOFs may have potential applications in physiological temperature sensing. - Graphical abstract: A near infrared luminescent MOFs thermometer (Nd{sub 0.054}Yb{sub 0.946}BTCmore » ) displays high relative sensitivity and excellent repeatability in the physiological temperature range (288–323 K). Display Omitted - Highlights: • A ratiometric near infrared luminescent MOFs thermometer (Nd{sub 0.676}Yb{sub 0.324}BTC) was prepared via a simple solvothermal method. • The maximum relative sensitivity of Nd{sub 0.676}Yb{sub 0.324}BTC is determined to be 1.187% K{sup −1} at 323 K. • Nd{sub 0.676}Yb{sub 0.324}BTC showed excellent repeatability in the physiological temperature range (288–323 K).« less

27 CFR 30.22 - Hydrometers and thermometers.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 105 to 125 0.2° N 125 to 145 0.2° P 145 to 165 0.2° Q 165 to 185 0.2° R 185 to 206 0.2° Thermometers are designated by type according to range of degrees Fahrenheit and are provided in ranges and subdivisions of degrees as follows: Type Range Subdivision Pencil type 10° to 100° 1° V-back 10° to 100° 1...

Noise performance of frequency modulation Kelvin force microscopy

PubMed Central

Deresmes, Dominique; Mélin, Thierry

2014-01-01

Summary Noise performance of a phase-locked loop (PLL) based frequency modulation Kelvin force microscope (FM-KFM) is assessed. Noise propagation is modeled step by step throughout the setup using both exact closed loop noise gains and an approximation known as “noise gain” from operational amplifier (OpAmp) design that offers the advantage of decoupling the noise performance study from considerations of stability and ideal loop response. The bandwidth can be chosen depending on how much noise is acceptable and it is shown that stability is not an issue up to a limit that will be discussed. With thermal and detector noise as the only sources, both approaches yield PLL frequency noise expressions equal to the theoretical value for self-oscillating circuits and in agreement with measurement, demonstrating that the PLL components neither modify nor contribute noise. Kelvin output noise is then investigated by modeling the surrounding bias feedback loop. A design rule is proposed that allows choosing the AC modulation frequency for optimized sharing of the PLL bandwidth between Kelvin and topography loops. A crossover criterion determines as a function of bandwidth, temperature and probe parameters whether thermal or detector noise is the dominating noise source. Probe merit factors for both cases are then established, suggesting how to tackle noise performance by probe design. Typical merit factors of common probe types are compared. This comprehensive study is an encouraging step toward a more integral performance assessment and a remedy against focusing on single aspects and optimizing around randomly chosen key values. PMID:24455457

Conventional superconductivity at 203 kelvin at high pressures in the sulfur hydride system.

PubMed

Drozdov, A P; Eremets, M I; Troyan, I A; Ksenofontov, V; Shylin, S I

2015-09-03

A superconductor is a material that can conduct electricity without resistance below a superconducting transition temperature, Tc. The highest Tc that has been achieved to date is in the copper oxide system: 133 kelvin at ambient pressure and 164 kelvin at high pressures. As the nature of superconductivity in these materials is still not fully understood (they are not conventional superconductors), the prospects for achieving still higher transition temperatures by this route are not clear. In contrast, the Bardeen-Cooper-Schrieffer theory of conventional superconductivity gives a guide for achieving high Tc with no theoretical upper bound--all that is needed is a favourable combination of high-frequency phonons, strong electron-phonon coupling, and a high density of states. These conditions can in principle be fulfilled for metallic hydrogen and covalent compounds dominated by hydrogen, as hydrogen atoms provide the necessary high-frequency phonon modes as well as the strong electron-phonon coupling. Numerous calculations support this idea and have predicted transition temperatures in the range 50-235 kelvin for many hydrides, but only a moderate Tc of 17 kelvin has been observed experimentally. Here we investigate sulfur hydride, where a Tc of 80 kelvin has been predicted. We find that this system transforms to a metal at a pressure of approximately 90 gigapascals. On cooling, we see signatures of superconductivity: a sharp drop of the resistivity to zero and a decrease of the transition temperature with magnetic field, with magnetic susceptibility measurements confirming a Tc of 203 kelvin. Moreover, a pronounced isotope shift of Tc in sulfur deuteride is suggestive of an electron-phonon mechanism of superconductivity that is consistent with the Bardeen-Cooper-Schrieffer scenario. We argue that the phase responsible for high-Tc superconductivity in this system is likely to be H3S, formed from H2S by decomposition under pressure. These findings raise hope for the

Influence of QBO on stratospheric Kelvin and Mixed Rossby gravity waves in high-top CMIP5 models

NASA Astrophysics Data System (ADS)

Indah Solihah, Karina; Lubis, Sandro W.; Setiawan, Sonni

2018-05-01

It is well established that quasi-biennial oscillation (QBO) has a substantial influence on Kelvin and mixed Rossby gravity (MRG) wave activity in the tropical lower stratosphere. In this study, we examined how QBO influences Kelvin and MRG wave activity in the lower stratosphere, based on nine high-top CMIP5 models. The results show that the Kelvin and MRG wave signals are stronger in the models with QBO, and relatively weaker in the models without QBO. The results are consistent with established theory, whereby upward-propagating Kelvin waves occurs more frequently during the easterly QBO phase, while upward-propagating MRG waves occurs during the westerly QBO phase. Without the QBO, the mean flow exhibits a near-zero easterly wind, which prevents the waves from propagating and penetrating into the stratosphere. Our analysis also shows that models with the QBO tend to have more robust signatures (in terms of amplitude and phase speed) of Kelvin and MRG waves.

Ingestible Thermometer Pill Aids Athletes in Beating the Heat

NASA Technical Reports Server (NTRS)

2006-01-01

Developed by Goddard Space Flight Center and the Johns Hopkins University Applied Physics Laboratory to monitor the core body temperature of astronauts during space flight, the ingestible "thermometer pill" has a silicone-coated exterior, with a microbattery, a quartz crystal temperature sensor, a space-aged telemetry system, and microminiaturized circuitry on the interior.

Corrections on the Thermometer Reading in an Air Stream

NASA Technical Reports Server (NTRS)

Van Der Maas, H J; Wynia, S

1940-01-01

A method is described for checking a correction formula, based partly on theoretical considerations, for adiabatic compression and friction in flight tests and determining the value of the constant. It is necessary to apply a threefold correction to each thermometer reading. They are a correction for adiabatic compression, friction and for time lag.

An electron beam linear scanning mode for industrial limited-angle nano-computed tomography.

PubMed

Wang, Chengxiang; Zeng, Li; Yu, Wei; Zhang, Lingli; Guo, Yumeng; Gong, Changcheng

2018-01-01

Nano-computed tomography (nano-CT), which utilizes X-rays to research the inner structure of some small objects and has been widely utilized in biomedical research, electronic technology, geology, material sciences, etc., is a high spatial resolution and non-destructive research technique. A traditional nano-CT scanning model with a very high mechanical precision and stability of object manipulator, which is difficult to reach when the scanned object is continuously rotated, is required for high resolution imaging. To reduce the scanning time and attain a stable and high resolution imaging in industrial non-destructive testing, we study an electron beam linear scanning mode of nano-CT system that can avoid mechanical vibration and object movement caused by the continuously rotated object. Furthermore, to further save the scanning time and study how small the scanning range could be considered with acceptable spatial resolution, an alternating iterative algorithm based on ℓ 0 minimization is utilized to limited-angle nano-CT reconstruction problem with the electron beam linear scanning mode. The experimental results confirm the feasibility of the electron beam linear scanning mode of nano-CT system.

An electron beam linear scanning mode for industrial limited-angle nano-computed tomography

NASA Astrophysics Data System (ADS)

Wang, Chengxiang; Zeng, Li; Yu, Wei; Zhang, Lingli; Guo, Yumeng; Gong, Changcheng

2018-01-01

Nano-computed tomography (nano-CT), which utilizes X-rays to research the inner structure of some small objects and has been widely utilized in biomedical research, electronic technology, geology, material sciences, etc., is a high spatial resolution and non-destructive research technique. A traditional nano-CT scanning model with a very high mechanical precision and stability of object manipulator, which is difficult to reach when the scanned object is continuously rotated, is required for high resolution imaging. To reduce the scanning time and attain a stable and high resolution imaging in industrial non-destructive testing, we study an electron beam linear scanning mode of nano-CT system that can avoid mechanical vibration and object movement caused by the continuously rotated object. Furthermore, to further save the scanning time and study how small the scanning range could be considered with acceptable spatial resolution, an alternating iterative algorithm based on ℓ0 minimization is utilized to limited-angle nano-CT reconstruction problem with the electron beam linear scanning mode. The experimental results confirm the feasibility of the electron beam linear scanning mode of nano-CT system.

The gallium melting-point standard: its role in manufacture and quality control of electronic thermometers for the clinical laboratory.

PubMed

Sostman, H E

1977-01-01

I discuss the traceability of calibration of electronic thermometers to thermometric constants of nature or to the National Bureau of Standards, form a manufacturer's basic standards through the manufacturing process to the user's laboratory. Useful electrical temperature sensors, their advantages, and means for resolving their disadvantages are described. I summarize our development of a cell for realizing the melting phase equilibrium of pure gallium (at 29.770 degrees C) as a thermometer calibration fixed point, and enumerate its advantages in the routine calibration verification of electrical thermometers in the clinical chemistry laboratory.

Time-lapse and slow-motion tracking of temperature changes: response time of a thermometer

NASA Astrophysics Data System (ADS)

Moggio, L.; Onorato, P.; Gratton, L. M.; Oss, S.

2017-03-01

We propose the use of a smartphone based time-lapse and slow-motion video techniques together with tracking analysis as valuable tools for investigating thermal processes such as the response time of a thermometer. The two simple experimental activities presented here, suitable also for high school and undergraduate students, allow one to measure in a simple yet rigorous way the response time of an alcohol thermometer and show its critical dependence on the properties of the surrounding environment giving insight into instrument characteristics, heat transfer and thermal equilibrium concepts.

Operational methods of thermodynamics. Volume 1 - Temperature measurement

NASA Astrophysics Data System (ADS)

Eder, F. X.

The principles of thermometry are examined, taking into account the concept of temperature, the Kelvin scale, the statistical theory of heat, negative absolute temperatures, the thermodynamic temperature scale, the thermodynamic temperature scale below 1 K, noise thermometry, temperature scales based on black-body radiation, acoustical thermometry, and the International Practical Temperature Scale 1968. Aspects of practical temperature measurement are discussed, giving attention to thermometers based on the expansion of a gas or a liquid, instruments utilizing the relative thermal expansion of two different metals, devices measuring the vapor pressure of a liquid, thermocouples, resistance thermometers, radiation pyrometers of various types, instruments utilizing the temperature dependence of a number of material characteristics, devices for temperature control, thermometer calibration, and aspects of thermometer installation and inertia. A description is presented of the approaches employed for the measurement of low temperatures.

Characteristics of a liquid-helium-free calibration apparatus for cryogenic thermometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shimazaki, T.

2013-09-11

Closed-cycle Joule-Thomson (JT) cryocoolers have been developed at National Metrology Institute of Japan (NMIJ)/National Institute of Advanced Industrial Science and Technology (AIST) with the aim of realizing a liquid-helium-free calibration apparatus for cryogenic thermometers between 0.65 K and 25 K. The latest JT cryocooler at NMIJ/AIST consists of a {sup 3}He JT cooling circuit and a pulse tube mechanical refrigerator. The characteristics of the apparatus including a residual gas analysis of the JT cooling circuit are presented in this paper. Currently the initial cool-down is performed using a heat-exchange gas. It normally takes about 30 h to reduce the temperaturemore » from room temperature to 5 K at the thermometer comparison block of the apparatus. The correct timing of the removal of the heatexchange gas is important for the efficient operation of the apparatus. Incomplete removal of the heat-exchange gas induces excess heat load on the apparatus and thermal disturbances. Some examples of abrupt temperature bursts are discussed in this paper. Mechanical refrigerators generate cyclic mechanical vibrations, and precision resistance thermometers are usually very sensitive to a mechanical vibration. The measured vibration level of the developed apparatus is reported. The damage to the apparatus due to the magnitude 9.0 earthquake on March 11, 2011, and possible countermeasures in the case of future earthquakes are also discussed.« less

The structure of [MnIII6 CrIII]3+ single-molecule magnets deposited in submono-layers and monolayers on surfaces studied by means of molecular resolved atomic force microscopy (AFM) and Kelvin Probe Force Microscopy in UHV

NASA Astrophysics Data System (ADS)

Heinzmann, U.; Gryzia, A.; Volkmann, T.; Brechling, A.; Hoeke, V.; Glaser, T.

2014-04-01

Single molecule magnets (SMM) deposited in submonolayers and monolayers have been analyzed with respect to their structures by means of non-contact AFM (topographic as well as damping mode) and Kelvin Probe Force Microscopy with molecular resolution.

Evaluation of a Teaching Kit for Family and Consumer Science Classrooms: Motivating Students to Use a Food Thermometer with Small Cuts of Meat

ERIC Educational Resources Information Center

Edwards, Zena; Edlefsen, Miriam; Hillers, Virginia; McCurdy, Sandra M.

2005-01-01

The U.S. Dept. of Agriculture recommends use of food thermometers to safely cook small cuts of meat, yet most consumers do not use them. Consumers lack knowledge about how and why to use food thermometers with small cuts of meat. Opportunities exist for family and consumer science classes to provide education about thermometers to adolescents, who…

Observations of Convectively Coupled Kelvin Waves forced by Extratropical Wave Activity

NASA Astrophysics Data System (ADS)

Kiladis, G. N.; Biello, J. A.; Straub, K. H.

2012-12-01

It is well established by observations that deep tropical convection can in certain situations be forced by extratropical Rossby wave activity. Such interactions are a well-known feature of regions of upper level westerly flow, and in particular where westerlies and equatorward wave guiding by the basic state occur at low enough latitudes to interact with tropical and subtropical moisture sources. In these regions convection is commonly initiated ahead of upper level troughs, characteristic of forcing by quasi-geostrophic dynamics. However, recent observational evidence indicates that extratropical wave activity is also associated with equatorial convection even in regions where there is a "critical line" to Rossby wave propagation at upper levels, that is, where the zonal phase speed of the wave is equal to the zonal flow speed. A common manifestation of this type of interaction involves the initiation of convectively coupled Kelvin waves, as well as mixed Rossby-gravity (MRG) waves. These waves are responsible for a large portion of the convective variability within the ITCZ over the Indian, Pacific, and Atlantic sectors, as well as within the Amazon Basin of South America. For example, Kelvin waves originating within the western Pacific ITCZ are often triggered by Rossby wave activity propagating into the Australasian region from the South Indian Ocean extratropics. At other times, Kelvin waves are seen to originate along the eastern slope of the Andes. In the latter case the initial forcing is sometimes linked to a low-level "pressure surge," initiated by wave activity propagating equatorward from the South Pacific storm track. In yet other cases, such as over Africa, the forcing appears to be related to wave activity in the extratropics which is not necessarily propagating into low latitudes, but appears to "project" onto the Kelvin structure, in line with past theoretical and modeling studies. Observational evidence for extratropical forcing of Kelvin and MRG

ecoSPEARS License Signing with Kelvin Manning

NASA Image and Video Library

2017-12-19

NASA Kennedy Space Center's Associate Director Kelvin Manning, center, signs a license agreement with the President and CEO of ecoSPEARS, which allows the company to commercially sell a soil remediation technology developed by a research team at Kennedy. The technology, known as Sorbent Polymer Extraction And Remediation System, is designed to capture and remove polychlorinated biphenyls (PCBs) from contaminated sediments in waterways and wetlands.

High-Resolution, Large-Area, Nano Imprint Lithography

DTIC Science & Technology

2009-08-27

oxides as the seed layers can provide implication as the general synthetic route for the spontaneous growth of metal - silicide nanowires in large...nano-island array preparation , we have successfully fabricated patterned magnetic recording media as described in Fig. 2. About ~30 nm diameter Si...that we fabricated at UCSD with 5-50 nm diameter magnetic islands was used, since a large- area, hard disk size preparation was necessary, and since a

Preliminary Results on New Prototypes of Precision Rh-0.5at%Fe Resistance Thermometers of Chinese Production

NASA Astrophysics Data System (ADS)

Pavese, F.; Szmyrka-Grzebyk, A.; Lipinski, L.; Manuszkiewicz, H.; Qiu, Ping; Zhang, Jin Tao; Lin, Peng; Li, Xing Wei

2008-02-01

Given the practical impossibility of obtaining new precision Rh-0.5at%Fe resistance thermometers in recent years, the possible re-starting of the production of such thermometers in Yunnan (China) was explored by Istituto Nazionale di Ricerca Metrologica (INRIM). Ten prototypes of the new production were made available in early 2006. The paper reports the preliminary data from the testing performed to date on these prototypes at National Institute of Metrology (NIM) and Instytut Niskich Temperatur i Badan Strukturalnych (INTiBS). Although a problem with the alloy composition was detected, the reproducibility results on thermal cycling are very encouraging. Resistance-temperature ( R- T) characteristics below 30 K, though not identical with those of similar thermometers formerly available from Tinsley and VNIIFTRI, are still suitable for accurate metrology.

Non Destructive 3D X-Ray Imaging of Nano Structures & Composites at Sub-30 NM Resolution, With a Novel Lab Based X-Ray Microscope

DTIC Science & Technology

2006-11-01

NON DESTRUCTIVE 3D X-RAY IMAGING OF NANO STRUCTURES & COMPOSITES AT SUB-30 NM RESOLUTION, WITH A NOVEL LAB BASED X- RAY MICROSCOPE S H Lau...article we describe a 3D x-ray microscope based on a laboratory x-ray source operating at 2.7, 5.4 or 8.0 keV hard x-ray energies. X-ray computed...tomography (XCT) is used to obtain detailed 3D structural information inside optically opaque materials with sub-30 nm resolution. Applications include

Novel combination of near-field s-SNOM microscopy with peak-force tapping for nano-chemical and nano-mechanical material characterization with sub-20 nm spatial resolution

NASA Astrophysics Data System (ADS)

Wagner, Martin; Carneiro, Karina; Habelitz, Stefan; Mueller, Thomas; BNS Team; UCSF Team

Heterogeneity in material systems requires methods for nanoscale chemical identification. Scattering scanning near-field microscopy (s-SNOM) is chemically sensitive in the infrared fingerprint region while providing down to 10 nm spatial resolution. This technique detects material specific tip-scattering in an atomic force microscope. Here, we present the first combination of s-SNOM with peak-force tapping (PFT), a valuable AFM technique that allows precise force control between tip and sample down to 10s of pN. The latter is essential for imaging fragile samples, but allows also quantitative extraction of nano-mechanical properties, e.g. the modulus. PFT can further be complemented by KPFM or conductive AFM for nano-electrical mapping, allowing access to nanoscale optical, mechanical and electrical information in a single instrument. We will address several questions ranging from graphene plasmonics to material distributions in polymers. We highlight a biological application where dental amelogenin protein was studied via s-SNOM to learn about its self-assembly into nanoribbons. At the same time PFT allows to track crystallization to distinguish protein from apatite crystals for which amelogenin is supposed to act as a template.

The LiteBIRD Satellite Mission: Sub-Kelvin Instrument

NASA Astrophysics Data System (ADS)

Suzuki, A.; Ade, P. A. R.; Akiba, Y.; Alonso, D.; Arnold, K.; Aumont, J.; Baccigalupi, C.; Barron, D.; Basak, S.; Beckman, S.; Borrill, J.; Boulanger, F.; Bucher, M.; Calabrese, E.; Chinone, Y.; Cho, S.; Crill, B.; Cukierman, A.; Curtis, D. W.; de Haan, T.; Dobbs, M.; Dominjon, A.; Dotani, T.; Duband, L.; Ducout, A.; Dunkley, J.; Duval, J. M.; Elleflot, T.; Eriksen, H. K.; Errard, J.; Fischer, J.; Fujino, T.; Funaki, T.; Fuskeland, U.; Ganga, K.; Goeckner-Wald, N.; Grain, J.; Halverson, N. W.; Hamada, T.; Hasebe, T.; Hasegawa, M.; Hattori, K.; Hattori, M.; Hayes, L.; Hazumi, M.; Hidehira, N.; Hill, C. A.; Hilton, G.; Hubmayr, J.; Ichiki, K.; Iida, T.; Imada, H.; Inoue, M.; Inoue, Y.; Irwin, K. D.; Ishino, H.; Jeong, O.; Kanai, H.; Kaneko, D.; Kashima, S.; Katayama, N.; Kawasaki, T.; Kernasovskiy, S. A.; Keskitalo, R.; Kibayashi, A.; Kida, Y.; Kimura, K.; Kisner, T.; Kohri, K.; Komatsu, E.; Komatsu, K.; Kuo, C. L.; Kurinsky, N. A.; Kusaka, A.; Lazarian, A.; Lee, A. T.; Li, D.; Linder, E.; Maffei, B.; Mangilli, A.; Maki, M.; Matsumura, T.; Matsuura, S.; Meilhan, D.; Mima, S.; Minami, Y.; Mitsuda, K.; Montier, L.; Nagai, M.; Nagasaki, T.; Nagata, R.; Nakajima, M.; Nakamura, S.; Namikawa, T.; Naruse, M.; Nishino, H.; Nitta, T.; Noguchi, T.; Ogawa, H.; Oguri, S.; Okada, N.; Okamoto, A.; Okamura, T.; Otani, C.; Patanchon, G.; Pisano, G.; Rebeiz, G.; Remazeilles, M.; Richards, P. L.; Sakai, S.; Sakurai, Y.; Sato, Y.; Sato, N.; Sawada, M.; Segawa, Y.; Sekimoto, Y.; Seljak, U.; Sherwin, B. D.; Shimizu, T.; Shinozaki, K.; Stompor, R.; Sugai, H.; Sugita, H.; Suzuki, J.; Tajima, O.; Takada, S.; Takaku, R.; Takakura, S.; Takatori, S.; Tanabe, D.; Taylor, E.; Thompson, K. L.; Thorne, B.; Tomaru, T.; Tomida, T.; Tomita, N.; Tristram, M.; Tucker, C.; Turin, P.; Tsujimoto, M.; Uozumi, S.; Utsunomiya, S.; Uzawa, Y.; Vansyngel, F.; Wehus, I. K.; Westbrook, B.; Willer, M.; Whitehorn, N.; Yamada, Y.; Yamamoto, R.; Yamasaki, N.; Yamashita, T.; Yoshida, M.

2018-05-01

Inflation is the leading theory of the first instant of the universe. Inflation, which postulates that the universe underwent a period of rapid expansion an instant after its birth, provides convincing explanation for cosmological observations. Recent advancements in detector technology have opened opportunities to explore primordial gravitational waves generated by the inflation through "B-mode" (divergent-free) polarization pattern embedded in the cosmic microwave background anisotropies. If detected, these signals would provide strong evidence for inflation, point to the correct model for inflation, and open a window to physics at ultra-high energies. LiteBIRD is a satellite mission with a goal of detecting degree-and-larger-angular-scale B-mode polarization. LiteBIRD will observe at the second Lagrange point with a 400 mm diameter telescope and 2622 detectors. It will survey the entire sky with 15 frequency bands from 40 to 400 GHz to measure and subtract foregrounds. The US LiteBIRD team is proposing to deliver sub-Kelvin instruments that include detectors and readout electronics. A lenslet-coupled sinuous antenna array will cover low-frequency bands (40-235 GHz) with four frequency arrangements of trichroic pixels. An orthomode-transducer-coupled corrugated horn array will cover high-frequency bands (280-402 GHz) with three types of single frequency detectors. The detectors will be made with transition edge sensor (TES) bolometers cooled to a 100 milli-Kelvin base temperature by an adiabatic demagnetization refrigerator. The TES bolometers will be read out using digital frequency multiplexing with Superconducting QUantum Interference Device (SQUID) amplifiers. Up to 78 bolometers will be multiplexed with a single SQUID amplifier. We report on the sub-Kelvin instrument design and ongoing developments for the LiteBIRD mission.

Resolution, sensitivity, and in vivo application of high-resolution computed tomography for titanium-coated polymethyl methacrylate (PMMA) dental implants.

PubMed

Cuijpers, Vincent M J I; Jaroszewicz, Jacub; Anil, Sukumaran; Al Farraj Aldosari, Abdullah; Walboomers, X Frank; Jansen, John A

2014-03-01

The aims of this study were (i) to determine the spatial resolution and sensitivity of micro- versus nano-computed tomography (CT) techniques and (ii) to validate micro- versus nano-CT in a dog dental implant model, comparative to histological analysis. To determine spatial resolution and sensitivity, standardized reference samples containing standardized nano- and microspheres were prepared in polymer and ceramic matrices. Thereafter, 10 titanium-coated polymer dental implants (3.2 mm in Ø by 4 mm in length) were placed in the mandible of Beagle dogs. Both micro- and nano-CT, as well as histological analyses, were performed. The reference samples confirmed the high resolution of the nano-CT system, which was capable of revealing sub-micron structures embedded in radiodense matrices. The dog implantation study and subsequent statistical analysis showed equal values for bone area and bone-implant contact measurements between micro-CT and histology. However, because of the limited sample size and field of view, nano-CT was not rendering reliable data representative of the entire bone-implant specimen. Micro-CT analysis is an efficient tool to quantitate bone healing parameters at the bone-implant interface, especially when using titanium-coated PMMA implants. Nano-CT is not suitable for such quantification, but reveals complementary morphological information rivaling histology, yet with the advantage of a 3D visualization. © 2013 John Wiley & Sons A/S. Published by Blackwell Publishing Ltd.

A multidimensional anisotropic strength criterion based on Kelvin modes

NASA Astrophysics Data System (ADS)

Arramon, Yves Pierre

A new theory for the prediction of multiaxial strength of anisotropic elastic materials was proposed by Biegler and Mehrabadi (1993). This theory is based on the premise that the total elastic strain energy of an anisotropic material subjected to multiaxial stress can be decomposed into dilatational and deviatoric modes. A multidimensional strength criterion may thus be formulated by postulating that the failure would occur when the energy stored in one of these modes has reached a critical value. However, the logic employed by these authors to formulate a failure criterion based on this theory could not be extended to multiaxial stress. In this thesis, an alternate criterion is presented which redresses the biaxial restriction by reformulating the surfaces of constant modal energy as surfaces of constant eigenstress magnitude. The resulting failure envelope, in a multidimensional stress space, is piecewise smooth. Each facet of the envelope is expected to represent the locus of failure data by a particular Kelvin mode. It is further shown that the Kelvin mode theory alone provides an incomplete description of the failure of some materials, but that this weakness can be addressed by the introduction of a set of complementary modes. A revised theory which combines both Kelvin and complementary modes is thus proposed and applied seven example materials: an isotropic concrete, tetragonal paperboard, two orthotropic softwoods, two orthotropic hardwoods and an orthotropic cortical bone. The resulting failure envelopes for these examples were plotted and, with the exception of concrete, shown to produce intuitively correct failure predictions.

A High-Resolution Measurement of Ball IR Black Paint's Low-Temperature Emissivity

NASA Technical Reports Server (NTRS)

Tuttle, Jim; Canavan, Ed; DiPirro, Mike; Li, Xiaoyi; Franck, Randy; Green, Dan

2011-01-01

High-emissivity paints are commonly used on thermal control system components. The total hemispheric emissivity values of such paints are typically high (nearly 1) at temperatures above about 100 Kelvin, but they drop off steeply at lower temperatures. A precise knowledge of this temperature-dependence is critical to designing passively-cooled components with low operating temperatures. Notable examples are the coatings on thermal radiators used to cool space-flight instruments to temperatures below 40 Kelvin. Past measurements of low-temperature paint emissivity have been challenging, often requiring large thermal chambers and typically producing data with high uncertainties below about 100 Kelvin. We describe a relatively inexpensive method of performing high-resolution emissivity measurements in a small cryostat. We present the results of such a measurement on Ball InfraRed BlackTM(BIRBTM), a proprietary surface coating produced by Ball Aerospace and Technologies Corp (BATC), which is used in spaceflight applications. We also describe a thermal model used in the error analysis.

Kelvin-Helmholtz Instability: Lessons Learned and Ways Forward

NASA Astrophysics Data System (ADS)

Masson, A.; Nykyri, K.

2018-06-01

The Kelvin-Helmholtz instability (KHI) is a ubiquitous phenomenon across the Universe, observed from 500 m deep in the oceans on Earth to the Orion molecular cloud. Over the past two decades, several space missions have enabled a leap forward in our understanding of this phenomenon at the Earth's magnetopause. Key results obtained by these missions are first presented, with a special emphasis on Cluster and THEMIS. In particular, as an ideal instability, the KHI was not expected to produce mass transport. Simulations, later confirmed by spacecraft observations, indicate that plasma transport in Kelvin-Helmholtz (KH) vortices can arise during non-linear stage of its development via secondary process. In addition to plasma transport, spacecraft observations have revealed that KHI can also lead to significant ion heating due to enhanced ion-scale wave activity driven by the KHI. Finally, we describe what are the upcoming observational opportunities in 2018-2020, thanks to a unique constellation of multi-spacecraft missions including: MMS, Cluster, THEMIS, Van Allen Probes and Swarm.

A planar nano-positioner driven by shear piezoelectric actuators

NASA Astrophysics Data System (ADS)

Dong, W.; Li, H.; Du, Z.

2016-08-01

A planar nano-positioner driven by the shear piezoelectric actuators is proposed in this paper based on inertial sliding theory. The performance of the nano-positioner actuated by different driving signals is analyzed and discussed, e.g. the resolution and the average velocity which depend on the frequency, the amplitude and the wave form of the driving curves. Based on the proposed design, a prototype system of the nano-positioner is developed by using a capacitive sensor as the measurement device. The experiment results show that the proposed nano-positioner is capable of outputting two-dimensional motions within an area of 10 mm × 10 mm at a maximum speed of 0.25 mm/s. The corresponding resolution can be as small as 21 nm. The methodology outlined in this paper can be employed and extended to shear piezoelectric actuators involved in high precision positioning systems.

Thermodynamics and historical relevance of a jetting thermometer made of Chinese zisha ceramic

NASA Astrophysics Data System (ADS)

Lee, Vincent; Attinger, Daniel

2016-07-01

Following a recent trend of scientific studies on artwork, we study here the thermodynamics of a thermometer made of zisha ceramic, related to the Chinese tea culture. The thermometer represents a boy who “urinates” shortly after hot water is poured onto his head. Long jetting distance is said to indicate that the water temperature is hot enough to brew tea. Here, a thermodynamic model describes the jetting phenomenon of that pee-pee boy. The study demonstrates how thermal expansion of an interior air pocket causes jetting. A thermodynamic potential is shown to define maximum jetting velocity. Seven optimization criteria to maximize jetting distance are provided, including two dimensionless numbers. Predicted jetting distances, jet durations, and temperatures agree very well with infrared and optical measurements. Specifically, the study confirms that jetting distances are sensitive enough to measure water temperature in the context of tea brewing. Optimization results show that longer jets are produced by large individuals, with low body mass index, with a boyhood of medium size inclined at an angle π/4. The study ends by considering the possibility that ceramic jetting artifacts like the pee-pee boy might have been the first thermometers known to mankind, before Galileo Galilei’s thermoscope.

Thermodynamics and historical relevance of a jetting thermometer made of Chinese zisha ceramic

PubMed Central

Lee, Vincent; Attinger, Daniel

2016-01-01

Following a recent trend of scientific studies on artwork, we study here the thermodynamics of a thermometer made of zisha ceramic, related to the Chinese tea culture. The thermometer represents a boy who “urinates” shortly after hot water is poured onto his head. Long jetting distance is said to indicate that the water temperature is hot enough to brew tea. Here, a thermodynamic model describes the jetting phenomenon of that pee-pee boy. The study demonstrates how thermal expansion of an interior air pocket causes jetting. A thermodynamic potential is shown to define maximum jetting velocity. Seven optimization criteria to maximize jetting distance are provided, including two dimensionless numbers. Predicted jetting distances, jet durations, and temperatures agree very well with infrared and optical measurements. Specifically, the study confirms that jetting distances are sensitive enough to measure water temperature in the context of tea brewing. Optimization results show that longer jets are produced by large individuals, with low body mass index, with a boyhood of medium size inclined at an angle π/4. The study ends by considering the possibility that ceramic jetting artifacts like the pee-pee boy might have been the first thermometers known to mankind, before Galileo Galilei’s thermoscope. PMID:27431925

Equally sloped tomography based X-ray full-field nano-CT at Shanghai Synchrotron Radiation Facility

NASA Astrophysics Data System (ADS)

Wang, Yudan; Ren, Yuqi; Zhou, Guangzhao; Du, Guohao; Xie, Honglan; Deng, Biao; Xiao, Tiqiao

2018-07-01

X-ray full-field nano-computed tomography (nano-CT) has non-destructive three-dimensional imaging capabilities with high spatial resolution, and has been widely applied to investigate morphology and structures in various areas. Conventional tomography reconstructs a 3D object from a large number of equal-angle projections. For nano-CT, it takes long collecting time due to the large projection numbers and long exposure time. Here, equally-sloped tomography (EST) based nano-CT was implemented and constructed on X-ray imaging beamline at the Shanghai Synchrotron Radiation Facility (SSRF) to overcome or alleviate these difficulties. Preliminary results show that hard TXM with the spatial resolution of 100 nm and the EST-based nano-CT with the ability of 3D nano non-destructive characterization have been realized. This technique promotes hard X-ray imaging capability to nano scales at SSRF and could have applications in many fields including nanomaterials, new energy and life sciences. The study will be helpful for the construction of the new full field X-ray nano-imaging beamline with the spatial resolution of 20 nm at SSRF phase II project.

Evaluation of platinum resistance thermometers

NASA Technical Reports Server (NTRS)

Daryabeigi, Kamran; Dillon-Townes, Lawrence A.

1988-01-01

An evaluation procedure for the characterization of industrial platinum resistance thermometers (PRTs) for use in the temperature range -120 to 160 C was investigated. This evaluation procedure consisted of calibration, thermal stability and hysteresis testing of four surface measuring PRTs. Five different calibration schemes were investigated for these sensors. The IPTS-68 formulation produced the most accurate result, yielding average sensor systematic error of 0.02 C and random error of 0.1 C. The sensors were checked for thermal stability by successive and thermal cycling between room temperature, 160 C, and boiling point of nitrogen. All the PRTs suffered from instability and hysteresis. The applicability of the self-heating technique as an in situ method for checking the calibration of PRTs located inside wind tunnels was investigated.

Interannual variability in equatorial Kelvin waves in the upper troposphere and lower stratosphere, and relation to the background equatorial wind

NASA Astrophysics Data System (ADS)

Suzuki, J.; Nishi, N.; Fujiwara, M.; Yoneyama, K.

2016-12-01

We investigated the influence of the background wind regime on interannual variability in equatorial Kelvin waves in the upper troposphere and lower stratosphere using the European Centre for Medium-Range Weather Forecasts 40-year reanalysis data. We focused on variability in the number of Kelvin wave events as a function of the background westerly wind, given by the zonal wind index (ZWI) in the equatorial western hemisphere. The ZWI measures the strength of the upper branch of the Walker circulation in the western hemisphere. Although the ZWI is well correlated with the sea surface temperature in the Niño-3.4 region, nearly half of the peaks of positive (negative) ZWI cases occurred outside of the typical La Niña (El Niño) season (December to February), respectively. In the positive ZWI (stronger westerly) cases, both convective activity over the western Pacific and extratropical Rossby waves were enhanced. Kelvin waves over the western hemisphere appeared frequently at 200 hPa but barely reached 100 hPa due to the strong westerly wind under this level. In the negative ZWI period, on the other hand, the number of Kelvin waves at 200 hPa decreased due to the weaker convection; Kelvin waves reached 100 hPa and propagated even farther upward. We also investigated the relationship between the ZWI and the phase speed of Kelvin waves. Kelvin waves with relatively slow phase speeds are found in negative ZWI cases, but are not found in positive ZWI cases due to the westerly background wind below the altitudes where Kelvin waves commonly propagate.

Development of a Standard Platinum Resistance Thermometer for Use up to the Copper Point

NASA Astrophysics Data System (ADS)

Tavener, J. P.

2015-08-01

The international temperature scale of 1990 defines temperatures in the range from 13.8 K to 1234.93 K () using a standard platinum resistance thermometer (SPRT) as an interpolating instrument. For temperatures above , the current designs of an SPRT require extreme care to avoid contamination, especially by metallic impurities, which can cause rapid and irreversible drift. This study investigates the performance of a new design of a high-temperature SPRT with the aim of improving the stability of the SPRTs and extending their temperature range. The prototype SPRTs have an alumina sheath, a sapphire support for the sensing element, which are aspirated with dry air and operated with a dc bias voltage to suppress the diffusion of metal-ion contaminants. Three prototype thermometers were exposed to temperatures near or above the copper freezing point, , for total exposure times in excess of 500 h and exhibited drifts in the triple-point resistance of less than 10 mK. The new design eliminates some of the problems associated with fused-silica sheaths and sensor-support structures and is a viable option for a high-accuracy thermometer for temperatures approaching.

Evaluation of the Use of Optical Fiber Thermometers for Thermal Control of the Quench Module Insert

NASA Technical Reports Server (NTRS)

Jones, Matthew R.; Farmer, Jeffrey T.; Breeding, Shawn P.

2001-01-01

Issues regarding the use of optical fiber thermometers to control heater settings in a microgravity vacuum furnace are addressed. It is desirable to use these probes in environments such as the International Space Station, because they can be operated without re-calibration for extended periods. However, the analysis presented in this paper shows that temperature readings obtained using optical fiber thermometers can be corrupted by emissions from the fiber when extended portions of the probe are exposed to elevated temperatures.

Evaluation of the Use of Optical Fiber Thermometers for Thermal Control of the Quench Module Insert

NASA Technical Reports Server (NTRS)

Jones, Matthew R.; Farmer, Jeffrey T.; Breeding, Shawn P.

1999-01-01

Issues regarding the use of optical fiber thermometers to control heater settings in a microgravity vacuum furnace are addressed. It is desirable to use these probes in environments such as the International Space Station, because they can be operated without re-calibration for extended periods. However, the analysis presented in this paper shows that temperature readings obtained using optical fiber thermometers are corrupted due to emissions from the fiber when extended portions of the probe are exposed to elevated temperatures.

Room temperature, very sensitive thermometer using a doubly clamped microelectromechanical beam resonator for bolometer applications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Y., E-mail: zhangya@iis.u-tokyo.ac.jp; Watanabe, Y.; Hosono, S.

We propose a room temperature, all electrical driving and detecting, very sensitive thermometer structure using a microelectromechanical (MEMS) resonator for bolometer applications. We have fabricated a GaAs doubly clamped MEMS beam resonator whose oscillation can be excited and detected by the piezoelectric effect. When a heating power is applied to a NiCr film deposited on the MEMS beam surface, internal thermal stress is generated in the beam, leading to a reduction in the resonance frequency. The present device detects the shift in the resonance frequency caused by heating and works as a very sensitive thermometer. When the resonator was drivenmore » by a voltage slightly below the threshold for the nonlinear, hysteretic oscillation, the thermometer showed a voltage responsivity of about 3300 V/W, while keeping a low noise spectral density of about 60 nV/Hz{sup 1/2}, demonstrating a noise equivalent power of <20 pW/Hz{sup 1/2} even at room temperature. The observed effect can be used for realizing high-sensitivity terahertz bolometers for room-temperature operation.« less

Evaluation of structural and thermophysical effects on the measurement accuracy of deep body thermometers based on dual-heat-flux method.

PubMed

Huang, Ming; Tamura, Toshiyo; Chen, Wenxi; Kanaya, Shigehiko

2015-01-01

To help pave a path toward the practical use of continuous unconstrained noninvasive deep body temperature measurement, this study aims to evaluate the structural and thermophysical effects on measurement accuracy for the dual-heat-flux method (DHFM). By considering the thermometer's height, radius, conductivity, density and specific heat as variables affecting the accuracy of DHFM measurement, we investigated the relationship between those variables and accuracy using 3-D models based on finite element method. The results of our simulation study show that accuracy is proportional to the radius but inversely proportional to the thickness of the thermometer when the radius is less than 30.0mm, and is also inversely proportional to the heat conductivity of the heat insulator inside the thermometer. The insights from this study would help to build a guideline for design, fabrication and optimization of DHFM-based thermometers, as well as their practical use. Copyright © 2014 Elsevier Ltd. All rights reserved.

A Virtual Instrument Panel and Serial Interface for the Parr 1672 Thermometer

ERIC Educational Resources Information Center

Salter, Gail; Range, Kevin; Salter, Carl

2005-01-01

The various features of a Visual Basic Program, which implements the 1672 Parr thermometer are described. The program permits remote control of the calorimetry experiment and also provides control for the flow of data and for file storage.

Kelvin Helmholtz Instability at the Equatorial Magnetotail Boundary: MHD Simulation and Comparison with Geotail Observations

NASA Technical Reports Server (NTRS)

Fairfield, Donald H.; Otto, A.

1999-01-01

On March 24, 1995 the Geotail spacecraft observed large fluctuations of the magnetic field and plasma properties in the Low Latitude Boundary Layer (LLBL) about 15 R(sub E) tailward of the dusk meridian. Although the magnetospheric and the magnetosheath field were strongly northward, the B(sub z) component showed strong short duration fluctuations in which B(sub z) could even reach negative values. We have used two-dimensional magnetohydrodynamic simulations with magnetospheric and magnetosheath input parameters specifically chosen for this. Geotail event to identify the processes which cause the observed boundary properties. It is shown that these fluctuations can be explained by the Kelvin-Helmholtz instability if the k vector of the instability has a component along the magnetic field direction. The simulation results show many of the characteristic properties of the Geotail observations. In particular, the quasi-periodic strong fluctuations are well explained by satellite crossings through the Kelvin-Helmholtz vortices. It is illustrated how the interior structure of the Kelvin-Helmholtz vortices leads to the rapid fluctuations in the Geotail observations. Our results suggest an average Kelvin-Helmholtz wavelength of about 5 R(sub E) with a vortex size of close to 2 R(sub E) for an average repetition time of 2.5 minutes. The growth time for these waves implies a source region of about 10 to 16 R(sub E) upstream from the location of the Geotail spacecraft (i.e., near the dusk meridian). The results also indicate a considerable mass transport of magnetosheath material into the magnetosphere by magnetic reconnection in the Kelvin-Helmholtz vortices.

A special MJO event with a double Kelvin wave structure

NASA Astrophysics Data System (ADS)

Zhu, Lili; Li, Tim

2017-04-01

The second Madden-Julian Oscillation (MJO) event during the field campaign of the Dynamics of the MJO/Cooperative Indian Ocean Experiment on Intraseasonal Variability in the Year 2011 (DYNAMO/CINDY2011) exhibi ted an unusual double rainband structure. Using a wavenumber-frequency spectral filtering method, we unveil that this double rainband structure arises primarily from the Kelvin wave component. The zonal phase speed of the double rainbands is about 7.9 degree per day in the equatorial Indian Ocean, being in the range of convectively coupled Kelvin wave phase speeds. The convection and circulation anomalies associated with the Kelvin wave component are characterized by two anomalous convective cells, with low-level westerly (easterly) and high (low) pressure anomalies to the west (east) of the convective centers, and opposite wind and pressure anomalies in the upper troposphere. Such a zonal wind-pressure phase relationship is consistent with the equatorial free-wave dynamics. While the free-atmospheric circulation was dominated by the first baroclinic mode vertical structure, moisture and vertical motion in the boundary layer led the convection. The convection and circulation structures derived based on the conventional MJO filter show a different characteristic. For example, the phase speed is slower (about 5.9 degree per day), and there were no double convective branches. This suggests that MJO generally involves multi-scales and it is incomplete to extract its signals by using the conventional filtering technique.

Operation of Kelvin Effect in the Activities of an Antifreeze Protein: A Molecular Dynamics Simulation Study.

PubMed

Midya, Uday Sankar; Bandyopadhyay, Sanjoy

2018-03-29

Ice growth and melting inhibition activities of antifreeze proteins (AFPs) are better explained by the adsorption-inhibition mechanism. Inhibition occurs as a result of the Kelvin effect induced by adsorbed protein molecules onto the surface of seed ice crystal. However, the Kelvin effect has not been explored by the state-of-the-art experimental techniques. In this work, atomistic molecular dynamics simulations have been carried out with Tenebrio molitor antifreeze protein ( TmAFP) placed at ice-water interface to probe the Kelvin effect in the mechanism of AFPs. Simulations show that, below equilibrium melting temperature, ice growth is inhibited through the convex ice-water interface formation toward the water phase and, above equilibrium melting temperature, ice melting is inhibited through the concave ice-water interface formation inward to ice phase. Simulations further reveal that the radius of curvature of the interface formed to stop the ice growth increases with decrease in the degree of supercooling. Our results are in qualitative agreement with the theoretical prediction of the Kelvin effect and thus reveal its operation in the activities of AFPs.

Response time correlations for platinum resistance thermometers

NASA Technical Reports Server (NTRS)

Pandey, D. K.; Ash, R. L.; Dillon-Townes, L. A.

1985-01-01

The 'plunge method' recommended by ASTM has been used to determine the time constant of 100-ohm platinum resistance thermometers (PRT) considered for use in the National Transonic Facility. It is shown that the response time of ventilated PRT can be correlated with the reciprocal of the heat transfer coefficient in a given field. Universal correlations are established for the 100- and 1000-ohm PRT with uncertainties of 20 and 30 percent, respectively. The correlations are found to be consistent with the uncertainty involved in heat transfer correlations available in the literature and are recommended for use in flowing liquids and gases.

Progress on 10 Kelvin cryo-cooled sapphire oscillator

NASA Technical Reports Server (NTRS)

Wang, Rabi T.; Dick, G. John; Diener, William A.

2004-01-01

We present recent progress on the 10 Kelvin Cryocooled Sapphire Oscillator (10K CSO). Included are incorporation of a new pulse tube cryocooler, cryocooler vibration comparisons between G-M and pulse-tube types, phase noise, and frequency stability tests. For the advantage of a single stage pulse tube cryocooler, we also present results for a 40K Compensated Sapphire Oscillator (40K CSO).

The Fourier-Kelvin Stellar Interferometer Mission Concept

NASA Technical Reports Server (NTRS)

Danchi, W. C.; Allen, R.; Benford, D.; Gezari, D.; Leisawitz, D.; Mundy, L.; Oegerle, William (Technical Monitor)

2002-01-01

The Fourier-Kelvin Stellar Interferometer (FKSI) is a mission concept for an imaging interferometer for the mid-infrared spectral region (5-30 microns). FKSI is conceived as a scientific and technological precursor to TPF as well as Space Infrared Interferometric Telescope (SPIRIT), Submillimeter Probe Evolution of Cosmic Structure (SPECS), and Single Aperture for Infrared Observatory (SAFIR). It will also be a high angular resolution system complementary to Next Generation Space Telescope (NGST). The scientific emphasis of the mission is on the evolution of protostellar systems, from just after the collapse of the precursor molecular cloud core, through the formation of the disk surrounding the protostar, the formation of planets in the disk, and eventual dispersal of the disk material. FKSI will also search for brown dwarfs and Jupiter mass and smaller planets, and could also play a very powerful role in the investigation of the structure of active galactic nuclei and extra-galactic star formation. We are in the process of studying alternative interferometer architectures and beam combination techniques, and evaluating the relevant science and technology tradeoffs. Some of the technical challenges include the development of the cryocooler systems necessary for the telescopes and focal plane array, light and stiff but well-damped truss systems to support the telescopes, and lightweight and coolable optical telescopes. The goal of the design study is to determine if a mid-infrared interferometry mission can be performed within the cost and schedule requirements of a Discovery class mission. At the present time we envision the FKSI as comprised of five one meter diameter telescopes arranged along a truss structure in a linear non-redundant array, cooled to 35 K. A maximum baseline of 20 meters gives a nominal resolution of 26 mas at 5 microns. Using a Fizeau beam combination technique, a simple focal plane camera could be used to obtain both Fourier and spectral

The evaluation of a clinical thermometer for measuring developer temperature in automatic film processors.

PubMed

Wilson, W B; Haus, A G; Nierman, C; Lillie, R; Batz, T; Moore, R

1993-01-01

In medical imaging, the temperature of the developer solution in the film processor affects film speed (radiation dose), film contrast, and film base plus fog. The National Council on Radiation Protection and Measurement (NCRP) Report 99 on Quality Assurance, and the American College of Radiology (ACR) Mammography Quality Control Manual for Radiologic Technologists, indicate that the developer temperature should be within +/- 0.5 degree F (+/- 0.3 degree C) of that recommended by the manufacturer for the specific film/developer combination being used. The accuracy and repeatability of the thermometer is most important. This paper describes the requirements of a thermometer for measuring the temperature of the developer solution and suggests an inexpensive but accurate device for doing so.

Detection of the fast Kelvin wave teleconnection due to El Niño-Southern Oscillation

NASA Astrophysics Data System (ADS)

Meyers, Steven D.; Melsom, Arne; Mitchum, Gary T.; O'Brien, James J.

1998-11-01

Previous analyses of the ocean state along the western American coast have often indicated unexpectedly slow and limited propagation of coastally trapped Kelvin waves associated with the El Niño-Southern Oscillation. In contrast, theoretical and numerical ocean models demonstrate that these Kelvin waves are a rapid and long-range teleconnection between the low- and high-latitude Pacific Ocean, strongly impacting both the surface coastal currents and nutrient upwelling. Sea level variations along the western coast of North America are reexamined under the assumption that tropically forced Kelvin waves are produced in bursts of several months duration. A cross-correlation analysis, restricted to mid-1982 to mid-1983, is performed between Galapagos Island and stations along western Central and North America. A coastally trapped Kelvin wave is revealed to propagate at a speed of 2-3 m s-1 from the tropical Pacific to the Aleutian Island Chain. The observed phase speed agrees with the estimated speed of a Kelvin wave based on the average density profile of the ocean near the coast. Weaker El Niño events in 1986/1987 and 1991/1992 appear to contain a combination of this remote signal and local wind forcing. The wave propagation speed calculated from the spectral phase is shown to be sensitive to the presence of other (noise) processes in the observations. This is demonstrated through an analysis of a synthetic sea level data set that contains many of the essential features of the real sea level data. A relatively small level of red noise can give a 100% expected error in the estimated propagation speed. This suggests a new explanation for this important inconsistency within dynamical oceanography.

Optical Fiber Thermometer Based on Fiber Bragg Gratings

NASA Astrophysics Data System (ADS)

Rosli, Ekbal Bin; Mohd. Noor, Uzer

2018-03-01

Fiber Bragg grating has generated much interest in use as sensors to measure strain, temperature, and other physical parameters. It also the most common component used to develop this sensor with the advantages of simple, intrinsic sensing elements, electrically passive operation, EMI immunity, high sensitivity, compact size and potentially low cost [6]. This paper reports the design of an optical fiber thermometer based on fiber Bragg gratings. The system was developed for detecting temperature and strain by monitoring the shift of Bragg wavelength. The shifting of Bragg wavelength is used to indicate the temperature and strain due to the change in the surrounding temperature and strain. When the temperature and strain reach the exact wavelength level of the system, the temperature and strain value will display on the Arduino liquid crystal display (LCD). The optical fiber will provide the broadband light source and after passing the FBG the Bragg wavelength into the optical spectrum analyzer (OSA). The system is based on FBG as a physical quantity sensor. The temperatures measured is taken from the water bath and that of the strain is provided by amount of slotted mass used. The outcome of this project is to characterize the Bragg wavelength shifting from the fiber Bragg grating output. As the conclusion, this project provides an efficient optical fiber thermometer in measuring temperature and strain in order to replace the use of conventional electrical instruments.

Software Products for Temperature Data Reduction of Platinum Resistance Thermometers (PRT)

NASA Technical Reports Server (NTRS)

Sherrod, Jerry K.

1998-01-01

The main objective of this project is to create user-friendly personal computer (PC) software for reduction/analysis of platinum resistance thermometer (PRT) data. Software products were designed and created to help users of PRT data with the tasks of using the Callendar-Van Dusen method. Sample runs are illustrated in this report.

The Evolution of the Celsius and Kelvin Temperature Scales and the State of the Art

NASA Astrophysics Data System (ADS)

Pellicer, Julio; Amparo Gilabert, M.; Lopez-Baeza, Ernesto

1999-07-01

A physical analysis is given of the evolution undergone by the Celsius and Kelvin temperature scales, from their definition to the present day. It is shown that in the temperature interval between the melting point of ice and the boiling point of water, the Celsius and Kelvin scales, both born centigrade by definition and actually become so afterwards by experimental determination as well, are not so any longer, either by definition or by experimental determination.

Coupled Kelvin-Helmholtz and Tearing Mode Instabilities at the Mercury's Magnetopause

NASA Astrophysics Data System (ADS)

Ivanovski, S. L.; Milillo, A.; Kartalev, M.; Massetti, S.

2018-05-01

A MHD approach for numerical simulations of coupled Kelvin-Helmholtz and tearing mode instabilities has been applied to Mercury’s magnetopause and used to perform a physical parameters study constrained by the MESSENGER data.

A novel diamond micro-/nano-machining process for the generation of hierarchical micro-/nano-structures

NASA Astrophysics Data System (ADS)

Zhu, Zhiwei; To, Suet; Ehmann, Kornel F.; Xiao, Gaobo; Zhu, Wule

2016-03-01

A new mechanical micro-/nano-machining process that combines rotary spatial vibrations (RSV) of a diamond tool and the servo motions of the workpiece is proposed and applied for the generation of multi-tier hierarchical micro-/nano-structures. In the proposed micro-/nano-machining system, the servo motion, as the primary cutting motion generated by a slow-tool-servo, is adopted for the fine generation of the primary surfaces with complex shapes. The RSV, as the tertiary cutting operation, is superimposed on the secondary fundamental rotary cutting motion to construct secondary nano-structures on the primary surface. Since the RSV system generally works at much higher frequencies and motion resolution than the primary and secondary motions, it leads to an inherent hierarchical cutting architecture. To investigate the machining performance, complex micro-/nano-structures were generated and explored by both numerical simulations and actual cutting tests. Rotary vibrations of the diamond tool at a constant rotational distance offer an inherent constant cutting velocity, leading to the ability for the generation of homogeneous micro-/nano-structures with fixed amplitudes and frequencies of the vibrations, even over large-scale surfaces. Furthermore, by deliberately combining the non-resonant three-axial vibrations and the servo motion, the generation of a variety of micro-/nano-structures with complex shapes and with flexibly tunable feature sizes can be achieved.

Tuned-circuit dual-mode Johnson noise thermometers

NASA Astrophysics Data System (ADS)

Shepard, R. L.; Carroll, R. M.; Falter, D. D.; Blalock, T. V.; Roberts, M. J.

1992-02-01

Dual-mode Johnson noise and direct current (DC) resistance thermometers can be used in control systems where prompt indications of temperature changes and long-term accuracy are needed. Such a thermometer is being developed for the SP-100 space nuclear electric power system that requires temperature measurement at 1400 K in space for 10 years, of which 7 are expected to be at full reactor power. Several direct coupled and transformer coupled, tuned resistance inductance capacitance (RLC) circuits that produce a single, continuous voltage signal were evaluated for noise temperature measurement. The simple direct coupled RLC circuit selected provides a mean squared noise voltage that depends only on the capacitance used and the temperature of the sensor, and it is independent of the value of or changes in the sensor resistance. These circuits provide a noise signal with long term accuracy but require integrating noise signals for a finite length of time. The four wire resistor for the noise temperature sensor allows simultaneous DC resistance measurements to be made that provide a prompt, continuous temperature indication signal. The DC current mode is employed continuously, and a noise voltage measurement is made periodically to correct the temperature indication. The differential noise voltage preamplifier used substantially reduces electromagnetic interference (EMI) in the system. A sensor has been tested that should provide good performance (+/- 1 percent accuracy) and long-term (10 year) reliability in space environments. Accurate noise temperature measurements were made at temperatures above 1300 K, where significant insulator shunting occurs, even though shunting does affect the dc resistance measurements and makes the system more susceptible to EMI.

Single-Mode, Supersonic Kelvin-Helmholtz Instability Experiment on OMEGA-EP

NASA Astrophysics Data System (ADS)

Wan, Wesley; Malamud, G.; Di Stefano, C.; Kuranz, C. C.; Drake, R.

2013-06-01

Laboratory laser experiments are able to produce and study phenomena that occur in astrophysical systems, allowing us to study mechanisms relevant to the formation, interaction, and destruction processes of stars and planets. These dynamic processes are strongly affected by hydrodynamic instabilities such as the Kelvin-Helmholtz instability, which arises when shear flow at an interface causes mixing between fluid layers. This instability is commonly observed at the boundary of cloud bands among gas planets, and can act as an atmospheric loss mechanism on planets with little to no intrinsic magnetic field. It is also observed in simulations of astrophysical systems including supernovae and wind-driven clumps. This poster discusses an upcoming experiment for the OMEGA-EP system that will produce a supersonic Kelvin-Helmholtz instability in the high-energy-density regime. This experiment will use a long laser pulse to create a sustained shock through two stratified layers separated by a seeded, single-mode perturbation. A high Mach number is believed to suppress the growth of the Kelvin-Helmholtz instability and, if sufficiently high, prevent growth entirely. We will be quantifying these effects using x-ray radiography. This work is funded by the NNSA-DS and SC-OFES Joint Program in High-Energy-Density Laboratory Plasmas, grant number DE-FG52-09NA29548, and by the National Laser User Facility Program, grant number DE-NA0000850, with additional support provided under Cooperative Agreement No. DE-FC52-08NA28302 through the Laboratory for Laser Energetics, University of Rochester.

Stability of some epoxy-encapsulated diode thermometers

NASA Technical Reports Server (NTRS)

Mangum, B. W.; Evans, G. A., Jr.

1986-01-01

The stability upon thermal cycling and handling of ten small, epoxy-encapsulated silicon diode thermometers at six temperatures in the range from liquid nitrogen temperatures to about 60 C. The nominal temperatures of measurement were -196, -78, 0, 20, 40, and 60 C, as measured on the International Practical Temperature Scale of 1968. Diodes were to be thermally cycled 15 to 20 times. Since NASA anticipates that the uncertainty in their temperature measurements will be + or - 50 mK, uncertainties as large as + or - 10 mK in the measurements of the evaluaton can be accommodated without deleteriously affecting the value of the results of the investigation.

Equatorial atmospheric Kelvin waves during El Niño episodes and their effect on stratospheric QBO.

PubMed

Das, Uma; Pan, C J

2016-02-15

Equatorial atmospheric Kelvin waves are investigated during a positive El Niño Southern Oscillation (ENSO) episode using temperature data retrieved from GPS Radio Occultation (RO) observations of FORMOSAT-3/COSMIC during the period from August 2006 to December 2013. Enhanced Kelvin wave amplitudes are observed during the El Niño episode of 2009-2010 and it is also observed that these amplitudes correlate with the Niño 3.4 index and also with outgoing longwave radiation and trade wind index. This study indicates that the enhanced equatorial atmospheric Kelvin wave amplitudes might be produced by geophysical processes that were involved in the onset and development of the El Niño episode. Further, easterly winds above the tropopause during this period favored the vertically upward propagation of these waves that induced a fast descending westerly regime by the end of 2010, where the zero-wind line is observed to take only 5 months to descend from 10 to 50 hPa. The current study presents observational evidence of enhanced Kelvin wave amplitudes during El Niño that has affected the stratospheric quasi-biennial oscillation (QBO) through wave-mean flow interactions. Earlier El Niño episodes of 1987 and 1998 are also qualitatively investigated, using reanalysis data. It is found that there might have been an enhancement in the equatorial Kelvin wave amplitudes during almost all El Niño episodes, however, an effect of a fast descending westerly is observed in the QBO only when the ambient zonal winds in the lower stratosphere favor the upward propagation of the Kelvin waves and consequently they interact with the mean flow. This study indicates that the El Niño and QBO are not linearly related and wave mean flow interactions play a very important role in connecting these two geophysical phenomena. Copyright © 2015 Elsevier B.V. All rights reserved.

Hybrid Plasmonic Microring Nano-Ruler.

PubMed

Du, Jing; Wang, Jian

2018-06-15

Surface plasmonic polariton (SPP) has attracted increasing interest for its ability of confining light in the subwavelength scale and breaking the diffraction limit. Recently, there have appeared several important developments of SPP applied in plasmon rulers, waveguides and resonators. By combing these concepts we present a novel hybrid plasmonic microring nano-ruler relying on the sensitive hybrid mode property and the microring resonator structure. The designed nano-ruler can measure distance in nanoscale resolution and offer adjustable sensitivity, which exceeds 14.8 as the distance is less than 5 nm by recording the transmission spectra and outstrips 200 dB/nm by observing the shift of output intensity. These demonstrations suggest that hybrid plasmonic microring nano-ruler could be a promising candidate enabling high-resoluation measurement.

Stable isomers and electronic, vibrational, and optical properties of WS2 nano-clusters: A first-principles study

NASA Astrophysics Data System (ADS)

Hafizi, Roohollah; Hashemifar, S. Javad; Alaei, Mojtaba; Jangrouei, MohammadReza; Akbarzadeh, Hadi

2016-12-01

In this paper, we employ an evolutionary algorithm along with the full-potential density functional theory (DFT) computations to perform a comprehensive search for the stable structures of stoichiometric (WS2)n nano-clusters (n = 1 - 9), within three different exchange-correlation functionals. Our results suggest that n = 5 and 8 are possible candidates for the low temperature magic sizes of WS2 nano-clusters while at temperatures above 500 Kelvin, n = 7 exhibits a comparable relative stability with n = 8. The electronic properties and energy gap of the lowest energy isomers were computed within several schemes, including semilocal Perdew-Burke-Ernzerhof and Becke-Lee-Yang-Parr functionals, hybrid B3LYP functional, many body based DFT+GW approach, ΔSCF method, and time dependent DFT calculations. Vibrational spectra of the lowest lying isomers, computed by the force constant method, are used to address IR spectra and thermal free energy of the clusters. Time dependent density functional calculation in a real time domain is applied to determine the full absorption spectra and optical gap of the lowest energy isomers of the WS2 nano-clusters.

Reliability of an infrared forehead skin thermometer for core temperature measurements.

PubMed

Kistemaker, J A; Den Hartog, E A; Daanen, H A M

2006-01-01

The SensorTouch thermometer performs an infrared measurement of the skin temperature above the Superficial Temporal Artery (STA). This study evaluates the validity and the accuracy of the SensorTouch thermometer. Two experiments were performed in which the body temperature was measured with a rectal sensor, with an oesophageal sensor and with the SensorTouch. After entering a warm chamber the SensorTouch underestimated the core temperature during the first 10 minutes. After that, the SensorTouch was not significantly different from the core temperature, with an average difference of 0.5 degrees C (SD 0.5 degrees C) in the first study and 0.3 degrees C (SD 0.2 degrees C) in the second study. The largest differences between the SensorTouch and the core temperature existed 15 minutes after the start of the exercise. During this period the SensorTouch was significantly higher than the core temperature. The SensorTouch did not provide reliable values of the body temperature during periods of increasing body temperature, but the SensorTouch might work under stable conditions.

Super-resolution for asymmetric resolution of FIB-SEM 3D imaging using AI with deep learning.

PubMed

Hagita, Katsumi; Higuchi, Takeshi; Jinnai, Hiroshi

2018-04-12

Scanning electron microscopy equipped with a focused ion beam (FIB-SEM) is a promising three-dimensional (3D) imaging technique for nano- and meso-scale morphologies. In FIB-SEM, the specimen surface is stripped by an ion beam and imaged by an SEM installed orthogonally to the FIB. The lateral resolution is governed by the SEM, while the depth resolution, i.e., the FIB milling direction, is determined by the thickness of the stripped thin layer. In most cases, the lateral resolution is superior to the depth resolution; hence, asymmetric resolution is generated in the 3D image. Here, we propose a new approach based on an image-processing or deep-learning-based method for super-resolution of 3D images with such asymmetric resolution, so as to restore the depth resolution to achieve symmetric resolution. The deep-learning-based method learns from high-resolution sub-images obtained via SEM and recovers low-resolution sub-images parallel to the FIB milling direction. The 3D morphologies of polymeric nano-composites are used as test images, which are subjected to the deep-learning-based method as well as conventional methods. We find that the former yields superior restoration, particularly as the asymmetric resolution is increased. Our super-resolution approach for images having asymmetric resolution enables observation time reduction.

Microvolume trace environmental analysis using peak-focusing online solid-phase extraction-nano-liquid chromatography-high-resolution mass spectrometry.

PubMed

Stravs, Michael A; Mechelke, Jonas; Ferguson, P Lee; Singer, Heinz; Hollender, Juliane

2016-03-01

Online solid-phase extraction was combined with nano-liquid chromatography coupled to high-resolution mass spectrometry (HRMS) for the analysis of micropollutants in environmental samples from small volumes. The method was validated in surface water, Microcystis aeruginosa cell lysate, and spent Microcystis growth medium. For 41 analytes, quantification limits of 0.1-28 ng/L (surface water) and 0.1-32 ng/L (growth medium) were obtained from only 88 μL of sample. In cell lysate, quantification limits ranged from 0.1-143 ng/L or 0.33-476 ng/g dry weight from a sample of 88 μL, or 26 μg dry weight, respectively. The method matches the sensitivity of established online and offline solid-phase extraction-liquid chromatography-mass spectrometry methods but requires only a fraction of the sample used by those techniques, and is among the first applications of nano-LC-MS for environmental analysis. The method was applied to the determination of bioconcentration in Microcystis aeruginosa in a laboratory experiment, and the benefit of coupling to HRMS was demonstrated in a transformation product screening.

Assessing the accuracy of globe thermometer method in predicting outdoor mean radiant temperature under Malaysia tropical microclimate

NASA Astrophysics Data System (ADS)

Khrit, N. G.; Alghoul, M. A.; Sopian, K.; Lahimer, A. A.; Elayeb, O. K.

2017-11-01

Assessing outdoor human thermal comfort and urban climate quality require experimental investigation of microclimatic conditions and their variations in open urban spaces. For this, it is essential to provide quantitative information on air temperature, humidity, wind velocity and mean radiant temperature. These parameters can be quantified directly except mean radiant temperature (Tmrt). The most accurate method to quantify Tmrt is integral radiation measurements (3-D shortwave and long-wave) which require using expensive radiometer instruments. To overcome this limitation the well-known globe thermometer method was suggested to calculate Tmrt. The aim of this study was to assess the possibility of using indoor globe thermometer method in predicting outdoor mean radiant temperature under Malaysia tropical microclimate. Globe thermometer method using small and large sizes of black-painted copper globes (50mm, 150mm) were used to estimate Tmrt and compare it with the reference Tmrt estimated by integral radiation method. The results revealed that the globe thermometer method considerably overestimated Tmrt during the middle of the day and slightly underestimated it in the morning and late evening. The difference between the two methods was obvious when the amount of incoming solar radiation was high. The results also showed that the effect of globe size on the estimated Tmrt is mostly small. Though, the estimated Tmrt by the small globe showed a relatively large amount of scattering caused by rapid changes in radiation and wind speed.

Can Hall effect trigger Kelvin-Helmholtz instability in sub-Alfvénic flows?

NASA Astrophysics Data System (ADS)

Pandey, B. P.

2018-05-01

In the Hall magnetohydrodynamics, the onset condition of the Kelvin-Helmholtz instability is solely determined by the Hall effect and is independent of the nature of shear flows. In addition, the physical mechanism behind the super- and sub-Alfvénic flows becoming unstable is quite different: the high-frequency right circularly polarized whistler becomes unstable in the super-Alfvénic flows whereas low-frequency, left circularly polarized ion-cyclotron wave becomes unstable in the presence of sub-Alfvénic shear flows. The growth rate of the Kelvin-Helmholtz instability in the super-Alfvénic case is higher than the corresponding ideal magnetohydrodynamic rate. In the sub-Alfvénic case, the Hall effect opens up a new, hitherto inaccessible (to the magnetohydrodynamics) channel through which the partially or fully ionized fluid can become Kelvin-Helmholtz unstable. The instability growth rate in this case is smaller than the super-Alfvénic case owing to the smaller free shear energy content of the flow. When the Hall term is somewhat smaller than the advection term in the induction equation, the Hall effect is also responsible for the appearance of a new overstable mode whose growth rate is smaller than the purely growing Kelvin-Helmholtz mode. On the other hand, when the Hall diffusion dominates the advection term, the growth rate of the instability depends only on the Alfvén -Mach number and is independent of the Hall diffusion coefficient. Further, the growth rate in this case linearly increases with the Alfvén frequency with smaller slope for sub-Alfvénic flows.

In-situ technique for checking the calibration of platinum resistance thermometers

NASA Technical Reports Server (NTRS)

Daryabeigi, Kamran; Dillon-Townes, Lawrence A.

1987-01-01

The applicability of the self-heating technique for checking the calibration of platinum resistance thermometers located inside wind tunnels was investigated. This technique is based on a steady state measurement of resistance increase versus joule heating. This method was found to be undesirable, mainly because of the fluctuations of flow variables during any wind tunnel testing.

Correlation of Handheld Infrared Skin Thermometer and Infrared Videothermography Device for Measurement of Corneal Temperature.

PubMed

Oztas, Zafer; Barut Selver, Ozlem; Akkin, Cezmi; Canturk, Ecem; Afrashi, Filiz

2016-05-01

In our study, we aimed to investigate the correlation of handheld infrared skin thermometer and videothermography device for the measurement of corneal temperature. Forty healthy individuals (80 eyes) were enrolled to the study. Participants underwent a detailed ophthalmologic examination and medical history review for excluding any ocular and systemic diseases. The measurements of the central corneal temperature were performed in a room having constant temperature, humidity, and brightness levels. To avoid any variability, all the temperature measurements were performed in the same examination room by a single examiner. The temperature was measured with a handheld infrared skin thermometer (MEDISANA, FTN) from the corneal surface. The same instrument was also used to measure the subjects' body temperature. Moreover, the subjects underwent the corneal temperature measurement by a noncontact videothermography device (Optris PI 450; Optris GmbH). The male to female ratio was 19:21 among the subjects. The mean age was 25.1±4.7 years. The mean body temperature was 36.93±0.33°C. The mean corneal temperatures measured by the handheld infrared skin thermometer and the ocular videothermography device were 36.94±0.28°C and 35.61±0.61°C, respectively (P<0.01). The mean temperature difference was 1.34±0.57°C, with a 95% confidence interval. There was a moderate correlation between the corneal temperatures measured by the 2 devices in the right, the left eyes, and both eyes, respectively (P=0.450, 0.539, 0.490). Handheld infrared skin thermometers can be used for the evaluation of the corneal temperature. These devices may provide a simple, practical, and cheaper way to detect the corneal temperature, and the widely performed corneal temperature measurements may afford us to understand the temperature variability in numerous ocular conditions in a better way.

Tympanic ear thermometer assessment of body temperature among patients with cognitive disturbances. An acceptable and ethically desirable alternative?

PubMed

Aadal, Lena; Fog, Lisbet; Pedersen, Asger Roer

2016-12-01

Investigation of a possible relation between body temperature measurements by the current generation of tympanic ear and rectal thermometers. In Denmark, a national guideline recommends the rectal measurement. Subsequently, the rectal thermometers and tympanic ear devices are the most frequently used and first choice in Danish hospital wards. Cognitive changes constitute challenges with cooperating in rectal temperature assessments. With regard to diagnosing, ethics, safety and the patients' dignity, the tympanic ear thermometer might comprise a desirable alternative to rectal noninvasive measurement of body temperature during in-hospital-based neurorehabilitation. A prospective, descriptive cohort study. Consecutive inclusion of 27 patients. Linear regression models were used to analyse 284 simultaneous temperature measurements. Ethical approval for this study was granted by the Danish Data Protection Agency, and the study was completed in accordance with the Helsinki Declaration 2008. About 284 simultaneous rectal and ear temperature measurements on 27 patients were analysed. The patient-wise variability of measured temperatures was significantly higher for the ear measurements. Patient-wise linear regressions for the 25 patients with at least three pairs of simultaneous ear and rectal temperature measurements showed large interpatient variability of the association. A linear relationship between the rectal body temperature assessment and the temperature assessment employing the tympanic thermometer is weak. Both measuring methods reflect variance in temperature, but ear measurements showed larger variation. © 2016 Nordic College of Caring Science.

Ultra-high Resolution Coherent X-ray Imaging of Nano-Materials

NASA Astrophysics Data System (ADS)

Shapiro, David

A revolution is underway in the field of x-ray microscopy driven by the develop of experimental, theoretical and computational means of producing a complete description of coherent imaging systems from x-ray diffraction data. The methods being developed not only allow for full quantification and removal of all optical aberrations but also extension of the numerical aperture to the diffraction limit. One such method under intensive development is x-ray ptychography. This is a scanned probe method that reconstructs a scattering object and its illumination from coherent diffraction data. Within the first few years of development at the Advanced Light Source (ALS), Lawrence Berkeley National Laboratory, this method has already achieved the highest resolution x-ray images ever recorded in two, three and four dimensions. With the ability of x-rays to penetrate significantly more matter than electrons, their short wavelength and their sensitivity to chemical and magnetic states of matter, x-ray ptychography is set to revolutionize how we see the nano-scale world. In this presentation I will briefly describe the technical framework for how various methods work and will give a detailed account of a practical implementation at the ALS along with various scientific applications. The Advanced Light Source is supported by the Director, Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy under Contract No. DE-AC02-05CH11231.

Note: Sub-Kelvin refrigeration with dry-coolers on a rotating system.

PubMed

Oguri, S; Ishitsuka, H; Choi, J; Kawai, M; Tajima, O

2014-08-01

We developed a cryogenic system on a rotating table that achieves sub-Kelvin conditions. The cryogenic system consists of a helium sorption cooler and a pulse tube cooler in a cryostat mounted on a rotating table. Two rotary-joint connectors for electricity and helium gas circulation enable the coolers to be operated and maintained with ease. We performed cool-down tests under a condition of continuous rotation at 20 rpm. We obtained a temperature of 0.23 K with a holding time of more than 24 h, thus complying with catalog specifications. We monitored the system's performance for four weeks; two weeks with and without rotation. A few-percent difference in conditions was observed between these two states. Most applications can tolerate such a slight difference. The technology developed is useful for various scientific applications requiring sub-Kelvin conditions on rotating platforms.

Nano-liquid chromatography applied to enantiomers separation.

PubMed

Fanali, Salvatore

2017-02-24

This paper presents the state of the art concerning the separation of chiral compounds by means of nano-liquid chromatography (nano-LC). The enantiomers' separation and determination are a subject of fundamental importance in various application fields such as pharmaceutical industry, biomedicine, food, agrochemical etc. Nano-LC is a miniaturized chromatographic technique offering some advantages over conventional ones such as low consumption of mobile phase, sample volume and amount of chiral stationary phase, reduced costs etc. This is reported in the first part of the paper illustrating the features of the nano-LC. In addition, chiral resolution methods are briefly illustrated. Some chiral selectors, used in high-performance liquid chromatography have also been applied in nano-LC including cyclodextrins, glycopeptide antibiotics, modified polysaccharides etc. This is discussed in the second part of the review. Finally some examples of the applications available in literature are reported. Copyright © 2016 Elsevier B.V. All rights reserved.

Thermal conductance modeling and characterization of the SuperCDMS-SNOLAB sub-Kelvin cryogenic system

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dhuley, R. C.; Hollister, M. I.; Ruschman, M. K.

The detectors of the Super Cryogenic Dark Matter Search experiment at SNOLAB (SuperCDMS SNOLAB) will operate in a seven-layered cryostat with thermal stages between room temperature and the base temperature of 15 mK. The inner three layers of the cryostat, which are to be nominally maintained at 1 K, 250 mK, and 15 mK, will be cooled by a dilution refrigerator via conduction through long copper stems. Bolted and mechanically pressed contacts, at and cylindrical, as well as exible straps are the essential stem components that will facilitate assembly/dismantling of the cryostat. These will also allow for thermal contractions/movements duringmore » cooldown of the sub-Kelvin system. To ensure that these components and their contacts meet their design thermal conductance, prototypes were fabricated and cryogenically tested. The present paper gives an overview of the SuperCDMS SNOLAB sub-Kelvin architecture and its conductance requirements. Results from the conductance measurements tests and from sub-Kelvin thermal modeling are discussed.« less

Modeling Kelvin Wave Cascades in Superfluid Helium

NASA Astrophysics Data System (ADS)

Boffetta, G.; Celani, A.; Dezzani, D.; Laurie, J.; Nazarenko, S.

2009-09-01

We study two different types of simplified models for Kelvin wave turbulence on quantized vortex lines in superfluids near zero temperature. Our first model is obtained from a truncated expansion of the Local Induction Approximation (Truncated-LIA) and it is shown to possess the same scalings and the essential behaviour as the full Biot-Savart model, being much simpler than the later and, therefore, more amenable to theoretical and numerical investigations. The Truncated-LIA model supports six-wave interactions and dual cascades, which are clearly demonstrated via the direct numerical simulation of this model in the present paper. In particular, our simulations confirm presence of the weak turbulence regime and the theoretically predicted spectra for the direct energy cascade and the inverse wave action cascade. The second type of model we study, the Differential Approximation Model (DAM), takes a further drastic simplification by assuming locality of interactions in k-space via using a differential closure that preserves the main scalings of the Kelvin wave dynamics. DAMs are even more amenable to study and they form a useful tool by providing simple analytical solutions in the cases when extra physical effects are present, e.g. forcing by reconnections, friction dissipation and phonon radiation. We study these models numerically and test their theoretical predictions, in particular the formation of the stationary spectra, and closeness of numerics for the higher-order DAM to the analytical predictions for the lower-order DAM.

Subcritical Kelvin-Helmholtz instability in a Hele-Shaw cell.

PubMed

Meignin, L; Gondret, P; Ruyer-Quil, C; Rabaud, M

2003-06-13

We investigate experimentally the subcritical behavior of the Kelvin-Helmholtz instability for a gas-liquid shearing flow in a Hele-Shaw cell. The subcritical curve separating the solutions of a stable plane interface and a fully saturated nonlinear wave train is determined. Experimental results are fitted by a fifth order complex Ginzburg-Landau equation whose linear coefficients are compared to theoretical ones.

Broadband infrared vibrational nano-spectroscopy using thermal blackbody radiation

DOE PAGES

O’Callahan, Brian T.; Lewis, William E.; Möbius, Silke; ...

2015-12-03

Infrared vibrational nano-spectroscopy based on scattering scanning near-field optical microscopy (s-SNOM) provides intrinsic chemical specificity with nanometer spatial resolution. Here we use incoherent infrared radiation from a 1400 K thermal blackbody emitter for broadband infrared (IR) nano-spectroscopy.With optimized interferometric heterodyne signal amplification we achieve few-monolayer sensitivity in phonon polariton spectroscopy and attomolar molecular vibrational spectroscopy. Near-field localization and nanoscale spatial resolution is demonstrated in imaging flakes of hexagonal boron nitride (hBN) and determination of its phonon polariton dispersion relation. The signal-to-noise ratio calculations and analysis for different samples and illumination sources provide a reference for irradiance requirements and the attainablemore » near-field signal levels in s-SNOM in general. As a result, the use of a thermal emitter as an IR source thus opens s-SNOM for routine chemical FTIR nano-spectroscopy.« less

Broadband infrared vibrational nano-spectroscopy using thermal blackbody radiation

DOE Office of Scientific and Technical Information (OSTI.GOV)

O’Callahan, Brian T.; Lewis, William E.; Möbius, Silke

Infrared vibrational nano-spectroscopy based on scattering scanning near-field optical microscopy (s-SNOM) provides intrinsic chemical specificity with nanometer spatial resolution. Here we use incoherent infrared radiation from a 1400 K thermal blackbody emitter for broadband infrared (IR) nano-spectroscopy.With optimized interferometric heterodyne signal amplification we achieve few-monolayer sensitivity in phonon polariton spectroscopy and attomolar molecular vibrational spectroscopy. Near-field localization and nanoscale spatial resolution is demonstrated in imaging flakes of hexagonal boron nitride (hBN) and determination of its phonon polariton dispersion relation. The signal-to-noise ratio calculations and analysis for different samples and illumination sources provide a reference for irradiance requirements and the attainablemore » near-field signal levels in s-SNOM in general. As a result, the use of a thermal emitter as an IR source thus opens s-SNOM for routine chemical FTIR nano-spectroscopy.« less

[The test of medical service of the implementation of modern methods of prophylaxis of acute respiratory infection in the forces].

PubMed

Alimov, A V; Aminev, R M; Ustinov, A E; Matreninskaia, E S

2011-01-01

In the article are presented the technologies, regular usage of which let attain important decrease of the level of airborne infections in the period of epidemic. These technologies are noncontact infared thermometer "Kelvin-kompakt" 201 (M1), medication in aerosol packing "Bakteroks Mentol" for the air disinfection in small rooms (medical squadron, unauthorized sick-room), photocatalytic air disinfectant "Airlife".

Evaluating gyro-viscosity in the Kelvin-Helmholtz instability by kinetic simulations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Umeda, Takayuki, E-mail: taka.umeda@nagoya-u.jp; Yamauchi, Natsuki; Wada, Yasutaka

2016-05-15

In the present paper, the finite-Larmor-radius (gyro-viscous) term [K. V. Roberts and J. B. Taylor, Phys. Rev. Lett. 8, 197–198 (1962)] is evaluated by using a full kinetic Vlasov simulation result of the Kelvin-Helmholtz instability (KHI). The velocity field and the pressure tensor are calculated from the high-resolution data of the velocity distribution functions obtained by the Vlasov simulation, which are used to approximate the Finite-Larmor-Radius (FLR) term according to Roberts and Taylor [Phys. Rev. Lett. 8, 197–198 (1962)]. The direct comparison between the pressure tensor and the FLR term shows an agreement. It is also shown that the anisotropicmore » pressure gradient enhanced the linear growth of the KHI when the inner product between the vorticity of the primary velocity shear layer and the magnetic field is negative, which is consistent with the previous FLR-magnetohydrodynamic simulation result. This result suggests that it is not sufficient for reproducing the kinetic simulation result by fluid simulations to include the FLR term (or the pressure tensor) only in the equation of motion for fluid.« less

Nano-imaging enabled via self-assembly

PubMed Central

McLeod, Euan; Ozcan, Aydogan

2014-01-01

SUMMARY Imaging object details with length scales below approximately 200 nm has been historically difficult for conventional microscope objective lenses because of their inability to resolve features smaller than one-half the optical wavelength. Here we review some of the recent approaches to surpass this limit by harnessing self-assembly as a fabrication mechanism. Self-assembly can be used to form individual nano- and micro-lenses, as well as to form extended arrays of such lenses. These lenses have been shown to enable imaging with resolutions as small as 50 nm half-pitch using visible light, which is well below the Abbe diffraction limit. Furthermore, self-assembled nano-lenses can be used to boost contrast and signal levels from small nano-particles, enabling them to be detected relative to background noise. Finally, alternative nano-imaging applications of self-assembly are discussed, including three-dimensional imaging, enhanced coupling from light-emitting diodes, and the fabrication of contrast agents such as quantum dots and nanoparticles. PMID:25506387

Dual-mode self-validating resistance/Johnson noise thermometer system

DOEpatents

Shepard, Robert L.; Blalock, Theron V.; Roberts, Michael J.

1993-01-01

A dual-mode Johnson noise and DC resistance thermometer capable of use in control systems where prompt indications of temperature changes and long term accuracy are needed. A resistance-inductance-capacitance (RLC) tuned circuit produces a continuous voltage signal for Johnson noise temperature measurement. The RLC circuit provides a mean-squared noise voltage that depends only on the capacitance used and the temperature of the sensor. The sensor has four leads for simultaneous coupling to a noise signal processor and to a DC resistance signal processor.

Pore size distribution calculation from 1H NMR signal and N2 adsorption-desorption techniques

NASA Astrophysics Data System (ADS)

Hassan, Jamal

2012-09-01

The pore size distribution (PSD) of nano-material MCM-41 is determined using two different approaches: N2 adsorption-desorption and 1H NMR signal of water confined in silica nano-pores of MCM-41. The first approach is based on the recently modified Kelvin equation [J.V. Rocha, D. Barrera, K. Sapag, Top. Catal. 54(2011) 121-134] which deals with the known underestimation in pore size distribution for the mesoporous materials such as MCM-41 by introducing a correction factor to the classical Kelvin equation. The second method employs the Gibbs-Thompson equation, using NMR, for melting point depression of liquid in confined geometries. The result shows that both approaches give similar pore size distribution to some extent, and also the NMR technique can be considered as an alternative direct method to obtain quantitative results especially for mesoporous materials. The pore diameter estimated for the nano-material used in this study was about 35 and 38 Å for the modified Kelvin and NMR methods respectively. A comparison between these methods and the classical Kelvin equation is also presented.

Research Update: Nanoscale surface potential analysis of MoS2 field-effect transistors for biomolecular detection using Kelvin probe force microscopy

NASA Astrophysics Data System (ADS)

Kim, Min Hyung; Park, Heekyeong; Lee, Hyungbeen; Nam, Kihwan; Jeong, Seokhwan; Omkaram, Inturu; Yoon, Dae Sung; Lee, Sei Young; Kim, Sunkook; Lee, Sang Woo

2016-10-01

We used high-resolution Kelvin probe force microscopy (KPFM) to investigate the immobilization of a prostate specific antigen (PSA) antibody by measuring the surface potential (SP) on a MoS2 surface over an extensive concentration range (1 pg/ml-100 μg/ml). After PSA antibody immobilization, we demonstrated that the SP on the MoS2 surface characterized by KPFM strongly correlated to the electrical signal of a MoS2 bioFET. This demonstration can not only be used to optimize the immobilization conditions for captured molecules, but can also be applied as a diagnostic tool to complement the electrical detection of a MoS2 FET biosensor.

Sonic Thermometer for High-Altitude Balloons

NASA Technical Reports Server (NTRS)

Bognar, John

2012-01-01

The sonic thermometer is a specialized application of well-known sonic anemometer technology. Adaptations have been made to the circuit, including the addition of supporting sensors, which enable its use in the high-altitude environment and in non-air gas mixtures. There is a need to measure gas temperatures inside and outside of superpressure balloons that are flown at high altitudes. These measurements will allow the performance of the balloon to be modeled more accurately, leading to better flight performance. Small thermistors (solid-state temperature sensors) have been used for this general purpose, and for temperature measurements on radiosondes. A disadvantage to thermistors and other physical (as distinct from sonic) temperature sensors is that they are subject to solar heating errors when they are exposed to the Sun, and this leads to issues with their use in a very high-altitude environment

Virus scaffolds as enzyme nano-carriers.

PubMed

Cardinale, Daniela; Carette, Noëlle; Michon, Thierry

2012-07-01

The cooperative organization of enzymes by cells is a key feature for the efficiency of living systems. In the field of nanotechnologies, effort currently aims at mimicking this natural organization. Nanoscale resolution and high-registration alignment are necessary to control enzyme distribution in nano-containers or on the surface of solid supports. Virus capsid self-assembly is driven by precise supramolecular combinations of protein monomers, which have made them attractive building blocks to engineer enzyme nano-carriers (ENCs). We discuss some examples of what in our opinion constitute the latest advances in the use of plant viruses, bacteriophages and virus-like particles (VLPs) as nano-scaffolds for enzyme selection, enzyme confinement and patterning, phage therapy, raw material processing, and single molecule enzyme kinetics studies. Copyright © 2012 Elsevier Ltd. All rights reserved.

NanoSIMS Reveals New Structural and Elemental Signatures of Early Life

NASA Technical Reports Server (NTRS)

Oehler, Dorothy Z.; Mostefaoui, Smail; Meibom, Anders; Selo, Madeleine; Robert, Francois; McKay, David S.

2006-01-01

The young technology of NanoSIMS is unlocking new information from organic matter in ancient sediments. We have used this technique to characterize sub-micron scale element composition of Proterozoic organics that are clearly biogenic as a guide for interpreting problematic structures in terrestrial or extraterrestrial samples. We used the NanoSIMS 50 of the National Museum of Natural History in Paris to map carbon, nitrogen (as CN), and sulfur in organic structures from the approximately 0.8 Ga Bitter Springs Formation. We analyzed spheroidal and filamentous microfossils as well as organic laminae that appeared amorphous by optical and scanning electron microscopy. In clear-cut microfossils, a coincidence between optical images and NanoSIMS element maps suggests a biological origin for the mapped carbon, sulfur, and nitrogen; this conclusion is supported by high resolution NanoSIMS maps showing identical spatial distributions of C, CN and S. High resolution images also demonstrate distinctive nano structure of the filaments and spheroids. In the amorphous laminae, NanoSIMS reveals morphologies reminiscent of compressed microfossils. Distinct CN/C ratios of the spheroids, filaments, and laminae may reflect their biological precursors (cell walls, cyanobacterial sheaths, and microbial communities/biofilms, respectively). Similar amorphous laminae comprise a preponderance of the organic matter in many Precambrian deposits. Thus it is possible that NanoSIMS will provide fresh insight into a large body of previously uninterpretable material. Additionally, NanoSIMS analysis may establish new biosignatures that will be helpful for assessing the origin and biogenicity of controversial Archean structures and any organic materials that may occur in Martian or other extraterrestrial samples.

Convectively coupled Kelvin waves in aquachannel simulations: 2. Life cycle and dynamical-convective coupling

NASA Astrophysics Data System (ADS)

Blanco, Joaquín. E.; Nolan, David S.; Mapes, Brian E.

2016-10-01

This second part of a two-part study uses Weather Research and Forecasting simulations with aquachannel and aquapatch domains to investigate the time evolution of convectively coupled Kelvin waves (CCKWs). Power spectra, filtering, and compositing are combined with object-tracking methods to assess the structure and phase speed propagation of CCKWs during their strengthening, mature, and decaying phases. In this regard, we introduce an innovative approach to more closely investigate the wave (Kelvin) versus entity (super cloud cluster or "SCC") dualism. In general, the composite CCKW structures represent a dynamical response to the organized convective activity. However, pressure and thermodynamic fields in the boundary layer behave differently. Further analysis of the time evolution of pressure and low-level moist static energy finds that these fields propagate eastward as a "moist" Kelvin wave (MKW), faster than the envelope of organized convection or SCC. When the separation is sufficiently large the SCC dissipates, and a new SCC generates to the east, in the region of strongest negative pressure perturbations. We revisit the concept itself of the "coupling" between convection and dynamics, and we also propose a conceptual model for CCKWs, with a clear distinction between the SCC and the MKW components.

An International Intercomparison of Argon Triple Point Calibration Facilities, Accommodating Long-stem Thermometers

NASA Astrophysics Data System (ADS)

Bloembergen, P.; Bonnier, G.; Ronsin, H.

1990-01-01

Argon triple point calibration facilities have been compared among eight laboratories with one transfer system, employing local long-stem standard platinum resistance thermometers. The apparatus intercompared, included a sealed cell and its associated cryostat. As is evidenced by the results of long-term investigations, previously performed at the INM, cells of the type employed may show a triple-point temperature, which is stable within the reproducibility of the measurements (simeq0,1 mK) over a period of about 10 years. At each laboratory the mean difference between the Argon triple-point temperature of the transfer cell (t) and the local cell (i) has been determined, using a standard resistance thermometer previously calibrated at the fixed points, according to the IPTS-68; associated repeatabilities are typically of the order of 0,1 mK. The reproducibility attained by measuring the mean difference in different laboratories, using cells of the same type and origin (INM), amounts to 0,4 mK.

NanoXCT: a novel technique to probe the internal architecture of pharmaceutical particles.

PubMed

Wong, Jennifer; D'Sa, Dexter; Foley, Matthew; Chan, John Gar Yan; Chan, Hak-Kim

2014-11-01

To demonstrate the novel application of nano X-ray computed tomography (NanoXCT) for visualizing and quantifying the internal structures of pharmaceutical particles. An Xradia NanoXCT-100, which produces ultra high-resolution and non-destructive imaging that can be reconstructed in three-dimensions (3D), was used to characterize several pharmaceutical particles. Depending on the particle size of the sample, NanoXCT was operated in Zernike Phase Contrast (ZPC) mode using either: 1) large field of view (LFOV), which has a two-dimensional (2D) spatial resolution of 172 nm; or 2) high resolution (HRES) that has a resolution of 43.7 nm. Various pharmaceutical particles with different physicochemical properties were investigated, including raw (2-hydroxypropyl)-beta-cyclodextrin (HβCD), poly (lactic-co-glycolic) acid (PLGA) microparticles, and spray-dried particles that included smooth and nanomatrix bovine serum albumin (BSA), lipid-based carriers, and mannitol. Both raw HβCD and PLGA microparticles had a network of voids, whereas spray-dried smooth BSA and mannitol generally had a single void. Lipid-based carriers and nanomatrix BSA particles resulted in low quality images due to high noise-to-signal ratio. The quantitative capabilities of NanoXCT were also demonstrated where spray-dried mannitol was found to have an average void volume of 0.117 ± 0.247 μm(3) and average void-to-material percentage of 3.5%. The single PLGA particle had values of 1993 μm(3) and 59.3%, respectively. This study reports the first series of non-destructive 3D visualizations of inhalable pharmaceutical particles. Overall, NanoXCT presents a powerful tool to dissect and observe the interior of pharmaceutical particles, including those of a respirable size.

Equatorial waves in a stratospheric GCM: Effects of vertical resolution. [GCM (general circulation model)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Boville, B.A.; Randel, W.J.

1992-05-01

Equatorially trapped wave modes, such as Kelvin and mixed Rossby-gravity waves, are believed to play a crucial role in forcing the quasi-biennial oscillation (QBO) of the lower tropical stratosphere. This study examines the ability of a general circulation model (GCM) to simulate these waves and investigates the changes in the wave properties as a function of the vertical resolution of the model. The simulations produce a stratopause-level semiannual oscillation but not a QBO. An unfortunate property of the equatorially trapped waves is that they tend to have small vertical wavelengths ([le] 15 km). Some of the waves, believed to bemore » important in forcing the QBO, have wavelengths as short as 4 km. The short vertical wavelengths pose a stringent computational requirement for numerical models whose vertical grid spacing is typically chosen based on the requirements for simulating extratropical Rossby waves (which have much longer vertical wavelengths). This study examines the dependence of the equatorial wave simulation of vertical resolution using three experiments with vertical grid spacings of approximately 2.8, 1.4, and 0.7 km. Several Kelvin, mixed Rossby-gravity, and 0.7 km. Several Kelvin, mixed Rossby-gravity, and inertio-gravity waves are identified in the simulations. At high vertical resolution, the simulated waves are shown to correspond fairly well to the available observations. The properties of the relatively slow (and vertically short) waves believed to play a role in the QBO vary significantly with vertical resolution. Vertical grid spacings of about 1 km or less appear to be required to represent these waves adequately. The simulated wave amplitudes are at least as large as observed, and the waves are absorbed in the lower stratosphere, as required in order to force the QBO. However, the EP flux divergence associated with the waves is not sufficient to explain the zonal flow accelerations found in the QBO. 39 refs., 17 figs., 1 tab.« less

Pumping liquid metal at high temperatures up to 1,673 kelvin

NASA Astrophysics Data System (ADS)

Amy, C.; Budenstein, D.; Bagepalli, M.; England, D.; Deangelis, F.; Wilk, G.; Jarrett, C.; Kelsall, C.; Hirschey, J.; Wen, H.; Chavan, A.; Gilleland, B.; Yuan, C.; Chueh, W. C.; Sandhage, K. H.; Kawajiri, Y.; Henry, A.

2017-10-01

Heat is fundamental to power generation and many industrial processes, and is most useful at high temperatures because it can be converted more efficiently to other types of energy. However, efficient transportation, storage and conversion of heat at extreme temperatures (more than about 1,300 kelvin) is impractical for many applications. Liquid metals can be very effective media for transferring heat at high temperatures, but liquid-metal pumping has been limited by the corrosion of metal infrastructures. Here we demonstrate a ceramic, mechanical pump that can be used to continuously circulate liquid tin at temperatures of around 1,473-1,673 kelvin. Our approach to liquid-metal pumping is enabled by the use of ceramics for the mechanical and sealing components, but owing to the brittle nature of ceramics their use requires careful engineering. Our set-up enables effective heat transfer using a liquid at previously unattainable temperatures, and could be used for thermal storage and transport, electric power production, and chemical or materials processing.

Electron-beam induced nano-etching of suspended graphene

PubMed Central

Sommer, Benedikt; Sonntag, Jens; Ganczarczyk, Arkadius; Braam, Daniel; Prinz, Günther; Lorke, Axel; Geller, Martin

2015-01-01

Besides its interesting physical properties, graphene as a two-dimensional lattice of carbon atoms promises to realize devices with exceptional electronic properties, where freely suspended graphene without contact to any substrate is the ultimate, truly two-dimensional system. The practical realization of nano-devices from suspended graphene, however, relies heavily on finding a structuring method which is minimally invasive. Here, we report on the first electron beam-induced nano-etching of suspended graphene and demonstrate high-resolution etching down to ~7 nm for line-cuts into the monolayer graphene. We investigate the structural quality of the etched graphene layer using two-dimensional (2D) Raman maps and demonstrate its high electronic quality in a nano-device: A 25 nm-wide suspended graphene nanoribbon (GNR) that shows a transport gap with a corresponding energy of ~60 meV. This is an important step towards fast and reliable patterning of suspended graphene for future ballistic transport, nano-electronic and nano-mechanical devices. PMID:25586495

Full data acquisition in Kelvin Probe Force Microscopy: Mapping dynamic electric phenomena in real space.

PubMed

Collins, Liam; Belianinov, Alex; Somnath, Suhas; Balke, Nina; Kalinin, Sergei V; Jesse, Stephen

2016-08-12

Kelvin probe force microscopy (KPFM) has provided deep insights into the local electronic, ionic and electrochemical functionalities in a broad range of materials and devices. In classical KPFM, which utilizes heterodyne detection and closed loop bias feedback, the cantilever response is down-sampled to a single measurement of the contact potential difference (CPD) per pixel. This level of detail, however, is insufficient for materials and devices involving bias and time dependent electrochemical events; or at solid-liquid interfaces, where non-linear or lossy dielectrics are present. Here, we demonstrate direct recovery of the bias dependence of the electrostatic force at high temporal resolution using General acquisition Mode (G-Mode) KPFM. G-Mode KPFM utilizes high speed detection, compression, and storage of the raw cantilever deflection signal in its entirety at high sampling rates. We show how G-Mode KPFM can be used to capture nanoscale CPD and capacitance information with a temporal resolution much faster than the cantilever bandwidth, determined by the modulation frequency of the AC voltage. In this way, G-Mode KPFM offers a new paradigm to study dynamic electric phenomena in electroactive interfaces as well as a promising route to extend KPFM to the solid-liquid interface.

Magnetic moment of solar plasma and the Kelvin force: -The driving force of plasma up-flow -

NASA Astrophysics Data System (ADS)

Shibasaki, Kiyoto

2017-04-01

Thermal plasma in the solar atmosphere is magnetized (diamagnetic). The magnetic moment does not disappear by collisions because complete gyration is not a necessary condition to have magnetic moment. Magnetized fluid is subjected to Kelvin force in non-uniform magnetic field. Generally, magnetic field strength decreases upwards in the solar atmosphere, hence the Kelvin force is directed upwards along the field. This force is not included in the fluid treatment of MHD. By adding the Kelvin force to the MHD equation of motion, we can expect temperature dependent plasma flows along the field which are reported by many observations. The temperature dependence of the flow speed is explained by temperature dependence of magnetic moment. From the observed parameters, we can infer physical parameters in the solar atmosphere such as scale length of the magnetic field strength and the friction force acting on the flowing plasma. In case of closed magnetic field lines, loop-top concentration of hot plasma is expected which is frequently observed.

Superconducting Effects in Optimization of Magnetic Penetration Thermometers for X-ray Microcalorimeters

NASA Technical Reports Server (NTRS)

Stevenson, Thomas R.; Balvin, M. A.; Denis, K. L.; Hsieh, W.-T.; Sadleir, J. E.; Bandler, Simon E.; Busch, Sarah E.; Merrell, W.; Kelly, Daniel P.; Nagler, Peter C.;

Science, Technology and Society--An Authentic Exploration of IR Thermometers Application in Schools

ERIC Educational Resources Information Center

Tse, Isaac Pak Hoi; Leung, Winston Kwok Kuen; Chan, Shing Yi

2004-01-01

"Science, Technology and Society" was identified an essential strand in the new Science Education curriculum guide. Shortly after the severe acute respiratory syndrome (SARS) threat to Hong Kong technical dealers introduced Infrared non-contact thermometers as a solution for schools to measure body temperature for a large number of…

Kelvin-Helmholtz instability of the Dirac fluid of charge carriers on graphene

NASA Astrophysics Data System (ADS)

Coelho, Rodrigo C. V.; Mendoza, Miller; Doria, Mauro M.; Herrmann, Hans J.

2017-11-01

We provide numerical evidence that a Kelvin-Helmholtz instability occurs in the Dirac fluid of electrons in graphene and can be detected in current experiments. This instability appears for electrons in the viscous regime passing though a micrometer-scale obstacle and affects measurements on the time scale of nanoseconds. A possible realization with a needle-shaped obstacle is proposed to produce and detect this instability by measuring the electric potential difference between contact points located before and after the obstacle. We also show that, for our setup, the Kelvin-Helmholtz instability leads to the formation of whirlpools similar to the ones reported in Bandurin et al. [Science 351, 1055 (2016), 10.1126/science.aad0201]. To perform the simulations, we develop a lattice Boltzmann method able to recover the full dissipation in a fluid of massless particles.

A Nano-indentation Identification Technique for Viscoelastic Constitutive Characteristics of Periodontal Ligaments

PubMed Central

Ashrafi, H.; Shariyat, M.

2016-01-01

Introduction Nano-indentation has recently been employed as a powerful tool for determining the mechanical properties of biological tissues on nano and micro scales. A majority of soft biological tissues such as ligaments and tendons exhibit viscoelastic or time-dependent behaviors. The constitutive characterization of soft tissues is among very important subjects in clinical medicine and especially, biomechanics fields. Periodontal ligament plays an important role in initiating tooth movement when loads are applied to teeth with orthodontic appliances. It is also the most accessible ligament in human body as it can be directly manipulated without any surgical intervention. From a mechanical point of view, this ligament can be considered as a thin interface made by a solid phase, consisting mainly of collagen fibers, which is immersed into a so-called ground substance. However, the viscoelastic constitutive effects of biological tissues are seldom considered rigorous during Nano-indentation tests. Methods In the present paper, a mathematical contact approach is developed to enable determining creep compliance and relaxation modulus of distinct periodontal ligaments, using constant–rate indentation and loading time histories, respectively. An adequate curve-fitting method is presented to determine these characteristics based on the Nano-indentation of rigid Berkovich tips. Generalized Voigt-Kelvin and Wiechert models are used to model constitutive equations of periodontal ligaments, in which the relaxation and creep functions are represented by series of decaying exponential functions of time. Results Time-dependent creep compliance and relaxation function have been obtained for tissue specimens of periodontal ligaments. Conclusion To improve accuracy, relaxation and creep moduli are measured from two tests separately. Stress relaxation effects appear more rapidly than creep in the periodontal ligaments. PMID:27672630

A Nano-indentation Identification Technique for Viscoelastic Constitutive Characteristics of Periodontal Ligaments.

PubMed

Ashrafi, H; Shariyat, M

2016-06-01

Nano-indentation has recently been employed as a powerful tool for determining the mechanical properties of biological tissues on nano and micro scales. A majority of soft biological tissues such as ligaments and tendons exhibit viscoelastic or time-dependent behaviors. The constitutive characterization of soft tissues is among very important subjects in clinical medicine and especially, biomechanics fields. Periodontal ligament plays an important role in initiating tooth movement when loads are applied to teeth with orthodontic appliances. It is also the most accessible ligament in human body as it can be directly manipulated without any surgical intervention. From a mechanical point of view, this ligament can be considered as a thin interface made by a solid phase, consisting mainly of collagen fibers, which is immersed into a so-called ground substance. However, the viscoelastic constitutive effects of biological tissues are seldom considered rigorous during Nano-indentation tests. In the present paper, a mathematical contact approach is developed to enable determining creep compliance and relaxation modulus of distinct periodontal ligaments, using constant-rate indentation and loading time histories, respectively. An adequate curve-fitting method is presented to determine these characteristics based on the Nano-indentation of rigid Berkovich tips. Generalized Voigt-Kelvin and Wiechert models are used to model constitutive equations of periodontal ligaments, in which the relaxation and creep functions are represented by series of decaying exponential functions of time. Time-dependent creep compliance and relaxation function have been obtained for tissue specimens of periodontal ligaments. To improve accuracy, relaxation and creep moduli are measured from two tests separately. Stress relaxation effects appear more rapidly than creep in the periodontal ligaments.

Magnetic bead detection using nano-transformers.

PubMed

Kim, Hyung Kwon; Hwang, Jong Seung; Hwang, Sung Woo; Ahn, Doyeol

2010-11-19

A novel scheme to detect magnetic beads using a nano-scale transformer with a femtoweber resolution is reported. We have performed a Faraday's induction experiment with the nano-transformer at room temperature. The transformer shows the linear output voltage responses to the sinusoidal input current. When magnetic beads are placed on the transformer, the output responses are increased by an amount corresponding to the added magnetic flux from the beads when compared with the case of no beads on the transformer. In this way, we could determine whether magnetic beads are on top of the transformer in a single particle level.

El Ni?o Pumping Up, Warm Kelvin Wave Surges Toward South America

NASA Image and Video Library

2009-11-12

ElNi?o is experiencing a late-fall resurgence. Sea-level height data from the NASA/European Ocean Surface Topography Mission/Jason-2 oceanography satellite show the equatorial Pacific has triggered a wave of warm water, known as a Kelvin wave.

El Niño Surges; Warm Kelvin Wave Headed for South America

NASA Image and Video Library

2009-12-17

The most recent sea-level height data from the NASA/European Ocean Surface Topography Mission/Jason-2 oceanography satellite show the continued eastward progression of a strong wave of warm water, known as a Kelvin wave, now approaching South America.

Assessing the role of the Kelvin-Helmholtz instability at the QCD cosmological transition

NASA Astrophysics Data System (ADS)

Mourão Roque, V. R. C.; Lugones, G.

2018-03-01

We performed numerical simulations with the PLUTO code in order to analyze the non-linear behavior of the Kelvin-Helmholtz instability in non-magnetized relativistic fluids. The relevance of the instability at the cosmological QCD phase transition was explored using an equation of state based on lattice QCD results with the addition of leptons. The results of the simulations were compared with the theoretical predictions of the linearized theory. For small Mach numbers up to Ms ~ 0.1 we find that both results are in good agreement. However, for higher Mach numbers, non-linear effects are significant. In particular, many initial conditions that look stable according to the linear analysis are shown to be unstable according to the full calculation. Since according to lattice calculations the cosmological QCD transition is a smooth crossover, violent fluid motions are not expected. Thus, in order to assess the role of the Kelvin-Helmholtz instability at the QCD epoch, we focus on simulations with low shear velocity and use monochromatic as well as random perturbations to trigger the instability. We find that the Kelvin-Helmholtz instability can strongly amplify turbulence in the primordial plasma and as a consequence it may increase the amount of primordial gravitational radiation. Such turbulence may be relevant for the evolution of the Universe at later stages and may have an impact in the stochastic gravitational wave background.

On-and-off chip cooling of a Coulomb blockade thermometer down to 2.8 mK

NASA Astrophysics Data System (ADS)

Palma, M.; Scheller, C. P.; Maradan, D.; Feshchenko, A. V.; Meschke, M.; Zumbühl, D. M.

2017-12-01

Cooling nanoelectronic devices below 10 mK is a great challenge since thermal conductivities become very small, thus creating a pronounced sensitivity to heat leaks. Here, we overcome these difficulties by using adiabatic demagnetization of both the electronic leads and the large metallic islands of a Coulomb blockade thermometer. This reduces the external heat leak through the leads and also provides on-chip refrigeration, together cooling the thermometer down to 2.8 ± 0.1 mK. We present a thermal model which gives a good qualitative account and suggests that the main limitation is heating due to pulse tube vibrations. With better decoupling, temperatures below 1 mK should be within reach, thus opening the door for μK nanoelectronics.

Ferromagnetic-Insulator-Based Superconducting Junctions as Sensitive Electron Thermometers

NASA Astrophysics Data System (ADS)

Giazotto, F.; Solinas, P.; Braggio, A.; Bergeret, F. S.

2015-10-01

We present an exhaustive theoretical analysis of charge and thermoelectric transport in a normal-metal-ferromagnetic-insulator-superconductor junction and explore the possibility of its use as a sensitive thermometer. We investigate the transfer functions and the intrinsic noise performance for different measurement configurations. A common feature of all configurations is that the best temperature-noise performance is obtained in the nonlinear temperature regime for a structure based on an Europium chalcogenide ferromagnetic insulator in contact with a superconducting Al film structure. For an open-circuit configuration, although the maximal intrinsic temperature sensitivity can achieve 10 nK Hz-1 /2 , a realistic amplifying chain will reduce the sensitivity up to 10 μ K Hz-1 /2 . To overcome this limitation, we propose a measurement scheme in a closed-circuit configuration based on state-of-the-art superconducting-quantum-interference-device detection technology in an inductive setup. In such a case, we show that temperature-noise can be as low as 35 nK Hz-1 /2 . We also discuss a temperature-to-frequency converter where the obtained thermovoltage developed over a Josephson junction operated in the dissipative regime is converted into a high-frequency signal. We predict that the structure can generate frequencies up to approximately 120 GHz and transfer functions up to 200 GHz /K at around 1 K. If operated as an electron thermometer, the device may provide temperature-noise lower than 35 nK Hz-1 /2 thereby being potentially attractive for radiation-sensing applications.

Magnetic Reconnection and the Kelvin-Helmholtz Instability

NASA Astrophysics Data System (ADS)

Knoll, D. A.; Chacon, L.; Brackbill, J. U.; Lapenta, G.

2002-11-01

Results are presented from a continuing study of magnetic reconnection caused by the evolution of a Kelvin-Helmholtz instability. To date we have studied 3-D compressible, subsonic and and sub-Alfvenic flow, with differential rotation (a gradient in vorticity parallel to the initial magnetic field) [1,2], as well as 2-D incompressible super-Alfvenic flow [3]. In both cases localized transient reconnection is observed on the Kelvin-Helmholtz time scale, and results indicate that the observed reconnection rate is insensitive to resistivity. In the present study we extend both the 2-D and the 3-D results found in [1,2,3]. In the extension of the 2-D work we focus on the fundamental differences in the nonlinear evolution of a low S simulation (S = 200) and a higher S simulation (S = 10,000). In the 3-D work we study the effects of a density discontinuity (present in [1] and not in [2]), along with study the effects of initial curved field lines in the absence of differential rotation. This basic plasma physics problem has possible application to dayside magnetosphere reconnection as a theoretical model for flux transfer events [1]. The general problem also has possible application to solar physics as it could provide a trigger mechanism for some class of coronal mass ejections. Both applications will be briefly discussed. [1] J.U. Brackbill and D.A. Knoll, Phys. Rev. Lett., vol. 86 (2001). [2] D.A. Knoll and J.U. Brackbill, Physics of Plasmas, to appear (2002) [3] D.A. Knoll and L. Chacon, Phys. Rev. Lett., vol. 88 (2002).

Epitaxial growth of pentacene on alkali halide surfaces studied by Kelvin probe force microscopy.

PubMed

Neff, Julia L; Milde, Peter; León, Carmen Pérez; Kundrat, Matthew D; Eng, Lukas M; Jacob, Christoph R; Hoffmann-Vogel, Regina

2014-04-22

In the field of molecular electronics, thin films of molecules adsorbed on insulating surfaces are used as the functional building blocks of electronic devices. Control of the structural and electronic properties of the thin films is required for reliably operating devices. Here, noncontact atomic force and Kelvin probe force microscopies have been used to investigate the growth and electrostatic landscape of pentacene on KBr(001) and KCl(001) surfaces. We have found that, together with molecular islands of upright standing pentacene, a new phase of tilted molecules appears near step edges on KBr. Local contact potential differences (LCPD) have been studied with both Kelvin experiments and density functional theory calculations. Our images reveal that differently oriented molecules display different LCPD and that their value is independent of the number of molecular layers. These results point to the formation of an interface dipole, which may be explained by a partial charge transfer from the pentacene to the surface. Moreover, the monitoring of the evolution of the pentacene islands shows that they are strongly affected by dewetting: Multilayers build up at the expense of monolayers, and in the Kelvin images, previously unknown line defects appear, which reveal the epitaxial growth of pentacene crystals.

Clinical accuracy of non-contact infrared thermometer from umbilical region in children: A new side.

PubMed

Apa, Hurşit; Gözmen, Salih; Keskin-Gözmen, Şükran; Aslan, Fatma; Bayram, Nuri; Devrim, İlker

2016-01-01

Measurement from axillary site with digital thermometer has been accepted as the most accurate method. But this method is time consuming. Tympanic and forehead measurements are often used but don't always seem to be more appropriate. Another site, umbilical region, could be an alternative site. This study aims to compare the measurements with axillary digital thermometer and non-contact infrared thermometers at sites from umbilicus and forehead to determine whether umbilical site could be used accurately in children. For each method, 2,048 measurements in total were performed. Using axillary method as gold standard, with a cut-off temperature of 38oC, the sensitivities and specificities, positive and negative predictive values of umbilical and forehead temperatures and area under the ROC curve were determined in non obese children. There was a significant positive correlation between axillary and umbilical temperatures with a correlation coefficient of 0.78. The average difference between the mean of both axillary and umbilical temperatures was -0.47 ± 0.65°C. The Bland-Altman plot showed good accuracy with only 2.5 % of the readings falling outside the 95% level of confidence. Umbilical measurements showed sensitivity of 71.7% and specificity of 95.8%. The area under the ROC curve was 0.93. The easy application may lead noncontact measurements from umbilicus site to be the preferable method for health care providers, but agreement limits mentioned in this study should be considered.

Observations of Equatorial Kelvin Waves and their Convective Coupling with the Atmosphere/Ocean Surface Layer

NASA Astrophysics Data System (ADS)

Conry, Patrick; Fernando, H. J. S.; Leo, Laura; Blomquist, Byron; Amelie, Vincent; Lalande, Nelson; Creegan, Ed; Hocut, Chris; MacCall, Ben; Wang, Yansen; Jinadasa, S. U. P.; Wang, Chien; Yeo, Lik-Khian

2016-11-01

Intraseasonal disturbances with their genesis in the equatorial Indian Ocean (IO) are an important component of global climate. The disturbances, which include Madden-Julian Oscillation and equatorial Kelvin and Rossby waves in the atmosphere and ocean, carry energy which affects El Niño, cyclogenesis, and monsoons. A recent field experiment in IO (ASIRI-RAWI) observed disturbances at three sites across IO with arrays of instruments probing from surface layer to lower stratosphere. During the field campaign the most pronounced planetary-scale disturbances were Kelvin waves in tropical tropopause layer. In Seychelles, quasi-biweekly westerly wind bursts were documented and linked to the Kelvin waves aloft, which breakdown in the upper troposphere due to internal shear instabilities. Convective coupling between waves' phase in upper troposphere and surface initiates rapid (turbulent) vertical transport and resultant wind bursts at surface. Such phenomena reveal linkages between planetary-scale waves and small-scale turbulence in the surface layer that can affect air-sea property exchanges and should be parameterized in atmosphere-ocean general circulation models. Funded by ONR Grants N00014-14-1-0279 and N00014-13-1-0199.

Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams.

PubMed

Coquelle, Nicolas; Brewster, Aaron S; Kapp, Ulrike; Shilova, Anastasya; Weinhausen, Britta; Burghammer, Manfred; Colletier, Jacques Philippe

2015-05-01

High-resolution structural information was obtained from lysozyme microcrystals (20 µm in the largest dimension) using raster-scanning serial protein crystallography on micro- and nano-focused beamlines at the ESRF. Data were collected at room temperature (RT) from crystals sandwiched between two silicon nitride wafers, thereby preventing their drying, while limiting background scattering and sample consumption. In order to identify crystal hits, new multi-processing and GUI-driven Python-based pre-analysis software was developed, named NanoPeakCell, that was able to read data from a variety of crystallographic image formats. Further data processing was carried out using CrystFEL, and the resultant structures were refined to 1.7 Å resolution. The data demonstrate the feasibility of RT raster-scanning serial micro- and nano-protein crystallography at synchrotrons and validate it as an alternative approach for the collection of high-resolution structural data from micro-sized crystals. Advantages of the proposed approach are its thriftiness, its handling-free nature, the reduced amount of sample required, the adjustable hit rate, the high indexing rate and the minimization of background scattering.

Report on AFRIMETS supplementary comparison: platinum resistance thermometer and digital thermometer calibrations against ITS-90 over the range -50 °C to 450 °C (AFRIMETS.T-S1)

NASA Astrophysics Data System (ADS)

Liedberg, Hans; Abdelaziz, Yasser; Tesfaye, Fitsum; Egadwa, Wilson; Norranim, Uthai; Rwashana, Simon; Kagoma, Alphonce; Ziagi, Adam; Kwong, Christian Ng Ha; Madeleine, Gilbert

2017-01-01

A Regional Metrology Organization (RMO) supplementary comparison of platinum resistance thermometer and digital thermometer (AFRIMETS.T-S1) was carried out by the National Metrology Institute of South Africa (NMISA), National Institute for Standards Egypt (NIS), National Metrology Institute of Ethiopia (NMIE), Kenya Bureau of Standards (KEBS), National Institute of Metrology Thailand (NIMT), Uganda National Bureau of Standards (UNBS), Tanzania Bureau of Standards (TBS), Mauritius Standards Bureau (MSB) and Seychelles Bureau of Standards (SBS) between March 2008 and October 2010. The temperature range of the inter comparison is -50 °C to 450 °C. The results of this comparison are reported here, along with descriptions of the Artefacts and devices used during measurement. This report also presents the uncertainty budget. The results are analysed and normalized error (En) values are reported. Main text To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCT, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).

Evaluation tests of platinum resistance thermometers for a cryogenic wind tunnel application

NASA Technical Reports Server (NTRS)

Germain, E. F.; Compton, E. C.

1984-01-01

Thirty-one commercially designed platinum resistance thermometers were evaluated for applicability to stagnation temperature measurements between -190 C and +65 C in the Langley Research Center's National Transonic Facility. Evaluation tests included X-ray shadowgraphs, calibrations before and after aging, and time constant measurements. Two wire-wound low thermal mass probes of a conventional design were chosen as most suitable for this cryogenic wind tunnel application.

Fractional Generalizations of Maxwell and Kelvin-Voigt Models for Biopolymer Characterization

PubMed Central

Jóźwiak, Bertrand; Orczykowska, Magdalena; Dziubiński, Marek

2015-01-01

The paper proposes a fractional generalization of the Maxwell and Kelvin-Voigt rheological models for a description of dynamic behavior of biopolymer materials. It was found that the rheological models of Maxwell-type do not work in the case of modeling of viscoelastic solids, and the model which significantly better describes the nature of changes in rheological properties of such media is the modified fractional Kelvin-Voigt model with two built-in springpots (MFKVM2). The proposed model was used to describe the experimental data from the oscillatory and creep tests of 3% (w/v) kuzu starch pastes, and to determine the values of their rheological parameters as a function of pasting time. These parameters provide a lot of additional information about structure and viscoelastic properties of the medium in comparison to the classical analysis of dynamic curves G’ and G” and shear creep compliance J(t). It allowed for a comprehensive description of a wide range of properties of kuzu starch pastes, depending on the conditions of pasting process. PMID:26599756

Nano-technology and nano-toxicology.

PubMed

Maynard, Robert L

2012-01-01

Rapid developments in nano-technology are likely to confer significant benefits on mankind. But, as with perhaps all new technologies, these benefits are likely to be accompanied by risks, perhaps by new risks. Nano-toxicology is developing in parallel with nano-technology and seeks to define the hazards and risks associated with nano-materials: only when risks have been identified they can be controlled. This article discusses the reasons for concern about the potential effects on health of exposure to nano-materials and relates these to the evidence of the effects on health of the ambient aerosol. A number of hypotheses are proposed and the dangers of adopting unsubstantiated hypotheses are stressed. Nano-toxicology presents many challenges and will need substantial financial support if it is to develop at a rate sufficient to cope with developments in nano-technology.

Nano-technology and nano-toxicology

PubMed Central

Maynard, Robert L.

2012-01-01

Rapid developments in nano-technology are likely to confer significant benefits on mankind. But, as with perhaps all new technologies, these benefits are likely to be accompanied by risks, perhaps by new risks. Nano-toxicology is developing in parallel with nano-technology and seeks to define the hazards and risks associated with nano-materials: only when risks have been identified they can be controlled. This article discusses the reasons for concern about the potential effects on health of exposure to nano-materials and relates these to the evidence of the effects on health of the ambient aerosol. A number of hypotheses are proposed and the dangers of adopting unsubstantiated hypotheses are stressed. Nano-toxicology presents many challenges and will need substantial financial support if it is to develop at a rate sufficient to cope with developments in nano-technology. PMID:22662021

Dual-sensing porphyrin-containing copolymer nanosensor as full-spectrum colorimeter and ultra-sensitive thermometer.

PubMed

Yan, Qiang; Yuan, Jinying; Kang, Yan; Cai, Zhinan; Zhou, Lilin; Yin, Yingwu

2010-04-28

A porphyrin-containing copolymer has dual-sensing in response to metal ions and temperature as a novel nanosensor. Triggered by ions, the sensor exhibits full-color tunable behavior as a cationic detector and colorimeter. Responding to temperature, the sensor displays an "isothermal" thermochromic point as an ultra-sensitive thermometer.

Cross-Sectional Investigations on Epitaxial Silicon Solar Cells by Kelvin and Conducting Probe Atomic Force Microscopy: Effect of Illumination.

PubMed

Narchi, Paul; Alvarez, Jose; Chrétien, Pascal; Picardi, Gennaro; Cariou, Romain; Foldyna, Martin; Prod'homme, Patricia; Kleider, Jean-Paul; I Cabarrocas, Pere Roca

2016-12-01

Both surface photovoltage and photocurrent enable to assess the effect of visible light illumination on the electrical behavior of a solar cell. We report on photovoltage and photocurrent measurements with nanometer scale resolution performed on the cross section of an epitaxial crystalline silicon solar cell, using respectively Kelvin probe force microscopy and conducting probe atomic force microscopy. Even though two different setups are used, the scans were performed on locations within 100-μm distance in order to compare data from the same area and provide a consistent interpretation. In both measurements, modifications under illumination are observed in accordance with the theory of PIN junctions. Moreover, an unintentional doping during the deposition of the epitaxial silicon intrinsic layer in the solar cell is suggested from the comparison between photovoltage and photocurrent measurements.

Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams

DOE Office of Scientific and Technical Information (OSTI.GOV)

Coquelle, Nicolas; CNRS, IBS, 38044 Grenoble; CEA, IBS, 38044 Grenoble

A raster scanning serial protein crystallography approach is presented, that consumes as low ∼200–700 nl of sedimented crystals. New serial data pre-analysis software, NanoPeakCell, is introduced. High-resolution structural information was obtained from lysozyme microcrystals (20 µm in the largest dimension) using raster-scanning serial protein crystallography on micro- and nano-focused beamlines at the ESRF. Data were collected at room temperature (RT) from crystals sandwiched between two silicon nitride wafers, thereby preventing their drying, while limiting background scattering and sample consumption. In order to identify crystal hits, new multi-processing and GUI-driven Python-based pre-analysis software was developed, named NanoPeakCell, that was able tomore » read data from a variety of crystallographic image formats. Further data processing was carried out using CrystFEL, and the resultant structures were refined to 1.7 Å resolution. The data demonstrate the feasibility of RT raster-scanning serial micro- and nano-protein crystallography at synchrotrons and validate it as an alternative approach for the collection of high-resolution structural data from micro-sized crystals. Advantages of the proposed approach are its thriftiness, its handling-free nature, the reduced amount of sample required, the adjustable hit rate, the high indexing rate and the minimization of background scattering.« less

Artifacts in time-resolved Kelvin probe force microscopy

DOE PAGES

Sadewasser, Sascha; Nicoara, Nicoleta; Solares, Santiago D.

2018-04-24

Kelvin probe force microscopy (KPFM) has been used for the characterization of metals, insulators, and semiconducting materials on the nanometer scale. Especially in semiconductors, the charge dynamics are of high interest. Recently, several techniques for time-resolved measurements with time resolution down to picoseconds have been developed, many times using a modulated excitation signal, e.g. light modulation or bias modulation that induces changes in the charge carrier distribution. For fast modulation frequencies, the KPFM controller measures an average surface potential, which contains information about the involved charge carrier dynamics. Here, we show that such measurements are prone to artifacts due tomore » frequency mixing, by performing numerical dynamics simulations of the cantilever oscillation in KPFM subjected to a bias-modulated signal. For square bias pulses, the resulting time-dependent electrostatic forces are very complex and result in intricate mixing of frequencies that may, in some cases, have a component at the detection frequency, leading to falsified KPFM measurements. Additionally, we performed fast Fourier transform (FFT) analyses that match the results of the numerical dynamics simulations. Small differences are observed that can be attributed to transients and higher-order Fourier components, as a consequence of the intricate nature of the cantilever driving forces. These results are corroborated by experimental measurements on a model system. In the experimental case, additional artifacts are observed due to constructive or destructive interference of the bias modulation with the cantilever oscillation. Also, in the case of light modulation, we demonstrate artifacts due to unwanted illumination of the photodetector of the beam deflection detection system. Lastly, guidelines for avoiding such artifacts are given.« less

Artifacts in time-resolved Kelvin probe force microscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sadewasser, Sascha; Nicoara, Nicoleta; Solares, Santiago D.

Kelvin probe force microscopy (KPFM) has been used for the characterization of metals, insulators, and semiconducting materials on the nanometer scale. Especially in semiconductors, the charge dynamics are of high interest. Recently, several techniques for time-resolved measurements with time resolution down to picoseconds have been developed, many times using a modulated excitation signal, e.g. light modulation or bias modulation that induces changes in the charge carrier distribution. For fast modulation frequencies, the KPFM controller measures an average surface potential, which contains information about the involved charge carrier dynamics. Here, we show that such measurements are prone to artifacts due tomore » frequency mixing, by performing numerical dynamics simulations of the cantilever oscillation in KPFM subjected to a bias-modulated signal. For square bias pulses, the resulting time-dependent electrostatic forces are very complex and result in intricate mixing of frequencies that may, in some cases, have a component at the detection frequency, leading to falsified KPFM measurements. Additionally, we performed fast Fourier transform (FFT) analyses that match the results of the numerical dynamics simulations. Small differences are observed that can be attributed to transients and higher-order Fourier components, as a consequence of the intricate nature of the cantilever driving forces. These results are corroborated by experimental measurements on a model system. In the experimental case, additional artifacts are observed due to constructive or destructive interference of the bias modulation with the cantilever oscillation. Also, in the case of light modulation, we demonstrate artifacts due to unwanted illumination of the photodetector of the beam deflection detection system. Lastly, guidelines for avoiding such artifacts are given.« less

Full-field x-ray nano-imaging at SSRF

NASA Astrophysics Data System (ADS)

Deng, Biao; Ren, Yuqi; Wang, Yudan; Du, Guohao; Xie, Honglan; Xiao, Tiqiao

2013-09-01

Full field X-ray nano-imaging focusing on material science is under developing at SSRF. A dedicated full field X-ray nano-imaging beamline based on bending magnet will be built in the SSRF phase-II project. The beamline aims at the 3D imaging of the nano-scale inner structures. The photon energy range is of 5-14keV. The design goals with the field of view (FOV) of 20μm and a spatial resolution of 20nm are proposed at 8 keV, taking a Fresnel zone plate (FZP) with outermost zone width of 25 nm. Futhermore, an X-ray nano-imaging microscope is under developing at the SSRF BL13W beamline, in which a larger FOV will be emphasized. This microscope is based on a beam shaper and a zone plate using both absorption contrast and Zernike phase contrast, with the optimized energy set to 10keV. The detailed design and the progress of the project will be introduced.

Kelvin probe microscopy and electronic transport measurements in reduced graphene oxide chemical sensors

NASA Astrophysics Data System (ADS)

Kehayias, Christopher E.; MacNaughton, Samuel; Sonkusale, Sameer; Staii, Cristian

2013-06-01

Reduced graphene oxide (RGO) is an electronically hybrid material that displays remarkable chemical sensing properties. Here, we present a quantitative analysis of the chemical gating effects in RGO-based chemical sensors. The gas sensing devices are patterned in a field-effect transistor geometry, by dielectrophoretic assembly of RGO platelets between gold electrodes deposited on SiO2/Si substrates. We show that these sensors display highly selective and reversible responses to the measured analytes, as well as fast response and recovery times (tens of seconds). We use combined electronic transport/Kelvin probe microscopy measurements to quantify the amount of charge transferred to RGO due to chemical doping when the device is exposed to electron-acceptor (acetone) and electron-donor (ammonia) analytes. We demonstrate that this method allows us to obtain high-resolution maps of the surface potential and local charge distribution both before and after chemical doping, to identify local gate-susceptible areas on the RGO surface, and to directly extract the contact resistance between the RGO and the metallic electrodes. The method presented is general, suggesting that these results have important implications for building graphene and other nanomaterial-based chemical sensors.

Kelvin probe microscopy and electronic transport measurements in reduced graphene oxide chemical sensors.

PubMed

Kehayias, Christopher E; MacNaughton, Samuel; Sonkusale, Sameer; Staii, Cristian

2013-06-21

Reduced graphene oxide (RGO) is an electronically hybrid material that displays remarkable chemical sensing properties. Here, we present a quantitative analysis of the chemical gating effects in RGO-based chemical sensors. The gas sensing devices are patterned in a field-effect transistor geometry, by dielectrophoretic assembly of RGO platelets between gold electrodes deposited on SiO2/Si substrates. We show that these sensors display highly selective and reversible responses to the measured analytes, as well as fast response and recovery times (tens of seconds). We use combined electronic transport/Kelvin probe microscopy measurements to quantify the amount of charge transferred to RGO due to chemical doping when the device is exposed to electron-acceptor (acetone) and electron-donor (ammonia) analytes. We demonstrate that this method allows us to obtain high-resolution maps of the surface potential and local charge distribution both before and after chemical doping, to identify local gate-susceptible areas on the RGO surface, and to directly extract the contact resistance between the RGO and the metallic electrodes. The method presented is general, suggesting that these results have important implications for building graphene and other nanomaterial-based chemical sensors.

Accuracy of infrared thermometers in very low birth weight infants and impact on newborn behavioural states.

PubMed

Jarvis, Melanie; Guy, Katelyn J; König, Kai

2013-06-01

To study the impact on newborn behavioural states and accuracy of three infrared thermometers compared with digital axillary thermometer measurements in very low birth weight infants. Single-centre prospective observational study. Preterm infants born <1500-g birth weight were eligible. Infants were observed for pre-measurement behaviour state using a five-point neonatal behaviour observation tool. One infrared temperature was taken from each of the devices, followed by an axillary measurement. Further behaviour-state observations were recorded following infrared and axillary measurements. One hundred measurements were collected from each infrared device among a cohort of 42 very low birth weight infants. Only one infrared device showed satisfactory agreement with bias -0.071 (95% limits of agreement -0.68 to 0.54). The other two devices demonstrated poor agreement: bias -1.34; 95% limits of agreement -2.62 to -0.5 and bias -0.56; 95% limits of agreement -1.38 to 0.25. Neonatal behavioural scores showed only minimal changes when infrared measurements were performed but increased significantly following axillary measurements. The difference between the two modalities was statistically significant with a mean increase of 1.44 points following axillary measurements (95% confidence interval 1.21 to 1.67, P < 0.001). Temperature measurements taken with infrared thermometers demonstrated less disruption to preterm infants' behavioural state, however accuracy of devices varied. © 2013 The Authors. Journal of Paediatrics and Child Health © 2013 Paediatrics and Child Health Division (Royal Australasian College of Physicians).

Time-Lapse and Slow-Motion Tracking of Temperature Changes: Response Time of a Thermometer

ERIC Educational Resources Information Center

Moggio, L.; Onorato, P.; Gratton, L. M.; Oss, S.

2017-01-01

We propose the use of a smartphone based time-lapse and slow-motion video techniques together with tracking analysis as valuable tools for investigating thermal processes such as the response time of a thermometer. The two simple experimental activities presented here, suitable also for high school and undergraduate students, allow one to measure…

Evidence for Secondary Flux Rope Generated by the Electron Kelvin-Helmholtz Instability in a Magnetic Reconnection Diffusion Region

NASA Astrophysics Data System (ADS)

Zhong, Z. H.; Tang, R. X.; Zhou, M.; Deng, X. H.; Pang, Y.; Paterson, W. R.; Giles, B. L.; Burch, J. L.; Tobert, R. B.; Ergun, R. E.; Khotyaintsev, Y. V.; Lindquist, P.-A.

2018-02-01

Secondary flux ropes are suggested to play important roles in energy dissipation and particle acceleration during magnetic reconnection. However, their generation mechanism is not fully understood. In this Letter, we present the first direct evidence that a secondary flux rope was generated due to the evolution of an electron vortex, which was driven by the electron Kelvin-Helmholtz instability in an ion diffusion region as observed by the Magnetospheric Multiscale mission. The subion scale (less than the ion inertial length) flux rope was embedded within the electron vortex, which contained a secondary electron diffusion region at the trailing edge of the flux rope. We propose that intense electron shear flow produced by reconnection generated the electron Kelvin-Helmholtz vortex, which induced a secondary reconnection in the exhaust of the primary X line and then led to the formation of the flux rope. This result strongly suggests that secondary electron Kelvin-Helmholtz instability is important for reconnection dynamics.

Evidence for Secondary Flux Rope Generated by the Electron Kelvin-Helmholtz Instability in a Magnetic Reconnection Diffusion Region.

PubMed

Zhong, Z H; Tang, R X; Zhou, M; Deng, X H; Pang, Y; Paterson, W R; Giles, B L; Burch, J L; Tobert, R B; Ergun, R E; Khotyaintsev, Y V; Lindquist, P-A

2018-02-16

Secondary flux ropes are suggested to play important roles in energy dissipation and particle acceleration during magnetic reconnection. However, their generation mechanism is not fully understood. In this Letter, we present the first direct evidence that a secondary flux rope was generated due to the evolution of an electron vortex, which was driven by the electron Kelvin-Helmholtz instability in an ion diffusion region as observed by the Magnetospheric Multiscale mission. The subion scale (less than the ion inertial length) flux rope was embedded within the electron vortex, which contained a secondary electron diffusion region at the trailing edge of the flux rope. We propose that intense electron shear flow produced by reconnection generated the electron Kelvin-Helmholtz vortex, which induced a secondary reconnection in the exhaust of the primary X line and then led to the formation of the flux rope. This result strongly suggests that secondary electron Kelvin-Helmholtz instability is important for reconnection dynamics.

Final report on SIM.T-S5: comparison of the calibration of 100 Ω platinum resistance thermometers

NASA Astrophysics Data System (ADS)

del Campo, D.; García, S.; Velasquez, A.; Medrano, J. A.; Solano, A.; Torres, H. E.

2015-01-01

An International Comparison on industrial Platinum Resistance Thermometers (PRTs) among the National Metrology Institutes (NMIs) of Spain, Panama, Honduras, El Salvador, Costa Rica and Nicaragua began in 2013 and was successfully completed in 2014. Two PRTs were circulated (hand carried) and compared in the range from -38.8 °C up to 250 °C. The Centro Español de Metrología (Spanish NMI), CEM, acted as the pilot laboratory providing the reference value of the comparison. The thermometers have shown an acceptable behavior throughout the comparison, therefore the results can be considered valid for comparing the measurement capabilities of the participant laboratories. The equivalence between the participant laboratories in the calibration of platinum resistance thermometers by comparison in the range from -38,8 °C up to 250 °C has been demonstrated in almost all cases. This report presents the results of this comparison and provides detailed information of the measurements performed by the participating laboratories. Main text. To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCT, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).

Observations of Kelvin-Helmholtz Waves Along the Dusk-Side Boundary of Mercury's Magnetosphere During MESSENGER's Third Flyby

NASA Technical Reports Server (NTRS)

Boardsen, Scott A.; Sundberg, Torgjoern; Slavin, James A.; Anderson, Brian J.; Korth, Haje; Solomon, Sean C.; Blomberg, Lars G.

2010-01-01

During the third MESSENGER flyby of Mercury on 29 September 2009, 15 crossings of the dusk-side magnetopause were observed in the magnetic field data over a 2-min period, during which the spacecraft traveled a distance of 0.2 R(sub M) (where R(sub M) is Mercury's radius). The quasi-periodic nature of the magnetic field variations during the crossings, the characteristic time separations of approx.16 s between pairs of crossings, and the variations of the magnetopause normal directions indicate that the signals are likely the signature of surface waves highly steepened at their leading edge that arose from the Kelvin-Helmholtz instability. At Earth, the Kelvin- Helmholtz instability is believed to lead to the turbulent transport of solar wind plasma into Earth's plasma sheet. This solar wind entry mechanism could also be important at Mercury. Citation: Boardsen, S. A., T. Sundberg, J. A.Slavin, B. J. Anderson, H. Korth, S. C. Solomon, and L. G. Blomberg (2010), Observations of Kelvin-Helmholtz waves along the dusk-side boundary of Mercury s magnetosphere during MESSENGER's third flyby,

A transverse Kelvin-Helmholtz instability in a magnetized plasma

NASA Technical Reports Server (NTRS)

Kintner, P.; Dangelo, N.

1977-01-01

An analysis is conducted of the transverse Kelvin-Helmholtz instability in a magnetized plasma for unstable flute modes. The analysis makes use of a two-fluid model. Details regarding the instability calculation are discussed, taking into account the ion continuity and momentum equations, the solution of a zero-order and a first-order component, and the properties of the solution. It is expected that the linear calculation conducted will apply to situations in which the plasma has experienced no more than a few growth periods.

Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams

PubMed Central

Coquelle, Nicolas; Brewster, Aaron S.; Kapp, Ulrike; Shilova, Anastasya; Weinhausen, Britta; Burghammer, Manfred; Colletier, Jacques-Philippe

2015-01-01

High-resolution structural information was obtained from lysozyme microcrystals (20 µm in the largest dimension) using raster-scanning serial protein crystallography on micro- and nano-focused beamlines at the ESRF. Data were collected at room temperature (RT) from crystals sandwiched between two silicon nitride wafers, thereby preventing their drying, while limiting background scattering and sample consumption. In order to identify crystal hits, new multi-processing and GUI-driven Python-based pre-analysis software was developed, named NanoPeakCell, that was able to read data from a variety of crystallographic image formats. Further data processing was carried out using CrystFEL, and the resultant structures were refined to 1.7 Å resolution. The data demonstrate the feasibility of RT raster-scanning serial micro- and nano-protein crystallography at synchrotrons and validate it as an alternative approach for the collection of high-resolution structural data from micro-sized crystals. Advantages of the proposed approach are its thriftiness, its handling-free nature, the reduced amount of sample required, the adjustable hit rate, the high indexing rate and the minimization of background scattering. PMID:25945583

Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams

DOE Office of Scientific and Technical Information (OSTI.GOV)

Coquelle, Nicolas; Brewster, Aaron S.; Kapp, Ulrike

High-resolution structural information was obtained from lysozyme microcrystals (20 µm in the largest dimension) using raster-scanning serial protein crystallography on micro- and nano-focused beamlines at the ESRF. Data were collected at room temperature (RT) from crystals sandwiched between two silicon nitride wafers, thereby preventing their drying, while limiting background scattering and sample consumption. In order to identify crystal hits, new multi-processing and GUI-driven Python-based pre-analysis software was developed, named NanoPeakCell, that was able to read data from a variety of crystallographic image formats. Further data processing was carried out using CrystFEL, and the resultant structures were refined to 1.7 Åmore » resolution. The data demonstrate the feasibility of RT raster-scanning serial micro- and nano-protein crystallography at synchrotrons and validate it as an alternative approach for the collection of high-resolution structural data from micro-sized crystals. Advantages of the proposed approach are its thriftiness, its handling-free nature, the reduced amount of sample required, the adjustable hit rate, the high indexing rate and the minimization of background scattering.« less

Raster-scanning serial protein crystallography using micro- and nano-focused synchrotron beams

DOE PAGES

Coquelle, Nicolas; Brewster, Aaron S.; Kapp, Ulrike; ...

2015-04-25

High-resolution structural information was obtained from lysozyme microcrystals (20 µm in the largest dimension) using raster-scanning serial protein crystallography on micro- and nano-focused beamlines at the ESRF. Data were collected at room temperature (RT) from crystals sandwiched between two silicon nitride wafers, thereby preventing their drying, while limiting background scattering and sample consumption. In order to identify crystal hits, new multi-processing and GUI-driven Python-based pre-analysis software was developed, named NanoPeakCell, that was able to read data from a variety of crystallographic image formats. Further data processing was carried out using CrystFEL, and the resultant structures were refined to 1.7 Åmore » resolution. The data demonstrate the feasibility of RT raster-scanning serial micro- and nano-protein crystallography at synchrotrons and validate it as an alternative approach for the collection of high-resolution structural data from micro-sized crystals. Advantages of the proposed approach are its thriftiness, its handling-free nature, the reduced amount of sample required, the adjustable hit rate, the high indexing rate and the minimization of background scattering.« less

Controlling the near-field excitation of nano-antennas with phase-change materials.

PubMed

Kao, Tsung Sheng; Chen, Yi Guo; Hong, Ming Hui

2013-01-01

By utilizing the strongly induced plasmon coupling between discrete nano-antennas and quantitatively controlling the crystalline proportions of an underlying Ge2Sb2Te5 (GST) phase-change thin layer, we show that nanoscale light localizations in the immediate proximity of plasmonic nano-antennas can be spatially positioned. Isolated energy hot-spots at a subwavelength scale can be created and adjusted across the landscape of the plasmonic system at a step resolution of λ/20. These findings introduce a new approach for nano-circuitry, bio-assay addressing and imaging applications.

Kelvin-Helmholtz instabilities as the source of inhomogeneous mixing in nova explosions.

PubMed

Casanova, Jordi; José, Jordi; García-Berro, Enrique; Shore, Steven N; Calder, Alan C

2011-10-19

Classical novae are thermonuclear explosions in binary stellar systems containing a white dwarf accreting material from a close companion star. They repeatedly eject 10(-4)-10(-5) solar masses of nucleosynthetically enriched gas into the interstellar medium, recurring on intervals of decades to tens of millennia. They are probably the main sources of Galactic (15)N, (17)O and (13)C. The origin of the large enhancements and inhomogeneous distribution of these species observed in high-resolution spectra of ejected nova shells has, however, remained unexplained for almost half a century. Several mechanisms, including mixing by diffusion, shear or resonant gravity waves, have been proposed in the framework of one-dimensional or two-dimensional simulations, but none has hitherto proven successful because convective mixing can only be modelled accurately in three dimensions. Here we report the results of a three-dimensional nuclear-hydrodynamic simulation of mixing at the core-envelope interface during nova outbursts. We show that buoyant fingering drives vortices from the Kelvin-Helmholtz instability, which inevitably enriches the accreted envelope with material from the outer white-dwarf core. Such mixing also naturally produces large-scale chemical inhomogeneities. Both the metallicity enhancement and the intrinsic dispersions in the abundances are consistent with the observed values.

Fabrication of micro/nano-structures by electrohydrodynamic jet technique

NASA Astrophysics Data System (ADS)

Wang, Dazhi; Zhao, Xiaojun; Lin, Yigao; Ren, Tongqun; Liang, Junsheng; Liu, Chong; Wang, Liding

2017-12-01

Electrohydrodynamic jet (E-Jet) is an approach to the fabrication of micro/nano-structures by the use of electrical forces. In this process, the liquid is subjected to electrical and mechanical forces to form a liquid jet, which is further disintegrated into droplets. The major advantage of the E-Jet technique is that the sizes of the jet formed can be at the nanoscale far smaller than the nozzle size, which can realize high printing resolution with less risk of nozzle blockage. The E-Jet technique, which mainly includes E-Jet deposition and E-Jet printing, has a wide range of applications in the fabrication of micro/nano-structures for micro/nano-electromechanical system devices. This technique is also considered a micro/nano-fabrication method with a great potential for commercial use. This study mainly reviews the E-Jet deposition/printing fundamentals, fabrication process, and applications.

The Fourier-Kelvin Stellar Interferometer (FKSI): Infrared Detection and Characterization of Exozodiacal Dust to Super-Earths, A Progress Report

NASA Technical Reports Server (NTRS)

Danchi, W.

2010-01-01

The Fourier-Kelvin Stellar Interferometer (FKSI) is a structurally connected infrared space interferometer with 0.5 m diameter telescopes on a 12.5 m baseline, and is passively cooled to approx.60K. The FKSI operates in the thermal infrared from 3-8 microns in a nulling (or starlight suppressing) mode for the detection and characterization of exoplanets, debris disks, extrasolar zodiacal dust levels. The FKSI will have the highest angular resolution of any infrared space instrument ever made with its nominal resolution of 40 mas at a 5 micron center wavelength. This resolution exceeds that of Spitzer by a factor of 38 and JWST by a factor of 5. The FKSI mission is conceived as a "probe class" or "mid-sized" strategic mission that utilizes technology advances from flagship projects like JWST, SIM, Spitzer, and the technology programs of TPF-I/Darwin. During the past year we began investigating an enhanced version of FKSI with 1-2 m diameter telescopes, passively cooled to 40K, on a 20-m baseline, with a sunshade giving a +/- 45 degree Field-of-Regard. This enhanced design is capable of detecting and characterizing the atmospheres of many 2 Earth-radius super-Earths and a few Earth-twins. We will report progress on the design of the enhanced mission concept and current status of the technologies needed for this mission.

Nano-imaging of single cells using STIM

NASA Astrophysics Data System (ADS)

Minqin, Ren; van Kan, J. A.; Bettiol, A. A.; Daina, Lim; Gek, Chan Yee; Huat, Bay Boon; Whitlow, H. J.; Osipowicz, T.; Watt, F.

2007-07-01

Scanning transmission ion microscopy (STIM) is a technique which utilizes the energy loss of high energy (MeV) ions passing through a sample to provide structural images. In this paper, we have successfully demonstrated STIM imaging of single cells at the nano-level using the high resolution capability of the proton beam writing facility at the Centre for Ion Beam Applications, National University of Singapore. MCF-7 breast cancer cells (American Type Culture Collection [ATCC]) were seeded on to silicon nitride windows, backed by a Hamamatsu pin diode acting as a particle detector. A reasonable contrast was obtained using 1 MeV protons and excellent contrast obtained using 1 MeV alpha particles. In a further experiment, nano-STIM was also demonstrated using cells seeded on to the pin diode directly, and high quality nano-STIM images showing the nucleus and multiple nucleoli were extracted before the detector was significantly damaged.

High-Temperature Thermometer Using Cr-Doped GdAlO3 Broadband Luminescence

NASA Technical Reports Server (NTRS)

Eldridge, Jeffrey; Chambers, Matthew

2011-01-01

A new concept has been developed for a high-temperature luminescence-based optical thermometer that both shows the desired temperature sensitivity in the upper temperature range of present state-of-the-art luminescence thermometers (above 1,300 C), while maintaining substantial stronger luminescence signal intensity that will allow these optical thermometers to operate in the presence of the high thermal background radiation typical of industrial applications. This objective is attained by using a Cr-doped GdAlO3 (Cr:GdAlO3) sensor with an orthorhombic perovskite structure, resulting in broadband luminescence that remains strong at high temperature due to the favorable electron energy level spacing of Cr:GdAlO3. The Cr:GdAlO3 temperature (and pressure) sensor can be incorporated into, or applied onto, a component s surface when a non-contact surface temperature measurement is desired, or alternatively, the temperature sensor can be attached to the end of a fiber-optic probe that can then be positioned at the location where the temperature measurement is desired. In the case of the fiber-optic probe, both the pulsed excitation and the luminescence emission travel through the fiber-optic light guide. In either case, a pulsed light source provides excitation of the luminescence, and the broadband luminescence emission is collected. Real-time temperature measurements are obtain ed using a least-squares fitting algorithm that determines the luminescence decay time, which has a known temperature dependence established by calibration. Due to the broad absorption and emission bands for Cr:GdAlO3, there is considerable flexibility in the choice of excitation wavelength and emission wavelength detection bands. The strategic choice of the GdAlO3 host is based on its high crystal field, phase stability, and distorted symmetry at the Cr3+ occupation sites. The use of the broadband emission for temperature sensing at high temperatures is a key feature of the invention and is

A melting-point-of gallium apparatus for thermometer calibration.

PubMed

Sostman, H E; Manley, K A

1978-08-01

We have investigated the equilibrium melting point of gallium as a temperature fixed-point at which to calibrate small thermistor thermometers, such as those used to measure temperature in enzyme reaction analysis and other temperature-dependent biological assays. We have determined that the melting temperature of "6N" (99.999% pure) gallium is 29.770 +/- 0.002 degrees C, and that the constant-temperature plateau can be prolonged for several hours. We have designed a simple automated apparatus that exploits this phenomenon and that permits routine calibration verification of thermistor temperature probes throughout the laboratory day. We describe the physics of the gallium melt, and the design and use of the apparatus.

Observations of Turbulence in a Kelvin-Helmholtz Event on 8 September 2015 by the Magnetospheric Multiscale Mission

NASA Technical Reports Server (NTRS)

Stawarz, J. E.; Eriksson, S.; Wilder, F. D.; Ergun, R. E.; Schwartz, S. J.; Pouquet, A.; Burch, J. L.; Giles, B. L.; Khotyaintsev, Y.; Le Contel, O.;

Probing nano-organization of astroglia with multi-color super-resolution microscopy.

PubMed

Heller, Janosch P; Michaluk, Piotr; Sugao, Kohtaroh; Rusakov, Dmitri A

2017-11-01

Astroglia are essential for brain development, homeostasis, and metabolic support. They also contribute actively to the formation and regulation of synaptic circuits, by successfully handling, integrating, and propagating physiological signals of neural networks. The latter occurs mainly by engaging a versatile mechanism of internal Ca 2+ fluctuations and regenerative waves prompting targeted release of signaling molecules into the extracellular space. Astroglia also show substantial structural plasticity associated with age- and use-dependent changes in neural circuitry. However, the underlying cellular mechanisms are poorly understood, mainly because of the extraordinary complex morphology of astroglial compartments on the nanoscopic scale. This complexity largely prevents direct experimental access to astroglial processes, most of which are beyond the diffraction limit of optical microscopy. Here we employed super-resolution microscopy (direct stochastic optical reconstruction microscopy; dSTORM), to visualize astroglial organization on the nanoscale, in culture and in thin brain slices, as an initial step to understand the structural basis of astrocytic nano-physiology. We were able to follow nanoscopic morphology of GFAP-enriched astrocytes, which adapt a flattened shape in culture and a sponge-like structure in situ, with GFAP fibers of varied diameters. We also visualized nanoscopic astrocytic processes using the ubiquitous cytosolic astrocyte marker proteins S100β and glutamine synthetase. Finally, we overexpressed and imaged membrane-targeted pHluorin and lymphocyte-specific protein tyrosine kinase (N-terminal domain) -green fluorescent protein (lck-GFP), to better understand the molecular cascades underlying some common astroglia-targeted fluorescence imaging techniques. The results provide novel, albeit initial, insights into the cellular organization of astroglia on the nanoscale, paving the way for function-specific studies. © 2017 Wiley Periodicals

Nano Mechanical Machining Using AFM Probe

NASA Astrophysics Data System (ADS)

Mostofa, Md. Golam

Complex miniaturized components with high form accuracy will play key roles in the future development of many products, as they provide portability, disposability, lower material consumption in production, low power consumption during operation, lower sample requirements for testing, and higher heat transfer due to their very high surface-to-volume ratio. Given the high market demand for such micro and nano featured components, different manufacturing methods have been developed for their fabrication. Some of the common technologies in micro/nano fabrication are photolithography, electron beam lithography, X-ray lithography and other semiconductor processing techniques. Although these methods are capable of fabricating micro/nano structures with a resolution of less than a few nanometers, some of the shortcomings associated with these methods, such as high production costs for customized products, limited material choices, necessitate the development of other fabricating techniques. Micro/nano mechanical machining, such an atomic force microscope (AFM) probe based nano fabrication, has, therefore, been used to overcome some the major restrictions of the traditional processes. This technique removes material from the workpiece by engaging micro/nano size cutting tool (i.e. AFM probe) and is applicable on a wider range of materials compared to the photolithographic process. In spite of the unique benefits of nano mechanical machining, there are also some challenges with this technique, since the scale is reduced, such as size effects, burr formations, chip adhesions, fragility of tools and tool wear. Moreover, AFM based machining does not have any rotational movement, which makes fabrication of 3D features more difficult. Thus, vibration-assisted machining is introduced into AFM probe based nano mechanical machining to overcome the limitations associated with the conventional AFM probe based scratching method. Vibration-assisted machining reduced the cutting forces

Fever detection in under 5 children in a tertiary health facility using the infrared tympanic thermometer in the oral mode.

PubMed

Edelu, Benedict O; Ojinnaka, Ngozi C; Ikefuna, Anthony N

2011-01-22

Monitoring of body temperature is an important clinical procedure in the care of sick children, especially the under-5 children, as many disease conditions present with fever. The oral mercury-in-glass thermometer which has relatively good accuracy cannot be used in children less than 5 years because it requires their cooperation. This study was aimed at using the infrared tympanic thermometer (IRTT) in oral mode to measure temperature in febrile and afebrile children less than 5 years. Rectal and tympanic temperatures were measured consecutively in 400 febrile and 400 afebrile under-5 children matched for age, using the mercury-in-glass thermometer and the IRTT in oral mode respectively. In the febrile children, the mean tympanic temperature was 38.6 ± 0.9°C, while the mean rectal temperature was 39.0 ± 0.8°C. In the afebrile group, the mean tympanic temperature was 37.0 ± 0.4°C, while the mean rectal temperature was 37.4 ± 0.3°C. The mean difference between rectal and tympanic temperatures in both groups was statistically significant. There was good correlation between the two temperatures. The tympanic thermometer used in the oral mode had a sensitivity of 87.3% and a specificity of 96.5%. The IRTT (oral mode) may not be reliable in estimating 'core' body temperature in children under the age of five years, but with a fairly good sensitivity and specificity, as well as its other advantages such as short duration of measurement, convenience and safety, it is a useful instrument for screening children with fever in a busy setup.

Nano-optical conveyor belt with waveguide-coupled excitation.

PubMed

Wang, Guanghui; Ying, Zhoufeng; Ho, Ho-pui; Huang, Ying; Zou, Ningmu; Zhang, Xuping

2016-02-01

We propose a plasmonic nano-optical conveyor belt for peristaltic transport of nano-particles. Instead of illumination from the top, waveguide-coupled excitation is used for trapping particles with a higher degree of precision and flexibility. Graded nano-rods with individual dimensions coded to have resonance at specific wavelengths are incorporated along the waveguide in order to produce spatially addressable hot spots. Consequently, by switching the excitation wavelength sequentially, particles can be transported to adjacent optical traps along the waveguide. The feasibility of this design is analyzed using three-dimensional finite-difference time-domain and Maxwell stress tensor methods. Simulation results show that this system is capable of exciting addressable traps and moving particles in a peristaltic fashion with tens of nanometers resolution. It is the first, to the best of our knowledge, report about a nano-optical conveyor belt with waveguide-coupled excitation, which is very important for scalability and on-chip integration. The proposed approach offers a new design direction for integrated waveguide-based optical manipulation devices and its application in large scale lab-on-a-chip integration.

Quantifying charge carrier concentration in ZnO thin films by Scanning Kelvin Probe Microscopy

PubMed Central

Maragliano, C.; Lilliu, S.; Dahlem, M. S.; Chiesa, M.; Souier, T.; Stefancich, M.

2014-01-01

In the last years there has been a renewed interest for zinc oxide semiconductor, mainly triggered by its prospects in optoelectronic applications. In particular, zinc oxide thin films are being widely used for photovoltaic applications, in which the determination of the electrical conductivity is of great importance. Being an intrinsically doped material, the quantification of its doping concentration has always been challenging. Here we show how to probe the charge carrier density of zinc oxide thin films by Scanning Kelvin Probe Microscopy, a technique that allows measuring the contact potential difference between the tip and the sample surface with high spatial resolution. A simple electronic energy model is used for correlating the contact potential difference with the doping concentration in the material. Limitations of this technique are discussed in details and some experimental solutions are proposed. Two-dimensional doping concentration images acquired on radio frequency-sputtered intrinsic zinc oxide thin films with different thickness and deposited under different conditions are reported. We show that results inferred with this technique are in accordance with carrier concentration expected for zinc oxide thin films deposited under different conditions and obtained from resistivity and mobility measurements. PMID:24569599

Viscoelastic Mapping of the Arterial Ovine System using a Kelvin Model

DTIC Science & Technology

2007-03-19

University Campus Box 8205 Raleigh, NC 27695. 2) Department of Physiology School of Medicine Universidad de la Republica General Flores 2125, PC: 11800...not differ significantly across locations. We also showed that for all locations, the inclusion of viscoelastic behavior, e.g., using the Kelvin model...All protocols were approved by the Research and Development Council of the Universidad de la Republica, and were conducted in accordance with the

Measuring the lateral charge-carrier mobility in metal-insulator-semiconductor capacitors via Kelvin-probe.

PubMed

Milotti, Valeria; Pietsch, Manuel; Strunk, Karl-Philipp; Melzer, Christian

2018-01-01

We report a Kelvin-probe method to investigate the lateral charge-transport properties of semiconductors, most notably the charge-carrier mobility. The method is based on successive charging and discharging of a pre-biased metal-insulator-semiconductor stack by an alternating voltage applied to one edge of a laterally confined semiconductor layer. The charge carriers spreading along the insulator-semiconductor interface are directly measured by a Kelvin-probe, following the time evolution of the surface potential. A model is presented, describing the device response for arbitrary applied biases allowing the extraction of the lateral charge-carrier mobility from experimentally measured surface potentials. The method is tested using the organic semiconductor poly(3-hexylthiophene), and the extracted mobilities are validated through current voltage measurements on respective field-effect transistors. Our widely applicable approach enables robust measurements of the lateral charge-carrier mobility in semiconductors with weak impact from the utilized contact materials.

Measuring the lateral charge-carrier mobility in metal-insulator-semiconductor capacitors via Kelvin-probe

NASA Astrophysics Data System (ADS)

Milotti, Valeria; Pietsch, Manuel; Strunk, Karl-Philipp; Melzer, Christian

2018-01-01

We report a Kelvin-probe method to investigate the lateral charge-transport properties of semiconductors, most notably the charge-carrier mobility. The method is based on successive charging and discharging of a pre-biased metal-insulator-semiconductor stack by an alternating voltage applied to one edge of a laterally confined semiconductor layer. The charge carriers spreading along the insulator-semiconductor interface are directly measured by a Kelvin-probe, following the time evolution of the surface potential. A model is presented, describing the device response for arbitrary applied biases allowing the extraction of the lateral charge-carrier mobility from experimentally measured surface potentials. The method is tested using the organic semiconductor poly(3-hexylthiophene), and the extracted mobilities are validated through current voltage measurements on respective field-effect transistors. Our widely applicable approach enables robust measurements of the lateral charge-carrier mobility in semiconductors with weak impact from the utilized contact materials.

Plasmonic Nanostructures for Nano-Scale Bio-Sensing

PubMed Central

Chung, Taerin; Lee, Seung-Yeol; Song, Eui Young; Chun, Honggu; Lee, Byoungho

2011-01-01

The optical properties of various nanostructures have been widely adopted for biological detection, from DNA sequencing to nano-scale single molecule biological function measurements. In particular, by employing localized surface plasmon resonance (LSPR), we can expect distinguished sensing performance with high sensitivity and resolution. This indicates that nano-scale detections can be realized by using the shift of resonance wavelength of LSPR in response to the refractive index change. In this paper, we overview various plasmonic nanostructures as potential sensing components. The qualitative descriptions of plasmonic nanostructures are supported by the physical phenomena such as plasmonic hybridization and Fano resonance. We present guidelines for designing specific nanostructures with regard to wavelength range and target sensing materials. PMID:22346679

Seasonal occurrence of sperm whales (Physeter macrocephalus) around Kelvin Seamount in the Sargasso Sea in relation to oceanographic processes

NASA Astrophysics Data System (ADS)

Wong, Sarah N. P.; Whitehead, Hal

2014-09-01

Sperm whales (Physeter macrocephalus) are widely distributed in all oceans, but they are clumped geographically, generally in areas associated with high primary and secondary productivity. The warm, clear waters of the Sargasso Sea are traditionally thought to be low in productivity, however recent surveys have found large numbers of sperm whales there. The New England Seamount Chain bisects the north-western portion of the Sargasso Sea, and might influence the mesoscale eddies associated with the Gulf Stream; creating areas of higher productivity within the Sargasso Sea. We investigated the seasonal occurrence of sperm whales over Kelvin Seamount (part of the New England Seamount Chain) and how it is influenced by oceanographic variables. An autonomous recording device was deployed over Kelvin Seamount from May to June 2006 and November 2006 to June 2007. A total of 6505 hourly two-minute recordings were examined for the presence of sperm whale echolocation clicks. Sperm whales were more prevalent around Kelvin in the spring (April to June: mean=51% of recordings contained clicks) compared to the winter (November to March: mean=16% of recordings contained clicks). Sperm whale prevalence at Kelvin was related to chlorophyll-a concentration four weeks previous, eddy kinetic energy and month. The mesoscale activity associated with the Gulf Stream and the Gulf Stream's interaction with the New England Seamount Chain likely play an important role in sperm whale occurrence in this area, by increasing productivity and perhaps concentration of cephalopod species.

Cross-correlation limit of a SQUID-based noise thermometer of the pMFFT type

NASA Astrophysics Data System (ADS)

Kirste, A.; Engert, J.

2018-03-01

The primary magnetic field fluctuation thermometer (pMFFT) is a SQUID-based noise thermometer for temperatures below 1 K, which complies with metrological requirements. It combines two signal channels in order to apply the cross-correlation technique, but it requires statistically independent noise signals for proper operation. In order to check the limit of the cross-correlation readout, we have performed zero measurements in the millikelvin range in a setup that is identical to the pMFFT, except for the removed temperature sensor. We examined the influence of different parameters such as SQUID working point or flux-lock loop parameters on the minimum cross-correlation signal down to 24 mK and below 100 kHz. Depending on the configuration, typical minimum SQUID-referred cross-power spectral densities of 1.5 × 10‑15 Φ _0^2/Hz or even smaller values were observed. For the pMFFT, considering its thermal noise spectrum, these flux densities correspond to a device noise temperature of ≤2.5 µK, thereby ensuring a negligible uncertainty contribution at the lower end of the PLTS-2000 (0.9 mK).

Topologically Optimized Nano-Positioning Stage Integrating with a Capacitive Comb Sensor.

PubMed

Chen, Tao; Wang, Yaqiong; Liu, Huicong; Yang, Zhan; Wang, Pengbo; Sun, Lining

2017-01-28

Nano-positioning technology has been widely used in many fields, such as microelectronics, optical engineering, and micro manufacturing. This paper presents a one-dimensional (1D) nano-positioning system, adopting a piezoelectric ceramic (PZT) actuator and a multi-objective topological optimal structure. The combination of a nano-positioning stage and a feedback capacitive comb sensor has been achieved. In order to obtain better performance, a wedge-shaped structure is used to apply the precise pre-tension for the piezoelectric ceramics. Through finite element analysis and experimental verification, better static performance and smaller kinetic coupling are achieved. The output displacement of the system achieves a long-stroke of up to 14.7 μm and high-resolution of less than 3 nm. It provides a flexible and efficient way in the design and optimization of the nano-positioning system.

Topologically Optimized Nano-Positioning Stage Integrating with a Capacitive Comb Sensor

PubMed Central

Chen, Tao; Wang, Yaqiong; Liu, Huicong; Yang, Zhan; Wang, Pengbo; Sun, Lining

2017-01-01

Nano-positioning technology has been widely used in many fields, such as microelectronics, optical engineering, and micro manufacturing. This paper presents a one-dimensional (1D) nano-positioning system, adopting a piezoelectric ceramic (PZT) actuator and a multi-objective topological optimal structure. The combination of a nano-positioning stage and a feedback capacitive comb sensor has been achieved. In order to obtain better performance, a wedge-shaped structure is used to apply the precise pre-tension for the piezoelectric ceramics. Through finite element analysis and experimental verification, better static performance and smaller kinetic coupling are achieved. The output displacement of the system achieves a long-stroke of up to 14.7 μm and high-resolution of less than 3 nm. It provides a flexible and efficient way in the design and optimization of the nano-positioning system. PMID:28134854

'Nano' Morphology and Element Signatures of Early Life on Earth: A New Tool for Assessing Biogenicity

NASA Technical Reports Server (NTRS)

Oehler, D. Z.; Mostefaoui, S.; Meibom, A.; Selo, M.; McKay, D. S.; Robert, F.

2006-01-01

The relatively young technology of NanoSIMS is unlocking an exciting new level of information from organic matter in ancient sediments. We are using this technique to characterize Proterozoic organic material that is clearly biogenic as a guide for interpreting controversial organic structures in either terrestrial or extraterrestrial samples. NanoSIMS is secondary ion mass spectrometry for trace element and isotope analysis at sub-micron resolution. In 2005, Robert et al. [1] combined NanoSIMS element maps with optical microscopic imagery in an effort to develop a new method for assessing biogenicity of Precambrian structures. The ability of NanoSIMS to map simultaneously the distribution of organic elements with a 50 nm spatial resolution provides new biologic markers that could help define the timing of life s development on Earth. The current study corroborates the work of Robert et al. and builds on their study by using NanoSIMS to map C, N (as CN), S, Si and O of both excellently preserved microfossils and less well preserved, non-descript organics in Proterozoic chert from the ca. 0.8 Ga Bitter Springs Formation of Australia.

Radially polarized tip-enhanced near-field coherent anti-Stokes Raman scattering microscopy for vibrational nano-imaging

NASA Astrophysics Data System (ADS)

Lin, Jian; Zi Jian Er, Kenneth; Zheng, Wei; Huang, Zhiwei

2013-08-01

We report a radially polarized tip-enhanced near-field coherent anti-Stokes Raman scattering (RP-TE-CARS) microscopy technique for high-contrast vibrational imaging of subcellular organelles at nano-scale resolutions. The radially polarized pump and Stokes laser beams are tightly focused onto the sample while a gold-coated metallic probe is placed at the upper surface of the sample to enhance the electric field and CARS signals. The back-scattered CARS signal is measured with the gold-coated nano-tip being stationary at the focal region of laser beams. The RP-TE-CARS signal is ˜6-fold higher than that using linearly polarized laser excitation. We demonstrate the good performance of the RP-TE-CARS technique developed by imaging sub-micron polystyrene beads and mitochondria at nano-scale resolutions.

A Novel SPM Probe with MOS Transistor and Nano Tip for Surface Electric Properties

NASA Astrophysics Data System (ADS)

Lee, Sang H.; Lim, Geunbae; Moon, Wonkyu

2007-03-01

In this paper, the novel SPM (Scanning Probe Microscope) probe with the planar MOS (Metal-Oxide-Semiconductor) transistor and the FIB (Focused Ion Beam) nano tip is fabricated for the surface electric properties. Since the MOS transistor has high working frequency, the device can overcome the speed limitation of EFM (Electrostatic Force Microscope) system. The sensitivity is also high, and no bulky device such as lock-in-amplifier is required. Moreover, the nano tip with nanometer scale tip radius is fabricated with FIB system, and the resolution can be improved. Therefore, the probe can rapidly detect small localized electric properties with high sensitivity and high resolution. The MOS transistor is fabricated with the common semiconductor process, and the nano tip is grown by the FIB system. The planar structure of the MOS transistor makes the fabrication process easier, which is the advantage on the commercial production. Various electric signals are applied using the function generator, and the measured data represent the well-established electric properties of the device. It shows the promising aspect of the local surface electric property detection with high sensitivity and high resolution.

THE KELVIN-HELMHOLTZ INSTABILITY AT CORONAL MASS EJECTION BOUNDARIES IN THE SOLAR CORONA: OBSERVATIONS AND 2.5D MHD SIMULATIONS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moestl, U. V.; Temmer, M.; Veronig, A. M., E-mail: ute.moestl@uni-graz.at

2013-03-20

The Atmospheric Imaging Assembly on board the Solar Dynamics Observatory observed a coronal mass ejection with an embedded filament on 2011 February 24, revealing quasi-periodic vortex-like structures at the northern side of the filament boundary with a wavelength of approximately 14.4 Mm and a propagation speed of about 310 {+-} 20 km s{sup -1}. These structures could result from the Kelvin-Helmholtz instability occurring on the boundary. We perform 2.5D numerical simulations of the Kelvin-Helmholtz instability and compare the simulated characteristic properties of the instability with the observations, where we obtain qualitative as well as quantitative accordance. We study the absencemore » of Kelvin-Helmholtz vortex-like structures on the southern side of the filament boundary and find that a magnetic field component parallel to the boundary with a strength of about 20% of the total magnetic field has stabilizing effects resulting in an asymmetric development of the instability.« less

Improved Readout Scheme for SQUID-Based Thermometry

NASA Technical Reports Server (NTRS)

Penanen, Konstantin

2007-01-01

An improved readout scheme has been proposed for high-resolution thermometers, (HRTs) based on the use of superconducting quantum interference devices (SQUIDs) to measure temperature- dependent magnetic susceptibilities. The proposed scheme would eliminate counting ambiguities that arise in the conventional scheme, while maintaining the superior magnetic-flux sensitivity of the conventional scheme. The proposed scheme is expected to be especially beneficial for HRT-based temperature control of multiplexed SQUIDbased bolometer sensor arrays. SQUID-based HRTs have become standard for measuring and controlling temperatures in the sub-nano-Kelvin temperature range in a broad range of low-temperature scientific and engineering applications. A typical SQUIDbased HRT that utilizes the conventional scheme includes a coil wound on a core made of a material that has temperature- dependent magnetic susceptibility in the temperature range of interest. The core and the coil are placed in a DC magnetic field provided either by a permanent magnet or as magnetic flux inside a superconducting outer wall. The aforementioned coil is connected to an input coil of a SQUID. Changes in temperature lead to changes in the susceptibility of the core and to changes in the magnetic flux detected by the SQUID. The SQUID readout instrumentation is capable of measuring magnetic-flux changes that correspond to temperature changes down to a noise limit .0.1 nK/Hz1/2. When the flux exceeds a few fundamental flux units, which typically corresponds to a temperature of .100 nK, the SQUID is reset. The temperature range can be greatly expanded if the reset events are carefully tracked and counted, either by a computer running appropriate software or by a dedicated piece of hardware.

Sensitivity and specificity of the Distress Impact Thermometer for the detection of psychological distress among CRC survivors.

PubMed

Craike, Melinda J; Livingston, Patricia M; Warne, Charles

2011-01-01

This study assessed the relative screening performance of the Distress Impact Thermometer (DIT) and cutoff levels with the established clinical case threshold of the Hospital Anxiety and Depression Scale (HADS) among a sample of colorectal cancer (CRC) survivors. Fifty-nine CRC survivors completed the DIT, HADS, and provided demographic information at baseline, and 45 of these patients completed the same measures at follow-up, giving a total of 104 participant data. Receiver operating characteristic (ROC) analysis was performed to determine the accuracy of the DIT compared to the HADS, with a cutoff score ≥8 on each HADS subscale (depression and anxiety) and ≥15 on the HADS total scale used to identify patients with psychological distress. The sample comprised slightly more males (63%) than females, with an average age of 59 years (SD = 9.53) and ranging from 33 to 77 years. The optimum DT cutoff score of ≥5 yielded a sensitivity of 60% and specificity of 86.1%; the area under the curve was 0.771 (95% confidence interval [CI] [0.646, 0.896]). For the depression subscale, the DT performed better on specificity than sensitivity, however the opposite was true for the anxiety subscale. The addition of an impact thermometer did not enhance screening performance. The results of this study provide support for a DT score of ≥5 for detecting psychological distress among CRC survivors and do not support the addition of an impact thermometer. The use of the DT might underestimate depression but overestimate anxiety.

On the role of the Kelvin wave in the westerly phase of the semiannual zonal wind oscillation

NASA Technical Reports Server (NTRS)

Dunkerton, T.

1979-01-01

The role of the Kelvin wave, discovered by Hirota (1978), in producing the westerly accelerations of the semiannual zonal wind oscillation in the tropical upper stratosphere is examined quantitatively. It is shown that, for reasonable values of the wave parameters, this Kelvin wave could indeed give rise to the observed accelerations. For the thermal damping rates of Dickinson (1973), the most likely range of phase speeds for a wavenumber 1 disturbance is from 45 to 60 m/sec. For 'photochemically accelerated' damping rates (Blake and Lindzen, 1973), a phase speed in excess of 70 m/sec would be required. The possibility of a significant modulation of the semiannual westerlies by the quasi-biennial oscillation is also suggested.

The three-dimensional evolution of a plane mixing layer. Part 1: The Kelvin-Helmholtz roll-up

NASA Technical Reports Server (NTRS)

Rogers, Michael M.; Moser, Robert D.

1991-01-01

The Kelvin Helmholtz roll up of three dimensional, temporally evolving, plane mixing layers were simulated numerically. All simulations were begun from a few low wavenumber disturbances, usually derived from linear stability theory, in addition to the mean velocity profile. The spanwise disturbance wavelength was taken to be less than or equal to the streamwise wavelength associated with the Kelvin Helmholtz roll up. A standard set of clean structures develop in most of the simulations. The spanwise vorticity rolls up into a corrugated spanwise roller, with vortex stretching creating strong spanwise vorticity in a cup shaped region at the vends of the roller. Predominantly streamwise rib vortices develop in the braid region between the rollers. For sufficiently strong initial three dimensional disturbances, these ribs collapse into compact axisymmetric vortices. The rib vortex lines connect to neighboring ribs and are kinked in the opposite direction of the roller vortex lines. Because of this, these two sets of vortex lines remain distinct. For certain initial conditions, persistent ribs do not develop. In such cases the development of significant three dimensionality is delayed. When the initial three dimensional disturbance energy is about equal to, or less than, the two dimensional fundamental disturbance energy, the evolution of the three dimensional disturbance is nearly linear (with respect to the mean and the two dimensional disturbances), at least until the first Kelvin Helmholtz roll up is completed.

Ratiometric near infrared luminescent thermometer based on lanthanide metal-organic frameworks

NASA Astrophysics Data System (ADS)

Yue, Dan; Zhang, Jun; Zhao, Dian; Lian, Xiusheng; Cui, Yuanjing; Yang, Yu; Qian, Guodong

2016-09-01

A near infrared luminescent MOFs thermometer (Nd0.676Yb0.324BTC) was prepared via a simple solvothermal method using Ln3+ (Ln=Nd, Yb) ions and 1, 3, 5-benznenetricarboxylic acid (H3BTC), and characterized by PXRD, TGA, ICP, and photoluminescence (PL) spectrum. These results indicate that the Nd0.676Yb0.324BTC displays high relative sensitivity and excellent repeatability in the physiological temperature range (288-323 K), and the maximum relative sensitivity is determined to be 1.187% K-1 at 323 K. These NIR luminescent MOFs may have potential applications in physiological temperature sensing.

An evaluation of a zero-heat-flux cutaneous thermometer in cardiac surgical patients.

PubMed

Eshraghi, Yashar; Nasr, Vivian; Parra-Sanchez, Ivan; Van Duren, Albert; Botham, Mark; Santoscoy, Thomas; Sessler, Daniel I

2014-09-01

Although core temperature can be measured invasively, there are currently no widely available, reliable, noninvasive thermometers for its measurement. We thus compared a prototype zero-heat-flux thermometer with simultaneous measurements from a pulmonary artery catheter. Specifically, we tested the hypothesis that zero-heat-flux temperatures are sufficiently accurate for routine clinical use. Core temperature was measured from the thermistor of a standard pulmonary artery catheter and with a prototype zero-heat-flux deep-tissue thermometer in 105 patients having nonemergent cardiac surgery. Zero-heat-flux probes were positioned on the lateral forehead and lateral neck. Skin surface temperature probes were attached to the forehead just adjacent to the zero-heat-flux probe. Temperatures were recorded at 1-minute intervals, excluding the period of cardiopulmonary bypass, and for the first 4 postoperative hours. Zero-heat-flux and pulmonary artery temperatures were compared with bias analysis; differences exceeding 0.5°C were considered to be potentially clinically important. The mean duration in the operating room was 279 ± 75 minutes, and the mean cross-clamp time was 118 ± 50 minutes. All subjects were monitored for an additional 4 hours in the intensive care unit. The average overall difference between forehead zero-heat-flux and pulmonary artery temperatures (i.e., forehead minus pulmonary artery) was -0.23°C (95% limits of agreement of ±0.82); 78% of the differences were ≤0.5°C. The average intraoperative temperature difference was -0.08°C (95% limits of agreement of ±0.88); 84% of the differences were ≤0.5°C. The average postoperative difference was -0.32°C (95% limits of agreement of ±0.75); 84% of the differences were ≤0.5°C. Bias and precision values for neck site were similar to the forehead values. Uncorrected forehead skin temperature showed an increasing negative bias as core temperature decreased. Core temperature can be noninvasively

Parent-Child Agreement Using the Spence Children's Anxiety Scale and a Thermometer in Children with Autism Spectrum Disorder

PubMed Central

May, T.; Cornish, K.; Rinehart, N. J.

2015-01-01

Children with Autism Spectrum Disorder (ASD) experience high anxiety which often prompts clinical referral and requires intervention. This study aimed to compare parent and child reports on the Spence Children's Anxiety Scale (SCAS) and a child-reported “worry thermometer” in 88 children aged 8–13 years, 44 with ASD and 44 age, gender, and perceptual IQ matched typically developing children. There were no gender differences in child report on the SCAS and worry thermometers. Results indicated generally good correlations between parent and child self-reported SCAS symptoms for typically developing children but poor agreement in parent-child ASD dyads. The worry thermometer child-report did not reflect child or parent reports on the SCAS. Findings suggest 8–13-year-old children with ASD may have difficulties accurately reporting their anxiety levels. The clinical implications were discussed. PMID:25922765

Breaking the Time Barrier in Kelvin Probe Force Microscopy: Fast Free Force Reconstruction Using the G-Mode Platform

DOE Office of Scientific and Technical Information (OSTI.GOV)

Collins, Liam; Ahmadi, Mahshid; Wu, Ting

The atomic force microscope (AFM) offers unparalleled insight into structure and material functionality across nanometer length scales. However, the spatial resolution afforded by the AFM tip is counterpoised by slow detection speeds compared to other common microscopy techniques (e.g. optical, scanning electron microscopy etc.). In this work, we develop an AFM imaging approach allowing ultrafast reconstruction of the tip-sample forces having ~2 orders of magnitude higher time resolution than standard detection methods. Fast free force recovery (F3R) overcomes the widely-viewed temporal bottleneck in AFM, i.e. the mechanical bandwidth of the cantilever, enabling time-resolved imaging at sub-bandwidth speeds. We demonstrate quantitativemore » recovery of electrostatic forces with ~10 µs temporal resolution, free from cantilever ring-down effects. We further apply the F3R method to Kelvin probe force microscopy (KPFM) measurements. F3R-KPFM is an open loop imaging approach (i.e. no bias feedback), allowing ultrafast surface potential measurements (e.g. < 20 µs) to be performed at regular KPFM scan speeds. F3R-KPFM is demonstrated for exploration of ion migration in organometallic halide perovskites materials and shown to allow spatio-temporal imaging of positively charged ion migration under applied electric field, as well as subsequent formation of accumulated charges at the perovskite/electrode interface. In this work we demonstrate quantitative F3R-KPFM measurements – however, we fully expect the F3R approach to be valid for all modes of non-contact AFM operation, including non-invasive probing of ultrafast electrical and magnetic dynamics.« less

Breaking the Time Barrier in Kelvin Probe Force Microscopy: Fast Free Force Reconstruction Using the G-Mode Platform

DOE PAGES

Collins, Liam; Ahmadi, Mahshid; Wu, Ting; ...

2017-08-06

The atomic force microscope (AFM) offers unparalleled insight into structure and material functionality across nanometer length scales. However, the spatial resolution afforded by the AFM tip is counterpoised by slow detection speeds compared to other common microscopy techniques (e.g. optical, scanning electron microscopy etc.). In this work, we develop an AFM imaging approach allowing ultrafast reconstruction of the tip-sample forces having ~2 orders of magnitude higher time resolution than standard detection methods. Fast free force recovery (F3R) overcomes the widely-viewed temporal bottleneck in AFM, i.e. the mechanical bandwidth of the cantilever, enabling time-resolved imaging at sub-bandwidth speeds. We demonstrate quantitativemore » recovery of electrostatic forces with ~10 µs temporal resolution, free from cantilever ring-down effects. We further apply the F3R method to Kelvin probe force microscopy (KPFM) measurements. F3R-KPFM is an open loop imaging approach (i.e. no bias feedback), allowing ultrafast surface potential measurements (e.g. < 20 µs) to be performed at regular KPFM scan speeds. F3R-KPFM is demonstrated for exploration of ion migration in organometallic halide perovskites materials and shown to allow spatio-temporal imaging of positively charged ion migration under applied electric field, as well as subsequent formation of accumulated charges at the perovskite/electrode interface. In this work we demonstrate quantitative F3R-KPFM measurements – however, we fully expect the F3R approach to be valid for all modes of non-contact AFM operation, including non-invasive probing of ultrafast electrical and magnetic dynamics.« less

Visualizing Microbial Biogeochemistry: NanoSIMS and Stable Isotope Probing (Invited)

NASA Astrophysics Data System (ADS)

Pett-Ridge, J.; Weber, P. K.

2009-12-01

Linking phylogenetic information to function in microbial communities is a key challenge for microbial ecology. Isotope-labeling experiments provide a useful means to investigate the ecophysiology of microbial populations and cells in the environment and allow measurement of nutrient transfers between cell types, symbionts and consortia. The combination of Nano-Secondary Ion Mass Spectrometry (NanoSIMS) analysis, in situ labeling and high resolution microscopy allows isotopic analysis to be linked to phylogeny and morphology and holds great promise for fine-scale studies of microbial systems. In NanoSIMS analysis, samples are sputtered with an energetic primary beam (Cs+, O-) liberating secondary ions that are separated by the mass spectrometer and detected in a suite of electron multipliers. Five isotopic species may be analyzed concurrently with spatial resolution as fine as 50nm. A high sensitivity isotope ratio ‘map’ can then be generated for the analyzed area. NanoSIMS images of 13C, 15N and Mo (a nitrogenase co-factor) localization in diazotrophic cyanobacteria show how cells differentially allocate resources within filaments and allow calculation of nutrient uptake rates on a cell by cell basis. Images of AM fungal hyphae-root and cyanobacteria-rhizobia associations indicate the mobilization and sharing (stealing?) of newly fixed C and N. In a related technique, “El-FISH”, stable isotope labeled biomass is probed with oligonucleotide-elemental labels and then imaged by NanoSIMS. In microbial consortia and cyanobacterial mats, this technique helps link microbial structure and function simultaneously even in systems with unknown and uncultivated microbes. Finally, the combination of re-engineered universal 16S oligonucleotide microarrays with NanoSIMS analyses may allow microbial identity to be linked to functional roles in complex systems such as mats and cellulose degrading hindgut communities. These newly developed methods provide correlated

Method for in-situ restoration of plantinum resistance thermometer calibration

DOEpatents

Carroll, Radford M.

1989-01-01

A method is provided for in-situ restoration of platinum resistance thermometers (PRT's) that have undergone surface oxide contamination and/or strain-related damage causing decalibration. The method, which may be automated using a programmed computer control arrangement, consists of applying a dc heating current to the resistive sensing element of the PRT of sufficient magnitude to heat the element to an annealing temperature and maintaining the temperature for a specified period to restore the element to a stress-free calibration condition. The process anneals the sensing element of the PRT without subjecting the entire PRT assembly to the annealing temperature and may be used in the periodic maintenance of installed PRT's.

Method for in-situ restoration of platinum resistance thermometer calibration

DOEpatents

Carroll, R.M.

1987-10-23

A method is provided for in-situ restoration of platinum resistance thermometers (PRT's) that have undergone surface oxide contamination and/or stain-related damage causing decalibration. The method, which may be automated using a programmed computer control arrangement, consists of applying a dc heating current to the resistive sensing element of the PRT of sufficient magnitude to heat the element to an annealing temperature and maintaining the temperature for a specified period to restore the element to a stress-free calibration condition. The process anneals the sensing element of the PRT without subjecting the entire PRT assembly to the annealing temperature and may be used in the periodic maintenance of installed PRT's. 1 fig.

Use of infrared emission detection thermometer in Chinese neonates.

PubMed

Ng, D K; Liu, Y S; Ho, J C

1999-07-01

To evaluate the reproducibility of Thermoscan, an infrared emission detection ear thermometer, and to establish the normal reference range of ear temperature in Chinese neonates. Neonates were recruited from the inpatients population with exclusion of those suffering from infections. Forty-nine neonates were recruited with 1,115 temperature taking sessions. Mean left ear temperature was 36.64 degrees C +/- 0.35 degree C. Mean right ear temperature was 36.64 degrees C +/- 0.37 degree C. Clinical repeatability for left and right ear was 0.17 degree C and 0.17 degree C, respectively. Thermoscan produced reproducible results in Chinese neonates. The normal range of ear temperature for Chinese neonates is 35 degrees C to 37 degrees C. Ear temperature > 37.8 degrees C should be regarded as fever.

Deployable Laboratory Applications of Nano- and Bio-Technology (Applications de nanotechnologie et biotechnologie destinees a un laboratoire deployable)

DTIC Science & Technology

2014-10-01

applications of present nano-/ bio -technology include advanced health and fitness monitoring, high-resolution imaging, new environmental sensor platforms...others areas where nano-/ bio -technology development is needed: • Sensors : Diagnostic and detection kits (gene-chips, protein-chips, lab-on-chips, etc...studies on chemo- bio nano- sensors , ultra-sensitive biochips (“lab-on-a-chip” and “cells-on-chips” devices) have been prepared for routine medical

Lennard-Jones fluids in two-dimensional nano-pores. Multi-phase coexistence and fluid structure

NASA Astrophysics Data System (ADS)

Yatsyshin, Petr; Savva, Nikos; Kalliadasis, Serafim

2014-03-01

We present a number of fundamental findings on the wetting behaviour of nano-pores. A popular model for fluid confinement is a one-dimensional (1D) slit pore formed by two parallel planar walls and it exhibits capillary condensation (CC): a first-order phase transition from vapour to capillary-liquid (Kelvin shift). Capping such a pore at one end by a third orthogonal wall forms a prototypical two-dimensional (2D) pore. We show that 2D pores possess a wetting temperature such that below this temperature CC remains of first order, above it becomes a continuous phase transition manifested by a slab of capillary-liquid filling the pore from the capping wall. Continuous CC exhibits hysteresis and can be preceded by a first-order capillary prewetting transition. Additionally, liquid drops can form in the corners of the 2D pore (remnant of 2D wedge prewetting). The three fluid phases, vapour, capillary-liquid slab and corner drops, can coexist at the pore triple point. Our model is based on the statistical mechanics of fluids in the density functional formulation. The fluid-fluid and fluid-substrate interactions are dispersive. We analyze in detail the microscopic fluid structure, isotherms and full phase diagrams. Our findings also suggest novel ways to control wetting of nano-pores. We are grateful to the European Research Council via Advanced Grant No. 247031 for support.

Modified Kelvin Equations for Capillary Condensation in Narrow and Wide Grooves

NASA Astrophysics Data System (ADS)

Malijevský, Alexandr; Parry, Andrew O.

2018-03-01

We consider the location and order of capillary condensation transitions occurring in deep grooves of width L and depth D . For walls that are completely wet by liquid (contact angle θ =0 ) the transition is continuous and its location is not sensitive to the depth of the groove. However, for walls that are partially wet by liquid, where the transition is first order, we show that the pressure at which it occurs is determined by a modified Kelvin equation characterized by an edge contact angle θE describing the shape of the meniscus formed at the top of the groove. The dependence of θE on the groove depth D relies, in turn, on whether corner menisci are formed at the bottom of the groove in the low density gaslike phase. While for macroscopically wide grooves these are always present when θ <45 ° we argue that their formation is inhibited in narrow grooves. This has a number of implications including that the local pinning of the meniscus and location of the condensation transition is different depending on whether the contact angle is greater or less than a universal value θ*≈31 °. Our arguments are supported by detailed microscopic density functional theory calculations that show that the modified Kelvin equation remains highly accurate even when L and D are of the order of tens of molecular diameters.

Effective reduction of p-nitrophenol by silver nanoparticle loaded on magnetic Fe3O4/ATO nano-composite

NASA Astrophysics Data System (ADS)

Karki, Hem Prakash; Ojha, Devi Prashad; Joshi, Mahesh Kumar; Kim, Han Joo

2018-03-01

A silver loaded hematite (Fe3O4) and antimony doped tin oxide (ATO) magnetic nano-composite (Ag-Fe3O4/ATO) was successfully synthesized by in situ one pot green and facile hydrothermal process. The formation of nano-composite, its structure, morphology, and stability were characterized by field emission scanning electron microscopy (FE-SEM), high resolution transmission electron microscopy (HRTEM), electron diffraction spectroscopy (EDS), elemental mapping by high resolution scanning transmission electron microscopy (STEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transform infra-red spectroscopy (FTIR). UV-vis spectroscopy was used to monitor the catalytic reduction of p-nitrophenol (PNP) into p-aminophenol (PAP) in presence of Ag-Fe3O4/ATO nano-composite with excess of sodium borohydride (NaBH4). The pseudo-first order kinetic equation could describe the reduction of p-nitrophenol with excess of NaBH4. For the first time, ATO surface was used for hydrothermal growth of silver and iron oxide magnetic nanoparticles. The in situ growth of these nanoparticles provided an effective bonding of components of the nano-composite over the surface of ATO nanoparticles. This nano-composite exhibited easy synthesis, high stability, cost effective and rapid separation using external magnet. The excellent catalytic and anti-bacterial activity of as-synthesized silver nano-composite makes it potential nano-catalyst for waste water treatment as well as biomedical application.

Why Was Kelvin's Estimate of the Earth's Age Wrong?

ERIC Educational Resources Information Center

Lovatt, Ian; Syed, M. Qasim

2014-01-01

This is a companion to our previous paper in which we give a published example, based primarily on Perry's work, of a graph of ln "y" versus "t" when "y" is an exponential function of "t". This work led us to the idea that Lord Kelvin's (William Thomson's) estimate of the Earth's age was…

Characterizing the Nano and Micro Structure of Concrete toImprove its Durability

DOE Office of Scientific and Technical Information (OSTI.GOV)

Monteiro, P.J.M.; Kirchheim, A.P.; Chae, S.

2009-01-13

New and advanced methodologies have been developed to characterize the nano and microstructure of cement paste and concrete exposed to aggressive environments. High resolution full-field soft X-ray imaging in the water window is providing new insight on the nano scale of the cement hydration process, which leads to a nano-optimization of cement-based systems. Hard X-ray microtomography images of ice inside cement paste and cracking caused by the alkali?silica reaction (ASR) enables three-dimensional structural identification. The potential of neutron diffraction to determine reactive aggregates by measuring their residual strains and preferred orientation is studied. Results of experiments using these tools aremore » shown on this paper.« less

Characterizing the nano and micro structure of concrete to improve its durability

DOE Office of Scientific and Technical Information (OSTI.GOV)

Monteiro, P.J.M.; Kirchheim, A.P.; Chae, S.

2008-10-22

New and advanced methodologies have been developed to characterize the nano and microstructure of cement paste and concrete exposed to aggressive environments. High resolution full-field soft X-ray imaging in the water window is providing new insight on the nano scale of the cement hydration process, which leads to a nano-optimization of cement-based systems. Hard X-ray microtomography images on ice inside cement paste and cracking caused by the alkali-silica reaction (ASR) enables three-dimensional structural identification. The potential of neutron diffraction to determine reactive aggregates by measuring their residual strains and preferred orientation is studied. Results of experiments using these tools willmore » be shown on this paper.« less

Design of a high speed, high resolution thermometry system for 1.5 GHz superconducting radio frequency cavities

NASA Astrophysics Data System (ADS)

Knobloch, Jens; Muller, Henry; Padamsee, Hasan

1994-11-01

Presented in this paper are the description and the test results of a new stationary thermometry system used to map the temperature of the outer surface of 1.5 GHz superconducting single-cell cavities during operation at 1.6 K. The system comprises 764 removable carbon thermometers whose signals are multiplexed and scanned by a Macintosh computer. A complete temperature map can be obtained in as little as 0.1 s at a temperature resolution of about 0.2 mK. Alternatively, it has been demonstrated that if the acquisition time is increased to several seconds, then a temperature resolution on the order of 30 μK is possible. To our knowledge, these are the fastest acquisition times so far achieved with L-band cavities at these resolutions.

Comparative Study on Cushion Performance Between 3D Printed Kelvin Structure and 3D Printed Lattice Structure

NASA Astrophysics Data System (ADS)

Priyadarshini, Lakshmi

Frequently transported packaging goods are more prone to damage due to impact, jolting or vibration in transit. Fragile goods, for example, glass, ceramics, porcelain are susceptible to mechanical stresses. Hence ancillary materials like cushions play an important role when utilized within package. In this work, an analytical model of a 3D cellular structure is established based on Kelvin model and lattice structure. The research will provide a comparative study between the 3D printed Kelvin unit structure and 3D printed lattice structure. The comparative investigation is based on parameters defining cushion performance such as cushion creep, indentation, and cushion curve analysis. The applications of 3D printing is in rapid prototyping where the study will provide information of which model delivers better form of energy absorption. 3D printed foam will be shown as a cost-effective approach as prototype. The research also investigates about the selection of material for 3D printing process. As cushion development demands flexible material, three-dimensional printing with material having elastomeric properties is required. Further, the concept of cushion design is based on Kelvin model structure and lattice structure. The analytical solution provides the cushion curve analysis with respect to the results observed when load is applied over the cushion. The results are reported on basis of attenuation and amplification curves.

Collision-Induced Infrared Absorption by Hydrogen-Helium gas mixtures at Thousands of Kelvin

NASA Astrophysics Data System (ADS)

Abel, Martin; Frommhold, Lothar; Li, Xiaoping; Hunt, Katharine L. C.

2010-10-01

The interaction-induced absorption by collisional pairs of H2 molecules is an important opacity source in the atmospheres of the outer planets and cool stars ^[1]. The emission spectra of cool white dwarf stars differ significantly in the infrared from the expected blackbody spectra of their cores, which is largely due to absorption by collisional H2--H2, H2--He, and H2--H complexes in the stellar atmospheres. Using quantum-chemical methods we compute the atmospheric absorption from hundreds to thousands of kelvin ^[2]. Laboratory measurements of interaction-induced absorption spectra by H2 pairs exist only at room temperature and below. We show that our results reproduce these measurements closely ^[2], so that our computational data permit reliable modeling of stellar atmosphere opacities even for the higher temperatures ^[2]. [1] L. Frommhold, Collision-Induced Absorption in Gases, Cambridge University Press, Cambridge, New York, 1993 and 2006 [2] Xiaoping Li, Katharine L. C. Hunt, Fei Wang, Martin Abel, and Lothar Frommhold, ``Collision-Induced Infrared Absorption by Molecular Hydrogen Pairs at Thousands of Kelvin'', International Journal of Spectroscopy, vol. 2010, Article ID 371201, 11 pages, 2010. doi: 10.1155/2010/371201

The Magnetohydrodynamic Kelvin-Helmholtz Instability: A Three-dimensional Study of Nonlinear Evolution

NASA Astrophysics Data System (ADS)

Ryu, Dongsu; Jones, T. W.; Frank, Adam

2000-12-01

We investigate through high-resolution three-dimensional simulations the nonlinear evolution of compressible magnetohydrodynamic flows subject to the Kelvin-Helmholtz instability. As in our earlier work, we have considered periodic sections of flows that contain a thin, transonic shear layer but are otherwise uniform. The initially uniform magnetic field is parallel to the shear plane but oblique to the flow itself. We confirm in three-dimensional flows the conclusion from our two-dimensional work that even apparently weak magnetic fields embedded in Kelvin-Helmholtz unstable plasma flows can be fundamentally important to nonlinear evolution of the instability. In fact, that statement is strengthened in three dimensions by this work because it shows how field-line bundles can be stretched and twisted in three dimensions as the quasi-two-dimensional Cat's Eye vortex forms out of the hydrodynamical motions. In our simulations twisting of the field may increase the maximum field strength by more than a factor of 2 over the two-dimensional effect. If, by these developments, the Alfvén Mach number of flows around the Cat's Eye drops to unity or less, our simulations suggest that magnetic stresses will eventually destroy the Cat's Eye and cause the plasma flow to self-organize into a relatively smooth and apparently stable flow that retains memory of the original shear. For our flow configurations, the regime in three dimensions for such reorganization is 4<~MAx<~50, expressed in terms of the Alfvén Mach number of the original velocity transition and the initial Alfvén speed projected to the flow plan. When the initial field is stronger than this, the flow either is linearly stable (if MAx<~2) or becomes stabilized by enhanced magnetic tension as a result of the corrugated field along the shear layer before the Cat's Eye forms (if MAx>~2). For weaker fields the instability remains essentially hydrodynamic in early stages, and the Cat's Eye is destroyed by the

Evidence of Boundary Reflection of Kelvin and First-Mode Rossby Waves from Topex/Poseidon Sea Level Data

NASA Technical Reports Server (NTRS)

Boulanger, Jean-Philippe; Fu, Lee-Lueng

1996-01-01

The TOPEX/POSEIDON sea level data lead to new opportunities to investigate some theoretical mechanisms suggested to be involved in the El Nino-Southern Oscillation phenomenon in the tropical Pacific ocean. In particular, we are interested in studying the western boundary reflection, a process crucial for the delayed action oscillator theory, by using the TOPEX/POSEIDON data from November 1992 to May 1995. We first projected the sea level data onto Kelvin and first-mode Ross waves. Then we estimated the contribution of wind forcing to these waves by using a single baroclinic mode simple wave model forced by the ERS-1 wind data. Wave propagation was clearly observed with amplitudes well explained by the wind forcing in the ocean interior. Evidence of wave reflection was detected at both the western and eastern boundaries of the tropical Pacific ocean. At the eastern boundary, Kelvin waves were seen to reflect as first-mode Rossby waves during the entire period. The reflection efficiency (in terms of wave amplitude) of the South American coasts was estimated to be 80% of that of an infinite meridional wall. At the western boundary, reflection was observed in April-August 1993, in January-June 1994, and, later, in December 1994 to February 1995. Although the general roles of these reflection events in the variability observed in the equatorial Pacific ocean are not clear, the data suggest that the reflections in January-June 1994 have played a role in the onset of the warm conditions observed in late 1994 to early 1995. Indeed, during the January-June 1994 period, as strong downwelling first-mode Rossby waves reflected into downwelling Kelvin waves, easterly wind and cold sea surface temperature anomalies located near the date line weakened and eventually reversed in June-July 1994. The presence of the warm anomalies near the date line then favored convection and westerly wind anomalies that triggered strong downwelling Kelvin waves propagating throughout the basin

Super-resolution optical microscopy for studying membrane structure and dynamics.

PubMed

Sezgin, Erdinc

2017-07-12

Investigation of cell membrane structure and dynamics requires high spatial and temporal resolution. The spatial resolution of conventional light microscopy is limited due to the diffraction of light. However, recent developments in microscopy enabled us to access the nano-scale regime spatially, thus to elucidate the nanoscopic structures in the cellular membranes. In this review, we will explain the resolution limit, address the working principles of the most commonly used super-resolution microscopy techniques and summarise their recent applications in the biomembrane field.

The Fourier-Kelvin Stellar Interferometer (FKSI): A Progress Report and Preliminary Results from Our Laboratory Testbed

NASA Technical Reports Server (NTRS)

Berry, Richard; Rajagopa, J.; Danchi, W. C.; Allen, R. J.; Benford, D. J.; Deming, D.; Gezari, D. Y.; Kuchner, M.; Leisawitz, D. T.; Linfield, R.

2005-01-01

The Fourier-Kelvin Stellar Interferometer (FKSI) is a mission concept for an imaging and nulling interferometer for the near-infrared to mid-infrared spectral region (3-8 microns). FKSI is conceived as a scientific and technological pathfinder to TPF/DARWIN as well as SPIRIT, SPECS, and SAFIR. It will also be a high angular resolution system complementary to JWST. The scientific emphasis of the mission is on the evolution of protostellar systems, from just after the collapse of the precursor molecular cloud core, through the formation of the disk surrounding the protostar, the formation of planets in the disk, and eventual dispersal of the disk material. FKSI will also search for brown dwarfs and Jupiter mass and smaller planets, and could also play a very powerful role in the investigation of the structure of active galactic nuclei and extra-galactic star formation. We report additional studies of the imaging capabilities of the FKSI with various configurations of two to five telescopes, studies of the capabilities of FKSI assuming an increase in long wavelength response to 10 or 12 microns (depending on availability of detectors), and preliminary results from our nulling testbed.

Sub-10-nm suspended nano-web formation by direct laser writing

NASA Astrophysics Data System (ADS)

Wang, Sihao; Yu, Ye; Liu, Hailong; Lim, Kevin T. P.; Madurai Srinivasan, Bharathi; Zhang, Yong Wei; Yang, Joel K. W.

2018-06-01

A diffraction-limited three-dimensional (3D) direct laser writing (DLW) system based on two-photon polymerization can routinely pattern structures at the 100 nm length scale. Several schemes have been developed to improve the patterning resolution of 3D DLW but often require customized resist formulations or multi-wavelength exposures. Here, we introduce a scheme to produce suspended nano-webs with feature sizes below 10 nm in IP-Dip resist using sub-threshold exposure conditions in a commercial DLW system. The narrowest suspended lines (nano-webs) measured 7 nm in width. Larger ∼20 nm nano-webs were patterned with ∼80% yield at increased laser powers. In addition, closely spaced nano-gaps with a center-to-center distance of 33 nm were produced by patterning vertically displaced suspended lines followed by metal deposition and liftoff. We provide hypotheses and present preliminary results for a mechanism involving the initiation of a percolative path and a strain-induced narrowing in the nano-web formation. Our approach allows selective features to be patterned with dimensions comparable to the sub-10 nm patterning capability of electron-beam lithography (EBL).

NanoSIMS for biological applications: Current practices and analyses

DOE PAGES

Nunez, Jamie R.; Renslow, Ryan S.; Cliff, III, John B.; ...

2017-09-27

Secondary ion mass spectrometry (SIMS) has become an increasingly utilized tool in biologically-relevant studies. Of these, high lateral resolution methodologies using the NanoSIMS 50/50L have been especially powerful within many biological fields over the past decade. Here, we provide a review of this technology, sample preparation and analysis considerations, examples of recent biological studies, data analysis, and current outlooks. Specifically, we offer an overview of SIMS and development of the NanoSIMS. We describe the major experimental factors that should be considered prior to NanoSIMS analysis and then provide information on best practices for data analysis and image generation, which includesmore » an in-depth discussion of appropriate colormaps. Additionally, we provide an open-source method for data representation that allows simultaneous visualization of secondary electron and ion information within a single image. Lastly, we present a perspective on the future of this technology and where we think it will have the greatest impact in near future.« less

NanoSIMS for biological applications: Current practices and analyses

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nunez, Jamie R.; Renslow, Ryan S.; Cliff, III, John B.

Secondary ion mass spectrometry (SIMS) has become an increasingly utilized tool in biologically-relevant studies. Of these, high lateral resolution methodologies using the NanoSIMS 50/50L have been especially powerful within many biological fields over the past decade. Here, we provide a review of this technology, sample preparation and analysis considerations, examples of recent biological studies, data analysis, and current outlooks. Specifically, we offer an overview of SIMS and development of the NanoSIMS. We describe the major experimental factors that should be considered prior to NanoSIMS analysis and then provide information on best practices for data analysis and image generation, which includesmore » an in-depth discussion of appropriate colormaps. Additionally, we provide an open-source method for data representation that allows simultaneous visualization of secondary electron and ion information within a single image. Lastly, we present a perspective on the future of this technology and where we think it will have the greatest impact in near future.« less

Kelvin-Helmholtz instability of counter-rotating discs

NASA Astrophysics Data System (ADS)

Quach, Dan; Dyda, Sergei; Lovelace, Richard V. E.

2015-01-01

Observations of galaxies and models of accreting systems point to the occurrence of counter-rotating discs where the inner part of the disc (r < r0) is corotating and the outer part is counter-rotating. This work analyses the linear stability of radially separated co- and counter-rotating thin discs. The strong instability found is the supersonic Kelvin-Helmholtz instability. The growth rates are of the order of or larger than the angular rotation rate at the interface. The instability is absent if there is no vertical dependence of the perturbation. That is, the instability is essentially three dimensional. The non-linear evolution of the instability is predicted to lead to a mixing of the two components, strong heating of the mixed gas, and vertical expansion of the gas, and annihilation of the angular momenta of the two components. As a result, the heated gas will free-fall towards the disc's centre over the surface of the inner disc.

Resolving the morphology of niobium carbonitride nano-precipitates in steel using atom probe tomography.

PubMed

Breen, Andrew J; Xie, Kelvin Y; Moody, Michael P; Gault, Baptiste; Yen, Hung-Wei; Wong, Christopher C; Cairney, Julie M; Ringer, Simon P

2014-08-01

Atom probe is a powerful technique for studying the composition of nano-precipitates, but their morphology within the reconstructed data is distorted due to the so-called local magnification effect. A new technique has been developed to mitigate this limitation by characterizing the distribution of the surrounding matrix atoms, rather than those contained within the nano-precipitates themselves. A comprehensive chemical analysis enables further information on size and chemistry to be obtained. The method enables new insight into the morphology and chemistry of niobium carbonitride nano-precipitates within ferrite for a series of Nb-microalloyed ultra-thin cast strip steels. The results are supported by complementary high-resolution transmission electron microscopy.

Application of Monte Carlo Method for Evaluation of Uncertainties of ITS-90 by Standard Platinum Resistance Thermometer

NASA Astrophysics Data System (ADS)

Palenčár, Rudolf; Sopkuliak, Peter; Palenčár, Jakub; Ďuriš, Stanislav; Suroviak, Emil; Halaj, Martin

2017-06-01

Evaluation of uncertainties of the temperature measurement by standard platinum resistance thermometer calibrated at the defining fixed points according to ITS-90 is a problem that can be solved in different ways. The paper presents a procedure based on the propagation of distributions using the Monte Carlo method. The procedure employs generation of pseudo-random numbers for the input variables of resistances at the defining fixed points, supposing the multivariate Gaussian distribution for input quantities. This allows taking into account the correlations among resistances at the defining fixed points. Assumption of Gaussian probability density function is acceptable, with respect to the several sources of uncertainties of resistances. In the case of uncorrelated resistances at the defining fixed points, the method is applicable to any probability density function. Validation of the law of propagation of uncertainty using the Monte Carlo method is presented on the example of specific data for 25 Ω standard platinum resistance thermometer in the temperature range from 0 to 660 °C. Using this example, we demonstrate suitability of the method by validation of its results.

Convectively coupled equatorial waves within the MJO during CINDY/DYNAMO: slow Kelvin waves as building blocks

NASA Astrophysics Data System (ADS)

Kikuchi, Kazuyoshi; Kiladis, George N.; Dias, Juliana; Nasuno, Tomoe

2018-06-01

This study examines the relationship between the MJO and convectively coupled equatorial waves (CCEWs) during the CINDY2011/DYNAMO field campaign using satellite-borne infrared radiation data, in order to better understand the interaction between convection and the large-scale circulation. The spatio-temporal wavelet transform (STWT) enables us to document the convective signals within the MJO envelope in terms of CCEWs in great detail, through localization of space-time spectra at any given location and time. Three MJO events that occurred in October, November, and December 2011 are examined. It is, in general, difficult to find universal relationships between the MJO and CCEWs, implying that MJOs are diverse in terms of the types of disturbances that make up its convective envelope. However, it is found in all MJO events that the major convective body of the MJO is made up mainly by slow convectively coupled Kelvin waves. These Kelvin waves have relatively fast phase speeds of 10-13 m s-1 outside of, and slow phase speeds of 8-9 m s-1 within the MJO. Sometimes even slower eastward propagating signals with 3-5 m s-1 phase speed show up within the MJO, which, as well as the slow Kelvin waves, appear to comprise major building blocks of the MJO. It is also suggested that these eastward propagating waves often occur coincident with n = 1 WIG waves, which is consistent with the schematic model from Nakazawa in 1988. Some practical aspects that facilitate use of the STWT are also elaborated upon and discussed.

A recipe to create nano-grains on dolomite

NASA Astrophysics Data System (ADS)

Røyne, Anja; Pluymakers, Anne

2017-04-01

Advances in imaging techniques in recent years have allowed for easy microstructure visualization at nano-resolution, and many studies have observed nano-grains in different materials, including rocks. An important example in geological systems is their seemingly ubiquitous occurrence on so-called mirror-like slip surfaces, produced in natural and experimental earthquakes of both carbonate and silicate rocks. It is, however, not yet clear whether these nano-grains can indeed be used as a reliable indicator of seismic slip. Since carbonates are prone to decarbonation at temperatures exceeding 550 - 600 °C, nano-grain formation may be formed due to heating rather than shear. In this study, we have investigated the effect of elevated temperatures on carbonate fault rocks. We used hand-polished mirror-like dolomite protolith, as well as natural fault mirror surfaces, obtained from the Foiana Fault Zone from the Southern Alps in Italy. The samples were heated to 200 to 800 degC in a 5 hour heating cycle, followed by slow cooling ( 12 h) to room temperature. Subsequently, we imaged the samples using SEM and AFM. Nano-grain formation on the surfaces of hand-polished samples starts around 400 ° C, and is pervasive at and above 600 ° C. Fault mirror samples are initially coated with naturally formed nano-grains and only very local patches on these surfaces display obvious morphological changes due to heating. Exposing both types of sample heated to 600 °C to DI water under the AFM shows rapid recrystallization and the formation of a more porous and blade-like crystal layer on the entire surface. This happens both in hand-polished and naturally polished surfaces. Fault mirror samples that have not been heated do not change when exposed to water. We have shown that nano-grains can form as a result of heating without shear, but that samples that have experienced high shear strain have a water- and heat-resistant coating composed of otherwise morphologically

Hollow Nanospheres Array Fabrication via Nano-Conglutination Technology.

PubMed

Zhang, Man; Deng, Qiling; Xia, Liangping; Shi, Lifang; Cao, Axiu; Pang, Hui; Hu, Song

2015-09-01

Hollow nanospheres array is a special nanostructure with great applications in photonics, electronics and biochemistry. The nanofabrication technique with high resolution is crucial to nanosciences and nano-technology. This paper presents a novel nonconventional nano-conglutination technology combining polystyrenes spheres (PSs) self-assembly, conglutination and a lift-off process to fabricate the hollow nanospheres array with nanoholes. A self-assembly monolayer of PSs was stuck off from the quartz wafer by the thiol-ene adhesive material, and then the PSs was removed via a lift-off process and the hollow nanospheres embedded into the thiol-ene substrate was obtained. Thiolene polymer is a UV-curable material via "click chemistry" reaction at ambient conditions without the oxygen inhibition, which has excellent chemical and physical properties to be attractive as the adhesive material in nano-conglutination technology. Using the technique, a hollow nanospheres array with the nanoholes at the diameter of 200 nm embedded into the rigid thiol-ene substrate was fabricated, which has great potential to serve as a reaction container, catalyst and surface enhanced Raman scattering substrate.

High-Resolution, Low-Cost Spectrometer-on-Chip

DTIC Science & Technology

2015-01-02

extracted for each PhCs for λ=400 and 500 nm, respectively; d) example of the spectral response of our prototype to two input filtered lights. aBeam...packed into the size of a USB key. Nano-spectrometers with a resolution down to 0.5 nm and a spectral range up to 229 nm were successfully demonstrated...Our miniaturized spectrometers are defining the state-of-the-art for on-chip spectroscopy, as well as in terms of spectral resolution and bandwidth

Kelvin waves in the tropical stratosphere observed in OMPS-LP ozone measurements

NASA Astrophysics Data System (ADS)

Randel, W. J.; Park, M.

2017-12-01

We investigate equatorial waves in the tropical stratosphere using OMPS limb profiler (LP) ozone measurements spanning 2012-2017. The OMPS-LP data show clear evidence of eastward propagating planetary-scale Kelvin waves with periods near 15-20 days, and these feature are strongly modulated by the background winds linked to the quasi-biennial oscillation (QBO). We study coherence between OMPS-LP ozone and GPS radio occultation temperature measurements, and use these analyses to evaluate data quality and variability in the tropical stratosphere.

Sphygmomanometers and thermometers as potential fomites of Staphylococcus haemolyticus: biofilm formation in the presence of antibiotics.

PubMed

Sued, Bruna Pinto Ribeiro; Pereira, Paula Marcele Afonso; Faria, Yuri Vieira; Ramos, Juliana Nunes; Binatti, Vanessa Batista; Santos, Kátia Regina Netto Dos; Seabra, Sérgio Henrique; Hirata, Raphael; Vieira, Verônica Viana; Mattos-Guaraldi, Ana Luíza; Pereira, José Augusto Adler

2017-03-01

The association between Staphylococcus haemolyticus and severe nosocomial infections is increasing. However, the extent to which fomites contribute to the dissemination of this pathogen through patients and hospital wards remains unknown. In the present study, sphygmomanometers and thermometers were evaluated as potential fomites of oxacillin-resistant S. haemolyticus (ORSH). The influence of oxacillin and vancomycin on biofilm formation by ORSH strains isolated from fomites was also investigated. The presence of ORSH on swabs taken from fomite surfaces in a Brazilian hospital was assessed using standard microbiological procedures. Antibiotic susceptibility profiles were determined by the disk diffusion method, and clonal distribution was assessed in pulsed-field gel electrophoresis (PFGE) assays. Minimum inhibitory concentrations (MICs) of oxacillin and vancomycin were evaluated via the broth microdilution method. Polymerase chain reaction (PCR) assays were performed to detect the mecA and icaAD genes. ORSH strains grown in media containing 1/4 MIC of vancomycin or oxacillin were investigated for slime production and biofilm formation on glass, polystyrene and polyurethane catheter surfaces. ORSH strains comprising five distinct PFGE types were isolated from sphygmomanometers (n = 5) and a thermometer (n = 1) used in intensive care units and surgical wards. ORSH strains isolated from fomites showed susceptibility to only linezolid and vancomycin and were characterised as multi-drug resistant (MDR). Slime production, biofilm formation and the survival of sessile bacteria differed and were independent of the presence of the icaAD and mecA genes, PFGE type and subtype. Vancomycin and oxacillin did not inhibit biofilm formation by vancomycin-susceptible ORSH strains on abiotic surfaces, including on the catheter surface. Enhanced biofilm formation was observed in some situations. Moreover, a sub-lethal dose of vancomycin induced biofilm formation by an ORSH strain on

Sphygmomanometers and thermometers as potential fomites of Staphylococcus haemolyticus: biofilm formation in the presence of antibiotics

PubMed Central

Sued, Bruna Pinto Ribeiro; Pereira, Paula Marcele Afonso; Faria, Yuri Vieira; Ramos, Juliana Nunes; Binatti, Vanessa Batista; dos Santos, Kátia Regina Netto; Seabra, Sérgio Henrique; Hirata, Raphael; Vieira, Verônica Viana; Mattos-Guaraldi, Ana Luíza; Pereira, José Augusto Adler

2017-01-01

BACKGROUND The association between Staphylococcus haemolyticus and severe nosocomial infections is increasing. However, the extent to which fomites contribute to the dissemination of this pathogen through patients and hospital wards remains unknown. OBJECTIVES In the present study, sphygmomanometers and thermometers were evaluated as potential fomites of oxacillin-resistant S. haemolyticus (ORSH). The influence of oxacillin and vancomycin on biofilm formation by ORSH strains isolated from fomites was also investigated. METHODS The presence of ORSH on swabs taken from fomite surfaces in a Brazilian hospital was assessed using standard microbiological procedures. Antibiotic susceptibility profiles were determined by the disk diffusion method, and clonal distribution was assessed in pulsed-field gel electrophoresis (PFGE) assays. Minimum inhibitory concentrations (MICs) of oxacillin and vancomycin were evaluated via the broth microdilution method. Polymerase chain reaction (PCR) assays were performed to detect the mecA and icaAD genes. ORSH strains grown in media containing 1/4 MIC of vancomycin or oxacillin were investigated for slime production and biofilm formation on glass, polystyrene and polyurethane catheter surfaces. FINDINGS ORSH strains comprising five distinct PFGE types were isolated from sphygmomanometers (n = 5) and a thermometer (n = 1) used in intensive care units and surgical wards. ORSH strains isolated from fomites showed susceptibility to only linezolid and vancomycin and were characterised as multi-drug resistant (MDR). Slime production, biofilm formation and the survival of sessile bacteria differed and were independent of the presence of the icaAD and mecA genes, PFGE type and subtype. Vancomycin and oxacillin did not inhibit biofilm formation by vancomycin-susceptible ORSH strains on abiotic surfaces, including on the catheter surface. Enhanced biofilm formation was observed in some situations. Moreover, a sub-lethal dose of vancomycin induced

Kelvin-Helmholtz instability of stratified jets.

NASA Astrophysics Data System (ADS)

Hanasz, M.; Sol, H.

1996-11-01

We investigate the Kelvin-Helmholtz instability of stratified jets. The internal component (core) is made of a relativistic gas moving with a relativistic bulk speed. The second component (sheath or envelope) flows between the core and external gas with a nonrelativistic speed. Such a two-component jet describes a variety of possible astrophysical jet configurations like e.g. (1) a relativistic electron-positron beam penetrating a classical electron-proton disc wind or (2) a beam-cocoon structure. We perform a linear stability analysis of such a configuration in the hydrodynamic, plane-parallel, vortex-sheet approximation. The obtained solutions of the dispersion relation show very apparent differences with respect to the single-jet solutions. Due to the reflection of sound waves at the boundary between sheet and external gas, the growth rate as a function of wavenumber presents a specific oscillation pattern. Overdense sheets can slow down the growth rate and contribute to stabilize the configuration. Moreover, we obtain the result that even for relatively small sheet widths the properties of sheet start to dominate the jet dynamics. Such effects could have important astrophysical implications, for instance on the origin of the dichotomy between radio-loud and radio-quiet objects.

Asymmetric Kelvin-Helmholtz Instability at Jupiter's Magnetopause Boundary: Implications for Corotation-Dominated Systems

NASA Astrophysics Data System (ADS)

Zhang, B.; Delamere, P. A.; Ma, X.; Burkholder, B.; Wiltberger, M.; Lyon, J. G.; Merkin, V. G.; Sorathia, K. A.

2018-01-01

The multifluid Lyon-Fedder-Mobarry (MFLFM) global magnetosphere model is used to study the interactions between solar wind and rapidly rotating, internally driven Jupiter magnetosphere. The MFLFM model is the first global simulation of Jupiter magnetosphere that captures the Kelvin-Helmholtz instability (KHI) in the critically important subsolar region. Observations indicate that Kelvin-Helmholtz vortices are found predominantly in the dusk sector. Our simulations explain that this distribution is driven by the growth of KHI modes in the prenoon and subsolar region (e.g., >10 local time) that are advected by magnetospheric flows to the dusk sector. The period of density fluctuations at the dusk terminator flank (18 magnetic local time, MLT) is roughly 1.4 h compared with 7.2 h at the dawn flank (6 MLT). Although the simulations are only performed using parameters of the Jupiter's magnetosphere, the results may also have implications for solar wind-magnetosphere interactions at other corotation-dominated systems such as Saturn. For instance, the simulated average azimuthal speed of magnetosheath flows exhibit significant dawn-dusk asymmetry, consistent with recent observations at Saturn. The results are particularly relevant for the ongoing Juno mission and the analysis of dawnside magnetopause boundary crossings for other planetary missions.

Symmetry classes of the anisotropy tensors of quasielastic materials and a generalized Kelvin approach

NASA Astrophysics Data System (ADS)

Ostrosablin, N. I.

2017-05-01

The anisotropy matrices (tensors) of quasielastic (Cauchy-elastic) materials were obtained for all classes of crystallographic symmetries in explicit form. The fourth-rank anisotropy tensors of such materials do not have the main symmetry, in which case the anisotropy matrix is not symmetric. As a result of introducing various bases in the space of symmetric stress and strain tensors, the linear relationship between stresses and strains is represented in invariant form similar to the form in which generalized Hooke's law is written for the case of anisotropic hyperelastic materials and contains six positive Kelvin eigen moduli. It is shown that the introduction of modified rotation-induced deformation in the strain space can cause a transition to the symmetric anisotropy matrix observed in the case of hyperelasticity. For the case of transverse isotropy, there are examples of determination of the Kelvin eigen moduli and eigen bases and the rotation matrix in the strain space. It is shown that there is a possibility of existence of quasielastic media with a skew-symmetric anisotropy matrix with no symmetric part. Some techniques for the experimental testing of the quasielasticity model are proposed.

Evolution of the magnesium incorporated amorphous calcium phosphate to nano-crystallized hydroxyapatite in alkaline solution

NASA Astrophysics Data System (ADS)

Zhang, Xiao-Juan; Lin, Dong-Yang; Yan, Xiao-Hui; Wang, Xiao-Xiang

2011-12-01

A homogeneous amorphous calcium phosphate (ACP) coating containing magnesium was achieved on titanium substrates by electrochemical deposition (ECD). Its amorphous structure is confirmed by transmission electron microscope (TEM) together with grazing reflection absorption infrared spectroscopy (IR) spectrometer. In the images of high-resolution transmission electron microscope (HRTEM), the ACP spheres are assembled by nano-particles with the diameter of 5-10 nm. In the alkaline environment, nucleation of hydroxyapatite (HAP) occurs on the surfaces of ACP spheres. By consuming the Ca and PO 4 ions inside the ACP spheres, the HAP nuclei grow outward. Confirmed by TEM, the ACP spheres converse to hollow HAP spheres composed of HAP nano-needles. The coating is finally constructed by the HAP nano-needles, which are themselves aggregated by numerous nano-particles.

Jason Celebrates 5th Anniversary as El Niño Builds, Warm Kelvin Wave Surges Toward South America

NASA Image and Video Library

2006-12-07

Recent sea-level height data from NASA Jason-1 altimetric satellite show that continuing weaker-than-normal trade winds in the western and central equatorial Pacific have triggered another strong, eastward moving, warm Kelvin wave.

Catalytic graphitization behavior of phenolic resins by addition of in situ formed nano-Fe particles

NASA Astrophysics Data System (ADS)

Rastegar, H.; Bavand-vandchali, M.; Nemati, A.; Golestani-Fard, F.

2018-07-01

This work presents the catalytic graphitization process of phenolic resins (PR's) by addition of in situ nano-Fe particles as catalyst. Pyrolysis treatments of prepared compositions including various contents of nano-Fe particles were carried out at 600-1200 °C for 3 h under reducing atmosphere and graphitization process were evaluated by different techniques such as X-Ray diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), High Resolution Transmission Electron Microscopy (HRTEM), Simultaneous Thermal Analysis (STA) and Raman spectroscopy that mainly performed to identify the phase and microstructural analysis, oxidation resistance and extend of graphitized carbon formation. Results indicate that, in situ graphitic carbon development were already observed after firing the samples at 800 °C for 3 h under reducing atmosphere, increasing temperature and amount of nano-Fe led to a more effective graphitization level. In addition, the different nano crystalline carbon shapes such as onion and bamboo like and carbon nanotubes (CNTs) were in situ identified during graphitization process of nano-Fe containing samples. It was suggested that formation of these different nano carbon structures related to nano-Fe catalyst behavior and the carbon shell growth.

Environmental risk assessment of engineered nano-SiO2 , nano iron oxides, nano-CeO2 , nano-Al2 O3 , and quantum dots.

PubMed

Wang, Yan; Nowack, Bernd

2018-05-01

Many research studies have endeavored to investigate the ecotoxicological hazards of engineered nanomaterials (ENMs). However, little is known regarding the actual environmental risks of ENMs, combining both hazard and exposure data. The aim of the present study was to quantify the environmental risks for nano-Al 2 O 3 , nano-SiO 2 , nano iron oxides, nano-CeO 2 , and quantum dots by comparing the predicted environmental concentrations (PECs) with the predicted-no-effect concentrations (PNECs). The PEC values of these 5 ENMs in freshwaters in 2020 for northern Europe and southeastern Europe were taken from a published dynamic probabilistic material flow analysis model. The PNEC values were calculated using probabilistic species sensitivity distribution (SSD). The order of the PNEC values was quantum dots < nano-CeO 2  < nano iron oxides < nano-Al 2 O 3  < nano-SiO 2 . The risks posed by these 5 ENMs were demonstrated to be in the reverse order: nano-Al 2 O 3  > nano-SiO 2  > nano iron oxides > nano-CeO 2  > quantum dots. However, all risk characterization values are 4 to 8 orders of magnitude lower than 1, and no risk was therefore predicted for any of the investigated ENMs at the estimated release level in 2020. Compared to static models, the dynamic material flow model allowed us to use PEC values based on a more complex parameterization, considering a dynamic input over time and time-dependent release of ENMs. The probabilistic SSD approach makes it possible to include all available data to estimate hazards of ENMs by considering the whole range of variability between studies and material types. The risk-assessment approach is therefore able to handle the uncertainty and variability associated with the collected data. The results of the present study provide a scientific foundation for risk-based regulatory decisions of the investigated ENMs. Environ Toxicol Chem 2018;37:1387-1395. © 2018 SETAC. © 2018 SETAC.

High resolution subsurface imaging using resonance-enhanced detection in 2nd-harmonic KPFM.

PubMed

Cadena, Maria Jose; Reifenberger, Ronald G; Raman, Arvind

2018-06-28

Second harmonic Kelvin probe force microscopy is a robust mechanism for subsurface imaging at the nanoscale. Here we exploit resonance-enhanced detection as a way to boost the subsurface contrast with higher force sensitivity using lower bias voltages, in comparison to the traditional off-resonance case. In this mode, the second harmonic signal of the electrostatic force is acquired at one of the eigenmode frequencies of the microcantilever. As a result, high-resolution subsurface images are obtained in a variety of nanocomposites. To further understand the subsurface imaging detection upon electrostatic forces, we use a finite element model that approximates the geometry of the probe and sample. This allows the investigation of the contrast mechanism, the depth sensitivity and lateral resolution depending on tip-sample properties. © 2018 IOP Publishing Ltd.

Anomalous electronic heat capacity of copper nanowires at sub-Kelvin temperatures

NASA Astrophysics Data System (ADS)

Viisanen, K. L.; Pekola, J. P.

2018-03-01

We have measured the electronic heat capacity of thin film nanowires of copper and silver at temperatures 0.1-0.3 K; the films were deposited by standard electron-beam evaporation. The specific heat of the Ag films of sub-100-nm thickness agrees with the bulk value and the free-electron estimate, whereas that of similar Cu films exceeds the corresponding reference values by one order of magnitude. The origin of the anomalously high heat capacity of copper films remains unknown for the moment. Based on the small heat capacity at low temperatures and the possibility to devise a tunnel probe thermometer on it, metal films form a promising absorber material, e.g., for microwave photon calorimetry.

Nano-Electrochemistry and Nano-Electrografting with an Original Combined AFM-SECM

PubMed Central

Ghorbal, Achraf; Grisotto, Federico; Charlier, Julienne; Palacin, Serge; Goyer, Cédric; Demaille, Christophe; Ben Brahim, Ammar

2013-01-01

This study demonstrates the advantages of the combination between atomic force microscopy and scanning electrochemical microscopy. The combined technique can perform nano-electrochemical measurements onto agarose surface and nano-electrografting of non-conducting polymers onto conducting surfaces. This work was achieved by manufacturing an original Atomic Force Microscopy-Scanning ElectroChemical Microscopy (AFM-SECM) electrode. The capabilities of the AFM-SECM-electrode were tested with the nano-electrografting of vinylic monomers initiated by aryl diazonium salts. Nano-electrochemical and technical processes were thoroughly described, so as to allow experiments reproducing. A plausible explanation of chemical and electrochemical mechanisms, leading to the nano-grafting process, was reported. This combined technique represents the first step towards improved nano-processes for the nano-electrografting. PMID:28348337

Collision-Induced Infrared Absorption by Collisional Complexes in Dense Hydrogen-Helium Gas Mixtures at Thousands of Kelvin

NASA Astrophysics Data System (ADS)

Abel, Martin; Frommhold, Lothar; Li, Xiaoping; Hunt, Katharine L. C.

2011-06-01

The interaction-induced absorption by collisional pairs of H{_2} molecules is an important opacity source in the atmospheres of the outer planets and cool stars. The emission spectra of cool white dwarf stars differ significantly in the infrared from the expected blackbody spectra of their cores, which is largely due to absorption by collisional H{_2}-H{_2}, H{_2}-He, and H{_2}-H complexes in the stellar atmospheres. Using quantum-chemical methods we compute the atmospheric absorption from hundreds to thousands of kelvin. Laboratory measurements of interaction-induced absorption spectra by H{_2} pairs exist only at room temperature and below. We show that our results reproduce these measurements closely, so that our computational data permit reliable modeling of stellar atmosphere opacities even for the higher temperatures. L. Frommhold, Collision-Induced Absorption in Gases, Cambridge University Press, Cambridge, New York, 1993 and 2006 Xiaoping Li, Katharine L. C. Hunt, Fei Wang, Martin Abel, and Lothar Frommhold, "Collision-Induced Infrared Absorption by Molecular Hydrogen Pairs at Thousands of Kelvin", International Journal of Spectroscopy, vol. 2010, Article ID 371201, 11 pages, 2010. doi: 10.1155/2010/371201 M. Abel, L. Frommhold, X. Li, and K. L. C. Hunt, "Collision-induced absorption by H{_2} pairs: From hundreds to thousands of Kelvin," J. Phys. Chem. A, published online, DOI: 10.1021/jp109441f L. Frommhold, M. Abel, F. Wang, M. Gustafsson, X. Li, and K. L. C. Hunt, "Infrared atmospheric emission and absorption by simple molecular complexes, from first principles", Mol. Phys. 108, 2265, 2010

Observations of Confinement of a Paramagnetic Liquid in Model Propellant Tanks in Microgravity by the Kelvin Force

NASA Technical Reports Server (NTRS)

Kuhlman, John; Gray, Donald D.; Barnard, Austin; Hazelton, Jennifer; Lechliter, Matthew; Starn, Andrew; Battleson, Charles; Glaspell, Shannon; Kreitzer, Paul; Leichliter, Michelle

2002-01-01

The magnetic Kelvin force has been proposed as an artificial gravity to control the orientation of paramagnetic liquid propellants such as liquid oxygen in a microgravity environment. This paper reports experiments performed in the NASA "Weightless Wonder" KC-135 aircraft, through the Reduced Gravity Student Flight Opportunities Program. The aircraft flies through a series of parabolic arcs providing about 25 s of microgravity in each arc. The experiment was conceived, designed, constructed, and performed by the undergraduate student team and their two faculty advisors. Two types of tanks were tested: square-base prismatic tanks 5 cm x 5 cm x 8.6 cm and circular cylinders 5 cm in diameter and 8.6 cm tall. The paramagnetic liquid was a 3.3 molar solution of MnCl2 in water. Tests were performed with each type of tank filled to depths of 1 cm and 4 cm. Each test compared a pair of tanks that were identical except that the base of one was a pole face of a 0.6 Tesla permanent magnet. The Kelvin force attracts paramagnetic materials toward regions of higher magnetic field. It was hypothesized that the Kelvin force would hold the liquid in the bottom of the tanks during the periods of microgravity. The tanks were installed in a housing that could slide on rails transverse to the flight direction. By manually shoving the housing, an identical impulse could be provided to each tank at the beginning of each period of microgravity. The resulting fluid motions were videotaped for later analysis.

Bloch-Nordsieck thermometers: one-loop exponentiation in finite temperature QED

NASA Astrophysics Data System (ADS)

Gupta, Sourendu; Indumathi, D.; Mathews, Prakash; Ravindran, V.

1996-02-01

We study the scattering of hard external particles in a heat bath in a real-time formalism for finite temperature QED. We investigate the distribution of the 4-momentum difference of initial and final hard particles in a fully covariant manner when the scale of the process, Q, is much larger than the temperature, T. Our computations are valid for all T subject to this constraint. We exponentiate the leading infra-red term at one-loop order through a resummation of soft (thermal) photon emissions and absorptions. For T > 0, we find that tensor structures arise which are not present at T = 0. These cant' thermal signatures. As a result, external particles can serve as thermometers introduced into the heat bath. We investigate the phase space origin of log( Q/ m) and log ( Q/ T) teens.

Measurement of body temperature in 300 dogs with a novel noncontact infrared thermometer on the cornea in comparison to a standard rectal digital thermometer.

PubMed

Kreissl, Hannah; Neiger, Reto

2015-01-01

To assess the accuracy of obtaining body temperatures in dogs with a noncontact infrared thermometer (NCIT) on the cornea compared with a rectal digital thermometer (RDT). Prospective single center study. University teaching hospital. Three hundred dogs presented with low, normal, or high body temperatures. Three body temperature readings were measured by an RDT and by an NCIT on the cornea of the left eye by 2 investigators (experienced and inexperienced). Results obtained by the 2 methods were compared. Median body temperature measured by the experienced investigator with the RDT and the NCIT were 38.3°C (range 35.5°C-41.1°C; 95% CI: 38.2-38.4°C) and 37.7°C (35.9°C-40.1°C; 95% CI: 37.7°C-37.9°C), respectively. Measurement of RDT as well as of NCIT correlated well between both investigators (rRDT = 0.94; rNCIT = 0.82; respectively, P < 0.001 for both methods). Mean RDT and NCIT-temperature correlated poorly (r = 0.43; P < 0.001) when taken by the experienced investigator and even less by the nonexperienced investigator (r = 0.38; P < 0.001). Repeatability of the NCIT revealed an unsatisfactory value (0.24°C) compared to RDT measurement (0.12°C). Agreement between both devices in measuring low, normal, and high values, calculated by Cohens-Kappa, was unsatisfactory (к = 0.201; P < 0.001). Calculating the receiver operating characteristic curve to determine the best threshold for fever (defined as RDT temperature >39.0°C) showed an area under the curve of 0.76. Mean discomfort score was significantly lower using NCIT compared to RDT measurement (P < 0.001). There was poor agreement between body temperatures obtained by RDT and NCIT. The corneal NCIT measurement tends to underrecognize hypothermic and hyperthermic conditions. Although the use of the NCIT yields faster results and is significantly more comfortable for the dog than the RDT measurement, it cannot be recommended in dogs at this time. © Veterinary Emergency and Critical Care Society 2015.

Micro/nano-computed tomography technology for quantitative dynamic, multi-scale imaging of morphogenesis.

PubMed

Gregg, Chelsea L; Recknagel, Andrew K; Butcher, Jonathan T

2015-01-01

Tissue morphogenesis and embryonic development are dynamic events challenging to quantify, especially considering the intricate events that happen simultaneously in different locations and time. Micro- and more recently nano-computed tomography (micro/nanoCT) has been used for the past 15 years to characterize large 3D fields of tortuous geometries at high spatial resolution. We and others have advanced micro/nanoCT imaging strategies for quantifying tissue- and organ-level fate changes throughout morphogenesis. Exogenous soft tissue contrast media enables visualization of vascular lumens and tissues via extravasation. Furthermore, the emergence of antigen-specific tissue contrast enables direct quantitative visualization of protein and mRNA expression. Micro-CT X-ray doses appear to be non-embryotoxic, enabling longitudinal imaging studies in live embryos. In this chapter we present established soft tissue contrast protocols for obtaining high-quality micro/nanoCT images and the image processing techniques useful for quantifying anatomical and physiological information from the data sets.

Nano-antenna in a photoconductive photomixer for highly efficient continuous wave terahertz emission

PubMed Central

Tanoto, H.; Teng, J. H.; Wu, Q. Y.; Sun, M.; Chen, Z. N.; Maier, S. A.; Wang, B.; Chum, C. C.; Si, G. Y.; Danner, A. J.; Chua, S. J.

2013-01-01

We report highly efficient continuous-wave terahertz (THz) photoconductive antenna based photomixer employing nano-gap electrodes in the active region. The tip-to-tip nano-gap electrode structure provides strong THz field enhancement and acts as a nano-antenna to radiate the THz wave generated in the active region of the photomixer. In addition, it provides good impedance matching to the THz planar antenna and exhibits a lower RC time constant, allowing more efficient radiation especially at the higher part of the THz spectrum. As a result, the output intensity of the photomixer with the new nano-gap electrode structure in the active region is two orders of magnitude higher than that of a photomixer with typical interdigitated electrodes. Significant improvement in the THz emission bandwidth was also observed. An efficient continuous wave THz source will greatly benefit compact THz system development for high resolution THz spectroscopy and imaging applications. PMID:24100840

SAO and Kelvin Waves in the EuroGRIPS GCMS and the UK Meteorological Offices Analyses

NASA Technical Reports Server (NTRS)

Amodei, M.; Pawson, S.; Scaife, A. A.; Lahoz, W.; Langematz, U.; Li, Ding Min; Simon, P.

2000-01-01

This work is an intercomparison of four tropospheric-stratospheric climate models, the Unified Model (UM) of the U.K. Meteorological Office (UKMO), the model of the Free University in Berlin (FUB). the ARPEGE-climat model of the National Center for Meteorological Research (CNRM), and the Extended UGAMP GCM (EUGCM) of the Center for Global Atmospheric Modelling (CGAM), against the UKMO analyses. This comparison has been made in the framework of the "GSM-Reality Intercomparison Project for SPARC" (GRIPS). SPARC (Stratospheric Processes and their Role in Climate) aims are to investigate the effects of the middle atmosphere on climate and the GRIPS purpose is to organized a comprehensive assessment of current Middle Atmosphere-Climate Models (MACMs). The models integrations were made without identical contraints e.g. boundary conditions, incoming solar radiation). All models are able to represent the dominant features of the extratropical circulation. In this paper, the structure of the tropical winds and the strengths of the Kelvin waves are examined. Explanations for the differences exhibited. between the models. as well as between models and analyses, are also proposed. In the analyses a rich spectrum of waves (eastward and westward) is present and contributes to drive the SAO (SemiAnnual Oscillation) and the QBO (Quasi-Biennal Oscillation). The amplitude of the Kelvin waves is close to the one observed in UARS (Upper Atmosphere Research Satellite) data. In agreement with observations, the Kelvin waves generated in the models propagate into the middle atmosphere as wave packets which underlines convective forcing origin. In most models, slow Kelvin waves propagate too high and are hence overestimated in the upper stratosphere and in the mesosphere, except for the UM which is more diffusive. These waves are not sufficient to force realistic westerlies of the QBO or SAO westerly phases. If the SAO is represented by all models only two of them are able to generate

Electrospray neutralization process and apparatus for generation of nano-aerosol and nano-structured materials

DOEpatents

Bailey, Charles L.; Morozov, Victor; Vsevolodov, Nikolai N.

2010-08-17

The claimed invention describes methods and apparatuses for manufacturing nano-aerosols and nano-structured materials based on the neutralization of charged electrosprayed products with oppositely charged electrosprayed products. Electrosprayed products include molecular ions, nano-clusters and nano-fibers. Nano-aerosols can be generated when neutralization occurs in the gas phase. Neutralization of electrospan nano-fibers with molecular ions and charged nano-clusters may result in the formation of fibrous aerosols or free nano-mats. Nano-mats can also be produced on a suitable substrate, forming efficient nano-filters.

Method to obtain carbon nano-onions by pyrolisys of propane

NASA Astrophysics Data System (ADS)

Garcia-Martin, Tomas; Rincon-Arevalo, Pedro; Campos-Martin, Gemma

2013-11-01

We present a new and simple method for carbon nano-onions (CNOs) production which is based on the pyrolysis of Propane. CNOs are originated in a laminar premixed Propane/Oxygen flame of approximately 1.8 of stoichiometric coefficient. The stream of gasses resulting from the combustion drives the carbon particles towards the aluminium surface on which nano-onions are deposited and collected. The structure and size of the deposited carbon onion on the metal wall are characterized by High Resolution Transmission Electron Microscopy technique (HRTEM). The experimental images show the presence of two different types of CNOs. The first particles have diameters in the range of 18-25 nm and the second ones around 10 nm.

Edge contact angle and modified Kelvin equation for condensation in open pores.

PubMed

Malijevský, Alexandr; Parry, Andrew O; Pospíšil, Martin

2017-08-01

We consider capillary condensation transitions occurring in open slits of width L and finite height H immersed in a reservoir of vapor. In this case the pressure at which condensation occurs is closer to saturation compared to that occurring in an infinite slit (H=∞) due to the presence of two menisci that are pinned near the open ends. Using macroscopic arguments, we derive a modified Kelvin equation for the pressure p_{cc}(L;H) at which condensation occurs and show that the two menisci are characterized by an edge contact angle θ_{e} that is always larger than the equilibrium contact angle θ, only equal to it in the limit of macroscopic H. For walls that are completely wet (θ=0) the edge contact angle depends only on the aspect ratio of the capillary and is well described by θ_{e}≈sqrt[πL/2H] for large H. Similar results apply for condensation in cylindrical pores of finite length. We test these predictions against numerical results obtained using a microscopic density-functional model where the presence of an edge contact angle characterizing the shape of the menisci is clearly visible from the density profiles. Below the wetting temperature T_{w} we find very good agreement for slit pores of widths of just a few tens of molecular diameters, while above T_{w} the modified Kelvin equation only becomes accurate for much larger systems.

A Systematic Study of Kelvin-Helmholtz Instability in Galaxy Clusters

NASA Astrophysics Data System (ADS)

Su, Yuanyuan

2017-09-01

Kelvin-Helmholtz instabilities (KHI) were observed at cold fronts in a handful of clusters. KHI are predicted at all cold fronts in hydro simulation of intracluster medium (ICM). Their presence and absence provides a unique probe of transport processes in the hot plasma, which are essential to the dissipation and redistribution of the energy in the ICM. We propose the first systematic study of the prevalence of KHI in galaxy clusters by analyzing the archived Chandra observations of a sample of 50 nearby galaxy clusters. We will associate the occurrence and properties of KHI rolls with various cluster parameters such as their gas temperature and density, and put constraints on effective transport coefficients in the ICM

The Missing Link Coupling the Foreshock to the Magnetosphere?: Impact of the Magnetosheath Velocity Fluctuations on the Growth of the Kelvin-Helmholtz instability.

NASA Astrophysics Data System (ADS)

Nykyri, K.; Dimmock, A. P.; Pulkkinen, T. I.; Otto, A.; Ma, X.

2014-12-01

Our statistical study of magnetosheath velocity fluctuations using 6+ years of THEMIS spacecraft measurements in Magnetosheath InterPlanetary Medium (MIPM) reference frame show that amplitudes of the velocity fluctuations are enhanced in the magnetosheath downstream of the quasi-parallel shock. The fluctuation amplitudes can be substantial and frequencies of these flcutuations can vary. We have examined the role of the i) amplitude, ii) frequency, iii) number of the modes, iv) as well as mode combinations of magnetosheath velocity fluctuations on the growth of Kelvin-Helmholtz Instability (KHI) using high-resolution macro-scale MHD simulations in magnetospheric inertial frame. The results show that even for the same magnetic field and plasma parameters across the magnetopause there can be major differences due to 'magnetosheath fluctuation state' on the growth and dynamical evolution of the KHI. This may provide the missing link how foreshock fluctuations couple to the magnetosphere and into the ionosphere

A comparison of absolute calibrations of a radiation thermometer based on a monochromator and a tunable source

NASA Astrophysics Data System (ADS)

Keawprasert, T.; Anhalt, K.; Taubert, D. R.; Sperling, A.; Schuster, M.; Nevas, S.

2013-09-01

An LP3 radiation thermometer was absolutely calibrated at a newly developed monochromator-based set-up and the TUneable Lasers in Photometry (TULIP) facility of PTB in the wavelength range from 400 nm to 1100 nm. At both facilities, the spectral radiation of the respective sources irradiates an integrating sphere, thus generating uniform radiance across its precision aperture. The spectral irradiance of the integrating sphere is determined via an effective area of a precision aperture and a Si trap detector, traceable to the primary cryogenic radiometer of PTB. Due to the limited output power from the monochromator, the absolute calibration was performed with the measurement uncertainty of 0.17 % (k = 1), while the respective uncertainty at the TULIP facility is 0.14 %. Calibration results obtained by the two facilities were compared in terms of spectral radiance responsivity, effective wavelength and integral responsivity. It was found that the measurement results in integral responsivity at the both facilities are in agreement within the expanded uncertainty (k = 2). To verify the calibration accuracy, the absolutely calibrated radiation thermometer was used to measure the thermodynamic freezing temperatures of the PTB gold fixed-point blackbody.

Barrier properties of nano silicon carbide designed chitosan nanocomposites.

PubMed

Pradhan, Gopal C; Dash, Satyabrata; Swain, Sarat K

2015-12-10

Nano silicon carbide (SiC) designed chitosan nanocomposites were prepared by solution technique. Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD) were used for studying structural interaction of nano silicon carbide (SiC) with chitosan. The morphology of chitosan/SiC nanocomposites was investigated by field emission scanning electron microscope (FESEM), and high resolution transmission electron microscope (HRTEM). The thermal stability of chitosan was substantially increased due to incorporation of stable silicon carbide nanopowder. The oxygen permeability of chitosan/SiC nanocomposites was reduced by three folds as compared to the virgin chitosan. The chemical resistance properties of chitosan were enhanced due to the incorporation of nano SiC. The biodegradability was investigated using sludge water. The tensile strength of chitosan/SiC nanocomposites was increased with increasing percentage of SiC. The substantial reduction in oxygen barrier properties in combination with increased thermal stability, tensile strength and chemical resistance properties; the synthesized nanocomposite may be suitable for packaging applications. Copyright © 2015 Elsevier Ltd. All rights reserved.

Kelvin probe microscopic visualization of charge storage at polystyrene interfaces with pentacene and gold

NASA Astrophysics Data System (ADS)

Dawidczyk, T. J.; Johns, G. L.; Ozgun, R.; Alley, O.; Andreou, A. G.; Markovic, N.; Katz, H. E.

2012-02-01

Charge carriers trapped in polystyrene (PS) were investigated with Kelvin probe microscopy (KPM) and thermally stimulated discharge current (TSDC). Lateral heterojunctions of pentacene/PS were scanned using KPM, effectively observing polarization along a side view of a lateral nonvolatile organic field-effect transistor dielectric interface. TSDC was used to observe charge migration out of PS films and to estimate the trap energy level inside the PS, using the initial rise method.

What model resolution is required in climatological downscaling over complex terrain?

NASA Astrophysics Data System (ADS)

El-Samra, Renalda; Bou-Zeid, Elie; El-Fadel, Mutasem

2018-05-01

This study presents results from the Weather Research and Forecasting (WRF) model applied for climatological downscaling simulations over highly complex terrain along the Eastern Mediterranean. We sequentially downscale general circulation model results, for a mild and wet year (2003) and a hot and dry year (2010), to three local horizontal resolutions of 9, 3 and 1 km. Simulated near-surface hydrometeorological variables are compared at different time scales against data from an observational network over the study area comprising rain gauges, anemometers, and thermometers. The overall performance of WRF at 1 and 3 km horizontal resolution was satisfactory, with significant improvement over the 9 km downscaling simulation. The total yearly precipitation from WRF's 1 km and 3 km domains exhibited < 10% bias with respect to observational data. The errors in minimum and maximum temperatures were reduced by the downscaling, along with a high-quality delineation of temperature variability and extremes for both the 1 and 3 km resolution runs. Wind speeds, on the other hand, are generally overestimated for all model resolutions, in comparison with observational data, particularly on the coast (up to 50%) compared to inland stations (up to 40%). The findings therefore indicate that a 3 km resolution is sufficient for the downscaling, especially that it would allow more years and scenarios to be investigated compared to the higher 1 km resolution at the same computational effort. In addition, the results provide a quantitative measure of the potential errors for various hydrometeorological variables.

Kelvin-Helmholtz instability: the ``atom'' of geophysical turbulence?

NASA Astrophysics Data System (ADS)

Smyth, William

2017-11-01

Observations of small-scale turbulence in Earth's atmosphere and oceans have most commonly been interpreted in terms of the Kolmogorov theory of isotropic turbulence, despite the fact that the observed turbulence is significantly anisotropic due to density stratification and sheared large-scale flows. I will describe an alternative picture in which turbulence consists of distinct events that occur sporadically in space and time. The simplest model for an individual event is the ``Kelvin-Helmholtz (KH) ansatz'', in which turbulence relieves the dynamic instability of a localized shear layer. I will summarize evidence that the KH ansatz is a valid description of observed turbulence events, using microstructure measurements from the equatorial Pacific ocean as an example. While the KH ansatz has been under study for many decades and is reasonably well understood, the bigger picture is much less clear. How are the KH events distributed in space and time? How do different events interact with each other? I will describe some tentative steps toward a more thorough understanding.

The Fourier Kelvin Stellar Interferometer (FKSI): A Progress Report and Update

NASA Technical Reports Server (NTRS)

Danchi, William C.; Barry, R. K.; Traub, W. A.; Unwin, S.

2008-01-01

The Fourier-Kelvin Stellar Interferometer (FKSI) mission is a two-telescope infrared space interferometer with a 12.5 meter baseline on a boom, operating from 3-8 (or 10) microns, and passively cooled to about 60 K. The main goals for the mission are the measurement an characterization of the exozodiacal light around nearby stars, debris disks, and characterization of the atmospheres of known exoplanets. We discuss progress on this mission in the context of the recent call from NASA for mission concepts for the upcoming National Academy of Sciences Decadal Survey, where it is considered a medium class mission ($600-800 million) in terms of the overall budget.

Kelvin probe force microscopy studies of the charge effects upon adsorption of carbon nanotubes and C60 fullerenes on hydrogen-terminated diamond

NASA Astrophysics Data System (ADS)

Kölsch, S.; Fritz, F.; Fenner, M. A.; Kurch, S.; Wöhrl, N.; Mayne, A. J.; Dujardin, G.; Meyer, C.

2018-01-01

Hydrogen-terminated diamond is known for its unusually high surface conductivity that is ascribed to its negative electron affinity. In the presence of acceptor molecules, electrons are expected to transfer from the surface to the acceptor, resulting in p-type surface conductivity. Here, we present Kelvin probe force microscopy (KPFM) measurements on carbon nanotubes and C60 adsorbed onto a hydrogen-terminated diamond(001) surface. A clear reduction in the Kelvin signal is observed at the position of the carbon nanotubes and C60 molecules as compared with the bare, air-exposed surface. This result can be explained by the high positive electron affinity of carbon nanotubes and C60, resulting in electron transfer from the surface to the adsorbates. When an oxygen-terminated diamond(001) is used instead, no reduction in the Kelvin signal is obtained. While the presence of a charged adsorbate or a difference in work function could induce a change in the KPFM signal, a charge transfer effect of the hydrogen-terminated diamond surface, by the adsorption of the carbon nanotubes and the C60 fullerenes, is consistent with previous theoretical studies.

Thermal Conductivity of Polymer/Nano-filler Blends

NASA Technical Reports Server (NTRS)

Ghose, Sayata; Watson, Kent A.; Delozier, Donovan M.; Working, Dennis C.; Connell, John W.; Smith, Joseph G.; Sun, Y. P.; Lin, Y.

2006-01-01

To improve the thermal conductivity of an ethylene vinyl acetate copolymer, Elvax 260 was compounded with three carbon based nano-fillers. Multiwalled carbon nanotubes (MWCNT), vapor grown carbon nanofibers (CNF) and expanded graphite (EG) were investigated. In an attempt to improve compatibility between the Elvax and nanofillers, MWCNTs and EGs were modified through non covalent and covalent attachment of alkyl groups. Ribbons were extruded to form samples in which the nanofillers were aligned, and samples were also fabricated by compression molding in which the nano-fillers were randomly oriented. The thermal properties were evaluated by DSC and TGA, and mechanical properties of the aligned samples were determined by tensile testing. The degree of dispersion and alignment of the nanoparticles were investigated using high-resolution scanning electron microscopy. Thermal conductivity measurements were performed using a Nanoflash technique. The thermal conductivity of the samples was measured in both the direction of alignment as well as perpendicular to that direction. The results of this study will be presented.

Nano-LC/MALDI-MS using a column-integrated spotting probe for analysis of complex biomolecule samples.

PubMed

Hioki, Yusaku; Tanimura, Ritsuko; Iwamoto, Shinichi; Tanaka, Koichi

2014-03-04

Nanoflow liquid chromatography (nano-LC) is an essential technique for highly sensitive analysis of complex biological samples, and matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) is advantageous for rapid identification of proteins and in-depth analysis of post-translational modifications (PTMs). A combination of nano-LC and MALDI-MS (nano-LC/MALDI-MS) is useful for highly sensitive and detailed analysis in life sciences. However, the existing system does not fully utilize the advantages of each technique, especially in the interface of eluate transfer from nano-LC to a MALDI plate. To effectively combine nano-LC with MALDI-MS, we integrated a nano-LC column and a deposition probe for the first time (column probe) and incorporated it into a nano-LC/MALDI-MS system. Spotting nanoliter eluate droplets directly from the column onto the MALDI plate prevents postcolumn diffusion and preserves the chromatographic resolution. A DHB prespotted plate was prepared to suit the fabricated column probe to concentrate the droplets of nano-LC eluate. The performance of the advanced nano-LC/MALDI-MS system was substantiated by analyzing protein digests. When the system was coupled with multidimensional liquid chromatography (MDLC), trace amounts of glycopeptides that spiked into complex samples were successfully detected. Thus, a nano-LC/MALDI-MS direct-spotting system that eliminates postcolumn diffusion was constructed, and the efficacy of the system was demonstrated through highly sensitive analysis of the protein digests or spiked glycopeptides.

A Study in HRT Resolution: Seeking Maximum Sensitivity Among Variations in Sensing Element Material

NASA Technical Reports Server (NTRS)

Morales, Jeremy M.

2005-01-01

The EXACT (Experiments Along Coexistence near Tricriticality) project endeavors to perform the most rigorous test to date of Renormalization Group theory. In most cases, the theory gives only approximate solutions, but it offers exact predictions in the case of the He-3-He-4 tricritical point. Currently, the project is focused on maximizing the performance of the low-temperature system's HRT (high resolution thermometer) near the tricritical point. The HRT uses a PdMn sensing element, the qualities of which change based on its Mn concentration and whether or not it is annealed. All sensing element combinations will be catalogued, and through the data, the optimum configuration will be reported.

Comparison between auricular and standard rectal thermometers for the measurement of body temperature in dogs

PubMed Central

Sousa, Marlos G.; Carareto, Roberta; Pereira-Junior, Valdo A.; Aquino, Monally C.C.

2011-01-01

Although the rectal mucosa remains the traditional site for measuring body temperature in dogs, an increasing number of clinicians have been using auricular temperature to estimate core body temperature. In this study, 88 mature healthy dogs had body temperatures measured with auricular and rectal thermometers. The mean temperature and confidence intervals were similar for each method, but Bland-Altman plots showed high biases and limits of agreement unacceptable for clinical purposes. The results indicate that auricular and rectal temperatures should not be interpreted interchangeably. PMID:21731094

Comparison between auricular and standard rectal thermometers for the measurement of body temperature in dogs.

PubMed

Sousa, Marlos G; Carareto, Roberta; Pereira-Junior, Valdo A; Aquino, Monally C C

2011-04-01

Although the rectal mucosa remains the traditional site for measuring body temperature in dogs, an increasing number of clinicians have been using auricular temperature to estimate core body temperature. In this study, 88 mature healthy dogs had body temperatures measured with auricular and rectal thermometers. The mean temperature and confidence intervals were similar for each method, but Bland-Altman plots showed high biases and limits of agreement unacceptable for clinical purposes. The results indicate that auricular and rectal temperatures should not be interpreted interchangeably.

Electronic structure of polycrystalline CVD-graphene revealed by Nano-ARPES

NASA Astrophysics Data System (ADS)

Chen, Chaoyu; Avila, José; Asensio, Maria C.

2017-06-01

The ability to explore electronic structure and their role in determining material’s macroscopic behaviour is essential to explain and engineer functions of material and device. Since its debut in 2004, graphene has attracted global research interest due to its unique properties. Chemical vapor deposition (CVD) has emerged as an important method for the massive preparation and production of graphene for various applications. Here by employing angle-resolved photoemission spectroscopy with nanoscale spatial resolution ˜ 100 nm (Nano-ARPES), we describe the approach to measure the electronic structure of polycrystalline graphene on copper foils, demonstrating the power of Nano-ARPES to detect the electronic structure of microscopic single crystalline domains, being fully compatible with conventional ARPES. Similar analysis could be employed to other microscopic materials

Nano-fEM: protein localization using photo-activated localization microscopy and electron microscopy.

PubMed

Watanabe, Shigeki; Richards, Jackson; Hollopeter, Gunther; Hobson, Robert J; Davis, Wayne M; Jorgensen, Erik M

2012-12-03

Mapping the distribution of proteins is essential for understanding the function of proteins in a cell. Fluorescence microscopy is extensively used for protein localization, but subcellular context is often absent in fluorescence images. Immuno-electron microscopy, on the other hand, can localize proteins, but the technique is limited by a lack of compatible antibodies, poor preservation of morphology and because most antigens are not exposed to the specimen surface. Correlative approaches can acquire the fluorescence image from a whole cell first, either from immuno-fluorescence or genetically tagged proteins. The sample is then fixed and embedded for electron microscopy, and the images are correlated (1-3). However, the low-resolution fluorescence image and the lack of fiducial markers preclude the precise localization of proteins. Alternatively, fluorescence imaging can be done after preserving the specimen in plastic. In this approach, the block is sectioned, and fluorescence images and electron micrographs of the same section are correlated (4-7). However, the diffraction limit of light in the correlated image obscures the locations of individual molecules, and the fluorescence often extends beyond the boundary of the cell. Nano-resolution fluorescence electron microscopy (nano-fEM) is designed to localize proteins at nano-scale by imaging the same sections using photo-activated localization microscopy (PALM) and electron microscopy. PALM overcomes the diffraction limit by imaging individual fluorescent proteins and subsequently mapping the centroid of each fluorescent spot (8-10). We outline the nano-fEM technique in five steps. First, the sample is fixed and embedded using conditions that preserve the fluorescence of tagged proteins. Second, the resin blocks are sectioned into ultrathin segments (70-80 nm) that are mounted on a cover glass. Third, fluorescence is imaged in these sections using the Zeiss PALM microscope. Fourth, electron dense structures are

ZEP520A cold-development technique and tool for ultimate resolution to fabricate 1Xnm bit pattern EB master mold for nano-imprinting lithography for HDD/BPM development

NASA Astrophysics Data System (ADS)

Kobayashi, Hideo; Iyama, Hiromasa

2012-06-01

Poor solvent developers are effective for resolution enhancement on a polymer-type EB resist such as ZEP520A. Another way is to utilize "cold-development" technique which was accomplished by a dip-development technique usually. We then designed and successfully built a single-wafer spin-development tool for the cold-development down to -10degC in order to dissolve difficulties of the dip-development. The cold-development certainly helped improve ZEP520A resolution and hole CD size uniformity, and achieved 35nm pitch BPM patterns with the standard developer ZED-N50, but not 25nm pitch yet. By employing a poor solvent mixture of iso-Propyl Alcohol (IPA) and Fluoro-Carbon (FC), 25nm pitch BPM patterns were accomplished. However, the cold-development showed almost no improvement on the IPA/FC mixture developer solvent. This paper describes cold-development technique and a tool, as well as its results, for ZEP520A resolution enhancement to fabricate 1Xnm bits (holes) for EB master-mold for Nano-Imprinting Lithography for 1Tbit/inch2 and 25nm pitch Bit Patterned Media development.

SiGe nano-heteroepitaxy on Si and SiGe nano-pillars.

PubMed

Mastari, M; Charles, M; Bogumilowicz, Y; Thai, Q M; Pimenta-Barros, P; Argoud, M; Papon, A M; Gergaud, P; Landru, D; Kim, Y; Hartmann, J M

2018-07-06

In this paper, SiGe nano-heteroepitaxy on Si and SiGe nano-pillars was investigated in a 300 mm industrial reduced pressure-chemical vapour deposition tool. An integration scheme based on diblock copolymer patterning was used to fabricate nanometre-sized templates for the epitaxy of Si and SiGe nano-pillars. Results showed highly selective and uniform processes for the epitaxial growth of Si and SiGe nano-pillars. 200 nm thick SiGe layers were grown on Si and SiGe nano-pillars and characterised by atomic force microscopy, x-ray diffraction and transmission electron microscopy. Smooth SiGe surfaces and full strain relaxation were obtained in the 650 °C-700 °C range for 2D SiGe layers grown either on Si or SiGe nano-pillars.

Linking environmental processes to the in situ functioning of microorganisms by high-resolution secondary ion mass spectrometry (NanoSIMS) and scanning transmission X-ray microscopy (STXM).

PubMed

Behrens, Sebastian; Kappler, Andreas; Obst, Martin

2012-11-01

Environmental microbiology research increasingly focuses on the single microbial cell as the defining entity that drives environmental processes. The interactions of individual microbial cells with each other, the environment and with higher organisms shape microbial communities and control the functioning of whole ecosystems. A single-cell view of microorganisms in their natural environment requires analytical tools that measure both cell function and chemical speciation at the submicrometre scale. Here we review the technical capabilities and limitations of high-resolution secondary ion mass spectrometry (NanoSIMS) and scanning transmission (soft) X-ray microscopy (STXM) and give examples of their applications. Whereas NanoSIMS can be combined with isotope-labelling, thereby localizing the distribution of cellular activities (e.g. carbon/nitrogen fixation/turnover), STXM provides information on the location and chemical speciation of metabolites and products of redox reactions. We propose the combined use of both techniques and discuss the technical challenges of their joint application. Both techniques have the potential to enhance our understanding of cellular mechanisms and activities that contribute to microbially mediated processes, such as the biogeochemical cycling of elements, the transformation of contaminants and the precipitation of mineral phases. © 2012 Society for Applied Microbiology and Blackwell Publishing Ltd.

Automation of the temperature elevation test in transformers with insulating oil.

PubMed

Vicente, José Manuel Esteves; Rezek, Angelo José Junqueira; de Almeida, Antonio Tadeu Lyrio; Guimarães, Carlos Alberto Mohallem

2008-01-01

The automation of the temperature elevation test is outlined here for both the oil temperature elevation and the determination of the winding temperature elevation. While automating this test it is necessary to use four thermometers, one three-phase wattmeter, a motorized voltage variator and a Kelvin bridge to measure the resistance. All the equipments must communicate with a microcomputer, which will have the test program implemented. The system to be outlined here was initially implemented in the laboratory and, due to the good results achieved, is already in use in some transformer manufacturing plants.

Sensing of single electrons using micro and nano technologies: a review

NASA Astrophysics Data System (ADS)

Jalil, Jubayer; Zhu, Yong; Ekanayake, Chandima; Ruan, Yong

2017-04-01

During the last three decades, the remarkable dynamic features of microelectromechanical systems (MEMS) and nanoelectromechanical systems (NEMS), and advances in solid-state electronics hold much potential for the fabrication of extremely sensitive charge sensors. These sensors have a broad range of applications, such as those involving the measurement of ionization radiation, detection of bio-analyte and aerosol particles, mass spectrometry, scanning tunneling microscopy, and quantum computation. Designing charge sensors (also known as charge electrometers) for electrometry is deemed significant because of the sensitivity and resolution issues in the range of micro- and nano-scales. This article reviews the development of state-of-the-art micro- and nano-charge sensors, and discusses their technological challenges for practical implementation.

Vertically aligned carbon nanofiber as nano-neuron interface for monitoring neural function

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ericson, Milton Nance; McKnight, Timothy E; Melechko, Anatoli Vasilievich

2012-01-01

Neural chips, which are capable of simultaneous, multi-site neural recording and stimulation, have been used to detect and modulate neural activity for almost 30 years. As a neural interface, neural chips provide dynamic functional information for neural decoding and neural control. By improving sensitivity and spatial resolution, nano-scale electrodes may revolutionize neural detection and modulation at cellular and molecular levels as nano-neuron interfaces. We developed a carbon-nanofiber neural chip with lithographically defined arrays of vertically aligned carbon nanofiber electrodes and demonstrated its capability of both stimulating and monitoring electrophysiological signals from brain tissues in vitro and monitoring dynamic information ofmore » neuroplasticity. This novel nano-neuron interface can potentially serve as a precise, informative, biocompatible, and dual-mode neural interface for monitoring of both neuroelectrical and neurochemical activity at the single cell level and even inside the cell.« less

Photoassisted Kelvin probe force microscopy at GaN surfaces: The role of polarity

NASA Astrophysics Data System (ADS)

Wei, J. D.; Li, S. F.; Atamuratov, A.; Wehmann, H.-H.; Waag, A.

2010-10-01

The behavior of GaN surfaces during photoassisted Kelvin probe force microscopy is demonstrated to be strongly dependant on surface polarity. The surface photovoltage of GaN surfaces illuminated with above-band gap light is analyzed as a function of time and light intensity. Distinct differences between Ga-polar and N-polar surfaces could be identified, attributed to photoinduced chemisorption of oxygen during illumination. These differences can be used for a contactless, nondestructive, and easy-performable analysis of the polarity of GaN surfaces.

A 10 nN resolution thrust-stand for micro-propulsion devices

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chakraborty, Subha; Courtney, Daniel G.; Shea, Herbert, E-mail: herbert.shea@epfl.ch

We report on the development of a nano-Newton thrust-stand that can measure up to 100 μN thrust from different types of microthrusters with 10 nN resolution. The compact thrust-stand measures the impingement force of the particles emitted from a microthruster onto a suspended plate of size 45 mm × 45 mm and with a natural frequency over 50 Hz. Using a homodyne (lock-in) readout provides strong immunity to facility vibrations, which historically has been a major challenge for nano-Newton thrust-stands. A cold-gas thruster generating up to 50 μN thrust in air was first used to validate the thrust-stand. Better thanmore » 10 nN resolution and a minimum detectable thrust of 10 nN were achieved. Thrust from a miniature electrospray propulsion system generating up to 3 μN of thrust was measured with our thrust-stand in vacuum, and the thrust was compared with that computed from beam diagnostics, obtaining agreement within 50 nN to 150 nN. The 10 nN resolution obtained from this thrust-stand matches that from state-of-the-art nano-Newton thrust-stands, which measure thrust directly from the thruster by mounting it on a moving arm (but whose natural frequency is well below 1 Hz). The thrust-stand is the first of its kind to demonstrate less than 3 μN resolution by measuring the impingement force, making it capable of measuring thrust from different types of microthrusters, with the potential of easy upscaling for thrust measurement at much higher levels, simply by replacing the force sensor with other force sensors.« less

A 10 nN resolution thrust-stand for micro-propulsion devices

NASA Astrophysics Data System (ADS)

Chakraborty, Subha; Courtney, Daniel G.; Shea, Herbert

2015-11-01

We report on the development of a nano-Newton thrust-stand that can measure up to 100 μN thrust from different types of microthrusters with 10 nN resolution. The compact thrust-stand measures the impingement force of the particles emitted from a microthruster onto a suspended plate of size 45 mm × 45 mm and with a natural frequency over 50 Hz. Using a homodyne (lock-in) readout provides strong immunity to facility vibrations, which historically has been a major challenge for nano-Newton thrust-stands. A cold-gas thruster generating up to 50 μN thrust in air was first used to validate the thrust-stand. Better than 10 nN resolution and a minimum detectable thrust of 10 nN were achieved. Thrust from a miniature electrospray propulsion system generating up to 3 μN of thrust was measured with our thrust-stand in vacuum, and the thrust was compared with that computed from beam diagnostics, obtaining agreement within 50 nN to 150 nN. The 10 nN resolution obtained from this thrust-stand matches that from state-of-the-art nano-Newton thrust-stands, which measure thrust directly from the thruster by mounting it on a moving arm (but whose natural frequency is well below 1 Hz). The thrust-stand is the first of its kind to demonstrate less than 3 μN resolution by measuring the impingement force, making it capable of measuring thrust from different types of microthrusters, with the potential of easy upscaling for thrust measurement at much higher levels, simply by replacing the force sensor with other force sensors.

Data Encoding using Periodic Nano-Optical Features

NASA Astrophysics Data System (ADS)

Vosoogh-Grayli, Siamack

Successful trials have been made through a designed algorithm to quantize, compress and optically encode unsigned 8 bit integer values in the form of images using Nano optical features. The periodicity of the Nano-scale features (Nano-gratings) have been designed and investigated both theoretically and experimentally to create distinct states of variation (three on states and one off state). The use of easy to manufacture and machine readable encoded data in secured authentication media has been employed previously in bar-codes for bi-state (binary) models and in color barcodes for multiple state models. This work has focused on implementing 4 states of variation for unit information through periodic Nano-optical structures that separate an incident wavelength into distinct colors (variation states) in order to create an encoding system. Compared to barcodes and magnetic stripes in secured finite length storage media the proposed system encodes and stores more data. The benefits of multiple states of variation in an encoding unit are 1) increased numerically representable range 2) increased storage density and 3) decreased number of typical set elements for any ergodic or semi-ergodic source that emits these encoding units. A thorough investigation has targeted the effects of the use of multi-varied state Nano-optical features on data storage density and consequent data transmission rates. The results show that use of Nano-optical features for encoding data yields a data storage density of circa 800 Kbits/in2 via the implementation of commercially available high resolution flatbed scanner systems for readout. Such storage density is far greater than commercial finite length secured storage media such as Barcode family with maximum practical density of 1kbits/in2 and highest density magnetic stripe cards with maximum density circa 3 Kbits/in2. The numerically representable range of the proposed encoding unit for 4 states of variation is [0 255]. The number of

Three-dimensional micro/nano-scale structure fabricated by combination of non-volatile polymerizable RTIL and FIB irradiation

PubMed Central

Kuwabata, Susumu; Minamimoto, Hiro; Inoue, Kosuke; Imanishi, Akihito; Hosoya, Ken; Uyama, Hiroshi; Torimoto, Tsukasa; Tsuda, Tetsuya; Seki, Shu

2014-01-01

Room-temperature ionic liquid (RTIL) has been widely investigated as a nonvolatile solvent as well as a unique liquid material because of its interesting features, e.g., negligible vapor pressure and high thermal stability. Here we report that a non-volatile polymerizable RTIL is a useful starting material for the fabrication of micro/nano-scale polymer structures with a focused-ion-beam (FIB) system operated under high-vacuum condition. Gallium-ion beam irradiation to the polymerizable 1-allyl-3-ethylimidazolium bis((trifluoromethane)sulfonyl)amide RTIL layer spread on a Si wafer induced a polymerization reaction without difficulty. What is interesting to note is that we have succeeded in provoking the polymerization reaction anywhere on the Si wafer substrate by using FIB irradiation with a raster scanning mode. By this finding, two- and three-dimensional micro/nano-scale polymer structure fabrications were possible at the resolution of 500,000 dpi. Even intricate three-dimensional micro/nano-figures with overhang and hollow moieties could be constructed at the resolution of approximately 100 nm. PMID:24430465

In situ thermomechanical testing methods for micro/nano-scale materials.

PubMed

Kang, Wonmo; Merrill, Marriner; Wheeler, Jeffrey M

2017-02-23

The advance of micro/nanotechnology in energy-harvesting, micropower, electronic devices, and transducers for automobile and aerospace applications has led to the need for accurate thermomechanical characterization of micro/nano-scale materials to ensure their reliability and performance. This persistent need has driven various efforts to develop innovative experimental techniques that overcome the critical challenges associated with precise mechanical and thermal control of micro/nano-scale specimens during material characterization. Here we review recent progress in the development of thermomechanical testing methods from miniaturized versions of conventional macroscopic test systems to the current state of the art of in situ uniaxial testing capabilities in electron microscopes utilizing either indentation-based microcompression or integrated microsystems. We discuss the major advantages/disadvantages of these methods with respect to specimen size, range of temperature control, ease of experimentation and resolution of the measurements. We also identify key challenges in each method. Finally, we summarize some of the important discoveries that have been made using in situ thermomechanical testing and the exciting research opportunities still to come in micro/nano-scale materials.

Electronic clinical predictive thermometer using logarithm for temperature prediction

NASA Technical Reports Server (NTRS)

Cambridge, Vivien J. (Inventor); Koger, Thomas L. (Inventor); Nail, William L. (Inventor); Diaz, Patrick (Inventor)

1998-01-01

A thermometer that rapidly predicts body temperature based on the temperature signals received from a temperature sensing probe when it comes into contact with the body. The logarithms of the differences between the temperature signals in a selected time frame are determined. A line is fit through the logarithms and the slope of the line is used as a system time constant in predicting the final temperature of the body. The time constant in conjunction with predetermined additional constants are used to compute the predicted temperature. Data quality in the time frame is monitored and if unacceptable, a different time frame of temperature signals is selected for use in prediction. The processor switches to a monitor mode if data quality over a limited number of time frames is unacceptable. Determining the start time on which the measurement time frame for prediction is based is performed by summing the second derivatives of temperature signals over time frames. When the sum of second derivatives in a particular time frame exceeds a threshold, the start time is established.

Mass production of polymer nano-wires filled with metal nano-particles.

PubMed

Lomadze, Nino; Kopyshev, Alexey; Bargheer, Matias; Wollgarten, Markus; Santer, Svetlana

2017-08-17

Despite the ongoing progress in nanotechnology and its applications, the development of strategies for connecting nano-scale systems to micro- or macroscale elements is hampered by the lack of structural components that have both, nano- and macroscale dimensions. The production of nano-scale wires with macroscale length is one of the most interesting challenges here. There are a lot of strategies to fabricate long nanoscopic stripes made of metals, polymers or ceramics but none is suitable for mass production of ordered and dense arrangements of wires at large numbers. In this paper, we report on a technique for producing arrays of ordered, flexible and free-standing polymer nano-wires filled with different types of nano-particles. The process utilizes the strong response of photosensitive polymer brushes to irradiation with UV-interference patterns, resulting in a substantial mass redistribution of the polymer material along with local rupturing of polymer chains. The chains can wind up in wires of nano-scale thickness and a length of up to several centimeters. When dispersing nano-particles within the film, the final arrangement is similar to a core-shell geometry with mainly nano-particles found in the core region and the polymer forming a dielectric jacket.

Imaging of current density distributions with a Nb weak-link scanning nano-SQUID microscope

PubMed Central

Shibata, Yusuke; Nomura, Shintaro; Kashiwaya, Hiromi; Kashiwaya, Satoshi; Ishiguro, Ryosuke; Takayanagi, Hideaki

2015-01-01

Superconducting quantum interference devices (SQUIDs) are accepted as one of the highest magnetic field sensitive probes. There are increasing demands to image local magnetic fields to explore spin properties and current density distributions in a two-dimensional layer of semiconductors or superconductors. Nano-SQUIDs have recently attracting much interest for high spatial resolution measurements in nanometer-scale samples. Whereas weak-link Dayem Josephson junction nano-SQUIDs are suitable to miniaturization, hysteresis in current-voltage (I-V) characteristics that is often observed in Dayem Josephson junction is not desirable for a scanning microscope. Here we report on our development of a weak-link nano-SQUIDs scanning microscope with small hysteresis in I-V curve and on reconstructions of two-dimensional current density vector in two-dimensional electron gas from measured magnetic field. PMID:26459874

Imaging of current density distributions with a Nb weak-link scanning nano-SQUID microscope

NASA Astrophysics Data System (ADS)

Shibata, Yusuke; Nomura, Shintaro; Kashiwaya, Hiromi; Kashiwaya, Satoshi; Ishiguro, Ryosuke; Takayanagi, Hideaki

2015-10-01

Superconducting quantum interference devices (SQUIDs) are accepted as one of the highest magnetic field sensitive probes. There are increasing demands to image local magnetic fields to explore spin properties and current density distributions in a two-dimensional layer of semiconductors or superconductors. Nano-SQUIDs have recently attracting much interest for high spatial resolution measurements in nanometer-scale samples. Whereas weak-link Dayem Josephson junction nano-SQUIDs are suitable to miniaturization, hysteresis in current-voltage (I-V) characteristics that is often observed in Dayem Josephson junction is not desirable for a scanning microscope. Here we report on our development of a weak-link nano-SQUIDs scanning microscope with small hysteresis in I-V curve and on reconstructions of two-dimensional current density vector in two-dimensional electron gas from measured magnetic field.

The Fourier-Kelvin Stellar Interferometer (FKSI): A Discovery Class TPF/DARWIN Pathfinder Mission Concept

NASA Technical Reports Server (NTRS)

Danchi, W. C.; Allen, R. J.; Benford, D. J.; Deming, D.; Gezan, D. Y.; Kuchner, M.; Leisawitz, D. T.; Linfield, R.; Millan-Gabet, R.; Monnier, J. D.

2003-01-01

The Fourier-Kelvin Stellar Interferometer (FKSI) is a mission concept for an imaging and nulling interferometer for the mid-infrared spectral region (5-30 microns). FKSI is conceived as a scientific and technological pathfinder to TPF/DARWIN as well as SPIRIT, SPECS, and SAFIR. It will also be a high angular resolution system complementary to NGST. The scientific emphasis of the mission is on the evolution of protostellar systems, from just after the collapse of the precursor molecular cloud core, through the formation of the disk surrounding the protostar, the formation of planets in the disk, and eventual dispersal of the disk material. FKSI will also search for brown dwarfs and Jupiter mass and smaller planets, and could also play a very powerful role in the investigation of the structure of active galactic nuclei and extra-galactic star formation. We have been studying alternative interferometer architectures and beam combination techniques, and evaluating the relevant science and technology tradeoffs. Some of the technical challenges include the development of the cryocooler systems necessary for the telescopes and focal plane array, light and stiff but well-damped truss systems to support the telescopes, and lightweight and coolable optical telescopes. We present results of detailed design studies of the FKSI starting with a design consisting of five one meter diameter telescopes arranged along a truss structure in a linear non-redundant array, cooled to 35 K. A maximum baseline of 20 meters gives a nominal resolution of 26 mas at 5 microns. Using a Fizeau beam combination technique, a simple focal plane camera could be used to obtain both Fourier and spectral data simultaneously for a given orientation of the array. The spacecraft will be rotated to give sufficient Fourier data to reconstruct complex images of a broad range of astrophysical sources. Alternative and simpler three and two telescope designs emphasizing nulling and spectroscopy also have been

Fabrication of a mini multi-fixed-point cell for the calibration of industrial platinum resistance thermometers

NASA Astrophysics Data System (ADS)

Ragay-Enot, Monalisa; Lee, Young Hee; Kim, Yong-Gyoo

2017-07-01

A mini multi-fixed-point cell (length 118 mm, diameter 33 mm) containing three materials (In-Zn eutectic (mass fraction 3.8% Zn), Sn and Pb) in a single crucible was designed and fabricated for the easy and economical fixed-point calibration of industrial platinum resistance thermometers (IPRTs) for use in industrial temperature measurements. The melting and freezing behaviors of the metals were investigated and the phase transition temperatures were determined using a commercial dry-block calibrator. Results showed that the melting plateaus are generally easy to realize and are reproducible, flatter and of longer duration. On the other hand, the freezing process is generally difficult, especially for Sn, due to the high supercooling required to initiate freezing. The observed melting temperatures at optimum set conditions were 143.11 °C (In-Zn), 231.70 °C (Sn) and 327.15 °C (Pb) with expanded uncertainties (k  = 2) of 0.12 °C, 0.10 °C and 0.13 °C, respectively. This multi-fixed-point cell can be treated as a sole reference temperature-generating system. Based on the results, the realization of melting points of the mini multi-fixed-point cell can be recommended for the direct calibration of IPRTs in industrial applications without the need for a reference thermometer.

Shear Modulus for Nonisotropic, Open-Celled Foams Using a General Elongated Kelvin Foam Model

NASA Technical Reports Server (NTRS)

Sullivan, Roy M.; Ghosn, Louis J.

2008-01-01

An equation for the shear modulus for nonisotropic, open-celled foams in the plane transverse to the elongation (rise) direction is derived using an elongated Kelvin foam model with the most general geometric description. The shear modulus was found to be a function of the unit cell dimensions, the solid material properties, and the cell edge cross-section properties. The shear modulus equation reduces to the relation derived by others for isotropic foams when the unit cell is equiaxed.

Plasmonic graded nano-disks as nano-optical conveyor belt.

PubMed

Kang, Zhiwen; Lu, Haifei; Chen, Jiajie; Chen, Kun; Xu, Fang; Ho, Ho-Pui

2014-08-11

We propose a plasmonic system consisting of nano-disks (NDs) with graded diameters for the realization of nano-optical conveyor belt. The system contains a couple of NDs with individual elements coded with different resonant wavelengths. By sequentially switching the wavelength and polarization of the excitation source, optically trapped target nano-particle can be transferred from one ND to another. The feasibility of such function is verified based on the three-dimensional finite-difference time-domain technique and the Maxwell stress tensor method. Our design may provide an alternative way to construct nano-optical conveyor belt with which target molecules can be delivered between trapping sites, thus enabling many on-chip optofluidic applications.

Resolution enhancement in coherent x-ray diffraction imaging by overcoming instrumental noise.

PubMed

Kim, Chan; Kim, Yoonhee; Song, Changyong; Kim, Sang Soo; Kim, Sunam; Kang, Hyon Chol; Hwu, Yeukuang; Tsuei, Ku-Ding; Liang, Keng San; Noh, Do Young

2014-11-17

We report that reference objects, strong scatterers neighboring weak phase objects, enhance the phase retrieval and spatial resolution in coherent x-ray diffraction imaging (CDI). A CDI experiment with Au nano-particles exhibited that the reference objects amplified the signal-to-noise ratio in the diffraction intensity at large diffraction angles, which significantly enhanced the image resolution. The interference between the diffracted x-ray from reference objects and a specimen also improved the retrieval of the phase of the diffraction signal. The enhancement was applied to image NiO nano-particles and a mitochondrion and confirmed in a simulation with a bacteria phantom. We expect that the proposed method will be of great help in imaging weakly scattering soft matters using coherent x-ray sources including x-ray free electron lasers.

Tympanic, Infrared Skin, and Temporal Artery Scan Thermometers Compared with Rectal Measurement in Children: A Real-Life Assessment

PubMed Central

Allegaert, Karel; Casteels, Kristina; van Gorp, Ilse; Bogaert, Guy

2014-01-01

Introduction Body temperature measurement in children is of clinical relevance. Although rectal measurement is the gold standard, less invasive tools have become available. We aimed to describe the accuracy of tympanic, infrared skin, or temporal artery scan thermometers compared with rectal measurement to reflect core temperature. Methods Rectal (Filac 3000; Covidien, Mechelen, Belgium), tympanic (AccuSystem Genius2 Typmanic Infrared Ear Thermometer, Covidien, Mechelen, Belgium), temporal artery scan (Exergen, Exergen Corp, Watertown, Massachusetts), and infrared (ThermoFlash Contactless Medical Electronic Thermometer, Visiomedlab, Paris, France) body temperature measurements were randomly performed and readings were collected once. Temperature readings were described as median and range, and observations were compared with rectal temperature readings (using Wilcoxon, Bland-Altman, sensitivity, and specificity tests). The child’s comfort was assessed by the child, parent, and nurse (using Likert scales) and ease of use was assessed by nurses (using visual analog scale). Results Based on observations in 294 (median age = 3.2 years, range = 0.02–17 years) children, the mean difference was 0.49°C (tympanic scan; P < 0.0001), 0.34°C (infrared skin scan; P < 0.0001), and 0°C (temporal artery scan; P = 0.9288), respectively, when compared with rectal temperature readings. Based on visual inspection of Bland-Altman plots, all tools overestimated the temperature at lower body temperature and underestimated the temperature at higher body temperature, resulting in a sensitivity of 22% to 41% and a specificity of 98% to 100% for rectal temperatures above 38°C. The Likert scale scores and the visual analog scale scores for rectal measurement were only slightly higher when compared with the other methods. Conclusions All noninvasive techniques underperformed compared with rectal measurement. The temporal artery scan deviations were smallest, but all noninvasive

Equivalence of the Kelvin-Planck statement of the second law and the principle of entropy increase

NASA Astrophysics Data System (ADS)

Sarasua, L. G.; Abal, G.

2016-09-01

We present a demonstration of the equivalence between the Kelvin-Planck statement of the second law and the principle of entropy increase. Despite the fundamental importance of these two statements, a rigorous treatment to establish their equivalence is missing in standard physics textbooks. The argument is valid under very general conditions, but is simple and suited to an undergraduate course.

The Effect of Nano Loading and Ultrasonic Compounding of EVA/LDPE/Nano-magnesium Hydroxide on Mechanical Properties and Distribution of Nano Particles

NASA Astrophysics Data System (ADS)

Azman, I. A.; Salleh, R. M.; Alauddin, S. M.; Shueb, M. I.

2018-05-01

Blends of Ethylene Vinyl Acetate (EVA) and Low-Density Polyethylene (LDPE) are promising composite which have good mechanical properties to environmental stress cracking. However, they lack fire resistant properties, which limits it usage in wire and cable industry. In order to improve flame retardancy ability, a range of nano-magnesium hydroxide (nano-MH) loading which is from 0 phr to maximum of 20 phr with ultrasonic extrusion 0-100 kHz frequencies have been introduced. Ultrasonic extrusion was used to improve the distribution of nano-MH. It was found that, 10 phr of nano loading with 100 kHz ultrasonic assisted has greater tensile strength compared to the nanocomposite without ultrasonication. Further increase of nano MH loading, will decrease the tensile properties. Better elongation at break was observed at10 phr nano-MH with the frequency of 50 kHz. The sample of 20 phr of nanoMH assisted with 50 kHz ultrasonic exhibits good flexural properties while 10 phr of nano-MH without the ultrasonic assisted demonstrates good in izod impact properties. From the evaluation of mechanical properties studied, it was found that 10 phr of nano-MH has shown the best performance among all the samples tested for EVA/LDPE/nano-MH composites. Transmission Electron Microscopy (TEM) has been conducted on 10 phr sample with different frequencies in order to observe the distribution of nano-MH particles. The sample with 100 kHz frequency shows more uniform dispersion of nano-MH in EVA/LDPE composites. This investigation indicates that the ultrasonic technology can enhance the mechanical properties studied as well as the dispersion of nano particles in the composite.

Equatorial Kelvin waves generated in the western tropical Pacific Ocean trigger mass and heat transport within the Middle America Trench off Costa Rica

NASA Astrophysics Data System (ADS)

Thomson, Richard E.; Davis, Earl E.

2017-07-01

Sequences of correlated seafloor temperature, current velocity, and acoustic backscatter events recorded at Ocean Drilling Program (ODP) sites at 4300 m depth in the Middle America Trench have been inferred to result from tidally induced turbidity currents generated in the vicinity of the 3300 m deep sill at the southern end of the trench. New data from the borehole observatories extend the temperature records to 11 years (November 2002 to December 2013) and confirm the highly episodic nature of the events. We present satellite altimetry data and ocean circulation model results to show that event timing is correlated with intraseasonal Kelvin wave motions in the equatorial Pacific. The observed temperature events had a mean (±1 standard deviation) occurrence interval of 61 (±24) days, which spans the periods of the first two baroclinic modes. Lag times between peak bottom water temperatures at the ODP sites and the passage of eastward-propagating Kelvin wave crests at locations in the eastern equatorial Pacific are consistent with the time for mode-1 waves to propagate to the southern end of the trench at a mean phase speed of 2.0 m s-1. Findings indicate that Kelvin wave currents augment tidal motions in the vicinity of the sill, triggering turbidity currents that travel northwestward along the trench axis at mean speeds of ˜0.1 m s-1. We conclude that mode-1 (or, possibly, mixed mode-1 and mode-2) baroclinic Kelvin waves generated by large-scale atmospheric processes in the western tropical Pacific lead to heat and mass transport deep within Middle America Trench in the eastern tropical Pacific.

Micro-CT and nano-CT analysis of filling quality of three different endodontic sealers.

PubMed

Huang, Yan; Celikten, Berkan; de Faria Vasconcelos, Karla; Ferreira Pinheiro Nicolielo, Laura; Lippiatt, Nicholas; Buyuksungur, Arda; Jacobs, Reinhilde; Orhan, Kaan

2017-12-01

To investigate voids in different root canal sealers using micro-CT and nano-CT, and to explore the feasibility of using nano-CT for quantitative analysis of sealer filling quality. 30 extracted mandibular central incisors were randomly assigned into three groups according to the applied root canal sealers (Total BC Sealer, Sure Seal Root, AH Plus) by the single cone technique. Subsequently, micro-CT and nano-CT were performed to analyse the incidence rate of voids, void fraction, void volume and their distribution in each sample. Micro-CT evaluation showed no significant difference among sealers for the incidence rate of voids or void fraction in the whole filling materials (p > 0.05), whereas a significant difference was found between AH Plus and the other two sealers using nano-CT (p < 0.05). All three sealers presented less void volume in the apical third; however, higher void volumes were observed in the apical and coronal thirds in AH Plus using micro-CT (p < 0.05), while nano-CT results displayed higher void volume in AH Plus among all the sealers and regions (p < 0.05). Bioactive sealers showed higher root filling rate, lower incidence rate of voids, void fraction and void volume than AH Plus under nano-CT analysis, when round root canals were treated by the single cone technique. The disparate results suggest that the higher resolution of nano-CT have a greater ability of distinguishing internal porosity, and therefore suggesting the potential use of nano-CT in quantitative analysis of filling quality of sealers.

Open Access Internet Resources for Nano-Materials Physics Education

NASA Astrophysics Data System (ADS)

Moeck, Peter; Seipel, Bjoern; Upreti, Girish; Harvey, Morgan; Garrick, Will

2006-05-01

Because a great deal of nano-material science and engineering relies on crystalline materials, materials physicists have to provide their own specific contributions to the National Nanotechnology Initiative. Here we briefly review two freely accessible internet-based crystallographic databases, the Nano-Crystallography Database (http://nanocrystallography.research.pdx.edu) and the Crystallography Open Database (http://crystallography.net). Information on over 34,000 full structure determinations are stored in these two databases in the Crystallographic Information File format. The availability of such crystallographic data on the internet in a standardized format allows for all kinds of web-based crystallographic calculations and visualizations. Two examples of which that are dealt with in this paper are: interactive crystal structure visualizations in three dimensions and calculations of lattice-fringe fingerprints for the identification of unknown nanocrystals from their atomic-resolution transmission electron microscopy images.

Note: Switching crosstalk on and off in Kelvin probe force microscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Polak, Leo, E-mail: l.polak@vu.nl; Wijngaarden, Rinke J.; Man, Sven de

2014-04-15

In Kelvin Probe Force Microscopy (KPFM) electronic crosstalk can occur between the excitation signal and probe deflection signal. Here, we demonstrate how a small modification to our commercial instrument enables us to literally switch the crosstalk on and off. We study in detail the effect of crosstalk on open-loop KPFM and compare with closed-loop KPFM. We measure the pure crosstalk signal and verify that we can correct for it in the data-processing required for open-loop KPFM. We also demonstrate that open-loop KPFM results are independent of the frequency and amplitude of the excitation signal, provided that the influence of crosstalkmore » has been eliminated.« less

Band Excitation Kelvin probe force microscopy utilizing photothermal excitation

DOE PAGES

Collins, Liam; Jesse, Stephen; Balke, Nina; ...

2015-03-13

A multifrequency open loop Kelvin probe force microscopy (KPFM) approach utilizing photothermal as opposed to electrical excitation is developed. Photothermal band excitation (PthBE)-KPFM is implemented here in a grid mode on a model test sample comprising a metal-insulator junction with local charge-patterned regions. Unlike the previously described open loop BE-KPFM, which relies on capacitive actuation of the cantilever, photothermal actuation is shown to be highly sensitive to the electrostatic force gradient even at biases close to the contact potential difference (CPD). PthBE-KPFM is further shown to provide a more localized measurement of true CPD in comparison to the gold standardmore » ambient KPFM approach, amplitude modulated KPFM. In conclusion, PthBE-KPFM data contain information relating to local dielectric properties and electronic dissipation between tip and sample unattainable using conventional single frequency KPFM approaches.« less

Kelvin-Mach Wake in a Two-Dimensional Fermi Sea

NASA Astrophysics Data System (ADS)

Kolomeisky, Eugene B.; Straley, Joseph P.

2018-06-01

The dispersion law for plasma oscillations in a two-dimensional electron gas in the hydrodynamic approximation interpolates between Ω ∝√{q } and Ω ∝q dependences as the wave vector q increases. As a result, downstream of a charged impurity in the presence of a uniform supersonic electric current flow, a wake pattern of induced charge density and potential is formed whose geometry is controlled by the Mach number M . For 1 Kelvin ship wake, and consisting of both transverse and diverging wave fronts, is found outside the Mach sector for M >√{2 }. These wakes also trail an external charge, traveling supersonically, a fixed distance away from the electron gas.

Calibrated work function mapping by Kelvin probe force microscopy

NASA Astrophysics Data System (ADS)

Fernández Garrillo, Pablo A.; Grévin, Benjamin; Chevalier, Nicolas; Borowik, Łukasz

2018-04-01

We propose and demonstrate the implementation of an alternative work function tip calibration procedure for Kelvin probe force microscopy under ultrahigh vacuum, using monocrystalline metallic materials with known crystallographic orientation as reference samples, instead of the often used highly oriented pyrolytic graphite calibration sample. The implementation of this protocol allows the acquisition of absolute and reproducible work function values, with an improved uncertainty with respect to unprepared highly oriented pyrolytic graphite-based protocols. The developed protocol allows the local investigation of absolute work function values over nanostructured samples and can be implemented in electronic structures and devices characterization as demonstrated over a nanostructured semiconductor sample presenting Al0.7Ga0.3As and GaAs layers with variable thickness. Additionally, using our protocol we find that the work function of annealed highly oriented pyrolytic graphite is equal to 4.6 ± 0.03 eV.

Interrogating Host-virus Interactions and Elemental Transfer Using NanoSIMS

NASA Astrophysics Data System (ADS)

Pasulka, A.; Thamatrakoln, K.; Poulos, B.; Bidle, K. D.; Sullivan, M. B.; Orphan, V. J.

2016-02-01

Marine viruses (bacteriophage and eukaryotic viruses) impact microbial food webs by influencing microbial community structure, carbon and nutrient flow, and serving as agents of gene transfer. While the collective impact of viral activity has become more apparent over the last decade, there is a growing need for single-cell and single-virus level measurements of the associated carbon and nitrogen transfer, which ultimately shape the biogeochemical impact of viruses in the upper ocean. Stable isotopes have been used extensively for understanding trophic relationships and elemental cycling in marine food webs. While single-cell isotope approaches such as nanoscale secondary ion mass spectrometry (nanoSIMS) have been more readily used to study trophic interactions between microorganisms, isotopic enrichment in viruses has not been described. Here we used nanoSIMS to quantify the transfer of stable isotopes (13C and 15N) from host to individual viral particles in two distinct unicellular algal-virus model systems. These model systems represent a eukaryotic phytoplankton (Emiliania huxleyi strain CCMP374) and its 200nm coccolithovirus (EhV207), as well as a cyanobacterial phytoplankton (Synechococcus WH8101) and its 80nm virus (Syn1). Host cells were grown on labeled media for multiple generations, subjected to viral infection, and then viruses were harvested after lysis. In both cases, nanoSIMS measurements were able to detect 13C and 15N in the resulting viral particles significantly above the background noise. The isotopic enrichment in the viral particles mirrored that of the host. Through use of these laboratory model systems, we quantified the sensitivity (ion counts), spatial resolution, and reproducibility, including sources of methodological and biological variability, in stable isotope incorporation into viral particles. Our findings suggest that nanoSIMS can be successfully employed to directly probe virus-host interactions at the resolution of individual

Effects of the Kelvin-Helmholtz surface instability on supersonic jets

NASA Technical Reports Server (NTRS)

Hardee, P. E.

1982-01-01

An exact numerical calculation is provided for of linear growth and phase velocity of Kelvin-Helmholtz unstable wave modes on a supersonic jet of cylindrical cross section. An expression for the maximally unstable wavenumber of each wave mode is found. Provided a sharp velocity discontinuity exists all wave modes are unstable. A combination of rapid jet expansion and velocity shear across a jet can effectively stabilize all wave modes. The more likely case of slow jet expansion and of velocity shear at the jet surface allows wave modes with maximally unstable wavelength longer than or on the order of the jet radius to grow. The relative energy in different wave modes and effect on the jet is investigated. Energy input into a jet resulting from surface instability is discussed.

Green chemistry synthesis of nano-cuprous oxide.

PubMed

Ceja-Romero, L R; Ortega-Arroyo, L; Ortega Rueda de León, J M; López-Andrade, X; Narayanan, J; Aguilar-Méndez, M A; Castaño, V M

2016-04-01

Green chemistry and a central composite design, to evaluate the effect of reducing agent, temperature and pH of the reaction, were employed to produce controlled cuprous oxide (Cu2O) nanoparticles. Response surface method of the ultraviolet-visible spectroscopy is allowed to determine the most relevant factors for the size distribution of the nanoCu2O. X-ray diffraction reflections correspond to a cubic structure, with sizes from 31.9 to 104.3 nm. High-resolution transmission electron microscopy reveals that the different shapes depend strongly on the conditions of the green synthesis.

MALDI-MS and NanoSIMS imaging techniques to study cnidarian-dinoflagellate symbioses.

PubMed

Kopp, C; Wisztorski, M; Revel, J; Mehiri, M; Dani, V; Capron, L; Carette, D; Fournier, I; Massi, L; Mouajjah, D; Pagnotta, S; Priouzeau, F; Salzet, M; Meibom, A; Sabourault, C

2015-04-01

Cnidarian-dinoflagellate photosynthetic symbioses are fundamental to biologically diverse and productive coral reef ecosystems. The hallmark of this symbiotic relationship is the ability of dinoflagellate symbionts to supply their cnidarian host with a wide range of nutrients. Many aspects of this association nevertheless remain poorly characterized, including the exact identity of the transferred metabolic compounds, the mechanisms that control their exchange across the host-symbiont interface, and the precise subcellular fate of the translocated materials in cnidarian tissues. This lack of knowledge is mainly attributed to difficulties in investigating such metabolic interactions both in situ, i.e. on intact symbiotic associations, and at high spatial resolution. To address these issues, we illustrate the application of two in situ and high spatial resolution molecular and ion imaging techniques-matrix-assisted laser desorption ionization mass spectrometry imaging (MALDI-MSI) and the nano-scale secondary-ion mass spectrometry (NanoSIMS) ion microprobe. These imaging techniques provide important new opportunities for the detailed investigation of many aspects of cnidarian-dinoflagellate associations, including the dynamics of cellular interactions. Copyright © 2014 Elsevier GmbH. All rights reserved.

Influence of a density increase on the evolution of the Kelvin-Helmholtz instability and vortices

DOE Office of Scientific and Technical Information (OSTI.GOV)

Amerstorfer, U. V.; Erkaev, N. V.; Institute of Computational Modelling, 660036 Krasnoyarsk

2010-07-15

Results of two-dimensional nonlinear numerical simulations of the magnetohydrodynamic Kelvin-Helmholtz instability are presented. A boundary layer of a certain width is assumed, which separates the plasma in the upper layer from the plasma in the lower layer. A special focus is given on the influence of a density increase toward the lower layer. The evolution of the Kelvin-Helmholtz instability can be divided into three different phases, namely, a linear growth phase at the beginning, followed by a nonlinear phase with regular structures of the vortices, and finally, a turbulent phase with nonregular structures. The spatial scales of the vortices aremore » about five times the initial width of the boundary layer. The considered configuration is similar to the situation around unmagnetized planets, where the solar wind (upper plasma layer) streams past the ionosphere (lower plasma layer), and thus the plasma density increases toward the planet. The evolving vortices might detach around the terminator of the planet and eventually so-called plasma clouds might be formed, through which ionospheric material can be lost. For the special case of a Venus-like planet, loss rates are estimated, which are of the order of estimated loss rates from observations at Venus.« less

Kelvin wave coupling from TIMED and GOCE: Inter/intra-annual variability and solar activity effects

NASA Astrophysics Data System (ADS)

Gasperini, Federico; Forbes, Jeffrey M.; Doornbos, Eelco N.; Bruinsma, Sean L.

2018-06-01

The primary mechanism through which energy and momentum are transferred from the lower atmosphere to the thermosphere is through the generation and propagation of atmospheric waves. It is becoming increasingly evident that a few waves from the tropical wave spectrum preferentially propagate into the thermosphere and contribute to modify satellite drag. Two of the more prominent and well-established tropical waves are Kelvin waves: the eastward-propagating 3-day ultra-fast Kelvin wave (UFKW) and the eastward-propagating diurnal tide with zonal wave number 3 (DE3). In this work, Sounding of the Atmosphere using Broadband Emission Radiometry (SABER) temperatures at 110 km and Gravity field and steady-state Ocean Circulation Explorer (GOCE) neutral densities and cross-track winds near 260 km are used to demonstrate vertical coupling in this height regime due to the UFKW and DE3. Significant inter- and intra-annual variability is found in DE3 and the UFKW, with evidence of latitudinal broadening and filtering of the latitude structures with height due to the effect of dissipation and mean winds. Additionally, anti-correlation between the vertical penetration of these waves to the middle thermosphere and solar activity level is established and explained through the effect of molecular dissipation.

Metabolic activity of uncultivated magnetotactic bacteria revealed by NanoSIMS

NASA Astrophysics Data System (ADS)

He, M.; Zhang, W.; Gu, L.; Pan, Y.; Lin, W.

2017-12-01

Microorganisms that exhibit magnetotaxis behavior, collectively known as the magnetotactic bacteria (MTB), are those whose motility is influenced by the Earth's magnetic field. MTB are a physiologically diverse group of bacteria with a unique feature of intracellular biomineralization of magnetosomes (Fe3O4 and/or Fe3S4) (Bazylinski et al., 2013). However, the ecophysiology of uncultivated MTB, especially those within the Nitrospirae phylum forming hundreds of bullet-shaped magnetite magnetosomes per cell, is still not well characterized (Lin et al., 2014). Nanoscale secondary ion mass spectrometry (NanoSIMS) is a powerful tool for revealing element distribution in nanometer-scale resolution, which opens exciting possibilities for the study of interactions between microorganisms and environments (Gao et al., 2016; Musat et al., 2016). Here we applied NanoSIMS to investigate the dynamics of carbon and nitrogen assimilations in two magnetotactic Nitrospirae populations at single cell level. Our NanoSIMS results confirmed the metabolic potential of Nitrospirae MTB proposed by genomic and metagenomic analysis and provided additional insights into the ecophysiology of uncultivated MTB. This study suggests that NanoSIMS-based analyses are powerful approaches for investigating and characterizing the ecological function of environmental microorganisms. References: Bazylinski D A., Lefèvre, C T., Schüler D., 2013. Magnetotactic Bacteria. 453-494.Lin W, Bazylinski DA, Xiao T, Wu L- F, Pan Y., 2014. Life with compass: diversity and biogeography of magnetotactic bacteria. Environ Microbiol, 16: 1462-2920.Gao D., Huang X., Tao Y., 2016. A critical review of NanoSIMS in analysis of microbial metabolic activities at single-cell level. Crit Rev Biotechnol, 36: 884-890.Musat N., Musat F., Weber PK., Pett-Ridge J., 2016. Tracking microbial interactions with NanoSIMS. Curr Opin Biotechnol, 41: 114-121.

Nano opto-mechanical systems (NOMS) as a proposal for tactile displays

NASA Astrophysics Data System (ADS)

Campo, E. M.; Roig, J.; Roeder, B.; Wenn, D.; Mamojka, B.; Omastova, M.; Terentjev, E. M.; Esteve, J.

2011-10-01

For over a decade, special emphasis has been placed in the convergence of different fields of science and technology, in an effort to serve human needs by way of enhancing human capabilities. The convergence of the Nano-Bio-Info-Cogni (NBIC) quartet will provide unique solutions to specific needs. This is the case of, Nano-opto mechanical Systems (NOMS), presented as a solution to tactile perception, both for the visually-impaired and for the general public. NOMS, based on photoactive polymer actuators and devices, is a much sought-after technology. In this scheme, light sources promote mechanical actuation producing a variety of nano-opto mechanical systems such as nano-grippers. In this paper, we will provide a series of specifications that the NOMS team is targeting towards the development of a tactile display using optically-activated smart materials. Indeed, tactile displays remain mainly mechanical, compromising reload speeds and resolution which inhibit 3D tactile representation of web interfaces. We will also discuss how advantageous NOMS tactile displays could be for the general public. Tactile processing based on stimulation delivered through the NOMS tablet, will be tested using neuropsychology methods, in particular event-related brain potentials. Additionally, the NOMS tablet will be instrumental to the development of basic neuroscience research.

Physical and magnetic properties of (Ba/Sr) substituted magnesium nano ferrites

NASA Astrophysics Data System (ADS)

Ateia, Ebtesam E.; Takla, E.; Mohamed, Amira T.

2017-10-01

In the presented paper, strontium (Sr) and barium (Ba) nano ferrites were synthesized by citrate auto combustion method. The investigated samples are characterized by X-ray diffraction technique (XRD), field emission scanning electron microscopy, high resolution transmission electron microscopy and energy dispersive X-ray spectroscopy. The structural properties of the obtained samples were examined by XRD analysis showing that the synthesized nanoparticles are in cubic spinel structure. The average crystallite sizes are in the range of 22.66 and 21.95 nm for Mg0.7Ba0.3Fe2O4 and Mg0.7 Sr0.3Fe2O4 respectively. The VSM analysis confirms the existence of ferromagnetic nature of Sr2+/Ba2+ substituted magnesium nano particles. Exchange interaction between hard (Sr/Ba) and soft (Mg) magnetic phases improves the structural and magnetic properties of nano ferrite particles. Rigidity modulus, longitudinal and shear wave velocities are predicted theoretically from Raman spectroscopy and structural data of the investigated spinel ferrite. The magnetic and structural properties of magnesium are enhanced by doping with barium and strontium nano particles. The saturation magnetization, remanent magnetization and coercivity reported on vibrating sample magnetometer curve illustrate the promising industrial and magnetic recording applications of the prepared samples.

Elemental and isotopic imaging of biological samples using NanoSIMS.

PubMed

Kilburn, Matt R; Clode, Peta L

2014-01-01

With its low detection limits and the ability to analyze most of the elements in the periodic table, secondary ion mass spectrometry (SIMS) represents one of the most versatile in situ analytical techniques available, and recent developments have resulted in significant advantages for the use of imaging mass spectrometry in biological and biomedical research. Increases in spatial resolution and sensitivity allow detailed interrogation of samples at relevant scales and chemical concentrations. Advances in dynamic SIMS, specifically with the advent of NanoSIMS, now allow the tracking of stable isotopes within biological systems at subcellular length scales, while static SIMS combines subcellular imaging with molecular identification. In this chapter, we present an introduction to the SIMS technique, with particular reference to NanoSIMS, and discuss its application in biological and biomedical research.

A broadening temperature sensitivity range with a core-shell YbEr@YbNd double ratiometric optical nanothermometer

NASA Astrophysics Data System (ADS)

Marciniak, L.; Prorok, K.; Francés-Soriano, L.; Pérez-Prieto, J.; Bednarkiewicz, A.

2016-02-01

The chemical architecture of lanthanide doped core-shell up-converting nanoparticles can be engineered to purposely design the properties of luminescent nanomaterials, which are typically inaccessible to their homogeneous counterparts. Such an approach allowed to shift the up-conversion excitation wavelength from ~980 to the more relevant ~808 nm or enable Tb or Eu up-conversion emission, which was previously impossible to obtain or inefficient. Here, we address the issue of limited temperature sensitivity range of optical lanthanide based nano-thermometers. By covering Yb-Er co-doped core nanoparticles with the Yb-Nd co-doped shell, we have intentionally combined temperature dependent Er up-conversion together with temperature dependent Nd --> Yb energy transfer, and thus have expanded the temperature response range ΔT of a single nanoparticle based optical nano-thermometer under single ~808 nm wavelength photo-excitation from around ΔT = 150 K to over ΔT = 300 K (150-450 K). Such engineered nanocrystals are suitable for remote optical temperature measurements in technology and biotechnology at the sub-micron scale.The chemical architecture of lanthanide doped core-shell up-converting nanoparticles can be engineered to purposely design the properties of luminescent nanomaterials, which are typically inaccessible to their homogeneous counterparts. Such an approach allowed to shift the up-conversion excitation wavelength from ~980 to the more relevant ~808 nm or enable Tb or Eu up-conversion emission, which was previously impossible to obtain or inefficient. Here, we address the issue of limited temperature sensitivity range of optical lanthanide based nano-thermometers. By covering Yb-Er co-doped core nanoparticles with the Yb-Nd co-doped shell, we have intentionally combined temperature dependent Er up-conversion together with temperature dependent Nd --> Yb energy transfer, and thus have expanded the temperature response range ΔT of a single nanoparticle

A bio-NanoRobot design for drosophila therapeutic cloning

NASA Astrophysics Data System (ADS)

Chang, Chia-Pin; Szu, Harold

2006-04-01

To investigate Somatic Cell Nuclear Transfer (SCNT), we choose the Drosophila cloning based on a recent experiment (Haigh, MacDonald, Lioyd, Gen. V.169,1165, 2005) to be improving the adulthood rate in 2-week turn-around time. Original 1% success rate might be due to three less certain key steps: (i) The double membranes of a nucleus has at its pore led to the attached Rough Endoplasmic Reticulum (ER), passing the genetic instruction to assemble amino acids, proteins and lipid at its smooth end. Also, any mismatch of nucleus with mitochondria (MT) having own small genome for energy production had led to reprogramming failure. (D. Wallace, UC Irvine, Nature,Vol. 439, pp.653). We ask "whether a guest DNA shall come with its servants, ER, MT, etc or not." It seemed to be logical to have a whole package replaced the embryonic host cell, equipped with all housekeeping, energy production and mitosis functionalities except the genetic information. To answer this hypothesis, we design a bio-NanoRobot having a surgical precision in removing the desired nucleus with or without its attached ER and MT material. The design is based on a real-time multiplexing principle of combining both the soft-contact-vision of the Nobel Laureate Binning called Atomic Force Microscope (AFM) and the hard-grasp-action called NanoRobot TM by Xi and Szu, 2004. However, applying it, we must re-design a new bio-NanoRobot, consisting of two parts: (a) multiple resolution analysis (MRA) using AI to control a dual-resolution vision system: the soft-contact-vision AFM co-registered with a on-contact high resolution imaging; and (b) two cantilever arms capable to hold and enucleate a cell. The calibration and automation are controlled by AI Case-Based reasoning (CBR) together with AI Blackboard (BB) of the taxonomy, necessary for integrating different tool's tolerance and resolution at the same location. Moreover, keeping the biological sample in one place, while a set of tools rotates upon it similar

Efficient fabrication method of nano-grating for 3D holographic display with full parallax views.

PubMed

Wan, Wenqiang; Qiao, Wen; Huang, Wenbin; Zhu, Ming; Fang, Zongbao; Pu, Donglin; Ye, Yan; Liu, Yanhua; Chen, Linsen

2016-03-21

Without any special glasses, multiview 3D displays based on the diffractive optics can present high resolution, full-parallax 3D images in an ultra-wide viewing angle. The enabling optical component, namely the phase plate, can produce arbitrarily distributed view zones by carefully designing the orientation and the period of each nano-grating pixel. However, such 3D display screen is restricted to a limited size due to the time-consuming fabricating process of nano-gratings on the phase plate. In this paper, we proposed and developed a lithography system that can fabricate the phase plate efficiently. Here we made two phase plates with full nano-grating pixel coverage at a speed of 20 mm²/mins, a 500 fold increment in the efficiency when compared to the method of E-beam lithography. One 2.5-inch phase plate generated 9-view 3D images with horizontal-parallax, while the other 6-inch phase plate produced 64-view 3D images with full-parallax. The angular divergence in horizontal axis and vertical axis was 1.5 degrees, and 1.25 degrees, respectively, slightly larger than the simulated value of 1.2 degrees by Finite Difference Time Domain (FDTD). The intensity variation was less than 10% for each viewpoint, in consistency with the simulation results. On top of each phase plate, a high-resolution binary masking pattern containing amplitude information of all viewing zone was well aligned. We achieved a resolution of 400 pixels/inch and a viewing angle of 40 degrees for 9-view 3D images with horizontal parallax. In another prototype, the resolution of each view was 160 pixels/inch and the view angle was 50 degrees for 64-view 3D images with full parallax. As demonstrated in the experiments, the homemade lithography system provided the key fabricating technology for multiview 3D holographic display.

A microfluidic thermometer: Precise temperature measurements in microliter- and nanoliter-scale volumes

PubMed Central

McKenzie, Brittney A.

2017-01-01

Measuring the temperature of a sample is a fundamental need in many biological and chemical processes. When the volume of the sample is on the microliter or nanoliter scale (e.g., cells, microorganisms, precious samples, or samples in microfluidic devices), accurate measurement of the sample temperature becomes challenging. In this work, we demonstrate a technique for accurately determining the temperature of microliter volumes using a simple 3D-printed microfluidic chip. We accomplish this by first filling “microfluidic thermometer” channels on the chip with substances with precisely known freezing/melting points. We then use a thermoelectric cooler to create a stable and linear temperature gradient along these channels within a measurement region on the chip. A custom software tool (available as online Supporting Information) is then used to find the locations of solid-liquid interfaces in the thermometer channels; these locations have known temperatures equal to the freezing/melting points of the substances in the channels. The software then uses the locations of these interfaces to calculate the temperature at any desired point within the measurement region. Using this approach, the temperature of any microliter-scale on-chip sample can be measured with an uncertainty of about a quarter of a degree Celsius. As a proof-of-concept, we use this technique to measure the unknown freezing point of a 50 microliter volume of solution and demonstrate its feasibility on a 400 nanoliter sample. Additionally, this technique can be used to measure the temperature of any on-chip sample, not just near-zero-Celsius freezing points. We demonstrate this by using an oil that solidifies near room temperature (coconut oil) in a microfluidic thermometer to measure on-chip temperatures well above zero Celsius. By providing a low-cost and simple way to accurately measure temperatures in small volumes, this technique should find applications in both research and educational

Nano-extrusion: a promising tool for continuous manufacturing of solid nano-formulations.

PubMed

Baumgartner, Ramona; Eitzlmayr, Andreas; Matsko, Nadejda; Tetyczka, Carolin; Khinast, Johannes; Roblegg, Eva

2014-12-30

Since more than 40% of today's drugs have low stability, poor solubility and/or limited ability to cross certain biological barriers, new platform technologies are required to address these challenges. This paper describes a novel continuous process that converts a stabilized aqueous nano-suspension into a solid oral formulation in a single step (i.e., the NANEX process) in order to improve the solubility of a model drug (phenytoin). Phenytoin nano-suspensions were prepared via media milling using different stabilizers. A stable nano-suspension was obtained using Tween(®) 80 as a stabilizer. The matrix material (Soluplus(®)) was gravimetrically fed into the hot melt extruder. The suspension was introduced through a side feeding device and mixed with the molten polymer to immediately devolatilize the water in the nano-suspension. Phenytoin nano-crystals were dispersed and embedded in the molten polymer. Investigation of the nano-extrudates via transmission electron microscopy and atomic force microscopy showed that the nano-crystals were embedded de-aggregated in the extrudates. Furthermore, no changes in the crystallinity (due to the mechanical and thermal stress) occurred. The dissolution studies confirmed that the prepared nano-extrudates increased the solubility of nano-crystalline phenytoin, regardless of the polymer. Our work demonstrates that NANEX represents a promising new platform technology in the design of novel drug delivery systems to improve drug performance. Copyright © 2014 Elsevier B.V. All rights reserved.

Dynamic transfer applied to secondary ion imaging over large scanned fields with the nanoSIMS 50 at high mass resolution

NASA Astrophysics Data System (ADS)

Slodzian, Georges; Wu, Ting-Di; Duprat, Jean; Engrand, Cécile; Guerquin-Kern, Jean-Luc

2017-12-01

Dynamic transfer is an adaptive optical approach used for coupling a scanning ion probe with the mass spectrometer designed for analyzing sputtered ions emanating from the probe impact. Its tuning is of crucial importance for getting uniform signal collection over large scanning fields and therefore scanning images free of vignetting in a context of high mass resolution. Revisiting the optical design of the NanoSIMS 50 instrument, where the same set of lenses focuses the primary ion probe on the sample and collects secondary ions from the sample, led us to develop novel experimental procedures to achieve dynamic transfer tuning and overcome instrumental imperfections. It is the case for scanning distortion that may be induced by the octopole used for correcting probe astigmatism and may cause irreducible vignetting on scanning images. We show that it is possible to develop complete tuning procedures by compromising temporarily on the sharpness of the probe focus. Most importantly, we show that, in a context of high mass resolution, the transfer does not significantly disturb isotopic ratios over large scanned fields provided external coils are properly adjusted to compensate ambient magnetic fields. Deepening the procedures led us to demonstrate that the scanning center of the probe may not coincide with the imaging center of COOL, Coaxial Objective Lenses forming the probe and extracting secondary ions. We have checked that bringing those two centers into coincidence resulted in a better image quality over large fields. In the present work, we show how to handle the secondary beam in order to position it before it enters the spectrometer. That capability is essential for optimizing transmission at high mass resolution by aligning the secondary beam axis on a given entrance axis of the spectrometer. These results led us to propose several instrumental improvements including the crucial interest of an additional octopole upstream in the primary ion probe column to

HPT: A High Spatial Resolution Multispectral Sensor for Microsatellite Remote Sensing

PubMed Central

Takahashi, Yukihiro; Sakamoto, Yuji; Kuwahara, Toshinori

2018-01-01

Although nano/microsatellites have great potential as remote sensing platforms, the spatial and spectral resolutions of an optical payload instrument are limited. In this study, a high spatial resolution multispectral sensor, the High-Precision Telescope (HPT), was developed for the RISING-2 microsatellite. The HPT has four image sensors: three in the visible region of the spectrum used for the composition of true color images, and a fourth in the near-infrared region, which employs liquid crystal tunable filter (LCTF) technology for wavelength scanning. Band-to-band image registration methods have also been developed for the HPT and implemented in the image processing procedure. The processed images were compared with other satellite images, and proven to be useful in various remote sensing applications. Thus, LCTF technology can be considered an innovative tool that is suitable for future multi/hyperspectral remote sensing by nano/microsatellites. PMID:29463022

3D positioning scheme exploiting nano-scale IR-UWB orthogonal pulses.

PubMed

Kim, Nammoon; Kim, Youngok

2011-10-04

In these days, the development of positioning technology for realizing ubiquitous environments has become one of the most important issues. The Global Positioning System (GPS) is a well-known positioning scheme, but it is not suitable for positioning in in-door/building environments because it is difficult to maintain line-of-sight condition between satellites and a GPS receiver. To such problem, various positioning methods such as RFID, WLAN, ZigBee, and Bluetooth have been developed for indoor positioning scheme. However, the majority of positioning schemes are focused on the two-dimension positioning even though three-dimension (3D) positioning information is more useful especially in indoor applications, such as smart space, U-health service, context aware service, etc. In this paper, a 3D positioning system based on mutually orthogonal nano-scale impulse radio ultra-wideband (IR-UWB) signals and cross array antenna is proposed. The proposed scheme uses nano-scale IR-UWB signals providing fine time resolution and high-resolution multiple signal specification algorithm for the time-of-arrival and the angle-of-arrival estimation. The performance is evaluated over various IEEE 802.15.4a channel models, and simulation results show the effectiveness of proposed scheme.

Combinatorial Nano-Bio Interfaces.

PubMed

Cai, Pingqiang; Zhang, Xiaoqian; Wang, Ming; Wu, Yun-Long; Chen, Xiaodong

2018-06-08

Nano-bio interfaces are emerging from the convergence of engineered nanomaterials and biological entities. Despite rapid growth, clinical translation of biomedical nanomaterials is heavily compromised by the lack of comprehensive understanding of biophysicochemical interactions at nano-bio interfaces. In the past decade, a few investigations have adopted a combinatorial approach toward decoding nano-bio interfaces. Combinatorial nano-bio interfaces comprise the design of nanocombinatorial libraries and high-throughput bioevaluation. In this Perspective, we address challenges in combinatorial nano-bio interfaces and call for multiparametric nanocombinatorics (composition, morphology, mechanics, surface chemistry), multiscale bioevaluation (biomolecules, organelles, cells, tissues/organs), and the recruitment of computational modeling and artificial intelligence. Leveraging combinatorial nano-bio interfaces will shed light on precision nanomedicine and its potential applications.

p{sup +}-doping analysis of laser fired contacts for silicon solar cells by Kelvin probe force microscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ebser, J., E-mail: Jan.Ebser@uni-konstanz.de; Sommer, D.; Fritz, S.

Local rear contacts for silicon passivated emitter and rear contact solar cells can be established by point-wise treating an Al layer with laser radiation and thereby establishing an electrical contact between Al and Si bulk through the dielectric passivation layer. In this laser fired contacts (LFC) process, Al can establish a few μm thick p{sup +}-doped Si region below the metal/Si interface and forms in this way a local back surface field which reduces carrier recombination at the contacts. In this work, the applicability of Kelvin probe force microscopy (KPFM) to the investigation of LFCs considering the p{sup +}-doping distributionmore » is demonstrated. The method is based on atomic force microscopy and enables the evaluation of the lateral 2D Fermi-level characteristics at sub-micrometer resolution. The distribution of the electrical potential and therefore the local hole concentration in and around the laser fired region can be measured. KPFM is performed on mechanically polished cross-sections of p{sup +}-doped Si regions formed by the LFC process. The sample preparation is of great importance because the KPFM signal is very surface sensitive. Furthermore, the measurement is responsive to sample illumination and the height of the applied voltage between tip and sample. With other measurement techniques like micro-Raman spectroscopy, electrochemical capacitance-voltage, and energy dispersive X-ray analysis, a high local hole concentration in the range of 10{sup 19 }cm{sup −3} is demonstrated in the laser fired region. This provides, in combination with the high spatial resolution of the doping distribution measured by KPFM, a promising approach for microscopic understanding and further optimization of the LFC process.« less

A Field Assessment of a Prototype Meter for Measuring the Wet-Bulb Globe-Thermometer Index

PubMed Central

Walters, J. D.

1968-01-01

A prototype electronic instrument for the direct measurement of the wet-bulb globe-thermometer index is described. An assessment is made of its accuracy, as compared with W.B.G.T. indices calculated from conventional thermometric data, and a comparison is made between W.B.G.T. values read from the meter and effective or corrected effective temperatures derived from separate thermometric and air velocity recording instruments in the same climates. The instrument proved to be reliable and accurate over a wide range of climates and is a useful self-contained device for use in habitability surveys and similar investigations. Images PMID:5663429

Linear and ultrafast nonlinear plasmonics of single nano-objects

NASA Astrophysics Data System (ADS)

Crut, Aurélien; Maioli, Paolo; Vallée, Fabrice; Del Fatti, Natalia

2017-03-01

Single-particle optical investigations have greatly improved our understanding of the fundamental properties of nano-objects, avoiding the spurious inhomogeneous effects that affect ensemble experiments. Correlation with high-resolution imaging techniques providing morphological information (e.g. electron microscopy) allows a quantitative interpretation of the optical measurements by means of analytical models and numerical simulations. In this topical review, we first briefly recall the principles underlying some of the most commonly used single-particle optical techniques: near-field, dark-field, spatial modulation and photothermal microscopies/spectroscopies. We then focus on the quantitative investigation of the surface plasmon resonance (SPR) of metallic nano-objects using linear and ultrafast optical techniques. While measured SPR positions and spectral areas are found in good agreement with predictions based on Maxwell’s equations, SPR widths are strongly influenced by quantum confinement (or, from a classical standpoint, surface-induced electron scattering) and, for small nano-objects, cannot be reproduced using the dielectric functions of bulk materials. Linear measurements on single nano-objects (silver nanospheres and gold nanorods) allow a quantification of the size and geometry dependences of these effects in confined metals. Addressing the ultrafast response of an individual nano-object is also a powerful tool to elucidate the physical mechanisms at the origin of their optical nonlinearities, and their electronic, vibrational and thermal relaxation processes. Experimental investigations of the dynamical response of gold nanorods are shown to be quantitatively modeled in terms of modifications of the metal dielectric function enhanced by plasmonic effects. Ultrafast spectroscopy can also be exploited to unveil hidden physical properties of more complex nanosystems. In this context, two-color femtosecond pump-probe experiments performed on individual

Enantiomeric separation of some demethylated analogues of clofibric acid by capillary zone electrophoresis and nano-liquid chromatography.

PubMed

Fantacuzzi, Marialuigia; Bettoni, Giancarlo; D'Orazio, Giovanni; Fanali, Salvatore

2006-03-01

The enantiomeric separation of some demethylated analogues of clofibric acid, namely 2-(6-chloro-benzothiazol-2-ylsulfanyl)-, 2-(6-methoxy-benzothiazol-2-ylsulfanyl)-, 2-(quinolin-2-yloxy)-, 2-(6-chloro-quinolin-2-yloxy)-, 2-(7-chloro-quinolin-4-yloxy)-propionic acid (compounds A-E, respectively), has been studied by CZE and nano-LC using for the first technique two beta-CD derivatives and vancomycin added to the BGE and vancomycin-modified silica particles for the second one, with the aim to find the optimum experimental conditions for the baseline resolution. The type and the concentration of the chiral selector added to the BGE, the buffer pH, the type of organic modifier and its concentration, the capillary temperature and the applied voltage played a very important role in the enantioresolution of the analysed compounds. The use of 6-monodeoxy-6-monoamino-beta-CD allowed to achieve baseline resolution of four of five clofibric acid derivatives in less than 10 min while heptakis-(2,3,6-tri-O-methyl)-beta-CD partially resolved the same compounds in their enantiomers. Employing vancomycin as the chiral selector in CZE, the counter-current partial filling method was chosen achieving baseline resolution of four analytes. All the studied compounds were enantioresolved employing a capillary column packed with vancomycin stationary phase by nano-LC, and the resolution was strongly influenced by the concentration of the organic modifier and by the pH of the mobile phase. The best results were achieved at pH 4.5 in presence of 60% of methanol (MeOH). However, longer analysis times were observed in the experiments carried out by nano-LC.

Chemical Imaging of the Cell Membrane by NanoSIMS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Weber, P K; Kraft, M L; Frisz, J F

2010-02-23

using a Cameca NanoSIMS 50 to probe membrane organization and test microdomain hypotheses. The NanoSIMS is an imaging secondary ion mass spectrometer with an unprecedented combination of spatial resolution, sensitivity and mass specificity. It has 50 nm lateral resolution and is capable of detecting 1 in 20 nitrogen atoms while excluding near-neighbor isobaric interferences. The tightly focused cesium ion beam is rastered across the sample to produce simultaneous, quantitative digital images of up to five different masses. By labeling each specific components of a membrane with a unique rare stable isotope or element and mapping the location of the labels with the NanoSIMS, the location of the each labeled component can be determined and quantified. This new approach to membrane composition analysis allows molecular interactions of biological membranes to be probed at length-scales relevant to lipid rafts (10s to 100s of nm) that were not previously possible. Results from our most recent experiments analyzing whole cells will be presented.« less

MAVEN Observations of Partially Developed Kelvin-Helmholtz Vortices at Mars.

NASA Technical Reports Server (NTRS)

Ruhunusiri, Suranga; Halekas, J. S.; McFadden, J. P.; Connerney, J. E. P.; Espley, J. R.; Harada, Y.; Livi, R.; Seki, C.; Mazelle, C.; Brain, D.

2016-01-01

We present preliminary results and interpretations for Mars Atmospheric and Volatile EvolutioN,(MAVEN) observations of magnetosheath-ionospheric boundary oscillations at Mars. Using centrifugal force arguments, we first predict that a signature of fully rolled up Kelvin-Helmholtz vortices at Mars is sheath ions that have a bulk motion toward the Sun. The sheath ions adjacent to a vortex should also accelerate to speeds higher than the mean sheath velocity. We also predict that while the ionospheric ions that are in the vortex accelerate antisunward, they never attain speeds exceeding that of the sheath ions, in stark contrast to KH vortices that arise at the Earths magnetopause. We observe accelerated sheath and ionospheric ions, but we do not observe sheath ions that have a bulk motion toward the Sun. Thus, we interpret these observations as KH vortices that have not fully rolled up.

Properties of the Average Distribution of Equatorial Kelvin Waves Investigated with the GROGRAT Ray Tracer

DTIC Science & Technology

2009-01-01

spheric quasi-biennial oscillation ( QBO ). In this paper we combine several measured data sets with the Gravity wave Regional Or Global RAy Tracer (GROGRAT...equatorial wave modes and a broad spectrum of gravity waves (GWs) Kelvin waves are one of the main drivers of the quasi-biennial oscil- lation ( QBO ) of the...and dy- namics in the stratosphere and mesosphere (even at high lati- tudes) are modulated or influenced by the QBO , showing the importance of the

Are nano-composites and nano-ionomers suitable for orthodontic bracket bonding?

PubMed

Uysal, Tancan; Yagci, Ahmet; Uysal, Banu; Akdogan, Gülsen

2010-02-01

The aim of this study was to test nano-composite (Filtek Supreme Plus Universal) and a newly introduced nano-ionomer (Ketac N100 Light Curing Nano-Ionomer) restorative to determine their shear bond strength (SBS) and failure site locations in comparison with a conventional light-cure orthodontic bonding adhesive (Transbond XT). Sixty freshly extracted human maxillary premolar teeth were arbitrarily divided into three equal groups. The brackets were bonded to the teeth in each group with different composites, according to the manufacturers' instructions. The SBS values of the brackets were recorded in Megapascals (MPa) using a universal testing machine. Adhesive remnant index scores were determined after failure of the brackets. The data were analysed using analysis of variance, Tukey honestly significant difference, and chi-square tests. The results demonstrated that group 1 (Transbond XT, mean: 12.60 +/- 4.48 MPa) had a higher SBS than that of group 2 (nano-composite, mean: 8.33 +/- 5.16 MPa; P < 0.05) and group 3 (nano-ionomer, mean: 6.14 +/- 2.12 MPa; P < 0.001). No significant differences in debond locations were found among the three groups. Nano-composites and nano-ionomers may be suitable for bonding since they fulfil the previously suggested SBS ranges for clinical acceptability, but they are inferior to a conventional orthodontic composite.

Stochastic volatility models and Kelvin waves

NASA Astrophysics Data System (ADS)

Lipton, Alex; Sepp, Artur

2008-08-01

We use stochastic volatility models to describe the evolution of an asset price, its instantaneous volatility and its realized volatility. In particular, we concentrate on the Stein and Stein model (SSM) (1991) for the stochastic asset volatility and the Heston model (HM) (1993) for the stochastic asset variance. By construction, the volatility is not sign definite in SSM and is non-negative in HM. It is well known that both models produce closed-form expressions for the prices of vanilla option via the Lewis-Lipton formula. However, the numerical pricing of exotic options by means of the finite difference and Monte Carlo methods is much more complex for HM than for SSM. Until now, this complexity was considered to be an acceptable price to pay for ensuring that the asset volatility is non-negative. We argue that having negative stochastic volatility is a psychological rather than financial or mathematical problem, and advocate using SSM rather than HM in most applications. We extend SSM by adding volatility jumps and obtain a closed-form expression for the density of the asset price and its realized volatility. We also show that the current method of choice for solving pricing problems with stochastic volatility (via the affine ansatz for the Fourier-transformed density function) can be traced back to the Kelvin method designed in the 19th century for studying wave motion problems arising in fluid dynamics.

Bilateral Comparison of Blackbodies for Clinical Infrared Ear Thermometers between NIMT and NMIJ

NASA Astrophysics Data System (ADS)

Manoi, A.; Norranim, U.; Kaneko, Y.; Ishii, J.

2014-04-01

This article describes the results of the bilateral comparison of blackbodies for infrared ear thermometers (IRETs) between the National Institute of Metrology (Thailand), NIMT, and the National Metrology Institute of Japan (NMIJ). The purpose of this comparison was to ensure consistency of the national radiance temperature scales for IRETs maintained by NIMT and NMIJ. Results of the measurements indicate differences in radiance temperature within 10 mK with a maximum measurement uncertainty of 64 mK. The equivalence of the radiance temperature scales realized by both NIMT and NMIJ in the range of 35 C to 42 C for IRET calibration is indicated. The results of this bilateral comparison can be used in terms of quality assurance and validation of calibration.

Magnetic Nano-Materials: Truly Sustainable Green Chemistry Nano Catalysis

EPA Science Inventory

We envisioned a novel nano-catalyst system, which can bridge the homogenous and heterogeneous system, and simultaneously be cheaper, easily accessible (sustainable) and possibly does not require elaborate work-up. Because of its nano-size, i.e. high surface area, the contact betw...

Integrating Landsat-8, Sentinel-2, and nano-satellite data for deriving atmospherically corrected vegetation indices at enhanced spatio-temporal resolution

NASA Astrophysics Data System (ADS)

Houborg, Rasmus; McCabe, Matthew F.; Ershadi, Ali

2017-04-01

Flocks of nano-satellites are emerging as an economic resource for overcoming spatio-temporal constraints of conventional single-sensor satellite missions. Planet Labs operates an expanding constellation of currently more than 40 CubeSats (30x10x10 cm3), which will facilitate daily capture of broadband RGB and near-infrared (NIR) imagery for every location on earth at a 3-5 m ground sampling distance. However, data acquired by these miniaturized satellites lack rigorous radiometric corrections and radiance conversions and should be used in synergy with high quality imagery required by conventional large satellites such as Landsat-8 (L8) and Sentinel-2 (S2) in order to realize the full potential of this game changing observational resource. This study integrates L8, S2 and Planet data acquired over sites in Saudi Arabia and the state of California for deriving cross-sensor consistent and atmospherically corrected Vegetation Indices (VI) that may serve as important metrics for vegetation growth, health, and productivity. An automated framework, based on 6S and satellite retrieved atmospheric state and aerosol inputs, is first applied to L8 and S2 at-sensor radiances for the production of atmospherically corrected VIs. Scale-consistent Planet RGB and NIR imagery is then related to the corrected VI data using a selective, scene-specific, and computationally fast machine learning approach. The developed technique uses the closest pair of Planet and L8/S2 scenes in the training of the predictive VI models and accounts for changes in cover conditions over the acquisition timespan. Application of the models to full resolution Planet imagery results in cross-sensor consistent VI estimates at the scale and time of the nano-satellite acquisition. The utility of the approach for reproducing spatial features in L8 and S2 based indices based on Planet imagery is evaluated. The technique is generic, computationally efficient, and extendable and serves well for implementation

Dynamic nano-imaging of label-free living cells using electron beam excitation-assisted optical microscope

PubMed Central

Fukuta, Masahiro; Kanamori, Satoshi; Furukawa, Taichi; Nawa, Yasunori; Inami, Wataru; Lin, Sheng; Kawata, Yoshimasa; Terakawa, Susumu

2015-01-01

Optical microscopes are effective tools for cellular function analysis because biological cells can be observed non-destructively and non-invasively in the living state in either water or atmosphere condition. Label-free optical imaging technique such as phase-contrast microscopy has been analysed many cellular functions, and it is essential technology for bioscience field. However, the diffraction limit of light makes it is difficult to image nano-structures in a label-free living cell, for example the endoplasmic reticulum, the Golgi body and the localization of proteins. Here we demonstrate the dynamic imaging of a label-free cell with high spatial resolution by using an electron beam excitation-assisted optical (EXA) microscope. We observed the dynamic movement of the nucleus and nano-scale granules in living cells with better than 100 nm spatial resolution and a signal-to-noise ratio (SNR) around 10. Our results contribute to the development of cellular function analysis and open up new bioscience applications. PMID:26525841

Dynamic nano-imaging of label-free living cells using electron beam excitation-assisted optical microscope.

PubMed

Fukuta, Masahiro; Kanamori, Satoshi; Furukawa, Taichi; Nawa, Yasunori; Inami, Wataru; Lin, Sheng; Kawata, Yoshimasa; Terakawa, Susumu

2015-11-03

Optical microscopes are effective tools for cellular function analysis because biological cells can be observed non-destructively and non-invasively in the living state in either water or atmosphere condition. Label-free optical imaging technique such as phase-contrast microscopy has been analysed many cellular functions, and it is essential technology for bioscience field. However, the diffraction limit of light makes it is difficult to image nano-structures in a label-free living cell, for example the endoplasmic reticulum, the Golgi body and the localization of proteins. Here we demonstrate the dynamic imaging of a label-free cell with high spatial resolution by using an electron beam excitation-assisted optical (EXA) microscope. We observed the dynamic movement of the nucleus and nano-scale granules in living cells with better than 100 nm spatial resolution and a signal-to-noise ratio (SNR) around 10. Our results contribute to the development of cellular function analysis and open up new bioscience applications.

Dynamic nano-imaging of label-free living cells using electron beam excitation-assisted optical microscope

NASA Astrophysics Data System (ADS)

Fukuta, Masahiro; Kanamori, Satoshi; Furukawa, Taichi; Nawa, Yasunori; Inami, Wataru; Lin, Sheng; Kawata, Yoshimasa; Terakawa, Susumu

2015-11-01

Optical microscopes are effective tools for cellular function analysis because biological cells can be observed non-destructively and non-invasively in the living state in either water or atmosphere condition. Label-free optical imaging technique such as phase-contrast microscopy has been analysed many cellular functions, and it is essential technology for bioscience field. However, the diffraction limit of light makes it is difficult to image nano-structures in a label-free living cell, for example the endoplasmic reticulum, the Golgi body and the localization of proteins. Here we demonstrate the dynamic imaging of a label-free cell with high spatial resolution by using an electron beam excitation-assisted optical (EXA) microscope. We observed the dynamic movement of the nucleus and nano-scale granules in living cells with better than 100 nm spatial resolution and a signal-to-noise ratio (SNR) around 10. Our results contribute to the development of cellular function analysis and open up new bioscience applications.

Probing the energy levels of perovskite solar cells via Kelvin probe and UV ambient pressure photoemission spectroscopy.

PubMed

Harwell, J R; Baikie, T K; Baikie, I D; Payne, J L; Ni, C; Irvine, J T S; Turnbull, G A; Samuel, I D W

2016-07-20

The field of organo-lead halide perovskite solar cells has been rapidly growing since their discovery in 2009. State of the art devices are now achieving efficiencies comparable to much older technologies like silicon, while utilising simple manufacturing processes and starting materials. A key parameter to consider when optimising solar cell devices or when designing new materials is the position and effects of the energy levels in the materials. We present here a comprehensive study of the energy levels present in a common structure of perovskite solar cell using an advanced macroscopic Kelvin probe and UV air photoemission setup. By constructing a detailed map of the energy levels in the system we are able to predict the importance of each layer to the open circuit voltage of the solar cell, which we then back up through measurements of the surface photovoltage of the cell under white illumination. Our results demonstrate the effectiveness of air photoemission and Kelvin probe contact potential difference measurements as a method of identifying the factors contributing to the open circuit voltage in a solar cell, as well as being an excellent way of probing the physics of new materials.

Multimodal non-linear optical imaging for the investigation of drug nano-/microcrystal-cell interactions.

PubMed

Darville, Nicolas; Saarinen, Jukka; Isomäki, Antti; Khriachtchev, Leonid; Cleeren, Dirk; Sterkens, Patrick; van Heerden, Marjolein; Annaert, Pieter; Peltonen, Leena; Santos, Hélder A; Strachan, Clare J; Van den Mooter, Guy

2015-10-01

Drug nano-/microcrystals are being used for sustained parenteral drug release, but safety and efficacy concerns persist as the knowledge of the in vivo fate of long-living particulates is limited. There is a need for techniques enabling the visualization of drug nano-/microcrystals in biological matrices. The aim of this work was to explore the potential of coherent anti-Stokes Raman scattering (CARS) microscopy, supported by other non-linear optical methods, as an emerging tool for the investigation of cellular and tissue interactions of unlabeled and non-fluorescent nano-/microcrystals. Raman and CARS spectra of the prodrug paliperidone palmitate (PP), paliperidone (PAL) and several suspension stabilizers were recorded. PP nano-/microcrystals were incubated with RAW 264.7 macrophages in vitro and their cellular disposition was investigated using a fully-integrated multimodal non-linear optical imaging platform. Suitable anti-Stokes shifts (CH stretching) were identified for selective CARS imaging. CARS microscopy was successfully applied for the selective three-dimensional, non-perturbative and real-time imaging of unlabeled PP nano-/microcrystals having dimensions larger than the optical lateral resolution of approximately 400nm, in relation to the cellular framework in cell cultures and ex vivo in histological sections. In conclusion, CARS microscopy enables the non-invasive and label-free imaging of (sub)micron-sized (pro-)drug crystals in complex biological matrices and could provide vital information on poorly understood nano-/microcrystal-cell interactions in future. Copyright © 2015 Elsevier B.V. All rights reserved.

Study on Locally Confined Deposition of Si Nanocrystals in High-Aspect-Ratio Si Nano-Pillar Arrays for Nano-Electronic and Nano-Photonic Applications II

DTIC Science & Technology

2010-12-03

photoluminescence characteristics of equivalent-size controlled silicon quantum dots by employing a nano-porous aluminum oxide membrane as the template for growing...synthesis of Si quantum dots (Si-QDs) embedded in low-temperature (500oC) annealed Si-rich SiOx nano-rod deposited in nano-porous anodic aluminum oxide ...characteristics of the equivalent-size controlled Si-QDs by employing the nano-porous AAO membrane as the template for growing Si-rich SiOx nano-rods

Development of a Timepix based detector for the NanoXCT project

NASA Astrophysics Data System (ADS)

Nachtrab, F.; Hofmann, T.; Speier, C.; Lučić, J.; Firsching, M.; Uhlmann, N.; Takman, P.; Heinzl, C.; Holmberg, A.; Krumm, M.; Sauerwein, C.

2015-11-01

The NanoXCT EU FP7 project [1] aims at developing a laboratory, i.e. bench top sized X-ray nano-CT system with a large field-of-view (FOV) for non-destructive testing needs in the micro- and nano-technology sector. The targeted voxel size is 50 nm at 0.175 mm FOV, the maximum FOV is 1 mm at 285 nm voxel size. Within the project a suitable X-ray source, detector and manipulation system have been developed. The system concept [2] omits the use of X-ray optics, to be able to provide a large FOV of up to 1 mm and to preserve the flexibility of state-of-the-art micro-CT systems. The targeted resolution will be reached via direct geometric magnification made possible by the development of a specialized high-flux nano-focus transmission X-ray tube. The end-user's demand for elemental analysis will be covered by energy-resolved measurement techniques, in particular a K-edge imaging method. Timepix [3] modules were chosen as the basis for the detector system, since a photon counting detector is advantageous for the long exposure times that come with very small focal spot sizes. Additional advantages are the small pixel size and adjustable energy threshold. To fulfill the requirements on field-of-view, a detector width 0> 300 pixels was needed. The NanoXCT detector consists of four Hexa modules with 500 μm silicon sensors supplied by X-ray Imaging Europe. An adapter board was developed to connect all four modules to one Fitpix3 readout. The final detector has an active area of 3072 × 512 pixels or approximately 17 × 3 cm2.In this contribution we present the development of the Timepix based NanoXCT detector, it's application in the NanoXCT project for CT and material specific measurements and the current status of results.

A 6-bit 4 GS/s pseudo-thermometer segmented CMOS DAC

NASA Astrophysics Data System (ADS)

Yijun, Song; Wenyuan, Li

2014-06-01

A 6-bit 4 GS/s, high-speed and power-efficient DAC for ultra-high-speed transceivers in 60 GHz band millimeter wave technology is presented. A novel pseudo-thermometer architecture is proposed to realize a good compromise between the fast conversion speed and the chip area. Symmetrical and compact floor planning and layout techniques including tree-like routing, cross-quading and common-centroid method are adopted to guarantee the chip is fully functional up to near-Nyquist frequency in a standard 0.18 μm CMOS process. Post simulation results corroborate the feasibility of the designed DAC, which canperform good static and dynamic linearity without calibration. DNL errors and INL errors can be controlled within ±0.28 LSB and ±0.26 LSB, respectively. SFDR at 4 GHz clock frequency for a 1.9 GHz near-Nyquist sinusoidal output signal is 40.83 dB and the power dissipation is less than 37 mW.

Direct nano-patterning of graphene with helium ion beams

NASA Astrophysics Data System (ADS)

Naitou, Y.; Iijima, T.; Ogawa, S.

2015-01-01

Helium ion microscopy (HIM) was used for direct nano-patterning of single-layer graphene (SLG) on SiO2/Si substrates. This technique involves irradiation of the sample with accelerated helium ions (He+). Doses of 2.0 × 1016 He+ cm-2 from a 30 kV beam induced a metal-insulator transition in the SLG. The resolution of HIM patterning on SLG was investigated by fabricating nanoribbons and nanostructures. Analysis of scanning capacitance microscopy measurements revealed that the spatial resolution of HIM patterning depended on the dosage of He+ in a non-monotonic fashion. Increasing the dose from 2.0 × 1016 to 5.0 × 1016 He+ cm-2 improved the spatial resolution to several tens of nanometers. However, doses greater than 1.0 × 1017 He+ cm-2 degraded the patterning characteristics. Direct patterning using HIM is a versatile approach to graphene fabrication and can be applied to graphene-based devices.

Thermodynamic Behavior of Nano-sized Gold Clusters on the (001) Surface

NASA Technical Reports Server (NTRS)

Paik, Sun M.; Yoo, Sung M.; Namkung, Min; Wincheski, Russell A.; Bushnell, Dennis M. (Technical Monitor)

2001-01-01

We have studied thermal expansion of the surface layers of the hexagonally reconstructed Au (001) surface using a classical Molecular Dynamics (MD) simulation technique with an Embedded Atomic Method (EAM) type many-body potential. We find that the top-most hexagonal layer contracts as temperature increases, whereas the second layer expands or contracts depending on the system size. The magnitude of expansion coefficient of the top layer is much larger than that of the other layers. The calculated thermal expansion coefficients of the top-most layer are about -4.93 x 10(exp -5)Angstroms/Kelvin for the (262 x 227)Angstrom cluster and -3.05 x 10(exp -5)Angstroms/Kelvin for (101 x 87)Angstrom cluster. The Fast Fourier Transform (FFT) image of the atomic density shows that there exists a rotated domain of the top-most hexagonal cluster with rotation angle close to 1 degree at temperature T less than 1000Kelvin. As the temperature increases this domain undergoes a surface orientational phase transition. These predictions are in good agreement with previous phenomenological theories and experimental studies.

High-resolution quantitative determination of dielectric function by using scattering scanning near-field optical microscopy

PubMed Central

Tranca, D. E.; Stanciu, S. G.; Hristu, R.; Stoichita, C.; Tofail, S. A. M.; Stanciu, G. A.

2015-01-01

A new method for high-resolution quantitative measurement of the dielectric function by using scattering scanning near-field optical microscopy (s-SNOM) is presented. The method is based on a calibration procedure that uses the s-SNOM oscillating dipole model of the probe-sample interaction and quantitative s-SNOM measurements. The nanoscale capabilities of the method have the potential to enable novel applications in various fields such as nano-electronics, nano-photonics, biology or medicine. PMID:26138665

To be nano or not to be nano?

NASA Astrophysics Data System (ADS)

Joachim, Christian

2005-02-01

Nanomaterials, nanostructures, nanostructured materials, nanoimprint, nanobiotechnology, nanophysics, nanochemistry, radical nanotechnology, nanosciences, nanooptics, nanoelectronics, nanorobotics, nanosoldiers, nanomedecine, nanoeconomy, nanobusiness, nanolawyer, nanoethics to name a few of the nanos. We need a clear definition of all these burgeoning fields for the sake of the grant attribution, for the sake of research program definition, and to avoid everyone being lost in so many nanos.

Conditions for the existence of Kelvin-Helmholtz instability in a CME

NASA Astrophysics Data System (ADS)

Páez, Andrés; Jatenco-Pereira, Vera; Falceta-Gonçcalves, Diego; Opher, Merav

The presence of Kelvin-Helmholtz instability (KHI) in the sheaths of Coronal Mass Ejections (CMEs) has been proposed and observed by several authors in the literature. In the present work, we assume their existence and propose a method to constrain the local properties, like the CME magnetic field intensity for the development of KHI. We study a CME in the initiation phase interacting with the slow solar wind (Zone I) and with the fast solar wind (Zone II). Based on the theory of magnetic KHI proposed by Chandrasekhar (1961) we found the radial heliocentric interval for the KHI existence, in particular we constrain it with the CME magnetic field intensity. We conclude that KHI may exist in both CME Zones but it is perceived that Zone I is more appropriated for the KHI formation.

Vector electric field measurement via position-modulated Kelvin probe force microscopy

NASA Astrophysics Data System (ADS)

Dwyer, Ryan P.; Smieska, Louisa M.; Tirmzi, Ali Moeed; Marohn, John A.

2017-10-01

High-quality spatially resolved measurements of electric fields are critical to understanding charge injection, charge transport, and charge trapping in semiconducting materials. Here, we report a variation of frequency-modulated Kelvin probe force microscopy that enables spatially resolved measurements of the electric field. We measure electric field components along multiple directions simultaneously by employing position modulation and lock-in detection in addition to numeric differentiation of the surface potential. We demonstrate the technique by recording linescans of the in-plane electric field vector in the vicinity of a patch of trapped charge in a 2,7-diphenyl[1]benzothieno[3,2-b][1]benzothiophene (DPh-BTBT) organic field-effect transistor. This technique is simple to implement and should be especially useful for studying electric fields in spatially inhomogeneous samples like organic transistors and photovoltaic blends.

Requirements Formulation and Dynamic Jitter Analysis for Fourier-Kelvin Stellar Interferometer

NASA Technical Reports Server (NTRS)

Liu, Kuo-Chia; Hyde, Tristram; Blaurock, Carl; Bolognese, Jeff; Howard, Joseph; Danchi, William

2004-01-01

The Fourier-Kelvin Stellar Interferometer (FKSI) has been proposed to detect and characterize extra solar giant planets. The baseline configuration for FKSI is a two- aperture, structurally connected nulling interferometer, capable of providing null depth less than lo4 in the infrared. The objective of this paper is to summarize the process for setting the top level requirements and the jitter analysis performed on FKSI to date. The first part of the paper discusses the derivation of dynamic stability requirements, necessary for meeting the FKSI nulling demands. An integrated model including structures, optics, and control systems has been developed to support dynamic jitter analysis and requirements verification. The second part of the paper describes how the integrated model is used to investigate the effects of reaction wheel disturbances on pointing and optical path difference stabilities.

Evolution of the magnetic field generated by the Kelvin-Helmholtz instability

DOE Office of Scientific and Technical Information (OSTI.GOV)

Modestov, M.; Bychkov, V.; Brodin, G.

2014-07-15

The Kelvin-Helmholtz instability in an ionized plasma is studied with a focus on the magnetic field generation via the Biermann battery (baroclinic) mechanism. The problem is solved by using direct numerical simulations of two counter-directed flows in 2D geometry. The simulations demonstrate the formation of eddies and their further interaction and merging resulting in a large single vortex. In contrast to general belief, it is found that the instability generated magnetic field may exhibit significantly different structures from the vorticity field, despite the mathematically identical equations controlling the magnetic field and vorticity evolution. At later stages of the nonlinear instabilitymore » development, the magnetic field may keep growing even after the hydrodynamic vortex strength has reached its maximum and started decaying due to dissipation.« less

A comparative study on accuracy of liquid crystal forehead, digital electronic axillary, infrared tympanic with glass-mercury rectal thermometer in infants and young children.

PubMed

Kongpanichkul, A; Bunjongpak, S

2000-09-01

This study was carried out to assess the accuracy of three devices namely, liquid crystal forehead, digital electronic axillary and infrared tympanic thermometer, using a glass-mercury rectal thermometer as the control. The subjects were two hundred children aged 0-48 months. The mean rectal temperature was 38.0 +/- 0.91 degrees C; forehead, 37.83 +/- 0.94 degrees C; tympanic, 37.77 +/- 0.95 degrees C, and axillary, 37.71 +/- 0.86 degrees C. Compared to the rectal temperature, all values were significantly lower (p < 0.05). Forehead, tympanic and axillary temperature differed from rectal temperature by at least 0.5 degrees C in 33.33 per cent, 23.5 per cent and 31.5 per cent of subjects, and at least 1 degrees C in 22 per cent, 1 per cent and 6 per cent of subjects respectively. Accuracy in detection of fever was 79 per cent for forehead, 85.5 per cent for tympanic and 84 per cent for axillary thermometry. Sensitivity of the three devices was 67-83 per cent in detection of fever and 64-77 per cent in detection of high fever. Tympanic thermometry had the best performance while forehead thermometry had the poorest. After using revised diagnostic threshold temperature by ROC curves, sensitivity of each device improved but accuracy was nearly the same. It is concluded that the three devices are not suitable as a substitute for a glass-mercury rectal thermometer in assessment of fever in infants and young children.

Nanoscale Resolution 3D Printing with Pin-Modified Electrified Inkjets for Tailorable Nano/Macrohybrid Constructs for Tissue Engineering.

PubMed

Kim, Jeong In; Kim, Cheol Sang

2018-04-18

Cells respond to their microenvironment, which is of a size comparable to that of the cells. The macroscale features of three-dimensional (3D) printing struts typically result in whole cell contact guidance (CCG). In contrast, at the nanoscale, where features are of a size similar to that of receptors of cells, the response of cells is more complex. The cell-nanotopography interaction involves nanoscale adhesion localized structures, which include cell adhesion-related particles that change in response to the clustering of integrin. For this reason, it is necessary to develop a technique for manufacturing tailorable nano/macrohybrid constructs capable of freely controlling the cellular activity. In this study, a hierarchical 3D nano- to microscale hybrid structure was fabricated by combinational processing of 3D printing and electrified inkjet spinning via pin motions. This method overcomes the disadvantages of conventional 3D printing, providing a novel combinatory technique for the fabrication of 3D hybrid constructs with excellent cell proliferation. Through a pin-modified electrified inkjet spinning, we have successfully fabricated customizable nano-/microscale hybrid constructs in a fibrous or mesh form, which can control the cell fate. We have conducted this study of cell-topography interactions from the fabrication approach to accelerate the development of next-generation 3D scaffolds.

The influence of the spectral emissivity of flat-plate calibrators on the calibration of IR thermometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cárdenas-García, D.; Méndez-Lango, E.

Flat Calibrators (FC) are an option for calibration of infrared thermometers (IT) with a fixed large target. FCs are neither blackbodies, nor gray-bodies; their spectral emissivity is lower than one and depends on wavelength. Nevertheless they are used as gray-bodies with a nominal emissivity value. FCs can be calibrated radiometrically using as reference a calibrated IR thermometer (RT). If an FC will be used to calibrate ITs that work in the same spectral range as the RT then its calibration is straightforward: the actual FC spectral emissivity is not required. This result is valid for any given fixed emissivity assessedmore » to the FC. On the other hand, when the RT working spectral range does not match with that of the ITs to be calibrated with the FC then it is required to know the FC spectral emissivity as part of the calibration process. For this purpose, at CENAM, we developed an experimental setup to measure spectral emissivity in the infrared spectral range, based on a Fourier transform infrared spectrometer. Not all laboratories have emissivity measurement capability in the appropriate wavelength and temperature ranges to obtain the spectral emissivity. Thus, we present an estimation of the error introduced when the spectral range of the RT used to calibrate an FC and the spectral ranges of the ITs to be calibrated with the FC do not match. Some examples are developed for the cases when RT and IT spectral ranges are [8,13] μm and [8,14] μm respectively.« less