Sample records for paint curing oven

  1. Adhesive bonded structural repair. II - Surface preparation procedures, tools, equipment and facilities

    NASA Astrophysics Data System (ADS)

    Wegman, Raymond F.; Tullos, Thomas R.

    1993-10-01

    A development status report is presented on the surface preparation procedures, tools, equipment, and facilities used in adhesively-bonded repair of aerospace and similar high-performance structures. These methods extend to both metallic and polymeric surfaces. Attention is given to the phos-anodize containment system, paint removal processes, tools for cutting composite prepreg and fabric materials, autoclaves, curing ovens, vacuum bagging, and controlled atmospheres.

  2. Strength of Geopolymer Cement Curing at Ambient Temperature by Non-Oven Curing Approaches: An Overview

    NASA Astrophysics Data System (ADS)

    Wattanachai, Pitiwat; Suwan, Teewara

    2017-06-01

    At the present day, a concept of environmentally friendly construction materials has been intensively studying to reduce the amount of releasing greenhouse gases. Geopolymer is one of the cementitious binders which can be produced by utilising pozzolanic wastes (e.g. fly ash or furnace slag) and also receiving much more attention as a low-CO2 emission material. However, to achieve excellent mechanical properties, heat curing process is needed to apply to geopolymer cement in a range of temperature around 40 to 90°C. To consume less oven-curing energy and be more convenience in practical work, the study on geopolymer curing at ambient temperature (around 20 to 25°C) is therefore widely investigated. In this paper, a core review of factors and approaches for non-oven curing geopolymer has been summarised. The performance, in term of strength, of each non-oven curing method, is also presented and analysed. The main aim of this review paper is to gather the latest study of ambient temperature curing geopolymer and to enlarge a feasibility of non-oven curing geopolymer development. Also, to extend the directions of research work, some approaches or techniques can be combined or applied to the specific properties for in-field applications and embankment stabilization by using soil-cement column.

  3. Effect of hydrated lime on compressive strength mortar of fly ash laterite soil geopolymer mortar

    NASA Astrophysics Data System (ADS)

    Wangsa, F. A.; Tjaronge, M. W.; Djamaluddin, A. R.; Muhiddin, A. B.

    2017-11-01

    This paper explored the suitability of fly ash, hydrated lime, and laterite soil with several activator (sodium hydroxide and sodium tiosulfate) to produce geopolymer mortar. Furthermore, the heat that released by hydrated lime was used instead of oven curing. In order to produce geopolymer mortar without oven curing, three variations of curing condition has been applied. Based on the result, all the curing condition showed that the hardener mortar can be produced and exhibited the increasing of compressive strength of geopolymer mortar from 3 days to 7 days without oven curing.

  4. 40 CFR 63.1179 - For curing ovens, what standards must I meet?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... operating limits for each curing oven: (1) Maintain the free-formaldehyde content of each resin lot and the formaldehyde content of each binder formulation at or below the specification ranges of the resin and binder...

  5. 40 CFR 63.1179 - For curing ovens, what standards must I meet?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... operating limits for each curing oven: (1) Maintain the free-formaldehyde content of each resin lot and the formaldehyde content of each binder formulation at or below the specification ranges of the resin and binder...

  6. Ultrasonic Coating and Holographic Exposure Technology. Phase 1

    DTIC Science & Technology

    2015-09-01

    introducing plaques to cure, which allowed the UV lamps to warm up. Temperature inside the UV oven could reach 35 °C if left on continuously. Curing time for...the deposition of thin films using an ultrasonic spray coater and patterning of the films using an ultraviolet ( UV ) laser. The main objectives for...required, and include such items as a corona discharge device, a UV curing oven, hot plate, and jigging for optics that were fabricated at Revision. Test

  7. 78 FR 26251 - Approval and Promulgation of Air Quality Implementation Plans; Texas; Revisions to Control of Air...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-05-06

    ... ovens used in wet-laid non-woven fiber mat manufacturing operations when nitrogen containing resins or other additives are used. These two actions affect NOx sources operating in the Dallas Fort-Worth (DFW... include low-temperature drying ovens and curing ovens used in wet-laid, non-woven fiber mat manufacturing...

  8. 2.45 GHz Microwave Processing and Its Influence on Glass Fiber Reinforced Plastics.

    PubMed

    Teufl, Daniel; Zaremba, Swen

    2018-05-18

    During the production of fiber-reinforced composite materials, liquid resin is introduced into the fiber material and cured, i.e., hardened. An elevated temperature is needed for this curing. Microwave curing of composites has been investigated for some time, but it has mostly been done using small domestic or laboratory equipment. However, no investigation has been carried out using an industrial-sized chamber-microwave for glass fiber-reinforced plastic (GFRP). Here, we show that microwave curing produces laminates of the same quality as oven-cured ones. The study shows that, if the process is done right, GFRP samples can be produced with an industrial scale microwave. Even if not fully cured, microwave samples show a glass transition temperature measured with DMA ( T g-DMA ) that is comparable to the T g-DMA according to the proposed cure cycle on the data sheet. Specific microwave-cured configurations show better inter-laminar shear strength than oven specimens. The results show that microwave-based heat introduction can be a beneficial curing method for GFRP laminates. A microwave-optimized process is faster and leads to better mechanical properties.

  9. 2.45 GHz Microwave Processing and Its Influence on Glass Fiber Reinforced Plastics

    PubMed Central

    Zaremba, Swen

    2018-01-01

    During the production of fiber-reinforced composite materials, liquid resin is introduced into the fiber material and cured, i.e., hardened. An elevated temperature is needed for this curing. Microwave curing of composites has been investigated for some time, but it has mostly been done using small domestic or laboratory equipment. However, no investigation has been carried out using an industrial-sized chamber-microwave for glass fiber-reinforced plastic (GFRP). Here, we show that microwave curing produces laminates of the same quality as oven-cured ones. The study shows that, if the process is done right, GFRP samples can be produced with an industrial scale microwave. Even if not fully cured, microwave samples show a glass transition temperature measured with DMA (Tg-DMA) that is comparable to the Tg-DMA according to the proposed cure cycle on the data sheet. Specific microwave-cured configurations show better inter-laminar shear strength than oven specimens. The results show that microwave-based heat introduction can be a beneficial curing method for GFRP laminates. A microwave-optimized process is faster and leads to better mechanical properties. PMID:29783684

  10. Effect of radiation light characteristics on surface hardness of paint-on resin for shade modification.

    PubMed

    Arikawa, Hiroyuki; Kanie, Takahito; Fujii, Koichi; Ban, Seiji

    2005-12-01

    The purpose of this study was to investigate the effect of radiation light characteristics--of different types of clinical light-curing unit--on polymerization efficiency, as determined by the surface hardness of light-cured paint-on resins. Four shades of paint-on resin for shade modification of restorative resins were used. Materials were cured using one laboratory and three clinical light-curing units with different light sources, namely tungsten-halogen, LED, plasma arc, and xenon flash lamps. Knoop hardness measurements were taken at both the top and bottom surfaces of the specimens to assess the mechanical properties and degree of polymerization. Both LED and plasma arc light units caused significantly poorer surface hardness than the halogen and laboratory xenon lights. In addition, the transparent shade was more sensitive to surface hardness than other chromatic shades. Our results indicated that the polymerization efficiency of paint-on resin was significantly influenced by the radiation light characteristics of clinical light-curing units.

  11. Effect of Molarity of Sodium Hydroxide and Curing Method on the Compressive Strength of Ternary Blend Geopolymer Concrete

    NASA Astrophysics Data System (ADS)

    Sathish Kumar, V.; Ganesan, N.; Indira, P. V.

    2017-07-01

    Concrete plays a vital role in the development of infrastructure and buildings all over the world. Geopolymer based cement-less concrete is one of the current findings in the construction industry which leads to a green environment. This research paper deals with the results of the use of Fly ash (FA), Ground Granulated Blast Furnace Slag (GGBS) and Metakaolin (MK) as a ternary blend source material in Geopolymer concrete (GPC). The aspects that govern the compressive strength of GPC like the proportion of source material, Molarity of Sodium Hydroxide (NaOH) and Curing methods were investigated. The purpose of this research is to optimise the local waste material and use them effectively as a ternary blend in GPC. Seven combinations of binder were made in this study with replacement of FA with GGBS and MK by 35%, 30%, 25%, 20%, 15%, 10%, 5% and 5%, 10%, 15%, 20%, 25%, 30%, 35% respectively. The molarity of NaOH solution was varied by 12M, 14M and 16M and two types of curing method were adopted, viz. Hot air oven curing and closed steam curing for 24 hours at 60°C (140°F). The samples were kept at ambient temperature till testing. The compressive strength was obtained after 7 days and 28 days for the GPC cubes. The test data reveals that the ternary blend GPC with molarity 14M cured by hot air oven produces the maximum compressive strength. It was also observed that the compressive strength of the oven cured GPC is approximately 10% higher than the steam cured GPC using the ternary blend.

  12. Improved method facilitates debulking and curing of phenolic impregnated asbestos

    NASA Technical Reports Server (NTRS)

    Gaines, P.

    1966-01-01

    Workpieces covered with phenolic impregnated asbestos tape and then wrapped with a specified thickness of nylon yarn under pressure, are debulked and cured in a standard oven. This method of debulking and curing is used in the fabrication of ablative chambers for the Gemini and Apollo attitude control engines.

  13. Study on compressive strength of self compacting mortar cubes under normal & electric oven curing methods

    NASA Astrophysics Data System (ADS)

    Prasanna Venkatesh, G. J.; Vivek, S. S.; Dhinakaran, G.

    2017-07-01

    In the majority of civil engineering applications, the basic building blocks were the masonry units. Those masonry units were developed as a monolithic structure by plastering process with the help of binding agents namely mud, lime, cement and their combinations. In recent advancements, the mortar study plays an important role in crack repairs, structural rehabilitation, retrofitting, pointing and plastering operations. The rheology of mortar includes flowable, passing and filling properties which were analogous with the behaviour of self compacting concrete. In self compacting (SC) mortar cubes, the cement was replaced by mineral admixtures namely silica fume (SF) from 5% to 20% (with an increment of 5%), metakaolin (MK) from 10% to 30% (with an increment of 10%) and ground granulated blast furnace slag (GGBS) from 25% to 75% (with an increment of 25%). The ratio between cement and fine aggregate was kept constant as 1: 2 for all normal and self compacting mortar mixes. The accelerated curing namely electric oven curing with the differential temperature of 128°C for the period of 4 hours was adopted. It was found that the compressive strength obtained from the normal and electric oven method of curing was higher for self compacting mortar cubes than normal mortar cube. The cement replacement by 15% SF, 20% MK and 25%GGBS obtained higher strength under both curing conditions.

  14. Determination of Significant Composite Processing Factors by Designed Experiment (MSFC Center Director's Discretionary Fund)

    NASA Technical Reports Server (NTRS)

    Finckenor, J. L.

    2003-01-01

    To determie composite material properties' effects from porcessing variables, a 3 factorial designed experiment with two replicates was conducted. The factors were cure method (oven versus autoclave), layup (hand versus tape-laying machine), and thickness (8 versus 52 ply). Four material systems were tested: AS4/3501-6, IM7/8551-7, IM7/F655 bismaleimide (BMI), and shear tests on IM7/F584. Material properties were G(sub 12), v(sub 12), E(sub 1c) and E(sub 2c). Since the samples were necessarily nonstandard, strengths, though recorded, cannot be considered valid. Void content was also compared. Autoclave curing helped material properties for the low modulus fiber material but showed little benefit for higher stiffness fibers. The number of plies was very important for epoxy composites but not for the BMI. E(sub 1) was generally unaffected by any factor. Particularly high void content did correlate to reduced properties. Autoclave curing reduced void content over oven curiing but a moderate amount of voids, less than 1 percent void content, didnot correlate with material properties. Oven cures and hand layups can produce high-quality parts. Part thickness of epoxy composites is important, though cure optimization may improve performance. Significant variations can be caused by processing and it is important that test coupons always reflect the layup and processes of the final part.

  15. 40 CFR Appendix A to Subpart IIIi... - Determination of Capture Efficiency of Automobile and Light-Duty Truck Spray Booth Emissions From...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... coating, i. 2.5.1You must weigh the blank panel. (Same as in bake oven panel test.) The mass of the blank... spray booth zones being tested. (Different than bake oven panel test.) This weighing must be conducted... and before the bake oven where the coating applied to the panel is cured, 2.5.5.2All of the flash-off...

  16. 40 CFR Appendix A to Subpart IIIi... - Determination of Capture Efficiency of Automobile and Light-Duty Truck Spray Booth Emissions From...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... coating, i. 2.5.1You must weigh the blank panel. (Same as in bake oven panel test.) The mass of the blank... spray booth zones being tested. (Different than bake oven panel test.) This weighing must be conducted... and before the bake oven where the coating applied to the panel is cured, 2.5.5.2All of the flash-off...

  17. 40 CFR Appendix A to Subpart IIIi... - Determination of Capture Efficiency of Automobile and Light-Duty Truck Spray Booth Emissions From...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... coating, i. 2.5.1You must weigh the blank panel. (Same as in bake oven panel test.) The mass of the blank... spray booth zones being tested. (Different than bake oven panel test.) This weighing must be conducted... and before the bake oven where the coating applied to the panel is cured, 2.5.5.2All of the flash-off...

  18. 40 CFR Appendix A to Subpart IIIi... - Determination of Capture Efficiency of Automobile and Light-Duty Truck Spray Booth Emissions From...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... coating, i. 2.5.1You must weigh the blank panel. (Same as in bake oven panel test.) The mass of the blank... spray booth zones being tested. (Different than bake oven panel test.) This weighing must be conducted... and before the bake oven where the coating applied to the panel is cured, 2.5.5.2All of the flash-off...

  19. 40 CFR Appendix A to Subpart IIIi... - Determination of Capture Efficiency of Automobile and Light-Duty Truck Spray Booth Emissions From...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... coating, i. 2.5.1You must weigh the blank panel. (Same as in bake oven panel test.) The mass of the blank... spray booth zones being tested. (Different than bake oven panel test.) This weighing must be conducted... and before the bake oven where the coating applied to the panel is cured, 2.5.5.2All of the flash-off...

  20. 40 CFR 63.3965 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ...; coating solvent flash-off, curing, and drying occurs within the capture system; and the removal or... spray booth and a curing oven. (b) Measuring capture efficiency. If the capture system does not meet... surface preparation activities and drying and curing time. (c) Liquid-to-uncaptured-gas protocol using a...

  1. 40 CFR 63.4165 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... system; coating solvent flash-off and coating, curing, and drying occurs within the capture system and... when being moved between a spray booth and a curing oven. (b) If the capture system does not meet both... surface preparation activities and drying or curing time. (c) Liquid-to-uncaptured-gas protocol using a...

  2. Characterization of concrete hardness by using sugarcane bagasse waste mixture by carbon oven curing process

    NASA Astrophysics Data System (ADS)

    Rino, Agus; Farida, Elvaswer, Dahlan, Dahyunir

    2017-01-01

    Sugarcane bagasse is one of the solid waste that can be processed as a mixture of structure materials. In the previous research, sugarcane bagasse has been processed and used as a mixture of portland cement, the manufacture of asbestos and also mixtures for manufacturing of brake pads that are frequently used in motor vehicle. Based on the previous research results, it is strongly necessary to develop a research about sugarcane bagasse for structure materials. The method used to determine the mechanical properties is tensile test and compression test. To obtain the intensity of material variations, it is needed to make various sizes of filtration carbon in the form of aggregate that is mixed into the tiles material. The size of the aggregate used in concrete material can be on 200 µm, 400 µm and 600 µm. This measure is taken in accordance with the size of the filtration apparatus. Furthermore, in obtaining sugarcane bagasse carbon, the researcher must do the oven curing process on 200 °C temperature and 3 hours in curing oven. In this research the best result is used bagasse powder mixtured 200 µm is 7. 2 MPa.

  3. Accelerated bridge paint test program.

    DOT National Transportation Integrated Search

    2011-07-06

    The accelerated bridge paint (AB-Paint) program evaluated a new Sherwin-Williams two-coat, : fast-curing paint system. The system is comprised of an organic zinc-rich primer (SW Corothane I : Galvapac One-Pack Zinc-Rich Primer B65 G11) and a polyurea...

  4. Rapid energy-efficient manufacturing of polymers and composites via frontal polymerization.

    PubMed

    Robertson, Ian D; Yourdkhani, Mostafa; Centellas, Polette J; Aw, Jia En; Ivanoff, Douglas G; Goli, Elyas; Lloyd, Evan M; Dean, Leon M; Sottos, Nancy R; Geubelle, Philippe H; Moore, Jeffrey S; White, Scott R

    2018-05-01

    Thermoset polymers and composite materials are integral to today's aerospace, automotive, marine and energy industries and will be vital to the next generation of lightweight, energy-efficient structures in these enterprises, owing to their excellent specific stiffness and strength, thermal stability and chemical resistance 1-5 . The manufacture of high-performance thermoset components requires the monomer to be cured at high temperatures (around 180 °C) for several hours, under a combined external pressure and internal vacuum 6 . Curing is generally accomplished using large autoclaves or ovens that scale in size with the component. Hence this traditional curing approach is slow, requires a large amount of energy and involves substantial capital investment 6,7 . Frontal polymerization is a promising alternative curing strategy, in which a self-propagating exothermic reaction wave transforms liquid monomers to fully cured polymers. We report here the frontal polymerization of a high-performance thermoset polymer that allows the rapid fabrication of parts with microscale features, three-dimensional printed structures and carbon-fibre-reinforced polymer composites. Precise control of the polymerization kinetics at both ambient and elevated temperatures allows stable monomer solutions to transform into fully cured polymers within seconds, reducing energy requirements and cure times by several orders of magnitude compared with conventional oven or autoclave curing approaches. The resulting polymer and composite parts possess similar mechanical properties to those cured conventionally. This curing strategy greatly improves the efficiency of manufacturing of high-performance polymers and composites, and is widely applicable to many industries.

  5. Instrumental physical analysis of microwaved glycerol citrate foams

    USDA-ARS?s Scientific Manuscript database

    Solid polyester glyceride polymers generated by microwave cooking were further cured in a conventional oven at 100 oC for 0, 6, 24, 48, or 72 hr and their physical properties were tested. Curing polyester glycerides resulted in decreased moisture content (MC), altered color, increased hydrated polym...

  6. Adjustable-Pressure Mandrel For Making Composite Tubes

    NASA Technical Reports Server (NTRS)

    Jacoy, Paul J.; Schmitigal, Wesley P.

    1993-01-01

    Inflatable inner mandrel enables application of any desired pressure (within reasonable limits) during curing stage in fabrication of fiber/matrix composite tube. Consists mainly of sheath of silicone rubber sealed on aluminum tube. Composite material laid up on mandrel and enclosed in rigid outer die. Sheath on inner mandrel inflated to requisite pressure and regulated during curing. Assembly then placed in oven and cured at specified temperature.

  7. Chemical curing in alkyd paints: An evaluation via FT-IR and NMR spectroscopies

    NASA Astrophysics Data System (ADS)

    Bartolozzi, G.; Marchiafava, V.; Mirabello, V.; Peruzzini, M.; Picollo, M.

    2014-01-01

    A study aimed at determining the time necessary for an alkyd paint to attain chemical curing is presented. In particular, the object of our investigation was an oil paint made by Winsor & Newton, namely French ultramarine (PB29) in the Griffin Alkyd “fast drying oil colour” series. Using this paint, we prepared several mock-ups on glass. These were left in the laboratory at room temperature in a piece of furniture with glass doors for a total of 70 days. Samples were taken at different times, and the changes in their composition were monitored by means of FT-IR and multinuclear NMR spectroscopic analyses. Since the cross-linking reactions involved in the formation of the pictorial film mainly affect the amount of carbon-carbon double bonds, we monitored the decrease in allyl, diallyl and vinyl protons and carbons. The data obtained from the use of both techniques led us to conclude that, in our particular experimental conditions, the chemical curing of the paint layer is reached within the first 70 days, thus establishing the beginning of the ageing phenomena.

  8. Method for applying photographic resists to otherwise incompatible substrates

    NASA Technical Reports Server (NTRS)

    Fuhr, W. (Inventor)

    1981-01-01

    A method for applying photographic resists to otherwise incompatible substrates, such as a baking enamel paint surface, is described wherein the uncured enamel paint surface is coated with a non-curing lacquer which is, in turn, coated with a partially cured lacquer. The non-curing lacquer adheres to the enamel and a photo resist material satisfactorily adheres to the partially cured lacquer. Once normal photo etching techniques are employed the lacquer coats can be easily removed from the enamel leaving the photo etched image. In the case of edge lighted instrument panels, a coat of uncured enamel is placed over the cured enamel followed by the lacquer coats and the photo resists which is exposed and developed. Once the etched uncured enamel is cured, the lacquer coats are removed leaving an etched panel.

  9. Microkinetic modeling of the autoxidative curing of an alkyd and oil-based paint model system

    NASA Astrophysics Data System (ADS)

    Oakley, Lindsay H.; Casadio, Francesca; Shull, Kenneth R.; Broadbelt, Linda J.

    2015-11-01

    Elucidating the curing and aging mechanisms of alkyd and other oil-based paints is valuable for the fields of conservation and bio-based coatings. Recent research has demonstrated the limitations of artificial aging in predicting the actual properties of paints that are hundreds of years old. Kinetic modeling offers pathways to develop a realistic and dynamic description of the composition of these oil-based paint coatings and facilitates the exploration of the effects of various environmental conditions on their long-term chemical stability. This work presents the construction of a kinetic Monte Carlo framework from elementary steps for the cobalt-catalyzed autoxidative curing of an ethyl linoleate model system up to the formation of single cross-links. Kinetic correlations for reaction families of similar chemistry are employed to reduce the number of parameters required to calculate rate constants in Arrhenius form. The model, developed from mechanisms proposed in the literature, shows good agreement with experiment for the formation of primary products in the early stages of curing. The model has also revealed that the mechanisms proposed in the literature for the formation of secondary products, such as volatile aldehydes, are still not well established, and alternative routes are under evaluation.

  10. The National Shipbuilding Research Program. Air Quality Best Management Practice (AQBMP) Resource Document for Shipyards

    DTIC Science & Technology

    1995-11-01

    Varnish Dipping Operations Checklist and Usage... Varnish Insulation...usually lower temperature units used to accelerate drying of varnish for motors, adhesives, paints, and plastics. Both drying ovens and furnaces can

  11. Piezoelectric paints as one approach to smart structural materials with health-monitoring capabilities

    NASA Astrophysics Data System (ADS)

    Egusa, Shigenori; Iwasawa, Naozumi

    1998-08-01

    Piezoelectric paints have a potential to change a conventional structural material into an intelligent material system with health-monitoring capabilities such as vibration sensing and damage detection. Such paints were prepared using lead zirconate titanate (PZT) ceramic powder as a pigment and epoxy resin as a binder. The obtained paints were coated on aluminum test specimens, and were cured at room temperature or at 150 0964-1726/7/4/002/img5, thus forming the paint films having different thicknesses of 25-300 0964-1726/7/4/002/img6. These films were then poled at room temperature, and were evaluated with regard to the sensitivities as vibration and acoustic emission sensors in the frequency ranges of 0-250 Hz and 0-1.0 MHz, respectively. This paper mainly describes the effects of the film thickness and the cure temperature on the poling behavior of the PZT/epoxy paint film. This paper describes also the application of the paint film as a vibration modal sensor integrated into a structural material.

  12. 40 CFR 63.4964 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... operation are applied within the capture system; coating solvent flash-off and coating, curing, and drying... parts enter the open shop environment when being moved between a spray booth and a curing oven. (b... from the beginning to the end of production, which includes surface preparation activities and drying...

  13. Isocyanate Exposure Below Analytical Detection When a Paint Brush and Roller Are Used to Apply Moisture-Cure Polyurethane Paint.

    PubMed

    Reeb-Whitaker, Carolyn K; Schoonover, Todd M

    2016-05-01

    Isocyanate exposure is known to be hazardous when polyurethane paints are applied with a spray gun, but less is known of exposure when paint is applied with a paint brush and roller. Concentrations of 1,6-hexamethylene diisocyanate (HDI) monomer and three HDI polymers were assessed when two moisture-cure polyurethane paints containing 31-35% isocyanates were applied with a paint roller and brush. Short-term 15-min samples were taken during paint application in an indoor test environment with no ventilation (n= 12); in an outdoor test environment (n= 11); and in an outdoor in-situ assessment (n= 22). The outdoor in-situ assessment involved the painting of a bus shelter and light poles at a public transit station over two night shifts. All isocyanate samples were below analytical detection. The analytical limits of detection for HDI monomer, HDI biuret, HDI isocyanurate, and HDI uretdione were 0.005, 0.84, 0.87, and 0.88 µg, respectively. The finding that isocyanate concentrations were below detection is attributed to the use of paint roller and brush which minimize paint aerosolization and the paint formulation itself which contained <1% of volatile HDI monomer. © The Author 2016. Published by Oxford University Press on behalf of the British Occupational Hygiene Society.

  14. Differential Curing In Fiber/Resin Laminates

    NASA Technical Reports Server (NTRS)

    Webster, Charles N.

    1989-01-01

    Modified layup schedule counteracts tendency toward delamination. Improved manufacturing process resembles conventional process, except prepregs partially cured laid on mold in sequence in degree of partial cure decreases from mold side to bag side. Degree of partial cure of each layer at time of layup selected by controlling storage and partial-curing temperatures of prepreg according to Arrhenius equation for rate of gel of resin as function of temperature and time from moment of mixing. Differential advancement of cure in layers made large enough to offset effect of advance bag-side heating in oven or autoclave. Technique helps prevent entrapment of volatile materials during manufacturing of fiber/resin laminates.

  15. Chemical curing in alkyd paints: an evaluation via FT-IR and NMR spectroscopies.

    PubMed

    Bartolozzi, G; Marchiafava, V; Mirabello, V; Peruzzini, M; Picollo, M

    2014-01-24

    A study aimed at determining the time necessary for an alkyd paint to attain chemical curing is presented. In particular, the object of our investigation was an oil paint made by Winsor & Newton, namely French ultramarine (PB29) in the Griffin Alkyd "fast drying oil colour" series. Using this paint, we prepared several mock-ups on glass. These were left in the laboratory at room temperature in a piece of furniture with glass doors for a total of 70 days. Samples were taken at different times, and the changes in their composition were monitored by means of FT-IR and multinuclear NMR spectroscopic analyses. Since the cross-linking reactions involved in the formation of the pictorial film mainly affect the amount of carbon-carbon double bonds, we monitored the decrease in allyl, diallyl and vinyl protons and carbons. The data obtained from the use of both techniques led us to conclude that, in our particular experimental conditions, the chemical curing of the paint layer is reached within the first 70 days, thus establishing the beginning of the ageing phenomena. Copyright © 2013 Elsevier B.V. All rights reserved.

  16. Solid freeform fabrication of biomaterials

    NASA Astrophysics Data System (ADS)

    Chu, Tien-Min Gabriel

    1999-12-01

    The biological performance of porous Hydroxyapatite (HA) is closely related to the pore architecture in the implants. The study on the effect of architecture to the biological performance of porous HA requires new manufacturing methods that can fabricate implants with controlled pores channels. In this thesis, four highly loaded HA and alumina suspensions were formulated and three different processes involving Solid Freeform Fabrication (SFF) were developed. An aqueous HA suspension in acrylamides was first formulated and the UV-curing properties were evaluated. With a medical grade HA powder, two non-aqueous HA suspensions were formulated: a 40 vol.% HA suspension in Hexanediol Diacrylate (HDDA) and a 40 vol.% HA suspension in 1:1 mix of Propoxylated Neopentyl Glycol Diacrylate (PNPGDA) and Isobomyl Acrylate (EBA). A 50 vol.% Alumina suspension in PNPGDA/IBA was also formulated. The effect of dispersant to the viscosity of the suspensions was characterized. In the Stereolithography (SL) method, the curing parameters of HA/HDDA and HA/PNPGDA/IBA were determined. Prototype HA implants with 1,700 mum internal channels were built directly on an SL Apparatus (SLA). The designed internal channel patterns were preserved after sintering. In the Ink-jet printing method, the high temperature flow behaviors of the suspensions were characterized. The effects of solids loading to the viscosity of the suspensions were modeled with Krieger-Dougherty equation. Leveling theory developed in paint industry was employed to analyze the self-leveling capability of the suspensions. In the indirect SL method, the thermal curing behavior of HA and alumina suspensions were characterized. The total cure time was measured and the curing kinetics was modeled. Negative molds for the implants were designed and built on SLA with epoxy resin. HA/PNPGDA/IBA was cast into the mold and cured in an oven. The binders and the epoxy mold were pyrolyzed and the green bodies sintered. Internal channels with sizes in the range of 420 to 968 gm with standard deviation less than 50 mum were successfully built. The formulation and characterization techniques developed in this thesis were useful for evaluating the suspensions for SFF process. The manufacturing process developed in this thesis have provided new methods for controlling the channel size in porous HA implants.

  17. Air formaldehyde and solvent concentrations during surface coating with acid-curing lacquers and paints in the woodworking and furniture industry.

    PubMed

    Thorud, Syvert; Gjolstad, Merete; Ellingsen, Dag G; Molander, Paal

    2005-06-01

    An investigation of contemporary exposure to formaldehyde and organic solvents has been carried out during surface coating with acid-curing lacquers and paints in the Norwegian woodworking and furniture industry over a period of 3 years. The investigation covered 27 factories of different sizes and with different types of production, and totally 557 parallel formaldehyde and solvent samples were collected. The formaldehyde concentration (geometric mean) was 0.15 ppm (range 0.01-1.48 ppm) with about 10% of the samples exceeding the Norwegian occupational exposure limit of 0.5 ppm. The solvent concentration as additive effect (geometric mean) was 0.13 (range 0.0004-5.08) and about 5% of the samples exceeded the Norwegian occupational exposure limit. The most frequently occurring solvents from acid-curing lacquers were n-butyl acetate, ethanol, ethyl acetate and 1-butanol, which were found in 88-98% of the samples. Toluene, n-butyl acetate and 1-butanol were the only solvents with maximum concentrations exceeding their respective occupational exposure limits. Curtain painting machine operators were exposed to the highest concentrations of both formaldehyde (geometric mean 0.51 ppm, range 0.08-1.48 ppm) and organic solvents (additive effect, geometric mean 1.18, range 0.02-5.08). Other painting application work tasks such as automatic and manual spray-painting, manual painting and dip painting, showed on average considerably lower concentrations of both formaldehyde (geometric means 0.07-0.16 ppm) and organic solvents (additive effect, geometric mean 0.02-0.18). Non-painting work tasks also displayed moderate concentrations of formaldehyde (geometric means 0.11-0.17 ppm) and organic solvents (additive effect, geometric mean 0.04-0.07).

  18. Strength Performance of Blended Ash Based Geopolymer Mortar

    NASA Astrophysics Data System (ADS)

    Zahib, Zaidahtulakmal M.; Kamaruddin, Kartini; Saman, Hamidah M.

    2018-03-01

    Geopolymer is a based on inorganic alumino-silicate binder system. Geopolymeric materials are formed using materials that containing silica and aluminium such as fly ash and rice husk ash, which activated by alkaline solution. This paper presents the study on the effect of replacement of SSA in RHA based geopolymer, types of curing and different molarity of NaOH used on the strength of Sewage Sludge Ash (SSA) and Rice Husk Ash (RHA) based geopolymer mortar incorporating with three (3) different mix proportions. Based geopolymer mortar was synthesized from treated sewage sludge and rice husk undergoing incineration process in producing ashes, activated with sodium silicate and sodium hydroxide solution by ratio of 2.5:1 and solution to ash ratio of 1:1. Molarity of 8M and 10M NaOH were used. The percentages of SSA replacement were 0%, 10% and 20% by weight. Compressive strength was conducted at age 7, 14 and 28 days to see the development of strength with two curing regimes, which are air curing and oven curing (60°C for 24 hours). From the research conducted, the ultimate compressive strength (6.28MPa) was obtained at zero replacement of SSA taken at 28 days of oven curing with 10M of NaOH. This shows that RHA, which is rich in silica content is enough to enhance the strength of geopolymer mortar especially with high molarity of NaOH.

  19. 40 CFR 60.493 - Performance test and compliance provisions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Beverage Can Surface Coating Industry § 60.493 Performance test and compliance provisions. (a) Section 60.8... operation Emission distribution Coater/flashoff (Se) Curing oven (Sh) Two-piece aluminum or steel can...

  20. KSC-2012-1575

    NASA Image and Video Library

    2012-03-01

    CAPE CANAVERAL, Fla. -- The heat shield tiles that will be installed to the backshell of the Orion Multi-Purpose Crew Vehicle's Exploration Flight Test EFT-1 capsule are in a Keith thermal automation oven in the Thermal Protection System Facility at NASA's Kennedy Space Center in Florida. Inside the oven, the tiles will be baked at 2,200 degrees F to cure their ceramic coating. EFT-1 will be used during Orion's first test flight in space. For more information, visit www.nasa.gov/orion. Photo credit: Frankie Martin

  1. KSC-2012-1576

    NASA Image and Video Library

    2012-03-01

    CAPE CANAVERAL, Fla. -- The heat shield tiles that will be installed to the backshell of the Orion Multi-Purpose Crew Vehicle's Exploration Flight Test EFT-1 capsule are in a Keith thermal automation oven in the Thermal Protection System Facility at NASA's Kennedy Space Center in Florida. Inside the oven, the tiles will be baked at 2,200 degrees F to cure their ceramic coating. EFT-1 will be used during Orion's first test flight in space. For more information, visit www.nasa.gov/orion. Photo credit: Frankie Martin

  2. Properties of cold-bonded lightweight artificial aggregate containing bottom ash with different curing regime

    NASA Astrophysics Data System (ADS)

    Mohamad Ibrahim, Norlia; Nizar Ismail, Khairul; Che Amat, Roshazita; Mohamad Ghazali, Mohamad Iqbal

    2018-03-01

    Cold-bonded pelletizing technique is frequently used in aggregate manufacturing process as it can minimise the energy consumption. It has contributed to both economical and environmental advantages because it helps to reduce the gas emissions problems. Bottom ash collected from municipal solid waste incineration (MSWI) plant was selected as raw material in this study and was utilised as a partial replacement for cement for artificial aggregate production. Several percentage of ash replacement was selected ranged from 10 to 50%. Aggregate pellets were subjected to different types of curing condition which is room-water (RW), room-room (RR), oven-room (OR) and oven-water (OW) condition. Properties of aggregate pellets were examined to obtain its density, water absorption, aggregate impact value (AIV) and specific gravity (SG). The results indicated that the most efficient curing regime is by exposing the aggregate in RW condition. The optimum aggregate was selected at 20% where it has satisfied the required density of 739.5kg/m3, and classified as strong aggregate with AIV 14. However, the water absorption of aggregate increased proportionately with the increment of ash content.

  3. ENVIRONMENTAL AND ENERGY BENEFITS OF MICROPROCESSOR CONTROL OF OVEN AIRFLOWS FROM METAL PAINTING OPERATIONS

    EPA Science Inventory

    In most industrial operations the percentage of the lower explosive limit (LEL) of VOC emissions typically remain at below 5 to 10 percent LEL at most metal coating operations. Although, monitors are available to determine solvent concentrations, they require manual corrective ac...

  4. Personnel Exposure to Airborne Isocyanates and Solvents During Shipboard Painting With 2-Pack Polyurethane Paints

    DTIC Science & Technology

    2008-12-01

    contain low volatility isocyanate prepolymers in addition to small quantities of volatile isocyanate monomers [2,3]. The monomers may become airborne as...vapour whilst the non-volatile prepolymers and partially cured oligomers may form aerosols during spray painting and sanding of the painted surface...JL (1992) “ Prepolymers of hexamethylene diisocyanate as a cause of occupational asthma” J. Allergy Clinical Immunol. 91 850-61. 5. Redlich CA, Bello

  5. Mechanical properties of geopolymer lightweight brick with styrofoam pellet

    NASA Astrophysics Data System (ADS)

    Abdullah, Mohd Mustafa Al Bakri; Tahir, Muhammad Faheem Mohd; Kadir, Aeslina Abdul; Hussin, Kamarudin; Samson, W. Saiful Iskandar W.

    2017-09-01

    The utilization of fly ash in brick as partial replacement of cement is gaining immense importance today, mainly on account of the improvement in the long-term durability of brick combined with ecological benefits. In this research, the lightweight brick was produced by using fly ash (class F) as a main material to replace Ordinary Portland Cement (OPC) in the composition of brick. Class F Fly Ash was mixed with an alkaline activator solution (a mixture of sodium silicate and NaOH), and styrofoam pellet was added to the geopolymer mixture to produce lightweight brick. The brick was prepared in two methods that is wet method and dry method due to different brick composition which is dry method for composition with sand and wet method for composition without sand. The bricks were cured in room temperature at 7 aging days. After 7 days, the compressive strength, water absorption, and density of the brick were investigated, where the optimum ratio for the best bricks has been determined from the lightweight density and has compressive strength more than minimum standard requirement. The best bricks are further produce for curing at 60°C in oven at 28 aging days. Those bricks also were characterized using optical microscope to measure the distribution of styrofoam in brick structure. From the result obtained, the brick that cured at 60°C in oven at 28 aging days has high strength compare to brick that cured in room temperature and at 7 day cured. The water absorption is decreasing as the curing temperature and aging days increased whereas density is increasing.

  6. Out of the Autoclave Fabrication of LaRC[TradeMark] PETI-9 Polyimide Laminates

    NASA Technical Reports Server (NTRS)

    Cano, Robert J.; Jensen, Brian J.

    2013-01-01

    The NASA Langley Research Center developed polyimide system, LaRC PETI-9, has successfully been processed into composites by high temperature vacuum assisted resin transfer molding (HT-VARTM). To extend the application of this high use temperature material to other out-of-autoclave (OOA) processing techniques, the fabrication of PETI- 9 laminates was evaluated using only a vacuum bag and oven cure. A LaRC PETI-9 polyimide solution in NMP was prepared and successfully utilized to fabricate unidirectional IM7 carbon fiber prepreg that was subsequently processed into composites with a vacuum bag and oven cure OOA process. Composite panels of good quality were successfully fabricated and mechanically tested. Processing characteristics, composite panel quality and mechanical properties are presented in this work. The resultant properties are compared to previously developed LaRC material systems processed by both autoclave and OOA techniques including the well characterized, autoclave processed LaRC PETI-5.

  7. Applications of Blue Light-curing Acrylic Resin to Forensic Sample Preparation and Microtomy.

    PubMed

    Groves, Ethan; Palenik, Christopher S

    2016-03-01

    This study discusses the results of an evaluation of a one-part blue light-curing acrylic resin for embedding trace evidence prior to the preparation of thin sections with a microtome. Through a comparison to several epoxy resins, the physical properties relevant to both trace evidence examination and analytical microscopy in general, including as viscosity, clarity, color, hardness, and cure speed, were explored. Finally, thin sections from paint samples embedded in this acrylic resin were evaluated to determine if, through smearing or impregnation, the resin contributed to the infrared spectra. The results of this study show that blue light-curing acrylic resins provide the desired properties of an embedding medium, generate high-quality thin sections, and can significantly simplify the preparation of paint chips, fibers and a multitude of other types of microscopic samples in the forensic trace evidence laboratory. © 2015 American Academy of Forensic Sciences.

  8. Center for Micro Air Vehicle Studies

    DTIC Science & Technology

    2013-02-01

    vacuum oven , unavailable at WSU. The vacuum oven was a crucial step in allowing the epoxy to cure properly, thereby providing the carbon fiber spars...weight of the Modified Standard model is 12g (without a battery). This model uses a 150mAh LiPo battery. The average “Big Bird ” model, weights...23.1g (without a battery), has a wingspan of 340mm and a length of 270mm average (Figure 26). The vehicle uses a 150mAh battery. The “Big Bird ” is a

  9. 40 CFR 63.1196 - What definitions should I be aware of?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... form mineral wool. Curing oven means a chamber in which heat is used to thermoset a binder on the... slag. It may be used as a thermal or acoustical insulation material or in the making of other products...

  10. 40 CFR 63.1196 - What definitions should I be aware of?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... form mineral wool. Curing oven means a chamber in which heat is used to thermoset a binder on the... slag. It may be used as a thermal or acoustical insulation material or in the making of other products...

  11. 40 CFR 63.1196 - What definitions should I be aware of?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... form mineral wool. Curing oven means a chamber in which heat is used to thermoset a binder on the... slag. It may be used as a thermal or acoustical insulation material or in the making of other products...

  12. Curing of Thick Thermoset Composite Laminates: Multiphysics Modeling and Experiments

    NASA Astrophysics Data System (ADS)

    Anandan, S.; Dhaliwal, G. S.; Huo, Z.; Chandrashekhara, K.; Apetre, N.; Iyyer, N.

    2017-11-01

    Fiber reinforced polymer composites are used in high-performance aerospace applications as they are resistant to fatigue, corrosion free and possess high specific strength. The mechanical properties of these composite components depend on the degree of cure and residual stresses developed during the curing process. While these parameters are difficult to determine experimentally in large and complex parts, they can be simulated using numerical models in a cost-effective manner. These simulations can be used to develop cure cycles and change processing parameters to obtain high-quality parts. In the current work, a numerical model was built in Comsol MultiPhysics to simulate the cure behavior of a carbon/epoxy prepreg system (IM7/Cycom 5320-1). A thermal spike was observed in thick laminates when the recommended cure cycle was used. The cure cycle was modified to reduce the thermal spike and maintain the degree of cure at the laminate center. A parametric study was performed to evaluate the effect of air flow in the oven, post cure cycles and cure temperatures on the thermal spike and the resultant degree of cure in the laminate.

  13. 78 FR 26300 - Approval and Promulgation of Air Quality Implementation Plans; Texas; Revisions to Control of Air...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-05-06

    ... curing ovens used in wet-laid non-woven fiber mat manufacturing operations when nitrogen containing resins or other additives are used. These two actions affect NO X sources operating in the Dallas Fort...

  14. 7 CFR 30.42 - Class 7; miscellaneous domestic types.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... nicotine content of not more than eight-tenths of one per cent (8/10 of 1%), oven dry weight, shall be..., flue-cured tobacco, but having a nicotine content of not more than eight-tenths of one percent (8/10 of...

  15. 7 CFR 30.42 - Class 7; miscellaneous domestic types.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... nicotine content of not more than eight-tenths of one per cent (8/10 of 1%), oven dry weight, shall be..., flue-cured tobacco, but having a nicotine content of not more than eight-tenths of one percent (8/10 of...

  16. 7 CFR 30.42 - Class 7; miscellaneous domestic types.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... nicotine content of not more than eight-tenths of one per cent (8/10 of 1%), oven dry weight, shall be..., flue-cured tobacco, but having a nicotine content of not more than eight-tenths of one percent (8/10 of...

  17. 7 CFR 30.42 - Class 7; miscellaneous domestic types.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... nicotine content of not more than eight-tenths of one per cent (8/10 of 1%), oven dry weight, shall be..., flue-cured tobacco, but having a nicotine content of not more than eight-tenths of one percent (8/10 of...

  18. Fast-Curing Epoxy and Acrylate Adhesive Development for Adverse Marine Conditions

    DTIC Science & Technology

    2013-07-01

    the bulk properties of the adhesive. Water contact can reduce the glass transition temperature, induce cracks , or initiate hydrolysis in which the...were the same as above except they were painted with gloss black enamel paint and allowed to dry 24 h prior to application of any adhesives

  19. A Meta-Analysis Of Corrosion Studies for Maritime Patrol and Reconnaissance Aircraft (MPRA)

    DTIC Science & Technology

    2016-09-01

    performed onsite. Aircraft rating was based upon the presence and/or extent of paint adhesion, paint cracking , clean ability, fluid damage, oxidation...because of corrosion control maintenance. No significant issues were observed related to paint cracking , fluid damage, corrosion, and clean ability of...HEXAMETHYLENEDIISOCYANATE 822-06-0 83194 X-310A; POLYURETHANE CATALYST XYLENE 1330-20-7 82649 X-530; HS EPOXY ENAMEL CURING SOLUTION BUTANOL 71-36-3

  20. 40 CFR 60.461 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... coil. Coating application station means that portion of the metal coil surface coating operation where.... Finish coat operation means the coating application station, curing oven, and quench station used to... operation means the application system used to apply an organic coating to the surface of any continuous...

  1. Chemical Products in the Home, Workshop and Garden. Proceed with Caution; Consumer Safety in the Home, II.

    ERIC Educational Resources Information Center

    Saskatchewan Consumer and Commercial Affairs, Regina.

    The average home has chemical products to clean floors, kill insects, clean ovens, thin paint, remove grease, and perform countless other chores. Many consumers remain unaware of the dangers these products bring into the home. This booklet provides information on the safe use, storage, and disposal of these products. The compounds found in…

  2. No-Oven, No-Autoclave Composite Processing

    NASA Technical Reports Server (NTRS)

    Rauscher, Michael D.

    2015-01-01

    Very large composite structures, such as those used in NASA's Space Launch System, push the boundaries imposed by current autoclaves. New technology is needed to maintain composite performance and free manufacturing engineers from the restraints of curing equipment size limitations. Recent efforts on a Phase II project by Cornerstone Research Group, Inc. (CRG), have advanced the technology and manufacturing readiness levels of a unique two-part epoxy resin system. Designed for room-temperature infusion of a dry carbon preform, the system includes a no-heat-added cure that delivers 350 F composite performance in a matter of hours. This no-oven, no-autoclave (NONA) composite processing eliminates part-size constraints imposed by infrastructure and lowers costs by increasing throughput and reducing capital-specific, process-flow bottlenecks. As a result of the Phase II activity, NONA materials and processes were used to make high-temperature composite tooling suitable for further production of carbon-epoxy laminates and honeycomb/ sandwich-structure composites with an aluminum core. The technology platform involves tooling design, resin infusion processing, composite part design, and resin chemistry. The various technology elements are combined to achieve a fully cured part. The individual elements are not unusual, but they are combined in such a way that enables proper management of the heat generated by the epoxy resin during cure. The result is a self-cured carbon/ epoxy composite part that is mechanically and chemically stable at temperatures up to 350 F. As a result of the successful SBIR effort, CRG has launched NONA Composites as a spinoff subsidiary. The company sells resin to end users, fabricates finished goods for customers, and sells composite tooling made with NONA materials and processes to composite manufacturers.

  3. Influence of Curing on the Strength Development of Calcium-Containing Geopolymer Mortar

    PubMed Central

    Li, Xueying; Wang, Zheng; Jiao, Zhenzhen

    2013-01-01

    This paper investigated the curing effects on the mechanical properties of calcium-containing geopolymer mortar. Three precursors are used: Class C fly ash, Class F fly ash plus calcium hydroxide and Class F fly ash plus slag. Curing conditions included: (1) standard curing at 20 ± 3 °C and RH 95% (C); (2) steam curing at 60 °C for 24 h (S); (3) steam curing at 60 °C for 6 h (S6); and (4) oven curing at 60 °C for 24 h (O), then the latter three followed by the standard curing. Under the standard conditions, the flexural strength and compressive strength of Class C fly ash geopolymer mortars developed quickly until the age of 7 days, followed by a gradual increase. Specimens with Class F fly ash plus Ca(OH)2 showed slow increase till the age of 28 days. Under these non-standard conditions (2–4), all specimens showed higher 3-day strength, while later strengths were either higher or lower than those in standard conditions, depending on the type of the precursor. PMID:28788377

  4. Influence of Curing on the Strength Development of Calcium-Containing Geopolymer Mortar.

    PubMed

    Li, Xueying; Wang, Zheng; Jiao, Zhenzhen

    2013-11-07

    This paper investigated the curing effects on the mechanical properties of calcium-containing geopolymer mortar. Three precursors are used: Class C fly ash, Class F fly ash plus calcium hydroxide and Class F fly ash plus slag. Curing conditions included: (1) standard curing at 20 ± 3 °C and RH 95% (C); (2) steam curing at 60 °C for 24 h (S); (3) steam curing at 60 °C for 6 h (S6); and (4) oven curing at 60 °C for 24 h (O), then the latter three followed by the standard curing. Under the standard conditions, the flexural strength and compressive strength of Class C fly ash geopolymer mortars developed quickly until the age of 7 days, followed by a gradual increase. Specimens with Class F fly ash plus Ca(OH)₂ showed slow increase till the age of 28 days. Under these non-standard conditions (2-4), all specimens showed higher 3-day strength, while later strengths were either higher or lower than those in standard conditions, depending on the type of the precursor.

  5. Warpage of QFN Package in Post Mold Cure Process of integrated circuit packaging

    NASA Astrophysics Data System (ADS)

    Sriwithoon, Nattha; Ugsornrat, Kessararat; Srisuwitthanon, Warayoot; Thonglor, Panakamon

    2017-09-01

    This research studied about warpage of QFN package in post mold cure process of integrated circuit (IC) packages using pre-plated (PPF) leadframe. For IC package, epoxy molding compound (EMC) are molded by cross linking of compound stiffness but incomplete crosslinked network and leading the fully cured thermoset by post mold cure (PMC) process. The cure temperature of PMC can change microstructure of EMC in term of stress inside the package and effect to warpage of the package due to coefficient of thermal expansion (CTE) between EMC and leadframe. In experiment, cure temperatures were varied to check the effect of internal stress due to different cure temperature after completed post mold cure for TDFN 2×3 8L. The cure temperature were varied with 180 °C, 170 °C, 160 °C, and 150°C with cure time 4 and 6 hours, respectively. For analysis, the TDFN 2×3 8L packages were analyzed the warpage by thickness gauge and scanning acoustic microscope (SAM) after take the test samples out from the oven cure. The results confirmed that effect of different CTE between EMC and leadframe due to different cure temperature resulting to warpage of the TDFN 2×3 8L packages.

  6. Antenna sunshield membrane

    NASA Technical Reports Server (NTRS)

    Bogorad, Alexander (Inventor); Bowman, Jr., Charles K. (Inventor); Meder, Martin G. (Inventor); Dottore, Frank A. (Inventor)

    1994-01-01

    An RF-transparent sunshield membrane covers an antenna reflector such as a parabolic dish. The blanket includes a single dielectric sheet of polyimide film 1/2-mil thick. The surface of the film facing away from the reflector is coated with a transparent electrically conductive coating such as vapor-deposited indium-tin oxide. The surface of the film facing the reflector is reinforced by an adhesively attached polyester or glass mesh, which in turn is coated with a white paint. In a particular embodiment of the invention, polyurethane paint is used. In another embodiment of the invention, a layer of paint primer is applied to the mesh under a silicone paint, and the silicone paint is cured after application for several days at room temperature to enhance adhesion to the primer.

  7. 40 CFR 63.1183 - How do I comply with the formaldehyde standards for existing, new, and reconstructed curing ovens?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... specification range, record the free-formaldehyde content specification range of the resin used, and the... that requires a binder formulation made with the resin containing the highest free-formaldehyde content specification range. Show compliance with the formaldehyde emission limits while the device for measuring...

  8. 40 CFR 63.1183 - How do I comply with the formaldehyde standards for existing, new, and reconstructed curing ovens?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... specification range, record the free-formaldehyde content specification range of the resin used, and the... that requires a binder formulation made with the resin containing the highest free-formaldehyde content specification range. Show compliance with the formaldehyde emission limits while the device for measuring...

  9. 40 CFR 63.1183 - How do I comply with the formaldehyde standards for existing, new, and reconstructed curing ovens?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... specification range, record the free-formaldehyde content specification range of the resin used, and the... that requires a binder formulation made with the resin containing the highest free-formaldehyde content specification range. Show compliance with the formaldehyde emission limits while the device for measuring...

  10. 40 CFR 63.1183 - How do I comply with the formaldehyde standards for existing, new, and reconstructed curing ovens?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... specification range, record the free-formaldehyde content specification range of the resin used, and the... that requires a binder formulation made with the resin containing the highest free-formaldehyde content specification range. Show compliance with the formaldehyde emission limits while the device for measuring...

  11. 40 CFR 63.1183 - How do I comply with the formaldehyde standards for existing, new, and reconstructed curing ovens?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... specification range, record the free-formaldehyde content specification range of the resin used, and the... that requires a binder formulation made with the resin containing the highest free-formaldehyde content specification range. Show compliance with the formaldehyde emission limits while the device for measuring...

  12. Lightweight Forms for Epoxy/Aramid Ducts

    NASA Technical Reports Server (NTRS)

    Mix, E. W.; Anderson, A. N.; Bedford, Donald L., Sr.

    1986-01-01

    Aluminum mandrels easy to remove. Lightweight aluminum mandrel for shaping epoxy/aramid ducts simplifies and speeds production. In new process, glass-reinforced epoxy/aramid cloth wrapped on aluminum mandrel. Stainless-steel flanges and other hardware fitted on duct and held by simple tooling. Entire assembly placed in oven to cure epoxy. After curing, assembly placed in alkaline bath dissolves aluminum mandrel in about 4 hours. Epoxy/aramid shell ready for use as duct. Aluminum mandrel used to make ducts of various inside diameters up to 6 in. Standard aluminum forms used. Conventional tube-bending equipment produces requisite curves in mandrels.

  13. Fiber-Reinforced Epoxy Composites and Methods of Making Same Without the Use of Oven or Autoclave

    NASA Technical Reports Server (NTRS)

    Barnell, Thomas J. (Inventor); Rauscher, Michael D. (Inventor); Stienecker, Rick D. (Inventor); Nickerson, David M. (Inventor); Tong, Tat H. (Inventor)

    2016-01-01

    Method embodiments for producing a fiber-reinforced epoxy composite comprise providing a mold defining a shape for a composite, applying a fiber reinforcement over the mold, covering the mold and fiber reinforcement thereon in a vacuum enclosure, performing a vacuum on the vacuum enclosure to produce a pressure gradient, insulating at least a portion of the vacuum enclosure with thermal insulation, infusing the fiber reinforcement with a reactive mixture of uncured epoxy resin and curing agent under vacuum conditions, wherein the reactive mixture of uncured epoxy resin and curing agent generates exothermic heat, and producing the fiber-reinforced epoxy composite having a glass transition temperature of at least about 100.degree. C. by curing the fiber reinforcement infused with the reactive mixture of uncured epoxy resin and curing agent by utilizing the exothermically generated heat, wherein the curing is conducted inside the thermally insulated vacuum enclosure without utilization of an external heat source or an external radiation source.

  14. Outgassing of Out-of-Autoclave Composite Primary Structures for Small Satellites

    NASA Astrophysics Data System (ADS)

    Komus, Alastair

    Out-of-autoclave vacuum-bagged-only (VBO) processing is capable of producing lower cost composite primary structures for small satellites than autoclave processing. However, the outgassing performance of VBO structures in a vacuum environment has not been examined. Panels were manufactured from CYCOM 5320-1 and TC275-1 carbon fiber/epoxy prepreg using VBO processing. The humidity level, pre-cure dwell time, and cure cycle parameters were varied during manufacturing. The degree of cure and glass transition temperature were shown to increase with increasing oven temperature. Processing humidity levels and the length of pre-cure dwell times had no discernable effect on the total mass loss (TML) and collected volatile condensable material (CVCM) that were outgassed under vacuum. Instead the TML was controlled by moisture saturation after manufacturing. Fourier transform infrared spectroscopy showed that epoxy oligomers were the primary CVCM. The study showed the VBO laminates had outgassing values that were comparable to the autoclave-cured laminates.

  15. Curing Effects on Interfacial Adhesion between Recycled Carbon Fiber and Epoxy Resin Heated by Microwave Irradiation

    PubMed Central

    Shimamoto, Daisuke; Hotta, Yuji

    2018-01-01

    The interfacial adhesion of recycled carbon fiber (CF) reinforced epoxy composite heated by microwave (MW) irradiation were investigated by changing the curing state of the epoxy resin. The recycled CF was recovered from the composite, which was prepared by vacuum-assisted resin transfer molding, by thermal degradation at 500 or 600 °C. Thermogravimetric analysis showed that the heating at 600 °C caused rough damage to the CF surface, whereas recycled CF recovered at 500 °C have few defects. The interfacial shear strength (IFSS) between recycled CF and epoxy resin was measured by a single-fiber fragmentation test. The test specimen was heated by MW after mixing the epoxy resin with a curing agent or pre-curing, in order to investigate the curing effects on the matrix resin. The IFSSs of the MW-irradiated samples were significantly varied by the curing state of the epoxy resin and the surface condition of recycled CF, resulting that they were 99.5 to 131.7% of oven heated samples Furthermore, rheological measurements showed that the viscosity and shrinking behaviors of epoxy resin were affected based on the curing state of epoxy resin before MW irradiation. PMID:29587422

  16. Curing Effects on Interfacial Adhesion between Recycled Carbon Fiber and Epoxy Resin Heated by Microwave Irradiation.

    PubMed

    Tominaga, Yuichi; Shimamoto, Daisuke; Hotta, Yuji

    2018-03-26

    The interfacial adhesion of recycled carbon fiber (CF) reinforced epoxy composite heated by microwave (MW) irradiation were investigated by changing the curing state of the epoxy resin. The recycled CF was recovered from the composite, which was prepared by vacuum-assisted resin transfer molding, by thermal degradation at 500 or 600 °C. Thermogravimetric analysis showed that the heating at 600 °C caused rough damage to the CF surface, whereas recycled CF recovered at 500 °C have few defects. The interfacial shear strength (IFSS) between recycled CF and epoxy resin was measured by a single-fiber fragmentation test. The test specimen was heated by MW after mixing the epoxy resin with a curing agent or pre-curing, in order to investigate the curing effects on the matrix resin. The IFSSs of the MW-irradiated samples were significantly varied by the curing state of the epoxy resin and the surface condition of recycled CF, resulting that they were 99.5 to 131.7% of oven heated samples Furthermore, rheological measurements showed that the viscosity and shrinking behaviors of epoxy resin were affected based on the curing state of epoxy resin before MW irradiation.

  17. Model study of modern oil-based paint media by triacylglycerol profiling in positive and negative ionization modes.

    PubMed

    Degano, Ilaria; La Nasa, Jacopo; Ghelardi, Elisa; Modugno, Francesca; Colombini, Maria Perla

    2016-12-01

    Lipid binders have traditionally been determined in paintings by using gas chromatography/mass spectrometry (GC/MS) to identify the characteristic profiles and ratios of fatty acids . However, the presence of mixtures in contemporary and modern oil paints makes the GC/MS determination of fatty acids insufficient to fully characterize the lipid binding media. In this study we prove that triacylglycerol (TAG) profiling by high-performance liquid chromatography with high-resolution tandem mass spectrometry, using ESI in positive and negative ionization modes is highly effective. We exploited this analytical approach to study the curing and degradation processes undergone by six plant oils used in the formulation of media in modern paints, using both natural and artificial ageing experiments. We believe that is the first time that a negative ionization mode has been applied for this purpose and that a survey with HPLC-ESI-Q-ToF has been carried out to study the ageing kinetics of plant oils. TAG profiling enabled us to study the evolution over time of the constituents of modern oils, with respect to curing and ageing. The data analyzed in this study demonstrate that our approach is efficient to study the oxidation of TAGs during ageing. The data also improve current knowledge on the properties of vegetable oils, which could lead to the development of new paint materials and conservation treatments for modern and contemporary works of art. Copyright © 2016 Elsevier B.V. All rights reserved.

  18. Neural Network Burst Pressure Prediction in Composite Overwrapped Pressure Vessels

    NASA Technical Reports Server (NTRS)

    Hill, Eric v. K.; Dion, Seth-Andrew T.; Karl, Justin O.; Spivey, Nicholas S.; Walker, James L., II

    2007-01-01

    Acoustic emission data were collected during the hydroburst testing of eleven 15 inch diameter filament wound composite overwrapped pressure vessels. A neural network burst pressure prediction was generated from the resulting AE amplitude data. The bottles shared commonality of graphite fiber, epoxy resin, and cure time. Individual bottles varied by cure mode (rotisserie versus static oven curing), types of inflicted damage, temperature of the pressurant, and pressurization scheme. Three categorical variables were selected to represent undamaged bottles, impact damaged bottles, and bottles with lacerated hoop fibers. This categorization along with the removal of the AE data from the disbonding noise between the aluminum liner and the composite overwrap allowed the prediction of burst pressures in all three sets of bottles using a single backpropagation neural network. Here the worst case error was 3.38 percent.

  19. DOE Office of Scientific and Technical Information (OSTI.GOV)

    Hoffman, D.M.; Jessop, E.S.; Swansiger, R.W.

    Cast cure, extrusion cast, and paste extrudable explosives have not been designed for transferring through long tortuous paths or into fine three dimensional shapes. To allow the crystalline explosive to flow a lubricating fluid is required. The energetic liquid ethane trinitrate (TMETN) was used as the lubricant to maximize the explosive energy. TMETN is a liquid nitrate ester which requires stabilization with conventional free radical stabilizers such as 2- nitrodiphenylamine, methyl-nitroanaline, or ethyl centrylite. Since these injection moldable explosives are expected to cure in place, a polyesterurethane binder based on polymeric isocyanate of hexamethylene diisocyanate and polycaprolactone polyols is dissolvedmore » in TMETN. The solubility of the polymer precursors in TMETN also reduces the energetic liquids sensitivity. The latent cure catalyst Dabco T-131 was used to minimize shrinkage associated with thermal expansion, reduce cost associated with oven cures, to give 4-6 hour potlife and overnight cure to handling strength. The product RX-08-HD is a new, low-viscosity, injection moldable explosive that can be extruded into complex, void-free shapes. Combined with appropriate design and other aspects of weaponization, RX-08-HD has produced outstanding results.« less

  20. Development of environmentally friendly coatings and paints using medium-chain-length poly(3-hydroxyalkanoates) as the polymer binder.

    PubMed

    van der Walle, G A; Buisman, G J; Weusthuis, R A; Eggink, G

    1999-01-01

    Unsaturated medium-chain-length poly(3-hydroxyalkanoates) (mcl-PHAs) produced by Pseudomonas putida from linseed oil fatty acids (LOFA) and tall oil fatty acids (TOFA), were used as the polymer binder in the formulation of high solid alkyd-like paints. The relatively high concentration of unsaturated alkyl side chains incorporated into the PHA resins resulted in oxidative drying PHA paints having excellent coating properties. The homogeneously pigmented PHA coatings yielded high-gloss, smooth and strong films upon curing and showed an excellent flexibility, a good adhesion to different substrates, cohesive film properties and resistance to chipping.

  1. Comparative static curing versus dynamic curing on tablet coating structures.

    PubMed

    Gendre, Claire; Genty, Muriel; Fayard, Barbara; Tfayli, Ali; Boiret, Mathieu; Lecoq, Olivier; Baron, Michel; Chaminade, Pierre; Péan, Jean Manuel

    2013-09-10

    Curing is generally required to stabilize film coating from aqueous polymer dispersion. This post-coating drying step is traditionally carried out in static conditions, requiring the transfer of solid dosage forms to an oven. But, curing operation performed directly inside the coating equipment stands for an attractive industrial application. Recently, the use of various advanced physico-chemical characterization techniques i.e., X-ray micro-computed tomography, vibrational spectroscopies (near infrared and Raman) and X-ray microdiffraction, allowed new insights into the film-coating structures of dynamically cured tablets. Dynamic curing end-point was efficiently determined after 4h. The aim of the present work was to elucidate the influence of curing conditions on film-coating structures. Results demonstrated that 24h of static curing and 4h of dynamic curing, both performed at 60°C and ambient relative humidity, led to similar coating layers in terms of drug release properties, porosity, water content, structural rearrangement of polymer chains and crystalline distribution. Furthermore, X-ray microdiffraction measurements pointed out different crystalline coating compositions depending on sample storage time. An aging mechanism might have occur during storage, resulting in the crystallization and the upward migration of cetyl alcohol, coupled to the downward migration of crystalline sodium lauryl sulfate within the coating layer. Interestingly, this new study clearly provided further knowledge into film-coating structures after a curing step and confirmed that curing operation could be performed in dynamic conditions. Copyright © 2013 Elsevier B.V. All rights reserved.

  2. Effects of coal-mine discharges on the quality of the Stonycreek River and its tributaries, Somerset and Cambria counties, Pennsylvania

    USGS Publications Warehouse

    Williams, Donald R.; Sams, James I.; Mulkerrin, Mary E.

    1996-01-01

    This report describes the results of a study by the U.S. Geological Survey, done in cooperation with the Somerset Conservation District, to locate and sample abandoned coal-mine discharges in the Stonycreek River Basin, to prioritize the mine discharges for remediation, and to determine the effects of the mine discharges on water quality of the Stonycreek River and its major tributaries. From October 1991 through November 1994, 270 abandoned coal-mine discharges were located and sampled. Discharges from 193 mines exceeded U.S. Environmental Protection Agency effluent standards for pH, discharges from 122 mines exceeded effluent standards for total-iron concentration, and discharges from 141 mines exceeded effluent standards for total-manganese concentration. Discharges from 94 mines exceeded effluent standards for all three constituents. Only 40 mine discharges met effluent standards for pH and concentrations of total iron and total manganese.A prioritization index (PI) was developed to rank the mine discharges with respect to their loading capacity on the receiving stream. The PI lists the most severe mine discharges in a descending order for the Stonycreek River Basin and for subbasins that include the Shade Creek, Paint Creek, Wells Creek, Quemahoning Creek, Oven Run, and Pokeytown Run Basins.Passive-treatment systems that include aerobic wetlands, compost wetlands, and anoxic limestone drains (ALD's) are planned to remediate the abandoned mine discharges. The successive alkalinity-producing-system treatment combines ALD technology with the sulfate reduction mechanism of the compost wetland to effectively remediate mine discharge. The water quality and flow of each mine discharge will determine which treatment system or combination of treatment systems would be necessary for remediation.A network of 37 surface-water sampling sites was established to determine stream-water quality during base flow. A series of illustrations show how water quality in the mainstem deteriorates downstream because of inflows from tributaries affected by acidic mine discharges. From the upstream mainstem site (site 801) to the outflow mainstem site (site 805), pH decreased from 6.8 to 4.2, alkalinity was completely depleted by inflow acidities, and total-iron discharges increased from 30 to 684 pounds per day. Total-manganese and total-sulfate discharges increased because neither constituent precipitates readily. Also, discharges of manganese and sulfate entering the mainstem from tributary streams have a cumulative effect.Oven Run and Pokeytown Run are two small tributary streams significantly affected by acidic mine drainage (AMD) that flow into the Stonycreek River near the town of Hooversville. The Pokeytown Run inflow is about 0.5 mile downstream from the Oven Run inflow. These two streams are the first major source of AMD flowing into the Stonycreek River. Data collected on the Stonycreek River above the Oven Run inflow and below the Pokeytown Run inflow show a decrease in pH from 7.6 to 5.1, a decrease in alkalinity concentration from 42 to 2 milligrams per liter, an increase in total sulfate discharge from 18 to 41 tons per day, and an increase in total iron discharge from 29 to 1,770 pounds per day. Data collected at three mainstem sites on the Stonycreek River below Oven Run and Pokeytown Run show a progressive deterioration in river water quality from AMD.Shade Creek and Paint Creek are other tributary streams to the Stonycreek River that have a significant negative effect on water quality of the Stonycreek River. One third of the abandoned-mine discharges sampled were in the Shade Creek and Paint Creek Basins.

  3. Solvent vapor collector

    DOEpatents

    Ellison, Kenneth; Whike, Alan S.

    1979-01-30

    A solvent vapor collector is mounted on the upstream inlet end of an oven having a gas-circulating means and intended for curing a coating applied to a strip sheet metal at a coating station. The strip sheet metal may be hot and solvent vapors are evaporated at the coating station and from the strip as it passes from the coating station to the oven. Upper and lower plenums within a housing of the collector are supplied with oven gases or air from the gas-circulating means and such gases or air are discharged within the collector obliquely in a downstream direction against the strip passing through that collector to establish downstream gas flows along the top and under surfaces of the strip so as, in turn, to induct solvent vapors into the collector at the coating station. A telescopic multi-piece shroud is usefully provided on the housing for movement between an extended position in which it overlies the coating station to collect solvent vapors released thereat and a retracted position permitting ready cleaning and adjustment of that coating station.

  4. Validation of the filament winding process model

    NASA Technical Reports Server (NTRS)

    Calius, Emilo P.; Springer, George S.; Wilson, Brian A.; Hanson, R. Scott

    1987-01-01

    Tests were performed toward validating the WIND model developed previously for simulating the filament winding of composite cylinders. In these tests two 24 in. long, 8 in. diam and 0.285 in. thick cylinders, made of IM-6G fibers and HBRF-55 resin, were wound at + or - 45 deg angle on steel mandrels. The temperatures on the inner and outer surfaces and inside the composite cylinders were recorded during oven cure. The temperatures inside the cylinders were also calculated by the WIND model. The measured and calculated temperatures were then compared. In addition, the degree of cure and resin viscosity distributions inside the cylinders were calculated for the conditions which existed in the tests.

  5. Performance of fly ash based geopolymer incorporating palm kernel shell for lightweight concrete

    NASA Astrophysics Data System (ADS)

    Razak, Rafiza Abd; Abdullah, Mohd Mustafa Al Bakri; Yahya, Zarina; Jian, Ang Zhi; Nasri, Armia

    2017-09-01

    A concrete which cement is totally replaced by source material such as fly ash and activated by highly alkaline solutions is known as geopolymer concrete. Fly ash is the most common source material for geopolymer because it is a by-product material, so it can get easily from all around the world. An investigation has been carried out to select the most suitable ingredients of geopolymer concrete so that the geopolymer concrete can achieve the desire compressive strength. The samples were prepared to determine the suitable percentage of palm kernel shell used in geopolymer concrete and cured for 7 days in oven. After that, other samples were prepared by using the suitable percentage of palm kernel shell and cured for 3, 14, 21 and 28 days in oven. The control sample consisting of ordinary Portland cement and palm kernel shell and cured for 28 days were prepared too. The NaOH concentration of 12M, ratio Na2SiO3 to NaOH of 2.5, ratio fly ash to alkaline activator solution of 2.0 and ratio water to geopolymer of 0.35 were fixed throughout the research. The density obtained for the samples were 1.78 kg/m3, water absorption of 20.41% and the compressive strength of 14.20 MPa. The compressive strength of geopolymer concrete is still acceptable as lightweight concrete although the compressive strength is lower than OPC concrete. Therefore, the proposed method by using fly ash mixed with 10% of palm kernel shell can be used to design geopolymer concrete.

  6. LBP Concerns in Producing Recycled Concrete Aggregate from Former Fort Ord Family Housing

    DTIC Science & Technology

    2007-01-01

    that hasten drying. They pull oxygen through the wet paint film to oxidize and cure the paint. These driers include lead naphthenate , lead resinates...They were out of the way of the active demolition work, and they were among the last to be removed . CCC took floor wipes at the three buildings...preceded by an “abate- ment activity” whereby all identified LBP was to be removed . However, the scope and effectiveness of this activity is

  7. Laboratory Studies of Containment in Underground Nuclear Tests.

    DTIC Science & Technology

    1980-01-31

    and filling the space between charge holder and tube with epoxy. The access tube is filled with epoxy. Vel t iug occurs when tile tube is drilled out...membrane is then stretched over the eud of the access tube and held in place by means of a Teflon ferrule and epoxy sa I . Tile membrane is filled with...electrically conductive silver -based paint. Two copper tabs are first embedded in the surface of the sphere during cast ing. After the grout is cured, the paint

  8. Measurement of the full-field polymerization shrinkage and depth of cure of dental composites using digital image correlation.

    PubMed

    Li, Jianying; Fok, Alex S L; Satterthwaite, Julian; Watts, David C

    2009-05-01

    The aim of this study was to measure the full-field polymerization shrinkage of dental composites using optical image correlation method. Bar specimens of cross-section 4mm x 2mm and length 10mm approximately were light cured with two irradiances, 450 mW/cm(2) and 180 mW/cm(2), respectively. The curing light was generated with Optilux 501 (Kerr) and the two different irradiances were achieved by adjusting the distance between the light tip and the specimen. A single-camera 2D measuring system was used to record the deformation of the composite specimen for 30 min at a frequency of 0.1 Hz. The specimen surface under observation was sprayed with paint to produce sufficient contrast to allow tracking of individual points on the surface. The curing light was applied to one end of the specimen for 40s during which the painted surface was fully covered. After curing, the cover was removed immediately so that deformation of the painted surface could be recorded by the camera. The images were then analyzed with specialist software and the volumetric shrinkage determined along the beam length. A typical shrinkage strain field obtained on a specimen surface was highly non-uniform, even at positions of constant distance from the irradiation surface, indicating possible heterogeneity in material composition and shrinkage behavior in the composite. The maximum volumetric shrinkage strain of approximately 1.5% occurred at a subsurface distance of about 1mm, instead of at the irradiation surface. After reaching its peak value, the shrinkage strain then gradually decreased with increasing distance along the beam length, before leveling off to a value of approximately 0.2% at a distance of 4-5mm. The maximum volumetric shrinkage obtained agreed well with the value of 1.6% reported by the manufacturer for the composite examined in this work. Using irradiance of 180 mW/cm(2) resulted in only slightly less polymerization shrinkage than using irradiance of 450 mW/cm(2). Compared to the other measurement methods, the image correlation method is capable of producing full-field information about the polymerization shrinkage behavior of dental composites.

  9. Process gas hear recovery

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Anderson, W.M.; Thurner, R.P.

    1977-01-01

    In considering the use of regenerative and recuperative heat exchangers for process-gas heat recovery general information regarding heat-exchanger effectiveness versus initial capital investment and operating costs is discussed. Specific examples for preheating combustion air for process furnaces and for using primary and secondary heat exchangers in conjunction with an air-pollution-control system for drying and curing ovens cover basic heat-exchanger design and application considerations as well as investment-payback factors.

  10. Cyanate Ester Resin Modified with Nano-particles for Inclusion in Continuous Fiber Reinforced Composites

    DTIC Science & Technology

    2011-02-25

    custom built rotating oven, to prevent settling during cure. The filler content in the test specimen are verified by thermogravimetric analysis (TGA...using a Shimadzu SA-CP3 centrifugal particle size analyzer. The moisture absorption of the nanoparticles was studied using a Q50 thermogravimetric ...low viscosity bisphenol E cyanate ester resin (BECy) resin reinforced with macro scale carbon fibers and negative CTE nanoparticles . Polymer

  11. Isocyanate-Free Elastomers as Replacements for Isocyanate-Cured Polyurethanes (Briefing Charts)

    DTIC Science & Technology

    2015-08-20

    Polyurethanes (Briefing Charts) 5a. CONTRACT NUMBER In-House 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 6. AUTHOR(S) Josiah T. Reams, Andrew J...Standard Form 298 (Rev. 8-98) Prescribed by ANSI Std. 239.18 1 Isocyanate-Free Elastomers as Replacements for Isocyanate-cured Polyurethanes ...paints, foams , sealants, and adhesives that also represent a significant source of occupational health risk for DoD and DOE. DISTRIBUTION A:  Approved

  12. A Durable Airfield Marking System.

    DTIC Science & Technology

    1985-06-01

    Resin is Mixed with the Black Curing Agent to Form the Epoxy Adhesive ..... ........... 17 14 The Gray Adhesive (White Resin Mixed with Black Curing...rubber 100 0 Polyester (peroxide-catalyzed) 100 0 Urethane 100 0 Epoxy polyamide 100 0 Acrylic latex (TT-P-1952) 100 0 Thermoplastic Tapes Type 1 100 0...suzmarrizes cost data co1parisons for traffic marking tapes, CAS tiles, fluorocarbon composites (Teflon ),and acrylic latex paint TT-P-1952. 8 -p °’. TABLE 2

  13. A Study for the Characteristic Changes Under the Repeated Thermal Exposure in the Process of Repairing Aircraft Sandwich Structures

    NASA Astrophysics Data System (ADS)

    Kim, Yun Hae; Han, Joong Won; Kim, Don Won; Choi, Byung Keun; Murakami, R.

    Delamination can be observed in the sound areas during and/or after a couple times exposure to the elevated curing temperature due to the repeated repair condition. This study was conducted for checking the degree of degradation of properties of the cured parts and delamination between skin prepreg and honeycomb core. Specimens with glass honeycomb sandwich construction and glass/epoxy prepreg were prepared. The specimens were cured 1 to 5 times at 260°F in an autoclave and each additionally exposed 50, 100 and 150 hours in the 260°F oven. Each specimen was tested for tensile strength, compressive strength, flatwise tensile strength and interlaminar shear strength. To monitor the characteristics of the resin itself, the cured resin was tested using DMA and DSC. As a results, the decrease of Tg value were observed in the specific specimen which is exposed over 50 hrs at 260°F. This means the change or degradative of resin properties is also related to the decrease of flatwise tensile properties. Accordingly, minimal exposure on the curing temperature is recommended for parts in order to prevent the delation and maintain the better condition.

  14. Microwave-Assisted Curing of Silicon Carbide-Reinforced Epoxy Composites: Role of Dielectric Properties

    NASA Astrophysics Data System (ADS)

    Pal, Ranu; Akhtar, M. J.; Kar, Kamal K.

    2018-05-01

    In this work, the dielectric properties of epoxy-based composites are significantly improved with the help of the silicon carbide (SiC) filler at an operating frequency of 2.45 GHz to make them ideal candidates for microwave curing. The improvement is due to enhancement of the interfacial polarization because of the presence of the SiC filler. The dielectric properties are measured using the microwave cavity perturbation method. The cavity structure is simulated using the COMSOL@Multiphysics software to verify the measured data in terms of the resonant frequency. Finally, all the SiC-based composites including the neat epoxy resin are heated in the 2.45 GHz microwave oven at 300 W for 20 min. The thermal and mechanical properties of all the cured composites are measured, and the data are compared with their room temperature pre-cured counterparts. The dielectric properties of composite samples using SiC as a reinforcing agent in the epoxy are found to be substantially improved compared with those of the pure epoxy sample, which actually leads to better curing of these composite using the 2.45 GHz microwave system.

  15. The Effect of Curing Temperature on the Fracture Toughness of Fiberglass Epoxy Composites

    NASA Astrophysics Data System (ADS)

    Ryan, Thomas J.

    The curing reaction in a thermoset polymer matrix composite is often accelerated by the addition of heat in an oven or autoclave. The heat added increases the rate of the polymerization reaction and cross-linking in the material. The cure cycle used (temperature, pressure and time) can therefore alter the final material properties. This research focuses on how the curing temperature (250, 275, 300 °F) affects the yield strength and the mode I interlaminar fracture toughness, GI, of a unidirectional S-2 glass epoxy composite. The test method that was used for the tension test was ASTM D3039 and the test method for the mode I interlaminar fracture toughness, the double cantilever beam (DCB) test, was ASTM D5528. The DCB specimens were fabricated with a non-adhesive insert at the midplane of the composite that serves as the initiatior of the delamination. Opening forces were then applied to the specimen, causing the crack propagation. The results show that increasing the cure temperature by 50 °F increased the tensile strength by 10% (86.54 - 94.73 ksi) and decreased the fracture toughness 20% (506.23 - 381.31 J/m 2). Thus, the curing temperature can cause a trade-off between these two properties, which means that the curing cycle will need to be altered based on the intended use and the required material properties.

  16. Simulation of Energy Savings in Automotive Coatings Processes

    NASA Astrophysics Data System (ADS)

    Gerini Romagnoli, Marco

    Recently, the automakers have become more and more aware of the environmental and economic impact of their manufacturing processes. The paint shop is the largest energy user in a vehicle manufacturing plant, and one way to reduce costs and energy usage is the optimization of this area. This project aims at providing a tool to model and simulate a paint shop, in order to run and analyze some scenarios and case studies, helping to take strategic decisions. Analytical computations and real data were merged to build a tool that can be used by FCA for their Sterling Heights plant. Convection and conduction heat losses were modeled for the dip processes and the ovens. Thermal balances were used to compute the consumptions of booths, decks and ovens, while pump and fan energy consumptions were modeled for each sub-process. The user acts on a calendar, scheduling a year of production, and the model predicts the energy consumption of the paint shop. Five scenarios were run to test different conditions and the influence of scheduling on the energy consumption. Two different sets of production schedules have been evaluated, the first one fulfilling the production requirement in one shift of 10 hours, at high rate, the second one using two 7-hour-long shifts at medium production rate. It was found that the unit cost was minimized in the warmest months of spring and fall, and system shutdown was a crucial factor to reduce energy consumption. A fifth hypothetical scenario was run, with a 4 month continuous production and an 8 month total shutdown, which reduced the energy consumption to a half of the best realistic scenario. When the plant was run in a two-shifts configuration, the cost to coat a vehicle was found to be 29 with weekend shutdown, and 39 without. In the one-shift configuration, the cost was slightly higher, but the difference was less than 5%. While the fifth scenario showed a consistent reduction of the unit cost, inventory and logistic expenses deriving from the production strategy make this scenario almost impossible to realize. A sensitivity analysis was run on several parameters influencing the energy consumption of the paint shop, and the booths set point temperature was found to be the most significant factor.

  17. Conveyorized Radio Frequency Cure of Epoxy Glass Composites.

    DTIC Science & Technology

    1980-05-01

    a conveyorized radio frequency oven. The conveyorized radio frequency 20-kilowatt (90-100 megahertz) dielectric heater was de - designed and...Process were de - termined with reference to property requirements specified in Table three of 8MS-8-196A. Although the BM-8,196A relates to material...requirements of the 8MS and agree with the values contained in the 3M certifying report. De - tailed test results are presented as Appendix J. In addition

  18. 40 CFR 63.6015 - What definitions apply to this subpart?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... cements, bead cements, tire building cements and solvents, green tire spray, blemish repair paints, side... in tire component identification; component storage; tire building; tire curing; and tire repair... of warm-up mills, extruders, calendars, tire building, or other tire component and tire manufacturing...

  19. An ecotoxicological study on tin- and bismuth-catalysed PDMS based coatings containing a surface-active polymer.

    PubMed

    Pretti, Carlo; Oliva, Matteo; Mennillo, Elvira; Barbaglia, Martina; Funel, Marco; Reddy Yasani, Bhaskar; Martinelli, Elisa; Galli, Giancarlo

    2013-12-01

    Novel films were prepared by condensation curing reaction of a poly(dimethyl siloxane) (PDMS) matrix with bismuth neodecanoate and dibutyltin diacetate catalysts. An ecotoxicological study was performed on the leachates of the coatings using the bacterium Vibrio fischeri, the unicellular alga Dunaliella tertiolecta, the crustacean Artemia salina and the fish Sparus aurata (larvae) as testing organisms. A copper-based self-polishing commercial paint was also tested as reference. The results showed that the tin-catalysed coatings and the copper paint were highly toxic against at least two of the four test organisms, whereas bismuth-catalysed coatings did not show any toxic effect. Moreover, the same biological assessment was also carried out on PDMS coatings containing a surface-active fluorinated polymer. The toxicity of the entire polymeric system resulted only from the tin catalyst used for the condensation curing reaction, as the bismuth catalysed coatings incorporating the surface-active polymer remained atoxic toward all the tested organisms. © 2013 Elsevier Inc. All rights reserved.

  20. Silver-Teflon coating improvement

    NASA Technical Reports Server (NTRS)

    Reed, M. W.

    1976-01-01

    Approximately forty adhesives were subjected to laboratory screening. Seven candidate adhesives were selected from the screening tests and evaluated in a thermal vacuum test on radiator panels similar to the anticipated flight hardware configuration. Several classes of adhesives based on epoxide, polyester, silicone, and urethane resin systems were tested. These included contact adhesives, heat cured adhesives, heat and pressure cured adhesives, pressure sensitive adhesives, and two part paint-on or spray-on adhesives. The panels were tested in a space environmental simulation laboratory chamber during the July 9-20, 1973 time span.

  1. High-performance liquid chromatographic determination of benzil in air as an indicator of emissions derived from polyester powder coatings.

    PubMed

    Pukkila, J; Kokotti, H; Peltonen, K

    1989-10-06

    A method to estimate occupational exposure to emissions from the curing of polyester powder paints was developed. The method is based on the monitoring only of a certain marker compound in workroom air in order to make the determinations easier. Benzil, reproducibly emitted from all the powders tested, was chosen as the indicator for curing (220 degrees C)-derived emissions. A method for the air sampling and high-performance liquid chromatographic benzil is described. Aspects of the use of marker compounds are discussed.

  2. Effect of monomer composition of polymer matrix on flexural properties of glass fibre-reinforced orthodontic archwire.

    PubMed

    Ohtonen, J; Vallittu, P K; Lassila, L V J

    2013-02-01

    To compare force levels obtained from glass fibre-reinforced composite (FRC) archwires. Specifically, FRC wires were compared with polymer matrices having different dimethacrylate monomer compositions. FRC material (E-glass provided by Stick Tech Ltd, Turku, Finland) with continuous unidirectional glass fibres and four different types of dimethacrylate monomer compositions for the resin matrix were tested. Cross-sectionally round FRC archwires fitting into the 0.3 mm slot of a bracket were divided into 16 groups with six specimens in each group. Glass fibres were impregnated by the manufacturer, and they were initially light-cured by hand light-curing unit or additionally post-cured in light-curing oven. The FRC archwire specimens were tested at 37°C according to a three-point bending test in dry and wet conditions using a span length of 10 mm and a crosshead speed of 1.0 mm/minute. The wires were loaded until final failure. The data were statistically analysed using analysis of variance (ANOVA). The dry FRC archwire specimens revealed higher load values than water stored ones, regardless of the polymer matrix. A majority of the FRC archwires showed higher load values after being post-cured. ANOVA revealed that the polymer matrix, curing method, and water storage had a significant effect (P < 0.05) on the flexural behaviour of the FRC archwire. Polymer matrix composition, curing method, and water storage affected the flexural properties and thus, force level and working range which could be obtained from the FRC archwire.

  3. Fire-Retardant Decorative Inks For Aircraft Interiors

    NASA Technical Reports Server (NTRS)

    Kourtides, D. A.; Nir, Z.; Mikroyannidis, J. A.

    1988-01-01

    Report describes testing of commercial and experimental fire retardants for incorporation into acrylic printing inks used on aircraft-interior sandwich panels. Films of acrylic ink containing fire-retardant additives prepared by casting on glass plates. Solvent evaporated in vacuum, cast films cured at 80 to 100 degree C for 30 minutes in air-circulating oven. Thermochemical properties of films examined by thermogravimetric analysis and differential scanning calorimetry (DSC). Samples of inks cast on sheets of polyvinylfloride (PVF), and their limiting oxygen indices and smoke evolution measured.

  4. Processing and Dynamic Failure Characterization of Novel Impact Absorbing Transparent Interpenetrating Polymer Networks (t-IPN)

    DTIC Science & Technology

    2013-07-05

    oven for the same curing treatment as before. The scanning electron microscope (SEM) photo in Figure 19 shows a typical sample with TMSPM and IPTES...Methacrylate-based Polymers,’ S. A . Bird , PhD Dissertation, Department of Polymer and Fiber Engineering, Auburn University, Summer 2013. ’Fracture Behavior...Polymer Networks with Polyurethane-poly(methyl methacrylate),’ K. C. Jajam, S. A . Bird , M. L. Auad, and H. V. Tippur, Polymer Testing, Vol. 32, pp

  5. Processing and Dynamic Failure Characterization of Novel Impact Absorbing Transparent Interpenetrating Polymer Networks (t-IPN)

    DTIC Science & Technology

    2014-02-01

    samples were placed into the oven for the same curing treatment as before. The scanning electron microscope (SEM) photo in Figure 19 shows a typical...Interpenetrating Polymer Networks with Polyurethane and Methacrylate-based Polymers,’ S. A . Bird , PhD Dissertation, Department of Polymer and Fiber Engineering...Jajam, H. V. Tippur, S. A . Bird , and M. L. Auad, Proceedings of the 50th SES Annual Technical Meeting and ASME-AMD Summer Meeting, Providence, RI

  6. KSC-2012-1587

    NASA Image and Video Library

    2012-03-01

    CAPE CANAVERAL, Fla. -- The heat shield tiles that will be installed to the backshell of the Orion Multi-Purpose Crew Vehicle's Exploration Flight Test EFT-1 capsule are removed from a Keith thermal automation oven. Inside, the tiles were baked at 2,200 degrees F to cure their ceramic coating. The work to manufacture and inspect the tiles is taking place in Kennedy's Thermal Protection System Facility. EFT-1 will be used during Orion's first test flight in space. For more information, visit www.nasa.gov/orion. Photo credit: Frankie Martin

  7. Progress Towards Microwave Ignition of Explosives

    NASA Astrophysics Data System (ADS)

    Curling, Mark; Collins, Adam; Dima, Gabriel; Proud, William

    2009-06-01

    Microwaves could provide a method of propellant ignition that does away with a traditional primer, making ammunition safer and suitable for Insensitive Munitions (IM) applications. By embedding a suitable material inside a propellant, it is postulated that microwaves could be used to stimulate hotspots, through direct heating or electrostatic discharge (arcing) across the energetic material. This paper reports on progress in finding these suitable materials. Graphite rod, magnetite cubes and powders of graphite, aluminium, copper oxide, and iron were irradiated in a conventional microwave oven. Temperature measurements were made using a shielded thermocouple and thermal paints. Only graphite rod and magnetite showed significant heating upon microwave exposure. The light output from arcing of iron, steel, iron pyrite, magnetite and graphite was measured in the same microwave oven as above. Sample mass and shape were correlated with arcing intensity. A strategy is proposed to create a homogeneous igniter material by embedding arcing materials within an insulator, Polymethylpentene (TPX). External discharges were transmitted through TPX, however no embedded samples were successful in generating an electrical breakdown suitable for propellant ignition.

  8. Multifunctional green nanostructured composites: preparation and characterization

    NASA Astrophysics Data System (ADS)

    Stieven Montagna, Larissa; Sizuka Oishi, Silvia; Faria Diniz, Milton; Larissa do Amaral Montanheiro, Thaís; Santos da Silva, Fábio; Passador, Fábio Roberto; Cerqueira Rezende, Mirabel

    2018-05-01

    The present research had as main purpose to develop and characterize multifunctional green nanocomposites based on poly(furfuryl alcohol) resin (PFA bioresin), derived from sugarcane bagasse reinforced with different contents of graphite nanosheets (GNS) (0.5, 1.0, 1.5 and 2.0 wt%) which were dispersed in PFA bioresin using an ultrasonic processor. The mixture was poured into silicone molds and cured at room temperature during 24 h followed by a post-cure at preheated oven in cycles of different temperatures. TEM analysis of GNS showed this filler consist of ultrathin and layered sheets. SEM micrographs of the cryogenic fracture of the nanocomposite presented the good interfacial adhesion between PFA bioresin and GNS. Moreover, upon GNS addition in the PFA bioresin, PFA/GNS nanocomposites demonstrated superior mechanical performance and better electrical conductivity than neat PFA bioresin.

  9. 21 CFR 177.2400 - Perfluorocarbon cured elastomers.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... (channel process of furnace combustion process) (CAS Reg. No. 1333-86-4) Not to exceed 15 parts per 100... Administration, 5100 Paint Branch Pkwy., College Park, MD 20740, or available for inspection at the National..., call 202-741-6030, or go to: http://www.archives.gov/federal_register/code_of_federal_regulations/ibr...

  10. 21 CFR 177.2400 - Perfluorocarbon cured elastomers.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... (channel process of furnace combustion process) (CAS Reg. No. 1333-86-4) Not to exceed 15 parts per 100... Administration, 5100 Paint Branch Pkwy., College Park, MD 20740, or available for inspection at the National..., call 202-741-6030, or go to: http://www.archives.gov/federal_register/code_of_federal_regulations/ibr...

  11. Material Property Characterization of AS4/VRM-34 Textile Laminates

    NASA Technical Reports Server (NTRS)

    Grenoble, Ray W.; Johnston, William M

    2013-01-01

    Several material properties (modulus, strengths, and fracture toughness) of a textile composite have been evaluated to provide input data to analytical models of Pultruded Rod Stiffened Efficient Unitized Structure (PRSEUS). The material system is based on warp-knitted preforms of AS4 carbon fibers and VRM-34 epoxy resin, which have been processed via resin infusion and oven curing. Tensile, compressive, shear, and fracture toughness properties have been measured at ambient and elevated temperatures. All specimens were tested in as-fabricated (dry) condition. Specimens were tested with and without through-thickness stitching.

  12. Exposure to methylhexahydrophthalic anhydride (MHHPA) in two workplaces of the electric industry.

    PubMed

    Pfäffli, Pirkko; Hämeilä, Mervi; Riala, Riitta; Tornaeus, Jarkko; Wirmoila, Ritva

    2004-04-01

    Methylhexahydrophthalic anhydride (MHHPA) is a hardener for hot-cured epoxy resins employed as insulators in the electric industry. MHHPA has only been measured as an ingredient with other alicyclic anhydrides, albeit there are also large processes which use only MHHPA. We collected MHHPA vapour in a set of devices: Teflon filter, glass spiral, TenaxTA tube connected consecutively together. Elution was performed with a solvent mixture of methyl-tert-butyl ether (70%), acetonitrile (30%), and acetic anhydride (0.5%). By capillary GC-ECD, the regression was linear (0.9994) in the practical low concentration range of 0.04-1 microg ml(-1) being equal to 0.001-0.035 mg m(-3) in 30 l of air. The exposure was measured in two factories manufacturing electric appliances. The assembled objects were first impregnated with a liquid epoxy/hardener mixture, and then the resin hardened at elevated temperature. In condenser manufacturing, the operators' 8 h exposure ranged from 0.068 to 0.118 mg m(-3), and the short-term exposure was during operation at ovens mean 1.90 mg m(-3). The impregnation of coiled resistors and transfer of them to ovens caused the worst exposures, short-term mean 3.846 mg m(-3) and long-term mean 2.191 mg m(-3). During the 'baking', the ovens were closed and evacuated, but when the hot objects were moved out of the ovens, they continued during chilling to emit MHHPA, mean 0.366 mg m(-3). In the adjacent areas, assembling, control rooms, offices, the exposure was still significant, 0.017-0.043 mg m(3), due to leaks from the high exposure areas. Mechanical general ventilation and local exhausts were functioning. Respirators were available for short supervising of the hot equipment.

  13. Chemorheology of in-mold coating for compression molded SMC applications

    NASA Astrophysics Data System (ADS)

    Ko, Seunghyun; Straus, Elliott J.; Castro, Jose M.

    2015-05-01

    In-mold coating (IMC) is applied to compression molded sheet molding compound (SMC) exterior automotive or truck body panels as an environmentally friendly alternative to make the surface conductive for subsequent electrostatic painting operations. The coating is a thermosetting liquid that when injected onto the surface of the part cures and bonds to provide a smooth conductive surface. In order to optimize the IMC process, it is essential to predict the time available for flow, that is the time before the thermosetting reaction starts (inhibition time) as well as the time when the coating has enough structural integrity so that the mold can be opened without damaging the part surface (cure time). To predict both the inhibition time and the cure time, it is critical to study the chemorheology of IMC. In this paper, we study the chemorheology for a typical commercial IMC system, and show its relevance to both the flow and cure time for the IMC stage during SMC compression molding.

  14. Creep of experimental short fiber-reinforced composite resin.

    PubMed

    Garoushi, Sufyan; Kaleem, Muhammad; Shinya, Akikazu; Vallittu, Pekka K; Satterthwaite, Julian D; Watts, David C; Lassila, Lippo V J

    2012-01-01

    The purpose of this study was to investigate the reinforcing effect of short E-glass fiber fillers oriented in different directions on composite resin under static and dynamic loading. Experimental short fiber-reinforced composite resin (FC) was prepared by mixing 22.5 wt% of short E-glass fibers, 22.5 wt% of resin, and 55 wt% of silane-treated silica fillers. Three groups of specimens (n=5) were tested: FC with isotropic fiber orientation, FC with anisotropic fiber orientation, and particulate-filled composite resin (PFC) as a control. Time-dependent creep and recovery were recorded. ANOVA revealed that after secondary curing in a vacuum oven and after storage in dry condition for 30 days, FC with isotropic fiber orientation (1.73%) exhibited significantly lower static creep value (p<0.05) than PFC (2.54%). For the different curing methods and storage conditions evaluated in this study, FC achieved acceptable static and dynamic creep values when compared to PFC.

  15. Advanced composite rudders for DC-10 aircraft: Design, manufacturing, and ground tests

    NASA Technical Reports Server (NTRS)

    Lehman, G. M.; Purdy, D. M.; Cominsky, A.; Hawley, A. V.; Amason, M. P.; Kung, J. T.; Palmer, R. J.; Purves, N. B.; Marra, P. J.; Hancock, G. R.

    1976-01-01

    Design synthesis, tooling and process development, manufacturing, and ground testing of a graphite epoxy rudder for the DC-10 commercial transport are discussed. The composite structure was fabricated using a unique processing method in which the thermal expansion characteristics of rubber tooling mandrels were used to generate curing pressures during an oven cure cycle. The ground test program resulted in certification of the rudder for passenger-carrying flights. Results of the structural and environmental tests are interpreted and detailed development of the rubber tooling and manufacturing process is described. Processing, tooling, and manufacturing problems encountered during fabrication of four development rudders and ten flight-service rudders are discussed and the results of corrective actions are described. Non-recurring and recurring manufacturing labor man-hours are tabulated at the detailed operation level. A weight reduction of 13.58 kg (33 percent) was attained in the composite rudder.

  16. Evaluation of some properties of two fiber-reinforced composite materials.

    PubMed

    Lassila, Lippo V J; Tezvergil, Arzu; Lahdenperä, Milla; Alander, Pasi; Shinya, Akiyoshi; Shinya, Akikazu; Vallittu, Pekka K

    2005-08-01

    Water sorption, flexural properties, bonding properties, and elemental composition of photopolymerizable resin-impregnated fiber-reinforced composite (FRC) materials (everStick C&B and BR-100) (FPD) were evaluated in this study. Bar-shaped specimens (2 x 2 x 25 mm) were prepared for water sorption and flexural strength testing. The specimens (n = 6) were polymerized either with a hand light-curing unit for 40 s or, additionally, in a light-curing oven for 20 min and stored in water for 30 days. Water sorption was measured during this time, followed by measurements of flexural strength and modulus. A shear bond strength test was performed to determine the bonding characteristics of polymerized FRC to composite resin luting cement (Panavia-F), (n = 15). The cement was bonded to the FRC substrate and the specimens were thermocycled 5000 times (5-55 degrees C) in water. SEM/EDS were analyzed to evaluate the elemental composition of the glass fibers and the fiber distribution in cross section. ANOVA showed significant differences in water sorption according to brand (p < 0.05). Water sorption of everStick C&B was 1.86 wt% (hand-unit polymerized) and 1.94 wt% (oven polymerized), whereas BR-100 was 1.07 wt% and 1.17 wt%, respectively. The flexural strength of everStick C&B after 30 days' water storage was 559 MPa (hand-unit polymerized) and 796 MPa (oven-polymerized); for BR-100, the values were 547 MPa and 689 MPa, respectively. Mean shear bond strength of composite resin cement to the FRC varied between 20.1 and 23.7 MPa, showing no statistical difference between the materials. SEM/EDS analysis revealed that fibers of both FRC materials consist of the same oxides (SiO2, CaO, and Al2O3) in ratios. The distribution of fibers in the cross section of specimens was more evenly distributed in everStick C&B than in BR-100. The results of this study suggest that there are some differences in the tested properties of the FRC materials.

  17. Treatment of White Phosphorus and Other Chemical Burn Injuries at One Burn Center Over a 51-year Period

    DTIC Science & Technology

    2004-01-01

    cellulose or lauryl sulfate , avoidance of copper- sulfate soaked pads, and use of prompt water or saline rinse following application [19–22,24]. These...0 1 1 Diesel 0 0 1 1 Oven cleaner 0 0 5 5 JP4 fuel 0 0 1 1 Phenol 0 2 2 4 Fluorocarbon 0 2 1 3 Paint thinner 0 1 0 1 Triethylene gycol 0 1 0 1 Sodium ...ammonia 6.8 3.7 Hydrochloric acid 5.6 3.1 Sulfuric acid 4.7 6.5 Polychlorinated biphenyls 2.8 23 Toluene 2.4 1.4 Sodium hydroxide 1.9 2.6 Nitric acid 1.5

  18. Self-regenerating and hybrid irreversible/reversible PDMS microfluidic devices.

    PubMed

    Shiroma, Letícia S; Piazzetta, Maria H O; Duarte-Junior, Gerson F; Coltro, Wendell K T; Carrilho, Emanuel; Gobbi, Angelo L; Lima, Renato S

    2016-05-16

    This paper outlines a straightforward, fast, and low-cost method to fabricate polydimethylsiloxane (PDMS) chips. Termed sandwich bonding (SWB), this method requires only a laboratory oven. Initially, SWB relies on the reversible bonding of a coverslip over PDMS channels. The coverslip is smaller than the substrate, leaving a border around the substrate exposed. Subsequently, a liquid composed of PDMS monomers and a curing agent is poured onto the structure. Finally, the cover is cured. We focused on PDMS/glass chips because of their key advantages in microfluidics. Despite its simplicity, this method created high-performance microfluidic channels. Such structures featured self-regeneration after leakages and hybrid irreversible/reversible behavior. The reversible nature was achieved by removing the cover of PDMS with acetone. Thus, the PDMS substrate and glass coverslip could be detached for reuse. These abilities are essential in the stages of research and development. Additionally, SWB avoids the use of surface oxidation, half-cured PDMS as an adhesive, and surface chemical modification. As a consequence, SWB allows surface modifications before the bonding, a long time for alignment, the enclosure of sub-micron channels, and the prototyping of hybrid devices. Here, the technique was successfully applied to bond PDMS to Au and Al.

  19. Self-regenerating and hybrid irreversible/reversible PDMS microfluidic devices

    PubMed Central

    Shiroma, Letícia S.; Piazzetta, Maria H. O.; Duarte-Junior, Gerson F.; Coltro, Wendell K. T.; Carrilho, Emanuel; Gobbi, Angelo L.; Lima, Renato S.

    2016-01-01

    This paper outlines a straightforward, fast, and low-cost method to fabricate polydimethylsiloxane (PDMS) chips. Termed sandwich bonding (SWB), this method requires only a laboratory oven. Initially, SWB relies on the reversible bonding of a coverslip over PDMS channels. The coverslip is smaller than the substrate, leaving a border around the substrate exposed. Subsequently, a liquid composed of PDMS monomers and a curing agent is poured onto the structure. Finally, the cover is cured. We focused on PDMS/glass chips because of their key advantages in microfluidics. Despite its simplicity, this method created high-performance microfluidic channels. Such structures featured self-regeneration after leakages and hybrid irreversible/reversible behavior. The reversible nature was achieved by removing the cover of PDMS with acetone. Thus, the PDMS substrate and glass coverslip could be detached for reuse. These abilities are essential in the stages of research and development. Additionally, SWB avoids the use of surface oxidation, half-cured PDMS as an adhesive, and surface chemical modification. As a consequence, SWB allows surface modifications before the bonding, a long time for alignment, the enclosure of sub-micron channels, and the prototyping of hybrid devices. Here, the technique was successfully applied to bond PDMS to Au and Al. PMID:27181918

  20. KSC-2012-1574

    NASA Image and Video Library

    2012-03-01

    CAPE CANAVERAL, Fla. -- Tim Wright, a United Space Alliance engineering manager at NASA's Kennedy Space Center in Florida, put the heat shield tiles that will be installed to the backshell of the Orion Multi-Purpose Crew Vehicle's Exploration Flight Test EFT-1 capsule in a Keith thermal automation oven. The tiles will be baked at 2,200 degrees F to cure their ceramic coating. The work to manufacture and inspect the tiles is taking place in Kennedy's Thermal Protection System Facility. EFT-1 will be used during Orion's first test flight in space. For more information, visit www.nasa.gov/orion. Photo credit: Frankie Martin

  1. KSC-2012-1586

    NASA Image and Video Library

    2012-03-01

    CAPE CANAVERAL, Fla. -- Tim Wright, a United Space Alliance engineering manager at NASA's Kennedy Space Center in Florida, removes the heat shield tiles that will be installed to the backshell of the Orion Multi-Purpose Crew Vehicle's Exploration Flight Test EFT-1 capsule from a Keith thermal automation oven. Inside, the tiles were baked at 2,200 degrees F to cure their ceramic coating. The work to manufacture and inspect the tiles is taking place in Kennedy's Thermal Protection System Facility. EFT-1 will be used during Orion's first test flight in space. For more information, visit www.nasa.gov/orion. Photo credit: Frankie Martin

  2. KSC-2012-1577

    NASA Image and Video Library

    2012-03-01

    CAPE CANAVERAL, Fla. -- Tim Wright, a United Space Alliance engineering manager at NASA's Kennedy Space Center in Florida, removes the heat shield tiles that will be installed to the backshell of the Orion Multi-Purpose Crew Vehicle's Exploration Flight Test EFT-1 capsule from a Keith thermal automation oven. Inside, the tiles were baked at 2,200 degrees F to cure their ceramic coating. The work to manufacture and inspect the tiles is taking place in Kennedy's Thermal Protection System Facility. EFT-1 will be used during Orion's first test flight in space. For more information, visit www.nasa.gov/orion. Photo credit: Frankie Martin

  3. Reaction of Pb(II) and Zn(II) with Ethyl Linoleate To Form Structured Hybrid Inorganic–Organic Complexes: A Model for Degradation in Historic Paint Films

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    MacDonald, Margaret G.; Palmer, Michael R.; Suchomel, Matthew R.

    To investigate soap formation in drying oils in historic paints, the reaction between metal acetates (K +, Zn 2+, Pb 2+) and ethyl linoleate (EL) was studied using optical microscopy, X-ray powder diffraction, and electron microscopy. Pb(II) and Zn(II) react rapidly with EL to form highly structured, spherulitic, luminescent crystallites that aggregate. Evidence from Fourier transform infrared (FTIR) and scanning electron microscopy/energy dispersive X-ray analysis and high-resolution synchrotron powder X-ray diffraction indicates that these are organic-inorganic hybrid complexes or coordination polymers. FTIR absorbance peaks at ca. 1540 cm -1 for Pb(II) and ca. 1580 cm -1 for Zn(II) are consistentmore » with the formation of carboxylate complexes. The complexes formed offer insight into the degradation processes observed in oil paint films, suggesting that soap formation is rapid when metal ions are solubilized and can occur with unsaturated fatty acids that are present in fresh oils. Finally, these complexes may account for the atypical luminescence observed in lead-containing cured oil paint films.« less

  4. Reaction of Pb(II) and Zn(II) with Ethyl Linoleate To Form Structured Hybrid Inorganic–Organic Complexes: A Model for Degradation in Historic Paint Films

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    MacDonald, Margaret G.; Palmer, Michael R.; Suchomel, Matthew R.

    To investigate soap formation in drying oils in historic paints, the reaction between metal acetates (K +, Zn 2+, Pb 2+) and ethyl linoleate (EL) was studied using optical microscopy, X-ray powder diffraction, and electron microscopy. Pb(II) and Zn(II) react rapidly with EL to form highly structured, spherulitic, luminescent crystallites that aggregate. Evidence from Fourier transform infrared (FTIR) and scanning electron microscopy/energy dispersive X-ray analysis and high-resolution synchrotron powder X-ray diffraction indicates that these are organic–inorganic hybrid complexes or coordination polymers. FTIR absorbance peaks at ca. 1540 cm –1 for Pb(II) and ca. 1580 cm –1 for Zn(II) are consistentmore » with the formation of carboxylate complexes. The complexes formed offer insight into the degradation processes observed in oil paint films, suggesting that soap formation is rapid when metal ions are solubilized and can occur with unsaturated fatty acids that are present in fresh oils. These complexes may account for the atypical luminescence observed in lead-containing cured oil paint films.« less

  5. Reaction of Pb(II) and Zn(II) with Ethyl Linoleate To Form Structured Hybrid Inorganic–Organic Complexes: A Model for Degradation in Historic Paint Films

    DOE PAGES

    MacDonald, Margaret G.; Palmer, Michael R.; Suchomel, Matthew R.; ...

    2016-09-07

    To investigate soap formation in drying oils in historic paints, the reaction between metal acetates (K +, Zn 2+, Pb 2+) and ethyl linoleate (EL) was studied using optical microscopy, X-ray powder diffraction, and electron microscopy. Pb(II) and Zn(II) react rapidly with EL to form highly structured, spherulitic, luminescent crystallites that aggregate. Evidence from Fourier transform infrared (FTIR) and scanning electron microscopy/energy dispersive X-ray analysis and high-resolution synchrotron powder X-ray diffraction indicates that these are organic-inorganic hybrid complexes or coordination polymers. FTIR absorbance peaks at ca. 1540 cm -1 for Pb(II) and ca. 1580 cm -1 for Zn(II) are consistentmore » with the formation of carboxylate complexes. The complexes formed offer insight into the degradation processes observed in oil paint films, suggesting that soap formation is rapid when metal ions are solubilized and can occur with unsaturated fatty acids that are present in fresh oils. Finally, these complexes may account for the atypical luminescence observed in lead-containing cured oil paint films.« less

  6. Fiber-reinforced composite substructure: load-bearing capacity of an onlay restoration and flexural properties of the material.

    PubMed

    Garoushi, Sufyan K; Lassila, Lippo V J; Tezvergil, Arzu; Vallittu, Pekka K

    2006-09-01

    The aim of this study was to determine the static load-bearing capacity of composite resin onlay restorations made of particulate filler composite (PFC) with two different types of fiber-reinforced composite (FRC) substructures. In addition, flexural properties of the material combination and the effect of polymerization devices were tested. Specimens were prepared to simulate an onlay restoration, which consisted of 2 to 3 mm of FRC layer as a substructure (short random and continuous bidirectional fiber orientation) and a 1 mm surface layer of PFC. Control specimens were prepared from plain PFC. In Group A the specimens were incrementally polymerized only with a hand-light curing unit for 40 s, while in Group B the specimens were post-cured in a light-curing oven for 15 min before they were statically loaded with a steel ball. Bar-shaped test specimens were prepared to measure the flexural properties of material combination using a three-point bending test (ISO 10477). Analysis of variance (ANOVA) revealed all specimens with a FRC substructure have higher values of static load-bearing capacity and flexural properties than those obtained with plain PFC (p<0.001). The load-bearing capacity of all the specimens decreased after post-curing and water storage. Restorations made from a material combination of FRC and PFC showed better mechanical properties than those obtained with plain PFC.

  7. Novel application of liquid chromatography/mass spectrometry for the characterization of drying oils in art: Elucidation on the composition of original paint materials used by Edvard Munch (1863-1944).

    PubMed

    La Nasa, Jacopo; Zanaboni, Marco; Uldanck, Daniele; Degano, Ilaria; Modugno, Francesca; Kutzke, Hartmut; Tveit, Eva Storevik; Topalova-Casadiego, Biljana; Colombini, Maria Perla

    2015-10-08

    Modern oil paints, introduced at the beginning of the 20th century, differ from those classically used in antiquity in their chemical and compositional features. The main ingredients were still traditional drying oils, often used in mixtures with less expensive oils and added with several classes of additives. Consequently, detailed lipid profiling, together with the study of lipid degradation processes, is essential for the knowledge and the conservation of paint materials used in modern and contemporary art. A multi-analytical approach based on mass spectrometry was used for the study of original paint materials from Munch's atelier, owned by the Munch Museum in Oslo. The results obtained in the analysis of paint tubes were compared with those obtained by characterizing a paint sample collected from one of the artist's sketches for the decoration of the Festival Hall of the University of Oslo (1909-1916). Py-GC/MS was used as screening method to evaluate the presence of lipid, proteic or polysaccaridic materials. GC/MS after hydrolysis and derivatization allowed us to determine the fatty acid profile of the paint tubes, and to evaluate the molecular changes associated to curing and ageing. The determination of the fatty acid profile is not conclusive for the characterization of complex mixtures of lipid materials, thus the characterization of the triglyceride profiles was performed using an analytical procedure based on HPLC-ESI-Q-ToF. This paper describes the first application of HPLC-ESI-Q-ToF for the acquisition of the triglyceride profile in a modern paint sample, showing the potentialities of liquid chromatography in the field of lipid characterization in modern paint materials. Moreover, our results highlighted that the application of this approach can contribute to address dating, authenticity and conservation issues relative to modern and contemporary artworks. Copyright © 2015. Published by Elsevier B.V.

  8. Thickness dependence of the poling and current-voltage characteristics of paint films made up of lead zirconate titanate ceramic powder and epoxy resin

    NASA Astrophysics Data System (ADS)

    Egusa, Shigenori; Iwasawa, Naozumi

    1995-11-01

    A specially prepared paint made up of lead zirconate titanate (PZT) ceramic powder and epoxy resin was coated on an aluminum plate and was cured at room temperature, thus forming the paint film of 25-300 μm thickness with a PZT volume fraction of 53%. The paint film was then poled at room temperature, and the poling behavior was determined by measuring the piezoelectric activity as a function of poling field. The poling behavior shows that the piezoelectric activity obtained at a given poling field increases with an increase in the film thickness from 25 to 300 μm. The current-voltage characteristic of the paint film, on the other hand, shows that the increase in the film thickness leads not only to an increase in the magnitude of the current density at a given electric field but also to an increase in the critical electric field at which the transition from the ohmic to space-charge-limited conduction takes place. This fact indicates that the amount of the space charge of electrons injected into the paint film decreases as the film thickness increases. Furthermore, comparison of the current-voltage characteristic of the paint film with that of a pure epoxy film reveals that the space charge is accumulated largely at the interface between the PZT and epoxy phases in the paint film. On the basis of this finding, a model is developed for the poling behavior of the paint film by taking into account a possible effect of the space-charge accumulation and a broad distribution of the electric field in the PZT phase. This model is shown to give an excellent fit to the experimental data of the piezoelectric activity obtained here as a function of poling field and film thickness.

  9. An Information Framework for Facility Operators

    DTIC Science & Technology

    1991-01-01

    and replacement products. Type: Type is used to decompose the building into smaller categories called arrangements, assemblies, parts, joints , and forro...are organized into crews and shops consisting of tradepersons responsible for building materials (concrete, masonry, metals, drywall , paint, etc...Comp Type (pre-cast, CIP) AS I Curing compound , sealant tyDe A S 04--- Masonry Comp Type (CMU, stone, glazed) A S I Manufacturer, style no., color no

  10. A Systems Approach to Depaint Chemistry

    DTIC Science & Technology

    2009-02-01

    continuous colored film by curing through solvent evaporation, oxidation, catylization or other means. – Vehicle: Film former, binder, resin or polymer...impart large changes in properties. – Suspending agents – Driers – Anti-Skinning Agents – Wetting Agents – Anti- Foaming Agents – Coalescing Agents ...volatile stripper inside the coating. Paint Release Agent Coating Removal Mechanism Zone1: PRA Layer Zone2: PRA Initial Permeation into coating system Epoxy

  11. Electron beams in research and technology

    NASA Astrophysics Data System (ADS)

    Mehnert, R.

    1995-11-01

    Fast electrons lose their energy by inelastic collisions with electrons of target molecules forming secondary electrons and excited molecules. Coulomb interaction of secondary electrons with valence electrons of neighboring molecules leads to the formation of radical cations, thermalized electrons, excited molecular states and radicals. The primary reactive species initiate chemical reactions in the materials irradiated. Polymer modifications using accelerated electrons such as cross-linking of cable insulation, tubes, pipes and moldings, vulcanization of elastomers, grafting of polymer surfaces, processing of foamed plastics and heat shrinkable materials have gained wide industrial acceptance. A steadily growing electron beam technology is curing of paints, lacquers, printing inks and functional coatings. Electron beam processing offers high productivity, the possibility to treat the materials at normal temperature and pressure, excellent process control and clean production conditions. On an industrial scale the most important application of fast electrons is curing of 100% reactive monomer/prepolymer systems. Mainly acrylates and epoxides are used to formulate functional coatings on substrates such as paper, foil, wood, fibre board and high pressure laminates. A survey is given about the reaction mechanism of curing, the characterization of cured coatings, and of some industrial application.

  12. Optimising Ambient Setting Bayer Derived Fly Ash Geopolymers

    PubMed Central

    Jamieson, Evan; Kealley, Catherine S.; van Riessen, Arie; Hart, Robert D.

    2016-01-01

    The Bayer process utilises high concentrations of caustic and elevated temperature to liberate alumina from bauxite, for the production of aluminium and other chemicals. Within Australia, this process results in 40 million tonnes of mineral residues (Red mud) each year. Over the same period, the energy production sector will produce 14 million tonnes of coal combustion products (Fly ash). Both industrial residues require impoundment storage, yet combining some of these components can produce geopolymers, an alternative to cement. Geopolymers derived from Bayer liquor and fly ash have been made successfully with a compressive strength in excess of 40 MPa after oven curing. However, any product from these industries would require large volume applications with robust operational conditions to maximise utilisation. To facilitate potential unconfined large-scale production, Bayer derived fly ash geopolymers have been optimised to achieve ambient curing. Fly ash from two different power stations have been successfully trialled showing the versatility of the Bayer liquor-ash combination for making geopolymers. PMID:28773513

  13. Optimising Ambient Setting Bayer Derived Fly Ash Geopolymers.

    PubMed

    Jamieson, Evan; Kealley, Catherine S; van Riessen, Arie; Hart, Robert D

    2016-05-19

    The Bayer process utilises high concentrations of caustic and elevated temperature to liberate alumina from bauxite, for the production of aluminium and other chemicals. Within Australia, this process results in 40 million tonnes of mineral residues (Red mud) each year. Over the same period, the energy production sector will produce 14 million tonnes of coal combustion products (Fly ash). Both industrial residues require impoundment storage, yet combining some of these components can produce geopolymers, an alternative to cement. Geopolymers derived from Bayer liquor and fly ash have been made successfully with a compressive strength in excess of 40 MPa after oven curing. However, any product from these industries would require large volume applications with robust operational conditions to maximise utilisation. To facilitate potential unconfined large-scale production, Bayer derived fly ash geopolymers have been optimised to achieve ambient curing. Fly ash from two different power stations have been successfully trialled showing the versatility of the Bayer liquor-ash combination for making geopolymers.

  14. Effect of basaltic pumice aggregate addition on the material properties of fly ash based lightweight geopolymer concrete

    NASA Astrophysics Data System (ADS)

    Top, Soner; Vapur, Hüseyin

    2018-07-01

    In this study, fly ash (FA) based geopolymer (GP) concretes were produced by using a mixture of basaltic pumice (BP) aggregates and a fly ash (Class F) for lightweight concrete production. ANOVA Yates' test technique was applied to find out the effective curing parameters. BP aggregates were ground four different fractions of particle sizes as -12 + 4 mm, -4+0.425 mm, -0.425 + 0 mm and the one containing the size distribution of Turkish Standard 802. Also, effects of the curing time in the oven were investigated. The uniaxial compressive strength (UCS) (20-55 MPa), the point load strength (4-14 kN), the water absorption (1.05%-17%), the Mohs hardness (5.5-3) and the sonic speed values (4.12-2.72 km/sn) were measured. Stress-strain curves were graphed. The density of the concrete ranged from 1700 kg/m3 to 1792 kg/m3 which confirm the lightweight concretes.

  15. The effect of filler addition and oven temperature to the antioxidant quality in the drying of Physalis angulata leaf extract obtained by subcritical water extraction

    NASA Astrophysics Data System (ADS)

    Susanti, R. F.; Natalia, Desy

    2016-11-01

    In traditional medicine, Physalis angulata which is well known as ceplukan in Indonesia, has been utilized to cure several diseases by conventional extraction in hot water. The investigation of the Swietenia mahagoni extract activity in modern medicine typically utilized organic solvents such as ethanol, methanol, chloroform and hexane in extraction. In this research, subcritical water was used as a solvent instead of organic solvent to extract the Pysalis angulata leaf part. The focus of this research was the investigation of extract drying condition in the presence of filler to preserve the quality of antioxidant in Swietenia mahagoni extract. Filler, which is inert, was added to the extract during drying to help absorb the water while protect the extract from exposure in heat during drying. The effects of filler types, concentrations and oven drying temperatures were investigated to the antioxidant quality covering total phenol and antioxidant activity. Aerosil and microcrystalline cellulose (MCC) were utilized as fillers with concentration was varied from 0-30 wt% for MCC and 0-15 wt% for aerosil. The oven drying temperature was varied from 40-60 oC. The results showed that compare to extract dried without filler, total phenol and antioxidant activity were improved upon addition of filler. The higher the concentration of filler, the better the antioxidant; however it was limited by the homogeneity of filler in the extract. Both of the variables (oven temperature and concentration) played an important role in the improvement of extract quality of Swietenia mahagoni leaf. It was related to the drying time which can be minimized to protect the deterioration of extract from heat. In addition, filler help to provide the powder form of extract instead of the typical extract form which is sticky and oily.

  16. 120 DEG C Cure, Durable, Corrosion Protection Powder Coatings for Temperature Sensitive Substrates

    DTIC Science & Technology

    2005-01-28

    Extrudate was passed through water-cooled pinch-rolls and collected onto a stainless steel belt; from exit of the extruder, approximately 60 sec... stainless steel belt; from exit of the extruder, approximately 60 sec. was required to reach ambient temperature. Production scale processing at...inherently free from volatile organic compounds, chromates, and hazardous air pollutants. Relative to the incumbent solvent-borne urethane paint

  17. KSC-08pd1968

    NASA Image and Video Library

    2008-07-14

    CAPE CANAVERAL, Fla. – In the tile shop at NASA's Kennedy Space Center, a Boeing Replacement Insulation 18, or BRI-18, tile bakes in a 2,200-degree oven to cure the ceramic coating. The baking is part of the process to prepare the tiles for installation on space shuttles. BRI-18 is the strongest material used for thermal insulation on the orbiters and, when coated to produce toughened unipiece fibrous insulation, provides a tile with extremely high-impact resistance. It is replacing other tiles on areas of the vehicle where impact risk is high, such as the landing gear doors, the wing leading edge and the external tank doors. Photo credit: NASA/Jim Grossmann

  18. Chemical composition and strength of dolomite geopolymer composites

    NASA Astrophysics Data System (ADS)

    Aizat, E. A.; Al Bakri, A. M. M.; Liew, Y. M.; Heah, C. Y.

    2017-09-01

    The chemical composition of dolomite and the compressive strength of dolomite geopolymer composites were studied. The both composites prepared with mechanical mixer manufactured by with rotor speed of 350 rpm and curing in the oven for 24 hours at 80˚C. XRF analysis showThe dolomite raw materials contain fewer amounts of Si and Al but high Ca in its composition. Dolomite geopolymer composites with 20M of NaOH shows greater and optimum compressive strength compared to dolomite geopolymer with other NaOH molarity. This indicated better interaction of dolomite raw material and alkaline activator need high molarity of NaOH in order to increase the reactivity of dolomite.

  19. KSC-08pd1966

    NASA Image and Video Library

    2008-07-14

    CAPE CANAVERAL, Fla. – In the tile shop at NASA's Kennedy Space Center, a worker places a Boeing Replacement Insulation 18, or BRI-18, tile in the oven. The tile will be baked at 2,200 degrees Fahrenheit to cure the ceramic coating, part of the process to prepare the tiles for installation on space shuttles. BRI-18 is the strongest material used for thermal insulation on the orbiters and, when coated to produce toughened unipiece fibrous insulation, provides a tile with extremely high-impact resistance. It is replacing other tiles on areas of the vehicle where impact risk is high, such as the landing gear doors, the wing leading edge and the external tank doors. Photo credit: NASA/Jim Grossmann

  20. Characterization of cobalt(II) chloride-modified condensation polyimide films

    NASA Technical Reports Server (NTRS)

    Rancourt, J. D.; Taylor, L. T.

    1988-01-01

    The effect of solvent extraction on the properties of cobalt(II) chloride-modified polyimide films was investigated. Solvent-cast films were prepared from solutions of cobalt chloride in poly(amide acid)/N,N-dimethylacetamide (DMAc) and were subsequently dried and cured in static air, forced air, or inert gas ovens with controlled humidity. The films were extracted by either of the three processes (1) soaking in a tray with distilled water at room temperature, (2) soxhlett extraction with distilled water, or (3) soxhell extraction with DMAc. Extraction with DMAc was found to remove both cobalt and chlorine from the films and to slightly increase bulk thermal stability and both surface resistivity and electrical resistivity.

  1. Simultaneous acoustic and dielectric real time curing monitoring of epoxy systems

    NASA Astrophysics Data System (ADS)

    Gkikas, G.; Saganas, Ch.; Grammatikos, S. A.; Aggelis, D. G.; Paipetis, A. S.

    2012-04-01

    The attainment of structural integrity of the reinforcing matrix in composite materials is of primary importance for the final properties of the composite structure. The detailed monitoring of the curing process on the other hand is paramount (i) in defining the optimal conditions for the impregnation of the reinforcement by the matrix (ii) in limiting the effects of the exotherm produced by the polymerization reaction which create unwanted thermal stresses and (iii) in securing optimal behavior in matrix controlled properties, such as off axis or shear properties and in general the durability of the composite. Dielectric curing monitoring is a well known technique for distinguishing between the different stages of the polymerization of a typical epoxy system. The technique successfully predicts the gelation and the vitrification of the epoxy and has been extended for the monitoring of prepregs. Recent work has shown that distinct changes in the properties of the propagated sound in the epoxy which undergoes polymerization is as well directly related to the gelation and vitrification of the resin, as well as to the attainment of the final properties of the resin system. In this work, a typical epoxy is simultaneously monitored using acoustic and dielectric methods. The system is isothermally cured in an oven to avoid effects from the polymerization exotherm. Typical broadband sensors are employed for the acoustic monitoring, while flat interdigital sensors are employed for the dielectric scans. All stages of the polymerization process were successfully monitored and the validity of both methods was cross checked and verified.

  2. Combined different dehydration pretreatments and torrefaction to upgrade fuel properties of hybrid pennisetum (Pennisetum americanum ×P. purpureum).

    PubMed

    Yu, Yan; Wang, Guanghui; Bai, Xiaopeng; Liu, Jude; Wang, Decheng; Wang, Zhiqin

    2018-05-16

    Different dehydrating methods combined with torrefaction were investigated to find the underlying mechanism that how dehydration process influence the degree of hornification. Hybrid pennisetum was selected as the experiment material. Oven-dried sample (ODS), crushed dried sample (CDS), and sun-cured dried sample (SDS) were torrefied under the temperature of 275 °C and 300 °C with the duration time of 60 min. The results showed that, changes in elevated carbon content and higher heating value (HHV) and reduced oxygen content of SDS were the most obvious under identical torrefaction conditions. Fuel ratio of SDS was enhanced most under 300 °C. It also had the highest devolatilization index (D i ). The combination of sun-cured dried with torrefaction under 300 °C caused lowest degree of irreversible hornification happened during dehydrating process, and different hornification degrees caused by different dehydrating methods effect the enhancement of fuel properties of lignocellulosic biomass material. Copyright © 2018 Elsevier Ltd. All rights reserved.

  3. Comparison of the Effect of Curing on the Properties of E-Glass/Cyanate modified Epoxy Cross Plied Laminates

    NASA Astrophysics Data System (ADS)

    Nallayan, W. Andrew; Vijayakumar, K. R.; Rasheed, Usama Tariq

    2017-05-01

    High performance polymer composite laminates that are used in Aerospace and Electronics industries requires laminates that are structurally rigid besides exhibiting high stiffness and good di electrical properties. They are required to be transparent to EM waves in order to transmit the signal with almost zero transmission loss. Response of the laminates under different loadings could hence establish a potent material combination with high structural strengths that could be used in sectors dealing with Signal transmissions. The results thus acquired can be used as a database for choosing relatively better materials for Radome and their advanced versions in the coming decades. To augment this, thin laminates with 4 plies with simple stacking configurations of 0/90/0/90 degrees as applicable to a cross plied laminates were fabricated with cyanate ester modified epoxy resin and 1200GSM E glass unidirectional fiber. Flexural and Impact strength were the properties identified for the accessing the structural responses of the Laminate as against room and oven curing conditions. FESEM images were applied to validate the experimental findings.

  4. Blackbody for metrological control of ear thermometers

    NASA Astrophysics Data System (ADS)

    Cárdenas-García, D.; Méndez-Lango, E.

    2013-09-01

    Body temperature is an important parameter in medical practice, and most of health diagnoses are made based upon measured temperature values. Non-contact measurements are attractive to both patients and physicians, and ear thermometers (ET) are part of the set of infrared thermometers for medical applications. ETs sense the tympanic membrane temperature which best represents body temperature. They take advantage of the natural high effective emissivity cavity that is formed as radiation source. To calibrate or to check the performance of ETs, we designed a high-emissivity spherical cavity as a blackbody source which can be placed in a dry block oven. Although the blackbody cavity can have any shape, we decided to build it spherical because its effective emissivity can be easily calculated in a closed form. The cavity is made of Aluminum to take advantage of its high thermal conductivity while its inner side is covered with a black paint to increase the cavity effective emissivity. Based on paint emissivity measurements and the geometrical shape, we calculated that the cavity has an effective emissivity higher than 0.999. Blackbody temperature is measured with a calibrated contact thermometer placed inside the bottom wall of the cavity. We present the design of the cavity, the experimental setup, and results of three commercial ETs compared with this cavity.

  5. Copper resinate: preparation, characterisation and study of degradation.

    PubMed

    Colombini, M P; Lanterna, G; Mairani, A; Matteini, M; Modugno, F; Rizzi, M

    2001-01-01

    This paper describes a method for the synthesis of Copper Resinate, which disappeared from artists' palettes in the eighteenth century. This was carried out by interpreting ancient recipes following a scientific approach. Its characterisation using Fourier Transform-Infrared Spectrometry and Gas Chromatography-Mass Spectrometry demonstrated that it is a mixture containing copper and oxidised abietic acids, mainly dehydroabietic and 7-oxo-dehydroabietic acids, formed during the preparation of the pigment and the curing of the paint layer. The composition of copper resinate paint layers, artificially aged by U.V. irradiation at 365 nm (UV), heating (T), and exposed to atmospheric pollutants (NOX) in a climatic chamber, was investigated. The combination of irradiation and temperature produced a change in colour along with a significant increase in the recovered amount of 7-oxo-dehydroabietic acid. The identification of copper resinate in a sample from an old painting should be related to the presence of the following resin compounds which are stable in the ageing process: dehydroabietic and 7-oxo-dehydroabietic acid pimaradienic acids. Photo-oxidation of the resin acids co-ordinated with copper seem to be the most probable decay mechanism responsible for the colour change in the pigment.

  6. Migration of DEHP and DINP into dust from PVC flooring products at different surface temperature.

    PubMed

    Jeon, Seunghwan; Kim, Ki-Tae; Choi, Kyungho

    2016-03-15

    Phthalates are important endocrine disrupting chemicals that have been linked to various adverse human health effects. Phthalates are ubiquitously present in indoor environment and could enter humans. Vinyl or PVC floorings have been recognized as one of important sources of phthalate release to indoor environment including house dust. In the present study, we estimated the migration of di(2-ethylhexyl)phthalate (DEHP) and di-isononyl phthalate (DINP) from the flooring materials into the dust under different heating conditions. For this purpose, a small chamber specifically designed for the present study and a Field and Laboratory Emission Cell (FLEC) were used, and four major types of PVC flooring samples including two UV curing paint coated, an uncoated residential, and a wax-coated commercial type were tested. Migration of DEHP was observed for an uncoated residential type and a wax-coated commercial type flooring. After 14 days of incubation, the levels of DEHP in the dust sample was determined at room temperature on average (standard deviation) at 384 ± 19 and 481 ± 53 μg/g, respectively. In contrast, migration of DINP was not observed. The migration of DEHP was strongly influenced by surface characteristics such as UV curing coating. In the residential flooring coated with UV curing paint, migration of DEHP was not observed at room temperature. But under the heated condition, the release of DEHP was observed in the dust in the FLEC. Migration of DEHP from flooring materials increased when the flooring was heated (50 °C). In Korea, heated flooring system, or 'ondol', is very common mode of heating in residential setting, therefore the contribution of PVC flooring to the total indoor DEHP exposure among general population is expected to be greater especially during winter season when the floor is heated. Copyright © 2015 Elsevier B.V. All rights reserved.

  7. KSC-08pd1967

    NASA Image and Video Library

    2008-07-14

    CAPE CANAVERAL, Fla. – In the tile shop at NASA's Kennedy Space Center, a worker reaches for the door to close the oven with the Boeing Replacement Insulation 18, or BRI-18, tile inside. The tile will be baked at 2,200 degrees Fahrenheit to cure the ceramic coating, part of the process to prepare the tiles for installation on space shuttles. BRI-18 is the strongest material used for thermal insulation on the orbiters and, when coated to produce toughened unipiece fibrous insulation, provides a tile with extremely high-impact resistance. It is replacing other tiles on areas of the vehicle where impact risk is high, such as the landing gear doors, the wing leading edge and the external tank doors. Photo credit: NASA/Jim Grossmann

  8. KSC-08pd1965

    NASA Image and Video Library

    2008-07-14

    CAPE CANAVERAL, Fla. – In the tile shop at NASA's Kennedy Space Center, a worker is ready to place a Boeing Replacement Insulation 18, or BRI-18, tile in the oven. The tile will be baked at 2,200 degrees Fahrenheit to cure the ceramic coating, part of the process to prepare the tiles for installation on space shuttles. BRI-18 is the strongest material used for thermal insulation on the orbiters and, when coated to produce toughened unipiece fibrous insulation, provides a tile with extremely high-impact resistance. It is replacing other tiles on areas of the vehicle where impact risk is high, such as the landing gear doors, the wing leading edge and the external tank doors. Photo credit: NASA/Jim Grossmann

  9. Competitive position of natural gas: Industrial baking

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Minsker, B.S.; Salama, S.Y.

    Industrial baking is one of the largest natural gas consumers in the food industry. In 1985, bread, rolls, cookies, and crackers accounted for over 82 percent of all baked goods production. Bread accounting for 46 percent of all production. The baking industry consumed approximately 16 trillion Btu in 1985. About 93 percent was natural gas, while distillate fuel oil accounted for seven percent, and electricity accounted for much less than one percent. The three main types of baking ovens are the single lap, tunnel, and Lanham ovens. In the single lap oven, trays carry the product back and forth throughmore » the baking chamber once. The single lap oven is the most common type of oven and is popular due to its long horizontal runs, extensive steam zone, and simple construction. The tunnel oven is slightly more efficient and more expensive that the single lap oven. IN the tunnel oven, the hearth is a motorized conveyor which passes in a straight line through a series of heating zones, with loading and unloading occurring at opposite ends of the oven. The advantages of the tunnel oven include flexibility with respect to pan size and simple, accurate top and bottom heat control. The tunnel oven is used exclusively in the cookie and cracker baking, with the product being deposited directly on the oven band. The most recently developed type of oven is the Lanham oven. The Lanham oven is the most efficient type of oven, with a per pound energy consumption approaching the practical minimum for baking bread. Between one--half and two--thirds of all new industrial baking ovens are Lanham ovens. In the Lanham oven, the product enters the oven near the top of the chamber, spirals down through a series of heating zones, and exits near the bottom of the oven. The oven is gas--fired directly by ribbon burners. 31 refs.« less

  10. 10 CFR 429.23 - Conventional cooking tops, conventional ovens, microwave ovens.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 3 2013-01-01 2013-01-01 false Conventional cooking tops, conventional ovens, microwave... Conventional cooking tops, conventional ovens, microwave ovens. (a) Sampling plan for selection of units for... and microwave ovens; and (2) For each basic model of conventional cooking tops, conventional ovens and...

  11. 10 CFR 429.23 - Conventional cooking tops, conventional ovens, microwave ovens.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 3 2014-01-01 2014-01-01 false Conventional cooking tops, conventional ovens, microwave... Conventional cooking tops, conventional ovens, microwave ovens. (a) Sampling plan for selection of units for... and microwave ovens; and (2) For each basic model of conventional cooking tops, conventional ovens and...

  12. 10 CFR 429.23 - Conventional cooking tops, conventional ovens, microwave ovens.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 10 Energy 3 2012-01-01 2012-01-01 false Conventional cooking tops, conventional ovens, microwave... Conventional cooking tops, conventional ovens, microwave ovens. (a) Sampling plan for selection of units for... and microwave ovens; and (2) For each basic model of conventional cooking tops, conventional ovens and...

  13. Acoustic emission analysis of fiber-reinforced composite in flexural testing.

    PubMed

    Alander, Pasi; Lassila, Lippo V J; Tezvergil, Arzu; Vallittu, Pekka K

    2004-05-01

    The aim of this study was to examine the emission of acoustic signals from six commercially available fiber-reinforced composites (FRC) used in the frameworks of fixed partial dentures in material bending. FRC test specimens were made of six commercially available fiber products of polyethylene or glass and five light-curing resins. FRC test specimens were polymerized with a hand light-curing unit or with a light-curing oven. The flexural test for determination of ultimate flexural strength of test specimens (n = 6) was based on the ISO 10477 standard after the specimens were stored in air or in water for two weeks. The acoustic emission (AE) signals were monitored during three-point loading test of the test specimens using a test with increasing loading levels until the specimens fractured. Generally, stress level required for the AE activity initiation ranged from 107 MPa (Ribbond) to 579 MPa (everStick). The ultimate flexural strength of FRC specimens were higher, ranging from 132 to 764 MPa, being highest with everStick and Vectris FRC, and lowest with Ribbond FRC. ANOVA showed a statistically significant difference between the initiation of AE activity and the ultimate flexural strength according to the brand (p < 0.001) storing conditions (p < 0.001) and polymerization procedure (p < 0.001). AE activity and ultimate flexural strength correlated significantly (p < 0.010, r = 0.887). The result of this study suggested that AE activity in FRC specimens started at a 19-32% lower stress level than occurred at final fracture.

  14. Research in Foundation Grouting with Cement

    DTIC Science & Technology

    1960-03-01

    grout is mixed. 2. For cracks of the order of 0.05 in., a grout in which the ratio[ of water to cement is 0.75 by volune gives the r’ost desirable 4... thickness of the order of t5 in. 4. 3hear tests on grout films fog-cured at 70 F for 28 days denon- stratel that increasing the pressure within the...alkaline water dripre.I through cracks in the concrete lidng of some of the penstock tunnels Jai daaged the paint an- metal -work. The uplift pressure

  15. Elevated Temperature, Residual Compressive Strength of Impact-Damaged Sandwich Structure Manufactured Out-of-Autoclave

    NASA Technical Reports Server (NTRS)

    Grimsley, Brian W.; Sutter, James K.; Burke, Eric R.; Dixon, Genevieve D.; Gyekenyesi, Thomas G.; Smeltzer, Stanley S.

    2012-01-01

    Several 1/16th-scale curved sandwich composite panel sections of a 10 m diameter barrel were fabricated to demonstrate the manufacturability of large-scale curved sections using minimum gauge, [+60/-60/0]s, toughened epoxy composite facesheets co-cured with low density (50 kilograms per cubic meters) aluminum honeycomb core. One of these panels was fabricated out of autoclave (OoA) by the vacuum bag oven (VBO) process using Cycom(Registered Trademark) T40-800b/5320-1 prepreg system while another panel with the same lay-up and dimensions was fabricated using the autoclave-cure, toughened epoxy prepreg system Cycom(Registered Trademark) IM7/977-3. The resulting 2.44 m x 2 m curved panels were investigated by non-destructive evaluation (NDE) at NASA Langley Research Center (NASA LaRC) to determine initial fabrication quality and then cut into smaller coupons for elevated temperature wet (ETW) mechanical property characterization. Mechanical property characterization of the sandwich coupons was conducted including edge-wise compression (EWC), and compression-after-impact (CAI) at conditions ranging from 25 C/dry to 150 C/wet. The details and results of this characterization effort are presented in this paper.

  16. Epilepsy through the ages: An artistic point of view.

    PubMed

    Ladino, Lady Diana; Rizvi, Syed; Téllez-Zenteno, Jose Francisco

    2016-04-01

    The historical allure of epilepsy transcends academic circles and serves as fascinating critique of the state of the times-its values, judgments, mythos, and people. Immortalized and laid bare in artistic renderings of epilepsy are societal truths, at times both disparately grandiose and grotesque. During the middle ages and Renaissance, the European discourse on epilepsy assumed religious fervor. Epilepsy was considered a demonic machination and its cure an act of divine intercession. A similar theme is found in the artistic depiction of epilepsy from the Inca and Aztec civilizations of that time. After the 19th century drew to a close, the ascendency of empiricism coincided with waning creative interest in epilepsy, with few paintings or pieces to capture insightful perspectives on the illness. In this paper, we review the relationship between art and epilepsy and present two contemporary paintings that convey current western perceptions. This article is part of a Special Issue entitled "Epilepsy, Art, and Creativity". Copyright © 2016 Elsevier Inc. All rights reserved.

  17. 78 FR 7939 - Energy Conservation Program: Test Procedures for Microwave Ovens (Active Mode)

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-02-04

    ...The U.S. Department of Energy (DOE) proposes to revise its test procedures for microwave ovens established under the Energy Policy and Conservation Act. The proposed amendments would add provisions for measuring the active mode energy use for microwave ovens, including both microwave-only ovens and convection microwave ovens. Specifically, DOE is proposing provisions for measuring the energy use of the microwave-only cooking mode for both microwave-only ovens and convection microwave ovens based on the testing methods in the latest draft version of the International Electrotechnical Commission Standard 60705, ``Household microwave ovens--Methods for measuring performance.'' DOE is proposing provisions for measuring the energy use of the convection-only cooking mode for convection microwave ovens based on the DOE test procedure for conventional ovens in our regulations. DOE is also proposing to calculate the energy use of the convection-microwave cooking mode for convection microwave ovens by apportioning the microwave-only mode and convection-only mode energy consumption measurements based on typical consumer use.

  18. 40 CFR 63.3165 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... purposes of this subpart, a bake oven air seal is not considered a natural draft opening in a PTE or a... between the bake oven air seal and the bake oven is into the bake oven. You may use lightweight strips of... as a natural draft opening. You cannot count air flowing from a bake oven air seal into a bake oven...

  19. Physical optics for oven-plate scattering prediction

    NASA Technical Reports Server (NTRS)

    Baldauf, J.; Lambert, K.

    1991-01-01

    An oven assembly design is described, which will be used to determine the effects of temperature on the electrical properties of materials which are used as coatings for metal plates. Experimentally, these plates will be heated to a very high temperature in the oven assembly, and measured using a microwave reflectance measurement system developed for the NASA Lewis Research Center, Near-Field Facility. One unknown in this measurement is the effect that the oven assembly will have on the reflectance properties of the plate. Since the oven will be much larger than the plate, the effect could potentially be significant as the size of the plate becomes smaller. Therefore, it is necessary to predict the effect of the oven on the measurement of the plate. A method for predicting the oven effect is described, and the theoretical oven effect is compared to experimental results of the oven material. The computer code which is used to predict the oven effect is also described.

  20. Effect of oven cooking method on formation of heterocyclic amines and quality characteristics of chicken patties: steam-assisted hybrid oven versus convection ovens.

    PubMed

    Isleroglu, Hilal; Kemerli, Tansel; Özdestan, Özgül; Uren, Ali; Kaymak-Ertekin, Figen

    2014-09-01

    The aim of this study was to evaluate effect of steam-assisted hybrid oven cooking method in comparison with convection ovens (natural and forced) on quality characteristics (color, hardness, cooking loss, soluble protein content, fat retention, and formation of heterocyclic aromatic amines) of chicken patties. The cooking experiments of chicken patties (n = 648) were conducted at oven temperatures of 180, 210, and 240°C until 3 different end point temperatures (75, 90, and 100°C) were reached. Steam-assisted hybrid oven cooking enabled faster cooking than convection ovens and resulted in chicken patties having lower a* and higher L* value, lower hardness, lower fat, and soluble protein content (P < 0.05), and higher cooking loss than convection ovens. Steam-assisted hybrid oven could reduce the formation of heterocyclic aromatic amines that have mutagenic and carcinogenic effects on humans. © 2014 Poultry Science Association Inc.

  1. 40 CFR 63.302 - Standards for by-product coke oven batteries.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... batteries. 63.302 Section 63.302 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.302 Standards for by-product coke oven batteries... oven emissions from each affected existing by-product coke oven battery that exceed any of the...

  2. 40 CFR 63.302 - Standards for by-product coke oven batteries.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... batteries. 63.302 Section 63.302 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.302 Standards for by-product coke oven batteries... oven emissions from each affected existing by-product coke oven battery that exceed any of the...

  3. 40 CFR 63.302 - Standards for by-product coke oven batteries.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... batteries. 63.302 Section 63.302 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.302 Standards for by-product coke oven batteries... oven emissions from each affected existing by-product coke oven battery that exceed any of the...

  4. 40 CFR 63.302 - Standards for by-product coke oven batteries.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... batteries. 63.302 Section 63.302 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.302 Standards for by-product coke oven batteries... oven emissions from each affected existing by-product coke oven battery that exceed any of the...

  5. 40 CFR 63.302 - Standards for by-product coke oven batteries.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... batteries. 63.302 Section 63.302 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.302 Standards for by-product coke oven batteries... oven emissions from each affected existing by-product coke oven battery that exceed any of the...

  6. Products cooked in preheated versus non-preheated ovens. Baking times, calculated energy consumption, and product quality compared.

    PubMed

    Odland, D; Davis, C

    1982-08-01

    Plain muffins, yellow cake, baked custard, apple pie, tuna casserole, frozen tuna casserole, cheese soufflé, and meat loaf were baked in preheated and non-preheated standard gas, continuous-clean gas, standard electric, and self-cleaning electric ovens. Products generally required 5 min. or less extra baking time when cooked in non-preheated rather than in preheated ovens. The variability in baking times often was less between preheated and non-preheated ovens than among oven types. Calculated energy consumption values showed that usually less energy was required to bake products in non-preheated than in preheated ovens; savings averaged about 10 percent. Few significant differences were found in physical measurements or eating quality either between preheated and non-preheated ovens or among oven types. Overall, for the products tested, findings confirmed that preheating the oven is not essential for good product quality and, therefore, is an unnecessary use of energy.

  7. Processing and properties of carbon nanofibers reinforced epoxy powder composites

    NASA Astrophysics Data System (ADS)

    Palencia, C.; Mazo, M. A.; Nistal, A.; Rubio, F.; Rubio, J.; Oteo, J. L.

    2011-11-01

    Commercially available CNFs (diameter 30-300 nm) have been used to develop both bulk and coating epoxy nanocomposites by using a solvent-free epoxy matrix powder. Processing of both types of materials has been carried out by a double-step process consisting in an initial physical premix of all components followed by three consecutive extrusions. The extruded pellets were grinded into powder and sieved. Carbon nanofibers powder coatings were obtained by electrostatic painting of the extruded powder followed by a curing process based in a thermal treatment at 200 °C for 25 min. On the other hand, for obtaining bulk carbon nanofibers epoxy composites, a thermal curing process involving several steps was needed. Gloss and mechanical properties of both nanocomposite coatings and bulk nanocomposites were improved as a result of the processing process. FE-SEM fracture surface microphotographs corroborate these results. It has been assessed the key role played by the dispersion of CNFs in the matrix, and the highly important step that is the processing and curing of the nanocomposites. A processing stage consisted in three consecutive extrusions has reached to nanocomposites free of entanglements neither agglomerates. This process leads to nanocomposite coatings of enhanced properties, as it has been evidenced through gloss and mechanical properties. A dispersion limit of 1% has been determined for the studied system in which a given dispersion has been achieved, as the bending mechanical properties have been increased around 25% compared with the pristine epoxy resin. It has been also demonstrated the importance of the thickness in the nanocomposite, as it involves the curing stage. The complex curing treatment carried out in the case of bulk nanocomposites has reached to reagglomeration of CNFs.

  8. [Influence of coke oven emissions on workers' blood pressure and electrocardiographic findings].

    PubMed

    Liang, J J; Yi, G L; Mao, G S; Wang, D M; Dai, X Y

    2016-09-20

    Objective: To investigate the influence of coke oven emissions on workers' blood pressure and electrocardiographic findings, and to provide a basis for the prevention and treatment of cardiovascular diseases. Methods: The concentration of coke oven emissions at the bottom, side, and top of coke ovens was determined in a coking plant. A total of 406 coke oven workers were enrolled as exposure group and 201 office staff members were enrolled as control group. Blood pressure and electrocardiographic findings were compared between the two groups, and the multivariate logistic regression analysis was performed to analyze the influencing factors for hypertension and abnormal electrocardiographic findings. Results: The concentration of coke oven emissions was the highest at the top of coke ovens, followed by the side and bottom of coke ovens, and there was a significant difference between the exposure group and the control group ( P <0.01). The exposure group had significantly higher detection rates of hypertension, abnormal electrocardiographic findings, and abnormal chest X-ray findings than the control group ( P <0.05). The logistic regression analysis showed that high concentration of coke oven emission and age were risk factors for hypertension and abnormal electrocardiographic findings ( P <0.05). The workers exposed to high-concentration coke oven emissions were more likely to experience hypertension and abnormal electrocardiographic findings than those exposed to low-concentration coke oven emissions ( OR =1.7 and 1.9). Conclusion: Besides lung injury, coke oven emissions also have adverse effects on the cardiovascular system. Therefore, more effective measures are needed to protect the health of coke oven workers.

  9. Design and development of pressure and repressurization purge system for reusable space shuttle multilayer insulation system

    NASA Technical Reports Server (NTRS)

    1972-01-01

    The experimental determination of purge bag materials properties, development of purge bag manufacturing techniques, experimental evaluation of a subscale purge bag under simulated operating conditions and the experimental evaluation of the purge pin concept for MLI purging are discussed. The basic purge bag material, epoxy fiberglass bounded by skins of FEP Teflon, showed no significant permeability to helium flow under normal operating conditions. Purge bag small scale manufacturing tests were conducted to develop tooling and fabrication techniques for use in full scale bag manufacture. A purge bag material layup technique was developed whereby the two plys of epoxy fiberglass enclosed between skins of FEP Teflon are vacuum bag cured in an oven in a single operation. The material is cured on a tool with the shape of a purge bag half. Plastic tooling was selected for use in bag fabrication. A model purge bag 0.6 m in diameter was fabricated and subjected to a series of structural and environmental tests simulating various flight type environments. Pressure cycling tests at high (450 K) and low (200 K) temperature as well as acoustic loading tests were performed. The purge bag concept proved to be structurally sound and was used for the full scale bag detailed design model.

  10. Corrosion-Control (CC) Program: Pilot Powder Coating Station Service Test.

    DTIC Science & Technology

    1986-03-14

    o CL oU C4 CL00 z ;,S Go 0 m~ CL - C9 uj4 U..~D o . ZC.F Go zz 2 0 I- - c t < m U, cc V V4 cg c ~ D GD...Spray Booth# Curing Oven and A2-58 UNIT TOTAL is_18 A2-1 1WOW - o 0 -1 Q S re. 10 U c Z. 2E E. a.E 8 tE 20 4AU ==- %A a 4 $AO - Lo 48 0 w 0 -IL .. 0.... 0...Laa 00 3-r Q’ IA E zo 0..0 -< 4o C a) Ia - o x c bi. l c *4 ’a a~~* coLo. 0V Ua- 41 w - a V 2 2 .8 h A a U to bo co i ac

  11. Protective Skins for Aerogel Monoliths

    NASA Technical Reports Server (NTRS)

    Leventis, Nicholas; Johnston, James C.; Kuczmarski, Maria A.; Meador, Ann B.

    2007-01-01

    A method of imparting relatively hard protective outer skins to aerogel monoliths has been developed. Even more than aerogel beads, aerogel monoliths are attractive as thermal-insulation materials, but the commercial utilization of aerogel monoliths in thermal-insulation panels has been inhibited by their fragility and the consequent difficulty of handling them. Therefore, there is a need to afford sufficient protection to aerogel monoliths to facilitate handling, without compromising the attractive bulk properties (low density, high porosity, low thermal conductivity, high surface area, and low permittivity) of aerogel materials. The present method was devised to satisfy this need. The essence of the present method is to coat an aerogel monolith with an outer polymeric skin, by painting or spraying. Apparently, the reason spraying and painting were not attempted until now is that it is well known in the aerogel industry that aerogels collapse in contact with liquids. In the present method, one prevents such collapse through the proper choice of coating liquid and process conditions: In particular, one uses a viscous polymer precursor liquid and (a) carefully controls the amount of liquid applied and/or (b) causes the liquid to become cured to the desired hard polymeric layer rapidly enough that there is not sufficient time for the liquid to percolate into the aerogel bulk. The method has been demonstrated by use of isocyanates, which, upon exposure to atmospheric moisture, become cured to polyurethane/polyurea-type coats. The method has also been demonstrated by use of commercial epoxy resins. The method could also be implemented by use of a variety of other resins, including polyimide precursors (for forming high-temperature-resistant protective skins) or perfluorinated monomers (for forming coats that impart hydrophobicity and some increase in strength).

  12. Validation of a combi oven cooking method for preparation of chicken breast meat for quality assessment.

    PubMed

    Zhuang, H; Savage, E M

    2008-10-01

    Quality assessment results of cooked meat can be significantly affected by sample preparation with different cooking techniques. A combi oven is a relatively new cooking technique in the U.S. market. However, there was a lack of published data about its effect on quality measurements of chicken meat. Broiler breast fillets deboned at 24-h postmortem were cooked with one of the 3 methods to the core temperature of 80 degrees C. Cooking methods were evaluated based on cooking operation requirements, sensory profiles, Warner-Bratzler (WB) shear and cooking loss. Our results show that the average cooking time for the combi oven was 17 min compared with 31 min for the commercial oven method and 16 min for the hot water method. The combi oven did not result in a significant difference in the WB shear force values, although the cooking loss of the combi oven samples was significantly lower than the commercial oven and hot water samples. Sensory profiles of the combi oven samples did not significantly differ from those of the commercial oven and hot water samples. These results demonstrate that combi oven cooking did not significantly affect sensory profiles and WB shear force measurements of chicken breast muscle compared to the other 2 cooking methods. The combi oven method appears to be an acceptable alternative for preparing chicken breast fillets in a quality assessment.

  13. 19. VIEW OF THE TWO ROWS OF COKE OVENS, LOOKING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    19. VIEW OF THE TWO ROWS OF COKE OVENS, LOOKING EAST. THE OVENS LIE TO THE EAST OF THE MINE BUILDINGS. BEEHIVE OVENS FORM THE ROW ON THE LEFT OF THE PHOTOGRAPH. THE RECTANGULAR OVENS ARE ON THE RIGHT. - Tower Hill No. 2 Mine, Approximately 0.47 mile Southwest of intersection of Stone Church Road & Township Route 561, Hibbs, Fayette County, PA

  14. 40 CFR 63.3165 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    .... For purposes of this subpart, a bake oven air seal is not considered a natural draft opening in a PTE... interface between the bake oven air seal and the bake oven is into the bake oven. You may use lightweight... air seal as a natural draft opening. You cannot count air flowing from a bake oven air seal into a...

  15. 40 CFR 63.3165 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    .... For purposes of this subpart, a bake oven air seal is not considered a natural draft opening in a PTE... interface between the bake oven air seal and the bake oven is into the bake oven. You may use lightweight... air seal as a natural draft opening. You cannot count air flowing from a bake oven air seal into a...

  16. Optimization of combined microwave-hot air roasting of malt based on energy consumption and neo-formed contaminants content.

    PubMed

    Akkarachaneeyakorn, S; Laguerre, J C; Tattiyakul, J; Neugnot, B; Boivin, P; Morales, F J; Birlouez-Aragon, I

    2010-05-01

    To produce specialty malt, malts were roasted by combined microwave-hot air at various specific microwave powers (SP = 2.5 to 3 W/g), microwave heating times (t(mw) = 3.3 to 3.5 min), oven temperatures (T(oven) = 180 to 220 degrees C), and oven heating times (t(oven) = 60 to 150 min). The response variables, color, energy consumption by microwave (E(mw)) and oven (E(oven)), total energy consumption (E(tot)), quantity of neo-formed contaminants (NFCs), which include hydroxymethylfurfural, furfural, furan, and acrylamide were determined. Response surface methodology (RSM) was performed to analyze and predict the optimum conditions for the specialty malt. Production using combined microwave-hot air roasting process based on minimum energy consumption and level of NFCs. At 95% confident level, SP, T(oven), and t(oven) were the most influencing effects with regard to E(tot), whereas t(mw) did not affect E(tot). T(oven) and t(oven) significantly affected malt color. Only T(oven) significantly influenced the NFCs content. The optimum parameters were: SP = 2.68 W/g for 3.44 min, T(oven) = 206 degrees C for 136 min for coffee malt, SP = 2.5 W/g for 3.48 min, T(oven) = 214 degrees C for 136 min for chocolate malt, and SP = 2.5 W/g for 3.48 min, T(oven) = 211 degrees C for 150 min for black malt. Comparing with conventional process, combined microwave-hot air reduced E(tot) by approximately 40%, 26%, and 26% for coffee, chocolate, and black malts, respectively, and reduced HMF, furfural, furan, and acrylamide contents by 40%, 18%, 23%, and 95%, respectively, for black malt. An important goal for research institutions and the brewery industry is to produce colored malt by combining microwave and hot air roasting, while saving energy, getting desirable color, and avoiding the formation of carcinogenic and toxic neo-formed contaminants (NFCs). Therefore, one objective of this study was to compare energy consumption and content of NFCs during roasting of malt by hot air-only and combined microwave-hot air processes as well as to determine the effect of specific power, microwave processing time, oven temperature, and oven processing time during combined microwave-hot air roasting. Another objective was to predict the optimum conditions for the production of coffee, chocolate, and black malts.

  17. 40 CFR 63.303 - Standards for nonrecovery coke oven batteries.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... batteries. 63.303 Section 63.303 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.303 Standards for nonrecovery coke oven batteries... existing nonrecovery coke oven battery that exceed any of the following emission limitations or...

  18. 40 CFR 63.303 - Standards for nonrecovery coke oven batteries.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... batteries. 63.303 Section 63.303 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.303 Standards for nonrecovery coke oven batteries... existing nonrecovery coke oven battery that exceed any of the following emission limitations or...

  19. 40 CFR 63.303 - Standards for nonrecovery coke oven batteries.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... batteries. 63.303 Section 63.303 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.303 Standards for nonrecovery coke oven batteries... existing nonrecovery coke oven battery that exceed any of the following emission limitations or...

  20. 40 CFR 63.303 - Standards for nonrecovery coke oven batteries.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... batteries. 63.303 Section 63.303 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.303 Standards for nonrecovery coke oven batteries... existing nonrecovery coke oven battery that exceed any of the following emission limitations or...

  1. 40 CFR 63.303 - Standards for nonrecovery coke oven batteries.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... batteries. 63.303 Section 63.303 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR... National Emission Standards for Coke Oven Batteries § 63.303 Standards for nonrecovery coke oven batteries... existing nonrecovery coke oven battery that exceed any of the following emission limitations or...

  2. Biomarkers of polycyclic aromatic hydrocarbon exposure in European coke oven workers.

    PubMed

    Talaska, Glenn; Thoroman, Jeff; Schuman, Brenda; Käfferlein, Heiko Udo

    2014-12-01

    Biomonitoring is an excellent method for capturing the results of all exposures, regardless of route. Coke oven workers include certain groups that have the potential for high exposure to polycyclic aromatic hydrocarbons (PAH) and other materials. Biomarkers of exposure to these agents include PAH metabolites as markers of internal dose and carcinogen-DNA adducts as measure of effective dose. The purpose of this study was to determine the levels of these biomarkers in persons with different job duties in a modern coke oven plant. We report that the mean levels of 1-hydroxypyrene (1HP) and carcinogen DNA adducts in the exfoliated urothelial cells of coke oven workers are increased the closer a group of workers is to the ovens and highest in the top oven workers with average 1HP level of 11.6 μg/l and 22 adducts per 10(9) unadducted nucleotides. Both 1HP and carcinogen DNA adduct levels increased in supervisors, area workers, side oven workers, top and side oven workers, and top oven workers, respectively. These data are the first to demonstrate an increase in target organ genotoxicity in coke oven workers and a relationship with other biomarkers. Future studies will determine the identity of the DNA adducts, their correlation with 1HP levels and the relationship between levels in individual workers. Copyright © 2014 Elsevier Ireland Ltd. All rights reserved.

  3. Influence of final baking technologies in partially baked frozen gluten-free bread quality.

    PubMed

    Aguilar, Núria; Albanell, Elena; Miñarro, Begoña; Gallardo, Joan; Capellas, Marta

    2015-03-01

    The effect of final baking in convection oven (FBC), microwave oven (FBM), and microwave oven with susceptor packaging material (FBMS) on partially baked (PB) frozen gluten-free bread characteristics was investigated. Specific volume and crust color of loaves were measured at day 0. Bread moisture, water activity, and crumb and crust texture (at 15, 45, and 90 min after baking) were analyzed at day 0 and after 28 d of frozen storage (-18 °C). Volatile compounds from breads baked in convection oven or microwave oven with susceptor packaging material were also evaluated. Bread finally baked in convection oven or in microwave oven with susceptor packaging increased crust browning. Crumb and roll hardness increased with time after final baking (measured at 15, 45, 90 min) and after 28 d of frozen storage. Bread finally baked in microwave oven was the hardest, due to high water losses. At day 0, bread finally baked in convection oven had softer crumb than bread finally baked in microwave oven with susceptor packaging but, after 28 d of frozen storage, there were no differences between them. Moreover, FBC and FBMS rendered gluten-free breads that could not be distinguished in a triangular test and had the same volatile compounds profile. In conclusion, FBMS could be an alternative to FBC. © 2015 Institute of Food Technologists®

  4. Reflow-oven-processing of pressureless sintered-silver interconnects

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Wereszczak, Andrew A.; Chen, Branndon R.; Oistad, Brian A.

    Here, a method was developed to pressurelessly fabricate strong and consistent sinterable-silver joints or interconnects using reflow oven heating. Circular sinterable-silver interconnects, having nominal diameter of 5 mm and 0.1 mm thickness were stencil printed, contact-dried, and then pressurelessly sinter-bonded to Au-plated direct copper bonded ceramic substrates at 250 °C in ambient air. That sintering was done in either a reflow oven or a convective oven (latter being a conventional heating source for processing sinterable-silver). Consistently strong (>40 MPa) interconnects were produced with reflow oven heating and were as strong as those produced with convective oven heating. This is significantmore » because reflow oven technology affords better potential for continuous mass production and it was shown that strong sintered-silver bonds can indeed be achieved with its use.« less

  5. Reflow-oven-processing of pressureless sintered-silver interconnects

    DOE PAGES

    Wereszczak, Andrew A.; Chen, Branndon R.; Oistad, Brian A.

    2018-01-04

    Here, a method was developed to pressurelessly fabricate strong and consistent sinterable-silver joints or interconnects using reflow oven heating. Circular sinterable-silver interconnects, having nominal diameter of 5 mm and 0.1 mm thickness were stencil printed, contact-dried, and then pressurelessly sinter-bonded to Au-plated direct copper bonded ceramic substrates at 250 °C in ambient air. That sintering was done in either a reflow oven or a convective oven (latter being a conventional heating source for processing sinterable-silver). Consistently strong (>40 MPa) interconnects were produced with reflow oven heating and were as strong as those produced with convective oven heating. This is significantmore » because reflow oven technology affords better potential for continuous mass production and it was shown that strong sintered-silver bonds can indeed be achieved with its use.« less

  6. Influence of staining solutions and whitening procedures on discoloration of hybrid composite resins.

    PubMed

    Garoushi, Sufyan; Lassila, Lippo; Hatem, Marwa; Shembesh, Muneim; Baady, Lugane; Salim, Ziad; Vallittu, Pekka

    2013-01-01

    The aim was to evaluate the color stability and water uptake of two hybrid composite resins polymerized in two different conditions after exposure to commonly consumed beverages. In addition, the effect of repolishing and bleaching on the stained composite was evaluated. Eighty specimens (12 mm × 12 mm × 3 mm) were made from two hybrid composite resins of shade A2. Forty specimens of each composite were divided into two groups (n = 20 per each) according to the curing method used (hand light cure HLC or oven light cure OLC). Then each group (HLC or OLC) was sub-divided randomly into four sub-groups (n = 5), which were immersed for 60 days in different beverages (distal water, coffee, tea and pepsi) and incubated at 37°C. Water uptake was measured during this time and followed by measurement of color difference (ΔE) by using a spectrophotometer. After complete staining, repolishing (grit 4000 FEPA at 300 rpm under water) and bleaching (40% hydrogen peroxide bleaching gel) were conducted. The repolished and bleached specimens were submitted to new color measurements. Color value of the specimens immersed in tea displayed the highest statistically significant (p < 0.05) mean color difference (ΔE) compared to other beverages, whereas the ΔE value of pepsi was significantly lower than the others. After staining of the composite resins, both the bleaching and repolishing were able to reduce the ΔE value. All beverages used affected the color stability of tested composite resins. The effect of beverages on color change of composites depends on type of beverage and water uptake value of resins used. A superior whitening effect was obtained with repolishing technique compared to bleaching.

  7. 40 CFR 60.391 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... truck including hoods, fenders, cargo boxes, doors, and grill opening panels. Bake oven means a device...-duty truck assembly lines between the coating application system (dip tank or spray booth) and the bake oven. Guide coat operation means the guide coat spray booth, flash-off area and bake oven(s) which are...

  8. 40 CFR 60.391 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... truck including hoods, fenders, cargo boxes, doors, and grill opening panels. Bake oven means a device...-duty truck assembly lines between the coating application system (dip tank or spray booth) and the bake oven. Guide coat operation means the guide coat spray booth, flash-off area and bake oven(s) which are...

  9. 40 CFR 60.391 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... truck including hoods, fenders, cargo boxes, doors, and grill opening panels. Bake oven means a device...-duty truck assembly lines between the coating application system (dip tank or spray booth) and the bake oven. Guide coat operation means the guide coat spray booth, flash-off area and bake oven(s) which are...

  10. 40 CFR 60.391 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... truck including hoods, fenders, cargo boxes, doors, and grill opening panels. Bake oven means a device...-duty truck assembly lines between the coating application system (dip tank or spray booth) and the bake oven. Guide coat operation means the guide coat spray booth, flash-off area and bake oven(s) which are...

  11. 40 CFR 60.391 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... truck including hoods, fenders, cargo boxes, doors, and grill opening panels. Bake oven means a device...-duty truck assembly lines between the coating application system (dip tank or spray booth) and the bake oven. Guide coat operation means the guide coat spray booth, flash-off area and bake oven(s) which are...

  12. Inhalation trauma due to overheating in a microwave oven.

    PubMed Central

    Zanen, A L; Rietveld, A P

    1993-01-01

    The microwave oven is a kitchen appliance that has become increasingly popular in recent years. In some instances the temperature in the microwave oven can become exceedingly high. A case is discussed of a patient with respiratory distress after inhalation of gas from an overheated microwave oven. Images PMID:8497834

  13. Environmentally benign sol-gel antifouling and foul-releasing coatings.

    PubMed

    Detty, Michael R; Ciriminna, Rosaria; Bright, Frank V; Pagliaro, Mario

    2014-02-18

    Biofouling on ships and boats, characterized by aquatic bacteria and small organisms attaching to the hull, is an important global issue, since over 80000 tons of antifouling paint is used annually. This biofilm, which can form in as little as 48 hours depending on water temperature, increases drag on watercraft, which greatly reduces their fuel efficiency. In addition, biofouling can lead to microbially induced corrosion (MIC) due to H2S formed by the bacteria, especially sulfate-reducing bacteria. When the International Maritime Organization (IMO) international convention banned the use of effective but environmentally damaging coatings containing tributyl tin in 2008, the development of clean and effective antifouling systems became more important than ever. New nonbiocidal coatings are now in high demand. Scientists have developed new polymers, materials, and biocides, including new elastomeric coatings that they have obtained by improving the original silicone (polydimethylsiloxane) formulation patented in 1975. However, the high cost of silicones, especially of fluoropolymer-modified silicones, has generally prevented their large-scale diffusion. In 2009, traditional antifouling coatings using cuprous oxide formulated in copolymer paints still represented 95% of the global market volume of anti-fouling paints. The sol-gel nanochemistry approach to functional materials has emerged as an attractive candidate for creating low fouling surfaces due to the unique structure and properties of silica-based coatings and of hybrid inorganic-organic silicas in particular. Sol-gel formulations easily bind to all types of surfaces, such as steel, fiberglass, aluminum, and wood. In addition, they can cure at room temperature and form thin glassy coatings that are markedly different from thick silicone elastomeric foul-releasing coatings. Good to excellent performance against biofouling, low cure temperatures, enhanced and prolonged chemical and physical stability, ease of application, and the waterborne nature of sol-gel coatings all support the diffusion of these paints to efficiently reduce the accumulation of fouling layers on valued surfaces immersed in marine or fluvial waters. Furthermore, sol-gel glassy coatings are transparent and can be effectively applied to optical devices, windows, and solar panels used in lake, fluvial, or marine environments. Sol-gel technology is eminently versatile, and the first generation sol-gel paints have already shown good performance. Even so, vast opportunities still exist for chemists to develop novel sol-gel derived coatings to both prevent biofouling and enhance the hydrodynamic properties of boat and ship hulls. Moreover, researchers have prepared and applied multifunctional sol-gel coatings providing protection against both biofouling and corrosion. They have tested these in the marine environment with good preliminary results. In this Account, we discuss some of our new strategies for the controlled functionalization of surfaces for the development of efficient antifouling and foul-releasing systems and summarize the main achievements with biocidal and nonbiocidal sol-gel coatings. We conclude by giving insight into the marine coatings and sol-gel products markets, providing arguments to justify our conclusion that the sol-gel coatings technology is now a mature platform for the development of economically viable and environmentally friendly antifouling and foul-release formulations of enhanced performance.

  14. In situ simultaneous strain and temperature measurement of adaptive composite materials using a fiber Bragg grating based sensor

    NASA Astrophysics Data System (ADS)

    Yoon, Hyuk-Jin; Costantini, Daniele M.; Michaud, Veronique; Limberger, Hans G.; Manson, Jan-Anders; Salathe, Rene P.; Kim, Chun-Gon; Hong, Chang-Sun

    2005-05-01

    An optical fiber sensor to simultaneously measure strain and temperature was designed and embedded into an adaptive composite laminate which exhibits a shape change upon thermal activation. The sensor is formed by two fiber Bragg gratings, which are written in optical fibers with different core dopants. The two gratings were spliced close to each other and a sensing element resulted with Bragg gratings of similar strain sensitivity but different response to temperature. This is due to the dependence of the fiber thermo-optic coefficient on core dopants and relative concentrations. The sensor was tested on an adaptive composite laminate made of unidirectional Kevlar-epoxy pre-preg plies. Several 150μm diameter pre-strained NiTiCu shape memory alloy wires were embedded in the composite laminate together with one fiber sensor. Simultaneous monitoring of strain and temperature during the curing process and activation in an oven was demonstrated.

  15. Notched Strength Allowables and Inplane Shear Strength of AS4/VRM-34 Textile Laminates

    NASA Technical Reports Server (NTRS)

    Grenoble, Ray W.; Johnston, William M.

    2013-01-01

    Notched and unnotched strength allowables were developed for a textile composite to provide input data to analytical structural models based on the Pultruded Rod Stiffened Efficient Unitized Structure (PRSEUS) concept. Filled-hole tensile strength, filled-hole compressive strength, and inplane shear strength along stitch lines have been measured. The material system evaluated in this study is based on warp-knitted preforms of AS4 carbon fibers and VRM-34 epoxy resin, which have been processed via resin infusion and oven curing. All specimens were tested in as-fabricated (dry) condition. Filled-hole strengths were evaluated with and without through-thickness stitching. The effects of scaling on filled-hole tensile strength were evaluated by testing specimens in two widths, but with identical width / hole-diameter ratios. Inplane shear specimens were stitched in two configurations, and two specimen thicknesses were tested for each stitch configuration.

  16. Modified Phenylethynyl Containing Imides for Secondary Bonding: Non-Autoclave, Low Temperature Processable Adhesives

    NASA Technical Reports Server (NTRS)

    Dezern, James F. (Technical Monitor); Chang, Alice C.

    1999-01-01

    As part of a program to develop structural adhesives for high performance aerospace applications, research continued on the development of modified phenylethynyl containing imides, LaRC(trademark)MPEIs. In previous reports, the polymer properties were controlled by varying the molecular weight, the amount of branching, and the phenylethynyl content and by blending with low molecular weight materials. This research involves changing the flexibility in the copolyimide backbone of the branched, phenylethynyl terminated adhesives. These adhesives exhibit excellent processability at pressures as low as 15 psi and temperatures as low as 288 C. The Ti/Ti lap shear specimens are processable in an autoclave or a temperature programmable oven under a vacuum bag at 288-300 C without external pressure. The cured polymers exhibit high mechanical properties and excellent solvent resistance. The chemistry and properties of these adhesives are presented.

  17. Multiple delivery cesium oven system for negative ion sources

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Bansal, G.; Bhartiya, S.; Pandya, K.

    2012-02-15

    Distribution of cesium in large negative ion beam sources to be operational in ITER, is presently based on the use of three or more cesium ovens, which operate simultaneously and are controlled remotely. However, use of multiple Cs ovens simultaneously is likely to pose difficulties in operation and maintenance of the ovens. An alternate method of Cs delivery, based on a single oven distribution system is proposed as one which could reduce the need of simultaneous operation of many ovens. A proof of principle experiment verifying the concept of a multinozzle distributor based Cs oven has been carried out atmore » Institute for Plasma Research. It is also observed that the Cs flux is not controlled by Cs reservoir temperature after few hours of operation but by the temperature of the distributor which starts behaving as a Cs reservoir.« less

  18. 40 CFR 63.304 - Standards for compliance date extension.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.304 Standards for compliance date extension. (a) An owner or operator of an existing coke oven battery (including a cold-idle coke oven battery), a padup rebuild, or a brownfield coke oven battery, may elect an extension of the compliance date for...

  19. 40 CFR 63.304 - Standards for compliance date extension.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.304 Standards for compliance date extension. (a) An owner or operator of an existing coke oven battery (including a cold-idle coke oven battery), a padup rebuild, or a brownfield coke oven battery, may elect an extension of the compliance date for...

  20. 40 CFR 63.304 - Standards for compliance date extension.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.304 Standards for compliance date extension. (a) An owner or operator of an existing coke oven battery (including a cold-idle coke oven battery), a padup rebuild, or a brownfield coke oven battery, may elect an extension of the compliance date for...

  1. 40 CFR 63.3171 - How do I demonstrate initial compliance?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... of electrodeposition bake oven emissions. You must show that the electrodeposition bake oven meets... of the exhaust gases from the bake oven to an add-on control device. For purposes of this showing, an electrodeposition bake oven air seal is not considered a natural draft opening provided you demonstrate that the...

  2. 40 CFR 63.3171 - How do I demonstrate initial compliance?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... of electrodeposition bake oven emissions. You must show that the electrodeposition bake oven meets... of the exhaust gases from the bake oven to an add-on control device. For purposes of this showing, an electrodeposition bake oven air seal is not considered a natural draft opening provided you demonstrate that the...

  3. 40 CFR 63.3171 - How do I demonstrate initial compliance?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... of electrodeposition bake oven emissions. You must show that the electrodeposition bake oven meets... of the exhaust gases from the bake oven to an add-on control device. For purposes of this showing, an electrodeposition bake oven air seal is not considered a natural draft opening provided you demonstrate that the...

  4. 40 CFR 63.3171 - How do I demonstrate initial compliance?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... of electrodeposition bake oven emissions. You must show that the electrodeposition bake oven meets... of the exhaust gases from the bake oven to an add-on control device. For purposes of this showing, an electrodeposition bake oven air seal is not considered a natural draft opening provided you demonstrate that the...

  5. 40 CFR 63.3176 - What definitions apply to this subpart?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... automobiles or light-duty trucks, including coating facilities and processes. Bake oven air seal means an entry or entry vestibule to or an exit or exit vestibule from a bake oven which isolates the bake oven... exit or exit vestibule) the bake oven. No significant VOC generating activity takes place in a bake...

  6. 40 CFR 63.3171 - How do I demonstrate initial compliance?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... of electrodeposition bake oven emissions. You must show that the electrodeposition bake oven meets... of the exhaust gases from the bake oven to an add-on control device. For purposes of this showing, an electrodeposition bake oven air seal is not considered a natural draft opening provided you demonstrate that the...

  7. 16 CFR 255.1 - General considerations.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... an uncooked chicken in the oven roasting bag and places the bag in one oven. He then takes a chicken roasting bag from a second oven, removes from the bag what appears to be a perfectly cooked chicken, tastes... conduct. Example 4: A well-known celebrity appears in an infomercial for an oven roasting bag that...

  8. 40 CFR 63.305 - Alternative standards for coke oven doors equipped with sheds.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries § 63.305 Alternative standards for coke oven doors equipped with sheds. (a) The owner or operator of a new or existing coke oven battery... the efficiency of the control device for removal of particulate matter by conducting measurements at...

  9. 40 CFR 63.305 - Alternative standards for coke oven doors equipped with sheds.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries § 63.305 Alternative standards for coke oven doors equipped with sheds. (a) The owner or operator of a new or existing coke oven battery... the efficiency of the control device for removal of particulate matter by conducting measurements at...

  10. 40 CFR 63.305 - Alternative standards for coke oven doors equipped with sheds.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries § 63.305 Alternative standards for coke oven doors equipped with sheds. (a) The owner or operator of a new or existing coke oven battery... the efficiency of the control device for removal of particulate matter by conducting measurements at...

  11. 40 CFR 63.305 - Alternative standards for coke oven doors equipped with sheds.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries § 63.305 Alternative standards for coke oven doors equipped with sheds. (a) The owner or operator of a new or existing coke oven battery... the efficiency of the control device for removal of particulate matter by conducting measurements at...

  12. 40 CFR 63.305 - Alternative standards for coke oven doors equipped with sheds.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries § 63.305 Alternative standards for coke oven doors equipped with sheds. (a) The owner or operator of a new or existing coke oven battery... the efficiency of the control device for removal of particulate matter by conducting measurements at...

  13. Sterilization of instruments in solar ovens.

    PubMed

    Jørgensen, A F; Nøhr, K; Boisen, F; Nøhr, J

    2002-01-01

    The sterilization of instruments in rural health clinics in less developed countries is an increasing problem as chemical methods can no longer be recommended and fuel wood is becoming increasingly scarce. It seems obvious, therefore, to utilize solar energy for sterilization purposes. A solar oven was designed and manufactured using local materials and simple tools. It was tested by physical, chemical and microbiological methods and, after successful testing, installed in a rural clinic. The oven was able to generate temperatures above 180 degrees C. On days with direct sunlight the oven fulfilled the international recommendations for hot air sterilization. The chemical indicators, Browne's tubes type 3 and 5, also changed colour. It was difficult to reach the right value for the sterilization effect during months with a low sun position. A moveable oven, or two ovens, must be installed to solve this problem. The solar oven has proven to be a realistic method for the sterilization of instruments. The solar oven is easy to make and use. It saves fuel and can be used in most tropical areas.

  14. Combination microwave ovens: an innovative design strategy.

    PubMed

    Tinga, Wayne R; Eke, Ken

    2012-01-01

    Reducing the sensitivity of microwave oven heating and cooking performance to load volume, load placement and load properties has been a long-standing challenge for microwave and microwave-convection oven designers. Conventional design problem and solution methods are reviewed to provide greater insight into the challenge and optimum operation of a microwave oven after which a new strategy is introduced. In this methodology, a special load isolating and energy modulating device called a transducer-exciter is used containing an iris, a launch box, a phase, amplitude and frequency modulator and a coupling plate designed to provide spatially distributed coupling to the oven. This system, when applied to a combined microwave-convection oven, gives astounding performance improvements to all kinds of baked and roasted foods including sensitive items such as cakes and pastries, with the only compromise being a reasonable reduction in the maximum available microwave power. Large and small metal utensils can be used in the oven with minimal or no performance penalty on energy uniformity and cooking results. Cooking times are greatly reduced from those in conventional ovens while maintaining excellent cooking performance.

  15. Characteristic analysis of peripheral blood mononuclear cell apoptosis in coke oven workers.

    PubMed

    Zhang, Hong Mei; Nie, Ji Sheng; Li, Xin; Niu, Qiao

    2012-01-01

    The aim of the present study was to determine the peripheral blood mononuclear cell (PBMC) apoptosis in coke oven workers so that we can take effective measures to protect coke oven workers. The subjects, 129 coke oven workers and 37 warehouse workers (controls), were investigated using a questionnaire to collect information about their age, working years, smoking and drinking habits, vocational history and other general information. The coke oven workers were divided into the oven-bottom group (34), oven-side group (48) and oven-top group (47) according to their working sites and environmental monitoring data. The concentration of benzo[a]pyrene (B[a]P) and the subjects' urinary 1-hydroxypyrene (1-OH-Py) levels were determined by HPLC. Additionally, the PBMCs were separated from blood samples, and the early and late apoptosis rates were determined by flow cytometry. The airborne B[a]P concentrations were 19.5 ± 13.2, 185.9 ± 38.6 and 1,623.5 ± 435.8 ng/m(3) at the bottom, side and top of the oven, respectively, and were higher than in the controls' workplaces 10.2 ± 7.6 ng/m(3). Urinary 1-OH-Py, indicating the B[a]P's internal exposure level, was significantly higher in the exposed groups than in the controls (p<0.05). Compared with the controls, the coke oven workers' PBMC apoptosis rates were significantly increased and increased in association with the B[a]P level. PBMC apoptosis increased in association with the 1-OH-Py level and coking operation years and decreased in association with years of alcohol consumption. PBMC apoptosis in the coke oven workers was associated with the 1-OH-Py level, coke operation years and years of alcohol consumption and may be induced by B[a]P.

  16. Changes in mechanical properties and morphology of elastomer coatings after immersion in salt solutions

    NASA Astrophysics Data System (ADS)

    Terán Arce, Fernando; Avci, Recep; Beech, Iwona; Cooksey, Keith; Wigglesworth-Cooksey, Barbara

    2004-03-01

    RTV11 (^TM GE Silicones) and Intersleek (^TM International Paints) are two elastomers of considerable significance to the navy and maritime industry for their application as fouling release coatings. Both materials are composed of polymeric matrices with embedded filler particles, which provide increased strength and durability to the elastomer. Using Atomic force microscopy (AFM), surface and bulk analysis techniques, we have found surface regions with microelastic properties, which correlate with the locations of filler particles inside the coatings. These particles are able to undergo elastic displacements of hundreds of nm inside the polymeric matrix during compression by the AFM tip. While elastic properties of Intersleek remain largely unchanged after immersion in salt solutions, roughening, embrittlement and stiffening occurs in RTV11 coatings depending on the amount of curing agent and humidity used during preparation and curing, respectively. Interestingly, such transformations are absent after immersion in pure water. In particle free regions, elastic moduli of RTV11 take values of 2 - 3 MPa before immersion in salt solutions. After immersion, those values increase 5 - 10 times.

  17. Space shuttle/food system study. Volume 2: Supporting appendices, oven study

    NASA Technical Reports Server (NTRS)

    1975-01-01

    Calculations and data regarding the development of a galley oven for use in the space shuttle are presented. Heat flow, heat transfer, and food heating characteristics are given for various oven designs. A design approach to guarantee structural reliability is also presented, in which the oven closure, door, and basic mounting points are considered.

  18. Effects of coke oven emissions and benzo[a]pyrene on blood pressure and electrocardiogram in coke oven workers.

    PubMed

    Yang, Kai; Jiang, Xuejun; Cheng, Shuqun; Chen, Chengzhi; Cao, Xianqing; Tu, Baijie

    2017-01-24

    To evaluate the effects of occupational exposures to coke oven emissions (COEs) and benzo[a]pyrene (B[a]P) on the prevalence of hypertension and abnormal electrocardiogram (ECG) in coke oven workers. We included 880 coke oven workers and 710 oxygen employees in the exposed and control groups, respectively. Blood pressure (BP), ECG, blood lipid levels, and glucose levels of all subjects were measured. COE and B[a]P concentrations at the bottom, side, and top of the oven and control plants were estimated by weighing and high-performance liquid chromatography. The COE concentration at the top and side was higher than that at the bottom (P < 0.05). The levels of B[a]P at the top and side significantly exceeded the limit value. Abnormal BP, ECG, the detection ratio of hypertension and left ventricular high voltage were significantly greater in the exposed group than in the control group (P < 0.05). The logistic regression analysis results revealed that age and B[a]P exposure were risk factors for hypertension in coke oven workers (P < 0.05) and both were risk factors for abnormal ECG (P < 0.05). Moreover, B[a]P exposure, age, and gender were risk factors for impaired fasting glucose in coke oven workers (P < 0.05). B[a]P and COE exposures are risk factors for hypertension and abnormal ECG in coke oven workers.

  19. 40 CFR 63.3165 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ..., a bake oven air seal is not considered a natural draft opening in a PTE or a temporary total enclosure provided you demonstrate that the direction of air movement across the interface between the bake oven air seal and the bake oven is into the bake oven. You may use lightweight strips of fabric or...

  20. 40 CFR 63.3165 - How do I determine the emission capture system efficiency?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ..., a bake oven air seal is not considered a natural draft opening in a PTE or a temporary total enclosure provided you demonstrate that the direction of air movement across the interface between the bake oven air seal and the bake oven is into the bake oven. You may use lightweight strips of fabric or...

  1. Effectiveness of modified 1-hour air-oven moisture methods for determining popcorn moisture

    USDA-ARS?s Scientific Manuscript database

    Two of the most commonly used approved grain moisture air-oven reference methods are the air oven method ASAE S352.2, which requires long heating time (72-h) for unground samples, and the AACC 44-15.02 air-oven method, which dries a ground sample for 1 hr, but there is specific moisture measurement ...

  2. 40 CFR 63.7351 - Who implements and enforces this subpart?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ...-product coke oven battery with vertical flues, fugitive pushing emissions in § 63.7292(a) for a by-product... coke oven battery, soaking for a by-product coke oven battery in § 63.7294(a), and quenching for a coke... for a by-product coke oven battery under § 63.6(h)(9). (3) Approval of major alternatives to test...

  3. 40 CFR Appendix A to Subpart L of... - Operating Coke Oven Batteries as of April 1, 1992

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 9 2010-07-01 2010-07-01 false Operating Coke Oven Batteries as of... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries Pt. 63, Subpt. L, App. A Appendix A to Subpart L of Part 63—Operating Coke Oven Batteries as of April 1, 1992 No. Plant Battery 1 ABC...

  4. 40 CFR Appendix A to Subpart L of... - Operating Coke Oven Batteries as of April 1, 1992

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 10 2013-07-01 2013-07-01 false Operating Coke Oven Batteries as of... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries Pt. 63, Subpt. L, App. A Appendix A to Subpart L of Part 63—Operating Coke Oven Batteries as of April 1, 1992 No. Plant Battery 1 ABC...

  5. 40 CFR Appendix A to Subpart L of... - Operating Coke Oven Batteries as of April 1, 1992

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 10 2014-07-01 2014-07-01 false Operating Coke Oven Batteries as of... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries Pt. 63, Subpt. L, App. A Appendix A to Subpart L of Part 63—Operating Coke Oven Batteries as of April 1, 1992 No. Plant Battery 1 ABC...

  6. 40 CFR Appendix A to Subpart L of... - Operating Coke Oven Batteries as of April 1, 1992

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 9 2011-07-01 2011-07-01 false Operating Coke Oven Batteries as of... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries Pt. 63, Subpt. L, App. A Appendix A to Subpart L of Part 63—Operating Coke Oven Batteries as of April 1, 1992 No. Plant Battery 1 ABC...

  7. 40 CFR Appendix A to Subpart L of... - Operating Coke Oven Batteries as of April 1, 1992

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 10 2012-07-01 2012-07-01 false Operating Coke Oven Batteries as of... SOURCE CATEGORIES National Emission Standards for Coke Oven Batteries Pt. 63, Subpt. L, App. A Appendix A to Subpart L of Part 63—Operating Coke Oven Batteries as of April 1, 1992 No. Plant Battery 1 ABC...

  8. Urinary 1-hydroxypyrene and 8-hydroxydeoxyguanosine levels among coke-oven workers for 2 consecutive days.

    PubMed

    Nguyen, Thi-To-Uyen; Kawanami, Shoko; Kawai, Kazuaki; Kasai, Hiroshi; Li, Yun-Shan; Inoue, Jinro; Ngoan, Le Tran; Horie, Seichi

    2014-01-01

    This study evaluated the levels of exposure to polycyclic aromatic hydrocarbons (PAHs) and their relationship with oxidative DNA damage among Vietnamese coke-oven workers. We collected urine from 36 coke-oven workers (exposed group) at the beginning and end of the shift on 2 consecutive days. We also collected urine from 78 medical staff (control group). Information was collected by questionnaire about smoking status, drinking habit, and working position. Urinary 1-hydroxypyrene (1-OHP) and 8-hydroxydeoxyguanosine (8-OH-dG) were measured using HPLC. All statistical analyses were performed with SPSS version 19. Urinary 1-OHP was significantly higher in the coke-oven workers than in the control group (p<0.05). Top-oven workers had the highest levels of internal exposure to PAHs, followed by side-oven and then bottom-oven workers (5.41, 4.41 and 1.35 ng/mg creatinine, respectively, at the end of the shift on day 2). Urinary 8-OH-dG was significantly higher in top- and side-oven workers at the end of the shift on day 2 (4.63 and 5.88 ng/mg creatinine, respectively) than in the control group (3.85 ng/mg creatinine). Based on a multi-regression analysis, smoking status had a significant effect on urinary 8-OH-dG (p=0.049). Urinary 1-OHP tended to have a positive correlation with urinary 8-OH-dG (p=0.070). Vietnamese coke-oven workers were exposed to PAHs during their work shift. Urinary 1-OHP exceeded the recommended limit, and elevated oxidative DNA damage occurred in top- and side-oven workers on the second day of work. A tendency for positive correlation was found between urinary 1-OHP and urinary 8-OH-dG.

  9. EXTERIOR VIEW, BEE HIVE COKE OVEN DOOR. Pratt Coal ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    EXTERIOR VIEW, BEE HIVE COKE OVEN DOOR. - Pratt Coal & Coke Company, Pratt Mines, Coke Ovens & Railroad, Bounded by First Street, Avenue G, Third Place, Birmingham Southern Railroad, Birmingham, Jefferson County, AL

  10. Effects of coke oven emissions and benzo[a]pyrene on blood pressure and electrocardiogram in coke oven workers

    PubMed Central

    Yang, Kai; Jiang, Xuejun; Cheng, Shuqun; Chen, Chengzhi; Cao, Xianqing; Tu, Baijie

    2016-01-01

    Objective: To evaluate the effects of occupational exposures to coke oven emissions (COEs) and benzo[a]pyrene (B[a]P) on the prevalence of hypertension and abnormal electrocardiogram (ECG) in coke oven workers. Methods: We included 880 coke oven workers and 710 oxygen employees in the exposed and control groups, respectively. Blood pressure (BP), ECG, blood lipid levels, and glucose levels of all subjects were measured. COE and B[a]P concentrations at the bottom, side, and top of the oven and control plants were estimated by weighing and high-performance liquid chromatography. Results: The COE concentration at the top and side was higher than that at the bottom (P < 0.05). The levels of B[a]P at the top and side significantly exceeded the limit value. Abnormal BP, ECG, the detection ratio of hypertension and left ventricular high voltage were significantly greater in the exposed group than in the control group (P < 0.05). The logistic regression analysis results revealed that age and B[a]P exposure were risk factors for hypertension in coke oven workers (P < 0.05) and both were risk factors for abnormal ECG (P < 0.05). Moreover, B[a]P exposure, age, and gender were risk factors for impaired fasting glucose in coke oven workers (P < 0.05). Conclusions: B[a]P and COE exposures are risk factors for hypertension and abnormal ECG in coke oven workers. PMID:27885241

  11. 40 CFR 63.5875 - How do I determine the capture efficiency of the enclosure on my wet-out area and the capture...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... efficiency of the enclosure on my wet-out area and the capture efficiency of my oven(s) for continuous... efficiency of the enclosure on my wet-out area and the capture efficiency of my oven(s) for continuous lamination/casting operations? (a) The capture efficiency of a wet-out area enclosure is assumed to be 100...

  12. Building a Low Cost Solar Oven: An Opportunity to Teach Thermodynamics

    NASA Astrophysics Data System (ADS)

    Nogueira, Ana

    2014-03-01

    We suggested building a solar oven using cardboard boxes, glass wool and metal plate as part of a school project permeated by the discussion of physical concepts. The main topics addressed are from the heat and thermodynamics areas, and for these themes we followed the standard books used in high school. We can work in a practical manner with the thermometer, along with the concept of temperature, measuring the temperature of the oven when cooking. To discuss how the oven works, we introduce the concept of heat as an energy flow of a body with a higher temperature to one with lower temperature. Threads as heat capacity and specific heat of a substance are introduced, also discussing the use of glass wool, which function is to prevent heat exchange from the oven's interior with the environment. It is possible to demonstrate the three forms of heat transfer using the solar oven, and how the greenhouse effect is harnessed. One can discuss topics such as electromagnetic radiation, black-body radiation and the Stefan-Boltzmann law. We surveyed the response curve of our oven and an estimate of its total solar energy absorption efficiency. The development of this project allows a good understanding of the operation principles of a solar oven. UNIMONTES.

  13. In vitro starch digestibility and expected glycemic index of pound cakes baked in two-cycle microwave-toaster and conventional oven.

    PubMed

    García-zaragoza, Francisco J; Sánchez-Pardo, María E; Ortiz-Moreno, Alicia; Bello-Pérez, Luis A

    2010-11-01

    Bread baking technology has an important effect on starch digestibility measured as its predicted glycemic index tested in vitro. The aim of this work was to evaluate the changes in predicted glycemic index of pound cake baked in a two-cycle microwave toaster and a conventional oven. The glycemic index was calculated from hydrolysis index values by the Granfeldt method. Non-significant differences (P > 0.05) were found in hydrolysis index (60.67 ± 3.96 for the product baked in microwave oven and 65.94 ± 4.09 for the product baked in conventional oven) and predicted glycemic index content (60.5 for product baked in microwave oven and 65 for the product baked in conventional oven) in freshly-baked samples. Results clearly demonstrate that the baking pound cake conventional process could be replicated using a two-cycle multifunction microwave oven, reducing the traditional baking time. Further research is required in order to achieve pound cake crumb uniformity.

  14. 25. DETAIL OF INSCRIPTION ON BAKE OVEN WHICH READS: PREMIUM ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    25. DETAIL OF INSCRIPTION ON BAKE OVEN WHICH READS: PREMIUM PATENT BAKE OVEN ROASTER BY ALFRED H. REIP NO. 337 BALT. STREET BALTIMORE - Hazelwood, 18611 Queen Anne Road, Upper Marlboro, Prince George's County, MD

  15. 65. INTERIOR VIEW OF THE LIMENITROGEN (CALCIUM CYANAMIDE) OVEN BUILDING, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    65. INTERIOR VIEW OF THE LIME-NITROGEN (CALCIUM CYANAMIDE) OVEN BUILDING, LOOKING AT 2 BANKS OF OVENS. MARCH 2, 1919. - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

  16. 5 Tips for Using Your Microwave Oven Safely

    MedlinePlus

    ... not being emitted in this situation.” How to Report Problems In the FDA’s experience, most microwave ovens ... FDA’s page on microwave ovens .) You also can report any suspected radiation-related problems or injuries directly ...

  17. Multiphoton laser ionization for energy conversion in barium vapor

    NASA Astrophysics Data System (ADS)

    Makdisi, Y.; Kokaj, J.; Afrousheh, K.; Mathew, J.; Nair, R.; Pichler, G.

    2013-03-01

    We have studied the ion detection of barium atoms in special heated ovens with a tungsten rod in the middle of the stainless steel tube. The tungsten rod was heated indirectly by the oven body heaters. A bias voltage between the cell body and the tungsten rod of 9 V was used to collect electrons, after the barium ions had been created. However, we could collect the electrons even without the bias voltage, although with ten times less efficiency. We studied the conditions for the successful bias-less thermionic signal detection using excimer/dye laser two-photon excitation of Rydberg states below and above the first ionization limit (two-photon wavelength at 475.79 nm). We employed a hot-pipe oven and heat-pipe oven (with inserted mesh) in order to generate different barium vapor distributions inside the oven. The thermionic signal increased by a factor of two under heat-pipe oven conditions.

  18. Evaluating the bakeout effectiveness of RTV-S691 silicone adhesive by measuring outgassing rate

    NASA Astrophysics Data System (ADS)

    Miyazaki, Eiji; Miura, Yuka; Numata, Osamu; Yamanaka, Riyo; Baba, Susumu; Ishizawa, Junichiro; Kimoto, Yugo; Tamura, Takashi

    2014-09-01

    Outgassing rate measurements are basically performed for fresh materials, e.g. just cured adhesives, paints, etc. and reveal a lot about how the material can behave as a contamination source. It is also important to determine the bakeout process sufficiently. In the present study, a typical silicone adhesive for use in space, RTV S-691, Wacker Chemie, was selected for the measurement. Two cured specimens, 40 × 40 mm in size, were applied for several isothermal tests under identical conditions: a specimen at 125 degrees C for 144 hours with CQCM at -193 degrees C to measure TML. Consequently, it was determined that the TML and TML rate could be reduced by bakeout as expected. It also emerged that a longer bakeout, i.e. a longer cumulative bakeout time, for the material would reduce the TML and TML rate more effectively. The results suggest that bakeout mainly affects the behavior in the "low-rate" phase, whereby the TML rate curve can be divided into two phases. The elapsed time for a specimen can also be considered the cumulative test time. Based on the cumulative elapsed time, the TML rate curve is replotted and a correlation emerges between the cumulative bakeout time and TML rate. The first measurement data of TML and the TML rate could be affected by the stored time from cure, which might result from the change in unreacted substances declining as the stored time elapsed.

  19. Rapid drying soils with microwave ovens.

    DOT National Transportation Integrated Search

    2002-07-01

    Soils are normally dried in either a convection oven or stove. Inspections of field and laboratory moisture content testing indicated that the typical drying durations for a convection oven and stove were, 24 hours and 60 minutes, respectively. The o...

  20. [The dose response decrease of lung function associated with the urinary polycyclic aromatic hydrocarbons metabolites in coke oven workers].

    PubMed

    Hu, Die; Deng, Qi-fei; Huang, Su-li; He, Yun-feng; Guo, Huan; Wu, Tang-chun

    2012-12-01

    To analyze the relationship between metabolites of polycyclic aromatic hydrocarbons (PAHs) and lung function in coke oven workers, and to provide scientific basis for further exploring the potential mechanism and developing the preventing strategies of the workers' early lung damage. We measured carbon monoxide, sulfur dioxide, benzene soluble matter, particulate matters, and PAHs at different workplaces of a coke oven plant. Detailed information on demography and occupational health condition of 912 workers were collected. We divided these workers into control group and coke oven group according to their workplaces and the different concentrations of COEs in the environment. We detected 10 urinary PAH metabolites and lung function using gas chromatography-mass spectrometry and spirometric tests, respectively. FEV(1.0) (91.12 ± 13.31) and FEV(1.0)/FVC (108.61 ± 20.37) of the coke oven group is significantly lower than the control group (94.16 ± 15.57, 113.45 ± 19.70). In the coke oven group, the hydroxyphenanthrene and 1-hydroxypyrene are negatively correlated with FEV(1.0)/FVC (β = -0.136, β = -0.100), Ptrend < 0.05 for all. The dose response decrease of lung function is associated with the urinary PAH metabolites in coke oven workers. Indicated that the long exposure to PAHs may cause the early lung damage in coke oven workers, phenanthrene and pyrene may be the main factors.

  1. Microwave ovens and food safety: preparation of Not-Ready-to-Eat products in standard and smart ovens.

    PubMed

    Schiffmann, Robert F

    2013-01-01

    The introduction of several Not-Ready-to-Eat (NRTE) products, beginning in 2007, has resulted in several recalls and has caused serious concerns about their safe-cooking in microwave ovens. These products are not fully-thermally processed prior to sale but depend upon the consumer to finish cooking them to the safe minimum temperatures, defined by the USDA, in order to destroy any sources of foodborne illnesses. While microwave ovens are a primary means of this finish-cooking step, they are known to cook foods unevenly in terms of temperature distribution, especially from a frozen state, and this may cause parts of the food to be below the required safe-temperature. Hence there are concerns regarding how reliably microwave ovens can provide the minimum required safe temperatures in order to avoid the possibility of foodborne illnesses. To determine this, temperature profiling tests were preformed upon three frozen NRTE entrées, heating them in eight new brand-name 1100-watt and 1200-watt microwave ovens in order to evaluate how well the minimum temperatures were reached throughout the products. By comparison, these same tests were repeated using three "smart" microwave ovens in which internal computer-control makes them user-independent. In addition, a comparison was also made of the microwave output power claimed by the manufacturers of these ovens to that determined using the IEC procedures.

  2. 22. VIEW OF A SINGLE BEEHIVE COKE OVEN SHOWING THE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    22. VIEW OF A SINGLE BEEHIVE COKE OVEN SHOWING THE INTERIOR STRUCTURE OF THE OVEN. - Tower Hill No. 2 Mine, Approximately 0.47 mile Southwest of intersection of Stone Church Road & Township Route 561, Hibbs, Fayette County, PA

  3. 28. CROSS SECTION OF A RECTANGULAR COKE OVEN SHOWING THE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    28. CROSS SECTION OF A RECTANGULAR COKE OVEN SHOWING THE INTERNAL STRUCTURE OF THE OVEN. - Tower Hill No. 2 Mine, Approximately 0.47 mile Southwest of intersection of Stone Church Road & Township Route 561, Hibbs, Fayette County, PA

  4. DETAIL OF BEEHIVE COKE OVEN DOOR, LOOKING NORTH; NOTE FIREBRICK ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    DETAIL OF BEEHIVE COKE OVEN DOOR, LOOKING NORTH; NOTE FIRE-BRICK ARCH AND IRON JAMB AND SILL - Nuttallburg Mine Complex, Coke Ovens, North side of New River, 2.7 miles upstream from Fayette Landing, Lookout, Fayette County, WV

  5. 16. 110 SANSOM STREET, OBLIQUE VIEW OF BAKE OVEN IN ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    16. 110 SANSOM STREET, OBLIQUE VIEW OF BAKE OVEN IN CELLAR (Note the double arch in front of the oven. The front arch supported the structural framing.) - James McCrea Houses, 108-110 Sansom Street, Philadelphia, Philadelphia County, PA

  6. [Association between aryl hydrocarbon receptor gene polymorphisms and chromosomal damage in coke-oven workers].

    PubMed

    Bin, Ping; Leng, Shuguang; Liang, Xuemiao; Cheng, Juan

    2007-11-01

    To investigate the association of single nucleotide polymorphisms (SNPs) or haplotypes of aryl hydrocarbon receptor (AHR) gene and chromosomal damage in peripheral blood lymphocytes among coke-oven workers. Eighty-nine coke-oven workers exposed to a high level of polycyclic aromatic hydrocarbons (PAHs) and sixty non-exposed workers were selected as the study subjects. Urinary 1-hydroxypyrene (1-OHPyr) levels were measured as the internal dose of PAHs exposure. The chromosomal damage in peripheral lymphocyte was measured by the cytokinesis-block micronucleus (CBMN) assay. Two SNPs in AHR gene, including rs6960165, rs2282885 were detected by PCR-RFLP. The AHR haplotypes were estimated by Bayesian statistical method with the software of PHASE Version 2.1. The associations between SNPs or haplotypes pairs and CBMN were assessed by analysis of covariance in the coke-oven workers and non-exposed workers. The level of 1-OHPyr among coke-oven workers was significantly higher than that among non-exposed workers (P < 0.01). The CBMN among coke-oven workers was significantly higher than that among non-exposed workers (P < 0.01). After adjusting the age and the level of 1-OHPyr, the different SNPs of AHR gene rs6960165 in coke-oven workers were related to the CBMN frequencies (P = 0.014), but no association between the different SNPs of AHR gene rs2282885 and the rates of CBMN was observed in coke-oven workers (P = 0.586), either in the controls (P = 0.308 and P = 0.415, respectively), the haplotypes in coke-oven workers were significantly related to the rates of CBMN (P = 0.007), while there was no significant association in non-exposed workers (P = 0.768). Our results suggested that SNPs rs6960165 or haplotypes of AHR were associated with the CBMN frequencies in coke-oven workers.

  7. TWO OF THE FORTYSIX EXTANT BEEHIVE COKE OVENS CONSTRUCTED BY ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    TWO OF THE FORTY-SIX EXTANT BEEHIVE COKE OVENS CONSTRUCTED BY JOHN NUTTALL DURING THE EARLY 1870S, LOOKING NORTHWEST - Nuttallburg Mine Complex, Coke Ovens, North side of New River, 2.7 miles upstream from Fayette Landing, Lookout, Fayette County, WV

  8. 4. DETAIL VIEW OF OVEN NO. 7 LOOKING NORTH, SHOWING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    4. DETAIL VIEW OF OVEN NO. 7 LOOKING NORTH, SHOWING REFRACTORY BRICK OF ARCHED OPENING READING 'H-W 8-61 48 ARCH' (HARBISON-WALKER) - Lucernemines Coke Works, Coke Ovens, 0.5 mile East of Lucerne, adjacent, Lucerne Mines, Indiana County, PA

  9. Feasibility study analysis for multi-function dual energy oven (case study: tapioca crackers small medium enterprise)

    NASA Astrophysics Data System (ADS)

    Soraya, N. W.; El Hadi, R. M.; Chumaidiyah, E.; Tripiawan, W.

    2017-12-01

    Conventional drying process is constrained by weather (cloudy / rainy), and requires wide drying area, and provides low-quality product. Multi-function dual energy oven is the appropriate technology to solve these problems. The oven uses solar thermal or gas heat for drying various type of products, including tapioca crackers. Investment analysis in technical, operational, and financial aspects show that the multi-function dual energy oven is feasible to be implemented for small medium enterprise (SME) processing tapioca crackers.

  10. Microwave Cooking Practices in Minnesota Food Service Establishments.

    PubMed

    Hedeen, Nicole; Reimann, David; Everstine, Karen

    2016-03-01

    Uneven cooking due to consumer use of microwave ovens to cook food products that have been prepared but are not ready to eat has been a documented risk factor in several foodborne disease outbreaks. However, the use of microwave ovens in restaurants and other food service establishments has not been well documented. The aim of this study was to describe the types of food service establishments that use microwave ovens, how these ovens are used, types of foods heated or cooked in these ovens, types of microwave ovens used in food service establishments, and the level of compliance with U.S. Food and Drug Administration (FDA) guidelines. From 2008 to 2009, the Minnesota Department of Health collected data from a convenience sample of 60 food establishments within the state. Facility types included fast-food restaurants, sit-down restaurants, school food service, nursing homes, hotels and motels, and daycare centers. Food preparation practices were classified as prep-serve, cookserve, or complex. Minnesota environmental health specialists administered a study questionnaire to managers during routine inspections. Establishments included in this study reported using microwave ovens primarily to warm commercial ready-to-eat products (67%) and to warm foods for palatability (50%). No minimum temperatures are required for these processes because these foods do not require pathogen destruction. However, food establishments using complex preparation practices more often reported using microwave ovens for multiple processes and for processes that require pathogen destruction. For establishments that did report microwave oven use for food requiring pathogen destruction, the majority of managers reported following most FDA recommendations for cooking and reheating for hot-holding potentially hazardous foods, but many did not report letting food stand for 2 min after cooking. Additional training on stand time after microwave cooking could be beneficial because of low reporting of this practice among study participants.

  11. 40 CFR 63.301 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS FOR SOURCE CATEGORIES National Emission Standards for Coke... implement the provisions of this subpart or its designated agent). Brownfield coke oven battery means a new coke oven battery that replaces an existing coke oven battery or batteries with no increase in the...

  12. 40 CFR 63.301 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS FOR SOURCE CATEGORIES National Emission Standards for Coke... implement the provisions of this subpart or its designated agent). Brownfield coke oven battery means a new coke oven battery that replaces an existing coke oven battery or batteries with no increase in the...

  13. 40 CFR 63.301 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS FOR SOURCE CATEGORIES National Emission Standards for Coke... implement the provisions of this subpart or its designated agent). Brownfield coke oven battery means a new coke oven battery that replaces an existing coke oven battery or batteries with no increase in the...

  14. 40 CFR 63.301 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS FOR SOURCE CATEGORIES National Emission Standards for Coke... implement the provisions of this subpart or its designated agent). Brownfield coke oven battery means a new coke oven battery that replaces an existing coke oven battery or batteries with no increase in the...

  15. Influence of electrical and hybrid heating on bread quality during baking.

    PubMed

    Chhanwal, N; Ezhilarasi, P N; Indrani, D; Anandharamakrishnan, C

    2015-07-01

    Energy efficiency and product quality are the key factors for any food processing industry. The aim of the study was to develop energy and time efficient baking process. The hybrid heating (Infrared + Electrical) oven was designed and fabricated using two infrared lamps and electric heating coils. The developed oven can be operated in serial or combined heating modes. The standardized baking conditions were 18 min at 220°C to produce the bread from hybrid heating oven. Effect of baking with hybrid heating mode (H-1 and H-2, hybrid oven) on the quality characteristics of bread as against conventional heating mode (C-1, pilot scale oven; C-2, hybrid oven) was studied. The results showed that breads baked in hybrid heating mode (H-2) had higher moisture content (28.87%), higher volume (670 cm(3)), lower crumb firmness value (374.6 g), and overall quality score (67.0) comparable to conventional baking process (68.5). Moreover, bread baked in hybrid heating mode showed 28% reduction in baking time.

  16. Binder Jetting: A Novel NdFeB Bonded Magnet Fabrication Process

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Paranthaman, M. Parans; Shafer, Christopher S.; Elliott, Amy M.

    2016-04-05

    Our goal of this research is to fabricate near-net-shape isotropic (Nd) 2Fe 14B-based (NdFeB) bonded magnets using a three dimensional printing process to compete with conventional injection molding techniques used for bonded magnets. Additive manufacturing minimizes the waste of critical materials and allows for the creation of complex shapes and sizes. The binder jetting process works similarly to an inkjet printer. A print-head passes over a bed of NdFeB powder and deposits a polymer binding agent to bind the layer of particles together. The bound powder is then coated with another layer of powder, building the desired shape in successivemore » layers of bonded powder. Upon completion, the green part and surrounding powders are placed in an oven at temperatures between 100°C and 150°C for 4–6 h to cure the binder. After curing, the excess powder can be brushed away to reveal the completed “green” part. Green magnet parts were then infiltrated with a clear urethane resin to achieve the measured density of the magnet of 3.47 g/cm 3 close to 46% relative to the NdFeB single crystal density of 7.6 g/cm 3. Magnetic measurements indicate that there is no degradation in the magnetic properties. In conclusion, this study provides a new pathway for preparing near-net-shape bonded magnets for various magnetic applications.« less

  17. Surface modification of commercial seawater reverse osmosis membranes by grafting of hydrophilic monomer blended with carboxylated multiwalled carbon nanotubes

    NASA Astrophysics Data System (ADS)

    Vatanpour, Vahid; Zoqi, Naser

    2017-02-01

    In this study, modification of commercial seawater reverse osmosis membranes was carried out with simultaneous use of surface grafting and nanoparticle incorporation. Membrane grafting with a hydrophilic acrylic acid monomer and thermal initiator was used to increase membrane surface hydrophilicity. The used nanomaterial was carboxylated multiwalled carbon nanotubes (MWCNTs), which were dispersed in the grafting solution and deposited on membrane surface to reduce fouling by creating polymer brushes and hydrodynamic resistance. Effectiveness of the grafting process (formation of graft layer on membrane surface) was proved by Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM) analyses. Increase of membrane surface hydrophilicity was approved with contact angle test. First, the grafting was performed on the membrane surfaces with different monomer concentrations, various contact times and several membrane curing times (three variables for optimization). The modified membranes were tested by a cross-flow setup using saline solution for permeability and rejection tests, and bovine serum albumin (BSA) solution for fouling test. The results showed that the modified membranes with 0.75 M of monomer, 3 min contact time and 80 min curing time in an oven at 50 °C presented the highest flux and lowest rejection decline related to the commercial reverse osmosis membrane. In the next step, the optimum grafting condition was selected and the nanotubes with different weight percentages were dispersed in the acrylic acid monomer solution. The membrane containing 0.25 wt% COOH-MWCNTs showed the highest fouling resistance.

  18. Volumetric dimensional changes of dental light-cured dimethacrylate resins after sorption of water or ethanol.

    PubMed

    Sideridou, Irini D; Karabela, Maria M; Vouvoudi, Evagelia Ch

    2008-08-01

    This study evaluated the influence of water and ethanol sorption on the volumetric dimensional changes of resins prepared by light curing of Bis-GMA, Bis-EMA, UDMA, TEGDMA or D(3)MA. The resin specimens (15mm diameterx1mm height) were immersed in water or ethanol 37+/-1 degrees C for 30 days. Volumetric changes of specimens were obtained via accurate mass measurements using Archimedes principle. The specimens were reconditioned by dry storage in an oven at 37+/-1 degrees C until constant mass was obtained and then immersed in water or ethanol for 30 days. The volumetric changes of specimens were determined and compared to those obtained from the first sorption. Resins showed similar volume increase during the first and second sorptions of water or ethanol. The volume increase due to water absorption is in the following order: poly-TEGDMA>poly-Bis-GMA>poly-UDMA>poly-Bis-EMA>poly-D(3)MA. On the contrary, the order in ethanol is poly-Bis-GMA>poly-UDMA>poly-TEGDMA>poly-Bis-EMA approximately poly-D(3)MA. The volume increase was found to depend linearly on the amount of water or ethanol absorbed. In the choice of monomers for preparation of composite resin matrix the volume increase in the resin after immersion in water or ethanol must be taken into account. Resins of Bis-EMA and D(3)MA showed the lowest values.

  19. 27. VIEW LOOKING THROUGH A RECTANGULAR COKE OVEN. NOTE THE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    27. VIEW LOOKING THROUGH A RECTANGULAR COKE OVEN. NOTE THE USE OF BOTH BRICK AND STONE IN THE CONSTRUCTION OF THE OVEN. - Tower Hill No. 2 Mine, Approximately 0.47 mile Southwest of intersection of Stone Church Road & Township Route 561, Hibbs, Fayette County, PA

  20. 75 FR 42579 - Energy Conservation Program for Consumer Products: Test Procedure for Microwave Ovens; Repeal of...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-07-22

    ... the usable baking space. If there is a selector switch for selecting the mode of operation of the oven, set it for normal baking. If an oven permits baking by either forced convection by using a fan, or...

  1. Fight for survival: the life of a Hansen's disease sufferer through his correspondence with Adolpho Lutz.

    PubMed

    Benchimol, Jaime Larry; Sá, Magali Romero; Alves da Cruz, Mônica de Souza; Magalhàes de Andrade, Márcio

    2003-01-01

    This project presents the complete set of letters between the family of a Hansen's disease (leprosy) sufferer in the state of Maranhão, in the Northeast of Brazil, and the doctor and bacteriologist Adolpho Lutz. For more than twenty years Fabricio Caldas de Oliveira and Numa Pires de Oliveira, father and son, exchanged a steady flow of letters with the scientist in pursuit of a cure for the disease that had assailed Numa since childhood. The 24 letters compiled here paint a unique portrait of the medical and social drama confronted by this family, and the results of the use of chaulmoogra oil and other medications in their search for alternative treatments.

  2. 21. VIEW OF A SINGLE BEEHIVE COKE OVEN. THE USE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    21. VIEW OF A SINGLE BEEHIVE COKE OVEN. THE USE OF BRICK AND STONE TO FACE THE OVEN WAS A TYPICAL CONSTRUCTION TECHNIQUE. - Tower Hill No. 2 Mine, Approximately 0.47 mile Southwest of intersection of Stone Church Road & Township Route 561, Hibbs, Fayette County, PA

  3. 40 CFR 63.313 - Implementation and enforcement.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Standards for Coke Oven Batteries § 63.313 Implementation and enforcement. (a) This subpart can be... shall notify the coke oven battery owner or operator that inspections and performance tests shall be... Administrator shall give the coke oven battery owner or operator at least 15 days notice that implementation...

  4. 40 CFR 63.7330 - What are my monitoring requirements?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... each baghouse applied to pushing emissions from a coke oven battery, you must at all times monitor the...(i). (e) For each by-product coke oven battery, you must monitor at all times the opacity of...

  5. 40 CFR 63.309 - Performance tests and procedures.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Standards for Coke Oven Batteries § 63.309 Performance tests and procedures. (a) Except as otherwise... coke oven battery, the results of which shall be used in accordance with procedures specified in this subpart to determine compliance with each of the applicable visible emission limitations for coke oven...

  6. 40 CFR 63.312 - Existing regulations and requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.312 Existing regulations and requirements. (a) The..., topside port lids, coke oven doors, and charging operations in effect on September 15, 1992, or which have... method of monitoring in effect on September 15, 1992, and that ensures coke oven emission reductions...

  7. 40 CFR 63.312 - Existing regulations and requirements.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.312 Existing regulations and requirements. (a) The..., topside port lids, coke oven doors, and charging operations in effect on September 15, 1992, or which have... method of monitoring in effect on September 15, 1992, and that ensures coke oven emission reductions...

  8. 40 CFR 63.309 - Performance tests and procedures.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Standards for Coke Oven Batteries § 63.309 Performance tests and procedures. (a) Except as otherwise... coke oven battery, the results of which shall be used in accordance with procedures specified in this subpart to determine compliance with each of the applicable visible emission limitations for coke oven...

  9. 40 CFR 63.306 - Work practice standards.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Standards for Coke Oven Batteries § 63.306 Work practice standards. (a) Work practice plan. On or before... plan for each coke oven battery. The plan shall be designed to achieve compliance with visible emission limitations for coke oven doors, topside port lids, offtake systems, and charging operations under this...

  10. 40 CFR 63.313 - Implementation and enforcement.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Standards for Coke Oven Batteries § 63.313 Implementation and enforcement. (a) This subpart can be... shall notify the coke oven battery owner or operator that inspections and performance tests shall be... Administrator shall give the coke oven battery owner or operator at least 15 days notice that implementation...

  11. 40 CFR 63.313 - Implementation and enforcement.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Standards for Coke Oven Batteries § 63.313 Implementation and enforcement. (a) This subpart can be... shall notify the coke oven battery owner or operator that inspections and performance tests shall be... Administrator shall give the coke oven battery owner or operator at least 15 days notice that implementation...

  12. 40 CFR 63.312 - Existing regulations and requirements.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.312 Existing regulations and requirements. (a) The..., topside port lids, coke oven doors, and charging operations in effect on September 15, 1992, or which have... method of monitoring in effect on September 15, 1992, and that ensures coke oven emission reductions...

  13. 40 CFR 63.312 - Existing regulations and requirements.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.312 Existing regulations and requirements. (a) The..., topside port lids, coke oven doors, and charging operations in effect on September 15, 1992, or which have... method of monitoring in effect on September 15, 1992, and that ensures coke oven emission reductions...

  14. 40 CFR 63.306 - Work practice standards.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... for Coke Oven Batteries § 63.306 Work practice standards. (a) Work practice plan. On or before... plan for each coke oven battery. The plan shall be designed to achieve compliance with visible emission limitations for coke oven doors, topside port lids, offtake systems, and charging operations under this...

  15. 40 CFR 63.310 - Requirements for startups, shutdowns, and malfunctions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... CATEGORIES National Emission Standards for Coke Oven Batteries § 63.310 Requirements for startups, shutdowns... or operator shall operate and maintain the coke oven battery and its pollution control equipment... operator of a coke oven battery shall develop, according to paragraph (c) of this section, a written...

  16. 40 CFR 63.306 - Work practice standards.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Standards for Coke Oven Batteries § 63.306 Work practice standards. (a) Work practice plan. On or before... plan for each coke oven battery. The plan shall be designed to achieve compliance with visible emission limitations for coke oven doors, topside port lids, offtake systems, and charging operations under this...

  17. 40 CFR 63.306 - Work practice standards.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Standards for Coke Oven Batteries § 63.306 Work practice standards. (a) Work practice plan. On or before... plan for each coke oven battery. The plan shall be designed to achieve compliance with visible emission limitations for coke oven doors, topside port lids, offtake systems, and charging operations under this...

  18. 40 CFR 63.309 - Performance tests and procedures.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Standards for Coke Oven Batteries § 63.309 Performance tests and procedures. (a) Except as otherwise... coke oven battery, the results of which shall be used in accordance with procedures specified in this subpart to determine compliance with each of the applicable visible emission limitations for coke oven...

  19. 40 CFR 63.7330 - What are my monitoring requirements?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... each baghouse applied to pushing emissions from a coke oven battery, you must at all times monitor the...(i). (e) For each by-product coke oven battery, you must monitor at all times the opacity of...

  20. 40 CFR 63.313 - Implementation and enforcement.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Standards for Coke Oven Batteries § 63.313 Implementation and enforcement. (a) This subpart can be... shall notify the coke oven battery owner or operator that inspections and performance tests shall be... Administrator shall give the coke oven battery owner or operator at least 15 days notice that implementation...

  1. 40 CFR 63.312 - Existing regulations and requirements.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.312 Existing regulations and requirements. (a) The..., topside port lids, coke oven doors, and charging operations in effect on September 15, 1992, or which have... method of monitoring in effect on September 15, 1992, and that ensures coke oven emission reductions...

  2. 40 CFR 63.7330 - What are my monitoring requirements?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... each baghouse applied to pushing emissions from a coke oven battery, you must at all times monitor the...(i). (e) For each by-product coke oven battery, you must monitor at all times the opacity of...

  3. 40 CFR 63.309 - Performance tests and procedures.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Standards for Coke Oven Batteries § 63.309 Performance tests and procedures. (a) Except as otherwise... coke oven battery, the results of which shall be used in accordance with procedures specified in this subpart to determine compliance with each of the applicable visible emission limitations for coke oven...

  4. 40 CFR 63.7330 - What are my monitoring requirements?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... baghouse applied to pushing emissions from a coke oven battery, you must at all times monitor the relative...(i). (e) For each by-product coke oven battery, you must monitor at all times the opacity of...

  5. 40 CFR 63.313 - Implementation and enforcement.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Standards for Coke Oven Batteries § 63.313 Implementation and enforcement. (a) This subpart can be... shall notify the coke oven battery owner or operator that inspections and performance tests shall be... Administrator shall give the coke oven battery owner or operator at least 15 days notice that implementation...

  6. 40 CFR 63.309 - Performance tests and procedures.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Standards for Coke Oven Batteries § 63.309 Performance tests and procedures. (a) Except as otherwise... coke oven battery, the results of which shall be used in accordance with procedures specified in this subpart to determine compliance with each of the applicable visible emission limitations for coke oven...

  7. 76 FR 65631 - Energy Conservation Program: Test Procedures for Microwave Ovens

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-10-24

    ... Conservation Program: Test Procedures for Microwave Ovens AGENCY: Office of Energy Efficiency and Renewable... (DOE) has initiated a test procedure rulemaking to develop active mode testing methodologies for... Federal Register a final rule for the microwave oven test procedure rulemaking (July TP repeal final rule...

  8. 78 FR 4015 - Energy Conservation Program: Test Procedures for Microwave Ovens

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-01-18

    ... Conservation Program: Test Procedures for Microwave Ovens AGENCY: Office of Energy Efficiency and Renewable... Energy (DOE) issued a supplemental notice of proposed rulemaking (SNOPR) to amend the test procedures for microwave ovens. That SNOPR proposed amendments to the DOE test procedure to incorporate provisions from the...

  9. Physics of the Microwave Oven

    ERIC Educational Resources Information Center

    Vollmer, Michael

    2004-01-01

    This is the first of two articles about the physics of microwave ovens. This article deals with the generation of microwaves in the oven and includes the operation of the magnetrons, waveguides and standing waves in resonant cavities. It then considers the absorption of microwaves by foods, discussing the dielectric relaxation of water,…

  10. 76 FR 27610 - Approval and Promulgation of Air Quality Implementation Plans; Maryland; Adoption of Control...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-05-12

    ..., freezers, water heaters, dishwashers, trash compactors, air conditioners, ovens, microwave ovens, and other... appliance product. A large appliance product is also defined as any organic surface-coated metal range, oven, microwave, refrigerator, freezer, washer, dryer, dishwasher, water heater, or trash compactor manufactured...

  11. Modification of a Microwave Oven for Laboratory Use.

    ERIC Educational Resources Information Center

    Andrews, Judith; Atkinson, George F.

    1984-01-01

    Discusses use of a domestic microwave oven for drying analytical samples with time savings compared to conventional ovens, providing a solution to the problem of loss of load as samples dry. Presents a system for examining emitted gases from drying process and reports results of several test dryings. (JM)

  12. 40 CFR 86.317-79 - Hydrocarbon analyzer specifications.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... flame ionization detector (HFID) analyzer. (b) Option. A non-heated flame ionization detector (FID) that... temperature oven housing the detector and sample-handling components. It shall maintain temperature with 2 °C of the set point. The detector, oven, and sample-handling components within the oven shall be...

  13. 40 CFR 86.317-79 - Hydrocarbon analyzer specifications.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... flame ionization detector (HFID) analyzer. (b) Option. A non-heated flame ionization detector (FID) that... temperature oven housing the detector and sample-handling components. It shall maintain temperature with 2 °C of the set point. The detector, oven, and sample-handling components within the oven shall be...

  14. 40 CFR 86.317-79 - Hydrocarbon analyzer specifications.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... flame ionization detector (HFID) analyzer. (b) Option. A non-heated flame ionization detector (FID) that... temperature oven housing the detector and sample-handling components. It shall maintain temperature with 2 °C of the set point. The detector, oven, and sample-handling components within the oven shall be...

  15. 40 CFR 86.317-79 - Hydrocarbon analyzer specifications.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... flame ionization detector (HFID) analyzer. (b) Option. A non-heated flame ionization detector (FID) that... temperature oven housing the detector and sample-handling components. It shall maintain temperature with 2 °C of the set point. The detector, oven, and sample-handling components within the oven shall be...

  16. More Experiments with Microwave Ovens

    ERIC Educational Resources Information Center

    Vollmer, Michael; Mollmann, Klaus-Peter; Karstadt, Detlef

    2004-01-01

    Microwave ovens can be used to perform exciting demonstrations that illustrate a variety of physics topics. Experiments discussed here show superheating, visualize the inhomogeneous heating that takes place in a microwave and also show how to use a mobile phone to detect radiation leaking from the oven. Finally eggs can give some spectacular…

  17. 75 FR 8963 - Agency Information Collection Activities; Proposed Collection; Comment Request; Reporting and...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-02-26

    ... Annual Report'' FDA Form 3642 ``General Correspondence'' FDA Form 3643 ``Microwave Oven Products Annual... Television Products'' FDA Form 3660 ``Guidance for Preparing Reports on Radiation Safety of Microwave Ovens... ``Abbreviated Reports on Radiation Safety for Microwave Products (Other than Microwave Ovens)'' The most likely...

  18. Eating on Demand

    NASA Technical Reports Server (NTRS)

    1998-01-01

    Under subcontract to McDonnell-Douglas Corporation, Enersyst Development Center developed air impingement technology through oven designs for NASA's Space Station Freedom. Jets of hot air at the top and bottom of the oven are focused on the food, rather than heating the oven cavity as in a traditional thermal oven. By heating the food directly, foods cook faster and more consistently, retaining flavor and texture. Several companies have licensed this technology, including KRh Thermal Systems, which has introduced a line of Hot Choice vending machines. Enersyst has also licensed the first home application to Thermador.

  19. The effect of occupational exposure to benzo[a]pyrene on neurobehavioral function in coke oven workers.

    PubMed

    Qiu, Chongying; Peng, Bin; Cheng, Shuqun; Xia, Yinyin; Tu, Baijie

    2013-03-01

    Coke oven workers are regularly exposed to polycyclic aromatic hydrocarbons (PAHs). Benzo[a]pyrene (B[a]P), known as an indicator species for PAH contamination, is a neurobehavioral toxicant. The purpose of the study was to evaluate the relationship between B[a]P exposure, a B[a]P-related urinary metabolite and neurobehavioral function among coke oven workers. Coke oven workers and oxygen factory workers participated in this study. B[a]P exposure was monitored by air sampling pump, and urinary 1-hydroxypyrene (1-OHP) level was detected with high performance liquid chromatography (HPLC). A questionnaire and the neurobehavioral core test battery (NCTB) were administered to all subjects. B[a]P-exposed workers were found to have higher urinary 1-OHP levels and worse NCTB performances on eight items than control workers. B[a]P concentrations were higher in the coke oven plant than that in the controls' workplace. The performances on simple reaction time, correct pursuit aiming, and error pursuit aiming decreased with increasing airborne B[a]P in coke oven workers. There were significant correlations between urinary 1-OHP level and six items of the NCTB. Occupational exposure to B[a]P is associated with neurobehavioral function impairment in coke oven workers. Copyright © 2012 Wiley Periodicals, Inc.

  20. Calibration and standardization of microwave ovens for fixation of brain and peripheral nerve tissue.

    PubMed

    Login, G R; Leonard, J B; Dvorak, A M

    1998-06-01

    Rapid and reproducible fixation of brain and peripheral nerve tissue for light and electron microscopy studies can be done in a microwave oven. In this review we report a standardized nomenclature for diverse fixation techniques that use microwave heating: (1) microwave stabilization, (2) fast and ultrafast primary microwave-chemical fixation, (3) microwave irradiation followed by chemical fixation, (4) primary chemical fixation followed by microwave irradiation, and (5) microwave fixation used in various combinations with freeze fixation. All of these methods are well suited to fix brain tissue for light microscopy. Fast primary microwave-chemical fixation is best for immunoelectron microscopy studies. We also review how the physical characteristics of the microwave frequency and the dimensions of microwave oven cavities can compromise microwave fixation results. A microwave oven can be calibrated for fixation when the following parameters are standardized: irradiation time; water load volume, initial temperature, and placement within the oven; fixative composition, volume, and initial temperature; and specimen container shape and placement within the oven. Using two recently developed calibration tools, the neon bulb array and the agar-saline-Giemsa tissue phantom, we report a simple calibration protocol that identifies regions within a microwave oven for uniform microwave fixation. Copyright 1998 Academic Press.

  1. [Cohort study of effects on lung function of coke oven workers exposured to coke oven emissions].

    PubMed

    Zhi, Yongfen; Zhang, Hongming; Li, Weixing; Hu, Zhipeng; Liu, Weihua; Li, Yangfan; Zheng, Jinpin

    2015-07-01

    Through comparative study on pulmonary function damage of coke oven workers exposed to coke oven emissions with the same group before and after five years, and further explore the relationship between the coke oven emissions and injury in pulmonary function of coke oven worker. Select a coking plant in Shanxi 165 coke oven workers (exposed group) and 52 auxiliary workers (control group) for the study, using a uniform questionnaire to collect workers' personal information. Fixed workplace air samples collected periodically. Air samples of benzo (a) pyrene concentrations was measured by high pressure liquid chromatograph. Pulmonary function of research object was measured by portable spirometer respectively in 2009 and 2013, and comparative analysis on it. The concentration of B(a)P was no significant difference in the same area between 5 years in 2009-2013. Compared with 2009, 2013 control workers lung function index and the abnormal rate had no significant difference (P > 0.05). But FVC%, FEV1.0%, MVV%, VC% and FEF25% of exposed workers in 2013 was significantly lower than in 2009, FVC%, FEV1.0%, VC% and FEF25% pulmonary dysfunction rate in 2013 was also significantly higher than in 2009, difference was statistically significant (P < 0.05). Workers emerging pulmonary function abnormalities mainly distributed in furnace roof and side. furnace roof group FVC%, FEV1.0%, VC% additional abnormal number (rate) was significantly higher than furnace floor and the control group (P < 0.05), and furnace side groop was significantly higher than the control group, the difference was statistically significant (P < 0.05). Multivariate Logistic regression analysis showed that after 5 years FVC%, FEV1% and VC% of abnormal lung function emerging adjusted OR of furnace roof workers were 7.939, 5.966 and 4.956. For abnormal of FVC%, FEV1%, VC% and MVV%, the contacting coke seniority is a risk factor. There is a positive interaction between contacting coke seniority and furnace roof (P < 0.05). Coke oven workers lung function damage associated with exposureing to coke oven emissions, coke oven emissions exposure level and exposure time are the main factors of coke oven workers in lung function damage, there is a positive interaction between the two factors.

  2. SU-E-T-112: Experimental Characterization of a Novel Thermal Reservoir for Consistent and Accurate Annealing of High-Sensitivity TLDs.

    PubMed

    Donahue, W; Bongiorni, P; Hearn, R; Rodgers, J; Nath, R; Chen, Z

    2012-06-01

    To develop and characterize a novel thermal reservoir for consistent and accurate annealing of high-sensitivity thermoluminescence dosimeters (TLD-100H) for dosimetry of brachytherapy sources. The sensitivity of TLD-100H is about 18 times that of TLD-100 which has clear advantages in for interstitial brachytherapy sources. However, the TLD-100H requires a short high temperature annealing cycle (15 min.) and opening and closing the oven door causes significant temperature fluctuations leading to unreliable measurements. A new thermal reservoir made of aluminum alloy was developed to provide stable temperature environment in a standard hot air oven. The thermal reservoir consisted of a 20 cm × 20 cm × 8 cm Al block with a machine-milled chamber in the middle to house the aluminum TLD holding tray. The thermal reservoir was placed inside the oven until it reaches thermal equilibrium with oven chamber. The temperatures of the oven chamber, heat reservoir, and TLD holding tray were monitored by two independent thermo-couples which interfaced digitally to a control computer. A LabView interface was written for monitoring and recording the temperatures in TLD holding tray, the thermal reservoir, and oven chamber. The temperature profiles were measured as a function of oven-door open duration. The settings for oven chamber temperature and oven door open-close duration were optimized to achieve a stable temperature of 240 0C in the TLD holding tray. Complete temperature profiles of the TLD annealing tray over the entire annealing process were obtained. A LabView interface was written for monitoring and recording the temperatures in TLD holding The use of the thermal reservoir has significantly reduced the temperature fluctuations caused by the opening of oven door when inserting the TLD holding tray into the oven chamber. It has enabled consistent annealing of high-sensitivity TLDs. A comprehensive characterization of a custom-built novel thermal reservoir for annealing high-sensitivity TLD has been carried out. It enabled consistent and accurate annealing of high- sensitivity TLDs which could significantly improve the efficiency of brachytherapy source characterizations. Supported in part by NIH grant R01-CA134627. © 2012 American Association of Physicists in Medicine.

  3. Mortality due to respiratory cancers in the coke oven plants of the Lorraine coalmining industry (Houillères du Bassin de Lorraine).

    PubMed Central

    Bertrand, J P; Chau, N; Patris, A; Mur, J M; Pham, Q T; Moulin, J J; Morviller, P; Auburtin, G; Figueredo, A; Martin, J

    1987-01-01

    The main activity of the Houillères du Bassin de Lorraine (Lorraine Collieries), employing 23,000 operatives and executives, is coalmining. The coke production is carried out by two coke oven plants with a workforce of respectively 747 and 552 workers. The coal coking process entails the emission of noxious products such as polycyclic aromatic hydrocarbons (PAH) from the ovens. The influence of occupational exposure on mortality due to respiratory cancers, and particularly to lung and upper respiratory and alimentary tracts cancer, was investigated among a cohort of 534 male workers from the two coke oven plants who had retired from work between 1963 and 1982. The job history of each subject has been precisely reconstructed by indicating the duration of exposure on the ovens, close to the ovens, and in maintenance occupations. The cohort mortality has been analysed according to the method of indirect standardisation with reference to the French male population and by a case-control study concerning the consumption of tobacco per cohort. The mortality due to lung cancer is 2.51 times higher than expected. This excess of mortality differs, but not significantly, between the two coke oven plants (standardised mortality ratio equals 3.05 and 1.75 respectively). It is not significantly higher among subjects exposed for more than five years, directly exposed on the ovens or working near the ovens or at maintenance occupations on the ovens (SMR = 2.78), than among those exposed for less than five years (SMR = 2.35) or those not exposed at all. Even taking into account the excess of mortality due to lung cancers in the Moselle district (1.6 time that of France), the excess of lung cancers does not seem to be explained by the regional factor, or by tobacco and alcohol consumption. Although no significant relation was offered between lung cancer and the duration of exposure to PAH, even when taking smoking habits into account, the carcinogenic role of occupational nuisances cannot be excluded. PMID:3651355

  4. 40 CFR 63.7351 - Who implements and enforces this subpart?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...-product coke oven battery with vertical flues, fugitive pushing emissions in § 63.7292(a) for a by-product coke oven battery with horizontal flues, fugitive pushing emissions in § 63.7293 for a non-recovery...

  5. 40 CFR 63.307 - Standards for bypass/bleeder stacks.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Standards for Coke Oven Batteries § 63.307 Standards for bypass/bleeder stacks. (a)(1) Except as otherwise... flow generated by the battery, which shall thereafter be operated and maintained. (2) Coke oven... operator of a brownfield coke oven battery or a padup rebuild shall install such a flare system before...

  6. 40 CFR 63.7351 - Who implements and enforces this subpart?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...-product coke oven battery with vertical flues, fugitive pushing emissions in § 63.7292(a) for a by-product coke oven battery with horizontal flues, fugitive pushing emissions in § 63.7293 for a non-recovery...

  7. 40 CFR 63.7300 - What are my operation and maintenance requirements?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... operation and maintenance of new or existing by-product coke oven batteries. Each plan must address, at a... emissions from a new or existing coke oven battery. Each plan must address at a minimum the elements in...

  8. 40 CFR 63.7351 - Who implements and enforces this subpart?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...-product coke oven battery with vertical flues, fugitive pushing emissions in § 63.7292(a) for a by-product coke oven battery with horizontal flues, fugitive pushing emissions in § 63.7293 for a non-recovery...

  9. 40 CFR 63.307 - Standards for bypass/bleeder stacks.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.307 Standards for bypass/bleeder stacks. (a)(1.... (2) Coke oven emissions shall not be vented to the atmosphere through bypass/bleeder stacks, except.... (3) The owner or operator of a brownfield coke oven battery or a padup rebuild shall install such a...

  10. 40 CFR 63.307 - Standards for bypass/bleeder stacks.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.307 Standards for bypass/bleeder stacks. (a)(1.... (2) Coke oven emissions shall not be vented to the atmosphere through bypass/bleeder stacks, except.... (3) The owner or operator of a brownfield coke oven battery or a padup rebuild shall install such a...

  11. 40 CFR 63.7300 - What are my operation and maintenance requirements?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... operation and maintenance of new or existing by-product coke oven batteries. Each plan must address, at a... emissions from a new or existing coke oven battery. Each plan must address at a minimum the elements in...

  12. 40 CFR 63.7300 - What are my operation and maintenance requirements?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... operation and maintenance of new or existing by-product coke oven batteries. Each plan must address, at a... emissions from a new or existing coke oven battery. Each plan must address at a minimum the elements in...

  13. 40 CFR 63.307 - Standards for bypass/bleeder stacks.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Standards for Coke Oven Batteries § 63.307 Standards for bypass/bleeder stacks. (a)(1) Except as otherwise... flow generated by the battery, which shall thereafter be operated and maintained. (2) Coke oven... operator of a brownfield coke oven battery or a padup rebuild shall install such a flare system before...

  14. 40 CFR 63.7294 - What work practice standard must I meet for soaking?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... CATEGORIES (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing... standard must I meet for soaking? (a) For each new and existing by-product coke oven battery, you must... from raw coke oven gas leaking from the collecting main through the damper, and emissions that result...

  15. 40 CFR 63.7351 - Who implements and enforces this subpart?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...-product coke oven battery with vertical flues, fugitive pushing emissions in § 63.7292(a) for a by-product coke oven battery with horizontal flues, fugitive pushing emissions in § 63.7293 for a non-recovery...

  16. 40 CFR 63.307 - Standards for bypass/bleeder stacks.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... National Emission Standards for Coke Oven Batteries § 63.307 Standards for bypass/bleeder stacks. (a)(1.... (2) Coke oven emissions shall not be vented to the atmosphere through bypass/bleeder stacks, except.... (3) The owner or operator of a brownfield coke oven battery or a padup rebuild shall install such a...

  17. 40 CFR 63.7300 - What are my operation and maintenance requirements?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... operation and maintenance of new or existing by-product coke oven batteries. Each plan must address, at a... emissions from a new or existing coke oven battery. Each plan must address at a minimum the elements in...

  18. 40 CFR 63.7300 - What are my operation and maintenance requirements?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and... operation and maintenance of new or existing by-product coke oven batteries. Each plan must address, at a... emissions from a new or existing coke oven battery. Each plan must address at a minimum the elements in...

  19. 76 FR 72332 - Energy Conservation Program: Test Procedure for Microwave Ovens

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-11-23

    ... Energy Conservation Program: Test Procedure for Microwave Ovens AGENCY: Office of Energy Efficiency and.... Department of Energy (DOE) published an interim final rule on March 9, 2011, amending its test procedures for... standby mode and off mode power use by microwave ovens. Those amendments incorporated into the DOE test...

  20. 40 CFR 63.3176 - What definitions apply to this subpart?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... facility which assembles automobiles or light-duty trucks, including coating facilities and processes. Bake oven air seal means an entry or entry vestibule to or an exit or exit vestibule from a bake oven which isolates the bake oven from the area immediately preceding (for an entry or entry vestibule) or immediately...

  1. 40 CFR 63.3176 - What definitions apply to this subpart?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... facility which assembles automobiles or light-duty trucks, including coating facilities and processes. Bake oven air seal means an entry or entry vestibule to or an exit or exit vestibule from a bake oven which isolates the bake oven from the area immediately preceding (for an entry or entry vestibule) or immediately...

  2. Portable oven air circulator

    DOEpatents

    Jorgensen, Jorgen A.; Nygren, Donald W.

    1983-01-01

    A portable air circulating apparatus for use in cooking ovens which is used to create air currents in the oven which transfer heat to cooking foodstuffs to promote more rapid and more uniform cooking or baking, the apparatus including a motor, fan blade and housing of metallic materials selected from a class of heat resistant materials.

  3. 40 CFR 63.3176 - What definitions apply to this subpart?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... facility which assembles automobiles or light-duty trucks, including coating facilities and processes. Bake oven air seal means an entry or entry vestibule to or an exit or exit vestibule from a bake oven which isolates the bake oven from the area immediately preceding (for an entry or entry vestibule) or immediately...

  4. 21 CFR 1030.10 - Microwave ovens.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... interlock on a fully assembled microwave oven shall not be operable by any part of the human body, or any... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Microwave ovens. 1030.10 Section 1030.10 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) RADIOLOGICAL...

  5. 21 CFR 1030.10 - Microwave ovens.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... interlock on a fully assembled microwave oven shall not be operable by any part of the human body, or any... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Microwave ovens. 1030.10 Section 1030.10 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) RADIOLOGICAL...

  6. Energy Use and Quality of Foods Cooked by Different Appliances.

    ERIC Educational Resources Information Center

    Odland, Dianne; And Others

    1987-01-01

    The authors compared energy consumption, cooking time, and quality of five foods cooked using electric range surface units and oven, induction cooktop, electric frypan, microwave oven, and toaster oven. The induction cooktop was among the most energy conserving. For most products, cooking treatment had little impact on quality. (Author/CH)

  7. 40 CFR 63.300 - Applicability.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ..., the provisions of this subpart apply to existing by-product coke oven batteries at a coke plant and to..., 1995, for existing by-product coke oven batteries subject to emission limitations in § 63.302(a)(1) or..., 2003, for existing by-product coke oven batteries subject to emission limitations in § 63.302(a)(2); (3...

  8. 40 CFR 63.7352 - What definitions apply to this subpart?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... standards; storm water runoff and production area clean up water except for water from the by-product...-product coke oven battery means a group of ovens connected by common walls, where coal undergoes destructive distillation under positive pressure to produce coke and coke oven gas from which by-products are...

  9. Effect of six different cooking techniques in the nutritional composition of two fish species previously selected as optimal for renal patient's diet.

    PubMed

    Castro-González, Isabel; Maafs-Rodríguez, Ana Gabriela; Pérez-Gil Romo, Fernando

    2015-07-01

    Benefits of fish consumption are widely known, but there is little information about nutrient values of raw and cooked fish. The aim was to study the impact that six cooking techniques have on the nutritional composition of two fish species with low content of adverse nutrients in renal diet. Raw and steamed, foiled with aluminum, foiled with banana leaf, gas oven-baked, microwave oven-coked and fried lightly samples were chemically analyzed to determine their protein, phosphorus and lipid content. Crevalle jack: all methods increased lipid and protein content and fatty acids (FA) varied in all cooking methods. Phosphorus decreased in the steamed and microwave oven-cooked samples. Red drum: foiled and fried lightly increased lipid content compared to the raw sample. FA concentration changed in all cooking methods. Protein increased with every technique and phosphorus decreased in the steamed and gas oven-baked samples. Renal patients should preferably consume crevalle jack steamed or microwave oven-cooked and red drum steamed or gas oven-baked.

  10. Study of hydroxymethylfurfural and furfural formation in cakes during baking in different ovens, using a validated multiple-stage extraction-based analytical method.

    PubMed

    Petisca, Catarina; Henriques, Ana Rita; Pérez-Palacios, Trinidad; Pinho, Olívia; Ferreira, Isabel M P L V O

    2013-12-15

    A procedure for extraction of hydroxymethylfurfural (HMF) and furfural from cakes was validated. Higher yield was achieved by multiple step extraction with water/methanol (70/30) and clarification with Carrez I and II reagents. Oven type and baking time strongly influenced HMF, moisture and volatile profile of model cakes, whereas furfural content was not significantly affected. No correlation was found between these parameters. Baking time influenced moisture and HMF formation in cakes from traditional and microwave ovens but not in steam oven cakes. Significant moisture decrease and HMF increase (3.63, 9.32, and 41.9 mg kg(-1)dw at 20, 40 and 60 min, respectively) were observed during traditional baking. Cakes baked by microwave also presented a significant increase of HMF (up to 16.84 mg kg(-1)dw at 2.5 min). Steam oven cakes possessed the highest moisture content and no significant differences in HMF and furfural. This oven is likely to form low HMF and furfural, maintaining cake moisture and aroma compounds. Copyright © 2013 Elsevier Ltd. All rights reserved.

  11. A Wireless Portable High Temperature Data Monitor for Tunnel Ovens

    PubMed Central

    Bayón, Ricardo Mayo; González Suárez, Víctor M.; Martín, Felipe Mateos; Lopera Ronda, Juan M.; Álvarez Antón, Juan C.

    2014-01-01

    Tunnel ovens are widely used in the food industry to produce biscuits and pastries. In order to obtain a high quality product, it is very important to control the heat transferred to each piece of dough during baking. This paper proposes an innovative, non-distorting, low cost wireless temperature measurement system, called “eBiscuit”, which, due to its size, format and location in the metal rack conveyor belt in the oven, is able to measure the temperature a real biscuit experience while baking. The temperature conditions inside the oven are over 200 °C for several minutes, which could damage the “eBiscuit” electronics. This paper compares several thermal insulating materials that can be used in order to avoid exceeding the maximum operational conditions (80 °C) in the interior of the “eBiscuit. The data registered is then transmitted to a base station where information can be processed to obtain an oven model. The experimental results with real tunnel ovens confirm its good performance, which allows detecting production anomalies early on. PMID:25120161

  12. Benzo[a]pyrene-induced neurobehavioral function and neurotransmitter alterations in coke oven workers.

    PubMed

    Niu, Qiao; Zhang, Hongmei; Li, Xin; Li, Meiqin

    2010-07-01

    To study alterations in neurobehavioral function and neurotransmitter levels in coke oven workers occupationally exposed to benzo[a]pyrene (B[a]P) and explore possible biomarkers of B[a]P neurotoxicity. 176 coke oven workers occupationally exposed to B[a]P and 48 warehouse workers (controls) were investigated by questionnaire. Emotional and cognitive function was investigated using the WHO/NCTB. B[a]P concentrations in the working environment, concentrations of monoamine and amino acid neurotransmitters, and levels of urinary 1-hydroxypyrene (1-OH-Py) were assayed by HPLC. Spectrophotometry was used to determine choline neurotransmitter concentrations. Airborne B[a]P concentrations were higher in the coke oven plant than in the controls' workplace, and 1-OH-Py levels were significantly increased in coke workers compared to controls (p=0.000). Digital span and order digital span scores indicated that learning and memory were significantly decreased in coke oven workers (p=0.006). Concentrations of norepinephrine (NE), dopamine, 5-hydroxytryptamine and homovanillic acid were lower, while levels of 5-hydroxyindoleacetic acid were higher in the exposed group compared to controls; the difference in NE was significant (p=0.000). Aspartic acid and gamma-aminobutyric acid levels were significantly decreased in coke oven workers compared to controls (p=0.004 and p=0.004). Acetylcholine (Ach) concentration was four- to fivefold greater in coke oven workers than in controls, while acetylcholine esterase (AchE) activity was significantly decreased (p=0.000 and p=0.012). Statistical analysis showed that digital span and order digital span scores were negatively correlated to Ach and positively correlated to AchE. Occupational B[a]P exposure may reduce coke oven workers' neurobehavioral function and monoamine, amino acid and choline neurotransmitter levels. Moreover, Ach and AchE correlated with neurobehavioral function; AchE has poor specificity, but Ach is a potential biomarker of B[a]P neurotoxicity in coke oven workers.

  13. RESOLVE OVEN Field Demonstration Unit for Lunar Resource Extraction

    NASA Technical Reports Server (NTRS)

    Paz, Aaron; Oryshchyn, Lara; Jensen, Scott; Sanders, Gerald B.; Lee, Kris; Reddington, Mike

    2013-01-01

    The Oxygen and Volatile Extraction Node (OVEN) is a subsystem within the Regolith & Environment Science and Oxygen & Lunar Volatile Extraction (RESOLVE) project. The purpose of the OVEN subsystem is to release volatiles from lunar regolith and extract oxygen by means of a hydrogen reduction reaction. The complete process includes receiving, weighing, sealing, heating, and disposing of core sample segments while transferring all gaseous contents to the Lunar Advanced Volatile Analysis (LAVA) subsystem. This document will discuss the design and performance of the OVEN Field Demonstration Unit (FDU), which participated in the 2012 RESOLVE field demonstration.

  14. Cross sectional study on lung function of coke oven workers: a lung function surveillance system from 1978 to 1990

    PubMed Central

    Wu, J; Kreis, I; Griffiths, D; Darling, C

    2002-01-01

    Aims: To determine the association between lung function of coke oven workers and exposure to coke oven emissions. Methods: Lung function data and detailed work histories for workers in recovery coke ovens of a steelworks were extracted from a lung function surveillance system. Multiple regressions were employed to determine significant predictors for lung function indices. The first sets of lung function tests for 613 new starters were pooled to assess the selection bias. The last sets of lung function tests for 834 subjects with one or more year of coke oven history were pooled to assess determinants of lung function. Results: Selection bias associated with the recruitment process was not observed among the exposure groups. For subjects with a history of one or more years of coke oven work, each year of working in the most exposed "operation" position was associated with reductions in FEV1 of around 9 ml (p = 0.006, 95% CI: 3 ml to 16 ml) and in FVC of around 12 ml (p = 0.002, 95% CI: 4 ml to 19 ml). Negative effects of smoking on lung function were also observed. Conclusions: Exposure to coke oven emissions was found to be associated with lower FEV1 and FVC. Effects of work exposure on lung function are similar to those found in other studies. PMID:12468747

  15. 40 CFR 761.72 - Scrap metal recovery ovens and smelters.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 31 2011-07-01 2011-07-01 false Scrap metal recovery ovens and..., AND USE PROHIBITIONS Storage and Disposal § 761.72 Scrap metal recovery ovens and smelters. Any person... § 761.60(b), metal surfaces in PCB remediation waste regulated under § 761.61, or metal surfaces in PCB...

  16. 40 CFR 63.7328 - How do I demonstrate initial compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance...); (b) You will operate each by-product coke oven battery and each capture system and control device applied to pushing emissions from a coke oven battery according to the procedures in the plans beginning...

  17. 40 CFR 63.7328 - How do I demonstrate initial compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial...); (b) You will operate each by-product coke oven battery and each capture system and control device applied to pushing emissions from a coke oven battery according to the procedures in the plans beginning...

  18. 40 CFR 63.7328 - How do I demonstrate initial compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial...); (b) You will operate each by-product coke oven battery and each capture system and control device applied to pushing emissions from a coke oven battery according to the procedures in the plans beginning...

  19. 76 FR 52350 - Coke Oven Emissions Standard; Extension of the Office of Management and Budget's (OMB) Approval...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-08-22

    ... DEPARTMENT OF LABOR Occupational Safety and Health Administration [Docket No. OSHA-2011-0181] Coke... requirements specified in the Standard on Coke Oven Emissions (29 CFR 1910.1029). DATES: Comments must be... obtaining information (29 U.S.C. 657). The information collection requirements in the Coke Oven Emissions...

  20. 40 CFR 63.7327 - How do I demonstrate initial compliance with the work practice standards that apply to me?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance... me? (a) For each by-product coke oven battery with vertical flues subject to the work practice...-product coke oven battery with horizontal flues subject to the work practice standards for fugitive...

  1. 40 CFR 63.7327 - How do I demonstrate initial compliance with the work practice standards that apply to me?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance... me? (a) For each by-product coke oven battery with vertical flues subject to the work practice...-product coke oven battery with horizontal flues subject to the work practice standards for fugitive...

  2. 40 CFR 63.7335 - How do I demonstrate continuous compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous... maintenance requirements that apply to me? (a) For each by-product coke oven battery, you must demonstrate... each coke oven battery with a capture system or control device applied to pushing emissions, you must...

  3. 40 CFR 63.7328 - How do I demonstrate initial compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial...); (b) You will operate each by-product coke oven battery and each capture system and control device applied to pushing emissions from a coke oven battery according to the procedures in the plans beginning...

  4. 40 CFR 63.7335 - How do I demonstrate continuous compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous... maintenance requirements that apply to me? (a) For each by-product coke oven battery, you must demonstrate... each coke oven battery with a capture system or control device applied to pushing emissions, you must...

  5. 40 CFR 98.172 - GHGs to report.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... combustion units include, but are not limited to, by-product recovery coke oven battery combustion stacks... flares that burn blast furnace gas or coke oven gas according to the procedures in § 98.253(b)(1) of...)(B) and § 98.253(b)(1)(iii)(C), you must use the default CO2 emission factors for coke oven gas and...

  6. 40 CFR 63.7327 - How do I demonstrate initial compliance with the work practice standards that apply to me?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance... me? (a) For each by-product coke oven battery with vertical flues subject to the work practice...-product coke oven battery with horizontal flues subject to the work practice standards for fugitive...

  7. 40 CFR 63.7328 - How do I demonstrate initial compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial...); (b) You will operate each by-product coke oven battery and each capture system and control device applied to pushing emissions from a coke oven battery according to the procedures in the plans beginning...

  8. 40 CFR 63.7335 - How do I demonstrate continuous compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous... maintenance requirements that apply to me? (a) For each by-product coke oven battery, you must demonstrate... each coke oven battery with a capture system or control device applied to pushing emissions, you must...

  9. 40 CFR 63.7335 - How do I demonstrate continuous compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous... maintenance requirements that apply to me? (a) For each by-product coke oven battery, you must demonstrate... each coke oven battery with a capture system or control device applied to pushing emissions, you must...

  10. 40 CFR 63.7327 - How do I demonstrate initial compliance with the work practice standards that apply to me?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance... me? (a) For each by-product coke oven battery with vertical flues subject to the work practice...-product coke oven battery with horizontal flues subject to the work practice standards for fugitive...

  11. 40 CFR 98.172 - GHGs to report.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... combustion units include, but are not limited to, by-product recovery coke oven battery combustion stacks... flares that burn blast furnace gas or coke oven gas according to the procedures in § 98.253(b)(1) of...)(B) and § 98.253(b)(1)(iii)(C), you must use the default CO2 emission factors for coke oven gas and...

  12. 40 CFR 98.172 - GHGs to report.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... combustion units include, but are not limited to, by-product recovery coke oven battery combustion stacks... except you must use the default CO2 emission factors for coke oven gas and blast furnace gas from Table C... flares according to the requirements in § 98.33(c)(2) using the emission factors for coke oven gas and...

  13. 40 CFR 98.172 - GHGs to report.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... combustion units include, but are not limited to, by-product recovery coke oven battery combustion stacks... flares that burn blast furnace gas or coke oven gas according to the procedures in § 98.253(b)(1) of...)(B) and § 98.253(b)(1)(iii)(C), you must use the default CO2 emission factors for coke oven gas and...

  14. 40 CFR 98.172 - GHGs to report.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... combustion units include, but are not limited to, by-product recovery coke oven battery combustion stacks... flares that burn blast furnace gas or coke oven gas according to the procedures in § 98.253(b)(1) of...)(B) and § 98.253(b)(1)(iii)(C), you must use the default CO2 emission factors for coke oven gas and...

  15. 40 CFR 63.7335 - How do I demonstrate continuous compliance with the operation and maintenance requirements that...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous... maintenance requirements that apply to me? (a) For each by-product coke oven battery, you must demonstrate... each coke oven battery with a capture system or control device applied to pushing emissions, you must...

  16. Evaluation of biomarkers in plasma, blood, and urine samples from coke oven workers: significance of exposure to polycyclic aromatic hydrocarbons.

    PubMed Central

    Ovrebø, S; Haugen, A; Farmer, P B; Anderson, D

    1995-01-01

    OBJECTIVE--The aim was to assess the significance of two biomarkers; antibody to benzo(a)pyrene DNA adducts and concentration of hydroxyethylvaline haemoglobin adducts in samples from a well studied group of coke oven workers. As a measure of exposure we have used 1-hydroxypyrene in urine. METHODS--Urine and blood samples were collected from coke oven workers and a control group. Samples from coke oven plant workers were collected in January and June. 1-Hydroxypyrene was measured in urine by high performance liquid chromatography (HPLC), antibodies to benzo(a)pyrene DNA adducts were measured by ELISA and hydroxyethylvaline haemoglobin adducts were measured by gas chromatography-mass spectrometry (GC-MS). RESULTS--Mean urinary 1-hydroxypyrene in samples from coke oven workers varied from 1.11 to 5.53 umol/mol creatinine and 0.14 umol/mol creatinine in the control group. Workers at the top side had the highest values of urinary 1-hydroxypyrene. Antibody to benzo(a)pyrene DNA adducts did not correlate with either 1-hydroxypyrene nor length of work at the coke oven plant. But antibody concentration in samples collected in January was predictive of the concentration in samples collected in June. A small non-significant increase in hydroxyethylvaline haemoglobin adducts was found in samples from coke oven workers relative to the control group when comparing smokers and nonsmokers separately. CONCLUSION--1-Hydroxypyrene correlates well with exposure groups based on job description. Antibodies to benzo(a)-pyrene DNA adducts was related to people and not exposure. Work at a coke oven plant might lead to increased hydroxyethylvaline haemoglobin adducts. PMID:8535495

  17. [Health risk assessment of coke oven PAHs emissions].

    PubMed

    Bo, Xin; Wang, Gang; Wen, Rou; Zhao, Chun-Li; Wu, Tie; Li, Shi-Bei

    2014-07-01

    Polycyclic aromatic hydrocarbons (PAHs) produced by coke oven are with strong toxicity and carcinogenicity. Taken typical coke oven of iron and steel enterprises as the case study, the dispersion and migration of 13 kinds of PAHs emitted from coke oven were analyzed using AERMOD dispersion model, the carcinogenic and non-carcinogenic risks at the receptors within the modeling domain were evaluated using BREEZE Risk Analyst and the Human Health Risk Assessment Protocol for Hazardous Waste Combustion (HHRAP) was followed, the health risks caused by PAHs emission from coke oven were quantitatively evaluated. The results indicated that attention should be paid to the non-carcinogenic risk of naphthalene emission (the maximum value was 0.97). The carcinogenic risks of each single pollutant were all below 1.0E-06, while the maximum value of total carcinogenic risk was 2.65E-06, which may have some influence on the health of local residents.

  18. Analysis and numerical simulation research of the heating process in the oven

    NASA Astrophysics Data System (ADS)

    Chen, Yawei; Lei, Dingyou

    2016-10-01

    How to use the oven to bake delicious food is the most concerned problem of the designers and users of the oven. For this intent, this paper analyzed the heat distribution in the oven based on the basic operation principles and proceeded the data simulation of the temperature distribution on the rack section. Constructing the differential equation model of the temperature distribution changes in the pan when the oven works based on the heat radiation and heat transmission, based on the idea of utilizing cellular automation to simulate heat transfer process, used ANSYS software to proceed the numerical simulation analysis to the rectangular, round-cornered rectangular, elliptical and circular pans and giving out the instantaneous temperature distribution of the corresponding shapes of the pans. The temperature distribution of the rectangular and circular pans proves that the product gets overcooked easily at the corners and edges of rectangular pans but not of a round pan.

  19. 40 CFR 63.7327 - How do I demonstrate initial compliance with the work practice standards that apply to me?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance Requirements § 63.7327... each by-product coke oven battery with vertical flues subject to the work practice standards for... than the compliance date that is specified in § 63.7283. (b) For each by-product coke oven battery with...

  20. 40 CFR 63.7324 - What procedures must I use to demonstrate initial compliance with the opacity limits?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance Requirements § 63.7324... of 15 percent for a by-product coke oven battery on a normal coking cycle or 20 percent for a by-product coke oven battery on batterywide extended coking, follow the test methods and procedures in...

  1. 40 CFR 63.7324 - What procedures must I use to demonstrate initial compliance with the opacity limits?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance Requirements § 63.7324... of 15 percent for a by-product coke oven battery on a normal coking cycle or 20 percent for a by-product coke oven battery on batterywide extended coking, follow the test methods and procedures in...

  2. 40 CFR 63.7324 - What procedures must I use to demonstrate initial compliance with the opacity limits?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance Requirements § 63.7324... of 15 percent for a by-product coke oven battery on a normal coking cycle or 20 percent for a by-product coke oven battery on batterywide extended coking, follow the test methods and procedures in...

  3. 40 CFR 63.7324 - What procedures must I use to demonstrate initial compliance with the opacity limits?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance Requirements § 63.7324... of 15 percent for a by-product coke oven battery on a normal coking cycle or 20 percent for a by-product coke oven battery on batterywide extended coking, follow the test methods and procedures in...

  4. Reference method for total water in lint cotton by automated oven drying combined with volumetric Karl Fischer titration

    USDA-ARS?s Scientific Manuscript database

    In a preliminary study to measure total water in lint cotton we demonstrated that volumetric Karl Fischer Titration of moisture transported by a carrier gas from an attached small oven is more accurate than standard oven drying in air. The objective of the present study was to assess the measuremen...

  5. Understanding the bias between moisture content by oven drying and water content by Karl Fischer titration at moisture equilibrium

    USDA-ARS?s Scientific Manuscript database

    Multiple causes of the difference between equilibrium moisture and water content have been found. The errors or biases were traced to the oven drying procedure to determine moisture content. The present paper explains the nature of the biases in oven drying and how it is possible to suppress one ...

  6. 40 CFR 63.7292 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? (a...

  7. 40 CFR 63.7291 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? (a...

  8. 40 CFR 63.7291 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? (a...

  9. 40 CFR 63.7292 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? (a...

  10. 40 CFR 63.7291 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? (a...

  11. 40 CFR 63.7292 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? (a...

  12. 40 CFR 63.7292 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? (a...

  13. 40 CFR 63.7291 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? (a...

  14. 40 CFR 63.7292 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with horizontal flues? (a...

  15. 40 CFR 63.7291 - What work practice standards must I meet for fugitive pushing emissions if I have a by-product...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? 63...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... meet for fugitive pushing emissions if I have a by-product coke oven battery with vertical flues? (a...

  16. Cooked yields, color, tenderness, and sensory traits of beef roasts cooked in an oven with steam generation versus a commercial convection oven to different endpoint temperatures.

    PubMed

    Bowers, L J; Dikeman, M E; Murray, L; Stroda, S L

    2012-10-01

    A CVap steam generation oven was compared with a Blodgett convection oven to examine effects on yields, cooked color, tenderness, and sensory traits of beef Longissimus lumborum (LL), Deep pectoralis (DP), and Biceps femoris (BF) muscles cooked to 1 of 3 temperatures (65.6, 71.1, or 76.7°C). Four roasts were cooked in the CVap for a constant time, and 2 roasts were cooked in the Blodgett until they reached target temperatures (3 replications). Cooking yields were higher (P<0.05) for BF and LL roasts in the CVap. Slice shear force (SSF) for BF roasts was lowest (P<0.05) in the CVap but lowest (P<0.05) for DP roasts in the Blodgett. No oven effect (P>0.05) was found for LL roasts. Sensory tenderness for BF roasts in the CVap was higher (P<0.05) than those in the Blodgett. Juiciness was higher (P<0.05) for LL roasts in the Blodgett. The CVap oven offers some tenderization (BF) and cooking yield advantages (BF and DP) over forced-air convection cooking. Copyright © 2012 Elsevier Ltd. All rights reserved.

  17. Frequency Distribution in Domestic Microwave Ovens and Its Influence on Heating Pattern.

    PubMed

    Luan, Donglei; Wang, Yifen; Tang, Juming; Jain, Deepali

    2017-02-01

    In this study, snapshots of operating frequency profiles of domestic microwave ovens were collected to reveal the extent of microwave frequency variations under different operation conditions. A computer simulation model was developed based on the finite difference time domain method to analyze the influence of the shifting frequency on heating patterns of foods in a microwave oven. The results showed that the operating frequencies of empty and loaded domestic microwave ovens varied widely even among ovens of the same model purchased on the same date. Each microwave oven had its unique characteristic operating frequencies, which were also affected by the location and shape of the load. The simulated heating patterns of a gellan gel model food when heated on a rotary plate agreed well with the experimental results, which supported the reliability of the developed simulation model. Simulation indicated that the heating patterns of a stationary model food load changed with the varying operating frequency. However, the heating pattern of a rotary model food load was not sensitive to microwave frequencies due to the severe edge heating overshadowing the effects of the frequency variations. © 2016 Institute of Food Technologists®.

  18. [Aerosol size distribution of organic carbon and elemental carbon on the top of coke oven and in the plant area].

    PubMed

    Liu, Xiao-Feng; Peng, Lin; Bai, Hui-Ling; Mu, Ling; Song, Chong-Fang

    2013-08-01

    In order to investigate the characteristic of organic carbon (OC) and elemental carbon (EC) in particles on the top of coke oven and in the plant area, the particle matter samples of five size fraction including < or = 1.4 microm, 1.4-2.1 microm, 2.1-4.2 microm, 4.2-10.2 microm and > or = 10.2 microm were collected using Staplex234 cascade impactor, and OC and EC were analyzed by Elementar Analysensysteme GmbH vario EL cube. The mass concentrations of OC and EC associated with TSP on the top of coke oven were 291.6 microg x m(-3) and 255.1 microg x m(-3), while those in the plant area were 377.8 microg x m(-3) and 151.7 microg x m(-3). The mass concentration of secondary organic carbon (SOC) in particles with size of < or = 1.4 microm was 147.3 microg x m(-3) in the plant area. The value of OC/EC in particles less than 2.1 microm was 1.3 on the top of coke oven. The mass concentration of EC in TSP in the plant area was lower than that on the top of coke oven, while the mass concentration of OC in the plant area was significantly higher than that on the top of coke oven. The mass concentrations of OC and EC associated with particles less than 10.2 microm in the plant area were far higher than those in the atmosphere of area where the coke plant is located. The OC and EC in particles, which were collected both on the top of coke oven and in the plant area, were mainly enriched in fine particles. The size distribution of OC showed a clear distinction between the coke oven top and the plant area, which revealed that OC in the plant area was more preferably enriched in fine particles than that on the top of coke oven, and the same size distribution of EC was found on the top of coke oven and in the plant area. In the plant area, the mass concentration of SOC and the contribution of SOC to OC increased with the decreasing diameter in particles with diameter of less than 10.2 microm.

  19. Synthesis and properties of hydroxy acrylic resin with high solid content

    NASA Astrophysics Data System (ADS)

    Yu, Zhen; Hu, Mingguang; Cui, Han; Xiao, Jijun

    2017-10-01

    Manufacturers of automotive repair finishes are tending to reduce more and more the level of volatile organic compounds in their paints in order to comply with increasingly strict environmental legislation. A high solid hydroxy acrylic resin was synthesised using CARDURA E10 and a type of hydroxyacrylic acid resin, its' acid value, hydroxylvalue, viscosity, structure, morphology was measured and film-forming properties after curing were characterised. The results show that the addition of CARDURA E10 in the copolymer composition significantly reduced the viscosity of the polymer system, improved the solid content of the resin and the physical properties of the coating. The hydroxyl acrylate resin with solid content of 90% and excellent comprehensive performance were successfully prepared by controlling the initiator dosage, polymerization temperature and monomer ratio.

  20. Impact of spatially correlated pore-scale heterogeneity on drying porous media

    NASA Astrophysics Data System (ADS)

    Borgman, Oshri; Fantinel, Paolo; Lühder, Wieland; Goehring, Lucas; Holtzman, Ran

    2017-07-01

    We study the effect of spatially-correlated heterogeneity on isothermal drying of porous media. We combine a minimal pore-scale model with microfluidic experiments with the same pore geometry. Our simulated drying behavior compares favorably with experiments, considering the large sensitivity of the emergent behavior to the uncertainty associated with even small manufacturing errors. We show that increasing the correlation length in particle sizes promotes preferential drying of clusters of large pores, prolonging liquid connectivity and surface wetness and thus higher drying rates for longer periods. Our findings improve our quantitative understanding of how pore-scale heterogeneity impacts drying, which plays a role in a wide range of processes ranging from fuel cells to curing of paints and cements to global budgets of energy, water and solutes in soils.

  1. Disinfection of Wastewater by Microwaves.

    DTIC Science & Technology

    1980-01-01

    used. Thermophilic B. stearothermophilus cells were used to try to determine if the mechanism of destruction was thermal. The microwave oven was set at...curve for E. coli B cells heated in a microwave oven temperature programed for 600 C ...... ............ 8 7. Survivor curve for B. stearothermophilus ...ATCC 12980 cells heated in a microwave oven temperature programed for 600 C. 98. Survivor curve for B. stearothermophilus AICC 12980 ........ 9 9

  2. Cooking with the Sun. How To Build and Use Solar Cookers.

    ERIC Educational Resources Information Center

    Halacy, Beth; Halacy, Dan

    For those working with solar energy and/or conservation and the careful use of resources, constructing a solar oven can be a fun and useful activity. This book describes the construction and use of solar ovens for cooking. Construction details are provided for two inexpensive solar ovens and a reflector hot plate that can then be used to cook 100…

  3. 40 CFR 63.7293 - What work practice standards must I meet for fugitive pushing emissions if I have a non-recovery...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... meet for fugitive pushing emissions if I have a non-recovery coke oven battery? 63.7293 Section 63.7293... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Emission... pushing emissions if I have a non-recovery coke oven battery? (a) You must meet the requirements in...

  4. 40 CFR 63.7293 - What work practice standards must I meet for fugitive pushing emissions if I have a non-recovery...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... meet for fugitive pushing emissions if I have a non-recovery coke oven battery? 63.7293 Section 63.7293... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Emission... pushing emissions if I have a non-recovery coke oven battery? (a) You must meet the requirements in...

  5. 40 CFR 63.7293 - What work practice standards must I meet for fugitive pushing emissions if I have a non-recovery...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... meet for fugitive pushing emissions if I have a non-recovery coke oven battery? 63.7293 Section 63.7293... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Emission... pushing emissions if I have a non-recovery coke oven battery? (a) You must meet the requirements in...

  6. 40 CFR 63.7293 - What work practice standards must I meet for fugitive pushing emissions if I have a non-recovery...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... meet for fugitive pushing emissions if I have a non-recovery coke oven battery? 63.7293 Section 63.7293... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Emission... pushing emissions if I have a non-recovery coke oven battery? (a) You must meet the requirements in...

  7. 40 CFR 63.7293 - What work practice standards must I meet for fugitive pushing emissions if I have a non-recovery...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... meet for fugitive pushing emissions if I have a non-recovery coke oven battery? 63.7293 Section 63.7293... Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Emission... pushing emissions if I have a non-recovery coke oven battery? (a) You must meet the requirements in...

  8. The effect of air thinning on dentin adhesive bond strength.

    PubMed

    Hilton, T J; Schwartz, R S

    1995-01-01

    The purpose of this study was to determine if air thinning three dentin adhesives would affect bond strength to dentin. Ninety human molars were mounted in acrylic and the occlusal surfaces ground to expose a flat dentin surface. Thirty teeth were randomly assigned to one of the following dentin bonding agent/composite combinations: A) Universal Bond 3/TPH (Caulk), B) All-Bond 2/Bis-Fil-P (Bisco), and C) Scotchbond Multi-Purpose/Z-100 (3m). The primers were applied following the manufacturers' instructions. The adhesives were applied by two methods. A thin layer of adhesive was applied with a brush to 15 specimens in each group and light cured. Adhesive was brushed on to the remaining 15 teeth in the group, air thinned for 3 seconds, and then polymerized. The appropriate composite was applied in 2 mm increments and light cured utilizing a 5 mm-in-diameter split Teflon mold. Following 3 months of water storage, all groups were shear tested to failure on an Instron Universal Testing Machine. Bond strength was significantly higher in all groups when the dentin bonding agent was painted on without being air thinned. Scotchbond Multi-Purpose had significantly higher bond strength than All-Bond 2, which had significantly higher bond strength than Universal Bond 3.

  9. [The working environment control of anhydride hardeners from an epoxy resin system].

    PubMed

    Matsumoto, Naomi; Yokota, Kozo; Johyama, Yasushi; Takakura, Toshiyuki

    2003-07-01

    Epoxy resins are widely used in adhesives, coatings, materials for molds and composites, and encapsulation. Acid anhydrides such as methyltetrahydrophthalic anhydride are being used as curing agents for epoxy resins. The anhydride hardeners are well-known industrial inhalant allergens, inducing predominantly type I allergies. In the electronic components industry, these substances have been consumed in large quantities. Therefore, safe use in the industry demands control of the levels of exposure causing allergic diseases in the workshop. We conducted a prospective survey of two electronics plants to clarify how to control the atmospheric level of the anhydrides in the work environment. Measurements of the levels of the anhydrides in air started according to the Working Environment Measurement Standards (Ministry of Labour Notification No. 46, 1976) in April 2000, along with improvements in the work environment. A value of 40 micrograms/m3 was adopted as the administrative control level to judge the propriety of the working environment control. A total of 2 unit work areas in both plants belonged to Control Class III. The exposure originated from manual loading, casting, uncured hot resins, and leaks in an impregnating-machine or curing ovens. In order to achieve the working environment control, complete enclosure of the source, installation of local exhaust ventilation, and improvement or maintenance of the local exhaust ventilation system were performed on the basis of the results of the working environment measurement, with the result that the work environment was improved (Control Class I). It became evident that these measures were effective just like other noxious substances.

  10. Operational test of micro-oven for 48Ca beam

    NASA Astrophysics Data System (ADS)

    Ozeki, K.; Kageyama, T.; Kidera, M.; Higurashi, Y.; Nakagawa, T.

    2014-02-01

    In order to supply a high-intensity and stable 48Ca beam from the RIKEN 18-GHz electron cyclotron resonance ion source, we are conducting operational tests of a micro-oven. A mixture of CaO and Al powders is placed into the crucible of the micro-oven and heated to produce metallic calcium by a reductive reaction. The successful production of a calcium beam was confirmed. In addition, we reduced the material consumption rate by using a so-called "hot liner," and we enhanced the beam intensity by applying a negative voltage bias to the micro-oven, the effect of which is similar to the effect of a "biased disk."

  11. Apparatus for making photovoltaic devices

    DOEpatents

    Foote, James B.; Kaake, Steven A. F.; Meyers, Peter V.; Nolan, James F.

    1994-12-13

    A process and apparatus (70) for making a large area photovoltaic device (22) that is capable of generating low cost electrical power. The apparatus (70) for performing the process includes an enclosure (126) providing a controlled environment in which an oven (156) is located. At least one and preferably a plurality of deposition stations (74,76,78) provide heated vapors of semiconductor material within the oven (156) for continuous elevated temperature deposition of semiconductor material on a sheet substrate (24) including a glass sheet (26) conveyed within the oven. The sheet substrate (24) is conveyed on a roller conveyor (184) within the oven (156) and the semiconductor material whose main layer (82) is cadmium telluride is deposited on an upwardly facing surface (28) of the substrate by each deposition station from a location within the oven above the roller conveyor. A cooling station (86) rapidly cools the substrate (24) after deposition of the semiconductor material thereon to strengthen the glass sheet of the substrate.

  12. Cancer mortality among coke oven workers.

    PubMed Central

    Redmond, C K

    1983-01-01

    The OSHA standard for coke oven emissions, which went into effect in January 1977, sets a permissible exposure limit to coke oven emissions of 150 micrograms/m3 benzene-soluble fraction of total particulate matter (BSFTPM). Review of the epidemiologic evidence for the standard indicates an excess relative risk for lung cancer as high as 16-fold in topside coke oven workers with 15 years of exposure or more. There is also evidence for a consistent dose-response relationship in lung cancer mortality when duration and location of employment at the coke ovens are considered. Dose-response models fitted to these same data indicate that, while excess risks may still occur under the OSHA standard, the predicted levels of increased relative risk would be about 30-50% if a linear dose-response model is assumed and 3-7% if a quadratic model is assumed. Lung cancer mortality data for other steelworkers suggest the predicted excess risk has probably been somewhat overestimated, but lack of information on important confounding factors limits further dose-response analysis. PMID:6653539

  13. A blackbody-pumped CO2-N2 transfer laser

    NASA Astrophysics Data System (ADS)

    Deyoung, R. J.; Higdon, N. S.

    1984-08-01

    A compact blackbody-pumped CO2-N2 transfer laser was constructed and the significant operating parameters were investigated. Lasing was achieved at 10.6 microns by passing preheated N2 through a 1.5-mm-diameter nozzle to a laser cavity where the N2 was mixed with CO2 and He. An intrinsic efficiency of 0.7 percent was achieved for an oven temperature of 1473 K and N2 oven pressure of 440 torr. The optimum laser cavity consisted of a back mirror with maximum reflectivity and an output mirror with 97.5-percent reflectivity. The optimum gas mixture was 1CO2/.5He/6N2. The variation of laser output was measured as a function of oven temperature, nozzle diameter, N2 oven pressure, He and CO2 partial pressures, nozzle-to-oven separation, laser cell temperature, and output laser mirror reflectivity. With these parameters optimized, outputs approaching 1.4 watts were achieved.

  14. Computational fluid dynamics modeling of bun baking process under different oven load conditions.

    PubMed

    Tank, A; Chhanwal, N; Indrani, D; Anandharamakrishnan, C

    2014-09-01

    A computational fluid dynamics (CFD) model was developed to study the temperature profile of the bun during baking process. Evaporation-condensation mechanism and effect of the latent heat during phase change of water was incorporated in this model to represent actual bun baking process. Simulation results were validated with experimental measurements of bun temperature at two different positions. Baking process is completed within 20 min, after the temperature of crumb become stable at 98 °C. Further, this study was extended to investigate the effect of partially (two baking trays) loaded and fully loaded (eight baking trays) oven on temperature profile of bun. Velocity and temperature profile differs in partially loaded and fully loaded oven. Bun placed in top rack showed rapid baking while bun placed in bottom rack showed slower baking due to uneven temperature distribution in the oven. Hence, placement of bun inside the oven affects temperature of bun and consequently, the quality of the product.

  15. Effectiveness of oxygen barrier oven bags in low temperature cooking on reduction of warmed-over flavor in beef roasts.

    PubMed

    Lepper-Blilie, A N; Berg, E P; Buchanan, D S; Keller, W L; Maddock-Carlin, K R; Berg, P T

    2014-03-01

    A 3×3×2 factorial was utilized to determine if roast size (small, medium, large), cooking method (open-pan, oven bag, vacuum bag), and heating process (fresh, reheated) prevented warmed-over flavor (WOF) in beef clod roasts. Fresh vacuum bag and reheated open-pan roasts had higher cardboardy flavor scores compared with fresh open-pan roast scores. Reheated roasts in oven and vacuum bags did not differ from fresh roasts for cardboardy flavor. Brothy and fat intensity were increased in reheated roasts in oven and vacuum bags compared with fresh roasts in oven and vacuum bags. Differences in TBARS were found in the interaction of heating process and roast size with the fresh and reheated large, and reheated medium roasts having the lowest values. Based on TBARS data, to prevent WOF in reheated beef roasts, a larger size roast in a cooking bag is the most effective method. Copyright © 2013 Elsevier Ltd. All rights reserved.

  16. A blackbody-pumped CO2-N2 transfer laser

    NASA Technical Reports Server (NTRS)

    Deyoung, R. J.; Higdon, N. S.

    1984-01-01

    A compact blackbody-pumped CO2-N2 transfer laser was constructed and the significant operating parameters were investigated. Lasing was achieved at 10.6 microns by passing preheated N2 through a 1.5-mm-diameter nozzle to a laser cavity where the N2 was mixed with CO2 and He. An intrinsic efficiency of 0.7 percent was achieved for an oven temperature of 1473 K and N2 oven pressure of 440 torr. The optimum laser cavity consisted of a back mirror with maximum reflectivity and an output mirror with 97.5-percent reflectivity. The optimum gas mixture was 1CO2/.5He/6N2. The variation of laser output was measured as a function of oven temperature, nozzle diameter, N2 oven pressure, He and CO2 partial pressures, nozzle-to-oven separation, laser cell temperature, and output laser mirror reflectivity. With these parameters optimized, outputs approaching 1.4 watts were achieved.

  17. Process for making photovoltaic devices and resultant product

    DOEpatents

    Foote, James B.; Kaake, Steven A. F.; Meyers, Peter V.; Nolan, James F.

    1996-07-16

    A process and apparatus (70) for making a large area photovoltaic device (22) that is capable of generating low cost electrical power. The apparatus (70) for performing the process includes an enclosure (126) providing a controlled environment in which an oven (156) is located. At least one and preferably a plurality of deposition stations (74,76,78) provide heated vapors of semiconductor material within the oven (156) for continuous elevated temperature deposition of semiconductor material on a sheet substrate (24) including a glass sheet (26) conveyed within the oven. The sheet substrate (24) is conveyed on a roller conveyor (184) within the oven (156) and the semiconductor material whose main layer (82) is cadmium telluride is deposited on an upwardly facing surface (28) of the substrate by each deposition station from a location within the oven above the roller conveyor. A cooling station (86) rapidly cools the substrate (24) after deposition of the semiconductor material thereon to strengthen the glass sheet of the substrate.

  18. Process for making photovoltaic devices and resultant product

    DOEpatents

    Foote, James B.; Kaake, Steven A. F.; Meyers, Peter V.; Nolan, James F.

    1995-11-28

    A process and apparatus (70) for making a large area photovoltaic device (22) that is capable of generating low cost electrical power. The apparatus (70) for performing the process includes an enclosure (126) providing a controlled environment in which an oven (156) is located. At least one and preferably a plurality of deposition stations (74,76,78) provide heated vapors of semiconductor material within the oven (156) for continuous elevated temperature deposition of semiconductor material on a sheet substrate (24) including a glass sheet (26) conveyed within the oven. The sheet substrate (24) is conveyed on a roller conveyor (184) within the oven (156) and the semiconductor material whose main layer (82) is cadmium telluride is deposited on an upwardly facing surface (28) of the substrate by each deposition station from a location within the oven above the roller conveyor. A cooling station (86) rapidly cools the substrate (24) after deposition of the semiconductor material thereon to strengthen the glass sheet of the substrate.

  19. Process for making photovoltaic devices and resultant product

    DOEpatents

    Foote, James B.; Kaake, Steven A. F.; Meyers, Peter V.; Nolan, James F.

    1993-09-28

    A process and apparatus (70) for making a large area photovoltaic device (22) that is capable of generating low cost electrical power. The apparatus (70) for performing the process includes an enclosure (126) providing a controlled environment in which an oven (156) is located. At least one and preferably a plurality of deposition stations (74,76,78) provide heated vapors of semiconductor material within the oven (156) for continuous elevated temperature deposition of semiconductor material on a sheet substrate (24) including a glass sheet (26) conveyed within the oven. The sheet substrate (24) is conveyed on a roller conveyor (184) within the oven (156) and the semiconductor material whose main layer (82) is cadmium telluride is deposited on an upwardly facing surface (28) of the substrate by each deposition station from a location within the oven above the roller conveyor. A cooling station (86) rapidly cools the substrate (24) after deposition of the semiconductor material thereon to strengthen the glass sheet of the substrate.

  20. Microwave Meat Roasting - A Computer Analysis for Cylindrical Roasts

    DTIC Science & Technology

    1977-07-01

    Temperatures for Various Oven Temperature Settings Table A2. Radiosity Values for Various Oven Temperature Settings Table A3. Radiant Energy Received by...the radiosities Jj, were written for the measured surface temperatures for each oven setting. Using the calculated radiosities , radiant heat...transfer to the roast was calculated by multiplying the difference in radiosities by the shape factor. Appendix A shows the details, and the slopes and

  1. Biomonitoring of polycyclic aromatic hydrocarbons from coke oven emissions and reproductive toxicity in nonsmoking workers.

    PubMed

    Jeng, Hueiwang Anna; Pan, Chih-Hong; Lin, Wen-Yi; Wu, Ming-Tsang; Taylor, Steven; Chang-Chien, Guo-Ping; Zhou, Guodong; Diawara, Norou

    2013-01-15

    The objective of the cross-sectional study was to assess whether exposure to polycyclic aromatic hydrocarbons (PAHs) from coke oven emissions contributed to alteration of semen quality and sperm DNA integrity in nonsmoking workers. Nonsmoking coke oven workers from a steel plant in Taiwan served as the exposure groups (topside-oven workers for the high exposure group and side-oven workers for the low exposure group), and administrators and security personnel in the plant served as the control. An exposure assessment was conducted to determine both particulate and gaseous phase of PAH levels and urinary 1-hydroxypyrene (1-OHP) levels. Semen quality was analyzed according to WHO guidelines. DNA fragmentation and bulky DNA adducts were measured to assess sperm DNA integrity. There was no significant difference in sperm concentrations, vitality, and DNA fragmentation between the exposed group and the control. The high exposure group experienced significantly lower percentages of normal morphology as compared with the control (p=0.0001). Bulky DNA adducts were detected in the exposed group that were significant higher than the control (p=0.04). Exposure to PAHs from coke-oven emissions could contribute to increased levels of bulky DNA adducts in sperm. Copyright © 2012 Elsevier B.V. All rights reserved.

  2. Temperature variations in sintering ovens for metal ceramic dental prostheses: non-destructive assessment using OCT

    NASA Astrophysics Data System (ADS)

    Sinescu, C.; Bradu, A.; Duma, V.-F.; Topala, F. I.; Negrutiu, M. L.; Podoleanu, A. G.

    2018-02-01

    We present a recent investigation regarding the use of optical coherence tomography (OCT) in the monitoring of the calibration loss of sintering ovens for the manufacturing of metal ceramic dental prostheses. Differences in the temperatures of such ovens with regard to their specifications lead to stress and even cracks in the prostheses material, therefore to the failure of the dental treatment. Evaluation methods of the ovens calibration consist nowadays of firing supplemental samples; this is subjective, expensive, and time consuming. Using an in-house developed swept source (SS) OCT system, we have demonstrated that a quantitative assessment of the internal structure of the prostheses, therefore of the temperature settings of the ovens can be made. Using en-face OCT images acquired at similar depths inside the samples, the differences in reflectivity allow for the evaluation of the differences in granulation (i.e., in number and size of ceramic grains) of the prostheses material. Fifty samples, divided in five groups, each sintered at different temperatures (lower, higher, or equal to the prescribed one) have been analyzed. The consequences of the temperature variations with regard to the one prescribed were determined. Rules-of-thumb were extracted to monitor objectively, using only OCT images of currently manufactured samples, the settings of the oven. The method proposed allows for avoiding producing prostheses with defects. While such rules-of-thumb achieve a qualitative assessment, an insight in our on-going work on the quantitative assessment of such losses of calibration on dental ovens using OCT is also made.

  3. Biodegradation of Fresh vs. Oven-Dried Inedible Crop Residue in a Continuously Stirred Tank Reactor

    NASA Technical Reports Server (NTRS)

    Crawford, Kamau; Strayer, Richard

    1998-01-01

    The degradation of soluble organics and mineral recovery from fresh and oven-dried biomass were compared in an Intermediate-Scale Aerobic Bioreactor (8 L working volume) to determine if drying crop residue improves performance in a continuously stirred tank reactor (CSTR). The study was conducted in an Intermediate-Scale Aerobic Bioreactor (ISAB) CSTR with dimensions of 390 mm height x 204 mm diameter. The pH in the bioreactor was controlled at 6.0, temperature at 30 C, and aeration at 7.0 L/min. Gases monitored were CO2 evolution and dissolved oxygen. Homogeneously mixed wheat cultures, used either fresh or oven-dried biomass and were leached, then placed in the ISAB for a 4-day degradation period. Studies found that mineral recovery was greater for leached oven-dried crop residue. However, after activity by the mixed microbial communities in the ISAB CSTR, there were little notable differences in the measured mineral recovery and degradation of soluble organic compounds. Degradation of soluble organic compounds was also shown to improve for leached oven-dried crop residue, but after mixing in the CSTR the degradation of the fresh biomass seemed to be slightly greater. Time for the biomass to turn in the CSTR appeared to be one factor for the experimental differences between the fresh and oven-dried biomass. Other factors, although not as defined, were the differing physical structures in the cell walls and varying microbial components of the fresh and oven-dried treatments due to changes in chemical composition after drying of the biomass.

  4. The Effect of Fermentation and Drying on Clicanthus Nutans Lindai Extract Chemical Constituents and Bioactivity

    NASA Astrophysics Data System (ADS)

    Lee, Y. Y.; Teh, P. S.; Kumaresan, S.; Tiong, C. H.

    2017-06-01

    In this study, two processes (fermentation and drying) were conducted on Clicanthus Nutans Lindau, which is well-known for its antioxidant activities. The aim of this research is to investigate the effects of these processes towards the Total Phenolic Content (TPC), antioxidant activity and the crude yield of the leaves. For the fermentation process, the fermentation time is varied for 6, 12, 24, 48 and 72 hours. For drying, oven drying (40, 45 and 50°C, freeze-drying and shade drying are investigated. Blanching was also conducted for oven dried samples (90°C for 1 minute). It was found that 12 hours fermentation produced the highest yield corresponding to Total Phenolic Content at 0.33 while 6 hours fermentation produced the highest Antioxidant Activity and yield at 2.218 x 10-10 mg/mL and 0.64 . On the other hand, 48 hours fermentation produced the highest overall extract yield at 0.64 . Analysis for antioxidant activity was carried out using 2,2-diphenyl-1-picrylhydrazyl (DPPH) and Folin-Ciocalteau method for Total Phenolic Content. Thermal inactivation kinetics (blanching) has been investigated for oven drying samples. Results showed that 40°C oven drying and 50°C oven drying with blanching has better retention of bioactive constituents. Blanching has no significant effect on phenolic content but has increased the crude extract for higher temperature oven drying. It has no positive effect on antioxidant activity. Drying is also a better processing method compared to fermentation as drying has slightly favorable results in all three aspects. Through comparison with extraction time of 60 minutes for 40°C oven drying and 6 hour fermented samples, yield of total phenolic content and overall yield of oven dried sample is higher than fermented sample by 4.14 and 0.39 respectively as well as showing better antioxidant activity.

  5. Coating Characterization with the Quartz Crystal Microbalance

    NASA Astrophysics Data System (ADS)

    Sturdy, Lauren F.

    The quartz crystal microbalance is a sensitive tool that can be used to measure the mass, modulus and phase angle of films of appropriate thicknesses. It is can be applied to systems with very varied properties, from liquid to solid, and under many different conditions. In this thesis its capabilities have been used to study the properties of several different systems of relevance to the coatings, art conservation, and rubber communities, in the process of which new techniques and tools were developed to analyze data and improve QCM data collection and experimental design. Alkyd resins, which have been used in artists' paints since the twentieth century, are the subject of the first studies. Alkyds are oil-modified polyesters. These resins are of interest because of their relatively recent use in art and how little is known of the mechanical properties in the early stages of cure. The QCM was shown to be sensitive to the curing process, changes in temperature, and mass change due to exposure to water. Kinetic studies during the first days of curing showed that the curing process can be divided into three regions. The first is dominated by solvent evaporation. In the second, oxygen absorption dominates and the mechanical properties change rapidly. The final stage extends from when the film is touch dry after about a day to years and is characterized by mass loss and continued increases in the modulus. Studying the curing at different temperatures revealed that the reactions do proceed much more rapidly at higher temperatures and an overall energy of activation was calculated for the curing process. The mechanical properties of alkyd resins containing zinc oxide, a white pigment, were studied with the QCM, nanoindentation and dynamic mechanical analysis. These measurements showed increases in the modulus with the inclusion of zinc oxide, and the QCM data showed that the second region started at earlier times as the pigment concentration was increased. Linseed oil is one of the starting materials for many alkyd resins and should cure similarly since the primary curing mechanisms are the same. It takes longer to cure than alkyds because it begins with no initial polymerization. Linseed oil was harder to study, as obtaining even films was difficult, multiple peaks at a single harmonic were observed, and the material properties during the early stages of curing led to a region where viscoelastic properties could not be calculated. To facilitate studying linseed oil, a multiple peak fitting method was developed to extract data from unusual peak shapes. With this ability, measurements at short times could be obtained despite poor film quality. Although linseed oil begins as a softer material than alkyds, its curing follows the same patterns as alkyd resins, exhibiting mass gain followed by mass loss, and sharp increases in modulus and decreases in phase angle during the early stages of curing. Having demonstrated the ability of the QCM to monitor curing, the QCM was also applied to uncrosslinked rubber systems. Rubbers, like the drying oils, contain double bonds which can react with oxygen, so first the oxidation of these materials was studied. In further studies oxidation was undesirable, so protocols were developed to limit oxidation. Measurements were made of homopolymers at different temperatures and the QCM measurements appear to be consistent with time-temperature superposition results obtained at lower frequencies. Blends of the various rubbers were studied and compared with models. The mechanical properties measured by the QCM were between the Voigt and Reuss predictions for most blends studied. Modeling the expected QCM response of layered rubbers matched the predictions of the Reuss model but not the measured values of the rubber blends, suggesting that the QCM is sensitive to different morphologies. Measurements with the QCM expanded our understanding of a variety of systems and proved to be a useful tool to measure mechanical changes during processes which are difficult to study by other methods.

  6. 26. DETAIL OF THE NORTH SIDE OF A RECTANGULAR COKE ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    26. DETAIL OF THE NORTH SIDE OF A RECTANGULAR COKE OVEN. THE OVENS ADDRESS, '140', APPEARS ABOVE THE CENTER OF THE OVEN. THE CUT STONES LINING THE OPENINGS ARE NUMBERED AND LABELED 'L' AND 'R', INDICATING THEIR PROPER PLACEMENT ALONG THE ARCH. THE CENTER STONE IS LABELED 'KEY.' - Tower Hill No. 2 Mine, Approximately 0.47 mile Southwest of intersection of Stone Church Road & Township Route 561, Hibbs, Fayette County, PA

  7. Effectiveness of the United Steel Workers of America Coke Oven Intervention Program.

    PubMed

    Parkinson, D K; Bromet, E J; Dew, M A; Dunn, L O; Barkman, M; Wright, M

    1989-05-01

    This paper describes the implementation and evaluation of the Coke Oven Intervention Program developed jointly by the United Steel Workers of America and the University of Pittsburgh. The program was offered on four occasions at each of seven coke oven plants over a 2-year period. Participants were compared with nonparticipating co-workers and controls from matched plants on knowledge of the Coke Oven Standard and workplace behaviors. Few baseline differences were found among participants, nonparticipants, and controls. Participants improved significantly as a result of the program, with those attending multiple programs accruing the greatest benefits. Panel controls interviewed on six occasions throughout the 2-year period showed little improvement. Reasons for and implications of the effectiveness of the program are discussed.

  8. Comparative carcinogenic potencies of particulates from diesel engine exhausts, coke oven emissions, roofing tar aerosols and cigarette smoke.

    PubMed Central

    Albert, R E

    1983-01-01

    Mammalian cell mutagenesis, transformation and skin tumorigenesis assays show similar results in comparing the potencies of diesel, coke oven, roofing tar and cigarette smoke particulates. These assay results are reasonably consistent with the comparative carcinogenic potencies of coke oven and roofing tar emissions as determined by epidemiological studies. The bacterial mutagenesis assay tends to show disproportionately high potencies, particularly with diesel particulates. Results to date encourage the approach to the assessment for carcinogenic risks from diesel emissions based on the use of epidemiological data on cancer induced by coke oven emissions, roofing tar particulates and cigarette smoke with the comparative potencies of these materials determined by in vivo and in vitro bioassays. PMID:6186481

  9. Dry, portable calorimeter for nondestructive measurement of the activity of nuclear fuel

    DOEpatents

    Beyer, Norman S.; Lewis, Robert N.; Perry, Ronald B.

    1976-01-01

    The activity of a quantity of heat-producing nuclear fuel is measured rapidly, accurately and nondestructively by a portable dry calorimeter comprising a preheater, an array of temperature-controlled structures comprising a thermally guarded temperature-controlled oven, and a calculation and control unit. The difference between the amounts of electric power required to maintain the oven temperature with and without nuclear fuel in the oven is measured to determine the power produced by radioactive disintegration and hence the activity of the fuel. A portion of the electronic control system is designed to terminate a continuing sequence of measurements when the standard deviation of the variations of the amount of electric power required to maintain oven temperature is within a predetermined value.

  10. Selective interference with pacemaker activity by electrical dental devices.

    PubMed

    Miller, C S; Leonelli, F M; Latham, E

    1998-01-01

    We sought to determine whether electromagnetic interference with cardiac pacemakers occurs during the operation of contemporary electrical dental equipment. Fourteen electrical dental devices were tested in vitro for their ability to interfere with the function of two Medtronics cardiac pacemakers (one a dual-chamber, bipolar Thera 7942 pacemaker, the other a single-chamber, unipolar Minix 8340 pacemaker). Atrial and ventricular pacemaker output and electrocardiographic activity were monitored by means of telemetry with the use of a Medtronics 9760/90 programmer. Atrial and ventricular pacing were inhibited by electromagnetic interference produced by the electrosurgical unit up to a distance of 10 cm, by the ultrasonic bath cleaner up to 30 cm, and by the magnetorestrictive ultrasonic scalers up to 37.5 cm. In contrast, operation of the amalgamator, electric pulp tester, composite curing light, dental handpieces, electric toothbrush, microwave oven, dental chair and light, ENAC ultrasonic instrument, radiography unit, and sonic scaler did not alter pacing rate or rhythm. These results suggest that certain electrosurgical and ultrasonic instruments may produce deleterious effects in medically fragile patients with cardiac pacemakers.

  11. Designing of Hybrid Structured Glass Laminated Transparent Nano Composites through Vacuum infusion Technique

    NASA Astrophysics Data System (ADS)

    Mukherji, A.; Tarapure, N. D.; Wakure, G. N.

    2017-05-01

    Glass is the most commonly used transparent material. However, glass is not suitable in applications where low weight, high strength is required. The present invention comprises a method of making a Transparent Glass Laminated Nano composite product. The product contains a Bidirectionally oriented E-Glass Fabric an essentially bidirectional yarn woven fabrics is stretched Bidirectionally by specially fabricated steel frame associated with both co and counter rotating device. These fibers include glass fibrics/cloths or mixtures of any of these. The synthetic fiber may be any synthetic silica based oven waived bi-directional or Uni-directional fabrics. Engaged gear provided in the device develops uniform tension on fabric, in both direction. Nano particle dispersed resin to be used is formulated with their respective curing agents and extenders. The formulated resin contains 0.1-0.5% of Nano additives and the product composed from 5-10 % of Glass fabric, between 10 to 20 % of ordinary glass, and between 60-80 % of the product is the Nano particles dispersed formulated resin, all measured by volume.

  12. Equipment for Hot-to-serve Foods

    NASA Technical Reports Server (NTRS)

    Smith, D. P.

    1985-01-01

    Patented surface heating devices with a much faster air-to-solid heat transfer rate than previous air ovens were developed. The accelerated surface heating can brown, sear or crisp much more rapidly than in conventional ovens so that partially prepared food can be finished quickly and tastefully immediately before serving. The crisp, freshly browned surfaces result from the faster heat transfer which does not dry out the food. The devices are then compared to convection ovens and microwave heating processes.

  13. Acoustic emission feedback control for control of boiling in a microwave oven

    DOEpatents

    White, Terry L.

    1991-01-01

    An acoustic emission based feedback system for controlling the boiling level of a liquid medium in a microwave oven is provided. The acoustic emissions from the medium correlated with surface boiling is used to generate a feedback control signal proportional to the level of boiling of the medium. This signal is applied to a power controller to automatically and continuoulsly vary the power applied to the oven to control the boiling at a selected level.

  14. Development of a high-temperature oven for the 28 GHz electron cyclotron resonance ion source.

    PubMed

    Ohnishi, J; Higurashi, Y; Kidera, M; Ozeki, K; Nakagawa, T

    2014-02-01

    We have been developing the 28 GHz ECR ion source in order to accelerate high-intensity uranium beams at the RIKEN RI-beam Factory. Although we have generated U(35+) beams by the sputtering method thus far, we began developing a high-temperature oven with the aim of increasing and stabilizing the beams. Because the oven method uses UO2, a crucible must be heated to a temperature higher than 2000 °C to supply an appropriate amount of UO2 vapor to the ECR plasma. Our high-temperature oven uses a tungsten crucible joule-heated with DC current of approximately 450 A. Its inside dimensions are ϕ11 mm × 13.5 mm. Since the crucible is placed in a magnetic field of approximately 3 T, it is subject to a magnetic force of approximately 40 N. Therefore, we used ANSYS to carefully design the crucible, which was manufactured by machining a tungsten rod. We could raise the oven up to 1900 °C in the first off-line test. Subsequently, UO2 was loaded into the crucible, and the oven was installed in the 28 GHz ECR ion source and was tested. As a result, a U(35+) beam current of 150 μA was extracted successfully at a RF power of approximately 3 kW.

  15. Analysis of temperature profile and electric field in natural rubber glove due to microwave heating: effects of waveguide position

    NASA Astrophysics Data System (ADS)

    Keangin, P.; Narumitbowonkul, U.; Rattanadecho, P.

    2018-01-01

    Natural rubber (NR) is the key raw material used in the manufacture of other products such as rubber band, tire and shoes. Recently, the NR is used in natural rubber glove ( NRG) manufacturing in the industrial and medical fields. This research aims to investigate the electromagnetic wave propagation and heat transfer in NRG due to heating with microwave energy within the microwave oven at a microwave frequency of 2.45 GHz. Three-dimensional model of NRG and microwave oven are considered in this work. The comparative effects of waveguide position on the electric field and temperature profile in NRG when subjected to microwave energy are discussed. The finite element method (FEM) is used to solve the transient Maxwell’s equation coupled with the transient heat transfer equation. The simulation results with computer programs are validated with experimental results. The placement of waveguides in three cases are left hand side of microwave oven, right hand side of microwave oven and left and right hand sides of microwave oven are investigated. The findings revealed that the placing the waveguide on the right side of the microwave oven gives the highest electric field and temperature profile. The values obtained provide an indication toward understanding the study of heat transfer in NRG during microwave heating in the industry.

  16. Assessment of thermal efficiency of heat recovery coke making

    NASA Astrophysics Data System (ADS)

    Tiwari, H. P.; Saxena, V. K.; Haldar, S. K.; Sriramoju, S. K.

    2017-08-01

    The heat recovery stamp charge coke making process is quite complicated due to the evolved volatile matter during coking, is partially combusted in oven crown and sole flue in a controlled manner to provide heat for producing metallurgical coke. Therefore, the control and efficient utilization of heat in the oven crown, and sole flue is difficult, which directly affects the operational efficiency. Considering the complexity and importance of thermal efficiency, evolution of different gases, combustion of gasses in oven crown and sole flue, and heating process of coke oven has been studied. A nonlinear regression methodology was used to predict temperature profile of different depth of coal cake during the coking. It was observed that the predicted temperature profile is in good agreement with the actual temperature profile (R2 = 0.98) and is validated with the actual temperature profile of other ovens. A complete study is being done to calculate the material balance, heat balance, and heat losses. This gives an overall understanding of heat flow which affects the heat penetration into the coal cake. The study confirms that 60% heat was utilized during coking.

  17. Inverse optimal design of the radiant heating in materials processing and manufacturing

    NASA Astrophysics Data System (ADS)

    Fedorov, A. G.; Lee, K. H.; Viskanta, R.

    1998-12-01

    Combined convective, conductive, and radiative heat transfer is analyzed during heating of a continuously moving load in the industrial radiant oven. A transient, quasi-three-dimensional model of heat transfer between a continuous load of parts moving inside an oven on a conveyor belt at a constant speed and an array of radiant heaters/burners placed inside the furnace enclosure is developed. The model accounts for radiative exchange between the heaters and the load, heat conduction in the load, and convective heat transfer between the moving load and oven environment. The thermal model developed has been used to construct a general framework for an inverse optimal design of an industrial oven as an example. In particular, the procedure based on the Levenberg-Marquardt nonlinear least squares optimization algorithm has been developed to obtain the optimal temperatures of the heaters/burners that need to be specified to achieve a prescribed temperature distribution of the surface of a load. The results of calculations for several sample cases are reported to illustrate the capabilities of the procedure developed for the optimal inverse design of an industrial radiant oven.

  18. Power Generator with Thermo-Differential Modules

    NASA Technical Reports Server (NTRS)

    Saiz, John R.; Nguyen, James

    2010-01-01

    A thermoelectric power generator consists of an oven box and a solar cooker/solar reflector unit. The solar reflector concentrates sunlight into heat and transfers the heat into the oven box via a heat pipe. The oven box unit is surrounded by five thermoelectric modules and is located at the bottom end of the solar reflector. When the heat is pumped into one side of the thermoelectric module and ejected from the opposite side at ambient temperatures, an electrical current is produced. Typical temperature accumulation in the solar reflector is approximately 200 C (392 F). The heat pipe then transfers heat into the oven box with a loss of about 40 percent. At the ambient temperature of about 20 C (68 F), the temperature differential is about 100 C (180 F) apart. Each thermoelectric module, generates about 6 watts of power. One oven box with five thermoelectric modules produces about 30 watts. The system provides power for unattended instruments in remote areas, such as space colonies and space vehicles, and in polar and other remote regions on Earth.

  19. Microwave Ovens

    MedlinePlus

    ... Commission (CPSC) Website Laws, Regulations & Standards Manufacturers of electronic radiation emitting products sold in the United States ... and Cosmetic Act (FFDCA), Chapter V, Subchapter C - Electronic Product Radiation Control . Manufacturers of microwave ovens are ...

  20. 3. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    3. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, 1957 INTERIOR OF OVEN CHAMBER. - Bricker Outdoor Bake Oven, Taneytown & Wheat Fields Roads, Gettysburg, Adams County, PA

  1. DOE Office of Scientific and Technical Information (OSTI.GOV)

    Senaratne, Ruwan, E-mail: rsenarat@physics.ucsb.edu; Rajagopal, Shankari V.; Geiger, Zachary A.

    We present a simple and inexpensive design for a multichannel effusive oven nozzle which provides improved atomic beam collimation and thus extended oven lifetimes. Using this design, we demonstrate an atomic lithium source suitable for trapped-atom experiments. At a nozzle temperature of 525 °C, the collimated atomic beam flux directly after the nozzle is 1.2 × 10{sup 14} atoms/s with a peak beam intensity greater than 5.0 × 10{sup 16} atoms/s/sr. This suggests an oven lifetime of several decades of continuous operation.

  2. 4. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    4. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, 1957 DETAIL OF EXTERIOR OF OVEN. - Bricker Outdoor Bake Oven, Taneytown & Wheat Fields Roads, Gettysburg, Adams County, PA

  3. 40 CFR 63.7280 - What is the purpose of this subpart?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and..., and battery stacks at coke oven batteries. This subpart also establishes requirements to demonstrate...

  4. 40 CFR 63.7280 - What is the purpose of this subpart?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and..., and battery stacks at coke oven batteries. This subpart also establishes requirements to demonstrate...

  5. 40 CFR 63.7280 - What is the purpose of this subpart?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and..., and battery stacks at coke oven batteries. This subpart also establishes requirements to demonstrate...

  6. 40 CFR 63.7280 - What is the purpose of this subpart?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and..., and battery stacks at coke oven batteries. This subpart also establishes requirements to demonstrate...

  7. 40 CFR 63.7280 - What is the purpose of this subpart?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... battery stacks at coke oven batteries. This subpart also establishes requirements to demonstrate initial...

  8. 1. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    1. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, 1957 EXTERIOR OF OVEN FROM THE SOUTHWEST. - Bricker Outdoor Bake Oven, Taneytown & Wheat Fields Roads, Gettysburg, Adams County, PA

  9. Microwave Oven Observations.

    ERIC Educational Resources Information Center

    Sumrall, William J.; Richardson, Denise; Yan, Yuan

    1998-01-01

    Explains a series of laboratory activities which employ a microwave oven to help students understand word problems that relate to states of matter, collect data, and calculate and compare electrical costs to heat energy costs. (DDR)

  10. Boundary Layer Transition Protuberance Tests at NASA JSC Arc-Jet Facility

    NASA Technical Reports Server (NTRS)

    Larin, M. E.; Marichalar, J. J.; Kinder, G. R.; Campbell, C. H.; Riccio, J. R.; Nquyen, T. Q.; DelPapa, S. V.; Pulsonetti, M. V.

    2009-01-01

    A series of arc-jet tests in support of the Shuttle Orbiter Boundary Layer Transition flight experiment was conducted in the Channel Nozzle of the NASA Johnson Space Center Atmospheric Reentry Materials and Structures Facility. The boundary layer trip was a protrusion of a certain height and geometry fabricated as part of a 6"x6" tile insert, a special test article made of the Boeing Rigid Insulation tile material and coated with the Reaction Cured Glass used for the bottom fuselage tiles of the Space Shuttle Orbiter. A total of five such tile inserts were manufactured: four with the 0.25-in. trip height, and one with the 0.35-in. trip height. The tile inserts were interchangeably installed in the center of the 24"x24" variable configuration tile array mounted in the 24"x24" test section of the channel nozzle. The objectives of the test series were to demonstrate that the boundary layer trip can safely withstand the Space Shuttle Orbiter flight-like re-entry environments and provide temperature data on the protrusion surface, surfaces of the nearby tiles upstream and downstream of the trip, as well as the bond line between the tiles and the structure. The targeted test environments were defined for the tip of the protrusion, away from the nominal surface of the tile array. The arc jet test conditions were approximated in order to produce the levels of the free stream total enthalpy at the protrusion height similar to those expected in flight. The test articles were instrumented with surface, sidewall and bond line thermocouples. Additionally, Tempilaq temperature-indicating paint was applied to the nominal tiles of the tile array in locations not interfering with the protrusion trip. Five different grades of paint were used that disintegrate at different temperatures between 1500 and 2000 deg F. The intent of using the paint was to gauge the RCG-coated tile surface temperature, as well as determine its usefulness for a flight experiment. This paper provides an overview of the channel nozzle arc jet, test articles and test conditions, as well as the results of the arc-jet tests including the measured temperature response of the test articles, their pre- and post-test surface scans, condition of the thermal paint, and continents on the protrusion tip heating achieved in tests compared to the computational fluid dynamics predictions.

  11. PERSPECTIVE VIEW LOOKING SOUTHWEST AT THE CYANAMIDE (LN) OVEN BUILDING, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    PERSPECTIVE VIEW LOOKING SOUTHWEST AT THE CYANAMIDE (L-N) OVEN BUILDING, AMMONIA SPHERES IN FOREGROUND. - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

  12. 40 CFR 63.7340 - What notifications must I submit and when?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...). (f) For each by-product coke oven battery with horizontal flues, you must notify the Administrator...

  13. 40 CFR 63.7340 - What notifications must I submit and when?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...). (f) For each by-product coke oven battery with horizontal flues, you must notify the Administrator...

  14. 40 CFR 63.7340 - What notifications must I submit and when?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...). (f) For each by-product coke oven battery with horizontal flues, you must notify the Administrator...

  15. 40 CFR 63.7340 - What notifications must I submit and when?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...). (f) For each by-product coke oven battery with horizontal flues, you must notify the Administrator...

  16. 40 CFR 63.7340 - What notifications must I submit and when?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... (CONTINUED) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and...). (f) For each by-product coke oven battery with horizontal flues, you must notify the Administrator...

  17. Ovenized microelectromechanical system (MEMS) resonator

    DOEpatents

    Olsson, Roy H; Wojciechowski, Kenneth; Kim, Bongsang

    2014-03-11

    An ovenized micro-electro-mechanical system (MEMS) resonator including: a substantially thermally isolated mechanical resonator cavity; a mechanical oscillator coupled to the mechanical resonator cavity; and a heating element formed on the mechanical resonator cavity.

  18. 2. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    2. Historic American Buildings Survey, Frederick Tilberg, Photographer August 25, 1957 DETAIL OF OVEN DOOR AND FRONT WALL. - Bricker Outdoor Bake Oven, Taneytown & Wheat Fields Roads, Gettysburg, Adams County, PA

  19. 63. Refrigerator, microwave oven, storage cabinet open, north side ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    63. Refrigerator, microwave oven, storage cabinet open, north side - Ellsworth Air Force Base, Delta Flight, Launch Control Facility, County Road CS23A, North of Exit 127, Interior, Jackson County, SD

  20. Estimation of Radiofrequency Power Leakage from Microwave Ovens for Dosimetric Assessment at Nonionizing Radiation Exposure Levels

    PubMed Central

    Lopez-Iturri, Peio; de Miguel-Bilbao, Silvia; Aguirre, Erik; Azpilicueta, Leire; Falcone, Francisco; Ramos, Victoria

    2015-01-01

    The electromagnetic field leakage levels of nonionizing radiation from a microwave oven have been estimated within a complex indoor scenario. By employing a hybrid simulation technique, based on coupling full wave simulation with an in-house developed deterministic 3D ray launching code, estimations of the observed electric field values can be obtained for the complete indoor scenario. The microwave oven can be modeled as a time- and frequency-dependent radiating source, in which leakage, basically from the microwave oven door, is propagated along the complete indoor scenario interacting with all of the elements present in it. This method can be of aid in order to assess the impact of such devices on expected exposure levels, allowing adequate minimization strategies such as optimal location to be applied. PMID:25705676

  1. Container for heat treating materials in microwave ovens

    DOEpatents

    Holcombe, Cressie E.; Dykes, Norman L.; Kimrey, Jr., Harold D.; Mills, James E.

    1989-01-01

    The efficiency of a microwave oven of a conventional two-source configuration and energy level is increased by providing the oven with a container for housing a refractory material to be treated. The container is formed of top and bottom walls transparent to microwaves while the sidewalls, in a circular configuration, are formed of a nonmetallic material opaque to microwave radiation reflecting the radiation penetrating the top and bottom walls radially inwardly into the center of the container wherein a casket of heat-insulating material is provided for housing the material to be heat treated. The reflection of the microwave radiation from the sidewalls increases the concentration of the microwaves upon the material being heat treated while the casket retains the heat to permit the heating of the material to a substantially higher temperature than achieveable in the oven without the container.

  2. Sperm quality and DNA integrity of coke oven workers exposed to polycyclic aromatic hydrocarbons.

    PubMed

    Jeng, Hueiwang Anna; Pan, Chih-Hong; Chao, Mu-Rong; Chiu, Chien-Chih; Zhou, Guodong; Chou, Chon-Kit; Lin, Wen-Yi

    2016-11-18

    The objective of this study was to assess sperm quality and deoxyribonucleic acid (DNA) integrity of coke oven workers exposed to polycyclic aromatic hydrocarbons (PAHs) as compared to control subjects. The coke oven workers (N = 52) and administrative staff (N = 35) of a steel plant served as the exposed and control groups, respectively. Exposure to PAHs was assessed by measuring 1-hydroxypyren. Analysis of sperm quality (concentration, motility, vitality, and morphology) was performed simultaneously with sperm DNA integrity analysis, including DNA fragmentation, denaturation, bulky DNA adducts, and 8-oxo-7,8-dihydro-2'-deoxyguanosine (8-oxo-dGuo). A questionnaire was conducted to collect demographic and potential confounding data. The coke oven workers had lower percentages of sperm motility, vitality and normal morphology than the control group, but the difference was not significant. For DNA integrity, the coke oven workers had significantly higher concentrations of bulky DNA adducts and 8-oxo-dGuo than the control subjects (p = 0.009 and p = 0.048, respectively). However, DNA fragmentation percentages did not significantly increase as compared to those in the subjects from the control group (p = 0.232). There was no correlation between sperm quality parameters and DNA integrity indicators. Occupational exposure of the coke oven workers to PAHs was associated with decreased sperm DNA integrity. Int J Occup Med Environ Health 2016;29(6):915-926. This work is available in Open Access model and licensed under a CC BY-NC 3.0 PL license.

  3. LSP Composite Susbtrate Manufacturing Processing Guide

    NASA Technical Reports Server (NTRS)

    Kovach, Daniel J.; Griess, Kenneth H.

    2013-01-01

    This document is intended to define Carbon Fiber Reinforced Plastic (CFRP) test panel configurations that can be employed for the purposes of evaluating the protection capabilities of Lightning Strike Protection (LSP) materials developed by the Aerospace Industry. The configurations are intended to provide consistent behavior in their response to simulated lightning strikes at pre-defined levels when tested by a capable vendor according to a test procedure written to enable consistent results (ref section 2.1.2). In response to an attachment of a simulated lightning strike on a CFRP panel, one can expect to see various levels of ablation and delamination, both through the thickness of the panel and with respect to the amount of panel surface area that exhibits damage. Panel configurations defined in this document include: An "unprotected" configuration 128694-1 (ref section 4.1), consisting of a cured CFRP laminate stackup of tape and fabric prepregs, coated with a typical aerospace primer and paint finishing scheme, attached to aluminum grounding bars intended to draw electrical current from the lightning attachment point to the panel edges and thus to ground. A "protected" configuration 128694-2 (ref section 4.1), wherein a layer of an LSP material form often used in the Aerospace Industry is included in the laminate stackup prior to cure. The CFRP materials, finishes and grounding arrangement for ths configuration are the same as for the "unprotected" configuration.

  4. Real-time measurement system for tracking birefringence, weight, thickness, and surface temperature during drying of solution cast coatings and films

    NASA Astrophysics Data System (ADS)

    Unsal, E.; Drum, J.; Yucel, O.; Nugay, I. I.; Yalcin, B.; Cakmak, M.

    2012-02-01

    This paper describes the design and performance of a new instrument to track temporal changes in physical parameters during the drying behavior of solutions, as well as curing of monomers. This real-time instrument follows in-plane and out-of-plane birefringence, weight, thickness, and surface temperature during the course of solidification of coatings and films through solvent evaporation and thermal or photocuring in a controlled atmosphere. It is specifically designed to simulate behavior of polymer solutions inside an industrial size, continuous roll-to-roll solution casting line and other coating operations where resins are subjected to ultraviolet (UV) curing from monomer precursors. Controlled processing parameters include air speed, temperature, initial cast thickness, and solute concentration, while measured parameters are thickness, weight, film temperature, in-plane and out-of-plane birefringence. In this paper, we illustrate the utility of this instrument with solution cast and dried poly (amide-imide)/DMAc (Dimethylacetamide) solution, water based black paint, and organo-modified clay/NMP (N-Methylpyrrolidone) solution. In addition, the physical changes that take place during UV photo polymerization of a monomer are tracked. This instrument is designed to be generic and it can be used for tracking any drying/swelling/solidification systems including paper, foodstuffs such as; grains, milk as well as pharmaceutical thin paste and slurries.

  5. High levels of medium-chain chlorinated paraffins and polybrominated diphenyl ethers on the inside of several household baking oven doors.

    PubMed

    Gallistl, Christoph; Sprengel, Jannik; Vetter, Walter

    2018-02-15

    Fat obtained by wipe tests on the inner surface of 21 baking ovens from Stuttgart (Germany) were analyzed for halogenated flame retardants (HFRs), namely polybrominated diphenyl ethers (PBDEs), decabromodiphenyl ethane (DBDPE), dechlorane plus (DP), short- and medium-chain chlorinated paraffins (SCCPs, MCCPs), as well as polychlorinated biphenyls (PCBs). In ~50% of the samples chlorinated paraffins (CPs) were present in the mg/g fat range, i.e. three to four orders of magnitude higher concentrated than the sum of all other target compounds. In contrast the remaining ~50% of the samples were free of CPs, while the other HFRs were comparable in CP-positive and CP-negative samples. The exceptionally high concentrations and exclusive presence of CPs in half of the samples produced strong evidence that these compounds were released from the baking oven itself. This hypothesis was supported by detection of MCCPs at even higher concentrations in the inner components of one dismantled baking oven. The release of substantial amounts of HFRs from the oven casing during its use may contribute to human exposure to these compounds, especially MCCPs and SCCPs. Copyright © 2017 Elsevier B.V. All rights reserved.

  6. Impact of volatile composition on the sensorial attributes of dried paprikas.

    PubMed

    Martín, Alberto; Hernández, Alejandro; Aranda, Emilio; Casquete, Rocio; Velázquez, Rocio; Bartolomé, Teresa; Córdoba, María G

    2017-10-01

    Here we characterised the aroma of smoked, oven-dried, and sun-dried paprikas by sensorial evaluation and analysis of their volatile profiles. The sensorial panel defined smoked paprikas as having an intense, persistent, smoked odour and flavour and the highest acceptability. The oven-dried paprikas had a fruity odour and flavour related with aroma notes to fresh peppers. The sun-dried paprikas were associated with straw aromas and the worse valued. The chemical classes of volatile compounds also defined the paprika types. The smoked paprikas were richer in alcohols, phenols, pyrroles, and pyranones, whereas the oven-dried samples were characterised by their aldehydes and terpenes. The sun-dried paprikas had significantly lower amounts of odorant substances than the smoked and oven-dried paprikas. The intensity, persistence and smokiness descriptors (associated with smoked paprika) were positively associated with phenols and alcohols. Aldehydes were positively correlated with a fruity descriptor, which defined oven-dried paprikas, and negatively correlated with intensity, persistence, smokiness, toasted, and dried pepper descriptors. The descriptor straw, which defined sun-dried paprikas, was negatively correlated with alcohols, phenols, furans, and pyrroles. Copyright © 2017 Elsevier Ltd. All rights reserved.

  7. GENERAL OVERVIEW, LOOKING NORTH FROM BEE HIVE COKE OVEN SITE. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    GENERAL OVERVIEW, LOOKING NORTH FROM BEE HIVE COKE OVEN SITE. - Pratt Coal & Coke Company, Pratt Mines, Tailings Pile, Bounded by First Street, Avenue G, Third Place, Birmingham Southern Railroad, Birmingham, Jefferson County, AL

  8. VIEW OF EIGHT COKE OVENS ON EAST SIDE OF TOWN ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    VIEW OF EIGHT COKE OVENS ON EAST SIDE OF TOWN OF ALVERTON, CONSTRUCTED OF YELLOW REFRACTORY BRICK. "WOODLAND M2" AND "BENEZETT - Alverton Coke Works, State Route 981, Alverton, Westmoreland County, PA

  9. 7. FIRST FLOOR, INTERIOR, DETAIL OF FISH SMOKING OVEN LOCATED ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    7. FIRST FLOOR, INTERIOR, DETAIL OF FISH SMOKING OVEN LOCATED IN NORTH END OF BUILDING, ALONG WEST WALL; LOOKING WEST - Gerber Sheet Metal Works Building, 128 Porthand Avenue, South, Minneapolis, Hennepin County, MN

  10. 76 FR 69122 - Energy Conservation Program: Energy Conservation Standards for Certain Consumer Products...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-11-08

    ..., Microwave Ovens, and Electric and Gas Kitchen Ranges and Ovens) and for Certain Commercial and Industrial... 431--ENERGY EFFICIENCY PROGRAM FOR CERTAIN COMMERCIAL AND INDUSTRIAL EQUIPMENT 0 1. The authority...

  11. Non-Ionizing Radiation Used in Microwave Ovens

    MedlinePlus

    ... Human Services (HHS), U.S. Food and Drug Administration (FDA) FDA's Center for Devices and Radiological Health (CDRH) sets ... public health. These standards can be viewed on FDA's Code of Federal Regulations on Microwave Ovens . FDA ...

  12. 62. Refrigerator, microwave oven, equipment storage at top, north side ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    62. Refrigerator, microwave oven, equipment storage at top, north side - Ellsworth Air Force Base, Delta Flight, Launch Control Facility, County Road CS23A, North of Exit 127, Interior, Jackson County, SD

  13. A finite element/level set model of polyurethane foam expansion and polymerization

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Rao, Rekha R.; Long, Kevin Nicholas; Roberts, Christine Cardinal

    Polyurethane foams are used widely for encapsulation and structural purposes because they are inexpensive, straightforward to process, amenable to a wide range of density variations (1 lb/ft3 - 50 lb/ft3), and able to fill complex molds quickly and effectively. Computational model of the filling and curing process are needed to reduce defects such as voids, out-of-specification density, density gradients, foam decomposition from high temperatures due to exotherms, and incomplete filling. This paper details the development of a computational fluid dynamics model of a moderate density PMDI structural foam, PMDI-10. PMDI is an isocyanate-based polyurethane foam, which is chemically blown withmore » water. The polyol reacts with isocyanate to produces the polymer. PMDI- 10 is catalyzed giving it a short pot life: it foams and polymerizes to a solid within 5 minutes during normal processing. To achieve a higher density, the foam is over-packed to twice or more of its free rise density of 10 lb/ft3. The goal for modeling is to represent the expansion, filling of molds, and the polymerization of the foam. This will be used to reduce defects, optimize the mold design, troubleshoot the processed, and predict the final foam properties. A homogenized continuum model foaming and curing was developed based on reaction kinetics, documented in a recent paper; it uses a simplified mathematical formalism that decouples these two reactions. The chemo-rheology of PMDI is measured experimentally and fit to a generalized- Newtonian viscosity model that is dependent on the extent of cure, gas fraction, and temperature. The conservation equations, including the equations of motion, an energy balance, and three rate equations are solved via a stabilized finite element method. The equations are combined with a level set method to determine the location of the foam-gas interface as it evolves to fill the mold. Understanding the thermal history and loads on the foam due to exothermicity and oven curing is very important to the results, since the kinetics, viscosity, and other material properties are all sensitive to temperature. Results from the model are compared to experimental flow visualization data and post-test X-ray computed tomography (CT) data for the density. Several geometries are investigated including two configurations of a mock structural part and a bar geometry to specifically test the density model. We have found that the model predicts both average density and filling profiles well. However, it under predicts density gradients, especially in the gravity direction. Further model improvements are also discussed for future work.« less

  14. An Orthotropic Oven for Loading Vapor Traps

    NASA Astrophysics Data System (ADS)

    Maddi, J.; Dinneen, T.; Gould, H.

    1998-05-01

    Orthotropic ovens(T. Dinneen, A. Ghiorso, and H. Gould, Rev. Sci. Inst. 67, 752 (1996) ) produce collimated beams of alkali atoms with high efficiency. They are useful for producing beams of rare species such as short-lived radioactive atoms. We describe the design and operation of the UHV orthotropic oven used in vapor-capture trapping and cooling(Z.-T. Lu, K.L. Corwin, K.R. Vogel, C.E. Wieman, T.P. Dinneen, J. Maddi, and H. Gould, Phys. Rev. Lett. 79, 994 (1997)) of ^221Fr, and recent improvments in its design.

  15. A short response time atomic source for trapped ion experiments

    NASA Astrophysics Data System (ADS)

    Ballance, T. G.; Goodwin, J. F.; Nichol, B.; Stephenson, L. J.; Ballance, C. J.; Lucas, D. M.

    2018-05-01

    Ion traps are often loaded from atomic beams produced by resistively heated ovens. We demonstrate an atomic oven which has been designed for fast control of the atomic flux density and reproducible construction. We study the limiting time constants of the system and, in tests with 40Ca, show that we can reach the desired level of flux in 12 s, with no overshoot. Our results indicate that it may be possible to achieve an even faster response by applying an appropriate one-off heat treatment to the oven before it is used.

  16. Effects of genetic polymorphisms of metabolic enzymes on cytokinesis-block micronucleus in peripheral blood lymphocyte among coke-oven workers

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Shuguang Leng; Yufei Dai; Yong Niu

    Exploring the associations between genetic polymorphisms of metabolic enzymes and susceptibility to polycyclic aromatic hydrocarbon (PAH)-induced chromosomal damage is of great significance for understanding PAH carcinogenesis. Cytochrome P450, glutathione S-transferase, microsomal epoxide hydrolase, NAD(P)H:quinone oxidoreductase, and N-acetyltransferase are PAH-metabolizing enzymes. In this study, we genotyped for the polymorphisms of these genes and assessed their effects on cytokinesis-block micronucleus (CBMN) frequencies in peripheral blood lymphocytes among 141 coke-oven workers and 66 non-coke-oven worker controls. The geometric means of urinary 1-hydroxypyrene levels in coke-oven workers and the controls were 12.0 and 0.7 {mu}mol/mol creatinine, respectively. The CBMN frequency (number of micronuclei permore » 1,000 binucleated lymphocytes) was significantly higher in coke-oven workers (9.5 {+-} 6.6) than in the controls. Among the coke-oven workers, age was positively associated with CBMN frequency; the mEH His{sup 113} variant genotype exhibited significantly lower CBMN frequency than did the Tyr{sup 113}/Tyr{sup 113} genotype; the low mEH activity phenotype exhibited a lower CBMN frequency than did the high mEH activity phenotype; the GSTP1 Val{sup 105}/Val{sup 105} genotype exhibited a higher CBMN frequency than did the GSTP1 Ile{sup 105}/Ile{sup 105} or Ile{sup 105}/Val{sup 105} genotypes; the joint effect of high mEH activity phenotype and GSTM1 null genotype on CBMN frequencies was also found. Gene-environment interactions between occupational PAH exposure and polymorphisms of mEH and/or GSTM1 were also evident. These results indicate that the mEH, GSTP1, and GSTM1 polymorphisms may play a role in sensitivity or genetic susceptibility to the genotoxic effects of PAH exposure in the coke-oven workers.« less

  17. Effects of cooking method and final core-temperature on cooking loss, lipid oxidation, nucleotide-related compounds and aroma volatiles of Hanwoo brisket

    PubMed Central

    2018-01-01

    Objective This study observed the effects of cooking method and final core temperature on cooking loss, lipid oxidation, aroma volatiles, nucleotide-related compounds and aroma volatiles of Hanwoo brisket (deep pectoralis). Methods Deep pectoralis muscles (8.65% of crude fat) were obtained from three Hanwoo steer carcasses with 1+ quality grade. Samples were either oven-roasted at 180°C (dry heat) or cooked in boiling water (moist heat) to final core temperature of 70°C (medium) or 77°C (well-done). Results Boiling method reduced more fat but retained more moisture than did the oven roasting method (p<0.001), thus no significant differences were found on cooking loss. However, samples lost more weight as final core temperature increased (p<0.01). Further, total saturated fatty acid increased (p = 0.02) while total monounsaturated fatty acid decreased (p = 0.03) as final core temperature increased. Regardless the method used for cooking, malondialdehyde (p<0.01) and free iron contents (p<0.001) were observed higher in samples cooked to 77°C. Oven roasting retained more inosinic acid, inosine and hypoxanthine in samples than did the boiling method (p<0.001), of which the concentration decreased as final core temperature increased except for hypoxanthine. Samples cooked to 77°C using oven roasting method released more intense aroma than did the others and the aroma pattern was discriminated based on the intensity. Most of aldehydes and pyrazines were more abundant in oven-roasted samples than in boiled samples. Among identified volatiles, hexanal had the highest area unit in both boiled and oven-roasted samples, of which the abundance increased as the final core temperature increased. Conclusion The boiling method extracted inosinic acid and rendered fat from beef brisket, whereas oven roasting intensified aroma derived from aldehydes and pyrazines and prevented the extreme loss of inosinic acid. PMID:28728407

  18. Evaluation of microwave oven heating for prediction of drug-excipient compatibilities and accelerated stability studies.

    PubMed

    Schou-Pedersen, Anne Marie V; Østergaard, Jesper; Cornett, Claus; Hansen, Steen Honoré

    2015-05-15

    Microwave ovens have been used extensively in organic synthesis in order to accelerate reaction rates. Here, a set up comprising a microwave oven combined with silicon carbide (SiC) plates for the controlled microwave heating of model formulations has been applied in order to investigate, if a microwave oven is applicable for accelerated drug stability testing. Chemical interactions were investigated in three selected model formulations of drug and excipients regarding the formation of ester and amide reaction products. In the accelerated stability studies, a design of experiments (DoE) approach was applied in order to be able to rank excipients regarding reactivity: Study A: cetirizine with PEG 400, sorbitol, glycerol and propylene glycol. Study B: 6-aminocaproic acid with citrate, acetate, tartrate and gluconate. Study C: atenolol with citric, tartaric, malic, glutaric, and sorbic acid. The model formulations were representative for oral solutions (co-solvents), parenteral solutions (buffer species) and solid dosage forms (organic acids applicable for solubility enhancement). The DoE studies showed overall that the same impurities were generated by microwave oven heating leading to temperatures between 150°C and 180°C as compared to accelerated stability studies performed at 40°C and 80°C using a conventional oven. Ranking of the reactivity of the excipients could be made in the DoE studies performed at 150-180°C, which was representative for the ranking obtained after storage at 40°C and 80°C. It was possible to reduce the time needed for drug-excipient compatibility testing of the three model formulations from weeks to less than an hour in the three case studies. The microwave oven is therefore considered to be an interesting alternative to conventional thermal techniques for the investigation of drug-excipient interactions during preformulation. Copyright © 2015 Elsevier B.V. All rights reserved.

  19. 40 CFR 63.308 - Standards for collecting mains.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Standards for Coke Oven Batteries § 63.308 Standards for collecting mains. (a) On and after November 15, 1993, the owner or operator of a by-product coke oven battery shall inspect the collecting main for...

  20. 40 CFR 63.308 - Standards for collecting mains.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Standards for Coke Oven Batteries § 63.308 Standards for collecting mains. (a) On and after November 15, 1993, the owner or operator of a by-product coke oven battery shall inspect the collecting main for...

  1. 40 CFR 63.308 - Standards for collecting mains.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... Standards for Coke Oven Batteries § 63.308 Standards for collecting mains. (a) On and after November 15, 1993, the owner or operator of a by-product coke oven battery shall inspect the collecting main for...

  2. GENERAL OVERVIEW, LOOKING NORTH FROM COKE OVEN SITE, HEIGHT C. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    GENERAL OVERVIEW, LOOKING NORTH FROM COKE OVEN SITE, HEIGHT C. 20 FEET. - Pratt Coal & Coke Company, Pratt Mines, Tailings Pile, Bounded by First Street, Avenue G, Third Place, Birmingham Southern Railroad, Birmingham, Jefferson County, AL

  3. 40 CFR 63.308 - Standards for collecting mains.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Standards for Coke Oven Batteries § 63.308 Standards for collecting mains. (a) On and after November 15, 1993, the owner or operator of a by-product coke oven battery shall inspect the collecting main for...

  4. 40 CFR 63.308 - Standards for collecting mains.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Standards for Coke Oven Batteries § 63.308 Standards for collecting mains. (a) On and after November 15, 1993, the owner or operator of a by-product coke oven battery shall inspect the collecting main for...

  5. 75 FR 77650 - Buy American Exceptions Under the American Recovery and Reinvestment Act of 2009

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-12-13

    ... Housing Authority for the purchase and installation of microwave ovens and Ground Fault Circuit... HUD on the basis that the relevant manufactured goods (GFCI outlets and microwave ovens) are not...

  6. DOE Office of Scientific and Technical Information (OSTI.GOV)

    V.T. Krivoshein; A.V. Makarov

    The sequence of pushing coke ovens is one of the most important aspects of battery operation. The sequence must satisfy a number of technical and process conditions: (1) achieve maximum heating-wall life by avoiding destructive expansion pressure in freshly charged ovens and during pushing of the finished coke; (2) ensure uniform brickwork temperature and prevent overheating by compensating for the high thermal flux in freshly charged ovens due to accumulated heat in adjacent ovens that are in the second half of the coking cycle; (3) ensure the most favorable working conditions and safety for operating personnel; (4) provide additional opportunitiesmore » for repair personnel to perform various types of work, such as replacing coke-machine rails, without interrupting coal production; (5) perform the maximum number of coke-machine operations simultaneously: pushing, charging, and cleaning doors, frames, and standpipe elbows; and (6) reduce electricity consumption by minimizing idle travel of coke machines.« less

  7. Thermocouple, multiple junction reference oven

    NASA Technical Reports Server (NTRS)

    Leblanc, L. P. (Inventor)

    1981-01-01

    An improved oven for maintaining the junctions of a plurality of reference thermocouples at a common and constant temperature is described. The oven is characterized by a cylindrical body defining a heat sink with axially extended-cylindrical cavity a singularized heating element which comprises a unitary cylindrical heating element consisting of a resistance heating coil wound about the surface of metallic spool with an axial bore defined and seated in the cavity. Other features of the oven include an annular array of radially extended bores defined in the cylindrical body and a plurality of reference thermocouple junctions seated in the bores in uniformly spaced relation with the heating element, and a temperature sensing device seated in the axial bore for detecting temperature changes as they occur in the spool and circuit to apply a voltage across the coil in response to detected drops in temperatures of the spool.

  8. Assessment of genotoxic exposure in Swedish coke-oven work by different methods of biological monitoring.

    PubMed

    Reuterwall, C; Aringer, L; Elinder, C G; Rannug, A; Levin, J O; Juringe, L; Onfelt, A

    1991-04-01

    This study evaluated the results of several biological methods used simultaneously to monitor coke-oven work. Blood samples from 44 male coke-oven workers and 48 male referents, matched for age and smoking/snuff consumption, were examined for cytogenetic damage in lymphocytes. Urinary thioether excretion was determined for 62, and urine mutagenicity for 31, of the subjects, who followed a standardized diet during the urine sampling. Exposure to polycyclic aromatic hydrocarbons varied with work task, the ambient air levels of benzo[a]pyrene sometimes exceeding 5 micrograms/m3. Cytogenetic damage, urine mutagenicity, and thioether excretion did not differ between the groups. The smokers, however, had significantly higher sister chromatid exchange frequencies, urine mutagenicity, and thioether excretion than the nonsmokers. The absence of biological indications of genotoxic exposure was unexpected and indicates that the studied methods are not adequate to assess the carcinogenic risks of Swedish coke-oven workers.

  9. Alternative control technology document for bakery oven emissions. Final report

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Sanford, C.W.

    The document was produced in response to a request by the baking industry for Federal guidance to assist in providing a more uniform information base for State decision-making with regard to control of bakery oven emissions. The information in the document pertains to bakeries that produce yeast-leavened bread, rolls, buns, and similar products but not crackers, sweet goods, or baked foodstuffs that are not yeast leavened. Information on the baking processes, equipment, operating parameters, potential emissions from baking, and potential emission control options are presented. Catalytic and regenerative oxidation are identified as the most appropriate existing control technologies applicable tomore » VOC emissions from bakery ovens. Cost analyses for catalytic and regenerative oxidation are included. A predictive formula for use in estimating oven emissions has been derived from source tests done in junction with the development of the document. Its use and applicability are described.« less

  10. A container for heat treating materials in microwave ovens

    DOEpatents

    Holcombe, C.E.; Dykes, N.L.; Kimrey, H.D. Jr.; Mills, J.E.

    1988-01-26

    The efficiency of a microwave oven of a conventional two-source configuration and energy level is increased by providing the oven with a container for housing a refractory material to be treated. The container is formed to top and bottom walls transparent to microwaves while the sidewalls, in a circular configuration, are formed of a nonmetallic material opaque to microwave radiation for reflecting the radiation penetrating the top and bottom walls radially inwardly into the center of the container wherein a casket of heat-insulating material is provided for housing the material to be heat treated. The reflection of the microwave radiation from the sidewalls increases the concentration of the microwaves upon the material being heat treated while the concentration of the microwaves upon the material being heat treated while the casket retains the heat to permit the heating of the material to a substantially higher temperature than achievable in the oven without the container.

  11. Art as a Means of Accessing Ourselves. Using Art in Psychotherapy.

    PubMed

    d'Errico, Immacolata

    2017-09-01

    Using art in psychotherapy could become an interesting instrument for the cure and the prevention of psychological and psychiatric problems. This belongs to that trend that sees the mediation of art as having big potential to go beyond the spoken word. Everybody knows that our emotions, thoughts, feelings, and so on, are living in the body and speaking through the body, in fact the symbolic dimension (art, music, dance, painting and so on) reconfigures the experience of living. In this form of therapy we use Art as a means of accessing ourselves and opening ourselves up to the world. The forms of artistic mediation that we mainly describe in the paper are the basic elements of tango and performative theatrical technique (Theatre of the Oppressed and Physical Theatre). In the final part of this paper a series of images illustrate specific cases in which the method and its outcomes are described.

  12. Geomagnetic paleointensity between 1300 and 1750 A.D. derived from a bread oven floor sequence in Lübeck, Germany

    NASA Astrophysics Data System (ADS)

    Schnepp, Elisabeth; Lanos, Philippe; Chauvin, Annick

    2009-08-01

    Geomagnetic paleointensities have been determined from a single archaeological site in Lübeck, Germany, where a sequence of 25 bread oven floors has been preserved in a bakery from medieval times until today. Age dating confines the time interval from about 1300 A.D. to about 1750 A.D. Paleomagnetic directions have been published from each oven floor and are updated here. The specimens have very stable directions and no or only weak secondary components. The oven floor material was characterized rock magnetically using Thellier viscosity indices, median destructive field values, Curie point determinations, and hysteresis measurements. Magnetic carriers are mixtures of SD, PSD, and minor MD magnetite and/or maghemite together with small amounts of hematite. Paleointensity was measured from selected specimens with the double-heating Thellier method including pTRM checks and determination of TRM anisotropy tensors. Corrections for anisotropy as well as for cooling rate turned out to be unnecessary. Ninety-two percent of the Thellier experiments passed the assigned acceptance criteria and provided four to six reliable paleointensity estimates per oven floor. Mean paleointensity values derived from 22 oven floors show maxima in the 15th and early 17th centuries A.D., followed by a decrease of paleointensity of about 20% until 1750 A.D. Together with the directions the record represents about 450 years of full vector secular variation. The results compare well with historical models of the Earth's magnetic field as well as with a selected high-quality paleointensity data set for western and central Europe.

  13. Microstructure, texture and colour development during crust formation on whole muscle chicken fillets.

    PubMed

    Barbut, S

    2013-01-01

    1. The development of crust during a 22-min period was evaluated in an oven, and in previously cooked-in-bag products (no crust) placed in an oven for 10 min. The oven-roasted products started to develop a thin (2-4 μm) crust layer after 4 min. At that point, the colour of the fillets turned white but no browning was observed. As roasting time increased, crust thickness and shear force increased, the product turned brown and eventually black at certain spots. 2. Light microscopy revealed the shrinking of muscle fibres close to the surface, as they also lost water. At a certain point, tears between the different layers started to appear. The inner muscle fibres also progressively shrank and the spaces between them increased. Microscopy of cook-in-bag products revealed no crust formation during heating. Upon moving to the oven, crust started to form but was much faster compared with the other products. 3. Cook-in-the-bag samples showed a higher rate of cook loss during the first 12 min (to internal 70°C) compared with oven heating. This could have been due to the fast heating rate in water and/or no crust formation. 4. White colour was fully formed on water-cooked fillets within 2 min (L* = 83), while it was gradually forming on oven-roasted samples (max L* of 79 after 12 min). 5. Shear force measurements showed an increase in both treatments up to 18 min, with a decrease thereafter (when dry crust started to crack).

  14. Enhancement of ibuprofen dissolution via wet granulation with beta-cyclodextrin.

    PubMed

    Ghorab, M K; Adeyeye, M C

    2001-08-01

    The purpose was to investigate the effect of wet granulation with beta-cyclodextrin (betaCD) on the enhancement of ibuprofen (IBU) dissolution. The effect of the granulation variables on the physical properties as well as the dissolution of tablets prepared from these granules was also examined. Granulation was performed using three granulating solvents: water, ethanol (95 vol%), and isopropanol. Granules were either oven-dried for 2 h or air-dried for 3 days. The granules or respective physical mixtures were compressed into tablets. Powder X-ray diffraction showed that oven-dried granulation resulted in less amorphous entities thatfacilitated IBU-betaCD complexation in solution and enhanced the dissolution of the corresponding tablets compared to the physical mixture with or without oven drying. In contrast, air-dried granulation did not cause any differences in the X-ray diffraction pattern (crystallinity) or the dissolution compared to the physical mixture without drying. Isopropanol and water, as granulating solvents, enhanced the dissolution of the oven-dried batches more than ethanol. The Differential scanning calorimetry (DSC) and Thermogravimetric analysis (TGA) data showed that tablets prepared from oven-dried granules, but not air-dried granules, had lower AH values and percent loss in weight, respectively, than those prepared from the physical mixture as a result of the expulsion of the water molecules from the betaCD cavity and enhancement of the complexation in solution. These results showed that oven-dried granulation of IBU and betaCD provided faster IBU dissolution than the physical mixture; air-dried granulation did not substantially affect the dissolution of IBU.

  15. Risk of Burns from Eruptions of Hot Water Overheated in Microwave Ovens

    MedlinePlus

    ... Products Risk of Burns from Eruptions of Hot Water Overheated in Microwave Ovens Share Tweet Linkedin Pin ... What Can Consumers Do to Avoid Super-Heated Water? Follow the precautions and recommendations found in the ...

  16. Coke oven emissions

    Integrated Risk Information System (IRIS)

    Coke oven emissions ; CASRN NA Human health assessment information on a chemical substance is included in the IRIS database only after a comprehensive review of toxicity data , as outlined in the IRIS assessment development process . Sections I ( Health Hazard Assessments for Noncarcinogenic Effects

  17. 40 CFR 63.7281 - Am I subject to this subpart?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... if you own or operate a coke oven battery at a coke plant that is (or is part of) a major source of...

  18. 40 CFR 63.7331 - What are the installation, operation, and maintenance requirements for my monitors?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous Compliance Requirements § 63... each by-product coke oven battery, you must install, operate, and maintain a COMS to measure and record...

  19. 40 CFR 63.7331 - What are the installation, operation, and maintenance requirements for my monitors?

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous Compliance Requirements § 63... each by-product coke oven battery, you must install, operate, and maintain a COMS to measure and record...

  20. 40 CFR 63.7281 - Am I subject to this subpart?

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... if you own or operate a coke oven battery at a coke plant that is (or is part of) a major source of...

  1. 1. GENERAL VIEW OF COKE WORKS LOOKING WEST, SHOWING OVENS ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    1. GENERAL VIEW OF COKE WORKS LOOKING WEST, SHOWING OVENS IN FOREGROUND, LARRY CAR TIPPLE TO THE RIGHT, AND COAL TIPPLE IN CENTERGROUND - Lucernemines Coke Works, 0.2 mile East of Lucerne, Lucerne Mines, Indiana County, PA

  2. 40 CFR 63.7281 - Am I subject to this subpart?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... if you own or operate a coke oven battery at a coke plant that is (or is part of) a major source of...

  3. 40 CFR 63.7281 - Am I subject to this subpart?

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... if you own or operate a coke oven battery at a coke plant that is (or is part of) a major source of...

  4. 40 CFR 63.7331 - What are the installation, operation, and maintenance requirements for my monitors?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous Compliance Requirements § 63... each by-product coke oven battery, you must install, operate, and maintain a COMS to measure and record...

  5. 40 CFR 63.7331 - What are the installation, operation, and maintenance requirements for my monitors?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Continuous Compliance Requirements § 63... each by-product coke oven battery, you must install, operate, and maintain a COMS to measure and record...

  6. 40 CFR 63.7281 - Am I subject to this subpart?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ...) National Emission Standards for Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery... if you own or operate a coke oven battery at a coke plant that is (or is part of) a major source of...

  7. The low-power potential of oven-controlled MEMS oscillators.

    PubMed

    Vig, John; Kim, Yoonkee

    2013-04-01

    It is shown that oven-controlled micro electromechanical systems (MEMS) oscillators have the potential of attaining a higher frequency stability, with a lower power consumption, than temperature-compensated crystal oscillators (TCXOs) and the currently manufactured MEMS oscillators.

  8. DETAIL INTERIOR VIEW OF THE CYANAMIDE (LN) OVEN BUILDING LOOKING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    DETAIL INTERIOR VIEW OF THE CYANAMIDE (L-N) OVEN BUILDING LOOKING SOUTHEAST AT INGERSOLL-RAND COMPRESSORS #BE565 & 564. (NOT ORIGINAL LOCATION). - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

  9. DETAIL INTERIOR VIEW OF THE CYANAMIDE (LN) OVEN BUILDING LOOKING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    DETAIL INTERIOR VIEW OF THE CYANAMIDE (L-N) OVEN BUILDING LOOKING NORTHWEST AT A C. 1932 CHICAGO PNEUMATIC COMPRESSOR. (NOT ORIGINAL LOCATION). - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

  10. DETAIL INTERIOR VIEW OF THE CYANAMIDE (LN) OVEN BUILDING LOOKING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    DETAIL INTERIOR VIEW OF THE CYANAMIDE (L-N) OVEN BUILDING LOOKING WEST AT INGERSOLL-RAND COMPRESSORS #BE565 & 564. (NOT ORIGINAL LOCATION). - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

  11. DETAIL INTERIOR VIEW OF THE CYANAMIDE (LN) OVEN BUILDING LOOKING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    DETAIL INTERIOR VIEW OF THE CYANAMIDE (L-N) OVEN BUILDING LOOKING NORTHEAST AT A C. 1932 CHICAGO PNEUMATIC COMPRESSOR. (NOT ORIGINAL LOCATION). - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

  12. Microwave Sterilization in School Microbiology.

    ERIC Educational Resources Information Center

    Wynn, Brian; Dixon, Angela

    1988-01-01

    Described are two investigations carried out in a high school biology department using a domestic microwave oven to compare the relative attributes of the autoclave and microwave oven in school use. Discussed are equipment, methods, and results of each investigation. (Author/CW)

  13. Risk Assessment Document for Coke Oven MACT Residual Risk

    EPA Pesticide Factsheets

    The residual risk analysis described in this report addresses four coke plants subject to the 1993coke oven MACT standards (40 CFR Part 63 Subpart L) and estimates potential risks due to HAPsemissions from facilities involved in coking operations.

  14. Oven Evaporates Isopropyl Alcohol Without Risk Of Explosion

    NASA Technical Reports Server (NTRS)

    Morgan, Gene E.; Hoult, William S.

    1996-01-01

    Ordinary convection oven with capacity of 1 ft.(sup3) modified for use in drying objects washed in isopropyl alcohol. Nitrogen-purge equipment and safety interlocks added to prevent explosive ignition of flammable solvent evaporating from object to be dried.

  15. 40 CFR 63.7320 - By what date must I conduct performance tests or other initial compliance demonstrations?

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance... coke oven battery stack by the compliance date that is specified in § 63.7283. (c) For each work...

  16. 40 CFR 60.421 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... stream to the reactor/crystallizer for synthetic and coke oven by-product ammonium sulfate manufacturing...-product from process streams generated during caprolactam manufacture. Coke oven by-product ammonium... ammonia recovered as a by-product from the manufacture of coke. Synthetic ammonium sulfate manufacturing...

  17. 40 CFR 60.421 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... stream to the reactor/crystallizer for synthetic and coke oven by-product ammonium sulfate manufacturing...-product from process streams generated during caprolactam manufacture. Coke oven by-product ammonium... ammonia recovered as a by-product from the manufacture of coke. Synthetic ammonium sulfate manufacturing...

  18. 40 CFR 63.7320 - By what date must I conduct performance tests or other initial compliance demonstrations?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... Hazardous Air Pollutants for Coke Ovens: Pushing, Quenching, and Battery Stacks Initial Compliance... coke oven battery stack by the compliance date that is specified in § 63.7283. (c) For each work...

  19. 40 CFR 60.421 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... stream to the reactor/crystallizer for synthetic and coke oven by-product ammonium sulfate manufacturing...-product from process streams generated during caprolactam manufacture. Coke oven by-product ammonium... ammonia recovered as a by-product from the manufacture of coke. Synthetic ammonium sulfate manufacturing...

  20. 40 CFR 60.421 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... stream to the reactor/crystallizer for synthetic and coke oven by-product ammonium sulfate manufacturing...-product from process streams generated during caprolactam manufacture. Coke oven by-product ammonium... ammonia recovered as a by-product from the manufacture of coke. Synthetic ammonium sulfate manufacturing...

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