Science.gov

Sample records for petra iii beamlines

  1. The Generic Beamline Concept of the PETRA III Undulator Beamlines

    SciTech Connect

    Hahn, U.; Peters, H. B.; Roehlsberger, R.; Schulte-Schrepping, H.

    2007-01-19

    The conversion of the PETRA storage ring at DESY to a third generation synchrotron radiation light source poses a challenge to the design of the beam transport system. The total power in the white beam will be as high as 7.5kW in the case of the 5m long undulator at 100mA. The power density will be 476 W/mm2 at 20m from the source. Upgrades to a beam current of 200mA have to be accounted for in the design of the beamline components. For the beam transport between the undulator and the experimental hall, the design of a generic beamline is presented. It contains all elements which are needed to guide the beam to the experiment. This generic beamline consists of the estimated maximum of components for this purpose. Special experimental needs may reduce the number of proposed devices in the generic part and add special optical devices close to the experiment, e. g. strong focusing. The paper focuses on the girder concept for all major beam transport components and the collimating shutter system which has to deal with the high power density of the PETRA III undulators.

  2. The High Energy Materials Science Beamline (HEMS) at PETRA III

    NASA Astrophysics Data System (ADS)

    Schell, Norbert; King, Andrew; Beckmann, Felix; Ruhnau, Hans-Ulrich; Kirchhof, René; Kiehn, Rüdiger; Müller, Martin; Schreyer, Andreas

    2010-06-01

    The HEMS Beamline at the German high-brilliance synchrotron radiation storage ring PETRA III is fully tunable between 30 and 250 keV and optimized for sub-micrometer focusing. Approximately 70 % of the beamtime will be dedicated to Materials Research. Fundamental research will encompass metallurgy, physics and chemistry with first experiments planned for the investigation of the relationship between macroscopic and micro-structural properties of polycrystalline materials, grain-grain-interactions, and the development of smart materials or processes. For this purpose a 3D-microsctructure-mapper has been designed. Applied research for manufacturing process optimization will benefit from high flux in combination with ultra-fast detector systems allowing complex and highly dynamic in-situ studies of micro-structural transformations, e.g. during welding processes. The beamline infrastructure allows accommodation of large and heavy user provided equipment. Experiments targeting the industrial user community will be based on well established techniques with standardized evaluation, allowing full service measurements, e.g. for tomography and texture determination. The beamline consists of a five meter in-vacuum undulator, a general optics hutch, an in-house test facility and three independent experimental hutches working alternately, plus additional set-up and storage space for long-term experiments. HEMS is under commissioning as one of the first beamlines running at PETRA III.

  3. New fast closing shutter for the PETRA III beamlines

    NASA Astrophysics Data System (ADS)

    Hahn, U.; Hesse, M.; Müller, S.; Peters, H.-B.; Timmann, B.; Wengler, R.; Zink, H.

    2008-03-01

    The conversion of the PETRA storage ring at the Deutsches Elektronen Synchrotron (DESY) to the third generation synchrotron radiation light source PETRAIII [1] poses a challenge to the design of the beamline transport system. One of these challenges is to supply 14 beamlines and experiments windowless with the extremely collimated undulator radiation from the storage ring. The windowless connection includes the risk of accidental venting of the storage ring by experiments connected to the beamlines. To stop the inrush of such an accidental venting fast closing shutter (FCS) systems with closing times in the 10msec range are mandatory. The strong radiation background in the storage ring tunnel requires the installation of all metal valves. A new small fast closing shutter with an aperture of 40mm fitting to the strong collimated undulator beams and with a closing time < 10msec was developed. The all metal sealing principle achieves leak rates smaller than 10mbarl/sec. This leak rate of the fast closing shutter combined with a standard all metal valve prevents venting of the storage ring and the beam time losses for all users. The mechanical and electronic layouts as well as first experiences with the new fast closing shutter system developed for PETRAIII are presented.

  4. The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III

    DOE PAGES

    Alexeev, P.; Asadchikov, V.; Bessas, D.; Butashin, A.; Deryabin, A.; Dill, F. -U.; Ehnes, A.; Herlitschke, M.; Hermann, R. P.; Jafari, A.; et al

    2016-02-23

    Here, we report on a high resolution sapphire backscattering monochromator installed at the Dynamics beamline P01 of PETRA III. The device enables nuclear resonance scattering experiments on M ossbauer isotopes with transition energies between 20 and 60 keV with sub-meV to meV resolution. In a first performance test with 119Sn nuclear resonance at a X-ray energy of 23.88 keV an energy resolution of 1.34 meV was achieved. Moreover, the device extends the field of nuclear resonance scattering at the PETRA III synchrotron light source to many further isotopes like 151Eu, 149Sm, 161Dy, 125Te and 121Sb.

  5. Time-resolved pump and probe x-ray absorption fine structure spectroscopy at beamline P11 at PETRA III.

    PubMed

    Göries, D; Dicke, B; Roedig, P; Stübe, N; Meyer, J; Galler, A; Gawelda, W; Britz, A; Geßler, P; Sotoudi Namin, H; Beckmann, A; Schlie, M; Warmer, M; Naumova, M; Bressler, C; Rübhausen, M; Weckert, E; Meents, A

    2016-05-01

    We report about the development and implementation of a new setup for time-resolved X-ray absorption fine structure spectroscopy at beamline P11 utilizing the outstanding source properties of the low-emittance PETRA III synchrotron storage ring in Hamburg. Using a high intensity micrometer-sized X-ray beam in combination with two positional feedback systems, measurements were performed on the transition metal complex fac-Tris[2-phenylpyridinato-C2,N]iridium(III) also referred to as fac-Ir(ppy)3. This compound is a representative of the phosphorescent iridium(III) complexes, which play an important role in organic light emitting diode (OLED) technology. The experiment could directly prove the anticipated photoinduced charge transfer reaction. Our results further reveal that the temporal resolution of the experiment is limited by the PETRA III X-ray bunch length of ∼103 ps full width at half maximum (FWHM). PMID:27250401

  6. Time-resolved pump and probe x-ray absorption fine structure spectroscopy at beamline P11 at PETRA III.

    PubMed

    Göries, D; Dicke, B; Roedig, P; Stübe, N; Meyer, J; Galler, A; Gawelda, W; Britz, A; Geßler, P; Sotoudi Namin, H; Beckmann, A; Schlie, M; Warmer, M; Naumova, M; Bressler, C; Rübhausen, M; Weckert, E; Meents, A

    2016-05-01

    We report about the development and implementation of a new setup for time-resolved X-ray absorption fine structure spectroscopy at beamline P11 utilizing the outstanding source properties of the low-emittance PETRA III synchrotron storage ring in Hamburg. Using a high intensity micrometer-sized X-ray beam in combination with two positional feedback systems, measurements were performed on the transition metal complex fac-Tris[2-phenylpyridinato-C2,N]iridium(III) also referred to as fac-Ir(ppy)3. This compound is a representative of the phosphorescent iridium(III) complexes, which play an important role in organic light emitting diode (OLED) technology. The experiment could directly prove the anticipated photoinduced charge transfer reaction. Our results further reveal that the temporal resolution of the experiment is limited by the PETRA III X-ray bunch length of ∼103 ps full width at half maximum (FWHM).

  7. Note: Comparison of grazing incidence small angle x-ray scattering of a titania sponge structure at the beamlines BW4 (DORIS III) and P03 (PETRA III)

    SciTech Connect

    Rawolle, M.; Koerstgens, V.; Ruderer, M. A.; Metwalli, E.; Guo, S.; Mueller-Buschbaum, P.; Herzog, G.; Benecke, G.; Schwartzkopf, M.; Buffet, A.; Perlich, J.; Roth, S. V.

    2012-10-15

    Grazing incidence small angle x-ray scattering (GISAXS) is a powerful technique for morphology investigation of nanostructured thin films. GISAXS measurements at the newly installed P03 beamline at the storage ring PETRA III in Hamburg, Germany, are compared to the GISAXS data from the beamline BW4 at the storage ring DORIS III, which had been used extensively for GISAXS investigations in the past. As an example, a titania thin film sponge structure is investigated. Compared to BW4, at beamline P03 the resolution of larger structures is slightly improved and a higher incident flux leads to a factor of 750 in scattered intensity. Therefore, the acquisition time in GISAXS geometry is reduced significantly at beamline P03.

  8. P03, the microfocus and nanofocus X-ray scattering (MiNaXS) beamline of the PETRA III storage ring: the microfocus endstation.

    PubMed

    Buffet, Adeline; Rothkirch, André; Döhrmann, Ralph; Körstgens, Volker; Abul Kashem, Mottakin M; Perlich, Jan; Herzog, Gerd; Schwartzkopf, Matthias; Gehrke, Rainer; Müller-Buschbaum, Peter; Roth, Stephan V

    2012-07-01

    The P03 beamline, also called the microfocus and nanofocus X-ray scattering (MiNaXS) beamline, exploits the excellent photon beam properties of the low-emittance source PETRA III to provide a microfocused/nanofocused beam with ultra-high intensity for time-resolved X-ray scattering experiments. The beamline has been designed to perform X-ray scattering in both transmission and reflection geometries. The microfocus endstation started user operation in May 2011. An overview of the beamline status and of some representative results highlighting the performance of the microfocus endstation at MiNaXS are given.

  9. Beamline P02.1 at PETRA III for high-resolution and high-energy powder diffraction.

    PubMed

    Dippel, Ann-Christin; Liermann, Hanns-Peter; Delitz, Jan Torben; Walter, Peter; Schulte-Schrepping, Horst; Seeck, Oliver H; Franz, Hermann

    2015-05-01

    Powder X-ray diffraction techniques largely benefit from the superior beam quality provided by high-brilliance synchrotron light sources in terms of photon flux and angular resolution. The High Resolution Powder Diffraction Beamline P02.1 at the storage ring PETRA III (DESY, Hamburg, Germany) combines these strengths with the power of high-energy X-rays for materials research. The beamline is operated at a fixed photon energy of 60 keV (0.207 Å wavelength). A high-resolution monochromator generates the highly collimated X-ray beam of narrow energy bandwidth. Classic crystal structure determination in reciprocal space at standard and non-ambient conditions are an essential part of the scientific scope as well as total scattering analysis using the real space information of the pair distribution function. Both methods are complemented by in situ capabilities with time-resolution in the sub-second regime owing to the high beam intensity and the advanced detector technology for high-energy X-rays. P02.1's efficiency in solving chemical and crystallographic problems is illustrated by presenting key experiments that were carried out within these fields during the early stage of beamline operation.

  10. Beamline P02.1 at PETRA III for high-resolution and high-energy powder diffraction

    PubMed Central

    Dippel, Ann-Christin; Liermann, Hanns-Peter; Delitz, Jan Torben; Walter, Peter; Schulte-Schrepping, Horst; Seeck, Oliver H.; Franz, Hermann

    2015-01-01

    Powder X-ray diffraction techniques largely benefit from the superior beam quality provided by high-brilliance synchrotron light sources in terms of photon flux and angular resolution. The High Resolution Powder Diffraction Beamline P02.1 at the storage ring PETRA III (DESY, Hamburg, Germany) combines these strengths with the power of high-energy X-rays for materials research. The beamline is operated at a fixed photon energy of 60 keV (0.207 Å wavelength). A high-resolution monochromator generates the highly collimated X-ray beam of narrow energy bandwidth. Classic crystal structure determination in reciprocal space at standard and non-ambient conditions are an essential part of the scientific scope as well as total scattering analysis using the real space information of the pair distribution function. Both methods are complemented by in situ capabilities with time-resolution in the sub-second regime owing to the high beam intensity and the advanced detector technology for high-energy X-rays. P02.1’s efficiency in solving chemical and crystallographic problems is illustrated by presenting key experiments that were carried out within these fields during the early stage of beamline operation. PMID:25931084

  11. Versatile sample environments and automation for biological solution X-ray scattering experiments at the P12 beamline (PETRA III, DESY)

    PubMed Central

    Blanchet, Clement E.; Spilotros, Alessandro; Schwemmer, Frank; Graewert, Melissa A.; Kikhney, Alexey; Jeffries, Cy M.; Franke, Daniel; Mark, Daniel; Zengerle, Roland; Cipriani, Florent; Fiedler, Stefan; Roessle, Manfred; Svergun, Dmitri I.

    2015-01-01

    A high-brilliance synchrotron P12 beamline of the EMBL located at the PETRA III storage ring (DESY, Hamburg) is dedicated to biological small-angle X-ray scattering (SAXS) and has been designed and optimized for scattering experiments on macromolecular solutions. Scatterless slits reduce the parasitic scattering, a custom-designed miniature active beamstop ensures accurate data normalization and the photon-counting PILATUS 2M detector enables the background-free detection of weak scattering signals. The high flux and small beam size allow for rapid experiments with exposure time down to 30–50 ms covering the resolution range from about 300 to 0.5 nm. P12 possesses a versatile and flexible sample environment system that caters for the diverse experimental needs required to study macromolecular solutions. These include an in-vacuum capillary mode for standard batch sample analyses with robotic sample delivery and for continuous-flow in-line sample purification and characterization, as well as an in-air capillary time-resolved stopped-flow setup. A novel microfluidic centrifugal mixing device (SAXS disc) is developed for a high-throughput screening mode using sub-microlitre sample volumes. Automation is a key feature of P12; it is controlled by a beamline meta server, which coordinates and schedules experiments from either standard or nonstandard operational setups. The integrated SASFLOW pipeline automatically checks for consistency, and processes and analyses the data, providing near real-time assessments of overall parameters and the generation of low-resolution models within minutes of data collection. These advances, combined with a remote access option, allow for rapid high-throughput analysis, as well as time-resolved and screening experiments for novice and expert biological SAXS users. PMID:25844078

  12. Characterization of the Support and Drive System of the PETRA III APPLE Undulator

    SciTech Connect

    Bahrdt, J.; Baecker, H.-J.; Frentrup, W.; Gaupp, A.; Gottschlich, S.; Kuhn, C.; Scheer, M.; Schulz, B.; Gast, M.; Englisch, U.; Schoeps, A.; Tischer, M.

    2010-06-23

    Helmholtzzentrum Berlin has built an APPLE II undulator for the storage ring PETRA III. The device has a total length of 5m and a minimum gap of 11mm. The high magnetic forces in particular in the inclined mode have been analyzed by means of finite element methods (FEM). Specific mechanic components such as flexible joints have been optimized to cope with the gap- and shift-dependent 3D-forces and a sophisticated control and drive system has been implemented. After completion of the device, detailed laser interferometer measurements for all operation modes have been performed. The data are compared to the FEM simulations.

  13. Residual Gas X-ray Beam Position Monitor Development for PETRA III

    SciTech Connect

    Ilinski, P.; Hahn, U.; Schulte-Schrepping, H.; Degenhardt, M.

    2007-01-19

    The development effort is driven by the need for a new type of x-ray beam position monitor (XBPM), which will detect the centre of gravity of the undulator beam. XBPMs based on the ionization of a residual gas are considered being the candidate for this future ''white'' undulator beam XBPMs. A number of residual gas XBPM prototypes for the PETRA III storage ring were developed and tested. Tests were performed at DESY and the ESRF, resolution of beam position up to 5 {mu}m is reported. The further development of the RGXBPMs will be focused on improvements of resolution, readout speed and reliability.

  14. Vibration measurements of high-heat-load monochromators for DESY PETRA III extension.

    PubMed

    Kristiansen, Paw; Horbach, Jan; Döhrmann, Ralph; Heuer, Joachim

    2015-07-01

    The requirement for vibrational stability of beamline optics continues to evolve rapidly to comply with the demands created by the improved brilliance of the third-generation low-emittance storage rings around the world. The challenge is to quantify the performance of the instrument before it is installed at the beamline. In this article, measurement techniques are presented that directly and accurately measure (i) the relative vibration between the two crystals of a double-crystal monochromator (DCM) and (ii) the absolute vibration of the second-crystal cage of a DCM. Excluding a synchrotron beam, the measurements are conducted under in situ conditions, connected to a liquid-nitrogen cryocooler. The investigated DCM utilizes a direct-drive (no gearing) goniometer for the Bragg rotation. The main causes of the DCM vibration are found to be the servoing of the direct-drive goniometer and the flexibility in the crystal cage motion stages. It is found that the investigated DCM can offer relative pitch vibration down to 48 nrad RMS (capacitive sensors, 0-5 kHz bandwidth) and absolute pitch vibration down to 82 nrad RMS (laser interferometer, 0-50 kHz bandwidth), with the Bragg axis brake engaged.

  15. Vibration measurements of high-heat-load monochromators for DESY PETRA III extension

    PubMed Central

    Kristiansen, Paw; Horbach, Jan; Döhrmann, Ralph; Heuer, Joachim

    2015-01-01

    The requirement for vibrational stability of beamline optics continues to evolve rapidly to comply with the demands created by the improved brilliance of the third-generation low-emittance storage rings around the world. The challenge is to quantify the performance of the instrument before it is installed at the beamline. In this article, measurement techniques are presented that directly and accurately measure (i) the relative vibration between the two crystals of a double-crystal monochromator (DCM) and (ii) the absolute vibration of the second-crystal cage of a DCM. Excluding a synchrotron beam, the measurements are conducted under in situ conditions, connected to a liquid-nitrogen cryocooler. The investigated DCM utilizes a direct-drive (no gearing) goniometer for the Bragg rotation. The main causes of the DCM vibration are found to be the servoing of the direct-drive goniometer and the flexibility in the crystal cage motion stages. It is found that the investigated DCM can offer relative pitch vibration down to 48 nrad RMS (capacitive sensors, 0–5 kHz bandwidth) and absolute pitch vibration down to 82 nrad RMS (laser interferometer, 0–50 kHz bandwidth), with the Bragg axis brake engaged. PMID:26134790

  16. ASAP3 - New Data Taking and Analysis Infrastructure for PETRA III

    NASA Astrophysics Data System (ADS)

    Strutz, M.; Gasthuber, M.; Aplin, S.; Dietrich, S.; Kuhn, M.; Ensslin, U.; Smirnov, G.; Lewendel, B.; Guelzow, V.

    2015-12-01

    Data taking and analysis infrastructures in HEP (High Energy Physics) have evolved during many years to a well known problem domain. In contrast to HEP, third generation synchrotron light sources, existing and upcoming free electron lasers are confronted with an explosion in data rates driven primarily by recent developments in 2D pixel array detectors. The next generation of detectors will produce data in the region upwards of 50 Gbytes per second. At synchrotrons, data was traditionally taken away by users following data taking using portable media. This will clearly not scale at all. We present first experiences of our new architecture and underlying services based on results taken from the resumption of data taking in April 2015. Technology choices were undertaking over a period of twelve month. The work involved a close collaboration between central IT, beamline controls, and beamline support staff. In addition a cooperation was established between DESY IT and IBM to include industrial research and development experience and skills. Our approach integrates HPC technologies for storage systems and protocols. In particular, our solution uses a single file-system instance with a multiple protocol access, while operating within a single namespace.

  17. Analysis of coupled-bunch instabilities for the NSLS-II storage ring with a 500 MHz 7-cell PETRA-III cavity

    NASA Astrophysics Data System (ADS)

    Bassi, G.; Blednykh, A.; Cheng, W.; Gao, F.; Rose, J.; Teytelman, D.

    2016-02-01

    The NSLS-II storage ring is designed to operate with superconducting RF-cavities with the aim to store an average current of 500 mA distributed in 1080 bunches, with a gap in the uniform filling for ion clearing. At the early stage of the commissioning (phase 1), characterized by a bare lattice without damping wigglers and without Landau cavities, a normal conducting 7-cell PETRA-III RF-cavity structure has been installed with the goal to store an average current of 25 mA. In this paper we discuss our analysis of coupled-bunch instabilities driven by the Higher Order Modes (HOMs) of the 7-cell PETRA-III RF-cavity. As a cure of the instabilities, we apply a well-known scheme based on a proper detuning of the HOMs frequencies based upon cavity temperature change, and the use of the beneficial effect of the slow head-tail damping at positive chromaticity to increase the transverse coupled-bunch instability thresholds. In addition, we discuss measurements of coupled-bunch instabilities observed during the phase 1 commissioning of the NSLS-II storage ring. In our analysis we rely, in the longitudinal case, on the theory of coupled-bunch instability for uniform fillings, while in the transverse case we complement our studies with numerical simulations with OASIS, a novel parallel particle tracking code for self-consistent simulations of collective effects driven by short and long-range wakefields.

  18. Development of a scanning transmission x-ray microscope for the beamline P04 at PETRA III DESY

    NASA Astrophysics Data System (ADS)

    Andrianov, Konstantin; Ewald, Johannes; Nisius, Thomas; Lühl, Lars; Malzer, Wolfgang; Kanngießer, Birgit; Wilhein, Thomas

    2016-01-01

    We present a scanning transmission x-ray microscope (STXM) built on top of our existing modular platform for high resolution imaging experiments. This platform consists of up to three separate vacuum chambers and custom designed piezo stages. These piezo stages are able to move precisely in x-, y- and z-direction, this makes it possible to adjust the components for different imaging modes. During recent experiments the endstation was operated mainly as a transmission x-ray microscope (TXM) [1, 2].

  19. PETRA Yearbook 1992-1993.

    ERIC Educational Resources Information Center

    Commission of the European Communities, Brussels (Belgium).

    This yearbook of PETRA, the European Community's program for providing youths with vocational training and preparing them for adulthood and work, contains 14 articles: "PETRA's Added Value" (Welbers); "Beyond the Fallen Wall" (Hanf); "Project Report: A Flyweight Becomes a Bricklayer"; "PETRA's Southern Tip" (Kourkouta, Chatzipanagiotou);…

  20. Gradient-Modulated PETRA MRI

    PubMed Central

    Kobayashi, Naoharu; Goerke, Ute; Wang, Luning; Ellermann, Jutta; Metzger, Gregory J.; Garwood, Michael

    2015-01-01

    Image blurring due to off-resonance and fast T2* signal decay is a common issue in radial ultrashort echo time MRI sequences. One solution is to use a higher readout bandwidth, but this may be impractical for some techniques like pointwise encoding time reduction with radial acquisition (PETRA), which is a hybrid method of zero echo time and single point imaging techniques. Specifically, PETRA has severe specific absorption rate (SAR) and radiofrequency (RF) pulse peak power limitations when using higher bandwidths in human measurements. In this study, we introduce gradient modulation (GM) to PETRA to reduce image blurring artifacts while keeping SAR and RF peak power low. Tolerance of GM-PETRA to image blurring was evaluated in simulations and experiments by comparing with the conventional PETRA technique. We performed inner ear imaging of a healthy subject at 7T. GM-PETRA showed significantly less image blurring due to off-resonance and fast T2* signal decay compared to PETRA. In in vivo imaging, GM-PETRA nicely captured complex structures of the inner ear such as the cochlea and semicircular canals. Gradient modulation can improve the PETRA image quality and mitigate SAR and RF peak power limitations without special hardware modification in clinical scanners. PMID:26771005

  1. Petra and the Nabataeans

    NASA Astrophysics Data System (ADS)

    Belmonte, Juan Antonio; González-García, A. César

    The Nabataeans built several monuments in Petra and elsewhere displaying decoration with a certain preference for astronomical motifs. A statistical analysis of the orientation of their sacred monuments demonstrates that astronomical orientations were often part of an elaborate plan and possibly reflect traces of the astral nature of Nabataean religion. Petra and other monuments in the ancient Nabataean kingdom demonstrate the interaction between landscape features and astronomical events. Among other things, the famous Ad Deir has revealed a fascinating ensemble of light and shadow effects, perhaps connected with the bulk of Nabataean mythology, while a series of suggestive solstitial and equinoctial alignments emanate from the impressive Urn Tomb, which might have helped bring about its selection as the cathedral of the city.

  2. The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III

    PubMed Central

    Liermann, H.-P.; Konôpková, Z.; Morgenroth, W.; Glazyrin, K.; Bednarčik, J.; McBride, E. E.; Petitgirard, S.; Delitz, J. T.; Wendt, M.; Bican, Y.; Ehnes, A.; Schwark, I.; Rothkirch, A.; Tischer, M.; Heuer, J.; Schulte-Schrepping, H.; Kracht, T.; Franz, H.

    2015-01-01

    A detailed description is presented of the Extreme Conditions Beamline P02.2 for micro X-ray diffraction studies of matter at simultaneous high pressure and high/low temperatures at PETRA III, in Hamburg, Germany. This includes performance of the X-ray optics and instrumental resolution as well as an overview of the different sample environments available for high-pressure studies in the diamond anvil cell. Particularly emphasized are the high-brilliance and high-energy X-ray diffraction capabilities of the beamline in conjunction with the use of fast area detectors to conduct time-resolved compression studies in the millisecond time regime. Finally, the current capability of the Extreme Conditions Science Infrastructure to support high-pressure research at the Extreme Conditions Beamline and other PETRA III beamlines is described. PMID:26134794

  3. A compact and low-weight sputtering unit for in situ investigations of thin film growth at synchrotron radiation beamlines

    SciTech Connect

    Walter, P.; Dippel, A.-C.; Pflaum, K.; Wernecke, J.; Blume, J.; Hurk, J. van den; Klemradt, U.

    2015-05-15

    In this work, we report on a highly variable, compact, and light high-vacuum sputter deposition unit designed for in situ experiments using synchrotron radiation facilities. The chamber can be mounted at various synchrotron beamlines for scattering experiments in grazing incidence geometry. The sample position and the large exit window allow to perform x-ray experiments up to large q values. The sputtering unit is easy to mount on existing experimental setups and can be remote-controlled. In this paper, we describe in detail the design and the performance of the new sputtering chamber and present the installation of the apparatus at different 3rd generation light sources. Furthermore, we describe the different measurement options and present some selected results. The unit has been successfully commissioned and is now available for users at PETRA III at DESY.

  4. A compact and low-weight sputtering unit for in situ investigations of thin film growth at synchrotron radiation beamlines.

    PubMed

    Walter, P; Dippel, A-C; Pflaum, K; Wernecke, J; van den Hurk, J; Blume, J; Klemradt, U

    2015-05-01

    In this work, we report on a highly variable, compact, and light high-vacuum sputter deposition unit designed for in situ experiments using synchrotron radiation facilities. The chamber can be mounted at various synchrotron beamlines for scattering experiments in grazing incidence geometry. The sample position and the large exit window allow to perform x-ray experiments up to large q values. The sputtering unit is easy to mount on existing experimental setups and can be remote-controlled. In this paper, we describe in detail the design and the performance of the new sputtering chamber and present the installation of the apparatus at different 3rd generation light sources. Furthermore, we describe the different measurement options and present some selected results. The unit has been successfully commissioned and is now available for users at PETRA III at DESY.

  5. Hadron production at PEP/PETRA

    SciTech Connect

    Yamamoto, H.

    1985-12-01

    Recent results on hadron production in e/sup +/e/sup -/ annihilation at PEP and PETRA are summarized. The topics included are: (1) inclusive hadron production, (2) gluon vs quark jet, (3) analysis of 3 jet events and (4) p - anti p correlations. Experimental data are compared with predictions of several models to reveal underlying physics. 47 refs., 18 figs.

  6. Recent results on baryon production at PETRA

    SciTech Connect

    Wu, S.L.

    1982-01-01

    One of the recent excitements at PETRA is the observation of the copious production of baryons. About a year ago, TASSO observed the inclusive production of protons and antiprotons. More recently JADE confirmed the inclusive antiproton spectrum to about 1 GeV/c and also observed the inclusive anti ..lambda.. spectrum to about 1.4 GeV/c, while TASSO obtained the ..lambda.. and anti-..lambda.. spectrum all the way up 10 GeV/c in momentum.

  7. G4beamline

    SciTech Connect

    2011-05-24

    G4beamline is a single-particle-tracking simulation code based on the Geant4 toolkit. It is specifically optimized for the realistic evaluation of beam lines. It is especially useful for evaluating future muon facilities.

  8. Hutch for CSX Beamlines

    SciTech Connect

    Ed Haas

    2012-12-12

    NSLS-II will produce x-rays 10,000 times brighter than NSLS. To keep people safe from intense x-rays in the new facility, special enclosures, called hutches, will surround particular sections of beamlines.

  9. Hutch for CSX Beamlines

    ScienceCinema

    Ed Haas

    2016-07-12

    NSLS-II will produce x-rays 10,000 times brighter than NSLS. To keep people safe from intense x-rays in the new facility, special enclosures, called hutches, will surround particular sections of beamlines.

  10. e/sup +/e/sup -/ collisions: results from PETRA

    SciTech Connect

    Hilger, E.

    1982-01-01

    A selection of most recent results obtained by the five experiments CELLO, JADE, MARK J, PLUTO, and TASSO at PETRA is presented. The many interesting new results include, for example, the observation of effects of 2nd order QCD, details of inclusive hadron production, and the measurement of the forward-backward asymmetry in lepton pair production due to weak and electromagnetic interference.

  11. Single-crystal diffraction at the Extreme Conditions beamline P02.2: procedure for collecting and analyzing high-pressure single-crystal data.

    PubMed

    Rothkirch, André; Gatta, G Diego; Meyer, Mathias; Merkel, Sébastien; Merlini, Marco; Liermann, Hanns Peter

    2013-09-01

    Fast detectors employed at third-generation synchrotrons have reduced collection times significantly and require the optimization of commercial as well as customized software packages for data reduction and analysis. In this paper a procedure to collect, process and analyze single-crystal data sets collected at high pressure at the Extreme Conditions beamline (P02.2) at PETRA III, DESY, is presented. A new data image format called `Esperanto' is introduced that is supported by the commercial software package CrysAlis(Pro) (Agilent Technologies UK Ltd). The new format acts as a vehicle to transform the most common area-detector data formats via a translator software. Such a conversion tool has been developed and converts tiff data collected on a Perkin Elmer detector, as well as data collected on a MAR345/555, to be imported into the CrysAlis(Pro) software. In order to demonstrate the validity of the new approach, a complete structure refinement of boron-mullite (Al5BO9) collected at a pressure of 19.4 (2) GPa is presented. Details pertaining to the data collections and refinements of B-mullite are presented. PMID:23955034

  12. The SLS optics beamline

    SciTech Connect

    Flechsig, U.; Abela, R.; Betemps, R.; Blumer, H.; Frank, K.; Jaggi, A.; MacDowell A.A.; Padmore, H.A.; Schonherr, V.; Ulrich, J.; Walther, H.; Zelenika, S.; Zumbach, C.

    2006-05-20

    A multipurpose beamline for tests and developments in the field of x-ray optics and synchrotron radiation instrumentation in general is under construction at the Swiss Light Source (SLS) bending magnet X05DA. The beamline uses a newly developed UHV compatible, 100 mm thick, brazed CVD diamond vacuum window. The very compact cryogenically cooled channel cut Si(111) monochromator and bendable 1:1 toroidal focusing mirror at 7:75 m from the source point are installed inside the shielding tunnel. The beamline covers a photon energy range of about 6 to 17 keV.We expect 5x1011 photons=s within a 100 mu m spot and a resolving power of 1300. The monochromator and focusing mirror can be retracted independently for unfocused monochromatic and focused ''white'' light operation respectively.

  13. Secure network for beamline control

    NASA Astrophysics Data System (ADS)

    Ohata, T.; Fukui, T.; Ishii, M.; Furukawa, Y.; Nakatani, T.; Matsushita, T.; Takeuchi, M.; Tanaka, R.; Ishikawa, T.

    2001-07-01

    In SPring-8, beamline control system is constructed with a highly available distributed network system. The socket based communication protocol is used for the beamline control mainly. Beamline users can control the equipment by sending simple control commands to a server process, which is running on a beamline-managing computer (Ohata et al., SPring-8 beamline control system, ICALEPCS'99, Trieste, Italy, 1999). At the beginning the network was based on the shared topology at all beamlines. Consequently, it has a risk for misapplication of the user's program to access different machines on the network system cross over beamlines. It is serious problem for the SPring-8 beamline control system, because all beamlines controlled with unified software interfaces. We introduced the switching technology and the firewalls to support network access control. Also the virtual networking (VLAN: IEEE 802.1Q) and the gigabit Ethernet technology (IEEE 802.3ab) are introduced. Thus the network security and the reliability are guaranteed at the higher level in SPring-8 beamline.

  14. APS beamline standard components handbook

    SciTech Connect

    Kuzay, T.M.

    1992-01-01

    It is clear that most Advanced Photon Source (APS) Collaborative Access Team (CAT) members would like to concentrate on designing specialized equipment related to their scientific programs rather than on routine or standard beamline components. Thus, an effort is in progress at the APS to identify standard and modular components of APS beamlines. Identifying standard components is a nontrivial task because these components should support diverse beamline objectives. To assist with this effort, the APS has obtained advice and help from a Beamline Standardization and Modularization Committee consisting of experts in beamline design, construction, and operation. The staff of the Experimental Facilities Division identified various components thought to be standard items for beamlines, regardless of the specific scientific objective of a particular beamline. A generic beamline layout formed the basis for this identification. This layout is based on a double-crystal monochromator as the first optical element, with the possibility of other elements to follow. Pre-engineering designs were then made of the identified standard components. The Beamline Standardization and Modularization Committee has reviewed these designs and provided very useful input regarding the specifications of these components. We realize that there will be other configurations that may require special or modified components. This Handbook in its current version (1.1) contains descriptions, specifications, and pre-engineering design drawings of these standard components. In the future, the APS plans to add engineering drawings of identified standard beamline components. Use of standard components should result in major cost reductions for CATs in the areas of beamline design and construction.

  15. Sun Cities: Thebes, Hattusha, and Petra: A Landscape Story

    NASA Astrophysics Data System (ADS)

    Belmonte, J. A.; González-García, A. C.

    2016-01-01

    The sky is a very important component of the landscape that has been lost in our modern, overcrowded, and excessively illuminated cities. However, this was not the case in the past. Astronomy played a highly relevant role in urban planning, especially in the organization of sacred spaces which were later surrounded by extensive civil urban areas. Today, archaeoastronomy approaches the minds of our ancestors studying the starry landscape and how it is printed in the terrain by the visualization and the orientation of sacred buildings. The sun was indeed the most important component of that celestial landscape and was the primary focus within a large set of unique cultures of great historical significance. In particular, we will study and compare the case of three sun cities: Thebes (Belmonte et al. 2009, Belmonte 2012), Hattusha (Gonzalez-Garcia & Belmonte 2011), and Petra (Belmonte et al. 2013), capitals of Egypt in the Middle and New Kingdoms, the Hittite Empire, and the Nabataean Kingdom, respectively. We will briefly discuss each of these cultures and will scrutinize their capital cities, showing how their strategic geographical position and orography were of key importance, but also how solar observation, and related hierophanies, played a relevant role in the orientation and location of some of their most significant monuments. In particular, we will focus on the great temple of Amun-Re in Karnak, Temple 1 in Hattusha (presumably devoted to the Solar Goddess of Arinna), and the “Monastery” at Petra.

  16. PLS photoemission electron microscopy beamline

    NASA Astrophysics Data System (ADS)

    Kang, Tai-Hee; Kim, Ki-jeong; Hwang, C. C.; Rah, S.; Park, C. Y.; Kim, Bongsoo

    2001-07-01

    The performance of a recently commissioned beamline at the Pohang Light Source (PLS) is described. The beamline, which is located at 4B1 at PLS, is a Varied Line Spacing (VLS) Plane Grating Monochromator (PGM) beamline. VLS PGM has become very popular because of the simple scanning mechanism and the fixed exit slit. The beamline which takes 3 mrad horizontal beam fan from bending magnet, covers the energy range 200-1000 eV for Photoemission Electron Microscopy (PEEM), X-ray Photoelectron Spectroscopy (XPS) and Magnetic Circular Dichroism (MCD) experiments. Simplicity of the optics and high flux with medium resolution were the design goals for these applications. The beamline consists of a horizontal focusing mirror, a vertical focusing mirror, VLS plane grating and exit slit. The source of PLS could be used as a virtual entrance slit because of its small size and stability. The flux and the resolution of the beamline at the experimental station have been measured using an ion chamber and a calibrated photodiode. Test images of PEEM from a standard sample were taken to illustrate the further performance of the beamline and PEEM station.

  17. SPring-8 Structural Biology Beamlines / Automatic Beamline Operation at RIKEN Structural Genomics Beamlines

    SciTech Connect

    Ueno, Go; Hasegawa, Kazuya; Okazaki, Nobuo; Sakai, Hisanobu; Kumasaka, Takashi; Yamamoto, Masaki

    2007-01-19

    RIKEN Structural Genomics Beamlines (BL26B1 and BL26B2) at SPring-8 have been constructed for high throughput protein crystallography. The beamline operation is automated cooperating with the sample changer robot. The operation software provides a centralized control utilizing the client and server architecture. The sample management system with the networked database has been implemented to accept dry-shipped crystals from distant users.

  18. High power photon beamline elements in the LBL/SSRL/EXXON Beamline VI

    SciTech Connect

    Hoyer, E.

    1992-09-01

    Beamline VI is a wiggler-based, multi-kilowatt, intense synchrotron radiation beamline installed SPEAR. The thermal design parameters for this beamline are presented and then design considerations and construction descriptions are given for many of the high-power photon beamline elements.

  19. Advanced beamline automation for biological crystallography experiments.

    PubMed

    Cork, Carl; O'Neill, James; Taylor, John; Earnest, Thomas

    2006-08-01

    An automated crystal-mounting/alignment system has been developed at Lawrence Berkeley National Laboratory and has been installed on three of the protein-crystallography experimental stations at the Advanced Light Source (ALS); it is currently being implemented at synchrotron crystallography beamlines at CHESS, NSLS and the APS. The benefits to using an automounter system include (i) optimization of the use of synchrotron beam time, (ii) facilitation of advanced data-collection techniques, (iii) collection of higher quality data, (iv) reduction of the risk to crystals and (v) exploration of systematic studies of experimental protocols. Developments on the next-generation automounter with improvements in robustness, automated alignment and sample tracking are under way, with an end-to-end data-flow process being developed to allow remote data collection and monitoring. PMID:16855300

  20. Beamline pulsing system for cyclotrons

    NASA Astrophysics Data System (ADS)

    Heikkinen, Jouko; Gustafsson, Jouni; Kivikoski, Markku; Liukkonen, Esko; Nieminen, Veikko

    A beamline pulsing system for cyclotrons is presented. The function of this system is to modify the structure of a cyclotron ion beam guided to the desired research target by a beamline. In some in-beam experiments, an adjustment of the time structure of the beam is sometimes needed. This kind of situation occurs if, for example, the life time of the target material is longer than the period corresponding to the beam frequency. In this case, the frequency of the ion pulses hitting the target is 10-21 MHz depending on the frequency of the acceleration voltage. The adjustment of the ion beam pulse frequency is carried out by a beamline deflector. Deflection is achieved by feeding a high-amplitude (10-15 kV) RF-signal between the deflection plates positioned into the beamline. This signal is generated from the cyclotron reference signal by frequency division, phase adjustment and amplification. Simulation and test results indicate that the specified deflection signal level is achieved with 1 kW of RF-power.

  1. Decay of sandstone monuments in Petra (Jordan): Gravity-induced stress as a stabilizing factor

    NASA Astrophysics Data System (ADS)

    Řihošek, Jaroslav; Bruthans, Jiří; Mašín, David; Filippi, Michal; Schweigstillova, Jana

    2016-04-01

    As demonstrated by physical experiments and numerical modeling the gravity-induced stress (stress in further text) in sandstone massive reduces weathering and erosion rate (Bruthans et al. 2014). This finding is in contrast to common view that stress threatens stability of man-made monuments carved to sandstone. Certain low- levels of gravity-induced stress can in fact stabilize and protect these forms against weathering and disintegration. The purpose of this investigation is to evaluate the effect of the stress on weathering of sandstone monuments at the Petra World Heritage Site in Jordan via field observations, salt weathering experiments, and physical and numerical modeling. Previous studies on weathering of Petra monuments have neglected the impact of stress, but the ubiquitous presence of stress-controlled landforms in Petra suggests that it has a substantial effect on weathering and erosion processes on man-made monuments and natural surfaces. Laboratory salt weathering experiments with cubes of Umm Ishrin sandstone from Petra demonstrated the inverse relationship between stress magnitude and decay rate. Physical modeling with Strelec locked sand from the Czech Republic was used to simulate weathering and decay of Petra monuments. Sharp forms subjected to water erosion decayed to rounded shapes strikingly similar to tombs in Petra subjected to more than 2000 years of weathering and erosion. The physical modeling results enabled visualization of the recession of monument surfaces in high spatial and temporal resolution and indicate that the recession rate of Petra monuments is far from constant both in space and time. Numerical modeling of stress fields confirms the physical modeling results. This novel approach to investigate weathering clearly demonstrates that increased stress decreases the decay rate of Petra monuments. To properly delineate the endangered zones of monuments, the potential damage caused by weathering agents should be combined with stress

  2. ALS beamline design requirements: A guide for beamline designers

    SciTech Connect

    1996-06-01

    This manual is written as a guide for researchers in designing beamlines and endstations acceptable for use at the ALS. It contains guidelines and policies related to personnel safety and equipment and vacuum protection. All equipment and procedures must ultimately satisfy the safety requirements set aside in the Lawrence Berkeley National Laboratory (LBNL) Health and Safety Manual (PUB-3000) which is available from the ALS User Office or on the World WideWeb from the LBNL Homepage (http:// www.lbl.gov).

  3. Particle searches in e/sup +/e/sup -/ experiments at PEP and PETRA

    SciTech Connect

    Lau, K.H.

    1982-10-01

    This talk reviews recent results in new particle searches performed by experiments at the high energy e/sup +/e/sup -/ storage rings PEP and PETRA. It concentrates on recent searches for: hadrons with a new quark flavor, spin-1/2 charged heavy leptons, spin-0 charged leptons, spin-0 point-like scalars or pseudoscalars, and neutral heavy leptons.

  4. SPring-8 beamline control system.

    PubMed

    Ohata, T; Konishi, H; Kimura, H; Furukawa, Y; Tamasaku, K; Nakatani, T; Tanabe, T; Matsumoto, N; Ishii, M; Ishikawa, T

    1998-05-01

    The SPring-8 beamline control system is now taking part in the control of the insertion device (ID), front end, beam transportation channel and all interlock systems of the beamline: it will supply a highly standardized environment of apparatus control for collaborative researchers. In particular, ID operation is very important in a third-generation synchrotron light source facility. It is also very important to consider the security system because the ID is part of the storage ring and is therefore governed by the synchrotron ring control system. The progress of computer networking systems and the technology of security control require the development of a highly flexible control system. An interlock system that is independent of the control system has increased the reliability. For the beamline control system the so-called standard model concept has been adopted. VME-bus (VME) is used as the front-end control system and a UNIX workstation as the operator console. CPU boards of the VME-bus are RISC processor-based board computers operated by a LynxOS-based HP-RT real-time operating system. The workstation and the VME are linked to each other by a network, and form the distributed system. The HP 9000/700 series with HP-UX and the HP 9000/743rt series with HP-RT are used. All the controllable apparatus may be operated from any workstation. PMID:15263588

  5. Design of the LBNF Beamline

    SciTech Connect

    Papadimitriou, V.; Andrews, R.; Hylen, J.; Kobilarcik, T.; Krafczyk, G.; Marchinonni, A.; Moore, C. D.; Schlabach, P.; Tariq, S.

    2015-08-30

    The Long Baseline Neutrino Facility (LBNF) will utilize a beamline located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band neutrino beam toward underground detectors placed at the SURF Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60-120 GeV) will be extracted from the MI-10 section of Fermilab’s Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are subsequently focused by magnetic horns into a 204 m long decay pipe where they decay into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial proton beam power is expected to be 1.2 MW; however, the facility is designed to be upgradeable to 2.4 MW. We discuss here the design status and the associated challenges as well as plans for improvements before baselining the facility.

  6. Design of the LBNE Beamline

    SciTech Connect

    Papadimitriou, Vaia; Andrews, Richard; Hylen, James; Kobilarcik, Thomas; Marchionni, Alberto; Moore, Craig D.; Schlabach, Phil; Tariq, Salman

    2015-02-05

    The Long Baseline Neutrino Experiment (LBNE) will utilize a beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a wide band beam of neutrinos toward a detector placed at the Sanford Underground Research Facility in South Dakota, about 1,300 km away. The main elements of the facility are a primary proton beamline and a neutrino beamline. The primary proton beam (60-120 GeV) will be extracted from the MI-10 section of Fermilab’s Main Injector. Neutrinos are produced after the protons hit a solid target and produce mesons which are sign selected and subsequently focused by a set of magnetic horns into a 204 m long decay pipe where they decay mostly into muons and neutrinos. The parameters of the facility were determined taking into account the physics goals, spacial and radiological constraints, and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be ~1.2 MW; however, the facility is designed to be upgradeable for 2.3 MW operation. We discuss here the status of the design and the associated challenges.

  7. Beamline 9.0.1 - a high-resolution undulator beamline for gas-phase spectroscopy

    SciTech Connect

    Bozek, J.D.; Heimann, P.A.; Mossessian, D.

    1997-04-01

    Beamline 9.0.1 at the Advanced Light Source is an undulator beamline with a Spherical Grating Monochromator (SGM) which provides very high resolution and flux over the photon energy range 20-320eV. The beamline has been used primarily by the atomic and molecular science community to conduct spectroscopy experiments using electron, ion and fluorescence photon detection. A description of the beamline and its performance will be provided in this abstract.

  8. After three decades of research, is the Nabataean city of Petra still under threat?

    NASA Astrophysics Data System (ADS)

    Gomez-Heras, M.; Lopez-Arce, P.; Bala'awi, F.; Ishakat, F.; Alvarez de Buergo, M.; Fort, R.; Wedekind, W.

    2012-04-01

    The year 2012 marks the 200th anniversary of the rediscovering of the Nabataean city of Petra (Jordan) by Swiss archaeologist Johann Ludwig Burckhardt. The city of Petra is one of the most singular built-heritage monumental sets in the world because of the size of the built structures, the extension in which these structures appear and the intricate relation between natural and built environment in the site. These are part of the reasons of its uniqueness that conducted to its inscription as a UNESCO World Heritage Site in 1985. However, the conservation and management of such a large archaeological site can be very challenging due to the diverse decay processes and agents operating on the site. As a result, the site conservation has been heavily hindered in the past and Petra was included in 1998, 2000 and 2002 in the former World Monuments Fund list of the one hundred most endangered sites (now World Monuments Watch). It also was described as one of the most endangered world heritage sites in the ICOMOS reports "Heritage at risk". Many studies on the decay processes that operate in Petra have been carried out from the point of view of earth sciences, from the first studies carried out in the 80's by many researchers from several countries, funded by very different funding schemes; sometimes working on different specific topics within the high variability of existing problems in Petra, but sometimes, working in parallel without communication. In addition to this, many of the studies carried out locally have not been published internationally and therefore neither have not reached the wider scientific community nor the local decision makers. Petra is, therefore, a good example of how a complex and large site may favour a research environment in which scientific results are fragmentary and synergies are not generated, moreover when it should be approached under inter and multidisciplinary teams. These synergies could be of great benefit, not only to the scientific

  9. BNL ATF II beamlines design

    SciTech Connect

    Fedurin, M.; Jing, Y.; Stratakis, D.; Swinson, C.

    2015-05-03

    The Brookhaven National Laboratory. Accelerator Test Facility (BNL ATF) is currently undergoing a major upgrade (ATF-II). Together with a new location and much improved facilities, the ATF will see an upgrade in its major capabilities: electron beam energy and quality and CO2 laser power. The electron beam energy will be increased in stages, first to 100-150 MeV followed by a further increase to 500 MeV. Combined with the planned increase in CO2 laser power (from 1-100 TW), the ATF-II will be a powerful tool for Advanced Accelerator research. A high-brightness electron beam, produced by a photocathode gun, will be accelerated and optionally delivered to multiple beamlines. Besides the energy range (up to a possible 500 MeV in the final stage) the electron beam can be tailored to each experiment with options such as: small transverse beam size (<10 um), short bunch length (<100 fsec) and, combined short and small bunch options. This report gives a detailed overview of the ATFII capabilities and beamlines configuration.

  10. Dismantling of the PETRA glove box: tritium contamination and inventory assessment

    SciTech Connect

    Wagner, R.

    2015-03-15

    The PETRA facility is the first installation in which experiments with tritium were carried out at the Tritium Laboratory Karlsruhe. After completion of two main experimental programs, the decommissioning of PETRA was initiated with the aim to reuse the glove box and its main still valuable components. A decommissioning plan was engaged to: -) identify the source of tritium release in the glove box, -) clarify the status of the main components, -) assess residual tritium inventories, and -) de-tritiate the components to be disposed of as waste. Several analytical techniques - calorimetry on small solid samples, wipe test followed by liquid scintillation counting for surface contamination assessment, gas chromatography on gaseous samples - were deployed and cross-checked to assess the remaining tritium inventories and initiate the decommissioning process. The methodology and the main outcomes of the numerous different tritium measurements are presented and discussed. (authors)

  11. An artistic and mythological study of a Nabatean female Sphinx from Petra, Jordan.

    NASA Astrophysics Data System (ADS)

    Almasri, Eyad R.; Al-Ajlouny, Fardous K.; Alghazawi, Raed Y.

    In 1967 the Group of Sculptures was discovered in Petra during clearance works organized by the Department of Antiquities in Jordan in the Temenos of Qasr el Bint around the Temenos Gate. One of these sculptures was a high relief statue of a female sphinx. Due to the paucity of information about this statue, this paper has been written to answer a number of questions: What was its original site or monument? When was it made? Who was the deity or deities it represented? Could there be another interpretation of its existence? The answers to the above provide enlightenment of Nabataean styles of carvings and an insight into their religious thoughts. Rgarding the interpretation of the Female Sphinx. Three ideas have been suggested. First, it can be the main Nabataean goddess Allat, "the mother of the gods". Second, it is an image of Petra as a goddess. Third, it is carved on the Temenos Gate as a guardian of Petra city in general and its holy monuments like temples and tombs in particular.

  12. Diagnostic X-Multi-Axis Beamline

    SciTech Connect

    Paul, A C

    2000-04-05

    Tomographic reconstruction of explosive events require time resolved multipal lines of sight. Considered here is a four (or eight) line of sight beam layout for a nominal 20 MeV 2000 Ampere 2 microsecond electron beam for generation of x-rays 0.9 to 5 meters from a given point, the ''firing point''. The requirement of a millimeter spatial x-ray source requires that the electron beam be delivered to the converter targets with sub-millimeter precision independent of small variations in beam energy and initial conditions. The 2 usec electron beam pulse allows for four bursts in each line, separated in time by about 500 microseconds. Each burst is divided by a electro-magnetic kicker into four (or eight) pulses, one for each beamline. The arrival time of the four (or eight) beam pulses at the x-ray target can be adjusted by the kicker timing and the sequence that the beams of each burst are switched into the different beamlines. There exists a simple conceptual path from a four beamline to a eight beamline upgrade. The eight line beamline is built up from seven unique types of sub-systems or ''blocks''. The beamline consists of 22 of these functional blocks and contains a total of 455 individual magnets, figure 1. The 22 blocks are inter-connected by a total of 30 straight line inter-block sections (IBS). Beamlines 1-4 are built from 12 blocks with conceptual layout structure shown in figure 2. Beamlines 5-8 are built with an additional 10 blocks with conceptual layout structure shown in figure 3. This beamline can be thought of as looking like a lollipop consisting of a 42 meter long stick leading to a 60 by 70 meter rectangular candy blob consisting of the eight lines of sight. The accelerator providing the electron beam is at the end of the stick and the firing point is at the center of the blob. The design allows for a two stage implementation. Beamlines 1-3 can be installed to provide a tomographic azimuthal resolution of 45 degrees. An upgrade can later be made

  13. Innovations in the design of mechanical components for a beamline -- The SRl`95 Workshop 2 summary

    SciTech Connect

    Kuzay, T.M.; Warwick, T.

    1995-12-31

    The Synchrotron Radiation Instrumentation 1995 Conference (SRI`95) was hosted by the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). Of the many workshops within the conference, the SRI`95 Workshop 2 was ``Innovations in the Design of Mechanical Components of a Beamline``. The workshop was attended well with over 140 registrants. The following topics were discussed. Industry`s perspective on the status and future was provided by Huber Diffrationtechnik, Oxford Instruments, and Kohzu Seiko Ltd. on goniometers/diffractometers, advanced manufacturing technique of high heat load components, such as the APS photon shutter, and the specialties of monochromators provided to the third-generation synchrotrons, respectively. This was followed by a description of the engineering of a dual function monochromator design for water-cooled diamond or cryogenically cooled silicon monochromators by CMC CAT/APS. Another category was the nagging problem of sensitivity of the photon beam position monitors (XBPM) to bending magnet radiation (``BM contamination``) and the undulator magnet gap changes. Problem descriptions and suggested solutions were provided by both the Advanced Light Source (ALS) and the APS. Other innovative ideas were the cooling schemes (enhanced cooling of beamline components using metallic porous meshes including cryo-cooled applications); Glidcop photon shutter design using microchannels at the ALS; and window/filter design, manufacture and operational experiences at CHESS and PETRA/HASYLAB. Additional discussions were held on designing for micromotions and precision in the optical support systems and smart user filter schemes. This is a summary of the presentations at the Workshop. 5 refs., 5 figs.

  14. RF deflector system for beamlines

    NASA Astrophysics Data System (ADS)

    Heikkinen, J.; Gustafsson, J.; Kivikoski, M.; Liukkonen, E.; Nieminen, V.

    1999-06-01

    In some in-beam experiments, an adjustment of the time structure of the cyclotron ion beam guided to the desired research target by a beamline is sometimes needed. This situation occurs if, for example, the decay times of the reaction products are too short compared to the period corresponding to the beam frequency. In the accelerator laboratory of the University of Jyväskylä the frequency of the ion pulses hitting the research target is 10-21 MHz depending on the frequency of the acceleration voltage. A RF deflector system was constructed to adjust the ion beam pulse frequency according to the respective requirements. A desired portion of the ion pulses are deflected by feeding a high-amplitude RF-signal between deflecting plates located into the beam line. The specified deflecting voltage amplitude of 10-15 kV is achieved with 1 kW of RF power.

  15. Real Beamline Optics from a Synthetic Beam

    SciTech Connect

    Ryan Bodenstein,Michael Tiefenback,Yves Roblin

    2010-05-01

    The Continuous Electron Beam Accelerator Facility (CEBAF) at Jefferson Lab can be described as a series of concatenated beamlines. Methods used to measure the Twiss parameters in closed orbit machines are not applicable in such open ended systems. We are using properly selected sets of real orbits in the accelerator, as one would for numerical analysis. The evolution of these trajectories along the beamline models the behavior of a synthetic beam which deterministically supplements beam profile-based Twiss parameter measurements and optimizes the efficiency of beamline tuning. Examples will be presented alongside a description of the process.

  16. 76 FR 54468 - Petra Pet, Inc. (a/k/a Petrapport) v. Panda Logistics Limited; Panda Logistics Co., Ltd. (f/k/a...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-09-01

    ... Petra Pet, Inc. (a/k/a Petrapport) v. Panda Logistics Limited; Panda Logistics Co., Ltd. (f/k/a panda... Petra Pet, Inc. (a/k/a Petrapport), hereinafter ``Complainant,'' against Respondents Panda Logistics Limited, Panda Logistics Co., Ltd. (f/k/a Panda Int'l Transportation Co., Ltd), and RDM Solutions...

  17. Microspectroscopy At Beamline 73 MAX-lab

    NASA Astrophysics Data System (ADS)

    Engdahl, Anders

    2010-02-01

    Presentation of some projects at the infrared microspectroscopy experimental station at beamline 73 MAX-lab. Among the subjects are found identification of organic residues in fossil material and examination of the chemistry in an old oak wood wreck.

  18. New SRC APPLE ll Variable Polarization Beamline

    SciTech Connect

    M Severson; M Bissen; M Fisher; G Rogers; R Reininger; M Green; D Eisert; B Tredinnick

    2011-12-31

    SRC has recently commissioned a new Varied Line-Spacing Plane Grating Monochromator (VLS-PGM) utilizing as its source a 1 m long APPLE II insertion device in short-straight-section 9 of the Aladdin storage ring. The insertion device reliably delivers horizontal, vertical, and right and left circularly polarized light to the beamline. Measurements from an in situ polarimeter can be used for undulator corrections to compensate for depolarizing effects of the beamline. The beamline has only three optical elements and covers the energy range from 11.1 to 270 eV using two varied line-spacing gratings. A plane mirror rotates to illuminate the gratings at the correct angle to cancel the defocus term at all photon energies. An exit slit and elliptical-toroid refocusing mirror complete the beamline. Using a 50 {mu}m exit slit, the beamline provides moderate to high resolution, with measured flux in the mid 10{sup 12} (photons/s/200 mA) range, and a spot size of 400 {mu}m horizontal by 30 {mu}m vertical.

  19. FLASH2 photon diagnostics and beamline concepts

    NASA Astrophysics Data System (ADS)

    Kuhlmann, M.; Plönjes, E.

    2013-05-01

    FLASH2 is a major extention to the soft X-ray free-electron laser FLASH at DESY. An additional variable-gap undulator line in a new separate tunnel and a new experimental hall will turn FLASH into a multi-beamline FEL user facility. Years of experience as single user facility have high impact on the planned photon diagnostics. Online measurements of intensity, position, wavelength, wavefront, and pulse length are optimized as well as photon beam manipulation tools such as a gas absorber and filters. The beamline system will be set up to cover a wide wavelength range with beamlines capable to deliver down to 0.8 nm in the 5th harmonic and 1st harmonics in the water window to cover the user community's high intrest in this wavelength range. In addition, other beamlines will cover the longer wavelengths from 6 nm - 40 nm and beyond. Proven concepts like the optical laser pump-and-probe instrument are taken over from the current operation scheme in an established way. Permanent endstations with specialized beamline layouts are foreseen. Civil construction and installations in the new FLASH2 tunnel are on-going, first beam is expected for end of 2013, and a first user experiment is anticipated for summer 2014.

  20. National synchrotron light source user's manual: Guide to the VUV and x-ray beamlines: Third edition

    SciTech Connect

    Gmuer, N.F.; Thomlinson, W.; White-DePace, S.

    1989-01-01

    This report contains information on the following topics: A Word on the Writing of Beamline Descriptions; Beamline Equipment Utilization for General Users; the Vacuum Ultraviolet (VUV) Storage Ring and Beamlines; VUV Beamline Descriptions--An Explanation; VUV Beamline Descriptions; X-Ray Storage Ring and Beamlines; X-Ray Beamline Descriptions--An Explanation; and X-Ray Beamline Descriptions.

  1. Status of the Dortmund TGM3-Beamline

    SciTech Connect

    Berges, U.; Westphal, C.; Dreiner, S.; Krause, M.

    2004-05-12

    The former TGM3 beamline at BESSYI was rebuilt at the DELTA storage ring, University of Dortmund, Germany. The beamline uses synchrotron radiation from a dipole bending magnet. The previous design of the beamline had to be adapted to an operation at DELTA. This included a motorized rotation of the first mirror, since that mirror is located within the radiation shield wall at DELTA. Also, further minor components had to be modified, adapted, or replaced. During the set-up at DELTA, previously known operation problems due to mechanical vibrations were eliminated by a complete new mounting of the optical components. The measured performance parameters at BESSYI are compared with calculated results for an operation at DELTA. The first commissioning experiments are currently carried out.

  2. nuSTORM Pion Beamline Design Update

    SciTech Connect

    Liu, A.; Bross, A.; Neuffer, D.; Lee, S. Y.

    2013-09-01

    A facility producing neutrinos from muons that decay in a racetrack ring can provide extremely well understood neutrino beams for oscillation physics and the search for sterile neutrinos. The “neutrinos from STORed Muons” (nuSTORM) facility based on this idea has been introduced by Bross, Neuffer et al. The design of the nuSTORM facility and the particle tracking have been presented in the paper of Liu, et al. This paper demonstrates the recent optimization results of the pion beamline, with G4beamline simulations. The optimum choice of pion beam center momentum, a new algorithm on fitting bivariate Gaussian distribution to the pion phase space data at the downstream side of the horn, and the comparison of the beamline performance with the optics designed based on Graphite and Inconel targets are also described.

  3. IR beamline at the Swiss Light Source

    NASA Astrophysics Data System (ADS)

    Ph, Lerch; L, Quaroni; J, Wambach; J, Schneider; B, Armstrong D.; D, Rossetti; L, Mueller F.; P, Peier; V, Schlott; L, Carroll; P, Friedli; H, Sigg; S, Stutz; M, Tran

    2012-05-01

    The infrared beamline at the Swiss light source uses dipole radiation and is designed to transport light to four experimental stations, A, B, C, D. Branch A is dedicated to far IR work in vacuum; branch B is a micro-spectrometer; branch C is dedicated to high resolution spectroscopy in the gas phase; branch D is a pump and probe set-up. This contribution describes the optical layout and provides a brief survey of currently available experimental stations. The beamline is in regular user operation since 2009.

  4. Neutral beamline with improved ion energy recovery

    DOEpatents

    Dagenhart, William K.; Haselton, Halsey H.; Stirling, William L.; Whealton, John H.

    1984-01-01

    A neutral beamline generator with unneutralized ion energy recovery is provided which enhances the energy recovery of the full energy ion component of the beam exiting the neutralizer cell of the beamline. The unneutralized full energy ions exiting the neutralizer are deflected from the beam path and the electrons in the cell are blocked by a magnetic field applied transverse to the beamline in the cell exit region. The ions, which are generated at essentially ground potential and accelerated through the neutralizer cell by a negative acceleration voltage, are collected at ground potential. A neutralizer cell exit end region is provided which allows the magnetic and electric fields acting on the exiting ions to be closely coupled. As a result, the fractional energy ions exiting the cell with the full energy ions are reflected back into the gas cell. Thus, the fractional energy ions do not detract from the energy recovery efficiency of full energy ions exiting the cell which can reach the ground potential interior surfaces of the beamline housing.

  5. Beamline smoothing of the Advanced Photon Source

    SciTech Connect

    Friedsam, H.; Penicka, M.; Zhao, S.

    1995-06-01

    This paper outlines a general beamline smoothing concept based on the use of First Principle Component analysis. Bean-dine smoothing is commonly used for the detection of blunders in the positioning of beam elements and to provide a smooth particle beam path with the fewest adjustments to individual beam components. It also provides the data for assessment of the achieved positioning quality.

  6. The APS beamline front end vacuum system

    SciTech Connect

    Nielsen, R.W.

    1993-10-15

    This report discusses the design of the vacuum system for the advanced photon source beamline front ends. Included in this report are discussions on: vacuum calculations, the differential pump; front end vacuum set points; cleaning methods and agents; and continuing and completed research and development.

  7. MSFC ESL Facility and Beamline Studies

    NASA Technical Reports Server (NTRS)

    Rogers, J. R.; Hyers, R. W.; Rathz, T. J.; Robinson, M. B.; Kelton, K. F.; Gangopadhyay, A. K.; Woo, G. L.; Fountain, G.; Huie, D.; Allen, T.; Curreri, Peter A. (Technical Monitor)

    2002-01-01

    The poster presentation provides an overview of the MSFC ESL facility. The technical capabilities and accomplishments of the facility are summarized. Future plans including the development of a pressurized processing chamber and additional high-energy X-ray beamline studies are outlined.

  8. The Advanced Light Source (ALS) Slicing Undulator Beamline

    SciTech Connect

    Heimann, P. A.; Glover, T. E.; Plate, D.; Brown, V. C.; Padmore, H. A.; Lee, H. J.; Schoenlein, R. W.

    2007-01-19

    A beamline optimized for the bunch slicing technique has been construction at the Advanced Light Source (ALS). This beamline includes an in-vacuum undulator, soft and hard x-ray beamlines and a femtosecond laser system. The soft x-ray beamline may operate in spectrometer mode, where an entire absorption spectrum is accumulated at one time, or in monochromator mode. The femtosecond laser system has a high repetition rate of 20 kHz to improve the average slicing flux. The performance of the soft x-ray branch of the ALS slicing undulator beamline will be presented.

  9. Human factors design for the BMIT biomedical beamlines

    NASA Astrophysics Data System (ADS)

    Miller, C. Denise; Wysokinski, Tomasz W.; Belev, George; Chapman, L. Dean

    2013-03-01

    Operation of a biomedical beamline poses a unique set of operational and instrumentation challenges for a synchrotron facility. From proper handling and care of live animals and animal tissues, to a user community drawn primarily from the medical and veterinary realms, the work of a biomedical beamline is unique when compared to other beamlines. At the Biomedical Imaging and Therapy (BMIT) beamlines at Canadian Light Source (CLS), operation of the beamlines is geared towards our user community of medical personnel, in addition to basic science researchers. Human factors considerations have been incorporated wherever possible on BMIT, including in the design of software and hardware, as well as ease-of-use features of beamline control stations and experiment hutches. Feedback from users continues to drive usability improvements to beamline operations.

  10. Performance measurements at the SLS SIM beamline

    SciTech Connect

    Flechsig, U.; Nolting, F.; Fraile Rodriguez, A.; Krempasky, J.; Quitmann, C.; Schmidt, T.; Spielmann, S.; Zimoch, D.

    2010-06-23

    The Surface/Interface: Microscopy beamline of the Swiss Light Source started operation in 2001. In 2007 the beamline has been significantly upgraded with a second refocusing section and a blazed grating optimized for high photon flux. Two Apple II type undulators with a plane grating monochromator using the collimated light scheme deliver photons with an energy from 90eV to about 2keV with variable polarization for the photoemission electron microscope (PEEM) as the primary user station. We measured a focus of (45x60) {mu}m({nu}xh) and a photon flux > 10{sup 12} photon/s for all gratings. Polarization switching within a few seconds is realized with the small bandpass of the monochromator and a slight detuning of the undulator.

  11. 1993 CAT workshop on beamline optical designs

    SciTech Connect

    Not Available

    1993-11-01

    An Advanced Photon Source (APS) Collaborative Access Team (CAT) Workshop on Beamline Optical Designs was held at Argonne National Laboratory on July 26--27, 1993. The goal of this workshop was to bring together experts from various synchrotron sources to provide status reports on crystal, reflecting, and polarizing optics as a baseline for discussions of issues facing optical designers for CAT beamlines at the APS. Speakers from the European Synchrotron Radiation Facility (ESRF), the University of Chicago, the National Synchrotron Light Source, and the University of Manchester (England) described single- and double-crystal monochromators, mirrors, glass capillaries, and polarizing optics. Following these presentations, the 90 participants divided into three working groups: Crystal Optics Design, Reflecting Optics, and Optics for Polarization Studies. This volume contains copies of the presentation materials from all speakers, summaries of the three working groups, and a ``catalog`` of various monochromator designs.

  12. An Updated AP2 Beamline TURTLE Model

    SciTech Connect

    Gormley, M.; O'Day, S.

    1991-08-23

    This note describes a TURTLE model of the AP2 beamline. This model was created by D. Johnson and improved by J. Hangst. The authors of this note have made additional improvements which reflect recent element and magnet setting changes. The magnet characteristics measurements and survey data compiled to update the model will be presented. A printout of the actual TURTLE deck may be found in appendix A.

  13. Nomenclature of SLC Arc beamline components

    SciTech Connect

    Silva, J.; Weng, W.T.

    1986-04-10

    This note defines I and C formal names for beamline components in the Arc as specified in the TRANSPORT decks ARCN FINAL and ARCS FINAL of June 5, 1985. The formal name consists of three fields: the primary name, the zone and the unit number. The general principles and guidelines are explained in Reference 1. The rationale and the final resolutions of the naming conventions for the Arc are explained.

  14. Beryllium window for an APS diagnostics beamline

    SciTech Connect

    Sheng, I.C.; Yang, B.X.; Sharma, Y.S.

    1997-09-01

    A beryllium (Be) window for an Advanced Photon Source (APS) diagnostics beamline has been designed and built. The window, which has a double concave axisymmetrical profile with a thickness of 0.5 mm at the center, receives 160 W/mm{sup 2} (7 GeV/100 mA stored beam) from an undulator beam. The window design as well as thermal and thermomechanical analyses, including thermal buckling of the Be window, are presented.

  15. Shielding Calculations for NSLS-II Beamlines.

    SciTech Connect

    Job,P.K.; Casey, W.R.

    2008-04-13

    Brookhaven National Laboratory is in the process of designing a new Electron Synchrotron for scientific research using synchrotron radiation. This facility, called the 'National Synchrotron Light Source II' (NSLS-II), will provide x-ray radiation of ultra-high brightness and exceptional spatial and energy resolution. It will also provide advanced insertion devices, optics, detectors, and robotics, and a suite of scientific instruments designed to maximize the scientific output of the facility. The project scope includes the design, construction, installation, and commissioning of the following accelerators: a 200 MeV linac, a booster accelerator operating from 200 MeV to 3.0 GeV, the storage ring which stores 500 mA current of electrons at an energy of 3.0 GeV and 56 beamlines for experiments. It is planned to operate the facility primarily in a top-off mode, thereby maintaining the maximum variation in stored beam current to < 1%. Because of the very demanding requirements for beam emittance and synchrotron radiation brilliance, the beam life-time is expected to be quite low, on the order of 2 hours. Each of the 56 beamlines will be unique in terms of the source properties and configuration. The shielding designs for five representative beamlines are discussed in this paper.

  16. LUCIA, a microfocus soft XAS beamline

    NASA Astrophysics Data System (ADS)

    Flank, A.-M.; Cauchon, G.; Lagarde, P.; Bac, S.; Janousch, M.; Wetter, R.; Dubuisson, J.-M.; Idir, M.; Langlois, F.; Moreno, T.; Vantelon, D.

    2006-05-01

    The beamline "LUCIA" (line for ultimate characterization by imaging and absorption) is a "tender" (0.8-8 keV) X-ray microprobe with capabilities for chemical speciation by micro-X-ray absorption spectroscopy (μ-XAS) and for elemental mapping by X-ray micro-fluorescence (μ-XRF). It allows the possibility to study heterogeneous samples at a micrometer scale and to combine these two element-specific and non-destructive techniques. A monochromatic beam of a few micrometer in size is incident on a sample which is mounted on a scanning x-y-z stage. μ-XRF shows the location of the elements, their relative abundances, and their association with other elements. One can take advantage of the monochromatic beam which allows separating out different elements by their absorption edges. After mapping the fluorescence, spots of interest can be analysed by XAS to determine the speciation (local chemistry, quantitative determination of the local geometric structure around the absorbing atom) of the elements and how they depend on the different components. Installed at first at the SLS of the Paul Scherrer Institute (Switzerland), the LUCIA beamline will be transferred to SOLEIL by the beginning of 2008. The energy range offered by the beamline corresponds to the best performances of SLS and SOLEIL in terms of brightness. It allows XAS experiments at the K edge of elements ranging from Na to Fe, L edges from Ni to Gd, and M edges of rare earths and actinides.

  17. Macromolecular crystallography beamline X25 at the NSLS

    PubMed Central

    Héroux, Annie; Allaire, Marc; Buono, Richard; Cowan, Matthew L.; Dvorak, Joseph; Flaks, Leon; LaMarra, Steven; Myers, Stuart F.; Orville, Allen M.; Robinson, Howard H.; Roessler, Christian G.; Schneider, Dieter K.; Shea-McCarthy, Grace; Skinner, John M.; Skinner, Michael; Soares, Alexei S.; Sweet, Robert M.; Berman, Lonny E.

    2014-01-01

    Beamline X25 at the NSLS is one of the five beamlines dedicated to macromolecular crystallography operated by the Brookhaven National Laboratory Macromolecular Crystallography Research Resource group. This mini-gap insertion-device beamline has seen constant upgrades for the last seven years in order to achieve mini-beam capability down to 20 µm × 20 µm. All major components beginning with the radiation source, and continuing along the beamline and its experimental hutch, have changed to produce a state-of-the-art facility for the scientific community. PMID:24763654

  18. Macromolecular crystallography beamline X25 at the NSLS.

    PubMed

    Héroux, Annie; Allaire, Marc; Buono, Richard; Cowan, Matthew L; Dvorak, Joseph; Flaks, Leon; Lamarra, Steven; Myers, Stuart F; Orville, Allen M; Robinson, Howard H; Roessler, Christian G; Schneider, Dieter K; Shea-McCarthy, Grace; Skinner, John M; Skinner, Michael; Soares, Alexei S; Sweet, Robert M; Berman, Lonny E

    2014-05-01

    Beamline X25 at the NSLS is one of the five beamlines dedicated to macromolecular crystallography operated by the Brookhaven National Laboratory Macromolecular Crystallography Research Resource group. This mini-gap insertion-device beamline has seen constant upgrades for the last seven years in order to achieve mini-beam capability down to 20 µm × 20 µm. All major components beginning with the radiation source, and continuing along the beamline and its experimental hutch, have changed to produce a state-of-the-art facility for the scientific community.

  19. Design of Beamline BL9 at Saga Light Source

    SciTech Connect

    Tanaka, Tooru; Ogawa, Hiroshi; Kamada, Masao; Nishio, Mitsuhiro; Guo, Qixin; Masuda, Masataka; Motooka, Teruaki; Kondo, Yuzi; Hayashida, Kazuki; Yoshimura, Daisuke; Setoyama, Hiroyuki; Okajima, Toshihiro

    2007-01-19

    Saga Light Source (SAGA-LS), which has been constructed at Tosu city in Saga prefecture, is a compact synchrotron light source with storage electron energy of 1.4 GeV. A new beamline for the development of advanced materials and processing has been designed, and is now under construction at BL9 of SAGA-LS. This beamline is one of the three bending magnet beamlines (BL9, BL12, and BL15) constructed by Saga Prefectural Government. In this paper, we describe the design and the expected optical performance of the beamline BL9 at SAGA-LS.

  20. SASE3: soft x-ray beamline at European XFEL

    NASA Astrophysics Data System (ADS)

    La Civita, Daniele; Gerasimova, Natalia; Sinn, Harald; Vannoni, Maurizio

    2014-09-01

    The European XFEL in Hamburg will be comprised of a linear accelerator and three Free-Electron-Laser beamlines (SASE1, SASE2 and SASE3) covering the energy range from 250 eV to 24 keV. It will provide up to 2700 pulses in trains of 600 microsecond duration at a repetition rate of 10 Hz. SASE3 beamline is the soft X-ray beamline (0.25 - 3 keV) and delivers photon pulses to SQS (Small Quantum System) and SCS (Spectroscopy & Coherent Scattering) experiments. The beamline is able to operate in both monochromatic and non-monochromatic mode. The latter provides the inherent FEL bandwidth at higher intensities. The beamline from photon source to experimental station is about 450 m long. The length of the beamline is related to the optics single-shotdamage issue. The almost diffraction-limited beam is propagated along the beamline with very long (up to 800 mm clear aperture), cooled (with eutectic bath) and super-polished (50 nrad RMS slope error and less than 3 nm PV residual height error) mirrors. The VLS-PG (variable line spacing - plane grating) monochromator covers the entire beamline energy range and its optical design is guided by the optimization of the energy resolving power, the minimization of the pulse broadening and the maximization of optics damage tolerance. Grating substrates are 530 mm long, eutectic cooled and present outstanding surface quality. The VLS parameters of the blazed profile are also a real challenge under manufacturing and measuring point of view. Adaptive optics in the horizontal (the second offset mirror) and vertical (monochromator premirror) plane are foreseen in the optical layout to increase the beamline tunability and to preserve the highly coherent beam properties. Beamline optical design, expected performance and also mechanical aspects of main beamline components are reported.

  1. APS beamline standard components handbook. Version 1.1

    SciTech Connect

    Kuzay, T.M.

    1992-01-01

    It is clear that most Advanced Photon Source (APS) Collaborative Access Team (CAT) members would like to concentrate on designing specialized equipment related to their scientific programs rather than on routine or standard beamline components. Thus, an effort is in progress at the APS to identify standard and modular components of APS beamlines. Identifying standard components is a nontrivial task because these components should support diverse beamline objectives. To assist with this effort, the APS has obtained advice and help from a Beamline Standardization and Modularization Committee consisting of experts in beamline design, construction, and operation. The staff of the Experimental Facilities Division identified various components thought to be standard items for beamlines, regardless of the specific scientific objective of a particular beamline. A generic beamline layout formed the basis for this identification. This layout is based on a double-crystal monochromator as the first optical element, with the possibility of other elements to follow. Pre-engineering designs were then made of the identified standard components. The Beamline Standardization and Modularization Committee has reviewed these designs and provided very useful input regarding the specifications of these components. We realize that there will be other configurations that may require special or modified components. This Handbook in its current version (1.1) contains descriptions, specifications, and pre-engineering design drawings of these standard components. In the future, the APS plans to add engineering drawings of identified standard beamline components. Use of standard components should result in major cost reductions for CATs in the areas of beamline design and construction.

  2. Functional description of APS beamline front ends

    SciTech Connect

    Kuzay, T.

    1993-02-01

    Traditional synchrotron sources were designed to produce bending magnet radiation and have proven to be an essential scientific tool. Currently, a new generation of synchrotron sources is being built that will be able to accommodate a large number of insertion device (ID) and high quality bending magnet (BM) sources. One example is the 7-GeV Advanced Photon Source (APS) now under construction at Argonne National Laboratory. The research and development effort at the APS is designed to fully develop the potential of this new generation of synchrotron sources. Of the 40 straight sections in the APS storage ring, 34 will be available for IDs. The remaining six sections are reserved for the storage ring hardware and diagnostics. Although the ring incorporates 80 BMs, only 40 of them can be used to extract radiation. The accelerator hardware shadows five of these 40 bending magnets, so the maximum number of BM sources on the lattice is 35. Generally, a photon beamline consists of four functional sections. The first section is the ID or the BM, which provides the radiation source. The second section, which is immediately outside the storage ring but inside a concrete shielding tunnel, is the front end, which is designed to control, define, and/or confine the x-ray beam. In the case of the APS, the front ends are designed to confine the photon beam. The third section, just outside the concrete shielding tunnel and on the experimental floor, is the first optics enclosure, which contains optics to filter and monochromatize the photon beam. The fourth section of a beamline consists of beam transports, additional optics, and experiment stations to do the scientific investigations. This document describes only the front ends of the APS beamlines.

  3. Recent results from the JADE collaboration at PETRA on e+e- annihilation to multihadrons

    SciTech Connect

    O'Neill, L.H. Jr.

    1981-01-01

    A search for production of a new quark flavor in multihadronic states from e+e- annihilation has been made up to an energy of 35.8 GeV in the center of mass. No evidence is seen for such production. A new statistical analysis by the JADE collaboration of the combined data of four PETRA experiments from a fine energy scan in the region 29.90 to 31.46 GeV in the center of mass sets new upper limits on the integrated cross section for a bound state consisting of a new flavor quark and antiquark. The ability of the JADE detector to measure dE/dx provides new upper bounds on the production of fractionally charged particles such as free quarks, or of heavy, integrally charged states such as long-lived B mesons. Finally the fractions of the final state energy carried by gamma rays and by neutral particles of all kinds are measured at center of mass energies from 12 to 35 GeV. The gamma ray and neutral energy fractions are approximately 26% and 38% respectively, while the fractional energy carried by neutrinos is less than 15%.

  4. Principal Components of Thermography analyses of the Silk Tomb, Petra (Jordan)

    NASA Astrophysics Data System (ADS)

    Gomez-Heras, Miguel; Alvarez de Buergo, Monica; Fort, Rafael

    2015-04-01

    This communication presents the results of an active thermography survey of the Silk Tomb, which belongs to the Royal Tombs compound in the archaeological city of Petra in Jordan. The Silk Tomb is carved in the variegated Palaeozoic Umm Ishrin sandstone and it is heavily backweathered due to surface runoff from the top of the cliff where it is carved. Moreover, the name "Silk Tomb" was given because of the colourful display of the variegated sandstone due to backweathering. A series of infrared images were taken as the façade was heated by sunlight to perform a Principal Component of Thermography analyses with IR view 1.7.5 software. This was related to indirect moisture measurements (percentage of Wood Moisture Equivalent) taken across the façade, by means of a Protimeter portable moisture meter. Results show how moisture retention is deeply controlled by lithological differences across the façade. Research funded by Geomateriales 2 S2013/MIT-2914 and CEI Moncloa (UPM, UCM, CSIC) through a PICATA contract and the equipment from RedLAbPAt Network

  5. Chemical and Mineralogical study of Nabataean painted pottery from Petra, Jordan.

    NASA Astrophysics Data System (ADS)

    Alawneh, Firas; Bala'awi, Fadi

    Nabataean pottery is distinguished by the thinness of its walls, which were sometimes only 1.5 mm thick. It was a pinkish/red color, often decorated by hand with dark brown flower and leaf designs. The typical (egg-shell) shallow open bowls productions were very difficult to make on the potter's wheel, demonstrating how skilled their craftsmen were Nabataean painted pottery from Petra Jordan were examined in order to determine the mineralogical characteristics of the raw pigment materials used for their production and to elucidate the ceramic manufacturing technologies employed. Optical microscopy, X-ray diffraction analysis (XRD) and scanning electron microscopy (SEM-EDS) were the analytical techniques used. The initial examination of the ceramic shreds in optical microscopy showed all samples to be identical in their paint and paste textures. The mineralogical composition of the paste (unpainted outer surface) is typical of a clay poor in calcium and fired at moderate-high temperature in an oxidizing atmosphere. The paste is composed of quartz, plagioclase, potassium feldspar, hematite, dolomite, and calcite. The latter two phases might be attributed to post-depositional contamination, since examination with both optical and scanning electron microscopes show fine carbonate particles deposited in the pores and cracks of the shred. The paint on the inner surface of the vessel, on the other hand is composed of hematite as a major phase with only some quartz and plagioclase.

  6. A Look at the AP2 Beamline

    SciTech Connect

    Gollwitzer, Keith; /Fermilab

    2001-01-08

    Some recent work has been done to look at improvements of transporting beam from the Lithium Lens to the Debuncher. This work has been done using the beamline modeling tools developed by Dave McGinnis. These tools, console application P143 and optimization code running MAD repeatedly on the Beam Physics UNIX system, were first used to match the Twiss and dispersion parameters at the end of AP2 to the Debuncher. Imaginary trims were then added to AP2 to study where additional trims could be used to help with beam control in small aperture areas.

  7. Applications of bent cylindrical mirrors to x-ray beamlines

    SciTech Connect

    Heald, S.M.

    1981-07-01

    Bent cylindrical mirrors are considered as substitutes for paraboloidal and ellipsoidal mirrors in x-ray beamlines. Analytic and raytracing studies are used to compare their optical performance with the corresponding ideal elements. Particular emphasis is placed on obtaining the practical limitations in the application of bent cylinders to typical beamline configurations.

  8. G4beamline Particle Tracking in Matter Dominated Beam Lines

    SciTech Connect

    T.J. Roberts, K.B. Beard, S. Ahmed, D. Huang, D.M. Kaplan

    2011-03-01

    The G4beamline program is a useful and steadily improving tool to quickly and easily model beam lines and experimental equipment without user programming. It has both graphical and command-line user interfaces. Unlike most accelerator physics codes, it easily handles a wide range of materials and fields, being particularly well suited for the study of muon and neutrino facilities. As it is based on the Geant4 toolkit, G4beamline includes most of what is known about the interactions of particles with matter. We are continuing the development of G4beamline to facilitate its use by a larger set of beam line and accelerator developers. A major new feature is the calculation of space-charge effects. G4beamline is open source and freely available at http://g4beamline.muonsinc.com

  9. Beam characterization at the KAERI UED beamline

    NASA Astrophysics Data System (ADS)

    Setiniyaz, Sadiq; Kim, Hyun Woo; Baek, In-Hyung; Nam, Jinhee; Chae, MoonSik; Han, Byung-Heon; Gudkov, Boris; Jang, Kyu Ha; Park, Sunjeong; Jeong, Young Uk; Miginsky, Sergey; Vinokurov, Nikolay

    2016-09-01

    The UED (ultrafast electron diffraction) beamline of the KAERI's (the Korea Atomic Energy Research Institute's) WCI (World Class Institute) Center has been successfully commissioned. We have measured the beam emittance by using the quadrupole scan technique and the charge by using a novel measurement system we have developed. In the quadrupole scan, a larger drift distance between the quadrupole and the screen is preferred because it gives a better thin-lens approximation. A high bunch-charge beam, however, will undergo emittance growth in the long drift caused by the space-charge force. We present a method that mitigates this growth by introducing a quadrupole scan with a short drift and without using the thin-lens approximation. The quadrupole in this method is treated as a thick lens, and the emittance is extracted by using the thick-lens equations. Apart from being precise, our method can be readily applied without making any change to the beamline and has no need for a big drift space. For charge measurement, we have developed a system consisting of an in-air Faraday cup (FC) and a preamplifier. Tests performed utilizing 3.3-MeV electrons show that the system was able to measure bunches with pulse durations of tens of femtoseconds at 10 fC sensitivity.

  10. Diagnostics Beamline for the SRF Gun Project

    SciTech Connect

    T. Kamps; V. Durr; K. Goldammer; D. Kramer; P. Kuske; J. Kuszynski; D. Lipka; F. Marhauser; T. Quast; D. Richter; U. Lehnert; P. Michel; J. Teichert; P. Evtushenko; I. Will

    2005-08-22

    A superconducting radio-frequency photo electron injector (SRF gun) is currently under construction by a collaboration of BESSY, DESY, FZR and MBI. The project aims at the design and setup of a CW SRF gun including a diagnostics beamline for the ELBE FEL and to address R&D issues on low emittance injectors for future light sources such as the BESSY FEL. Of critical importance for the injector performance is the control of the electron beam parameters. For this reason a compact diagnostics beamline is under development serving a multitude of operation settings ranging from low-charge (77pC), low-emittance (1 mm mrad) mode to high-charge (2.5nC) operation of the gun. For these operation modes beam dynamics simulations are resulting in boundary conditions for the beam instrumentation. Proven and mature technology is projected wherever possible, for example for current and beam position monitoring. The layout of the beam profile and emittance measurement systems is described. For the bunch length, which varies between 5 ps and 50 ps, two schemes using electro-optical sampling and Cherenkov radiation are detailed. The beam energy and energy spread is measured with a 180-degree spectrometer.

  11. Neutral beamline with improved ion energy recovery

    DOEpatents

    Kim, Jinchoon

    1984-01-01

    A neutral beamline employing direct energy recovery of unneutralized residual ions is provided which enhances the energy recovery of the full energy ion component of the beam exiting the neutralizer cell, and thus improves the overall neutral beamline efficiency. The unneutralized full energy ions exiting the neutralizer are deflected from the beam path and the electrons in the cell are blocked by a magnetic field applied transverse to the beam direction in the neutral izer exit region. The ions which are generated at essentially ground potential and accelerated through the neutralizer cell by a negative acceleration voltage are collected at ground potential. A neutralizer cell exit end region is provided which allows the magnetic and electric fields acting on the exiting ions to be loosely coupled. As a result, the fractional energy ions exiting the cell are reflected onto and collected at an interior wall of the neutralizer formed by the modified end geometry, and thus do not detract from the energy recovery efficiency of full energy ions exiting the cell. Electrons within the neutralizer are prevented from exiting the neutralizer end opening by the action of crossed fields drift (ExB) and are terminated to a collector collar around the downstream opening of the neutralizer. The correct combination of the extended neutralizer end structure and the magnet region is designed so as to maximize the exit of full energy ions and to contain the fractional energy ions.

  12. The mammography project at the SYRMEP beamline.

    PubMed

    Dreossi, D; Abrami, A; Arfelli, F; Bregant, P; Casarin, K; Chenda, V; Cova, M A; Longo, R; Menk, R-H; Quai, E; Quaia, E; Rigon, L; Rokvic, T; Sanabor, D; Tonutti, M; Tromba, G; Vascotto, A; Zanconati, F; Castelli, E

    2008-12-01

    A clinical program for X-ray phase contrast (PhC) mammography with synchrotron radiation (SR) has been started in March 2006 at the SYRMEP beamline of Elettra, the SR facility in Trieste, Italy. The original beamline layout has been modified substantially and a clinical facility has been realized. In order to fulfill all security requirements, dedicated systems have been designed and implemented, following redundancy criteria and "fail safe" philosophy. Planar radiographic images are obtained by scanning simultaneously the patient and the detector through the stationary and laminar SR beam. In this first phase of the project a commercial screen-film system has been used as image receptor. Upon approval by the respective authorities, the mammography program is about half way to conclusion. Up to now about 50 patients have been examined. The patients are volunteers recruited by the radiologist after conventional examinations at the hospital resulted in an uncertain diagnosis. As an example one case of PhC SR mammography is shown and compared to conventional digital mammography. Preliminary analysis shows the high diagnostic quality of the PhC SR images that were acquired with equal or less delivered dose compared to the conventional ones. PMID:18617344

  13. Diagnostics for the LCLS Photoinjector Beamline

    SciTech Connect

    Limborg-Deprey, C.; Dowell, D.; Schmerge, J.F.; /SLAC

    2006-03-17

    Two spectrometers have been added to the LCLS photoinjector beamline. The first one will be located close to the exit of the Photoinjector RF gun. With this diagnostic, we will measure beam energy, energy spread (correlated and uncorrelated), possibly deleterious structure in the longitudinal phase space induced by longitudinal space charge force, and slice thermal emittance ... This extensive characterization of the 5MeV electron bunch will be made possible by combining this spectrometer with other diagnostics (YAG screens and Cerenkov Radiator). A second spectrometer located at the end of the beamline has been designed to characterize the 6 dimensional phase space of the 135MeV beam to be injected in the main accelerator. At that second spectrometer station, we will measure energy, energy spread (correlated and uncorrelated), longitudinal phase space, slice emittances ... Those last two measurements require using this spectrometer in combination with the transverse RF deflecting cavity and with the quadrupole scan emittance station. The designs of these two spectrometers have been supported by simulations from MAD and PARMELA.

  14. A heat transfer study for beamline components in high-power wiggler and undulator beamlines. Part I. Beam stops

    SciTech Connect

    Bedzyk, M. J.; Keeffe, M. J.; Schildkamp, W.; Shen, Q.

    1989-07-01

    The heat transfer capabilities of beam stops in CHESS wiggler and undulator beamlines is described. The thermal analysis for the design of these crucial in-vacuum beamline components is based on the use of a finite element analysis computer calculation and experimental heat loading tests.

  15. A new compact soft x-ray spectrometer for resonant inelastic x-ray scattering studies at PETRA III

    SciTech Connect

    Yin, Z. E-mail: simone.techert@desy.de; Peters, H. B.; Hahn, U.; Viefhaus, J.; Agåker, M.; Nordgren, J.; Hage, A.; Reininger, R.; Siewert, F.; Techert, S. E-mail: simone.techert@desy.de

    2015-09-15

    We present a newly designed compact grating spectrometer for the energy range from 210 eV to 1250 eV, which would include the Kα{sub 1,2} emission lines of vital elements like C, N, and O. The spectrometer is based on a grazing incidence spherical varied line spacing grating with 2400 l/mm at its center and a radius of curvature of 58 542 mm. First, results show a resolving power of around 1000 at an energy of 550 eV and a working spectrometer for high vacuum (10{sup −4} mbar) environment without losing photon intensity.

  16. Protecting Unesco World Heritage PROPERTIES'S Integrity: the Role of Recording and Documentation in Risk Management for PETRA

    NASA Astrophysics Data System (ADS)

    Santana Quintero, M.; Cesaro, G.; Ishakat, F.; Vandesande, A.; Vileikis, O.; Vadafari, A.; Paolini, A.; Van Balen, K.; Fakhoury, L.

    2012-07-01

    Risk management - as it has been defined - involves the decision-making process following a risk assessment (Ball, Watt, 2003). It is the process that involves managing to minimize losses and impacts on the significant of historic structures and to reach the balance between gaining and losing opportunities. This contribution explains the "heritage information" platform developed using low-cost recording, documentation and information management tools to serve as container for assessments resulting from the application of a risk methodology at a pilot area of the Petra Archaeological Park, in particular those that permit digitally and cost effective to prepare an adequate baseline record to identify disturbances and threats. Furthermore, this paper will reflect on the issue of mapping the World Heritage property's boundaries by illustrating a methodology developed during the project and further research to overcome the lack of boundaries and buffer zone for the protection of the Petra World Heritage site, as identified in this project. This paper is based on on-going field project from a multidisciplinary team of experts from the Raymond Lemaire International Centre for Conservation (University of Leuven), UNESCO Amman, Petra Development Tourism and Region Authority (PDTRA), and Jordan's Department of Antiquities (DoA), as well as, experts from Jordan. The recording and documentation approach included in this contribution is part of an on-going effort to develop a methodology for mitigating (active and preventive) risks on the Petra Archaeological Park (Jordan). The risk assessment has been performed using non-intrusive techniques, which involve simple global navigation satellite system (GNSS), photography, and structured visual inspection, as well as, a heritage information framework based on Geographic Information Systems. The approach takes into consideration the comparison of vulnerability to sites with the value assessment to prioritize monuments at risk based

  17. Possibility of observing color-symmetry violation in the two-photon experiments of PLUTO at PETRA

    SciTech Connect

    Efremov, A.; Ivanov, S.

    1982-01-01

    The two-photon processes being studied by the PLUTO group at PETRA are discussed from the point of view of study of color symmetry. The reaction which is cleanest theoretically is the annihilation of two photons into two hadron jets with large transverse momentum. The PLUTO results for this process are compared with calculations using QCD and the calculations in the model of electrostrong interactions with violation of color symmetry. It is not clear whether the departure of the experimental results from QCD is due to an important role of higher twists or to the violation of color symmetry. (AIP)

  18. Damage Assessment and Digital 2D-3D Documentation of PetraTreasury

    NASA Astrophysics Data System (ADS)

    Bala'awi, Fadi; Alshawabkeh, Yahya; Alawneh, Firas; Masri, Eyed al

    The treasury is the icon monument of the world heritage site of ancient Petra city. Unfortunately, this important part of the world's cultural heritage is gradually being diminished due to weathering and erosion problems. This give rise to the need to have a comprehensive study and full documentation of the monument in order to evaluate its status. In this research a comprehensive approach utilizing 2D-3D documentation of the structure using laser scanner and photogrammetry is carried parallel with a laboratory analysis and a correlation study of the salt content and the surface weathering forms. In addition, the research extends to evaluate a set of chemical and physical properties of the case study monument. Studies of stone texture and spatial distribution of soluble salts were carried out at the monument in order to explain the mechanism of the weathering problem. Then a series of field work investigations and laboratory work were undertaken to study the effect of relative humidity, temperature, and wind are the main factors in the salt damage process. The 3D modelling provides accurate geometric and radiometric properties of the damage shape. In order to support the visual quality of 3D surface details and cracks, a hybrid approach combining data from the laser scanner and the digital imagery was developed. Based on the findings, salt damage appears to be one of the main problems at this monument. Although, the total soluble salt content are quite low, but the salts contamination is all over the tested samples in all seasons, with higher concentrations at deep intervals. The thermodynamic calculations carried out by this research have also shown that salt damage could be minimised by controlling the surrounding relative humidity conditions. This measure is undoubtedly the most challenging of all, and its application, if deemed feasible, should be carried out in parallel with other conservation measures.

  19. Innovations in the design of mechanical components for a beamline{emdash}The SRI{close_quote}95 Workshop 2 Summary

    SciTech Connect

    Kuzay, T.; Warwick, T. |

    1996-09-01

    The Synchrotron Radiation Instrumentation 1995 Conference (SRI{close_quote}95) was hosted by the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). Of the many workshops within the conference, the SRI{close_quote}95 Workshop 2 was {open_quote}{open_quote}Innovations in the Design of Mechanical Components of a Beamline.{close_quote}{close_quote} The workshop was well attended with over 140 registrants. The following topics were discussed. Industry{close_quote}s perspective on the status and future was provided by Huber Diffraktionstechnik GMBH on goniometers/diffractometers, Oxford Instruments on advanced manufacturing technique of high heat load components, such as the APS photon shutter, and Kohzu Seiki Co. Ltd. on the specialties of monochromators provided to the third-generation synchrotrons. This was followed by a description of the engineering of a dual function monochromator design for water-cooled diamond or cryogenically cooled silicon monochromators by CMC CAT/APS. Another category was the nagging problem of sensitivity of the photon beam position monitors (XBPM) to bending magnet radiation ({open_quote}{open_quote}BM contamination{close_quote}{close_quote}) and the undulator magnet gap changes. Problem descriptions and suggested solutions were provided by both the Advanced Light Source (ALS) and the APS. Other innovative ideas were the cooling schemes (enhanced cooling of beamline components using metallic porous meshes including cryo-cooled applications); Glidcop photon shutter design using microchannels at the ALS; and window/filter design, manufacture and operational experiences at CHESS and PETRA/HASYLAB. Additional discussions were held on designing for micromotions and precision in the optical support systems and smart user filter schemes. This is a summary of the presentations at the Workshop. {copyright} {ital 1996 American Institute of Physics.}

  20. Commissioning of a microprobe-XRF beamline (BL-16) on Indus-2 synchrotron source

    NASA Astrophysics Data System (ADS)

    Tiwari, M. K.; Gupta, P.; Sinha, A. K.; Garg, C. K.; Singh, A. K.; Kane, S. R.; Garg, S. R.; Lodha, G. S.

    2012-06-01

    We report commissioning of the microprobe-XRF beamline on Indus-2 synchrotron source. The beamline has been recently made operational and is now open for the user's experiments. The beamline comprises of Si(111) double crystal monochromator and Kirkpatrick-Baez focusing optics. The beamline covers wide photon energy range of 4 - 20 keV using both collimated and micro-focused beam modes. The design details and the first commissioning results obtained using this beamline are presented.

  1. Commissioning of a microprobe-XRF beamline (BL-16) on Indus-2 synchrotron source

    SciTech Connect

    Tiwari, M. K.; Gupta, P.; Sinha, A. K.; Garg, C. K.; Singh, A. K.; Kane, S. R.; Garg, S. R.; Lodha, G. S.

    2012-06-05

    We report commissioning of the microprobe-XRF beamline on Indus-2 synchrotron source. The beamline has been recently made operational and is now open for the user's experiments. The beamline comprises of Si(111) double crystal monochromator and Kirkpatrick-Baez focusing optics. The beamline covers wide photon energy range of 4 - 20 keV using both collimated and micro-focused beam modes. The design details and the first commissioning results obtained using this beamline are presented.

  2. Moly99 Production Facility: Report on Beamline Components, Requirements, Costs

    SciTech Connect

    Bishofberger, Kip A.

    2015-12-23

    In FY14 we completed the design of the beam line for the linear accelerator production design concept. This design included a set of three bending magnets, quadrupole focusing magnets, and octopoles to flatten the beam on target. This design was generic and applicable to multiple different accelerators if necessary. In FY15 we built on that work to create specifications for the individual beam optic elements, including power supply requirements. This report captures the specification of beam line components with initial cost estimates for the NorthStar production facility.This report is organized as follows: The motivation of the beamline design is introduced briefly, along with renderings of the design. After that, a specific list is provided, which accounts for each beamline component, including part numbers and costs, to construct the beamline. After that, this report details the important sections of the beamline and individual components. A final summary and list of follow-on activities completes this report.

  3. Optical pseudomotors for soft x-ray beamlines.

    PubMed

    Pedreira, P; Sics, I; Sorrentino, A; Pereiro, E; Aballe, L; Foerster, M; Pérez-Dieste, V; Escudero, C; Nicolas, J

    2016-05-01

    Optical elements of soft x-ray beamlines usually have motorized translations and rotations that allow for the fine alignment of the beamline. This is to steer the photon beam at some positions and to correct the focus on slits or on sample. Generally, each degree of freedom of a mirror induces a change of several parameters of the beam. Inversely, several motions are required to actuate on a single optical parameter, keeping the others unchanged. We define optical pseudomotors as combinations of physical motions of the optical elements of a beamline, which allow modifying one optical parameter without affecting the others. We describe a method to obtain analytic relationships between physical motions of mirrors and the corresponding variations of the beam parameters. This method has been implemented and tested at two beamlines at ALBA, where it is used to control the focus of the photon beam and its position independently.

  4. A hard X-ray nanoprobe beamline for nanoscale microscopy

    PubMed Central

    Winarski, Robert P.; Holt, Martin V.; Rose, Volker; Fuesz, Peter; Carbaugh, Dean; Benson, Christa; Shu, Deming; Kline, David; Stephenson, G. Brian; McNulty, Ian; Maser, Jörg

    2012-01-01

    The Hard X-ray Nanoprobe Beamline (or Nanoprobe Beamline) is an X-ray microscopy facility incorporating diffraction, fluorescence and full-field imaging capabilities designed and operated by the Center for Nanoscale Materials and the Advanced Photon Source at Sector 26 of the Advanced Photon Source at Argonne National Laboratory. This facility was constructed to probe the nanoscale structure of biological, environmental and material sciences samples. The beamline provides intense focused X-rays to the Hard X-ray Nanoprobe (or Nanoprobe) which incorporates Fresnel zone plate optics and a precision laser sensing and control system. The beamline operates over X-ray energies from 3 to 30 keV, enabling studies of most elements in the periodic table, with a particular emphasis on imaging transition metals. PMID:23093770

  5. Transport from the Recycler Ring to the Antiproton Source Beamlines

    SciTech Connect

    Xiao, M.; /Fermilab

    2012-05-14

    In the post-NOvA era, the protons are directly transported from the Booster ring to the Recycler ring rather than the Main Injector. For Mu2e and g-2 project, the Debuncher ring will be modified into a Delivery ring to deliver the protons to both Mu2e and g-2 experiments. Therefore, it requires the transport of protons from the Recycler Ring to the Delivery ring. A new transfer line from the Recycler ring to the P1 beamline will be constructed to transport proton beam from the Recycler Ring to existing Antiproton Source beamlines. This new beamline provides a way to deliver 8 GeV kinetic energy protons from the Booster to the Delivery ring, via the Recycler, using existing beam transport lines, and without the need for new civil construction. This paper presents the Conceptual Design of this new beamline.

  6. ALS beamlines for independent investigators: A summary of the capabilities and characteristics of beamlines at the ALS

    SciTech Connect

    Not Available

    1992-08-01

    There are two mods of conducting research at the ALS: To work as a member of a participating research team (PRT). To work as a member of a participating research team (PRT); to work as an independent investigator; PRTs are responsible for building beamlines, end stations, and, in some cases, insertion devices. Thus, PRT members have privileged access to the ALS. Independent investigators will use beamline facilities made available by PRTs. The purpose of this handbook is to describe these facilities.

  7. Beamline Insertions Manager at Jefferson Lab

    SciTech Connect

    Johnson, Michael C.

    2015-09-01

    The beam viewer system at Jefferson Lab provides operators and beam physicists with qualitative and quantitative information on the transverse electron beam properties. There are over 140 beam viewers installed on the 12 GeV CEBAF accelerator. This paper describes an upgrade consisting of replacing the EPICS-based system tasked with managing all viewers with a mixed system utilizing EPICS and high-level software. Most devices, particularly the beam viewers, cannot be safely inserted into the beam line during high-current beam operations. Software is partly responsible for protecting the machine from untimely insertions. The multiplicity of beam-blocking and beam-vulnerable devices motivates us to try a data-driven approach. The beamline insertions application components are centrally managed and configured through an object-oriented software framework created for this purpose. A rules-based engine tracks the configuration and status of every device, along with the beam status of the machine segment containing the device. The application uses this information to decide on which device actions are allowed at any given time.

  8. Status of the LBNE Neutrino Beamline

    SciTech Connect

    Papadimitriou, Vaia; /Fermilab

    2011-12-01

    The Long Baseline Neutrino Experiment (LBNE) will utilize a neutrino beamline facility located at Fermilab to carry out a compelling research program in neutrino physics. The facility will aim a beam of neutrinos toward a detector placed at the Homestake Mine in South Dakota. The neutrinos are produced in a three-step process. First, protons from the Main Injector (60-120 GeV) hit a solid target and produce mesons. Then, the charged mesons are focused by a set of focusing horns into the decay pipe, towards the far detector. Finally, the mesons that enter the decay pipe decay into neutrinos. The parameters of the facility were determined taking into account several factors including the physics goals, the Monte Carlo modeling of the facility, spacial and radiological constraints and the experience gained by operating the NuMI facility at Fermilab. The initial beam power is expected to be {approx}700 kW, however some of the parameters were chosen to be able to deal with a beam power of 2.3 MW. We discuss here the status of the conceptual design and the associated challenges.

  9. D3, the new diffractometer for the macromolecular crystallography beamlines of the Swiss Light Source

    PubMed Central

    Fuchs, Martin R.; Pradervand, Claude; Thominet, Vincent; Schneider, Roman; Panepucci, Ezequiel; Grunder, Marcel; Gabadinho, Jose; Dworkowski, Florian S. N.; Tomizaki, Takashi; Schneider, Jörg; Mayer, Aline; Curtin, Adrian; Olieric, Vincent; Frommherz, Uli; Kotrle, Goran; Welte, Jörg; Wang, Xinyu; Maag, Stephan; Schulze-Briese, Clemens; Wang, Meitian

    2014-01-01

    A new diffractometer for microcrystallography has been developed for the three macromolecular crystallography beamlines of the Swiss Light Source. Building upon and critically extending previous developments realised for the high-resolution endstations of the two undulator beamlines X06SA and X10SA, as well as the super-bend dipole beamline X06DA, the new diffractometer was designed to the following core design goals. (i) Redesign of the goniometer to a sub-micrometer peak-to-peak cylinder of confusion for the horizontal single axis. Crystal sizes down to at least 5 µm and advanced sample-rastering and scanning modes are supported. In addition, it can accommodate the new multi-axis goniometer PRIGo (Parallel Robotics Inspired Goniometer). (ii) A rapid-change beam-shaping element system with aperture sizes down to a minimum of 10 µm for microcrystallography measurements. (iii) Integration of the on-axis microspectrophotometer MS3 for microscopic sample imaging with 1 µm image resolution. Its multi-mode optical spectroscopy module is always online and supports in situ UV/Vis absorption, fluorescence and Raman spectroscopy. (iv) High stability of the sample environment by a mineral cast support construction and by close containment of the cryo-stream. Further features are the support for in situ crystallization plate screening and a minimal achievable detector distance of 120 mm for the Pilatus 6M, 2M and the macromolecular crystallography group’s planned future area detector Eiger 16M. PMID:24562555

  10. An approach to better understanding of salt weathering on stone monuments - the "petraSalt" research project

    NASA Astrophysics Data System (ADS)

    Heinrichs, K.; Azzam, R.

    2012-04-01

    Salt weathering is known as a major cause of damage on stone monuments. However, processes and mechanisms of salt weathering still can not be explained satisfactorily. From the expertś point of view, better understanding of salt weathering deserves further comprehensive in-situ investigation jointly addressing active salt weathering processes and controlling factors. The 'petraSalt' research project takes this approach. The rock-cut monuments of Petra / Jordan were selected for studies, since stone type and spectra of monument exposure regimes, environmental influences, salt loading and weathering damage are representative for many stone monuments worldwide. The project aims at real-time / real-scale weathering models that depict characteristic interdependencies between stone properties, monument exposure regimes, environmental influences, salt loading and salt weathering damage. These models are expected to allow reliable rating and interpretation of aggressiveness and damage potential of the salt weathering regimes considering their variability under range of lithology, monument exposure scenarios, environmental conditions and time. The methodological approach systematically combines assessment of weathering damage (type, extent, spatial distribution and progression of damage), assessment of monument exposure characteristics and environmental influences acting on the monuments (monument orientation / geometry, lithology, rain impact, water run-off, rising humidity, wind impact, insolation, heating-cooling and drying-wetting behaviour, etc.), engineering geological studies (structural discontinuities and related failure processes) and investigation of salt loading (type, concentration, spatial distribution and origin of salt, salt crystallization / dissolution, phase transitions, etc.). Besides established methods, very innovative technologies are applied in the course of investigation such as high-resolution 3D terrestrial laser scanning (TLS) and wireless

  11. Diamond beamline I07: a beamline for surface and interface diffraction.

    PubMed

    Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

    2016-09-01

    Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8-30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid-liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying. PMID:27577783

  12. Diamond beamline I07: a beamline for surface and interface diffraction.

    PubMed

    Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

    2016-09-01

    Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8-30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid-liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying.

  13. Diamond beamline I07: a beamline for surface and interface diffraction

    PubMed Central

    Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam

    2016-01-01

    Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8–30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing-incidence techniques including surface X-ray diffraction, grazing-incidence small- (and wide-) angle X-ray scattering, X-ray reflectivity and grazing-incidence X-ray diffraction. A method for deflecting the X-rays (a double-crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid–liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh-vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low-energy electron diffraction and X-ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X-ray diffraction from nanoparticles during alloying. PMID:27577783

  14. X-ray Microscopy Beamlines at SSRF--Present Status and Future Plan

    SciTech Connect

    Xu, H.; Yu, X.; Tai, R.

    2011-09-09

    The Shanghai Synchrotron Radiation Facility (SSRF) is a 3.5-GeV third-generation light source. The facility has been open for user experiments since May, 2009. This high-brightness x-ray source is an ideal platform for x-ray microscopy. Presently, SSRF has three beamlines related to x-ray microscopy or imaging, namely the soft x-ray spectromicroscopy beamline (STXM), the hard x-ray microfocusing beamline, and the x-ray imaging beamline. The construction of SSRF phase-II beamlines will be carried out during 2011-2017. Seven additional beamlines for x-ray microscopy or imaging will be built.

  15. Provenance of white marbles from the nabatean sites of Qase Al Bint and colonnaded street baths at Petra, Jordan

    NASA Astrophysics Data System (ADS)

    Abu-Jaber, Nizar; al-Saad, Ziad; Shiyyab, Adnan; Degryse, Patrick

    Intercultural relations and trade are important components of understanding of historical interrelationships between regions and cultures. One of the most interesting objects of trade is stone, because of the expense and difficulty of its transport. Thus, the source of marble used in the Nabatean city of Petra was investigated using established petrological, geochemical and isotopic analyses. Specifically, marble from Qasr al Bint and the Colonnaded Street baths were sampled and investigated. The results of these analyses show that the marbles came from sources in Asia Minora and Greece. The most likely sources of the marble are the quarries of Thasos, Penteli, Prokennesos and Dokimeion. The choice of marble followed the desired utilitarian and aesthetic function of the stone. These results show that active trade in stone was part of the cultural interaction of the period.

  16. Low cost 3D-modelling of a complex archaeological site using aerial photography in the hinterland of Petra, Jordan

    NASA Astrophysics Data System (ADS)

    Emaus, R.; Goossens, R.

    2015-02-01

    Individual archaeological sites can sometimes show a complex morphology. One such site is the Roman quarries located one kilometre northwest of the Roman fortress at Udhruh, in the hinterland of Petra. In archaeology there are various platforms such as balloons, kites and unmanned aerial vehicles (uav's) from which low altitude aerial photographs can be taken that have been proven to work. All with their specific advantages above others in different circumstances. By designing a very distinct setup for the kite and optimizing the workflow accordingly, an effective and steady platform for the camera was created. The Quarries were photographed from the air and the images then provided enough material to accurately create a 3D model of the site.

  17. New Beamlines For Protein Crystallography At The EMBL-Outstation Hamburg

    NASA Astrophysics Data System (ADS)

    Hermes, C.; Gehrmann, T.; Jahn, D.; Ristau, U.; Robrahn, B.; Siambanis, T.

    2004-05-01

    Three new beamlines for Protein Crystallography were built up on a bending magnet fan of the DORIS III storage ring. A 10 mrad wide fan of white Synchrotron Radiation (SR) is evenly distributed among 3 individual stations: X12, a central, wavelength-tunable station intended for anomalous scattering experiments (MAD) and fixed wavelength, high intensity stations symmetrically on either side. The fixed wavelength beamlines X11 & X13 comprise triangular, asymmetrically cut Si (111) monochromators as horizontally focusing optical elements. The tunable station is based on a fixed-exit, horizontally focusing double crystal monochromator system. Vertical focusing is achieved on all three lines by trapezoidal shaped, continuous Rh-coated mirrors which can be dynamically bent. In all three lines the X-ray beam can be examined at various points on its way through the optical system by removable screens and PIN-diode based intensity monitors. Purpose built crystallographic end-stations complete the set-up. The design of individual components and their performance will be described.

  18. A small and robust active beamstop for scattering experiments on high-brilliance undulator beamlines.

    PubMed

    Blanchet, Clement E; Hermes, Christoph; Svergun, Dmitri I; Fiedler, Stefan

    2015-03-01

    A small active in-vacuum beamstop has been developed to monitor the flux of intense third-generation synchrotron X-ray beams protecting the downstream detector from the direct beam. Standard active beamstops, where a built-in diode directly absorbs the beam, have limitations in size and lifetime. In the present design, a silicon PIN diode detects the photons back-scattered from a cavity in the beamstop. This approach drastically reduces the radiation dose on the diode and thus increases its lifetime. The beamstop with a diameter of 2 mm has been fabricated to meet the requirements for the P12 bioSAXS beamline of EMBL Hamburg at PETRA III (DESY). The beamstop is in regular user operation at the beamline and displays a good response over the range of energies tested (6-20 keV). Further miniaturization of the diode is easily possible as its size is not limited by the PIN diode used. PMID:25723949

  19. A small and robust active beamstop for scattering experiments on high-brilliance undulator beamlines

    PubMed Central

    Blanchet, Clement E.; Hermes, Christoph; Svergun, Dmitri I.; Fiedler, Stefan

    2015-01-01

    A small active in-vacuum beamstop has been developed to monitor the flux of intense third-generation synchrotron X-ray beams protecting the downstream detector from the direct beam. Standard active beamstops, where a built-in diode directly absorbs the beam, have limitations in size and lifetime. In the present design, a silicon PIN diode detects the photons back-scattered from a cavity in the beamstop. This approach drastically reduces the radiation dose on the diode and thus increases its lifetime. The beamstop with a diameter of 2 mm has been fabricated to meet the requirements for the P12 bioSAXS beamline of EMBL Hamburg at PETRA III (DESY). The beamstop is in regular user operation at the beamline and displays a good response over the range of energies tested (6–20 keV). Further miniaturization of the diode is easily possible as its size is not limited by the PIN diode used. PMID:25723949

  20. A beamline for macromolecular crystallography at the Advanced Light Source

    SciTech Connect

    Padmore, H.A.; Earnest, T.; Kim, S.H.; Thompson, A.C.; Robinson, A.L.

    1994-08-01

    A beamline for macromolecular crystallography has been designed for the ALS. The source will be a 37-pole wiggler with a, 2-T on-axis peak field. The wiggler will illuminate three beamlines, each accepting 3 mrad of horizontal aperture. The central beamline will primarily be used for multiple-wavelength anomalous dispersion measurements in the wavelength range from 4 to 0.9 {angstrom}. The beamline optics will comprise a double-crystal monochromator with a collimating pre-mirror and a double-focusing mirror after the monochromator. The two side stations will be used for fixed-wavelength experiments within the wavelength range from 1.5 to 0.95 {angstrom}. The optics will consist of a conventional vertically focusing cylindrical mirror followed by an asymmetrically cut curved-crystal monochromator. This paper presents details of the optimization of the wiggler source for crystallography, gives a description of the beamline configuration, and discusses the reasons for the choices made.

  1. 08B1-1: an automated beamline for macromolecular crystallography experiments at the Canadian Light Source.

    PubMed

    Fodje, Michel; Grochulski, Pawel; Janzen, Kathryn; Labiuk, Shaunivan; Gorin, James; Berg, Russ

    2014-05-01

    Beamline 08B1-1 is a recently commissioned bending-magnet beamline at the Canadian Light Source. The beamline is designed for automation and remote access. Together with the undulator-based beamline 08ID-1, they constitute the Canadian Macromolecular Crystallography Facility. This paper describes the design, specifications, hardware and software of beamline 08B1-1. A few scientific results using data obtained at the beamline will be highlighted.

  2. Far-Infrared Beamline at the Canadian Light Source

    NASA Astrophysics Data System (ADS)

    Billinghurst, Brant E.; May, Tim E.

    2014-06-01

    The far-infrared beamline at the Canadian Light Source is a state of the art user facility, which offers significantly more far-infrared brightness than conventional globar sources. The infrared radiation is collected from a bending magnet through a 55 X 37 mrad2 port to a Bruker IFS 125 HR spectrometer, which is equipped with a nine compartment scanning arm, allowing it to achieve spectral resolution better than 0.001 cm-1. Currently the beamline can achieve signal to noise ratios up to 8 times that which can be achieved using a traditional thermal source. This talk will provide an overview of the the beamline, and the capabilities available to users, recent and planned improvements including the addition of a Glow Discharge cell and advances in Coherent Synchrotron Radiation. Furthermore, the process of acquiring access to the facility will be covered.

  3. Status and evolution of the ESRF beamline ID19

    SciTech Connect

    Weitkamp, Timm; Tafforeau, Paul; Boller, Elodie; Cloetens, Peter; Valade, Jean-Paul; Bernard, Pascal; Baruchel, Jose; Peyrin, Francoise; Helfen, Lukas

    2010-04-06

    The ESRF synchrotron beamline ID19, dedicated to full-field parallel-beam imaging techniques such as phase-contrast and absorption microtomography and X-ray topography, is one of the most versatile instruments of its kind. This paper presents key characteristics of ID19 in its present form, names examples for research and development performed on the beamline, and outlines the plans for an upgrade on the beamline in coming years, to adapt to the growing needs of the user community. The technical goals envisioned include an increase in available beam size and maximum photon energy, and a substantial increase in flux density for applications using beams of small and intermediate size.

  4. Status and evolution of the ESRF beamline ID19

    NASA Astrophysics Data System (ADS)

    Weitkamp, Timm; Tafforeau, Paul; Boller, Elodie; Cloetens, Peter; Valade, Jean-Paul; Bernard, Pascal; Peyrin, Françoise; Ludwig, Wolfgang; Helfen, Lukas; Baruchel, José

    2010-04-01

    The ESRF synchrotron beamline ID19, dedicated to full-field parallel-beam imaging techniques such as phase-contrast and absorption microtomography and X-ray topography, is one of the most versatile instruments of its kind. This paper presents key characteristics of ID19 in its present form, names examples for research and development performed on the beamline, and outlines the plans for an upgrade on the beamline in coming years, to adapt to the growing needs of the user community. The technical goals envisioned include an increase in available beam size and maximum photon energy, and a substantial increase in flux density for applications using beams of small and intermediate size.

  5. Distributed control of protein crystallography beamline 5.0 using CORBA

    SciTech Connect

    Timossi, Chris

    1999-09-24

    The Protein Crystallography Beamline at Berkeley Lab's Advanced Light Source is a facility that is being used to solve the structure of proteins. The software that is being used to control this beamline uses Java for user interface applications which communicate via CORBA with workstations that control the beamline hardware. We describe the software architecture for the beamline and our experiences after two years of operation.

  6. APS beamline standard components handbook, Version 1. 3

    SciTech Connect

    Hahn, U.; Shu, D.; Kuzay, T.M.

    1993-02-01

    This Handbook in its current version (1.3) contains descriptions, specifications, and preliminary engineering design drawings for many of the standard components. The design status and schedules have been provided wherever possible. In the near future, the APS plans to update engineering drawings of identified standard beamline components and complete the Handbook. The completed version of this Handbook will become available to both the CATs and potential vendors. Use of standard components should result in major cost reductions for CATs in the areas of beamline design and construction.

  7. The Materials Science beamline upgrade at the Swiss Light Source

    PubMed Central

    Willmott, P. R.; Meister, D.; Leake, S. J.; Lange, M.; Bergamaschi, A.; Böge, M.; Calvi, M.; Cancellieri, C.; Casati, N.; Cervellino, A.; Chen, Q.; David, C.; Flechsig, U.; Gozzo, F.; Henrich, B.; Jäggi-Spielmann, S.; Jakob, B.; Kalichava, I.; Karvinen, P.; Krempasky, J.; Lüdeke, A.; Lüscher, R.; Maag, S.; Quitmann, C.; Reinle-Schmitt, M. L.; Schmidt, T.; Schmitt, B.; Streun, A.; Vartiainen, I.; Vitins, M.; Wang, X.; Wullschleger, R.

    2013-01-01

    The Materials Science beamline at the Swiss Light Source has been operational since 2001. In late 2010, the original wiggler source was replaced with a novel insertion device, which allows unprecedented access to high photon energies from an undulator installed in a medium-energy storage ring. In order to best exploit the increased brilliance of this new source, the entire front-end and optics had to be redesigned. In this work, the upgrade of the beamline is described in detail. The tone is didactic, from which it is hoped the reader can adapt the concepts and ideas to his or her needs. PMID:23955029

  8. Upgrades to the Fermilab NuMI beamline

    SciTech Connect

    Martens, Michael A.; Childress, Sam; Grossman, Nancy; Hurh, Patrick; Hylen, James; Marchionni, Alberto; McCluskey, Elaine; Moore, Craig Damon; Reilly, Robert; Tariq, Salman; Wehmann, Alan; /Fermilab

    2007-06-01

    The NuMI beamline at Fermilab has been delivering high-intensity muon neutrino beams to the MINOS experiment since the spring of 2005. A total of 3.4 x 10{sup 20} protons has been delivered to the NuMI target and a maximum beam power of 320 kW has been achieved. An upgrade of the NuMI facility increasing the beam power capability to 700 kW is planned as part of the NOvA experiment. The plans for this upgrade are presented and the possibility of upgrading the NuMI beamline to handle 1.2 MW is considered.

  9. Kinematic mounting systems for NSLS beamlines and experiments

    SciTech Connect

    Oversluizen, T.; Stoeber, W.; Johnson, E.D.

    1991-01-01

    Methods for kinematically mounting equipment are well established, but applications at synchrotron radiation facilities are subject to constraints not always encountered in more traditional laboratory settings. Independent position adjustment of beamline components can have significant benefits in terms of minimizing time spent aligning, and maximizing time spent acquiring data. In this paper, we use examples taken from beamlines at the NSLS to demonstrate approaches for optimization of the reproducibility, stability, excursion, and set-up time for various situations. From our experience, we extract general principles which we hope will be useful for workers at other synchrotron radiation facilities. 7 refs., 4 figs.

  10. True 3D kinematic analysis for slope instability assessment in the Siq of Petra (Jordan), from high resolution TLS

    NASA Astrophysics Data System (ADS)

    Gigli, Giovanni; Margottini, Claudio; Spizzichino, Daniele; Ruther, Heinz; Casagli, Nicola

    2016-04-01

    Most classifications of mass movements in rock slopes use relatively simple, idealized geometries for the basal sliding surface, like planar sliding, wedge sliding, toppling or columnar failures. For small volumes, the real sliding surface can be often well described by such simple geometries. Extended and complex rock surfaces, however, can exhibit a large number of mass movements, also showing various kind of kinematisms. As a consequence, the real situation in large rock surfaces with a complicate geometry is generally very complex and a site depending analysis, such as fieldwork and compass, cannot be comprehensive of the real situation. Since the outstanding development of terrestrial laser scanner (TLS) in recent years, rock slopes can now be investigated and mapped through high resolution point clouds, reaching the resolution of few mm's and accuracy less than a cm in most advanced instruments, even from remote surveying. The availability of slope surface digital data can offer a unique chance to determine potential kinematisms in a wide distributed area for all the investigated geomorphological processes. More in detail the proposed method is based on the definition of least squares fitting planes on clusters of points extracted by moving a sampling cube on the point cloud. If the associated standard deviation is below a defined threshold, the cluster is considered valid. By applying geometric criteria it is possible to join all the clusters lying on the same surface; in this way discontinuity planes can be reconstructed, rock mass geometrical properties are calculated and, finally, potential kinematisms established. The Siq of Petra (Jordan), is a 1.2 km naturally formed gorge, with an irregular horizontal shape and a complex vertical slope, that represents the main entrance to Nabatean archaeological site. In the Siq, discontinuities of various type (bedding, joints, faults), mainly related to geomorphological evolution of the slope, lateral stress

  11. Beamline Control and Instrumentation System using Industrial Interface Techniques

    NASA Astrophysics Data System (ADS)

    Enz, F.

    2010-06-01

    How should a beamline be designed, which satisfies the needs and requirements of scientists and is easy to build and operate? Today, most control and instrumentation systems for beamlines are based on scientific requirements. Scientific details of the beamline, e.g. vacuum and beam physics details; are usually extensively described. However, control system specifications are often reduced to few requirements, e.g. which beam-related device to use. Lots of these systems work perfectly from the physicist's point of view, but are hard to bring into service and operate and difficult to extend with additional equipment. To overcome this, the engineering company ENZ has developed components using industrial standard interfaces to guarantee high flexibility for equipment extension. Using special interface boards and galvanic isolation offers increased stability of motion control axes. This saves resources during commissioning and service. A control system was developed and installed at a Soft-X-ray beamline at ASP Melbourne. It is operated under EPICs on distributed embedded IOC's based on PC-hardware. Motion and vacuum systems, measurement devices, e.g. a Low-Current Monitor (LoCuM) for beam position monitoring, and parts of the equipment protection system were developed and most of them tested in cooperation with DELTA at the Technical University of Dortmund.

  12. A modular optics design for the LBNE beamline

    SciTech Connect

    Johnstone, John A.; /Fermilab

    2010-10-01

    Protons extracted from the Main Injector (MI) in the MI-60 straight section are transported 84 m through quadrupole Q106 in the NuMI stub, at which point two 6-3-120 vertical switching magnets, followed by three EPB vertical dipoles, steer the beam into the main body of the LBNE beamline. From Q106 in NuMI the LBNE beamline transports these protons 722.0 m to the LBNE target, located 41.77 m (137.0 ft) below the MI beamline center (BLC) elevation, on a trajectory aimed towards DUSEL. Bending is provided (predominantly) by 34 long (6 m) MI-style IDA/IDB and 8 short (4 m) IDC/IDD dipoles [through 48.36{sup o} horizontally and -5.844{sup o} (net) vertically]. Optical properties are defined by 49 quadrupoles (grouped functionally into 44 focusing centers) of the proven MI beamline-style 3Q60/3Q120 series. All focusing centers are equipped with redesigned MI-style IDS orbit correctors and dual-plane beam position monitors (BPM's). Ample space is available in each arc cell to accommodate ion pumps and diagnostic instrumentation. Parameters of the main magnets are listed in a table.

  13. Beamline Control and Instrumentation System using Industrial Interface Techniques

    SciTech Connect

    Enz, F.

    2010-06-23

    How should a beamline be designed, which satisfies the needs and requirements of scientists and is easy to build and operate? Today, most control and instrumentation systems for beamlines are based on scientific requirements. Scientific details of the beamline, e.g. vacuum and beam physics details; are usually extensively described. However, control system specifications are often reduced to few requirements, e.g. which beam-related device to use. Lots of these systems work perfectly from the physicist's point of view, but are hard to bring into service and operate and difficult to extend with additional equipment. To overcome this, the engineering company ENZ has developed components using industrial standard interfaces to guarantee high flexibility for equipment extension. Using special interface boards and galvanic isolation offers increased stability of motion control axes. This saves resources during commissioning and service. A control system was developed and installed at a Soft-X-ray beamline at ASP Melbourne. It is operated under EPICs on distributed embedded IOC's based on PC-hardware. Motion and vacuum systems, measurement devices, e.g. a Low-Current Monitor (LoCuM) for beam position monitoring, and parts of the equipment protection system were developed and most of them tested in cooperation with DELTA at the Technical University of Dortmund.

  14. A synchrotron beamline for delivering high purity vacuum ultraviolet photons

    NASA Astrophysics Data System (ADS)

    Cavasso Filho, R. L.; Homen, M. G. P.; Fonseca, P. T.; Naves de Brito, A.

    2007-11-01

    We report on the current status and performance of the toroidal grating monochromator beamline at the Brazilian Synchrotron Light Laboratory (Laboratório Nacional de Luz Síncrotron). This beamline provides photons in the vacuum ultraviolet and soft x-ray regions from 12to330eV with three interchangeable gratings. We report on the improvement, which allows the possibility of choosing the light polarization degree from linear to almost circular. Here, we also describe the development of a new apparatus, namely, the mirror-inserted harmonic attenuator and calibrating-device with a long length (MIRHACLLE). All beamlines based on diffraction gratings suffer from the problem of high harmonics contaminations to some extent. The MIRHACLLE provides a way to efficiently suppress high harmonics from 25% to 1ppm in a grazing incidence bending magnet beamline. Its principle of operation relays on the absorption of the high energy photons in a gas phase region. It allows negligible high harmonics contamination for photon energies ranging from 12eV to the gas first ionization threshold, 21.6eV, in the case of neon. We also demonstrate the possibility to use this device for energy calibration and resolution evaluation together with any experiment needing its filtering capabilities. The device is also very cost effective compared to other filters presented previously in the literature.

  15. Nuclear resonant scattering beamline at the Advanced Photon Source

    SciTech Connect

    Alp, E.E.; Mooney, T.M.; Toellner, T.; Sturhahn, W.

    1993-09-01

    The principal and engineering aspects of a dedicated synchrotron radiation beamline under construction at the Advanced Photon Source for nuclear resonant scattering purposes are explained. The expected performance in terms of isotopes to be studied, flux, and timing properties is discussed.

  16. Aberration analysis calculations for synchrotron radiation beamline design

    SciTech Connect

    McKinney, W.R.; Howells, M.; Padmore, H.A.

    1997-09-01

    The application of ray deviation calculations based on aberration coefficients for a single optical surface for the design of beamline optical systems is reviewed. A systematic development is presented which allows insight into which aberration may be causing the rays to deviate from perfect focus. A new development allowing analytical calculation of line shape is presented.

  17. Canadian macromolecular crystallography facility: a suite of fully automated beamlines.

    PubMed

    Grochulski, Pawel; Fodje, Michel; Labiuk, Shaunivan; Gorin, James; Janzen, Kathryn; Berg, Russ

    2012-06-01

    The Canadian light source is a 2.9 GeV national synchrotron radiation facility located on the University of Saskatchewan campus in Saskatoon. The small-gap in-vacuum undulator illuminated beamline, 08ID-1, together with the bending magnet beamline, 08B1-1, constitute the Canadian Macromolecular Crystallography Facility (CMCF). The CMCF provides service to more than 50 Principal Investigators in Canada and the United States. Up to 25% of the beam time is devoted to commercial users and the general user program is guaranteed up to 55% of the useful beam time through a peer-review process. CMCF staff provides "Mail-In" crystallography service to users with the highest scored proposals. Both beamlines are equipped with very robust end-stations including on-axis visualization systems, Rayonix 300 CCD series detectors and Stanford-type robotic sample auto-mounters. MxDC, an in-house developed beamline control system, is integrated with a data processing module, AutoProcess, allowing full automation of data collection and data processing with minimal human intervention. Sample management and remote monitoring of experiments is enabled through interaction with a Laboratory Information Management System developed at the facility.

  18. VESPERS: A Beamline for Combined XRF and XRD Measurements

    NASA Astrophysics Data System (ADS)

    Feng, Renfei; Gerson, Andrea; Ice, Gene; Reininger, Ruben; Yates, Brian; McIntyre, Stewart

    2007-01-01

    VESPERS (VEry Sensitive Elemental and Structural Probe Employing Radiation from a Synchrotron) is a bending magnet beamline that is just beginning construction at the Canadian Light Source. The beamline has several novel design elements that are intended to increase its operating flexibility and availability to users. First, there is a requirement to deliver a microscopic beam with a variable bandwidth, thus enabling the generation of Laue diffraction patterns and high yield X-ray fluorescence spectra from the same region preferably simultaneously. Thus, the bandpass of the VESPERS monochromator can be readily changed to focus radiation into the same 2-4 micron diameter area that is either polychromatic or having a bandwidth of 10%, 1.6% or 0.01%. This allows the user to change the diffraction pattern to suit the complexity of the crystal and the spectral signal to noise ratio to suit the detection sensitivity required. Second, the beamline is designed to have two branches capable of operating simultaneously and virtually independently using the same primary optics. These design features are accomplished using four separate beams originating at four pinholes at the entry to the Primary Optical Enclosure. The compound focus design uses spherical mirrors to focus both polychromatic and pre-monochromatic beams onto the intermediate slits. A pair of bendable K-B mirrors in the experimental hutch is used to demagnify the beam further down to micron size. The photon energy of this beamline is 6-30 keV.

  19. The Nanoscience Beamline (I06) at Diamond Light Source

    SciTech Connect

    Dhesi, S. S.; Cavill, S. A.; Potenza, A.; Marchetto, H.; Mott, R. A.; Steadman, P.; Peach, A.; Shepherd, E. L.; Ren, X.; Wagner, U. H.; Reininger, R.

    2010-06-23

    The Nanoscience beamline (I06) is one of seven Diamond Phase-I beamlines which has been operational since January 2007 delivering polarised soft x-rays, for a PhotoEmission Electron Microscope (PEEM) and branchline, in the energy range 80-2100 eV. The beamline is based on a collimated plane grating monochromator with sagittal focusing elements, utilising two APPLE II helical undulator sources, and has been designed for high flux density at the PEEM sample position. A {approx}5 {mu}m ({sigma}) diameter beam is focussed onto the sample in the PEEM allowing a range of experiments using x-ray absorption spectroscopy (XAS), x-ray magnetic circular dichroism (XMCD) and x-ray magnetic linear dichroism (XMLD) as contrast mechanisms. The beamline is also equipped with a branchline housing a 6T superconducting magnet for XMCD and XMLD experiments. The magnet is designed to move on and off the branchline which allows a diverse range of experiments.

  20. Neutral beamline with improved ion-energy recovery

    SciTech Connect

    Dagenhart, W.K.; Haselton, H.H.; Stirling, W.L.; Whealton, J.H.

    1981-04-13

    A neutral beamline generator with unneutralized ion energy recovery is provided which enhances the energy recovery of the full energy ion component of the beam exiting the neutralizer cell of the beamline. The unneutralized full energy ions exiting the neutralizer are deflected from the beam path and the electrons in the cell are blocked by a magnetic field applied transverse to the beamline in the cell exit region. The ions, which are generated at essentially ground potential and accelerated through the neutralizer cell by a negative acceleration voltage, are collected at ground potential. A neutralizer cell exit end region is provided which allows the magnetic and electric fields acting on the exiting ions to be closely coupled. As a result, the fractional energy ions exiting the cell with the full energy ions are reflected back into the gas cell. Thus, the fractional energy ions do not detract from the energy recovery efficiency of full energy ions exiting the cell which can reach the ground potential interior surfaces of the beamline housing.

  1. The INE-Beamline for actinide science at ANKA

    SciTech Connect

    Rothe, J.; Dardenne, K.; Denecke, M. A.; Kienzler, B.; Loeble, M.; Metz, V.; Steppert, M.; Vitova, T.; Geckeis, H.; Butorin, S.; Seibert, A.; Walther, C.

    2012-04-15

    Since its inauguration in 2005, the INE-Beamline for actinide research at the synchrotron source ANKA (KIT North Campus) provides dedicated instrumentation for x-ray spectroscopic characterization of actinide samples and other radioactive materials. R and D work at the beamline focuses on various aspects of nuclear waste disposal within INE's mission to provide the scientific basis for assessing long-term safety of a final nuclear waste repository. The INE-Beamline is accessible for the actinide and radiochemistry community through the ANKA proposal system and the European Union Integrated Infrastructure Initiative ACTINET-I3. Experiments with activities up to 1 x 10{sup +6} times the European exemption limit are feasible within a safe but flexible containment concept. Measurements with monochromatic radiation are performed at photon energies varying between {approx}2.1 keV (P K-edge) and {approx}25 keV (Pd K-edge), including the lanthanide L-edges and the actinide M- and L3-edges up to Cf. The close proximity of the INE-Beamline to INE controlled area labs offers infrastructure unique in Europe for the spectroscopic and microscopic characterization of actinide samples. The modular beamline design enables sufficient flexibility to adapt sample environments and detection systems to many scientific questions. The well-established bulk techniques x-ray absorption fine structure (XAFS) spectroscopy in transmission and fluorescence mode have been augmented by advanced methods using a microfocused beam, including (confocal) XAFS/x-ray fluorescence detection and a combination of (micro-)XAFS and (micro-)x-ray diffraction. Additional instrumentation for high energy-resolution x-ray emission spectroscopy has been successfully developed and tested.

  2. Beamline 9.3.2 - a high-resolution, bend-magnet beamline with circular polarization capability

    SciTech Connect

    Moler, E.J.; Hussain, Z.; Howells, M.R.

    1997-04-01

    Beamline 9.3.2 is a high resolution, SGM beamline on an ALS bending magnet with access to photon energies from 30-1500 eV. Features include circular polarization capability, a rotating chamber platform that allows switching between experiments without breaking vacuum, an active feedback system that keeps the beam centered on the entrance slit of the monochromator, and a bendable refocusing mirror. The beamline optics consist of horizontally and vertically focussing mirrors, a Spherical Grating Monochromator (SGM) with movable entrance and exit slits, and a bendable refocussing mirror. In addition, a movable aperature has been installed just upstream of the vertically focussing mirror which can select the x-rays above or below the plane of the synchrotron storage ring, allowing the user to select circularly or linearly polarized light. Circularly polarized x-rays are used to study the magnetic properties of materials. Beamline 9.3.2 can supply left and right circularly polarized x-rays by a computer controlled aperture which may be placed above or below the plane of the synchrotron storage ring. The degree of linear and circular polarization has been measured and calibrated.

  3. Conceptual Design of a Dedicated SAXS Beamline at NSRRC

    NASA Astrophysics Data System (ADS)

    Liu, D. G.; Tseng, P. C.; Tsang, K. L.; Jeng, U.; Chang, C. H.; Fung, H. S.; Liu, C. Y.; Chung, S. C.; Tang, M. T.; Song, Y. F.; Liang, K. S.

    2007-01-01

    A dedicated small-angle X-ray scattering (SAXS) beamline using a new X-ray source generated by an In-Acromat superconducting wiggler (IASW6) insertion device is under construction at the National Synchrotron Radiation Research Center (NSRRC). The IASW6 with peak magnetic field of 3.1 T, magnet period of 6.1 cm, and total length of 96 cm, can provide a photon flux ˜ 1012 - 1013photons/s/0.1%bw in the energy range of 5 - 23 keV. Taking the central 0.2 mard horizontal radiation fan from the source with a beam divergence of 200 and 392 μrad in the vertical and horizontal directions, respectively, the dedicated SAXS beamline is oriented for nano to meso-structural research in soft matter, including liquid crystals, macromolecular solutions, polymers, as well as in nanoparticles, ceramic, and alloys. The SAXS beamline adopts the design of the double-monochromator used in the beamline SIYBLS at ALS, which integrates a Si(111) double crystal monochromator (DCM) and a Mo/B4C double multilayer monochromator (DMM) into one cradle for fast exchange between the two monochrmators. Equipped with a collimating mirror (CM) and a toroidal focusing mirror (FM) with 1:1 focusing ratio, this beamline provides two types of SAXS measurements: high-Q resolution and high flux, by using either the DCM or DMM. The SAXS beamline also provides energy scan with an energy resolution from 1 to 10 eV for anomalous SAXS (ASAXS) measurements. A specially coated reflecting mirror is also installed after FM to provide a suitable photon beam for grazing incident SAXS of liquid surfaces. Ray tracing simulation results show that at 8 keV and with DCM, a high quality photon beam of beam size (0.5 mm) and beam divergence (± 50 μrad) with a flux of ˜ 1011 photons/s can be obtained for high-Q resolution SAXS measurement. The photon flux can be increased by one order of magnitude when the DMM is used; however, the beam size and divergence are both slightly increased.

  4. The ID23-2 structural biology microfocus beamline at the ESRF

    PubMed Central

    Flot, David; Mairs, Trevor; Giraud, Thierry; Guijarro, Matias; Lesourd, Marc; Rey, Vicente; van Brussel, Denis; Morawe, Christian; Borel, Christine; Hignette, Olivier; Chavanne, Joel; Nurizzo, Didier; McSweeney, Sean; Mitchell, Edward

    2010-01-01

    The first phase of the ESRF beamline ID23 to be constructed was ID23-1, a tunable MAD-capable beamline which opened to users in early 2004. The second phase of the beamline to be constructed is ID23-2, a monochromatic microfocus beamline dedicated to macromolecular crystallography experiments. Beamline ID23-2 makes use of well characterized optical elements: a single-bounce silicon (111) monochromator and two mirrors in Kirkpatrick–Baez geometry to focus the X-ray beam. A major design goal of the ID23-2 beamline is to provide a reliable, easy-to-use and routine microfocus beam. ID23-2 started operation in November 2005, as the first beamline dedicated to microfocus macromolecular crystallography. The beamline has taken the standard automated ESRF macromolecular crystallography environment (both hardware and software), allowing users of ID23-2 to be rapidly familiar with the microfocus environment. This paper describes the beamline design, the special considerations taken into account given the microfocus beam, and summarizes the results of the first years of the beamline operation. PMID:20029119

  5. The crystallography beamline I711 at MAX II.

    PubMed

    Cerenius, Y; Ståhl, K; Svensson, L A; Ursby, T; Oskarsson, A; Albertsson, J; Liljas, A

    2000-07-01

    A new X-ray crystallographic beamline is operational at the MAX II synchrotron in Lund. The beamline has been in regular use since August 1998 and is used both for macro- and small molecule diffraction as well as powder diffraction experiments. The radiation source is a 1.8 T multipole wiggler. The beam is focused vertically by a bendable mirror and horizontally by an asymmetrically cut Si(111) monochromator. The wavelength range is 0.8-1.55 A with a measured flux at 1 A of more than 10(11) photons s(-1) in 0.3 mm x 0.3 mm at the sample position. The station is currently equipped with a Mar345 imaging plate, a Bruker Smart 1000 area CCD detector and a Huber imaging-plate Guinier camera. An ADSC 210 area CCD detector is planned to be installed during 2000. PMID:16609196

  6. Compact Double Multilayer Monochromator for SAXS Beamline at PLS

    SciTech Connect

    Kim, S. N.; Kim, M. J.; Lee, C. S.; Kim, J. H.; Koo, C. J.

    2007-01-19

    The DMM (Double Multilayer Monochromator) is one of the most important components to increase the efficiency of experiments in SAXS beamline. The DMM of SAXS beamline was consisted of x, z stages to decrease the alignment error and 6 movement systems to raise efficiency of adjustment. To determine the type of 1st mirror holder, we simulated heat-transfer and structural analysis with ANSYS code and confirmed the deformation and slope error of the mirror face. With rocking width and weighted standard deviation, we found the optimized results in the mirror systems. To cope with the high precise alignment of pitch and roll direction, CMM and interferometer (HP 5529A) were used. This equipment was installed on Feb, 2006.

  7. An Undulator-Wiggler Beamline for Spectromicroscopy at SRC

    SciTech Connect

    Reininger, R.; De Stasio, G.; Bissen, M.; Severson, M.

    2004-05-12

    A high-flux medium-energy-resolution beamline based on an existing insertion device is being constructed at SRC. The insertion device will be operated as an undulator up to {approx}400 eV and as a wiggler at higher energies. The beamline will be dedicated mainly to X-ray PhotoElectron Emission spectroMicroscopy (X-PEEM) and will cover the energy range 75-2000 eV. The most relevant requirement for high-resolution and high-sensitivity X-PEEM is a high flux density on the sample surface. This will allow spatial resolutions on the order of a few nanometers, and a minimum detection limit on the order of 10 parts per million, using the already existing Spectromicroscope for PHotoelectron Imaging of Nanostructures with X-rays (SPHINX). To maximize the flux at the sample position, the beamline does not include an entrance slit and has only three optical elements on the beam path: an ellipsoidal mirror, a variable-line-spacing plane grating, and a re-focusing ellipsoidal mirror. The first ellipsoidal mirror provides the converging light to one of the three gratings needed to cover the beamline energy range. The position of the fixed exit slit is at the focus of the ellipsoidal mirror when the grating is tuned to zero order. The second ellipsoidal mirror demagnifies the beam at the exit slit plane by a factor of two. More than 1012 photons/s are expected at the sample position between 100 and 1200 eV onto a spot having a FWHM of 25 {mu}m vertical and 70 {mu}m horizontal at a resolving power of {approx}1000.

  8. An Undulator-Wiggler Beamline for Spectromicroscopy at SRC

    NASA Astrophysics Data System (ADS)

    Reininger, R.; De Stasio, G.; Bissen, M.; Severson, M.

    2004-05-01

    A high-flux medium-energy-resolution beamline based on an existing insertion device is being constructed at SRC. The insertion device will be operated as an undulator up to ˜400 eV and as a wiggler at higher energies. The beamline will be dedicated mainly to X-ray PhotoElectron Emission spectroMicroscopy (X-PEEM) and will cover the energy range 75-2000 eV. The most relevant requirement for high-resolution and high-sensitivity X-PEEM is a high flux density on the sample surface. This will allow spatial resolutions on the order of a few nanometers, and a minimum detection limit on the order of 10 parts per million, using the already existing Spectromicroscope for PHotoelectron Imaging of Nanostructures with X-rays (SPHINX). To maximize the flux at the sample position, the beamline does not include an entrance slit and has only three optical elements on the beam path: an ellipsoidal mirror, a variable-line-spacing plane grating, and a re-focusing ellipsoidal mirror. The first ellipsoidal mirror provides the converging light to one of the three gratings needed to cover the beamline energy range. The position of the fixed exit slit is at the focus of the ellipsoidal mirror when the grating is tuned to zero order. The second ellipsoidal mirror demagnifies the beam at the exit slit plane by a factor of two. More than 1012 photons/s are expected at the sample position between 100 and 1200 eV onto a spot having a FWHM of 25 μm vertical and 70 μm horizontal at a resolving power of ˜1000.

  9. The Soft X-ray Spectromicroscopy Beamline at SSRF

    SciTech Connect

    Guo, Z.; Tai, R.; Wand, Y.; Yan, R.; Chen, M.; Wu, Y.; Chen, J.; Xue, S.; Xu, H.

    2011-09-09

    Commissioning of the soft x-ray spectromicroscopy beanmline at SSRF was formally started on Dec 26, 2008. Beamline performance has reached or surpassed the designing goals according to the measurements by domestic experts, especially for its high energy resolution and high spatial resolution. Since its first operation by users on May 6, 2009, tens of experiments have been conducted, and some preliminary exciting results have been acquired.

  10. Attosecond beamline with actively stabilized and spatially separated beam paths.

    PubMed

    Huppert, M; Jordan, I; Wörner, H J

    2015-12-01

    We describe a versatile and compact beamline for attosecond spectroscopy. The setup consists of a high-order harmonic source followed by a delay line that spatially separates and then recombines the extreme-ultraviolet (XUV) and residual infrared (IR) pulses. The beamline introduces a controlled and actively stabilized delay between the XUV and IR pulses on the attosecond time scale. A new active-stabilization scheme combining a helium-neon-laser and a white-light interferometer minimizes fluctuations and allows to control delays accurately (26 as rms during 1.5 h) over long time scales. The high-order-harmonic-generation region is imaged via optical systems, independently for XUV and IR, into an interaction volume to perform pump-probe experiments. As a consequence of the spatial separation, the pulses can be independently manipulated in intensity, polarization, and frequency content. The beamline can be combined with a variety of detectors for measuring attosecond dynamics in gases, liquids, and solids.

  11. Attosecond beamline with actively stabilized and spatially separated beam paths

    NASA Astrophysics Data System (ADS)

    Huppert, M.; Jordan, I.; Wörner, H. J.

    2015-12-01

    We describe a versatile and compact beamline for attosecond spectroscopy. The setup consists of a high-order harmonic source followed by a delay line that spatially separates and then recombines the extreme-ultraviolet (XUV) and residual infrared (IR) pulses. The beamline introduces a controlled and actively stabilized delay between the XUV and IR pulses on the attosecond time scale. A new active-stabilization scheme combining a helium-neon-laser and a white-light interferometer minimizes fluctuations and allows to control delays accurately (26 as rms during 1.5 h) over long time scales. The high-order-harmonic-generation region is imaged via optical systems, independently for XUV and IR, into an interaction volume to perform pump-probe experiments. As a consequence of the spatial separation, the pulses can be independently manipulated in intensity, polarization, and frequency content. The beamline can be combined with a variety of detectors for measuring attosecond dynamics in gases, liquids, and solids.

  12. Design and Simulation of the nuSTORM Pion Beamline

    SciTech Connect

    Liu, A.; Neuffer, D.; Bross, A.

    2015-08-15

    The nuSTORM (neutrinos from STORed Muons) proposal presents a detailed design for a neutrino facility based on a muon storage ring, with muon decay in the production straight section of the ring providing well defined neutrino beams. The facility includes a primary high-energy proton beam line, a target station with pion production and collection, and a pion beamline for pion transportation and injection into a muon decay ring. The nuSTORM design uses “stochastic injection”, in which pions are directed by a chicane, referred to as the Orbit Combination Section (OCS), into the production straight section of the storage ring. Pions that decay within that straight section provide muons within the circulating acceptance of the ring. Furthermore, the design enables injection without kickers or a separate pion decay transport line. The beam line that the pions traverse before being extracted from the decay ring is referred to as the pion beamline. Our paper describes the design and simulation of the pion beamline, and includes full beam dynamics simulations of the system.

  13. Construction status of CXI beamline at PAL-XFEL

    NASA Astrophysics Data System (ADS)

    Park, Jaehyun; Nam, Ki-Hyun; Kim, Sangsoo; Kim, Bongsoo; Ko, In Soo; Cho, Moohyun

    2015-05-01

    Pohang Accelerator Laboratory X-ray Free Electron Laser (PAL-XFEL) is a research facility currently under construction. It will provide ultra-bright (assuming 1 X 1012 photons/pulse at 12.4 keV) and ultra-short (10-60 femtosecond) X-ray pulses. The CXI (Coherent X-ray Imaging) end-station, which will be constructed for hard X-ray beamline at the PAL-XFEL, is designed to deliver brilliant hard x-rays (2-20 keV) and to measure diffraction signals with forward scattering geometry, mainly. Not only will it offer imaging studies of biological, chemical and physical samples by the "diffract-before-destroy" technique, but will also be helpful in high field hard x-ray physics and material science. The scientific programs are currently aimed at serial femtosecond crystallography (SFX) for macromolecular systems and coherent diffraction imaging for bio specimens and nano structures etc. In this paper, we describe the details of the beamline layout, X-ray focusing optics (Kirkpatrick-Baez mirror and Beryllium CRLs) and sample delivery system (liquid jet/LCP sample injector, fixed target system) that will be installed at the CXI beamline.

  14. Design and Simulation of the nuSTORM Pion Beamline

    DOE PAGES

    Liu, A.; Neuffer, D.; Bross, A.

    2015-08-15

    The nuSTORM (neutrinos from STORed Muons) proposal presents a detailed design for a neutrino facility based on a muon storage ring, with muon decay in the production straight section of the ring providing well defined neutrino beams. The facility includes a primary high-energy proton beam line, a target station with pion production and collection, and a pion beamline for pion transportation and injection into a muon decay ring. The nuSTORM design uses “stochastic injection”, in which pions are directed by a chicane, referred to as the Orbit Combination Section (OCS), into the production straight section of the storage ring. Pionsmore » that decay within that straight section provide muons within the circulating acceptance of the ring. Furthermore, the design enables injection without kickers or a separate pion decay transport line. The beam line that the pions traverse before being extracted from the decay ring is referred to as the pion beamline. Our paper describes the design and simulation of the pion beamline, and includes full beam dynamics simulations of the system.« less

  15. MERLIN - A meV Resolution Beamline at the ALS

    SciTech Connect

    Reininger, Ruben; Bozek, John; Chuang, Y.-D.; Howells, Malcolm; Kelez, Nicholas; Prestemon, Soren; Marks, Steve; Warwick, Tony; Hussain, Zahid; Jozwiak, Chris; Lanzara, Alessandra; Hasan, M. Zahid

    2007-01-19

    An ultra-high resolution beamline is being constructed at the Advanced Light Source (ALS) for the study of low energy excitations in strongly correlated systems with the use of high-resolution inelastic scattering and angle-resolved photoemission. This new beamline, given the acronym Merlin (for meV resolution line), will cover the energy range 10-150 eV. The monochromator has fixed entrance and exit slits and a plane mirror that can illuminate a spherical grating at the required angle of incidence (as in the SX-700 mechanism). The monochromator can be operated in two different modes. In the highest resolution mode, the energy scanning requires translating the monochromator chamber (total travel 1.1 m) as well as rotating the grating and the plane mirror in front of the grating. The resolution in this mode is practically determined by the slits width. In the second mode, the scanning requires rotating the grating and the plane mirror. This mode can be used to scan a few eV without a significant resolution loss. The source for the beamline is a 1.9 m long, 90 mm period quasi periodic EPU. The expected flux at the sample is higher than 1011 photons/s at a resolving power of 5 x 104 in the energy range 16-130 eV. A second set of gratings can be used to obtain higher flux at the expense of resolution.

  16. SIBYLS - A SAXS and protein crystallography beamline at the ALS

    SciTech Connect

    Trame, Christine; MacDowell, Alastair A.; Celestre, Richard S.; Padmore, Howard A.; Cambie, Daniella; Domning, Edward E.; Duarte, Robert M.; Kelez, Nicholas; Plate, David W.; Holton, James M.; Frankel, Kenneth; Tsutakawa, Susan; Tsuruta, Hiro; Tainer, John A.; Cooper, Priscilla K.

    2003-08-22

    The new Structurally Integrated BiologY for Life Sciences (SIBYLS) beamline at the Advanced Light Source will be dedicated to Macromolecular Crystallography (PX) and Small Angle X-ray Scattering (SAXS). SAXS will provide structural information of macromolecules in solutions and will complement high resolution PX studies on the same systems but in a crystalline state. The x-ray source is one of the 5 Tesla superbend dipoles recently installed at the ALS that allows for a hard x-ray program to be developed on the relatively low energy Advanced Light Source (ALS) ring (1.9 GeV). The beamline is equipped with fast interchangeable monochromator elements, consisting of either a pair of single Si(111) crystals for crystallography, or a pair of multilayers for the SAXS mode data collection (E/{Delta}E {approx} 1/110). Flux rates with Si(111) crystals for PX are measured as 2 x 10{sup 11} hv/sec/400 mA through a 100 {micro}m pinhole at 12.4 KeV. For SAXS the flux is up to 3 x 10{sup 13} photons/sec at 10 KeV with all apertures open when using the multilayer monochromator elements. The performance characteristics of this unique beamline will be described.

  17. ADLIB—A simple database framework for beamline codes

    NASA Astrophysics Data System (ADS)

    Mottershead, C. Thomas

    1993-12-01

    There are many well developed codes available for beamline design and analysis. A significant fraction of each of these codes is devoted to processing its own unique input language for describing the problem. None of these large, complex, and powerful codes does everything. Adding a new bit of specialized physics can be a difficult task whose successful completion makes the code even larger and more complex. This paper describes an attempt to move in the opposite direction, toward a family of small, simple, single purpose physics and utility modules, linked by an open, portable, public domain database framework. These small specialized physics codes begin with the beamline parameters already loaded in the database, and accessible via the handful of subroutines that constitute ADLIB. Such codes are easier to write, and inherently organized in a manner suitable for incorporation in model based control system algorithms. Examples include programs for analyzing beamline misalignment sensitivities, for simulating and fitting beam steering data, and for translating among MARYLIE, TRANSPORT, and TRACE3D formats.

  18. Attosecond beamline with actively stabilized and spatially separated beam paths.

    PubMed

    Huppert, M; Jordan, I; Wörner, H J

    2015-12-01

    We describe a versatile and compact beamline for attosecond spectroscopy. The setup consists of a high-order harmonic source followed by a delay line that spatially separates and then recombines the extreme-ultraviolet (XUV) and residual infrared (IR) pulses. The beamline introduces a controlled and actively stabilized delay between the XUV and IR pulses on the attosecond time scale. A new active-stabilization scheme combining a helium-neon-laser and a white-light interferometer minimizes fluctuations and allows to control delays accurately (26 as rms during 1.5 h) over long time scales. The high-order-harmonic-generation region is imaged via optical systems, independently for XUV and IR, into an interaction volume to perform pump-probe experiments. As a consequence of the spatial separation, the pulses can be independently manipulated in intensity, polarization, and frequency content. The beamline can be combined with a variety of detectors for measuring attosecond dynamics in gases, liquids, and solids. PMID:26724005

  19. The Imaging and Coherence Beamline I13 at Diamond

    SciTech Connect

    Rau, C.; Wagner, U.; Pesic, Z.

    2011-09-09

    The coherence and imaging beamline I13 is dedicated to hard x-ray imaging on the micro- and nano-lengthscale, performing microscopy either in direct or reciprocal space. For both, lens-based and lensless imaging, two independent stations will be operated in a separate building at a distance of 250 m from the source. The imaging branch will perform in-line phase contrast imaging and tomography over a large field of view in the 6- to 35-keV energy range. In addition, it will be possible to switch to full-field microscopy with 50-nm spatial resolution. Other microscopies will be developed according to the scientific needs. Resolution beyond the limitations given by the detector and x-ray optics will be achieved with techniques working in the far field. Coherent x-ray diffraction (CXRD) and other coherent diffraction imaging techniques such as ptychography will also be implemented on the same 'coherence' branch. The beamline hosts a number of innovative features such as the so-called 'mini-beta' layout for electron optics in the storage ring or new concepts for beamline instrumentation. The stations will be operational in 2011.

  20. Upgrade of SPring-8 Beamline Network with VLAN Technology over Gigabit Ethernet

    NASA Astrophysics Data System (ADS)

    Ishii, Miho

    The beamline network system at SPring-8 consists of three LANs; a BL-LAN for beamline component control, a BL-USER-LAN for beamline experimental users and an OA-LAN for the information services. These LANs are interconnected by a firewall system. Since the network traffic and the number of beamlines have increased, we upgraded the backbone of BL-USER-LAN from Fast Ethernet to Gigabit Ethernet. And then, to establish the independency of a beamline and to raise flexibility of every beamline, we also introduced the IEEE802.1Q Virtual LAN (VLAN) technology into the BL-USER-LAN. We discuss here a future plan to build the firewall system with hardware load balancers.

  1. MARS, a new beamline for radioactive matter studies at SOLEIL

    NASA Astrophysics Data System (ADS)

    Solari, Pier Lorenzo; Schlutig, Sandrine; Hermange, Hervé; Sitaud, Bruno

    2009-11-01

    MARS (Multi Analyses on Radioactive Samples) beamline is the hard X-ray bending magnet beamline dedicated to the study of radioactive matter of the new French synchrotron SOLEIL. The beamline, which has been built thanks to a close partnership and support by the CEA, has been designed to provide X-rays in the energy range of 3.5 keV to 35 keV. This allows to encompass M and L absorption edges of actinides, as well as K edges of transition metals (that are present in alloys and fuel claddings) up to heavy halogens, rare gases and alkalis (fission products in nuclear fuels). The MARS project aims to extend the possibilities of synchrotron based X-ray characterizations towards a wider variety of radioactive elements and a wider variety of techniques than what is currently available at other facilities. Thus, its specific and innovative infrastructure has been optimized in order to carry out analyses on materials with activities up to 18.5 GBq per sample for α and β emitters and 2 GBq for γ and n emitters. So, today, more than 70 different elements and more than 350 different isotopes have been proposed for studies on the beamline by the involved user community. The arrangement of the different elements in the optics hutch is based on an original scheme which permits to have two alternative optical configurations (monochromatic or dispersive) depending on the nature of experiments to be performed. At least three main techniques are progressively being proposed on the three complementary end-stations located in the experimental hutch: transmission and high resolution powder diffraction (TXRD and HRXRD), standard and dispersive X-ray absorption spectroscopy (XAS and EDXAS) and X-ray fluorescence (XRF). In addition, by using the KB optics, a micro-focused beam will be available on the second station of the monochromatic branch. The beamline is currently under commissioning. The first two experimental stations, using the monochromatic branch, are scheduled to be

  2. Gas bremsstrahlung shielding calculation for first optic enclosure of ILSF medical beamline

    NASA Astrophysics Data System (ADS)

    Beigzadeh Jalali, H.; Salimi, E.; Rahighi, J.

    2016-10-01

    Gas bremsstrahlung is generated in high energy electron storage ring accompanies the synchrotron radiation into the beamlines and strike the various components of the beamline. In this paper, radiation shielding calculation for secondary gas bremsstrahlung is performed for the first optics enclosure (FOE) of medical beamline of the Iranian Light Source Facility (ILSF). Dose equivalent rate (DER) calculation is accomplished using FLUKA Monte Carlo code. A comprehensive study of DER distribution at the back wall, sides and roof is given.

  3. Advanced light source vacuum policy and vacuum guidelines for beamlines and experiment endstations

    SciTech Connect

    Hussain, Z.

    1995-08-01

    The purpose of this document is to: (1) Explain the ALS vacuum policy and specifications for beamlines and experiment endstations. (2) Provide guidelines related to ALS vacuum policy to assist in designing beamlines which are in accordance with ALS vacuum policy. This document supersedes LSBL-116. The Advanced Light Source is a third generation synchrotron radiation source whose beam lifetime depends on the quality of the vacuum in the storage ring and the connecting beamlines. The storage ring and most of the beamlines share a common vacuum and are operated under ultra-high-vacuum (UHV) conditions. All endstations and beamline equipment must be operated so as to avoid contamination of beamline components, and must include proper safeguards to protect the storage ring vacuum from an accidental break in the beamline or endstation vacuum systems. The primary gas load during operation is due to thermal desorption and electron/photon induced desorption of contaminants from the interior of the vacuum vessel and its components. The desorption rates are considerably higher for hydrocarbon contamination, thus considerable emphasis is placed on eliminating these sources of contaminants. All vacuum components in a beamline and endstation must meet the ALS vacuum specifications. The vacuum design of both beamlines and endstations must be approved by the ALS Beamline Review Committee (BRC) before vacuum connections to the storage ring are made. The vacuum design is first checked during the Beamline Design Review (BDR) held before construction of the beamline equipment begins. Any deviation from the ALS vacuum specifications must be approved by the BRC prior to installation of the equipment on the ALS floor. Any modification that is incorporated into a vacuum assembly without the written approval of the BRC is done at the user`s risk and may lead to rejection of the whole assembly.

  4. HERMES: a soft X-ray beamline dedicated to X-ray microscopy.

    PubMed

    Belkhou, Rachid; Stanescu, Stefan; Swaraj, Sufal; Besson, Adrien; Ledoux, Milena; Hajlaoui, Mahdi; Dalle, Didier

    2015-07-01

    The HERMES beamline (High Efficiency and Resolution beamline dedicated to X-ray Microscopy and Electron Spectroscopy), built at Synchrotron SOLEIL (Saint-Auban, France), is dedicated to soft X-ray microscopy. The beamline combines two complementary microscopy methods: XPEEM (X-ray Photo Emitted Electron Microscopy) and STXM (Scanning Transmission X-ray Microscopy) with an aim to reach spatial resolution below 20 nm and to fully exploit the local spectroscopic capabilities of the two microscopes. The availability of the two methods within the same beamline enables the users to select the appropriate approach to study their specific case in terms of sample environment, spectroscopy methods, probing depth etc. In this paper a general description of the beamline and its design are presented. The performance and specifications of the beamline will be reviewed in detail. Moreover, the article is aiming to demonstrate how the beamline performances have been specifically optimized to fulfill the specific requirements of a soft X-ray microscopy beamline in terms of flux, resolution, beam size etc. Special attention has been dedicated to overcome some limiting and hindering problems that are usually encountered on soft X-ray beamlines such as carbon contamination, thermal stability and spectral purity.

  5. SAGE III

    Atmospheric Science Data Center

    2016-06-15

    SAGE III Data and Information The Stratospheric Aerosol and Gas ... on the spacecraft. SAGE III produced L1 and L2 scientific data from 5/07/2002 until 12/31/2005. The flight of the second instrument is as ... Guide Documents:  Project Guide Data Products User's Guide  (PDF) Relevant Documents:  ...

  6. ELIMED, MEDical and multidisciplinary applications at ELI-Beamlines

    NASA Astrophysics Data System (ADS)

    Schillaci, F.; Anzalone, A.; Cirrone, G. A. P.; Carpinelli, M.; Cuttone, G.; Cutroneo, M.; De Martinis, C.; Giove, D.; Korn, G.; Maggiore, M.; Manti, L.; Margarone, D.; Musumarra, A.; Perozziello, F. M.; Petrovic, I.; Pisciotta, P.; Renis, M.; Ristic-Fira, A.; Romano, F.; Romano, F. P.; Schettino, G.; Scuderi, V.; Torrisi, L.; Tramontana, A.; Tudisco, S.

    2014-04-01

    ELI-Beamlines is one of the pillars of the pan-European project ELI (Extreme Light Infrastructure). It will be an ultra high-intensity, high repetition-rate, femtosecond laser facility whose main goal is generation and applications of high-brightness X-ray sources and accelerated charged particles in different fields. Particular care will be devoted to the potential applicability of laser-driven ion beams for medical treatments of tumors. Indeed, such kind of beams show very interesting peculiarities and, moreover, laser-driven based accelerators can really represent a competitive alternative to conventional machines since they are expected to be more compact in size and less expensive. The ELIMED project was launched thanks to a collaboration established between FZU-ASCR (ELI-Beamlines) and INFN-LNS researchers. Several European institutes have already shown a great interest in the project aiming to explore the possibility to use laser-driven ion (mostly proton) beams for several applications with a particular regard for medical ones. To reach the project goal several tasks need to be fulfilled, starting from the optimization of laser-target interaction to dosimetric studies at the irradiation point at the end of a proper designed transport beam-line. Researchers from LNS have already developed and successfully tested a high-dispersive power Thomson Parabola Spectrometer, which is the first prototype of a more performing device to be used within the ELIMED project. Also a Magnetic Selection System able to produce a small pencil beam out of a wide energy distribution of ions produced in laser-target interaction has been realized and some preliminary work for its testing and characterization is in progress. In this contribution the status of the project will be reported together with a short description of the of the features of device recently developed.

  7. The BALDER Beamline at the MAX IV Laboratory

    NASA Astrophysics Data System (ADS)

    Klementiev, K.; Norén, K.; Carlson, S.; Sigfridsson Clauss, K. G. V.; Persson, I.

    2016-05-01

    X-ray absorption spectroscopy (XAS) includes well-established methods to study the local structure around the absorbing element - extended X-ray absorption fine structure (EXAFS), and the effective oxidation number or to quantitatively determine the speciation of an element in a complex matrix - X-ray absorption near-edge structure (XANES). The increased brilliance and intensities available at the new generation of synchrotron light sources makes it possible to study, in-situ and in-operando, much more dilute systems with relevance for natural systems, as well as the micro-scale variability and dynamics of chemical reactions on the millisecond time-scale. The design of the BALDER beamline at the MAX IV Laboratory 3 GeV ring has focused on a high flux of photons in a wide energy range, 2.4-40 keV, where the K-edge is covered for the elements S to La, and the L 3-edge for all elements heavier than Sb. The overall design of the beamline will allow large flexibility in energy range, beam size and data collection time. The other focus of the beamline design is the possibility to perform multi-technique analyses on samples. Development of sample environment requires focus on implementation of auxiliary methods in such a way that techniques like Fourier transform infrared (FTIR) spectroscopy, UV-Raman spectroscopy, X-ray diffraction and/or mass spectrometry can be performed simultaneously as the XAS study. It will be a flexible system where different instruments can be plugged in and out depending on the needs for the particular investigation. Many research areas will benefit from the properties of the wiggler based light source and the capabilities to perform in-situ and in-operando measurements, for example environmental and geochemical sciences, nuclear chemistry, catalysis, materials sciences, and cultural heritage.

  8. Mini-beam collimator enables microcrystallography experiments on standard beamlines

    PubMed Central

    Fischetti, Robert F.; Xu, Shenglan; Yoder, Derek W.; Becker, Michael; Nagarajan, Venugopalan; Sanishvili, Ruslan; Hilgart, Mark C.; Stepanov, Sergey; Makarov, Oleg; Smith, Janet L.

    2009-01-01

    The high-brilliance X-ray beams from undulator sources at third-generation synchrotron facilities are excellent tools for solving crystal structures of important and challenging biological macromolecules and complexes. However, many of the most important structural targets yield crystals that are too small or too inhomogeneous for a ‘standard’ beam from an undulator source, ∼25–50 µm (FWHM) in the vertical and 50–100 µm in the horizontal direction. Although many synchrotron facilities have microfocus beamlines for other applications, this capability for macromolecular crystallography was pioneered at ID-13 of the ESRF. The National Institute of General Medical Sciences and National Cancer Institute Collaborative Access Team (GM/CA-CAT) dual canted undulator beamlines at the APS deliver high-intensity focused beams with a minimum focal size of 20 µm × 65 µm at the sample position. To meet growing user demand for beams to study samples of 10 µm or less, a ‘mini-beam’ apparatus was developed that conditions the focused beam to either 5 µm or 10 µm (FWHM) diameter with high intensity. The mini-beam has a symmetric Gaussian shape in both the horizontal and vertical directions, and reduces the vertical divergence of the focused beam by 25%. Significant reduction in background was achieved by implementation of both forward- and back-scatter guards. A unique triple-collimator apparatus, which has been in routine use on both undulator beamlines since February 2008, allows users to rapidly interchange the focused beam and conditioned mini-beams of two sizes with a single mouse click. The device and the beam are stable over many hours of routine operation. The rapid-exchange capability has greatly facilitated sample screening and resulted in several structures that could not have been obtained with the larger focused beam. PMID:19240333

  9. Advanced Beamline Design for Fermilab's Advanced Superconducting Test Accelerator

    SciTech Connect

    Prokop, Christopher

    2014-01-01

    The Advanced Superconducting Test Accelerator (ASTA) at Fermilab is a new electron accelerator currently in the commissioning stage. In addition to testing superconducting accelerating cavities for future accelerators, it is foreseen to support a variety of Advanced Accelerator R&D (AARD) experiments. Producing the required electron bunches with the expected flexibility is challenging. The goal of this dissertation is to explore via numerical simulations new accelerator beamlines that can enable the advanced manipulation of electron bunches. The work especially includes the design of a low-energy bunch compressor and a study of transverse-to-longitudinal phase space exchangers.

  10. Time-resolved neutron imaging at ANTARES cold neutron beamline

    NASA Astrophysics Data System (ADS)

    Tremsin, A. S.; Dangendorf, V.; Tittelmeier, K.; Schillinger, B.; Schulz, M.; Lerche, M.; Feller, W. B.

    2015-07-01

    In non-destructive evaluation with X-rays light elements embedded in dense, heavy (or high-Z) matrices show little contrast and their structural details can hardly be revealed. Neutron radiography, on the other hand, provides a solution for those cases, in particular for hydrogenous materials, owing to the large neutron scattering cross section of hydrogen and uncorrelated dependency of neutron cross section on the atomic number. The majority of neutron imaging experiments at the present time is conducted with static objects mainly due to the limited flux intensity of neutron beamline facilities and sometimes due to the limitations of the detectors. However, some applications require the studies of dynamic phenomena and can now be conducted at several high intensity beamlines such as the recently rebuilt ANTARES beam line at the FRM-II reactor. In this paper we demonstrate the capabilities of time resolved imaging for repetitive processes, where different phases of the process can be imaged simultaneously and integrated over multiple cycles. A fast MCP/Timepix neutron counting detector was used to image the water distribution within a model steam engine operating at 10 Hz frequency. Within <10 minutes integration the amount of water was measured as a function of cycle time with a sub-mm spatial resolution, thereby demonstrating the capabilities of time-resolved neutron radiography for the future applications. The neutron spectrum of the ANTARES beamline as well as transmission spectra of a Fe sample were also measured with the Time Of Flight (TOF) technique in combination with a high resolution beam chopper. The energy resolution of our setup was found to be ~ 0.8% at 5 meV and ~ 1.7% at 25 meV. The background level (most likely gammas and epithermal/fast neutrons) of the ANTARES beamline was also measured in our experiments and found to be on the scale of 3% when no filters are installed in the beam. Online supplementary data available from stacks.iop.org/jinst/10

  11. Implementation of the beamline controls at the Florence accelerator laboratory

    NASA Astrophysics Data System (ADS)

    Carraresi, L.; Mirto, F. A.

    2008-05-01

    The new Tandetron accelerator in Florence, with many different beamlines, has required a new organization of all the control signals of the used equipment (slow control). We present our solution, which allows us the control of all the employed instruments simultaneously from a number of different workplaces. All of our equipment has been designed to be Ethernet based and this is the key to accomplish two very important requirements: simultaneous remote control from many computers and electrical isolation to achieve a lower noise level. The control of the instruments requires only one Ethernet network and no particular interfaces or drivers on the computers.

  12. Advanced beamline design for Fermilab's Advanced Superconducting Test Accelerator

    NASA Astrophysics Data System (ADS)

    Prokop, Christopher R.

    The Advanced Superconducting Test Accelerator (ASTA) at Fermilab is a new electron accelerator currently in the commissioning stage. In addition to testing superconducting accelerating cavities for future accelerators, it is foreseen to support a variety of Advanced Accelerator R&D (AARD) experiments. Producing the required electron bunches with the expected flexibility is challenging. The goal of this dissertation is to explore via numerical simulations new accelerator beamlines that can enable the advanced manipulation of electron bunches. The work especially includes the design of a low-energy bunch compressor and a study of transverse-to-longitudinal phase space exchangers.

  13. The electron spectroscopy for chemical analysis microscopy beamline data acquisition system at ELETTRA

    NASA Astrophysics Data System (ADS)

    Gariazzo, C.; Krempaska, R.; Morrison, G. R.

    1996-07-01

    The electron spectroscopy for chemical analysis (ESCA) microscopy data acquisition system enables the user to control the imaging and spectroscopy modes of operation of the beamline ESCA microscopy at ELETTRA. It allows the user to integrate all experiment, beamline and machine operations in one single environment. The system also provides simple data analysis for both spectra and images data to guide further data acquisition.

  14. Plastique: A synchrotron radiation beamline for time resolved fluorescence in the frequency domain

    NASA Astrophysics Data System (ADS)

    De Stasio, Gelsomina; Zema, N.; Antonangeli, F.; Savoia, A.; Parasassi, T.; Rosato, N.

    1991-06-01

    PLASTIQUE is the only synchrotron radiation beamline in the world that performs time resolved fluorescence experiments in frequency domain. These experiments are extremely valuable sources of information on the structure and dynamics of molecules. We describe the beamline and some initial data.

  15. Performance of IR-VUV normal incidence monochromator beamline at UVSOR

    NASA Astrophysics Data System (ADS)

    Fukui, K.; Miura, H.; Nakagawa, H.; Shimoyama, I.; Nakagawa, K.; Okamura, H.; Nanba, T.; Hasumoto, M.; Kinoshita, T.

    2001-07-01

    The beamline BL7B at the UVSOR facility for solid-state spectroscopy has been opening for users after reconstruction. This beamline consists of a 3 m normal incidence monochromator and covers the spectral range from the vacuum ultraviolet to the infrared region. The optical configuration and the performance, such as photon number, purity and resolving power, are reported.

  16. The performance of a cryogenically cooled monochromator for an in-vacuum undulator beamline.

    PubMed

    Zhang, Lin; Lee, Wah Keat; Wulff, Michael; Eybert, Laurent

    2003-07-01

    The channel-cut silicon monochromator on beamline ID09 at the European Synchrotron Radiation Facility is indirectly cooled from the sides by liquid nitrogen. The thermal slope error of the diffracting surface is calculated by finite-element analysis and the results are compared with experiments. The slope error is studied as a function of cooling coefficients, beam size, position of the footprint and power distribution. It is found that the slope error versus power curve can be divided into three regions: (i). The linear region: the thermal slope error is linearly proportional to the power. (ii). The transition region: the temperature of the Si crystal is close to 125 K; the thermal slope error is below the straight line extrapolated from the linear curve described above. (iii). The non-linear region: the temperature of the Si crystal is higher than 125 K and the thermal slope error increases much faster than the power. Heat-load tests were also performed and the measured rocking-curve widths are compared with those calculated by finite-element modeling. When the broadening from the intrinsic rocking-curve width and mounting strain are included, the calculated rocking-curve width versus heat load is in excellent agreement with experiment. PMID:12824931

  17. Performance of beamline 9.3.1 at the ALS: Flux and resolution measurements

    SciTech Connect

    Uehara, Y.; Fischer, G.; Kring, J.; Perera, R.C.C.

    1997-04-01

    Beamline 9.3.1 at the ALS is a windowless beamline, covering the 1-6 keV photon-energy range. This beamline is the first monochromatic hard x-ray beamline in the ALS, and designed to achieve the goals of high energy resolution, and preservation of the high brightness from the ALS. It consists of a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator and two toroidal mirrors which are positioned before and after the monochromator. The construction of the beamline was completed in December of 1995, with imperfect mirrors. In this report, the authors describe the experimental results of absolute flux measurements and x-ray absorption measurements of gases and solid samples using the present set of mirrors.

  18. The Protein Micro-Crystallography Beamlines for Targeted Protein Research Program

    NASA Astrophysics Data System (ADS)

    Hirata, Kunio; Yamamoto, Masaki; Matsugaki, Naohiro; Wakatsuki, Soichi

    In order to collect proper diffraction data from outstanding micro-crystals, a brand-new data collection system should be designed to provide high signal-to noise ratio in diffraction images. SPring-8 and KEK-PF are currently developing two micro-beam beamlines for Targeted Proteins Research Program by MEXT of Japan. The program aims to reveal the structure and function of proteins that are difficult to solve but have great importance in both academic research and industrial application. At SPring-8, a new 1-micron beam beamline for protein micro-crystallography, RIKEN Targeted Proteins Beamline (BL32XU), is developed. At KEK-PF a new low energy micro-beam beamline, BL-1A, is dedicated for SAD micro-crystallography. The two beamlines will start operation in the end of 2010. The present status of the research and development for protein micro-crystallography will be presented.

  19. Commissioning and first results of scanning type EXAFS beamline (BL-09) at INDUS-2 synchrotron source

    SciTech Connect

    Poswal, A. K. Agrawal, A. Yadav, A. K. Nayak, C. Basu, S. Bhattachryya, D.; Jha, S. N.; Sahoo, N. K.; Kane, S. R.; Garg, C. K.

    2014-04-24

    An Energy Scanning X-ray Absorption Fine Structure spectroscopy beamline has recently been installed and commissioned at BL-09 bending magnet port of INDUS-2 synchrotron source, Indore. The beamline uses an UHV compatible fixed exit double crystal monochromator (DCM) with two Si (111) crystals. Two grazing incidence cylindrical mirrors are also used in this beamline; the pre-mirror is used as a collimating mirror while the post mirror is used for vertical focusing and higher harmonic rejection. In this beamline it is possible to carry out EXAFS measurements both in transmission and fluorescence mode on various types of samples, using Ionization chamber detectors and solid state drift detector respectively. In this paper, results from first experiments of the Energy Scanning EXAFS beamline are presented.

  20. Design, Installation, and Initial Commissioning of the MTA Beamline

    SciTech Connect

    Moore, Craig; Anderson, John; Garcia, Fernanda; Gerardi, Michael; Johnstone, Carol; Kobilarcik, Thomas; Kucera, Michael; Kufer, Mathew; Newhart, Duane; Rakhno, Igor; Vogel, Gregory; /Fermilab

    2010-05-01

    A new experimental area designed to develop, test and verify muon ionization cooling apparatus using the 400-MeV Fermilab Linac proton beam has been fully installed and is presently being commissioned. Initially, this area was used for cryogenic tests of liquid-hydrogen absorbers for the MUCOOL R&D program and, now, for high-power beam tests of absorbers, high-gradient rf cavities in the presence of magnetic fields (including gas-filled cavities), and other prototype muon-cooling apparatus. The experimental scenarios being developed for muon facilities involve collection, capture, and cooling of large-emittance, high-intensity muon beams--{approx}10{sup 13} muons, so that conclusive tests of the apparatus require full Linac beam, which is 1.6 x 10{sup 13} p/pulse. To support the muon cooling facility, this new primary beamline extracts and transports beam directly from the Linac to the test facility. The design concept for the MuCool facility is taken from an earlier proposal [1], but modifications were necessary to accommodate high-intensity beam, cryogenics, and the increased scale of the cooling experiments. Further, the line incorporates a specialized section and utilizes a different mode of operation to provide precision measurements of Linac beam parameters. This paper reports on the technical details of the MuCool beamline for both modes.

  1. NSLS transvenous coronary angiography beamline upgrade and advanced technology initiatives

    NASA Astrophysics Data System (ADS)

    Gmür, N. F.; Chapman, D.; Thomlinson, W.; Thompson, A. C.; Lavender, W. M.; Scalia, K.; Malloy, N.; Mangano, J.; Jacob, J.

    1995-02-01

    Since October 1990, the coronary anatomies of a total of 16 patients (male and female) have been imaged at the National Synchrotron Light Source (NSLS) as part of the Dual Energy Digital Subtraction Transvenous Coronary Angiography research program. This program takes place in the Synchrotron Medical Research Facility (SMERF) on the X17B2 wiggler beamline. Encouraged by the success of the initial patient images, the NSLS has recently embarked on an ambitious upgrade effort. This effort covers all aspects of the X17B2 beamline and includes improved radiation shielding, a Laue monochromator assembly, a computer-controlled five motion patient scanning chair assembly, a fast low-noise image acquisition system, and a modularized patient safety system. These improvements will allow major advances in imaging patients based on ECG signal gating and multiple view imaging. Two advanced technology initiatives are underway with industrial collaborators. One will develop real-time image acquisition and display of the subtracted digital images. The second will develop a compact x-ray source of medical imaging. The source will be a linear electron accelerator creating characteristic radiation line emissions.

  2. Microfocusing at the PG1 beamline at FLASH

    DOE PAGES

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rubhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Gunter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines andmore » limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Lastly, aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented.« less

  3. Microfocusing at the PG1 beamline at FLASH

    SciTech Connect

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rubhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Gunter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Lastly, aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented.

  4. Dedicated Beamline Facilities for Catalytic Research. Synchrotron Catalysis Consortium (SCC)

    SciTech Connect

    Chen, Jingguang; Frenkel, Anatoly; Rodriguez, Jose; Adzic, Radoslav; Bare, Simon R.; Hulbert, Steve L.; Karim, Ayman; Mullins, David R.; Overbury, Steve

    2015-03-04

    Synchrotron spectroscopies offer unique advantages over conventional techniques, including higher detection sensitivity and molecular specificity, faster detection rate, and more in-depth information regarding the structural, electronic and catalytic properties under in-situ reaction conditions. Despite these advantages, synchrotron techniques are often underutilized or unexplored by the catalysis community due to various perceived and real barriers, which will be addressed in the current proposal. Since its establishment in 2005, the Synchrotron Catalysis Consortium (SCC) has coordinated significant efforts to promote the utilization of cutting-edge catalytic research under in-situ conditions. The purpose of the current renewal proposal is aimed to provide assistance, and to develop new sciences/techniques, for the catalysis community through the following concerted efforts: Coordinating the implementation of a suite of beamlines for catalysis studies at the new NSLS-II synchrotron source; Providing assistance and coordination for catalysis users at an SSRL catalysis beamline during the initial period of NSLS to NSLS II transition; Designing in-situ reactors for a variety of catalytic and electrocatalytic studies; Assisting experimental set-up and data analysis by a dedicated research scientist; Offering training courses and help sessions by the PIs and co-PIs.

  5. NSLS transvenous coronary angiography beamline upgrade and advanced technology initiatives

    SciTech Connect

    Gmuer, N.F.; Chapman, D.; Thomlinson, W.; Thompson, A.C.; Lavender, W.M.; Scalia, K.; Malloy, N.; Mangano, J.; Jacob, J.

    1994-11-01

    Since October 1990, the coronary anatomies of a total of 16 patients (male and female) have been imaged at the National Synchrotron Light Source (NSLS) as part of the Dual Energy Digital Subtraction Transvenous Coronary Angiography research program. This program takes place in the Synchrotron Medical Research Facility (SMERF) on the X17B2 wiggler beamline. Encouraged by the success of the initial patient images, the NSLS has recently embarked on an ambitious upgrade effort. This effort covers all aspects of the X17B2 beamline and includes improved radiation shielding, a Laue monochromator assembly, a computer-controlled 5 motion patient scanning chair assembly, a fast low-noise image acquisition system, and a modularized patient safety system. These improvements will allow major advances in imaging patients based on ECG signal gating and multiple view imaging. Two advanced technology initiatives are underway with industrial collaborators. One will develop real-time image acquisition and display of the subtracted digital images. The second will develop a compact x-ray source for medical imaging. The source will be a linear electron accelerator creating characteristic radiation line emissions.

  6. The Diamond Beamline I13L for Imaging and Coherence

    SciTech Connect

    Rau, C.; Wagner, U.; Peach, A.; Singh, B.; Wilkin, G.; Jones, C.; Robinson, I. K.

    2010-06-23

    I13L is the first long beamline at Diamond dedicated to imaging and coherence. Two independent branches will operate in the energy range of 6-30 keV with spatial resolution on the micro- to nano-lengthscale. The Imaging branch is dedicated to imaging and tomography with In-line phase contrast and full-field microscopy on the micron to nano-length scale. Ultimate resolution will be achieved on the Coherence branch at I13L with imaging techniques in the reciprocal space. The experimental stations will be located about 250 m from the source, taking advantage of the coherence properties of the source. The beamline has some outstanding features such as the mini-beta layout of the storage ring's straight section. The optical layout is optimized for beam stability and high optical quality to preserve the coherent radiation. In the experimental stations several methods will be available, starting for the first user with in-line phase contrast imaging on the imaging branch and Coherent X-ray Diffraction (CXRD) on the coherence branch.

  7. Commissioning of the Spherical Grating Monochromator Soft X-ray Spectroscopy Beamline at the Canadian Light Source

    SciTech Connect

    Regier, T.; Paulsen, J.; Wright, G.; Coulthard, I.; Tan, K.; Blyth, R. I. R.; Sham, T. K.

    2007-01-19

    The Spherical Grating Monochromator (SGM) is a Dragon type soft x-ray beamline designed to provide users at the Canadian Light Source (CLS) with monochromatic photons with energies between 250 and 2000 eV. Commissioning of the beamline began in the spring of 2005 and is expected to be completed in July 2006. Aspects of the commissioning process included the use of an object oriented approach to developing the beamline controls, the employment of a beam based alignment procedure and a large amount of user involvement. A description of the beamline and the commissioning techniques used is presented, along with examples of the beamline performance and capabilities.

  8. MX1: a bending-magnet crystallography beamline serving both chemical and macromolecular crystallography communities at the Australian Synchrotron

    PubMed Central

    Cowieson, Nathan Philip; Aragao, David; Clift, Mark; Ericsson, Daniel J.; Gee, Christine; Harrop, Stephen J.; Mudie, Nathan; Panjikar, Santosh; Price, Jason R.; Riboldi-Tunnicliffe, Alan; Williamson, Rachel; Caradoc-Davies, Tom

    2015-01-01

    MX1 is a bending-magnet crystallography beamline at the 3 GeV Australian Synchrotron. The beamline delivers hard X-rays in the energy range from 8 to 18 keV to a focal spot at the sample position of 120 µm FWHM. The beamline endstation and ancillary equipment facilitate local and remote access for both chemical and biological macromolecular crystallography. Here, the design of the beamline and endstation are discussed. The beamline has enjoyed a full user program for the last seven years and scientific highlights from the user program are also presented. PMID:25537608

  9. MX1: a bending-magnet crystallography beamline serving both chemical and macromolecular crystallography communities at the Australian Synchrotron.

    PubMed

    Cowieson, Nathan Philip; Aragao, David; Clift, Mark; Ericsson, Daniel J; Gee, Christine; Harrop, Stephen J; Mudie, Nathan; Panjikar, Santosh; Price, Jason R; Riboldi-Tunnicliffe, Alan; Williamson, Rachel; Caradoc-Davies, Tom

    2015-01-01

    MX1 is a bending-magnet crystallography beamline at the 3 GeV Australian Synchrotron. The beamline delivers hard X-rays in the energy range from 8 to 18 keV to a focal spot at the sample position of 120 µm FWHM. The beamline endstation and ancillary equipment facilitate local and remote access for both chemical and biological macromolecular crystallography. Here, the design of the beamline and endstation are discussed. The beamline has enjoyed a full user program for the last seven years and scientific highlights from the user program are also presented.

  10. Shielding Design Aspects of SR Beamlines for 3-GeV And 8-GeV Class Synchrotron Radiation Facilities

    SciTech Connect

    Asano, Yoshihiro; Liu, James C.; Rokni, Sayed; /SLAC

    2007-09-24

    Differences in synchrotron radiation beamline shielding design between the facilities of 3 GeV class and 8 GeV class are discussed with regard to SLAC SSRL and SPring-8 beamlines. Requirements of beamline shielding as well as the accelerator shielding depend on the stored electron energy, and here some factors in beamline shielding depending on the stored energy in particular, are clarified, namely the effect of build up, the effect of double scattering of photons at branch beamlines, and the spread of gas bremsstrahlung.

  11. Undulator beamline of the Brockhouse sector at the Canadian Light Source

    SciTech Connect

    Diaz, B. E-mail: skycia@uoguelph.ca; Gomez, A.; Duffy, A.; Hallin, E.; Meyer, B.; Kycia, S. E-mail: skycia@uoguelph.ca

    2014-08-15

    The Brockhouse project at the Canadian Light Source plans the construction of three beamlines, two wiggler beamlines, and one undulator beamline, that will be dedicated to x-ray diffraction and scattering. In this work, we will describe the undulator beamline main components and performance parameters, obtained from ray tracing using XOP-SHADOW codes. The undulator beamline will operate from 4.95 to 21 keV, using a 20 mm period hybrid undulator placed upstream of the wiggler in the same straight section. The beamline optics design was developed in cooperation with the Brazilian Synchrotron - LNLS. The beamline will have a double crystal monochromator with the options of Si(111) or Si(311) crystal pairs followed by two mirrors in the KB configuration to focus the beam at the sample position. The high brilliance of the undulator source will produce a very high flux of ∼10{sup 13} photons/s and high energy resolution into a small focus of 170 μm horizontal and 20-60 μm vertical, depending on the optical configuration and energy chosen. Two multi-axis goniometer experimental stations with area detectors and analyzers are foreseen to enable diffraction, resonant and inelastic scattering experiments, and SAXS/WAXS experiments with high resolution and time resolving capabilities.

  12. The ID23-1 structural biology beamline at the ESRF.

    PubMed

    Nurizzo, Didier; Mairs, Trevor; Guijarro, Matias; Rey, Vicente; Meyer, Jens; Fajardo, Pablo; Chavanne, Joel; Biasci, Jean Claude; McSweeney, Sean; Mitchell, Edward

    2006-05-01

    The demand for access to macromolecular crystallography synchrotron beam time continues to increase. To meet this demand the ESRF has constructed a dual station beamline using a canted undulator system as the X-ray source. The first phase of the beamline to be constructed is ID23-1, a tunable MAD-capable station with a mini-focus X-ray beam. The beamline makes use of well characterized optical elements: a channel-cut monochromator with a high-precision toroidal mirror to focus the X-ray beam. The beamline has been conceived with the aim of providing high levels of automation to create an industrial-like environment for protein crystallography. A new software suite has been developed to permit reliable easy operation for the beamline users and beamline staff. High levels of diagnostics are built in to allow rapid trouble-shooting. These developments are now being exported to the ESRF macromolecular crystallography beamline complex and have been made in a modular fashion to facilitate transportability to other synchrotrons.

  13. The ELIMED transport and dosimetry beamline for laser-driven ion beams

    NASA Astrophysics Data System (ADS)

    Romano, F.; Schillaci, F.; Cirrone, G. A. P.; Cuttone, G.; Scuderi, V.; Allegra, L.; Amato, A.; Amico, A.; Candiano, G.; De Luca, G.; Gallo, G.; Giordanengo, S.; Guarachi, L. Fanola; Korn, G.; Larosa, G.; Leanza, R.; Manna, R.; Marchese, V.; Marchetto, F.; Margarone, D.; Milluzzo, G.; Petringa, G.; Pipek, J.; Pulvirenti, S.; Rizzo, D.; Sacchi, R.; Salamone, S.; Sedita, M.; Vignati, A.

    2016-09-01

    A growing interest of the scientific community towards multidisciplinary applications of laser-driven beams has led to the development of several projects aiming to demonstrate the possible use of these beams for therapeutic purposes. Nevertheless, laser-accelerated particles differ from the conventional beams typically used for multiscipilinary and medical applications, due to the wide energy spread, the angular divergence and the extremely intense pulses. The peculiarities of optically accelerated beams led to develop new strategies and advanced techniques for transport, diagnostics and dosimetry of the accelerated particles. In this framework, the realization of the ELIMED (ELI-Beamlines MEDical and multidisciplinary applications) beamline, developed by INFN-LNS (Catania, Italy) and that will be installed in 2017 as a part of the ELIMAIA beamline at the ELI-Beamlines (Extreme Light Infrastructure Beamlines) facility in Prague, has the aim to investigate the feasibility of using laser-driven ion beams for multidisciplinary applications. In this contribution, an overview of the beamline along with a detailed description of the main transport elements as well as the detectors composing the final section of the beamline will be presented.

  14. Target for the NuMI Neutrino Beam-line

    NASA Astrophysics Data System (ADS)

    Hylen, James

    1998-04-01

    The NUMI beam-line which will be built at Fermi National Accelerator Laboratory will produce a neutrino beam by striking a target with a 120 GeV proton beam, collecting the produced π^+ with a magnetic focusing system, and letting the pions decay as they travel down an evacuated pipe. The target must be able to withstand the projected beam intensity of 4x10^13 protons per 1 millisecond beam spill, with a repetition rate of 1.9 seconds. A long, thin, relatively low density target is the most efficient configuration for the neutrino beam line, as the required high energy pions can exit the sides of the target before re-interacting. The proton beam spot size will be of order 1 mm RMS. Graphite and Beryllium are being evaluated as potential target materials.

  15. The Optical Design of the PEP-II Injection Beamlines

    SciTech Connect

    Fieguth, Ted

    2003-05-23

    The optical design of the PEP-II electron and positron Injection Beamlines is described. Use of the existing high power, low emittance beams available from the SLC damping rings require that pulsed extraction of 9.0 GeV electrons and 3.1 GeV positrons for injection into the PEP-II rings occur in the early sectors of the accelerator. More than 5 kilometers of new beam transport lines have been designed and are being constructed to bring these beams to their respective rings. The optical design maximizes the tolerance to errors especially to those contributing to beam size and position jitter. Secondly, the design minimizes costs by utilizing existing components or component designs and minimizing the number required. Here we discuss important attributes including choice of lattice, specification of error tolerances, including errors in construction, alignment, field errors, power supply stability, and orbit correction.

  16. Development of a Niobium Bellow for Beamline Connections

    SciTech Connect

    Larry Turlington; John Brawley; Robert Manus; Stephen Manning; Samuel Morgan; Gary Slack; Peter Kneisel

    2003-09-01

    Superconducting cavities in an accelerator assembly are usually connected at the beampipes by stainless steel bellows. They operate at an intermediate temperature, compensating for alignment tolerances on the cavity beamlines and for thermal contraction during cooldown to cryogenic temperatures. This transition from one cavity to the next in a cavity string is typically of the order of 3/2 wavelength along with approximately half a wavelength taken up by the bellows. If one could incorporate a niobium bellows in the beam pipe, this distance could be reduced by half a wave length. In the case of a big accelerator such as TESLA the overall cavity length for the accelerator could be reduced by roughly 10% or 2000 m. In terms of cost savings this would amount to several million dollars. Based on this estimate we have begun to develop a niobium bellows to be used on a 2.75 inch diameter beamline. It is made from 0.3 mm thick niobium sheet, rolled into a tube and secured by a longitudinal full penetration electron beam weld; the weld is made with a high speed a narrow, focused beam reducing the heat affected zone, thus limiting the grain growth, which could affect the formability. Subsequently, two convolutions have been pressed into this tube in a 2-stage process, using an external die and a polyurethane internal expander. Niobium cuffs and flanges were electron beam welded to the formed bellows, which facilitated leak testing and allowed some measurements of compression/expansion and bending. In this contribution the fabrication process and the subsequent mechanical and vacuum tests with the bellows will be described.

  17. Microfocusing at the PG1 beamline at FLASH

    PubMed Central

    Dziarzhytski, Siarhei; Gerasimova, Natalia; Goderich, Rene; Mey, Tobias; Reininger, Ruben; Rübhausen, Michael; Siewert, Frank; Weigelt, Holger; Brenner, Günter

    2016-01-01

    The Kirkpatrick–Baez (KB) refocusing mirror system installed at the PG1 branch of the plane-grating monochromator beamline at the soft X-ray/XUV free-electron laser in Hamburg (FLASH) is designed to provide tight aberration-free focusing down to 4 µm × 6 µm full width at half-maximum (FWHM) on the sample. Such a focal spot size is mandatory to achieve ultimate resolution and to guarantee best performance of the vacuum-ultraviolet (VUV) off-axis parabolic double-monochromator Raman spectrometer permanently installed at the PG1 beamline as an experimental end-station. The vertical beam size on the sample of the Raman spectrometer, which operates without entrance slit, defines and limits the energy resolution of the instrument which has an unprecedented design value of 2 meV for photon energies below 70 eV and about 15 meV for higher energies up to 200 eV. In order to reach the designed focal spot size of 4 µm FWHM (vertically) and to hold the highest spectrometer resolution, special fully motorized in-vacuum manipulators for the KB mirror holders have been developed and the optics have been aligned employing wavefront-sensing techniques as well as ablative imprints analysis. Aberrations like astigmatism were minimized. In this article the design and layout of the KB mirror manipulators, the alignment procedure as well as microfocus optimization results are presented. PMID:26698054

  18. First results from the high-brightness x-ray spectroscopy beamline at ALS

    SciTech Connect

    Perera, R.C.C.; Ng, W.; Jones, G.

    1997-04-01

    Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goal of high brightness at the sample for use in the X-ray Atomic and Molecular Spectroscopy (XAMS) science, surface and interface science, biology and x-ray optical development programs at ALS. X-ray absorption and time of flight photo emission measurements in 2 - 5 keV photon energy in argon along with the flux, resolution, spot size and stability of the beamline will be discussed. Prospects for future XAMS measurements will also be presented.

  19. Design Concept and Performance of the Soft X-ray Beamline HiSOR-BL14

    SciTech Connect

    Sawada, M.; Namatame, H.; Yaji, K.; Nagira, M.; Kimura, A.; Taniguchi, M.

    2007-01-19

    The soft X-ray beamline HiSOR-BL14 has been constructed at Hiroshima Synchrotron Radiation Center, aimed at absorption spectroscopy and photoelectron spectroscopy with linearly and circularly polarized light. The beamline layout is based on a Dragon-type design with a spherical grating monochromator. The beamline is able to accept synchrotron radiation from the bending magnet part of the HiSOR ring with a wide solid angle. The large horizontal angular acceptance and vertical one contribute to high photon flux and controllability of light polarization, respectively. Our performance test indicates that high resolving power has been achieved with sufficient photon flux to carry out spectroscopic experiments.

  20. Imaging in real and reciprocal space at the Diamond beamline I13

    NASA Astrophysics Data System (ADS)

    Rau, C.; Wagner, U. H.; Vila-Comamala, J.; Bodey, A.; Parson, A.; García-Fernández, M.; De Fanis, A.; Pešić, Z.

    2016-01-01

    The Diamond Imaging and Coherence beamline I13 consists of two independent branchlines for imaging in real and reciprocal space. Different microscopies are available providing a range of spatial resolution from 5µm to potentially 5nm. The beamline operates in the energy range of 6-35keV covering different scientific areas such as biomedicine, materials science and geophysics. Several original devices have been developed at the beamline, such as the EXCALIBUR photon counting detector and the combined robot arms for coherent X-ray diffraction.

  1. Beamline stability measurements with a stretched wire system in the FFTB

    SciTech Connect

    Assmann, R.; Salsberg, C.; Montag, C.

    1996-09-01

    Beamline stability is of great importance for future linear colliders where tolerances generally are in the micron to sub-micron range. A stretched wire system in the sealed FFTB tunnel at SLAC was used to monitor beamline motion with a sub-micron resolution. In future linear colliders low frequency changes of the beamline alignment (< 0.1 Hz) lead to untolerable quasistatical misalignments and betatron oscillations. Since it requires time to correct those errors, it is very important to determine how often corrections are needed. The authors present the measurements, discuss the systematics of the stretched wire system and compare the observations with the ATL-model for ground motion.

  2. Characterization of the new NSLS infrared microspectroscopy beamline U10B

    SciTech Connect

    Carr, G.L.

    1999-07-19

    The first of several new infrared beamlines, built on a modified bending magnet port of the NSLS VUV ring, is now operational for mid-infrared microspectroscopy. The port simultaneously delivers 40 mrad by 40 mrad to two separate beamlines and spectrometer endstations designated U10A and U10B. The latter is equipped with a scanning infrared microspectrometer. The combination of this instrument and high brightness synchrotron radiation makes diffraction-limited microspectroscopy practical. This paper describes the beamline's performance and presents quantitative information on the diffraction-limited resolution.

  3. CHARACTERIZATION OF THE NEW NSLS INFARED MICROSPECTROSCOPY BEAMLINE U10B.

    SciTech Connect

    CARR,G.L.

    1999-07-19

    The first of several new infrared beamlines, built on a modified bending magnet port of the NSLS VUV ring, is now operational for mid-infrared microspectroscopy. The port simultaneously delivers 40 mrad by 40 mrad to two separate beamlines and spectrometer endstations designated U10A and U10B. The latter is equipped with a scanning infrared microspectrometer. The combination of this instrument and high brightness synchrotron radiation makes diffraction-limited microspectroscopy practical. This paper describes the beamline's performance and presents quantitative information on the diffraction-limited resolution.

  4. Progress of projection computed tomography by upgrading of the beamline 37XU of SPring-8

    NASA Astrophysics Data System (ADS)

    Terada, Yasuko; Suzuki, Yoshio; Uesugi, Kentaro; Miura, Keiko

    2016-01-01

    Beamline 37XU at SPring-8 has been upgraded for nano-focusing applications. The length of the beamline has been extended to 80 m. By utilizing this length, the beamline has advantages for experiments such as X-ray focusing, X-ray microscopic imaging and X-ray computed tomography. Projection computed tomography measurements were carried out at experimental hutch 3 located 80 m from the light source. CT images of a microcapsule have been successfully obtained with a wide X-ray energy range.

  5. Recent Major Improvements to the ALS Sector 5 MacromolecularCrystallography Beamlines

    SciTech Connect

    Morton, Simon A.; Glossinger, James; Smith-Baumann, Alexis; McKean, John P.; Trame, Christine; Dickert, Jeff; Rozales, Anthony; Dauz,Azer; Taylor, John; Zwart, Petrus; Duarte, Robert; Padmore, Howard; McDermott, Gerry; Adams, Paul

    2007-07-01

    Although the Advanced Light Source (ALS) was initially conceived primarily as a low energy (1.9GeV) 3rd generation source of VUV and soft x-ray radiation it was realized very early in the development of the facility that a multipole wiggler source coupled with high quality, (brightness preserving), optics would result in a beamline whose performance across the optimal energy range (5-15keV) for macromolecular crystallography (MX) would be comparable to, or even exceed, that of many existing crystallography beamlines at higher energy facilities. Hence, starting in 1996, a suite of three beamlines, branching off a single wiggler source, was constructed, which together formed the ALS Macromolecular Crystallography Facility. From the outset this facility was designed to cater equally to the needs of both academic and industrial users with a heavy emphasis placed on the development and introduction of high throughput crystallographic tools, techniques, and facilities--such as large area CCD detectors, robotic sample handling and automounting facilities, a service crystallography program, and a tightly integrated, centralized, and highly automated beamline control environment for users. This facility was immediately successful, with the primary Multiwavelength Anomalous Diffraction beamline (5.0.2) in particular rapidly becoming one of the foremost crystallographic facilities in the US--responsible for structures such as the 70S ribosome. This success in-turn triggered enormous growth of the ALS macromolecular crystallography community and spurred the development of five additional ALS MX beamlines all utilizing the newly developed superconducting bending magnets ('superbends') as sources. However in the years since the original Sector 5.0 beamlines were built the performance demands of macromolecular crystallography users have become ever more exacting; with growing emphasis placed on studying larger complexes, more difficult structures, weakly diffracting or smaller

  6. Welding III.

    ERIC Educational Resources Information Center

    Allegheny County Community Coll., Pittsburgh, PA.

    Instructional objectives and performance requirements are outlined in this course guide for Welding III, an advanced course in arc welding offered at the Community College of Allegheny County to provide students with the proficiency necessary for industrial certification. The course objectives, which are outlined first, specify that students will…

  7. Safety Analysis Report: X17B2 beamline Synchrotron Medical Research Facility

    SciTech Connect

    Gmuer, N.F.; Thomlinson, W.

    1990-02-01

    This report contains a safety analysis for the X17B2 beamline synchrotron medical research facility. Health hazards, risk assessment and building systems are discussed. Reference is made to transvenous coronary angiography. (LSP)

  8. Measurements from a Compact Cost-Effective Beamline for the THC14 PET Cyclotron

    SciTech Connect

    Dehnel, M. P.; Theroux, J.; Christensen, T.; Stewart, T. M.; Roeder, M.; Sirot, P.; Fasse, D.; Brasile, J. P.; Raoult, F.; Buckley, K.

    2009-03-10

    The THC14 PET Cyclotron produced by THALES specifies two compact cost-effective beamlines for high current PET radioisotope production. The design and development of the beamline system was reported previously in NIM B 261 (2007) pp 809-812. This paper describes the successful testing of this compact beamline at the first installation. A series of measurement data are presented starting from low current scintillator image data, higher current beam diagnostic data (baffles, collimators, targets) and finally a simultaneous dual beam run on Faraday Cups. The beamline system has proven to be a flexible and valuable tool for optimizing high current beam intensity distribution on target in a well-instrumented manner. This ability to tailor the beam characteristics for the target is particularly important as high power targets are developed which can handle very high beam currents.

  9. New Soft X-ray Beamline (BL10) at the SAGA Light Source

    SciTech Connect

    Yoshimura, D.; Setoyama, H.; Okajima, T.

    2010-06-23

    A new soft X-ray beamline (BL10) at the SAGA Light Source (SAGA-LS) was constructed at the end of 2008. Commissioning of this new beamline started at the beginning of 2009. Synchrotron radiation from a variably polarizing undulator (APPLE-II) can be used in this beamline. The obtained light is monochromatized by a varied-line-spacing plane grating monochromator with the variable included angle mechanism. Its designed resolving power and photon flux are 3,000-10,000 and 10{sup 12}-10{sup 9} photons/s at 300 mA, respectively. The performance test results were generally satisfactory. An overview of the optical design of the beamline and the current status of commissioning are reported.

  10. Upgrades to the XAFS2 beamline control system and to the endstation at the LNLS

    NASA Astrophysics Data System (ADS)

    Figueroa, S. J. A.; Mauricio, J. C.; Murari, J.; Beniz, D. B.; Piton, J. R.; Slepicka, H. H.; Falcão de Sousa, M.; Espíndola, A. M.; Levinsky, A. P. S.

    2016-05-01

    The XAFS2 is a general-purpose X-ray absorption beamline. It is the second one built at the LNLS. After approximately 7 years in operation this beamline has been substantially updated in order to improve its experimental possibilities. Recently arrived, a 4-circle Huber diffractometer has been incorporated to perform combined experiments. This collects XRD patterns with the XAFS. Through the development of a new sampling environment it is now also possible to perform these measurements in situ/operando conditions. Other upgrades include a complete remodelling of the beamline software and its control system. The following new systems are crucial for the next steps that are currently underway at the beamline, namely, (i) enabling remote access for users and (ii) the testing of QEXAFS measurements.

  11. Wiggler-base Hard X-ray Spectroscopy Beamline at CLS

    SciTech Connect

    Jiang, D. T.; Chen, N.; Sheng, W.

    2007-01-19

    The CLS 06ID-1 Hard X-ray Micro-Analysis Beamline (HXMA) is a general purpose hard X-ray spectroscopy beamline (5 to 40 keV) designed to serve users in XAFS, diffraction and microprobe communities. The beamline uses the synchrotron radiation from a superconducting wiggler. The primary beamline optics include a 1.2 m water-cooled silicon collimating mirror (separate Rh and Pt coating stripes), a liquid nitrogen cooled double crystal monochromator (Kohzu CMJ-1) housing two crystal pairs (Si 111 and 220), and a 1.15 m long water-cooled silicon toroidal focusing mirror (separate Rh and Pt coating stripes). All mirrors are equipped with dynamical meridian benders. The experimental hutch hosts three experimental setups for XAFS, diffraction and microprobe, respectively. Primary design considerations and some commissioning results are discussed.

  12. Development of soft X-ray polarized light beamline on Indus-2 synchrotron radiation source

    SciTech Connect

    Phase, D. M. Gupta, Mukul Potdar, S. Behera, L. Sah, R. Gupta, Ajay

    2014-04-24

    This article describes the development of a soft x-ray beamline on a bending magnet source of Indus-2 storage ring (2.5 GeV) and some preliminary results of x-ray absorption spectroscopy (XAS) measurements using the same. The beamline layout is based on a spherical grating monochromator. The beamline is able to accept synchrotron radiation from the bending magnet port BL-1 of the Indus-2 ring with a wide solid angle. The large horizontal and vertical angular acceptance contributes to high photon flux and selective polarization respectively. The complete beamline is tested for ultrahigh vacuum (UHV) ∼ 10{sup −10} mbar. First absorption spectrum was obtained on HOPG graphite foil. Our performance test indicates that modest resolving power has been achieved with adequate photon flux to carry out various absorption experiments.

  13. Transverse to longitudinal emittance exchange beamline at the A0 photoinjector.

    SciTech Connect

    Fililler, R. P.; Edwards, D. A.; Koeth, T.; Harkay, K. C.; Kim, K.-J.; Edwards, H. T.; Accelerator Systems Division; Fermilab; Rutgers Univ.

    2007-08-01

    The FNAL A0 Photoinjector is being reconfigured to test the principal of transverse to longitudinal emittance exchange as proposed by Cornacchia and Emma, Kim and Sessler, and others. The ability to perform such an exchange could have major advantages to FELs by reducing the transverse emittance. Several schemes to carry out the exchange are possible and will be reported separately. At the Fermilab A0 Photoinjector we are constructing a beamline to demonstrate this transverse to longitudinal emittance exchange. This beamline will consist of a dogleg, a TM{sub 110} 5 cell copper cavity, and another dogleg. The beamline is designed to reuse the bunch compressor dipoles of the photoinjector, along with some existing diagnostics. Beamline layout and simulations are presented. Emittance dilution effects are also discussed.

  14. The beamline for the second axis of the dual axis radiographic hydrodynamic test facility

    SciTech Connect

    Caporaso, G J; Chen, Y J; Fawley, W M; Lee, E P; Paul, A C; Westenkow, G

    1999-03-23

    During normal DARHT II operation, the beam exiting the accelerator will be well characterized by its nominal design parameters of 20-MeV, 2000-Amperes, 2-{micro}sec-pulse length, and 3 cm-mr unnormalized emittance. Normal operation will have the beam delivered to a beam dump via several DC magnets. A 2-way kicker magnet is used to deflect portions of the beam into the straight ahead beamline leading to either a diagnostic beamline or to the converter target beamline. During start up and or beam development periods, the beam exiting the accelerator may have parameters outside the acceptable range of values for normal operation. The Enge beamline must accommodate this range of unacceptable beam parameters, delivering the entire 80 KiloJoule of beam to the dump even though the energy, emittance, and/or match is outside the nominal design range.

  15. High-throughput Toroidal Grating Beamline for Photoelectron Spectroscopy at CAMD

    PubMed Central

    Kizilkaya, O; Jiles, R W; Patterson, M C; Thibodeaux, C A; Poliakoff, E D; Sprunger, P T; Kurtz, R L; Morikawa, E

    2016-01-01

    A 5 meter toroidal grating (5m-TGM) beamline has been commissioned to deliver 28 mrad of bending magnet radiation to an ultrahigh vacuum endstation chamber to facilitate angle resolved photoelectron spectroscopy. The 5m-TGM beamline is equipped with Au-coated gratings with 300, 600 and 1200 lines/mm providing monochromatized synchrotron radiation in the energy ranges 25-70 eV, 50–120 eV and 100–240 eV, respectively. The beamline delivers excellent flux (~1014-1017 photons/sec/100mA) and a combined energy resolution of 189 meV for the beamline (at 1.0 mm slit opening) and HA-50 hemispherical analyzer was obtained at the Fermi level of polycrystalline gold crystal. Our preliminary photoelectron spectroscopy results of phenol adsorption on TiO2 (110) surface reveals the metal ion (Ti) oxidation. PMID:27134636

  16. A microprobe-XRF Beamline on Indus-2 Synchrotron Light Source

    NASA Astrophysics Data System (ADS)

    Tiwari, M. K.; Kane, S. R.; Sinha, A. K.; Garg, C. K.; Singh, A. K.; Gupta, P.; Garg, S. R.; Lodha, G. S.; Deb, S. K.

    2013-03-01

    A microfocus x-ray fluorescence (XRF) beamline has been setup on Indus-2 synchrotron light source. The beamline works in the x-ray energy range of 4-20 keV. The optics of the beamline comprises of a Si(111) double crystal monochromator for energy tunability and a Kirkpatrick-Baez (KB) based grazing incidence focusing optics. Microprobe XRF scanning over a region of the sample is possible using a 5-axis sample scanning stage. The beamline provides an energy resolution ~ 10-3 -10-4 with a photon flux density of the order of ~ 108 ph/sec./mm2/100mA for the collimated unfocused beam. Measured performance, various attractive features and some initial commissioning results are presented.

  17. New soft X-ray beamline BL07LSU at SPring-8

    PubMed Central

    Yamamoto, Susumu; Senba, Yasunori; Tanaka, Takashi; Ohashi, Haruhiko; Hirono, Toko; Kimura, Hiroaki; Fujisawa, Masami; Miyawaki, Jun; Harasawa, Ayumi; Seike, Takamitsu; Takahashi, Sunao; Nariyama, Nobuteru; Matsushita, Tomohiro; Takeuchi, Masao; Ohata, Toru; Furukawa, Yukito; Takeshita, Kunikazu; Goto, Shunji; Harada, Yoshihisa; Shin, Shik; Kitamura, Hideo; Kakizaki, Akito; Oshima, Masaharu; Matsuda, Iwao

    2014-01-01

    A new soft X-ray beamline, BL07LSU, has been constructed at SPring-8 to perform advanced soft X-ray spectroscopy for materials science. The beamline is designed to achieve high energy resolution (E/ΔE> 10000) and high photon flux [>1012 photons s−1 (0.01% bandwidth)−1] in the photon energy range 250–2000 eV with controllable polarization. To realise this state-of-the-art performance, a novel segmented cross undulator was developed and adopted as a light source. The details of the undulator light source and beamline monochromator design are described. The achieved performance of the beamline, such as the photon flux, energy resolution and the state of polarization, is reported. PMID:24562556

  18. The electron spectro-microscopy beamline at National Synchrotron Light Source II: A wide photon energy range, micro-focusing beamline for photoelectron spectro-microscopies

    SciTech Connect

    Reininger, R.; Hulbert, S. L.; Chubar, O.; Vescovo, E.; Johnson, P. D.; Valla, T.; Sadowski, J. T.; Starr, D. E.

    2012-02-15

    A comprehensive optical design for a high-resolution, high-flux, wide-energy range, micro-focused beamline working in the vacuum ultraviolet and soft x-ray photon energy range is proposed. The beamline is to provide monochromatic radiation to three photoelectron microscopes: a full-field x-ray photoelectron emission microscope and two scanning instruments, one dedicated to angle resolved photoemission spectroscopy ({mu}-ARPES) and one for ambient pressure x-ray photoelectron spectroscopy and scanning photoelectron microscopy (AP-XPS/SPEM). Microfocusing is achieved with state of the art elliptical cylinders, obtaining a spot size of 1 {mu}m for ARPES and 0.5 {mu}m for AP-XPS/SPEM. A detailed ray tracing analysis quantitatively evaluates the overall beamline performances.

  19. A modified post damping ring bunch compressor beamline for the TESLA linear collider

    SciTech Connect

    Philippe R.-G. Piot; Winfried Decking

    2004-03-23

    We propose a modified bunch compressor beamline, downstream of the damping ring, for the TESLA linear collider. This modified beamline uses a third harmonic radio-frequency section based on the 3.9 GHz superconducting cavity under development at Fermilab. In our design the beam deceleration is about {approx}50 MeV instead of {approx}450 MeV in the original design proposed.

  20. Fundamental neutron physics beamline at the spallation neutron source at ORNL

    DOE PAGES

    Fomin, N.; Greene, G. L.; Allen, R. R.; Cianciolo, V.; Crawford, C.; Tito, T. M.; Huffman, P. R.; Iverson, E. B.; Mahurin, R.; Snow, W. M.

    2014-11-04

    In this paper, we describe the Fundamental Neutron Physics Beamline (FnPB) facility located at the Spallation Neutron Source at Oak Ridge National Laboratory. The FnPB was designed for the conduct of experiments that investigate scientific issues in nuclear physics, particle physics, astrophysics and cosmology using a pulsed slow neutron beam. Finally, we present a detailed description of the design philosophy, beamline components, and measured fluxes of the polychromatic and monochromatic beams.

  1. The Low Density Matter (LDM) beamline at FERMI: optical layout and first commissioning

    PubMed Central

    Svetina, Cristian; Grazioli, Cesare; Mahne, Nicola; Raimondi, Lorenzo; Fava, Claudio; Zangrando, Marco; Gerusina, Simone; Alagia, Michele; Avaldi, Lorenzo; Cautero, Giuseppe; de Simone, Monica; Devetta, Michele; Di Fraia, Michele; Drabbels, Marcel; Feyer, Vitaliy; Finetti, Paola; Katzy, Raphael; Kivimäki, Antti; Lyamayev, Viktor; Mazza, Tommaso; Moise, Angelica; Möller, Thomas; O’Keeffe, Patrick; Ovcharenko, Yevheniy; Piseri, Paolo; Plekan, Oksana; Prince, Kevin C.; Sergo, Rudi; Stienkemeier, Frank; Stranges, Stefano; Coreno, Marcello; Callegari, Carlo

    2015-01-01

    The Low Density Matter (LDM) beamline has been built as part of the FERMI free-electron laser (FEL) facility to serve the atomic, molecular and cluster physics community. After the commissioning phase, it received the first external users at the end of 2012. The design and characterization of the LDM photon transport system is described, detailing the optical components of the beamline. PMID:25931066

  2. MxCuBE: a synchrotron beamline control environment customized for macromolecular crystallography experiments.

    PubMed

    Gabadinho, José; Beteva, Antonia; Guijarro, Matias; Rey-Bakaikoa, Vicente; Spruce, Darren; Bowler, Matthew W; Brockhauser, Sandor; Flot, David; Gordon, Elspeth J; Hall, David R; Lavault, Bernard; McCarthy, Andrew A; McCarthy, Joanne; Mitchell, Edward; Monaco, Stéphanie; Mueller-Dieckmann, Christoph; Nurizzo, Didier; Ravelli, Raimond B G; Thibault, Xavier; Walsh, Martin A; Leonard, Gordon A; McSweeney, Sean M

    2010-09-01

    The design and features of a beamline control software system for macromolecular crystallography (MX) experiments developed at the European Synchrotron Radiation Facility (ESRF) are described. This system, MxCuBE, allows users to easily and simply interact with beamline hardware components and provides automated routines for common tasks in the operation of a synchrotron beamline dedicated to experiments in MX. Additional functionality is provided through intuitive interfaces that enable the assessment of the diffraction characteristics of samples, experiment planning, automatic data collection and the on-line collection and analysis of X-ray emission spectra. The software can be run in a tandem client-server mode that allows for remote control and relevant experimental parameters and results are automatically logged in a relational database, ISPyB. MxCuBE is modular, flexible and extensible and is currently deployed on eight macromolecular crystallography beamlines at the ESRF. Additionally, the software is installed at MAX-lab beamline I911-3 and at BESSY beamline BL14.1.

  3. Automatic sample Dewar for MX beam-line

    SciTech Connect

    Charignon, T.; Tanchon, J.; Trollier, T.; Ravex, A.; Theveneau, P.

    2014-01-29

    It is very common for crystals of large biological macromolecules to show considerable variation in quality of their diffraction. In order to increase the number of samples that are tested for diffraction quality before any full data collections at the ESRF*, an automatic sample Dewar has been implemented. Conception and performances of the Dewar are reported in this paper. The automatic sample Dewar has 240 samples capability with automatic loading/unloading ports. The storing Dewar is capable to work with robots and it can be integrated in a full automatic MX** beam-line. The samples are positioned in the front of the loading/unloading ports with and automatic rotating plate. A view port has been implemented for data matrix camera reading on each sample loaded in the Dewar. At last, the Dewar is insulated with polyurethane foam that keeps the liquid nitrogen consumption below 1.6 L/h. At last, the static insulation also makes vacuum equipment and maintenance unnecessary. This Dewar will be useful for increasing the number of samples tested in synchrotrons.

  4. Neutrino Flux Prediction for the NuMI Beamline

    SciTech Connect

    Soplin, Leonidas Aliaga

    2016-01-01

    The determination of the neutrino flux in any conventional neutrino beam presents a challenge for the current and future short and long baseline neutrino experiments. The uncertainties associated with the production and attenuation of the hadrons in the beamline materials along with those associated with the beam optics have a big effect in the flux spectrum knowledge. For experiments like MINERvA, understanding the flux is crucial since it enters directly into every neutrino-nucleus cross-sections measurements. The foundation of this work is predicting the neutrino flux at MINERvA using dedicated measurements of hadron production in hadron-nucleus collisions and incorporating in-situ MINERvA data that can provide additional constraints. This work also includes the prospect for predicting the flux at other detectors like the NOvA Near detector. The procedure and conclusions of this thesis will have a big impact on future hadron production experiments and on determining the flux for the upcoming DUNE experiment.

  5. Neutrino Flux Prediction for the NuMI Beamline

    SciTech Connect

    Aliaga Soplin, Leonidas

    2016-01-01

    The determination of the neutrino flux in any conventional neutrino beam presents a challenge for the current and future short and long baseline neutrino experiments. The uncertainties associated with the production and attenuation of the hadrons in the beamline materials along with those associated with the beam optics have a big effect in the flux spectrum knowledge. For experiments like MINERvA, understanding the flux is crucial since it enters directly into every neutrino-nucleus cross-sections measurements. The foundation of this work is predicting the neutrino flux at MINERvA using dedicated measurements of hadron production in hadron-nucleus collisions and incorporating in-situ MINERvA data that can provide additional constraints. This work also includes the prospect for predicting the flux at other detectors like the NOvA Near detector. The procedure and conclusions of this thesis will have a big impact on future hadron production experiments and on determining the fl ux for the upcoming DUNE experiment.

  6. Students on the Beamline: classroom, research, and discovery

    NASA Astrophysics Data System (ADS)

    Patry, J.; Walker, T.

    2012-12-01

    High level research is mainly the focus of trained scientists who possess a science specific background. The Canadian Light Source outreach service has developed a two stage research immersion approach which brings together students, teachers, and renowned scientists: Students on the Beamline. The first stage offers a training session for teachers to develop their professional competencies in regards to authentic science research and the synchrotron facility. During the second stage, students from classrooms apply a research protocol of their own design with the help of their teacher and synchrotron scientists. During this presentation, we will first explain the professional approach of the training. In the second part, two experiments designed by students will be presented which are geophysically based so to speak: Study of the Meteoritic Melt Sheet of the Manicouagan Basin and Effects of Olivine on the capture of NOx. Results have shown that teachers bring in the classroom a more authentic and new experience in research application. As for the students, their unique research has contributed to the increase of our knowledge and a better understanding of the scientific inquiry process.Scientist and teacher working together on the synchrotron

  7. Improved monochromator design for high heat load beamlines at CHESS

    SciTech Connect

    Smolenski, K.; Pahl, R.; Doing, P.; Conolly, C.; Clark, B.; Ehen, J.; Shen, Q.

    1996-09-01

    The use of water-cooling channels in silicon x-ray monochromators for the Cornell High Energy Synchrotron Source (CHESS) high power wiggler beamlines has been studied by finite element analysis. The efficiency from channels of different dimensions, ranging from 25 mm to 2 mm width and 5 mm depth, has been calculated. The new crystals are designed to replace the indirect cooled monochromators currently used at CHESS wiggler stations. At typical operation parameters of 150 mA electron current at 5.3 GeV and a gap of 40 mm, the 24-pole wiggler at CHESS provides an x-ray beam with a total power of 2.7 kW at the monochromator. Procedures have been developed for fabrication of internally cooled crystals using a silver-glass dye attach paste. Tests of a new crystal with a conventional x-ray source revealed very small amounts of residual strain. Experiments with synchrotron radiation are scheduled in the near future. {copyright} {ital 1996 American Institute of Physics.}

  8. Emittance measurements in Grumman 1 MeV beamline

    SciTech Connect

    Debiak, T.; Gammel, G.; Melnychuk, S.

    1992-12-01

    The emittance of a 30 keV H{sup {minus}} beam has been measured with an Allison type electrostatic analyser at two positions separated by 85 cm along the Grumman 1 MeV beamline LEBT at low currents (about 4 mA, no Cs{sub 2}O additive in the source) and at higher currents (10-15 mA, with Cs{sub 2}O additive in the source). No emittance growth was observed between the two positions, but, at the higher current level, the emittance was about 60% higher than at the low current level ({Sigma}{sub n},rms = .0045 {pi} cm-mrad vs. 0070 {pi} cm-mrad). Argon was then introduced up to a partial pressure of 4x10{sup {minus}5} torr, and the emittance decreased back to a range corresponding to that found at the lower currents. However, beam noise was observed at the downstream position, and there is evidence for a small amount of emittance growth (<20%) between the two positions.

  9. Optimized baffle and aperture placement in neutral beamlines

    SciTech Connect

    Stone, R.; Duffy, T.; Vetrovec, J.

    1983-11-23

    Most neutral beamlines contain an iron-core ion-bending magnet that requires shielding between the end of the neutralizer and this magnet. This shielding allows the gas pressure to drop prior to the beam entering the magnet and therefore reduces beam losses in this drift region. We have found that the beam losses can be reduced even further by eliminating the iron-core magnet and the magnetic shielding altogether. The required bending field can be supplied by current coils without the iron poles. In addition, placement of the baffles and apertures can affect the cold gas entering the plasma region and the losses in the neutral beam due to re-ionization. In our study we varied the placement of the baffles, which determine the amount of pumping in each chamber, and the apertures, which determine the beam loss. Our results indicate that a baffle/aperture configuration can be set for either minimum cold gas into the plasma region or minimum beam losses, but not both.

  10. Detectors Requirements for the ODIN Beamline at ESS

    NASA Astrophysics Data System (ADS)

    Morgano, Manuel; Lehmann, Eberhard; Strobl, Markus

    The upcoming high intensity pulsed spallationneutron source ESS, now in construction in Sweden, will provide unprecedented opportunities for neutron science worldwide. In particular, neutron imaging will benefit from the time structure of the source and its high brilliance. These features will unlock new opportunities at the imaging beamline ODIN, but only if suitable detectors are employed and, in some cases, upgraded. In this paper, we highlight the current state-of-the-art for neutron imaging detectors, pointing out that, while no single presently existing detector can fulfill all the requirements currently needed to exploit the source to its limits, the wide range of applications of ODIN can be successfully covered by a suite of current state-of-the-art detectors. Furthermore we speculate on improvements to the current detector technologies that would expand the range of the existing detectors and application range and we outline a strategy to have the best possible combined system for the foreseen day 1 operations of ODIN in 2019.

  11. Optimization of High-Energy Implanter Beamline Pumping

    SciTech Connect

    LaFontaine, Marvin; Pharand, Michel; Huang Yongzhang; Pokidov, Ilya; Ferrara, Joseph

    2006-11-13

    A high-energy implanter process chamber and its pumping configuration were designed to minimize the residual gas density in the endstation. A modified Nastran trade mark sign finite-element analysis (FEA) code was used to calculate the pressure distribution and gas flow within the process chamber. The modified FE method was readily applied to the internal geometry of the scan chamber, the corrector magnet waveguide, and the process chamber, which included the scan arm assembly, 300mm wafer, and plasma electron flood gun (PEF). Using the modified Nastran code, the gas flow and pressure distribution within the beamline geometry were calculated. The gas load consisted of H2, which is generated by photoresist (PR) outgassing from the 300mm wafer, and Xe from the plasma electron flood gun. Several pumping configurations were assessed, with each consisting of various locations and pumping capacities of vacuum pumps. The pressure distribution results for each configuration are presented, along with pumping efficiency results which are helpful in selecting the optimum pump configuration. The analysis results were compared to measured data, indicating a good correlation between the two.

  12. Upgrade of beamline BL08B at Taiwan Light Source from a photon-BPM to a double-grating SGM beamline.

    PubMed

    Yuh, Jih Young; Lin, Shan Wei; Huang, Liang Jen; Fung, Hok Sum; Lee, Long Life; Chen, Yu Joung; Cheng, Chiu Ping; Chin, Yi Ying; Lin, Hong Ji

    2015-09-01

    During the last 20 years, beamline BL08B has been upgraded step by step from a photon beam-position monitor (BPM) to a testing beamline and a single-grating beamline that enables experiments to record X-ray photo-emission spectra (XPS) and X-ray absorption spectra (XAS) for research in solar physics, organic semiconductor materials and spinel oxides, with soft X-ray photon energies in the range 300-1000 eV. Demands for photon energy to extend to the extreme ultraviolet region for applications in nano-fabrication and topological thin films are increasing. The basic spherical-grating monochromator beamline was again upgraded by adding a second grating that delivers photons of energy from 80 to 420 eV. Four end-stations were designed for experiments with XPS, XAS, interstellar photoprocess systems (IPS) and extreme-ultraviolet lithography (EUVL) in the scheduled beam time. The data from these experiments show a large count rate in core levels probed and excellent statistics on background normalization in the L-edge adsorption spectrum. PMID:26289286

  13. DESIGN OF VISIBLE DIAGNOSTIC BEAMLINE FOR NSLS2 STORAGE RING

    SciTech Connect

    Cheng, W.; Fernandes, H.; Hseuh, H.; Kosciuk, B.; Krinsky, S.; Singh, O.

    2011-03-28

    A visible synchrotron light monitor (SLM) beam line has been designed at the NSLS2 storage ring, using the bending magnet radiation. A retractable thin absorber will be placed in front of the first mirror to block the central x-rays. The first mirror will reflect the visible light through a vacuum window. The light is guided by three 6-inch diameter mirrors into the experiment hutch. In this paper, we will describe design work on various optical components in the beamline. The ultra high brightness NSLS-II storage ring is under construction at Brookhaven National Laboratory. It will have 3GeV, 500mA electron beam circulating in the 792m ring, with very low emittance (0.9nm.rad horizontal and 8pm.rad vertical). The ring is composed of 30 DBA cells with 15 fold symmetry. Three damping wigglers will be installed in long straight sections 8, 18 and 28 to lower the emittance. While electrons pass through the bending magnet, synchrotron radiation will be generated covering a wide spectrum. There are other insertion devices in the storage ring which will generate shorter wavelength radiation as well. Synchrotron radiation has been widely used as diagnostic tool to measure the transverse and longitudinal profile. Three synchrotron light beam lines dedicated for diagnostics are under design and construction for the NSLS-II storage ring: two x-ray beam lines (pinhole and CRL) with the source points from Cell 22 BM{_}A (first bending in the DBA cell) and Cell22 three-pole wiggler; the third beam line is using visible part of radiation from Cell 30 BM{_}B (second bending magnet from the cell). Our paper focuses on the design of the visible beam line - SLM.

  14. Numerical analysis of partially coherent radiation at soft x-ray beamline.

    PubMed

    Meng, Xiangyu; Xue, Chaofan; Yu, Huaina; Wang, Yong; Wu, Yanqing; Tai, Renzhong

    2015-11-16

    A new model for numerical analysis of partially coherent x-ray at synchrotron beamlines is presented. The model is based on statistical optics. Four-dimensional coherence function, Mutual Optical Intensity (MOI), is applied to describe the wavefront of the partially coherent light. The propagation of MOI through optical elements in the beamline is deduced with numerical calculation. The coherence of x-ray through beamlines can be acquired. We applied the model to analyze the coherence in the STXM beamline at SSRF, and got the coherence length of the beam at the endstation. To verify the theoretical results, the diffraction experiment of a single slit was performed and the diffraction pattern was simulated to get the coherence length, (31 ± 3.0) µm × (25 ± 2.1) µm (H × V), which had a good agreement with the theoretical results, (30.7 ± 0.6) µm × (31 ± 5.3) µm (H × V). The model is applicable to analyze the coherence in synchrotron beamlines.

  15. The vacuum ultraviolet beamline/endstations at NSRL dedicated to combustion research.

    PubMed

    Zhou, Zhongyue; Du, Xuewei; Yang, Jiuzhong; Wang, Yizun; Li, Chaoyang; Wei, Shen; Du, Liangliang; Li, Yuyang; Qi, Fei; Wang, Qiuping

    2016-07-01

    An undulator-based vacuum ultraviolet (VUV) beamline (BL03U), intended for combustion chemistry studies, has been constructed at the National Synchrotron Radiation Laboratory (NSRL) in Hefei, China. The beamline is connected to the newly upgraded Hefei Light Source (HLS II), and could deliver photons in the 5-21 eV range, with a photon flux of 10(13) photons s(-1) at 10 eV when the beam current is 300 mA. The monochromator of the beamline is equipped with two gratings (200 lines mm(-1) and 400 lines mm(-1)) and its resolving power is 3900 at 7.3 eV for the 200 lines mm(-1) grating and 4200 at 14.6 eV for the 400 lines mm(-1) grating. The beamline serves three endstations which are designed for respective studies of premixed flame, fuel pyrolysis in flow reactor, and oxidation in jet-stirred reactor. Each endstation contains a reactor chamber, an ionization chamber where the molecular beam intersects with the VUV light, and a home-made reflectron time-of-flight mass spectrometer. The performance of the beamline and endstations with some preliminary results is presented here. The ability to detect reactive intermediates (e.g. H, O, OH and hydroperoxides) is advantageous in combustion chemistry research. PMID:27359154

  16. High resolution neutron imaging capabilities at BOA beamline at Paul Scherrer Institut

    NASA Astrophysics Data System (ADS)

    Tremsin, A. S.; Morgano, M.; Panzner, T.; Lehmann, E.; Filgers, U.; Vallerga, J. V.; McPhate, J. B.; Siegmund, O. H. W.; Feller, W. B.

    2015-06-01

    The cold neutron spectrum of the Beamline for neutron Optics and other Applications (BOA) at Paul Scherrer Institut enables high contrast neutron imaging because neutron cross sections for many materials increase with neutron wavelength. However, for many neutron imaging applications, spatial resolution can be as important as contrast. In this paper the neutron transmission imaging capabilities of an MCP/Timepix detector installed at the BOA beamline are presented, demonstrating the possibilities for studying sub-20 μm features in various samples. In addition to conventional neutron radiography and microtomography, the high degree of neutron polarization at the BOA beamline can be very attractive for imaging of magnetic fields, as demonstrated by our measurements. We also show that a collimated cold neutron beamline combined with a high resolution detector can produce image artifacts, (e.g. edge enhancements) due to neutron refraction and scattering. The results of our experiments indicate that the BOA beamline is a valuable addition to neutron imaging facilities, providing improved and sometimes unique capabilities for non-destructive studies with cold neutrons.

  17. Design of the Structural Biology Center beamlines at the APS (abstract)

    NASA Astrophysics Data System (ADS)

    Rosenbaum, Gerd; Westrbrook, Edwin M.

    1996-09-01

    The Structural Biology Center-CAT will develop and operate a sector of the APS as a user facility for studies in macromolecular crystallography. The techniques applied will include multiple-energy anomalous dispersion (MAD) phasing and polychromatic (Laue) data collection. Data will be recorded on a high resolution CCD-area detector. The SBC is constructing two beamlines, one for radiation from an undulator and one for radiation from a bending magnet. The x ray optics of both beamlines are designed to produce a highly demagnified image of the source in order to match the focal size with the sizes of the sample and the resolution element of the detector. Vertical focusing is achieved by a flat, cylindrically bent mirror. Horizontal focusing is achieved by sagittally bending the second crystal of a double crystal-monochromator. The double-crystal monochromators of both beamlines have a constant exit height output beam. On the undulator beamline, two double-crystal monochromators are installed in series—one with Si-111 crystals and the second with Si-220 crystals—in order to facilitate quick change between high flux and narrow bandwidth. For the heat-loaded first crystals, the liquid-nitrogen-cooled, thin-web design being developed by the APS has been adopted. On the bending magnet beamline, three crystals (Si-111, Si-220, Si-400) are mounted side-by-side on the first crystal stage and translated into the beam is required.

  18. CAT Guide and Beamline Directory. A key to APS Collaborative Access Teams

    SciTech Connect

    1999-07-08

    The Advanced Photon Source (APS), a national user facility for synchrotrons radiation research, is located at Argonne National Laboratory, approximately 25 miles southwest of Chicago, Illinois. The APS is considered a third-generation synchrotrons radiation facility (specifically designed to accommodate insertion devices to serve as radiation sources) and is one of three such facilities in the world. Currently, it is the most brilliant source in the United States for research in such diverse fields as biology, medicine, materials science, chemistry, geology, agriculture and soil science, physics, and manufacturing technology. Researchers use the APS either as members of Collaborative Access Teams (CATS) or as Independent Investigators (IIs). CATS are responsible for designing, building, and operating beamlines in one or more sectors, each sector consisting of an insertion-device (ID) beamline and a bending-magnet (BM) beamline. Each beamline is designed to accommodate a specific type of research program(s) and is optimized accordingly. CAT members are entitled to use 75% of the available beam time to pursue CAT research goals. The remaining 25% of the available beam time must be made available to IIs. This document was written to help prospective IIs determine which beamlines are suitable for their specific experiments.

  19. The vacuum ultraviolet beamline/endstations at NSRL dedicated to combustion research.

    PubMed

    Zhou, Zhongyue; Du, Xuewei; Yang, Jiuzhong; Wang, Yizun; Li, Chaoyang; Wei, Shen; Du, Liangliang; Li, Yuyang; Qi, Fei; Wang, Qiuping

    2016-07-01

    An undulator-based vacuum ultraviolet (VUV) beamline (BL03U), intended for combustion chemistry studies, has been constructed at the National Synchrotron Radiation Laboratory (NSRL) in Hefei, China. The beamline is connected to the newly upgraded Hefei Light Source (HLS II), and could deliver photons in the 5-21 eV range, with a photon flux of 10(13) photons s(-1) at 10 eV when the beam current is 300 mA. The monochromator of the beamline is equipped with two gratings (200 lines mm(-1) and 400 lines mm(-1)) and its resolving power is 3900 at 7.3 eV for the 200 lines mm(-1) grating and 4200 at 14.6 eV for the 400 lines mm(-1) grating. The beamline serves three endstations which are designed for respective studies of premixed flame, fuel pyrolysis in flow reactor, and oxidation in jet-stirred reactor. Each endstation contains a reactor chamber, an ionization chamber where the molecular beam intersects with the VUV light, and a home-made reflectron time-of-flight mass spectrometer. The performance of the beamline and endstations with some preliminary results is presented here. The ability to detect reactive intermediates (e.g. H, O, OH and hydroperoxides) is advantageous in combustion chemistry research.

  20. Investigation of the heat handling capabilities of DIII-D neutral beamline internal components

    SciTech Connect

    Phillips, J.C.; Baxi, C.B.; Hong, R.

    1993-10-01

    The current DIII-D neutral beam system is a nominal five second pulse length upgrade of a previous design rated for only 500 msec operation. While the ion sources are rated for 60 sec operation, in practice pulse lengths are limited both by the beamline internal components ability to handle the fraction of the power which is scraped off, and by the power supplies ability to provide pulse lengths of greater than 5 sec. This paper examines the capability of the existing DIII-D neutral beamline heat removing components both in terms of present and desired operating parameters. To date, at 2.5 MW per ion source, pulses are limited to 3.5 sec by beamline internal components, while at lower ratings of 2.0 MW per ion source, up to 5 sec pulses have been achieved. Recent advances and demonstration of the extraction of 3.5 MW per DIII-D ion source give an even wider window of operating conditions. A full series of beamline thermocouple data has been collected to determine the heat loading and implied surface temperatures for the various DIII-D neutral beamline internal components. These data will be presented along with an analysis of the needs for specific component upgrades, given a desire for 10 sec operation.

  1. Design of the X-ray Nanoprobe Beamline at the Taiwan Photon Source

    NASA Astrophysics Data System (ADS)

    Chang, S. H.; Yin, G. C.; Wang, D. J.; Chang, C. H.; Juang, J. M.; Huang, L. J.; Liu, C. Y.; Chang, C. F.; Chu, C. H.; Tang, M. T.

    2013-03-01

    The X-ray Nanoprobe (XNP) Beamline Project has been granted as one of the first seven beamlines at the Taiwan Photon Source (TPS). The XNP beamline and the associated instruments are designed to utilize the highly brilliant TPS light source for resolving the atomic, chemical and electronic structures of semiconductor-based devices with tens nm spatial resolution in tomographic and nondestructive manners. The beamline optics is deliberated to deliver focal spot around 40 nm with photon flux in the level of 1010 photons/sec. The stability of the focal position will be highly improved by operating the double crystal monochromator (DCM) in horizontally diffracting geometry, with minor sacrifice in energy resolution. The relative movement between sample and focusing optics is controlled by ultra-precise linear translational/flexure stages and monitored by laser interferometers. The end stations will provide conventional X-ray probes including, X-ray fluorescence (XRF), X-ray absorption fine structures (XAFS), X-ray excited optical luminescence (XEOL), and the emerging techniques, such as the Bragg-ptychography (BP) to overcome the spatial resolution set by the focusing optics. A novel scanning mechanism incorporating surface diffraction and BP for mapping the 3D interfacial strains is under development. The XNP beamline and associated instruments are expected to take the first synchrotron light by the end of 2015.

  2. Application of partially coherent wavefront propagation calculations for design of coherence-preserving synchrotron radiation beamlines

    NASA Astrophysics Data System (ADS)

    Chubar, Oleg; Chu, Yong S.; Kaznatcheev, Konstantine; Yan, Hanfei

    2011-09-01

    Ultra-low emittance third-generation synchrotron radiation (SR) sources, such as NSLS-II and MAX-IV, will offer excellent opportunities for further development of experimental techniques exploiting X-ray coherence. However, even in these new SR sources, the radiation produced by relativistic electrons (in undulators, wigglers and bending magnets) will remain only partially coherent in the X-ray spectral range. "Extraction" of "coherent portion" of the radiation flux and its transport to sample without loss of coherence must be performed by dedicated SR beamlines, optimized for particular types of experiments. Detailed quantitative prediction of partially coherent X-ray beam properties at propagation through optical elements, which is required for the optimization of such beamlines, can only be obtained from accurate and efficient physical-optics based numerical simulations. Examples of such simulations, made for NSLS-II beamlines, using "Synchrotron Radiation Workshop" (SRW) computer code, are presented. Special attention is paid to the numerical analysis of the basic properties of partially coherent undulator radiation beam and its distinctions from the Gaussian beam. Performance characteristics of importance for particular beamlines, such as radiation spot size and flux at sample vs size of secondary source aperture for high-resolution microscopy beamlines, are predicted by the simulations.

  3. Neutron imaging options at the BOA beamline at Paul Scherrer Institut

    NASA Astrophysics Data System (ADS)

    Morgano, M.; Peetermans, S.; Lehmann, E. H.; Panzner, T.; Filges, U.

    2014-08-01

    The BOA beamline at the Swiss spallation neutron source SINQ at Paul Scherrer Institut is a flexible instrument used mainly for testing novel techniques and devices for neutron scattering and optics, but, due to the large and relatively homogeneous field of view, it can be successfully used for experiments in the field of neutron imaging. The beamline allows also for the exploitation of advanced imaging concepts such as polarized neutron imaging and diffractive neutron imaging. In this paper we present the characterization of the BOA beamline in the light of its neutron imaging capabilities. We show also the different techniques that can be employed there as user-friendly plugins for non-standard neutron imaging experiments.

  4. Soft x-ray beamline BL7A at the UVSOR

    SciTech Connect

    Murata, T. ); Matsukawa, T. ); Naoe, S. ); Horigome, T.; Matsudo, O.; Watanabe, M. )

    1992-01-01

    A vacuum-compatible double-crystal monochromator with constant exit-beam height has been installed and operated for several years at beamline BL7A at the UVSOR facility at the Institute for Molecular Science, Okazaki, Japan, The beamline is used both for the photons from a normal bending-magnet section and those from a 4 T superconducting three-pole horizontal wiggler. Various pairs of monochromator crystals are being used with sufficient intensity and signal to noise ratio of the output signal. Basic structure of the beamline, the mechanism of the monochromator, and some typical spectra of materials with absorption edges between 850 eV and 4 keV are reported.

  5. Mirror and grating surface figure requirements for grazing incidence synchrotron radiation beamlines: Power loading effects

    SciTech Connect

    Hulbert, S.L.; Sharma, S.

    1987-01-01

    At present, grazing incidence mirrors are used almost exclusively as the first optical element in VUV and soft x-ray synchrotron radiation beamlines. The performance of these mirrors is determined by thermal and mechanical stress-induced figure errors as well as by figure errors remaining from the grinding and polishing process. With the advent of VUV and soft x-ray undulators and wigglers has come a new set of thermal stress problems related to both the magnitude and the spatial distribution of power from these devices. In many cases the power load on the entrance slits and gratings in these beamlines is no longer negligible. The dependence of thermally-induced front-end mirror figure errors on various storage ring and insertion device parameters (especially those at the National Synchrotron Light Source) and the effects of these figure errors on two classes of soft x-ray beamlines are presented.

  6. High heat load crystal cooling strategies for an APS wiggler beamline

    SciTech Connect

    Beno, M.A.; Knapp, G.S.; Engbretson, M.

    1997-07-01

    High energy wigglers produce extremely high total powers. For example, the insertion device for one beamline of the Basic Energy Sciences Synchrotron Research Center (BESSRC) is an elliptical multipole wiggler (EMPW) which can generate circularly polarized X-rays on axis and produces a total power of {approximately}8 kW. This insertion device will be used to simultaneously provide x-rays to three branch lines, a branch equipped with a normal double crystal monochromator feeding a scattering and spectroscopy station, and two branches with single-bounce horizontally deflecting monochromators for Compton scattering and High Energy Diffraction. The crystal optics for this type of device require substantially different heat load solutions than those used for undulator beamlines. We will discuss how the beam is split and shared among the beamline branch lines and present the crystal cooling strategies employed for both the double-crystal monochromator and horizontally deflecting single-bounce monochromators.

  7. Light flux density threshold at which protein denaturation is induced by synchrotron radiation circular dichroism beamlines.

    PubMed

    Miles, A J; Janes, Robert W; Brown, A; Clarke, D T; Sutherland, J C; Tao, Y; Wallace, B A; Hoffmann, S V

    2008-07-01

    New high-flux synchrotron radiation circular dichroism (SRCD) beamlines are providing important information for structural biology, but can potentially cause denaturation of the protein samples under investigation. This effect has been studied at the new CD1 dedicated SRCD beamline at ISA in Denmark, where radiation-induced thermal damage effects were observed, depending not only on the radiation flux but also on the focal spot size of the light. Comparisons with similar studies at other SRCD facilities worldwide has lead to the estimation of a flux density threshold under which SRCD beamlines should be operated when samples are to be exposed to low-wavelength vacuum ultraviolet radiation for extended periods of time.

  8. Optical Design of VLS-PGM Soft X-Ray Beamline on Indus-2

    SciTech Connect

    Prasad, T. T.; Modi, M. H.; Lodha, G. S.

    2010-06-23

    The optical design of a soft x-ray beamline on the bending magnet of Indus-2 synchrotron source is presented. A Varied Line Spacing Plane Grating Monochromator (VLS-PGM) was adopted with Hettrick type optics. The VLS-PGM consists of a spherical mirror and three interchangeable gratings of line densities 1200 l/mm, 400 l/mm and 150 l/mm to efficiently cover the energy region 50-1500 eV. The VLS groove parameters were obtained by minimizing defocus aberration, coma and spherical aberration. The overall performance of the beamline was estimated by detailed raytracing calculations. The beamline design, results of the raytracing calculations and the expected performances are presented.

  9. Soft x-ray spectroscopy undulator beamline at the Advanced Photon Source

    SciTech Connect

    Randall, K.J.; Xu, Z.; Moore, J.F.; Gluskin, E.

    1997-09-01

    Construction of the high-resolution soft x ray spectroscopy undulator beamline, 2ID-C, at the Advanced Photon Source (APS) has been completed. The beamline, one of two soft x ray beamlines at the APS, will cover the photon energy range from 500 to 3,000 eV, with a maximum resolving power between 7,000 and 14,000. The optical design is based on a spherical grating monochromator (SGM) giving both high resolution and high flux throughput. Photon flux is calculated to be approximately 10{sup 12}--10{sup 13} photons per second with a beam size of approximately 1 x 1 mm{sup 2} at the sample.

  10. A telescope proton recoil spectrometer for fast neutron beam-lines

    NASA Astrophysics Data System (ADS)

    Cazzaniga, C.; Rebai, M.; Tardocchi, M.; Croci, G.; Nocente, M.; Ansell, S.; Frost, C. D.; Gorini, G.

    2015-07-01

    Fast neutron measurements were performed on the VESUVIO beam-line at the ISIS spallation source using a new telescope proton recoil spectrometer. Neutrons interact on a plastic target. Proton production is mainly due to elastic scattering on hydrogen nuclei and secondly due to interaction with carbon nuclei. Recoil protons are measured by a proton spectrometer, which uses in coincidence a 2.54 cm thick YAP scintillator and a 500μm thick silicon detector, measuring the full proton recoil energy and the partial deposited energy in transmission, respectively. Recoil proton spectroscopy measurements (up to Ep = 60MeV) have been interpreted by using Monte Carlo simulations of the beam-line. This instrument is of particular interest for the characterization of the ChipIr beam-line at ISIS, which was designed to feature an atmospheric-like neutron spectrum for the irradiation of micro-electronics.

  11. High-brightness beamline for x-ray spectroscopy at the ALS

    SciTech Connect

    Perera, R.C.C.; Jones, G.; Lindle, D.W.

    1997-04-01

    Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goals of high energy resolution, high flux, and high brightness at the sample. When completed later this year, it will be the first ALS monochromatic hard x-ray beamline, and its brightness will be an order of magnitude higher than presently available in this energy range. In addition, it will provide flux and resolution comparable to any other beamline now in operation. To achieve these goals, two technical improvements, relative to existing x-ray beamlines, were incorporated. First, a somewhat novel optical design for x-rays, in which matched toroidal mirrors are positioned before and after the double-crystal monochromator, was adopted. This configuration allows for high resolution by passing a collimated beam through the monochromator, and for high brightness by focusing the ALS source on the sample with unit magnification. Second, a new {open_quotes}Cowan type{close_quotes} double-crystal monochromator based on the design used at NSLS beamline X-24A was developed. The measured mechanical precision of this new monochromator shows significant improvement over existing designs, without using positional feedback available with piezoelectric devices. Such precision is essential because of the high brightness of the radiation and the long distance (12 m) from the source (sample) to the collimating (focusing) mirror. This combination of features will provide a bright, high resolution, and stable x-ray beam for use in the x-ray spectroscopy program at the ALS.

  12. The SEXTANTS beamline at SOLEIL: a new facility for elastic, inelastic and coherent scattering of soft X-rays

    NASA Astrophysics Data System (ADS)

    Sacchi, M.; Jaouen, N.; Popescu, H.; Gaudemer, R.; Tonnerre, J. M.; Chiuzbaian, S. G.; Hague, C. F.; Delmotte, A.; Dubuisson, J. M.; Cauchon, G.; Lagarde, B.; Polack, F.

    2013-03-01

    SEXTANTS is a new SOLEIL beamline dedicated to soft X-ray scattering techniques. The beamline, covering the 50-1700 eV energy range, features two Apple-II undulators for polarization control and a fixed-deviation monochromator. Two branch-lines host three end-stations for elastic, inelastic and coherent scattering experiments.

  13. The macromolecular crystallography beamlines at BESSY II of the Helmholtz-Zentrum Berlin: Current status and perspectives

    NASA Astrophysics Data System (ADS)

    Mueller, Uwe; Förster, Ronald; Hellmig, Michael; Huschmann, Franziska U.; Kastner, Alexandra; Malecki, Piotr; Pühringer, Sandra; Röwer, Martin; Sparta, Karine; Steffien, Michael; Ühlein, Monika; Wilk, Piotr; Weiss, Manfred S.

    2015-07-01

    For a little over a decade now, the Macromolecular Crystallography (MX) group at the Helmholtz-Zentrum Berlin (HZB) has been operating three state-of-the-art synchrotron beamlines for MX at the BESSY II storage ring in Berlin. The three HZB-MX beamlines, BL14.1, BL14.2 and BL14.3, serve a stable and growing user community of currently more than 100 independent research groups from Berlin, Germany and Europe. Every year, the beamlines provide close to 200 days of MX-beamtime. Over time, the HZB-MX beamlines and endstations, in particular BL14.1, have been continually developed and upgraded and, since 2010, they operate as the most productive MX beamlines in Germany. The environment of the beamlines includes various ancillary equipment as well as additional facilities, such as office space adjacent to the beamlines, a sample preparation laboratory, a safety level 1 biology laboratory (HZB-MX BioLab) and all necessary computing resources. In this paper, the current status of the beamlines as well as the ongoing developments are described.

  14. Soft-x-ray and vacuum-ultraviolet beamlines at the National Synchrotron Light Source 700-MeV storage ring

    SciTech Connect

    Williams, G.P.; Howells, M.R.

    1982-01-01

    We summarize the characteristics of the first beamlines which are being installed and commissioned at the National Synchrotron Light Source (NSLS) 700 MeV storage ring at Brookhaven National Laboratory. We also give a progress report as of July 1982 on the early stages of beamline alignment and operation in which particular attention is paid to the 5 beamlines which NSLS has developed. The report describes in detail a novel method for beamline alignment which is of general application.

  15. Optimization of the soft x-ray transmission microscopy beamline at the ALBA light source

    NASA Astrophysics Data System (ADS)

    Sorrentino, Andrea; Pereiro, Eva; Valcárcel, Ricardo; Ferrer, Salvador; Nicolas, Josep

    2013-09-01

    Mistral is the soft X-ray full field microscopy beamline at the ALBA light source. The beamline is designed to have large source acceptance and to provide constant magnification at the exit slit for photon energies between 270 and 2600 eV. The monochromator is a variation of the Petersen plane grating monochromator in which a variable line spacing grating is used to maintain the beam focused at the exit slit, independently of the fixed focus constant, and to cancel aberrations. We present the alignment strategy used to compensate errors of the optical elements, and report about the commissioning results.

  16. The 7BM beamline at the APS: a facility for time-resolved fluid dynamics measurements

    PubMed Central

    Kastengren, Alan; Powell, Christopher F.; Arms, Dohn; Dufresne, Eric M.; Gibson, Harold; Wang, Jin

    2012-01-01

    In recent years, X-ray radiography has been used to probe the internal structure of dense sprays with microsecond time resolution and a spatial resolution of 15 µm even in high-pressure environments. Recently, the 7BM beamline at the Advanced Photon Source (APS) has been commissioned to focus on the needs of X-ray spray radiography measurements. The spatial resolution and X-ray intensity at this beamline represent a significant improvement over previous time-resolved X-ray radiography measurements at the APS. PMID:22713903

  17. APS beamline standard components handbook, Version 1.3. Revision 1

    SciTech Connect

    Hahn, U.; Shu, D.; Kuzay, T.M.

    1993-02-01

    This Handbook in its current version (1.3) contains descriptions, specifications, and preliminary engineering design drawings for many of the standard components. The design status and schedules have been provided wherever possible. In the near future, the APS plans to update engineering drawings of identified standard beamline components and complete the Handbook. The completed version of this Handbook will become available to both the CATs and potential vendors. Use of standard components should result in major cost reductions for CATs in the areas of beamline design and construction.

  18. The New Structural Materials Science Beamlines BL8A and 8B at Photon Factory

    SciTech Connect

    Nakao, A.; Sugiyama, H.; Koyama, A.; Watanabe, K.

    2010-06-23

    BL8A and 8B are new beamlines for structural materials science at Photon Factory. The primary characteristics of both beamlines are similar. The incident beam is monochromatized by the Si(111) double-flat crystal monochromator and focused at the sample position by a Rh-coated bent cylindrical quartz mirror. The Weissenberg-camera-type imaging-plate (IP) diffractometers were installed. The X-ray diffraction experiments for structural studies of strongly correlated materials, such as transition metals, molecular conductors, endohedral fullerenes, nano-materials, etc, are conducted at these stations.

  19. The X-ray Fluorescence Microscopy Beamline at the Australian Synchrotron

    SciTech Connect

    Paterson, D.; Jonge, M. D. de; Howard, D. L.; Lewis, W.; McKinlay, J.; Starritt, A.; Kusel, M.; Ryan, C. G.; Kirkham, R.; Moorhead, G.; Siddons, D. P.

    2011-09-09

    A hard x-ray micro-nanoprobe has commenced operation at the Australian Synchrotron providing versatile x-ray fluorescence microscopy across an incident energy range from 4 to 25 keV. Two x-ray probes are used to collect {mu}-XRF and {mu}-XANES for elemental and chemical microanalysis: a Kirkpatrick-Baez mirror microprobe for micron resolution studies and a Fresnel zone plate nanoprobe capable of 60-nm resolution. Some unique aspects of the beamline design and operation are discussed. An advanced energy dispersive x-ray fluorescence detection scheme named Maia has been developed for the beamline, which enables ultrafast x-ray fluorescence microscopy.

  20. Analysis of the optical design of the NSLS-II coherent hard x-ray beamline

    NASA Astrophysics Data System (ADS)

    Fluerasu, Andrei; Chubar, Oleg; Kaznatcheev, Konstantine; Baltser, Jana; Wiegart, Lutz; Evans-Lutterodt, Kenneth; Carlucci-Dayton, Mary; Berman, Lonny

    2011-09-01

    Ultra-low emittance third-generation synchrotron radiation sources such as the NSLS-II offer excellent opportunities for the development of experimental techniques exploiting x-ray coherence. Coherent light scattered by a heterogeneous sample produces a speckle pattern characteristic for the specific arrangement of the scatterers. This may vary over time, and the resultant intensity fluctuations can be measured and analyzed to provide information about the sample dynamics. X-ray photon correlation spectroscopy (XPCS) extends the capability of dynamic light scattering to opaque and turbid samples and extends the measurements of time evolution to nanometer length scales. As a consequence XPCS became crucial in the study of dynamics in systems including, but not being limited to, colloids, polymers, complex fluids, surfaces and interfaces, phase ordering alloys, etc. In this paper we present the conceptual optical design and the theoretical performance of the Coherent Hard X-ray (CHX) beamline at NSLS-II, dedicated to XPCS and other coherent scattering techniques. For the optical design of this beamline, there is a tradeoff between the coherence needed to distinguish individual speckles and the phase acceptance (high intensity) required to measure fast dynamics with an adequate signal-to-noise level. As XPCS is a "photon hungry" technique, the beamline optimization requires maximizing the signal-to-noise ratio of the measured intensity-intensity autocorrelation function. The degree of coherence, as measured by a two-slit (Young) experiment, is used to characterize the speckle pattern visibilities. The beamline optimization strategy consists of maximization of the on-sample intensity while keeping the degree of coherence within the 0.1-0.5 range. The resulted design deviates substantially from an ad-hoc modification of a hard x-ray beamline for XPCS measurements. The CHX beamline will permit studies of complex systems and measurements of bulk dynamics down to the

  1. Analysis of the optical design of the NSLS-II Coherent Hard X-ray beamline

    SciTech Connect

    Fluerasu A.; Chubar, O.; Kaznatcheev, K.; Baltser, J.; Wiegart, Lutz; Evans-Lutterodt, K.; Carlucci-Dayton, M.; Berman, L.

    2011-08-21

    Ultra-low emittance third-generation synchrotron radiation sources such as the NSLS-II offer excellent opportunities for the development of experimental techniques exploiting x-ray coherence. Coherent light scattered by a heterogeneous sample produces a speckle pattern characteristic for the specific arrangement of the scatterers. This may vary over time, and the resultant intensity fluctuations can be measured and analyzed to provide information about the sample dynamics. X-ray photon correlation spectroscopy (XPCS) extends the capability of dynamic light scattering to opaque and turbid samples and extends the measurements of time evolution to nanometer length scales. As a consequence XPCS became crucial in the study of dynamics in systems including, but not being limited to, colloids, polymers, complex fluids, surfaces and interfaces, phase ordering alloys, etc. In this paper we present the conceptual optical design and the theoretical performance of the Coherent Hard X-ray (CHX) beamline at NSLS-II, dedicated to XPCS and other coherent scattering techniques. For the optical design of this beamline, there is a tradeoff between the coherence needed to distinguish individual speckles and the phase acceptance (high intensity) required to measure fast dynamics with an adequate signal-to-noise level. As XPCS is a 'photon hungry' technique, the beamline optimization requires maximizing the signal-to-noise ratio of the measured intensity-intensity autocorrelation function. The degree of coherence, as measured by a two-slit (Young) experiment, is used to characterize the speckle pattern visibilities. The beamline optimization strategy consists of maximization of the on-sample intensity while keeping the degree of coherence within the 0.1-0.5 range. The resulted design deviates substantially from an ad-hoc modification of a hard x-ray beamline for XPCS measurements. The CHX beamline will permit studies of complex systems and measurements of bulk dynamics down to the

  2. Beamline BL-07 at Indus-2: a facility for microfabrication research.

    PubMed

    Dhamgaye, V P; Lodha, G S; Gowri Sankar, B; Kant, C

    2014-01-01

    The X-ray lithography beamline on Indus-2 is now operational, with two modes of operation. With a pair of X-ray mirrors it is possible to tune the energy spectrum between 1 and 20 keV with a controlled spectral bandwidth. In its 'no optics' mode, hard X-rays up to 40 keV are available. Features and performance of the beamline are presented along with some example structures. Structures fabricated include honeycomb structures in PMMA using a stainless steel stencil mask and a compound refractive X-ray lens using a polyimide-gold mask in SU-8. PMID:24365946

  3. New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team

    SciTech Connect

    Xiao, Y. M. Chow, P.; Boman, G.; Bai, L. G.; Rod, E.; Bommannavar, A.; Kenney-Benson, C.; Sinogeikin, S.; Shen, G. Y.

    2015-07-15

    The 16 ID-D (Insertion Device - D station) beamline of the High Pressure Collaborative Access Team at the Advanced Photon Source is dedicated to high pressure research using X-ray spectroscopy techniques typically integrated with diamond anvil cells. The beamline provides X-rays of 4.5-37 keV, and current available techniques include X-ray emission spectroscopy, inelastic X-ray scattering, and nuclear resonant scattering. The recent developments include a canted undulator upgrade, 17-element analyzer array for inelastic X-ray scattering, and an emission spectrometer using a polycapillary half-lens. Recent development projects and future prospects are also discussed.

  4. Positron beam optics for the 2D-ACAR spectrometer at the NEPOMUC beamline

    NASA Astrophysics Data System (ADS)

    Ceeh, H.; Weber, J. A.; Hugenschmidt, C.; Leitner, M.; Boni, P.

    2014-04-01

    In the last year a conventional 2D-ACAR spectrometer has been set up and brought to operation at TUM. Once the NEPOMUC beamline is extended to the new experimental hall at the research reactor FRM-II the conventional 2D-ACAR spectrometer will be upgraded with a second sample chamber in order to be integrated to the NEPOMUC beamline facility. This spectrometer will add a complete new quality to 2D-ACAR experiments as it allows to track the evolution of the electronic structure from the surface to the bulk. We present the design features of the positron beam optics and the sample environment.

  5. Neutron imaging experiments at E-12 beam-line of CIRUS

    SciTech Connect

    Agrawal, Ashish; Kashyap, Yogesh; Shukla, Mayank; Sarkar, P. S.; Sinha, Amar

    2013-02-05

    Neutron imaging beam-line at E-12 beam port of CIRUS reactor India has been developed to implement Neutron tomography, phase contrast imaging and dynamic imaging techniques for various applications. Several experiments on these techniques have been carried out successfully. Neutron radiography and tomography has been used to study blisters formation in pressure tube along with many other applications. Similarly phase contrast imaging has been used to study its feasibility for better contrast in radiographic images. Dynamic imaging has been applied to study the melting of pure and impure lead under heat. In this paper we report the details of various experiments performed at this beam-line.

  6. Commissioning of Angle Dispersive X-ray Diffraction Beamline on Indus-2

    SciTech Connect

    Sinha, A. K.; Sagdeo, Archna; Gupta, Pooja; Kumar, Ashok; Singh, M. N.; Gupta, R. K.; Kane, S. R.; Deb, S. K.

    2011-07-15

    An Angle dispersive x-ray diffraction (ADXRD) beamline on bending magnet source of Indus-2 synchrotron (2.5 GeV, 300 mA) has been commissioned, for the study of single and polycrystalline samples. The beamline optics is based on vertically focusing Pt-coated pre and post mirrors and sagittal focusing Si (311) based double crystal monochromator. Experimental station consists of a six circle diffractometer equipped with scintillation detector and an image plate area detector for powder diffraction. XRD experiments have been performed to study single crystal and polycrystalline samples.

  7. Data acquisition and control software for XRD beamline at Indus-2

    SciTech Connect

    Kane, Sanjeev R.; Garg, C. K.; Sinha, A. K.

    2010-06-23

    X-ray diffraction (XRD) beamline is under commissioning on Indus-2 synchrotron radiation facility. The experimental setup of XRD beamline consists of a six-circle diffractometer and various detector systems such as scintillation detector, ionization chamber and image plate. The diffractometer can be controlled via EIA232 serial interface or Ethernet. Standard data acquisition software with a graphical user interface has been developed using LabVIEW. A firm safety and error handling scheme is implemented for failsafe operation of the experimental station. This paper describes in detail the data acquisition and control software for the experimental station.

  8. Diamond monochromators for APS undulator-A beamlines

    SciTech Connect

    Blasdell, R.C.; Assoufid, L.A.; Mills, D.M.

    1995-09-01

    There has been considerable interest in the use of diamonds in high heat load monochromators (HHLMs) in the last several years. The superb thermal and mechanical properties of single crystal diamonds serve to minimize distortions caused by a given thermal load, while the low x-ray absorption cross-section reduces both the total power deposited in the crystal as well as the peak (volumetric) power density. The primary obstacle for the widespread use of diamonds at present is a lack of ready availability of perfect single crystals of the desired size and orientation. Although it is possible to obtain near-perfect natural diamonds of the size and orientation required for use on an undulator beamline, the selection process is generally one of trial and error. Near perfect synthetic diamonds can currently be obtained in the minimum necessary size (typically 4-5 mm on a side). A collaborative agreement has been made between the staff of the Advanced Photon Source (APS), the European Synchrotron Radiation Facility (ESRF), and the Super Photon Ring-8 GeV (SPring-8) to explore the use of diamonds as high heat load monochromators and is on-going. One of the avenues of research is to push for improved perfection and size of synthetic diamonds. Sumitomo Electric Corporation of Japan has agreed to work with staff from SPring-8 to grow [100] oriented perfect single crystal diamonds of 10 x 10 x 1 mm{sup 3} size by 1996/1997 (from which one could also cut pieces with the large face parallel to the (111) planes). They have taken the first step in producing an essentially perfect 4 x 4 x 1 mm{sup 3} type II diamond with less than 5 {mu}rad (1 arc second) strain (measured over the entire surface). The authors believe progress in the production of synthetic diamonds, as well as improvement in ties with suppliers of natural diamonds, should make available a relatively large number of high quality diamonds of moderate size within the next several years.

  9. Correlated single-crystal electronic absorption spectroscopy and X-ray crystallography at NSLS beamline X26-C

    SciTech Connect

    Orville, A.M.; Buono, R.; Cowan, M.; Heroux, A.; Shea-McCarthy, G.; Schneider, D. K.; Skinner, J. M.; Skinner, M. J.; Stoner-Ma, D.; Sweet, R. M.

    2011-05-01

    The research philosophy and new capabilities installed at NSLS beamline X26-C to support electronic absorption and Raman spectroscopies coupled with X-ray diffraction are reviewed. This beamline is dedicated full time to multidisciplinary studies with goals that include revealing the relationship between the electronic and atomic structures in macromolecules. The beamline instrumentation has been fully integrated such that optical absorption spectra and X-ray diffraction images are interlaced. Therefore, optical changes induced by X-ray exposure can be correlated with X-ray diffraction data collection. The installation of Raman spectroscopy into the beamline is also briefly reviewed. Data are now routinely generated almost simultaneously from three complementary types of experiments from the same sample. The beamline is available now to the NSLS general user population.

  10. Note: Construction of x-ray scattering and x-ray absorption fine structure beamline at the Pohang Light Source

    SciTech Connect

    Lee, Ik-Jae; Yu, Chung-Jong; Yun, Young-Duck; Lee, Chae-Soon; Seo, In Deuk; Kim, Hyo-Yun; Lee, Woul-Woo; Chae, Keun Hwa

    2010-02-15

    A new hard x-ray beamline, 10B KIST-PAL beamline (BL10B), has been designed and constructed at the Pohang Light Source (PLS) in Korea. The beamline, operated by Pohang Accelerator Laboratory-Korean Institute of Science and Technology consortium, is dedicated to x-ray scattering (XRS) and x-ray absorption fine structure (XAFS) experiments. X rays with photon energies from 4.0 to 16.0 keV are delivered to the experimental station passing a collimating mirror, a fixed-exit double-crystal Si(111) monochromator, and a toroidal mirror. Basic experimental equipments for XAFS measurement, a high resolution diffractometry, an image plate detector system, and a hot stage have been prepared for the station. From our initial commissioning and performance testing of the beamline, it is observed that BL10B beamline can perform XRS and XAFS measurements successfully.

  11. Correlated Single-Crystal Electronic Absorption Spectroscopy and X-ray Crystallography at NSLS Beamline X26-C

    SciTech Connect

    A Orville; R Buono; M Cowan; A Heroux; G Shea-McCarthy; D Schneider; J Skinner; M Skinner; D Stoner-Ma; R Sweet

    2011-12-31

    The research philosophy and new capabilities installed at NSLS beamline X26-C to support electronic absorption and Raman spectroscopies coupled with X-ray diffraction are reviewed. This beamline is dedicated full time to multidisciplinary studies with goals that include revealing the relationship between the electronic and atomic structures in macromolecules. The beamline instrumentation has been fully integrated such that optical absorption spectra and X-ray diffraction images are interlaced. Therefore, optical changes induced by X-ray exposure can be correlated with X-ray diffraction data collection. The installation of Raman spectroscopy into the beamline is also briefly reviewed. Data are now routinely generated almost simultaneously from three complementary types of experiments from the same sample. The beamline is available now to the NSLS general user population.

  12. A summary of recent experimental results from Mark J: High energy e/sup +/e/sup /minus// collisions at PETRA: Report Number 131

    SciTech Connect

    Adeva, B.; Barber, D.P.; Becker, U.; Berdugo, J.; Bohm, A.; Branson, J.G.; Burger, J.D.; Capell, M.; Cerrada, M.; Chang, C.C.

    1983-12-01

    The PETRA electron-positron collider at DESY in Hamburg, Federal Republic of Germany, began operating in 1978, with four intersection regions devoted to experiments. In the intervening five years, five detector devices, CELLO, JADE, MARK-J, PLUTO and TASSO have accumulated and published a substantial variety of experimental results. The limits of validity of Quantum Electro-Dynamics (QED) have been extended; the pointlike nature of leptons and quarks have been probed at exceedingly small distances; the Glashow, Weinberg and Salam (GWS) '' standard electroweak model'' has been tested and found to describe interactions remarkably well; the predicted interference between electromagnetic and weak forces has been conclusively demonstrated; events with three jets have been discovered and interpreted as resulting from gluons, as predicted by Quantum Chromo-Dynamics (QCD); the sixth, ''top,'' quark has not been found yet, although an energy search for ''toponium'' (top + antitop) has been carried out up to 43.1 GeV center of mass energy. An integrated luminosity of about 100 pb/sup /minus/1/ mostly at energies above 30 GeV, has produced a very large sample of events. The present paper is a complete review and up-dating of all MARK-J physics results either published or unpublished. Since the amount of interesting information is so large, we realized that a coherent summation could be of substantial usefulness to the community. In order that this review can serve many needs, we include, a brief description of the apparatus and the data acquisition and analysis.

  13. Characterization of the high-energy neutron beam of the PRISMA beamline using a diamond detector

    NASA Astrophysics Data System (ADS)

    Cazzaniga, C.; Frost, C. D.; Minniti, T.; Schooneveld, E.; Perelli Cippo, E.; Tardocchi, M.; Rebai, M.; Gorini, G.

    2016-07-01

    The high-energy neutron component (En > 10 MeV) of the neutron spectrum of PRISMA, a beam-line at the ISIS spallation source, has been characterized for the first time. Neutron measurements using a Single-crystal Diamond Detector at a short-pulse source are obtained by a combination of pulse height and time of flight analysis. An XY scan provides a 2D map of the high-energy neutron beam which has a diameter of about 40 mm. The high neutron flux, that has been found to be (3.8 ± 0.7) · 105 cm‑2s‑1 for En > 10 MeV in the centre, opens up for a possible application of the beam-line as a high-energy neutron irradiation position. Results are of interest for the development of the ChipIR beam-line, which will feature an atmospheric-like neutron spectrum for chip irradiation experiment. Furthermore, these results demonstrate that diamond detectors can be used at spallation sources to investigate the transport of high-energy neutrons down instruments which is of interest in general to designers as high-energy neutrons are a source of background in thermal beamlines.

  14. Partially coherent wavefront propagation simulations for inelastic x-ray scattering beamline including crystal optics

    NASA Astrophysics Data System (ADS)

    Suvorov, Alexey; Cai, Yong Q.; Sutter, John P.; Chubar, Oleg

    2014-09-01

    Up to now simulation of perfect crystal optics in the "Synchrotron Radiation Workshop" (SRW) wave-optics computer code was not available, thus hindering the accurate modelling of synchrotron radiation beamlines containing optical components with multiple-crystal arrangements, such as double-crystal monochromators and high-energy-resolution monochromators. A new module has been developed for SRW for calculating dynamical diffraction from a perfect crystal in the Bragg case. We demonstrate its successful application to the modelling of partially-coherent undulator radiation propagating through the Inelastic X-ray Scattering (IXS) beamline of the National Synchrotron Light Source II (NSLS-II) at Brookhaven National Laboratory. The IXS beamline contains a double-crystal and a multiple-crystal highenergy- resolution monochromator, as well as complex optics such as compound refractive lenses and Kirkpatrick-Baez mirrors for the X-ray beam transport and shaping, which makes it an excellent case for benchmarking the new functionalities of the updated SRW codes. As a photon-hungry experimental technique, this case study for the IXS beamline is particularly valuable as it provides an accurate evaluation of the photon flux at the sample position, using the most advanced simulation methods and taking into account parameters of the electron beam, details of undulator source, and the crystal optics.

  15. Mass and charge overlaps in beamline implantation into compound semiconductor materials

    NASA Astrophysics Data System (ADS)

    Current, M. I.; Eddy, R.; Hudak, C.; Serfass, J.; Mount, G.

    2012-11-01

    Mass overlaps occurring as a result of extraction of ions from an arc discharge and gas collisions, producing molecular break up and charge exchange in the accelerator beamline, are examined for ion implantation into compound semiconductors. The effects of the choice of plasma gas elements for Be+ implants are examined as an example.

  16. The Structural Biology Center 19ID undulator beamline: facility specifications and protein crystallographic results

    PubMed Central

    Rosenbaum, Gerd; Alkire, Randy W.; Evans, Gwyndaf; Rotella, Frank J.; Lazarski, Krzystof; Zhang, Rong-Guang; Ginell, Stephan L.; Duke, Norma; Naday, Istvan; Lazarz, Jack; Molitsky, Michael J.; Keefe, Lisa; Gonczy, John; Rock, Larry; Sanishvili, Ruslan; Walsh, Martin A.; Westbrook, Edwin; Joachimiak, Andrzej

    2008-01-01

    The 19ID undulator beamline of the Structure Biology Center has been designed and built to take full advantage of the high flux, brilliance and quality of X-ray beams delivered by the Advanced Photon Source. The beamline optics are capable of delivering monochromatic X-rays with photon energies from 3.5 to 20 keV (3.5–0.6 Å wavelength) with fluxes up to 8–18 × 1012 photons s−1 (depending on photon energy) onto cryogenically cooled crystal samples. The size of the beam (full width at half-maximum) at the sample position can be varied from 2.2 mm × 1.0 mm (horizontal × vertical, unfocused) to 0.083 mm × 0.020 mm in its fully focused configuration. Specimen-to-detector distances of between 100 mm and 1500 mm can be used. The high flexibility, inherent in the design of the optics, coupled with a κ-geometry goniometer and beamline control software allows optimal strategies to be adopted in protein crystallographic experiments, thus maximizing the chances of their success. A large-area mosaic 3 × 3 CCD detector allows high-quality diffraction data to be measured rapidly to the crystal diffraction limits. The beamline layout and the X-ray optical and endstation components are described in detail, and the results of representative crystallographic experiments are presented. PMID:16371706

  17. Novel characteristics of VUV insertion device beamlines at the Advanced Light Source

    SciTech Connect

    Warwick, T.; Heimann, P.

    1991-10-01

    The design of VUV beamlines for the Advanced Light Source is discussed. Features of the design serve to illustrate the careful attention required in order to preserve the performance of the low emittance ``third generation`` storage ring, operating with insertion devices. 11 refs.

  18. Novel characteristics of VUV insertion device beamlines at the Advanced Light Source

    SciTech Connect

    Warwick, T.; Heimann, P.

    1991-10-01

    The design of VUV beamlines for the Advanced Light Source is discussed. Features of the design serve to illustrate the careful attention required in order to preserve the performance of the low emittance third generation'' storage ring, operating with insertion devices. 11 refs.

  19. Neutrinos from the NuMI beamline in the MiniBooNE detector

    SciTech Connect

    Aguilar-Arevalo, Alexis A.

    2006-07-11

    With the startup of the NuMI beamline early in 2005, the MiniBooNE detector has the unique opportunity to be the first user of an off-axis neutrino beam (110 mrad off-axis). MiniBooNE is assembling a rich sample of neutrino interactions from this source.

  20. Characteristics and performance of the Los Alamos VUV beamline at the NSLS

    NASA Astrophysics Data System (ADS)

    Bartlett, R. J.; Trela, W. J.; Michaud, F. D.; Southworth, S. H.; Alkire, R. W.; Roy, P.; Rothe, R.; Walsh, P. J.; Shinn, N.

    1988-04-01

    We describe the design and performance of the Los Alamos VUV synchrotron radiation beamline, U3C, on the VUV ring of the National Synchrotron Light Source at Brookhaven National Laboratory. The beamline uses separate function optics to collect and focus the horizontally and vertically diverging beam. The monochromator is a grazing incidence Rowland circle instrument of the extended grasshopper design (ERG). A postmonochromator refocusing mirror is used to focus or collimate the diverging beam from the monochromator. The beamline control and diagnostics systems are also discussed. Particular emphasis in the design has been placed on the reduction of stray and harmonic light. Higher order light is reduced by a grazing angle mirror low pass filter installed immediately downstream from the monochromator while stray light is reduced through the use of baffles and thin film filters. Also included in the line is a differential pumping section that permits gas phase and other experiments requiring pressures in the 10 -5 to 10 -4 Torr range to be coupled to the beamline.

  1. The multi-purpose hard X-ray beamline BL10 at the DELTA storage ring.

    PubMed

    Lützenkirchen-Hecht, D; Wagner, R; Szillat, S; Hüsecken, A K; Istomin, K; Pietsch, U; Frahm, Ronald

    2014-07-01

    The layout and the characteristics of the hard X-ray beamline BL10 at the superconducting asymmetric wiggler at the 1.5 GeV Dortmund Electron Accelerator DELTA are described. This beamline is equipped with a Si(111) channel-cut monochromator and is dedicated to X-ray studies in the spectral range from ∼4 keV to ∼16 keV photon energy. There are two different endstations available. While X-ray absorption studies in different detection modes (transmission, fluorescence, reflectivity) can be performed on a designated table, a six-axis kappa diffractometer is installed for X-ray scattering and reflectivity experiments. Different detector set-ups are integrated into the beamline control software, i.e. gas-filled ionization chambers, different photodiodes, as well as a Pilatus 2D-detector are permanently available. The performance of the beamline is illustrated by high-quality X-ray absorption spectra from several reference compounds. First applications include temperature-dependent EXAFS experiments from liquid-nitrogen temperature in a bath cryostat up to ∼660 K by using a dedicated furnace. Besides transmission measurements, fluorescence detection for dilute sample systems as well as surface-sensitive reflection-mode experiments are presented.

  2. Characterization of the high-energy neutron beam of the PRISMA beamline using a diamond detector

    NASA Astrophysics Data System (ADS)

    Cazzaniga, C.; Frost, C. D.; Minniti, T.; Schooneveld, E.; Perelli Cippo, E.; Tardocchi, M.; Rebai, M.; Gorini, G.

    2016-07-01

    The high-energy neutron component (En > 10 MeV) of the neutron spectrum of PRISMA, a beam-line at the ISIS spallation source, has been characterized for the first time. Neutron measurements using a Single-crystal Diamond Detector at a short-pulse source are obtained by a combination of pulse height and time of flight analysis. An XY scan provides a 2D map of the high-energy neutron beam which has a diameter of about 40 mm. The high neutron flux, that has been found to be (3.8 ± 0.7) · 105 cm-2s-1 for En > 10 MeV in the centre, opens up for a possible application of the beam-line as a high-energy neutron irradiation position. Results are of interest for the development of the ChipIR beam-line, which will feature an atmospheric-like neutron spectrum for chip irradiation experiment. Furthermore, these results demonstrate that diamond detectors can be used at spallation sources to investigate the transport of high-energy neutrons down instruments which is of interest in general to designers as high-energy neutrons are a source of background in thermal beamlines.

  3. Thermal management for LLNL/UC/SSRL bending magnet beamline VIII at Stanford Synchrotron Radiation Laboratory

    SciTech Connect

    Berglin, E.J.; Younger, F.C.

    1986-05-01

    All the important heat loads on the elements of Beamline VIII are cataloged. The principal elements are identified and their heat loads tabulated for various loading scenarios. The expected heat loads are those from normal operations including the anticipated performance improvements planned for the SPEAR ring and from abnormal operations due to positional perturbations of the electron beam. (LEW)

  4. Photostimulated phosphor based image plate detection system for HRVUV beamline at Indus-1 synchrotron radiation source

    NASA Astrophysics Data System (ADS)

    Haris, K.; Singh, Param Jeet; Shastri, Aparna; Sunanda, K.; Babita, K.; Rao, S. V. N. Bhaskara; Ahmad, Shabbir; Tauheed, A.

    2014-12-01

    A high resolution vacuum ultraviolet (HRVUV) beamline based on a 6.65 m off-plane Eagle spectrometer is in operation at the Indus-1 synchrotron radiation source, RRCAT, Indore, India. To facilitate position sensitive detection and fast spectral recording, a new BaFBr:Eu2+ phosphor based image plate (IP) detection system interchangeable with the existing photomultiplier (PMT) scanning system has been installed on this beamline. VUV photoabsorption studies on Xe, O2, N2O and SO2 are carried out to evaluate the performance of the IP detection system. An FWHM of ~0.5 Å is achieved for the Xe atomic line at 1469.6 Å. Reproducibility of spectra is found to be within the experimental resolution. Compared to the PMT scanning system, the IP shows several advantages in terms of sensitivity, recording time and S/N ratio, which are highlighted in the paper. This is the first report of incorporation of an IP detection system in a VUV beamline using synchrotron radiation. Commissioning of the new detection system is expected to greatly enhance the utilization of the HRVUV beamline as a number of spectroscopic experiments which require fast recording times combined with a good signal to noise ratio are now feasible.

  5. TIME-RESOLVED INFRARED SPECTROSCOPY IN THE U121R BEAMLINE AT THE NSLS

    SciTech Connect

    CARR,G.L.; LAVEIGNE,J.D.; LOBO,R.P.S.M.; REITZE,D.H.; TANNER,D.B.

    1999-07-19

    A facility for performing time-resolved infrared spectroscopy has been developed at the NSLS, primarily at beamline U12IR. The pulsed IR light from the synchrotron is used to perform pump-probe spectroscopy. The authors present here a description of the facility and results for the relaxation of photoexcitations in both a semiconductor and superconductor.

  6. Paraxial SGM beamlines for coherence experiments at the Advanced Light Source

    SciTech Connect

    Warwick, Anthony I; Warwick, Anthony I; Howells, Malcolm

    2008-07-24

    Beamlines have been designed for coherence experiments at the ALS based on brightness preserving spherical grating monochromators. The operation is almost paraxial so that a very simple scheme can deliver the modest spectral resolution required, with just two focusing optics, one of which is the spherical grating.

  7. Focusing, collimation and flux throughput at the IMCA-CAT bending-magnet beamline at the Advanced Photon Source.

    PubMed

    Koshelev, Irina; Huang, Rong; Graber, Timothy; Meron, Mati; Muir, J Lewis; Lavender, William; Battaile, Kevin; Mulichak, Anne M; Keefe, Lisa J

    2009-09-01

    The IMCA-CAT bending-magnet beamline was upgraded with a collimating mirror in order to achieve the energy resolution required to conduct high-quality multi- and single-wavelength anomalous diffraction (MAD/SAD) experiments without sacrificing beamline flux throughput. Following the upgrade, the bending-magnet beamline achieves a flux of 8 x 10(11) photons s(-1) at 1 A wavelength, at a beamline aperture of 1.5 mrad (horizontal) x 86 microrad (vertical), with energy resolution (limited mostly by the intrinsic resolution of the monochromator optics) deltaE/E = 1.5 x 10(-4) (at 10 kV). The beamline operates in a dynamic range of 7.5-17.5 keV and delivers to the sample focused beam of size (FWHM) 240 microm (horizontally) x 160 microm (vertically). The performance of the 17-BM beamline optics and its deviation from ideally shaped optics is evaluated in the context of the requirements imposed by the needs of protein crystallography experiments. An assessment of flux losses is given in relation to the (geometric) properties of major beamline components.

  8. A comparison of three different ray trace programs for x-ray and infrared synchrotron beamline designs

    SciTech Connect

    Irick, S.C.; Jung, C.R.

    1997-07-01

    There are a number of ray trace programs currently used for the design of synchrotron beamlines. While several of these programs have been written and used mostly within the programmer`s institution, many have also been available to the general public. This paper discusses three such programs. One is a commercial product oriented for the general optical designer (not specifically for synchrotron beamlines). One is designed for synchrotron beamlines and is free with restricted availability. Finally, one is designed for synchrotron beamlines and is used primarily in one institution. The wealth of information from general optical materials and components catalogs is readily available in the commercial program for general optical designs. This makes the design of an infrared beamline easier from the standpoint of component selection. However, this program is not easily configured for synchrotron beamline designs, particularly for a bending magnet source. The synchrotron ray trace programs offer a variety of sources, but generally are not as easy to use from the standpoint of the user interface. This paper shows ray traces of the same beamline Optikwerks, SHADOW, and RAY, and compares the results.

  9. 7-GeV advanced photon source beamline initiative: Conceptual design report

    SciTech Connect

    Not Available

    1993-05-01

    The DOE is building a new generation 6-7 GeV Synchrotron Radiation Source known as the Advanced Photon Source (APS) at Argonne National Laboratory. This facility, to be completed in FY 1996, can provide 70 x-ray sources of unprecedented brightness to meet the research needs of virtually all scientific disciplines and numerous technologies. The technological research capability of the APS in the areas of energy, communications and health will enable a new partnership between the DOE and US industry. Current funding for the APS will complete the current phase of construction so that scientists can begin their applications in FY 1996. Comprehensive utilization of the unique properties of APS beams will enable cutting-edge research not currently possible. It is now appropriate to plan to construct additional radiation sources and beamline standard components to meet the excess demands of the APS users. In this APS Beamline Initiative, 2.5-m-long insertion-device x-ray sources will be built on four straight sections of the APS storage ring, and an additional four bending-magnet sources will also be put in use. The front ends for these eight x-ray sources will be built to contain and safeguard access to these bright x-ray beams. In addition, funds will be provided to build standard beamline components to meet scientific and technological research demands of the Collaborative Access Teams. The Conceptual Design Report (CDR) for the APS Beamline Initiative describes the scope of all the above technical and conventional construction and provides a detailed cost and schedule for these activities. The document also describes the preconstruction R&D plans for the Beamline Initiative activities and provides the cost estimates for the required R&D.

  10. Nanoscopium: a Scanning Hard X-ray Nanoprobe Beamline at Synchrotron Soleil

    NASA Astrophysics Data System (ADS)

    Somogyi, A.; Polack, F.; Moreno, T.

    2010-06-01

    Nanoscopium is the single scanning hard X-ray nano-probe beamline planned at SOLEIL. This ˜155 m long beamline will fully exploit the high brilliance and coherence characteristics of the X-ray beam both for diffraction limited focusing and for contrast formation. It will offer the most advanced imaging techniques in multimodal mode and will be a research tool for a wide user community working in the fields of earth-, environmental-, and life-sciences. The different μ-μnano-probe techniques offered by the beamline will permit elemental mapping at trace (ppm) levels (scanning XRF), speciation mapping (XANES), phase gradient mapping (scanning differential phase contrast), and density-contrast based imaging of internal structures (coherent diffraction imaging) in the 30 nm to 1 μm spatial resolution range, also in "in situ conditions". Nanoscopium will cover the 5-20 keV energy range. The stability of the nanobeam will be ensured by horizontally reflecting beamline optics (a sagitally and a tangentially pre-focusing mirror, horizontally reflecting monochromators) in front of the overfilled secondary source. Trade-off between high energy resolution (ΔE/E˜10-4) and high flux (1011 ph/s with ΔE/E˜10-2) will be achieved by two interchangeable monochromators (a double crystal and a double multilayer one). KB mirror and FZP lenses will be used as focusing devices. The beamline is in the design and construction phase. It is foreseen to be open for users at the beginning of 2013.

  11. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules

    PubMed Central

    Bowler, Matthew W.; Nurizzo, Didier; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine; Caserotto, Hugo; Delagenière, Solange; Dobias, Fabian; Flot, David; Giraud, Thierry; Guichard, Nicolas; Guijarro, Mattias; Lentini, Mario; Leonard, Gordon A.; McSweeney, Sean; Oskarsson, Marcus; Schmidt, Werner; Snigirev, Anatoli; von Stetten, David; Surr, John; Svensson, Olof; Theveneau, Pascal; Mueller-Dieckmann, Christoph

    2015-01-01

    MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined. PMID:26524320

  12. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules.

    PubMed

    Bowler, Matthew W; Nurizzo, Didier; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine; Caserotto, Hugo; Delagenière, Solange; Dobias, Fabian; Flot, David; Giraud, Thierry; Guichard, Nicolas; Guijarro, Mattias; Lentini, Mario; Leonard, Gordon A; McSweeney, Sean; Oskarsson, Marcus; Schmidt, Werner; Snigirev, Anatoli; von Stetten, David; Surr, John; Svensson, Olof; Theveneau, Pascal; Mueller-Dieckmann, Christoph

    2015-11-01

    MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined. PMID:26524320

  13. MASSIF-1: a beamline dedicated to the fully automatic characterization and data collection from crystals of biological macromolecules.

    PubMed

    Bowler, Matthew W; Nurizzo, Didier; Barrett, Ray; Beteva, Antonia; Bodin, Marjolaine; Caserotto, Hugo; Delagenière, Solange; Dobias, Fabian; Flot, David; Giraud, Thierry; Guichard, Nicolas; Guijarro, Mattias; Lentini, Mario; Leonard, Gordon A; McSweeney, Sean; Oskarsson, Marcus; Schmidt, Werner; Snigirev, Anatoli; von Stetten, David; Surr, John; Svensson, Olof; Theveneau, Pascal; Mueller-Dieckmann, Christoph

    2015-11-01

    MASSIF-1 (ID30A-1) is an ESRF undulator beamline operating at a fixed wavelength of 0.969 Å (12.8 keV) that is dedicated to the completely automatic characterization of and data collection from crystals of biological macromolecules. The first of the ESRF Upgrade MASSIF beamlines to be commissioned, it has been open since September 2014, providing a unique automated data collection service to academic and industrial users. Here, the beamline characteristics and details of the new service are outlined.

  14. Expected thermal deformation and wavefront preservation of a cryogenic Si monochromator for Cornell ERL beamlines

    PubMed Central

    Huang, Rong; Bilderback, Donald H.; Finkelstein, Kenneth

    2014-01-01

    Cornell energy-recovery linac (ERL) beamlines will have higher power density and higher fractional coherence than those available at third-generation sources; therefore the capability of a monochromator for ERL beamlines has to be studied. A cryogenic Si monochromator is considered in this paper because the perfect atomic structure of Si crystal is needed to deliver highly coherent radiation. Since neither the total heat load nor the power density alone can determine the severity of crystal deformation, a metric called modified linear power density is used to gauge the thermal deformation. For all ERL undulator beamlines, crystal thermal deformation profiles are simulated using the finite-element analysis tool ANSYS, and wavefront propagations are simulated using Synchrotron Radiation Workshop. It is concluded that cryogenic Si monochromators will be suitable for ERL beamlines in general. PMID:24562557

  15. National Synchrotron Light Source user`s manual: Guide to the VUV and x-ray beamlines. Fifth edition

    SciTech Connect

    Gmuer, N.F.

    1993-04-01

    The success of the National Synchrotron Light Source is based, in large part, on the size of the user community and the diversity of the scientific and technical disciplines represented by these users. As evidence of this success, the VUV Ring has just celebrated its 10th anniversary and the X-ray Ring will do the same in 1995. In order to enhance this success, the NSLS User`s Manual: Guide to the VUV and X-Ray Beamlines - Fifth Edition, is being published. This Manual presents to the scientific community-at-large the current and projected architecture, capabilities and research programs of the various VUV and X-ray beamlines. Also detailed is the research and computer equipment a General User can expect to find and use at each beamline when working at the NSLS. The Manual is updated periodically in order to keep pace with the constant changes on these beamlines.

  16. Expected thermal deformation and wavefront preservation of a cryogenic Si monochromator for Cornell ERL beamlines.

    PubMed

    Huang, Rong; Bilderback, Donald H; Finkelstein, Kenneth

    2014-03-01

    Cornell energy-recovery linac (ERL) beamlines will have higher power density and higher fractional coherence than those available at third-generation sources; therefore the capability of a monochromator for ERL beamlines has to be studied. A cryogenic Si monochromator is considered in this paper because the perfect atomic structure of Si crystal is needed to deliver highly coherent radiation. Since neither the total heat load nor the power density alone can determine the severity of crystal deformation, a metric called modified linear power density is used to gauge the thermal deformation. For all ERL undulator beamlines, crystal thermal deformation profiles are simulated using the finite-element analysis tool ANSYS, and wavefront propagations are simulated using Synchrotron Radiation Workshop. It is concluded that cryogenic Si monochromators will be suitable for ERL beamlines in general.

  17. Guide to LIBXSIF, a Library for Parsing the Extended Standard Input Format of Accelerated Beamlines(LCC-0060)

    SciTech Connect

    Tenenbaum, P

    2003-12-03

    We describe LIBXSIF, a standalone library for parsing the Extended Standard Input Format of accelerator beamlines. Included in the description are: documentation of user commands; full description of permitted accelerator elements and their attributes; the construction of beamline lists; the mechanics of adding LIBXSIF to an existing program; and ''under the hood'' details for users who wish to modify the library or are merely morbidly curious.

  18. 2-ps Hard X-Ray Streak Camera Measurements at Sector 7 Beamline of the Advanced Photon Source

    SciTech Connect

    Chollet, M.; Ahr, B.; Walko, D.A.; Rose-Petruck, C.; Adams, B.

    2011-08-02

    A hard X-ray streak camera capable of 2-ps time resolution is in operation at the Sector 7 beamline of the Advanced Photon Source. It is used for laser-pump, X-ray probe experiments using the Ti:Sapphire femtosecond laser system installed on the beamline. This streak camera, combined with standardized and prealigned experimental setups, can perform time-resolved liquid-phase absorption spectroscopy, reflectivity, and diffraction experiments.

  19. PARALLEL MEASUREMENT AND MODELING OF TRANSPORT IN THE DARHT II BEAMLINE ON ETA II

    SciTech Connect

    Chambers, F W; Raymond, B A; Falabella, S; Lee, B S; Richardson, R A; Weir, J T; Davis, H A; Schultze, M E

    2005-05-31

    To successfully tune the DARHT II transport beamline requires the close coupling of a model of the beam transport and the measurement of the beam observables as the beam conditions and magnet settings are varied. For the ETA II experiment using the DARHT II beamline components this was achieved using the SUICIDE (Simple User Interface Connecting to an Integrated Data Environment) data analysis environment and the FITS (Fully Integrated Transport Simulation) model. The SUICIDE environment has direct access to the experimental beam transport data at acquisition and the FITS predictions of the transport for immediate comparison. The FITS model is coupled into the control system where it can read magnet current settings for real time modeling. We find this integrated coupling is essential for model verification and the successful development of a tuning aid for the efficient convergence on a useable tune. We show the real time comparisons of simulation and experiment and explore the successes and limitations of this close coupled approach.

  20. Calibration and standards beamline 6.3.2 at the ALS

    SciTech Connect

    Underwood, J.H.; Gullikson, E.M.; Koike, M.

    1997-04-01

    More sophisticated optics for the x-ray, soft x-ray and far ultraviolet spectral regions being developed for synchrotron radiation research and many other applications, require accurate calibration and standards facilities for measuring reflectivity of mirrors and multilayer coatings, transmission of thin films, bandpass of multilayers, efficiency of gratings or detectors, etc. For this purpose beamline 6.3.2 was built at the ALS. Its energy coverage, versatility, simplicity and convenience also make it useful for a wide range of other experiments. The paper describes the components of this beamline, consisting of: a four jaw aperture; a horizontal focusing mirror; a monochromator; exit slit; vertical focusing mirror; mechanical and vacuum system; reflectometer; filter wheels; and data acquisition system.

  1. Jefferson Lab Hall A Beamline Instrumentation and Calibration for GMP experiment

    NASA Astrophysics Data System (ADS)

    Gautam, Thir Narayan

    2015-10-01

    The nucleon electromagnetic form factors characterize the distributions of electric charge and magnetization current inside the nucleon and thus reflect the internal structure determined by Quantum Chromodynamics. The GMp experiment is a first experiment run in Hall A at Jefferson Lab after the upgrade to double the beam energy with the goal to precisely measure electron-proton elastic cross section in the Q2 range of 7 to 17 GeV2 with an accuracy of better than 2%; several time better than existing data at the highest Q2. In order to achieve this accuracy, a determination of the accumulated beam charge of better than 0.5% is required. The new 12 GeV beamline was commissioned during the spring of 2015, with the main instrumentation consisting of beam charge and position monitors. In this talk, the procedures and the results of the calibrations of these beamline components will be presented.

  2. Directly water-cooled crystal development for SPring-8 bending magnet beamlines

    NASA Astrophysics Data System (ADS)

    Takeshita, Kunikazu; Goto, Shunji; Ishikawa, Tetsuya

    2007-09-01

    The directly water-cooled first crystal of the SPring-8 standard monochromator for bending magnet beamlines has been developed. Thanks to the bonding technique, the performance of the new crystal has been improved without decreasing the cooling efficiency. The finite element analyses show the deformation of the crystal by the hydraulic pressure and by the crystal clamping is negligible small, which were dominated for the previous crystal. Both Si(111) and Si(311) crystal were evaluated in SPring-8 beamlines, the deformation induced while the bonding process is comparable to the thermal deformation. and long-term endurance test shows the lifetime of the O-ring becomes long because they are not on the direct path of the SR beam. Although the overall performance is insufficient, much improvement was shown.

  3. Energy optimization of a regular macromolecular crystallography beamline for ultra-high-resolution crystallography

    SciTech Connect

    Rosenbaum, Gerd; Ginell, Stephan L.; Chen, Julian C.-H.

    2015-01-01

    In this study, a practical method for operating existing undulator synchrotron beamlines at photon energies considerably higher than their standard operating range is described and applied at beamline 19-ID of the Structural Biology Center at the Advanced Photon Source enabling operation at 30 keV. Adjustments to the undulator spectrum were critical to enhance the 30 keV flux while reducing the lower- and higher-energy harmonic contamination. A Pd-coated mirror and Al attenuators acted as effective low- and high-bandpass filters. The resulting flux at 30 keV, although significantly lower than with X-ray optics designed and optimized for this energy, allowed for accurate data collection on crystals of the small protein crambin to 0.38 Å resolution.

  4. In-vacuum sensors for the beamline components of the ITER neutral beam test facility

    NASA Astrophysics Data System (ADS)

    Dalla Palma, M.; Pasqualotto, R.; Sartori, E.; Spagnolo, S.; Spolaore, M.; Veltri, P.

    2016-11-01

    Embedded sensors have been designed for installation on the components of the MITICA beamline, the prototype ITER neutral beam injector (Megavolt ITER Injector and Concept Advancement), to derive characteristics of the particle beam and to monitor the component conditions during operation for protection and thermal control. Along the beamline, the components interacting with the particle beam are the neutralizer, the residual ion dump, and the calorimeter. The design and the positioning of sensors on each component have been developed considering the expected beam-surface interaction including non-ideal and off-normal conditions. The arrangement of the following instrumentation is presented: thermal sensors, strain gages, electrostatic probes including secondary emission detectors, grounding shunt for electrical currents, and accelerometers.

  5. Energy optimization of a regular macromolecular crystallography beamline for ultra-high-resolution crystallography

    DOE PAGES

    Rosenbaum, Gerd; Ginell, Stephan L.; Chen, Julian C.-H.

    2015-01-01

    In this study, a practical method for operating existing undulator synchrotron beamlines at photon energies considerably higher than their standard operating range is described and applied at beamline 19-ID of the Structural Biology Center at the Advanced Photon Source enabling operation at 30 keV. Adjustments to the undulator spectrum were critical to enhance the 30 keV flux while reducing the lower- and higher-energy harmonic contamination. A Pd-coated mirror and Al attenuators acted as effective low- and high-bandpass filters. The resulting flux at 30 keV, although significantly lower than with X-ray optics designed and optimized for this energy, allowed for accuratemore » data collection on crystals of the small protein crambin to 0.38 Å resolution.« less

  6. A Superbend X-Ray Microdiffraction Beamline at the Advanced Light Source

    SciTech Connect

    Tamura, N.; Kunz, M.; Chen, K.; Celestre, R.S.; MacDowell, A.A.; Warwick, T.

    2009-03-10

    Beamline 12.3.2 at the Advanced Light Source is a newly commissioned beamline dedicated to x-ray microdiffraction. It operates in both monochromatic and polychromatic radiation mode. The facility uses a superconducting bending magnet source to deliver an X-ray spectrum ranging from 5 to 22 keV. The beam is focused down to {approx} 1 um size at the sample position using a pair of elliptically bent Kirkpatrick-Baez mirrors enclosed in a vacuum box. The sample placed on high precision stages can be raster-scanned under the microbeam while a diffraction pattern is taken at each step. The arrays of diffraction patterns are then analyzed to derive distribution maps of phases, strain/stress and/or plastic deformation inside the sample.

  7. The PGM-Beamline at the Undulator U55 at DELTA

    SciTech Connect

    Berges, U.; Westphal, C.; Krause, M.; Schuermann, M.; Dreiner, S.; Follath, R.; Schaefers, F.

    2004-05-12

    A beamline for linearly polarized light radiation from an undulator is being commissioned at DELTA, an University synchrotron facility. The electron beam in the undulator as a radiation source is mapped by the first optical element onto an intermediate focus. Mirror M1 has a large acceptance angle in order to provide a stable performance if small electron beam displacements occur. The intermediate focus is demagnified onto the sample providing a focus spot size of 70 x 30{mu}m2. The PGM (Plane Grating Monochromator) based beamline works with collimated light allowing a flexible use of the monochromator. Depending on user demands, it can be operated by at high spectral resolution, high flux mode, or at high order suppression.

  8. Modeling of the primary proton beamline of the Fermilab NuMI project

    SciTech Connect

    Sergei Striganov et al.

    2001-08-14

    The 120 GeV primary proton beamline for the NuMI-MINOS [1] experiment at Fermilab will transport one of the most intense high-energy beams ever constructed. in parallel operation with the Collider program, 80% of the intensity capability of the Fermilab Main Injector can be sent to NuMI. Radiation safety pertaining to residual activity, damage of equipment and irradiation of groundwater is a primary concern. A particular challenge is that this beam will be transported to and targeted in a cavern excavated in rock in an aquifer region. A model of the beamline, including transport elements and excavated enclosures, has been built in the radiation simulation program MARS. This model has been used to determine limits for allowable beam loss, and to study effects of instabilities and of various failure types. Some results obtained with this model are presented.

  9. Recent developments on techniques for differential phase imaging at the medical beamline of ELETTRA

    NASA Astrophysics Data System (ADS)

    Arfelli, F.; Pelliccia, D.; Cedola, A.; Astolfo, A.; Bukreeva, I.; Cardarelli, P.; Dreossi, D.; Lagomarsino, S.; Longo, R.; Rigon, L.; Sodini, N.; Menk, R. H.

    2013-06-01

    Over the last decade different phase contrast approaches have been exploited at the medical beamline SYRMEP of the synchrotron radiation facility Elettra in Trieste, Italy. In particular special focus has been drawn to analyzer based imaging and the associated imaging theory and processing. Analyzer based Imaging (ABI) and Diffraction Enhanced Imaging (DEI) techniques have been successfully applied in several biomedical applications. Recently it has been suggested to translate the acquired knowledge in this field towards a Thomson Backscattering Source (TBS), which is presently under development at the Frascati National Laboratories of INFN (Istituto Nazionale di Fisica Nucleare) in Rome, Italy. Such source is capable of producing intense and quasi-monochromatic hard X-ray beams. For the technical implementation of biomedical phase imaging at the TBS a grating interferometer for differential phase contrast imaging has been designed and successfully tested at SYRMEP beamline.

  10. A multipurpose monochromator for the BESSRC CAT beamlines at the APS X-ray facility

    SciTech Connect

    Jung, M.; Beno, M.A.; Cowan, P.L.

    1996-05-01

    The Basic Energy Science Synchrotron Radiation Center Collaborative Access Team (BESSRC-CAT) is constructing x-ray beamlines at two sectors of the Advanced Photon Source facility. In most of the beamlines the first optical element will be a monochromator, so that a standard design for this critical component is advantageous. The mnochromator is a double crystal, fixed exit scheme with a constant offset designed for UHV windowless operation. In this design, the crystals are mounted on a turntable with the first crystal at the center of rotation. Mechanical linkages are used to correctly position the second crystal and maintain a constant offset. The authors report here the final test results achieved on an optical table with an autocollimator and the first measurements with x-rays from the bending magnet.

  11. Photon-beam stabilization systems for the MX2 beamline at LNLS

    NASA Astrophysics Data System (ADS)

    Sanfelici, Lucas; de Mattos, Fernando

    2011-09-01

    The MX2, a wiggler beamline dedicated to macromolecular crystallography, started routinely operating for users in 2007. Late in the commissioning phase, several experiments started to be conducted in order to characterize photon-beam stability. At that time, position movements of typically 150 μm per shift and severe energy drifts reaching 0.8 eV/h were observed at sample position, which would certainly spoil the MAD experiments. The severity of this scenario for a recently delivered beamline led us to install temperature sensors and inclinometers along the optical hutch, besides performing exhaustive tests to clarify the disturbance paths. To elucidate the main instability mechanisms, three control systems for beam stabilization were considered—position stabilization, ground motion canceling and, the most important of all, temperature control for the optical hutch. Results and perspectives are presented hereafter.

  12. Undulator beamline optimization with integrated chicanes for X-ray free-electron-laser facilities.

    PubMed

    Prat, Eduard; Calvi, Marco; Ganter, Romain; Reiche, Sven; Schietinger, Thomas; Schmidt, Thomas

    2016-07-01

    An optimization of the undulator layout of X-ray free-electron-laser (FEL) facilities based on placing small chicanes between the undulator modules is presented. The installation of magnetic chicanes offers the following benefits with respect to state-of-the-art FEL facilities: reduction of the required undulator length to achieve FEL saturation, improvement of the longitudinal coherence of the FEL pulses, and the ability to produce shorter FEL pulses with higher power levels. Numerical simulations performed for the soft X-ray beamline of the SwissFEL facility show that optimizing the advantages of the layout requires shorter undulator modules than the standard ones. This proposal allows a very compact undulator beamline that produces fully coherent FEL pulses and it makes possible new kinds of experiments that require very short and high-power FEL pulses. PMID:27359133

  13. Indus-2 X-ray lithography beamline for X-ray optics and material science applications

    SciTech Connect

    Dhamgaye, V. P. Lodha, G. S.

    2014-04-24

    X-ray lithography is an ideal technique by which high aspect ratio and high spatial resolution micro/nano structures are fabricated using X-rays from synchrotron radiation source. The technique has been used for fabricating optics (X-ray, visible and infrared), sensors and actuators, fluidics and photonics. A beamline for X-ray lithography is operational on Indus-2. The beamline offers wide lithographic window from 1-40keV photon energy and wide beam for producing microstructures in polymers upto size ∼100mm × 100mm. X-ray exposures are possible in air, vacuum and He gas environment. The air based exposures enables the X-ray irradiation of resist for lithography and also irradiation of biological and liquid samples.

  14. Surveying and optical tooling technologies combined to align a skewed beamline at the LAMPF accelerator

    SciTech Connect

    Bauke, W.; Clark, D.A.; Trujillo, P.B.

    1985-01-01

    Optical Tooling evolved from traditional surveying, and both technologies are sometimes used interchangeably in large industrial installations, since the instruments and their specialized adapters and supports complement each other well. A unique marriage of both technologies was accomplished in a novel application at LAMPF, the Los Alamos Meson Physics Facility. LAMPF consists of a linear accelerator with multiple target systems, one of which had to be altered to accommodate a new beamline for a neutrino experiment. The new line was to be installed into a crowded beam tunnel and had to be skewed and tilted in compound angles to avoid existing equipment. In this paper we describe how Optical Tooling was used in conjunction with simple alignment and reference fixtures to set fiducials on the magnets and other mechanical components of the beamline, and how theodolites and sight levels were then adapted to align these components along the calculated skew planes. Design tolerances are compared with measured alignment results.

  15. New developments at the INE-Beamline for actinide research at ANKA

    NASA Astrophysics Data System (ADS)

    Brendebach, B.; Dardenne, K.; Denecke, M. A.; Rothe, J.; Vitova, T.

    2007-11-01

    The INE-Beamline for actinide research at the synchrotron source Ångströmquelle Karlsruhe (ANKA) completed its first year of operation in October 2006. Experiments on radioactive samples with activities up to 10 6 times the limit of exemption at X-ray energies from around 2.1 keV (P K-edge) to 25 keV (Pd K-edge) are possible. Three recent instrumental developments at the Nuclear Waste Disposal (INE)-Beamline are presented: a Quick-XAFS mode of operating the Lemonnier-type monochromator in fixed exit for time-resolved experiments, total electron yield detection, and the use of one-dimensional compound refractive lenses, fabricated at the Institut für Mikrostrukturtechnik (IMT) at Forschungszentrum Karlsruhe (FZK), as a virtual slit for surface sensitive X-ray studies. Future upgrades for lowering the attainable energy, installing a microfocus option, and commissioning a cryostat for radioactive samples are planned.

  16. Vertical synchrotron radiation beamline for proximity X-ray lithography: Theoretical analysis

    NASA Astrophysics Data System (ADS)

    Bukreeva, Inna N.; Kozhevnikov, Igor V.

    1997-02-01

    The general physical principles of operation of the vertical beamline of synchrotron radiation (SR) intended for proximity X-ray lithography are considered. An optical system provides a deflection of the SR beam to the vertical plane, a cutoff of the hard X-rays, a uniform illumination of a wafer, a normal incidence of X-ray beam onto a mask, and a small enough divergency of the radiation. A vertical SR beamline makes it possible to circumvent the expensive development of vertical-plane displacement steppers and to use the conventional horizontal ones, to exclude the scanning of the SR beam across the mask and to reduce the requirements imposed on the accuracy of alignment of a gap between the mask and the wafer.

  17. Design, fabrication and test of the steering magnet for the KOMAC beamline

    NASA Astrophysics Data System (ADS)

    Chung, Bo-Hyun

    2015-10-01

    The Korea Multi-purpose Accelerator Complex (KOMAC) is operating a 100-MeV proton linac. The beamline facility of the KOMAC has both a 20-MeV beam and a 100-MeV beam for users. Steering magnets are added to the beamlines to adjust the position of the beam on the target. The uniformity and the harmonics of the magnetic field are computed by using the Poisson code, and the integrated magnetic field is computed by using the CST EM Studio. The designed magnets were fabricated, and the field's uniformity and the integrated field were measured. The designed and fabricated steering magnets were characterized, and the results are presented in this paper. The results are expected to improve the beam performance, in particular, accurate delivery to the target.

  18. Dedicated Max-Planck beamline for the in situ investigation of interfaces and thin films

    SciTech Connect

    Stierle, A.; Steinhaeuser, A.; Ruehm, A.; Renner, F.U.; Weigel, R.; Kasper, N.; Dosch, H.

    2004-12-01

    A dedicated beamline for the Max-Planck-Institut fuer Metallforschung was recently taken into operation at the Angstroemquelle Karlsruhe (ANKA). Here we describe the layout of the beamline optics and the experimental end-station, consisting of a heavy duty multiple circle diffractometer. For both a new design was realized, combining a maximum flexibility in the beam properties [white, pink (focused) monochromatic, energy range 6-20 keV] with a special diffractometer for heavy sample environments up to 500 kg, that can be run in different geometrical modes. In addition the angular-reciprocal space transformations for the diffractometer in use are derived, which allows an operation of the instrument in the convenient six circle mode. As an example, results from surface x-ray diffraction on a Cu{sub 3}Au(111) single crystal are presented.

  19. Ultrahigh contrast from a frequency-doubled chirped-pulse-amplification beamline.

    PubMed

    Hillier, David; Danson, Colin; Duffield, Stuart; Egan, David; Elsmere, Stephen; Girling, Mark; Harvey, Ewan; Hopps, Nicholas; Norman, Michael; Parker, Stefan; Treadwell, Paul; Winter, David; Bett, Thomas

    2013-06-20

    This paper describes frequency-doubled operation of a high-energy chirped-pulse-amplification beamline. Efficient type-I second-harmonic generation was achieved using a 3 mm thick 320 mm aperture KDP crystal. Shots were fired at a range of energies achieving more than 100 J in a subpicosecond, 527 nm laser pulse with a power contrast of 10(14). PMID:23842168

  20. Fast continuous energy scan with dynamic coupling of the monochromator and undulator at the DEIMOS beamline.

    PubMed

    Joly, L; Otero, E; Choueikani, F; Marteau, F; Chapuis, L; Ohresser, P

    2014-05-01

    In order to improve the efficiency of X-ray absorption data recording, a fast scan method, the Turboscan, has been developed on the DEIMOS beamline at Synchrotron SOLEIL, consisting of a software-synchronized continuous motion of the monochromator and undulator motors. This process suppresses the time loss when waiting for the motors to reach their target positions, as well as software dead-time, while preserving excellent beam characteristics.

  1. Use of object-oriented techniques in a beam-line control system

    SciTech Connect

    Myers, D.R.; Rueden, W. von; Butler, H.; Yang, J.

    1994-12-31

    The authors describe the use of object-oriented programming in the control and data-acquisition system for the upgraded CERN neutrino beam-line. C++ in conjunction with Posix threads running under Lynx-OS have been used in several front-end PCs. These communicate using Remote Procedure Calls over ethernet with a workstation running the commercial supervisory package, FactoryLink.

  2. Phase-space analysis and experimental results for secondary focusing at X-ray beamlines

    SciTech Connect

    Huang, Rong; Meron, Mati; Kujala, Naresh; Barrea, Raul A.

    2011-11-17

    Micro-focusing optical devices at synchrotron beamlines usually have a limited acceptance, but more flux can be intercepted if such optics are used to focus secondary sources created by the primary optics. Flux throughput can be maximized by placing the secondary focusing optics close to or exactly at the secondary source position. However, standard methods of beamline optics analysis, such as the lens equation or matching the mirror surface to an ellipse, work poorly when the source-to-optics distance is very short. In this paper the general characteristics of the focusing of beams with Gaussian profiles by a 'thin lens' are analysed under the paraxial approximation in phase space, concluding that the focusing of a beam with a short source-to-optics distance is distinct from imaging the source; slope errors are successfully included in all the formulas so that they can be used to calculate beamline focusing with good accuracy. A method is also introduced to use the thin-lens result to analyse the micro-focusing produced by an elliptically bent trapezoid-shaped Kirkpatrick-Baez mirror. The results of this analysis are in good agreement with ray-tracing simulations and are confirmed by the experimental results of the secondary focusing at the 18-ID Bio-CAT beamline (at the APS). The result of secondary focusing carried out at 18-ID using a single-bounce capillary can also be explained using this phase-space analysis. A discussion of the secondary focusing results is presented at the end of this paper.

  3. High-throughput beamline for attosecond pulses based on toroidal mirrors with microfocusing capabilities

    SciTech Connect

    Frassetto, F.; Poletto, L.; Trabattoni, A.; Anumula, S.; Sansone, G.; Calegari, F.; Nisoli, M.

    2014-10-15

    We have developed a novel attosecond beamline designed for attosecond-pump/attosecond probe experiments. Microfocusing of the Extreme-ultraviolet (XUV) radiation is obtained by using a coma-compensated optical configuration based on the use of three toroidal mirrors controlled by a genetic algorithm. Trains of attosecond pulses are generated with a measured peak intensity of about 3 × 10{sup 11} W/cm{sup 2}.

  4. Pulse generation and preamplification for long pulse beamlines of Orion laser facility.

    PubMed

    Hillier, David I; Winter, David N; Hopps, Nicholas W

    2010-06-01

    We describe the pulse generation, shaping, and preamplification system for the nanosecond beamlines of the Orion laser facility. The system generates shaped laser pulses of up to approximately 1 J of 100 ps-5 ns duration with a programmable temporal profile. The laser has a 30th-power supergaussian spatial profile and is diffraction limited. The system is capable of imposing 2D smoothing by spectral dispersion upon the beam, which will produce a nonuniformity of 10% rms at the target.

  5. A soft x-ray beamline for quantitative nanotomography using ptychography

    NASA Astrophysics Data System (ADS)

    van Riessen, Grant A.; Junker, Mark; Phillips, Nicholas W.; Peele, Andrew G.

    2013-09-01

    Soft X-ray nanotomography using ptychography allows quantitative imaging of the internal structure of biological and materials samples with high sensitivity. In this work, we describe progress toward the implementation of an interferometer-controlled microscope located at a beamline that provides coherent ux over the photon energy range of 200 to 2000 eV. Recent experimental results are presented to illustrate the potential for two- and three-dimensional imaging at the nanoscale.

  6. Optimizing the Stark-decelerator beamline for the trapping of cold molecules using evolutionary strategies

    SciTech Connect

    Gilijamse, Joop J.; Kuepper, Jochen; Hoekstra, Steven; Vanhaecke, Nicolas; Meerakker, Sebastiaan Y. T. van de; Meijer, Gerard

    2006-06-15

    We demonstrate feedback control optimization for the Stark deceleration and trapping of neutral polar molecules using evolutionary strategies. In a Stark-decelerator beamline, pulsed electric fields are used to decelerate OH radicals and subsequently store them in an electrostatic trap. The efficiency of the deceleration and trapping process is determined by the exact timings of the applied electric field pulses. Automated optimization of these timings yields an increase of 40% of the number of trapped OH radicals.

  7. High-throughput beamline for attosecond pulses based on toroidal mirrors with microfocusing capabilities.

    PubMed

    Frassetto, F; Trabattoni, A; Anumula, S; Sansone, G; Calegari, F; Nisoli, M; Poletto, L

    2014-10-01

    We have developed a novel attosecond beamline designed for attosecond-pump/attosecond probe experiments. Microfocusing of the Extreme-ultraviolet (XUV) radiation is obtained by using a coma-compensated optical configuration based on the use of three toroidal mirrors controlled by a genetic algorithm. Trains of attosecond pulses are generated with a measured peak intensity of about 3 × 10(11) W/cm(2).

  8. IR and THz Beamlines at the Metrology Light Source of the PTB

    NASA Astrophysics Data System (ADS)

    Müller, Ralph; Hoehl, Arne; Klein, Roman; Serdyukov, Anton; Ulm, Gerhard; Feikes, Jörg; von Hartrott, Michael; Schade, Ulrich; Wüstefeld, Godehard

    2010-02-01

    The low-energy electron storage ring Metrology Light Source (MLS), a dedicated synchrotron radiation source, is in user operation since April 2008. As a special option it provides coherent synchrotron radiation (CSR) in the THz range when it is operated in a low-α mode with short electron bunches. At the MLS three beamlines dedicated to the use of IR and THz radiation were designed, built and commissioned.

  9. The materials science X-ray beamline BL8 at the DELTA storage ring

    SciTech Connect

    Luetzenkirchen-Hecht, D.; Wagner, R.; Frahm, R.; Herdt, A.

    2010-06-23

    The instrumentation of the hard X-ray beamline BL8 at the 1.5 GeV Dortmund Electron Accelerator DELTA is described, and the properties of the X-ray optical elements are presented together with experimental data of different fields of research. The beamline, which makes use of the photons emitted by a superconducting asymmetric wiggler, is dedicated to X-ray studies--especially X-ray absorption spectroscopy (XAS)--in the spectral range from about 1 keV to ca. 25 keV photon energy using three different monochromators, namely YB{sub 66}(400), Si(111) and Si(311). The endstation comprises a 6-axis diffractometer that is capable of carrying heavy loads related to non-ambient sample environments such as high pressure cells, cryostats or even complete ultrahigh vacuum systems. X-ray absorption spectra from several reference compounds illustrate the performance of the beamline optics concerning e.g. energy range, energy resolution and beam stability. Fluorescence detection enables the investigation of dilute sample systems, and surface sensitive reflection mode experiments are possible for thin film studies.

  10. Time-Resolved Research at the Advanced Photon Source Beamline 7-ID

    SciTech Connect

    Dufresne, Eric M.; Adams, Bernhard; Arms, Dohn A.; Chollet, Matthieu; Landahl, Eric C.; Li, Yuelin; Walko, Donald A.; Wang, Jin

    2010-08-02

    The Sector 7 undulator beamline (7-ID) of the Advanced Photon Source (APS) is dedicated to time-resolved x-ray research and is capable of ultrafast measurements on the order of 100 ps. Beamline 7-ID has a laser laboratory featuring a Ti:Sapphire system (average power of 2.5W, pulse duration <50 fs, repetition rate 1-5 kHz) that can be synchronized to the bunch pattern of the storage ring. The laser is deliverable to x-ray enclosures, which contain diffractometers, as well as motorized optical tables for table-top experiments. Beamline 7-ID has a single APS Undulator A and uses a diamond (111) double-crystal monochromator, providing good energy resolution over a range of 6-24 keV. Available optics include Kirkpatrick-Baez (KB) mirrors to microfocus the x-ray beam. A variety of time-resolved diffraction and spectroscopy research is available at 7-ID, with experiments being done in the atomic, molecular, optical, chemistry, and solid state (bulk and surface) fields.

  11. Time-Resolved Research at the Advanced Photon Source Beamline 7-ID

    SciTech Connect

    Dufresne, Eric M.; Adams, Bernhard; Arms, Dohn A.; Chollet, Matthieu; Li, Yuelin; Walko, Donald A.; Wang Jin; Landahl, Eric C.

    2010-06-23

    The Sector 7 undulator beamline (7-ID) of the Advanced Photon Source (APS) is dedicated to time-resolved x-ray research and is capable of ultrafast measurements on the order of 100 ps. Beamline 7-ID has a laser laboratory featuring a Ti:Sapphire system (average power of 2.5 W, pulse duration <50 fs, repetition rate 1-5 kHz) that can be synchronized to the bunch pattern of the storage ring. The laser is deliverable to x-ray enclosures, which contain diffractometers, as well as motorized optical tables for table-top experiments. Beamline 7-ID has a single APS Undulator A and uses a diamond (111) double-crystal monochromator, providing good energy resolution over a range of 6-24 keV. Available optics include Kirkpatrick-Baez (KB) mirrors to microfocus the x-ray beam. A variety of time-resolved diffraction and spectroscopy research is available at 7-ID, with experiments being done in the atomic, molecular, optical, chemistry, and solid state (bulk and surface) fields.

  12. Upgraded ESRF BM29 beamline for SAXS on macromolecules in solution.

    PubMed

    Pernot, Petra; Round, Adam; Barrett, Ray; De Maria Antolinos, Alejandro; Gobbo, Alexandre; Gordon, Elspeth; Huet, Julien; Kieffer, Jerôme; Lentini, Mario; Mattenet, Muriel; Morawe, Christian; Mueller-Dieckmann, Christoph; Ohlsson, Staffan; Schmid, Werner; Surr, John; Theveneau, Pascal; Zerrad, Louiza; McSweeney, Sean

    2013-07-01

    Small-angle X-ray scattering (SAXS) measurements of proteins in solution are becoming increasingly popular with biochemists and structural biologists owing to the presence of dedicated high-throughput beamlines at synchrotron sources. As part of the ESRF Upgrade program a dedicated instrument for performing SAXS from biological macromolecules in solution (BioSAXS) has been installed at the renovated BM29 location. The optics hutch has been equipped with new optical components of which the two principal elements are a fixed-exit double multilayer monochromator and a 1.1 m-long toroidal mirror. These new dedicated optics give improved beam characteristics (compared with the previous set-up on ID14-3) regarding the energy tunability, flux and focusing at the detector plane leading to reduced parasitic scattering and an extended s-range. User experiments on the beamline have been successfully carried out since June 2012. A description of the new BioSAXS beamline and the set-up characteristics are presented together with examples of obtained data.

  13. Hard X-ray XAFS beamline, BL5S1, at AichiSR

    NASA Astrophysics Data System (ADS)

    Tabuchi, M.; Asakura, H.; Morimoto, H.; Watanabe, N.; Takeda, Y.

    2016-05-01

    A XAFS beamline, BL5S1, had been operated at Aichi Synchrotron Radiation Center, Japan since March 2013. The beamline was designed for the measurements in the energy range from 5 to 20 keV. The photon flux of 6 x 1010 at around 9 keV and beam spot size of 0.5 x 0.3 mm at sample position are as good as designed. For the standard transmission XAFS measurement, both of the step- and quick- scan modes are available. Energy resolution at around 9keV is good enough to discuss the energy shift of the order of 0.1 eV or higher even when the measurements are conducted in the quick-scan mode. With several kinds of detectors for fluorescence and/or CEY detection mode measurements, and various kinds of sample holders which are supported by the XAFS measurement software, users easily obtain spectra for their samples. Such a standard, well operated and easy to access XAFS beamline must be very important to broaden the base of the XAFS society further.

  14. A beamline systems model for Accelerator-Driven Transmutation Technology (ADTT) facilities

    NASA Astrophysics Data System (ADS)

    Todd, Alan M. M.; Paulson, C. C.; Peacock, M. A.; Reusch, M. F.

    1995-09-01

    A beamline systems code, that is being developed for Accelerator-Driven Transmutation Technology (ADTT) facility trade studies, is described. The overall program is a joint Grumman, G. H. Gillespie Associates (GHGA) and Los Alamos National Laboratory effort. The GHGA Accelerator Systems Model (ASM) has been adopted as the framework on which this effort is based. Relevant accelerator and beam transport models from earlier Grumman systems codes are being adapted to this framework. Preliminary physics and engineering models for each ADTT beamline component have been constructed. Examples noted include a Bridge Coupled Drift Tube Linac (BCDTL) and the accelerator thermal system. A decision has been made to confine the ASM framework principally to beamline modeling, while detailed target/blanket, balance-of-plant and facility costing analysis will be performed externally. An interfacing external balance-of-plant and facility costing model, which will permit the performance of iterative facility trade studies, is under separate development. An ABC (Accelerator Based Conversion) example is used to highlight the present models and capabilities.

  15. Beamlines at synchrotron radiation facilities: The link between the user and the machine

    SciTech Connect

    Johnson, E.D.; Hulbert, S.L.; Berman, L.E.

    1991-12-01

    At this point in time the literature is full of excellent review articles which describe the operating principles of optical systems for utilizing the unique radiation provided by synchrotron storage rings. In general, the perspective provided by this body of work is that of the end user-experimenter cum optics designer. Nominal design specifications of the accelerator are usually assumed, and the impact of operation in a performance envelope which may represent either degraded or enhanced machine performance is seldom considered. In this article, we have attempted to remove ourselves from this (our own usual) perspective and look instead at the beamline as a transfer function to map from the machine to the users experiment. We open first with an introduction to the perspective of the experimentalist, and some general considerations for the interaction of beamline hardware with the machine. We then discuss phase space representations of some common components of beamlines, and then treat some important classes of crystal and geometric optics in monochromators. We then close with a discussion of some of the common features of these optical systems, and the impact of the machine on user experiments.

  16. Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines

    PubMed Central

    Alcock, Simon G.; Nistea, Ioana; Sutter, John P.; Sawhney, Kawal; Fermé, Jean-Jacques; Thellièr, Christophe; Peverini, Luca

    2015-01-01

    Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the ‘junction effect’: a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts. PMID:25537582

  17. MagneDyn: the beamline for magneto dynamics studies at FERMI.

    PubMed

    Svetina, Cristian; Mahne, Nicola; Raimondi, Lorenzo; Caretta, Antonio; Casarin, Barbara; Dell'Angela, Martina; Malvestuto, Marco; Parmigiani, Fulvio; Zangrando, Marco

    2016-01-01

    The future Magneto Dynamics (MagneDyn) beamline will be devoted to study the electronic states and the local magnetic properties of excited and transient states of complex systems by means of the time-resolved X-ray absorption spectroscopy technique. The beamline will use FERMI's high-energy source covering the wavelength range from 60 nm down to 1.3 nm. An on-line photon energy spectrometer will allow spectra to be measured with high resolution while delivering most of the beam to the end-stations. Downstream the beam will be possibly split and delayed, by means of a delay line, and then focused with a set of active Kirkpatrick-Baez mirrors. These mirrors will be able to focus the radiation in one of the two MagneDyn experimental chambers: the electromagnet end-station and the resonant inelastic X-ray scattering end-station. After an introduction of the MagneDyn scientific case, the layout will be discussed showing the expected performances of the beamline. PMID:26698050

  18. The HB-2D Polarized Neutron Development Beamline at the High Flux Isotope Reactor

    NASA Astrophysics Data System (ADS)

    Crow, Lowell; Hamilton, WA; Zhao, JK; Robertson, JL

    2016-09-01

    The Polarized Neutron Development beamline, recently commissioned at the HB-2D position on the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory, provides a tool for development and testing of polarizers, polarized neutron devices, and prototyping of polarized neutron techniques. With available monochromators including pyrolytic graphite and polarizing enriched Fe-57 (Si), the instrument has operated at 4.25 and 2.6 Å wavelengths, using crystal, supermirror, or He-3 polarizers and analyzers in various configurations. The Neutron Optics and Development Team has used the beamline for testing of He-3 polarizers for use at other HFIR and Spallation Neutron Source (SNS) instruments, as well as a variety of flipper devices. Recently, we have acquired new supermirror polarizers which have improved the instrument performance. The team and collaborators also have continuing demonstration experiments of spin-echo focusing techniques, and plans to conduct polarized diffraction measurements. The beamline is also used to support a growing use of polarization techniques at present and future instruments at SNS and HFIR.

  19. Upgrades to the XRD1 beamline optics and endstation at the LNLS

    NASA Astrophysics Data System (ADS)

    Canova, H.; Fontoura, A.; Neuenschwander, R. T.; Diaz, B.; Rodella, C. B.

    2014-03-01

    XRD1 was the first X-ray diffraction beamline to be built at the LNLS and after approximately 12 years of operation it was substantially updated to improve beam stability, increase the reliability of the monochromator movement as well as provide an experimental hutch that would meet the demands of users. The improvements included the construction of an independent concrete slab below the mirror and monochromator to minimize the vibrations originating from the floor. In addition, the installation of new monochromator mechanisms as well as the replacement of the two Si(111) crystals were performed in order to attain higher precision, stability and reproducibility during operation. Moreover, the diffractometer was replaced by a 3-circle heavy duty diffractometer from Newport to collect XRD patterns primarily in capillary geometry. A robotic arm was installed for fast and automated replacement of samples as well as to secure a cryojet or a hot air blower in front of the sample during measurements. In addition, a housing equipped with 24 Mythen detectors was installed at the beamline allowing for extremely fast data acquisition. Another upgrade was the integration of motors and control systems from PXI National Instruments and Galil controllers with Phytron. These systems are crucial for the next upgrade that is underway at the beamline: enabling remote access for users to collect their measurements without the need to travel to the LNLS.

  20. Recent advances in software for beamline design, accelerator operations and personnel training

    NASA Astrophysics Data System (ADS)

    Gillespie, George H.; Hill, Barrey W.; Martono, Hendy; Moore, John M.

    2000-03-01

    Accelerators are finding new applications in research, industry, medicine, as well as other fields, and there is a growing need for new tools to improve the productivity of scientists and engineers involved with these emerging accelerator applications. Several advances in computer software have been made that focus on meeting those needs. This paper summarizes recent work in the development of a unique software framework designed specifically to support the accelerator community: the Multi-Platform Shell for Particle Accelerator Related Codes (SPARC MP). SPARC MP includes a sophisticated beamline object model, an extensive library of GUI components, and supports a variety of particle optics codes and add-on tools. This framework has been used to create the Particle Beam Optics Laboratory (PBO Lab TM) family of software applications. PBO Lab has been used for beamline design, as a computer aid for teaching particle optics, and to support accelerator operations. Several popular charged particle optics programs, including MARYLIE, TRANSPORT, TURTLE and TRACE 3-D, have been integrated with a new version of PBO Lab. The modeling and simulation capabilities of these codes allow PBO Lab to support a wide spectrum of accelerator types. New external data interface tools are available to import beamline parameters from other sources, for example, to utilize magnet strengths generated by a control system. An overview of the new version of PBO Lab is presented.

  1. Characterization of a next-generation piezo bimorph X-ray mirror for synchrotron beamlines.

    PubMed

    Alcock, Simon G; Nistea, Ioana; Sutter, John P; Sawhney, Kawal; Fermé, Jean Jacques; Thellièr, Christophe; Peverini, Luca

    2015-01-01

    Piezo bimorph mirrors are versatile active optics used on many synchrotron beamlines. However, many bimorphs suffer from the `junction effect': a periodic deformation of the optical surface which causes major aberrations to the reflected X-ray beam. This effect is linked to the construction of such mirrors, where piezo ceramics are glued directly below the thin optical substrate. In order to address this problem, a next-generation bimorph with piezos bonded to the side faces of a monolithic substrate was developed at Thales-SESO and optimized at Diamond Light Source. Using metrology feedback from the Diamond-NOM, the optical slope error was reduced to ∼ 0.5 µrad r.m.s. for a range of ellipses. To maximize usability, a novel holder was built to accommodate the substrate in any orientation. When replacing a first-generation bimorph on a synchrotron beamline, the new mirror significantly improved the size and shape of the reflected X-ray beam. Most importantly, there was no evidence of the junction effect even after eight months of continuous beamline usage. It is hoped that this new design will reinvigorate the use of active bimorph optics at synchrotron and free-electron laser facilities to manipulate and correct X-ray wavefronts.

  2. A beamline systems model for Accelerator-Driven Transmutation Technology (ADTT) facilities

    SciTech Connect

    Todd, Alan M. M.; Paulson, C. C.; Peacock, M. A.; Reusch, M. F.

    1995-09-15

    A beamline systems code, that is being developed for Accelerator-Driven Transmutation Technology (ADTT) facility trade studies, is described. The overall program is a joint Grumman, G. H. Gillespie Associates (GHGA) and Los Alamos National Laboratory effort. The GHGA Accelerator Systems Model (ASM) has been adopted as the framework on which this effort is based. Relevant accelerator and beam transport models from earlier Grumman systems codes are being adapted to this framework. Preliminary physics and engineering models for each ADTT beamline component have been constructed. Examples noted include a Bridge Coupled Drift Tube Linac (BCDTL) and the accelerator thermal system. A decision has been made to confine the ASM framework principally to beamline modeling, while detailed target/blanket, balance-of-plant and facility costing analysis will be performed externally. An interfacing external balance-of-plant and facility costing model, which will permit the performance of iterative facility trade studies, is under separate development. An ABC (Accelerator Based Conversion) example is used to highlight the present models and capabilities.

  3. Thin conductive diamond films as beam intensity monitors for soft x-ray beamlines.

    PubMed

    Kummer, K; Fondacaro, A; Yakhou-Harris, F; Sessi, V; Pobedinskas, P; Janssens, S D; Haenen, K; Williams, O A; Hees, J; Brookes, N B

    2013-03-01

    Quantitative analysis of X-ray absorption and dichroism data requires knowledge of the beamline photon flux during the measurements. We show that thin conductive (B-doped) diamond thin films can be an alternative to the widely used gold meshes for monitoring the beam intensity of soft X-ray beamlines in situ. Limited by the carbon extended x-ray absorption fine structure oscillations, the diamond films become applicable beginning from about 600 eV photon energy, where the important transition metal edges and the rare-earth edges are found. The 100 nm and 250 nm thick free-standing diamond films were grown and tested against standard gold meshes in real-life dichroism experiments performed at beamline ID08 of the European Synchrotron Radiation Facility, Grenoble, France. Quantitative agreement was found between the two experimental data sets. The films feature an extremely high transmission of about 90% and, at the same time, yield a sufficiently strong and clean reference signal. Furthermore, the thin films do not affect the shape of the transmitted beam. X-rays passing mesh-type monitors are subject to diffraction effects, which widen the beam and become particularly disturbing for small beamsizes in the micrometer range. PMID:23556850

  4. Thin conductive diamond films as beam intensity monitors for soft x-ray beamlines

    SciTech Connect

    Kummer, K.; Fondacaro, A.; Yakhou-Harris, F.; Sessi, V.; Brookes, N. B.; Pobedinskas, P.; Janssens, S. D.; Haenen, K.; Williams, O. A.; Hees, J.

    2013-03-15

    Quantitative analysis of X-ray absorption and dichroism data requires knowledge of the beamline photon flux during the measurements. We show that thin conductive (B-doped) diamond thin films can be an alternative to the widely used gold meshes for monitoring the beam intensity of soft X-ray beamlines in situ. Limited by the carbon extended x-ray absorption fine structure oscillations, the diamond films become applicable beginning from about 600 eV photon energy, where the important transition metal edges and the rare-earth edges are found. The 100 nm and 250 nm thick free-standing diamond films were grown and tested against standard gold meshes in real-life dichroism experiments performed at beamline ID08 of the European Synchrotron Radiation Facility, Grenoble, France. Quantitative agreement was found between the two experimental data sets. The films feature an extremely high transmission of about 90% and, at the same time, yield a sufficiently strong and clean reference signal. Furthermore, the thin films do not affect the shape of the transmitted beam. X-rays passing mesh-type monitors are subject to diffraction effects, which widen the beam and become particularly disturbing for small beamsizes in the micrometer range.

  5. Suite of three protein crystallography beamlines with single superconducting bend magnet as the source

    SciTech Connect

    MacDowell, Alastair A.; Celestre, Richard S.; Howells, Malcolm; McKinney, Wayne; Krupnick, James; Cambie, Daniella; Domning, Edward E; Duarte, Robert M.; Kelez, Nicholas; Plate, David W.; Cork, Carl W.; Earnest, Thomas N.; Dickert, Jeffery; Meigs, George; Ralston, Corie; Holton, James M.; Alber, Thomas; Berger, James M.; Agard, David A.; Padmore, Howard A.

    2004-08-01

    At the Advanced Light Source (ALS), three protein crystallography (PX) beamlines have been built that use as a source one of the three 6 Tesla single pole superconducting bending magnets (superbends) that were recently installed in the ring. The use of such single pole superconducting bend magnets enables the development of a hard x-ray program on a relatively low energy 1.9 GeV ring without taking up insertion device straight sections. The source is of relatively low power, but due to the small electron beam emittance, it has high brightness. X-ray optics are required to preserve the brightness and to match the illumination requirements for protein crystallography. This was achieved by means of a collimating premirror bent to a plane parabola, a double crystal monochromator followed by a toroidal mirror that focuses in the horizontal direction with a 2:1 demagnification. This optical arrangement partially balances aberrations from the collimating and toroidal mirrors such that a tight focused spot size is achieved. The optical properties of the beamline are an excellent match to those required by the small protein crystals that are typically measured. The design and performance of these new beamlines are described.

  6. Optical Design in Phase-Space for the I13L X-Ray Imaging and Coherence Beamline at Diamond using XPHASY

    SciTech Connect

    Wagner, Ulrich H.; Rau, Christoph

    2010-06-23

    I13L is a 250 m long beamline for imaging and coherent diffraction currently under construction at the Diamond Light Source. For modeling the beamline optics the phase-space based ray-tracing code XPHASY was developed, as general ray-tracing codes for x-rays do not easily allow studying the propagation of coherence along the beamline. In contrast to computational intensive wave-front propagation codes, which fully describe the propagation of a photon-beam along a beamline but obscure the impact of individual optical components onto the beamline performance, this code allows to quickly calculate the photon-beam propagation along the beamline and estimate the impact of individual components.In this paper we will discuss the optical design of the I13L coherence branch from the perspective of phase-space by using XPHASY. We will demonstrate how the phase-space representation of a photon-beam allows estimating the coherence length at any given position along the beamline. The impact of optical components on the coherence length and the effect of vibrations on the beamline performance will be discussed. The paper will demonstrate how the phase-space representation of photon-beams allows a more detailed insight into the optical performance of a coherence beamline than ray-tracing in real space.

  7. Design of a large acceptance, high efficiency energy selection system for the ELIMAIA beam-line

    NASA Astrophysics Data System (ADS)

    Schillaci, F.; Maggiore, M.; Andó, L.; Cirrone, G. A. P.; Cuttone, G.; Romano, F.; Scuderi, V.; Allegra, L.; Amato, A.; Gallo, G.; Korn, G.; Leanza, R.; Margarone, D.; Milluzzo, G.; Petringa, G.

    2016-08-01

    A magnetic chicane based on four electromagnetic dipoles is going to be realized by INFN-LNS to be used as an Energy Selection System (ESS) for laser driven proton beams up to 300 MeV and C6+ up to 70 MeV/u. The system will provide, as output, ion beams with a contrallable energy spread varying from 5% up to 20% according to the aperture slit size. Moreover, it has a very wide acceptance in order to ensure a very high transmission efficiency and, in principle, it has been designed to be used also as an active energy modulator. This system is the core element of the ELIMED (ELI-Beamlines MEDical and Multidisciplinary applications) beam transport, dosimetry and irradiation line that will be developed by INFN-LNS (It) and installed at the ELI-Beamlines facility in Prague (Cz). ELIMED will be the first user's open transport beam-line where a controlled laser-driven ion beam will be used for multidisciplinary research. The definition of well specified characteristics, both in terms of performance and field quality, of the magnetic chicane is crucial for the system realization, for the accurate study of the beam dynamics and for the proper matching with the Permanent Magnet Quadrupoles (PMQs) used as a collection system already designed. Here, the design of the magnetic chicane is described in details together with the adopted solutions in order to realize a robust system form the magnetic point of view. Moreover, the first preliminary transport simulations are also described showing the good performance of the whole beam line (PMQs+ESS).

  8. Mini-beam collimator enables micro-crystallography experiments on standard beamlines.

    SciTech Connect

    Fischetti, R. F.; Xu, S.; Yoder, D. W.; Becker, M.; Venugopalan, N.; Sanishvili, R.; Hilgart, M. C.; Stepanov, S.; Makarov, O.; Smith, J. L.; Biosciences Division

    2009-01-01

    The high-brilliance X-ray beams from undulator sources at third-generation synchrotron facilities are excellent tools for solving crystal structures of important and challenging biological macromolecules and complexes. However, many of the most important structural targets yield crystals that are too small or too inhomogeneous for a 'standard' beam from an undulator source, 25-50 {micro}m (FWHM) in the vertical and 50-100 {micro}m in the horizontal direction. Although many synchrotron facilities have microfocus beamlines for other applications, this capability for macromolecular crystallography was pioneered at ID-13 of the ESRF. The National Institute of General Medical Sciences and National Cancer Institute Collaborative Access Team (GM/CA-CAT) dual canted undulator beamlines at the APS deliver high-intensity focused beams with a minimum focal size of 20 {micro}m x 65 {micro}m at the sample position. To meet growing user demand for beams to study samples of 10 {micro}m or less, a 'mini-beam' apparatus was developed that conditions the focused beam to either 5 {micro}m or 10 {micro}m (FWHM) diameter with high intensity. The mini-beam has a symmetric Gaussian shape in both the horizontal and vertical directions, and reduces the vertical divergence of the focused beam by 25%. Significant reduction in background was achieved by implementation of both forward- and back-scatter guards. A unique triple-collimator apparatus, which has been in routine use on both undulator beamlines since February 2008, allows users to rapidly interchange the focused beam and conditioned mini-beams of two sizes with a single mouse click. The device and the beam are stable over many hours of routine operation. The rapid-exchange capability has greatly facilitated sample screening and resulted in several structures that could not have been obtained with the larger focused beam.

  9. Pulse generation and preamplification for long pulse beamlines of Orion laser facility.

    PubMed

    Hillier, David I; Winter, David N; Hopps, Nicholas W

    2010-06-01

    We describe the pulse generation, shaping, and preamplification system for the nanosecond beamlines of the Orion laser facility. The system generates shaped laser pulses of up to approximately 1 J of 100 ps-5 ns duration with a programmable temporal profile. The laser has a 30th-power supergaussian spatial profile and is diffraction limited. The system is capable of imposing 2D smoothing by spectral dispersion upon the beam, which will produce a nonuniformity of 10% rms at the target. PMID:20517369

  10. SYNCH: A program for design and analysis of synchrotrons and beamlines -- user`s guide

    SciTech Connect

    Garren, A.A.; Kenney, A.S.; Courant, E.D.; Russell, A.D.; Syphers, M.J.

    1993-12-31

    SYNCH is a computer program for use in the design and analysis of synchrotrons, storage rings, and beamlines. It has a large repertoire of commands that can be accessed in a flexible way. The input statements and the results of the calculations they invoke are saved in an internal database so that this information may be shared by other statements. SYNCH is the first accelerator program to organize its input in the form of a language. The statements, which resemble sentences, provide a natural way of describing lattices and invoking relevant calculations. The organization of the program is modular, so that it has been possible to expand its capabilities progressively.

  11. The New X-Ray Lithography Beamline BL1 At DELTA

    SciTech Connect

    Lietz, D.; Paulus, M.; Sternemann, C.; Berges, U.; Hippert, B.; Tolan, M.

    2010-06-23

    Lithography using synchrotron radiation in the x-ray regime provides a powerful method to produce mechanical components of sub-millimeter size with a very good quality for microtechnological applications. In recent years the demand for x-ray lithography beamtime for industrial production of microparts increased rapidly resulting in the development of new experimental endstations at synchrotron radiation sources dedicated for the production of micromechanical devices. We present in this work the layout of the new x-ray lithography beamline BL1 at the synchrotron radiation source DELTA in Dortmund and discuss first results of exposure tests.

  12. The Stanford Automated Mounter: Pushing the limits of sample exchange at the SSRL macromolecular crystallography beamlines

    DOE PAGES

    Russi, Silvia; Song, Jinhu; McPhillips, Scott E.; Cohen, Aina E.

    2016-02-24

    The Stanford Automated Mounter System, a system for mounting and dismounting cryo-cooled crystals, has been upgraded to increase the throughput of samples on the macromolecular crystallography beamlines at the Stanford Synchrotron Radiation Lightsource. This upgrade speeds up robot maneuvers, reduces the heating/drying cycles, pre-fetches samples and adds an air-knife to remove frost from the gripper arms. As a result, sample pin exchange during automated crystal quality screening now takes about 25 s, five times faster than before this upgrade.

  13. FXI: a full-field imaging beamline at NSLS-II

    NASA Astrophysics Data System (ADS)

    Lee, Wah-Keat; Reininger, Ruben; Loo, William; Gambella, Richard; O'Hara, Steven; Chu, Yong S.; Zhong, Zhong; Wang, Jun

    2015-09-01

    The Full-field X-ray Imaging (FXI) beamline at the NSLS-II is designed for optimum performance of a transmission x-ray microscope (TXM). When complete, FXI will enable the TXM to obtain individual 2D projection images at 30 nm spatial resolution and up to 40 microns field of view (FOV) with exposure times of < 50 ms per image. A complete 3D nanotomography data set should take less than 1 minute. This will open opportunities for many real-time in-operando studies.

  14. Justification for the development of a bending magnet beamline at sector 10 at the APS.

    SciTech Connect

    Kemner, K. M.; Biosciences Division

    2006-09-18

    The long-planned and much-needed merger of EnviroCAT into the Materials Research Collaborative Access Team (MR-CAT) will provide dedicated state-of-the-art facilities that are critical to research on a broad range of issues in environmental sciences. These CATs will focus on developing a bending magnet (BM) beamline for x-ray absorption fine structure (XAFS) and micro x-ray analysis of environmental samples through integration with existing insertion device (ID) capabilities in XAFS, micro x-ray analysis, and x-ray scattering. In addition, the expanded MR-CAT will serve as the hub of personnel and laboratory infrastructure support for molecular environmental science and biogeochemical science at the Advanced Photon Source (APS). In conjunction with the merger of EnviroCAT into MR-CAT, the US Environmental Protection Agency (EPA) will become a member institution of MR-CAT, joining the present members (University of Notre Dame, Illinois Institute of Technology, University of Florida, British Petroleum, and Argonne's Chemical Engineering and Biosciences Division). The motivation for blending capabilities meeting the needs of EnviroCAT users into the MR-CAT facilities is the explosion of synchrotron-radiation-based research in the field known as molecular environmental science (MES). This research is driven largely by the need to remediate contaminated environmental materials and to understand the scientific foundations that govern contaminant transport in the environment. Synchrotron radiation is playing a crucial role in solving environmental science problems by offering x-ray-based analytical techniques for detailed molecular- and atomic-level studies of these systems. This document focuses on the scientific justification for developing a specific type of BM beamline capability at Sector 10 for XAFS and micro x-ray analysis to support the growing MES community. However, the modification of Sector 10 will meet other future needs by providing (1) an existing undulator

  15. Synchrotron X-ray Optics Testing at Beamline 1-BM at the Advanced Photon Source

    NASA Astrophysics Data System (ADS)

    Macrander, Albert; Kujala, Naresh

    2014-03-01

    Beamline 1-BM at the Advanced Photon Source has been reconfigured, in part for testing of synchrotron optics with both monochromatic and white beams. Monochromatic energies between 6 and 30 keV are available. Primary agendas include both white beam and monochromatic beam topography, Talbot grating interferometry for measurement of coherence lengths and wavefronts, and micro-focusing. Recent examples will include topography of sapphire , tests of Kirkpatrick-Baez mirrors, and tests of multilayer Laue lenses. Analyzers for Inelastic X-ray Scattering has also been characterized by two user groups. Supported from U.S. DOE, Office of Science, Contract No. DE-AC-02-06CH11357.

  16. The Stanford Automated Mounter: pushing the limits of sample exchange at the SSRL macromolecular crystallography beamlines

    PubMed Central

    Russi, Silvia; Song, Jinhu; McPhillips, Scott E.; Cohen, Aina E.

    2016-01-01

    The Stanford Automated Mounter System, a system for mounting and dismounting cryo-cooled crystals, has been upgraded to increase the throughput of samples on the macromolecular crystallography beamlines at the Stanford Synchrotron Radiation Lightsource. This upgrade speeds up robot maneuvers, reduces the heating/drying cycles, pre-fetches samples and adds an air-knife to remove frost from the gripper arms. Sample pin exchange during automated crystal quality screening now takes about 25 s, five times faster than before this upgrade. PMID:27047309

  17. SUNY beamline facilities at the National Synchrotron Light Source (Final Report)

    SciTech Connect

    Coppens, Philip

    2003-06-22

    The DOE sponsored SUNY synchrotron project has involved close cooperation among faculty at several SUNY campuses. A large number of students and postdoctoral associates have participated in its operation which was centered at the X3 beamline of the National Synchrotron Light Source at Brookhaven National Laboratory. Four stations with capabilities for Small Angle Scattering, Single Crystal and Powder and Surface diffraction and EXAFS were designed and operated with capability to perform experiments at very low as well as elevated temperatures and under high vacuum. A large amount of cutting-edge science was performed at the facility, which in addition provided excellent training for students and postdoctoral scientists in the field.

  18. CDApps: integrated software for experimental planning and data processing at beamline B23, Diamond Light Source

    PubMed Central

    Hussain, Rohanah; Benning, Kristian; Javorfi, Tamas; Longo, Edoardo; Rudd, Timothy R.; Pulford, Bill; Siligardi, Giuliano

    2015-01-01

    The B23 Circular Dichroism beamline at Diamond Light Source has been operational since 2009 and has seen visits from more than 200 user groups, who have generated large amounts of data. Based on the experience of overseeing the users’ progress at B23, four key areas requiring the most assistance are identified: planning of experiments and note-keeping; designing titration experiments; processing and analysis of the collected data; and production of experimental reports. To streamline these processes an integrated software package has been developed and made available for the users. The subsequent article summarizes the main features of the software. PMID:25723950

  19. Magnetic shielding of an electron beamline in a hadron accelerator enclosure

    SciTech Connect

    Kroc, T.K.; Schmidt, C.W.; Shemyakin, A.; /Fermilab

    2005-05-01

    The Fermilab Electron Cooling Project requires the operation of a 4.34 MeV electron beam in the same enclosure that houses the 120, 150 GeV Main Injector. Effective shielding of the magnetic fields from the ramped electrical busses and local static fields is necessary to maintain the high beam quality and recirculation efficiency required by the electron cooling system. This paper discusses the operational tolerances and the design of the beamline shielding, bus design, and bus shielding as well as experimental results from the prototype and final installation.

  20. Target and orbit feedback simulations of a muSR beamline at BNL

    SciTech Connect

    MacKay, W. W.; Fischer, W.; Blaskiewicz, M.; Pile, P.

    2015-05-03

    Well-polarized positive surface muons are a tool to measure the magnetic properties of materials since the precession rate of the spin can be determined from the observation of the positron directions when the muons decay. The use of the AGS complex at BNL has been explored for a muSR facility previously. Here we report simulations of a beamline with a target inside a solenoidal field, and of an orbit feed-back system with single muon beam positioning monitors based on technology available today

  1. Synchrotron total reflection X-ray fluorescence at BL-16 microfocus beamline of Indus-2

    SciTech Connect

    Tiwari, M. K. Singh, A. K. Das, Gangadhar Chowdhury, Anupam Lodha, G. S.

    2014-04-24

    Determination of ultra trace elements is important in many disciplines both in basic and applied sciences. Numerous applications show their importance in medical science, environmental science, materials science, food processing and semiconductor industries and in maintaining the quality control of ultra pure chemicals and reagents. We report commissioning of a synchrotron based total reflection x-ray fluorescence (TXRF) facility on the BL-16 microfocus beamline of Indus-2. This paper describes the performance of the BL-16 TXRF spectrometer and the detailed description of its capabilities through examples of measured results.

  2. Analysis of order contamination from toroidal grating monochromator of Indus-1 reflectivity beamline

    SciTech Connect

    Gupta, R. K.; Modi, Mohammed H.; Lodha, G. S.

    2012-06-05

    The synchrotron radiation spectra of toroidal grating monochromators (TGM) often contaminated by significant amounts of higher orders. Quantitative estimation of order contamination is essential in order to perform quantitative spectroscopy measurements. At Indus-1 reflectivity beamline higher order contaminations from TGM monochromator are experimentally determined using a reflection grating analyzer. It is found that the order contamination in wavelength range of 50-200 A is less than 15%. Use of edge filters reduces the order contamination level below 5% in this wavelength range.

  3. Achieving Vibration Stability of the NSLS-II Hard X-ray Nanoprobe Beamline

    SciTech Connect

    Simos, N.; Chu, Y. S.; Broadbent, A.; Nazaretski, E.; Margulies, L.; Dyling, O.; Shen, Q.; Fallier, M.

    2011-09-09

    The hard x-ray nanoprobe (HXN) beamline of the National Synchrotron Light Source II (NSLS-II) requires high levels of stability in order to achieve the desired instrument resolution. To ensure that the design of the endstation helps meet the stringent criteria and that natural and cultural vibration is mitigated both passively and actively, a comprehensive study complimentary to the design process has been undertaken. Vibration sources that have the potential to disrupt sensitive experiments such as wind, traffic, and NSLS II operating systems have been studied using state-of-the-art simulations and an array of field data. Further, final stage vibration isolation principles have been explored.

  4. X-ray Experiments for Students at the SLS Optics Beamline

    SciTech Connect

    Flechsig, U.; Jaggi, A.; Krempasky, J.; Oberta, P.; Spielmann, S.; Veen, J. F. van der; Als-Nielsen, J.

    2010-06-23

    We present a X-ray training course for students. The course covers fundamental properties of synchrotron radiation and basic techniques like scattering and absorption. We prepared ten experiments together with a tutorial. The whole course takes about a week. A first student group from the University of Copenhagen passed the course in June 2009. The experiments were performed at the optics beamline of the Swiss Light Source which can be part-time allocated for training purposes. Two experiments are described in more detail: scattering from a hanging drop of water turning into ice and measurement of the power of a pink synchrotron beam using a simple calorimeter.

  5. BioSAXS Sample Changer: a robotic sample changer for rapid and reliable high-throughput X-ray solution scattering experiments

    PubMed Central

    Round, Adam; Felisaz, Franck; Fodinger, Lukas; Gobbo, Alexandre; Huet, Julien; Villard, Cyril; Blanchet, Clement E.; Pernot, Petra; McSweeney, Sean; Roessle, Manfred; Svergun, Dmitri I.; Cipriani, Florent

    2015-01-01

    Small-angle X-ray scattering (SAXS) of macromolecules in solution is in increasing demand by an ever more diverse research community, both academic and industrial. To better serve user needs, and to allow automated and high-throughput operation, a sample changer (BioSAXS Sample Changer) that is able to perform unattended measurements of up to several hundred samples per day has been developed. The Sample Changer is able to handle and expose sample volumes of down to 5 µl with a measurement/cleaning cycle of under 1 min. The samples are stored in standard 96-well plates and the data are collected in a vacuum-mounted capillary with automated positioning of the solution in the X-ray beam. Fast and efficient capillary cleaning avoids cross-contamination and ensures reproducibility of the measurements. Independent temperature control for the well storage and for the measurement capillary allows the samples to be kept cool while still collecting data at physiological temperatures. The Sample Changer has been installed at three major third-generation synchrotrons: on the BM29 beamline at the European Synchrotron Radiation Facility (ESRF), the P12 beamline at the PETRA-III synchrotron (EMBL@PETRA-III) and the I22/B21 beamlines at Diamond Light Source, with the latter being the first commercial unit supplied by Bruker ASC. PMID:25615861

  6. BioSAXS Sample Changer: a robotic sample changer for rapid and reliable high-throughput X-ray solution scattering experiments.

    PubMed

    Round, Adam; Felisaz, Franck; Fodinger, Lukas; Gobbo, Alexandre; Huet, Julien; Villard, Cyril; Blanchet, Clement E; Pernot, Petra; McSweeney, Sean; Roessle, Manfred; Svergun, Dmitri I; Cipriani, Florent

    2015-01-01

    Small-angle X-ray scattering (SAXS) of macromolecules in solution is in increasing demand by an ever more diverse research community, both academic and industrial. To better serve user needs, and to allow automated and high-throughput operation, a sample changer (BioSAXS Sample Changer) that is able to perform unattended measurements of up to several hundred samples per day has been developed. The Sample Changer is able to handle and expose sample volumes of down to 5 µl with a measurement/cleaning cycle of under 1 min. The samples are stored in standard 96-well plates and the data are collected in a vacuum-mounted capillary with automated positioning of the solution in the X-ray beam. Fast and efficient capillary cleaning avoids cross-contamination and ensures reproducibility of the measurements. Independent temperature control for the well storage and for the measurement capillary allows the samples to be kept cool while still collecting data at physiological temperatures. The Sample Changer has been installed at three major third-generation synchrotrons: on the BM29 beamline at the European Synchrotron Radiation Facility (ESRF), the P12 beamline at the PETRA-III synchrotron (EMBL@PETRA-III) and the I22/B21 beamlines at Diamond Light Source, with the latter being the first commercial unit supplied by Bruker ASC. PMID:25615861

  7. BioSAXS Sample Changer: a robotic sample changer for rapid and reliable high-throughput X-ray solution scattering experiments.

    PubMed

    Round, Adam; Felisaz, Franck; Fodinger, Lukas; Gobbo, Alexandre; Huet, Julien; Villard, Cyril; Blanchet, Clement E; Pernot, Petra; McSweeney, Sean; Roessle, Manfred; Svergun, Dmitri I; Cipriani, Florent

    2015-01-01

    Small-angle X-ray scattering (SAXS) of macromolecules in solution is in increasing demand by an ever more diverse research community, both academic and industrial. To better serve user needs, and to allow automated and high-throughput operation, a sample changer (BioSAXS Sample Changer) that is able to perform unattended measurements of up to several hundred samples per day has been developed. The Sample Changer is able to handle and expose sample volumes of down to 5 µl with a measurement/cleaning cycle of under 1 min. The samples are stored in standard 96-well plates and the data are collected in a vacuum-mounted capillary with automated positioning of the solution in the X-ray beam. Fast and efficient capillary cleaning avoids cross-contamination and ensures reproducibility of the measurements. Independent temperature control for the well storage and for the measurement capillary allows the samples to be kept cool while still collecting data at physiological temperatures. The Sample Changer has been installed at three major third-generation synchrotrons: on the BM29 beamline at the European Synchrotron Radiation Facility (ESRF), the P12 beamline at the PETRA-III synchrotron (EMBL@PETRA-III) and the I22/B21 beamlines at Diamond Light Source, with the latter being the first commercial unit supplied by Bruker ASC.

  8. DEIMOS: A beamline dedicated to dichroism measurements in the 350–2500 eV energy range

    SciTech Connect

    Ohresser, P. Otero, E.; Choueikani, F.; Chen, K.; Stanescu, S.; Deschamps, F.; Moreno, T.; Polack, F.; Lagarde, B.; Daguerre, J.-P.; Marteau, F.; Scheurer, F.; Joly, L.; Muller, B.; Kappler, J.-P.; Bunau, O.; Sainctavit, Ph.

    2014-01-15

    The DEIMOS (Dichroism Experimental Installation for Magneto-Optical Spectroscopy) beamline was part of the second phase of the beamline development at French Synchrotron SOLEIL (Source Optimisée de Lumière à Energie Intermédiaire du LURE) and opened to users in March 2011. It delivers polarized soft x-rays to perform x-ray absorption spectroscopy, x-ray magnetic circular dichroism, and x-ray linear dichroism in the energy range 350–2500 eV. The beamline has been optimized for stability and reproducibility in terms of photon flux and photon energy. The main end-station consists in a cryo-magnet with 2 split coils providing a 7 T magnetic field along the beam or 2 T perpendicular to the beam with a controllable temperature on the sample from 370 K down to 1.5 K.

  9. DEIMOS: a beamline dedicated to dichroism measurements in the 350-2500 eV energy range.

    PubMed

    Ohresser, P; Otero, E; Choueikani, F; Chen, K; Stanescu, S; Deschamps, F; Moreno, T; Polack, F; Lagarde, B; Daguerre, J-P; Marteau, F; Scheurer, F; Joly, L; Kappler, J-P; Muller, B; Bunau, O; Sainctavit, Ph

    2014-01-01

    The DEIMOS (Dichroism Experimental Installation for Magneto-Optical Spectroscopy) beamline was part of the second phase of the beamline development at French Synchrotron SOLEIL (Source Optimisée de Lumière à Energie Intermédiaire du LURE) and opened to users in March 2011. It delivers polarized soft x-rays to perform x-ray absorption spectroscopy, x-ray magnetic circular dichroism, and x-ray linear dichroism in the energy range 350-2500 eV. The beamline has been optimized for stability and reproducibility in terms of photon flux and photon energy. The main end-station consists in a cryo-magnet with 2 split coils providing a 7 T magnetic field along the beam or 2 T perpendicular to the beam with a controllable temperature on the sample from 370 K down to 1.5 K.

  10. Development and applications of rectangular box-type explosively bonded structures for high-heat-load beamline components

    NASA Astrophysics Data System (ADS)

    Shu, D.; Chang, J.; Kuzay, T. M.; Brasher, D. G.

    2001-07-01

    Explosive bonding technology is a good choice to join dissimilar materials, such as 304L stainless steel and GlidCop AL-15, and is used extensively in making the advanced photon source (APS) high-heat-load beamline and front-end components. It is a bonding method in which the controlled energy of a detonating explosive is used to create a metallurgical bond between two or more similar or dissimilar materials. In recent years, special explosive bonding units with rectangular box-type joints were developed for the APS new high-heat-load beamline components. Based on this new technique, the box form of the component could be built in two halves first, then welded together. Therefore, beamline designers have more freedom to optimize the cooling surface geometry.

  11. In crystallo optical spectroscopy (icOS) as a complementary tool on the macromolecular crystallography beamlines of the ESRF

    PubMed Central

    von Stetten, David; Giraud, Thierry; Carpentier, Philippe; Sever, Franc; Terrien, Maxime; Dobias, Fabien; Juers, Douglas H.; Flot, David; Mueller-Dieckmann, Christoph; Leonard, Gordon A.; de Sanctis, Daniele; Royant, Antoine

    2015-01-01

    The analysis of structural data obtained by X-ray crystallo­graphy benefits from information obtained from complementary techniques, especially as applied to the crystals themselves. As a consequence, optical spectroscopies in structural biology have become instrumental in assessing the relevance and context of many crystallographic results. Since the year 2000, it has been possible to record such data adjacent to, or directly on, the Structural Biology Group beamlines of the ESRF. A core laboratory featuring various spectrometers, named the Cryobench, is now in its third version and houses portable devices that can be directly mounted on beamlines. This paper reports the current status of the Cryobench, which is now located on the MAD beamline ID29 and is thus called the ID29S-Cryobench (where S stands for ‘spectroscopy’). It also reviews the diverse experiments that can be performed at the Cryobench, highlighting the various scientific questions that can be addressed. PMID:25615856

  12. Photon transport of the superradiant TeraFERMI THz beamline at the FERMI free-electron laser.

    PubMed

    Svetina, Cristian; Mahne, Nicola; Raimondi, Lorenzo; Perucchi, Andrea; Di Pietro, Paola; Lupi, Stefano; Schmidt, Bernhard; Zangrando, Marco

    2016-01-01

    TeraFERMI is the new terahertz (THz) beamline for pump-probe studies on the femtosecond time-scale, under construction at the FERMI free-electron laser (FEL) facility in Trieste, Italy. The beamline will take advantage of the coherent radiation emitted by the spent electrons from the FEL undulators, before being dumped. This will result in short, coherent, high-power THz pulses to be used as a pump beam, in order to modulate structural properties of matter, thereby inducing phase transitions. The TeraFERMI beamline collects THz radiation in the undulator hall and guides it along a beam pipe which is approximately 30 m long, extending across the safety hutch and two shielding walls. Here the optical design, which will allow the efficient transport of the emitted THz radiation in the experimental hall, is presented. PMID:26698051

  13. Parallel-beam imaging at the ESRF beamline ID19: current status and plans for the future

    NASA Astrophysics Data System (ADS)

    Weitkamp, T.; Tafforeau, P.; Boller, E.; Cloetens, P.; Valade, J.-P.; Bernard, P.; Peyrin, F.; Ludwig, W.; Helfen, L.; Baruchel, J.

    2010-06-01

    The ESRF synchrotron beamline ID19, dedicated to full-field parallel-beam imaging techniques such as phase-contrast and absorption microtomography and X-ray topography, is one of the most versatile instruments of its kind. This paper presents key characteristics of ID19 in its present form, names examples for research and development performed on the beamline, and outlines the plans for an upgrade on the beamline in coming years, to adapt to the growing needs of the user community. The technical goals envisioned include an increase in available beam size and maximum photon energy, and a substantial increase in flux density for applications using beams of small and intermediate size.

  14. CITY III Operator's Manual.

    ERIC Educational Resources Information Center

    Envirometrics, Inc., Washington, DC.

    CITY III is a computer-assisted simulation game of an urban system involving player operation of and interaction with economic, social, and government components. The role of operator in the game is to take the handwritten inputs (decisions) from the CITY III participants, process them, and return output which initiates the next round of…

  15. SUPERSTARS III: K-2.

    ERIC Educational Resources Information Center

    North Carolina State Dept. of Public Education, Raleigh.

    SUPERSTARS III is a K-8 program designed as an enrichment opportunity for self-directed learners in mathematics. The basic purpose of SUPERSTARS III is to provide the extra challenge that self-motivated students need in mathematics and to do so in a structured, long-term program that does not impinge on the normal classroom routine or the…

  16. Facilitating best practices in collecting anomalous scattering data for de novo structure solution at the ESRF Structural Biology Beamlines

    PubMed Central

    de Sanctis, Daniele; Oscarsson, Marcus; Popov, Alexander; Svensson, Olof; Leonard, Gordon

    2016-01-01

    The constant evolution of synchrotron structural biology beamlines, the viability of screening protein crystals for a wide range of heavy-atom derivatives, the advent of efficient protein labelling and the availability of automatic data-processing and structure-solution pipelines have combined to make de novo structure solution in macromolecular crystallography a less arduous task. Nevertheless, the collection of diffraction data of sufficient quality for experimental phasing is still a difficult and crucial step. Here, some examples of good data-collection practice for projects requiring experimental phasing are presented and recent developments at the ESRF Structural Biology beamlines that have facilitated these are illustrated. PMID:26960128

  17. Facilitating best practices in collecting anomalous scattering data for de novo structure solution at the ESRF Structural Biology Beamlines.

    PubMed

    de Sanctis, Daniele; Oscarsson, Marcus; Popov, Alexander; Svensson, Olof; Leonard, Gordon

    2016-03-01

    The constant evolution of synchrotron structural biology beamlines, the viability of screening protein crystals for a wide range of heavy-atom derivatives, the advent of efficient protein labelling and the availability of automatic data-processing and structure-solution pipelines have combined to make de novo structure solution in macromolecular crystallography a less arduous task. Nevertheless, the collection of diffraction data of sufficient quality for experimental phasing is still a difficult and crucial step. Here, some examples of good data-collection practice for projects requiring experimental phasing are presented and recent developments at the ESRF Structural Biology beamlines that have facilitated these are illustrated.

  18. Mechanical Design of a Spherical Grating Monochromator for the Microspectroscopy Beamline PolLux at the Swiss Light Source

    SciTech Connect

    Henein, Simon; Frommherz, Ulrich; Betemps, Robin; Kalt, Herbert; Ellenberger, Urs; Flechsig, Uwe; Raabe, Joerg

    2007-01-19

    This paper describes a new monochromator design for a bending magnet beamline of the Swiss Light Source synchrotron facility. The beamline optics is based on a horizontally deflecting spherical grating monochromator (SGM) with two gratings at a constant deviation angle. It covers a photon energy range from 200 eV to 1000 eV. This paper concentrates on the original flexure-based mechanisms with partially parallel kinematics invented and designed for this monochromator, as well as on the lessons learned from the assembly and testing of the system.

  19. Vacuum upgrade and enhanced performances of the double imaging electron/ion coincidence end-station at the vacuum ultraviolet beamline DESIRS.

    PubMed

    Tang, Xiaofeng; Garcia, Gustavo A; Gil, Jean-François; Nahon, Laurent

    2015-12-01

    We report here the recent upgrade of the SAPHIRS permanent photoionization end-station at the DESIRS vacuum ultraviolet beamline of synchrotron SOLEIL, whose performances have been enhanced by installing an additional double-skimmer differential chamber. The smaller molecular beam profile obtained at the interaction region has increased the mass resolution of the double imaging photoelectron photoion coincidence (i(2)PEPICO) spectrometer, DELICIOUS III, installed in the photoionization chamber of the SAPHIRS endstation, by a factor of two, to M/ΔM ∼ 1700 (FWHM). The electron kinetic energy resolution offered by the velocity map imaging (VMI) part of the spectrometer has been improved down to 2.8% (ΔE/E) as we show on the N2 photoionization case in the double skimmer configuration. As a representative example of the overall state-of-the-art i(2)PEPICO performances, experimental results of the dissociation of state-selected O2(+)(B(2)∑(g)(-), v(+) = 0-6) molecular ions performed at the fixed photon energy of hν = 21.1 eV are presented. PMID:26724007

  20. Vacuum upgrade and enhanced performances of the double imaging electron/ion coincidence end-station at the vacuum ultraviolet beamline DESIRS

    NASA Astrophysics Data System (ADS)

    Tang, Xiaofeng; Garcia, Gustavo A.; Gil, Jean-François; Nahon, Laurent

    2015-12-01

    We report here the recent upgrade of the SAPHIRS permanent photoionization end-station at the DESIRS vacuum ultraviolet beamline of synchrotron SOLEIL, whose performances have been enhanced by installing an additional double-skimmer differential chamber. The smaller molecular beam profile obtained at the interaction region has increased the mass resolution of the double imaging photoelectron photoion coincidence (i2PEPICO) spectrometer, DELICIOUS III, installed in the photoionization chamber of the SAPHIRS endstation, by a factor of two, to M/ΔM ˜ 1700 (FWHM). The electron kinetic energy resolution offered by the velocity map imaging (VMI) part of the spectrometer has been improved down to 2.8% (ΔE/E) as we show on the N2 photoionization case in the double skimmer configuration. As a representative example of the overall state-of-the-art i2PEPICO performances, experimental results of the dissociation of state-selected O2+ (B 2 ∑ g - , v+ = 0-6) molecular ions performed at the fixed photon energy of hν = 21.1 eV are presented.

  1. The life science X-ray scattering beamline at NSLS-II

    SciTech Connect

    DiFabio, Jonathan; Yang, Lin; Chodankar, Shirish; Pjerov, Sal; Jakoncic, Jean; Lucas, Michael; Krywka, Christina; Graziano, Vito

    2015-09-30

    We report the current development status of the High Brightness X-ray Scattering for Life Sciences (or Life Science X-ray Scattering, LiX) beamline at the NSLS-II facility of Brookhaven National Laboratory. This instrument will operate in the x-ray energy range of 2.1-18 keV, provide variable beam sizes from 1 micron to ~0.5 mm, and support user experiments in three scientific areas: (1) high-throughput solution scattering, in-line size exclusion chromatography and flow mixers-based time-resolved solution scattering of biological macro-molecules, (2) diffraction from single- and multi-layered lipid membranes, and (3) scattering-based scanning probe imaging of biological tissues. In order to satisfy the beam stability required for these experiments and to switch rapidly between different types of experiments, we have adopted a secondary source with refractive lenses for secondary focusing, a detector system consisting of three Pilatus detectors, and specialized experimental modules that can be quickly exchanged and each dedicated to a defined set of experiments. The construction of this beamline is on schedule for completion in September 2015. User experiments are expected to start in Spring 2016.

  2. The life science X-ray scattering beamline at NSLS-II

    DOE PAGES

    DiFabio, Jonathan; Yang, Lin; Chodankar, Shirish; Pjerov, Sal; Jakoncic, Jean; Lucas, Michael; Krywka, Christina; Graziano, Vito

    2015-09-30

    We report the current development status of the High Brightness X-ray Scattering for Life Sciences (or Life Science X-ray Scattering, LiX) beamline at the NSLS-II facility of Brookhaven National Laboratory. This instrument will operate in the x-ray energy range of 2.1-18 keV, provide variable beam sizes from 1 micron to ~0.5 mm, and support user experiments in three scientific areas: (1) high-throughput solution scattering, in-line size exclusion chromatography and flow mixers-based time-resolved solution scattering of biological macro-molecules, (2) diffraction from single- and multi-layered lipid membranes, and (3) scattering-based scanning probe imaging of biological tissues. In order to satisfy the beammore » stability required for these experiments and to switch rapidly between different types of experiments, we have adopted a secondary source with refractive lenses for secondary focusing, a detector system consisting of three Pilatus detectors, and specialized experimental modules that can be quickly exchanged and each dedicated to a defined set of experiments. The construction of this beamline is on schedule for completion in September 2015. User experiments are expected to start in Spring 2016.« less

  3. Characterization of a mini-multileaf collimator in a proton beamline

    SciTech Connect

    Daartz, J.; Bangert, M.; Bussiere, M. R.; Engelsman, M.; Kooy, H. M.

    2009-05-15

    A mini-multileaf collimator (MMLC) was mounted as a field shaping collimator in a proton beamline at the Massachusetts General Hospital. The purpose is to evaluate the device's dosimetric and mechanical properties for the use in a proton beamline. For this evaluation, the authors compared MMLC and brass aperture shaped dose distributions with regard to lateral and depth dose properties. The lateral fall off is generally broader with the MMLC, with difference varying with proton range from 0.2 to 1.2 mm. Central axis depth dose curves did not show a difference in peak-to-entrance ratio, peak width, distal fall off, or range. Two-dimensional dose distributions to investigate the conformity of MMLC shaped doses show that the physical leaf width of {approx_equal}2.5 mm does not have a significant impact. All differences seen in dose distribution shaped by the MMLC versus brass apertures were shown to be clinically insignificant. Measured neutron doses of 0.03-0.13 mSv/Gy for a closed brass beam block (depending on range) are very low compared to the previously published data. Irradiation of the tungsten MMLC, however, produced 1.5-1.8 times more neutrons than brass apertures. Exposure of the staff resulting from activation of the device is below regulatory limits. The measurements established an equivalency between aperture and MMLC shaped dose distributions.

  4. Support for the Advanced Polymers Beamline at the National Synchrotron Light Source

    SciTech Connect

    Hsiao, Benjamin S

    2008-10-01

    The primary focus of the X27C beamline is to investigate frontier polymer science and engineering problems with emphasis on real-time studies of structures, morphologies and dynamics from atomic, nanoscopic, microscopic to mesoscopic scales using simultaneous small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) techniques. The scientific merit of this project is as follows. Currently, many unique sample chambers for in-situ synchrotron studies, developed by the PI (B. Hsiao) and Co-PI (B. Chu), are available for general users of X27C at NSLS. These instruments include a gel/melt spinning apparatus, a continuous fiber drawing apparatus, a tensile stretching apparatus, a high pressure X-ray cell using supercritical carbon dioxide, a parallel plate strain-controlled shear stage and a dynamic rheometer for small-strain oscillatory deformation study. Based on the use of these instruments in combination with synchrotron X-rays, many new insights into the relationships between processing and structure have been obtained in recent years. The broader impact of this project is as follows. The X27C beamline is the first synchrotron facility in the United States dedicated to chemistry/materials research (with emphasis on polymers). The major benefit of this facility to the materials community is that no extensive synchrotron experience and equipment preparation are required from general users to carry out cutting-edge experiments.

  5. Non-destructive single-pass low-noise detection of ions in a beamline

    SciTech Connect

    Schmidt, Stefan; Murböck, Tobias; Birkl, Gerhard; Andelkovic, Zoran; Vogel, Manuel; Nörtershäuser, Wilfried; Stahl, Stefan

    2015-11-15

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles’ beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar{sup 13+}) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections.

  6. Low-cycle-fatigue behavior of copper materials and their use in synchrotron beamline components

    SciTech Connect

    Wang, Z.; Nian, T.; Ryding, D.; Kuzay, T.M.

    1993-09-01

    The third generation synchrotron facilities such as the 7-GeV Advanced Photon Source Project (APS) generate x-ray beams with very high heat loads and heat flux levels. The front-end and beamline components are required to sustain total heat loads of 5 to 15 kW and heat flux levels exceeding 400 W/mm{sup 2}. Grazing geometry and enhanced heat transfer techniques are used in the design of such components to reduce heat flux levels below the 30 W/mm{sup 2} level, which is sustainable by the special copper materials routinely used in the component design. Although the resulting maximum surface temperatures can be sustained, the structural stresses and the fatigue issues remain viable concerns for the copper, particularly under brazing or bonding of the parts. Brazing and bonding are almost always utilized in the design of the components, and the drastically lowered yield stress of the annealed copper subjected to bonding temperatures above 400{degree}C is a real concern. Such materials with reduced post-bonding stress levels easily reach yield point under thermal stresses during ordinary use on the beamline. The resulting plastic deformation in each load cycle may cause low-cycle-fatigue problems. The two common copper materials are OFHC and Glidcop. This paper critically reviews the available literature for low-cycle-fatigue properties, of OFHC at the elevated temperatures typically found in synchrotron operations.

  7. Non-destructive single-pass low-noise detection of ions in a beamline

    NASA Astrophysics Data System (ADS)

    Schmidt, Stefan; Murböck, Tobias; Andelkovic, Zoran; Birkl, Gerhard; Nörtershäuser, Wilfried; Stahl, Stefan; Vogel, Manuel

    2015-11-01

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles' beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar13+) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections.

  8. Non-destructive single-pass low-noise detection of ions in a beamline.

    PubMed

    Schmidt, Stefan; Murböck, Tobias; Andelkovic, Zoran; Birkl, Gerhard; Nörtershäuser, Wilfried; Stahl, Stefan; Vogel, Manuel

    2015-11-01

    We have conceived, built, and operated a device for the non-destructive single-pass detection of charged particles in a beamline. The detector is based on the non-resonant pick-up and subsequent low-noise amplification of the image charges induced in a cylindrical electrode surrounding the particles' beam path. The first stage of the amplification electronics is designed to be operated from room temperature down to liquid helium temperature. The device represents a non-destructive charge counter as well as a sensitive timing circuit. We present the concept and design details of the device. We have characterized its performance and show measurements with low-energy highly charged ions (such as Ar(13+)) passing through one of the electrodes of a cylindrical Penning trap. This work demonstrates a novel approach of non-destructive, low noise detection of charged particles which is, depending on the bunch structure, suitable, e.g., for ion traps, low-energy beamlines or accelerator transfer sections. PMID:26628124

  9. Application of Goubau Surface Wave Transmission Line for Improved Bench Testing of Diagnostic Beamline Elements

    SciTech Connect

    John Musson, Keith Cole, Sheldon Rubin

    2009-05-01

    In-air test fixtures for beamline elements typically utilize an X-Y positioning stage, and a wire antenna excited by an RF source. In most cases, the antenna contains a standing wave, and is useful only for coarse alignment measurements in CW mode. A surface-wave (SW) based transmission line permits RF energy to be launched on the wire, travel through the beamline component, and then be absorbed in a load. Since SW transmission lines employ travelling waves, the RF energy can be made to resemble the electron beam, limited only by ohmic losses and dispersion. Although lossy coaxial systems are also a consideration, the diameter of the coax introduces large uncertainties in centroid location. A SW wire is easily constructed out of 200 micron magnet wire, which more accurately approximates the physical profile of the electron beam. Benefits of this test fixture include accurate field mapping, absolute calibration for given beam currents, Z-axis independence, and temporal response measurements of sub-nanosecond pulse structures. Descriptions of the surface wave launching technique, transmission line, and instrumentation are presented, along with measurement data.

  10. UV-CD12: synchrotron radiation circular dichroism beamline at ANKA

    PubMed Central

    Bürck, Jochen; Roth, Siegmar; Windisch, Dirk; Wadhwani, Parvesh; Moss, David; Ulrich, Anne S.

    2015-01-01

    Synchrotron radiation circular dichroism (SRCD) is a rapidly growing technique for structure analysis of proteins and other chiral biomaterials. UV-CD12 is a high-flux SRCD beamline installed at the ANKA synchrotron, to which it had been transferred after the closure of the SRS Daresbury. The beamline covers an extended vacuum-UV to near-UV spectral range and has been open for users since October 2011. The current end-station allows for temperature-controlled steady-state SRCD spectroscopy, including routine automated thermal scans of microlitre volumes of water-soluble proteins down to 170 nm. It offers an excellent signal-to-noise ratio over the whole accessible spectral range. The technique of oriented circular dichroism (OCD) was recently implemented for determining the membrane alignment of α-helical peptides and proteins in macroscopically oriented lipid bilayers as mimics of cellular membranes. It offers improved spectral quality <200 nm compared with an OCD setup adapted to a bench-top instrument, and accelerated data collection by a factor of ∼3. In addition, it permits investigations of low hydrated protein films down to 130 nm using a rotatable sample cell that avoids linear dichroism artifacts. PMID:25931105

  11. Neutral beamline with ion energy recovery based on magnetic blocking of electrons

    DOEpatents

    Stirling, William L.

    1982-01-01

    A neutral beamline generator with energy recovery of the full-energy ion ponent of the beam based on magnetic blocking of electrons is provided. Ions from a positive ion source are accelerated to the desired beam energy from a slightly positive potential level with respect to ground through a neutralizer cell by means of a negative acceleration voltage. The unneutralized full-energy ion component of the beam exiting the neutralizer are retarded and slightly deflected and the electrons in the neutralizer are blocked by a magnetic field generated transverse to the beamline. An electron collector in the form of a coaxial cylinder surrounding and protruding axial a few centimeters beyond the neutralizer exit terminates the electrons which exit the neutralizer in an E x B drift to the collector when the collector is biased a few hundred volts positive with respect to the neutralizer voltage. The neutralizer is operated at the negative acceleration voltage, and the deflected full energy ions are decelerated and the charge collected at ground potential thereby expending none of their energy received from the acceleration power supply.

  12. Neutral beamline with ion energy recovery based on magnetic blocking of electrons

    DOEpatents

    Stirling, W.L.

    1980-07-01

    A neutral beamline generator with energy recovery of the full-energy ion component of the beam based on magnetic blocking of electrons is provided. Ions from a positive ion source are accelerated to the desired beam energy from a slightly positive potential level with respect to ground through a neutralizer cell by means of a negative acceleration voltage. The unneutralized full-energy ion component of the beam exiting the neutralizer are retarded and slightly deflected and the elecrons in the neutralizer are blocked by a magnetic field generated transverse to the beamline. An electron collector in the form of a coaxial cylinder surrounding and protruding axial a few centimeters beyond the neutralizer exit terminates the electrons which exit the neutralizer in an E x B drift to the collector when the collector is biased a few hundred volts positive with respect to the neutralizer voltage. The neutralizer is operated at the negative acceleration voltage. The neutralizer is operated at the negative acceleration voltage, and the deflected full energy ions are decelerated and the charge collected at ground potential thereby expending none of their energy received from the acceleration power supply.

  13. Double-crystal monochromator as the first optical element in BESSRC-CAT beamlines

    SciTech Connect

    Beno, M.A.; Ramanathan, M.

    1996-09-01

    The first optical element in the BESSRC-CAT beamlines at the Advanced Photon Source will be a monochromator, so that a standard design for this critical component is advantageous. The monochromator we have designed is a double-crystal, fixed-exit scheme with a constant offset designed for UHV operation, thereby allowing windowless operation of the beamlines. The crystals are mounted on a turntable with the first crystal at the center of rotation. A mechanical linkage is used to correctly position the second crystal and maintain a constant offset. The main drive for the rotary motion is provided by a vacuum-compatible Huber goniometer isolated from the main vacuum chamber. Rotary motion of the primary monochromator stage is accomplished by using two adjacent vacuum chambers connected only by the small annular opening around a hollow stainless steel shaft, which connects the Huber goniometer to the turntable on which the crystals are mounted. The design of the monochromator is such that it can accommodate both water and liquid nitrogen cooling for the crystal optics. The basic design for the monochromator linkage mechanism will be presented along with details of the monochromator chamber. The results of initial optical tests of the monochromator system using tilt sensors and a precision autocollimator will also be given. {copyright} {ital 1996 American Institute of Physics.}

  14. First tests of the ion irradiation and implantation beamline at the CMAM

    NASA Astrophysics Data System (ADS)

    Jiménez-Rey, D.; Benedicto, M.; Muñoz-Martín, A.; Bachiller-Perea, D.; Olivares, J.; Climent-Font, A.; Gómez-Ferrer, B.; Rodríguez, A.; Narros, J.; Maira, A.; Álvarez, J.; Nakbi, A.; Zucchiatti, A.; de Aragón, F.; García, J. M.; Vila, R.

    2014-07-01

    The implantation and irradiation beamline of the Tandem ion accelerator of the Centro de Micro Análisis de Materiales (CMAM), in Madrid, has been recently completed with a beam sweep and monitoring system, and a cryostat/furnace. These new implementations convert the beamline into a versatile tool to implant ions, between H and Au2, in different materials with precise control of the sample temperature, which may be varied between -180 °C and 600 °C. The size of the swept area on target may be as large as 10 × 10 cm2. The implantation chamber also allows carrying out in situ or/and on line analyses during the irradiations by means of advanced optical measurements, as well as ion beam analyses (IBA). These advancements can be employed in novel applications such as the fabrication of optical waveguides and irradiation tests of structural and functional materials for future fusion reactors. The results of beam tests and first experiments are shown.

  15. New Developments at the XMaS Beamline For Magnetic and High Resolution Diffraction

    SciTech Connect

    Thompson, P.B.J.; Bouchenoire, L.; Brown, S.D.; Mannix, D.; Paul, D.F.; Lucas, C.; Kervin, J.; Cooper, M.J.; Arakawa, P.; Laughon, G.

    2004-05-12

    We report here on a number of developments that include enhancements of the sample environment on the XMaS beamline and the flux available at low energy. A 4 Tesla superconducting magnet has been designed to fit within the Euler cradle of a six circle Huber diffractometer, allowing scattering in both horizontal and vertical planes. The geometry of the magnet allows the application of longitudinal, transverse horizontal, and vertical fields. A further conventional magnet ({approx} 0.1 T) to minimize air absorption at low energies ({approx} 3KeV) has been designed for two circle applications, such as reflectivity. A novel in-vacuum slit screen has been developed, also minimizing absorption at low energies. New equipment for performing in-situ studies of surfaces in the electrochemical environment has been developed to allow control of the solution and sample temperature over the region of -5C to 80C. Preliminary experiments on the surface reconstructions of Au(111) in an electrolyte have been performed, whilst commissioning at the same time a MAR CCD detector for the beamline.

  16. Particle optics and accelerator modeling software for industrial and laboratory beamline design

    NASA Astrophysics Data System (ADS)

    Gillespie, George H.; Hill, Barrey W.

    1998-04-01

    The expanding variety of accelerator applications in research and industry places increased demands upon scientists and engineers involved in developing new accelerator and beamline designs. Computer codes for particle optics simulation have always played an important role in the design process and enhanced software tools offer the promise of improved productivity for beamline designers. This paper summarizes recent work on the development of advanced graphic user interface (GUI) software components, that can be linked directly to many of the standard particle optics programs used in the accelerator community, and which are aimed at turning that promise of improved productivity into a reality. An object oriented programming (OOP) approach has been adopted and a number of GUI components have been developed that run on several different operating systems. The emphasis is on assisting users in the setup and running of the optics programs without requiring any knowledge of the format, syntax, or similar requirements of the input. The components are being linked with several popular optics programs, including TRANSPORT, TURTLE, TRACE 3-D and PARMILA, to form integrated easy-to-use applications. Several advanced applications linking the GUI components with Lie algebra and other high-order simulation codes, as well as system level and facility modeling codes, are also under development. An overview of the work completed to date is presented, and examples of the new tools running on the Windows 95 operating system are illustrated.

  17. Evaluation of different synchrotron beamline configurations for X-ray fluorescence analysis of environmental samples.

    PubMed

    Barberie, Sean R; Iceman, Christopher R; Cahill, Catherine F; Cahill, Thomas M

    2014-08-19

    Synchrotron radiation X-ray fluorescence (SR-XRF) is a powerful elemental analysis tool, yet synchrotrons are large, multiuser facilities that are generally not amenable to modification. However, the X-ray beamlines from synchrotrons can be modified by simply including X-ray filters or removing monochromators to improve the SR-XRF analysis. In this study, we evaluated four easily applied beamline configurations for the analysis of three representative environmental samples, namely a thin aerosol sample, an intermediate thickness biological sample, and a thick rare earth mineral specimen. The results showed that the "white beam" configuration, which was simply the full, polychromatic output of the synchrotron, was the optimal configuration for the analysis of thin samples with little mass. The "filtered white beam" configuration removed the lower energy X-rays from the excitation beam so it gave better sensitivity for elements emitting more energetic X-rays. The "filtered white beam-filtered detector" configuration sacrifices the lower energy part of the spectrum (<15 keV) for improved sensitivity in the higher end (∼26 to 48 keV range). The use of a monochromatic beam, which tends to be the standard mode of operation for most SR-XRF analyses reported in the literature, gave the least sensitive analysis.

  18. Surface and interface analysis of nanomaterials at microfocus beamline (BL-16) of Indus-2

    NASA Astrophysics Data System (ADS)

    Das, Gangadhar; Khooha, Ajay; Kane, S. R.; Singh, A. K.; Tiwari, M. K.

    2016-05-01

    Analysis of chemical nature and electronic structure at the interface of a thin film medium is important in many technological applications as well as to understand overall efficiency of a thin film device. Synchrotron radiation based x-ray spectroscopy is a promising technique to study interface nature of the nanomaterials with atomic resolutions. A combined x-ray reflectivity and grazing incidence x-ray fluorescence measurement facility has been recently constructed at the BL-16 microfocus beamline of Indus-2 synchrotron facility to accomplish surface-interface microstructural characterization of thin layered materials. It is also possible to analyze contaminates or adsorbed ad-atoms on the surface of the thin nanostructure materials. The BL-16 beamline also provides an attractive platform to perform a variety of analytical research activities especially in the field of micro x-ray fluorescence and ultra-trace elements analysis using Synchrotron radiation. We describe various salient features of the BL-16 reflectometer experimental station and the detailed description of its capabilities through the measured results, obtained for various thin layered nanomaterials.

  19. Elliptically polarizing undulator beamline 4.0.1 for magnetic spectroscopy at the Advanced Light Source

    SciTech Connect

    Martynov, V.V.; Young, A.T.; Padmore, H.A.

    1996-08-01

    A beamline for high resolution spectroscopy with elliptically polarized X-rays is described.The working energy range is large, from 20 eV to above 1800 eV. The resolving power is on the order of 10,000 at low energies (20-200 eV) and 6000 at high energies (200-1800 eV). This is achieved using a variable deviation angle plane grating monochromator. A single grating, with one line density and a varying groove depth, is used to cover the entire energy range. The beamline has been designed to operate with either one or two x-ray beams propagating simultaneously through the monochromator and to the experimental station. Switching between polarizations at rates of 0.1 Hz and slower is accomplished in the single beam mode by alternating the output of the elliptically polarized undulator source between left and right polarization. Fast polarization switching, at rates of 100-1000 Hz, is provided in the two beam mode by mechanical chopping between two photon beams, one of which is right circularly polarized, and the other left circularly polarized.

  20. High-Resolution and Low-Temperature Photoemission Spectroscopy at the Hisor Helical-Undulator Beamline

    NASA Astrophysics Data System (ADS)

    Arita, Masashi; Shimada, Kenya; Namatame, Hirofumi; Taniguchi, Masaki

    We report an experimental system dedicated for high-resolution and low-temperature photoemission spectroscopy installed on the helical-undulator beamline of a compact 700 MeV electron-storage ring (HiSOR) at Hiroshima University. A 3 m off-plane Eagle normal-incidence monochromator at the beamline covers the photon-energy range of hν = 4-40 eV. From the photoemission spectra near the Fermi edge of evaporated Au film, the total energy resolution was estimated to be 4.5 and 7.5 meV at hν = 7.1 and 22.6 eV, respectively. We have also performed photoemission measurements of Yb metal, which demonstrated highly bulk-sensitive spectra for the excitation by low energy photon. The high-resolution photoemission spectra of Y1 - xCaxTiO3 with x = 0.41 in the vicinity of the boundary between the metallic and insulating phases exhibited anomalous temperature dependence in comparison with those of normal metals.

  1. Ultrafast beam dump materials and mirror coatings tested with the ELI beamlines LIDT test station

    NASA Astrophysics Data System (ADS)

    Durák, Michal; Kramer, Daniel; Velpula, Praveen K.; Cupal, Josef; Medřík, TomáÅ.¡; Hřebíček, Jan; Golasowski, Jiří; Peceli, Davorin; Fekete, Ladislav; Å tepán, Václav; Kozlová, Michaela; Rus, Bedřich

    2015-11-01

    The ELI Beamlines project will deliver ultrafast laser pulses with peak powers up to 10PW available every minute and PW class beams at 10Hz complemented by a 10TW 1kHz beamline. To properly determine damage thresholds of involved optical components in conditions similar to the operational environment and with expected laser parameters, a high vacuum LIDT test station was constructed at PALS facility. Our study presents results of ISO based S-on-1 and R-on-1 tests in femtosecond regime (50fs, 800nm, 10Hz/1kHz) performed on two different types of coatings: a) highabsorption black coatings with low outgassing rates, intended for use as a beam dump surface; and b) high-reflectivity, low-dispersion 45° AOI ultrafast mirror coatings. Testing of absorptive coatings was accompanied with QMS residual gas analysis to verify, that high intensity laser radiation approaching the damage threshold does not increase concentration of volatile organic compounds in the vacuum chamber. In case of HR mirror coatings, we also investigate the effect of cleaning on LIDT value, comparing characteristic S-on-1 curves of given sample with values obtained after 12h immersion in ethanol-water solution.

  2. Antithrombin III blood test

    MedlinePlus

    ... be due to: Bone marrow transplant Disseminated intravascular coagulation (DIC) AT III deficiency, an inherited condition Liver ... Schmaier AH, Miller JL. Coagulation and fibrinolysis. In: McPherson ... Management by Laboratory Methods . 22nd ed. Philadelphia, PA: ...

  3. A new optical scheme for large-extraction small-aberration vacuum-ultraviolet synchrotron radiation beamlines.

    PubMed

    Moreno, Thierry

    2016-09-01

    Vacuum-ultraviolet radiation delivered by bending-magnet sources is used at numerous synchrotron radiation facilities worldwide. As bending-magnet radiation is inherently much less collimated compared with undulator sources, the generation of high-quality intense bending-magnet vacuum-ultraviolet photon beams is extremely demanding in terms of the optical layout due to the necessary larger collection apertures. In this article, an optimized optical layout which takes into account both the optical and electron beam properties is proposed. This layout delivers an improved beam emittance of over one order of magnitude compared with existing vacuum-ultraviolet bending-magnet beamlines that, up to now, do not take into account electron beam effects. The arrangement is made of two dedicated mirrors, a cylindrical and a cone-shaped one, that focus independently both the horizontal and the vertical emission of a bending-magnet source, respectively, and has been already successfully applied in the construction of the infrared beamline at the Brazilian synchrotron. Using this scheme, two vacuum-ultraviolet beamline designs based on a SOLEIL synchrotron bending-magnet source are proposed and analysed. They would be useful for future upgrades to the DISCO beamline at SOLEIL and could be readily implemented at other synchrotron radiation facilities.

  4. A decade of user operation on the macromolecular crystallography MAD beamline ID14-4 at the ESRF.

    PubMed

    McCarthy, Andrew A; Brockhauser, Sandor; Nurizzo, Didier; Theveneau, Pascal; Mairs, Trevor; Spruce, Darren; Guijarro, Matias; Lesourd, Marc; Ravelli, Raimond B G; McSweeney, Sean

    2009-11-01

    ID14-4 at the ESRF is the first tunable undulator-based macromolecular crystallography beamline that can celebrate a decade of user service. During this time ID14-4 has not only been instrumental in the determination of the structures of biologically important molecules but has also contributed significantly to the development of various instruments, novel data collection schemes and pioneering radiation damage studies on biological samples. Here, the evolution of ID14-4 over the last decade is presented, and some of the major improvements that were carried out in order to maintain its status as one of the most productive macromolecular crystallography beamlines are highlighted. The experimental hutch has been upgraded to accommodate a high-precision diffractometer, a sample changer and a large CCD detector. More recently, the optical hutch has been refurbished in order to improve the X-ray beam quality on ID14-4 and to incorporate the most modern and robust optical elements used at other ESRF beamlines. These new optical elements will be described and their effect on beam stability discussed. These studies may be useful in the design, construction and maintenance of future X-ray beamlines for macromolecular crystallography and indeed other applications, such as those planned for the ESRF upgrade.

  5. A new optical scheme for large-extraction small-aberration vacuum-ultraviolet synchrotron radiation beamlines.

    PubMed

    Moreno, Thierry

    2016-09-01

    Vacuum-ultraviolet radiation delivered by bending-magnet sources is used at numerous synchrotron radiation facilities worldwide. As bending-magnet radiation is inherently much less collimated compared with undulator sources, the generation of high-quality intense bending-magnet vacuum-ultraviolet photon beams is extremely demanding in terms of the optical layout due to the necessary larger collection apertures. In this article, an optimized optical layout which takes into account both the optical and electron beam properties is proposed. This layout delivers an improved beam emittance of over one order of magnitude compared with existing vacuum-ultraviolet bending-magnet beamlines that, up to now, do not take into account electron beam effects. The arrangement is made of two dedicated mirrors, a cylindrical and a cone-shaped one, that focus independently both the horizontal and the vertical emission of a bending-magnet source, respectively, and has been already successfully applied in the construction of the infrared beamline at the Brazilian synchrotron. Using this scheme, two vacuum-ultraviolet beamline designs based on a SOLEIL synchrotron bending-magnet source are proposed and analysed. They would be useful for future upgrades to the DISCO beamline at SOLEIL and could be readily implemented at other synchrotron radiation facilities. PMID:27577766

  6. Research at and Operation of the Materials Science Beamline (X-11) at the National Synchrotron Light Source. Final Report

    SciTech Connect

    Sayers, Dale E.

    2003-10-15

    This is the final report for DOE DE-FG02-89ER45384. An overview of the operational history and status of beamline X-11A at the end of the contract period, and a brief review of the core science program at NCSU and the scientific results of X-11A since the last progress report is also presented.

  7. Evaluation of SNS Beamline Shielding Configurations using MCNPX Accelerated by ADVANTG

    SciTech Connect

    Risner, Joel M; Johnson, Seth R.; Remec, Igor; Bekar, Kursat B.

    2015-01-01

    Shielding analyses for the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory pose significant computational challenges, including highly anisotropic high-energy sources, a combination of deep penetration shielding and an unshielded beamline, and a desire to obtain well-converged nearly global solutions for mapping of predicted radiation fields. The majority of these analyses have been performed using MCNPX with manually generated variance reduction parameters (source biasing and cell-based splitting and Russian roulette) that were largely based on the analyst's insight into the problem specifics. Development of the variance reduction parameters required extensive analyst time, and was often tailored to specific portions of the model phase space. We previously applied a developmental version of the ADVANTG code to an SNS beamline study to perform a hybrid deterministic/Monte Carlo analysis and showed that we could obtain nearly global Monte Carlo solutions with essentially uniform relative errors for mesh tallies that cover extensive portions of the model with typical voxel spacing of a few centimeters. The use of weight window maps and consistent biased sources produced using the FW-CADIS methodology in ADVANTG allowed us to obtain these solutions using substantially less computer time than the previous cell-based splitting approach. While those results were promising, the process of using the developmental version of ADVANTG was somewhat laborious, requiring user-developed Python scripts to drive much of the analysis sequence. In addition, limitations imposed by the size of weight-window files in MCNPX necessitated the use of relatively coarse spatial and energy discretization for the deterministic Denovo calculations that we used to generate the variance reduction parameters. We recently applied the production version of ADVANTG to this beamline analysis, which substantially streamlined the analysis process. We also tested importance function

  8. A Soft X-Ray (300-1000 eV) Active Grating Monochromator Beamline at NSRRC

    SciTech Connect

    Fung, H. S.; Yuh, J. Y.; Huang, L. J.; Tseng, T. C.; Perng, S. Y.; Wang, D. J.; Tsang, K. L.; Chung, S. C.

    2007-01-19

    To accommodate the growing number of users in the soft X-ray spectroscopy research at NSRRC, we have developed a modified Dragon-type beamline, namely the active grating monochromator (AGM) beamline. In this beamline, a selected photon beam of 9 mrad radiation fan in the horizontal direction from a bending magnet is focused horizontally by a tangential elliptical mirror to a position 1.7 m after exit slit, and vertically by a cylindrical vertical focusing mirror (VFM) onto the entrance slit. After the entrance slit, the photon beam is energy-dispersed and vertically focused by an active grating onto the fixed exit slit. During the energy scan, the radius and shape of the active grating are adjusted accordingly, and therefore the defocus and coma aberrations terms can be effectively eliminated, and hence the energy resolution is optimized. Following the exit slit, the dispersed photon beam is refocused by a toroidal mirror onto the sample. Shadow ray-tracing program is employed to simulate the beamline performance. Results show that the energy resolution can reach 10000, 6000, and 3500 in the energy ranges of 300-400 eV, 400-600 eV, and above 600 eV, respectively. The total photon flux at sample position should reach 1x1012 phs/sec/200mA/0.1%BW, and the focused beam size at sample position is estimated to be 1 mm x 0.2 mm (H x V, FWHM). This beamline is currently under construction and will be ready for commission in December, 2006.

  9. Developments in optics and performance at BL13-XALOC, the macromolecular crystallography beamline at the Alba Synchrotron

    PubMed Central

    Juanhuix, Jordi; Gil-Ortiz, Fernando; Cuní, Guifré; Colldelram, Carles; Nicolás, Josep; Lidón, Julio; Boter, Eva; Ruget, Claude; Ferrer, Salvador; Benach, Jordi

    2014-01-01

    BL13-XALOC is currently the only macromolecular crystallography beamline at the 3 GeV ALBA synchrotron near Barcelona, Spain. The optics design is based on an in-vacuum undulator, a Si(111) channel-cut crystal monochromator and a pair of KB mirrors. It allows three main operation modes: a focused configuration, where both mirrors can focus the beam at the sample position to 52 µm × 5.5 µm FWHM (H × V); a defocused configuration that can match the size of the beam to the dimensions of the crystals or to focus the beam at the detector; and an unfocused configuration, where one or both mirrors are removed from the photon beam path. To achieve a uniform defocused beam, the slope errors of the mirrors were reduced down to 55 nrad RMS by employing a novel method that has been developed at the ALBA high-accuracy metrology laboratory. Thorough commissioning with X-ray beam and user operation has demonstrated an excellent energy and spatial stability of the beamline. The end-station includes a high-accuracy single-axis diffractometer, a removable mini-kappa stage, an automated sample-mounting robot and a photon-counting detector that allows shutterless operation. The positioning tables of the diffractometer and the detector are based on a novel and highly stable design. This equipment, together with the operation flexibility of the beamline, allows a large variety of types of crystals to be tackled, from medium-sized crystals with large unit-cell parameters to microcrystals. Several examples of data collections measured during beamline commissioning are described. The beamline started user operation on 18 July 2012. PMID:24971961

  10. The SYRMEP Beamline of Elettra: Clinical Mammography and Bio-medical Applications

    SciTech Connect

    Tromba, G.; Abrami, A.; Casarin, K.; Chenda, V.; Dreossi, D.; Mancini, L.; Menk, R. H.; Quai, E.; Sodini, N.; Vascotto, A.; Longo, R.; Arfelli, F.; Castelli, E.; Astolfo, A.; Bregant, P.; Brun, F.; Hola, M.; Kaiser, J.

    2010-07-23

    At the SYnchrotron Radiation for MEdical Physics (SYRMEP) beamline of Elettra Synchrotron Light Laboratory in Trieste (Italy), an extensive research program in bio-medical imaging has been developed since 1997. The core program carried out by the SYRMEP collaboration concerns the use of Synchrotron Radiation (SR) for clinical mammography with the aim of improving the diagnostic performance of the conventional technique. The first protocol with patients, started in 2006 has been completed at the end of 2009 and the data analysis is now in progress.Regarding applications different from clinical imaging, synchrotron X-ray computed microtomography (micro-CT) is the most used technique, both in absorption and phase contrast. A new software tool, Pore3D, has been developed to perform a quantitative morphological analysis on the reconstructed slices and to access textural information of the sample under study.

  11. Acoustic methods for high-throughput protein crystal mounting at next-generation macromolecular crystallographic beamlines.

    PubMed

    Roessler, Christian G; Kuczewski, Anthony; Stearns, Richard; Ellson, Richard; Olechno, Joseph; Orville, Allen M; Allaire, Marc; Soares, Alexei S; Héroux, Annie

    2013-09-01

    To take full advantage of advanced data collection techniques and high beam flux at next-generation macromolecular crystallography beamlines, rapid and reliable methods will be needed to mount and align many samples per second. One approach is to use an acoustic ejector to eject crystal-containing droplets onto a solid X-ray transparent surface, which can then be positioned and rotated for data collection. Proof-of-concept experiments were conducted at the National Synchrotron Light Source on thermolysin crystals acoustically ejected onto a polyimide `conveyor belt'. Small wedges of data were collected on each crystal, and a complete dataset was assembled from a well diffracting subset of these crystals. Future developments and implementation will focus on achieving ejection and translation of single droplets at a rate of over one hundred per second. PMID:23955046

  12. Dedicated High-Resolution Powder Diffraction Beamline at the Advanced Photon Source

    SciTech Connect

    Lee, Peter L.; Beno, Mark A.; Shu Deming; Ramanathan, Mohan; Mitchell, John F.; Jorgensen, James D.; Von Dreele, Robert B.

    2004-05-12

    A high-resolution x-ray powder diffraction beamline that exploits the high flux, high energy resolution, and precise energy tuning of the third-generation synchrotron source will be built at the Advanced Photon Source (APS). The goal is to establish a high-resolution high-throughput dedicated powder instrument at the APS to serve the powder community. We describe design of the instrument that is able to measure a complete high-resolution powder pattern in one hour or less, uses automation to optimize throughput, has the ability to readily tune over a wide range of x-ray energies quickly and easily covering important absorption edges for resonant data measurements, and has the ability to accommodate various environmental devices for high-temperature, low-temperature or time-resolved data collection.

  13. The RIKEN Materials Science Beamline at SPring-8: Towards Visualization of Electrostatic Interaction

    SciTech Connect

    Kato, Kenichi; Higuchi, Masakazu; Hirose, Raita; Matsuda, Ryotaro; Kitagawa, Susumu; Takemoto, Michitaka; Kim, Jungeun; Ha, Sunyeo; Takata, Masaki

    2010-06-23

    In order to visualize molecular interaction by the experimental electrostatic potential analysis we have optimized the optical parameters and developed the high-resolution Debye-Scherrer camera at the RIKEN materials science beamline, BL44B2 of SPring-8. For the purpose the camera was designed to be equipped with the hybrid X-ray detector system. One is the conventional detector, the imaging plate readout off-line to carry out high d(interplanar spacing)-resolution measurements and the other is the CCD detector, which can be operated in a camera at variable distances for high angle-resolution measurements. In addition we have been developing an in-situ properties measurement system to visualize the electrostatic interaction completely synchronized with material functions.

  14. Versatile variable temperature insert at the DEIMOS beamline for in situ electrical transport measurements.

    PubMed

    Joly, L; Muller, B; Sternitzky, E; Faullumel, J G; Boulard, A; Otero, E; Choueikani, F; Kappler, J P; Studniarek, M; Bowen, M; Ohresser, P

    2016-05-01

    The design and the first experiments are described of a versatile cryogenic insert used for its electrical transport capabilities. The insert is designed for the cryomagnet installed on the DEIMOS beamline at the SOLEIL synchrotron dedicated to magnetic characterizations through X-ray absorption spectroscopy (XAS) measurements. This development was spurred by the multifunctional properties of novel materials such as multiferroics, in which, for example, the magnetic and electrical orders are intertwined and may be probed using XAS. The insert thus enables XAS to in situ probe this interplay. The implementation of redundant wiring and careful shielding also enables studies on operating electronic devices. Measurements on magnetic tunnel junctions illustrate the potential of the equipment toward XAS studies of in operando electronic devices.

  15. First photon-shutter development for APS insertion device beamline front ends

    NASA Astrophysics Data System (ADS)

    Shu, Deming; Nian, H. L. Thomas; Wang, Zhibi; Collins, Jeffrey T.; Ryding, David G.; Kuzay, Tuncer M.

    1993-02-01

    One of the most critical components on the Advanced Photon Source (APS) insertion device (ID) beamline front ends is the first photon shutter. It operates in two modes to fully intercept the high total power and high-heat-flux ID photon beam in seconds (normal mode) or in less than 100 ms (emergency fast mode). It is designed to operate in ultra high vacuum (UHV). The design incorporates a multi-channel rectangular bar, bent in a `hockey stick' configuration, with two-point suspension. The flanged end is an articulated bellows with rolling hinges. The actuation end is a spring-assisted, pneumatic fail-safe flexural pivot type. The coolant (water) channels incorporate brazed copper foam to enhance the heat transfer, a tube technology particular to the APS. The design development, and material aspects, as well as the extensive thermal and vibrational analyses in support of the design, are presented in this paper.

  16. Strategies and limitations for fluorescence detection of XAFS at high flux beamlines

    DOE PAGES

    Heald, Steve M.

    2015-02-17

    The issue of detecting the XAFS signal from dilute samples is discussed in detail with the aim of making best use of high flux beamlines that provide up to 1013photons-1. Various detection methods are compared, including filters with slits, solid state detectors, crystal analyzers and combinations of these. These comparisons rely on simulations that use experimentally determined parameters. It is found that inelastic scattering places a fundamental limit on detection, and that it is important to take proper account of the polarization dependence of the signals. The combination of a filter–slit system with a solid state detector is a promisingmore » approach. With an optimized system good performance can be obtained even if the total count rate is limited to 107Hz. Detection schemes with better energy resolution can help at the largest dilutions if their collection efficiency and count rate limits can be improved.« less

  17. Strategies and limitations for fluorescence detection of XAFS at high flux beamlines

    SciTech Connect

    Heald, Steve M.

    2015-02-17

    The issue of detecting the XAFS signal from dilute samples is discussed in detail with the aim of making best use of high flux beamlines that provide up to 1013photons-1. Various detection methods are compared, including filters with slits, solid state detectors, crystal analyzers and combinations of these. These comparisons rely on simulations that use experimentally determined parameters. It is found that inelastic scattering places a fundamental limit on detection, and that it is important to take proper account of the polarization dependence of the signals. The combination of a filter–slit system with a solid state detector is a promising approach. With an optimized system good performance can be obtained even if the total count rate is limited to 107Hz. Detection schemes with better energy resolution can help at the largest dilutions if their collection efficiency and count rate limits can be improved.

  18. Advanced photoelectric effect experiment beamline at Elettra: A surface science laboratory coupled with Synchrotron Radiation.

    PubMed

    Panaccione, G; Vobornik, I; Fujii, J; Krizmancic, D; Annese, E; Giovanelli, L; Maccherozzi, F; Salvador, F; De Luisa, A; Benedetti, D; Gruden, A; Bertoch, P; Polack, F; Cocco, D; Sostero, G; Diviacco, B; Hochstrasser, M; Maier, U; Pescia, D; Back, C H; Greber, T; Osterwalder, J; Galaktionov, M; Sancrotti, M; Rossi, G

    2009-04-01

    We report the main characteristics of the advanced photoelectric effect experiments beamline, operational at Elettra storage ring, featuring a fully independent double branch scheme obtained by the use of chicane undulators and able to keep polarization control in both linear and circular mode. The paper describes the novel technical solutions adopted, namely, (a) the design of a quasiperiodic undulator resulting in optimized suppression of higher harmonics over a large photon energy range (10-100 eV), (b) the thermal stability of optics under high heat load via cryocoolers, and (c) the end station interconnected setup allowing full access to off-beam and on-beam facilities and, at the same time, the integration of users' specialized sample growth chambers or modules.

  19. Improved High-Heat-Load Graphite Filter Design At CHESS Wiggler Beamlines

    SciTech Connect

    Savino, James J.; Shen Qun; Strieter, Gretchen; Fontes, Ernest; Pauling, Alan K.

    2004-05-12

    Conductively cooled highly-oriented pyrolytic graphite (HOPG) filters have been used at CHESS wiggler beamlines to protect downstream beryllium windows under high heat loads. In the past beam currents above 350 mA have caused excessively high temperatures on the existing HOPG filters, resulting in rapid sublimation of the graphite and drastic shortening of filter lifetimes. A new filter design which eliminates some drawbacks of the existing design is described. The new design utilizes a slotted water jet, which cools a thin, 'compliant' graphite-copper braze joint. Heat-transfer enhancements should enable an installed filter to survive beam currents of 450 mA. Optimization of design features and analysis results are discussed.

  20. Mirror and grating surface figure requirements for grazing incidence synchrotron radiation beamlines: Power loading effects

    SciTech Connect

    Hulbert, S.L.; Sharma, S.

    1987-10-21

    At present, grazing incidence mirrors are used almost exclusively as the first optical element in VUV and soft x-ray synchrotron radiation beam lines. The performance of these mirrors is determined by thermal and mechanical stress-induced figure errors as well as by figure errors remaining from the grinding and polishing process. With the advent of VUV and soft x-ray undulators and wigglers has come a new set of thermal stress problems related to both the magnitude and the spatial distribution of power from these devices. In many cases the power load on the entrance slits and gratings in these beamlines is no longer negligible. The dependence of thermally-induced front-end mirror figure errors on various storage ring and insertion device parameters (especially those at the NSLS) and the effects of these figure errors on a class of soft x-ray beam lines are presented. 17 refs., 5 figs., 2 tabs.

  1. Advanced photoelectric effect experiment beamline at Elettra: A surface science laboratory coupled with Synchrotron Radiation

    SciTech Connect

    Panaccione, G.; Vobornik, I.; Fujii, J.; Krizmancic, D.; Annese, E.; Giovanelli, L.; Maccherozzi, F.; Salvador, F.; De Luisa, A.; Benedetti, D.; Gruden, A.; Bertoch, P.; Rossi, G.; Polack, F.; Cocco, D.; Sostero, G.; Diviacco, B.; Hochstrasser, M.; Maier, U.; Pescia, D.; and others

    2009-04-15

    We report the main characteristics of the advanced photoelectric effect experiments beamline, operational at Elettra storage ring, featuring a fully independent double branch scheme obtained by the use of chicane undulators and able to keep polarization control in both linear and circular mode. The paper describes the novel technical solutions adopted, namely, (a) the design of a quasiperiodic undulator resulting in optimized suppression of higher harmonics over a large photon energy range (10-100 eV), (b) the thermal stability of optics under high heat load via cryocoolers, and (c) the end station interconnected setup allowing full access to off-beam and on-beam facilities and, at the same time, the integration of users' specialized sample growth chambers or modules.

  2. Report on the value engineering workshop on APS beamline front ends

    SciTech Connect

    Kuzay, T.

    1993-01-01

    A formal value engineering evaluation process was developed to address the front end components of the beamlines for the Advanced Photon Source (APS). This process (described in Section 2) involved an information phase, a creative phase, a judgment phase, a development phase, and a recommendation phase. Technical experts from other national laboratories and industry were invited to a two-day Value Engineering Workshop on November 5-6, 1992. The results of this Workshop are described in Section 4. Following the Workshop, various actions by the APS staff led to the redesign of the front end components, which are presented in Sections 5 and 6. The cost benefit analysis is presented in Section 7. It is important of realize that an added benefit of the Workshop was to obtain numerous design evaluations and enhancements of the front end components by experts in the field. As the design work proceeds to Title II completion, the APS staff is including many of these suggestions.

  3. A Johann-type X-ray emission spectrometer at the Rossendorf beamline.

    PubMed

    Kvashnina, Kristina O; Scheinost, Andreas C

    2016-05-01

    This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies. PMID:27140166

  4. Report of the Census Task Force on beamline control system requirements

    SciTech Connect

    Barsotti, E.J.; Bartlett, J.F.; Bogert, V.D.; Borcherding, F.O.; Butler, J.; Czarapata, P.C.; Spalding, W.J.; Thomas, A.D.

    1986-10-02

    A special task force was appointed to study the experience with the present beamline control system at Fermilab and to make recommendations in this area. The charge of the committee and the list of its members are appended. In order to carry out its assignment, the committee conducted a series of meetings in which it discussed the controls situation in general and the best way to approach the user community. The various groups of users were identified, and a letter was written to representatives of these groups asking questions concerning the present system and future needs. The committee met with each group to discuss the response to these questions. Written summaries of the discussions are appended. Conclusions are drawn regarding current problems, systematic upgrades and specific recommendations. (LEW)

  5. Highly efficient beamline and spectrometer for inelastic soft X-ray scattering at high resolution.

    PubMed

    Lai, C H; Fung, H S; Wu, W B; Huang, H Y; Fu, H W; Lin, S W; Huang, S W; Chiu, C C; Wang, D J; Huang, L J; Tseng, T C; Chung, S C; Chen, C T; Huang, D J

    2014-03-01

    The design, construction and commissioning of a beamline and spectrometer for inelastic soft X-ray scattering at high resolution in a highly efficient system are presented. Based on the energy-compensation principle of grating dispersion, the design of the monochromator-spectrometer system greatly enhances the efficiency of measurement of inelastic soft X-rays scattering. Comprising two bendable gratings, the set-up effectively diminishes the defocus and coma aberrations. At commissioning, this system showed results of spin-flip, d-d and charge-transfer excitations of NiO. These results are consistent with published results but exhibit improved spectral resolution and increased efficiency of measurement. The best energy resolution of the set-up in terms of full width at half-maximum is 108 meV at an incident photon energy tuned about the Ni L3-edge.

  6. The Scanning X-Ray Microprobe at the Esrf ``X-Ray Microscopy'' Beamline

    NASA Astrophysics Data System (ADS)

    Susini, J.; Salomé, M.; Fayard, B.; Ortega, R.; Kaulich, B.

    The development of high brilliance X-ray sources coupled with advances in manufacturing technologies of focusing optics has led to significant improvements in submicrometer probes for spectroscopy, diffraction and imaging applications. For instance, X-ray microscopy in the 1-10 keV energy range is better-suited for analyzing trace elements in fluorescence yield. This article will be biased towards submicron fluorescence microscopy developed on the ID21 beamline at the ESRF. The main technical developments, involving new focusing lenses or novel phase contrast method, are presented. Strengths and weaknesses of X-ray microscopy and spectromicroscopy techniques are discussed and illustrated by examples in biology, materials science and geology.

  7. Achieving Vibration Stability of the NSLS-II Hard X-ray Nanoprobe Beamline

    SciTech Connect

    Simos, N.; Chu, Y. N.; Broadbent, A.; Nazaretski, E.; Margulies, L.; Dyling, O.; Shen, Q.; Fallier, M.

    2010-08-30

    The Hard X-ray Nanoprobe (HXN) Beamline of National Synchrotron Light Source II (NSLS-lI) requires high levels of stability in order to achieve the desired instrument resolution. To ensure that the design of the endstation helps meet the stringent criteria and that natural and cultural vibration is mitigated both passively and actively, a comprehensive study complimentary to the design process has been undertaken. Vibration sources that have the potential to disrupt sensitive experiments such as wind, traffic and NSLS II operating systems have been studied using state of the art simulations and an array of field data. Further, final stage vibration isolation principles have been explored in order to be utilized in supporting endstation instruments. This paper presents results of the various study aspects and their influence on the HXN design optimization.

  8. A Johann-type X-ray emission spectrometer at the Rossendorf beamline.

    PubMed

    Kvashnina, Kristina O; Scheinost, Andreas C

    2016-05-01

    This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.

  9. Coherent Bragg nanodiffraction at the hard X-ray Nanoprobe beamline

    PubMed Central

    Hruszkewycz, S. O.; Holt, M. V.; Maser, J.; Murray, C. E.; Highland, M. J.; Folkman, C. M.; Fuoss, P. H.

    2014-01-01

    Bragg coherent diffraction with nanofocused hard X-ray beams provides unique opportunities for quantitative in situ studies of crystalline structure in nanoscale regions of complex materials and devices by a variety of diffraction-based techniques. In the case of coherent diffraction imaging, a major experimental challenge in using nanoscale coherent beams is maintaining a constant scattering volume such that coherent fringe visibility is maximized and maintained over the course of an exposure lasting several seconds. Here, we present coherent Bragg diffraction patterns measured from different nanostructured thin films at the Sector 26 Nanoprobe beamline at the Advanced Photon Source and demonstrate that with nanoscale positional control, coherent diffraction patterns can be measured with source-limited fringe visibilities more than 50% suitable for imaging by coherent Bragg ptychography techniques. PMID:24470418

  10. A new experiment station on beamline 4B7A at Beijing Synchrotron Radiation Facility

    NASA Astrophysics Data System (ADS)

    Zheng, L.; Zhao, Y. D.; Tang, K.; Ma, C. Y.; Hong, C. H.; Han, Y.; Cui, M. Q.; Guo, Z. Y.

    2014-11-01

    A new experiment station was installed on beamline 4B7A at Beijing Synchrotron Radiation Facility (BSRF), making it possible to record X-ray absorption fine structure (XAFS) spectrum in three modes over an energy range from 1750 eV to 6000 eV. A 13-element Si(Li) array detector and a single-element SDD detector were used to acquire data in partial fluorescence yield (PFY) mode. Two low-pressure noble gas ion chambers were adopted for measuring XAFS in transmission mode. In total electron yield (TEY) mode the current of sample is recorded. Solid, wet and liquid samples were suitable for this experimental station. Some representative results obtained from this station were shown and discussed.

  11. Midinfrared beamline at the National Synchrotron Light Source port U2B

    SciTech Connect

    Carr, G.L. ); Hanfland, M. ); Williams, G.P. )

    1995-02-01

    A new infrared beamline has been developed on a conventional dipole bending magnet port of the vacuum ultraviolet ring at the National Synchrotron Light Source. The port provides approximately 12 mrad horizontal and 8 mrad vertical aperture, which limits the useful spectral range to wavelengths less than 20 [mu]m. Though the total flux across the midinfrared is less than that from a globar source, the calculated brightness is at least two orders of magnitude greater. Also, the synchrotron source delivers light in subnanosecond pulses. The developing experimental programs include studies of hydrogen and other materials at extremely high pressures, and time-resolved studies of infrared sensor materials. The measurement results presented here, characterizing the actual brightness advantage and spectroscopic performance, demonstrate the synchrotron's remarkable advantage for microspectroscopic studies.

  12. ELI-Beamlines: development of next generation short-pulse laser systems

    NASA Astrophysics Data System (ADS)

    Rus, B.; Bakule, P.; Kramer, D.; Naylon, J.; Thoma, J.; Green, J. T.; Antipenkov, R.; Fibrich, M.; Novák, J.; Batysta, F.; Mazanec, T.; Drouin, M. A.; Kasl, K.; Baše, R.; Peceli, D.; Koubíková, L.; Trojek, P.; Boge, R.; Lagron, J. C.; Vyhlídka, Å.; Weiss, J.; Cupal, J.,; Hřebíček, J.; Hříbek, P.; Durák, M.; Polan, J.; Košelja, M.; Korn, G.; Horáček, M.; Horáček, J.; Himmel, B.; Havlíček, T.; Honsa, A.; Korouš, P.; Laub, M.; Haefner, C.; Bayramian, A.; Spinka, T.; Marshall, C.; Johnson, G.; Telford, S.; Horner, J.; Deri, B.; Metzger, T.; Schultze, M.; Mason, P.; Ertel, K.; Lintern, A.; Greenhalgh, J.; Edwards, C.; Hernandez-Gomez, C.; Collier, J.; Ditmire, T.,; Gaul, E.; Martinez, M.; Frederickson, C.; Hammond, D.; Malato, C.; White, W.; Houžvička, J.

    2015-05-01

    Overview of the laser systems being built for ELI-Beamlines is presented. The facility will make available high-brightness multi-TW ultrashort laser pulses at kHz repetition rate, PW 10 Hz repetition rate pulses, and kilojoule nanosecond pulses for generation of 10 PW peak power. The lasers will extensively employ the emerging technology of diode-pumped solid-state lasers (DPSSL) to pump OPCPA and Ti:sapphire broadband amplifiers. These systems will provide the user community with cutting-edge laser resources for programmatic research in generation and applications of high-intensity X-ray sources, in particle acceleration, and in dense-plasma and high-field physics.

  13. Design of an elliptically bent refocus mirror for the MERLIN beamline at the advanced light source

    NASA Astrophysics Data System (ADS)

    Kelez, Nicholas; Chuang, Yi-De; Smith-Baumann, Alexis; Franck, Keith; Duarte, R.; Lanzara, A.; Hasan, M. Z.; Dessau, D. S.; Chiang, T. C.; Shen, Z.-X.; Hussain, Zahid

    2007-11-01

    There is an increasing demand for well-focused beam with high quality imaging of the full field to further explore the potential of novel instruments. For beamlines operating at focal point, mechanical benders have often been used to shape the refocusing mirror into an ideal elliptical cylinder. Unfortunately, the limited number of couplings for these mechanisms requires specific substrate side-shaping, often calculated using beam bending theory [J.H. Underwood, Space Sci. Instrum. 3 (1977) 259; M. Howells et al., Opt. Eng. 39 (2000) 2748; T. Warwick et al., Document available at OSTI website: http://www.osti.gov/energycitations/servlets/purl/842557-JYZCS3/native/], to meet demanding figure requirements. Here, we use finite element analysis (FEA) to validate the side-shaping algorithm and then couple the output with SHADOW to evaluate mirror performance when an ideal ellipse is not achieved.

  14. Benchtop Nonresonant X-ray Emission Spectroscopy: Coming Soon to Laboratories and XAS Beamlines Near You?

    NASA Astrophysics Data System (ADS)

    Mortensen, Devon R.; Seidler, Gerald T.; Ditter, Alexander S.; Glatzel, Pieter

    2016-05-01

    Recently developed instrumentation at the University of Washington has allowed for nonresonant x-ray emission spectra (XES) to be measured in a laboratory-setting with an inexpensive, easily operated system. We present a critical evaluation of this equipment by means of Kβ and valence-level XES measurements for several Co compounds. We find peak count rates of ∼5000/s for concentrated samples and a robust relative energy scale with reproducibility of 25 meV or better. We furthermore find excellent agreement with synchrotron measurements with only modest loss in energy resolution. Instruments such as ours, based on only conventional sources that are widely sold for elemental analysis by x-ray fluorescence, can fill an important role to diversify the research applications of XES both by their presence in non-synchrotron laboratories and by their use in conjunction with XAFS beamlines where the complementarity of XAFS and XES holds high scientific potential.

  15. Universal imaging: Dissociative ionization of polyatomic molecules, chemical dynamics beamline 9.0.2

    SciTech Connect

    Ahmed, M.; Chen, D.; Suits, A.G.

    1997-04-01

    A third endstation was recently added to the Chemical Dynamics beamline, designed to exploit the high flux broadband undulator light for a range of studies of reactive scattering, photochemistry and photoionization processes using time-of-flight mass spectroscopy coupled with position-sensitive detection. Two molecular beam sources are fixed at right angles, with the undulator light, or laser beams, intersecting the molecular beams at 45{degrees}. To date, beamline experiments have included a study of dissociative photoionization of a variety of molecules including N{sub 2}O and SF{sub 6}. In this mode, a single molecular beam source is used, with the tunable undulator light inducing, in SF{sub 6} for example, the process SF{sub 6} {r_arrow} SF{sub 6}{sup +} + e{sup {minus}} {r_arrow} SF{sub 5}{sup +} + F + e{sup {minus}}. The SF{sub 5}{sup +} ions are accelerated up the flight tube, mass selected and detected as a function of position on a phosphor screen viewed by a CCD camera. The position directly reveals the recoil speed (or translational energy release) and angular distribution for the dissociative ionization process. Furthermore, this measurement is obtained for all recoil speeds and angles simultaneously. Such detailed angular information has not previously been obtained for dissociative ionization processes; typically ion time-of-flight profiles are deconvoluted to yield rough insight into the angular distributions. The recorded image is actually a 2-dimensional projection of the nascent 3-dimensional velocity distribution, but established tomographic techniques enable the authors to reconstruct the 3-D distribution.

  16. Predicted optical performance of the GM/CA@APS micro-focus beamline

    NASA Astrophysics Data System (ADS)

    Fischetti, Robert F.; Yoder, Derek; Xu, Shenglan; Makarov, Oleg; Ogata, Craig; Smith, Janet L.

    2013-03-01

    GM/CA at the APS has developed microcrystallography capabilities for structural biology applications. The robust, quad, mini-beam collimators, which enable users to rapidly select between a 5, 10 or 20 micron diameter beam or a scatter guard for the full focused beam, are coupled with several powerful automated software tools that are built into the beamline control system JBluIce-EPICS. Recent successes at beamlines around the world in solving structures from microcrystals (2 - 10 microns) have led to increased demand for high-intensity micro-focus beams. We have designed a new micro-focus endstation to increase the intensity in mini- and micro-beams at GM/CA by one to two orders of magnitude to meet this growing demand. The new optical design is based on the well-established approach of using two-stage demagnification. The existing bimorph mirrors, arranged in a Kirkpatrick-Baez geometry, focus the beam onto slits located upstream of the sample whereby the slit aperture defines a secondary source, that is reimaged with a second pair of mirrors. This design incorporates two focal modes: a mini-beam mode where the beam is focused to 20-micron diameter and a micro-beam mode where it is focused to 5-microns. The size of the secondary source aperture can be varied rapidly (seconds) to adjust the beam size at the sample position in two ranges 20 - 3 micron and 5 - 1 micron. The second set of mirrors will each have two super polished ellipses allowing quick (minutes) interchange between modes.

  17. Predicted optical performance of the GM/CA@APS micro-focus beamline

    PubMed Central

    Fischetti, Robert F.; Yoder, Derek; Xu, Shenglan; Makarov, Oleg; Ogata, Craig; Smith, Janet L.

    2014-01-01

    GM/CA at the APS has developed microcrystallography capabilities for structural biology applications. The robust, quad, mini-beam collimators, which enable users to rapidly select between a 5, 10 or 20 micron diameter beam or a scatter guard for the full focused beam, are coupled with several powerful automated software tools that are built into the beamline control system JBluIce-EPICS. Recent successes at beamlines around the world in solving structures from microcrystals (2 – 10 microns) have led to increased demand for high-intensity micro-focus beams. We have designed a new micro-focus endstation to increase the intensity in mini- and micro-beams at GM/CA by one to two orders of magnitude to meet this growing demand. The new optical design is based on the well-established approach of using two-stage demagnification. The existing bimorph mirrors, arranged in a Kirkpatrick-Baez geometry, focus the beam onto slits located upstream of the sample whereby the slit aperture defines a secondary source, that is reimaged with a second pair of mirrors. This design incorporates two focal modes: a mini-beam mode where the beam is focused to 20-micron diameter and a micro-beam mode where it is focused to 5-microns. The size of the secondary source aperture can be varied rapidly (seconds) to adjust the beam size at the sample position in two ranges 20 – 3 micron and 5 – 1 micron. The second set of mirrors will each have two super polished ellipses allowing quick (minutes) interchange between modes. PMID:25383086

  18. Preliminary measurements on the new TOF system installed at the AMS beamline of INFN-LABEC

    NASA Astrophysics Data System (ADS)

    Palla, L.; Castelli, L.; Czelusniak, C.; Fedi, M. E.; Giuntini, L.; Liccioli, L.; Mandò, P. A.; Martini, M.; Mazzinghi, A.; Ruberto, C.; Schiavulli, L.; Sibilia, E.; Taccetti, F.

    2015-10-01

    A high resolution time of flight (TOF) system has been developed at LABEC, the 3 MV Tandem accelerator laboratory in Florence, in order to improve the sensitivity of AMS measurements on carbon samples with ultra-low concentration and also to measure other isotopes, such as 129I. The system can be employed to detect and identify residual interfering particles originated from the break-up of molecular isobars. The set-up has been specifically designed for low energy heavy ions: it consists of two identical time pick-off stations, each made up of a thin conductive foil and a Micro-Channel Plate (MCP) multiplier. The beamline is also equipped with a silicon detector, installed downstream the stop TOF station. In this paper the design of the new system and the implemented readout electronics are presented. The tests performed on the single time pick-off station are reported: they show that the maximum contribution to the timing resolution given by both the intrinsic MCP resolution and the electronics is ⩽500 ps (FWHM). For these tests, single particle pulsed beams of 2-5 MeV protons and 10 MeV 12C3+ ions, to simulate typical AMS conditions, were used. The preliminary TOF and TOF-E (TOF-energy) measurements performed with carbon beams after the installation of the new system on the AMS beam line are also discussed. These measurements were performed using the foil-MCP as the start stage and a silicon detector as the stop stage. The spectra acquired with carbon ions suggest the presence of a small residual background from neighboring masses reaching the end of the beamline with the same energy as the rare isotope.

  19. Conceptual design of the neutral beamline for TPX long pulse operation

    SciTech Connect

    Wright, K.E.; Dahlgren, F.; Fan, H.M.; Grisham, L.R.; Hammersand, F.G.; Kamperschroer, J.H.; Lontai, L.M.; Oldaker, M.E.; Rogoff, P.

    1993-11-01

    The Tokamak Physics Experiment (TPX) will require a minimum of 8.0 megawatts of Neutral Beam beating power to be injected into the plasma for pulse lengths up to one thousand (1000) seconds to meet the experimental objectives. The Neutral Beam Injection System (NBIS) for initial operation on TPX will consist of one neutral beamline (NBL) with three Ion sources. Provisions will be made for a total of three NBLs. The NBIS will provide S.S MW of 120 keV D{sup 0} and 2.S MW of partial-energy D{sup 0} at 60 keV and 40 keV. The system also provides for measuring the neutral beam power, limits excess cold gas from entering the torus, and provides independent power, control, and protection for each individual ion source and accelerating structure. The Neutral Beam/Torus Connecting Duct (NB/TCD) includes a vacuum valve, an electrical insulating break, alignment bellows, vacuum seals, internal energy absorbing protective elements, beam diagnostics and bakeout capability. The NBL support structure will support the NBL, which will weigh approximately 80 tons at the proper elevation and withstand a seismic event. The NBIS currently operational on the Tokamak Fusion Test Reactor (TFTR) at the Princeton Plasma Physics Laboratory (PPPL) is restricted to injection pulse lengths of two (2) seconds by the limited capability of various energy absorbers. This paper describes the modifications and improvements which will be implemented for the TFTR Neutral Beamlines and the NB/TCD to satisfy the TPX requirements.

  20. Rotating and semi-stationary multi-beamline architecture study for cardiac CT imaging

    NASA Astrophysics Data System (ADS)

    Wang, Jiao; Fitzgerald, Paul; Gao, Hewei; Jin, Yannan; Wang, Ge; De Man, Bruno

    2014-03-01

    Over the past decade, there has been abundant research on future cardiac CT architectures and corresponding reconstruction algorithms. Multiple cardiac CT concepts have been published, including third-generation single-source CT with wide-cone coverage, dual-source CT, and electron-beam CT, etc. In this paper, we apply a Radon space analysis method to two multi-beamline architectures: triple-source CT and semi-stationary ring-source CT. In our studies, we have considered more than thirty cardiac CT architectures and triple-source CT was identified as a promising solution, offering approximately a three-fold advantage in temporal resolution, which can significantly reduce motion artifacts due to the moving heart and lungs. In this work, we describe a triple-source CT architecture with all three beamlines (i.e. source-detector pairs) limited to the cardiac field of view in order to eliminate the radiation dose outside the cardiac region. We also demonstrate the capability of performing full field of view imaging when desired, by shifting the detectors. Ring-source dual-rotating-detector CT is another architecture of interest, which offers the opportunity to provide high temporal resolution using a full-ring stationary source. With this semi-stationary architecture, we found that the azimuthal blur effect can be greater than in a fully-rotating CT system. We therefore propose novel scanning modes to reduce the azimuthal blur in ring-source rotating detector CT. Radon space analysis method proves to be a useful method in CT system architecture study.

  1. Cleaning and outgassing studies of machinable tungsten for beamline safety shutters

    SciTech Connect

    Liu, C.; Ryding, D.; Nielsen, R.W.; Kruy, T.L.; Kuzay, T.M.

    1996-09-01

    Machinable tungsten blocks are used as safety shutters in the front ends and the beamlines at the Advanced Photon Source (APS). The machinable tungsten used is characterized as a UHV-compatible metal by the vendor and was developed through a joint research effort with the APS. However, because of the inherent porosity in the sintered tungsten metal, it may present a vacuum problem and has to be subjected to strict vacuum testing before it is put on the beamlines. We have chosen specially heat-treated machinable tungsten with a density of 18 g/cm{sup 3} for safety shutters. In-house-developed, environmentally friendly vacuum cleaning procedures were used. In this paper, we present results of thermal outgassing tests for machinable tungsten safety shutter sets. Each set consists of five blocks and has a total area of 4500 cm{sup 2}. A cleaning procedure using alkaline detergent ultrasonic washes, deionized water rinses, and a 500{degree}C vacuum furnace baking was used before outgassing measurements. Outgassing rates 10 hours after initial pump down at room temperature reached {approximately}1.60{times}10{sup {minus}10} Torr{center_dot}l{center_dot}s{sup {minus}1}{center_dot}cm{sup {minus}2} for machinable tungsten and {approximately}1.56{times}10{sup {minus}10} Torr{center_dot}l{center_dot}s{sup {minus}1}{center_dot}cm{sup {minus}2} for the stainless steel vacuum chamber. The outgassing rate of machinable tungsten 24 hours after an {ital in} {ital situ} 48 h bake at 160{degree}C is also comparable to that of the stainless steel vacuum chamber. The importance of a 500{degree}C vacuum furnace baking has been confirmed by outgassing studies for machinable tungsten sets that were not subject to vacuum furnace baking. {copyright} {ital 1996 American Institute of Physics.}

  2. Commissioning of a Soft X-ray Beamline PF-BL-16A with a Variable-Included-Angle Varied-Line-Spacing Grating Monochromator

    SciTech Connect

    Amemiya, Kenta; Toyoshima, Akio; Kikuchi, Takashi; Kosuge, Takashi; Nigorikawa, Kazuyuki; Sumii, Ryohei; Ito, Kenji

    2010-06-23

    The design and commissioning of a new soft X-ray beamline, BL-16A, at the Photon Factory is presented. The beamline consists of a pre-focusing mirror, an entrance slit, a variable-included-angle varied-line-spacing plane grating monochromator, and a post-focusing system as usual, and provides circularly and linearly polarized soft X rays in the energy range 200-1500 eV with an APPLE-II type undulator. The commissioning procedure for the beamline optics is described in detail, especially the check of the focal position for the zero-th order and diffracted X rays.

  3. The CAT-ACT Beamline at ANKA: A new high energy X-ray spectroscopy facility for CATalysis and ACTinide research

    NASA Astrophysics Data System (ADS)

    Zimina, A.; Dardenne, K.; Denecke, M. A.; Grunwaldt, J. D.; Huttel, E.; Lichtenberg, H.; Mangold, S.; Pruessmann, T.; Rothe, J.; Steininger, R.; Vitova, T.

    2016-05-01

    A new hard X-ray beamline for CATalysis and ACTinide research has been built at the synchrotron radiation facility ANKA. The beamline design is dedicated to X-ray spectroscopy, including ‘flux hungry’ photon-in/photon-out and correlative techniques with a special infrastructure for radionuclide and catalysis research. The CAT-ACT beamline will help serve the growing need for high flux/hard X-ray spectroscopy in these communities. The design, the first spectra and the current status of this project are reported.

  4. The GALAXIES beamline at the SOLEIL synchrotron: inelastic X-ray scattering and photoelectron spectroscopy in the hard X-ray range.

    PubMed

    Rueff, J P; Ablett, J M; Céolin, D; Prieur, D; Moreno, Th; Balédent, V; Lassalle-Kaiser, B; Rault, J E; Simon, M; Shukla, A

    2015-01-01

    The GALAXIES beamline at the SOLEIL synchrotron is dedicated to inelastic X-ray scattering (IXS) and photoelectron spectroscopy (HAXPES) in the 2.3-12 keV hard X-ray range. These two techniques offer powerful complementary methods of characterization of materials with bulk sensitivity, chemical and orbital selectivity, resonant enhancement and high resolving power. After a description of the beamline components and endstations, the beamline capabilities are demonstrated through a selection of recent works both in the solid and gas phases and using either IXS or HAXPES approaches. Prospects for studies on liquids are discussed.

  5. The GALAXIES beamline at the SOLEIL synchrotron: inelastic X-ray scattering and photoelectron spectroscopy in the hard X-ray range.

    PubMed

    Rueff, J P; Ablett, J M; Céolin, D; Prieur, D; Moreno, Th; Balédent, V; Lassalle-Kaiser, B; Rault, J E; Simon, M; Shukla, A

    2015-01-01

    The GALAXIES beamline at the SOLEIL synchrotron is dedicated to inelastic X-ray scattering (IXS) and photoelectron spectroscopy (HAXPES) in the 2.3-12 keV hard X-ray range. These two techniques offer powerful complementary methods of characterization of materials with bulk sensitivity, chemical and orbital selectivity, resonant enhancement and high resolving power. After a description of the beamline components and endstations, the beamline capabilities are demonstrated through a selection of recent works both in the solid and gas phases and using either IXS or HAXPES approaches. Prospects for studies on liquids are discussed. PMID:25537606

  6. The BioCAT undulator beamline 18ID: A facility for biological non-crystalline diffraction and x-ray absorption spectroscopy at the APS

    SciTech Connect

    Fischetti, R.; Stepanov, S.; Rosenbaum, G.; Barrea, R.; Black, E.; Gore, D.; Heurich, R.; Kondrashkina, E.; Kropf, A.J.; Wang, S.; Zhang, K.; Irving, T.C.; Bunker, G.B.

    2008-07-02

    The 18ID undulator beamline of the Biophysics Collaborative Access Team at the Advanced Photon Source, Argonne, IL, USA, is a high-performance instrument designed for, and dedicated to, the study of partially ordered and disordered biological materials using the techniques of small-angle X-ray scattering, fiber diffraction, and X-ray absorption spectroscopy. The beamline and associated instrumentation are described in detail and examples of the representative experimental results are presented.

  7. Implementation and performance of SIBYLS: a dual endstation small-angle X-ray scattering and macromolecular crystallography beamline at the Advanced Light Source.

    PubMed

    Classen, Scott; Hura, Greg L; Holton, James M; Rambo, Robert P; Rodic, Ivan; McGuire, Patrick J; Dyer, Kevin; Hammel, Michal; Meigs, George; Frankel, Kenneth A; Tainer, John A

    2013-02-01

    The SIBYLS beamline (12.3.1) of the Advanced Light Source at Lawrence Berkeley National Laboratory, supported by the US Department of Energy and the National Institutes of Health, is optimized for both small-angle X-ray scattering (SAXS) and macromolecular crystallography (MX), making it unique among the world's mostly SAXS or MX dedicated beamlines. Since SIBYLS was commissioned, assessments of the limitations and advantages of a combined SAXS and MX beamline have suggested new strategies for integration and optimal data collection methods and have led to additional hardware and software enhancements. Features described include a dual mode monochromator [containing both Si(111) crystals and Mo/B(4)C multilayer elements], rapid beamline optics conversion between SAXS and MX modes, active beam stabilization, sample-loading robotics, and mail-in and remote data collection. These features allow users to gain valuable insights from both dynamic solution scattering and high-resolution atomic diffraction experiments performed at a single synchrotron beamline. Key practical issues considered for data collection and analysis include radiation damage, structural ensembles, alternative conformers and flexibility. SIBYLS develops and applies efficient combined MX and SAXS methods that deliver high-impact results by providing robust cost-effective routes to connect structures to biology and by performing experiments that aid beamline designs for next generation light sources. PMID:23396808

  8. Implementation and performance of SIBYLS: a dual endstation small-angle X-ray scattering and macromolecular crystallography beamline at the Advanced Light Source

    PubMed Central

    Classen, Scott; Hura, Greg L.; Holton, James M.; Rambo, Robert P.; Rodic, Ivan; McGuire, Patrick J.; Dyer, Kevin; Hammel, Michal; Meigs, George; Frankel, Kenneth A.; Tainer, John A.

    2013-01-01

    The SIBYLS beamline (12.3.1) of the Advanced Light Source at Lawrence Berkeley National Laboratory, supported by the US Department of Energy and the National Institutes of Health, is optimized for both small-angle X-ray scattering (SAXS) and macromolecular crystallography (MX), making it unique among the world’s mostly SAXS or MX dedicated beamlines. Since SIBYLS was commissioned, assessments of the limitations and advantages of a combined SAXS and MX beamline have suggested new strategies for integration and optimal data collection methods and have led to additional hardware and software enhancements. Features described include a dual mode monochromator [containing both Si(111) crystals and Mo/B4C multilayer elements], rapid beamline optics conversion between SAXS and MX modes, active beam stabilization, sample-loading robotics, and mail-in and remote data collection. These features allow users to gain valuable insights from both dynamic solution scattering and high-resolution atomic diffraction experiments performed at a single synchrotron beamline. Key practical issues considered for data collection and analysis include radiation damage, structural ensembles, alternative conformers and flexibility. SIBYLS develops and applies efficient combined MX and SAXS methods that deliver high-impact results by providing robust cost-effective routes to connect structures to biology and by performing experiments that aid beamline designs for next generation light sources. PMID:23396808

  9. A Next-Generation Hard X-Ray Nanoprobe Beamline for In Situ Studies of Energy Materials and Devices

    NASA Astrophysics Data System (ADS)

    Maser, Jörg; Lai, Barry; Buonassisi, Tonio; Cai, Zhonghou; Chen, Si; Finney, Lydia; Gleber, Sophie-Charlotte; Jacobsen, Chris; Preissner, Curt; Roehrig, Chris; Rose, Volker; Shu, Deming; Vine, David; Vogt, Stefan

    2014-01-01

    The Advanced Photon Source is developing a suite of new X-ray beamlines to study materials and devices across many length scales and under real conditions. One of the flagship beamlines of the APS upgrade is the In Situ Nanoprobe (ISN) beamline, which will provide in situ and operando characterization of advanced energy materials and devices under varying temperatures, gas ambients, and applied fields, at previously unavailable spatial resolution and throughput. Examples of materials systems include inorganic and organic photovoltaic systems, advanced battery systems, fuel cell components, nanoelectronic devices, advanced building materials and other scientifically and technologically relevant systems. To characterize these systems at very high spatial resolution and trace sensitivity, the ISN will use both nanofocusing mirrors and diffractive optics to achieve spots sizes as small as 20 nm. Nanofocusing mirrors in Kirkpatrick-Baez geometry will provide several orders of magnitude increase in photon flux at a spatial resolution of 50 nm. Diffractive optics such as zone plates and/or multilayer Laue lenses will provide a highest spatial resolution of 20 nm. Coherent diffraction methods will be used to study even small specimen features with sub-10 nm relevant length scale. A high-throughput data acquisition system will be employed to significantly increase operations efficiency and usability of the instrument. The ISN will provide full spectroscopy capabilities to study the chemical state of most materials in the periodic table, and enable X-ray fluorescence tomography. In situ electrical characterization will enable operando studies of energy and electronic devices such as photovoltaic systems and batteries. We describe the optical concept for the ISN beamline, the technical design, and the approach for enabling a broad variety of in situ studies. We furthermore discuss the application of hard X-ray microscopy to study defects in multi-crystalline solar cells, one

  10. A Next-Generation Hard X-Ray Nanoprobe Beamline for In Situ Studies of Energy Materials and Devices

    SciTech Connect

    Maser, Jong; Lai, Barry; Buonassisi, Toni; Cai, Zhonghou; Chen, Si; Finney, Lydia; Gleber, Sophie-Charlotte; Jacobsen, Chris; Preissner, Curt; Chris Roehrig; Rose, Volker; Shu, Deming; Vine, David; Vogt, Stefan

    2013-08-20

    The Advanced Photon Source is developing a suite of new X-ray beamlines to study materials and devices across many length scales and under real conditions. One of the flagship beamlines of the APS upgrade is the In Situ Nanoprobe (ISN) beamline, which will provide in situ and operando characterization of advanced energy materials and devices under varying temperatures, gas ambients, and applied fields, at previously unavailable spatial resolution and throughput. Examples of materials systems include inorganic and organic photovoltaic systems, advanced battery systems, fuel cell components, nanoelectronic devices, advanced building materials and other scientifically and technologically relevant systems. To characterize these systems at very high spatial resolution and trace sensitivity, the ISN will use both nanofocusing mirrors and diffractive optics to achieve spots sizes as small as 20 nm. Nanofocusing mirrors in Kirkpatrick–Baez geometry will provide several orders of magnitude increase in photon flux at a spatial resolution of 50 nm. Diffractive optics such as zone plates and/or multilayer Laue lenses will provide a highest spatial resolution of 20 nm. Coherent diffraction methods will be used to study even small specimen features with sub-10 nm relevant length scale. A high-throughput data acquisition system will be employed to significantly increase operations efficiency and usability of the instrument. The ISN will provide full spectroscopy capabilities to study the chemical state of most materials in the periodic table, and enable X-ray fluorescence tomography. In situ electrical characterization will enable operando studies of energy and electronic devices such as photovoltaic systems and batteries. We also describe the optical concept for the ISN beamline, the technical design, and the approach for enabling a broad variety of in situ studies. Furthermore, we discuss the application of hard X-ray microscopy to study defects in multi-crystalline solar

  11. Redesign and Reconstruction of the Equipment Protection Systems for the Upgrading Front Ends and Beamlines at BSRF

    SciTech Connect

    Xiong Shenshou; Tan Yinglei; Wu Xuehui

    2007-01-19

    The BEPC(Beijing Electron-Positron Collider) is upgraded to be BEPCII, a two-ring Electron-Positron collider. Due to the construction of the BEPCII and upgrade of the existing front ends and beamlines, all the existing EPSs(Equipment Protection Systems) have to be redesigned and reconstructed at BSRF. All the redesigned EPSs for the upgrading front ends and beamlines are a PLC- and SCADA-based equipment protection and control and monitoring system. The EPSs are used to protect BEPCII two storage rings vacuum against vacuum failures in a beamline, as well as to protect the front-end and beamline components from being damaged by synchrotron radiation. For the high-power wiggler beam lines, a fast movable mask is used to protect the blade of a fast-closing valve from damage when the fast-closing valve is triggered to close, which does not need to dump the electron beam running in BEPCII outer ring. In addition, all redesigned PLC- based EPSs are used to communicate with the same centralized monitoring computer to monitor a variety of parameters from all PLC- based EPS systems. The monitoring computer runs the SCADA (Supervisory Control And Data Acquisition) software with its own web server. Graphical HMI interfaces are used to display a few overall views of all front-end equipment operation status and the further detailed information for each EPS in a different pop-up window. On the web services, the SCADA-based centralized monitoring system provides a web browse function, etc. The design of the reconstructed systems is described in this paper.

  12. The CG-1D neutron imaging beamline at the Oak Ridge National Laboratory High Flux Isotope Reactor

    SciTech Connect

    Santodonato, Louis J; Bilheux, Hassina Z; Bailey, William Barton; Bilheux, Jean-Christophe; Nguyen, Phong T; Tremsin, Anton S; Selby, Douglas L; Walker, Lakeisha MH

    2015-01-01

    The Oak Ridge National Laboratory Neutron Sciences Directorate has installed a neutron imaging beamline at the High Flux Isotope Reactor (HFIR) cold guide hall. CG-1D is one of the three instruments that make up the CG1 instrument suite. The beamline optics and detector have recently been upgraded to meet the needs of the neutron imaging community (better smoothing of guide system artifacts, higher flux or spatial resolution). These upgrades comprise a new diffuser/aperture system, two new detectors, a He-filled flight tube and silicon (Si) windows. Shielding inside the flight tube, beam scrapers and a beam stop ensure that biological dose is less than 50 Sv/hr outside of the radiation boundary. A set of diffusers and apertures (pinhole geometry) has been installed at the exit of the guide system to allow motorized L/D variation. Samples sit on a translation/rotation stage for alignment and tomography purposes. Detectors for the CG-1D beamline are (1) an ANDOR DW936 charge coupled device (CCD) camera with a field of view of approximately 7 cm x 7 cm and ~ 80 microns spatial resolution and 1 frame per second time resolution, (2) a new Micro-Channel Plate (MCP) detector with a 2.8 cm x 2.8 cm field of view and 55 microns spatial resolution, and 5 s timing capability. 6LiF/ZnS scintillators of thickness varying from 50 to 200 microns are being used at this facility. An overview of the beamline upgrade and preliminary data is presented here.

  13. New Developments at the ALS High-Pressure Beamline 12.2.2

    NASA Astrophysics Data System (ADS)

    Kunz, M.; MacDowell, A. A.; Yan, J.; Beavers, C. C. G.; Doran, A.; Williams, Q. C.

    2015-12-01

    ALS-beamline 12.2.2 celebrated its 10-year anniversary as a beamline collaboratively operated by the ALS and COMPRES. The anniversary coincided with a major rebuild and expansion of its capabilities for in-situ high-pressure and high-temperature X-ray diffraction. A rebuild of the 12.2.2 laser heating table was completed and commissioned in the past year. The new design relies on a vertically positioned small (~1m x 1m) breadboard that is placed perpendicularly to the incident X-ray beam next to the sample stage. Upstream and downstream viewing-, IR-laser and pyrometry-optics are mounted on opposite surfaces of the breadboard. On-line ruby fluorescence optics including a blue diode laser are also mounted on the upstream surface. The much reduced dimensions of the design lead to smaller mechanical lever arms and thus to a significant suppression of vibrations. This was confirmed in the commissioning phase with high-quality optical images (~ 2 μm resolution) as well as a very stable hotspot in DAC samples. A further optimized pyrometry code was cross-calibrated against thermal expansions of Pt and Ta, and was found to agree with those values within experimental uncertainties. Pyrometry relies on imaging the full hot-spot onto a spectrometer and combining the thus obtained average temperature with an intensity map collected at 700 nm to produce a temperature contour map of the entire sample chamber. Besides axial laser heating, double-sided radial laser heating is also being developed and commissioned. The X-ray source of 12.2.2 makes it an ideal station to focus on high-pressure single crystal diffraction. The present set-up operates parasitically with a single rotation axis on the in-situ laser heating powder diffraction sample stage in concert with a fast (15 fps) amorphous silicon/diode array detector. Although this set-up poses limitations with respect to accessible reciprocal space, high pressure single crystal structure solution and refinements of organic

  14. Guidelines for beamline and front-end radiation shielding design at the Advanced Photon Source.

    SciTech Connect

    Fernandez, P.; X-Ray Science Division

    2008-09-11

    Shielding for the APS will be such that the individual radiation worker dose will be as low as reasonably achievable (ALARA). The ALARA goals for the APS are to keep the total of the work-related radiation exposure (exposure coming from other than natural or medical sources) as far below 500 person-mrem per year, collective total effective dose equivalent, as reasonably achievable. For an individual APS radiation worker, the goal is to keep the maximum occupational total effective dose equivalent of any one employee as far below 200 mrem/yr as reasonably achievable. The ALARA goal for APS beamline scientists is to keep the total of the work-related radiation exposure (exposure coming from other than natural or medical sources) as far below 100 person-mrem per year, collective total effective dose equivalent, as reasonably achievable. For an individual APS beamline scientist, the goal is to keep the maximum occupational total effective dose equivalent of any one scientist as far below 50 mrem/yr as reasonably achievable. The dose is actively monitored by the radiation monitors on the storage ring wall in each sector and by the frequent area surveys performed by the health physics personnel. For cases in which surveys indicate elevated hourly dose rates that may impact worker exposure, additional local shielding is provided to reduce the radiation field to an acceptable level. Passive area monitors are used throughout the facility to integrate doses in various areas. The results are analyzed for trends of increased doses, and shielding in these areas is evaluated and improved, as appropriate. The APS policy for on-site nonradiation workers in the vicinity of the APS facilities requires that the average nonradiation worker dose be below 0.2 mSv/yr (20 mrem/yr). In addition, the dose at the site boundary from all pathways is required to be below 0.1 mSv/yr (10 mrem/yr). For future modifications of the facility, the doses shall be evaluated and additional shielding

  15. Beamlines of the biomedical imaging and therapy facility at the Canadian light source - part 3

    NASA Astrophysics Data System (ADS)

    Wysokinski, Tomasz W.; Chapman, Dean; Adams, Gregg; Renier, Michel; Suortti, Pekka; Thomlinson, William

    2015-03-01

    The BioMedical Imaging and Therapy (BMIT) facility provides synchrotron-specific imaging and radiation therapy capabilities [1-4]. We describe here the Insertion Device (ID) beamline 05ID-2 with the beam terminated in the SOE-1 (Secondary Optical Enclosure) experimental hutch. This endstation is designed for imaging and therapy research primarily in animals ranging in size from mice to humans to horses, as well as tissue specimens including plants. Core research programs include human and animal reproduction, cancer imaging and therapy, spinal cord injury and repair, cardiovascular and lung imaging and disease, bone and cartilage growth and deterioration, mammography, developmental biology, gene expression research as well as the introduction of new imaging methods. The source for the ID beamline is a multi-pole superconducting 4.3 T wiggler [5]. The high field gives a critical energy over 20 keV. The high critical energy presents shielding challenges and great care must be taken to assess shielding requirements [6-9]. The optics in the POE-1 and POE-3 hutches [4,10] prepare a monochromatic beam that is 22 cm wide in the last experimental hutch SOE-1. The double crystal bent-Laue or Bragg monochromator, or the single-crystal K-edge subtraction (KES) monochromator provide an energy range appropriate for imaging studies in animals (20-100+ keV). SOE-1 (excluding the basement structure 4 m below the experimental floor) is 6 m wide, 5 m tall and 10 m long with a removable back wall to accommodate installation and removal of the Large Animal Positioning System (LAPS) capable of positioning and manipulating animals as large as a horse [11]. This end-station also includes a unique detector positioner with a vertical travel range of 4.9 m which is required for the KES imaging angle range of +12.3° to -7.3°. The detector positioner also includes moveable shielding integrated with the safety shutters. An update on the status of the other two end-stations at BMIT, described

  16. In crystallo optical spectroscopy (icOS) as a complementary tool on the macromolecular crystallography beamlines of the ESRF

    SciTech Connect

    Stetten, David von; Giraud, Thierry; Carpentier, Philippe; Sever, Franc; Terrien, Maxime; Dobias, Fabien; Juers, Douglas H.; Flot, David; Mueller-Dieckmann, Christoph; Leonard, Gordon A.; Sanctis, Daniele de; Royant, Antoine

    2015-01-01

    The current version of the Cryobench in crystallo optical spectroscopy facility of the ESRF is presented. The diverse experiments that can be performed at the Cryobench are also reviewed. The analysis of structural data obtained by X-ray crystallography benefits from information obtained from complementary techniques, especially as applied to the crystals themselves. As a consequence, optical spectroscopies in structural biology have become instrumental in assessing the relevance and context of many crystallographic results. Since the year 2000, it has been possible to record such data adjacent to, or directly on, the Structural Biology Group beamlines of the ESRF. A core laboratory featuring various spectrometers, named the Cryobench, is now in its third version and houses portable devices that can be directly mounted on beamlines. This paper reports the current status of the Cryobench, which is now located on the MAD beamline ID29 and is thus called the ID29S-Cryobench (where S stands for ‘spectroscopy’). It also reviews the diverse experiments that can be performed at the Cryobench, highlighting the various scientific questions that can be addressed.

  17. Medical research and multidisciplinary applications with laser-accelerated beams: the ELIMED netwotk at ELI-Beamlines

    NASA Astrophysics Data System (ADS)

    Tramontana, A.; Anzalone, A.; Candiano, G.; Carpinelli, M.; Cirrone, G. A. P.; Cuttone, G.; Korn, G.; Licciardello, T.; Maggiore, M.; Manti, L.; Margarone, D.; Musumarra, A.; Perozziello, F.; Pisciotta, P.; Raffaele, L.; Romano, F.; Romano, F. P.; Stancampiano, C.; Schillaci, F.; Scuderi, V.; Torrisi, L.; Tudisco, S.

    2014-04-01

    Laser accelerated proton beams represent nowadays an attractive alternative to the conventional ones and they have been proposed in different research fields. In particular, the interest has been focused in the possibility of replacing conventional accelerating machines with laser-based accelerators in order to develop a new concept of hadrontherapy facilities, which could result more compact and less expensive. With this background the ELIMED (ELIMED: ELI-Beamlines MEDical applications) research project has been launched by LNS-INFN researchers (Laboratori Nazionali del Sud-Istituto Nazionale di Fisica Nucleare, Catania, IT) and ASCR-FZU researchers (Academy of Sciences of the Czech Republic-Fyzikální ústar, Prague, Cz), within the pan-European ELI-Beamlines facility framework. Its main purposes are the demonstration of future applications in hadrontherapy of optically accelerated protons and the realization of a laser-accelerated ion transport beamline for multidisciplinary applications. Several challenges, starting from laser-target interaction and beam transport development, up to dosimetric and radiobiological issues, need to be overcome in order to reach the final goals. The design and the realization of a preliminary beam handling and dosimetric system and of an advanced spectrometer for high energy (multi-MeV) laser-accelerated ion beams will be shortly presented in this work.

  18. Long-Working-Distance Kirkpatrick-Baez Mirrors for Hard X-ray Beamlines at SPring-8

    SciTech Connect

    Yumoto, H.; Koyama, T.

    2011-09-09

    We designed and installed two types of long-working-distance Kirkpatrick-Baez (KB) mirrors and mirror manipulators, which were customized into each experiment for hard x-ray undulator beamlines at SPring-8. For the BL32XU RIKEN Targeted Proteins beamline, 400-mm-long KB focusing mirrors for a beam size of 1 {mu}m with a 730-mm-long working distance were designed for carrying out the structural analysis of protein microcrystals. We realized a focusing beam size of 0.9x0.9 {mu}m{sup 2}(FWHM) and a focusing intensity of 6x10{sup 10} (photons/s) at an x-ray energy of 12.4 keV. For the BL19LXU RIKEN SR Physics beamline, we developed KB mirrors for 100-nm focusing with a 100-mm-working distance for the purpose of nano-focus x-ray diffraction. A focusing beam size of 100x100 nm{sup 2}(FWHM) and a high focusing intensity of 3.7x10{sup 10} (photons/s) at an x-ray energy of 12.4 keV were realized.

  19. TEMPO: a New Insertion Device Beamline at SOLEIL for Time Resolved Photoelectron Spectroscopy Experiments on Solids and Interfaces

    SciTech Connect

    Polack, F.; Silly, M.; Chauvet, C.; Lagarde, B.; Bergeard, N.; Izquierdo, M.; Chubar, O.; Krizmancic, D.; Ribbens, M.; Duval, J.-P.; Basset, C.; Kubsky, S.; Sirotti, F.

    2010-06-23

    A new insertion device beamline is now operational on straight section 8 at the SOLEIL synchrotron radiation source in France. The beamline and the experimental station were developed to optimize the study of the dynamics of electronic and magnetic properties of materials. Here we present the main technical characteristics of the installation and the general principles behind them. The source is composed of two APPLE II type insertion devices. The monochromator with plane gratings and spherical mirrors is working in the energy range 40-1500 eV. It is equipped with VLS, VGD gratings to allow the user optimization of flux or higher harmonics rejection. The observed resonance structures measured in gas phase enable us to determine the available energy resolution: a resolving power higher than 10000 is obtained at the Ar 2p, N 1s and Ne K-edges when using all the optical elements at full aperture. The total flux as a function of the measured photon energy and the characterization of the focal spot size complete the beamline characterization.

  20. Long-Working-Distance Kirkpatrick-Baez Mirrors for Hard X-ray Beamlines at SPring-8

    NASA Astrophysics Data System (ADS)

    Yumoto, H.; Koyama, T.; Hirata, K.; Kawano, Y.; Ueno, G.; Nisawa, A.; Hikima, T.; Takeshita, S.; Ohsumi, H.; Ito, K.; Tanaka, Y.; Arima, T.; Ohashi, H.; Yamamoto, M.; Goto, S.

    2011-09-01

    We designed and installed two types of long-working-distance Kirkpatrick-Baez (KB) mirrors and mirror manipulators, which were customized into each experiment for hard x-ray undulator beamlines at SPring-8. For the BL32XU RIKEN Targeted Proteins beamline, 400-mm-long KB focusing mirrors for a beam size of 1 μm with a 730-mm-long working distance were designed for carrying out the structural analysis of protein microcrystals. We realized a focusing beam size of 0.9×0.9 μm2 (FWHM) and a focusing intensity of 6×1010 (photons/s) at an x-ray energy of 12.4 keV. For the BL19LXU RIKEN SR Physics beamline, we developed KB mirrors for 100-nm focusing with a 100-mm-working distance for the purpose of nano-focus x-ray diffraction. A focusing beam size of 100×100 nm2 (FWHM) and a high focusing intensity of 3.7×1010 (photons/s) at an x-ray energy of 12.4 keV were realized.

  1. Performance of the Compact Visual Beam Imaging System on the GM/CA BM Beamline at the APS

    NASA Astrophysics Data System (ADS)

    Xu, S.; Ogata, C. M.; Makarov, O.; Corcoran, S.; Ferguson, D.; Fischetti, R. F.

    2013-03-01

    A typical problem encountered on a beamline with a sagittal focusing monochromator is the difficulty of optimizing the crystal alignment because the full width of the monochromatic, unfocused beam cannot be visualized. This problem is particularly acute on beamlines that accept a wide swath of radiation combined with a fixed experimental setup consisting of constrained apertures that only allow the focused beam to pass through to the sample position. To address this problem, an imaging system has been designed and implemented on the GM/CA bending magnet beamline at the Advanced Photon Source, Argonne National Laboratory. This imaging system consists of a 30mm × 50mm flat YAG crystal, right angle prism/mirror and video camera located downstream of the vertical collimating mirror, sagittally focusing monochromator and vertical focusing mirror. The YAG crystal was installed in a 6-way vacuum cross in the beam path, and was mounted on a linear translation feedthrough allowing remote controlled insertion and removal of the crystal from the beam path. The CCD camera was mounted outside the vacuum chamber and views the x-ray induced scintillation from the YAG crystal through a window. This visualizer allows one to optimize the twist, yaw and roll of the second crystal, facilitates proper sagittal focusing and serves as a remote controlled diagnostic tool. An overview of the design and the performance of the imaging system will be presented.

  2. Single-Crystal Raman Spectroscopy and X-ray Crystallography at Beamline X26-C of the NSLS

    SciTech Connect

    D Stoner-Ma; J Skinner; D Schneider; M Cowan; R Sweet; A Orville

    2011-12-31

    Three-dimensional structures derived from X-ray diffraction of protein crystals provide a wealth of information. Features and interactions important for the function of macromolecules can be deduced and catalytic mechanisms postulated. Still, many questions can remain, for example regarding metal oxidation states and the interpretation of 'mystery density', i.e. ambiguous or unknown features within the electron density maps, especially at {approx}2 {angstrom} resolutions typical of most macromolecular structures. Beamline X26-C at the National Synchrotron Light Source (NSLS), Brookhaven National Laboratory (BNL), provides researchers with the opportunity to not only determine the atomic structure of their samples but also to explore the electronic and vibrational characteristics of the sample before, during and after X-ray diffraction data collection. When samples are maintained under cryo-conditions, an opportunity to promote and follow photochemical reactions in situ as a function of X-ray exposure is also provided. Plans are in place to further expand the capabilities at beamline X26-C and to develop beamlines at NSLS-II, currently under construction at BNL, which will provide users access to a wide array of complementary spectroscopic methods in addition to high-quality X-ray diffraction data.

  3. ID16B: a hard X-ray nanoprobe beamline at the ESRF for nano-analysis.

    PubMed

    Martínez-Criado, Gema; Villanova, Julie; Tucoulou, Rémi; Salomon, Damien; Suuronen, Jussi-Petteri; Labouré, Sylvain; Guilloud, Cyril; Valls, Valentin; Barrett, Raymond; Gagliardini, Eric; Dabin, Yves; Baker, Robert; Bohic, Sylvain; Cohen, Cédric; Morse, John

    2016-01-01

    Within the framework of the ESRF Phase I Upgrade Programme, a new state-of-the-art synchrotron beamline ID16B has been recently developed for hard X-ray nano-analysis. The construction of ID16B was driven by research areas with major scientific and societal impact such as nanotechnology, earth and environmental sciences, and bio-medical research. Based on a canted undulator source, this long beamline provides hard X-ray nanobeams optimized mainly for spectroscopic applications, including the combination of X-ray fluorescence, X-ray diffraction, X-ray excited optical luminescence, X-ray absorption spectroscopy and 2D/3D X-ray imaging techniques. Its end-station re-uses part of the apparatus of the earlier ID22 beamline, while improving and enlarging the spectroscopic capabilities: for example, the experimental arrangement offers improved lateral spatial resolution (∼50 nm), a larger and more flexible capability for in situ experiments, and monochromatic nanobeams tunable over a wider energy range which now includes the hard X-ray regime (5-70 keV). This paper describes the characteristics of this new facility, short-term technical developments and the first scientific results. PMID:26698084

  4. A Beamline for High-Pressure Studies at the Advanced Light Sourcewith a Superconducting Bending Magnet as the Source

    SciTech Connect

    Kunz, Martin; MacDowell, Alastair A.; Caldwell, Wendel A.; Cambie, Daniella; Celestre, Richard S.; Domning, Edward E.; Duarte,Robert M.; Gleason, Arianna E.; Glossinger, James M.; Kelez, Nicholas; Plate, David W.; Yu, Tony; Zaug, Joeseph M.; Padmore, Howard A.; Jeanloz,Raymond; Alivisatos, A. Paul; Clark, Simon M.

    2005-06-30

    A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on Beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 Tesla superconducting bending magnet (superbend). Useful x-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness preserving optics of the beamline. These optics are comprised of: a plane parabola collimating mirror (M1), followed by a Kohzu monochromator vessel with a Si(111) crystals (E/DE {approx}7000) and a W/B4C multilayers (E/DE {approx} 100), and then a toroidal focusing mirror (M2) with variable focusing distance. The experimental enclosure contains an automated beam positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detectors (CCD or image-plate detector). Future developments aim at the installation of a second end station dedicated for in situ laser-heating on one hand and a dedicated high-pressure single-crystal station, applying both monochromatic as well as polychromatic techniques.

  5. A BEAMLINE FOR HIGH PRESSURE STUDIES AT THE ADVANCED LIGHT SOURCE WITH A SUPERCONDUCTING BENDING MAGNET AS THE SOURCE

    SciTech Connect

    Kunz, M; MacDowell, A A; Caldwell, W A; Cambie, D; Celestre, R S; Domning, E E; Duarte, R M; Gleason, A; Glossinger, J; Kelez, N; Plate, D W; Yu, T; Zaug, J M; Padmore, H A; Jeanloz, R; Alivisatos, A P; Clark, S M

    2005-04-19

    A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on Beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 Tesla superconducting bending magnet (superbend). Useful x-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness preserving optics of the beamline. These optics are comprised of: a plane parabola collimating mirror (M1), followed by a Kohzu monochromator vessel with a Si(111) crystals (E/{Delta}E {approx} 7000) and a W/B{sub 4}C multilayer (E/{Delta}E {approx} 100), and then a toroidal focusing mirror (M2) with variable focusing distance. The experimental enclosure contains an automated beam positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detectors (CCD or image-plate detector). Future developments aim at the installation of a second end station dedicated for in situ laser-heating on one hand and a dedicated high-pressure single-crystal station, applying both monochromatic as well as polychromatic techniques.

  6. SAMRAI: A novel variably polarized angle-resolved photoemission beamline in the VUV region at UVSOR-II

    SciTech Connect

    Kimura, Shin-Ichi; Ito, Takahiro; Hosaka, Masahito; Katoh, Masahiro; Sakai, Masahiro; Nakamura, Eiken; Kondo, Naonori; Horigome, Toshio; Hayashi, Kenji; Goto, Tomohiro; Ejima, Takeo; Soda, Kazuo

    2010-05-15

    A novel variably polarized angle-resolved photoemission spectroscopy beamline in the vacuum-ultraviolet (VUV) region has been installed at the UVSOR-II 750 MeV synchrotron light source. The beamline is equipped with a 3 m long APPLE-II type undulator with horizontally/vertically linear and right/left circular polarizations, a 10 m Wadsworth type monochromator covering a photon energy range of 6-43 eV, and a 200 mm radius hemispherical photoelectron analyzer with an electron lens of a {+-}18 deg. acceptance angle. Due to the low emittance of the UVSOR-II storage ring, the light source is regarded as an entrance slit, and the undulator light is directly led to a grating by two plane mirrors in the monochromator while maintaining a balance between high-energy resolution and high photon flux. The energy resolving power (h{nu}/{Delta}h{nu}) and photon flux of the monochromator are typically 1x10{sup 4} and 10{sup 12} photons/s, respectively, with a 100 {mu}m exit slit. The beamline is used for angle-resolved photoemission spectroscopy with an energy resolution of a few meV covering the UV-to-VUV energy range.

  7. JBluIce-EPICS: a fast and flexible open-source beamline control system for macromolecular crystallography

    NASA Astrophysics Data System (ADS)

    Stepanov, S.; Hilgart, M.; Makarov, O.; Pothineni, S. B.; Yoder, D.; Ogata, C.; Sanishvili, R.; Venugopalan, N.; Becker, M.; Clift, M.; Smith, J. L.; Fischetti, R. F.

    2013-03-01

    This paper overviews recent advances in the JBluIce-EPICS open-source control system designed at the macromolecular crystallography beamlines of the National Institute of General Medical Sciences and National Cancer Institute at the Advanced Photon Source (GM/CA@APS). We discuss some technical highlights of this system distinguishing it from the competition, such as reduction of software layers to only two, possibility to operate JBluIce in parallel with other beamline controls, plugin-enabled architecture where the plugins can be written in any programming language, and utilization of the whole power of the Java integrated development environment in the Graphical User Interface. Then, we demonstrate how these highlights help to make JBluIce fast, easily adaptable to new beamline developments, and intuitive for users. In particular, we discuss several recent additions to the system including a bridge between crystal rastering and data collection, automatic detection of raster polygons from optical crystal centering, background data processing, and a pathway to a fully automated pipeline from crystal screening to solving crystal structure.

  8. Plutonium (III) and uranium (III) nitrile complexes

    SciTech Connect

    Enriquez, A. E.; Matonic, J. H.; Scott, B. L.; Neu, M. P.

    2002-01-01

    Iodine oxidation of uranium and plutonium metals in tetrahydrofuran and pyridine form AnI{sub 3}(THF){sub 4} and AnI{sub 3}(py){sub 4} (An = Pu, U). These compounds represent convenient entries Into solution An(III) chemistry in organic solvents. Extensions of the actinide metal oxidation methodology in nitrile solvents by I{sub 2}, AgPF{sub 6}, and TIPF{sub 6} are presented here. Treatment of Pu{sup 0} in acetonitrile with iodine yields a putative PuI{sub 3}(NCMe){sub x} intermediate which can be trapped with the tripodal nitrogen donor ligand tpza (tpza = (tris[(2-pyrazinyl)methyl]amine)) and forms the eight-coordinate complex (tpza)PuI{sub 3}(NCMe). Treatment of excess U{sup 0} metal by iodine in acetonitrile afforded a brown crystalline mixed valence complex, [U(NCMe){sub 9}][UI{sub 6}][I], instead of UI{sub 3}(NCMe){sub 4}. The analogous reaction in bezonitrile forms red crystalline UI{sub 4}(NCPh){sub 4}. In contrast, treatment of UI{sub 3}(THF){sub 4} with excess acetonitrile cleanly generates [U(NCMe){sub 9}][I]{sub 3}. Oxidation of Pu{sup 0} by either TI(I) or Ag(I) hexafluorophosphate salts generates a nine-coordinate homoleptic acetonitrile adduct [Pu(NCMe){sub 9}][PF{sub 6}]{sub 3}. Attempts to oxidize U{sub 0} with these salts were unsuccessful.

  9. Cranial mononeuropathy III - diabetic type

    MedlinePlus

    ... gov/ency/article/000692.htm Cranial mononeuropathy III - diabetic type To use the sharing features on this page, please enable JavaScript. Cranial mononeuropathy III -- diabetic type -- is usually a complication of diabetes that causes ...

  10. I12: the Joint Engineering, Environment and Processing (JEEP) beamline at Diamond Light Source.

    PubMed

    Drakopoulos, Michael; Connolley, Thomas; Reinhard, Christina; Atwood, Robert; Magdysyuk, Oxana; Vo, Nghia; Hart, Michael; Connor, Leigh; Humphreys, Bob; Howell, George; Davies, Steve; Hill, Tim; Wilkin, Guy; Pedersen, Ulrik; Foster, Andrew; De Maio, Nicoletta; Basham, Mark; Yuan, Fajin; Wanelik, Kaz

    2015-05-01

    I12 is the Joint Engineering, Environmental and Processing (JEEP) beamline, constructed during Phase II of the Diamond Light Source. I12 is located on a short (5 m) straight section of the Diamond storage ring and uses a 4.2 T superconducting wiggler to provide polychromatic and monochromatic X-rays in the energy range 50-150 keV. The beam energy enables good penetration through large or dense samples, combined with a large beam size (1 mrad horizontally × 0.3 mrad vertically). The beam characteristics permit the study of materials and processes inside environmental chambers without unacceptable attenuation of the beam and without the need to use sample sizes which are atypically small for the process under study. X-ray techniques available to users are radiography, tomography, energy-dispersive diffraction, monochromatic and white-beam two-dimensional diffraction/scattering and small-angle X-ray scattering. Since commencing operations in November 2009, I12 has established a broad user community in materials science and processing, chemical processing, biomedical engineering, civil engineering, environmental science, palaeontology and physics.

  11. Versatile attosecond beamline in a two-foci configuration for simultaneous time-resolved measurements

    SciTech Connect

    Locher, R.; Lucchini, M. Herrmann, J.; Sabbar, M.; Weger, M.; Ludwig, A.; Gallmann, L.; Keller, U.; Castiglioni, L.; Greif, M.; Hengsberger, M.

    2014-01-15

    We present our attoline which is a versatile attosecond beamline at the Ultrafast Laser Physics Group at ETH Zurich for attosecond spectroscopy in a variety of targets. High-harmonic generation (HHG) in noble gases with an infrared (IR) driving field is employed to generate pulses in the extreme ultraviolet (XUV) spectral regime for XUV-IR cross-correlation measurements. The IR pulse driving the HHG and the pulse involved in the measurements are used in a non-collinear set-up that gives independent access to the different beams. Single attosecond pulses are generated with the polarization gating technique and temporally characterized with attosecond streaking. This attoline contains two target chambers that can be operated simultaneously. A toroidal mirror relay-images the focus from the first chamber into the second one. In the first interaction region a dedicated double-target allows for a simple change between photoelectron/photoion measurements with a time-of-flight spectrometer and transient absorption experiments. Any end station can occupy the second interaction chamber. A surface analysis chamber containing a hemispherical electron analyzer was employed to demonstrate successful operation. Simultaneous RABBITT measurements in two argon jets were recorded for this purpose.

  12. Current status of the CXI beamline at the PAL-XFEL

    NASA Astrophysics Data System (ADS)

    Park, Jaehyun; Kim, Sangsoo; Nam, Ki-Hyun; Kim, Bongsoo; Ko, In Soo

    2016-09-01

    The Pohang Accelerator Laboratory's X-ray free electron laser (PAL-XFEL) is a research facility currently under construction. It will provide ultra-bright (1 × 1012 photons/pulse at 12.4 keV) and ultra-short (10 - 60 femtosecond) X-ray pulses. The CXI (coherent X-ray imaging) hard X-ray experimental station is designed to deliver brilliant hard X-rays (2 - 20.4 keV) and to measure diffraction signals with a forward scattering geometry. It will not only offer imaging studies of biological, chemical and physical samples with the "diffraction-before-destruction" scheme, but also be helpful in high-field hard X-ray physics and material science. The scientific programs are currently aimed at serial femtosecond crystallography (SFX) and coherent diffraction imaging (CDI) for bio specimens, nano materials, etc. In this paper, we describe the beamline layout, beam diagnostics, X-ray focusing optics, sample environments and detector system at the CXI experimental hutch.

  13. Direct detection of antiprotons with the Timepix3 in a new electrostatic selection beamline

    NASA Astrophysics Data System (ADS)

    Pacifico, N.; Aghion, S.; Alozy, J.; Amsler, C.; Ariga, A.; Ariga, T.; Bonomi, G.; Bräunig, P.; Bremer, J.; Brusa, R. S.; Cabaret, L.; Caccia, M.; Campbell, M.; Caravita, R.; Castelli, F.; Cerchiari, G.; Chlouba, K.; Cialdi, S.; Comparat, D.; Consolati, G.; Demetrio, A.; Di Noto, L.; Doser, M.; Dudarev, A.; Ereditato, A.; Evans, C.; Ferragut, R.; Fesel, J.; Fontana, A.; Gerber, S.; Giammarchi, M.; Gligorova, A.; Guatieri, F.; Haider, S.; Holmestad, H.; Huse, T.; Jordan, E.; Kellerbauer, A.; Kimura, M.; Krasnický, D.; Lagomarsino, V.; Lansonneur, P.; Lawler, G.; Lebrun, P.; Llopart, X.; Malbrunot, C.; Mariazzi, S.; Marx, L.; Matveev, V.; Mazzotta, Z.; Nebbia, G.; Nedelec, P.; Oberthaler, M.; Pagano, D.; Penasa, L.; Petracek, V.; Pistillo, C.; Prelz, F.; Prevedelli, M.; Ravelli, L.; Resch, L.; Røhne, O. M.; Rotondi, A.; Sacerdoti, M.; Sandaker, H.; Santoro, R.; Scampoli, P.; Smestad, L.; Sorrentino, F.; Spacek, M.; Storey, J.; Strojek, I. M.; Testera, G.; Tietje, I.; Tlustos, L.; Widmann, E.; Yzombard, P.; Zavatarelli, S.; Zmeskal, J.; Zurlo, N.

    2016-09-01

    We present here the first results obtained employing the Timepix3 for the detection and tagging of annihilations of low energy antiprotons. The Timepix3 is a recently developed hybrid pixel detector with advanced Time-of-Arrival and Time-over-Threshold capabilities and has the potential of allowing precise kinetic energy measurements of low energy charged particles from their time of flight. The tagging of the characteristic antiproton annihilation signature, already studied by our group, is enabled by the high spatial and energy resolution of this detector. In this study we have used a new, dedicated, energy selection beamline (GRACE). The line is symbiotic to the AEgIS experiment at the CERN Antiproton Decelerator and is dedicated to detector tests and possibly antiproton physics experiments. We show how the high resolution of the Timepix3 on the Time-of-Arrival and Time-over-Threshold information allows for a precise 3D reconstruction of the annihilation prongs. The presented results point at the potential use of the Timepix3 in antimatter-research experiments where a precise and unambiguous tagging of antiproton annihilations is required.

  14. BEER - The Beamline for European Materials Engineering Research at the ESS

    NASA Astrophysics Data System (ADS)

    Fenske, J.; Rouijaa, M.; Šaroun, J.; Kampmann, R.; Staron, P.; Nowak, G.; Pilch, J.; Beran, P.; Šittner, P.; Strunz, P.; Brokmeier, H.-G.; Ryukhtin, V.; Kadeřávek, L.; Strobl, M.; Müller, M.; Lukáš, P.; Schreyer, A.

    2016-09-01

    The Beamline for European Materials Engineering Research (BEER) will be built at the European Spallation Source (ESS). The diffractometer utilizes the high brilliance of the long-pulse neutron source and offers high instrument flexibility. It includes a novel chopper technique that extracts several short pulses out of the long pulse, leading to substantial intensity gain of up to an order of magnitude compared to pulse shaping methods for materials with high crystal symmetry. This intensity gain is achieved without compromising resolution. Materials of lower crystal symmetry or multi-phase materials will be investigated by additional pulse shaping methods. The different chopper set-ups and advanced beam extracting techniques offer an extremely broad intensity/resolution range. Furthermore, BEER offers an option of simultaneous SANS or imaging measurements without compromising diffraction investigations. This flexibility opens up new possibilities for in-situ experiments studying materials processing and performance under operation conditions. To fulfil this task, advanced sample environments, dedicated to thermo-mechanical processing, are foreseen.

  15. DESIGN AND PERFORMANCE OF THE MATCHING BEAMLINE BETWEEN THE BNL EBIS AND AN RFQ.

    SciTech Connect

    ALESSI,J.; BEEBE, E.; BRODOWSKI, J.; KPONOU, A.; OKAMURA, M.; PIKIN, A.; RAPARIA, D.; RITTER, J.; SNYDSTRUP, L. ZAJIC, V.

    2007-06-25

    A part of a new EBIS-based heavy ion preinjector, the low energy beam transport (LEBT) section between the high current EBIS and the RFQ is a challenging design, because it must serve many functions. In addition to the requirement to provide an efficient matching between the EBIS and the RFQ, this line must serve as a fast ''switchyard'', allowing singly charged ions from external sources to be transported into the EBIS trap region, and extracted, highly charged ions to be deflected to off-axis diagnostics (time-of-flight or emittance). The space charge of the 5-10 mA extracted heavy ion beam is a major consideration in the design, and the space charge force varies for different ion beams having Q/m from 1-0.16. The line includes electrostatic lenses, spherical and parallel-plate deflectors, magnetic solenoid, and diagnostics for measuring current, charge state distributions, emittance, and profile. A prototype of this beamline has been built, and results of tests are presented.

  16. Development of a monochromator system for the APS X-ray BESSRC beamlines

    SciTech Connect

    Beno, M.A.; Knapp, G.S.; Ramanathan, M.

    1997-03-01

    The authors have designed a double crystal, fixed exit monochromator which allows windowless operation of the APS beamlines. The crystals are mounted on a turntable with the first crystal at the center of rotation. A mechanical linkage is used to correctly position the second crystal and maintain a constant offset. The monochromator is designed with two adjacent vacuum chambers, one containing the drive mechanism, a vacuum compatible Huber goniometer, and another chamber containing a turntable on which the monochromator linkage and crystals are mounted. The small annular opening around a hollow stainless steel shaft which connects the Huber goniometer to the turntable is the only passage between the two adjacent chambers. The design of the monochromator is such that it can accommodate water, liquid nitrogen or galium cooling for the crystal optics. The basic design for the monochromator linkage mechanism is presented along with details of the monochromator chamber. The results of initial optical tests of the monochromator system using tilt sensors and a precision autocollimator will also be given.

  17. The Clinical Trials Program at the ESRF Biomedical Beamline ID17: Status and Remaining Steps

    SciTech Connect

    Requardt, H.; Bravin, A.; Prezado, Y.; Braeuer-Krisch, E.; Renier, M.; Brochard, Th.; Berkvens, P.; Nemoz, C.; Berruyer, G.; Esteve, F.; Elleaume, H.; Adam, J.-F.; Blattmann, H.; Laissue, J. A.; Kaser-Hotz, B.

    2010-06-23

    For several years the ID17 Biomedical beamline at the ESRF has developed synchrotron radiation therapy preclinical programmes to treat aggressive brain tumours. Two techniques have been developed at the ESRF:a) The Microbeam Radiation Therapy (MRT) using spatially fractionated 'white beam' (energies 50-300 keV) irradiation (beam widths 25-100 {mu}m, spacing between beams 200-400 {mu}m ) with extremely high dose rates (up to about 20 kGy/s) and depositing very high doses (300-1000 Gy) in the targeted tissue.b) The Stereotactic Synchrotron Radiation Therapy (SSRT) using spatially homogeneous monochromatic beam with the energy closely above that of the K-edge of a contrast- or chemotherapeutical agent (iodine, gadolinium, platinum) loaded into the tumour volume for obtaining a dose-enhancement. In 2005 an International review panel of oncology experts has recommended to move to clinical trials on humans in SSRT and on large animals in MRT. The works required for this program were launched in autumn 2007 with constructing a new, dedicated experimental hutch for MRT and a major upgrade of the existing sample-positioning station to a patient-positioning station for SSRT. In parallel, safety systems are developed and progressively implemented and a patient treatment-planning system developed.

  18. Simulating wavefront correction via deformable mirrors at x-ray beamlines

    NASA Astrophysics Data System (ADS)

    Pardini, Tommaso; Poyneer, Lisa A.; Plinta, Audrey; Cavaco, Jeffrey L.; Pivovaroff, Michael J.

    2012-10-01

    Deformable mirrors (DMs) have been successfully used in astronomical adaptive optics at visible and near-infrared wavelengths, greatly reducing atmospheric-induced aberrations. Building upon the extensive techniques and methods developed for these applications, we propose to extend this capability to the soft and hard x-ray regime in order to take full advantage of the beam quality characteristic of new facilities such as the National Synchrotron Light Source (NSLS-II), and the Linac Coherent Light Source (LCLS). Achieving this goal challenges both current mirror manufacturing techniques and wavefront propagation modeling. Lawrence Livermore National Laboratory (LLNL), in collaboration with Northrop Grumman AOA Xinetics Inc., is currently developing an x-ray deformable mirror to correct for wave-front aberrations introduced along the beam path of a typical x-ray beamline. To model the expected performance of such a mirror, we have developed a simulation based on the wavefront propagation code PROPER. We will present the current implementation of the software, which models actuation of a deformable mirror and evaluates its effect on wavefront correction.

  19. I12: the Joint Engineering, Environment and Processing (JEEP) beamline at Diamond Light Source

    PubMed Central

    Drakopoulos, Michael; Connolley, Thomas; Reinhard, Christina; Atwood, Robert; Magdysyuk, Oxana; Vo, Nghia; Hart, Michael; Connor, Leigh; Humphreys, Bob; Howell, George; Davies, Steve; Hill, Tim; Wilkin, Guy; Pedersen, Ulrik; Foster, Andrew; De Maio, Nicoletta; Basham, Mark; Yuan, Fajin; Wanelik, Kaz

    2015-01-01

    I12 is the Joint Engineering, Environmental and Processing (JEEP) beamline, constructed during Phase II of the Diamond Light Source. I12 is located on a short (5 m) straight section of the Diamond storage ring and uses a 4.2 T superconducting wiggler to provide polychromatic and monochromatic X-rays in the energy range 50–150 keV. The beam energy enables good penetration through large or dense samples, combined with a large beam size (1 mrad horizontally × 0.3 mrad vertically). The beam characteristics permit the study of materials and processes inside environmental chambers without unacceptable attenuation of the beam and without the need to use sample sizes which are atypically small for the process under study. X-ray techniques available to users are radiography, tomography, energy-dispersive diffraction, monochromatic and white-beam two-dimensional diffraction/scattering and small-angle X-ray scattering. Since commencing operations in November 2009, I12 has established a broad user community in materials science and processing, chemical processing, biomedical engineering, civil engineering, environmental science, palaeontology and physics. PMID:25931103

  20. Type III Hyperlipoproteinaemia

    PubMed Central

    Borrie, Peter

    1969-01-01

    Eighteen patients with type III hyperlipoproteinaemia, diagnosed on the basis of skin lesions, serum lipids, and lipoprotein electrophoresis, have been fully investigated over a period of 15 years. The incidence of coronary artery disease was only slightly increased, and was not increased at all among first-degree relatives. Peripheral occlusive arterial disease was probably more common. An increased incidence of carbohydrate intolerance was found in neither the patients nor their relatives. The effects of treatment on the skin were uniformly good. ImagesFig. 1Fig. 2 PMID:5783124

  1. POPULATION III HYPERNOVAE

    SciTech Connect

    Smidt, Joseph; Whalen, Daniel J.; Wiggins, Brandon K.; Even, Wesley; Fryer, Chris L.; Johnson, Jarrett L.

    2014-12-20

    Population III supernovae have been of growing interest of late for their potential to directly probe the properties of the first stars, particularly the most energetic events that are visible near the edge of the observable universe. Until now, hypernovae, the unusually energetic Type Ib/c supernovae that are sometimes associated with gamma-ray bursts, have been overlooked as cosmic beacons at the highest redshifts. In this, the latest of a series of studies on Population III supernovae, we present numerical simulations of 25-50 M {sub ☉} hypernovae and their light curves done with the Los Alamos RAGE and SPECTRUM codes. We find that they will be visible at z = 10-15 to the James Webb Space Telescope and z = 4-5 to the Wide-Field Infrared Survey Telescope, tracing star formation rates in the first galaxies and at the end of cosmological reionization. If, however, the hypernova crashes into a dense shell ejected by its progenitor, it is expected that a superluminous event will occur that may be seen at z ∼ 20 in the first generation of stars.

  2. Jet-Cooled Spectroscopy on the Ailes Infrared Beamline of the Synchrotron Radiation Facility Soleil

    NASA Astrophysics Data System (ADS)

    Georges, Robert

    2015-06-01

    The Advanced Infrared Line Exploited for Spectroscopy (AILES) extracts the bright far infrared (FIR) synchrotron continuum of the third generation radiation facility SOLEIL. This beamline is equipped with a high resolution (10-3 cm-1) Bruker IFS125 Fourier transform spectrometer which can be operated in the FIR but also in the mid and near infrared by using its internal conventional sources. The jet-AILES consortium (IPR, PhLAM, MONARIS, SOLEIL) has implemented a supersonic-jet apparatus on the beamline to record absorption spectra at very low temperature (5-50 K) and in highly supersaturated gaseous conditions. Heatable slit-nozzles of various lengths and widths are used to set properly the stagnation conditions. A mechanical pumping (roots pumps) was preferred for its ability to evacuate important mass flow rates and therefore to boost the experimental sensitivity of the set-up, the counterpart being a non-negligible consumption of both carrier (argon, helium or nitrogen) and spectroscopic gases. Various molecular systems were investigated up to now using the Jet-AILES apparatus. The very low temperature achieved in the gas expansion was either used to simplify the rotation-vibration structure of monomers, such as SF6, CF4 or naphthalene, or to stabilize the formation of weakly bonded molecular complexes such as the trimer of HF or the dimer of acetic acid. The nucleation of water vapor and the nuclear spin conversion of water were also investigated under free-jet conditions in the mid infrared. High-resolution spectroscopy and analysis of the νb{2} + νb{3} combination band of SF6 in a supersonic jet expansion. V. Boudon, P. Asselin, P. Soulard, M. Goubet, T. R. Huet, R. Georges, O. Pirali, P. Roy, Mol. Phys. 111, 2154-2162 (2013) The far infrared spectrum of naphthalene characterized by high resolution synchrotron FTIR spectroscopy and anharmonic DFT calculations. O. Pirali, M. Goubet, T.R. Huet, R. Georges, P. Soulard, P. Asselin, J. Courbe, P. Roy and M

  3. Performances and first experimental results of BACH, the beamline for dichroism and scattering experiments at ELETTRA

    SciTech Connect

    Zangrando, M.; Zacchigna, M.; Bondino, F.; Finazzi, M.; Pardini, T.; Plate, M.; Rochow, R.; Cocco, D.; Parmigiani, F.

    2004-05-12

    BACH, the new soft x-ray beamline for polarization dependent experiments at the Italian synchrotron radiation facility ELETTRA, has been commissioned, characterized and opened to external users. Based on two APPLE II undulators, it covers an energy range between 35 eV and 1600 eV with the control of the light polarization. The monochromator works either in high resolution or high flux mode. Resolving powers of 16000 at 50 eV, 12000 at 90 eV, more than 12000 at 400 eV, 15000 at 534 eV and 6600 at 867 eV have been achieved with the three high resolution gratings. The resolving powers of the high flux grating, which covers the 290 - 1600 eV range, have been measured reaching 7000 at 400 eV and 2200 at 867 eV. The fluxes, in the high resolution mode, range between 4{center_dot}1011 photons/s at 125 eV and 2{center_dot}1010 photons/s at about 1100 eV. Using the high flux grating with the best resolution achievable 1.7{center_dot}1011 photons/s impinge on the sample at 900 eV. Two branches are installed after the monochromator allowing the set-up of two different experimental stations. One of them, besides several facilities for surface preparation and analysis, hosts a compact inelastic soft x-ray spectrometer (ComIXS) dedicated to x-ray emission experiments exploiting the small spot (10 {mu}m in the vertical direction) on the sample. The other branch hosts a liquid helium cryostat equipped with a superconducting coil to perform absorption and transmission experiments with temperatures down to 2 K and magnetic field up to {+-}7 T.

  4. Dose calculations using MARS for Bremsstrahlung beam stops and collimators in APS beamline stations.

    SciTech Connect

    Dooling, J.; Accelerator Systems Division

    2010-11-01

    The Monte Carlo radiation transport code MARS is used to model the generation of gas bremsstrahlung (GB) radiation from 7-GeV electrons which scatter from residual gas atoms in undulator straight sections within the Advanced Photon Source (APS) storage ring. Additionally, MARS is employed to model the interactions of the GB radiation with components along the x-ray beamlines and then determine the expected radiation dose-rates that result. In this manner, MARS can be used to assess the adequacy of existing shielding or the specifications for new shielding when required. The GB radiation generated in the 'thin-target' of an ID straight section will consist only of photons in a 1/E-distribution up to the full energy of the stored electron beam. Using this analytical model, the predicted GB power for a typical APS 15.38-m insertion device (ID) straight section is 4.59 x 10{sup -7} W/nTorr/mA, assuming a background gas composed of air (Z{sub eff} = 7.31) at room temperature (293K). The total GB power provides a useful benchmark for comparisons between analytical and numerical approaches. We find good agreement between MARS and analytical estimates for total GB power. The extended straight section 'target' creates a radial profile of GB, which is highly peaked centered on the electron beam. The GB distribution reflects the size of the electron beam that creates the radiation. Optimizing the performance of MARS in terms of CPU time per incident trajectory requires the use of a relatively short, high-density gas target (air); in this report, the target density is {rho}L = 2.89 x 10{sup -2} g/cm{sup 2} over a length of 24 cm. MARS results are compared with the contact dose levels reported in TB-20, which used EGS4 for radiation transport simulations. Maximum dose-rates in 1 cc of tissue phantom form the initial basis for comparison. MARS and EGS4 results are approximately the same for maximum 1-cc dose-rates and attenuation in the photon-dominated regions; for thicker

  5. Performance Characteristics of Beamline 6.3.1 from 200 eV to 2000 eV at the Advanced Light Source

    NASA Astrophysics Data System (ADS)

    Nachimuthu, P.; Underwood, J. H.; Kemp, C. D.; Gullikson, E. M.; Lindle, D. W.; Shuh, D. K.; Perera, R. C. C.

    2004-05-01

    Bend magnet beamline 6.3.1 at the Advanced Light Source operates from 200 eV to 2000 eV, primarily used for x-ray absorption fine structure investigations. The beamline optics consist of a compact, entrance-slitless, Hettrick-Underwood type variable-line-spacing plane-grating monochromator and refocusing mirrors to provide a 25 μm × 500 μm spot at the focal point in the reflectometer end station. Wavelength is scanned by the simple rotation of the grating and illuminates a fixed exit slit. The LabView based beamline control and data acquisition computer code has been implemented to provide a convenient interface to the user. The dedicated end station is a reflectometer that is isolated from the beamline by a differential ion pump. The reflectometer can position samples to within 4 μm with an angular position of 0.002°, has total electron and fluorescence yield detectors, and pumps down in about 30 minutes. External end stations can be mounted downstream of the reflectometer as well. The versatility and simplicity of beamline 6.3.1 have made it useful for a wide range of applications such as the characterization of optical components, reflective coatings, and the investigation of a diverse range of materials in both the solid state and in solution.

  6. Final Technical Report on STTR Project DE-FG02-06ER86281 Particle Tracking in Matter-Dominated Beam Lines (G4beamline)

    SciTech Connect

    Muons, Inc.

    2011-05-19

    This project has been for software development of the G4beamline [1] program, which is a particle-tracking simulation program based on the Geant4 toolkit [2], optimized for beam lines. This program can perform more realistic simulations than most alternatives, while being significantly easier to use by physicists. This project has fostered the general acceptance of G4beamline within the muon community, and has assisted in expanding its role outside that community. During this project, the G4beamline user community has grown from about a half-dozen users to more than 200 users around the world. This project also validated our business decision to keep G4beamline an open-source program, judging that an STTR project would provide more development resources than would marketing and selling the program. G4beamline is freely available to the physics community, and has been well validated against experiments and other codes within its domain. Muons, Inc. continues to support and develop the program, and a major part of the company's continued success and growth is directly related to our expertise in applying this program to interesting applications.

  7. The new NCPSS BL19U2 beamline at the SSRF for small-angle X-ray scattering from biological macromolecules in solution1

    PubMed Central

    Li, Na; Li, Xiuhong; Wang, Yuzhu; Liu, Guangfeng; Zhou, Ping; Wu, Hongjin; Hong, Chunxia; Bian, Fenggang; Zhang, Rongguang

    2016-01-01

    The beamline BL19U2 is located in the Shanghai Synchrotron Radiation Facility (SSRF) and is its first beamline dedicated to biological material small-angle X-ray scattering (BioSAXS). The electrons come from an undulator which can provide high brilliance for the BL19U2 end stations. A double flat silicon crystal (111) monochromator is used in BL19U2, with a tunable monochromatic photon energy ranging from 7 to 15 keV. To meet the rapidly growing demands of crystallographers, biochemists and structural biologists, the BioSAXS beamline allows manual and automatic sample loading/unloading. A Pilatus 1M detector (Dectris) is employed for data collection, characterized by a high dynamic range and a short readout time. The highly automated data processing pipeline SASFLOW was integrated into BL19U2, with help from the BioSAXS group of the European Molecular Biology Laboratory (EMBL, Hamburg), which provides a user-friendly interface for data processing. The BL19U2 beamline was officially opened to users in March 2015. To date, feedback from users has been positive and the number of experimental proposals at BL19U2 is increasing. A description of the new BioSAXS beamline and the setup characteristics is given, together with examples of data obtained. PMID:27738413

  8. Pseudo Class III malocclusion

    PubMed Central

    Al-Hummayani, Fadia M.

    2016-01-01

    The treatment of deep anterior crossbite is technically challenging due to the difficulty of placing traditional brackets with fixed appliances. This case report represents a none traditional treatment modality to treat deep anterior crossbite in an adult pseudo class III malocclusion complicated by severely retruded, supraerupted upper and lower incisors. Treatment was carried out in 2 phases. Phase I treatment was performed by removable appliance “modified Hawley appliance with inverted labial bow,” some modifications were carried out to it to suit the presented case. Positive overbite and overjet was accomplished in one month, in this phase with minimal forces exerted on the lower incisors. Whereas, phase II treatment was performed with fixed appliances (braces) to align teeth and have proper over bite and overjet and to close posterior open bite, this phase was accomplished within 11 month. PMID:27052290

  9. The CHX Beamline at NSLS-II: a Tool to probe Structure and Dynamics in Soft-Condensed Matter

    NASA Astrophysics Data System (ADS)

    Fluerasu, Andrei; Wiegart, Lutz

    2012-02-01

    The Coherent Hard X-ray (CHX) beamline currently under construction at NSLS-II (Brookhaven National Laboratory) will serve as an optimized tool for the study of structure and dynamics in soft condensed matter. The unprecedented coherent flux will enable the study of dynamics in soft matter systems down to microsecond time scales via X-ray Photon Correlation Spectroscopy (XPCS). The available scattering geometries such as (GI)SAXS and (GI)WAXS can be used in a simultaneous fashion to collect static and dynamic scattering information on length scales ranging from supramolecular assemblies to atomic distances.

  10. Fabrication of compound refractive lens using soft and deep X-ray lithography beamline on Indus-2

    SciTech Connect

    Dhamgaye, V. P.; Lodha, G. S.

    2012-06-05

    X-ray compound refractive lenses (CRL) have been fabricated using Soft and Deep X-ray lithography (SDXRL) beamline on Indus-2. Upto 50 parabolic lenses are fabricated in PMMA using 1X X-ray mask. The mask contains of 20 micron thick gold absorbing pattern on polyimide membrane. The lens fabrication is done by exposing 500 {mu}m thick PMMA sheets to 5-12keV X-rays from Indus-2. The fabricated CRL will be suitable for generating focused X-ray beam of Indus-2 bending magnet source.

  11. A new on-axis multimode spectrometer for the macromolecular crystallography beamlines of the Swiss Light Source

    PubMed Central

    Owen, Robin L.; Pearson, Arwen R.; Meents, Alke; Boehler, Pirmin; Thominet, Vincent; Schulze-Briese, Clemens

    2009-01-01

    X-ray crystallography at third-generation synchrotron sources permits tremendous insight into the three-dimensional structure of macromolecules. Additional information is, however, often required to aid the transition from structure to function. In situ spectroscopic methods such as UV–Vis absorption and (resonance) Raman can provide this, and can also provide a means of detecting X-ray-induced changes. Here, preliminary results are introduced from an on-axis UV–Vis absorption and Raman multimode spectrometer currently being integrated into the beamline environment at X10SA of the Swiss Light Source. The continuing development of the spectrometer is also outlined. PMID:19240329

  12. A new method to suppress high-order harmonics for a synchrotron radiation soft X-ray beamline

    NASA Astrophysics Data System (ADS)

    Guo, Zhi-Ying; Xing, Hai-Ying; Hong, Cai-Hao; Tang, Kun; Han, Yong; Chen, Dong-Liang; Zhao, Yi-Dong

    2015-04-01

    A feasible and convenient method is proposed to suppress higher-harmonics for a varied-line-spacing plane grating monochromator in the soft X-ray region. Related calculations and experiments demonstrate that decreasing the included angle slightly by changing the parameter of the exit arm length can significantly improve light purity. This method is suitable and has been used for experiments of detector calibration in beamline 4B7B at the Beijing Synchrotron Radiation Facility (BSRF). Supported by National Natural Science Foundation of China (11375227, 61204008)

  13. Augmentation of Quick-EXAFS measurement facility at the energy scanning EXAFS beamline at INDUS-2 SRS

    SciTech Connect

    Poswal, A. K. Agrawal, Ankur; Bhattachryya, D.; Jha, S. N.; Sahoo, N. K.

    2015-06-24

    In this paper implementation of Quick-EXAFS data acquisition facility at the Energy Scanning EXAFS beamline(BL-09) at INDUS-2 synchrotron source, Indore is presented. By adopting a continuous-scan mode in the Double Crystal monochromator (DCM), a high signal-to-noise ratio is maintained and the acquisition time is reduced to few seconds. The quality of spectra and repeatability is checked by measuring standards. The present mode of data acquisition would enable EXAFS measurement for in-situ studies even in fluorescence mode.

  14. Multipurpose modular experimental station for the DiProI beamline of Fermi@Elettra free electron laser.

    PubMed

    Pedersoli, Emanuele; Capotondi, Flavio; Cocco, Daniele; Zangrando, Marco; Kaulich, Burkhard; Menk, Ralf H; Locatelli, Andrea; Mentes, Tevfik O; Spezzani, Carlo; Sandrin, Gilio; Bacescu, Daniel M; Kiskinova, Maya; Bajt, Saša; Barthelmess, Miriam; Barty, Anton; Schulz, Joachim; Gumprecht, Lars; Chapman, Henry N; Nelson, A J; Frank, Matthias; Pivovaroff, Michael J; Woods, Bruce W; Bogan, Michael J; Hajdu, Janos

    2011-04-01

    We present a compact modular apparatus with a flexible design that will be operated at the DiProI beamline of the Fermi@Elettra free electron laser (FEL) for performing static and time-resolved coherent diffraction imaging experiments, taking advantage of the full coherence and variable polarization of the short seeded FEL pulses. The apparatus has been assembled and the potential of the experimental setup is demonstrated by commissioning tests with coherent synchrotron radiation. This multipurpose experimental station will be open to general users after installation at the Fermi@Elettra free electron laser in 2011.

  15. Multipurpose modular experimental station for the DiProI beamline of Fermi@Elettra free electron laser

    NASA Astrophysics Data System (ADS)

    Pedersoli, Emanuele; Capotondi, Flavio; Cocco, Daniele; Zangrando, Marco; Kaulich, Burkhard; Menk, Ralf H.; Locatelli, Andrea; Mentes, Tevfik O.; Spezzani, Carlo; Sandrin, Gilio; Bacescu, Daniel M.; Kiskinova, Maya; Bajt, Saša; Barthelmess, Miriam; Barty, Anton; Schulz, Joachim; Gumprecht, Lars; Chapman, Henry N.; Nelson, A. J.; Frank, Matthias; Pivovaroff, Michael J.; Woods, Bruce W.; Bogan, Michael J.; Hajdu, Janos

    2011-04-01

    We present a compact modular apparatus with a flexible design that will be operated at the DiProI beamline of the Fermi@Elettra free electron laser (FEL) for performing static and time-resolved coherent diffraction imaging experiments, taking advantage of the full coherence and variable polarization of the short seeded FEL pulses. The apparatus has been assembled and the potential of the experimental setup is demonstrated by commissioning tests with coherent synchrotron radiation. This multipurpose experimental station will be open to general users after installation at the Fermi@Elettra free electron laser in 2011.

  16. Multipurpose modular experimental station for the DiProI beamline of Fermi@Elettra free electron laser.

    PubMed

    Pedersoli, Emanuele; Capotondi, Flavio; Cocco, Daniele; Zangrando, Marco; Kaulich, Burkhard; Menk, Ralf H; Locatelli, Andrea; Mentes, Tevfik O; Spezzani, Carlo; Sandrin, Gilio; Bacescu, Daniel M; Kiskinova, Maya; Bajt, Saša; Barthelmess, Miriam; Barty, Anton; Schulz, Joachim; Gumprecht, Lars; Chapman, Henry N; Nelson, A J; Frank, Matthias; Pivovaroff, Michael J; Woods, Bruce W; Bogan, Michael J; Hajdu, Janos

    2011-04-01

    We present a compact modular apparatus with a flexible design that will be operated at the DiProI beamline of the Fermi@Elettra free electron laser (FEL) for performing static and time-resolved coherent diffraction imaging experiments, taking advantage of the full coherence and variable polarization of the short seeded FEL pulses. The apparatus has been assembled and the potential of the experimental setup is demonstrated by commissioning tests with coherent synchrotron radiation. This multipurpose experimental station will be open to general users after installation at the Fermi@Elettra free electron laser in 2011. PMID:21529017

  17. The electron spectro-microscopy beamline at National Synchrotron Light Source II: A wide photon energy range, micro-focusing beamlinefor photoelectron spectro-microscopies

    SciTech Connect

    Reininger R.; Hulbert L.; Johnson P.D.; Sadowski, J.T.; Starr, D.E.; Chubar, O.; Valla, T.; Vescovo, E.

    2012-02-13

    A comprehensive optical design for a high-resolution, high-flux, wide-energy range, micro-focused beamline working in the vacuum ultraviolet and soft x-ray photon energy range is proposed. The beamline is to provide monochromatic radiation to three photoelectron microscopes: a full-field x-ray photoelectron emission microscope and two scanning instruments, one dedicated to angle resolved photoemission spectroscopy ({micro}-ARPES) and one for ambient pressure x-ray photoelectron spectroscopy and scanning photoelectron microscopy (AP-XPS/SPEM). Microfocusing is achieved with state of the art elliptical cylinders, obtaining a spot size of 1 {micro}m for ARPES and 0.5 {micro}m for AP-XPS/SPEM. A detailed ray tracing analysis quantitatively evaluates the overall beamline performances.

  18. High-pressure beamline (PLANET) at the spallation neutron source, J-PARC (Invited)

    NASA Astrophysics Data System (ADS)

    Kagi, H.; Hattori, T.; Arima, H.; Utsumi, W. S.; Komatsu, K.; Nagai, T.; Yagi, T.

    2009-12-01

    spectrometer covers d spacing from 0.2 Å to 4.1 Å at 90° bank within the first frame and the resolution is less than 0.5% in Δd/d. We will overview the future of the PLANET beamline.

  19. PROXIMA 2A - A New Fully Tunable Micro-focus Beamline for Macromolecular Crystallography

    NASA Astrophysics Data System (ADS)

    Duran, D.; Le Couster, S.; Desjardins, K.; Delmotte, A.; Fox, G.; Meijers, R.; Moreno, T.; Savko, M.; Shepard, William

    2013-03-01

    PROXIMA 2 is the first canted beamline at the French National Synchrotron Source SOLEIL, and it will provide two independent and tunable experimental stations, PX2-A & PX2-B, dedicated to macromolecular crystallography. The first station, PX2-A, is currently under construction. The source is an in-vacuum U24 undulator, and the optical layout includes a cryogenically cooled channel-cut Si[111] monochromator, a convex horizontal pre-focussing mirror (HPM) and a pair of focusing bimorph mirrors in Kirkpatrick-Baez (KB) configuration. This innovative optical scheme, harnesses a convex mirror to produce a virtual secondary source, which permits the KB mirrors to refocus the X-rays down to 5 μm from a relatively large horizontal source size. In fully focussed mode, the cross-section of the beam at the sample position will be approximately 5.0 μm × 3.5 μm (H×V FWHM) delivering a photon flux of 1×1013 - 4×1011 ph/s over the range of 5 - 15 keV with a desired positional stability better than 0.5 μm rms over several hours. To achieve such stability, the supports for the optical elements are designed to minimise the effects of vibrations transmitted from the surroundings, and accelerometers will be mounted in situ to monitor these effects. For long term drifts, the experimental hutch is temperature controlled to within 0.1°C, and a preparation laboratory acts as a buffer zone. Two types of X-ray Beam Position Monitors (XBPMs), single crystal CVD diamond and thin foil-diode devices, have been developed to improve their robustness and signal-noise ratio. Due to the limitations of space, three compact and modular "slit boxes" have been designed: These vessels house a variety of beam conditioning elements such as slits, XBPMs, attenuators, imagers and a fast shutter. At the end of the station, a micro-diffractometer and an area detector (ADSC Q315) have already been installed, and the first X-ray diffraction data with unfocussed beam from test crystals are of excellent

  20. SUPERSTARS III: 3-5.

    ERIC Educational Resources Information Center

    North Carolina State Dept. of Public Education, Raleigh.

    SUPERSTARS III is a K-8 program designed as an enrichment opportunity for self-directed learners in mathematics. The basic purpose of SUPERSTARS III is to provide the extra challenge that self-motivated students need in mathematics and to do so in a structured, long-term program that does not impinge on the normal classroom routine or the…