Deformation sequence of Baltimore gneiss domes, USA, assessed from porphyroblast Foliation Intersection Axes

NASA Astrophysics Data System (ADS)

Yeh, Meng-Wan

2007-05-01

The NE-SW trending gneiss domes around Baltimore, Maryland, USA, have been cited as classic examples of mantled gneiss domes formed by diapiric rise of migmatitic gneisses [Eskola, P., 1949. The problem of mantled gneiss domes. Quarterly Journal of Geological Society of London 104/416, 461-476]. However, 3-D analysis of porphyroblast-matrix foliation relations and porphyroblast inclusion trail geometries suggests that they are the result of interference between multiple refolding of an early-formed nappe. A succession of six FIA (Foliation Intersection Axes) sets, based upon relative timing of inclusion texture in garnet and staurolite porphyroblasts, revealed 6 superposed deformation phases. The successions of inclusion trail asymmetries, formed around these FIAs, document the geometry of deformation associated with folding and fabric development during discrete episodes of bulk shortening. Exclusive top to NW shear asymmetries of curvature were recorded by inclusion trails associated with the vertical collapsing event within the oldest FIA set (NE-SW trend). This strongly indicates a large NE-SW-striking, NW-verging nappe had formed early during this deformation sequence. This nappe was later folded into NE-SW-trending up-right folds by coaxial shortening indicated by an almost equal proportion of both inclusion trail asymmetries documented by the second N-S-trending FIA set. These folds were then amplified by later deformation, as the following FIA sets showed an almost equal proportion of both inclusion trail asymmetries.

A Customizable Flow Injection System for Automated, High Throughput, and Time Sensitive Ion Mobility Spectrometry and Mass Spectrometry Measurements

DOE Office of Scientific and Technical Information (OSTI.GOV)

Orton, Daniel J.; Tfaily, Malak M.; Moore, Ronald J.

To better understand disease conditions and environmental perturbations, multi-omic studies (i.e. proteomic, lipidomic, metabolomic, etc. analyses) are vastly increasing in popularity. In a multi-omic study, a single sample is typically extracted in multiple ways and numerous analyses are performed using different instruments. Thus, one sample becomes many analyses, making high throughput and reproducible evaluations a necessity. One way to address the numerous samples and varying instrumental conditions is to utilize a flow injection analysis (FIA) system for rapid sample injection. While some FIA systems have been created to address these challenges, many have limitations such as high consumable costs, lowmore » pressure capabilities, limited pressure monitoring and fixed flow rates. To address these limitations, we created an automated, customizable FIA system capable of operating at diverse flow rates (~50 nL/min to 500 µL/min) to accommodate low- and high-flow instrument sources. This system can also operate at varying analytical throughputs from 24 to 1200 samples per day to enable different MS analysis approaches. Applications ranging from native protein analyses to molecular library construction were performed using the FIA system. The results from these studies showed a highly robust platform, providing consistent performance over many days without carryover as long as washing buffers specific to each molecular analysis were utilized.« less

The power of FIA Phase 3 Crown-Indicator variables to detect change

Treesearch

William Bechtold; KaDonna Randolph; Stanley Zarnoch

2009-01-01

The goal of Phase 3 Detection Monitoring as implemented by the Forest Inventory and Analysis Program is to identify forest ecosystems where conditions might be deteriorating in subtle ways over large areas. At the relatively sparse sampling intensity of the Phase 3 plot network, a rough measure of success for the forest health indicators developed for this purpose is...

Estimating forest floor fuels in eastern U.S. forests

Treesearch

David C. Chojnacky; Steven G. McNulty; Jennifer Moore Myers; Michael K. Gavazzi

2005-01-01

The Forest Inventory Analysis (FIA) program (U.S. Department of Agriculture, Forest Service) systematically samples the nation's forests and currently measures variable related to down woody material (DWM) on a subsample of its plots in the third phase of a 3-phase sampling design. This paper focuses on: (1) compiling estimates of DWM within limitations of...

Flow injection spectrophotometric determination of V(V) involving on-line separation using a poly(vinylidene fluoride-co-hexafluoropropylene)-based polymer inclusion membrane.

PubMed

Yaftian, Mohammad Reza; Almeida, M Inês G S; Cattrall, Robert W; Kolev, Spas D

2018-05-01

A poly(vinylidene fluoride-co-hexafluoropropylene)-based polymer inclusion membrane (PIM) using Cyphos® IL 101 (i.e. trihexyl(tetradecyl)phosphonium chloride) as the carrier and 2-nitrophenyl octyl ether as a plasticizer in a mass ratio of 55/35/10 was employed for the on-line extractive separation of V(V) prior to its spectrophotometric determination in a flow injection analysis (FIA) system using xylenol orange as the colorimetric reagent. The selectivity of the membrane allowed the determination of V(V) in sulfate solutions in the presence of a variety of cations and anions. The interference of molybdenum(VI) was eliminated by off-line extraction using the same PIM. A univariate sequential optimization of the newly developed FIA system was conducted and under optimal conditions the system is characterized by a linear concentration range of 0.5-8.0mgL -1 , detection limit of 0.08mgL -1 and sample throughput of 4h -1 . The relative standard deviation at the 3mgL -1 level of V(V) was 2.9% based on 8 replicate determinations. The membrane was stable, which was reflected by the standard deviation value for determinations over three consecutive days (24 determinations of 3mgL -1 V(V)) of 3.6%. The newly developed FIA system was applied to the determination of V(V) in water and dietary supplements samples and a good agreement with inductively coupled plasma optical emission spectrometry was observed. Copyright © 2018 Elsevier B.V. All rights reserved.

Evaluation of a direct injection nebulizer interface for flow injection analysis and high performance liquid chromatography with inductively coupled plasma-atomic emission spectroscopic detection

DOE Office of Scientific and Technical Information (OSTI.GOV)

LaFreniere, K.E.

A direct injection nebulizer (DIN) was designed, developed, and evaluated to determine its potential utilization as an effective interface for flow injection analysis (FIA) and high performance liquid chromatography (HPLC) coupled with inductively coupled plasma-atomic emission spectroscopic detection. The analytical figures of merit for the DIN when used as an interface for FIA-ICP-AES were found to be comparable to or better than those obtained with conventional pneumatic nebulization in terms of limits of detection (LODs), reproducibility, linearity, and interelement effects. Stable plasma operation was maintained for the DIN sample introduction of a variety of pure organic solvents, including acetonitrile, methanol,more » methylisobutylketone, and pyridine. The HPLC-DIN-ICP-AES facility was specifically applied for the speciation of inorganic and organometallic species contained in synthetic mixtures, vanilla extracts, and a variety of energy-related materials, such as shale oil process water, coal extracts, shale oil, crude oil, and an SRC II. Suggestions for future research are also considered. 227 refs., 44 figs., 15 tabs.« less

Development and comparison of three diagnostic immunoassay formats for the detection of azoxystrobin.

PubMed

Furzer, Gordon S; Veldhuis, Linda; Hall, J Christopher

2006-02-08

The currently accepted method of detection for azoxystrobin, a strobilurin fungicide, involves a labor-intensive organic solvent extraction and gas chromatography analysis. Three diagnostic assay formats, i.e., enzyme-linked immunosorbent assay (ELISA), fluorescence polarization (FP), and time-resolved fluorescence (TR-FIA), were developed and compared with regard to detection and quantification of azoxystrobin in grape extract and river, lake, and well water samples. These three assay formats require no initial sample extraction and were not affected by any of the environmental matrices tested, and each had a linear working range of 0-400 pg/mL. The polyclonal antibodies used for each of the immunoassays were specific to azoxystrobin; that is, the highest cross-reactivity to other pesticides observed was 5.7%. The limits of detection of the immunoassays were similar at 3 (ELISA), 46 (FP), and 28 (TR-FIA) pg/mL, as were the respective IC50 values of 306, 252, and 244 pg/mL. Each of the three immunoassays developed was less labor-intensive and approximately 100-fold more sensitive than the gas chromatographic method. While the three formats were comparable in terms of performance, the fluorescence polarization assay was the least labor-intensive and required the least time to perform.

Profiles of alpha-melanocyte-stimulating hormone in the Japanese flounder as revealed by a newly developed time-resolved fluoroimmunoassay and immunohistochemistry.

PubMed

Amiya, Noriko; Amano, Masafumi; Takahashi, Akiyoshi; Yamanome, Takeshi; Yamamori, Kunio

2007-03-01

Profiles of alpha-melanocyte-stimulating hormone (alpha-MSH) in the Japanese flounder were examined by a newly developed time-resolved fluoroimmunoassay (TR-FIA) and immunohistochemistry. A TR-FIA for alpha-MSH was newly developed, and its levels in the pituitary gland and plasma of Japanese flounder reared in a white or black tank for 5 months were compared. A competitive assay using two antibodies was performed among secondary antibodies in the solid phase, alpha-MSH antibodies, samples, and europium-labeled Des-Ac-alpha-MSH. The sensitivity of the assay, defined as twice the standard deviation at a zero dose, was 0.98 ng/ml (49 pg/well). The intra- and interassay coefficients of variation of the assay were 8.8% (n=8) and 17.3% (n=5), respectively, at about 50% binding. Cross-reactivities of Des-Ac-alpha-MSH and Di-Ac-alpha-MSH were about 100%. Cross-reactivities of adrenocorticotropic hormone, salmon gonadotropin-releasing hormone (sGnRH), and chicken GnRH-II were less than 0.2%, and that of melanin-concentrating hormone was less than 2.0% at 50% binding. Displacement curves of serially twofold-diluted hypothalamus extract, pituitary gland extract, and plasma extract of Japanese flounder with the assay buffer were parallel to the alpha-MSH standard curve. Moreover, displacement curves of serially twofold-diluted hypothalamus and/or pituitary gland extract of masu salmon, goldfish, red seabream, Japanese eel, tiger puffer, and barfin flounder with the assay buffer were also parallel to the alpha-MSH standard. In Japanese flounder, total immunoreactive (ir)-alpha-MSH levels in the pituitary gland were lower in the black tank, whereas those in the plasma tended to be higher in the black tank, suggesting that the synthesis and release of alpha-MSH are higher in the black tank. alpha-MSH-ir cells were detected in the pars intermedia and a small part of the pars distalis of the pituitary gland. alpha-MSH-ir cell bodies were located in the basal hypothalamus and alpha-MSH-ir fibers were distributed not only in the hypothalamus but also in the telencephalon, midbrain, cerebellum, and medulla oblongata, suggesting that alpha-MSH functions as a neuromodulator in the brain.

Urban FIA: where we have been, where we are, and where we are going

Treesearch

Mark Majewsky

2015-01-01

The FIA program has been inventorying the Nation’s forestland since the 1930s. The focus of the CORE FIA program is to capture trees that meet the FIA definition of forestland, in doing so it excludes trees that do not. Leadership recognized the need to fill this gap and the 2014 Farm Bill has instructed FIA to “Implement an annualized inventory of trees in urban...

Forests of Ohio, 2013

Treesearch

Richard H. Widmann

2014-01-01

This publication provides an overview of the forest resources in Ohio based upon inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 2001, FIA has implemented an annual inventory in Ohio....

Forests of Maryland, 2013

Treesearch

T.W. Lister; S.A. Pugh

2014-01-01

This publication provides an overview of forest resources in Maryland based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 2004, FIA has employed an annual inventory measuring data...

Forests of Maine, 2015

Treesearch

Emily S. Huff; William H. McWilliams

2016-01-01

This publication provides an overview of the forest resources in Maine based upon inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 1999, FIA has implemented an annual inventory...

Forests of Pennsylvania, 2013

Treesearch

George L. McCaskill

2014-01-01

This publication provides an overview of the forest resources in Pennsylvania based upon inventories conducted by the USDA Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 1999, FIA has implemented an annual inventory...

Forests of Maine, 2013

Treesearch

George L. McCaskill

2014-01-01

This publication provides an overview of the forest resources in Maine based upon inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 1999, FIA has implemented an annual inventory...

Opportunities to improve monitoring of temporal trends with FIA panel data

Treesearch

Raymond Czaplewski; Michael Thompson

2009-01-01

The Forest Inventory and Analysis (FIA) Program of the Forest Service, Department of Agriculture, is an annual monitoring system for the entire United States. Each year, an independent "panel" of FIA field plots is measured. To improve accuracy, FIA uses the "Moving Average" or "Temporally Indifferent" method to combine estimates from...

Forests of Maine, 2014

Treesearch

George L. McCaskill

2015-01-01

This publication provides an overview of the forest resources in Maine based upon inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 1999, FIA has implemented an annual inventory...

The effects of removing condition boundaries on FIA estimates

Treesearch

David Gartner; Gregory Reams

2002-01-01

When Forest Inverltory and Analysis (FIA) changed to the national standards for the inventory system, plots with lnultiplc condition codes were introduced to the Southern Station's FIA unit. FIA maps up to five different conditions on completely or partially forested 1124-acre subplots. This change has madc producing inventory estimates more complex because the...

Forests of Delaware, 2013

Treesearch

T.W. Lister; S.A. Pugh

2014-01-01

This publication provides an overview of forest resources in Delaware based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 2004, FIA has employed an annual inventory measuring data...

Timing of isoclinal folds in multiply deformed high metamorphic grade region using FIA succession

NASA Astrophysics Data System (ADS)

Cao, Hui; Cai, Zhihui

2013-04-01

Multiply deformed and isoclinally folded interlayered high metamorphic grade gneisses and schists can be very difficult rocks for resolving early formed stratigraphic and structural relationships. When such rocks contain porphyroblasts a new approach is possible because of the way in which porphyroblast growth is affected by crenulation versus reactivation of compositional layering. The asymmetries of the overprinting foliations preserved as inclusion trails that define the FIAs can be used to investigate whether an enigmatic isoclinal fold is an antiform or synform. This approach also reveals when the fold first formed during the tectonic history of the region. Isoclinally folded rocks in the Arkansas River region of Central Colorado contain relics of fold hinges that have been very difficult to ascertain whether they are antiforms or synforms because of younger refolding effects and the locally truncated nature of coarse compositional layering. With the realization that rocks with a schistosity parallel to bedding (S0 parallel S1) have undergone lengthy histories of deformation that predate the obvious first deformation came recognition that large scale regional folds can form early during this process and be preserved throughout orogenesis. This extensive history is lost within the matrix because of reactivational shear on the compositional layering. However, it can be extracted by measuring FIAs. Recent work using this approach has revealed that the trends of axial planes of all map scale folds, when plotted on a rose diagram, strikingly reflect the FIA trends. That is, although it was demonstrated that the largest scale regional folds commonly form early in the total history, other folds can form and be preserved from subsequent destruction in the strain shadows of plutons or through the partitioning of deformation due to heterogeneities at depth.

Forests of New York, 2013

Treesearch

Richard H. Widmann

2014-01-01

This publication provides an overview of the forest resources in New York based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at http://fia.fs.fed.us. Since 2003, FIA has implemented an annual inventory in New...

Forests of West Virginia, 2013

Treesearch

Richard H. Widmann

2014-01-01

This publication provides an overview of the forest resources in West Virginia based upon inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the FIA program is available online at http://fia.fs.fed.us. Since 2004, FIA has implemented an annual inventory in West Virginia. For...

The Effects of Removing Condition Boundaries on FIA Estimates

Treesearch

David Gartner; Gregory Reams

2005-01-01

When Forest Inventory and Analysis (FIA) changed to the national standards for the inventory system, plots with multiple condition codes were introduced to the Southern Station's FIA unit. FIA maps up to five different conditions on completely or partially forested 1/24-acre subplots. This change has made producing inventory estimates more complex because the data...

Access and Use of FIA Data Through FIA Spatial Data Services

Treesearch

Elizabeth LaPoint

2005-01-01

Forest Inventory and Analysis (FIA) Spatial Data Services (SDS) was established in May 2002 to facilitate outside access to FIA data and allow use of georeferenced plot data while protecting the confidentiality of plot locations. Modification of the Food Security Act of 1985 legislated the protection of information on plot location and ownership. Penalties were put in...

A 30-meter spatial database for the nation's forests

Treesearch

Raymond L. Czaplewski

2002-01-01

The FIA vision for remote sensing originated in 1992 with the Blue Ribbon Panel on FIA, and it has since evolved into an ambitious performance target for 2003. FIA is joining a consortium of Federal agencies to map the Nation's land cover. FIA field data will help produce a seamless, standardized, national geospatial database for forests at the scale of 30-m...

Comparing Minnesota land cover/use area estimates using NRI and FIA data

Treesearch

Veronica C. Lessard; Mark H. Hansen; Mark D. Nelson

2002-01-01

Areas for land cover/use categories on non-Federal land in Minnesota were estimated from Forest Inventory and Analysis (FIA) data and National Resources Inventory (NRI) data. Six common land cover/use categories were defined, and the NRI and FIA land cover/use categories were assigned to them. Area estimates for these categories were calculated from the FIA and NRI...

Sampling protocol, estimation, and analysis procedures for the down woody materials indicator of the FIA program

Treesearch

Christopher Woodall

2005-01-01

The Forest Inventory and Analysis (FIA) program of the USDA Forest Service conducts a national inventory of forests of the United States. A subset of FIA permanent inventory plots are sampled every year for numerous indicators of forest health ranging from soils to understory vegetation. Down woody material (DWM) is an FIA indicator that provides estimates of forest...

Recent Electrochemical and Optical Sensors in Flow-Based Analysis

PubMed Central

Chailapakul, Orawon; Ngamukot, Passapol; Yoosamran, Alongkorn; Siangproh, Weena; Wangfuengkanagul, Nattakarn

2006-01-01

Some recent analytical sensors based on electrochemical and optical detection coupled with different flow techniques have been chosen in this overview. A brief description of fundamental concepts and applications of each flow technique, such as flow injection analysis (FIA), sequential injection analysis (SIA), all injection analysis (AIA), batch injection analysis (BIA), multicommutated FIA (MCFIA), multisyringe FIA (MSFIA), and multipumped FIA (MPFIA) were reviewed.

Pilot Inventory of FIA plots traditionally called `nonforest'

Treesearch

Rachel Riemann

2003-01-01

Forest-inventory data were collected on plots defined as ?nonforest? by the USDA Forest Service?s Forest Inventory and Analysis (FIA) unit. Nonforest plots may have trees on them, but they do not fit FIA?s definition of forest because the area covered by trees is too small, too sparsely populated by trees, too narrow (e.g., trees between fields or in the middle of a...

Verification of the Jenkins and FIA sapling biomass equations for hardwood species in Maine

Treesearch

Andrew S. Nelson; Aaron R. Weiskittel; Robert G. Wagner; Michael R. Saunders

2012-01-01

In 2009, the Forest Inventory and Analysis Program (FIA) updated its biomass estimation protocols by switching to the component ratio method to estimate biomass of medium and large trees. Additionally, FIA switched from using regional equations to the current FIA aboveground sapling biomass equations that predict woody sapling (2.5 to 12.4 cm d.b.h.) biomass using the...

Using FIA data to assess current and potential future tree species importance values in the eastern United States

Treesearch

Louis Iverson; Anantha Prasad; Anantha Prasad

2003-01-01

FIA data are extremely valuable for evaluating regional variation in forest distribution. We have processed and summarized FIA data to show four patterns across the Eastern United States: 1) the number and density of FIA forested plots by state, 2) current importance values and frequencies for several species within 20 x 20 km blocks, 3) tree diversity by block, and 4...

Using FIA data to assess current and potential future tree species importance values in the eastern United States

Treesearch

Louis Iverson; Anantha Prasad

2002-01-01

FIA data are extremely valuable for evaluating regional variation in forest distribution. We have processed and summarized FIA data to show four patterns across the Eastern United States: 1) the number and density of FIA forested plots by state, 2) current importance values and frequencies for several species within 20 x 20 km blocks, 3) tree diversity by block, and 4...

Evaluation of a direct injection nebulizer interface for flow injection analysis and high performance liquid chromatography with inductively coupled plasma-atomic emission spectroscopic detection

DOE Office of Scientific and Technical Information (OSTI.GOV)

LaFreniere, K.E.

A direct injection nebulizer (DIN) was designed, developed and evaluated to determine its potential utilization as an effective interface for flow injection analysis (FIA) and high performance liquid chromatography (HPLC) coupled with inductively coupled plasma-atomic emission spectroscopic detection. The analytical figures of merit for the DIN when used as an interface for FIA-ICP-AES were found to be comparable to or better than those obtained with conventional pneumatic nebulization in terms of limits of detection (LODs), reproducibility, linearity, and interelement effects. In the HPLC mode, the LODDs were found to be comparable to those obtained by continuous-flow sample introduction into themore » ICP, or inferior by up to only a factor of four. Stable plasma operation was maintained for the DIN sample introduction of a variety of pure organic solvents, including acetonitrile, methanol, methyl-isobutylketone, and pyridine. The HPLC-DIN-ICP-AES facility was specifically applied for the speciation of inorganic and organo-metallic species contained in synthetic mixtures, vanilla extracts and a variety of energy-related materials, such as shale oil process water, coal extracts, shale oil, crude oil, and an SRC II. Suggestions for future research are also considered.« less

On-line ionic liquid-based preconcentration system coupled to flame atomic absorption spectrometry for trace cadmium determination in plastic food packaging materials.

PubMed

Martinis, Estefanía M; Olsina, Roberto A; Altamirano, Jorgelina C; Wuilloud, Rodolfo G

2009-05-15

A novel on-line preconcentration method based on liquid-liquid (L-L) extraction with room temperature ionic liquids (RTILs) coupled to flame atomic absorption spectrometry (FAAS) was developed for cadmium determination in plastic food packaging materials. The methodology is based on the complexation of Cd with 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (5-Br-PADAP) reagent after sample digestion followed by extraction of the complex with the RTIL 1-butyl-3-methylimidazolium hexafluorophosphate ([C(4)mim][PF(6)]). The mixture was loaded into a flow injection analysis (FIA) manifold and the RTIL rich-phase was retained in a microcolumn filled with silica gel. The RTIL rich-phase was then eluted directly into FAAS. A enhancement factor of 35 was achieved with 20 mL of sample. The limit of detection (LOD), obtained as IUPAC recommendation, was 6 ng g(-1) and the relative standard deviation (R.S.D.) for 10 replicates at 10 microg L(-1) Cd concentration level was 3.9%, calculated at the peak heights. The calibration graph was linear and a correlation coefficient of 0.9998 was achieved. The accuracy of the method was evaluated by both a recovery study and comparison of results with direct determination by electrothermal atomic absorption spectrometry (ETAAS). The method was successfully applied for Cd determination in plastic food packaging materials and Cd concentrations found were in the range of 0.04-10.4 microg g(-1).

Forests of Maine, 2016

Treesearch

Brett J. Butler

2017-01-01

This publication provides an overview of the forest resources in Maine based upon inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Information about the national and regional FIA program is available online at www.fia.fs.fed.us....

Current status of chestnut in eastern US forests

Treesearch

William H. McWiliams; Tonya W. Lister; Elizabeth B. LaPoint; Anita K. Rose; John S. Vissage

2006-01-01

The USDA Forest Service, Forest Inventory and Analysis (FIA) program provides the opportunity to assess the current distribution of American chestnut (Castanea dentata (Marsh.) Borkh) and prospective trends. Assessing chestnut using the FIA data was challenging because of the coarse nature of the FIA sample and chestnut's rarity in natural...

Spatially Locating FIA Plots from Pixel Values

Treesearch

Greg C. Liknes; Geoffrey R. Holden; Mark D. Nelson; Ronald E. McRoberts

2005-01-01

The USDA Forest Service Forest Inventory and Analysis (FIA) program is required to ensure the confidentiality of the geographic locations of plots. To accommodate user requests for data without releasing actual plot coordinates, FIA creates overlays of plot locations on various geospatial data, including satellite imagery. Methods for reporting pixel values associated...

From detection monitoring to evaluation monitoring - a case study involving crown dieback in northern white-cedar

Treesearch

KaDonna Randolph; William Bechtold; Randall Morin; Stanley Zarnoch

2009-01-01

The Forest Inventory and Analysis (FIA) Phase 3 plot network is a crucial part of the U.S. Forest Health Monitoring program's detection monitoring system, where select indicators are monitored for signals that may indicate deteriorating forest health. When a negative signal is identified, evaluation monitoring provides a mechanism whereby a potential problem can...

Assessing soil compaction on Forest Inventory & Analysis phase 3 field plots using a pocket penetrometer

Treesearch

Michael C. Amacher; Katherine P. O' Neill

2004-01-01

Soil compaction is an important indicator of soil quality, yet few practical methods are available to quantitatively measure this variable. Although an assessment of the areal extent of soil compaction is included as part of the soil indicator portion of the Forest Inventory & Analysis (FIA) program, no quantitative measurement of the degree of soil compaction...

Forests of Illinois, 2015

Treesearch

Susan Crocker; Brett Butler

2016-01-01

This publication provides an overview of forest resources in Illinois based on an annual inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. Information about the FIA program is available at...

Coordination, Cooperation, and Collaboration between FIA and NRI

Treesearch

Raymond L. Czaplewski; James Rack; Veronica C. Lessard; David F. Heinzen; Susan Ploetz; Thomas L. Schmidt; Earl C. Leatherberry

2005-01-01

The USDA Forest Service conducts a detailed survey of the Nation's forests through the Forest Inventory and Analysis (FIA) program. The USDA Natural Resources Service conducts an entirely separate survey, the National Resources Inventory (NRI), to monitor status and trends in the Nation's soil and other natural resources. Blue Ribbon Panels for both FIA and...

Forests of Ohio, 2016

Treesearch

Thomas A. Albright

2017-01-01

This resource update provides an overview of the forest resources in Ohio based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly.1 Information about the national and regional FIA...

Cartographic standards to improve maps produced by the Forest Inventory and Analysis program

Treesearch

Charles H. (Hobie) Perry; Mark D. Nelson

2009-01-01

The Forest Service, U.S. Department of Agriculture's Forest Inventory and Analysis (FIA) program is incorporating an increasing number of cartographic products in reports, publications, and presentations. To create greater quality and consistency within the national FIA program, a Geospatial Standards team developed cartographic design standards for FIA map...

National FIA plot intensification procedure report

Treesearch

Jock A. Blackard; Paul L. Patterson

2014-01-01

The Forest Inventory and Analysis (FIA) program of the U.S. Forest Service (USFS) measures a spatially distributed base grid of forest inventory plots across the United States. The sampling intensity of plots may be increased in some regions when warranted by specific inventory objectives. Several intensification methods have been developed within FIA and USFS National...

The role of flow injection analysis within the framework of an automated laboratory

PubMed Central

Stockwell, Peter B.

1990-01-01

Flow Injection Analysis (FIA) was invented at roughly the same time by two quite dissimilar research groups [1,2]. FIA was patented by both groups in 1974; a year also marked by the publication of the first book on automatic chemical analysis [3]. This book was a major undertaking for its authors and it is hoped that it has added to the knowledge of those analysts attempting to automate their work or to increase the level of computerization/automation and thus reduce staffing commitments. This review discusses the role of FIA in laboratory automation, the advantages and disadvantages of the FIA approach, and the part it could play in future developments. It is important to stress at the outset that the FIA approach is all too often closely paralleled with convention al continuous flow analysis (CFA). This is a mistake for many reasons, none the least of which because of the considerable success of the CFA approach in contrast to the present lack of penetration in the commercial market-place of FIA instrumentation. PMID:18925262

Soil Carbon Variability and Change Detection in the Forest Inventory Analysis Database of the United States

NASA Astrophysics Data System (ADS)

Wu, A. M.; Nater, E. A.; Dalzell, B. J.; Perry, C. H.

2014-12-01

The USDA Forest Service's Forest Inventory Analysis (FIA) program is a national effort assessing current forest resources to ensure sustainable management practices, to assist planning activities, and to report critical status and trends. For example, estimates of carbon stocks and stock change in FIA are reported as the official United States submission to the United Nations Framework Convention on Climate Change. While the main effort in FIA has been focused on aboveground biomass, soil is a critical component of this system. FIA sampled forest soils in the early 2000s and has remeasurement now underway. However, soil sampling is repeated on a 10-year interval (or longer), and it is uncertain what magnitude of changes in soil organic carbon (SOC) may be detectable with the current sampling protocol. We aim to identify the sensitivity and variability of SOC in the FIA database, and to determine the amount of SOC change that can be detected with the current sampling scheme. For this analysis, we attempt to answer the following questions: 1) What is the sensitivity (power) of SOC data in the current FIA database? 2) How does the minimum detectable change in forest SOC respond to changes in sampling intervals and/or sample point density? Soil samples in the FIA database represent 0-10 cm and 10-20 cm depth increments with a 10-year sampling interval. We are investigating the variability of SOC and its change over time for composite soil data in each FIA region (Pacific Northwest, Interior West, Northern, and Southern). To guide future sampling efforts, we are employing statistical power analysis to examine the minimum detectable change in SOC storage. We are also investigating the sensitivity of SOC storage changes under various scenarios of sample size and/or sample frequency. This research will inform the design of future FIA soil sampling schemes and improve the information available to international policy makers, university and industry partners, and the public.

Varicella Zoster Virus and Large Vessel Vasculitis, the Absence of an Association.

PubMed

Procop, Gary W; Eng, Charis; Clifford, Alison; Villa-Forte, Alexandra; Calabrese, Leonard H; Roselli, Eric; Svensson, Lars; Johnston, Douglas; Pettersson, Gosta; Soltesz, Edward; Lystad, Lisa; Perry, Julian D; Blandford, Alexander; Wilson, Deborah A; Hoffman, Gary S

2017-01-01

It is controversial whether microorganisms play a role in the pathogenesis of large and medium vessel vasculitides (eg, giant cell arteritis [GCA], Takayasu arteritis [TAK] and focal idiopathic aortitis [FIA]). Recent studies have reported the presence of Varicella Zoster Virus (VZV) within formalin-fixed, paraffin-embedded temporal arteries and aortas of about three-quarters or more of patients with these conditions, and in a minority of controls. In a prospective study, we sought to confirm these findings using DNA extracted from vessels that were harvested under surgically aseptic conditions and snap frozen. DNA samples extracted from 11 surgically sterile temporal arteries and 31 surgically sterile thoracic aortas were used in an attempt to identify the vessel-associated VZV genome. Two different validated PCR methods were used. Thirty-one thoracic aorta aneurysm specimens included biopsies from 8 patients with GCA, 2 from patients with TAK, 6 from patients with FIA, and 15 from patients without vasculitis, who had non-inflammatory aneurysms. Eleven temporal artery biopsies were collected from 5 patients with GCA and 6 controls. The presence of VZV was not identified in either the specimens from patients with large vessel vasculitis or from the controls. Using surgically sterile snap-frozen specimens, we were unable to confirm recent reports of the presence of VZV in either aortas or temporal arteries from patients with large vessel vasculitis or controls.

Varicella Zoster Virus and Large Vessel Vasculitis, the Absence of an Association

PubMed Central

Procop, Gary W.; Eng, Charis; Clifford, Alison; Villa-Forte, Alexandra; Calabrese, Leonard H.; Roselli, Eric; Svensson, Lars; Johnston, Douglas; Pettersson, Gosta; Soltesz, Edward; Lystad, Lisa; Perry, Julian D.; Blandford, Alexander; Wilson, Deborah A.; Hoffman, Gary S.

2017-01-01

Objective It is controversial whether microorganisms play a role in the pathogenesis of large and medium vessel vasculitides (eg, giant cell arteritis [GCA], Takayasu arteritis [TAK] and focal idiopathic aortitis [FIA]). Recent studies have reported the presence of Varicella Zoster Virus (VZV) within formalin-fixed, paraffin-embedded temporal arteries and aortas of about three-quarters or more of patients with these conditions, and in a minority of controls. In a prospective study, we sought to confirm these findings using DNA extracted from vessels that were harvested under surgically aseptic conditions and snap frozen. Methods and Results DNA samples extracted from 11 surgically sterile temporal arteries and 31 surgically sterile thoracic aortas were used in an attempt to identify the vessel-associated VZV genome. Two different validated PCR methods were used. Thirty-one thoracic aorta aneurysm specimens included biopsies from 8 patients with GCA, 2 from patients with TAK, 6 from patients with FIA, and 15 from patients without vasculitis, who had non-inflammatory aneurysms. Eleven temporal artery biopsies were collected from 5 patients with GCA and 6 controls. The presence of VZV was not identified in either the specimens from patients with large vessel vasculitis or from the controls. Conclusions Using surgically sterile snap-frozen specimens, we were unable to confirm recent reports of the presence of VZV in either aortas or temporal arteries from patients with large vessel vasculitis or controls. PMID:28758156

FIA Estimation in the New Millennium

Treesearch

Francis A. Roesch

2001-01-01

In the new millennium, Forest Inventory and Analysis (FIA) will deliver most of its database information directly to the users over the Internet. This assumption indicates the need for a GIS-based estimation system to support the information delivery system. Presumably, as the data set evolves, it will free FIA and the users from exclusive estimation within political...

Overview of the National Inventory and Monitoring Applications Center (NIMAC)

Treesearch

Charles T. Scott

2009-01-01

The National Inventory and Monitoring Applications Center (NIMAC) was created by the Forest Inventory and Analysis (FIA) program in 2006. NIMAC addresses a growing need, expressed by FIA partners, for technical assistance in designing and implementing monitoring plans for forests at scales finer than that provided by the FIA standard inventory. NIMAC's goal is to...

Estimating number and size of forest patches from FIA plot data

Treesearch

Mark D. Nelson; Andrew J. Lister; Mark H. Hansen

2009-01-01

Forest inventory and analysis (FIA) annual plot data provide for estimates of forest area, type, volume, growth, and other attributes. Estimates of forest landscape metrics, such as those describing abundance, size, and shape of forest patches, however, typically are not derived from FIA plot data but from satellite image-based land cover maps. Associating image-based...

Combining FIA plot data with topographic variables: Are precise locations needed?

Treesearch

Stephen P. Prisley; Huei-Jin Wang; Philip J Radtke; John Coulston

2009-01-01

Plot data from the USFS FIA program could be combined with terrain variables to attempt to explain how terrain characteristics influence forest growth, species composition, productivity, fire behavior, wildlife habitat, and other phenomena. While some types of analyses using FIA data have been shown to be insensitive to precision of plot locations, it has been...

The hexagon/panel system for selecting FIA plots under an annual inventory

Treesearch

Gary J. Brand; Mark D. Nelson; Daniel G. Wendt; Kevin K. Nimerfro

2000-01-01

Forest Inventory and Analysis (FIA) is changing to an annual nationwide forest inventory. This paper describes the sampling grid used to distribute FIA plots across the landscape and to allocate them to a particular measurement year. We also describe the integration of the F1A and Forest Health Monitoring (FHM) plot networks.

Forests of Maryland, 2016

Treesearch

Tonya W. Lister

2017-01-01

This publication provides an overview of forest resources in Maryland based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. From 2004-2013, FIA employed an annual inventory measuring data on 20 percent of all sample plots each year in Maryland. Beginning in 2014, FIA is on a 7-year cycle...

Forests of Maryland, 2015

Treesearch

Tonya Lister; Richard Widmann

2016-01-01

This publication provides an overview of forest resources in Maryland based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. From 2004-2013, FIA employed an annual inventory, measuring 20 percent of all sample plots each year in Maryland. Beginning in 2014, FIA is on a 7-year cycle,...

Landsat TM Classifications For SAFIS Using FIA Field Plots

Treesearch

William H. Cooke; Andrew J. Hartsell

2001-01-01

Wall-to-wall Landsat Thematic Mapper (TM) classification efforts in Georgia require field validation. We developed a new crown modeling procedure based on Forest Health Monitoring (FHM) data to test Forest Inventory and Analysis (FIA) data. These models simulate the proportion of tree crowns that reflect light on a FIA subplot basis. We averaged subplot crown...

Southern forest inventory and analysis volume equation user’s guide

Treesearch

Christopher M. Oswalt; Roger C. Conner

2011-01-01

Reliable volume estimation procedures are fundamental to the mission of the Forest Inventory and Analysis (FIA) program. Moreover, public access to FIA program procedures is imperative. Here we present the volume estimation procedures used by the southern FIA program of the U.S. Department of Agriculture Forest Service Southern Research Station. The guide presented...

Forests of New York, 2016

Treesearch

Thomas A. Albright; Anthony C. Olsen

2017-01-01

This resource update provides an overview of the forest resources in New York based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly.1Information about the national and regional FIA...

Forests of Maryland, 2014

Treesearch

T.W. Lister; R.H. Widmann

2015-01-01

This publication provides an overview of forest resources in Maryland based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. From 2004-2013, FIA employed an annual inventory measuring data on 20 percent of all sample plots each year in Maryland. Beginning in 2014, FIA is on a 7-year cycle...

On FIA Variables For Ecological Use

Treesearch

David C. Chojnacky

2001-01-01

The Forest Inventory and Analysis (FIA) program collects or calculates over 300 variables for its national network of permanent forest plots. However, considerable ecological analysis can be done with only a few key variables. Two examples--Mexican spotted owl habitat in New Mexico and down deadwood in Maine--are used to illustrate the potential of FIA data for...

Moving from status to trends: Forest Inventory and Analysis (FIA) symposium 2012

Treesearch

Randall S. Morin; Greg C. Liknes

2012-01-01

These proceedings report invited presentations and contributions to the 2012 biennial Forest Inventory and Analysis (FIA) Symposium, which was hosted by the Research and Development branch of the U.S. Forest Service. As the only comprehensive and continuous census of the forests in the United States, FIA provides strategic information needed to evaluate sustainability...

Regression and Geostatistical Techniques: Considerations and Observations from Experiences in NE-FIA

Treesearch

Rachel Riemann; Andrew Lister

2005-01-01

Maps of forest variables improve our understanding of the forest resource by allowing us to view and analyze it spatially. The USDA Forest Service's Northeastern Forest Inventory and Analysis unit (NE-FIA) has used geostatistical techniques, particularly stochastic simulation, to produce maps and spatial data sets of FIA variables. That work underscores the...

Summary of mortality statistics and forest health monitoring results for the Northeastern United States

Treesearch

William H. McWilliams; Stanford L. Arner; Charles J. Barnett

1997-01-01

The USDA Forest Service's Forest Inventory and Analysis (FIA) program and the Forest Health Monitoring (FHM) program maintain networks of sample locations providing coarse-scale information that characterize general indicators of forest health. Tree mortality is the primary FIA variable for analyzing forest health. Recent FIA inventories of New York, Pennsylvania...

Regional differences in vitamin D levels and incidence of food-induced anaphylaxis in South Korea.

PubMed

Kim, Si-Heon; Ban, Ga-Young; Park, Hae-Sim; Kim, Su-chin; Ye, Young-Min

2016-03-01

Previous studies have suggested low vitamin D as a potential risk factor for food allergy/anaphylaxis. However, few studies have investigated the association between vitamin D and food-induced anaphylaxis (FIA) in South Korea. To examine regional differences in serum vitamin D levels and FIA incidence. We used nationwide data collected from 2011 to 2013. Data on vitamin D were obtained from the Korea National Health and Nutrition Examination Survey; data on FIA were obtained from the Health Insurance and Assessment Service. Districts were grouped into region 1 (lower solar radiation) and region 2 (higher solar radiation). We examined differences in FIA incidence and vitamin D levels between the regions, adjusting for age. The study included 2,814 patients with FIA and 15,367 people with available serum vitamin D measurements. Age-adjusted FIA incidence was 2.2 per 100,000 person-years in region 1 and 1.8 per 100,000 person-years in region 2 (relative risk, 1.23; 95% confidence interval, 1.09-1.39). Age-adjusted serum vitamin D levels were 16.5 ng/mL in region 1 and 17.8 ng/mL in region 2 (mean difference, 1.3 ng/mL; 95% confidence interval, 0.9-1.9). After stratification by age, sex, and area of residence, region 1 still had higher FIA incidence and lower vitamin D levels than region 2. The present study found a higher incidence of FIA in regions with lower vitamin D levels in the population. Further investigation is necessary to identify any direct associations between vitamin D and food allergy/anaphylaxis. Copyright © 2016 American College of Allergy, Asthma & Immunology. Published by Elsevier Inc. All rights reserved.

An evaluation of the properties of the variance estimator used by FIA

Treesearch

John P. Brown; James A. Westfall

2012-01-01

The Forest Inventory and Analysis (FIA) program of the U.S. Forest Service currently conducts inventories utilizing the protocols of the national enhanced FIA Program. Due to the permanent locations of the sample plots, the stratification of the population occurs after the selection of sample units, i.e., post-stratification. In situations where the population is of...

The National Inventory of Down Woody Materials: Methods, Outputs, and Future Directions

Treesearch

Christopher W. Woodall

2003-01-01

The Forest Inventory and Analysis Program (FIA) of the USDA Forest Service conducts a national inventory of forests of the United States. A subset of FIA permanent inventory plots are sampled every year for numerous forest health indicators ranging fiom soils to understory vegetation. Down woody material (DWM) is an FIA indicator that refines estimation of forest...

Estimating and circumventing the effects of perturbing and swapping inventory plot locations

Treesearch

Ronald E. McRoberts; Geoffrey R. Holden; Mark D. Nelson; Greg C. Liknes; Warren K. Moser; Andrew J. Lister; Susan L. King; Elizabeth B. LaPoint; John W. Coulston; W. Brad Smith; Gregory A. Reams

2005-01-01

The Forest Inventory and Analysis (FIA) program of the USDA Forest Service reports data and information about the Nation's forest resources. Increasingly, users request that FIA data and information be reported and distributed in a geospatial context, and they request access to exact plot locations for their own analyses. However, the FIA program is constrained by...

An overview of inventory and monitoring and the Role of FIA in National Assessments

Treesearch

W. Brad Smith

2006-01-01

This paper presents a brief conceptual overview of inventory and monitoring and the role of the Forest Inventory and Analysis (FIA) program in national assessments. FIA has become a focal point of national inventory and monitoring and kept national leadership as well as forest resource research and management professionals apprised, through periodic reports to Congress...

Forest Inventory and Analysis (FIA) Symposium 2008; October 21-23, 2008; Park City, UT

Treesearch

Will McWilliams; Gretchen Moisen; Ray Czaplewski

2009-01-01

These proceedings report invited presentations and contributions to the 2008 Biennial Forest Inventory and Analysis (FIA) Symposia, which was hosted by the Research and Development branch of the U.S. Forest Service. As the only comprehensive and continuous census of the forests in the USA, FIA provides strategic information needed to evaluate sustainability of current...

Variable Selection Strategies for Small-area Estimation Using FIA Plots and Remotely Sensed Data

Treesearch

Andrew Lister; Rachel Riemann; James Westfall; Mike Hoppus

2005-01-01

The USDA Forest Service's Forest Inventory and Analysis (FIA) unit maintains a network of tens of thousands of georeferenced forest inventory plots distributed across the United States. Data collected on these plots include direct measurements of tree diameter and height and other variables. We present a technique by which FIA plot data and coregistered...

FIA BioSum: a tool to evaluate financial costs, opportunities and effectiveness of fuel treatments.

Treesearch

Jeremy Fried; Glenn Christensen

2004-01-01

FIA BioSum, a tool developed by the USDA Forest Services Forest Inventory and Analysis (FIA) Program, generates reliable cost estimates, identifies opportunities and evaluates the effectiveness of fuel treatments in forested landscapes. BioSum is an analytic framework that integrates a suite of widely used computer models with a foundation of attribute-rich,...

Northeastern FIA Tree Taper Study: Current Status and Future Work

Treesearch

James A. Westfall; Charles T. Scott

2005-01-01

The northeastern unit of the Forest Inventory and Analysis program (NE-FIA) is engaged in an ongoing project to develop regionwide tree taper equations. Sampling intensity is based on NE-FIA plot data and is stratified by species, diameter class, and height class. To date, modeling research has been aimed largely at evaluating existing model forms (and hybrids thereof...

The Application of FIA-based Data to Wildlife Habitat Modeling: A Comparative Study

Treesearch

Thomas C., Jr. Edwards; Gretchen G. Moisen; Tracey S. Frescino; Randall J. Schultz

2005-01-01

We evaluated the capability of two types of models, one based on spatially explicit variables derived from FIA data and one using so-called traditional habitat evaluation methods, for predicting the presence of cavity-nesting bird habitat in Fishlake National Forest, Utah. Both models performed equally well, in measures of predictive accuracy, with the FIA-based model...

Impact of Definitions of FIA Variables and Compilation Procedures on Inventory Compilation Results in Georgia

Treesearch

Brock Stewart; Chris J. Cieszewski; Michal Zasada

2005-01-01

This paper presents a sensitivity analysis of the impact of various definitions and inclusions of different variables in the Forest Inventory and Analysis (FIA) inventory on data compilation results. FIA manuals have been changing recently to make the inventory consistent between all the States. Our analysis demonstrates the importance (or insignificance) of different...

Development of carbon response trajectories using FIA plot data and FVS growth simulator: challenges of a large scale simulation project

Treesearch

James B. McCarter; Sean Healey

2015-01-01

The Forest Carbon Management Framework (ForCaMF) integrates Forest Inventory and Analysis (FIA) plot inventory data, disturbance histories, and carbon response trajectories to develop estimates of disturbance and management effects on carbon pools for the National Forest System. All appropriate FIA inventory plots are simulated using the Forest Vegetation Simulator (...

A statistically valid method for using FIA plots to guide spectral class rejection in producing stratification maps

Treesearch

Michael L. Hoppus; Andrew J. Lister

2002-01-01

A Landsat TM classification method (iterative guided spectral class rejection) produced a forest cover map of southern West Virginia that provided the stratification layer for producing estimates of timberland area from Forest Service FIA ground plots using a stratified sampling technique. These same high quality and expensive FIA ground plots provided ground reference...

Measuring Forest Area Loss Over Time Using FIA Plots and Satellite Imagery

Treesearch

Michael L. Hoppus; Andrew J. Lister

2005-01-01

How accurately can FIA plots, scattered at 1 per 6,000 acres, identify often rare forest land loss, estimated at less than 1 percent per year in the Northeast? Here we explore this question mathematically, empirically, and by comparing FIA plot estimates of forest change with satellite image based maps of forest loss. The mathematical probability of exactly estimating...

Pushing boundaries: new directions in inventory techniques and applications: Forest Inventory and Analysis (FIA) symposium 2015

Treesearch

Sharon M. Stanton; Glenn A. Christensen

2016-01-01

These proceedings report invited presentations and contributions to the 2015 Forest Inventory and Analysis (FIA) Symposium, which was hosted by the Research and Development branch of the U.S. Forest Service. As the only comprehensive and continuous census of the forests in the United States, FIA provides strategic information needed to evaluate sustainability of...

Comparison of Programs Used for FIA Inventory Information Dissemination and Spatial Representation

Treesearch

Roger C. Lowe; Chris J. Cieszewski

2005-01-01

Six online applications developed for the interactive display of Forest Inventory and Analysis (FIA) data in which FIA database information and query results can be viewed as or selected from interactive geographic maps are compared. The programs evaluated are the U.S. Department of Agriculture Forest Service?s online systems; a SAS server-based mapping system...

Calibration of the STEMS diameter growth model using FIA data

Treesearch

Veronica C. Lessard

2000-01-01

The diameter growth model used in STEMS, the Stand and Tree Evaluation and Modeling System, was originally calibrated using data from permanent growth plots in Minnesota, Wisconsin, and Michigan. Because the model has been applied in predicting growth using Forest Inventory and Analysis (FIA) data, it was appropriate to refit the model to FIA data. The model was...

Efficiency and precision for estimating timber and non-timber attributes using Landsat-based stratification methods in two-phase sampling in northwest California

Treesearch

Antti T. Kaartinen; Jeremy S. Fried; Paul A. Dunham

2002-01-01

Three Landsat TM-based GIS layers were evaluated as alternatives to conventional, photointerpretation-based stratification of FIA field plots. Estimates for timberland area, timber volume, and volume of down wood were calculated for California's North Coast Survey Unit of 2.5 million hectares. The estimates were compared on the basis of standard errors,...

An assessment of the impact of FIA's default assumptions on the estimates of coarse woody debris volume and biomass

Treesearch

Vicente J. Monleon

2009-01-01

Currently, Forest Inventory and Analysis estimation procedures use Smalian's formula to compute coarse woody debris (CWD) volume and assume that logs lie horizontally on the ground. In this paper, the impact of those assumptions on volume and biomass estimates is assessed using 7 years of Oregon's Phase 2 data. Estimates of log volume computed using Smalian...

Estimators used in the New Mexico inventory: practical implications of "truly" random nonresponse within each stratum

Treesearch

Paul L. Patterson; Sara A. Goeking

2012-01-01

The annual forest inventory of New Mexico began as an accelerated inventory, and 8 of the 10 Phase 2 panels were sampled between 2008 and 2011. The inventory includes a large proportion of nonresponse. FIA's estimation process uses post-stratification and assumes that nonresponse occurs at random within each stratum. We construct an estimator for the New Mexico...

Testing of Lithium-Sulfur Dioxide Cells for Waste Disposal Hazards.

DTIC Science & Technology

1980-10-01

r AD-AO90 785 WAPORA INC CHEVY CHASE NO F/G 10/3 TESTING OF LITHIUM-SULFUR DIOXIDE CELLS FOR WASTE DISPOSAL HAZA-ETC(U) OCT 80 D B BOIES OAAK20-79-C... TESTING ION T HUM -SUFU DIXD-EL ORWSEDSOA Daved B. pBli else 69stributonsi nlmied.e OCTOBELE198 Fia PRepr for Peio OCT 23198008 STRYUIO AELETOISRSA...34 cell Toxic waste Sulfur dioxide vapor pressure Structural Integrity Test Ignitable waste Extraction procedure results Corrosive waste ftactive waste

Extending and Intensifying the FIA Inventory of Down Forest Fuels: Boundary Waters Canoe Area and Pictured Rocks National Lakeshore

Treesearch

Christopher W. Woodall; Bruce Leutscher

2005-01-01

The sampling design for the Forest Inventory and Analysis (FIA) program of the U.S. Department of Agriculture Forest Service allows intensification of fuel inventory sampling in areas of ?special interest? and implementation of fuel sampling protocol by non-FIA personnel. The objective of this study is to evaluate the contribution of sampling intensification/extension...

A GIS-based tool for estimating tree canopy cover on fixed-radius plots using high-resolution aerial imagery

Treesearch

Sara A. Goeking; Greg C. Liknes; Erik Lindblom; John Chase; Dennis M. Jacobs; Robert. Benton

2012-01-01

Recent changes to the Forest Inventory and Analysis (FIA) Program's definition of forest land precipitated the development of a geographic information system (GIS)-based tool for efficiently estimating tree canopy cover for all FIA plots. The FIA definition of forest land has shifted from a density-related criterion based on stocking to a 10 percent tree canopy...

A diameter growth model for the SRS FIA

Treesearch

David Gartner

2015-01-01

Changes in the national Forest Inventory and Analysis (FIA) processing system required the Southern Research Station’s FIA unit to create a diameter growth model to estimate the growth of trees that could not be measured at both ends of a measurement interval. Examples of such trees are trees that have died or been harvested, and trees that grow over the minimum...

Austin's urban FIA: seamless rural to urban resource monitoring in Texas

Treesearch

Chris Edgar; Burl Carraway

2015-01-01

In 2014 Urban Forest Inventory and Analysis (Urban-FIA) was implemented for the first time ever in Austin, Texas. Work was accelerated and a full complement of plots in the city was measured in six months. In 2015 results are to be released in an FIA report and data made available in a publicly accessible database. In this presentation we discuss the importance of...

Improving FIA trend analysis through model-based estimation using landsat disturbance maps and the forest vegetation simulator

Treesearch

Sean P. Healey; Gretchen G. Moisen; Paul L. Patterson

2012-01-01

The Forest Inventory and Analysis (FIA) Program's panel system, in which 10-20 percent of the sample is measured in any given year, is designed to increase the currency of FIA reporting and its sensitivity to factors operating at relatively fine temporal scales. Now that much of the country has completed at least one measurement cycle over all panels, there is an...

A national analytical quality assurance program: Developing guidelines and analytical tools for the forest inventory and analysis program

Treesearch

Phyllis C. Adams; Glenn A. Christensen

2012-01-01

A rigorous quality assurance (QA) process assures that the data and information provided by the Forest Inventory and Analysis (FIA) program meet the highest possible standards of precision, completeness, representativeness, comparability, and accuracy. FIA relies on its analysts to check the final data quality prior to release of a State’s data to the national FIA...

The evolution of Wisconsin's urban FIA program—yesterday today and tomorrow

Treesearch

Andrew M. Stoltman; Richard B. Rideout

2015-01-01

In 2002, Wisconsin was part of two pilot projects in cooperation with the US Forest Service. The first was a street tree assessment, and the second was an urban FIA project. The data generated by these pilots changed the way that Wisconsin DNRs’ Urban Forestry Program conducts its business. Although there have been several urban FIA pilot projects throughout the U.S.,...

Predictability of Seasonal Rainfall over the Greater Horn of Africa

NASA Astrophysics Data System (ADS)

Ngaina, J. N.

2016-12-01

The El Nino-Southern Oscillation (ENSO) is a primary mode of climate variability in the Greater of Africa (GHA). The expected impacts of climate variability and change on water, agriculture, and food resources in GHA underscore the importance of reliable and accurate seasonal climate predictions. The study evaluated different model selection criteria which included the Coefficient of determination (R2), Akaike's Information Criterion (AIC), Bayesian Information Criterion (BIC), and the Fisher information approximation (FIA). A forecast scheme based on the optimal model was developed to predict the October-November-December (OND) and March-April-May (MAM) rainfall. The predictability of GHA rainfall based on ENSO was quantified based on composite analysis, correlations and contingency tables. A test for field-significance considering the properties of finiteness and interdependence of the spatial grid was applied to avoid correlations by chance. The study identified FIA as the optimal model selection criterion. However, complex model selection criteria (FIA followed by BIC) performed better compared to simple approach (R2 and AIC). Notably, operational seasonal rainfall predictions over the GHA makes of simple model selection procedures e.g. R2. Rainfall is modestly predictable based on ENSO during OND and MAM seasons. El Nino typically leads to wetter conditions during OND and drier conditions during MAM. The correlations of ENSO indices with rainfall are statistically significant for OND and MAM seasons. Analysis based on contingency tables shows higher predictability of OND rainfall with the use of ENSO indices derived from the Pacific and Indian Oceans sea surfaces showing significant improvement during OND season. The predictability based on ENSO for OND rainfall is robust on a decadal scale compared to MAM. An ENSO-based scheme based on an optimal model selection criterion can thus provide skillful rainfall predictions over GHA. This study concludes that the negative phase of ENSO (La Niña) leads to dry conditions while the positive phase of ENSO (El Niño) anticipates enhanced wet conditions

Average Stand Age from Forest Inventory Plots Does Not Describe Historical Fire Regimes in Ponderosa Pine and Mixed-Conifer Forests of Western North America.

PubMed

Stevens, Jens T; Safford, Hugh D; North, Malcolm P; Fried, Jeremy S; Gray, Andrew N; Brown, Peter M; Dolanc, Christopher R; Dobrowski, Solomon Z; Falk, Donald A; Farris, Calvin A; Franklin, Jerry F; Fulé, Peter Z; Hagmann, R Keala; Knapp, Eric E; Miller, Jay D; Smith, Douglas F; Swetnam, Thomas W; Taylor, Alan H

Quantifying historical fire regimes provides important information for managing contemporary forests. Historical fire frequency and severity can be estimated using several methods; each method has strengths and weaknesses and presents challenges for interpretation and verification. Recent efforts to quantify the timing of historical high-severity fire events in forests of western North America have assumed that the "stand age" variable from the US Forest Service Forest Inventory and Analysis (FIA) program reflects the timing of historical high-severity (i.e. stand-replacing) fire in ponderosa pine and mixed-conifer forests. To test this assumption, we re-analyze the dataset used in a previous analysis, and compare information from fire history records with information from co-located FIA plots. We demonstrate that 1) the FIA stand age variable does not reflect the large range of individual tree ages in the FIA plots: older trees comprised more than 10% of pre-stand age basal area in 58% of plots analyzed and more than 30% of pre-stand age basal area in 32% of plots, and 2) recruitment events are not necessarily related to high-severity fire occurrence. Because the FIA stand age variable is estimated from a sample of tree ages within the tree size class containing a plurality of canopy trees in the plot, it does not necessarily include the oldest trees, especially in uneven-aged stands. Thus, the FIA stand age variable does not indicate whether the trees in the predominant size class established in response to severe fire, or established during the absence of fire. FIA stand age was not designed to measure the time since a stand-replacing disturbance. Quantification of historical "mixed-severity" fire regimes must be explicit about the spatial scale of high-severity fire effects, which is not possible using FIA stand age data.

Average Stand Age from Forest Inventory Plots Does Not Describe Historical Fire Regimes in Ponderosa Pine and Mixed-Conifer Forests of Western North America

PubMed Central

Stevens, Jens T.; Safford, Hugh D.; North, Malcolm P.; Fried, Jeremy S.; Gray, Andrew N.; Brown, Peter M.; Dolanc, Christopher R.; Dobrowski, Solomon Z.; Falk, Donald A.; Farris, Calvin A.; Franklin, Jerry F.; Fulé, Peter Z.; Hagmann, R. Keala; Knapp, Eric E.; Miller, Jay D.; Smith, Douglas F.; Swetnam, Thomas W.; Taylor, Alan H.

2016-01-01

Quantifying historical fire regimes provides important information for managing contemporary forests. Historical fire frequency and severity can be estimated using several methods; each method has strengths and weaknesses and presents challenges for interpretation and verification. Recent efforts to quantify the timing of historical high-severity fire events in forests of western North America have assumed that the “stand age” variable from the US Forest Service Forest Inventory and Analysis (FIA) program reflects the timing of historical high-severity (i.e. stand-replacing) fire in ponderosa pine and mixed-conifer forests. To test this assumption, we re-analyze the dataset used in a previous analysis, and compare information from fire history records with information from co-located FIA plots. We demonstrate that 1) the FIA stand age variable does not reflect the large range of individual tree ages in the FIA plots: older trees comprised more than 10% of pre-stand age basal area in 58% of plots analyzed and more than 30% of pre-stand age basal area in 32% of plots, and 2) recruitment events are not necessarily related to high-severity fire occurrence. Because the FIA stand age variable is estimated from a sample of tree ages within the tree size class containing a plurality of canopy trees in the plot, it does not necessarily include the oldest trees, especially in uneven-aged stands. Thus, the FIA stand age variable does not indicate whether the trees in the predominant size class established in response to severe fire, or established during the absence of fire. FIA stand age was not designed to measure the time since a stand-replacing disturbance. Quantification of historical “mixed-severity” fire regimes must be explicit about the spatial scale of high-severity fire effects, which is not possible using FIA stand age data. PMID:27196621

Interpreting whether isoclinal folds are antiforms or synforms using FIA succession

NASA Astrophysics Data System (ADS)

Cao, H.

2012-12-01

Using the asymmetries of the overprinting foliations preserved as inclusion trails that define the FIAs to investigate whether an enigmatic isoclinal fold in the region is an antiform or synform. This approach also reveals when the fold first formed during the tectonic history of the region. Multiply deformed and isoclinally folded interlayered high metamorphic grade gneisses and schists can be very difficult rocks for resolving early formed stratigraphic and structural relationships. When such rocks contain porphyroblasts a new approach is possible because of the way in which porphyroblast growth is affected by crenulation versus reactivation of compositional layering (Bell et al., 2003). Isoclinally folded rocks in the Arkansas River region of South Central Colorado contain relics of fold hinges that have been very difficult to ascertain whether they are antiforms or synforms because of younger refolding effects and the locally truncated nature of coarse compositional layering. With the realization that rocks with a schistosity parallel to bedding (S0 parallel S1) have undergone lengthy histories of deformation that predate the obvious first deformation (e.g. Bell et al., 2003; Sayab, 2006; Yeh, 2007) came recognition that large scale regional folds can form early during this process and be preserved throughout orogenesis (e.g., Ham and Bell, 2004; Bell and Newman, 2006. This extensive history is lost within the matrix because of reactivational shear on the compositional layering (Bell et al., 1998, 2003, 2004, 2005; Ham and Bell, 2004). However, it can be extracted by measuring FIAs. Recent work using this approach has revealed that the trends of axial planes of all map scale folds, when plotted on a rose diagram, strikingly reflect the FIA trends (e.g., Sanislav, 2009; Shah, 2009). That is, although it was demonstrated by Bell et al. (2003) that the largest scale regional folds commonly form early in the total history, other folds can form and be preserved from subsequent destruction in the strain shadows of plutons or through the partitioning of deformation due to heterogeneities at depth.

An assessment of invasive plant species monitored by the Northern Research Station Forest Inventory and Analysis Program, 2005 through 2010

Treesearch

Cassandra M. Kurtz

2013-01-01

Invasive plant species are a worldwide concern due to the high ecological and economic costs associated with their presence. This document describes the plant characteristics and regional distribution of the 50 invasive plant species monitored from 2005 through 2010 on forested Phase 2 (P2) Forest Inventory and Analysis (FIA) plots in the 24 states of the Northern...

Utility of tree crown condition indicators to predict tree survival using remeasured Forest Inventory and Analysis data

Treesearch

Randall S. Morin; Jim Steinman; KaDonna C. Randolph

2012-01-01

The condition of tree crowns is an important indicator of tree and forest health. Crown conditions have been evaluated during surveys of Forest Inventory and Analysis (FIA) Phase 3 (P3) plots since 1999. In this study, remeasured data from 39,357 trees in the northern United States were used to assess the probability of survival among various tree species using the...

Evaluating elevated levels of crown dieback among northern white-cedar (Thuja occidentalis L.) trees in Maine and Michigan: a summary of evaluation monitoring

Treesearch

KaDonna Randolph; William A. Bechtold; Randall S. Morin; Stanley J. Zarnoch

2012-01-01

Analysis of crown condition data for the 2006 national technical report of the Forest Health Monitoring (FHM) Program of the Forest Service, U.S. Department of Agriculture, exposed clusters of phase 3 plots (by the Forest Inventory and Analysis [FIA] Program of the Forest Service) with northern white-cedar (Thuja occidentalis L.) crown dieback...

Determination of glutamine and glutamic acid in mammalian cell cultures using tetrathiafulvalene modified enzyme electrodes.

PubMed

Mulchandani, A; Bassi, A S

1996-01-01

Tetrathiafulvalene (TTF) mediated amperometric enzyme electrodes have been developed for the monitoring of L-glutamine and L-glutamic acid in growing mammalian cell cultures. The detection of glutamine was accomplished by a coupled enzyme system comprised of glutaminase plus glutamate oxidase, while the detection of glutamic acid was carried out by a single enzyme, glutamate oxidase. The appropriate enzyme(s) were immoblized on the Triton-X treated surface of tetrathiafulvalene modified carbon paste electrodes by adsorption, in conjunction with entrapment by an electrochemically deposited copolymer film of 1,3-phenylenediamine and resorcinol. Operating conditions for the glutamine enzyme electrode were optimized with respect to the amount of enzymes immoblized, pH, temperature and mobile phase flow rate for operation in a flow injection (FIA) system. When applied to glutamine and glutamic acid measurements in mammalian cell culture in FIA, the results obtained with enzyme electrodes were in excellent agreement with those determined by enzymatic analysis.

Doing more with the core: Proceedings of the 2017 Forest Inventory and Analysis (FIA) Science Stakeholder Meeting; 2017 October 24- 26; Park City, UT

Treesearch

Sean P. Healey; Vicki M. Berrett

2017-01-01

The Forest Service’s Forest Inventory and Analysis Program (FIA) is the primary source of information about our forests’ status and trends. A network of nationally consistent field observations forms FIA’s core, and active collaboration with clients and peer organizations ensures that the resulting inventory remains agile, comprehensive, and relevant. An FIA Science...

Development of a Highly Specific Fluorescence Immunoassay for Detection of Diisobutyl Phthalate in Edible Oil Samples.

PubMed

Cui, Xiping; Wu, Panpan; Lai, Dan; Zheng, Shengwu; Chen, Yingshan; Eremin, Sergei A; Peng, Wei; Zhao, Suqing

2015-10-28

The diisobutyl phthalate (DiBP) hapten containing an amino group was synthesized successfully, and the polyclonal antibody against 4-amino phthalate-bovine serum albumin (BSA) was developed. On the basis of the polyclonal antibody, a rapid and sensitive indirect competitive fluorescence immunoassay (icFIA) has been established to detect DiBP in edible oil samples for the first time. Under the optimized conditions, the quantitative working range of the icFIA was from 10.47 to 357.06 ng/mL (R(2) = 0.991), exhibiting a detection limit of 5.82 ng/mL. In this assay, the specific results showed that other similar phthalates did not significantly interfere with the analysis, with the cross-reactivity less than 1.5%, except for that of DiBAP. Thereafter, DiBP contamination in edible oil samples was detected by icFIA, with the recovery being from 79 to 103%. Furthermore, the reliability of icFIA was validated by gas chromatography-mass spectrometry (GC-MS). Therefore, the developed icFIA is suitable for monitoring DiBP in some edible oil samples.

Effect of lipoarabinomannan from Mycobacterium avium subsp avium in Freund's incomplete adjuvant on the immune response of cattle.

PubMed

Colavecchia, S B; Jolly, A; Fernández, B; Fontanals, A M; Fernández, E; Mundo, S L

2012-02-01

The aim of the present study was to determine whether lipoarabinomannan (LAM), in combination with Freund's incomplete adjuvant (FIA), was able to improve cell-mediated and antibody-mediated immune responses against ovalbumin (OVA) in cattle. Twenty-three calves were assigned to four treatment groups, which were subcutaneously immunized with either OVA plus FIA, OVA plus FIA and LAM from Mycobacterium avium subsp avium, FIA plus LAM, or FIA alone. Lymphoproliferation, IFN-γ production and cell subpopulations on peripheral blood mononuclear cells before and 15 days after treatment were evaluated. Delayed hypersensitivity was evaluated on day 57. Specific humoral immune response was measured by ELISA. Inoculation with LAM induced higher levels of lymphoproliferation and IFN-γ production in response to ConA and OVA (P < 0.05). Specific antibody titers were similar in both OVA-immunized groups. Interestingly, our results showed that the use of LAM in vaccine preparations improved specific cell immune response evaluated by lymphoproliferation and IFN-γ production by at least 50 and 25%, respectively, in cattle without interfering with tuberculosis and paratuberculosis diagnosis.

Effect of lipoarabinomannan from Mycobacterium avium subsp avium in Freund's incomplete adjuvant on the immune response of cattle

PubMed Central

Colavecchia, S.B.; Jolly, A.; Fernández, B.; Fontanals, A.M.; Fernández, E.; Mundo, S.L.

2012-01-01

The aim of the present study was to determine whether lipoarabinomannan (LAM), in combination with Freund's incomplete adjuvant (FIA), was able to improve cell-mediated and antibody-mediated immune responses against ovalbumin (OVA) in cattle. Twenty-three calves were assigned to four treatment groups, which were subcutaneously immunized with either OVA plus FIA, OVA plus FIA and LAM from Mycobacterium avium subsp avium, FIA plus LAM, or FIA alone. Lymphoproliferation, IFN-γ production and cell subpopulations on peripheral blood mononuclear cells before and 15 days after treatment were evaluated. Delayed hypersensitivity was evaluated on day 57. Specific humoral immune response was measured by ELISA. Inoculation with LAM induced higher levels of lymphoproliferation and IFN-γ production in response to ConA and OVA (P < 0.05). Specific antibody titers were similar in both OVA-immunized groups. Interestingly, our results showed that the use of LAM in vaccine preparations improved specific cell immune response evaluated by lymphoproliferation and IFN-γ production by at least 50 and 25%, respectively, in cattle without interfering with tuberculosis and paratuberculosis diagnosis. PMID:22286534

Fort Drum Preliminary Fiscal Impact Analysis: Technical Appendices,

DTIC Science & Technology

1986-01-01

the requirements for on-base construction with those for private sector construction. (Private sector construction demand accounts for construction...persons with key construction skills. There will be some phasing in and out of these jobs, which is accounted for in the FIA model. Service Sector The...a nonservice industry accounts for 5 percent of the total production in ,: the ROI and 10 percent of total production in the state, then half of the

Loss of Life, Evacuation and Emergency Management: Comparison and Application to Case Studies in the USA

DTIC Science & Technology

2013-01-22

eK ay a nd M cC le lla nd G ra ha m Katrina HEC -FIA LifeSim Figure 1: Comparison of loss of life models (based on Johnstone et al., 2005...Katrina HEC FIA Lifesim Application: flood types Levee breaching, river , coastal Levee breaching, river , coastal levee breaching, dam failure...Mortality – Overtopping with breach Center Side of American River (OTSC) Figure 31: Mortality for the HEC -FIA method for the two

Application of Forest Inventory and Analysis (FIA) data to estimate the amount of old growth forest and snag density in the Northern Region of the National Forest System

Treesearch

Raymond L. Czaplewski

2004-01-01

This report discusses valid use of data produced by the Forest Service?s Forest Inventory and Analysis (FIA) program and used by the Northern Region of the National Forest System to analyze the compliance of individual National Forests with their Standards and Guidelines. It emphasizes use of FIA data on snag density and the percentage of forest area that meets the...

Interactions of foreign interstitial and substitutional atoms in bcc iron from ab initio calculations

NASA Astrophysics Data System (ADS)

You, Y.; Yan, M. F.

2013-05-01

C and N atoms are the most frequent foreign interstitial atoms (FIAs), and often incorporated into the surface layers of steels to enhance their properties by thermochemical treatments. Al, Si, Ti, V, Cr, Mn, Co, Ni, Cu, Nb and Mo are the most common alloying elements in steels, also can be called foreign substitutional atoms (FSAs). The FIA and FSA interactions play an important role in the diffusion of C and N atoms, and the microstructures and mechanical properties of surface modified layers. Ab initio calculations based on the density functional theory are carried out to investigate FIA interactions with FSA in ferromagnetic bcc iron. The FIA-FSA interactions are analyzed systematically from five aspects, including interaction energies, density of states (DOS), bond populations, electron density difference maps and local magnetic moments.

Evaluation of a new rapid diagnostic test for the detection of influenza and RSV.

PubMed

Gómez, Sara; Prieto, Columbiana; Vera, Carmen; R Otero, Joaquín; Folgueira, Lola

2016-05-01

Influenza viruses and respiratory syncytial virus (RSV) can cause an acute respiratory disease that occurs seasonally in epidemic waves. This retrospective study was conducted to evaluate the Sofia(®) Influenza A+B and the Sofia(®) RSV fluorescence immunoassays (FIAs), two novel rapid detection tests (RDTs) for influenza A and B and RSV. Two hundred and nine breath samples were selected from patients with respiratory symptoms determined to be positive/negative for influenza A, influenza B or RSV using one of the reference diagnostic techniques, cell culture and/or RT-PCR (Simplexa™Flu A/B & RSV). The Sofia Influenza A+B FIA was tested on 123 samples (63 from children and 60 from adults) and the Sofia RSV FIA was tested on 86 pediatric samples. Sensitivity and specificity values of both assays were calculated assuming the reference techniques as the gold standard. Sensitivity and specificity values for the Sofia Influenza A+B FIA were 73.1% and 97.8%, respectively. Sensitivity and specificity values for the Sofia RSV FIA were 87.5% and 86.7%, respectively. The sensitivity results obtained for the two assays were considerably higher than those reported for other RDTs. In conclusion, the Sofia Influenza A+B and the Sofia RSV FIAs are appropriate tools for the rapid diagnosis of these viruses. Copyright © 2015 Elsevier España, S.L.U. y Sociedad Española de Enfermedades Infecciosas y Microbiología Clínica. All rights reserved.

FIA: An Open Forensic Integration Architecture for Composing Digital Evidence

NASA Astrophysics Data System (ADS)

Raghavan, Sriram; Clark, Andrew; Mohay, George

The analysis and value of digital evidence in an investigation has been the domain of discourse in the digital forensic community for several years. While many works have considered different approaches to model digital evidence, a comprehensive understanding of the process of merging different evidence items recovered during a forensic analysis is still a distant dream. With the advent of modern technologies, pro-active measures are integral to keeping abreast of all forms of cyber crimes and attacks. This paper motivates the need to formalize the process of analyzing digital evidence from multiple sources simultaneously. In this paper, we present the forensic integration architecture (FIA) which provides a framework for abstracting the evidence source and storage format information from digital evidence and explores the concept of integrating evidence information from multiple sources. The FIA architecture identifies evidence information from multiple sources that enables an investigator to build theories to reconstruct the past. FIA is hierarchically composed of multiple layers and adopts a technology independent approach. FIA is also open and extensible making it simple to adapt to technological changes. We present a case study using a hypothetical car theft case to demonstrate the concepts and illustrate the value it brings into the field.

Microfluidic Flow Injection Analysis with Thermal Lens Microscopic Detection for Determination of NGAL

NASA Astrophysics Data System (ADS)

Radovanović, Tatjana; Liu, Mingqiang; Likar, Polona; Klemenc, Matjaž; Franko, Mladen

2015-06-01

A combined microfluidic flow injection analysis-thermal lens microscopy (FIA-TLM) system was applied for determination of neutrophil gelatinase-associated lipocalin (NGAL)—a biomarker of acute kidney injury. NGAL was determined following a commercial ELISA assay and transfer of the resulting solution into the FIA-TLM system with a 100 m deep microchannel. At an excitation power of 100 mW, the FIA-TLM provided about seven times lower limits of detection (1.5 pg as compared to a conventional ELISA test, and a sample throughput of six samples per minute, which compares favorably with sample throughput of the microtiter plate reader, which reads 96 wells in about 30 min. Comparison of results for NGAL in plasma samples from healthy individuals and for NGAL dynamics in patients undergoing coronary angiography measured with transmission mode spectrometry on a microtiter plate reader and with FIA-TLM showed good agreement. In addition to improved LOD, the high sensitivity of FIA-TLM offers possibilities of a further reduction of the total reaction time of the NGAL ELISA test by sacrificing some of the sensitivity while reducing the duration of individual incubation steps.

General constraints on sampling wildlife on FIA plots

USGS Publications Warehouse

Bailey, L.L.; Sauer, J.R.; Nichols, J.D.; Geissler, P.H.; McRoberts, Ronald E.; Reams, Gregory A.; Van Deusen, Paul C.; McWilliams, William H.; Cieszewski, Chris J.

2005-01-01

This paper reviews the constraints to sampling wildlife populations at FIA points. Wildlife sampling programs must have well-defined goals and provide information adequate to meet those goals. Investigators should choose a State variable based on information needs and the spatial sampling scale. We discuss estimation-based methods for three State variables: species richness, abundance, and patch occupancy. All methods incorporate two essential sources of variation: detectability estimation and spatial variation. FIA sampling imposes specific space and time criteria that may need to be adjusted to meet local wildlife objectives.

Fluorescence Immunoassay for Cocaine Detection.

PubMed

Nakayama, Hiroshi; Kenjjou, Noriko; Shigetoh, Nobuyuki; Ito, Yuji

2016-04-01

A fluorescence immunoassay (FIA) has been developed for the detection of cocaine using norcocaine labeled with merocyanine dye and a monoclonal antibody specific to cocaine. Using this FIA, the detection range for cocaine was between 20.0 and 1700 μg/L with a limit of detection of 20.0 μg/L. Other cocaine derivatives did not interfere significantly with the detection when using this immunoassay technique with cross-reactivity values of less than 20%. Thus this FIA could be considered a useful tool for the detection of cocaine.

Micro-flow injection system for the urinary protein assay.

PubMed

Nishihama, Syouhei; Imabayashi, Hisano; Matoba, Tomoko; Toya, Chika; Watanabe, Kosuke; Yoshizuka, Kazuharu

2008-02-15

A urinary protein assay has been investigated, employing a micro-flow injection analysis (muFIA) combined with an adsorptive separation of protein from analyte. The adsorptive separation part of protein in the artificial urine with ceramic hydroxyapatite is integrated on the muFIA chip, since the interference of other components coexisting in urine occurs in the conventional FIA system. The typical FI peak can be obtained following the adsorption-elution process of the protein prior to the detection, and the protein concentration in artificial urine can be quantitatively determined.

A multi-scale assessment of forest primary production across the eastern USA using Forest Inventory and Analysis (FIA) and MODIS data

NASA Astrophysics Data System (ADS)

Kwon, Youngsang

As evidence of global warming continues to increase, being able to predict the relationship between forest growth rate and climate factors will be vital to maintain the sustainability and productivity of forests. Comprehensive analyses of forest primary production across the eastern US were conducted using remotely sensed MODIS and field-based FIA datasets. This dissertation primarily explored spatial patterns of gross and net carbon uptake in the eastern USA, and addressed three objectives. 1) Examine the use of pixel- and plot-scale screening variables to validate MODIS GPP predictions with Forest Inventory and Analysis (FIA) NPP measures. 2) Assess the net primary production (NPP) from MODIS and FIA at increasing levels of spatial aggregation using a hexagonal tiling system. 3) Assess the carbon use efficiency (CUE) calculated using a direct ratio of MODIS NPP to MODIS GPP and a standardized ratio of FIA NPP to MODIS GPP. The first objective was analyzed using total of 54,969 MODIS pixels and co-located FIA plots to validate MODIS GPP estimates. Eight SVs were used to test six hypotheses about the conditions under which MODIS GPP would be most strongly validated. SVs were assessed in terms of the tradeoff between improved relations and reduced number of samples. MODIS seasonal variation and FIA tree density were the two most efficient SVs followed by basic quality checks for each data set. The sequential application of SVs provided an efficient dataset of 17,090 co-located MODIS pixels and FIA plots, that raised the Pearson's correlation coefficient from 0.01 for the complete dataset of 54,969 plots to 0.48 for this screened subset of 17,090 plots. The second objective was addressed by aggregating data over increasing spatial extents so as to not lose plot- and pixel-level information. These data were then analyzed to determine the optimal scale with which to represent the spatial pattern of NPP. The results suggested an optimal scale of 390 km2. At that scale MODIS and FIA were most strongly correlated while maximizing the number of observation. The maps conveyed both local-scale spatial structure from FIA and broad-scale climatic trends from MODIS. The third objective examined whether carbon use efficiency (CUE) was constant or variable in relation to forest types, and to geographic and climatic variables. The results indicated that while CUEs exhibited unclear patterns by forest types, CUEs are variable to other environmental variables. CUEs are most strongly related to the climatic factors of precipitation followed by temperature. More complex and weaker relationships were found for the geographic factors of latitude and altitude, as they reflected a combination of phenomenological driving forces. The results of the three objectives will help us to identify factors that control carbon cycles and to quantify forest productivity. This will help improve our knowledge about how forest primary productivity may change in relation to ongoing climate change.

Development of an automated flow injection analysis system for determination of phosphate in nutrient solutions.

PubMed

Karadağ, Sevinç; Görüşük, Emine M; Çetinkaya, Ebru; Deveci, Seda; Dönmez, Koray B; Uncuoğlu, Emre; Doğu, Mustafa

2018-01-25

A fully automated flow injection analysis (FIA) system was developed for determination of phosphate ion in nutrient solutions. This newly developed FIA system is a portable, rapid and sensitive measuring instrument that allows on-line analysis and monitoring of phosphate ion concentration in nutrient solutions. The molybdenum blue method, which is widely used in FIA phosphate analysis, was adapted to the developed FIA system. The method is based on the formation of ammonium Mo(VI) ion by reaction of ammonium molybdate with the phosphate ion present in the medium. The Mo(VI) ion then reacts with ascorbic acid and is reduced to the spectrometrically measurable Mo(V) ion. New software specific for flow analysis was developed in the LabVIEW development environment to control all the components of the FIA system. The important factors affecting the analytical signal were identified as reagent flow rate, injection volume and post-injection flow path length, and they were optimized using Box-Behnken experimental design and response surface methodology. The optimum point for the maximum analytical signal was calculated as 0.50 mL min -1 reagent flow rate, 100 µL sample injection volume and 60 cm post-injection flow path length. The proposed FIA system had a sampling frequency of 100 samples per hour over a linear working range of 3-100 mg L -1 (R 2  = 0.9995). The relative standard deviation (RSD) was 1.09% and the limit of detection (LOD) was 0.34 mg L -1 . Various nutrient solutions from a tomato-growing hydroponic greenhouse were analyzed with the developed FIA system and the results were found to be in good agreement with vanadomolybdate chemical method findings. © 2018 Society of Chemical Industry. © 2018 Society of Chemical Industry.

Utility of Endoanal Ultrasonography in Assessment of Primary and Recurrent Anal Fistulas and for Detection of Associated Anal Sphincter Defects.

PubMed

Emile, Sameh Hany; Magdy, Alaa; Youssef, Mohamed; Thabet, Waleed; Abdelnaby, Mahmoud; Omar, Waleed; Khafagy, Wael

2017-11-01

Tridimensional endoanal ultrasonography (3D-EAUS) has been used for the assessment of various anorectal lesions. Previous studies have reported good accuracy of 3D-EAUS in preoperative assessment of fistula-in-ano (FIA). This study aimed to assess the diagnostic utility of 3D-EAUS in preoperative evaluation of primary and recurrent FIA and its role in detection of associated anal sphincter (AS) defects. Prospectively collected data of patients with FIA who were investigated with 3D-EAUS were reviewed. The findings of EAUS were compared with the intraoperative findings, the reference standard, to find the degree of agreement regarding the position of the internal opening (IO) and primary tract (PT), and presence of secondary tracts using kappa (k) coefficient test. A subgroup analysis was performed to compare the accuracy and sensitivity of EAUS for primary and recurrent FIA. Of the patients, 131 were included to the study. EAUS had an overall accuracy of 87, 88.5, and 89.5% in detection of IO, PT, and AS defects, respectively. There was very good concordance between the findings of EAUS and intraoperative findings for the investigated parameters (kappa = 0.748, 0.83, 0.935), respectively. Accuracy and sensitivity of EAUS in recurrent FIA were insignificantly lower than primary cases. EAUS detected occult AS defects in 5.3% of the patients studied. The diagnostic utility of 3D-EAUS was comparable in primary and recurrent FIA. 3D-EAUS was able to detect symptomatic and occult AS defects with higher accuracy than clinical examination.

Controlled-Release Personal Use Arthropod Repellent Formulation. Phase 3

DTIC Science & Technology

1987-08-26

Polyethylene Glycol (200) Glyceryl Monotallowate (Varonic L1420) 54.2 lbs. Glyceryl Stearate/ Sodium Lauryl Sulfate (Lexemul AS) 129.3 lbs. Propylene... Sulfate 6-0 Xr ________ (Le.ernul AS) - 0.65__ * 13W00 Cetyl Palmitate (W,xenol 816) 2,600 Xg. Ci Zq! 167 2.2___ 10026 Poyproplen Gycol (15) Stenryl...1 Stearate7Sodium lAu 1l Sulfate T- 4fIa- TW _ - ________ Lex emul AS)__________ ____ _______ 2.41 11315 /Prop lene Glycol D1 cap" lateDf~caerate

Loss of Life, Evacuation and Emergency Management - Application of Dutch Models to US Case Studies

DTIC Science & Technology

2012-12-18

Risks to people M es o: Z on e or lo ca tio n Instability tests Jonkman 1953 D eK ay a nd M cC le lla nd G ra ha m Katrina HEC -FIA...mortality functions (Jonkman) o 2.2.2 New Orleans / Katrina mortality functions (Jonkman) o 2.2.3 HEC FIA approach (USACE) o 2.2.4. Loss of life methods...comparison (USACE) • 2.3 Dutch Evacuation and Evacuaid approach (Kolen) o 2.3.1 Evacuation approach implemented in HEC FIA (USACE) o 2.3.2 Evacuation

State of the art in on-line techniques coupled to flow injection analysis FIA/on-line- a critical review

PubMed Central

Puchades, R.; Maquieira, A.; Atienza, J.; Herrero, M. A.

1990-01-01

Flow injection analysis (FIA) has emerged as an increasingly used laboratory tool in chemical analysis. Employment of the technique for on-line sample treatment and on-line measurement in chemical process control is a growing trend. This article reviews the recent applications of FlA. Most papers refer to on-line sample treatment. Although FIA is very well suited to continuous on-line process monitoring, few examples have been found in this areamost of them have been applied to water treatment or fermentation processes. PMID:18925271

Elicitation of macrophages from the peritoneal cavity of channel catfish

USGS Publications Warehouse

Jenkins, J.A.; Klesius, P.H.

1998-01-01

Four chemicals were evaluated for elicitation of macrophages in peritoneal cavities of 250-300g healthy channel catfish Ictalurus punctatus. Cellular exudates were collected at 3, 5, 7, 10, 14, and 20 d following intraperitoneal injections with squalene, Freund's incomplete adjuvant (FIA), goat serum, thioglycollate, or as a control, phosphate-buffered saline. Injection with either squalene or FIA induced significantly greater (P ??? 0.0001) macrophage recruitment than the other chemicals. The effectiveness of squalene and FIA was compared further by macrophage collection daily for 7 d. Squalene and FIA elicited similarly high macrophage responses (P ??? 0.0450), the highest being 3.43 x 106 macrophages/mL (SE, 2.4 x l06) at 99% purity at day 2 and 2.1 X 106 macrophages/mL (SE, 0.7 x 106) at day 14 at 80% purity, respectively. In both experiments, the time after injection was not statistically significant, nor was there an interaction between time and chemicals. The occurrence of cells other than macrophages decreased with time to yield macrophage recoveries of 47-99% for squalene and 30-80% for FIA. Two subsets of macrophages were observed by means of flow cytometry. As demonstrated by chemiluminescence, the squalene-elicited cells produced high-energy oxygen compounds important to the phagocytic process.

Comparison of Sofia Legionella FIA and BinaxNOW® Legionella urinary antigen card in two national reference centers.

PubMed

Beraud, L; Gervasoni, K; Freydiere, A M; Descours, G; Ranc, A G; Vandenesch, F; Lina, G; Gaia, V; Jarraud, S

2015-09-01

The Sofia Legionella Fluorescence Immunoassay (FIA; Quidel) is a recently introduced rapid immunochromatographic diagnostic test for Legionnaires' disease using immunofluorescence technology designed to enhance its sensitivity. The aim of this study was to evaluate its performance for the detection of urinary antigens for Legionella pneumophila serogroup 1 in two National Reference Centers for Legionella. The sensitivity and specificity of the Sofia Legionella FIA test were determined in concentrated and nonconcentrated urine samples, before and after boiling, in comparison with the BinaxNOW® Legionella Urinary Antigen Card (UAC; Alere). Compared with BinaxNOW® Legionella UAC, the sensitivity of the Sofia Legionella test was slightly higher in nonconcentrated urine samples and was identical in concentrated urine samples. The specificity of the Sofia Legionella FIA test was highly reduced by the concentration of urine samples. In nonconcentrated samples, a lack of specificity was observed in 2.3 % of samples, all of them resolved by heat treatment. The Sofia Legionella FIA is a sensitive test for detecting Legionella urinary antigens with no previous urine concentration. However, all positive samples have to be re-tested after boiling to reach a high specificity. The reading is automatized on the Sofia analyzer, which can be connected to laboratory information systems, facilitating accurate and rapid reporting of results.

A profile of Wisconsin's private forest landowers

Treesearch

Earl C. Leatherberry

2000-01-01

In 1997, the USDA Forest Service, & Forest Inventory and Analysis (FIA) Program at the North Central Research Station in St. Paul, Minnesota contacted approximately 3,000 private forest landowners in Wisconsin as part of acomprehensive statewide survey. FIA routinely collects and analyzes forest resources data.

Data bases for forest inventory in the North-Central Region.

Treesearch

Jerold T. Hahn; Mark H. Hansen

1985-01-01

Describes the data collected by the Forest Inventory and Analysis (FIA) Research Work Unit at the North Central Forest Experiment Station. Explains how interested parties may obtain information from the databases either through direct access or by special requests to the FIA database manager.

A profile of Wisconsin''s private forest landowners

Treesearch

Earl C. Leatherberry

2001-01-01

In 1997, the USDA Forest Service, Forest Inventory and Analysis (FIA) Program at the North Central Research Station in St. Paul, Minnesota contacted approximately 3,000 private forest landowners in Wisconsin as part of a comprehensive statewide survey. FIA routinely collects and analyzes forest resources data.

Allometric scaling theory applied to FIA biomass estimation

Treesearch

David C. Chojnacky

2002-01-01

Tree biomass estimates in the Forest Inventory and Analysis (FIA) database are derived from numerous methodologies whose abundance and complexity raise questions about consistent results throughout the U.S. A new model based on allometric scaling theory ("WBE") offers simplified methodology and a theoretically sound basis for improving the reliability and...

Multiple value forest surveys in the Midsouth states

Treesearch

Victor A. Rudis

1990-01-01

State-of-the-art achievement and limitations in integrating water, range, wildlife, and recreation ("nontimber") inventories with forest surveys of the USDA-Forest Service, Southern Forest Experiment station, Forest Inventory and Analysis (FIA) Unit are reviewed.The FIA Unit surveys private and public forests in 7 Midsouth states:Alabama, Arkansas, Louisiana...

FIAMODEL: Users Guide Version 3.0.

Treesearch

Scott A. Pugh; David D. Reed; Kurt S. Pregitzer; Patrick D. Miles

2002-01-01

FIAMODEL is a geographic information system (GIS program used to summarize Forest Inventory and Analysis (FIA, USDA Forest Service) data such as volume. The model runs in ArcView and allows users to select FIA plots with heads-up-digitizing, overlays of digital map layers, or queries based on specific plot attributes.

Forest land area estimates from vegetation continuous fields

Treesearch

Mark D. Nelson; Ronald E. McRoberts; Matthew C. Hansen

2004-01-01

The USDA Forest Service's Forest Inventory and Analysis (FIA) program provides data, information, and knowledge about our Nation's forest resources. FIA regional units collect data from field plots and remotely sensed imagery to produce statistical estimates of forest extent (area); volume, growth, and removals; and health and condition. There is increasing...

Advancements in LiDAR-based registration of FIA field plots

Treesearch

Demetrios Gatziolis

2012-01-01

Meaningful integration of National Forest Inventory field plot information with spectral imagery acquired from satellite or airborne platforms requires precise plot registration. Global positioning system-based plot registration procedures, such as the one employed by the Forest Inventory and Analysis (FIA) Program, yield plot coordinates that, although adequate for...

Forests of Massachusetts, 2016

Treesearch

Brett J. Butler

2017-01-01

This report provides an overview of forest resources in Massachusetts based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station.Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2011-2016 with comparisons made to 2007-...

Forests of Massachusetts, 2013

Treesearch

Brett J. Butler

2014-01-01

This report provides an overview of forest resources in Massachusetts based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2009-2013 with comparisons made to 2003-...

Forests of North Dakota, 2013

Treesearch

David E. Haugen

2014-01-01

This resource update provides an overview of forest resources in North Dakota based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the North Dakota Forest Service. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Connecticut, 2013

Treesearch

Brett J. Butler

2014-01-01

This report provides an overview of forest resources in Connecticut based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2009-2013 with comparisons made to 2003-...

Forests of Michigan, 2013

Treesearch

Scott A. Pugh

2014-01-01

This publication provides an overview of forest resources in Michigan based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Since 1999, FIA has employed an annual inventory measuring data on a nominal 20 percent of sample plots each year. For the 2013 inventory, estimates for current...

Forests of Minnesota, 2013

Treesearch

Patrick D. Miles; Curtis VanderSchaaf

2014-01-01

This science update provides an overview of forest resources in Minnesota based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Minnesota Department of Natural Resources. Estimates are based on field data, collected using the FIA annualized sample design, for the...

Forests of Missouri, 2013

Treesearch

Ronald J. Piva; Thomas B. Treiman

2014-01-01

This science update provides an overview of forest resources in Missouri based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Missouri Department of Conservation. Estimates are based on field data, collected using the FIA annualized sample design, for the...

Forests of Iowa, 2013

Treesearch

Mark D. Nelson; Matt Brewer

2014-01-01

This resource update provides an overview of forest resources in Iowa based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Iowa Department of Natural Resources. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Vermont, 2013

Treesearch

Randall S. Morin; Scott A. Pugh

2014-01-01

This publication provides an overview of forest resources in Vermont based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Since 1999, FIA has employed an annual inventory measuring data on a nominal 20 percent of sample plots each year. For the 2013 inventory, estimates for current...

Forests of New Hampshire, 2013

Treesearch

Randall S. Morin; Scott A. Pugh

2014-01-01

This publication provides an overview of forest resources in New Hampshire based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Since 1999, FIA has employed an annual inventory measuring data on a nominal 20 percent of sample plots each year. For the 2013 inventory, estimates for...

Forests of Indiana, 2013

Treesearch

Dale D. Gormanson

2014-01-01

This resource update provides an overview of forest resources in Indiana based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Indiana Department of Natural Resources. Estimates are based on field data collected using the FIA annualized strategic sample design and...

Forests of North Carolina, 2013

Treesearch

Mark J. Brown

2015-01-01

This periodic resource update provides an overview of forest resources in North Carolina based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the North Carolina Forest Service. Data estimates are based on field data collected using the FIA annualized sample design...

Forests of Michigan, 2014

Treesearch

Scott A. Pugh

2015-01-01

This resource update provides an overview of forest resources in Michigan based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly.* The annual inventory started in 1999. For the 2014...

Forests of Connecticut, 2015

Treesearch

Brett J. Butler

2016-01-01

This report provides an overview of forest resources in Connecticut based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2010-2015 with comparisons made to 2005-...

Point pattern analysis of FIA data

Treesearch

Chris Woodall

2002-01-01

Point pattern analysis is a branch of spatial statistics that quantifies the spatial distribution of points in two-dimensional space. Point pattern analysis was conducted on stand stem-maps from FIA fixed-radius plots to explore point pattern analysis techniques and to determine the ability of pattern descriptions to describe stand attributes. Results indicate that the...

Tree crown conditions in Missouri, 2000-2003

Treesearch

KaDonna C. Randolph; W. Keith Moser

2009-01-01

The Forest Service, U.S. Department of Agriculture, Forest Inventory and Analysis (FIA) Program uses visual assessments of tree crown condition to monitor changes and trends in forest health. This report describes three FIA tree crown condition indicators (crown dieback, crown density, and foliage transparency) and sapling crown vigor measured in Missouri between 2000...

Forests of Oklahoma, 2013

Treesearch

S. Lambert; J.T. Vogt.; J. Cooper

2015-01-01

This resource update provides an overview of forest resources in Oklahoma based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station, in cooperation with Oklahoma Forestry Services (OFS). Estimates are based on field data collected using the FIA annualized sample design and are updated yearly...

Kansas' forest resources, 2005

Treesearch

W. Keith Moser; Gary J. Brand; Melissa Powers

2007-01-01

The USDA Forest Service, Northern Research Station, Forest Inventory and Analysis (NRS-FIA) program is changing to a Web-based, dynamically linked reporting system. As part of the process, this year NRS-FIA is producing this abbreviated summary of 2005 data. This resource bulletin reports on area, volume, and biomass using data from 2001 through 2005. Estimates from...

Forests of Iowa, 2017

Treesearch

Mark D. Nelson; Tivon E. Feeley

2018-01-01

This resource update provides an overview of forest resources in Iowa based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Iowa Department of Natural Resources. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Understanding macroscale invasion patterns and processes with FIA data

Treesearch

Songlin Fei; Basil V. Iannone III; Christopher M. Oswalt; Qinfeng Guo; Kevin M. Potter; Sonja N. Oswalt; Bryan C. Pijanowski; Gabriela C. Nunez-Mir

2015-01-01

Using empirical data from FIA, we modeled invasion richness and invasion prevalence as functions of 22 factors reflective of propagule pressure and/or habitat invasibility across the continental US. Our statistical models suggest that both propagule pressure and habitat invasibility contribute to macroscale patterns of forest plant invasions. Our investigation provides...

Forests of Georgia, 2013

Treesearch

T.J. Brandeis

2015-01-01

This resource update provides an overview of forest resources in Georgia based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Georgia Forestry Commission. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly....

Forests of Missouri, 2015

Treesearch

Ronald J. Piva; Thomas B. Treiman

2016-01-01

This resource update provides an overview of forest resources in Missouri based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Missouri Department of Conservation. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Pennsylvania, 2015

Treesearch

Richard H. Widmann

2016-01-01

This resource update provides an overview of the forest resources in Pennsylvania based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station (NRS). Estimates are based on field data collected using the FIA annualized sample design and are updated yearly1(see footnote 1, page 2). Information...

Forests of Michigan, 2015

Treesearch

Scott A. Pugh; Charles Paulson; Brett J. Butler

2016-01-01

This resource update provides an overview of forest resources in Michigan based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. The annual inventory started in 1999. For the 2015...

Forests of Ohio, 2015

Treesearch

Richard H. Widmann

2016-01-01

This resource update provides an overview of the forest resources in Ohio based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly.1(See footnotes on page 4.) Information about the...

Forests of Michigan, 2016

Treesearch

Charles Paulson; Scott A. Pugh

2017-01-01

This resource update provides an overview of forest resources in Michigan based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. The annual inventory started in 1999. For the 2016...

Forests of Massachusetts, 2015

Treesearch

Brett J. Butler

2016-01-01

This report provides an overview of forest resources in Massachusetts based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station.Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2010-2015 with comparisons made to 2005-...

Statistical properties of alternative national forest inventory area estimators

Treesearch

Francis Roesch; John Coulston; Andrew D. Hill

2012-01-01

The statistical properties of potential estimators of forest area for the USDA Forest Service's Forest Inventory and Analysis (FIA) program are presented and discussed. The current FIA area estimator is compared and contrasted with a weighted mean estimator and an estimator based on the Polya posterior, in the presence of nonresponse. Estimator optimality is...

Forest of North Dakota, 2016

Treesearch

David E. Haugen

2017-01-01

This resource update provides an overview of forest resources in North Dakota based on an inventory conducted by the USDA Forest Service, Forest Inventory and Analysis (FIA) program within the Northern Research Station in cooperation with the North Dakota Forest Service. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of North Carolina, 2014

Treesearch

Mark Brown; Samuel Lambert

2016-01-01

This periodic resource update provides an overview of forest resources in North Carolina based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the North Carolina Forest Service. Data estimates are based on field data collected using the FIA annualized sample design...

Forests of North Dakota, 2017

Treesearch

Charles S. Paulson

2018-01-01

This resource update provides an overview of forest resources in North Dakota based on an inventory conducted by the USDA Forest Service, Forest Inventory and Analysis (FIA) program within the Northern Research Station in cooperation with the North Dakota Forest Service. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Pennsylvania, 2016

Treesearch

Thomas A. Albright

2017-01-01

This resource update provides an overview of the forest resources in Pennsylvania based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. Information about the national and regional...

Forests of New Jersey, 2015

Treesearch

Susan J. Crocker; Brett J. Butler

2016-01-01

This publication provides an overview of forest resources in New Jersey based on an annual inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station. Estimates are based on field data collected using an annualized sample design and are updated yearly. Information about the FIA program is available at...

Forests of Connecticut, 2016

Treesearch

Brett J. Butler

2017-01-01

This report provides an overview of forest resources in Connecticut based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2011-2016 with comparisons made to 2007-...

Forests of Missouri, 2017

Treesearch

Thomas C. Goff

2018-01-01

This resource update provides an overview of forest resources in Missouri based on an inventory conducted by the USDA Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Missouri Department of Conservation. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Michigan, 2017

Treesearch

Scott A. Pugh

2018-01-01

This resource update provides an overview of forest resources in Michigan based on inventories conducted by the USDA Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. The annual inventory started in 1999. For the 2017...

Forests of Missouri, 2016

Treesearch

Ronald J. Piva; Thomas B. Treiman

2017-01-01

This resource update provides an overview of forest resources in Missouri based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Missouri Department of Conservation. Estimates are based on field data collected using the FIA annualized sample design and are updated...

An Analysis of Losses to the Southern Commercial Timberland Base

Treesearch

Ian A. Munn; David Cleaves

1998-01-01

Demographic and physical factors influencing the conversion of commercial timberland iu the south to non-forestry uses between the last two Forest Inventory Analysis (FIA) surveys were investigated. GIS techniques linked Census data and FIA plot level data. Multinomial logit regression identified factors associated with losses to the timberland base. Conversion to...

Forests of New Jersey, 2016

Treesearch

Susan J. Crocker; Greg C. Liknes

2017-01-01

This publication provides an overview of forest resources in New Jersey following an inventory by the U.S. Forest Service, Forest Inventory and Analysis program (FIA), Northern Research Station (NRS). Estimates are derived from field data collected using an annualized sample design and are updated yearly. Beginning in 2014, NRS-FIA switched to a 7-year cycle length....

Tiger 2000 and FIA

Treesearch

Joseph McCollum; Dennis Jacobs

2002-01-01

legal foundations of the FIA (Forest Inventory and Analysis) progrdm are laid out. Upon those foundations are built a geographical definition of the United States and its conlponents, and how applying that definition might change from decade to decade. Along the way, the American system of weights and measures as well as the unusual geography of the commonwealth of...

Remote Sensing Precision Requirements For FIA Estimation

Treesearch

Mark H. Hansen

2001-01-01

In this study the National Land Cover Data (NLCD) available from the Multi-Resolution Land Characteristics Consortium (MRLC) is used for stratification in the estimation of forest area, timberland area, and growing-stock volume from the first year (1999) of annual FIA data collected in Indiana, Iowa, Minnesota, and Missouri. These estimates show that with improvements...

Forests of Iowa, 2015

Treesearch

Mark D. Nelson; Matt Brewer; Dacia M. Meneguzzo; Kathryne. Clark

2016-01-01

This resource update provides an overview of forest resources in Iowa based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Iowa Department of Natural Resources. Estimates are based on field data collected using the FIA annualized sample design and are updated...

An evaluation of FIA's stand age variable

Treesearch

John D. Shaw

2015-01-01

The Forest Inventory and Analysis Database (FIADB) includes a large number of measured and computed variables. The definitions of measured variables are usually well-documented in FIA field and database manuals. Some computed variables, such as live basal area of the condition, are equally straightforward. Other computed variables, such as individual tree volume,...

Precise FIA plot registration using field and dense LIDAR data

Treesearch

Demetrios Gatziolis

2009-01-01

Precise registration of forest inventory and analysis (FIA) plots is a prerequisite for an effective fusion of field data with ancillary spatial information, which is an approach commonly employed in the mapping of various forest parameters. Although the adoption of Global Positioning System technology has improved the precision of plot coordinates obtained during...

Mississippi, 2012 forest inventory and analysis factsheet

Treesearch

Sonja N. Oswalt

2013-01-01

This science update provides an overview of forest resources in Mississippi based on an inventory conducted by the U.S. Department of Agriculture Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Mississippi Forestry Commission. Data estimates are based on field data collected using the FIA annualized...

Mississippi, 2011 forest inventory and analysis factsheet

Treesearch

Sonja N. Oswalt

2013-01-01

This science update provides an overview of forest resources in Mississippi based on an inventory conducted by the U.S. Department of Agriculture Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Mississippi Forestry Commission. Data estimates are based on field data collected using the FIA annualized...

Forests of Alabama, 2015

Treesearch

Andy Hartsell

2016-01-01

This resource update provides an overview of forest resources in Alabama based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Alabama Forestry Commission. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly....

Forests of Indiana, 2015

Treesearch

Dale D. Gormanson

2016-01-01

This resource update provides an overview of forest resources in Indiana based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Indiana Department of Natural Resources. Estimates are based on field data collected using the FIA annualized strategic sample design and...

Forests of Indiana, 2016

Treesearch

Dale D. Gormanson; Cassandra M. Kurtz

2017-01-01

This resource update provides an overview of forest resources in Indiana based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Indiana Department of Natural Resources. Estimates are based on field data collected using the FIA annualized strategic sample design and...

Forests of Louisiana, 2014

Treesearch

S.N. Oswalt

2017-01-01

This resource update provides an overview of forest resources in Louisiana based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. The estimates presented in this update are for the...

Forests of Louisiana, 2012

Treesearch

S.N. Oswalt

2014-01-01

This resource update provides an overview of forest resources in Louisiana based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Mississippi Forestry Commission. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Iowa, 2014

Treesearch

Mark D. Nelson; Matt Brewer; Brett J. Butler; Scott A. Pugh

2015-01-01

This resource update provides an overview of forest resources in Iowa based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Iowa Department of Natural Resources. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Massachusetts, 2014

Treesearch

Brett J. Butler; Susan J. Crocker

2015-01-01

This report provides an overview of forest resources in Massachusetts based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2009-2014 with comparisons made to 2005-...

Forests of Pennsylvania, 2014

Treesearch

Richard H. Widmann

2015-01-01

This resource update provides an overview of the forest resources in Pennsylvania based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly (see footnote 1 on page 4). Information about...

Forests of Oklahoma, 2014

Treesearch

S. Lambert; K. Randolph; J. Cooper

2015-01-01

This resource update provides an overview of forest resources in Oklahoma based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station, in cooperation with Oklahoma Forestry Services. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly,...

Forests of Indiana, 2014

Treesearch

Dale D. Gormanson; Ronald J. Piva

2015-01-01

This resource update provides an overview of forest resources in Indiana based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Indiana Department of Natural Resources. Estimates are based on field data collected using the FIA annualized strategic sample design and...

Forests of Kentucky, 2014

Treesearch

Thomas Brandeis; Andy Hartsell; KaDonna Randolph; Sonja Oswalt; Consuelo Brandeis

2016-01-01

This resource update provides an overview of forest resources in Kentucky based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. The estimates presented in this update are...

Forests of Alabama, 2014

Treesearch

Andy Hartsell

2016-01-01

This resource update provides an overview of forest resources in Alabama based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Alabama Forestry Commission. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly....

Forests of Wisconsin, 2014

Treesearch

Charles H. Perry

2015-01-01

This resource update provides an overview of forest resources in Wisconsin based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Wisconsin Department of Natural Resources (WDNR). Data estimates are based on field data collected using the FIA annualized sample...

Forests of Ohio, 2014

Treesearch

Richard H. Widmann

2015-01-01

This resource update provides an overview of the forest resources in Ohio based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. (See footnote on page 4.) Information about the...

Forests of Connecticut, 2014

Treesearch

Brett J. Butler; Susan J. Crocker

2015-01-01

This report provides an overview of forest resources in Connecticut based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2009-2014 with comparisons made to 2005-...

Forests of North Dakota, 2014

Treesearch

D.E. Haugen; S.A. Pugh

2014-01-01

This resource update provides an overview of forest resources in North Dakota based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the North Dakota Forest Service. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Georgia, 2014

Treesearch

Thomas Brandeis; Andy Hartsell

2015-01-01

This resource update provides an overview of forest resources in Georgia based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Georgia Forestry Commission. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly....

SOLE: enhanced FIA data analysis capabilities

Treesearch

Michael Spinney; Paul Van Deusen

2009-01-01

The Southern On Line Estimator (SOLE), is an Internet-based annual forest inventory and analysis (FIA) data analysis tool developed cooperatively by the National Council for Air and Stream Improvement and the Forest Service, U.S. Department of Agriculture's Forest Inventory and Analysis program at the Southern Research Station. Recent development of SOLE has...

Correct county areas with sidebars for Virginia

Treesearch

Joseph M. McCollum; Dale Gormanson; John Coulston

2009-01-01

Historically, Forest Inventory and Analysis (FIA) has processed field inventory data at the county level and county estimates of land area were constrained to equal those reported by the Census Bureau. Currently, the Southern Research Station FIA unit processes field inventory data at the survey unit level (groups of counties with similar ecological characteristics)....

Forests of Wisconsin, 2017

Treesearch

Cassandra M. Kurtz

2018-01-01

This resource update provides an overview of forest resources in Wisconsin based on an inventory conducted by the USDA Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Wisconsin Department of Natural Resources. Estimates are based on field data collected using the FIA annualized sample design and are...

Forests of Florida, 2012

Treesearch

M.J. Brown; Jarek. Nowak

2014-01-01

This periodic resource update provides an overview of forest resources in Florida based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Florida Forest Service. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Iowa, 2016

Treesearch

Mark D. Nelson; Tivon E. Feeley; Cassandra M. Kurtz

2017-01-01

This resource update provides an overview of forest resources in Iowa based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Iowa Department of Natural Resources. Estimates are based on field data collected using the FIA annualized sample design and are updated...

Forests of Oklahoma, 2012

Treesearch

S. Lambert; J.A. Cooper

2014-01-01

This resource update provides an overview of forest resources in Oklahoma based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station, in cooperation with Oklahoma Forestry Services (OFS). Estimates are based on field data collected using the FIA annualized sample design and are updated yearly...

Inventory-based landscape-scale simulation of management effectiveness and economic feasibility with BioSum

Treesearch

Jeremy S. Fried; Larry D. Potts; Sara M. Loreno; Glenn A. Christensen; R. Jamie Barbour

2017-01-01

The Forest Inventory and Analysis (FIA)-based BioSum (Bioregional Inventory Originated Simulation Under Management) is a free policy analysis framework and workflow management software solution. It addresses complex management questions concerning forest health and vulnerability for large, multimillion acre, multiowner landscapes using FIA plot data as the initial...

Refining FIA plot locations using LiDAR point clouds

Treesearch

Charlie Schrader-Patton; Greg C. Liknes; Demetrios Gatziolis; Brian M. Wing; Mark D. Nelson; Patrick D. Miles; Josh Bixby; Daniel G. Wendt; Dennis Kepler; Abbey Schaaf

2015-01-01

Forest Inventory and Analysis (FIA) plot location coordinate precision is often insufficient for use with high resolution remotely sensed data, thereby limiting the use of these plots for geospatial applications and reducing the validity of models that assume the locations are precise. A practical and efficient method is needed to improve coordinate precision. To...

FIA forest inventory data for wildlife habitat assessment

Treesearch

David C. Chojnacky

2000-01-01

The Forest Inventory and Analysis (FIA) program of the USDA Forest Service maintains a network of permanent plots to monitor changing forest conditions. These plots were originally established to monitor the nation's timber supply; however, these data have great potential for evaluating other forest resources. To demonstrate a wildlife application, an assessment...

Forests of Wisconsin, 2015

Treesearch

Charles H. Perry

2016-01-01

This Resource Update provides an overview of forest resources in Wisconsin based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Wisconsin Department of Natural Resources (WDNR). Data estimates are based on field data collected using the FIA annualized sample...

Anomalous dismeter distribution shifts estimated from FIA inventories through time

Treesearch

Francis A. Roesch; Paul C. Van Deusen

2010-01-01

In the past decade, the United States Department of Agriculture Forest Service’s Forest Inventory and Analysis Program (FIA) has replaced regionally autonomous, periodic, state-wide forest inventories using various probability proportional to tree size sampling designs with a nationally consistent annual forest inventory design utilizing systematically spaced clusters...

An Ion-Selective Electrode/Flow-Injection Analysis Experiment: Determination of Potassium in Serum.

ERIC Educational Resources Information Center

Meyerhoff, Mark E.; Kovach, Paul M.

1983-01-01

Describes a low-cost, senior-level, instrumental analysis experiment in which a home-made potassium tubular flow-through electrode is constructed and incorporated into a flow injection analysis system (FIA). Also describes experiments for evaluating the electrode's response properties, examining basic FIA concepts, and determining potassium in…

General Constraints on Sampling Wildlife on FIA Plots

Treesearch

Larissa L. Bailey; John R. Sauer; James D. Nichols; Paul H. Geissler

2005-01-01

This paper reviews the constraints to sampling wildlife populations at FIA points. Wildlife sampling programs must have well-defined goals and provide information adequate to meet those goals. Investigators should choose a State variable based on information needs and the spatial sampling scale. We discuss estimation-based methods for three State variables: species...

Sensitivity of FIA Volume Estimates to Changes in Stratum Weights and Number of Strata

Treesearch

James A. Westfall; Michael Hoppus

2005-01-01

In the Northeast region, the USDA Forest Service Forest Inventory and Analysis (FIA) program utilizes stratified sampling techniques to improve the precision of population estimates. Recently, interpretation of aerial photographs was replaced with classified remotely sensed imagery to determine stratum weights and plot stratum assignments. However, stratum weights...

A new Link for Geographic analyses of Inventory Data

Treesearch

David Reed; Kurt Pregitzer; Scott A. Pugh; Patrick D. Miles

2001-01-01

The USDA Forest Service Forest Inventory and Analysis (FIA)data are widely used throughout the United States for analyses of forest status and trends, landscape-level forest composition, and other forest characteristics. A new software product, FIAMODEL, is available for analyzing FIA data within the ArcView? (ESRI, Inc.)geographic information system. The software...

Integrating Spatial Components into FIA Models of Forest Resources: Some Technical Aspects

Treesearch

Pat Terletzky; Tracey Frescino

2005-01-01

We examined two software packages to determine their feasibility of implementing spatially explicit, forest resource models that integrate Forest Inventory and Analysis data (FIA). ARCINFO and Interactive Data Language (IDL) were examined for their input requirements, speed of processing, storage requirements, and flexibility of implementing. Implementations of two...

Forests of Florida, 2013

Treesearch

Mark Brown; J.. Nowak

2016-01-01

This periodic resource update provides an overview of forest resources in Florida based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Florida Forest Service. Estimates are based on field data collected using the FIA annualized sample design and are updated...

FIESTA—An R estimation tool for FIA analysts

Treesearch

Tracey S. Frescino; Paul L. Patterson; Gretchen G. Moisen; Elizabeth A. Freeman

2015-01-01

FIESTA (Forest Inventory ESTimation for Analysis) is a user-friendly R package that was originally developed to support the production of estimates consistent with current tools available for the Forest Inventory and Analysis (FIA) National Program, such as FIDO (Forest Inventory Data Online) and EVALIDator. FIESTA provides an alternative data retrieval and reporting...

Forests of Alabama, 2016

Treesearch

A. Hartsell

2017-01-01

This resource update provides an overview of forest resources in Alabama based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Alabama Forestry Commission. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly....

Forests of Wisconsin, 2013

Treesearch

Charles H. Perry

2014-01-01

This resource update provides an overview of forest resources in Wisconsin based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Northern Research Station in cooperation with the Wisconsin Department of Natural Resources. Data estimates are based on field data collected using the FIA annualized sample design and...

Location uncertainty and the tri-areal design

Treesearch

Francis A. Roesch

2007-01-01

The U.S. Department of Agriculture Forest Service Forest Inventory and Analysis Program (FIA) uses a field plot design that incorporates multiple sample selection mechanisms. Not all of the five FIA units currently use the entire suite of available sample selection mechanisms. These sampling selection mechanisms could be described in a number of ways with respect to...

Oklahoma, 2011 - forest inventory and analysis factsheet

Treesearch

Jason A. Cooper

2013-01-01

This science update summarizes the findings of the statewide annual inventory of the forest resource attributes in Oklahoma conducted by the Southern Forest Inventory and Analysis (FIA) program in cooperation with the Oklahoma Forestry Services. The 77 counties of Oklahoma are consolidated into seven FIA survey units— southeast (unit 1), northeast (unit 2), north...

Forests of Rhode Island, 2013

Treesearch

Brett J. Butler

2014-01-01

This report provides an overview of forest resources in Rhode Island based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2009-2013 with comparisons made to 2003-...

Forests of east Texas, 2013

Treesearch

K.J.W. Dooley; T.J. Brandeis

2014-01-01

This resource update provides an overview of forest resources in east Texas based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Texas A&M Forest Service. Forest resource estimates are based on field data collected using the FIA annualized sample design and...

Estimating mangrove in Florida: trials monitoring rare ecosystems

Treesearch

Mark J. Brown

2015-01-01

Mangrove species are keystone components in coastal ecosystems and are the interface between forest land and sea. Yet, estimates of their area have varied widely. Forest Inventory and Analysis (FIA) data from ground-based sample plots provide one estimate of the resource. Initial FIA estimates of the mangrove resource in Florida varied dramatically from those compiled...

Effect of inventory method on niche models: random versus systematic error

Treesearch

Heather E. Lintz; Andrew N. Gray; Bruce McCune

2013-01-01

Data from large-scale biological inventories are essential for understanding and managing Earth's ecosystems. The Forest Inventory and Analysis Program (FIA) of the U.S. Forest Service is the largest biological inventory in North America; however, the FIA inventory recently changed from an amalgam of different approaches to a nationally-standardized approach in...

Improving Forest Inventory and Analysis efficiency with common land unit information

Treesearch

Greg C. Liknes; Mark D. Nelson

2009-01-01

The Forest Service, U.S. Department of Agriculture's (USDA's) Northern Research Station Forest Inventory and Analysis program (NRS-FIA) examines inventory locations on digital aerial imagery to determine if the land use at each plot location meets the FIA definition of forest and thereby becomes a field visit site. This manual image-interpretation effort...

Adding net growth, removals, and mortality estimates for biomass and carbon in FIADB

Treesearch

Jeffery A. Turner

2015-01-01

Traditional growth, removals, and mortality (GRM) estimates produced from Forest Inventory and Analysis (FIA) periodic inventories were limited to changes in volume on timberland. Estimates on forestland were added in the east as the first installment of annual inventory plots was remeasured. The western FIA units have begun annual remeasurement, precipitating the need...

Forest Inventory and Analysis and Forest Health Monitoring: Piecing the Quilt

Treesearch

Joseph M. McCollum; Jamie K. Cochran

2005-01-01

Against the backdrop of a discussion about patchwork quilt assembly, the authors present background information on global grids. They show how to compose hexagons, an important task in systematically developing a subset of Forest Health Monitoring (FHM) Program plots from Forest Inventory and Analysis (FIA) plots. Finally, they outline the FHM and FIA grids, along with...

Forests of Delaware, 2015

Treesearch

Tonya Lister; Richard Widmann

2016-01-01

This publication provides an overview of forest resources in Delaware based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. From 2004-2013, FIA employed an annual inventory with a cycle length of 5 years, measuring data on 20 percent of all sample plots each year in Delaware. Beginning...

Forests of New York, 2015

Treesearch

Richard H. Widmann

2016-01-01

This resource update provides an overview of the forest resources in New York based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly.1(See footnote on page 4). Information about the...

Forests of Rhode Island, 2015

Treesearch

Brett J. Butler

2016-01-01

This report provides an overview of forest resources in Rhode Island based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2010-2015 with comparisons made to 2005-...

Forests of Rhode Island, 2016

Treesearch

Brett J. Butler

2017-01-01

This report provides an overview of forest resources in Rhode Island based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2011-2016 with comparisons made to 2007-...

Forests of Delaware, 2016

Treesearch

Stephen Potter

2017-01-01

This publication provides an overview of forest resources in Delaware based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. From 2004-2013, FIA employed an annual inventory with a cycle length of 5 years, measuring data on 20 percent of all sample plots each year in Delaware. Beginning...

TIGER 2000 and FIA

Treesearch

Joseph McCollum; Dennis Jacobs

2005-01-01

The legal foundations of the FIA (Forest Inventory and Analysis) program are laid out. Upon those foundations are built a geographical definition of the United States and its components, and how applying that definition might change from decade to decade. Along the way, the American system of weights and measures as well as the unusual geography of the Commonwealth of...

Comparing Forest/Nonforest Classifications of Landsat TM Imagery for Stratifying FIA Estimates of Forest Land Area

Treesearch

Mark D. Nelson; Ronald E. McRoberts; Greg C. Liknes; Geoffrey R. Holden

2005-01-01

Landsat Thematic Mapper (TM) satellite imagery and Forest Inventory and Analysis (FIA) plot data were used to construct forest/nonforest maps of Mapping Zone 41, National Land Cover Dataset 2000 (NLCD 2000). Stratification approaches resulting from Maximum Likelihood, Fuzzy Convolution, Logistic Regression, and k-Nearest Neighbors classification/prediction methods were...

Using classified Landsat Thematic Mapper data for stratification in a statewide forest inventory

Treesearch

Mark H. Hansen; Daniel G. Wendt

2000-01-01

The 1998 Indiana/Illinois forest inventory (USDA Forest Service, Forest Inventory and Analysis (FIA)) used Landsat Thematic Mapper (TM) data for stratification. Classified images made by the National Gap Analysis Program (GAP) stratified FIA plots into four classes (nonforest, nonforest/ forest, forest/nonforest, and forest) based on a two pixel forest edge buffer zone...

Forests of east Texas, 2016

Treesearch

Kerry Dooley

2018-01-01

This resource update provides an overview of forest resources in east Texas based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station (SRS) in cooperation with Texas A&M Forest Service. The 254 counties of Texas are consolidated into seven FIA survey units—Southeast (unit 1),...

Using Classified Landsat Thematic Mapper Data for Stratification in a Statewide Forest Inventory

Treesearch

Mark H. Hansen; Daniel G. Wendt

2000-01-01

The 1998 Indiana/Illinois forest inventory (USDA Forest Service, Forest Inventory and Analysis (FIA)) used Landsat Thematic Mapper (TM} data for stratification. Classified images made by the National Gap Analysis Program (GAP) stratified FIA plots into four classes (nonforest, nonforest/forest, forest/nonforest, and forest) based on a two pixel forest edge buffer zone...

A primer of nonresponse in the US Forest Inventory and Analysis program

Treesearch

Paul L. Patterson; John W. Coulston; Francis A. Roesch; James A. Westfall; Andrew D. Hill

2012-01-01

Nonresponse caused by denied access and hazardous conditions are a concern for the USDA Forest Service, Forest Inventory and Analysis (FIA) program, whose mission is to quantify status and trends in forest resources across the USA. Any appreciable amount of nonresponse can cause bias in FIA's estimates of population parameters. This paper will quantify the...

Mapping Forest Inventory and Analysis forest land use: timberland, reserved forest land, and other forest land

Treesearch

Mark D. Nelson; John Vissage

2007-01-01

The Forest Inventory and Analysis (FIA) program produces area estimates of forest land use within three subcategories: timberland, reserved forest land, and other forest land. Mapping these subcategories of forest land requires the ability to spatially distinguish productive from unproductive land, and reserved from nonreserved land. FIA field data were spatially...

Predicting bird habitat quality from a geospatial analysis of FIA data

Treesearch

John M. Tirpak; D. Todd Jones-Farrand; Frank R., III Thompson; Daniel J. Twedt; Mark D. Nelson; William B., III Uihlein

2009-01-01

The ability to assess the influence of site-scale forest structure on avian habitat suitability at an ecoregional scale remains a major methodological constraint to effective biological planning for forest land birds in North America. We evaluated the feasibility of using forest inventory and analysis (FIA) data to define vegetation structure within forest patches,...

Alabama, 2010 forest inventory and analysis factsheet

Treesearch

Andrew J. Hartsell

2011-01-01

FIA was initially established to monitor the Nation’s timber supply and the amount of commercially available resources. These early surveys were not concerned with the forests, species, and tree sizes that were not considered commercially viable. Early FIA reported only on growing-stock trees on timberlands, i.e., commercially important tree species and sizes on...

On-Line Analysis of Southern FIA Data

Treesearch

Michael P. Spinney; Paul C. Van Deusen; Francis A. Roesch

2006-01-01

The Southern On-Line Estimator (SOLE) is a web-based FIA database analysis tool designed with an emphasis on modularity. The Java-based user interface is simple and intuitive to use and the R-based analysis engine is fast and stable. Each component of the program (data retrieval, statistical analysis and output) can be individually modified to accommodate major...

Forests of New York, 2014

Treesearch

Richard H. Widmann

2015-01-01

This resource update provides an overview of the forest resources in New York based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design and are updated yearly. (See footnote on page 4). Information about the...

Forests of Delaware, 2014

Treesearch

T.W. Lister; R.H. Widmann

2015-01-01

This publication provides an overview of forest resources in Delaware based on inventories conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. From 2004-2013, FIA employed an annual inventory with a cycle length of 5 years, measuring data on 20 percent of all sample plots each year in Delaware. Beginning...

Forests of Rhode Island, 2014

Treesearch

Brett J. Butler; Susan J. Crocker

2015-01-01

This report provides an overview of forest resources in Rhode Island based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program of the Northern Research Station. Estimates are based on field data collected using the FIA annualized sample design. Results are for the measurement years 2009-2014 with comparisons made to 2005-...

Forests of Illinois, 2014

Treesearch

Susan J. Crocker

2015-01-01

This publication provides an overview of forest resource attributes for Illinois based on an annual inventory conducted by the Forest Inventory and Analysis (FIA) program of the Northern Research Station (NRS) of the U.S. Forest Service. These estimates, along with web-posted core tables, are updated annually. In 2014, NRS-FIA changed from a 5- to a 7-year inventory...

Forests of New Jersey, 2014

Treesearch

Susan J. Crocker

2015-01-01

This publication provides an overview of forest resource attributes for New Jersey based on an annual inventory conducted by the Forest Inventory and Analysis (FIA) program of the Northern Research Station (NRS) of the U.S. Forest Service. These estimates, along with web-posted core tables, are updated annually. In 2014, NRS-FIA changed from a 5- to a 7-year inventory...

Challenges of working with FIADB17 data: the SOLE experience

Treesearch

Michael Spinney; Paul Van Deusen

2007-01-01

The Southern On Line Estimator (SOLE) is an Internet-based Forest Inventory and Analysis (FIA) data analysis tool. SOLE is based on data downloaded from the publicly available FIA database (FIADB) and summarized by plot condition. The tasks of downloading, processing, and summarizing FIADB data require specialized expertise in inventory theory and data manipulation....

Landscape scale mapping of forest inventory data by nearest neighbor classification

Treesearch

Andrew Lister

2009-01-01

One of the goals of the Forest Service, U.S. Department of Agriculture's Forest Inventory and Analysis (FIA) program is large-area mapping. FIA scientists have tried many methods in the past, including geostatistical methods, linear modeling, nonlinear modeling, and simple choropleth and dot maps. Mapping methods that require individual model-based maps to be...

Estimating down deadwood from FIA forest inventory variables in Maine

Treesearch

David C. Chojnacky; Linda S. Heath

2002-01-01

Down deadwood (DDW) is a carbon component important in the function and structure of forest ecosystems, but estimating DDW is problematic because these data are not widely available in forest inventory databases. However, DDW data were collected on USDA Forest Service Forest Inventory and Analysis (FIA) plots during Maine's 1995 inventory. This study examines ways...

Estimating down dead wood from FIA forest inventory variables in Maine

Treesearch

David C. Chojnacky; Linda S. Heath

2002-01-01

Down deadwood (DDW) is a carbon component important in the function and structure of forest ecosystems, but estimating DDW is problematic because these data are not widely available in forest inventory databases. However, DDW data were collected on USDA Forest Service Forest Inventory and Analysis (FIA) plots during Maine's 1995 inventory. This study examines ways...

Vision for the Future of FIA: Paean to Progress, Possibilities, and Partners

Treesearch

Susan L. King; Charles T. Scott

2006-01-01

The Forest Inventory and Analysis (FIA) program of the U.S. Department of Agriculture Forest Service has made significant progress implementing the annualized inventory in 46 States in 2004. Major increases in program performance included the availability of plot data and the plots? corresponding approximate coordinates. A mill site study and biomass models were used...

What does nonforest land contribute to the global carbon balance?

Treesearch

Jennifer C. Jenkins; Rachel Riemann

2002-01-01

An inventory of land traditionally called "nonforest" and therefore not sampled by the Forest Inventory and Analysis (FIA) program was implemented by the FIA unit at the Northeastern Station in 1999 for five counties in Maryland. Biomass and biomass increment were estimated from the nonforest inventory data using techniques developed for application to large-...

South Carolina, 2010 forest inventory and analysis factsheet

Treesearch

Roger C. Conner

2011-01-01

The Forest Inventory and Analysis (FIA) Program implemented a nationally consistent annual inventory system in 1998. Under the new design, one-fifth of all inventory plots in South Carolina are visited each year. The southern FIA unit, working cooperatively with South Carolina Forestry Commission crews, established the State’s initial annual inventory plots during the...

Forests of East Texas, 2014

Treesearch

Thomas J. Brandeis

2015-01-01

This resource update provides an overview of forest resources in east Texas derived from an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) Program at the Southern Research Station in cooperation with the Texas A&M Forest Service. These estimates are based on field data collected using the FIA annualized sample design and are...

Fire effects assessment using FIA data in the northern and central Rocky Mountains

Treesearch

Theresa B. Jain; Ralph Their; Wilson Michael

2003-01-01

Wildfires of 2000 and 2001 burned thousands of hectares in the Northern Rocky Mountains. Within the fire parameters, 162 Forest Inventory and Analysis (FIA) plots burned in Idaho and Montana where pre-wildfire information on forest structure, vegetation composition, soil productivity, and surface fuels was documented; thus providing a unique opportunity to assess...

Broad-Scale Assessment of Fuel Treatment Opportunities

Treesearch

Patrick D. Miles; Kenneth E. Skog; Wayne D. Shepperd; Elizabeth D. Reinhardt; Roger D. Fight

2006-01-01

The Forest Inventory and Analysis (FIA) program has produced estimates of the extent and composition of the Nation?s forests for several decades. FIA data have been used with a flexible silvicultural thinning option, a fire hazard model for preharvest and postharvest fire hazard assessment, a harvest economics model, and geospatial data to produce a Web-based tool to...

Evaluating Classified MODIS Satellite Imagery as a Stratification Tool

Treesearch

Greg C. Liknes; Mark D. Nelson; Ronald E. McRoberts

2004-01-01

The Forest Inventory and Analysis (FIA) program of the USDA Forest Service collects forest attribute data on permanent plots arranged on a hexagonal network across all 50 states and Puerto Rico. Due to budget constraints, sample sizes sufficient to satisfy national FIA precision standards are seldom achieved for most inventory variables unless the estimation process is...

Lava, VOG, and tropical forests: working with the FIA program in Hawaii

Treesearch

Thomas McGinley; Ashley Lehman

2015-01-01

In the winter of 2009, the Pacific Northwest Research Station initiated the ground implementation of their Forest Inventory and Analysis (FIA) program on the Hawaiian Islands. In the Pacific, people from the indigenous to the transplanted, hold intrinsic and utilitarian values of their forests that often differ considerably from values of mainstream mainland USA. These...

Estimating tree cavity distributions from historical FIA data

Treesearch

Mark D. Nelson; Charlotte Roy

2012-01-01

Tree cavities provide important habitat features for a variety of wildlife species. We describe an approach for using historical FIA data to estimate the number of trees containing cavities during the 1990s in seven states of the Upper Midwest. We estimated a total of 280 million cavity-containing trees. Iowa and Missouri had the highest percentages of cavity-...

The virtual analyst program: automated data mining, error analysis, and reporting

Treesearch

W. Keith Moser; Mark H. Hansen; Patrick Miles; Ronald E. McRoberts

2007-01-01

The Forest Inventory and Analysis (FIA) program of the U.S. Department of Agriculture Forest Service conducts ongoing comprehensive inventories of the forest resources of the United States. The Northern Region FIA (NFIA) program has three tasks: (1) core reporting function, which produces the annual and 5-year inventory reports; (2) forest health measurements; and (3)...

FIAMODEL : a new link for geographic analyses of inventory data

Treesearch

David Reed; Kurt Pregitzer; Scott A. Pugh; Patrick Miles

2001-01-01

The USDA Forest Service Forest Inventory and Analysis (FIA) data are widely used throughtout the United States for analyses of forest status and trends, landscape-level forest composition, and other forest characteristics. A new software product, FIAMODEL, is available for analyzing FIA data within the ArcView (ESRI,Inc.) geographic information system. The software...

Building the Forest Inventory and Analysis Tree-Ring Data set

Treesearch

Robert J. DeRose; John D. Shaw; James N. Long

2017-01-01

The Interior West Forest Inventory and Analysis (IW-FIA) program measures forestland conditions at great extent with relatively high spatial resolution, including the collection of tree-ring data. We describe the development of an unprecedented spatial tree-ring data set for the IW-FIA that enhances the baseline plot data by incorporating ring-width increment measured...

Forest Resources of Isle Royale National Park 2010

Treesearch

Wilfred J. Previant; Linda M. Nagel; Scott A. Pugh; Christopher W. Woodall

2012-01-01

This publication provides a baseline overview of forest resources for Isle Royale National Park (Isle Royale) using data from the Forest Inventory and Analysis (FIA) Program of the U.S. Department of Agriculture, Forest Service. The availability of permanent FIA plots allows for the first-ever comparison of Isle Royale's forest conditions (2006-2010) to reserved...

Fragmentation statistics for FIA: designing an approach

Treesearch

Rachel Riemann; Andrew Lister; Michael Hoppus; Tonya Lister

2002-01-01

The USDA Forest Inventory and Analysis (FIA) program collects data on the amount of forest, as well as on characteristics such as forest type, tree volume, species composition, and size and age classes. However, little data are obtained nationwide on forest fragmentation-how that forest is distributed and in what land use/land cover context-factors that can...

Texas, 2008 forest inventory and analysis factsheet

Treesearch

James Bentley

2011-01-01

This science update summarizes the findings of the first statewide annual inventory conducted by the Southern Forest Inventory and Analysis (FIA) Program in cooperation with the Texas Forest Service of the forest resource attributes in Texas. The 254 counties of Texas are consolidated into seven FIA survey units—southeast (unit 1), the northeast (unit 2), the north...

Forests of east Texas, 2015

Treesearch

Kerry J.W. Dooley

2017-01-01

This resource update provides an overview of forest resources in east Texas based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station (SRS) in cooperation with Texas A&M Forest Service. The 254 counties of Texas are consolidated into seven FIA survey units—Southeast (unit 1),...

Hardwood Projections For Southeastern U.S.

Treesearch

William Bechtold

1988-01-01

Much of what is covered here is based on data collected by the Forest Inventory and Analysis (FIA) Work Unit of the Forest Service Southeastern Forest Experiment Station. Southeast FIA is responsible of monitoring the forest resources of Florida, Georgia, North Carolina, South Carolina, and Virginia. The first survey of the Southeast began in Florida in 1934. Our field...

The poor man's Geographic Information System: plot expansion factors

Treesearch

Paul C. Van Deusen

2007-01-01

Plot expansion factors can serve as a crude Geographic Information System for users of Forest Inventory and Analysis (FIA) data. Each FIA plot has an associated expansion factor that is often interpreted as the number of forested acres that the plot represents. The derivation of expansion factors is discussed and it is shown that the mapped plot design requires a...

Relating FIA data to habitat classifications via tree-based models of canopy cover

Treesearch

Mark D. Nelson; Brian G. Tavernia; Chris Toney; Brian F. Walters

2012-01-01

Wildlife species-habitat matrices are used to relate lists of species with abundance of their habitats. The Forest Inventory and Analysis Program provides data on forest composition and structure, but these attributes may not correspond directly with definitions of wildlife habitats. We used FIA tree data and tree crown diameter models to estimate canopy cover, from...

Puerto Rico's forest inventory: adapting the forest inventory and analysis program to a Caribbean island.

Treesearch

T. J. Brandeis

2003-01-01

Rapid Changes in vegetation over short distances, high species diversity, and fragmented landscape challege the implementation of the Forest service's Forest inventory and Analysis (FIA)program on Puerto Rico. Applying the hexagonal FIA grid as used on the continental United States, the Forest service is installing a new forest sampling and monitoring framework...

D.B.H. and Survival Analysis: A New Methodology for Assessing Forest Inventory Mortality

Treesearch

Christopher W. Woodall; Patricia L. Grambsch; William Thomas

2005-01-01

Tree mortality has typically been assessed in Forest Inventory and Analysis (FIA) studies through summaries of mortality by location, species, and causal agents. Although these methods have historically been used for most of FIA's tree mortality analyses, they are inadequate for robust assessment of mortality trends and dynamics. To offer a new method of analyzing...

A density management diagram for even-aged ponderosa pine stands

Treesearch

James N. Long; John D. Shaw

2005-01-01

We developed a density management diagram (DMD) for ponderosa pine using Forest Inventory and Analysis (FIA) data. Analysis plots were drawn from all FIA plots in the western United States on which ponderosa pine occurred. A total of 766 plots met the criteria for analysis. Selection criteria were for purity, defined as ponderosa pine basal area 80% of plot basal area...

East Texas, 2011 forest inventory and analysis factsheet

Treesearch

Jason A. Cooper; James W. Bentley

2012-01-01

This science update summarizes the findings of the annual inventory conducted by the Southern Forest Inventory and Analysis (FIA) Program in cooperation with the Texas Forest Service of the forest resource attributes in east Texas. The 254 counties of Texas are consolidated into 7 FIA survey units—southeast (unit 1), northeast (unit 2), north central (unit 3), south (...

Updating the southern nonnative plant watch list: the future of NNIP Monitoring in the south

Treesearch

Christopher M. Oswalt; Sonja N. Oswalt; Lewis Zimmerman

2012-01-01

The Southern Research Station (SRS) Forest Inventory and Analysis (FIA) Program began monitoring nonnative invasive plant (NNIP) species in 2001 in response to a growing desire to track potential forest health threats on United States forest land. The SRS-FIA NNIP program has produced significant results and contributed considerably to the understanding of the...

Analyzing lichen indicator data in the Forest Inventory and Analysis Program

Treesearch

Susan Will-Wolf

2010-01-01

Lichens are one of several forest health indicators sampled every year for a subset of plots on the permanent grid established by the Forest Inventory and Analysis (FIA) Program of the U.S. Department of Agriculture Forest Service. This report reviews analysis procedures for standard FIA lichen indicator data. Analyses of lichen data contribute to state, regional, and...

A density management diagram for even-aged Sierra Nevada mixed-conifer stands

Treesearch

James N. Long; John D. Shaw

2012-01-01

We have developed a density management diagram (DMD) for even-aged mixed-conifer stands in the Sierra Nevada Mountains using forest inventory and analysis (FIA) data. Analysis plots were drawn from FIA plots in California, southern Oregon, and western Nevada which included those conifer species associated with the mixed-conifer forest type. A total of 204 plots met the...

A Guide to nonnative invasive plants inventoried in the north by Forest Inventory and Analysis

Treesearch

Cassandra Olson; Anita F. Cholewa

2009-01-01

The Forest Inventory and Analysis (FIA) program of the U.S. Forest Service is an ongoing endeavor mandated by Congress to determine the extent, condition, volume, growth, and depletions of timber on the Nation's forest land. FIA has responded to a growing demand for other information about our forests including, but not limited to,...

i-Tree and urban FIA—what's the connection?

Treesearch

David J. Nowak

2015-01-01

The i-Tree program (www.itreetools.org) was developed to assess ecosystem services and values from trees and forests based on measured forest data. The i-Tree program is currently being integrated with FIA data to assess various ecosystem services and values from urban FIA data. This presentation will overview the history and use of i-Tree; the various tools of i-Tree...

Lichens, ozone, and forest health - exploring cross-indicator analyses with FIA data

Treesearch

Susan Will-Wolf; Sarah Jovan

2009-01-01

Does air pollution risk represented by a lichen bioindicator of air pollution, an ozone bioindicator, or a combination of both, correlate with forest health as reflected by condition of tree crowns and other variables? We conducted pilot analyses to answer this question using Forest Inventory and Analysis (FIA) data from the Sierra Nevada region of California and the...

Using Forest Service forest inventory and analysis data to estimate regional oak decline and oak mortality

Treesearch

Kathryn W. Kromroy; Jennifer Juzwik; Paul Castillo; Mark H. Hansen

2008-01-01

Damage and mortality data are collected as part of the US Forest Service, Forest Inventory and Analysis (FIA) ongoing assessments of the nation's timberlands. The usefulness and value of FIA tree data in assessing historical levels of oak decline and oak mortality were investigated for seven Midwestern states. The data were collected during two periodic...

Landscape Builder: software for the creation of initial landscapes for LANDIS from FIA data

Treesearch

William Dijak

2013-01-01

I developed Landscape Builder to create spatially explicit landscapes as starting conditions for LANDIS Pro 7.0 and LANDIS II landscape forest simulation models from classified satellite imagery and Forest Inventory and Analysis (FIA) data collected over multiple years. LANDIS Pro and LANDIS II models project future landscapes by simulating tree growth, tree species...

A comparison of FIA plot data derived from image pixels and image objects

Treesearch

Charles E. Werstak

2012-01-01

The use of Forest Inventory and Analysis (FIA) plot data for producing continuous and thematic maps of forest attributes (e.g., forest type, canopy cover, volume, and biomass) at the regional level from satellite imagery can be challenging due to differences in scale. Specifically, classification errors that may result from assumptions made between what the field data...

A comparison of carbon stock estimates and projections for the northeastern United States

Treesearch

Richard G. MacLean; Mark J. Ducey; Coeli M. Hoover

2014-01-01

We conducted a comparison of carbon stock estimates produced by three different methods using regional data from the USDA Forest Service Forest Inventory and Analysis (FIA). Two methods incorporated by the Forest Vegetation Simulator (FVS) were compared to each other and to the current FIA component ratio method. We also examined the uncalibrated performance of FVS...

How might FIA deliver more information on status and trends of non-timber forest products?

Treesearch

Stephen P. Prisley

2015-01-01

Data from the Forest Inventory and Analysis program (including the Timber Products Output portion) are critical for assessing the sustainability of US timber production. Private sector users of this information rely on it for strategic planning, and their strong support of the FIA program has helped to ensure funding and program viability. Non-timber forest products...

Descriptive statistics of tree crown condition in the Southern United States and impacts on data analysis and interpretation

Treesearch

KaDonna C. Randolph

2006-01-01

The U.S. Department of Agriculture Forest Service, Forest Inventory and Analysis Program (FIA) utilizes visual assessments of tree crown condition to monitor changes and trends in forest health. This report describes and discusses distributions of three FIA crown condition indicators (crown density, crown dieback, and foliage transparency) for trees in the Southern...

Forest biomass estimated from MODIS and FIA data in the Lake States: MN, WI and MI, USA

Treesearch

Daolan Zheng; Linda S. Heath; Mark J. Ducey

2007-01-01

This study linked the Moderate Resolution Imaging Spectrometer and USDA Forest Service, Forest Inventory and Analysis (FIA) data through empirical models established using high-resolution Landsat Enhanced Thematic Mapper Plus observations to estimate aboveground biomass (AGB) in three Lake States in the north-central USA. While means obtained from larger sample sizes...

East Texas, 2012—Forest Inventory and Analysis Factsheet

Treesearch

Thomas J. Brandeis; Jason A. Cooper; James W. Bentley

2014-01-01

This science update summarizes the findings of the statewide annual inventory of the forest resource attributes in Texas conducted by the Southern Forest Inventory and Analysis (FIA) Program in cooperation with the Texas A&M Forest Service. The 254 counties of Texas are consolidated into seven FIA survey units—southeast (unit 1), northeast (unit 2), north central (...

Forest inventory and analysis data for FVS modelers

Treesearch

Patrick D. Miles

2008-01-01

The USDA Forest Service, Forest Inventory and Analysis (FIA) program has been in continuous operation for over 70 years. FIA’s primary objective is to determine the extent, condition, volume, growth, and depletion of timber on the Nation’s forest land. To accomplish this objective, FIA collects sample plot information on all ownerships across the United States.

Spatial Information Needs on the Fishlake National Forest: Can FIA Help?

Treesearch

Robert B., Jr. Campbell; Renee A. O' Brien

2005-01-01

National forest staff members are frequently challenged to make assessments with existing information. They rarely have the time or resources to go to the field to gather new data specific to the question at hand. Forest Inventory and Analysis (FIA) data have proved useful in the past, but there is an increasing need for spatial depictions of forest resources to...

Rapid assessment of wildfire damage using Forest Inventory data: A case in Georgia

Treesearch

Richard A. Harper; John W. Coulsten; Jeffery A. Turner

2009-01-01

The rapid assessment of damage caused by natural disasters is essential for planning the appropriate amount of disaster relief funds and public communication. Annual Forest Inventory and Analysis (FIA) data provided initial estimates of damage to timberland in a timely manner to State leaders during the 2007 Georgia Bay Complex Wildfire in southeast Georgia. FIA plots...

Distributing FIA Information onto Segmented Landsat Thematic Mapper Images Stratified with Industrial Ground Data

Treesearch

Tripp Lowe; Chris Cieszewski; Michael Zasada; Jarek Zawadzki

2005-01-01

The ability to evaluate the ecological and economical effects of proposed modifications to Georgia's best management practices is an important issue in the State. We have incorporated tabular FIA data with Landsat Thematic Mapper satellite images and other spatial data to model Georgia's forested land and assess the area, volume, age, and site quality...

Summary and findings of the 2006 BLM Forest Lands Report

Treesearch

Tim Bottomley; Jim Menlove

2009-01-01

In 2006, the Bureau of Land Management (BLM) contracted with the Forest Service Forest Inventory and Analysis Program (FIA) to assist in the preparation of a report specific to all forest lands under the administration of the BLM. The BLM requested that the FIA provide information on the extent and general conditions of BLM- managed forests and woodlands, within...

Comparing alternatives for increasing sampling intensity in forest inventories

Treesearch

J. Blackard; P. Patterson

2014-01-01

Each of the U.S. Forest Service’s Forest Inventory and Analysis (FIA) regions has an occasional need to intensify the national sampling grid. A variety of methodologies exist within the various FIA regions and National Forest Systems regions for constructing plot intensifications, and there is no consensus on a national procedure The primary objectives of this paper...

A stem-map model for predicting tree canopy cover of Forest Inventory and Analysis (FIA) plots

Treesearch

Chris Toney; John D. Shaw; Mark D. Nelson

2009-01-01

Tree canopy cover is an important stand characteristic that affects understory light, fuel moisture, decomposition rates, wind speed, and wildlife habitat. Canopy cover also is a component of most definitions of forest land used by US and international agencies. The USDA Forest Service Forest Inventory and Analysis (FIA) Program currently does not provide a national...

An assessment of garlic mustard in northern U.S. forests

Treesearch

Cassandra M. Kurtz; Mark H. Hansen

2014-01-01

This publication is part of a series that provides an overview of the presence of invasive plant species monitored on an extensive systematic network of plots measured by the Forest Inventory and Analysis (FIA) program of the U.S. Forest Service, Northern Research Station (NRS). Each research note features one of the invasive plants monitored on forested plots by FIA...

Statistics and quality assurance for the Northern Research Station Forest Inventory and Analysis Program, 2016

Treesearch

Dale D. Gormanson; Scott A. Pugh; Charles J. Barnett; Patrick D. Miles; Randall S. Morin; Paul A. Sowers; Jim Westfall

2017-01-01

The U.S. Forest Service Forest Inventory and Analysis (FIA) program collects sample plot data on all forest ownerships across the United States. FIA's primary objective is to determine the extent, condition, volume, growth, and use of trees on the Nation's forest land through a comprehensive inventory and analysis of the Nation's forest resources. The...

Forest Inventory and Analysis National Data Quality Assessment Report for 2000 to 2003

Treesearch

James E. Pollard; James A. Westfall; Paul L. Patterson; David L. Gartner; Mark Hansen; Olaf Kuegler

2006-01-01

The Forest Inventory and Analysis program (FIA) is the key USDA Forest Service (USFS) program that provides the information needed to assess the status and trends in the environmental quality of the Nation's forests. The goal of the FIA Quality Assurance (QA) program is to provide a framework to assure the production of complete, accurate and unbiased forest...

Using FIA inventory plot data to assess NTFP production possibilities

Treesearch

Jobriath Kauffman; James Chamberlain; Stephen Prisley

2015-01-01

The US Forest Service, Forest Inventory and Analysis (FIA) program collects data on a wealth of variables related to trees and understory species in forests. Some of these trees and plants produce non-timber forest products (NTFPs; e.g., seeds, fruit, bark, sap, roots) that are harvested for their culinary and medicinal values. As example, the cones of Pinus...

Model-based time-series analysis of FIA panel data absent re-measurements

Treesearch

Raymond L. Czaplewski; Mike T. Thompson

2013-01-01

An epidemic of lodgepole pine (Pinus contorta) mortality from the mountain pine beetle (Dendroctonus ponderosae) has swept across the Interior West. Aerial surveys monitor the areal extent of the epidemic, but only Forest Inventory and Analysis (FIA) field data support a detailed assessment at the tree level. Dynamics of the lodgepole pine population occur at a more...

Analyzing Regional FIA Data In The ArcView Geographic Information System

Treesearch

David Reed; Scott Pugh; Pat Miles; Kurt Pregitzer

2001-01-01

The ArcView? Geographic Information System (GIS)is probably the GIS that is most widely used by federal and state natural resource management agencies, industries, and non-profit institutions. As such, there is a great deal of expertise and comfort with this package within the FIA user community. The North Central Research Station and Michigan Technological University...

Alternatives to estimate statewide changes in aspen cover type volumes

Treesearch

Curtis L. VanderSchaaf

2015-01-01

For Minnesota, the only data available to conduct regional or state-wide level assessments across all ownerships is the Forest Inventory and Analysis Program (FIA). Some of the many alternatives available to estimate regional changes in standing volume are referred to here as 1.) FIA alternative, 2.) a commonly applied growth and yield system referred to as Walters and...

Understory vegetation data quality assessment for the Interior West Forest and Inventory Analysis program

Treesearch

Paul L. Patterson; Renee A. O' Brien

2011-01-01

The Interior West Forest Inventory and Analysis (IW-FIA) program of the USDA Forest Service collects field data on understory vegetation structure that have broad applications. In IW-FIA one aspect of quality assurance is assessed based on the repeatability of field measurements. The understory vegetation protocol consists of two suites of measurements; (1) the...

Integration of a Capacitive EIS Sensor into a FIA System for pH and Penicillin Determination

PubMed Central

Rolka, David; Poghossian, Arshak; Schöning, Michael J.

2004-01-01

A field-effect based capacitive EIS (electrolyte-insulator-semiconductor) sensor with a p-Si-SiO2-Ta2O5 structure has been successfully integrated into a commercial FIA (flow-injection analysis) system and system performances have been proven and optimised for pH and penicillin detection. A flow-through cell was designed taking into account the requirement of a variable internal volume (from 12 μl up to 48 μl) as well as an easy replacement of the EIS sensor. FIA parameters (sample volume, flow rate, distance between the injection valve and the EIS sensor) have been optimised in terms of high sensitivity and reproducibility as well as a minimum dispersion of the injected sample zone. An acceptable compromise between different FIA parameters has been found. For the cell design used in this study, best results have been achieved with a flow rate of 1.4 ml/min, distance between the injection valve and the EIS sensor of 6.5 cm, probe volume of 0.75 ml, cell internal volume of 12 μl. A sample throughput of at least 15 samples/h was typically obtained.

The combination of four analytical methods to explore skeletal muscle metabolomics: Better coverage of metabolic pathways or a marketing argument?

PubMed

Bruno, C; Patin, F; Bocca, C; Nadal-Desbarats, L; Bonnier, F; Reynier, P; Emond, P; Vourc'h, P; Joseph-Delafont, K; Corcia, P; Andres, C R; Blasco, H

2018-01-30

Metabolomics is an emerging science based on diverse high throughput methods that are rapidly evolving to improve metabolic coverage of biological fluids and tissues. Technical progress has led researchers to combine several analytical methods without reporting the impact on metabolic coverage of such a strategy. The objective of our study was to develop and validate several analytical techniques (mass spectrometry coupled to gas or liquid chromatography and nuclear magnetic resonance) for the metabolomic analysis of small muscle samples and evaluate the impact of combining methods for more exhaustive metabolite covering. We evaluated the muscle metabolome from the same pool of mouse muscle samples after 2 metabolite extraction protocols. Four analytical methods were used: targeted flow injection analysis coupled with mass spectrometry (FIA-MS/MS), gas chromatography coupled with mass spectrometry (GC-MS), liquid chromatography coupled with high-resolution mass spectrometry (LC-HRMS), and nuclear magnetic resonance (NMR) analysis. We evaluated the global variability of each compound i.e., analytical (from quality controls) and extraction variability (from muscle extracts). We determined the best extraction method and we reported the common and distinct metabolites identified based on the number and identity of the compounds detected with low analytical variability (variation coefficient<30%) for each method. Finally, we assessed the coverage of muscle metabolic pathways obtained. Methanol/chloroform/water and water/methanol were the best extraction solvent for muscle metabolome analysis by NMR and MS, respectively. We identified 38 metabolites by nuclear magnetic resonance, 37 by FIA-MS/MS, 18 by GC-MS, and 80 by LC-HRMS. The combination led us to identify a total of 132 metabolites with low variability partitioned into 58 metabolic pathways, such as amino acid, nitrogen, purine, and pyrimidine metabolism, and the citric acid cycle. This combination also showed that the contribution of GC-MS was low when used in combination with other mass spectrometry methods and nuclear magnetic resonance to explore muscle samples. This study reports the validation of several analytical methods, based on nuclear magnetic resonance and several mass spectrometry methods, to explore the muscle metabolome from a small amount of tissue, comparable to that obtained during a clinical trial. The combination of several techniques may be relevant for the exploration of muscle metabolism, with acceptable analytical variability and overlap between methods However, the difficult and time-consuming data pre-processing, processing, and statistical analysis steps do not justify systematically combining analytical methods. Copyright © 2017 Elsevier B.V. All rights reserved.

Polyphenols Determination in Olive Oil Samples Based on a Thick Film Voltammetric Sensor and a Tyrosinase Biosensor

NASA Astrophysics Data System (ADS)

Capannesi, Cecilia; Palchetti, Ilaria; Mascini, Marco

2000-12-01

The aim of the present work was to compare different techniques to evaluate the variation with the storage time and storage conditions in the phenolic content of an extra-virgin olive oil. A disposable screen-printed sensor (SPE) was coupled with differential pulse voltammetry (DPV) to determine the phenolic fractions after extraction with glycine buffer; DPV parameters were chosen in order to study oxidation peak of oleuropein, that was used as reference compound. Moreover a tyrosinase based biosensor operating in organic solvent (hexane) was assembled, using an amperometric oxygen probe as transducer. Calibration curves were realised in flow injection analysis (F.I.A.) using phenol as substrate. Both of these methods are easy to operate, require no extraction (biosensor) or a rapid extraction procedure (SPE), and the analysis time is short (min.). The results obtained with these two innovative procedures were compared with classical spectrophotometric assay using the Folin-Ciocalteau reagent. Other extra-virgin olive oil quality parameters were investigated with classical methods in order to better define the alteration process and results are reported.

The determination of levofloxacin by flow injection analysis using UV detection, potentiometry, and conductometry in pharmaceutical preparations.

PubMed

Altiokka, G; Atkosar, Z; Can, N O

2002-10-15

A flow injection analysis (FIA) using UV detection, potentiometry and conductometry for levofloxacin (LVF) are described in this study. The best solvent system was found to consist of 0.2 M acetate buffer at pH 3 having 10% MeOH. A flow rate of 1 ml min(-1) was pumped and active material was detected at 288 nm. The detection limit (LOD) and limit of quantification (LOQ) for FIA were calculated to be 3 x 10(-7) M (S/N = 3) and 1 x 10(-7) M (S/N = 10), respectively. In the analysis of tablets, the RSD values were found to be 0.83, 0.98 and 0.99 for FIA, potentiometric and conductometric methods, respectively. Copyright 2002 Elsevier Science B.V.

Field strategies for the calibration and validation of high-resolution forest carbon maps: Scaling from plots to a three state region MD, DE, & PA, USA.

NASA Astrophysics Data System (ADS)

Dolan, K. A.; Huang, W.; Johnson, K. D.; Birdsey, R.; Finley, A. O.; Dubayah, R.; Hurtt, G. C.

2016-12-01

In 2010 Congress directed NASA to initiate research towards the development of Carbon Monitoring Systems (CMS). In response, our team has worked to develop a robust, replicable framework to quantify and map aboveground forest biomass at high spatial resolutions. Crucial to this framework has been the collection of field-based estimates of aboveground tree biomass, combined with remotely detected canopy and structural attributes, for calibration and validation. Here we evaluate the field- based calibration and validation strategies within this carbon monitoring framework and discuss the implications on local to national monitoring systems. Through project development, the domain of this research has expanded from two counties in MD (2,181 km2), to the entire state of MD (32,133 km2), and most recently the tri-state region of MD, PA, and DE (157,868 km2) and covers forests in four major USDA ecological providences. While there are approximately 1000 Forest Inventory and Analysis (FIA) plots distributed across the state of MD, 60% fell in areas considered non-forest or had conditions that precluded them from being measured in the last forest inventory. Across the two pilot counties, where population and landuse competition is high, that proportion rose to 70% Thus, during the initial phases of this project 850 independent field plots were established for model calibration following a random stratified design to insure the adequate representation of height and vegetation classes found across the state, while FIA data were used as an independent data source for validation. As the project expanded to cover the larger spatial tri-state domain, the strategy was flipped to base calibration on more than 3,300 measured FIA plots, as they provide a standardized, consistent and available data source across the nation. An additional 350 stratified random plots were deployed in the Northern Mixed forests of PA and the Coastal Plains forests of DE for validation.

Invasive plant monitoring for northern U.S. forests

Treesearch

William H. McWilliams; Randall S. Morin; Katherine Johnson; W. Keith Moser; James A. Westfall

2012-01-01

Invasive plants are monitored through canopy cover estimates for a list of species developed by FIA for the northern region of the U.S. that is integrated with a national list. Nearly all of the invasive plants on the NRS-FIA list are exotic species, but a few native species are listed. Highly invasive native species such as rhizomatous fern are absent, making the list...

Disentangling forest change from forest inventory change: A case study from the US Interior West

Treesearch

Sara A. Goeking

2015-01-01

Long-term trends in forest attributes are typically assessed using strategic inventories such as the US Department of Agriculture (USDA) Forest Service’s Forest Inventory and Analysis (FIA) program. The implicit assumption of any trend analysis is that data are comparable over time. The 1998 Farm Bill tasked FIA with implementing nationally consistent protocols,...

The FIA Panel Design and Compatible Estimators for the Components of Change

Treesearch

Francis A. Roesch

2006-01-01

The FIA annual panel design and its relation to compatible estimation systems for the components of change are discussed. Estimation for the traditional components of growth, as presented by Meyer (1953, Forest Mensuration) is bypassed in favor of a focus on estimation for the discrete analogs to Eriksson’s (1995, For. Sci. 41(4):796- 822) time invariant redefinitions...

Repeated measures from FIA data facilitates analysis across spatial scales of tree growth responses to nitrogen deposition from individual trees to whole ecoregions

Treesearch

Charles H. (Hobie) Perry; Kevin J. Horn; R. Quinn Thomas; Linda H. Pardo; Erica A.H. Smithwick; Doug Baldwin; Gregory B. Lawrence; Scott W. Bailey; Sabine Braun; Christopher M. Clark; Mark Fenn; Annika Nordin; Jennifer N. Phelan; Paul G. Schaberg; Sam St. Clair; Richard Warby; Shaun Watmough; Steven S. Perakis

2015-01-01

The abundance of temporally and spatially consistent Forest Inventory and Analysis data facilitates hierarchical/multilevel analysis to investigate factors affecting tree growth, scaling from plot-level to continental scales. Herein we use FIA tree and soil inventories in conjunction with various spatial climate and soils data to estimate species-specific responses of...

Volume equations for the Northern Research Station's Forest Inventory and Analysis Program as of 2010

Treesearch

Patrick D. Miles; Andrew D. Hill

2010-01-01

The U.S. Forest Service's Forest Inventory and Analysis (FIA) program collects sample plot data on all forest ownerships across the United States. This report documents the methodology used to estimate live-tree gross, net, and sound volume for the 24 States inventoried by the Northern Research Station's (NRS) FIA unit. Sound volume is of particular interest...

Use of ancillary data to improve the analysis of forest health indicators

Treesearch

Dave Gartner

2013-01-01

In addition to its standard suite of mensuration variables, the Forest Inventory and Analysis (FIA) program of the U.S. Forest Service also collects data on forest health variables formerly measured by the Forest Health Monitoring program. FIA obtains forest health information on a subset of the base sample plots. Due to the sample size differences, the two sets of...

A Manual for the Identification of Invasive Plants in Southern Forests

Treesearch

Lewis Zimmerman

2012-01-01

This manual was created specifically for use by the U.S. Forest Service Southern Research Station (SRS), Forest Inventory and Analysis (FIA) field survey crews. The SRS FIA unit currently collects data on 33 invasive plants or groups across 13 States. The ability to accurately identify plant species in the field is a crucial component of monitoring a species’ presence...

Using interpreted large scale aerial photo data to enhance satellite-based mapping and explore forest land definitions

Treesearch

Tracey S. Frescino; Gretchen G. Moisen

2009-01-01

The Interior-West, Forest Inventory and Analysis (FIA), Nevada Photo-Based Inventory Pilot (NPIP), launched in 2004, involved acquisition, processing, and interpretation of large scale aerial photographs on a subset of FIA plots (both forest and nonforest) throughout the state of Nevada. Two objectives of the pilot were to use the interpreted photo data to enhance...

Using Forest Inventory and Analysis data to model plant-climate relationships

Treesearch

Nicholas L. Crookston; Gerald E. Rehfeldt; Marcus V. Warwell

2007-01-01

Forest Inventory and Analysis (FIA) data from 11 Western conterminous States were used to (1) estimate and map the climatic profiles of tree species and (2) explore how to include climate variables in individual tree growth equations used in the Forest Vegetation Simulator (FVS). On the first front, we found the FIA data to be useful as training data in Breiman's...

Potentials for mutually beneficial collaboration between FIA specialists and IEG-40 pathologists and geneticists working on fusiform rust

Treesearch

Ellis Cowling; KaDonna Randolph

2013-01-01

The purpose of this article is to encourage development of an enduring mutually beneficial collaboration between data and information analysts in the US Forest Service’s "Enhanced Forest Inventory and Analysis (FIA) Program" and forest pathologists and geneticists in the information exchange group (IEG) titled "Genetics and Breeding of Southern Forest...

The role of strategic forest inventories in aiding land management decision-making: Examples from the U.S

Treesearch

W. Keith Moser; Renate Bush; John D. Shaw; Mark H. Hansen; Mark D. Nelson

2010-01-01

A major challenge for today’s resource managers is the linking of standand landscape-scale dynamics. The U.S. Forest Service has made major investments in programs at both the stand- (national forest project) and landscape/regional (Forest Inventory and Analysis [FIA] program) levels. FIA produces the only comprehensive and consistent statistical information on the...

Diameter growth models using FIA data from the Northeastern, Southern, and North Central Research Stations

Treesearch

Veronica C. Lessard; Ronald E. McRoberts; Margaret R. Holdaway

2000-01-01

Nonlinear, individual-tree, distance-independent annual diameter growth models are presented for species in two ecoregions defined by R.G. Bailey in the northern Lake States and in parts of the central and southern regions of the U.S. The models were calibrated using Forest Inventory and Analysis (FIA) data from undisturbed plots on land classified as timberland across...

Using FIA and landsat observations to improve the spatial and temporal resolution of forest carbon estimates

Treesearch

Karen Schleeweis; Chengquan Huang; Khaldoun Rishmawi; Feng Aron Zhao; Jeffery G. Masek; Richard K. Houghton; Samuel N. Goward

2015-01-01

For nearly a decade, the USFS FIA, NASA, and the University of Maryland have collaborated on the NASA/NACP funded North American Forest Dynamics (NAFD) project, and developed new approaches for annual mapping of CONUS forest dynamics (1984-2011). Building on this foundation of empirical research and results, the collaboration will continue with a new Carbon Cycle...

Wall-to-wall Landsat TM classifications for Georgia in support of SAFIS using FIA plots for training and verification

Treesearch

William H. Cooke; Andrew J. Hartsell

2000-01-01

Wall-to-wall Landsat TM classification efforts in Georgia require field validation. Validation uslng FIA data was testing by developing a new crown modeling procedure. A methodology is under development at the Southern Research Station to model crown diameter using Forest Health monitoring data. These models are used to simulate the proportion of tree crowns that...

Mortality rates associated with crown health for eastern forest tree species

Treesearch

Randall S. Morin; KaDonna C. Randolph; Jim Steinman

2015-01-01

The condition of tree crowns is an important indicator of tree and forest health. Crown conditions have been evaluated during inventories of the US Forest Service Forest Inventory and Analysis (FIA) program since 1999. In this study, remeasured data from 55,013 trees on 2616 FIA plots in the eastern USA were used to assess the probability of survival among various tree...

Going public: accessing urban data and producing population estimates using the urban FIA database

Treesearch

Chris Edgar; Mark Hatfield

2015-01-01

In this presentation we describe the urban forest inventory database (U-FIADB) and demonstrate how to use the database to produce population estimates. Examples from the recently completed City of Austin inventory will be used to demonstrate the capabilities of the database. We will identify several features of U-FIADB that are different from the FIA database (FIADB)...

Fresh Ideas, Perspectives, and Protocols Associated with Forest Inventory and Analysis Surveys: Graduate Reports, 1974 to July 2001

Treesearch

Victor A. Rudis

2003-01-01

Graduate M.S. theses and Ph.D. dissertations were searched to provide a body of information associated with the U.S. Department of Agriculture, Forest Service, Forest Inventory and Analysis (FIA) database. Authors' abstracts were included if available in electronic form and published since 1974. Novel technical and nontraditional FIA data uses, as well as the...

Monitoring Across Borders: 2010 Joint Meeting of the Forest Inventory and Analysis (FIA) Symposium and the Southern Mensurationists

Treesearch

Will McWilliams; Francis A. Roesch

2012-01-01

These proceedings represent the range of topics covered during the 2010 Joint Meeting of the Forest Inventory and Analysis (FIA) Symposium and the Southern Mensurationists, October 5-7, 2010 in Knoxville, TN. The meeting was a gathering of forest scientists with a quantitative leaning and, as such, the papers discuss the aspects of the observation, estimation, modeling...

Integrating forest inventory and analysis data into a LIDAR-based carbon monitoring system

Treesearch

Kristofer D. Johnson; Richard Birdsey; Andrew O Finley; Anu Swantaran; Ralph Dubayah; Craig Wayson; Rachel Riemann

2014-01-01

Forest Inventory and Analysis (FIA) data may be a valuable component of a LIDAR-based carbon monitoring system, but integration of the two observation systems is not without challenges. To explore integration methods, two wall-to-wall LIDAR-derived biomass maps were compared to FIA data at both the plot and county levels in Anne Arundel and Howard Counties in Maryland...

Forest Inventory and Analysis (FIA) annual inventory answers the question: What is happening to pinyon-juniper woodlands?

Treesearch

John D. Shaw; Brytten E. Steed; Larry T. DeBlander

2005-01-01

Widespread mortality in the pinyon-juniper forest type is associated with several years of drought in the southwestern United States. A complex of drought, insects, and disease is responsible for pinyon mortality rates approaching 100% in some areas, while other areas have experienced little or no mortality. Implementation of the Forest Inventory and Analysis (FIA)...

A new FIA-Type strategic inventory (NFI)

Treesearch

Richard A. Grotefendt; Hans T. Schreuder

2006-01-01

New remote sensing technologies are now available to lower the cost of doing strategic surveys. A new sampling approach for the Forest Inventory and Analysis program (FIA) of the U.S.D.A. Forest Service is discussed involving a bi-sampling unit (BSU) that is composed of a field sample unit (FSU) centered within a large scale (1:1,000 to 1:3,000) photo sample unit (PSU...

Farmers and woods: a look at woodlands and woodland-owner intentions in the heartland

Treesearch

W. Keith Moser; Earl C. Leatherberry; Mark H. Hansen; Brett Butler

2005-01-01

This paper reports the results of a pilot study that explores the relationship between farm woodland owners` stated intentions for owning woodland, and their use of the land, with the structure and composition of the woodland. Two databases maintained by the USDA Forest Service, Forest Inventory and Analysis (FIA) program were used in the analysis-- the FIA forest...

Monitoring nontimber forest products using forest inventory data: an example with slippery elm bark

Treesearch

Jobriath S. Kauffman; Stephen P. Prisley; James L. Chamberlain

2015-01-01

The USDA Forest Service Forest Inventory and Analysi (FIA) program collects data on a wealth of variables related to trees in forests. Some of these trees produce nontimber forest products (NTFPs) (e.g., fruit, bark and sap) that are harvested for culinary, decorative, building, and medicinal purposes. At least 11 tree species inventoried by FIA are valued for their...

The national forest inventory of the United States of America

Treesearch

Ronald E. McRoberts

2008-01-01

The mission of the Forest Inventory and Analysis (FIA) program of the Forest Service, U.S. Department of Agriculture, is to conduct the national forest inventory of the United States of America for purposes of estimating the area of forest land; the volume, growth, and removal of forest resources; and the health of the forest. Users of FIA data, estimates, and related...

Impact of ecological and socioeconomic determinants on the spread of tallow tree in southern forest lands

Treesearch

Yuan Tan; Joseph Z. Fan; Christopher M. Oswalt

2010-01-01

Based on USDA Forest Service Forest Inventory and Analysis (FIA) database, relationships between the presence of tallow tree and related driving variables including forest landscape metrics, stand and site conditions, as well as natural and anthropogenic disturbances were analyzed for the southern states infested by tallow trees. Of the 9,966 re-measured FIA plots in...

Development and Validation of Spatially Explicit Habitat Models for Cavity-nesting Birds in Fishlake National Forest, Utah

Treesearch

Randall A., Jr. Schultz; Thomas C., Jr. Edwards; Gretchen G. Moisen; Tracey S. Frescino

2005-01-01

The ability of USDA Forest Service Forest Inventory and Analysis (FIA) generated spatial products to increase the predictive accuracy of spatially explicit, macroscale habitat models was examined for nest-site selection by cavity-nesting birds in Fishlake National Forest, Utah. One FIA-derived variable (percent basal area of aspen trees) was significant in the habitat...

Leveraging FIA data for analysis beyond forest reports: examples from the world of carbon

Treesearch

Brian F. Walters; Grant M. Domke; Christopher W. Woodall

2015-01-01

The Forest Inventory and Analysis program of the USDA Forest Service is the go-to source for data to estimate carbon stocks and stock changes for the annual national greenhouse gas inventory (NGHGI) of the United States. However, the different pools of forest carbon have not always been estimated directly from FIA measurements. As part of the new forest carbon...

Adding value to the FIA inventory: combining FIA data and satellite observations to estimate forest disturbance

Treesearch

Todd A. Schroeder; Gretchen G. Moisen; Sean P. Healey; Warren B. Cohen

2012-01-01

In addition to being one of the primary drivers of the net terrestrial carbon budget, forest disturbance also plays a critical role in regulating the surface energy balance, promoting biodiversity, and creating wildlife habitat. With climate change and an ever growing human population poised to alter the frequency and severity of disturbance regimes across the globe,...

New Mexico Forest Inventory and Analysis: American Recovery and Reinvestment Act Project, Field Report: 2010-2012

Treesearch

Mary Stuever; John Capuano

2014-01-01

For a 3-year period, from 2010-2012, the New Mexico Forestry Division utilized contractors to collect Forest Inventory and Analysis (FIA) data in New Mexico. Funded through the American Recovery and Reinvestment Act, the State partnered with the Interior West FIA Program. Together, both agencies collected data on approximately 6,450 plots. This effort represents the...

Trends in standing biomass in Interior West forests: Reassessing baseline data from periodic inventories

Treesearch

Sara A. Goeking

2012-01-01

Trends in U.S. forest biomass and carbon are assessed using Forest Inventory and Analysis (FIA) data relative to baseline assessments from the 1990s. The integrity of baseline data varies by state and depends largely on the comparability of periodic versus annual forest inventory data. In most states in the Interior West FIA region, the periodic inventory's sample...

The enhanced forest inventory and analysis program of the USDA forest service: historical perspective and announcements of statistical documentation

Treesearch

Ronald E. McRoberts; William A. Bechtold; Paul L. Patterson; Charles T. Scott; Gregory A. Reams

2005-01-01

The Forest Inventory and Analysis (FIA) program of the USDA Forest Service has initiated a transition from regional, periodic inventories to an enhanced national FIA program featuring annual measurement of a proportion of plots in each state, greater national consistency, and integration with the ground sampling component of the Forest Health Monitoring (FHM) program...

US Commercial Air Tour Crashes, 2000–2011: Burden, Fatal Risk Factors, and FIA Score Validation

PubMed Central

Ballard, Sarah-Blythe; Beaty, Leland P.; Baker, Susan P.

2013-01-01

Introduction This study provides new public health data concerning the US commercial air tour industry. Risk factors for fatality in air tour crashes were analyzed to determine the value of the FIA score in predicting fatal outcomes. Methods Using the Federal Aviation Administration’s (FAA) General Aviation and Air Taxi Survey and National Transportation Safety Board data, the incidence of commercial air tour crashes from 2000 through 2010 was calculated. Fatality risk factors for crashes occurring from 2000 through 2011 were analyzed using regression methods. The FIA score, Li and Baker’s fatality risk index, was validated using receiver operating characteristic (ROC) curves. Results The industry-wide commercial air tour crash rate was 2.7 per 100,000 flight hours. The incidence rates of Part 91 and 135 commercial air tour crashes were 3.4 and 2.3 per 100,000 flight hours, respectively (relative risk [RR] 1.5, 95% confidence interval [CI] 1.1–2.1, P=0.015). Of the 152 air tour crashes that occurred from 2000 through 2011, 30 (20%) involved at least one fatality and, on average, 3.5 people died per fatal crash. Fatalities were associated with three major risk factors: fire (Adjusted odds ratio [AOR] 5.1, 95% CI 1.5–16.7, P=0.008), instrument meteorological conditions (AOR 5.4, 95% CI 1.1–26.4, P=0.038), and off-airport location (AOR 7.2, 95% CI 1.6–33.2, P=0.011). The area under the FIA Score’s ROC curve was 0.79 (95% CI 0.71–0.88). Discussion Commercial air tour crash rates were high relative to similar commercial aviation operations. Disparities between Part 91 and 135 air tour crash rates reflect regulatory disparities that require FAA action. The FIA Score appeared to be a valid measurement of fatal risk in air tour crashes. The FIA should prioritize interventions that address the three major risk factors identified by this study. PMID:23631935

Unruptured intracranial aneurysms in the Familial Intracranial Aneurysm and International Study of Unruptured Intracranial Aneurysms cohorts: differences in multiplicity and location.

PubMed

Mackey, Jason; Brown, Robert D; Moomaw, Charles J; Sauerbeck, Laura; Hornung, Richard; Gandhi, Dheeraj; Woo, Daniel; Kleindorfer, Dawn; Flaherty, Matthew L; Meissner, Irene; Anderson, Craig; Connolly, E Sander; Rouleau, Guy; Kallmes, David F; Torner, James; Huston, John; Broderick, Joseph P

2012-07-01

Familial predisposition is a recognized nonmodifiable risk factor for the formation and rupture of intracranial aneurysms (IAs). However, data regarding the characteristics of familial IAs are limited. The authors sought to describe familial IAs more fully, and to compare their characteristics with a large cohort of nonfamilial IAs. The Familial Intracranial Aneurysm (FIA) study is a multicenter international study with the goal of identifying genetic and other risk factors for formation and rupture of IAs in a highly enriched population. The authors compared the FIA study cohort with the International Study of Unruptured Intracranial Aneurysms (ISUIA) cohort with regard to patient demographic data, IA location, and IA multiplicity. To improve comparability, all patients in the ISUIA who had a family history of IAs or subarachnoid hemorrhage were excluded, as well as all patients in both cohorts who had a ruptured IA prior to study entry. Of 983 patients enrolled in the FIA study with definite or probable IAs, 511 met the inclusion criteria for this analysis. Of the 4059 patients in the ISUIA study, 983 had a previous IA rupture and 657 of the remainder had a positive family history, leaving 2419 individuals in the analysis. Multiplicity was more common in the FIA patients (35.6% vs 27.9%, p<0.001). The FIA patients had a higher proportion of IAs located in the middle cerebral artery (28.6% vs 24.9%), whereas ISUIA patients had a higher proportion of posterior communicating artery IAs (13.7% vs 8.2%, p=0.016). Heritable structural vulnerability may account for differences in IA multiplicity and location. Important investigations into the underlying genetic mechanisms of IA formation are ongoing.

Greater Rupture Risk for Familial as Compared to Sporadic Unruptured Intracranial Aneurysms

PubMed Central

Broderick, Joseph P.; Brown, Robert D.; Sauerbeck, Laura; Hornung, Richard; Huston, John; Woo, Daniel; Anderson, Craig; Rouleau, Guy; Kleindorfer, Dawn; Flaherty, Matthew L.; Meissner, Irene; Foroud, Tatiana; Moomaw, E. Charles J.; Connolly, E. Sander

2009-01-01

Background The risk of intracranial aneurysm (IA) rupture in asymptomatic members of families who have multiple affected individuals is not known. Methods First-degree unaffected relatives of those with a familial history of IA who had a history of smoking or hypertension but no known IA were offered cerebral magnetic resonance angiography (MRA) and followed yearly as part of an NINDS-funded study of familial IA (FIA Study). Results 2874 subjects from 542 FIA families were enrolled. After study enrollment, MRAs were performed in 548 FIA family members with no known history of IA. Of these 548 subjects, 113 subjects (20.6%) had 148 IAs by MRA of whom 5 subjects had IA >= 7 mm. Two subjects with an unruptured IA by MRA/CTA (3 mm and 4mm ACOM) subsequently had rupture of their IA. This represents an annual rate of 1.2 ruptures per 100 subjects (1.2% per year, 95% CI of 0.14% to 4.3% per year). None of the 435 subjects with a negative MRA have had a ruptured IA. Survival curves between the MRA positive and negative cohorts were significantly different (p = 0.004). This rupture rate of unruptured IA in the FIA cohort of 1.2% per year is approximately 17 times higher than the rupture rate for subjects with an unruptured IA in the International Study of Unruptured Aneurysm Study with a matched distribution of IA size and location - 0.069% per year. Conclusions Small unruptured IAs in patients from FIA families may have a higher risk of rupture than sporadic unruptured IAs of similar size, which should be considered in the management of these patients. PMID:19228834

Greater rupture risk for familial as compared to sporadic unruptured intracranial aneurysms.

PubMed

Broderick, Joseph P; Brown, Robert D; Sauerbeck, Laura; Hornung, Richard; Huston, John; Woo, Daniel; Anderson, Craig; Rouleau, Guy; Kleindorfer, Dawn; Flaherty, Matthew L; Meissner, Irene; Foroud, Tatiana; Moomaw, E Charles J; Connolly, E Sander

2009-06-01

The risk of intracranial aneurysm (IA) rupture in asymptomatic members of families who have multiple affected individuals is not known. First-degree unaffected relatives of those with a familial history of IA who had a history of smoking or hypertension but no known IA were offered cerebral MR angiography (MRA) and followed yearly as part of a National Institute of Neurological Diseases and Stroke-funded study of familial IA (Familial Intracranial Aneurysm [FIA] Study). A total of 2874 subjects from 542 FIA Study families were enrolled. After study enrollment, MRAs were performed in 548 FIA Study family members with no known history of IA. Of these 548 subjects, 113 subjects (20.6%) had 148 IAs by MRA of whom 5 subjects had IA >or=7 mm. Two subjects with an unruptured IA by MRA/CT angiography (3-mm and 4-mm anterior communicating artery) subsequently had rupture of their IA. This represents an annual rate of 1.2 ruptures per 100 subjects (1.2% per year; 95% CI, 0.14% to 4.3% per year). None of the 435 subjects with a negative MRA have had a ruptured IA. Survival curves between the MRA-positive and -negative cohorts were significantly different (P=0.004). This rupture rate of unruptured IA in the FIA Study cohort of 1.2% per year is approximately 17 times higher than the rupture rate for subjects with an unruptured IA in the International Study of Unruptured Aneurysm Study with a matched distribution of IA size and location 0.069% per year. Small unruptured IAs in patients from FIA Study families may have a higher risk of rupture than sporadic unruptured IAs of similar size, which should be considered in the management of these patients.

Recent Development in Optical Chemical Sensors Coupling with Flow Injection Analysis

PubMed Central

Ojeda, Catalina Bosch; Rojas, Fuensanta Sánchez

2006-01-01

Optical techniques for chemical analysis are well established and sensors based on these techniques are now attracting considerable attention because of their importance in applications such as environmental monitoring, biomedical sensing, and industrial process control. On the other hand, flow injection analysis (FIA) is advisable for the rapid analysis of microliter volume samples and can be interfaced directly to the chemical process. The FIA has become a widespread automatic analytical method for more reasons; mainly due to the simplicity and low cost of the setups, their versatility, and ease of assembling. In this paper, an overview of flow injection determinations by using optical chemical sensors is provided, and instrumentation, sensor design, and applications are discussed. This work summarizes the most relevant manuscripts from 1980 to date referred to analysis using optical chemical sensors in FIA.

Characteristics of pinyon-juniper woodlands in Grand Staircase-Escalante National Monument: Changes since Monument establishment and prospects for future monitoring

Treesearch

Christopher Witt; John D. Shaw

2010-01-01

Recent data from the USDA Forest Service Forest Inventory and Analysis (FIA) program have documented spatial and temporal patterns of drought-related mortality across woodlands of the Southwest (Shaw et al. 2005). In the early 1990s, FIA collected data on forested land now included in Grand Staircase-Escalante National Monument (GSENM or the Monument) as part of a...

Remeasured FIA plots reveal tree-level diameter growth and tree mortality impacts of nitrogen deposition on California’s forests

Treesearch

Mark E. Fenn; Jeremy S. Fried; Haiganoush K. Preisler; Andrzej Bytnerowicz; Susan Schilling; Sarah Jovan; Olaf Kuegler

2015-01-01

The air in California’s forests spans a broad range of purity, from virtually no locally generated pollutants to highly elevated levels of pollutants in forests downwind of urban and agricultural source areas. Ten-year remeasurement data from Forest Inventory and Analysis (FIA) plots in California were used in combination with modelled atmospheric nitrogen (N)...

Baseline results from the Lichen Community Indicator Program in the Pacific Northwest: Air quality patterns and evidence of a nitrogen pollution problem

Treesearch

Sarah Jovan

2009-01-01

Why Are Epiphytic Lichen Communities Important? Lichens are one of the bioindicators used by the Forest Inventory and Analysis (FIA) Program to monitor forest health. To obtain data for use in its Lichen Community Indicator Program, FIA samples a regular network of permanent field plots to determine the composition of epiphytic, i.e., tree dwelling, lichen communities...

Modeling opportunities and feasibility of siting wood-fired electrical generating facilities to facilitate landscape-scale fuel treatment with FIA BioSum.

Treesearch

Jeremy S. Fried; Glenn Christensen; Dale Weyermann; R. Jamie Barbour; Roger Fight; Bruce Hiserote; Guy Pinjuv

2005-01-01

Utilization of small diameter trees is viewed by many as the key to making landscape-scale fuel treatment financially feasible. But little capacity currently exists for utilizing such material and capacity of sufficient scale to have a significant impact on the economics of small diameter removals will only be added if predictable feedstocks can be assured. The FIA...

The 2014 tanana inventory pilot: A USFS-NASA partnership to leverage advanced remote sensing technologies for forest inventory

Treesearch

Hans-Erik Andersen; Chad Babcock; Robert Pattison; Bruce Cook; Doug Morton; Andrew Finley

2015-01-01

Interior Alaska (approx. 112 million forested acres in size) is the last remaining forested area within the United States where the Forest Inventory and Analysis (FIA) program is not currently implemented. A joint NASA-FIA inventory pilot project was carried out in 2014 to increase familiarity with interior Alaska logistics and evaluate the utility of state-of-the-art...

Placing man in regional landscape classification: Use of Forest Survey data to assess human influences for southern U.S. forest ecosystems

Treesearch

Victor A. Rudis; John B. Tansey

1991-01-01

Information from plots surveyed by U.S.D.A., Forest Service, Forest Inventory and Analysis (FIA) units provides a basis for classifying human-dominated ecosystems at the regional scale of resolution.Attributes include forest stand measures, evidence of human influence, and other disturbances.Data from recent FIA surveys suggest that human influences are common to...

Stratifying FIA Ground Plots Using A 3-Year Old MRLC Forest Cover Map and Current TM Derived Variables Selected By "Decision Tree" Classification

Treesearch

Michael Hoppus; Stan Arner; Andrew Lister

2001-01-01

A reduction in variance for estimates of forest area and volume in the state of Connecticut was accomplished by stratifying FIA ground plots using raw, transformed and classified Landsat Thematic Mapper (TM) imagery. A US Geological Survey (USGS) Multi-Resolution Landscape Characterization (MRLC) vegetation cover map for Connecticut was used to produce a forest/non-...

Methods and equations for estimating aboveground volume, biomass, and carbon for trees in the U.S. forest inventory, 2010

Treesearch

Christopher W. Woodall; Linda S. Heath; Grant M. Domke; Michael C. Nichols

2011-01-01

The U.S. Forest Service, Forest Inventory and Analysis (FIA) program uses numerous models and associated coefficients to estimate aboveground volume, biomass, and carbon for live and standing dead trees for most tree species in forests of the United States. The tree attribute models are coupled with FIA's national inventory of sampled trees to produce estimates of...

Building capacity for providing canopy cover and canopy height at FIA plot locations using high-resolution imagery and leaf-off LiDAR

Treesearch

Rachel Riemann; Jarlath O' Neil-Dunne; Greg C. Liknes

2012-01-01

Tree canopy cover and canopy height information are essential for estimating volume, biomass, and carbon; defining forest cover; and characterizing wildlife habitat. The amount of tree canopy cover also influences water quality and quantity in both rural and urban settings. Tree canopy cover and canopy height are currently collected at FIA plots either in the field or...

Using FIA and GIS Data to Estimate Areas and Volumes of Potential Stream Management Zones and Road Beautifying Buffers

Treesearch

Michael Zasada; Chris J. Cieszewski; Roger C. Lowe; Jarek Zawadzki; Mike Clutter; Jacek P. Siry

2005-01-01

Georgia Stream Management Zones (SMZ) are voluntary and have an unknown extent and impact. We use FIA data, Landsat TM imagery, and GAP and other GIS data to estimate the acreages and volumes of these buffers. We use stream data classified into trout, perennial, and intermittent, combined with DEM files containing elevation values, to assess buffers with widths...

The role of pre-field operations at four forest inventory units: We can see the trees, not just the forest

Treesearch

Sara A. Goeking; Greg C. Liknes

2009-01-01

The Forest Inventory and Analysis (FIA) program attempts to inventory all forested lands throughout the United States. Each of the four FIA units has developed a process to minimize inventory costs by refraining from visiting those plots in the national inventory grid that are undoubtedly nonforest. We refer to this process as pre-field operations. Until recently, the...

Synergistic use of FIA plot data and Landsat 7 ETM+ images for large area forest mapping

Treesearch

Chengquan Huang; Limin Yang; Collin Homer; Michael Coan; Russell Rykhus; Zheng Zhang; Bruce Wylie; Kent Hegge; Andrew Lister; Michael Hoppus; Ronald Tymcio; Larry DeBlander; William Cooke; Ronald McRoberts; Daniel Wendt; Dale Weyermann

2002-01-01

FIA plot data were used to assist in classifying forest land cover from Landsat imagery and relevant ancillary data in two regions of the U.S.: one around the Chesapeake Bay area and the other around Utah. The overall accuracies for the forest/nonforest classification were over 90 percent and about 80 percent, respectively, in the two regions. The accuracies for...

Using SaTScanTM spatial-scan software with national forest inventory data: a case study in South Carolina

Treesearch

KaDonna Randolph

2017-01-01

The USDA Forest Service Forest Inventory and Analysis (FIA) program makes and keeps current an inventory of all forest land in the United States. To comply with privacy laws while at the same time offering its data to the public, FIA makes approximate plot locations available through a process known as perturbing ("fuzzing") and swapping. The free spatial...

Preparation of Forest Inventory and Analysis (FIA) and State Soil Geographic Data Base (STATSGO) data for global change research in the Eastern United States

Treesearch

Loius R. Iverson; Anantha M. G. Prasad; Charles T. Scott

1996-01-01

The USDA Forest Service's Forest Inventory and Analysis (FIA) and the Natural Resource Conservation Service's State Soil Geographic (STATSGO) data bases provide valuable natural resource data that can be analyzed at the national scale. When coupled with other data (e.g., climate), these data bases can provide insights into factors associated with current and...

Incorporation of Precipitation Data Into FIA Analyses: A Case Study of Factors Influencing Susceptibility to Oak Decline in Southern Missouri, U.S.A.

Treesearch

W. Keith Moser; Greg Liknes; Mark Hansen; Kevin Nimerfro

2005-01-01

The Forest Inventory and Analysis program at the North Central Research Station focuses on understanding the forested ecosystems in the North Central and Northern Great Plains States through analyzing the results of annual inventories. The program also researches techniques for data collection and analysis. The FIA process measures the above-ground vegetation and the...

Change detection for soil carbon in the forest inventory and analysis

Treesearch

An-Min Wu; Edward A. Nater; Charles H. Perry; Brent J. Dalzell; Barry T. Wilson

2015-01-01

Estimates of carbon stocks and stock changes in the U.S. Department of Agriculture Forest Service’s Forest Inventory and Analysis (FIA) Program are reported as the official United States submission to the UN Framework Convention on Climate Change. Soil, as a critical component of the forest carbon stocks, has been sampled in about 10-year intervals in FIA with the re-...

Feasibility of high-density climate reconstruction based on Forest Inventory and Analysis (FIA) collected tree-ring data

Treesearch

R. Justin DeRose; Shih-Yu Wang; John D. Shaw

2013-01-01

This study introduces a novel tree-ring dataset, with unparalleled spatial density, for use as a climate proxy. Ancillary Douglas fir and pinyon pine tree-ring data collected by the U.S. Forest Service Forest Inventory and Analysis Program (FIA data) were subjected to a series of tests to determine their feasibility as climate proxies. First, temporal coherence between...

Assessing land ownership as a driver of change in the distribution, structure, and composition of California's forests.

NASA Astrophysics Data System (ADS)

Easterday, K.; Kelly, M.; McIntyre, P. J.

2015-12-01

Climate change is forecasted to have considerable influence on the distribution, structure, and function of California's forests. However, human interactions with forested landscapes (e.g. fire suppression, resource extraction and etc.) have complicated scientific understanding of the relative contributions of climate change and anthropogenic land management practices as drivers of change. Observed changes in forest structure towards smaller, denser forests across California have been attributed to both climate change (e.g. increased temperatures and declining water availability) and management practices (e.g. fire suppression and logging). Disentangling how these drivers of change act both together and apart is important to developing sustainable policy and land management practices as well as enhancing knowledge of human and natural system interactions. To that end, a comprehensive historical dataset - the Vegetation Type Mapping project (VTM) - and a modern forest inventory dataset (FIA) are used to analyze how spatial variations in vegetation composition and structure over a ~100 year period can be explained by land ownership.Climate change is forecasted to have considerable influence on the distribution, structure, and function of California's forests. However, human interactions with forested landscapes (e.g. fire suppression, resource extraction and etc.) have complicated scientific understanding of the relative contributions of climate change and anthropogenic land management practices as drivers of change. Observed changes in forest structure towards smaller, denser forests across California have been attributed to both climate change (e.g. increased temperatures and declining water availability) and management practices (e.g. fire suppression and logging). Disentangling how these drivers of change act both together and apart is important to developing sustainable policy and land management practices as well as enhancing knowledge of human and natural system interactions. To that end, a comprehensive historical dataset - the Vegetation Type Mapping project (VTM) - and a modern forest inventory dataset (FIA) are used to analyze how spatial variations in vegetation composition and structure over a ~100 year period can be explained by land ownership.

Implementing a national process for estimating growth, removals, and mortality at the Pacific Northwest’s Forest Inventory and Analysis’s Region: modeling diameter growth

Treesearch

Olaf. Kuegler

2015-01-01

The Pacific Northwest Research Station’s Forest Inventory and Analysis Unit began remeasurement of permanently located FIA plots under the annualized design in 2011. With remeasurement has come the need to implement the national FIA system for compiling estimates of forest growth, removals, and mortality. The national system requires regional diameter-growth models to...

Statistics and quality assurance for the Northern Research Station Forest Inventory and Analysis Program

Treesearch

Dale D. Gormanson; Scott A. Pugh; Charles J. Barnett; Patrick D. Miles; Randall S. Morin; Paul A. Sowers; James A. Westfall

2018-01-01

The U.S. Forest Service Forest Inventory and Analysis (FIA) program collects sample plot data on all forest ownerships across the United States. FIA’s primary objective is to determine the extent, condition, volume, growth, and use of trees on the Nation’s forest land through a comprehensive inventory and analysis of the Nation’s forest resources. The FIA program...

Reducing uncertainty and increasing consistency: technical improvements to forest carbon pool estimation using the national forest inventory of the US

Treesearch

C.W. Woodall; G.M. Domke; J. Coulston; M.B. Russell; J.A. Smith; C.H. Perry; S.M. Ogle; S. Healey; A. Gray

2015-01-01

The FIA program does not directly measure forest C stocks. Instead, a combination of empirically derived C estimates (e.g., standing live and dead trees) and models (e.g., understory C stocks related to stand age and forest type) are used to estimate forest C stocks. A series of recent refinements in FIA estimation procedures have sought to reduce the uncertainty...

A report on the potential use of USDA Forest Service forest inventory and analysis data by the Bureau of Land Management

Treesearch

Bill Williams; Tracey S. Frescino; Larry T. DeBlander; Sharon W. Woudenberg; Michael Wilson

2006-01-01

The Bureau of Land Management (BLM) does not have a consistent internal program or source of vegetation data to use for strategic level planning, such as in resource management plans. This technical note discusses and evaluates the potential of the USDA Forest Service Forest Inventory and Analysis (FIA) Program to assist the BLM in filling this data gap. The FIA...

Assessing the impact of a mountain pine beetle infestation on stand structure of lodgepole pine forests in Colorado using the Forest Inventory and Analysis Annual forest inventory

Treesearch

Michael T. Thompson

2017-01-01

The Forest Inventory and Analysis (FIA) annual inventory system began in Colorado in 2002, which coincided with the onset of a major mountain pine beetle (Dendroctonus ponderosae) epidemic. The mortality event, coupled with 11 years of annual inventory data, provided an opportunity to assess the usefulness of the FIA annual inventory system for quantifying the effects...

Forest inventory and analysis program in the Western U.S.

Treesearch

Ashley Lehman

2015-01-01

The Pacific Northwest (PNW) Research Station’s Forest Inventory and Analysis (FIA) program of the USDA Forest Service monitors and reports on the status and trends of the Pacific Island’s forest resources and ecosystem services. Since 2001 the FIA program has partnered with State and Private Forestry’s, Region 5 and the local governments in the U.S. Affiliated Western...

Forest inventory and analysis program in the Western U.S

Treesearch

Ashley Lehman

2015-01-01

The Pacific Northwest (PNW) Research Station’s Forest Inventory and Analysis (FIA) program of the USDA Forest Service monitors and reports on the status and trends of the Pacific Island’s forest resources and ecosystem services. Since 2001 the FIA program has partnered with State and Private Forestry’s, Region 5 and the local governments in the U.S. Affiliated Western...

FIA data and species diversity—successes and failures using multivariate analysis techniques, spatial lag and error models and hot-spot analysis

Treesearch

Andrew J. Hartsell

2015-01-01

This study will investigate how global and local predictors differ with varying spatial scale in relation to species evenness and richness in the gulf coastal plain. Particularly, all-live trees >= one-inch d.b.h. Forest Inventory and Analysis (FIA) data was used as the basis for the study. Watersheds are defined by the USGS 12 digit hydrologic units. The...

Progress in adapting k-NN methods for forest mapping and estimation using the new annual Forest Inventory and Analysis data

Treesearch

Reija Haapanen; Kimmo Lehtinen; Jukka Miettinen; Marvin E. Bauer; Alan R. Ek

2002-01-01

The k-nearest neighbor (k-NN) method has been undergoing development and testing for applications with USDA Forest Service Forest Inventory and Analysis (FIA) data in Minnesota since 1997. Research began using the 1987-1990 FIA inventory of the state, the then standard 10-point cluster plots, and Landsat TM imagery. In the past year, research has moved to examine...

A New Microfluidic Polymer Chip with an Embedded Cationic Surfactant Ion-selective Optode as a Detector for the Determination of Cationic Surfactants.

PubMed

Ashagre, Mekonnen Abiyot; Masadome, Takashi

2018-01-01

A new microfluidic polymer chip with an embedded cationic surfactant (CS) ion-selective optode (CS-optode) as a detector of flow-injection analysis (FIA) for the determination of CSs was developed. The optode sensing membrane is based on a poly(vinyl chloride) membrane plasticized with 2-nitrophenyl octyl ether containing tetrabromophenolphthalein ethyl ester. Under the optimal flow conditions of the FIA system, the CS-optode showed a good linear relationship between the peak heights in the absorbance, and the concentrations of CS in a concentration range from 50 to 400 μmol dm -3 . The sample throughput of the present system for the determination of a CS ion (300 μmol dm -3 zephiramine) was ca. 11 samples h -1 . The proposed FIA system was applied to determine the level of CS in dental rinses.

Determination of uranium in clinical and environmental samples by FIAS-ICPMS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Karpas, Z.; Lorber, A.; Halicz, L.

Uranium may enter the human body through ingestion or inhalation. Ingestion of uranium compounds through the diet, mainly drinking water, is a common occurrence, as these compounds are present in the biosphere. Inhalation of uranium-containing particles is mainly an occupational safety problem, but may also take place in areas where uranium compounds are abundant. The uranium concentration in urine samples may serve as an indication of the total uranium body content. A method based on flow injection and inductively coupled plasma mass spectrometry (FIAS-ICPMS) was found to be most suitable for determination of uranium in clinical samples (urine and serum),more » environmental samples (seawater, wells and carbonate rocks) and in liquids consumed by humans (drinking water and commercial beverages). Some examples of the application of the FIAS-ICPMS method are reviewed and presented here.« less

Improving adjuvant systems for polyclonal egg yolk antibody (IgY) production in laying hens in terms of productivity and animal welfare.

PubMed

Marcq, Christopher; Marlier, Didier; Beckers, Yves

2015-05-15

The antibody production in the egg yolks of immunized laying hens is seen as a way of improving animal welfare compared with conventional production by mammals. Immunoglobulin Y (IgY) technology, however, has still to address welfare issues linked to the widespread use of an adjuvant in vaccines. Currently, Freund's adjuvants, complete (FCA) or incomplete (FIA), remain the standard. This study sought to evaluate various approaches used to enhance egg yolk antibody production in terms of both productivity and avian welfare. The outer membrane protein (OMP) of Salmonella Typhimurium was used as the prototype antigen. At 20 weeks of age, 56 ISA Brown hens, with specific-Salmonella-free status, were divided into seven groups (n=8) and received an initial intramuscular immunization. Hens in the two negative control groups received phosphate buffered saline (PBS) or FIA alone. Hens in the other groups received 80μg of Salmonella OMP emulsified with one of the following adjuvants: 200μl of FIA alone (T1); 200μl of FIA supplemented with 8μg of C-phosphate-guanosine oligodeoxynucleotides (CpG-ODN) (T2); and 280μl of Montanide ISA 70 VG (T4). Birds in the T3 group received the antigen in emulsion with FIA and were given the tested immunostimulatory component (l-carnitine) via their feed (100mg/kg). A positive control group (PC) received FCA for the first and final immunizations and FIA for the other boosters. Immunization was repeated after 20, 46, 82 and 221 days. Eggs were collected regularly until 242 days after the first immunization and the anti-Salmonella Typhimurium activities in the yolk were determined by ELISA. After 242 days, the birds were euthanized and the injection sites were evaluated for gross and microscopic lesions. Among the tested immunostimulatory approaches, supplementation of FIA with CpG-ODN led to a significant and long-lasting enhancement of the specific antibody response. This treatment was even higher than the positive benchmark using FCA in the first immunization. The study results showed that a clinical examination of injection sites is insufficient for drawing conclusions about the local tolerance of vaccines. Tissue damage was noticeable in all treatment groups. The birds receiving the Montanide adjuvant, however, had fewer and less severe lesions. Given these limited side-effects, Montanide ISA 70 VG could provide the depot effect needed to ensure the immunomodulatory efficiency of CpG-ODN. The association of these two adjuvants could prove a promising alternative to Freund's adjuvants (FA). Copyright © 2015 Elsevier B.V. All rights reserved.

Establishing a standard calibration methodology for MOSFET detectors in computed tomography dosimetry.

PubMed

Brady, S L; Kaufman, R A

2012-06-01

The use of metal-oxide-semiconductor field-effect transistor (MOSFET) detectors for patient dosimetry has increased by ~25% since 2005. Despite this increase, no standard calibration methodology has been identified nor calibration uncertainty quantified for the use of MOSFET dosimetry in CT. This work compares three MOSFET calibration methodologies proposed in the literature, and additionally investigates questions relating to optimal time for signal equilibration and exposure levels for maximum calibration precision. The calibration methodologies tested were (1) free in-air (FIA) with radiographic x-ray tube, (2) FIA with stationary CT x-ray tube, and (3) within scatter phantom with rotational CT x-ray tube. Each calibration was performed at absorbed dose levels of 10, 23, and 35 mGy. Times of 0 min or 5 min were investigated for signal equilibration before or after signal read out. Calibration precision was measured to be better than 5%-7%, 3%-5%, and 2%-4% for the 10, 23, and 35 mGy respective dose levels, and independent of calibration methodology. No correlation was demonstrated for precision and signal equilibration time when allowing 5 min before or after signal read out. Differences in average calibration coefficients were demonstrated between the FIA with CT calibration methodology 26.7 ± 1.1 mV cGy(-1) versus the CT scatter phantom 29.2 ± 1.0 mV cGy(-1) and FIA with x-ray 29.9 ± 1.1 mV cGy(-1) methodologies. A decrease in MOSFET sensitivity was seen at an average change in read out voltage of ~3000 mV. The best measured calibration precision was obtained by exposing the MOSFET detectors to 23 mGy. No signal equilibration time is necessary to improve calibration precision. A significant difference between calibration outcomes was demonstrated for FIA with CT compared to the other two methodologies. If the FIA with a CT calibration methodology was used to create calibration coefficients for the eventual use for phantom dosimetry, a measurement error ~12% will be reflected in the dosimetry results. The calibration process must emulate the eventual CT dosimetry process by matching or excluding scatter when calibrating the MOSFETs. Finally, the authors recommend that the MOSFETs are energy calibrated approximately every 2500-3000 mV. © 2012 American Association of Physicists in Medicine.

Using GIS to integrate FIA and remotely sensed data to estimate the invasibility of major forest types by non-native invasive plants in the Upper Midwest, USA

Treesearch

Zhaofei Fan; W. Keith Moser; Michael K. Crosby; Weiming Yu

2012-01-01

Non-native invasive plants (NNIP) are rapidly spreading into natural ecosystems such as forests in the Upper Midwest. Using the strategic inventory data from the 2005-2006 U.S. Department of Agriculture, Forest Service’s Forest Inventory and Analysis (FIA) program and forest land cover data, we estimated the regional-invasibility patterns of NNIPs for major...

Bridging the gap between data analysis and data collection in FIA and forest monitoring globally: successes, research findings, and lessons learned from the Western US and Southeast Asia

Treesearch

Leif Mortenson

2015-01-01

Globally, national forest inventories (NFI) require a large work force typically consisting of multiple teams spread across multiple locations in order to successfully capture a given nation’s forest resources. This is true of the Forest Inventory and Analysis (FIA) program in the US and in many inventories in developing countries that are supported by USFS...

Measurement of forest disturbance and regrowth with Landsat and forest inventory and analysis data: anticipated benefits from forest and inventory analysis' collaboration with the national aeronautics and space administration and university partners

Treesearch

Sean Healey; Gretchen Moisen; Jeff Masek; Warren Cohen; Sam Goward; < i> et al< /i>

2007-01-01

The Forest Inventory and Analysis (FIA) program has partnered with researchers from the National Aeronautics and Space Administration, the University of Maryland, and other U.S. Department of Agriculture Forest Service units to identify disturbance patterns across the United States using FIA plot data and time series of Landsat satellite images. Spatially explicit...

Become Related: FIAS, an Intensive Early Intervention for Young Children with Autism Spectrum Disorders.

PubMed

Herbrecht, Evelyn; Kievit, Esther; Spiegel, René; Dima, Diana; Goth, Kirstin; Schmeck, Klaus

2015-01-01

In autism spectrum disorders (ASDs), impairments in fundamental social abilities and a lack of interest in social stimuli become apparent early in life. These impairments are thought to negatively affect further brain and behavioural development. Early intensive interventions can help to attenuate social-development and other risk factors and, thus, to ameliorate the deficits associated with ASDs. We present FIAS, an intensive early intervention approach for young children with ASD, which aims at developing children's social motivation. During 18 days, therapists work continuously for 6 h a day with the affected child, involving the whole family in a day care setting. Follow-up care at home over 1 year as well as fresh-up interventions and inclusion in kindergarten or a play group should stabilise the effects and help to respond to further challenges. Here, we present observations from the first 12 patients (25-48 months of age) treated according to the FIAS approach. We evaluated changes in core autistic symptoms and level of functioning after the 18 days of intensive intervention. Beyond standardised assessment, two innovative video-based instruments (Autism Behaviour Coding System and Evaluationsfragebogen) have been developed to assess autistic symptoms and interaction parameters during intervention. Improvements were noted in most core autistic symptom domains, with the highest effect sizes in domains like eye contact, communication, repetitive behaviour, imitation, motivation and reciprocity. In addition, the level of functioning significantly improved. The first evaluation of the FIAS approach shows promising results, as the FIAS intervention appears to improve core autistic symptom domains as well as the level of everyday functioning. Limitations of this study are the small sample size and the lack of a control group. A more comprehensive and longitudinal evaluation is in progress; this will focus on the stability of the observed effects and will attempt to identify potential predictors of treatment response. © 2015 S. Karger AG, Basel.

Antibody response in sheep following immunization with Streptococcus bovis in different adjuvants.

PubMed

Shu, Q; Bir, S H; Gill, H S; Duan, E; Xu, Y; Hiliard; Rowe, J B

2001-01-01

Recent studies have shown that immunization with Streptococcus bovis using Freund's complete adjuvant (FCA) may confer protection against lactic acidosis in sheep. The major objective of this study was to compare the antibody responses to S. bovis in a practically acceptable adjuvant (Freund's incomplete adjuvant (FIA); QuilA; dextran sulphate (Dex); Imject Alum; or Gerbu) and in FCA. Thirty-five sheep were randomly allocated to 7 treatment groups. Six groups were immunized with S. bovis in an adjuvant; the other group served as the non-immunization control. The primary immunization was administered intramuscularly on day 0. followed by a booster injection on day 28. Immunization with FCA induced the highest saliva and serum antibody responses. The saliva antibody concentrations in the FIA and QuilA groups were significantly higher than those in the Alum, Dex and Gerbu groups (p < 0.01). The serum antibody concentration in the FIA group was significantly higher than those in the QuilA, Alum. Dex and Gerbu groups (p < 0.01). Immunization enhanced the antibody level in faeces (p < 0.05), but there was no significant difference between the different adjuvant groups (p > 0.05). Seven and 14 days following booster immunization, the saliva antibody levels induced by QuilA and/or FIA were comparable with the level stimulated by FCA (p > 0.05). There was a strongly positive correlation (R2 = 0.770, p < 0.01) between the antibody concentrations in salival and serum. Compared with the controls, a higher faecal dry matter content was observed in the animals immunized with either FCA or QuilA. The change in faecal dry matter content was positively associated with the faecal antibody concentration (R2 = 0.441, p < 0.05). These results indicate that FIA and QuilA were effective at inducing high levels of antibody responses to S. bovis, and suggest that either Freund's incomplete adjuvant or QuilA may be useful for preparing a practically acceptable vaccine against lactic acidosis.

Validation of amino-acids measurement in dried blood spot by FIA-MS/MS for PKU management.

PubMed

Bruno, C; Dufour-Rainfray, D; Patin, F; Vourc'h, P; Guilloteau, D; Maillot, F; Labarthe, F; Tardieu, M; Andres, C R; Emond, P; Blasco, H

2016-09-01

Phenylketonuria (PKU) is a metabolic disorder leading to high concentrations of phenylalanine (Phe) and low concentrations of tyrosine (Tyr) in blood and brain that may be neurotoxic. This disease requires a regular monitoring of plasma Phe and Tyr as well as branched-chain amino-acids concentrations to adapt the Phe-restricted diet and other therapy that may be prescribed in PKU. We validated a Flow Injection Analysis tandem Mass Spectrometry (FIA-MS/MS) to replace the enzymatic method routinely used for neonatal screening in order to monitor in parallel to Phe, Tyr and branched-chain amino-acids not detected by the enzymatic method. We ascertained the performances of the method: linearity, detection and quantification limits, contamination index, accuracy. We cross validated the FIA-MS/MS and enzymatic methods and we evaluated our own reference ranges to monitor Phe, Tyr, Leu, Val on 59 dried blood spots of normal controls. We also evaluated Tyr, Leu and Val concentrations in PKU patients to detect some potential abnormalities, not evaluated by the enzymatic method. We developed a rapid method with excellent performances including precision and accuracy <15%. We noted an excellent correlation of Phe concentrations between FIA-MS/MS and enzymatic methods (p<0.0001) based on our database which are similar to references ranges published. We observed that 50% of PKU patients had lower concentrations of Tyr, Leu and/or Val that could not be detected by the enzymatic method. Based on laboratory accreditation recommendations, we validated a robust, rapid and reliable FIA-MS/MS method to monitor plasma Phe concentrations but also Tyr, Leu and Val concentrations, suitable for PKU management. We evaluated our own reference ranges of concentration for a routine application of this method. Copyright © 2016 The Canadian Society of Clinical Chemists. Published by Elsevier Inc. All rights reserved.

Analysis of Pooled FIA and Remote Sensing Data for Fiber Supply Assessment at the Warnell School of Forest Resources at the University of Georgia - Other Studies and Effective Information Dissemination

Treesearch

Chris J. Cieszewski; Michael Zasada; Tripp Lowe; Bruce Borders; Mike Clutter; Richard F. Daniels; Robert I. Elle; Robert Izlar; Jarek Zawadzki

2005-01-01

We provide here a short description of the origin, current work, and future outlook of the Fiber Supply Assessment program at the D.B. Warnell School of Forest Resources, University of Georgia, whose work includes various analyses of FIA data. Since 1997, the program has intended to assist the implementation of the new Southern Annual Forest Inventory System through...

Estimating the number of tree species in forest populations using current vegetation survey and forest inventory and analysis approximation plots and grid intensities

Treesearch

Hans T. Schreuder; Jin-Mann S. Lin; John Teply

2000-01-01

We estimate number of tree species in National Forest populations using the nonparametric estimator. Data from the Current Vegetation Survey (CVS) of Region 6 of the USDA Forest Service were used to estimate the number of tree species with a plot close in size to the Forest Inventory and Analysis (FIA) plot and the actual CVS plot for the 5.5 km FIA grid and the 2.7 km...

Development and validation of a FIA/UV-vis method for pK(a) determination of oxime based acetylcholinesterase reactivators.

PubMed

Musil, Karel; Florianova, Veronika; Bucek, Pavel; Dohnal, Vlastimil; Kuca, Kamil; Musilek, Kamil

2016-01-05

Acetylcholinesterase reactivators (oximes) are compounds used for antidotal treatment in case of organophosphorus poisoning. The dissociation constants (pK(a1)) of ten standard or promising acetylcholinesterase reactivators were determined by ultraviolet absorption spectrometry. Two methods of spectra measurement (UV-vis spectrometry, FIA/UV-vis) were applied and compared. The soft and hard models for calculation of pK(a1) values were performed. The pK(a1) values were recommended in the range 7.00-8.35, where at least 10% of oximate anion is available for organophosphate reactivation. All tested oximes were found to have pK(a1) in this range. The FIA/UV-vis method provided rapid sample throughput, low sample consumption, high sensitivity and precision compared to standard UV-vis method. The hard calculation model was proposed as more accurate for pK(a1) calculation. Copyright © 2015 Elsevier B.V. All rights reserved.

Areas of Agreement and Disagreement Regarding Ponderosa Pine and Mixed Conifer Forest Fire Regimes: A Dialogue with Stevens et al.

PubMed Central

Odion, Dennis C.; Hanson, Chad T.; Baker, William L.; DellaSala, Dominick A.; Williams, Mark A.

2016-01-01

In a recent PLOS ONE paper, we conducted an evidence-based analysis of current versus historical fire regimes and concluded that traditionally defined reference conditions of low-severity fire regimes for ponderosa pine (Pinus ponderosa) and mixed-conifer forests were incomplete, missing considerable variability in forest structure and fire regimes. Stevens et al. (this issue) agree that high-severity fire was a component of these forests, but disagree that one of the several sources of evidence, stand age from a large number of forest inventory and analysis (FIA) plots across the western USA, support our findings that severe fire played more than a minor role ecologically in these forests. Here we highlight areas of agreement and disagreement about past fire, and analyze the methods Stevens et al. used to assess the FIA stand-age data. We found a major problem with a calculation they used to conclude that the FIA data were not useful for evaluating fire regimes. Their calculation, as well as a narrowing of the definition of high-severity fire from the one we used, leads to a large underestimate of conditions consistent with historical high-severity fire. The FIA stand age data do have limitations but they are consistent with other landscape-inference data sources in supporting a broader paradigm about historical variability of fire in ponderosa and mixed-conifer forests than had been traditionally recognized, as described in our previous PLOS paper. PMID:27195808

Areas of Agreement and Disagreement Regarding Ponderosa Pine and Mixed Conifer Forest Fire Regimes: A Dialogue with Stevens et al.

PubMed

Odion, Dennis C; Hanson, Chad T; Baker, William L; DellaSala, Dominick A; Williams, Mark A

2016-01-01

In a recent PLOS ONE paper, we conducted an evidence-based analysis of current versus historical fire regimes and concluded that traditionally defined reference conditions of low-severity fire regimes for ponderosa pine (Pinus ponderosa) and mixed-conifer forests were incomplete, missing considerable variability in forest structure and fire regimes. Stevens et al. (this issue) agree that high-severity fire was a component of these forests, but disagree that one of the several sources of evidence, stand age from a large number of forest inventory and analysis (FIA) plots across the western USA, support our findings that severe fire played more than a minor role ecologically in these forests. Here we highlight areas of agreement and disagreement about past fire, and analyze the methods Stevens et al. used to assess the FIA stand-age data. We found a major problem with a calculation they used to conclude that the FIA data were not useful for evaluating fire regimes. Their calculation, as well as a narrowing of the definition of high-severity fire from the one we used, leads to a large underestimate of conditions consistent with historical high-severity fire. The FIA stand age data do have limitations but they are consistent with other landscape-inference data sources in supporting a broader paradigm about historical variability of fire in ponderosa and mixed-conifer forests than had been traditionally recognized, as described in our previous PLOS paper.

Chitosan-guar gum-silver nanoparticles hybrid matrix with immobilized enzymes for fabrication of beta-glucan and glucose sensing photometric flow injection system.

PubMed

Bagal-Kestwal, Dipali R; Kestwal, Rakesh Mohan; Hsieh, Wen-Ting; Chiang, Been-Huang

2014-01-01

Simple and fast photometric flow injection analysis system was developed for sensing of β-1,3-glucan from medicinal mushroom Ganoderma lucidum during fermentation. For this purpose, the chitosan-guar gum-silver nanoparticle-beta glucanase (Ch-GG-AgNPs-βG) beads and Ch-GG-AgNPs-GOD (glucose oxidase) beads were prepared. The bead packed mini-columns were then used to assemble a flow injection analysis (FIA) system for the detection of β-(1→3)-d-glucan biomarker or glucose. This colorimetric flow system can detect glucose and glucan with detection limits as low as 50ngmL(-1) and 100ngmL(-1) (S/N=3), respectively. The analysis time of this FIA was approximately 40s, which is faster than the previously reported glucan sensors. The glucose and glucan calibration curves were obtained in the range of 0.25-1.25μgmL(-1) (R(2)=0.988) and 0.2-1.0μgmL(-1)(R(2)=0.979), respectively. The applicability of the nano-bio-composite FIA sensor system for spiked and real β-(1→3)-d-glucan samples were tested, and the accuracy of the results were greater than 95%. Thus, the designed FIA provides a simple, interference free and rapid tool for monitoring glucose and β-glucan content, which can be used for various food samples with a little modification. Copyright © 2013 Elsevier B.V. All rights reserved.

Characterization and measurement of natural gas trace constituents. Volume 1. Arsenic. Final report, June 1989-October 1993

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chao, S.S.; Attari, A.

1995-01-01

The discovery of arsenic compounds, as alkylarsines, in natural gas prompted this research program to develop reliable measurement techniques needed to assess the efficiency of removal processes for these environmentally sensitive substances. These techniques include sampling, speciation, quantitation and on-line instrumental methods for monitoring the total arsenic concentration. The current program has yielded many products, including calibration standards, arsenic-specific sorbents, sensitive analytical methods and instrumentation. Four laboratory analytical methods have been developed and successfully employed for arsenic determination in natural gas. These methods use GC-AED and GC-MS instruments to speciate alkylarsines, and peroxydisulfate extraction with FIAS, special carbon sorbent withmore » XRF and an IGT developed sorbent with GFAA for total arsenic measurement.« less

Dataset of timberland variables used to assess forest conditions in two Southeastern United States' fuelsheds

DOE PAGES

Parish, Esther S.; Dale, Virginia H.; Tobin, Emma; ...

2017-05-27

The data presented in this article are related to the research article entitled “How is wood-based pellet production affecting forest conditions in the southeastern United States?” (Dale et al., 2017). This article describes how United States Forest Service (USFS) Forest Inventory and Analysis (FIA) data from multiple state inventories were aggregated and used to extract ten annual timberland variables for trend analysis in two case study bioenergy fuelshed areas. This dataset is made publically available to enable critical or extended analyses of changes in forest conditions, either for the fuelshed areas supplying the ports of Savannah, Georgia and Chesapeake, Virginia,more » or for other southeastern US forested areas contributing biomass to the export wood pellet industry.« less

Dataset of timberland variables used to assess forest conditions in two Southeastern United States' fuelsheds

DOE Office of Scientific and Technical Information (OSTI.GOV)

Parish, Esther S.; Dale, Virginia H.; Tobin, Emma

The data presented in this article are related to the research article entitled “How is wood-based pellet production affecting forest conditions in the southeastern United States?” (Dale et al., 2017). This article describes how United States Forest Service (USFS) Forest Inventory and Analysis (FIA) data from multiple state inventories were aggregated and used to extract ten annual timberland variables for trend analysis in two case study bioenergy fuelshed areas. This dataset is made publically available to enable critical or extended analyses of changes in forest conditions, either for the fuelshed areas supplying the ports of Savannah, Georgia and Chesapeake, Virginia,more » or for other southeastern US forested areas contributing biomass to the export wood pellet industry.« less

Flow injection analysis of organic peroxide explosives using acid degradation and chemiluminescent detection of released hydrogen peroxide.

PubMed

Mahbub, Parvez; Zakaria, Philip; Guijt, Rosanne; Macka, Mirek; Dicinoski, Greg; Breadmore, Michael; Nesterenko, Pavel N

2015-10-01

The applicability of acid degradation of organic peroxides into hydrogen peroxide in a pneumatically driven flow injection system with chemiluminescence reaction with luminol and Cu(2+) as a catalyst (FIA-CL) was investigated for the fast and sensitive detection of organic peroxide explosives (OPEs). The target OPEs included hexamethylene triperoxide diamine (HMTD), triacetone triperoxide (TATP) and methylethyl ketone peroxide (MEKP). Under optimised conditions maximum degradations of 70% and 54% for TATP and HMTD, respectively were achieved at 162 µL min(-1), and 9% degradation for MEKP at 180 µL min(-1). Flow rates were precisely controlled in this single source pneumatic pressure driven multi-channel FIA system by model experiments on mixing of easily detectable component solutions. The linear range for detection of TATP, HMTD and H2O2 was 1-200 µM (r(2)=0.98-0.99) at both flow rates, while that for MEKP was 20-200 µM (r(2)=0.97) at 180 µL min(-1). The detection limits (LODs) obtained were 0.5 µM for TATP, HMTD and H2O2 and 10 µM for MEKP. The detection times varied from 1.5 to 3 min in this FIA-CL system. Whilst the LOD for H2O2 was comparable with those reported by other investigators, the LODs and analysis times for TATP and HMTD were superior, and significantly, this is the first time the detection of MEKP has been reported by FIA-CL. Copyright © 2015 Elsevier B.V. All rights reserved.

Elicitors and co-factors in food-induced anaphylaxis in adults

PubMed Central

2013-01-01

Food-induced anaphylaxis (FIA) in adults is often insufficiently diagnosed. One reason is related to the presence of co-factors like exercise, alcohol, additives and non-steroidal anti-inflammatory drugs. The objective of this analysis was to retrospectively investigate the role of co-factors in patients with FIA. 93 adult patients with suspected FIA underwent double-blind, placebo-controlled food challenges with suspected allergens and co-factors. The elicitors of anaphylaxis were identified in 44/93 patients. 27 patients reacted to food allergens upon challenge, 15 patients reacted only when a co-factor was co-exposed with the allergen. The most common identified allergens were celery (n = 7), soy, wheat (n = 4 each) and lupine (n = 3). Among the co-factors food additives (n = 8) and physical exercise (n = 6) were most frequent. In 10 patients more than one co-factor and/or more than one food allergen was necessary to elicit a positive reaction. The implementation of co-factors into the challenge protocol increases the identification rate of elicitors in adult food anaphylactic patients. PMID:24262093

A recombinant truncated surface immunogenic protein (tSip) plus adjuvant FIA confers active protection against Group B streptococcus infection in tilapia.

PubMed

He, Yang; Wang, Kai-Yu; Xiao, Dan; Chen, De-Fang; Huang, Lingyuan; Liu, Tianqiang; Wang, Jun; Geng, Yi; Wang, Er-Long; Yang, Qian

2014-12-05

Tilapia is an important agricultural fish that has been plagued by Group B streptococcus (GBS) infections in recent years, some of them severe. It is well-known that surface immunogenicity protein (Sip) is an effective vaccine against GBS. Since Sip was not expressed in either E. coli BL21 or E. coli Rosetta, we removed the N-terminal signal peptide and LysM of the virus to produce purified truncated Sip (tSip(1)), which multiplied easily in an E. coli host. The antibody's ability to recognize and combine with GBS was determined by Western-blot and specific staining in vitro. The relative percentage of survival (RPS), antibody titers, bacterial recovery, and pathologic morphology were monitored in vivo to evaluate the immune effects. Freund's incomplete adjuvant (FIA) plus tSip and aluminum hydroxide gel (AH) plus tSip were also evaluated. It revealed that tSip mixed with FIA was an effective vaccine against GBS in tilapia, while AH is toxic to tilapia. Copyright © 2014. Published by Elsevier Ltd.

Ferrum nano particles and multiwall carbon nano tubes based electrode as FIA detector for determination of amino acids in hypothalamus microdialysis fluids

NASA Astrophysics Data System (ADS)

Sun, L.; Wang, J.; Wang, Y. T.; Yu, L.; Peng, H.; Zhu, J. Z.

2017-01-01

An amperometric electrode based on multiwall carbon nanotubes (MWCNTs) and Fe nanoparticles (NPs) has been successfully fabricated. Combined with Flow Injection Analysis (FIA) and chromatography separation column, the electrode exhibits linear response in the concentration range of 0.1 -12 μM and the sensitivity of 30.0 nA μM-1 for most of amino acids. The determination of 17 amino acids in the hypothalamus microdialysis fluids of guinea pigs, illustrates that the electrode is a powerful tool to investigate physiology and pathology mechanisms

Multi-Scale Mapping of Vegetation Biomass

NASA Astrophysics Data System (ADS)

Hudak, A. T.; Fekety, P.; Falkowski, M. J.; Kennedy, R. E.; Crookston, N.; Smith, A. M.; Mahoney, P.; Glenn, N. F.; Dong, J.; Kane, V. R.; Woodall, C. W.

2016-12-01

Vegetation biomass mapping at multiple scales is important for carbon inventory and monitoring, reporting, and verification (MRV). Project-level lidar collections allow biomass estimation with high confidence where associated with field plot measurements. Predictive models developed from such datasets are customarily used to generate landscape-scale biomass maps. We tested the feasibility of predicting biomass in landscapes surveyed with lidar but without field plots, by withholding plot datasets from a reduced model applied to the landscapes, and found support for a generalized model in the northern Idaho ecoregion. We are also upscaling a generalized model to all forested lands in Idaho. Our regional modeling approach is to sample the 30-m biomass predictions from the landscape-scale maps and use them to train a regional biomass model, using Landsat time series, topographic derivatives, and climate variables as predictors. Our regional map validation approach is to aggregate the regional, annual biomass predictions to the county level and compare them to annual county-level biomass summarized independently from systematic, field-based, annual inventories conducted by the US Forest Inventory and Analysis (FIA) Program nationally. A national-scale forest cover map generated independently from 2010 PALSAR data at 25-m resolution is being used to mask non-forest pixels from the aggregations. Effects of climate change on future regional biomass stores are also being explored, using biomass estimates projected from stand-level inventory data collected in the National Forests and comparing them to FIA plot data collected independently on public and private lands, projected under the same climate change scenarios, with disturbance trends extracted from the Landsat time series. Our ultimate goal is to demonstrate, focusing on the ecologically diverse Northwest region of the USA, a carbon monitoring system (CMS) that is accurate, objective, repeatable, and transparent.

Integrating LIDAR and forest inventories to fill the trees outside forests data gap.

PubMed

Johnson, Kristofer D; Birdsey, Richard; Cole, Jason; Swatantran, Anu; O'Neil-Dunne, Jarlath; Dubayah, Ralph; Lister, Andrew

2015-10-01

Forest inventories are commonly used to estimate total tree biomass of forest land even though they are not traditionally designed to measure biomass of trees outside forests (TOF). The consequence may be an inaccurate representation of all of the aboveground biomass, which propagates error to the outputs of spatial and process models that rely on the inventory data. An ideal approach to fill this data gap would be to integrate TOF measurements within a traditional forest inventory for a parsimonious estimate of total tree biomass. In this study, Light Detection and Ranging (LIDAR) data were used to predict biomass of TOF in all "nonforest" Forest Inventory and Analysis (FIA) plots in the state of Maryland. To validate the LIDAR-based biomass predictions, a field crew was sent to measure TOF on nonforest plots in three Maryland counties, revealing close agreement at both the plot and county scales between the two estimates. Total tree biomass in Maryland increased by 25.5 Tg, or 15.6%, when biomass of TOF were included. In two counties (Carroll and Howard), there was a 47% increase. In contrast, counties located further away from the interstate highway corridor showed only a modest increase in biomass when TOF were added because nonforest conditions were less common in those areas. The advantage of this approach for estimating biomass of TOF is that it is compatible with, and explicitly separates TOF biomass from, forest biomass already measured by FIA crews. By predicting biomass of TOF at actual FIA plots, this approach is directly compatible with traditionally reported FIA forest biomass, providing a framework for other states to follow, and should improve carbon reporting and modeling activities in Maryland.

Doppler Endoscopic Probe as a Guide to Risk Stratification and Definitive Hemostasis of Peptic Ulcer Bleeding

PubMed Central

Jensen, Dennis M.; Ohning, Gordon V.; Kovacs, Thomas OG; Ghassemi, Kevin A.; Jutabha, Rome; Dulai, Gareth S.; Machicado, Gustavo A.

2015-01-01

Background and Aims For more than 4 decades endoscopists have relied on ulcer stigmata for risk stratification and as a guide to hemostasis. None used arterial blood flow underneath stigmata to predict outcomes. For patients with severe peptic ulcer bleeding (PUBs), we used Doppler endoscopic probe (DEP) for: 1. detection of blood flow underlying stigmata of recent hemorrhage (SRH), 2. quantitating rates of residual arterial blood flow under SRH after visually directed standard endoscopic treatment, and 3. comparing risks of rebleeding and actual 30 day rebleed rates for spurting arterial bleeding (Forrest – FIA) and oozing bleeding (FIB). Methods Prospective cohort study of 163 consecutive patients with severe PUBs and different SRH. Results All blood flow detected by DEP was arterial. Detection rates were 87.4% in major SRH - spurting arterial bleeding (FIA), non bleeding visible vessel (FIIA), clot (FIIB) - and significantly lower at 42.3% (p<0.0001) for intermediate group of oozing bleeding (FIB) or flat spot (FIIC). For spurting bleeding (FIA) vs. oozing (FIB), baseline DEP arterial flow was 100% vs. 46.7%; residual blood flow detected after endoscopic hemostasis was 35.7% vs. 0%; and 30 day rebleed rates were 28.6% vs. 0% (all p<0.05). Conclusions 1. For major SRH vs. oozing or spot, the arterial blood flow detection rates by DEP was significantly higher, indicating a higher rebleed risk. 2. Before and after endoscopic treatment, spurting FIA PUB’s had significantly higher rates of blood flow detection than oozing FIB PUB’s and a significantly higher 30 rebleed rate. 3. DEP is recommended as a new endoscopic guide with SRH to improve risk stratification and potentially definitive hemostasis for PUBs. PMID:26318834

U.S. Civil Air Show Crashes, 1993 to 2013

PubMed Central

Ballard, Sarah-Blythe; Osorio, Victor B.

2016-01-01

This study provides new public health data about U.S. civil air shows. Risk factors for fatalities in civil air show crashes were analyzed. The value of the FIA score in predicting fatal outcomes was evaluated. With the use of the FAA’s General Aviation and Air Taxi Survey and the National Transportation Safety Board’s data, the incidence of civil air show crashes from 1993 to 2013 was calculated. Fatality risk factors for crashes were analyzed by means of regression methods. The FIA index was validated to predict fatal outcomes by using the factors of fire, instrument conditions, and away-from-airport location, and was evaluated through receiver operating characteristic (ROC) curves. The civil air show crash rate was 31 crashes per 1,000 civil air events. Of the 174 civil air show crashes that occurred during the study period, 91 (52%) involved at least one fatality; on average, 1.1 people died per fatal crash. Fatalities were associated with four major risk factors: fire [adjusted odds ratio (AOR) = 7.1, 95% confidence interval (CI) = 2.4 to 20.6, P < .001], pilot error (AOR = 5.2, 95% CI = 1.8 to 14.5, P = .002), aerobatic flight (AOR = 3.6, 95% CI = 1.6 to 8.2, P = .002), and off-airport location (AOR = 3.4, 95% CI = 1.5 to 7.5, P = .003). The area under the FIA score’s ROC curve was 0.71 (95% CI = 0.64 to 0.78). Civil air show crashes were marked by a high risk of fatal outcomes to pilots in aerobatic performances but rare mass casualties. The FIA score was not a valid measurement of fatal risk in civil air show crashes. PMID:27773963

Wide-range screening of psychoactive substances by FIA-HRMS: identification strategies.

PubMed

Alechaga, Élida; Moyano, Encarnación; Galceran, Maria Teresa

2015-06-01

Recreational drugs (illicit drugs, human and veterinary medicines, legal highs, etc.) often contain lacing agents and adulterants which are not related to the main active ingredient. Serious side effects and even the death of the consumer have been related to the consumption of mixtures of psychoactive substances and/or adulterants, so it is important to know the actual composition of recreational drugs. In this work, a method based on flow injection analysis (FIA) coupled with high-resolution mass spectrometry (HRMS) is proposed for the fast identification of psychoactive substances in recreational drugs and legal highs. The FIA and HRMS working conditions were optimized in order to detect a wide range of psychoactive compounds. As most of the psychoactive substances are acid-base compounds, methanol-0.1 % aqueous formic acid (1:1 v/v) as a carrier solvent and electrospray in both positive ion mode and negative ion mode were used. Two data acquisition modes, full scan at high mass resolution (HRMS) and data-dependent tandem mass spectrometry (ddMS/HRMS) with a quadrupole-Orbitrap mass analyzer were used, resulting in sufficient selectivity for identification of the components of the samples. A custom-made database containing over 450 substances, including psychoactive compounds and common adulterants, was built to perform a high-throughput target and suspect screening. Moreover, online accurate mass databases and mass fragmenter software were used to identify unknowns. Some examples, selected among the analyzed samples of recreational drugs and legal highs using the FIA-HRMS(ddMS/HRMS) method developed, are discussed to illustrate the screening strategy used in this study. The results showed that many of the analyzed samples were adulterated, and in some cases the sample composition did not match that of the supposed marketed substance.

U.S. Civil Air Show Crashes, 1993 to 2013: Burden, Fatal Risk Factors, and Evaluation of a Risk Index for Aviation Crashes.

PubMed

Ballard, Sarah-Blythe; Osorio, Victor B

2015-01-01

This study provides new public health data about U.S. civil air shows. Risk factors for fatalities in civil air show crashes were analyzed. The value of the FIA score in predicting fatal outcomes was evaluated. With the use of the FAA's General Aviation and Air Taxi Survey and the National Transportation Safety Board's data, the incidence of civil air show crashes from 1993 to 2013 was calculated. Fatality risk factors for crashes were analyzed by means of regression methods. The FIA index was validated to predict fatal outcomes by using the factors of fire, instrument conditions, and away-from-airport location, and was evaluated through receiver operating characteristic (ROC) curves. The civil air show crash rate was 31 crashes per 1,000 civil air events. Of the 174 civil air show crashes that occurred during the study period, 91 (52%) involved at least one fatality; on average, 1.1 people died per fatal crash. Fatalities were associated with four major risk factors: fire [adjusted odds ratio (AOR) = 7.1, 95% confidence interval (CI) = 2.4 to 20.6, P < .001], pilot error (AOR = 5.2, 95% CI = 1.8 to 14.5, P = .002), aerobatic flight (AOR = 3.6, 95% CI = 1.6 to 8.2, P = .002), and off-airport location (AOR = 3.4, 95% CI = 1.5 to 7.5, P = .003). The area under the FIA score's ROC curve was 0.71 (95% CI = 0.64 to 0.78). Civil air show crashes were marked by a high risk of fatal outcomes to pilots in aerobatic performances but rare mass casualties. The FIA score was not a valid measurement of fatal risk in civil air show crashes.

HRMS Profile of a Hazelnut Skin Proanthocyanidin-rich Fraction with Antioxidant and Anti-Candida albicans Activities.

PubMed

Piccinelli, Anna Lisa; Pagano, Imma; Esposito, Tiziana; Mencherini, Teresa; Porta, Amalia; Petrone, Anna Maria; Gazzerro, Patrizia; Picerno, Patrizia; Sansone, Francesca; Rastrelli, Luca; Aquino, Rita Patrizia

2016-01-27

Roasted hazelnut skins (RHS) represent a byproduct of kernel industrial processing. In this research, a RHS extract (RHS-M) and its fraction RHS-M-F3 enriched in proanthocyanidins (PAs), with antioxidant activity, were characterized in terms of total phenolic compound and PA contents. RHS-M and RHS-M-F3 showed antifungal properties against Candida albicans SC5314 (MIC2 = 3.00 and 0.10 μg/mL and MIC0 = 5.00 and 0.50 μg/mL, respectively), determined by the microbroth dilution method and Candida albicans morphological analysis. No cytotoxic effect on HEKa and HDFa cell lines was exhibited by RHS-M and RHS-M-F3. The metabolite profiling of RHS-M and RHS-M-F3 was performed by thiolysis followed by HPLC-UV-HRMS analysis and a combination of HRMS-FIA and HPLC-HRMS(n). Extract and fraction contain oligomeric PAs (mDP of 7.3 and 6.0, respectively, and DP up to 10) mainly constituted by B-type oligomers of (epi)-catechin. Also, (epi)-gallocatechin and gallate derivatives were identified as monomer units, and A-type PAs were detected as minor compounds.

Bienzymatic Biosensor for Rapid Detection of Aspartame by Flow Injection Analysis

PubMed Central

Radulescu, Maria-Cristina; Bucur, Bogdan; Bucur, Madalina-Petruta; Radu, Gabriel Lucian

2014-01-01

A rapid, simple and stable biosensor for aspartame detection was developed. Alcohol oxidase (AOX), carboxyl esterase (CaE) and bovine serum albumin (BSA) were immobilised with glutaraldehyde (GA) onto screen-printed electrodes modified with cobalt-phthalocyanine (CoPC). The biosensor response was fast. The sample throughput using a flow injection analysis (FIA) system was 40 h−1 with an RSD of 2.7%. The detection limits for both batch and FIA measurements were 0.1 μM for methanol and 0.2 μM for aspartame, respectively. The enzymatic biosensor was successfully applied for aspartame determination in different sample matrices/commercial products (liquid and solid samples) without any pre-treatment step prior to measurement. PMID:24412899

Bienzymatic biosensor for rapid detection of aspartame by flow injection analysis.

PubMed

Radulescu, Maria-Cristina; Bucur, Bogdan; Bucur, Madalina-Petruta; Radu, Gabriel Lucian

2014-01-09

A rapid, simple and stable biosensor for aspartame detection was developed. Alcohol oxidase (AOX), carboxyl esterase (CaE) and bovine serum albumin (BSA) were immobilised with glutaraldehyde (GA) onto screen-printed electrodes modified with cobalt-phthalocyanine (CoPC). The biosensor response was fast. The sample throughput using a flow injection analysis (FIA) system was 40 h⁻¹ with an RSD of 2.7%. The detection limits for both batch and FIA measurements were 0.1 µM for methanol and 0.2 µM for aspartame, respectively. The enzymatic biosensor was successfully applied for aspartame determination in different sample matrices/commercial products (liquid and solid samples) without any pre-treatment step prior to measurement.

Determination of initiation of DNA replication before and after nuclear formation in Xenopus egg cell free extracts

PubMed Central

1993-01-01

Xenopus egg extracts prepared before and after egg activation retain M- and S-phase specific activity, respectively. Staurosporine, a potent inhibitor of protein kinase, converted M-phase extracts into interphase- like extracts that were capable of forming nuclei upon the addition of sperm DNA. The nuclei formed in the staurosporine treated M-phase extract were incapable of replicating DNA, and they were unable to initiate replication upon the addition of S-phase extracts. Furthermore, replication was inhibited when the staurosporine-treated M- phase extract was added in excess to the staurosporine-treated S-phase extract before the addition of DNA. The membrane-depleted S-phase extract supported neither nuclear formation nor replication; however, preincubation of sperm DNA with these extracts allowed them to form replication-competent nuclei upon the addition of excess staurosporine- treated M-phase extract. These results demonstrate that positive factors in the S-phase extracts determined the initiation of DNA replication before nuclear formation, although these factors were unable to initiate replication after nuclear formation. PMID:8253833

Artificial Intelligence Research Branch future plans

NASA Technical Reports Server (NTRS)

Stewart, Helen (Editor)

1992-01-01

This report contains information on the activities of the Artificial Intelligence Research Branch (FIA) at NASA Ames Research Center (ARC) in 1992, as well as planned work in 1993. These activities span a range from basic scientific research through engineering development to fielded NASA applications, particularly those applications that are enabled by basic research carried out in FIA. Work is conducted in-house and through collaborative partners in academia and industry. All of our work has research themes with a dual commitment to technical excellence and applicability to NASA short, medium, and long-term problems. FIA acts as the Agency's lead organization for research aspects of artificial intelligence, working closely with a second research laboratory at the Jet Propulsion Laboratory (JPL) and AI applications groups throughout all NASA centers. This report is organized along three major research themes: (1) Planning and Scheduling: deciding on a sequence of actions to achieve a set of complex goals and determining when to execute those actions and how to allocate resources to carry them out; (2) Machine Learning: techniques for forming theories about natural and man-made phenomena; and for improving the problem-solving performance of computational systems over time; and (3) Research on the acquisition, representation, and utilization of knowledge in support of diagnosis design of engineered systems and analysis of actual systems.

National-scale aboveground biomass geostatistical mapping with FIA inventory and GLAS data: Preparation for sparsely sampled lidar assisted forest inventory

NASA Astrophysics Data System (ADS)

Babcock, C. R.; Finley, A. O.; Andersen, H. E.; Moskal, L. M.; Morton, D. C.; Cook, B.; Nelson, R.

2017-12-01

Upcoming satellite lidar missions, such as GEDI and IceSat-2, are designed to collect laser altimetry data from space for narrow bands along orbital tracts. As a result lidar metric sets derived from these sources will not be of complete spatial coverage. This lack of complete coverage, or sparsity, means traditional regression approaches that consider lidar metrics as explanatory variables (without error) cannot be used to generate wall-to-wall maps of forest inventory variables. We implement a coregionalization framework to jointly model sparsely sampled lidar information and point-referenced forest variable measurements to create wall-to-wall maps with full probabilistic uncertainty quantification of all inputs. We inform the model with USFS Forest Inventory and Analysis (FIA) in-situ forest measurements and GLAS lidar data to spatially predict aboveground forest biomass (AGB) across the contiguous US. We cast our model within a Bayesian hierarchical framework to better model complex space-varying correlation structures among the lidar metrics and FIA data, which yields improved prediction and uncertainty assessment. To circumvent computational difficulties that arise when fitting complex geostatistical models to massive datasets, we use a Nearest Neighbor Gaussian process (NNGP) prior. Results indicate that a coregionalization modeling approach to leveraging sampled lidar data to improve AGB estimation is effective. Further, fitting the coregionalization model within a Bayesian mode of inference allows for AGB quantification across scales ranging from individual pixel estimates of AGB density to total AGB for the continental US with uncertainty. The coregionalization framework examined here is directly applicable to future spaceborne lidar acquisitions from GEDI and IceSat-2. Pairing these lidar sources with the extensive FIA forest monitoring plot network using a joint prediction framework, such as the coregionalization model explored here, offers the potential to improve forest AGB accounting certainty and provide maps for post-model fitting analysis of the spatial distribution of AGB.

A cohabitation challenge to compare the efficacies of vaccines for bacterial kidney disease (BKD) in chinook salmon Oncorhynchus tshawytscha

USGS Publications Warehouse

Alcorn, S.; Murray, A.L.; Pascho, R.J.; Varney, J.

2005-01-01

The relative efficacies of 1 commercial and 5 experimental vaccines for bacterial kidney disease (BKD) were compared through a cohabitation waterborne challenge. Groups of juvenile chinook salmon Oncorhynchus tshawytscha were vaccinated with one of the following: (1) killed Renibacterium salmoninarum ATCC 33209 (Rs 33209) cells; (2) killed Rs 33209 cells which had been heated to 37??C for 48 h, a process that destroys the p57 protein; (3) killed R. salmoninarum MT239 (Rs MT239) cells; (4) heated Rs MT239 cells; (5) a recombinant version of the p57 protein (r-p57) emulsified in Freund's incomplete adjuvant (FIA); (6) the commercial BKD vaccine Renogen; (7) phosphate-buffered saline (PBS) emulsified with an equal volume of FIA; or (8) PBS alone. Following injection, each fish was marked with a subcutaneous fluorescent latex tag denoting its treatment group and the vaccinated fish were combined into sham and disease challenge tanks. Two weeks after these fish were vaccinated, separate groups of fish were injected with either PBS or live R. salmoninarum GL64 and were placed inside coated-wire mesh cylinders (liveboxes) in the sham and disease challenge tanks, respectively. Mortalities in both tanks were recorded for 285 d. Any mortalities among the livebox fish were replaced with an appropriate cohort (infected with R. salmoninarum or healthy) fish. None of the bacterins evaluated in this study induced protective immunity against the R. salmoninarum shed from the infected livebox fish. The percentage survival within the test groups in the R. salmoninarum challenge tank ranged from 59% (heated Rs MT239 bacterin) to 81 % (PBS emulsified with FIA). There were no differences in the percentage survival among the PBS-, PBS/FIA-, r-p57-and Renogen-injected groups. There also were no differences in survival among the bacterin groups, regardless of whether the bacterial cells had been heated or left untreated prior to injection. ?? Inter-Research 2005.

New overlay measurement technique with an i-line stepper using embedded standard field image alignment marks for wafer bonding applications

NASA Astrophysics Data System (ADS)

Kulse, P.; Sasai, K.; Schulz, K.; Wietstruck, M.

2017-06-01

In the last decades the semiconductor technology has been driven by Moore's law leading to high performance CMOS technologies with feature sizes of less than 10 nm [1]. It has been pointed out that not only scaling but also the integration of novel components and technology modules into CMOS/BiCMOS technologies is becoming more attractive to realize smart and miniaturized systems [2]. Driven by new applications in the area of communication, health and automation, new components and technology modules such as BiCMOS embedded RF-MEMS, high-Q passives, Sibased microfluidics and InP-SiGe BiCMOS heterointegration have been demonstrated [3-6]. In contrast to standard VLSI processes fabricated on front side of the silicon wafer, these new technology modules require addition backside processing of the wafer; thus an accurate alignment between the front and backside of the wafer is mandatory. In previous work an advanced back to front side alignment technique and implementation into IHP's 0.25/0.13 μm high performance SiGe:C BiCMOS backside process module has been presented [7]. The developed technique enables a high resolution and accurate lithography on the backside of BiCMOS wafer for additional backside processing. In addition to the aforementioned back side process technologies, new applications like Through-Silicon Vias (TSV) for interposers and advanced substrate technologies for 3D heterogeneous integration demand not only single wafer fabrication but also processing of wafer stacks provided by temporary and permanent wafer bonding [8]. Therefore, the available overlay measurement techniques are not suitable if overlay and alignment marks are realized at the bonding interface of a wafer stack which consists of both a silicon device and a silicon carrier wafer. The former used EVG 40NT automated overlay measurement system, which use two opposite positioned microscopes inspecting simultaneous the wafer back and front side, is not capable measuring embedded overlay marks. In this work, the non-contact infrared alignment system of the Nikon i-line Stepper NSR-SF150 for both the alignment and the overlay determination of bonded wafer stacks with embedded alignment marks are used to achieve an accurate alignment between the different wafer sides. The embedded field image alignment (FIA) marks of the interface and the device wafer top layer are measured in a single measurement job. By taking the offsets between all different FIA's into account, after correcting the wafer rotation induced FIA position errors, hence an overlay for the stacked wafers can be determined. The developed approach has been validated by a standard back to front side application. The overlay was measured and determined using both, the EVG NT40 automated measurement system with special overlay marks and the measurement of the FIA marks of the front and back side layer. A comparison of both results shows mismatches in x and y translations smaller than 200 nm, which is relatively small compared to the overlay tolerances of +/-500 nm for the back to front side process. After the successful validation of the developed technique, special wafer stacks with FIA alignment marks in the bonding interface are fabricated. Due to the super IR light transparency of both doubled side polished wafers, the embedded FIA marks generate a stable and clear signal for accurate x and y wafer coordinate positioning. The FIA marks of the device wafer top layer were measured under standard condition in a developed photoresist mask without IR illumination. Following overlay calculation shows an overlay of less than 200 nm, which enables very accurate process condition for highly scaled TSV integration and advanced substrate integration into IHP's 0.25/0.13 μm SiGe:C BiCMOS technology. The presented method can be applied for both the standard back to front side process technologies and also new temporary and permanent wafer bonding applications.

A novel approach for determination of free fatty acids in vegetable oils by a flow injection system with manual injection.

PubMed

Ayyildiz, H Filiz; Kara, Huseyin; Sherazi, S T H

2011-12-01

A non-aqueous flow injection method for determining free fatty acid (FFA) content in corn and sunflower oil samples was developed. A single-line manifold system was built by modification of an HPLC for flow injection analysis (FIA). Without pre-treatment, oil samples were injected into a n-propanol solution containing KOH and phenolphthalein (PHP). The main parameters, such as flow rate of carrier phase, length, geometry, inner diameters of the coils and reagent concentration were all optimized. The proposed FIA method was validated for precision, accuracy, linear region, limit of detection (LOD) and limit of quantification (LOQ). The intra- and inter-day measurements of the precision of the method were found to be within the limits of acceptance criteria (RSD < 1%), and were rugged when the method was performed by a different analyst. The linear concentration range was calculated as 0.09-1.50 and 0.07-1.40 FFA% for corn and sunflower oils, correspondingly. The LOD and LOQ were found to be 7.53 × 10(-4)-2.28 × 10(-3) oleic acid % and 7.11 × 10(-4)-2.23 × 10(-3) oleic acid % for corn and sunflower oils, respectively. The results were compared with those obtained by the AOCS (Ca-5a-40) method using statistical t and F tests, and a significant difference was not observed between the methods at a 95% confidence level. The proposed method is suitable for quality control of routine applications due to its simplicity, high sample throughput, and economy of solvents and sample, offering considerable promise as a low cost analytical system that needs minimum human intervention over long periods of time.

The Use of Flow-Injection Analysis with Chemiluminescence Detection of Aqueous Ferrous Iron in Waters Containing High Concentrations of Organic Compounds

PubMed Central

Borman, Christopher J.; Sullivan, B. Patrick; Eggleston, Carrick M.; Colberg, Patricia J. S.

2009-01-01

An evaluation of flow-injection analysis with chemiluminescence detection (FIA-CL) to quantify Fe2+(aq) in freshwaters was performed. Iron-coordinating and/or iron-reducing compounds, dissolved organic matter (DOM), and samples from two natural water systems were used to amend standard solutions of Fe2+(aq). Slopes of the response curves from ferrous iron standards (1 – 100 nM) were compared to the response curves of iron standards containing the amendments. Results suggest that FIA-CL is not suitable for systems containing ascorbate, hydroxylamine, cysteine or DOM. Little or no change in sensitivity occurred in solutions of oxalate and glycine or in natural waters with little organic matter. PMID:22408532

Hydrocarbon group type determination in jet fuels by high performance liquid chromatography

NASA Technical Reports Server (NTRS)

Antoine, A. C.

1977-01-01

Results are given for the analysis of some jet and diesel fuel samples which were prepared from oil shale and coal syncrudes. Thirty-two samples of varying chemical composition and physical properties were obtained. Hydrocarbon types in these samples were determined by fluorescent indicator adsorption (FIA) analysis, and the results from three laboratories are presented and compared. Recently, rapid high performance liquid chromatography (HPLC) methods have been proposed for hydrocarbon group type analysis, with some suggestion for their use as a replacement of the FIA technique. Two of these methods were used to analyze some of the samples, and these results are also presented and compared. Two samples of petroleum-based Jet A fuel are similarly analyzed.

Biosensing of glucose in flow injection analysis system based on glucose oxidase-quantum dot modified pencil graphite electrode.

PubMed

Sağlam, Özlem; Kızılkaya, Bayram; Uysal, Hüseyin; Dilgin, Yusuf

2016-01-15

A novel amperometric glucose biosensor was proposed in flow injection analysis (FIA) system using glucose oxidase (GOD) and Quantum dot (ZnS-CdS) modified Pencil Graphite Electrode (PGE). After ZnS-CdS film was electrochemically deposited onto PGE surface, GOD was immobilized on the surface of ZnS-CdS/PGE through crosslinking with chitosan (CT). A pair of well-defined reversible redox peak of GOD was observed at GOD/CT/ZnS-CdS/PGE based on enzyme electrode by direct electron transfer between the protein and electrode. Further, obtained GOD/CT/ZnS-CdS/PGE offers a disposable, low cost, selective and sensitive electrochemical biosensing of glucose in FIA system based on the decrease of the electrocatalytic response of the reduced form of GOD to dissolved oxygen. Under optimum conditions (flow rate, 1.3mL min(-1); transmission tubing length, 10cm; injection volume, 100μL; and constant applied potential, -500mV vs. Ag/AgCl), the proposed method displayed a linear response to glucose in the range of 0.01-1.0mM with detection limit of 3.0µM. The results obtained from this study would provide the basis for further development of the biosensing using PGE based FIA systems. Copyright © 2015 Elsevier B.V. All rights reserved.

Estimation of soil organic carbon in forests of the United States

NASA Astrophysics Data System (ADS)

Domke, G. M.; Perry, C. H.; Walters, B. F.; Woodall, C. W.; Nave, L. E.; Swanston, C.

2015-12-01

Soil organic carbon (SOC) is the largest terrestrial carbon (C) sink on earth and management of this pool is a critical component of global efforts to mitigate atmospheric C concentrations. Soil organic carbon is also a key indicator of soil quality as it affects essential biological, chemical, and physical soil functions such as nutrient cycling, water retention, and soil structure maintenance. Much of the SOC on earth is found in forest ecosystems and is thought to be relatively stable. That said, there is growing evidence that SOC may be sensitive to disturbance and global change drivers. In the United States (US), SOC in forests is monitored by the national forest inventory (NFI) conducted by the Forest Inventory and Analysis (FIA) program within the US Department of Agriculture, Forest Service. The FIA program currently uses SOC predictions based on SSURGO/STATSGO data to populate the NFI. Most of estimates of SOC in forests from the SSURGO/STATSGO data are based primarily upon expert opinion and lack systematic field observations. The FIA program has been consistently measuring soil attributes as part of the NFI since 2001 and has amassed an extensive inventory of SOC in forests in the conterminous US and coastal Alaska. Here we present estimates of SOC obtained using data from the NFI and International Soil Carbon Network and describe the modeling framework used to compile estimates for United Nations Framework Convention on Climate Change reporting.

Estimating aboveground live understory vegetation carbon in the United States

NASA Astrophysics Data System (ADS)

Johnson, Kristofer D.; Domke, Grant M.; Russell, Matthew B.; Walters, Brian; Hom, John; Peduzzi, Alicia; Birdsey, Richard; Dolan, Katelyn; Huang, Wenli

2017-12-01

Despite the key role that understory vegetation plays in ecosystems and the terrestrial carbon cycle, it is often overlooked and has few quantitative measurements, especially at national scales. To understand the contribution of understory carbon to the United States (US) carbon budget, we developed an approach that relies on field measurements of understory vegetation cover and height on US Department of Agriculture Forest Service, Forest Inventory and Analysis (FIA) subplots. Allometric models were developed to estimate aboveground understory carbon. A spatial model based on stand characteristics and remotely sensed data was also applied to estimate understory carbon on all FIA plots. We found that most understory carbon was comprised of woody shrub species (64%), followed by nonwoody forbs and graminoid species (35%) and seedlings (1%). The largest estimates were found in temperate or warm humid locations such as the Pacific Northwest and southeastern US, thus following the same broad trend as aboveground tree biomass. The average understory aboveground carbon density was estimated to be 0.977 Mg ha-1, for a total estimate of 272 Tg carbon across all managed forest land in the US (approximately 2% of the total aboveground live tree carbon pool). This estimate is more than twice as low as previous FIA modeled estimates that did not rely on understory measurements, suggesting that this pool may currently be overestimated in US National Greenhouse Gas reporting.

Determination of Total Selenium in Infant Formulas: Comparison of the Performance of FIA and MCFA Flow Systems

PubMed Central

Pistón, Mariela; Knochen, Moisés

2012-01-01

Two flow methods, based, respectively, on flow-injection analysis (FIA) and on multicommutated flow analysis (MCFA), were compared with regard to their use for the determination of total selenium in infant formulas by hydride-generation atomic absorption spectrometry. The method based on multicommutation provided lower detection and quantification limits (0.08 and 0.27 μg L−1 compared to 0.59 and 1.95 μ L−1, resp.), higher sampling frequency (160 versus. 70 samples per hour), and reduced reagent consumption. Linearity, precision, and accuracy were similar for the two methods compared. It was concluded that, while both methods proved to be appropriate for the purpose, the MCFA-based method exhibited a better performance. PMID:22505923

A microfluidic flow injection system for DNA assay with fluids driven by an on-chip integrated pump based on capillary and evaporation effects.

PubMed

Xu, Zhang-Run; Zhong, Chong-Hui; Guan, Yan-Xia; Chen, Xu-Wei; Wang, Jian-Hua; Fang, Zhao-Lun

2008-10-01

A miniaturized flow injection analysis (FIA) system integrating a micropump on a microfluidic chip based on capillary and evaporation effects was developed. The pump was made by fixing a filter paper plug with a vent tube at the channel end, it requires no peripheral equipment and provides steady flow in the microl min(-1) range for FIA operation. Valve-free sample injection was achieved at nanolitre level using an array of slotted vials. The practical applicability of the system was demonstrated by DNA assay with laser-induced fluorescence (LIF) detection. A precision of 1.6% RSD (10.0 ng microl(-1), n=15) was achieved with a sampling throughput of 76 h(-1) and sample consumption of 95 nl.

Optimization by infusion of multiple reaction monitoring transitions for sensitive quantification of peptides by liquid chromatography/mass spectrometry.

PubMed

Alghanem, Bandar; Nikitin, Frédéric; Stricker, Thomas; Duchoslav, Eva; Luban, Jeremy; Strambio-De-Castillia, Caterina; Muller, Markus; Lisacek, Frédérique; Varesio, Emmanuel; Hopfgartner, Gérard

2017-05-15

In peptide quantification by liquid chromatography/mass spectrometry (LC/MS), the optimization of multiple reaction monitoring (MRM) parameters is essential for sensitive detection. We have compared different approaches to build MRM assays, based either on flow injection analysis (FIA) of isotopically labelled peptides, or on the knowledge and the prediction of the best settings for MRM transitions and collision energies (CE). In this context, we introduce MRMOptimizer, an open-source software tool that processes spectra and assists the user in selecting transitions in the FIA workflow. MS/MS spectral libraries with CE voltages from 10 to 70 V are automatically acquired in FIA mode for isotopically labelled peptides. Then MRMOptimizer determines the optimal MRM settings for each peptide. To assess the quantitative performance of our approach, 155 peptides, representing 84 proteins, were analysed by LC/MRM-MS and the peak areas were compared between: (A) the MRMOptimizer-based workflow, (B1) the SRMAtlas transitions set used 'as-is'; (B2) the same SRMAtlas set with CE parameters optimized by Skyline. 51% of the three most intense transitions per peptide were shown to be common to both A and B1/B2 methods, and displayed similar sensitivity and peak area distributions. The peak areas obtained with MRMOptimizer for transitions sharing either the precursor ion charge state or the fragment ions with the SRMAtlas set at unique transitions were increased 1.8- to 2.3-fold. The gain in sensitivity using MRMOptimizer for transitions with different precursor ion charge state and fragment ions (8% of the total), reaches a ~ 11-fold increase. Isotopically labelled peptides can be used to optimize MRM transitions more efficiently in FIA than by searching databases. The MRMOptimizer software is MS independent and enables the post-acquisition selection of MRM parameters. Coefficients of variation for optimal CE values are lower than those obtained with the SRMAtlas approach (B2) and one additional peptide was detected. Copyright © 2017 John Wiley & Sons, Ltd. Copyright © 2017 John Wiley & Sons, Ltd.

Allometric Scaling and Resource Limitations Model of Total Aboveground Biomass in Forest Stands: Site-scale Test of Model

NASA Astrophysics Data System (ADS)

CHOI, S.; Shi, Y.; Ni, X.; Simard, M.; Myneni, R. B.

2013-12-01

Sparseness in in-situ observations has precluded the spatially explicit and accurate mapping of forest biomass. The need for large-scale maps has raised various approaches implementing conjugations between forest biomass and geospatial predictors such as climate, forest type, soil property, and topography. Despite the improved modeling techniques (e.g., machine learning and spatial statistics), a common limitation is that biophysical mechanisms governing tree growth are neglected in these black-box type models. The absence of a priori knowledge may lead to false interpretation of modeled results or unexplainable shifts in outputs due to the inconsistent training samples or study sites. Here, we present a gray-box approach combining known biophysical processes and geospatial predictors through parametric optimizations (inversion of reference measures). Total aboveground biomass in forest stands is estimated by incorporating the Forest Inventory and Analysis (FIA) and Parameter-elevation Regressions on Independent Slopes Model (PRISM). Two main premises of this research are: (a) The Allometric Scaling and Resource Limitations (ASRL) theory can provide a relationship between tree geometry and local resource availability constrained by environmental conditions; and (b) The zeroth order theory (size-frequency distribution) can expand individual tree allometry into total aboveground biomass at the forest stand level. In addition to the FIA estimates, two reference maps from the National Biomass and Carbon Dataset (NBCD) and U.S. Forest Service (USFS) were produced to evaluate the model. This research focuses on a site-scale test of the biomass model to explore the robustness of predictors, and to potentially improve models using additional geospatial predictors such as climatic variables, vegetation indices, soil properties, and lidar-/radar-derived altimetry products (or existing forest canopy height maps). As results, the optimized ASRL estimates satisfactorily resemble the FIA aboveground biomass in terms of data distribution, overall agreement, and spatial similarity across scales. Uncertainties are quantified (ranged from 0.2 to 0.4) by taking into account the spatial mismatch (FIA plot vs. PRISM grid), heterogeneity (species composition), and an example bias scenario (= 0.2) in the root system extents.

Solvent extraction system for plutonium colloids and other oxide nano-particles

DOEpatents

Soderholm, Lynda; Wilson, Richard E; Chiarizia, Renato; Skanthakumar, Suntharalingam

2014-06-03

The invention provides a method for extracting plutonium from spent nuclear fuel, the method comprising supplying plutonium in a first aqueous phase; contacting the plutonium aqueous phase with a mixture of a dielectric and a moiety having a first acidity so as to allow the plutonium to substantially extract into the mixture; and contacting the extracted plutonium with second a aqueous phase, wherein the second aqueous phase has a second acidity higher than the first acidity, so as to allow the extracted plutonium to extract into the second aqueous phase. The invented method facilitates isolation of plutonium polymer without the formation of crud or unwanted emulsions.

Optimized and validated flow-injection spectrophotometric analysis of topiramate, piracetam and levetiracetam in pharmaceutical formulations.

PubMed

Hadad, Ghada M; Abdel-Salam, Randa A; Emara, Samy

2011-12-01

Application of a sensitive and rapid flow injection analysis (FIA) method for determination of topiramate, piracetam, and levetiracetam in pharmaceutical formulations has been investigated. The method is based on the reaction with ortho-phtalaldehyde and 2-mercaptoethanol in a basic buffer and measurement of absorbance at 295 nm under flow conditions. Variables affecting the determination such as sample injection volume, pH, ionic strength, reagent concentrations, flow rate of reagent and other FIA parameters were optimized to produce the most sensitive and reproducible results using a quarter-fraction factorial design, for five factors at two levels. Also, the method has been optimized and fully validated in terms of linearity and range, limit of detection and quantitation, precision, selectivity and accuracy. The method was successfully applied to the analysis of pharmaceutical preparations.

Solvent Extraction of Rare Earth Elements from a Nitric Acid Leach Solution of Apatite by Mixtures of Tributyl Phosphate and Di-(2-ethylhexyl) Phosphoric Acid

NASA Astrophysics Data System (ADS)

Ferdowsi, Ali; Yoozbashizadeh, Hossein

2017-12-01

Solvent extraction of rare earths from nitrate leach liquor of apatite using mixtures of tributyl phosphate (TBP) and di-(2-ethylhexyl) phosphoric acid (D2EHPA) was studied. The effects of nitrate and hydrogen ion concentration of the aqueous phase as well as the composition and concentration of extractants in the organic phase on the extraction behavior of lanthanum, cerium, neodymium, and yttrium were investigated. The distribution ratio of REEs increases by increasing the nitrate concentration in aqueous phase and concentration of extractants in organic phase, but the hydrogen ion concentration in aqueous phase has a decreasing effect. Yttrium as a heavy rare earth is more sensitive to these parameters than light rare earth elements. Although the composition of organic phase has a minor effect on the extraction of light rare earths, the percent of extraction of yttrium decreases dramatically by increasing the TBP content of organic phase. Mixtures of TBP and D2EHPA can show either synergism or antagonism extraction depending on the concentration and composition of extractants in organic phase. The best condition for separating rare earth elements in groups of heavy and light REEs can be achieved at high nitrate concentration, low H+ concentration, and high concentration of D2EHPA in organic phase. Separation of Ce and La by TBP and D2EHPA is practically impossible in the studied conditions; however, low nitrate concentration and high hydrogen ion concentration in aqueous phase and low concentration of extractants in organic phase favor the separation of Nd from other light rare earth elements.

SOLVENT EXTRACTION PROCESS

DOEpatents

Jonke, A.A.

1957-10-01

In improved solvent extraction process is described for the extraction of metal values from highly dilute aqueous solutions. The process comprises contacting an aqueous solution with an organic substantially water-immiscible solvent, whereby metal values are taken up by a solvent extract phase; scrubbing the solvent extract phase with an aqueous scrubbing solution; separating an aqueous solution from the scrubbed solvent extract phase; and contacting the scrubbed solvent phase with an aqueous medium whereby the extracted metal values are removed from the solvent phase and taken up by said medium to form a strip solution containing said metal values, the aqueous scrubbing solution being a mixture of strip solution and an aqueous solution which contains mineral acids anions and is free of the metal values. The process is particularly effective for purifying uranium, where one starts with impure aqueous uranyl nitrate, extracts with tributyl phosphate dissolved in carbon tetrachloride, scrubs with aqueous nitric acid and employs water to strip the uranium from the scrubbed organic phase.

Sulfur Speciation and Extraction in Jet A (Briefing Charts)

DTIC Science & Technology

2015-08-16

Extraction fluid: denatured ethanol from Fisher Scientific and deionized water – Jet A fuel , approximately 500-800 ppm sulfur by weight – Data...Outline • Background • Experimental Setup – Extraction of sulfur compounds from fuel to alcohol/water extraction fluid – Each rinse is...Hydrophobic / Oleophillic Membrane Oleophobic / Hydrophillic Membrane Emulsion Phase Fuel Phase Water (Extraction Fluid) Phase DISTRIBUTION A

Methodological challenges in evaluating health care financing equity in data-poor contexts: lessons from Ghana, South Africa and Tanzania.

PubMed

Borghi, Josephine; Ataguba, John; Mtei, Gemini; Akazili, James; Meheus, Filip; Rehnberg, Clas; Di, McIntyre

2009-01-01

Measurement of the incidence of health financing contributions across socio-economic groups has proven valuable in informing health care financing reforms. However, there is little evidence as to how to carry out financing incidence analysis (FIA) in lower income settings. We outline some of the challenges faced when carrying out a FIA in Ghana, Tanzania and South Africa and illustrate how innovative techniques were used to overcome data weaknesses in these settings. FIA was carried out for tax, insurance and out-of-pocket (OOP) payments. The primary data sources were Living Standards Measurement Surveys (LSMS) and household surveys conducted in each of the countries; tax authorities and insurance funds also provided information. Consumption expenditure and a composite index of socioeconomic status (SES) were used to assess financing equity. Where possible conventional methods of FIA were applied. Numerous challenges were documented and solution strategies devised. LSMS are likely to underestimate financial contributions to health care by individuals. For tax incidence analysis, reported income tax payments from secondary sources were severely under-reported. Income tax payers and shareholders could not be reliably identified. The use of income or consumption expenditure to estimate income tax contributions was found to be a more reliable method of estimating income tax incidence. Assumptions regarding corporate tax incidence had a huge effect on the progressivity of corporate tax and on overall tax progressivity. LSMS consumption categories did not always coincide with tax categories for goods subject to excise tax (e.g., wine and spirits were combined, despite differing tax rates). Tobacco companies, alcohol distributors and advertising agencies were used to provide more detailed information on consumption patterns for goods subject to excise tax by income category. There was little guidance on how to allocate fuel levies associated with 'public transport' use. Hence, calculations of fuel tax on public transport were based on individual expenditure on public transport, the average cost per kilometre and average rates of fuel consumption for each form of transport. For insurance contributions, employees will not report on employer contributions unless specifically requested to and are frequently unsure of their contributions. Therefore, we collected information on total health insurance contributions from individual schemes and regulatory authorities. OOP payments are likely to be under-reported due to long recall periods; linking OOP expenditure and illness incidence questions--omitting preventive care; and focusing on the last service used when people may have used multiple services during an illness episode. To derive more robust estimates of financing incidence, we collected additional primary data on OOP expenditures together with insurance enrolment rates and associated payments. To link primary data to the LSMS, a composite index of SES was used in Ghana and Tanzania and non-durable expenditure was used in South Africa. We show how data constraints can be overcome for FIA in lower income countries and provide recommendations for future studies.

Recovery of Ni Metal from Spent Catalyst with Emulsion Liquid Membrane Using Cyanex 272 as Extractant

NASA Astrophysics Data System (ADS)

Yuliusman; Huda, M.; Ramadhan, I. T.; Farry, A. R.; Wulandari, P. T.; Alfia, R.

2018-03-01

In this study was conducted to recover nickel metal from spent nickel catalyst resulting from hydrotreating process in petroleum industry. The nickel extraction study with the emulsion liquid membrane using Cyanex 272 as an extractant to extract and separate nickel from the feed phase solution. Feed phase solution was preapred from spent catalyst using sulphuric acid. Liquid membrane consists of a kerosene as diluent, a Span 80 as surfactant, a Cyanex 272 as carrier and sulphuric acid solutions have been used as the stripping solution. The important parameters governing the permeation of nickel and their effect on the separation process have been studied. These parameters are surfactant concentration, extractant concentration feed phase pH. The optimum conditions of the emulsion membrane making process is using 0.06 M Cyanex 272, 8% w/v SPAN 80, 0.05 M H2SO4, internal phase extractant / phase volume ratio: 1/1, and stirring speed 1150 rpm for 60 Minute that can produce emulsion membrane with stability level above 90% after 4 hours. In the extraction process with optimum condition pH 6 for feed phase, ratio of phase emulsion/phase of feed: 1/2, and stirring speed 175 rpm for 15 minutes with result 81.51% nickel was extracted.

Forests of Alabama, 2013

Treesearch

A. Hartsell

2014-01-01

This resource update provides an overview of forest resources in Alabama based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Alabama Forestry Commission.

Forests of Virginia, 2016

Treesearch

T.J. Brandeis; A.J. Hartsell; K.C. Randolph; C.M. Oswalt

2018-01-01

This resource update provides an overview of forest resources in Virginia based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the Virginia Department of Forestry.

Determination of the titratable acidity and the pH of wine based on potentiometric flow injection analysis.

PubMed

Vahl, Katja; Kahlert, Heike; von Mühlen, Lisandro; Albrecht, Anja; Meyer, Gabriele; Behnert, Jürgen

2013-07-15

A FIA system using a pH-sensitive detector based on a graphite/quinhydrone/silicone composite electrode was applied to determine sequentially the titratable acidity and the pH of wine, as well as the sum of calcium and magnesium ions. For all measurements the same FIA configuration was used employing different carrier solutions. The results for the determination of acidity and pH are in good agreement with those obtained by classical potentiometric titrations and by pH measurements using a conventional glass electrode. The standard deviation was less than 1.5% for both kinds of measurements and the sample volume was 150 μL. The method allows about 40 determinations of titratable acidity per hour and 30 pH measurements per hour. The titration method can be adjusted to the legal requirements in USA and Europe. Copyright © 2013 Elsevier B.V. All rights reserved.

Flow-injection assay of catalase activity.

PubMed

Ukeda, Hiroyuki; Adachi, Yukiko; Sawamura, Masayoshi

2004-03-01

A novel flow-injection assay (FIA) system with a double line for catalase activity was constructed in which an oxidase is immobilized and the substrate is continuously pumped to reduce the dissolved oxygen and to generate a given level of hydrogen peroxide. The catalase in a sample decomposed the hydrogen peroxide, and thus the increase in dissolved oxygen dependent on the activity was amperometrically monitored using a Clark-type oxygen electrode. Among the examined several oxidases, uricase was most suitable for the continuous formation of hydrogen peroxide from a consideration of the stability and the conversion efficiency. Under the optimum conditions, a linear calibration curve was obtained in the range from 21 to 210 units/mg and the reproducibility (CV) was better than 2% by 35 successive determinations of 210 units/ml catalase preparation. The sampling frequency was about 15 samples/h. The present FIA system was applicable to monitor the inactivation of catalase by glycation.

Development and characterization of a FIA system for selective assay of L-ascorbic acid in food samples.

PubMed

Vig, Attila; Igloi, Attila; Adanyi, Nora; Gyemant, Gyongyi; Csutoras, Csaba; Kiss, Attila

2010-10-01

An amperometric detector and an enzymatic reaction were combined for the measurement of L-ascorbic acid. The enzyme cell (containing immobilized ascorbate oxidase) was connected to a flow injection analyzer (FIA) system with a glassy carbon electrode as an amperometric detector. During optimization and measurements two sample injectors were used, one before and one after the enzyme cell, thus eliminating the background interferences. Subtraction of the signal area given in the presence of enzyme from the one given in the absence of enzyme was applied for measuring analyte concentrations and calibration at 400 mV. Analysis capacity of system is 25 samples/hour. The relative standard deviation (RSD) was below 5% (5 times repeated, 400 μmol/L conc.), linearity up to 400 μmol/L, limit of detection (LOD) 5 μmol/L, fitting of calibration curve in 25-400 μmol/L range was R (2) = 0.99.

[Determination of aluminum in sediments by atomic absorption spectrophotometer without FIA spectrophotometric analysis].

PubMed

Zhao, Zhen-yi; Han, Guang-xi; Song, Xi-ming; Luo, Zhi-xiong

2008-06-01

To search for a new method of determining, we developed a new flow injection analyzer, applied to the atomic absorption spectrophotometer, relying on it without flame in place of visible spectrophotometer, and studied the appropriate condition for the determination of aluminum in sediments, thus built up a kind of new analytical test technique. Three peak and two valley absorption values (A1, A2, A3, A4 and A5) can be continuously obtained simultaneously that all can be used for quantitative analysis, then we discussed its theory and experiment technique. Based on the additivity of absorbance (A = A1+A2+A3+A4+ A5), the sensitivity of FIA is enhanced, and its precision and linear relation are also good, raising the efficiency of AAS. The simple method has been applied to determining Al in sediments, and the results are satisfactory.

Amperometric Glucose Sensor Using Thermostable Co-Factor Binding Glucose Dehydrogenase

NASA Astrophysics Data System (ADS)

Nakazawa, Yukie; Yamazaki, Tomohiko; Tsugawa, Wakako; Ikebukuro, Kazunori; Sode, Koji

A thermostable mediator-type enzyme glucose sensor was constructed. The electrode was fabricated using chemically cross-linked thermostable co-factor binding glucose dehydrogenase (GDH) from thermophilic bacteria in carbon paste matrix. The electrode responded directly proportional to D-glucose concentration from 0.01 mM to 3 mM in stirred buffer containing 1 mM 1-methoxyphenazinemethosulfate as a mediator with the steady-state mode. The storage stability was examined by incubating the enzyme electrode at 50oC during the measurement. The cross-linked GDH immobilized electrode showed good storage stability. Ninety percent of its initial response was retained after incubation in buffer solution for 9 days at 50oC. The flow injection analysis (FIA) glucose sensing system was also constructed by immobilizing the cross-linked GDH and ferrocene as a mediator in the carbon paste matrix. The FIA system was able to measure 600 samples for 100 h.

Thermometric sensing of peroxide in organic media. Application to monitor the stability of RBP-retinol-HRP complex.

PubMed

Ramanathan, K; Jönsson, B R; Danielsson, B

2000-08-01

The stability of horseradish peroxidase (HRP) in aqueous and organic solvents is applied to develop a simple thermometric procedure to detect the binding of retinoic acid-HRP conjugate to retinol binding protein (RBP). Butanone peroxide (BP) in organic phase and hydrogen peroxide in aqueous phase is detected thermometrically on a HRP column, immobilized by cross-linking with glutaraldehyde on controlled pore glass (CPG). Acetone, acetonitrile, methanol, and 2-butanol are used for detection of BP, in the flow injection analysis (FIA) mode. A linear range between 1 and 50 mM BP is obtained in all the organic solvents with a precision of 5-7% (CV%). The magnitude and nature of the thermometric response is significantly different in each organic solvent. The stability of HRP in the organic phase is used to study the stability of a retinoic acid-HRP conjugate bound to immobilized RBP. The response of HRP (to 20 mM BP) in the retinoic acid-HRP conjugate is used as an indicator of the stability of the RBP-retinoic acid-HRP complex, after challenges with various organic/aqueous solvents. Both immobilized HRP and RBP are stable at least for 6 months. The effect of o-phenylene diamine on the thermometric response of HRP is also investigated. A scheme for the design of a thermometric retinol (vitamin A) biosensor is proposed.

Simulated Gastrointestinal Digestion, Bioaccessibility and Antioxidant Capacity of Polyphenols from Red Chiltepin (Capsicum annuum L. Var. glabriusculum) Grown in Northwest Mexico.

PubMed

Ovando-Martínez, Maribel; Gámez-Meza, Nohemí; Molina-Domínguez, Claudia Celeste; Hayano-Kanashiro, Corina; Medina-Juárez, Luis Angel

2018-06-01

Chiltepin, a wild chili mostly used in different traditional foods and traditional medicine in Northwest Mexico, represents a source of polyphenols. However, studies about the bioaccessibility of polyphenols as a parameter to measure the nutritional quality and bioefficacy of them in the fruit after consumption are scarce. Chiltepin showed phenolic acids and flavonoids contents between 387 and 65 μg/g, respectively. Nevertheless, these values decreased after the digestion process. Before digestion, gallic acid, 4-hydroxibenzoinc acid, chlorogenic acid, caffeic acid, p-coumaric acid, quercetin and luteolin were the main polyphenols found in chiltepin by HPLC-DAD and confirmed by FIA-ESI-IT-MS/MS. Gallic and chlorogenic acids were non-detected in the gastric phase, while only p-coumaric acid (5.35 ± 3.89 μg/g), quercetin (5.91 ± 0.92 μg/g) and luteolin (2.86 ± 0.62 μg/g) were found in the intestinal phase. The bioaccessibility of phenolic acids, flavonoids, and total polyphenols after the intestinal phase was around 24, 17 and 23%, respectively. Overall, results indicated that release of polyphenols from chiltepin fruit might be affected by the food matrix and gastrointestinal conditions due to the low bioaccessibility values observed.

Two-dimensional solid-phase extraction strategy for the selective enrichment of aminoglycosides in milk.

PubMed

Shen, Aijin; Wei, Jie; Yan, Jingyu; Jin, Gaowa; Ding, Junjie; Yang, Bingcheng; Guo, Zhimou; Zhang, Feifang; Liang, Xinmiao

2017-03-01

An orthogonal two-dimensional solid-phase extraction strategy was established for the selective enrichment of three aminoglycosides including spectinomycin, streptomycin, and dihydrostreptomycin in milk. A reversed-phase liquid chromatography material (C 18 ) and a weak cation-exchange material (TGA) were integrated in a single solid-phase extraction cartridge. The feasibility of two-dimensional clean-up procedure that experienced two-step adsorption, two-step rinsing, and two-step elution was systematically investigated. Based on the orthogonality of reversed-phase and weak cation-exchange procedures, the two-dimensional solid-phase extraction strategy could minimize the interference from the hydrophobic matrix existing in traditional reversed-phase solid-phase extraction. In addition, high ionic strength in the extracts could be effectively removed before the second dimension of weak cation-exchange solid-phase extraction. Combined with liquid chromatography and tandem mass spectrometry, the optimized procedure was validated according to the European Union Commission directive 2002/657/EC. A good performance was achieved in terms of linearity, recovery, precision, decision limit, and detection capability in milk. Finally, the optimized two-dimensional clean-up procedure incorporated with liquid chromatography and tandem mass spectrometry was successfully applied to the rapid monitoring of aminoglycoside residues in milk. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Process for radioisotope recovery and system for implementing same

DOEpatents

Meikrantz, David H [Idaho Falls, ID; Todd, Terry A [Aberdeen, ID; Tranter, Troy J [Idaho Falls, ID; Horwitz, E Philip [Naperville, IL

2009-10-06

A method of recovering daughter isotopes from a radioisotope mixture. The method comprises providing a radioisotope mixture solution comprising at least one parent isotope. The at least one parent isotope is extracted into an organic phase, which comprises an extractant and a solvent. The organic phase is substantially continuously contacted with an aqueous phase to extract at least one daughter isotope into the aqueous phase. The aqueous phase is separated from the organic phase, such as by using an annular centrifugal contactor. The at least one daughter isotope is purified from the aqueous phase, such as by ion exchange chromatography or extraction chromatography. The at least one daughter isotope may include actinium-225, radium-225, bismuth-213, or mixtures thereof. A liquid-liquid extraction system for recovering at least one daughter isotope from a source material is also disclosed.

Process for radioisotope recovery and system for implementing same

DOEpatents

Meikrantz, David H.; Todd, Terry A.; Tranter, Troy J.; Horwitz, E. Philip

2007-01-02

A method of recovering daughter isotopes from a radioisotope mixture. The method comprises providing a radioisotope mixture solution comprising at least one parent isotope. The at least one parent isotope is extracted into an organic phase, which comprises an extractant and a solvent. The organic phase is substantially continuously contacted with an aqueous phase to extract at least one daughter isotope into the aqueous phase. The aqueous phase is separated from the organic phase, such as by using an annular centrifugal contactor. The at least one daughter isotope is purified from the aqueous phase, such as by ion exchange chromatography or extraction chromatography. The at least one daughter isotope may include actinium-225, radium-225, bismuth-213, or mixtures thereof. A liquid-liquid extraction system for recovering at least one daughter isotope from a source material is also disclosed.

Extraction and characterization of polysaccharides from Semen Cassiae by microwave-assisted aqueous two-phase extraction coupled with spectroscopy and HPLC.

PubMed

Chen, Zhi; Zhang, Wei; Tang, Xunyou; Fan, Huajun; Xie, Xiujuan; Wan, Qiang; Wu, Xuehao; Tang, James Z

2016-06-25

A novel and rapid method for simultaneous extraction and separation of the different polysaccharides from Semen Cassiae (SC) was developed by microwave-assisted aqueous two-phase extraction (MAATPE) in a one-step procedure. Using ethanol/ammonium sulfate system as a multiphase solvent, the effects of MAATPE on the extraction of polysaccharides from SC such as the composition of the ATPS, extraction time, temperature and solvent-to-material ratio were investigated by UV-vis analysis. Under the optimum conditions, the yields of polysaccharides were 4.49% for the top phase, 8.80% for the bottom phase and 13.29% for total polysaccharides, respectively. Compared with heating solvent extraction and ultrasonic assisted extraction, MAATPE exhibited the higher extraction yields in shorter time. Fourier-transform infrared spectra showed that two polysaccharides extracted from SC to the top and bottom phases by MAATPE were different from each other in their chemical structures. Through acid hydrolysis and PMP derivatization prior to HPLC, analytical results by indicated that a polysaccharide of the top phases was a relatively homogeneous homepolysaccharide composed of dominant gucose glucose while that of the bottom phase was a water-soluble heteropolysaccharide with multiple components of glucose, xylose, arabinose, galactose, mannose and glucuronic acid. Molar ratios of monosaccharides were 95.13:4.27:0.60 of glucose: arabinose: galactose for the polysaccharide from the top phase and 62.96:14.07:6.67: 6.67:5.19:4.44 of glucose: xylose: arabinose: galactose: mannose: glucuronic acid for that from the bottom phase, respectively. The mechanism for MAATPE process was also discussed in detail. MAATPE with the aid of microwave and the selectivity of the ATPS not only improved yields of the extraction, but also obtained a variety of polysaccharides. Hence, it was proved as a green, efficient and promising alternative to simultaneous extraction of polysaccharides from SC. Copyright © 2016 Elsevier Ltd. All rights reserved.

Quick, easy, cheap, effective, rugged, and safe sample preparation approach for pesticide residue analysis using traditional detectors in chromatography: A review.

PubMed

Rahman, Md Musfiqur; Abd El-Aty, A M; Kim, Sung-Woo; Shin, Sung Chul; Shin, Ho-Chul; Shim, Jae-Han

2017-01-01

In pesticide residue analysis, relatively low-sensitivity traditional detectors, such as UV, diode array, electron-capture, flame photometric, and nitrogen-phosphorus detectors, have been used following classical sample preparation (liquid-liquid extraction and open glass column cleanup); however, the extraction method is laborious, time-consuming, and requires large volumes of toxic organic solvents. A quick, easy, cheap, effective, rugged, and safe method was introduced in 2003 and coupled with selective and sensitive mass detectors to overcome the aforementioned drawbacks. Compared to traditional detectors, mass spectrometers are still far more expensive and not available in most modestly equipped laboratories, owing to maintenance and cost-related issues. Even available, traditional detectors are still being used for analysis of residues in agricultural commodities. It is widely known that the quick, easy, cheap, effective, rugged, and safe method is incompatible with conventional detectors owing to matrix complexity and low sensitivity. Therefore, modifications using column/cartridge-based solid-phase extraction instead of dispersive solid-phase extraction for cleanup have been applied in most cases to compensate and enable the adaptation of the extraction method to conventional detectors. In gas chromatography, the matrix enhancement effect of some analytes has been observed, which lowers the limit of detection and, therefore, enables gas chromatography to be compatible with the quick, easy, cheap, effective, rugged, and safe extraction method. For liquid chromatography with a UV detector, a combination of column/cartridge-based solid-phase extraction and dispersive solid-phase extraction was found to reduce the matrix interference and increase the sensitivity. A suitable double-layer column/cartridge-based solid-phase extraction might be the perfect solution, instead of a time-consuming combination of column/cartridge-based solid-phase extraction and dispersive solid-phase extraction. Therefore, replacing dispersive solid-phase extraction with column/cartridge-based solid-phase extraction in the cleanup step can make the quick, easy, cheap, effective, rugged, and safe extraction method compatible with traditional detectors for more sensitive, effective, and green analysis. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Preliminary evaluation of monolithic column high-performance liquid chromatography with tris(2,2'-bipyridyl)ruthenium(II) chemiluminescence detection for the determination of quetiapine in human body fluids.

PubMed

Bellomarino, Sara A; Brown, Allyson J; Conlan, Xavier A; Barnett, Neil W

2009-03-15

High-performance liquid chromatography (HPLC) with tris(2,2'-bipyridyl)ruthenium(II) chemiluminescence detection methodology is reported for the determination of the atypical antipsychotic drug quetiapine and the observation of its major active and inactive metabolites in human urine and serum. The method uses a monolithic chromatographic column allowing high flow rates of 3 mLmin(-1) enabling rapid quantification. Flow injection analysis (FIA) with tris(2,2'-bipyridyl)ruthenium(II) chemiluminescence detection and HPLC time of flight mass spectrometry (TOF-MS) were used for the determination of quetiapine in a pharmaceutical preparation to establish its suitability as a calibration standard. The limit of detection achieved with FIA was 2 x 10(-11) molL(-1) in simple aqueous solution. The limits of detection achieved with HPLC were 7 x 10(-8) and 2 x 10(-10) molL(-1) in urine and serum, respectively. The calibration range for FIA was between 5 x 10(-9) and 1 x 10(-6) molL(-1). The calibration ranges for HPLC were between 1 x 10(-7)-1 x 10(-4) and 1 x 10(-8)-1 x 10(-4) molL(-1) in urine and serum, respectively. The quetiapine concentrations in patient samples were found to be 3 x 10(-6) molL(-1) in urine and 7 x 10(-7) molL(-1) in serum. Without the need for preconcentration, the HPLC detection limits compared favourably with those in previously published methodologies. The metabolites were identified using HPLC-TOF-MS.

Forests of South Carolina, 2015

Treesearch

T.J. Brandeis; A. Hartsell; C. Brandeis; K. Randolph; S. Oswalt

2016-01-01

This resource update provides an overview of forest resources in South Carolina based on an inventory conducted by the U.S. Forest Service, Forest Inventory and Analysis (FIA) program at the Southern Research Station in cooperation with the South Carolina Forestry Commission.

Measurement of dielectric constant of organic solvents by indigenously developed dielectric probe

NASA Astrophysics Data System (ADS)

Keshari, Ajay Kumar; Rao, J. Prabhakar; Rao, C. V. S. Brahmmananda; Ramakrishnan, R.; Ramanarayanan, R. R.

2018-04-01

The extraction, separation and purification of actinides (uranium and plutonium) from various matrices are an important step in nuclear fuel cycle. One of the separation process adopted in an industrial scale is the liquid-liquid extraction or solvent extraction. Liquid-liquid extraction uses a specific ligand/extractant in conjunction with suitable diluent. Solvent extraction or liquid-liquid extraction, involves the partitioning of the solute between two immiscible phases. In most cases, one of the phases is aqueous, and the other one is an organic solvent. The solvent used in solvent extraction should be selective for the metal of interest, it should have optimum distribution ratio, and the loaded metal from the organic phase should be easily stripped under suitable experimental conditions. Some of the important physical properties which are important for the solvent are density, viscosity, phase separation time, interfacial surface tension and the polarity of the extractant.

Projeto do sistema anti-ressonante da fiação dos transdutores para o detector Mario Schenberg

NASA Astrophysics Data System (ADS)

Vieira, S. J.., Jr.; Melo, J. L.

2003-08-01

O detector de ondas gravitacionais Mario Schenberg está sendo projetado e construído pelo grupo Gráviton. Sua construção está ocorrendo no Laboratório de Estado Sólido e Baixas Temperaturas (LESBT) da Universidade de São Paulo, na cidade de São Paulo. Esse detector possui uma massa ressonante esférica de cobre-alumínio, com 65 cm de diâmetro, pesando aproximadamente 1150 Kg, suspensa por um sistema de isolamento vibracional, que se encontra em fase de testes preliminares. A real eficácia desse sistema, entretanto, só poderá ser comprovada quando o detector estiver aparelhado com, pelo menos, um transdutor eletromecânico de altíssima sensibilidade acoplado à massa ressonante. Neste momento, não só este sistema de isolamento vibracional será posto em teste, como o do projeto da fiação que transporta os sinais de microondas até os transdutores e destes para a pré-amplificação. Apesar dessa fiação ter sido projetada para não apresentar nenhum contato com a superfície esférica da antena, de maneira a não haver nenhuma transmissão de ruído vibracional do laboratório para esta, deve-se minimizar o ruído microfônico produzido nessa fiação por oscilações mecânicas, uma vez que ela não utiliza nenhum sistema de isolamento vibracional. Com o intuito de resolver este problema, projetamos uma estrutura, formada por pequenos cilindros conectados por barras, a qual não terá nenhuma ressonância mecânica na faixa de freqüências de interesse para detecção (3000 - 3400 Hz). Desta forma, as vibrações nessa faixa não serão amplificadas. O projeto foi feito usando iterativamente, de maneira a otimizar os resultados obtidos, o programa de elementos finitos Msc/Nastran. Através de simulações feitas neste programa, determinamos os parâmetros geométricos ideais a serem utilizados, os quais proporcionam a maior região espectral de interesse livre de ressonâncias.

Quantitative ionspray liquid chromatographic/tandem mass spectrometric determination of reserpine in equine plasma.

PubMed

Anderson, M A; Wachs, T; Henion, J D

1997-02-01

A method based on ionspray liquid chromatography/tandem mass spectrometry (LC/MS/MS) was developed for the determination of reserpine in equine plasma. A comparison was made of the isolation of reserpine from plasma by liquid-liquid extraction and by solid-phase extraction. A structural analog, rescinnamine, was used as the internal standard. The reconstituted extracts were analyzed by ionspray LC/MS/MS in the selected reaction monitoring (SRM) mode. The calibration graph for reserpine extracted from equine plasma obtained using liquid-liquid extraction was linear from 10 to 5000 pg ml-1 and that using solid-phase extraction from 100 to 5000 pg ml-1. The lower level of quantitation (LLQ) using liquid-liquid and solid-phase extraction was 50 and 200 pg ml-1, respectively. The lower level of detection for reserpine by LC/MS/MS was 10 pg ml-1. The intra-assay accuracy did not exceed 13% for liquid-liquid and 12% for solid-phase extraction. The recoveries for the LLQ were 68% for liquid-liquid and 58% for solid-phase extraction.

Solvent Extraction of Sodium Hydroxide Using Alkylphenols and Fluorinated Alcohols: Understanding the Extraction Mechanism by Equilibrium Modeling

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kang, Hyun-Ah; Engle, Nancy L.; Bonnesen Peter V.

2004-03-29

In the present work, it has been the aim to examine extraction efficiencies of nine proton-ionizable alcohols (HAs) in 1-octanol and to identify both the controlling equilibria and predominant species involved in the extraction process within a thermochemical model. Distribution ratios for sodium (DNa) extraction were measured as a function of organic-phase HA and aqueous-phase NaOH molarity at 25 °C. Extraction efficiency follows the expected order of acidity of the HAs, 4-(tert-octyl) phenol (HA 1a) and 4-noctyl- a,a-bis-(trifluoromethyl)benzyl alcohol (HA 2a) being the most efficient extractants among the compounds tested. By use of the equilibrium-modeling program SXLSQI, a model formore » the extraction of NaOH has been advanced based on an ion-pair extraction by the diluent to give organic-phase Na+OH- and corresponding free ions and cation exchange by the weak acids to form monomeric organic-phase Na+A- and corresponding free organic-phase ions.« less

A review on solid phase extraction of actinides and lanthanides with amide based extractants.

PubMed

Ansari, Seraj A; Mohapatra, Prasanta K

2017-05-26

Solid phase extraction is gaining attention from separation scientists due to its high chromatographic utility. Though both grafted and impregnated forms of solid phase extraction resins are popular, the later is easy to make by impregnating a given organic extractant on to an inert solid support. Solid phase extraction on an impregnated support, also known as extraction chromatography, combines the advantages of liquid-liquid extraction and the ion exchange chromatography methods. On the flip side, the impregnated extraction chromatographic resins are less stable against leaching out of the organic extractant from the pores of the support material. Grafted resins, on the other hand, have a higher stability, which allows their prolong use. The goal of this article is a brief literature review on reported actinide and lanthanide separation methods based on solid phase extractants of both the types, i.e., (i) ligand impregnation on the solid support or (ii) ligand functionalized polymers (chemically bonded resins). Though the literature survey reveals an enormous volume of studies on the extraction chromatographic separation of actinides and lanthanides using several extractants, the focus of the present article is limited to the work carried out with amide based ligands, viz. monoamides, diamides and diglycolamides. The emphasis will be on reported applied experimental results rather than on data pertaining fundamental metal complexation. Copyright © 2017 Elsevier B.V. All rights reserved.

Ecosystem Services Derived from Headwater Catchments

EPA Science Inventory

We used data from the USEPA’s wadeable streams assessment (WSA), US Forest Service’s forest inventory and analysis (FIA), and select USFS experimental forests (EF) to investigate potential ecosystems services derived from headwater catchments. C, N, and P inputs to these catchmen...

Forests of Mississippi, 2014

Treesearch

S.N. Oswalt

2015-01-01

This resource update provides an overview of forest resources in Mississippi based on an inventory conducted by the Forest Inventory and Analysis (FIA) Program at the Southern Research Station of the Forest Service, U.S. Department of Agriculture in cooperation with the Mississippi Forestry Commission.

A combination strategy for extraction and isolation of multi-component natural products by systematic two-phase solvent extraction-(13)C nuclear magnetic resonance pattern recognition and following conical counter-current chromatography separation: Podophyllotoxins and flavonoids from Dysosma versipellis (Hance) as examples.

PubMed

Yang, Zhi; Wu, Youqian; Wu, Shihua

2016-01-29

Despite of substantial developments of extraction and separation techniques, isolation of natural products from natural resources is still a challenging task. In this work, an efficient strategy for extraction and isolation of multi-component natural products has been successfully developed by combination of systematic two-phase liquid-liquid extraction-(13)C NMR pattern recognition and following conical counter-current chromatography separation. A small-scale crude sample was first distributed into 9 systematic hexane-ethyl acetate-methanol-water (HEMWat) two-phase solvent systems for determination of the optimum extraction solvents and partition coefficients of the prominent components. Then, the optimized solvent systems were used in succession to enrich the hydrophilic and lipophilic components from the large-scale crude sample. At last, the enriched components samples were further purified by a new conical counter-current chromatography (CCC). Due to the use of (13)C NMR pattern recognition, the kinds and structures of major components in the solvent extracts could be predicted. Therefore, the method could collect simultaneously the partition coefficients and the structural information of components in the selected two-phase solvents. As an example, a cytotoxic extract of podophyllotoxins and flavonoids from Dysosma versipellis (Hance) was selected. After the systematic HEMWat system solvent extraction and (13)C NMR pattern recognition analyses, the crude extract of D. versipellis was first degreased by the upper phase of HEMWat system (9:1:9:1, v/v), and then distributed in the two phases of the system of HEMWat (2:8:2:8, v/v) to obtain the hydrophilic lower phase extract and lipophilic upper phase extract, respectively. These extracts were further separated by conical CCC with the HEMWat systems (1:9:1:9 and 4:6:4:6, v/v). As results, total 17 cytotoxic compounds were isolated and identified. In general, whole results suggested that the strategy was very efficient for the systematic extraction and isolation of biological active components from the complex biomaterials. Copyright © 2016 Elsevier B.V. All rights reserved.

Plasma and Serum Metabolite Association Networks: Comparability within and between Studies Using NMR and MS Profiling.

PubMed

Suarez-Diez, Maria; Adam, Jonathan; Adamski, Jerzy; Chasapi, Styliani A; Luchinat, Claudio; Peters, Annette; Prehn, Cornelia; Santucci, Claudio; Spyridonidis, Alexandros; Spyroulias, Georgios A; Tenori, Leonardo; Wang-Sattler, Rui; Saccenti, Edoardo

2017-07-07

Blood is one of the most used biofluids in metabolomics studies, and the serum and plasma fractions are routinely used as a proxy for blood itself. Here we investigated the association networks of an array of 29 metabolites identified and quantified via NMR in the plasma and serum samples of two cohorts of ∼1000 healthy blood donors each. A second study of 377 individuals was used to extract plasma and serum samples from the same individual on which a set of 122 metabolites were detected and quantified using FIA-MS/MS. Four different inference algorithms (ARANCE, CLR, CORR, and PCLRC) were used to obtain consensus networks. The plasma and serum networks obtained from different studies showed different topological properties with the serum network being more connected than the plasma network. On a global level, metabolite association networks from plasma and serum fractions obtained from the same blood sample of healthy people show similar topologies, and at a local level, some differences arise like in the case of amino acids.

Characterisation of chamomile volatiles by simultaneous distillation solid-phase extraction in comparison to hydrodistillation and simultaneous distillation extraction.

PubMed

Krüger, Hans

2010-05-01

A new method for complete separation of steam-volatile organic compounds is described using the example of chamomile flowers. This method is based on the direct combination of hydrodistillation and solid-phase extraction in a circulation apparatus. In contrast to hydrodistillation and simultaneous distillation extraction (SDE), an RP-18 solid phase as adsorptive material is used rather than a water-insoluble solvent. Therefore, a prompt and complete fixation of all volatiles takes place, and the circulation of water-soluble bisabololoxides as well as water-soluble and thermolabile en-yne-spiroethers is inhibited. This so-called simultaneous distillation solid-phase extraction (SD-SPE) provides extracts that better characterise the real composition of the vapour phase, as well as the composition of inhalation vapours, than do SDE extracts or essential oils obtained by hydrodistillation. The data indicate that during inhalation therapy with chamomile, the bisabololoxides and spiroethers are more strongly involved in the inhaling activity than so far assumed. Georg Thieme Verlag KG Stuttgart New York.

Development of "ultrasound-assisted dynamic extraction" and its combination with CCC and CPC for simultaneous extraction and isolation of phytochemicals.

PubMed

Zhang, Yuchi; Liu, Chunming; Li, Jing; Qi, Yanjuan; Li, Yuchun; Li, Sainan

2015-09-01

A new method for the extraction of medicinal herbs termed ultrasonic-assisted dynamic extraction (UADE) was designed and evaluated. This technique was coupled with counter-current chromatography (CCC) and centrifugal partition chromatography (CPC) and then applied to the continuous extraction and online isolation of chemical constituents from Paeonia lactiflora Pall (white peony) roots. The mechanical parameters, including the pitch and diameter of the shaft, were optimized by means of mathematical modeling. Furthermore, the configuration and mechanism of online UADE coupled with CCC and CPC were elaborated. The stationary phases of the two-phase solvent systems from CCC and CPC were utilized as the UADE solution. The extraction solution was pumped into the sample loop and then introduced into the CCC column; the target compounds were eluted with the lower aqueous phase of the two-phase solvent system. During the CCC separation, the extraction solution was continuously fed in the sample loop by turning the ten-port valve; the extraction solution was then pumped into the CPC column and eluted by the mobile phase of the two-phase solvent system mentioned above. When the first cycle of the UADE/CCC/CPC was completed, the second cycle experiment could be carried out, and so on. Four target compounds (albiflorin, benzoylpaeoniflorin, paeoniflorin, and galloylpaeoniflorin) with purities above 94.96% were successfully extracted and isolated online using the two-phase solvent system comprising ethyl acetate-n-butanol-ethanol-water (1:3.5:2:4.5, v/v/v/v). Compared with conventional extraction methods, the instrumental setup of the present method offers the advantages of automation and systematic extraction and isolation of natural products. Crown Copyright © 2015. Published by Elsevier B.V. All rights reserved.

Determination of hexavalent chromium in industrial hygiene samples using ultrasonic extraction and flow injection analysis.

PubMed

Wang, J; Ashley, K; Kennedy, E R; Neumeister, C

1997-11-01

A simple, fast, and sensitive method was developed for the determination of hexavalent chromium (CrVI) in workplace samples. Ultrasonic extraction in alkaline solutions with 0.05 M (NH4)2SO4-0.05 M NH3 provided good extraction efficiency of CrVI from the sample and allowed the retention of CrVI on an ion-exchange resin (95%). The CrVI in the sample solution was then separated as an anion from trivalent chromium [CrIII] and other cations by elution from the anion-exchange resin with 0.5 M (NH4)2SO4 in 0.1 M NH3 (pH 8) buffer solution. The eluate was then acidified with hydrochloric acid and complexed with 1,5-diphenylcarbazide reagent prior to flow injection analysis. By analyzing samples with and without oxidation of CrIII to CrVI using CeIV, the method can measure CrVI and total Cr. For optimizing the separation and determination procedure, preliminary trials conducted with two certified reference materials (CRMs 013-050 and NIST 1633a) and three spiked samples (ammonia buffer solution, cellulose ester filters and acid washed sand) indicated that the recovery of CrVI was quantitative (> 90%) with this method. The limit of detection for FIA-UV/VIS determination of the Cr-diphenylcarbazone complex was in the sub-nanogram range (0.11 ng). The technique was also applied successfully to a workplace coal fly ash sample that was collected from a power plant and paint chips that were collected from a heating gas pipe and a university building. The principal advantages of this method are its simplicity, sensitivity, speed and potential portability for field analysis.

I-line stepper based overlay evaluation method for wafer bonding applications

NASA Astrophysics Data System (ADS)

Kulse, P.; Sasai, K.; Schulz, K.; Wietstruck, M.

2018-03-01

In the last decades the semiconductor technology has been driven by Moore's law leading to high performance CMOS technologies with feature sizes of less than 10 nm [1]. It has been pointed out that not only scaling but also the integration of novel components and technology modules into CMOS/BiCMOS technologies is becoming more attractive to realize smart and miniaturized systems [2]. Driven by new applications in the area of communication, health and automation, new components and technology modules such as BiCMOS embedded RF-MEMS, high-Q passives, Sibased microfluidics and InP-SiGe BiCMOS heterointegration have been demonstrated [3-6]. In contrast to standard VLSI processes fabricated on front side of the silicon wafer, these new technology modules additionally require to process the backside of the wafer; thus require an accurate alignment between the front and backside of the wafer. In previous work an advanced back to front side alignment technique and implementation into IHP's 0.25/0.13 µm high performance SiGe:C BiCMOS backside process module has been presented [7]. The developed technique enables a high resolution and accurate lithography on the backside of BiCMOS wafer for additional backside processing. In addition to the aforementioned back side process technologies, new applications like Through-Silicon Vias (TSV) for interposers and advanced substrate technologies for 3D heterogeneous integration demand not only single wafer fabrication but also processing of wafer stacks provided by temporary and permanent wafer bonding [8-9]. In this work, the non-contact infrared alignment system of the Nikon® i-line Stepper NSR-SF150 for both alignment and the overlay determination of bonded wafer stacks with embedded alignment marks are used to achieve an accurate alignment between the different wafer sides. The embedded field image alignment (FIA) marks of the interface and the device wafer top layer are measured in a single measurement job. By taking the offsets between all different FIA's into account, after correcting the wafer rotation induced FIA position errors, hence an overlay for the stacked wafers can be determined. The developed approach has been validated by a standard front side resist in resist experiment. After the successful validation of the developed technique, special wafer stacks with FIA alignment marks in the bonding interface are fabricated and exposed. Following overlay calculation shows an overlay of less than 200 nm, which enables very accurate process condition for highly scaled TSV integration and advanced substrate integration into IHP's 0.25/0.13 µm SiGe:C BiCMOS technology. The developed technique also allows using significantly smaller alignment marks (i.e. standard FIA alignment marks). Furthermore, the presented method is used, in case of wafer bow related overlay tool problems, for the overlay evaluation of the last two metal layers from production wafers prepared in IHP's standard 0.25/0.13 µm SiGe:C BiCMOS technology. In conclusion, the exposure and measurement job can be done with the same tool, minimizing the back to front side/interface top layer misalignment which leads to a significant device performance improvement of backside/TSV integrated components and technologies.

Dual-wavelength phase-shifting digital holography selectively extracting wavelength information from wavelength-multiplexed holograms.

PubMed

Tahara, Tatsuki; Mori, Ryota; Kikunaga, Shuhei; Arai, Yasuhiko; Takaki, Yasuhiro

2015-06-15

Dual-wavelength phase-shifting digital holography that selectively extracts wavelength information from five wavelength-multiplexed holograms is presented. Specific phase shifts for respective wavelengths are introduced to remove the crosstalk components and extract only the object wave at the desired wavelength from the holograms. Object waves in multiple wavelengths are selectively extracted by utilizing 2π ambiguity and the subtraction procedures based on phase-shifting interferometry. Numerical results show the validity of the proposed technique. The proposed technique is also experimentally demonstrated.

Phase 1 remediation of jet fuel contaminated soil and groundwater at JFK International Airport using dual phase extraction and bioventing

DOE Office of Scientific and Technical Information (OSTI.GOV)

Roth, R.; Bianco, P. Rizzo, M.; Pressly, N.

1995-12-31

Soil and groundwater contaminated with jet fuel at Terminal One of the JFK International Airport in New York have been remediated using dual phase extraction (DPE) and bioventing. Two areas were remediated using 51 DPE wells and 20 air sparging/air injection wells. The total area remediated by the DPE wells is estimated to be 4.8 acres. Groundwater was extracted to recover nonaqueous phase and aqueous phase jet fuel from the shallow aquifer and treated above ground by the following processes; oil/water separation, iron-oxidation, flocculation, sedimentation, filtration, air stripping and liquid-phase granular activated carbon (LPGAC) adsorption. The extracted vapors were treatedmore » by vapor-phase granular activated carbon (VPGAC) adsorption in one area, and catalytic oxidation and VPGAC adsorption in another area. After 6 months of remediation, approximately 5,490 lbs. of volatile organic compounds (VOCs) were removed by soil vapor extraction (SVE), 109,650 lbs. of petroleum hydrocarbons were removed from the extracted groundwater, and 60,550 lbs. of petroleum hydrocarbons were biologically oxidized by subsurface microorganisms. Of these three mechanisms, the rate of petroleum hydrocarbon removal was the highest for biological oxidation in one area and by groundwater extraction in another area.« less

Michigan's forest resources, 2009

Treesearch

S.A. Pugh

2010-01-01

This publication provides an overview of forest resource attributes for Michigan based on an annual inventory (2005-2009) conducted by the Forest Inventory and Analysis (FIA) program of the Northern Research Station, U.S. Forest Service. These estimates, along with web-posted core tables, are updated annually.

Nebraska's forest resources, 2008

Treesearch

D.M. Meneguzzo

2010-01-01

This publication provides an overview of forest resource attributes for Nebraska based on an annual inventory conducted by the Forest Inventory and Analysis (FIA) program at the Northern Research Station of the USDA Forest Service. These estimates, along with web-posted core tables, will be updated annually.

Separation of rare earths from transition metals by liquid-liquid extraction from a molten salt hydrate to an ionic liquid phase.

PubMed

Rout, Alok; Binnemans, Koen

2014-02-28

The solvent extraction of trivalent rare-earth ions and their separation from divalent transition metal ions using molten salt hydrates as the feed phase and an undiluted fluorine-free ionic liquid as the extracting phase were investigated in detail. The extractant was tricaprylmethylammonium nitrate, [A336][NO3], and the hydrated melt was calcium nitrate tetrahydrate, Ca(NO3)2·4H2O. The extraction behavior of rare-earth ions was studied for solutions of individual elements, as well as for mixtures of rare earths in the hydrated melt. The influence of different extraction parameters was investigated: the initial metal loading in the feed phase, percentage of water in the feed solution, equilibration time, and the type of hydrated melt. The extraction of rare earths from Ca(NO3)2·4H2O was compared with extraction from CaCl2·4H2O by [A336][Cl] (Aliquat 336). The nitrate system was found to be the better one. The extraction and separation of rare earths from the transition metals nickel, cobalt and zinc were also investigated. Remarkably high separation factors of rare-earth ions over transition metal ions were observed for extraction from Ca(NO3)2·4H2O by the [A336][NO3] extracting phase. Furthermore, rare-earth ions could be separated efficiently from transition metal ions, even in melts with very high concentrations of transition metal ions. Rare-earth oxides could be directly dissolved in the Ca(NO3)2·4H2O phase in the presence of small amounts of Al(NO3)3·9H2O or concentrated nitric acid. The efficiency of extraction after dissolving the rare-earth oxides in the hydrated nitrate melt was identical to extraction from solutions with rare-earth nitrates dissolved in the molten phase. The stripping of the rare-earth ions from the loaded ionic liquid phase and the reuse of the recycled ionic liquid were also investigated in detail.

Feasibility of Surfactant-Free Supported Emulsion Liquid Membrane Extraction

NASA Technical Reports Server (NTRS)

Hu, Shih-Yao B.; Li, Jin; Wiencek, John M.

2001-01-01

Supported emulsion liquid membrane (SELM) is an effective means to conduct liquid-liquid extraction. SELM extraction is particularly attractive for separation tasks in the microgravity environment where density difference between the solvent and the internal phase of the emulsion is inconsequential and a stable dispersion can be maintained without surfactant. In this research, dispersed two-phase flow in SELM extraction is modeled using the Lagrangian method. The results show that SELM extraction process in the microgravity environment can be simulated on earth by matching the density of the solvent and the stripping phase. Feasibility of surfactant-free SELM (SFSELM) extraction is assessed by studying the coalescence behavior of the internal phase in the absence of the surfactant. Although the contacting area between the solvent and the internal phase in SFSELM extraction is significantly less than the area provided by regular emulsion due to drop coalescence, it is comparable to the area provided by a typical hollow-fiber membrane. Thus, the stripping process is highly unlikely to become the rate-limiting step in SFSELM extraction. SFSELM remains an effective way to achieve simultaneous extraction and stripping and is able to eliminate the equilibrium limitation in the typical solvent extraction processes. The SFSELM design is similar to the supported liquid membrane design in some aspects.

[Growth inhibition of the four species of red tide microalgae by extracts from Enteromorpha prolifera extracted with the five solvents].

PubMed

Sun, Ying-Ying; Liu, Xiao-Xiao; Wang, Chang-Hai

2010-06-01

To study the effects of extracts of Enteromorpha prolifera on the growth of the four species of red tide microalgae (Amphidinium hoefleri, Karenia mikimitoi, Alexandrium tamarense and Skeletonema costatum), the extracts were extracted with five solvents (methanol, acetone, ethyl acetate, chloroform and petroleum ether), respectively. Based on the observation of algal morphology and the measurement of algal density, cell size and the contents of physiological indicators (chlorophyll, protein and polysaccharide), the results showed methanol extracts of E. prolifera had the strongest action. The inhibitory effects of A. hoefleri, K. mikimitoi, A. tamarense and S. costatum by the methanol extracts were 54.0%, 48.1%, 44.0% and 37.5% in day 10, respectively. The extracts of E. prolifera extracted with methanol, acetone and ethyl acetate caused cavities, pieces and pigment reduction in cells, and those with chloroform and petroleum ether caused goffers on cells. The extracts of E. prolifera extracted with all the five solvents decreased athletic ability of the cells, among which those extracted with ethyl acetate, chloroform and petroleum ether decreased cell size of test microalgae. The further investigation found that the methanol extracts significantly decreased contents of chlorophyll, protein and polysaccharide in the cells of those microalgae. The inhibitory effect of chlorophyll, protein and polysaccharide contents of four species of microalgae by the methanol extracts was about 51%. On the basis of the above experiments, dry powder of E. prolifera were extracts with methanol, and extracts were obtained. The methanol extracts were partitioned to petroleum ether phase, ethyl acetate phase, n-butanol phase and distilled water phase by liquid-liquid fractionation, and those with petroleum ether and ethyl acetate significantly inhibited the growth of all test microalgae, and the inhibitory effect of four species of microalgae by those two extracts was above 25% in day 10. Our researches expressed that antialgal substances in E. prolifera extracted with methanol were obtained. And two fractions (petroleum ether phase and ethyl acetate phase) that inhibited the growth of all test microalgae were obtained when the methanol extracts was fractionated by liquid-liquid fractionation.

Aptamer-functionalized Fe3 O4 magnetic nanoparticles as a solid-phase extraction adsorbent for the selective extraction of berberine from Cortex phellodendri.

PubMed

Jiang, Ling-Feng; Chen, Bo-Cheng; Chen, Ben; Li, Xue-Jian; Liao, Hai-Lin; Zhang, Wen-Yan; Wu, Lin

2017-07-01

The extraction adsorbent was fabricated by immobilizing the highly specific recognition and binding of aptamer onto the surface of Fe 3 O 4 magnetic nanoparticles, which not only acted as recognition elements to recognize and capture the target molecule berberine from the extract of Cortex phellodendri, but also could favor the rapid separation and purification of the bound berberine by using an external magnet. The developed solid-phase extraction method in this work was useful for the selective extraction and determination of berberine in Cortex phellodendri extracts. Various conditions such as the amount of aptamer-functionalized Fe 3 O 4 magnetic nanoparticles, extraction time, temperature, pH value, Mg 2+ concentration, elution time and solvent were optimized for the solid-phase extraction of berberine. Under optimal conditions, the purity of berberine extracted from Cortex phellodendri was as high as 98.7% compared with that of 4.85% in the extract, indicating that aptamer-functionalized Fe 3 O 4 magnetic nanoparticles-based solid-phase extraction method was very effective for berberine enrichment and separation from a complex herb extract. The applicability and reliability of the developed solid-phase extraction method were demonstrated by separating berberine from nine different concentrations of one Cortex phellodendri extract. The relative recoveries of the spiked solutions of all the samples were between 95.4 and 111.3%, with relative standard deviations ranging between 0.57 and 1.85%. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Using precursor ion scan of 184 with liquid chromatography-electrospray ionization-tandem mass spectrometry for concentration normalization in cellular lipidomic studies.

PubMed

Chao, Hsi-Chun; Chen, Guan-Yuan; Hsu, Lih-Ching; Liao, Hsiao-Wei; Yang, Sin-Yu; Wang, San-Yuan; Li, Yu-Liang; Tang, Sung-Chun; Tseng, Yufeng Jane; Kuo, Ching-Hua

2017-06-08

Cellular lipidomic studies have been favored approaches in many biomedical research areas. To provide fair comparisons of the studied cells, it is essential to perform normalization of the determined concentration before lipidomic analysis. This study proposed a cellular lipidomic normalization method by measuring the phosphatidylcholine (PC) and sphingomyelin (SM) contents in cell extracts. To provide efficient analysis of PC and SM in cell extracts, flow injection analysis-electrospray ionization-tandem mass spectrometry (FIA-ESI-MS/MS) with a precursor ion scan (PIS) of m/z 184 was used, and the parameters affecting the performance of the method were optimized. Good linearity could be observed between the cell extract dilution factor and the reciprocal of the total ion chromatogram (TIC) area in the PIS of m/z 184 within the dilution range of 1- to 16-fold (R 2  = 0.998). The calibration curve could be used for concentration adjustment of the unknown concentration of a cell extract. The intraday and intermediate precisions were below 10%. The accuracy ranged from 93.0% to 105.6%. The performance of the new normalization method was evaluated using different numbers of HCT-116 cells. Sphingosine, ceramide (d18:1/18:0), SM (d18:1/18:0) and PC (16:1/18:0) were selected as the representative test lipid species, and the results showed that the peak areas of each lipid species obtained from different cell numbers were within a 20% variation after normalization. Finally, the PIS of 184 normalization method was applied to study ischemia-induced neuron injury using oxygen and glucose deprivation (OGD) on primary neuronal cultured cells. Our results showed that the PIS of 184 normalization method is an efficient and effective approach for concentration normalization in cellular lipidomic studies. Copyright © 2017 Elsevier B.V. All rights reserved.

Characterization and optimization of low cost microfluidic thread based electroanalytical device for micro flow injection analysis.

PubMed

Agustini, Deonir; Bergamini, Márcio F; Marcolino-Junior, Luiz Humberto

2017-01-25

The micro flow injection analysis (μFIA) is a powerful technique that uses the principles of traditional flow analysis in a microfluidic device and brings a number of improvements related to the consumption of reagents and samples, speed of analysis and portability. However, the complexity and cost of manufacturing processes, difficulty in integrating micropumps and the limited performance of systems employing passive pumps are challenges that must be overcome. Here, we present the characterization and optimization of a low cost device based on cotton threads as microfluidic channel to perform μFIA based on passive pumps with good analytical performance in a simple, easy and inexpensive way. The transport of solutions is made through cotton threads by capillary force facilitated by gravity. After studying and optimizing several features related to the device, were obtained a flow rate of 2.2 ± 0.1 μL s -1 , an analytical frequency of 208 injections per hour, a sample injection volume of 2.0 μL and a waste volume of approximately 40 μL per analysis. For chronoamperometric determination of naproxen, a detection limit of 0.29 μmol L -1 was reached, with a relative standard deviation (RSD) of 1.69% between injections and a RSD of 3.79% with five different devices. Thus, based on the performance presented by proposed microfluidic device, it is possible to overcome some limitations of the μFIA systems based on passive pumps and allow expansion in the use of this technique. Copyright © 2016 Elsevier B.V. All rights reserved.

Flow-injection amperometric determination of glucose using a biosensor based on immobilization of glucose oxidase onto Au seeds decorated on core Fe₃O₄ nanoparticles.

PubMed

Samphao, Anchalee; Butmee, Preeyanut; Jitcharoen, Juthamas; Švorc, Ľubomír; Raber, Georg; Kalcher, Kurt

2015-09-01

An amperometric biosensor based on chemisorption of glucose oxidase (GOx) on Au seeds decorated on magnetic core Fe3O4 nanoparticles (Fe3O4@Au) and their immobilization on screen-printed carbon electrode bulk-modified with manganese oxide (SPCE{MnO2}) was designed for the determination of glucose. The Fe3O4@Au/GOx modified SPCE{MnO2} was used in a flow-injection analysis (FIA) arrangement. The experimental conditions were investigated in amperometric mode with the following optimized parameters: flow rate 1.7 mL min(-1), applied potential +0.38 V, phosphate buffer solution (PBS; 0.1 mol L(-1), pH 7.0) as carrier and 3.89 unit mm(-2) enzyme glucose oxidase loading on the active surface of the SPCE. The designed biosensor in FIA arrangement yielded a linear dynamic range for glucose from 0.2 to 9.0 mmol L(-1) with a sensitivity of 2.52 µA mM(-1) cm(-2), a detection limit of 0.1 mmol L(-1) and a quantification limit of 0.3 mmol L(-1). Moreover, a good repeatability of 2.8% (number of measurements n=10) and a sufficient reproducibility of 4.0% (number of sensors n=3) were achieved. It was found that the studied system Fe3O4@Au facilitated not only a simpler enzyme immobilization but also provided wider linear range. The practical application of the proposed biosensor for FIA quantification of glucose was tested in glucose sirup samples, honeys and energy drinks with the results in good accordance with those obtained by an optical glucose meter and with the contents declared by the producers. Copyright © 2015. Published by Elsevier B.V.

Analysis And Assessment Of Forest Cover Change For The State Of Wisconsin

NASA Astrophysics Data System (ADS)

Perry, C. H.; Nelson, M. D.; Stueve, K.; Gormanson, D.

2010-12-01

The Forest Inventory and Analysis (FIA) program of the USDA Forest Service is charged with documenting the status and trends of forest resources of the United States. Since the 1930s, FIA has implemented an intensive field campaign that collects measurements on plots distributed across all ownerships, historically completing analyses which include estimates of forest area, volume, mortality, growth, removals, and timber products output in various ways, such as by ownership, region, or State. Originally a periodic inventory, FIA has been measuring plots on an annual basis since the passage of the Agriculture Research, Extension and Education Reform Act of 1998 (Farm Bill). The resulting change in sampling design and intensity presents challenges to establishing baseline and measuring changes in forest area and biomass. A project jointly sponsored by the Forest Service and the National Aeronautics and Space Agency (NASA) titled “Integrating Landscape-scale Forest Measurements with Remote Sensing and Ecosystem Models to Improve Carbon Management Decisions” seeks to improve estimates of landscape- and continental-scale carbon dynamics and causes of change for North American forest land, and to use this information to support land management decisions. Specifically, we are developing and applying methods to scale up intensive biomass and carbon measurements from the field campaign to larger land management areas while simultaneously estimating change in the above-ground forest carbon stocks; the State of Wisconsin is being used as the testbed for this large-scale integration remote sensing with field measurements. Once defined, the temporal and spatial patterns of forest resources by watershed for Lake Superior and Lake Michigan outputs are being integrated into water quality assessments for the Great Lakes.

Removal of copper and iron by polyurethane foam column in FIA system for the determination of nickel in pierced ring.

PubMed

Vongboot, Monnapat; Suesoonthon, Monrudee

2015-01-01

Polyurethane foam (PUF) mini-column was used to eliminate copper and iron for the determination of nickel in pierced rings. The PUF mini-column was connected to FIA system for on-line sorption of copper and iron in complexes form of CuSCN(+) and FeSCN(2+). For this season, the acid solution containing a mixture of Ni(II), Fe(III), Cu(II) and SCN(-) ions was firstly flew into the PUF column. Then, the percolated solution which Fe(III) and Cu(II) ions is separated from analysis was injected into FIA system to react with 4-(2-pyridylazo) resorcinol (PAR) reagent in basic condition which this method is called pH gradient technique. The Ni-PAR complexes obtained were measured theirs absorbance at 500 nm by UV visible spectrophotometer. In this study, it was found that Cu(II) and Fe(III) were completely to form complexes with 400 mmol/L KSCN and entirely to eliminate in acidic condition at pH 3.0. In the optimum condition of these experiments, the method provided the linear relationship between absorbance and the concentration of Ni(II) in the range from 5.00 to 30.00 mg/L. Linear equation is y=0.0134x+0.0033 (R(2)=0.9948). Precision, assessed in the term of the relative standard deviation, RSD, and accuracy for multiple determinations obtained in values of 0.77-1.73% and 97.4%, respectively. The level of an average amount of Ni(II) in six piercing rings was evaluated to be 14.78 mg/g. Copyright © 2014 Elsevier B.V. All rights reserved.

Sensor-based auto-focusing system using multi-scale feature extraction and phase correlation matching.

PubMed

Jang, Jinbeum; Yoo, Yoonjong; Kim, Jongheon; Paik, Joonki

2015-03-10

This paper presents a novel auto-focusing system based on a CMOS sensor containing pixels with different phases. Robust extraction of features in a severely defocused image is the fundamental problem of a phase-difference auto-focusing system. In order to solve this problem, a multi-resolution feature extraction algorithm is proposed. Given the extracted features, the proposed auto-focusing system can provide the ideal focusing position using phase correlation matching. The proposed auto-focusing (AF) algorithm consists of four steps: (i) acquisition of left and right images using AF points in the region-of-interest; (ii) feature extraction in the left image under low illumination and out-of-focus blur; (iii) the generation of two feature images using the phase difference between the left and right images; and (iv) estimation of the phase shifting vector using phase correlation matching. Since the proposed system accurately estimates the phase difference in the out-of-focus blurred image under low illumination, it can provide faster, more robust auto focusing than existing systems.

Sensor-Based Auto-Focusing System Using Multi-Scale Feature Extraction and Phase Correlation Matching

PubMed Central

Jang, Jinbeum; Yoo, Yoonjong; Kim, Jongheon; Paik, Joonki

2015-01-01

This paper presents a novel auto-focusing system based on a CMOS sensor containing pixels with different phases. Robust extraction of features in a severely defocused image is the fundamental problem of a phase-difference auto-focusing system. In order to solve this problem, a multi-resolution feature extraction algorithm is proposed. Given the extracted features, the proposed auto-focusing system can provide the ideal focusing position using phase correlation matching. The proposed auto-focusing (AF) algorithm consists of four steps: (i) acquisition of left and right images using AF points in the region-of-interest; (ii) feature extraction in the left image under low illumination and out-of-focus blur; (iii) the generation of two feature images using the phase difference between the left and right images; and (iv) estimation of the phase shifting vector using phase correlation matching. Since the proposed system accurately estimates the phase difference in the out-of-focus blurred image under low illumination, it can provide faster, more robust auto focusing than existing systems. PMID:25763645

Assessing North American Forest Disturbance from the Landsat Archive

NASA Technical Reports Server (NTRS)

Masek, Jeffrey G.; Wolfe, Robert; Hall, Forrest; Cohen, Warren; Kennedy, Robert; Powell, Scott; Goward, Samuel; Huang, Chengquan; Healey, Sean; Moisen, Gretchen

2007-01-01

Forest disturbances are thought to play a major role in controlling land-atmosphere fluxes of carbon. Under the auspices of the North American Carbon Program, the LEDAPS (Landsat Ecosystem Disturbance Adaptive Processing System) and NACP-FIA projects have been analyzing the Landsat satellite record to assess rates of forest disturbance across North America. In the LEDAPS project, wall-to-wall Landsat imagery for the period 1975-2000 has been converted to surface reflectance and analyzed for decadal losses (disturbance) or gains (regrowth) in biomass using a spectral "disturbance index". The NACP-FIA project relies on a geographic sample of dense Landsat image time series, allowing both disturbance rates and recovery trends to be characterized. Preliminary results for the 1990's indicate high rates of harvest within the southeastern US, Eastern Canada, and the Pacific Northwest, with spatially averaged (approx.50x50 km) turnover periods as low as 25-40 years. Lower rates of disturbance are found in the Rockies and Northeastern US.

Flow Injection Analysis with Electrochemical Detection for Rapid Identification of Platinum-Based Cytostatics and Platinum Chlorides in Water

PubMed Central

Kominkova, Marketa; Heger, Zbynek; Zitka, Ondrej; Kynicky, Jindrich; Pohanka, Miroslav; Beklova, Miroslava; Adam, Vojtech; Kizek, Rene

2014-01-01

Platinum-based cytostatics, such as cisplatin, carboplatin or oxaliplatin are widely used agents in the treatment of various types of tumors. Large amounts of these drugs are excreted through the urine of patients into wastewaters in unmetabolised forms. This phenomenon leads to increased amounts of platinum ions in the water environment. The impacts of these pollutants on the water ecosystem are not sufficiently investigated as well as their content in water sources. In order to facilitate the detection of various types of platinum, we have developed a new, rapid, screening flow injection analysis method with electrochemical detection (FIA-ED). Our method, based on monitoring of the changes in electrochemical behavior of analytes, maintained by various pH buffers (Britton-Robinson and phosphate buffer) and potential changes (1,000, 1,100 and 1,200 mV) offers rapid and cheap selective determination of platinum-based cytostatics and platinum chlorides, which can also be present as contaminants in water environments. PMID:24499878

Aqueous two-phase assisted by ultrasound for the extraction of anthocyanins from Lycium ruthenicum Murr.

PubMed

Qin, Benlin; Liu, Xuecong; Cui, Haiming; Ma, Yue; Wang, Zimin; Han, Jing

2017-10-21

In this study, an efficient ultrasound-assisted aqueous two-phase extraction method was used for the extraction of anthocyanins from Lycium ruthenicum Murr. An ethanol/ammonium sulfate system was chosen for the aqueous two-phase system due to its fine partitioning and recycling behaviors. Single-factor experiments were conducted to determine the optimized composition of the system, and the response surface methodology was used for the further optimization of the ultrasound-assisted aqueous two-phase extraction. The optimal conditions were as follows: a salt concentration of 20%, an ethanol concentration of 25%, an extraction time of 33.7 min, an extraction temperature of 25°C, a liquid/solid ratio of 50:1 w/w, pH value of 3.98, and an ultrasound power of 600 W. Under the above conditions, the yields of anthocyanins reached 4.71 mg/g dry sample. For the further purification, D-101 resin was used, and the purity of anthocyanins reached 25.3%. In conclusion, ultrasound-assisted aqueous two-phase extraction was an efficient, ecofriendly, and economical method, and it may be a promising technique for extracting bioactive components from plants.

Antitumor activity of ethanol extract from Hippophae rhamnoides L. leaves towards human acute myeloid leukemia cells in vitro.

PubMed

Zhamanbaeva, G T; Murzakhmetova, M K; Tuleukhanov, S T; Danilenko, M P

2014-12-01

We studied the effects of ethanol extract from Hippophae rhamnoides L. leaves on the growth and differentiation of human acute myeloid leukemia cells (KG-1a, HL60, and U937). The extract of Hippophae rhamnoides L. leaves inhibited cell growth depending on the cell strain and extract dose. In a high concentration (100 μg/ml), the extract also exhibited a cytotoxic effect on HL60 cells. Hippophae rhamnoides L. leaves extract did not affect cell differentiation and did not modify the differentiating effect of calcitriol, active vitamin D metabolite. Inhibition of cell proliferation was paralleled by paradoxical accumulation of phase S cells (synthetic phase) with a reciprocal decrease in the count of G1 cells (presynthetic phase). The extract in a concentration of 100 μg/ml induced the appearance of cells with a subdiploid DNA content (sub-G1 phase cells), which indicated induction of apoptosis. The antiproliferative effect of Hippophae rhamnoides L. extract on acute myeloid leukemia cells was at least partially determined by activation of the S phase checkpoint, which probably led to deceleration of the cell cycle and apoptosis induction.

Preconcentration of aqueous dyes through phase-transfer liquid-phase microextraction with a room-temperature ionic liquid.

PubMed

Chen, Hsiu-Liang; Chang, Shuo-Kai; Lee, Chia-Ying; Chuang, Li-Lin; Wei, Guor-Tzo

2012-09-12

In this study, we employed the room-temperature ionic liquid [bmim][PF(6)] as both ion-pair agent and an extractant in the phase-transfer liquid-phase microextraction (PTLPME) of aqueous dyes. In the PTLPME method, a dye solution was added to the extraction solution, comprising a small amount of [bmim][PF(6)] in a relatively large amount of CH(2)Cl(2), which serves as the disperser solvent to an extraction solution. Following extraction, CH(2)Cl(2) was evaporated from the extractant, resulting in the extracted dyes being concentrated in a small volume of the ionic liquid phase to increase the enrichment factor. The enrichment factors of for the dye Methylene Blue, Neutral Red, and Methyl Red were approximately 500, 550 and 400, respectively; their detection limits were 0.014, 0.43, and 0.02 μg L(-1), respectively, with relative standard deviations of 4.72%, 4.20%, and 6.10%, respectively. Copyright © 2012 Elsevier B.V. All rights reserved.

Characterization of rhamnolipids by liquid chromatography/mass spectrometry after solid-phase extraction.

PubMed

Behrens, Beate; Engelen, Jeannine; Tiso, Till; Blank, Lars Mathias; Hayen, Heiko

2016-04-01

Rhamnolipids are surface-active agents with a broad application potential that are produced in complex mixtures by bacteria of the genus Pseudomonas. Analysis from fermentation broth is often characterized by laborious sample preparation and requires hyphenated analytical techniques like liquid chromatography coupled to mass spectrometry (LC-MS) to obtain detailed information about sample composition. In this study, an analytical procedure based on chromatographic method development and characterization of rhamnolipid sample material by LC-MS as well as a comparison of two sample preparation methods, i.e., liquid-liquid extraction and solid-phase extraction, is presented. Efficient separation was achieved under reversed-phase conditions using a mixed propylphenyl and octadecylsilyl-modified silica gel stationary phase. LC-MS/MS analysis of a supernatant from Pseudomonas putida strain KT2440 pVLT33_rhlABC grown on glucose as sole carbon source and purified by solid-phase extraction revealed a total of 20 congeners of di-rhamnolipids, mono-rhamnolipids, and their biosynthetic precursors 3-(3-hydroxyalkanoyloxy)alkanoic acids (HAAs) with different carbon chain lengths from C8 to C14, including three rhamnolipids with uncommon C9 and C11 fatty acid residues. LC-MS and the orcinol assay were used to evaluate the developed solid-phase extraction method in comparison with the established liquid-liquid extraction. Solid-phase extraction exhibited higher yields and reproducibility as well as lower experimental effort.

Separation of phenolic acids from sugarcane rind by online solid-phase extraction with high-speed counter-current chromatography.

PubMed

Geng, Ping; Fang, Yingtong; Xie, Ronglong; Hu, Weilun; Xi, Xingjun; Chu, Qiao; Dong, Genlai; Shaheen, Nusrat; Wei, Yun

2017-02-01

Sugarcane rind contains some functional phenolic acids. The separation of these compounds from sugarcane rind is able to realize the integrated utilization of the crop and reduce environment pollution. In this paper, a novel protocol based on interfacing online solid-phase extraction with high-speed counter-current chromatography (HSCCC) was established, aiming at improving and simplifying the process of phenolic acids separation from sugarcane rind. The conditions of online solid-phase extraction with HSCCC involving solvent system, flow rate of mobile phase as well as saturated extent of absorption of solid-phase extraction were optimized to improve extraction efficiency and reduce separation time. The separation of phenolic acids was performed with a two-phase solvent system composed of butanol/acetic acid/water at a volume ratio of 4:1:5, and the developed online solid-phase extraction with HSCCC method was validated and successfully applied for sugarcane rind, and three phenolic acids including 6.73 mg of gallic acid, 10.85 mg of p-coumaric acid, and 2.78 mg of ferulic acid with purities of 60.2, 95.4, and 84%, respectively, were obtained from 150 mg sugarcane rind crude extracts. In addition, the three different elution methods of phenolic acids purification including HSCCC, elution-extrusion counter-current chromatography and back-extrusion counter-current chromatography were compared. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Experimental and computational studies on molecularly imprinted solid-phase extraction for gonyautoxins 2,3 from dinoflagellate Alexandrium minutum.

PubMed

Lian, Ziru; Li, Hai-Bei; Wang, Jiangtao

2016-08-01

An innovative and effective extraction procedure based on molecularly imprinted solid-phase extraction (MISPE) was developed for the isolation of gonyautoxins 2,3 (GTX2,3) from Alexandrium minutum sample. Molecularly imprinted polymer microspheres were prepared by suspension polymerization and and were employed as sorbents for the solid-phase extraction of GTX2,3. An off-line MISPE protocol was optimized. Subsequently, the extract samples from A. minutum were analyzed. The results showed that the interference matrices in the extract were obviously cleaned up by MISPE procedures. This outcome enabled the direct extraction of GTX2,3 in A. minutum samples with extraction efficiency as high as 83 %, rather significantly, without any need for a cleanup step prior to the extraction. Furthermore, computational approach also provided direct evidences of the high selective isolation of GTX2,3 from the microalgal extracts.

Long-lived interaction between hydrothermal and magmatic fluids in the Soultz-sous-Forêts granitic system (Rhine Graben, France)

NASA Astrophysics Data System (ADS)

Gardien, Véronique; Rabinowicz, Michel; Vigneresse, Jean-Louis; Dubois, Michel; Boulvais, Philippe; Martini, Rossana

2016-03-01

The 5 km deep drilling at Soultz-sous-Forêts samples a granitic intrusion under its sedimentary cover. Core samples at different depths allow study of the evolving conditions of fluid-rock interaction, from the syn-tectonic emplacement of Hercynian granites at depth until post-cooling history and alteration close to the surface. Hydrogen, carbon and oxygen isotope compositions of CO2 and H2O have been measured in fluid inclusions trapped in magmatic quartz within samples collected along the drill core. Early Fluid Inclusions Assemblage (FIA) contains aqueous carbonic fluids whereas the latest FIA are H2O-rich. In the early FIA, the amount of CO2 and the δ13C value both decrease with depth, revealing two distinct sources of carbon, one likely derived from sedimentary carbonates (δ13C = - 2‰ V-PDB) and another from the continental crust (δ13C = - 9‰ V-PDB). The carbon isotope composition of bulk granites indicates a third carbon source of organic derivation (δ13C = - 20‰ V-PDB). Using a δD - δ18O plot, we argue that the water trapped in quartz grains is mainly of meteoric origin somewhat mixed with magmatic water. The emplacement of the Soultz-sous-Forêts granite pluton occurred in a North 030-040° wrench zone. After consolidation of the granite mush at 600 °C, sinistral shear (γ 1) concentrated the final leucocratic melt in vertical planes oriented along (σ1, σ2). Crystallization of this residual leucocratic melt occurred while shearing was still active. At a temperature of 550 °C, crystallization ended with the formation of vertical quartz veins spaced about 5 mm, and exhibiting a width of several cm. The quartz veins form a connected network of a few kilometers in height, generated during hydrothermal contraction of the intrusion. Quartz crystallization led to the exsolution of 30% by volume of the aqueous fluid. As quartz grains were the latest solid phase still plastic, shearing localized inside the connected quartz network. Aqueous fluid was thus concentrated in these vertical channels. Eventually, when the channels intersected the top of the crack network, water boiling caused the formation of primary inclusions. At the same temperature, the saline magmatic waters, which were denser than the meteoric waters, initiated thermohaline convection with the buoyant "cold" hydrothermal water layer. This mechanism can explain the mixing of surface and deep-seated fluids in the same primary inclusions trapped during the crystallization of magmatic minerals. This study, which separately considers fluid-rock interactions at the level of successive mineral facies, brings new insights into how fluids may be different, their origin and composition, and depending on tectono-thermal conditions, bears implications for eventual ore forming processes.

The Chemistry of Separations Ligand Degradation by Organic Radical Cations

DOE PAGES

Mezyk, Stephen P.; Horne, Gregory P.; Mincher, Bruce J.; ...

2016-12-01

Solvent based extractions of used nuclear fuel use designer ligands in an organic phase extracting ligand complexed metal ions from an acidic aqueous phase. These extractions will be performed in highly radioactive environments, and the radiation chemistry of all these complexants and their diluents will play a major role in determining extraction efficiency, separation factors, and solvent-recycle longevity. Although there has been considerable effort in investigating ligand damage occurring in acidic water radiolysis conditions, only minimal fundamental kinetic and mechanistic data has been reported for the degradation of extraction ligands in the organic phase. Extraction solvent phases typically use normalmore » alkanes such as dodecane, TPH, and kerosene as diluents. The radiolysis of such diluents produce a mixture of radical cations (R •+), carbon-centered radicals (R •), solvated electrons, and molecular products such as hydrogen. Typically, the radical species will preferentially react with the dissolved oxygen present to produce relatively inert peroxyl radicals. This isolates the alkane radical cation species, R •+ as the major radiolytically-induced organic species that can react with, and degrade, extraction agents in this phase. Here we report on our recent studies of organic radical cation reactions with various ligands. Elucidating these parameters, and combining them with the known acidic aqueous phase chemistry, will allow a full, fundamental, understanding of the impact of radiation on solvent extraction based separation processes to be achieved.« less

Three phases hollow fiber LPME combined with HPLC-UV for extraction, preconcentration and determination of valerenic acid in Valeriana officinalis.

PubMed

Mirzaei, Mohamad; Dinpanah, Hossein

2011-07-01

In the present work, the applicability of hollow fiber-based liquid phase microextraction (HF-LPME) was evaluated for the extraction and preconcentration of valerenic acid prior to its determination by reversed-phase HPLC/UV. The target drug was extracted from 5.0 mL of aqueous solution with pH 3.5 into an organic extracting solvent (dihexyl ether) impregnated in the pores of a hollow fiber and finally back extracted into 10 μ L of aqueous solution with pH 9.5 located inside the lumen of the hollow fiber. In order to obtain high extraction efficiency, the parameters affecting the HF-LPME, including pH of the donor and acceptor phases, type of organic phase, ionic strength, the volume ratio of donor to acceptor phase, stirring rate and extraction time were studied and optimized. Under the optimized conditions, enrichment factor up to 446 was achieved and the relative standard deviation (RSD) of the method was 4.36% (n = 9). The linear range was 7.5-850 μg L⁻¹ with correlation coefficient (r²=0.999), detection limits was 2.5 μg L⁻¹ and the LOQ was 7.5 μg L⁻¹. The proposed method was evaluated by extraction and determination of valerenic acid in some Iranian wild species of Valerianaceae. Copyright © 2011 Elsevier B.V. All rights reserved.

The Chemistry of Separations Ligand Degradation by Organic Radical Cations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mezyk, Stephen P.; Horne, Gregory P.; Mincher, Bruce J.

Solvent based extractions of used nuclear fuel use designer ligands in an organic phase extracting ligand complexed metal ions from an acidic aqueous phase. These extractions will be performed in highly radioactive environments, and the radiation chemistry of all these complexants and their diluents will play a major role in determining extraction efficiency, separation factors, and solvent-recycle longevity. Although there has been considerable effort in investigating ligand damage occurring in acidic water radiolysis conditions, only minimal fundamental kinetic and mechanistic data has been reported for the degradation of extraction ligands in the organic phase. Extraction solvent phases typically use normalmore » alkanes such as dodecane, TPH, and kerosene as diluents. The radiolysis of such diluents produce a mixture of radical cations (R •+), carbon-centered radicals (R •), solvated electrons, and molecular products such as hydrogen. Typically, the radical species will preferentially react with the dissolved oxygen present to produce relatively inert peroxyl radicals. This isolates the alkane radical cation species, R •+ as the major radiolytically-induced organic species that can react with, and degrade, extraction agents in this phase. Here we report on our recent studies of organic radical cation reactions with various ligands. Elucidating these parameters, and combining them with the known acidic aqueous phase chemistry, will allow a full, fundamental, understanding of the impact of radiation on solvent extraction based separation processes to be achieved.« less

Method for separating water soluble organics from a process stream by aqueous biphasic extraction

DOEpatents

Chaiko, David J.; Mego, William A.

1999-01-01

A method for separating water-miscible organic species from a process stream by aqueous biphasic extraction is provided. An aqueous biphase system is generated by contacting a process stream comprised of water, salt, and organic species with an aqueous polymer solution. The organic species transfer from the salt-rich phase to the polymer-rich phase, and the phases are separated. Next, the polymer is recovered from the loaded polymer phase by selectively extracting the polymer into an organic phase at an elevated temperature, while the organic species remain in a substantially salt-free aqueous solution. Alternatively, the polymer is recovered from the loaded polymer by a temperature induced phase separation (cloud point extraction), whereby the polymer and the organic species separate into two distinct solutions. The method for separating water-miscible organic species is applicable to the treatment of industrial wastewater streams, including the extraction and recovery of complexed metal ions from salt solutions, organic contaminants from mineral processing streams, and colorants from spent dye baths.

Isolation and recovery of selected polybrominated diphenyl ethers from human serum and sheep serum: coupling reversed-phase solid-phase disk extraction and liquid-liquid extraction techniques with a capillary gas chromatographic electron capture negative ion mass spectrometric determinative technique.

PubMed

Loconto, Paul R; Isenga, David; O'Keefe, Michael; Knottnerus, Mark

2008-01-01

Polybrominated diphenyl ethers (PBDEs) are isolated and recovered with acceptable percent recoveries from human serum via liquid-liquid extraction and column chromatographic cleanup and fractionation with quantitation using capillary gas chromatography-mass spectrometry with electron capture negative ion and selected ion monitoring. PBDEs are found in unspiked serum. An alternative sample preparation approach is developed using sheep serum that utilizes a formic acid pre-treatment followed by reversed-phase solid-phase disk extraction and normal-phase solid-phase cleanup using acidified silica gel that yields>50% recoveries. When these percent recoveries are combined with a minimized phase ratio for human serum and very low instrument detection limits, method detection limits below 500 parts-per-trillion are realized.

Mapping young forest in Wisconsin

Treesearch

Mark Nelson; Kirk Stueve; Charles Perry; Dale Gormanson; Chengquan Huang; Sean. Healey

2012-01-01

Population declines of early successional forest-associated wildlife species have been linked to declines in habitat abundance. Forest Inventory and Analysis (FIA) data can be used to estimate composition and change in 'young' forest, but such information typically lacks spatial specificity for determining landscape patterns that also affect habitat...

Physically incorporated extraction phase of solid-phase microextraction by sol-gel technology.

PubMed

Liu, Wenmin; Hu, Yuan; Zhao, Jinghong; Xu, Yuan; Guan, Yafeng

2006-01-13

A sol-gel method for the preparation of solid-phase microextraction (SPME) fiber was described and evaluated. The extraction phase of poly(dimethysiloxane) (PDMS) containing 3% vinyl group was physically incorporated into the sol-gel network without chemical bonding. The extraction phase itself is then partly crosslinked at 320 degrees C, forming an independent polymer network and can withstand desorption temperature of 290 degrees C. The headspace extraction of BTX by the fiber SPME was evaluated and the detection limit of o-xylene was down to 0.26 ng/l. Extraction and determination of organophosphorus pesticides (OPPs) in water, orange juice and red wine by the SPME-GC thermionic specified detector (TSD) was validated. Limits of detection of the method for OPPs were below 10 ng/l except methidathion. Relative standard deviations (RSDs) were in the range of 1-20% for pesticides being tested.

Changes Caused by Fruit Extracts in the Lipid Phase of Biological and Model Membranes

PubMed Central

Pruchnik, Hanna; Oszmiański, Jan; Sarapuk, Janusz; Kleszczyńska, Halina

2010-01-01

The aim of the study was to determine changes incurred by polyphenolic compounds from selected fruits in the lipid phase of the erythrocyte membrane, in liposomes formed of erythrocyte lipids and phosphatidylcholine liposomes. In particular, the effect of extracts from apple, chokeberry, and strawberry on the red blood cell morphology, on packing order in the lipid hydrophilic phase, on fluidity of the hydrophobic phase, as well as on the temperature of phase transition in DPPC liposomes was studied. In the erythrocyte population, the proportions of echinocytes increased due to incorporation of polyphenolic compounds. Fluorimetry with a laurdan probe indicated increased packing density in the hydrophilic phase of the membrane in presence of polyphenolic extracts, the highest effect being observed for the apple extract. Using the fluorescence probes DPH and TMA-DPH, no effect was noted inside the hydrophobic phase of the membrane, as the lipid bilayer fluidity was not modified. The polyphenolic extracts slightly lowered the phase transition temperature of phosphatidylcholine liposomes. The studies have shown that the phenolic compounds contained in the extracts incorporate into the outer region of the erythrocyte membrane, affecting its shape and lipid packing order, which is reflected in the increasing number of echinocytes. The compounds also penetrate the outer part of the external lipid layer of liposomes formed of natural and DPPC lipids, changing its packing order. PMID:21423329

Dissolved organic carbon (DOC) in soil extracts investigated by FT-ICR-MS

NASA Astrophysics Data System (ADS)

Hofmann, D.; Steffen, D.; Jablonowski, N. D.; Burauel, P.

2012-04-01

Soil drying and rewetting usually increases the release of xenobiotics like pesticides present in agricultural soils. Besides the effect on the release of two aged 14C-labeled pesticide residues we focus on the characterisation of simultaneously remobilized dissolved organic carbon (DOC) to gain new insights into structure and stability aspects of soil organic carbon fractions. The test soil (gleyic cambisol; Corg 1.2%, pH 7.2) was obtained from the upper soil layer of two individual outdoor lysimeter studies containing either environmentally long-term aged 14C residues of the herbicide ethidimuron (0-10 cm depth; time of aging: 9 years) or methabenzthiazuron (0-30 cm depth; time of aging: 17 years). Soil samples (10 g dry soil equivalents) were (A=dry/wet) previously dried (45°C) or (B=wet/wet) directly mixed with pure water (1+2, w:w), shaken (150 rpm, 1 h), and centrifuged (2000 g). This extraction procedure was repeated several individual times, for both setups. The first three individual extractions, respectively were used for further investigations. Salt was removed from samples prior analysis because of a possible quench effect in the electrospray (ESI) source by solid phase extraction (SPE) with Chromabond C18 Hydra-cartridges (Macherey-Nagel) and methanol as backextraction solvent. The so preconcentrated and desalted samples were introduced by flow injection analysis (FIA) in a fourier transform ion cyclotron resonance mass spectrometer (FT-ICR-MS), equipped with an ESI source and a 7 T supra-conducting magnet (LTQ-FT Ultra, ThermoFisher Scientific). This technique is the key technique for complex natural systems attributed by their outstanding mass resolution (used 400.000 at m/z 400 Da) and mass accuracy (≤ 1ppm) by simultaneously providing molecular level details of thousands of compounds and was successful applied for the investigations of natural organic matter (NOM) different sources like marine and surface water, soil, sediment, bog and crude oil. The characteristics of measured DOM mass spectra were demonstrated. Furthermore, an algorithm to compute all chemically relevant C,H,O-, C,H,(O,S),N- as well as C,H,(O),S molecular compositions, designed and exercised by ourself using Scilab routines, was used for entire structure elucidation. Various methods for data evaluation of such an amount of peaks are applied to describe the characteristics of DOC. The van Krevelen diagram is widely used to classify the DOC compounds regarding polarity and aromaticity, whereas the Kendrick diagram allow to identify ions with elemental formulas that differ only in CH2, and molecular formulas with similar Kendrick Mass Defect (KMD) can be sorted by nominal mass series. Both kind of diagrams were developed and results are discussed together with the findings of ETD, MBT, and metabolites after soil drying and rewetting. Overall, the results suggest that intermittent soil drying and rewetting alters the disaggregation of soil aggregates, resulting in a release of entrapped organic carbon as well as pesticide molecules.