Evaluation of losses in transmission of machinery for development of mineral deposits in conditions of variable load

NASA Astrophysics Data System (ADS)

Zvonarev, I. E.; Ivanov, S. L.

2017-10-01

The influence of individual elements of machines transmissions on the operation of the whole system is shown. The approach of determining the resource of operation of systems elements based on the energy theory is presented. The formulas for determining the total energy resource of the reducer are given. The influence of individual elements of the system on each other is indicated. The principle of researching the system by the method of equivalent circuits is substantiated. The weakest places of transmission (gears, bearing supports and shafts) are determined. A mathematical model of a mechanical transmission was developed. To test the adequacy of the mathematical model, the stand for obtaining experimental data was designed. The description of the stand and the principle of its operation are given. Experimental data are presented. A comparative analysis of modeling and experimental data is carried out and the adequacy of the developed mathematical model is proved. The principle of determining the resource of the system as a whole for the element with the minimal resource of work is suggested.

Experimental Determination of Aerodynamic Damping in a Three-Stage Transonic Axial-Flow Compressor. Degree awarded by Case Western Reserve Univ.

NASA Technical Reports Server (NTRS)

Newman, Frederick A.

1988-01-01

Rotor blade aerodynamic damping is experimentally determined in a three-stage transonic axial flow compressor having design aerodynamic performance goals of 4.5:1 pressure ratio and 65.5 lbm/sec weight flow. The combined damping associated with each mode is determined by a least squares fit of a single degree of freedom system transfer function to the nonsynchronous portion of the rotor blade strain gauge output power spectra. The combined damping consists of aerodynamic and structural and mechanical damping. The aerodynamic damping varies linearly with the inlet total pressure for a given equivalent speed, equivalent mass flow, and pressure ratio while structural and mechanical damping are assumed to be constant. The combined damping is determined at three inlet total pressure levels to obtain the aerodynamic damping. The third stage rotor blade aerodynamic damping is presented and discussed for 70, 80, 90, and 100 percent design equivalent speed. The compressor overall performance and experimental Campbell diagrams for the third stage rotor blade row are also presented.

Determination of chlorine in atmosphere by kinetic spectrophotometry.

PubMed

Meng, Jian-Xin; Wang, Xiao-Bo; Ruan, Ge-Lan; Li, Guo-Qiang; Deng, Zhao-Xia

2005-03-01

A kinetic method for determination of chlorine in air was described in the present work. The method based on fading of methyl orange (MO) containing solution in air absorption process. A determination limit of 2.64 microg L(-1) was found. With the present method, chlorine concentration could be determined in several minutes with convenient manipulation. As concentration variation of methyl orange in the absorption solution did not affect the experimental results, fabrication and preservation of the stock absorption is also convenient. The present method is promising in monitoring chlorine concentration in atmosphere.

Determination of chlorine in atmosphere by kinetic spectrophotometry

NASA Astrophysics Data System (ADS)

Meng, Jian-Xin; Wang, Xiao-Bo; Ruan, Ge-Lan; Li, Guo-Qiang; Deng, Zhao-Xia

2005-03-01

A kinetic method for determination of chlorine in air was described in the present work. The method based on fading of methyl orange (MO) containing solution in air absorption process. A determination limit of 2.64 μg L -1 was found. With the present method, chlorine concentration could be determined in several minutes with convenient manipulation. As concentration variation of methyl orange in the absorption solution did not affect the experimental results, fabrication and preservation of the stock absorption is also convenient. The present method is promising in monitoring chlorine concentration in atmosphere.

Comparison of three nondestructive and contactless techniques for investigations of recombination parameters on an example of silicon samples

NASA Astrophysics Data System (ADS)

Chrobak, Ł.; Maliński, M.

2018-06-01

This paper presents a comparison of three nondestructive and contactless techniques used for determination of recombination parameters of silicon samples. They are: photoacoustic method, modulated free carriers absorption method and the photothermal radiometry method. In the paper the experimental set-ups used for measurements of the recombination parameters in these methods as also theoretical models used for interpretation of obtained experimental data have been presented and described. The experimental results and their respective fits obtained with these nondestructive techniques are shown and discussed. The values of the recombination parameters obtained with these methods are also presented and compared. Main advantages and disadvantages of presented methods have been discussed.

Detonation Product EOS Studies: Using ISLS to Refine Cheetah

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zaug, J M; Howard, W M; Fried, L E

2001-08-08

Knowledge of an effective interatomic potential function underlies any effort to predict or rationalize the properties of solids and liquids. The experiments we undertake are directed towards determination of equilibrium and dynamic properties of simple fluids at densities sufficiently high that traditional computational methods and semi-empirical forms successful at ambient conditions may require reconsideration. In this paper we present high-pressure and temperature experimental sound speed data on a simple fluid, methanol. Impulsive Stimulated Light Scattering (ISLS) conducted on diamond-anvil cell (DAC) encapsulated samples offers an experimental approach to determine cross-pair potential interactions through equation of state determinations. In addition themore » kinetics of structural relaxation in fluids can be studied. We compare our experimental results with our thermochemical computational model Cheetah. Computational models are systematically improved with each addition of experimental data.« less

Study of an instrument for sensing errors in a telescope wavefront

NASA Technical Reports Server (NTRS)

Golden, L. J.; Shack, R. V.; Slater, D. N.

1973-01-01

Partial results are presented of theoretical and experimental investigations of different focal plane sensor configurations for determining the error in a telescope wavefront. The coarse range sensor and fine range sensors are used in the experimentation. The design of a wavefront error simulator is presented along with the Hartmann test, the shearing polarization interferometer, the Zernike test, and the Zernike polarization test.

A Dye-Tracer Technique for Experimentally Obtaining Impingement Characteristics of Arbitrary Bodies and a Method for Determining Droplet Size Distribution

NASA Technical Reports Server (NTRS)

VonGlahn, Uwe H.; Gelder, Thomas F.; Smyers, William H., Jr.

1955-01-01

A dye-tracer technique has been developed whereby the quantity of dyed water collected on a blotter-wrapped body exposed to an air stream containing a dyed-water spray cloud can be colorimetrically determined in order to obtain local collection efficiencies, total collection efficiency, and rearward extent of impingement on the body. In addition, a method has been developed whereby the impingement characteristics obtained experimentally for a body can be related to theoretical impingement data for the same body in order to determine the droplet size distribution of the impinging cloud. Several cylinders, a ribbon, and an aspirating device to measure cloud liquid-water content were used in the studies presented herein for the purpose of evaluating the dye-tracer technique. Although the experimental techniques used in the dye-tracer technique require careful control, the methods presented herein should be applicable for any wind tunnel provided the humidity of the air stream can be maintained near saturation.

Experimental method for determination of bending and torsional rigidities of advanced composite laminates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Maeda, Takenori

1995-11-01

This paper presents an experimental method for the determination of the bending and torsional rigidities of advanced fiber composite laminates with the aid of laser holographic interferometry. The proposed method consists of a four-point bending test and a resonance test. The bending rigidity ratio (D{sub 12}/D{sub 22}) can be determined from the fringe patterns of the four-point bending test. The bending rigidities (D{sub 11} and D{sub 22}) and the torsional rigidity (D{sub 66}) are calculated from the natural frequencies of cantilever plates of the resonance test. The test specimens are carbon/epoxy cross-ply laminates. The adequacy of the experimental method ismore » confirmed by comparing the measured rigidities with the theoretical values obtained from classical lamination theory (CLT) by using the measured tensile properties. The results show that the present method can be used to evaluate the rigidities of orthotropic laminates with reasonably good accuracy.« less

Optimal Experimental Design for Model Discrimination

PubMed Central

Myung, Jay I.; Pitt, Mark A.

2009-01-01

Models of a psychological process can be difficult to discriminate experimentally because it is not easy to determine the values of the critical design variables (e.g., presentation schedule, stimulus structure) that will be most informative in differentiating them. Recent developments in sampling-based search methods in statistics make it possible to determine these values, and thereby identify an optimal experimental design. After describing the method, it is demonstrated in two content areas in cognitive psychology in which models are highly competitive: retention (i.e., forgetting) and categorization. The optimal design is compared with the quality of designs used in the literature. The findings demonstrate that design optimization has the potential to increase the informativeness of the experimental method. PMID:19618983

Determining octanol-water partition coefficients for extremely hydrophobic chemicals by combining "slow stirring" and solid-phase microextraction.

PubMed

Jonker, Michiel T O

2016-06-01

Octanol-water partition coefficients (KOW ) are widely used in fate and effects modeling of chemicals. Still, high-quality experimental KOW data are scarce, in particular for very hydrophobic chemicals. This hampers reliable assessments of several fate and effect parameters and the development and validation of new models. One reason for the limited availability of experimental values may relate to the challenging nature of KOW measurements. In the present study, KOW values for 13 polycyclic aromatic hydrocarbons were determined with the gold standard "slow-stirring" method (log KOW 4.6-7.2). These values were then used as reference data for the development of an alternative method for measuring KOW . This approach combined slow stirring and equilibrium sampling of the extremely low aqueous concentrations with polydimethylsiloxane-coated solid-phase microextraction fibers, applying experimentally determined fiber-water partition coefficients. It resulted in KOW values matching the slow-stirring data very well. Therefore, the method was subsequently applied to a series of 17 moderately to extremely hydrophobic petrochemical compounds. The obtained KOW values spanned almost 6 orders of magnitude, with the highest value measuring 10(10.6) . The present study demonstrates that the hydrophobicity domain within which experimental KOW measurements are possible can be extended with the help of solid-phase microextraction and that experimentally determined KOW values can exceed the proposed upper limit of 10(9) . Environ Toxicol Chem 2016;35:1371-1377. © 2015 SETAC. © 2015 SETAC.

Experimental Study of Unshrouded Impeller Pump Stage Sensitivity to Tip Clearance

NASA Technical Reports Server (NTRS)

Williams, Robert W.; Zoladz, Thomas; Storey, Anne K.; Skelley, Stephen E.

2002-01-01

This viewgraph presentation provides information on an experiment. Its objective is to experimentally determine unshrouded impeller performance sensitivity to tip clearance. The experiment included: Determining impeller efficiency at scaled operating conditions in water at MSFC's Pump Test Equipment (PTE) Facility; Testing unshrouded impeller at three different tip clearances; Testing each tip clearance configuration at on- and off-design conditions, and collecting unsteady- and steady-state data in each configuration; Determining impeller efficiency directly using drive line torquemeter and pump inlet and exit total pressure measurements.

Current Experimental Basis for Modeling Ice Accretions on Swept Wings

NASA Technical Reports Server (NTRS)

Vargas, Mario

2005-01-01

This work presents a review of the experimental basis for modeling ice accretions on swept wings. Experimental work related to ice accretion physics on swept wings conducted between 1954 and 2004 is reviewed. Proposed models or explanations of scallop formations are singled out and discussed. Special emphasis is placed on reviewing the work done to determine the basic macroscopic mechanisms of scallop formation. The role of feather growth and its connection to scallop growth is discussed. Conceptual steps in modeling scallop formations are presented. Research elements needed for modeling are discussed.

FUNDAMENTAL AREAS OF PHENOMENOLOGY(INCLUDING APPLICATIONS): Experimental Investigation of Quality of Lensless Ghost Imaging with Pseudo-Thermal Light

NASA Astrophysics Data System (ADS)

Shen, Xia; Bai, Yan-Feng; Qin, Tao; Han, Shen-Sheng

2008-11-01

Factors influencing the quality of lensless ghost imaging are investigated. According to the experimental results, we find that the imaging quality is determined by the number of independent sub light sources on the imaging plane of the reference arm. A qualitative picture based on advanced wave optics is presented to explain the physics behind the experimental phenomena. The present results will be helpful to provide a basis for improving the quality of ghost imaging systems in future works.

Experimental investigation of the dynamics of a brake shoe

NASA Astrophysics Data System (ADS)

Ivanova, T. B.; Erdakova, N. N.; Karavaev, Yu. L.

2016-12-01

The experimental stand is described and the results of investigation of the motion of a brake shoe are presented. In the noncritical region, the friction coefficient is determined experimentally. It is shown that its value corresponds to the condition of uniqueness of the solution for construction of this brake shoe. The dynamics observed in the paradoxical-motion region is described.

Integrated Structural Biology for α-Helical Membrane Protein Structure Determination.

PubMed

Xia, Yan; Fischer, Axel W; Teixeira, Pedro; Weiner, Brian; Meiler, Jens

2018-04-03

While great progress has been made, only 10% of the nearly 1,000 integral, α-helical, multi-span membrane protein families are represented by at least one experimentally determined structure in the PDB. Previously, we developed the algorithm BCL::MP-Fold, which samples the large conformational space of membrane proteins de novo by assembling predicted secondary structure elements guided by knowledge-based potentials. Here, we present a case study of rhodopsin fold determination by integrating sparse and/or low-resolution restraints from multiple experimental techniques including electron microscopy, electron paramagnetic resonance spectroscopy, and nuclear magnetic resonance spectroscopy. Simultaneous incorporation of orthogonal experimental restraints not only significantly improved the sampling accuracy but also allowed identification of the correct fold, which is demonstrated by a protein size-normalized transmembrane root-mean-square deviation as low as 1.2 Å. The protocol developed in this case study can be used for the determination of unknown membrane protein folds when limited experimental restraints are available. Copyright © 2018 Elsevier Ltd. All rights reserved.

Research of interaction between technological and material parameters during densification of sunflower hulls

NASA Astrophysics Data System (ADS)

Križan, Peter; Matúš, Miloš; Beniak, Juraj; Šooš, Ľubomír

2018-01-01

During the biomass densification can be recognized various technological variables and also material parameters which significantly influences the final solid biofuels (pellets) quality. In this paper, we will present the research findings concerning relationships between technological and material variables during densification of sunflower hulls. Sunflower hulls as an unused source is a typical product of agricultural industry in Slovakia and belongs to the group of herbaceous biomass. The main goal of presented experimental research is to determine the impact of compression pressure, compression temperature and material particle size distribution on final biofuels quality. Experimental research described in this paper was realized by single-axis densification, which was represented by experimental pressing stand. The impact of mentioned investigated variables on the final briquettes density and briquettes dilatation was determined. Mutual interactions of these variables on final briquettes quality are showing the importance of mentioned variables during the densification process. Impact of raw material particle size distribution on final biofuels quality was also proven by experimental research on semi-production pelleting plant.

Removal of biofilms by impinging water droplets

NASA Astrophysics Data System (ADS)

Cense, A. W.; van Dongen, M. E. H.; Gottenbos, B.; Nuijs, A. M.; Shulepov, S. Y.

2006-12-01

The process of impinging water droplets on Streptococcus mutans biofilms was studied experimentally and numerically. Droplets were experimentally produced by natural breakup of a cylindrical liquid jet. Droplet diameter and velocity were varied between 20 and 200 μm and between 20 and 100 m/s, respectively. The resulting erosion process of the biofilm was determined experimentally with high-speed recording techniques and a quantitative relationship between the removal rate, droplet size, and velocity was determined. The shear stress and the pressure on the surface during droplet impact were determined by numerical simulations, and a qualitative agreement between the experiment and the simulation was obtained. Furthermore, it was shown that the stresses on the surface are strongly reduced when a water film is present.

Mechanistic modeling of modular co-rotating twin-screw extruders.

PubMed

Eitzlmayr, Andreas; Koscher, Gerold; Reynolds, Gavin; Huang, Zhenyu; Booth, Jonathan; Shering, Philip; Khinast, Johannes

2014-10-20

In this study, we present a one-dimensional (1D) model of the metering zone of a modular, co-rotating twin-screw extruder for pharmaceutical hot melt extrusion (HME). The model accounts for filling ratio, pressure, melt temperature in screw channels and gaps, driving power, torque and the residence time distribution (RTD). It requires two empirical parameters for each screw element to be determined experimentally or numerically using computational fluid dynamics (CFD). The required Nusselt correlation for the heat transfer to the barrel was determined from experimental data. We present results for a fluid with a constant viscosity in comparison to literature data obtained from CFD simulations. Moreover, we show how to incorporate the rheology of a typical, non-Newtonian polymer melt, and present results in comparison to measurements. For both cases, we achieved excellent agreement. Furthermore, we present results for the RTD, based on experimental data from the literature, and found good agreement with simulations, in which the entire HME process was approximated with the metering model, assuming a constant viscosity for the polymer melt. Copyright © 2014. Published by Elsevier B.V.

Investigation of composite materials property requirements for sonic fatigue research

NASA Technical Reports Server (NTRS)

Patrick, H. V. L.

1985-01-01

Experimental techniques for determining the extensional and bending stiffness characteristics for symmetric laminates are presented. Vibrational test techniques for determining the dynamic modulus and material damping are also discussed. Partial extensional stiffness results intially indicate that the laminate theory used for predicting stiffness is accurate. It is clearly shown that the laminate theory can only be as accurate as the physical characteristics describing the lamina, which may vary significantly. It is recommended that all of the stiffness characteristics in both extension and bending be experimentally determined to fully verify the laminate theory. Dynamic modulus should be experimentally evaluated to determine if static data adequately predicts dynamic behavior. Material damping should also be ascertained because laminate damping is an order of magnitude greater than found in common metals and can significantly effect the displacement response of composite panels.

Determination of thermal diffusivities of cylindrical bodies being cooled

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dincer, I.

1996-09-01

This paper deals with the development of an analytical model for determining the thermal diffusivities of the individual solid cylindrical bodies subjected to cooling is presented. Applications of this model were made using the experimental center temperature data obtained from the cylindrical products (e.g., cucumber and grape) during air cooling at the flow velocity of 2 m/s. As an experimental result, the thermal diffusivities of products were found to be 1.45{times}10{sup {minus}7} m{sup 2}/s for cucumber and 1.68{times}10{sup {minus}7} m{sup 2}/s for grape. It can be concluded that the present model is capable of determining the thermal diffusivities of cylindricalmore » bodies during cooling in a simple and effective form.« less

Detonation Product EOS Studies: Using ISLS to Refine Cheetah

NASA Astrophysics Data System (ADS)

Zaug, J. M.; Howard, W. M.; Fried, L. E.; Hansen, D. W.

2002-07-01

Knowledge of an effective interatomic potential function underlies any effort to predict or rationalize the properties of solids and liquids. The experiments we undertake are directed towards determination of equilibrium and dynamic properties of simple fluids at densities sufficiently high that traditional computational methods and semi-empirical forms successful at ambient conditions may require reconsideration. In this paper we present high-pressure and temperature experimental sound speed data on a simple fluid, methanol. Impulsive Stimulated Light Scattering (ISLS) conducted on diamond-anvil cell (DAC) encapsulated samples offers an experimental approach to determine cross-pair potential interactions through equation of state determinations. In addition the kinetics of structural relaxation in fluids can be studied. We compare our experimental results with our thermochemical computational model Cheetah. Experimentally grounded computational models provide a good basis to confidently understand the chemical nature of reactions at extreme conditions.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yoder Jr, Graydon L; Heatherly, Dennis Wayne; Williams, David F

A small molten fluoride salt experiment has been constructed and tested to develop experimental techniques for application in liquid fluoride salt systems. There were five major objectives in developing this test apparatus: Allow visual observation of the salt during testing (how can lighting be introduced, how can pictures be taken, what can be seen) Determine if IR photography can be used to examine components submerged in the salt Determine if the experimental configuration provides salt velocity sufficient for collection of corrosion data for future experimentation Determine if a laser Doppler velocimeter can be used to quantify salt velocities. Acquire naturalmore » circulation heat transfer data in fluoride salt at temperatures up to 700oC All of these objectives were successfully achieved during testing with the exception of the fourth: acquiring velocity data using the laser Doppler velocimeter. This paper describes the experiment and experimental techniques used, and presents data taken during natural circulation testing.« less

Determination of the top quark mass circa 2013: methods, subtleties, perspectives

NASA Astrophysics Data System (ADS)

Juste, Aurelio; Mantry, Sonny; Mitov, Alexander; Penin, Alexander; Skands, Peter; Varnes, Erich; Vos, Marcel; Wimpenny, Stephen

2014-10-01

We present an up-to-date overview of the problem of top quark mass determination. We assess the need for precision in the top mass extraction in the LHC era together with the main theoretical and experimental issues arising in precision top mass determination. We collect and document existing results on top mass determination at hadron colliders and map the prospects for future precision top mass determination at e+e- colliders. We present a collection of estimates for the ultimate precision of various methods for top quark mass extraction at the LHC.

Experimental limits on weak annihilation contributions to decays.

PubMed

Rosner, J L; Adam, N E; Alexander, J P; Berkelman, K; Cassel, D G; Duboscq, J E; Ecklund, K M; Ehrlich, R; Fields, L; Gibbons, L; Gray, R; Gray, S W; Hartill, D L; Heltsley, B K; Hertz, D; Jones, C D; Kandaswamy, J; Kreinick, D L; Kuznetsov, V E; Mahlke-Krüger, H; Meyer, T O; Onyisi, P U E; Patterson, J R; Peterson, D; Phillips, E A; Pivarski, J; Riley, D; Ryd, A; Sadoff, A J; Schwarthoff, H; Shi, X; Stroiney, S; Sun, W M; Wilksen, T; Weinberger, M; Athar, S B; Avery, P; Breva-Newell, L; Patel, R; Potlia, V; Stoeck, H; Yelton, J; Rubin, P; Cawlfield, C; Eisenstein, B I; Karliner, I; Kim, D; Lowrey, N; Naik, P; Sedlack, C; Selen, M; Thaler, J J; White, E J; Wiss, J; Shepherd, M R; Asner, D M; Edwards, K W; Besson, D; Pedlar, T K; Cronin-Hennessy, D; Gao, K Y; Gong, D T; Hietala, J; Kubota, Y; Klein, T; Lang, B W; Poling, R; Scott, A W; Smith, A; Dobbs, S; Metreveli, Z; Seth, K K; Tomaradze, A; Zweber, P; Ernst, J; Arms, K; Severini, H; Dytman, S A; Love, W; Mehrabyan, S; Mueller, J A; Savinov, V; Li, Z; Lopez, A; Mendez, H; Ramirez, J; Huang, G S; Miller, D H; Pavlunin, V; Sanghi, B; Shipsey, I P J; Adams, G S; Anderson, M; Cummings, J P; Danko, I; Napolitano, J; He, Q; Muramatsu, H; Park, C S; Thorndike, E H; Coan, T E; Gao, Y S; Liu, F; Stroynowski, R; Artuso, M; Boulahouache, C; Blusk, S; Butt, J; Li, J; Menaa, N; Mountain, R; Nisar, S; Randrianarivony, K; Redjimi, R; Sia, R; Skwarnicki, T; Stone, S; Wang, J C; Zhang, K; Csorna, S E; Bonvicini, G; Cinabro, D; Dubrovin, M; Lincoln, A; Weinstein, A J; Briere, R A; Chen, G P; Chen, J; Ferguson, T; Tatishvili, G; Vogel, H; Watkins, M E

2006-03-31

We present the first experimental limits on high-q2 contributions to charmless semileptonic decays of the form expected from the weak annihilation (WA) decay mechanism. Such contributions could bias determinations of /Vub/ from inclusive measurements of B-->Xulupsilon. Using a wide range of models based on available theoretical input we set a limit of GammaWA/Gammab-->u<7.4% (90% confidence level) on the WA fraction, and assess the impact on previous inclusive determinations of /Vub/.

Determination of extra trajectory parameters of projectile layout motion

NASA Astrophysics Data System (ADS)

Ishchenko, A.; Burkin, V.; Faraponov, V.; Korolkov, L.; Maslov, E.; Diachkovskiy, A.; Chupashev, A.; Zykova, A.

2017-11-01

The paper presents a brief description of the experimental track developed and implemented on the base of the RIAMM TSU for external trajectory investigations on determining the main aeroballistic parameters of various shapes projectiles, in the wide velocity range. There is comparison between the experimentally obtained dependence of the fin-stabilized projectile mock-up aerodynamic drag coefficient on the Mach number with the 1958 aerodynamic drag law and aerodynamic tests of the same mock-up

Comparison of two methods for detection of strain localization in sheet forming

NASA Astrophysics Data System (ADS)

Lumelskyj, Dmytro; Lazarescu, Lucian; Banabic, Dorel; Rojek, Jerzy

2018-05-01

This paper presents a comparison of two criteria of strain localization in experimental research and numerical simulation of sheet metal forming. The first criterion is based on the analysis of the through-thickness thinning (through-thickness strain) and its first time derivative in the most strained zone. The limit strain in the second method is determined by the maximum of the strain acceleration. Experimental and numerical investigation have been carried out for the Nakajima test performed for different specimens of the DC04 grade steel sheet. The strain localization has been identified by analysis of experimental and numerical curves showing the evolution of strains and their derivatives in failure zones. The numerical and experimental limit strains calculated from both criteria have been compared with the experimental FLC evaluated according to the ISO 12004-2 norm. It has been shown that the first method predicts formability limits closer to the experimental FLC. The second criterion predicts values of strains higher than FLC determined according to ISO norm. These values are closer to the strains corresponding to the fracture limit. The results show that analysis of strain evolution allows us to determine strain localization in numerical simulation and experimental studies.

Strain gage based determination of mixed mode SIFs

NASA Astrophysics Data System (ADS)

Murthy, K. S. R. K.; Sarangi, H.; Chakraborty, D.

2018-05-01

Accurate determination of mixed mode stress intensity factors (SIFs) is essential in understanding and analysis of mixed mode fracture of engineering components. Only a few strain gage determination of mixed mode SIFs are reported in literatures and those also do not provide any prescription for radial locations of strain gages to ensure accuracy of measurement. The present investigation experimentally demonstrates the efficacy of a proposed methodology for the accurate determination of mixed mode I/II SIFs using strain gages. The proposed approach is based on the modified Dally and Berger's mixed mode technique. Using the proposed methodology appropriate gage locations (optimal locations) for a given configuration have also been suggested ensuring accurate determination of mixed mode SIFs. Experiments have been conducted by locating the gages at optimal and non-optimal locations to study the efficacy of the proposed approach. The experimental results from the present investigation show that highly accurate SIFs (0.064%) can be determined using the proposed approach if the gages are located at the suggested optimal locations. On the other hand, results also show the very high errors (212.22%) in measured SIFs possible if the gages are located at non-optimal locations. The present work thus clearly substantiates the importance of knowing the optimal locations of the strain gages apriori in accurate determination of SIFs.

Optimal Experimental Design for Model Discrimination

ERIC Educational Resources Information Center

Myung, Jay I.; Pitt, Mark A.

2009-01-01

Models of a psychological process can be difficult to discriminate experimentally because it is not easy to determine the values of the critical design variables (e.g., presentation schedule, stimulus structure) that will be most informative in differentiating them. Recent developments in sampling-based search methods in statistics make it…

Open web system of Virtual labs for nuclear and applied physics

NASA Astrophysics Data System (ADS)

Saldikov, I. S.; Afanasyev, V. V.; Petrov, V. I.; Ternovykh, M. Yu

2017-01-01

An example of virtual lab work on unique experimental equipment is presented. The virtual lab work is software based on a model of real equipment. Virtual labs can be used for educational process in nuclear safety and analysis field. As an example it includes the virtual lab called “Experimental determination of the material parameter depending on the pitch of a uranium-water lattice”. This paper included general description of this lab. A description of a database on the support of laboratory work on unique experimental equipment which is included this work, its concept development are also presented.

Experimental Techniques for Thermodynamic Measurements of Ceramics

NASA Technical Reports Server (NTRS)

Jacobson, Nathan S.; Putnam, Robert L.; Navrotsky, Alexandra

1999-01-01

Experimental techniques for thermodynamic measurements on ceramic materials are reviewed. For total molar quantities, calorimetry is used. Total enthalpies are determined with combustion calorimetry or solution calorimetry. Heat capacities and entropies are determined with drop calorimetry, differential thermal methods, and adiabatic calorimetry . Three major techniques for determining partial molar quantities are discussed. These are gas equilibration techniques, Knudsen cell methods, and electrochemical techniques. Throughout this report, issues unique to ceramics are emphasized. Ceramic materials encompass a wide range of stabilities and this must be considered. In general data at high temperatures is required and the need for inert container materials presents a particular challenge.

Experimental spectroscopy for the high-school Physics curriculum

NASA Astrophysics Data System (ADS)

Kinra, Rajeev; Karpetis, Adonios

2008-11-01

The present work explores the feasibility of including spectroscopic experiments in high-school physics curricula. Two experimental optics ``modules'' were constructed for this purpose: (a) a simple CCD detector, in combination with appropriate filters, was used for the measurement of solar spectra and the determination of the sun's surface temperature; (b) the same detector was used, in combination with a transmissive diffraction grating and some miniature optics, to form a spectrophotometer that can be used for the determination of spectra with high resolution. Both modules were designed and constructed with portability and low cost in mind, and their objective is to introduce experimental spectroscopy to high school students in an intriguing, educational and phase-appropriate manner without sacrificing scientific rigor. A large variety of experiments may be designed around the basic devices that were built during this work, and a number of possible examples will be presented, from research on plant phototropism to human color cognition.

Comparison of Coupled Radiative Flow Solutions with Project Fire 2 Flight Data

NASA Technical Reports Server (NTRS)

Olynick, David R.; Henline, W. D.; Chambers, Lin Hartung; Candler, G. V.

1995-01-01

A nonequilibrium, axisymmetric, Navier-Stokes flow solver with coupled radiation has been developed for use in the design or thermal protection systems for vehicles where radiation effects are important. The present method has been compared with an existing now and radiation solver and with the Project Fire 2 experimental data. Good agreement has been obtained over the entire Fire 2 trajectory with the experimentally determined values of the stagnation radiation intensity in the 0.2-6.2 eV range and with the total stagnation heating. The effects of a number of flow models are examined to determine which combination of physical models produces the best agreement with the experimental data. These models include radiation coupling, multitemperature thermal models, and finite rate chemistry. Finally, the computational efficiency of the present model is evaluated. The radiation properties model developed for this study is shown to offer significant computational savings compared to existing codes.

Dominant modal decomposition method

NASA Astrophysics Data System (ADS)

Dombovari, Zoltan

2017-03-01

The paper deals with the automatic decomposition of experimental frequency response functions (FRF's) of mechanical structures. The decomposition of FRF's is based on the Green function representation of free vibratory systems. After the determination of the impulse dynamic subspace, the system matrix is formulated and the poles are calculated directly. By means of the corresponding eigenvectors, the contribution of each element of the impulse dynamic subspace is determined and the sufficient decomposition of the corresponding FRF is carried out. With the presented dominant modal decomposition (DMD) method, the mode shapes, the modal participation vectors and the modal scaling factors are identified using the decomposed FRF's. Analytical example is presented along with experimental case studies taken from machine tool industry.

The Evolution of the Celsius and Kelvin Temperature Scales and the State of the Art

NASA Astrophysics Data System (ADS)

Pellicer, Julio; Amparo Gilabert, M.; Lopez-Baeza, Ernesto

1999-07-01

A physical analysis is given of the evolution undergone by the Celsius and Kelvin temperature scales, from their definition to the present day. It is shown that in the temperature interval between the melting point of ice and the boiling point of water, the Celsius and Kelvin scales, both born centigrade by definition and actually become so afterwards by experimental determination as well, are not so any longer, either by definition or by experimental determination.

Experimental vibration damping characteristics of the third-stage rotor of a three-stage transonic axial-flow compressor

NASA Technical Reports Server (NTRS)

Newman, Frederick A.

1988-01-01

Rotor blade aerodynamic damping is experimentally determined in a three-stage transonic axial flow compressor having design aerodynamic performance goals of 4.5:1 pressure ratio and 65.5 lbm/sec weight flow. The combined damping associated with each mode is determined by a least squares fit of a single degree of freedom system transfer function to the nonsynchronous portion of the rotor blade strain gage output power spectra. The combined damping consists of the aerodynanmic damping and the structural and mechanical damping. The aerodynamic damping varies linearly with the inlet total pressure for a given corrected speed, weight flow, and pressure ratio while the structural and mechanical damping is assumed to remain constant. The combined damping is determined at three inlet total pressure levels to obtain the aerodynamic damping. The third-stage rotor blade aerodynamic damping is presented and discussed for the design equivalent speed with the stator blades reset for maximum efficiency. The compressor overall performance and experimental Campbell diagrams for the third-stage rotor blade row are also presented.

Experimental Vibration Damping Characteristics of the Third-stage Rotor of a Three-stage Transonic Axial-flow Compressor

NASA Technical Reports Server (NTRS)

Newman, Frederick A.

1988-01-01

Rotor blade aerodynamic damping is experimentally determined in a three-stage transonic axial flow compressor having design aerodynamic performance goals of 4.5:1 pressure ratio and 65.5 lbm/sec weight flow. The combined damping associated with each mode is determined by a least squares fit of a single degree of freedom system transfer function to the nonsynchronous portion of the rotor blade strain gage output power spectra. The combined damping consists of the aerodynamic damping and the structural and mechanical damping. The aerodynamic damping varies linearly with the inlet total pressure for a given corrected speed, weight flow, and pressure ratio while the structural and mechanical damping is assumed to remain constant. The combined damping is determined at three inlet total pressure levels to obtain the aerodynamic damping. The third-stage rotor blade aerodynamic damping is presented and discussed for the design equivalent speed with the stator blades reset for maximum efficiency. The compressor overall preformance and experimental Campbell diagrams for the third-stage rotor blade row are also presented.

Applicability of discovery science approach to determine biological effects of mobile phone radiation.

PubMed

Leszczynski, Dariusz; Nylund, Reetta; Joenväärä, Sakari; Reivinen, Jukka

2004-02-01

We argue that the use of high-throughput screening techniques, although expensive and laborious, is justified and necessary in studies that examine biological effects of mobile phone radiation. The "case of hsp27 protein" presented here suggests that even proteins with only modestly altered (by exposure to mobile phone radiation) expression and activity might have an impact on cell physiology. However, this short communication does not attempt to present the full scientific evidence that is far too large to be presented in a single article and that is being prepared for publication in three separate research articles. Examples of the experimental evidence presented here were designed to show the flow of experimental process demonstrating that the use of high-throughput screening techniques might help in rapid identification of the responding proteins. This, in turn, can help in speeding up of the process of determining whether these changes might affect human health.*

Plasma proteins in the acquired denture pellicle enhance substrate surface free energy and Candida albicans phospholipase and proteinase activities.

PubMed

Custodio, William; Silva, Wander J; Paes Leme, Adriana F; Cury, Jaime A; Del Bel Cury, Altair A

2015-11-01

The objective of the present study was to determine if blood plasma proteins could change the proteome of the acquired denture pellicle by label-free quantitative proteomics. As pellicle proteome modulates the interaction between substrates and Candida cells, we investigated its effect on the surface free energy (SFE) of the coated resin and on Candida albicans phospholipase and aspartyl proteinase activities. Poly(methylmethacrylate) discs were exposed to saliva (control) or saliva enriched with blood plasma (experimental group). The pellicle proteome was analyzed by mass spectrometry coupled with liquid chromatography. SFE was determined by acid-base technique. After biofilm formation, phospholipase and proteinase activities were determined accordingly to classic plate methods. Data were analyzed by two-way anova and Tukey test (P < 0.05). α-Amylase, cystatins, mucins, and host-immune system proteins were the main proteins identified in the control group. Fibrinogen and albumin were observed only in the experimental group. Coated discs of the experimental group presented an increased SFE (P < 0.05). For both enzymes tested, the experimental group showed higher proteolytic activity (P < 0.001). Blood plasma changes the proteome of the acquired denture pellicle, increasing surface free energy and the activity of Candida albicans phospholipase and aspartyl proteinase. © 2014 Wiley Publishing Asia Pty Ltd.

Direct experimental determination of the topological winding number of skyrmions in Cu2OSeO3

NASA Astrophysics Data System (ADS)

Zhang, S. L.; van der Laan, G.; Hesjedal, T.

2017-02-01

The mathematical concept of topology has brought about significant advantages that allow for a fundamental understanding of the underlying physics of a system. In magnetism, the topology of spin order manifests itself in the topological winding number which plays a pivotal role for the determination of the emergent properties of a system. However, the direct experimental determination of the topological winding number of a magnetically ordered system remains elusive. Here, we present a direct relationship between the topological winding number of the spin texture and the polarized resonant X-ray scattering process. This relationship provides a one-to-one correspondence between the measured scattering signal and the winding number. We demonstrate that the exact topological quantities of the skyrmion material Cu2OSeO3 can be directly experimentally determined this way. This technique has the potential to be applicable to a wide range of materials, allowing for a direct determination of their topological properties.

DETERMINATION OF HENRY'S LAW CONSTANTS OF SELECTED PRIORITY POLLUTANTS

EPA Science Inventory

The Henry's law constants (H) for 41 selected priority pollutants were determined to characterize these pollutants and provide information on their fate as they pass through wastewater treatment systems. All experimental values presented for H are averages of two or more replicat...

The Determination of Calcium in Dietary Supplement Tablets by Ion-Exchange.

ERIC Educational Resources Information Center

Dietz, Mark L.

1986-01-01

An experimental simple ion-exchange experiment in which the amount of calcium present in dietary supplement tablets has been developed is described and some typical student results for several brands of tablets are presented. (JN)

Experimental uncertainty survey and assessment. [Space Shuttle Main Engine testing

NASA Technical Reports Server (NTRS)

Coleman, Hugh W.

1992-01-01

An uncertainty analysis and assessment of the specific impulse determination during Space Shuttle Main Engine testing is reported. It is concluded that in planning and designing tests and in interpreting the results of tests, the bias and precision components of experimental uncertainty should be considered separately. Recommendations for future research efforts are presented.

Experimental Aerodynamic Derivatives of a Sinusoidally Oscillating Airfoil in Two-Dimensional Flow

NASA Technical Reports Server (NTRS)

Halfman, Robert L

1952-01-01

Experimental measurements of the aerodynamic reactions on a symmetrical airfoil oscillating harmonically in a two-dimensional flow are presented and analyzed. Harmonic motions include pure pitch and pure translation, for several amplitudes and superimposed on an initial angle of attack, as well as combined pitch and translation. The apparatus and testing program are described briefly and the necessary theoretical background is presented. In general, the experimental results agree remarkably well with the theory, especially in the case of the pure motions. The net work per cycle for a motion corresponding to flutter is experimentally determined to be zero. Considerable consistent data for pure pitch were obtained from a search of available reference material, and several definite Reynolds number effects are evident.

Structural characterization of a first-generation articulated-truss joint for space crane application

NASA Technical Reports Server (NTRS)

Sutter, Thomas R.; Wu, K. Chauncey; Riutort, Kevin T.; Laufer, Joseph B.; Phelps, James E.

1992-01-01

A first-generation space crane articulated-truss joint was statically and dynamically characterized in a configuration that approximated an operational environment. The articulated-truss joint was integrated into a test-bed for structural characterization. Static characterization was performed by applying known loads and measuring the corresponding deflections to obtain load-deflection curves. Dynamic characterization was performed using modal testing to experimentally determine the first six mode shapes, frequencies, and modal damping values. Static and dynamic characteristics were also determined for a reference truss that served as a characterization baseline. Load-deflection curves and experimental frequency response functions are presented for the reference truss and the articulated-truss joint mounted in the test-bed. The static and dynamic experimental results are compared with analytical predictions obtained from finite element analyses. Load-deflection response is also presented for one of the linear actuators used in the articulated-truss joint. Finally, an assessment is presented for the predictability of the truss hardware used in the reference truss and articulated-truss joint based upon hardware stiffness properties that were previously obtained during the Precision Segmented Reflector (PSR) Technology Development Program.

The Structure of the Protonated Serine Octamer.

PubMed

Scutelnic, Valeriu; Perez, Marta A S; Marianski, Mateusz; Warnke, Stephan; Gregor, Aurelien; Rothlisberger, Ursula; Bowers, Michael T; Baldauf, Carsten; von Helden, Gert; Rizzo, Thomas R; Seo, Jongcheol

2018-06-20

The amino acid serine has long been known to form a protonated "magic-number" cluster containing eight monomer units that shows an unusually high abundance in mass spectra and has a remarkable homochiral preference. Despite many experimental and theoretical studies, there is no consensus on a Ser 8 H + structure that is in agreement with all experimental observations. Here, we present the structure of Ser 8 H + determined by a combination of infrared spectroscopy and ab initio molecular dynamics simulations. The three-dimensional structure that we determine is ∼25 kcal mol -1 more stable than the previous most stable published structure and explains both the homochiral preference and the experimentally observed facile replacement of two serine units.

Two-photon absorption in oxazole derivatives: An experimental and quantum chemical study

NASA Astrophysics Data System (ADS)

Silva, D. L.; De Boni, L.; Correa, D. S.; Costa, S. C. S.; Hidalgo, A. A.; Zilio, S. C.; Canuto, S.; Mendonca, C. R.

2012-05-01

Experimental and theoretical studies on the two-photon absorption properties of two oxazole derivatives: 2,5-diphenyloxazole (PPO) and 2-(4-biphenylyl)-5-phenyl-1,3,4-oxadiazole (PBD) are presented. The two-photon absorption cross-section spectra were determined by means of the Z-scan technique, from 460 up to 650 nm, and reached peak values of 84 GM for PBD and 27 GM for PPO. Density Functional Theory and response function formalism are used to determine the molecular structures and the one- and two-photon absorption properties and to assist in the interpretation of the experimental results. The Polarizable Continuum Model in one-photon absorption calculations is used to estimate solvent effects.

Experimental determination of quantum-well lifetime effect on large-signal resonant tunneling diode switching time

DOE Office of Scientific and Technical Information (OSTI.GOV)

Growden, Tyler A.; Berger, Paul R., E-mail: pberger@ieee.org; Brown, E. R.

An experimental determination is presented of the effect the quantum-well lifetime has on a large-signal resonant tunneling diode (RTD) switching time. Traditional vertical In{sub 0.53}Ga{sub 0.47}As/AlAs RTDs were grown, fabricated, and characterized. The switching time was measured with a high-speed oscilloscope and found to be close to the sum of the calculated RC-limited 10%–90% switching time and the quantum-well quasibound-state lifetime. This method displays experimental evidence that the two intrinsic resonant-tunneling characteristic times act independently, and that the quasibound-state lifetime then serves as a quantum-limit on the large-signal speed of RTDs.

Experimental investigation of particle surface interactions for turbomachinery application

NASA Astrophysics Data System (ADS)

Hamed, A.; Tabakoff, W.

This paper describes an experimental investigation to determine the particle restitution characteristics after impacting solid targets in a particulate flow wind tunnel. The tests simulate the two phase flow conditions encountered in turbomachinery operating in particle laden flow environments. Both incoming and rebounding velocities are measured using a three color Argon Ion laser in backward scattered mode through a window in the tunnel section containing the impact target. The experimental results are presented for ash particles impinging on RENE 41 targets at different impact conditions. The presented results are applicable to particle dynamics simulations in gas turbine engines and to the prediction of the associated blade surface erosion.

Investigation of activation cross-sections of deuteron induced reactions on vanadium up to 40 MeV

NASA Astrophysics Data System (ADS)

Tárkányi, F.; Ditrói, F.; Takács, S.; Hermanne, A.; Baba, M.; Ignatyuk, A. V.

2011-08-01

Experimental excitation functions for deuteron induced reactions up to 40 MeV on natural vanadium were measured with the activation method using a stacked foil irradiation technique. From high resolution gamma spectrometry cross-section data for the production of 51Cr, 48V, 48,47,46Sc and 47Ca were determined. Comparisons with the earlier published data are presented and results for values predicted by different theoretical codes are included. Thick target yields were calculated from a fit to our experimental excitation curves and compared with the earlier experimental data. Depth distribution curves used for thin layer activation (TLA) are also presented.

Stress Induced Degradation Modes in CIGSS Minimodules (Presentation)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kempe, M. D.; Terwilliger, K.; Tarrant, D.

2008-05-01

The experimental objectives of this report are: (1) compare the performance of modules exposed to high temperature and humidity; (2) determine the effects of different encapsulants on long term stability of CIGSS modules; and (3) analyze failure modes to determine areas in need of improvement.

The Construction of an Embankment with Frozen Soil.

DTIC Science & Technology

1980-05-01

Idewlrty by block numlbe) Inls paper presents the construction procedure, data and analysis from an experimental field program to determine the rippability ...finite element computer solution. Also the frozen chunks, produced in the ripping operation, were analyzed to determine the rippability of the frozen

Determination of minor and trace elements in kidney stones by x-ray fluorescence analysis

NASA Astrophysics Data System (ADS)

Srivastava, Anjali; Heisinger, Brianne J.; Sinha, Vaibhav; Lee, Hyong-Koo; Liu, Xin; Qu, Mingliang; Duan, Xinhui; Leng, Shuai; McCollough, Cynthia H.

2014-03-01

The determination of accurate material composition of a kidney stone is crucial for understanding the formation of the kidney stone as well as for preventive therapeutic strategies. Radiations probing instrumental activation analysis techniques are excellent tools for identification of involved materials present in the kidney stone. In particular, x-ray fluorescence (XRF) can be very useful for the determination of minor and trace materials in the kidney stone. The X-ray fluorescence measurements were performed at the Radiation Measurements and Spectroscopy Laboratory (RMSL) of department of nuclear engineering of Missouri University of Science and Technology and different kidney stones were acquired from the Mayo Clinic, Rochester, Minnesota. Presently, experimental studies in conjunction with analytical techniques were used to determine the exact composition of the kidney stone. A new type of experimental set-up was developed and utilized for XRF analysis of the kidney stone. The correlation of applied radiation source intensity, emission of X-ray spectrum from involving elements and absorption coefficient characteristics were analyzed. To verify the experimental results with analytical calculation, several sets of kidney stones were analyzed using XRF technique. The elements which were identified from this techniques are Silver (Ag), Arsenic (As), Bromine (Br), Chromium (Cr), Copper (Cu), Gallium (Ga), Germanium (Ge), Molybdenum (Mo), Niobium (Nb), Rubidium (Rb), Selenium (Se), Strontium (Sr), Yttrium (Y), Zirconium (Zr). This paper presents a new approach for exact detection of accurate material composition of kidney stone materials using XRF instrumental activation analysis technique.

True temperature measurement on metallic surfaces using a two-color pyroreflectometer method.

PubMed

Hernandez, D; Netchaieff, A; Stein, A

2009-09-01

In the most common case of optical pyrometry, the major obstacle in determining the true temperature is the knowledge of the thermo-optical properties for in situ conditions. We present experimental results obtained with a method able to determine the true temperature of metallic surfaces above 500 degrees C when there is not parasitic effect by surrounding radiation. The method is called bicolor pyroreflectometry and it is based on Planck's law, Kirchhoff's law, and the assumption of identical reflectivity indicatrixes for the target surface at two different close wavelengths (here, 1.3 and 1.55 microm). The diffusion factor eta(d), the key parameter of the method, is introduced to determine the convergence temperature T(*), which is expected to be equal to the true temperature T. Our goal is to asses this method for different metallic surfaces. The validation of this method is made by comparison with thermocouples. Measurements were made for tungsten, copper, and aluminum samples of different roughnesses, determined by a rugosimeter. After introducing a theoretical model for two-color pyroreflectometry, we give a description of the experimental setup and present experimental applications of the subject method. The quality of the results demonstrates the usefulness of two-color pyroreflectometry to determine the temperatures of hot metals when the emissivity is not known and for the commercially important case of specular surfaces.

Heat storage in alloy transformations

NASA Technical Reports Server (NTRS)

Birchenall, C. E.; Gueceri, S. I.; Farkas, D.; Labdon, M. B.; Nagaswami, N.; Pregger, B.

1981-01-01

The feasibility of using metal alloys as thermal energy storage media was determined. The following major elements were studied: (1) identification of congruently transforming alloys and thermochemical property measurements; (2) development of a precise and convenient method for measuring volume change during phase transformation and thermal expansion coefficients; (3) development of a numerical modeling routine for calculating heat flow in cylindrical heat exchangers containing phase change materials; and (4) identification of materials that could be used to contain the metal alloys. Several eutectic alloys and ternary intermetallic phases were determined. A method employing X-ray absorption techniques was developed to determine the coefficients of thermal expansion of both the solid and liquid phases and the volume change during phase transformation from data obtained during one continuous experimental test. The method and apparatus are discussed and the experimental results are presented. The development of the numerical modeling method is presented and results are discussed for both salt and metal alloy phase change media.

Joint surface modeling with thin-plate splines.

PubMed

Boyd, S K; Ronsky, J L; Lichti, D D; Salkauskas, K; Chapman, M A; Salkauskas, D

1999-10-01

Mathematical joint surface models based on experimentally determined data points can be used to investigate joint characteristics such as curvature, congruency, cartilage thickness, joint contact areas, as well as to provide geometric information well suited for finite element analysis. Commonly, surface modeling methods are based on B-splines, which involve tensor products. These methods have had success; however, they are limited due to the complex organizational aspect of working with surface patches, and modeling unordered, scattered experimental data points. An alternative method for mathematical joint surface modeling is presented based on the thin-plate spline (TPS). It has the advantage that it does not involve surface patches, and can model scattered data points without experimental data preparation. An analytical surface was developed and modeled with the TPS to quantify its interpolating and smoothing characteristics. Some limitations of the TPS include discontinuity of curvature at exactly the experimental surface data points, and numerical problems dealing with data sets in excess of 2000 points. However, suggestions for overcoming these limitations are presented. Testing the TPS with real experimental data, the patellofemoral joint of a cat was measured with multistation digital photogrammetry and modeled using the TPS to determine cartilage thicknesses and surface curvature. The cartilage thickness distribution ranged between 100 to 550 microns on the patella, and 100 to 300 microns on the femur. It was found that the TPS was an effective tool for modeling joint surfaces because no preparation of the experimental data points was necessary, and the resulting unique function representing the entire surface does not involve surface patches. A detailed algorithm is presented for implementation of the TPS.

On investigating wall shear stress in two-dimensional plane turbulent wall jets

NASA Astrophysics Data System (ADS)

Mehdi, Faraz; Johansson, Gunnar; White, Christopher; Naughton, Jonathan

2012-11-01

Mehdi & White [Exp Fluids 50:43-51(2011)] presented a full momentum integral based method for determining wall shear stress in zero pressure gradient turbulent boundary layers. They utilized the boundary conditions at the wall and at the outer edge of the boundary layer. A more generalized expression is presented here that uses just one boundary condition at the wall. The method is mathematically exact and has an advantage of having no explicit streamwise gradient terms. It is successfully applied to two different experimental plane turbulent wall jet datasets for which independent estimates of wall shear stress were known. Complications owing to experimental inaccuracies in determining wall shear stress from the proposed method are also discussed.

Ion beam-based studies for tribological phenomena

NASA Astrophysics Data System (ADS)

Racolta, P. M.; Popa-Simil, L.; Alexandreanu, B.

1996-06-01

Custom-designed experiments based on the Thin Layer Activation technique (TLA) were completed, providing information on the wear level of some engine components with additional data on transfer and adhesion of material between metallic friction couples using the RBS method. RBS experimental results concerning material transfer for a steel-brass friction couple are presented and discussed in the paper. Also, the types and concentrations of the wear products in used lubricant oils were determined by in-air PIXE. A sequential lubricant filtering-based procedure for determining the dimension distribution of the resulting radioactive wear particles by low level γ-spectrometry is presented. Experimental XRF spectra showing the non-homogeneous distribution of the retained waste particles on the filtering paper are shown.

Multiple-path model of spectral reflectance of a dyed fabric.

PubMed

Rogers, Geoffrey; Dalloz, Nicolas; Fournel, Thierry; Hebert, Mathieu

2017-05-01

Experimental results are presented of the spectral reflectance of a dyed fabric as analyzed by a multiple-path model of reflection. The multiple-path model provides simple analytic expressions for reflection and transmission of turbid media by applying the Beer-Lambert law to each path through the medium and summing over all paths, each path weighted by its probability. The path-length probability is determined by a random-walk analysis. The experimental results presented here show excellent agreement with predictions made by the model.

Thermal desorption of metals from tungsten single crystal surfaces

NASA Technical Reports Server (NTRS)

Bauer, E.; Bonczek, F.; Poppa, H.; Todd, G.

1975-01-01

After a short review of experimental methods used to determine desorption energies and frequencies the assumptions underlying the theoretical analysis of experimental data are discussed. Recent experimental results on the flash desorption of Cu, Ag, and Au from clean, well characterized W (110) and (100) surfaces are presented and analyzed in detail with respect to the coverage dependence. The results obtained clearly reveal the limitations of previous analytical methods and of the experimental technique per se (such as structure and phase changes below and in the temperature region in which desorption occurs).

Experimental Investigation of the Momentum Method for Determining Profile Drag

NASA Technical Reports Server (NTRS)

Goett, Harry J

1939-01-01

Report presents the results of an experimental investigation conducted in the full-scale tunnel to determine the accuracy of the Jones and the Betz equations for computing profile drag from total and static pressure surveys in the wake of wings. Surveys were made behind 6 by 8-foot airfoils of the NACA 0009, and 0018 sections at zero lift and behind the NACA 0012 at positive lifts. The surveys were made at various spanwise positions and at distances behind the airfoil ranging from 0.05c to 3.00c.

Lee side flow for slender delta wings of finite thickness

NASA Technical Reports Server (NTRS)

Szodruch, J. G.

1980-01-01

An experimental and theoretical investigation carried out to determine the lee side flow field over delta wings at supersonic speeds is presented. A theoretical method to described the flow field is described, where boundary conditions as a result of the experimental study are needed. The computed flow field with shock induced separation is satisfactory.

Conversion of microwave signals by superconducting films in the resistive state

NASA Technical Reports Server (NTRS)

Yeru, I. I.; Peskovatskiy, S. A.; Sulima, V. S.

1984-01-01

The main characteristics of a superconducting thin film microwave mixer, i.e., conversion efficiency and bandwidth are analyzed. The optimum operating regime of the nonlinear element is determined. Results of calculations are compared with the experimental ones. Experimental data on the noise in the superconducting films in a wide frequency range are presented.

Wavelet transform fast inverse light scattering analysis for size determination of spherical scatterers

PubMed Central

Ho, Derek; Kim, Sanghoon; Drake, Tyler K.; Eldridge, Will J.; Wax, Adam

2014-01-01

We present a fast approach for size determination of spherical scatterers using the continuous wavelet transform of the angular light scattering profile to address the computational limitations of previously developed sizing techniques. The potential accuracy, speed, and robustness of the algorithm were determined in simulated models of scattering by polystyrene beads and cells. The algorithm was tested experimentally on angular light scattering data from polystyrene bead phantoms and MCF-7 breast cancer cells using a 2D a/LCI system. Theoretical sizing of simulated profiles of beads and cells produced strong fits between calculated and actual size (r2 = 0.9969 and r2 = 0.9979 respectively), and experimental size determinations were accurate to within one micron. PMID:25360350

Molecular Diffusion Coefficients: Experimental Determination and Demonstration.

ERIC Educational Resources Information Center

Fate, Gwendolyn; Lynn, David G.

1990-01-01

Presented are laboratory methods which allow the demonstration and determination of the diffusion coefficients of compounds ranging in size from water to small proteins. Included are the procedures involving the use of a spectrometer, UV cell, triterated agar, and oxygen diffusion. Results including quantification are described. (CW)

Effects of auditory information on self-motion perception during simultaneous presentation of visual shearing motion

PubMed Central

Tanahashi, Shigehito; Ashihara, Kaoru; Ujike, Hiroyasu

2015-01-01

Recent studies have found that self-motion perception induced by simultaneous presentation of visual and auditory motion is facilitated when the directions of visual and auditory motion stimuli are identical. They did not, however, examine possible contributions of auditory motion information for determining direction of self-motion perception. To examine this, a visual stimulus projected on a hemisphere screen and an auditory stimulus presented through headphones were presented separately or simultaneously, depending on experimental conditions. The participant continuously indicated the direction and strength of self-motion during the 130-s experimental trial. When the visual stimulus with a horizontal shearing rotation and the auditory stimulus with a horizontal one-directional rotation were presented simultaneously, the duration and strength of self-motion perceived in the opposite direction of the auditory rotation stimulus were significantly longer and stronger than those perceived in the same direction of the auditory rotation stimulus. However, the auditory stimulus alone could not sufficiently induce self-motion perception, and if it did, its direction was not consistent within each experimental trial. We concluded that auditory motion information can determine perceived direction of self-motion during simultaneous presentation of visual and auditory motion information, at least when visual stimuli moved in opposing directions (around the yaw-axis). We speculate that the contribution of auditory information depends on the plausibility and information balance of visual and auditory information. PMID:26113828

Desynchronization of stochastically synchronized chemical oscillators

DOE Office of Scientific and Technical Information (OSTI.GOV)

Snari, Razan; Tinsley, Mark R., E-mail: mark.tinsley@mail.wvu.edu, E-mail: kshowalt@wvu.edu; Faramarzi, Sadegh

Experimental and theoretical studies are presented on the design of perturbations that enhance desynchronization in populations of oscillators that are synchronized by periodic entrainment. A phase reduction approach is used to determine optimal perturbation timing based upon experimentally measured phase response curves. The effectiveness of the perturbation waveforms is tested experimentally in populations of periodically and stochastically synchronized chemical oscillators. The relevance of the approach to therapeutic methods for disrupting phase coherence in groups of stochastically synchronized neuronal oscillators is discussed.

Theory and experimental results of transfer-NOE experiments. 1. The influence of the off rate versus cross-relaxation rates

NASA Astrophysics Data System (ADS)

Lippens, R. M.; Cerf, C.; Hallenga, K.

The theory of the transferred nuclear Overhauser effect is presented in the framework of an extended relaxation matrix representation. This matrix representation allows a coherent description of all one- and two-dimensional experiments. We present analytical solutions for the buildup of magnetization in the 2D transfer-NOE experiment, for all ratios of the off rate k to the cross-relaxation rates R involved. We show that systematic deviations in distance determination occur when the off rate becomes comparable to or smaller than the relaxation rates. Experimental results on the peptide/protein system oxytocin/neurophysin confirming this analysis are presented. The importance of residual mobility in the bound ligand, as demonstrated by the experimental data, is also discussed.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jin Fengtao; Yuan Jianmin

The experimental transmission spectrum of a hot bromine plasma [J. E. Bailey et al., J. Quant. Spectrosc. Radiat. Transf. 81, 31 (2003)] has been simulated by using a detailed level accounting model (DLA). With assumption of the local thermodynamic equilibrium, the major absorption lines of the experimental spectrum are well reproduced by the present DLA calculation, and the details of the absorption line shapes are used to determine the temperature of the plasma. In contrast to the results of two former statistical models, where the temperature was determined via a global fitting to the experimental data, the present DLA diagnosesmore » the plasma temperature by the line ratios of different charge states in the 2p{yields}3d transition groups resulting in a temperature of 37 eV. It is shown that a change of 1 eV in temperature could cause perceptible changes in the simulated spectrum. It is also shown that the 2p{sub 1/2}{yields}3d{sub 3/2} absorptions have been overestimated by the statistical models.« less

The Effect of Presentation Strategy on Reading Comprehension of Iranian Intermediate EFL Learners

ERIC Educational Resources Information Center

Khoshsima, Hooshang; Rezaeiantiyar, Forouzan

2014-01-01

The present experimental study primarily aimed at examining the effect of presentation strategy on reading comprehension of Iranian intermediate EFL learners. To determine the effect of this strategy, 61 students who enrolled in English Language Center of Chabahar Maritime University were initially selected and then divided randomly into two…

Acid Rain Analysis by Standard Addition Titration.

ERIC Educational Resources Information Center

Ophardt, Charles E.

1985-01-01

The standard addition titration is a precise and rapid method for the determination of the acidity in rain or snow samples. The method requires use of a standard buret, a pH meter, and Gran's plot to determine the equivalence point. Experimental procedures used and typical results obtained are presented. (JN)

Effects of an intervention with teachers in the physical education context: A Self-Determination Theory approach

PubMed Central

2017-01-01

Framed within Self-Determination Theory, the purpose of the present study was to test the effects of a training program with physical education (PE) teachers. Participants were 21 high school PE teachers (experimental group, n = 10; control group, n = 11), and their 836 students, aged 12 to 16 years. Teachers in the experimental group received a training program consisting of strategies to support autonomy, competence, and relatedness need satisfaction. A repeated measures ANCOVA was carried out for each dependent variable. After the intervention, students in the experimental group significantly increased their scores on autonomy support, relatedness support, autonomy satisfaction, autonomous motivation, controlled motivation, and intention to be physically active, as compared to the control group. These findings emphasize the utility of a training program with PE teachers to promote the students’ psychological need satisfaction, and hence, self-determined motivation toward PE classes. PMID:29284027

Experimental investigation of supersonic low pressure air plasma flows obtained with different arc-jet operating conditions

NASA Astrophysics Data System (ADS)

Lago, Viviana; Ndiaye, Abdoul-Aziz

2012-11-01

A stationary arc-jet plasma flow at low pressure is used to simulate some properties of the gas flow surrounding a vehicle during its entry into celestial body's atmospheres. This paper presents an experimental study concerning plasmas simulating a re-entry into our planet. Optical measurements have been carried out for several operating plasma conditions in the free stream, and in the shock layer formed in front of a flat cylindrical plate, placed in the plasma jet. The analysis of the spectral radiation enabled the identification of the emitting species, the determination of the rotational and vibrational temperatures in the free-stream and in the shock layer and the determination of the distance of the shock to the flat plate face. Some plasma fluid parameters like, stagnation pressure, specific enthalpy and heat flux have been determined experimentally along the plasma-jet axis.

Determination of Important Nuclear Fragmentation Processes for Human Space Radiation Protection

NASA Technical Reports Server (NTRS)

Lin, Zi-Wei

2007-01-01

We present a semi-analytical method to determine which partial cross sections of nuclear fragmentations most affect the shielded dose equivalent due to exposure to galactic cosmic rays. The cross sections thus determined will require more theoretical and/or experimental studies in order for us to better predict, reduce and mitigate the radiation exposure in human space explorations.

An Improvement of the Anisotropy and Formability Predictions of Aluminum Alloy Sheets

NASA Astrophysics Data System (ADS)

Banabic, D.; Comsa, D. S.; Jurco, P.; Wagner, S.; Vos, M.

2004-06-01

The paper presents an yield criterion for orthotropic sheet metals and its implementation in a theoretical model in order to calculate the Forming Limit Curves. The proposed yield criterion has been validated for two aluminum alloys: AA3103-0 and AA5182-0, respectively. The biaxial tensile test of cross specimens has been used for the determination of the experimental yield locus. The new yield criterion has been implemented in the Marciniak-Kuczynski model for the calculus of limit strains. The calculated Forming Limit Curves have been compared with the experimental ones, determined by frictionless test: bulge test, plane strain test and uniaxial tensile test. The predicted Forming Limit Curves using the new yield criterion are in good agreement with the experimental ones.

OSCILLATOR STRENGTHS OF VIBRIONIC EXCITATIONS OF NITROGEN DETERMINED BY THE DIPOLE (γ, γ) METHOD

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liu, Ya-Wei; Kang, Xu; Xu, Long-Quan

2016-03-10

The oscillator strengths of the valence-shell excitations of molecular nitrogen have significant applicational values in studies of the Earth's atmosphere and interstellar gases. In this work, the absolute oscillator strengths of the valence-shell excitations of molecular nitrogen in 12.3–13.4 eV were measured by the novel dipole (γ, γ) method, in which the high-resolution inelastic X-ray scattering is operated at a negligibly small momentum transfer and can simulate the photoabsorption process. Because the experimental technique used in the present work is distinctly different from those used previously, the present experimental results give an independent cross-check to previous experimental and theoretical data.more » The excellent coincidence of the present results with the dipole (e, e) and those that were extrapolated indicates that the present oscillator strengths can serve as benchmark data.« less

Exploring the resonant vibration of thin plates: Reconstruction of Chladni patterns and determination of resonant wave numbers.

PubMed

Tuan, P H; Wen, C P; Chiang, P Y; Yu, Y T; Liang, H C; Huang, K F; Chen, Y F

2015-04-01

The Chladni nodal line patterns and resonant frequencies for a thin plate excited by an electronically controlled mechanical oscillator are experimentally measured. Experimental results reveal that the resonant frequencies can be fairly obtained by means of probing the variation of the effective impedance of the exciter with and without the thin plate. The influence of the extra mass from the central exciter is confirmed to be insignificant in measuring the resonant frequencies of the present system. In the theoretical aspect, the inhomogeneous Helmholtz equation is exploited to derive the response function as a function of the driving wave number for reconstructing experimental Chladni patterns. The resonant wave numbers are theoretically identified with the maximum coupling efficiency as well as the maximum entropy principle. Substituting the theoretical resonant wave numbers into the derived response function, all experimental Chladni patterns can be excellently reconstructed. More importantly, the dispersion relationship for the flexural wave of the vibrating plate can be determined with the experimental resonant frequencies and the theoretical resonant wave numbers. The determined dispersion relationship is confirmed to agree very well with the formula of the Kirchhoff-Love plate theory.

Technical Note: Determination of the SCS initial abstraction ratio in an experimental watershed in Greece

NASA Astrophysics Data System (ADS)

Baltas, E. A.; Dervos, N. A.; Mimikou, M. A.

2007-11-01

The present study was conducted in an experimental watershed in Attica, Greece, using observed rainfall/runoff events. The objective of the study was the determination of the initial abstraction ratio of the watershed. The average ratio (Ia/S) of the entire watershed was equal to 0.014. The corresponding ratio at a subwatershed was 0.037. The difference was attributed to the different spatial distribution of landuses and geological formations at the extent of the watershed. Both of the determined ratios are close to the ratio value of 0.05 that has been suggested from many studies for the improvement of the SCS-CN method.

Modal Damping Ratio and Optimal Elastic Moduli of Human Body Segments for Anthropometric Vibratory Model of Standing Subjects.

PubMed

Gupta, Manoj; Gupta, T C

2017-10-01

The present study aims to accurately estimate inertial, physical, and dynamic parameters of human body vibratory model consistent with physical structure of the human body that also replicates its dynamic response. A 13 degree-of-freedom (DOF) lumped parameter model for standing person subjected to support excitation is established. Model parameters are determined from anthropometric measurements, uniform mass density, elastic modulus of individual body segments, and modal damping ratios. Elastic moduli of ellipsoidal body segments are initially estimated by comparing stiffness of spring elements, calculated from a detailed scheme, and values available in literature for same. These values are further optimized by minimizing difference between theoretically calculated platform-to-head transmissibility ratio (TR) and experimental measurements. Modal damping ratios are estimated from experimental transmissibility response using two dominant peaks in the frequency range of 0-25 Hz. From comparison between dynamic response determined form modal analysis and experimental results, a set of elastic moduli for different segments of human body and a novel scheme to determine modal damping ratios from TR plots, are established. Acceptable match between transmissibility values calculated from the vibratory model and experimental measurements for 50th percentile U.S. male, except at very low frequencies, establishes the human body model developed. Also, reasonable agreement obtained between theoretical response curve and experimental response envelop for average Indian male, affirms the technique used for constructing vibratory model of a standing person. Present work attempts to develop effective technique for constructing subject specific damped vibratory model based on its physical measurements.

Determination of the Minimum Use Level of Fuel System Icing Inhibitor (FSII) in JP-8 That Will Provide Adquate Icing Inhibition and Biostatic Protection for Air Force Aircraft

DTIC Science & Technology

2013-12-01

experimental studies and analyses performed and the resulting recommendations. Results from the present effort indicated that a minimum use limit of... experimental studies performed and the resulting recommendations regarding the minimum on-board use limit of FSII while maintaining safe operability...sumping. A detailed summary of the experimental efforts and results are provided in a separate report (Balster et al., 2010). For the ATCC

Probing of the interfacial Heisenberg and Dzyaloshinskii-Moriya exchange interaction by magnon spectroscopy.

PubMed

Zakeri, Khalil

2017-01-11

This Topical Review presents an overview of the recent experimental results on the quantitative determination of the magnetic exchange parameters in ultrathin magnetic films and multilayers grown on different substrates. The experimental approaches for probing both the symmetric Heisenberg and the antisymmetric Dzyaloshinskii-Moriya exchange interaction in ultrathin magnetic films and at interfaces are discussed in detail. It is explained how the experimental spectrum of magnetic excitations can be used to quantify the strength of these interactions.

Theoretical and experimental study of aerodynamics, heat transfer and performance of a radial turbine

NASA Technical Reports Server (NTRS)

Tabakoff, W.

1975-01-01

A two-dimensional finite difference numerical technique is presented to determine the temperature distribution in a solid blade of a radial turbine guide vane. A computer program is written in FORTRAN 4 for the IBM 370/165 computer. The computer results obtained from these programs have a similar behavior and trend as those obtained by experimental results.

The experimental determination of the coefficient of hydraulic resistance of a perforated plate with a layer of balls adjoining to it

NASA Astrophysics Data System (ADS)

Smorchkova, Yu V.; Varava, A. N.; Dedov, A. V.; Zakharenkov, A. V.; Komov, A. T.

2017-10-01

The results of an experimental study of the hydrodynamics of a perforated plate with a layer of balls adjoining to it are presented herein. The experiments were carried out in the fluid flow range from 0.1 to 0.6 kg/s, at a fluid temperature of 19 °C.

Experimental Demonstration of Isomorphism.

ERIC Educational Resources Information Center

Kamenicek, J.; Melicharek, M.

2000-01-01

Describes some simple experiments related to the properties of crystals. Illustrates isomorphism using single crystals of alum. Presents experiments for determining how various mixture compositions affect the growth of salt crystals. (WRM)

Quantitative surface topography determination by Nomarski reflection microscopy. 2: Microscope modification, calibration, and planar sample experiments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hartman, J.S.; Gordon, R.L.; Lessor, D.L.

1980-09-01

The application of reflective Nomarski differential interference contrast microscopy for the determination of quantitative sample topography data is presented. The discussion includes a review of key theoretical results presented previously plus the experimental implementation of the concepts using a commercial Momarski microscope. The experimental work included the modification and characterization of a commercial microscope to allow its use for obtaining quantitative sample topography data. System usage for the measurement of slopes on flat planar samples is also discussed. The discussion has been designed to provide the theoretical basis, a physical insight, and a cookbook procedure for implementation to allow thesemore » results to be of value to both those interested in the microscope theory and its practical usage in the metallography laboratory.« less

Evaluation of microcrack thermal shock damage in ceramics: Modeling and experiment

NASA Technical Reports Server (NTRS)

Chu, Y. C.; Hefetz, M.; Rokhlin, S. I.

1992-01-01

In this paper we present an experimental and theoretical study of the effect of microcrack damage on ceramic properties. For the experimental investigation, ceramic samples of aluminum oxide and reaction bonded silicon nitride (RBSN) are used. Thermal shock treatment from different temperatures up to 1000 C is applied to produce the microcracks. Both surface and bulk ultrasonic wave methods are used to correlate the change of elastic constants to microstructural degradation and to determine the change in elastic anisotropy induced by microcrack damage. For the theoretical investigation, damage mechanics, which relates microstructural damage to material service life and mechanical failure, is used. The change in elastic properties due to microcrack damage calculated from the theoretical model is compared with the experimental results for determination of the applicability of damage theory. It is shown that two independent experimental methods (bulk wave and surface wave) give the same results for shear moduli of damaged ceramics. The experimental results aagree reasonably well with the moduli predicted from the cracked solid model.

A Correlation for Forced Convective Boiling Heat Transfer of Refrigerants in a Microfin Tube

NASA Astrophysics Data System (ADS)

Momoki, Satoru; Yu, Jian; Koyama, Shigeru; Fujii, Tetsu; Honda, Hiroshi

The experimental study is reported on the forced convective boiling of pure refrigerants HCFC22, HFC134a and HCFC123 flowing in a horizontal microfin tube. The local heat transfer coefficient defined based on the actual inside surface area is measured in the ranges of mass velocity of 200 to 400 kg/m2s, heat flux of 5 to 64 kW/m2 and reduced pressure of 0.07 to 0.24. Using the Chen-type model, a new correlation for microfin tubes is proposed considering the enhancement effect of microfins on both the convective heat transfer and the nucleate boiling components. In the convective heat transfer component, the correlation to predict the heat transfer coefficient of liquid-only flow is determined from preliminary experiments on single-phase flow in microfin tubes, and the two-phase flow enhancement factor is determined from the present experimental data. For the nucleate boiling component, the correlation of Takamatsu et al. for smooth tube is modified. The prediction of the present correlation agrees well with present experimental data, and is available for several microfin tubes which were tested by other researchers.

Determination of Thermal Conductivity of Silicate Matrix for Applications in Effective Media Theory

NASA Astrophysics Data System (ADS)

Fiala, Lukáš; Jerman, Miloš; Reiterman, Pavel; Černý, Robert

2018-02-01

Silicate materials have an irreplaceable role in the construction industry. They are mainly represented by cement-based- or lime-based materials, such as concrete, cement mortar, or lime plaster, and consist of three phases: the solid matrix and air and water present in the pores. Therefore, their effective thermal conductivity depends on thermal conductivities of the involved phases. Due to the time-consuming experimental determination of the effective thermal conductivity, its calculation by means of homogenization techniques presents a reasonable alternative. In the homogenization theory, both volumetric content and particular property of each phase need to be identified. For porous materials the most problematic part is to accurately identify thermal conductivity of the solid matrix. Due to the complex composition of silicate materials, the thermal conductivity of the matrix can be determined only approximately, based on the knowledge of thermal conductivities of its major compounds. In this paper, the thermal conductivity of silicate matrix is determined using the measurement of a sufficiently large set of experimental data. Cement pastes with different open porosities are prepared, dried, and their effective thermal conductivity is determined using a transient heat-pulse method. The thermal conductivity of the matrix is calculated by means of extrapolation of the effective thermal conductivity versus porosity functions to zero porosity. Its practical applicability is demonstrated by calculating the effective thermal conductivity of a three-phase silicate material and comparing it with experimental data.

Motivation for proposed experimentation in the realm of accelerated E. M. systems: A preliminary design for an experiment

NASA Technical Reports Server (NTRS)

Post, E. J.

1970-01-01

An experiment, designed to determine the difference between fields-magnetic and electric-surrounding a uniformly moving charge as contrasted with the fields surrounding an accelerated charge, is presented. A thought experiment is presented to illustrate the process.

Comparison of the Experimental Performance of Ferroelectric CPW Circuits with Method of Moment Simulations and Conformal Mapping

NASA Technical Reports Server (NTRS)

VanKeuls, Fred W.; Chevalier, Chris T.; Miranda, Felix A.; Carlson, C. M.; Rivkin, T. V.; Parilla, P. A.; Perkins, J. D.; Ginley, D. S.

2001-01-01

Experimental measurements of coplanar waveguide (CPW) circuits atop thin films of ferroelectric Ba(x)Sr(1-x)TiO3 (BST) were made as a function bias from 0 to 200 V and frequency from 0.045 to 20 GHz. The resulting phase shifts are compared with method of moments electromagnetic simulations and a conformal mapping analysis to determine the dielectric constant of the BST films. Based on the correlation between the experimental and the modeled data, an analysis of the extent to which the electromagnetic simulators provide reliable values for the dielectric constant of the ferroelectric in these structures has been performed. In addition, to determine how well the modeled data compare with experimental data, the dielectric constant values were also compared to low frequency measurements of interdigitated capacitor circuits on the same films. Results of these comparisons will be presented.

Experimental pretesting of public health campaigns: a case study.

PubMed

Whittingham, Jill; Ruiter, Robert A C; Zimbile, Filippo; Kok, Gerjo

2008-01-01

The aim of the present study is to demonstrate the merits of evaluating new public health campaign materials in the developmental phase using an experimental design. This is referred to as experimental pretesting. In practice, most new materials are tested only after they have been distributed using nonexperimental or quasiexperimental designs. In cases where materials are pretested prior to distribution, pretesting is usually done using qualitative research methods such as focus groups. Although these methods are useful, they cannot reliably predict the effectiveness of new campaign materials in a developmental phase. Therefore, we suggest when pretesting new materials, not only qualitative research methods but also experimental research methods must be used. The present study discusses an experimental pretest study of new campaign materials intended for distribution in a national sexually transmitted infection (STI) AIDS prevention campaign in the Netherlands. The campaign material tested was the storyline of a planned television commercial on safe sex. A storyboard that consisted of drawings and text was presented to members of the target population, namely, students between the ages of 14 and 16 enrolled in vocational schools. Results showed positive effects on targeted determinants of safe sexual behavior. The advantages, practical implications, and limitations of experimental pretesting are discussed.

Vibrational excitation of water by electron impact

DOE Office of Scientific and Technical Information (OSTI.GOV)

Khakoo, M. A.; Winstead, C.; McKoy, V.

2009-05-15

Experimental and calculated differential cross sections (DCSs) for electron-impact excitation of the (010) bending mode and unresolved (100) symmetric and (001) antisymmetric stretching modes of water are presented. Measurements are reported at incident energies of 1-100 eV and scattering angles of 10 deg. - 130 deg. and are normalized to the elastic-scattering DCSs for water determined earlier by our group. The calculated cross sections are obtained in the adiabatic approximation from fixed-nuclei, electronically elastic scattering calculations using the Schwinger multichannel method. The present results are compared to available experimental and theoretical data.

Minimum-Risk Path Finding by an Adaptive Amoebal Network

NASA Astrophysics Data System (ADS)

Nakagaki, Toshiyuki; Iima, Makoto; Ueda, Tetsuo; Nishiura, Yasumasa; Saigusa, Tetsu; Tero, Atsushi; Kobayashi, Ryo; Showalter, Kenneth

2007-08-01

When two food sources are presented to the slime mold Physarum in the dark, a thick tube for absorbing nutrients is formed that connects the food sources through the shortest route. When the light-avoiding organism is partially illuminated, however, the tube connecting the food sources follows a different route. Defining risk as the experimentally measurable rate of light-avoiding movement, the minimum-risk path is exhibited by the organism, determined by integrating along the path. A model for an adaptive-tube network is presented that is in good agreement with the experimental observations.

Preliminary analysis of problem of determining experimental performance of air-cooled turbine II : methods for determining cooling-air-flow characteristics

NASA Technical Reports Server (NTRS)

Ellerbrock, Herman H , Jr

1950-01-01

In the determination of the performance of an air-cooled turbine, the cooling-air-flow characteristics between the root and the tip of the blades must be evaluated. The methods, which must be verified and the unknown functions evaluated, that are expected to permit the determination of pressure, temperature, and velocity through the blade cooling-air passages from specific investigation are presented.

Numerical analysis and experimental research of the rubber boot of the joint drive vehicle

NASA Astrophysics Data System (ADS)

Ziobro, Jan

2016-04-01

The article presents many numerical studies and experimental research of the drive rubber boot of the joint drive vehicle. Performance requirements have been discussed and the required coefficients of the mathematical model for numerical simulation have been determined. The behavior of living in MSC.MARC environment was examined. In the analysis the following have been used: hyperplastic two-parameter model of the Mooney-Rivlin material, large displacements procedure, safe contact condition, friction on the sides of the boots. 3D numerical model of the joint bootwas analyzed under influence of the forces: tensile, compressive, centrifugal and angular. Numerous results of studies have been presented. An appropriate test stand was built and comparison of the results of the numerical analysis and the results of experimental studies was made. Numerous requests and recommendations for utilitarian character have been presented.

Real-time determination of laser beam quality by modal decomposition.

PubMed

Schmidt, Oliver A; Schulze, Christian; Flamm, Daniel; Brüning, Robert; Kaiser, Thomas; Schröter, Siegmund; Duparré, Michael

2011-03-28

We present a real-time method to determine the beam propagation ratio M2 of laser beams. The all-optical measurement of modal amplitudes yields M2 parameters conform to the ISO standard method. The experimental technique is simple and fast, which allows to investigate laser beams under conditions inaccessible to other methods.

’Coxiella Burnetii’ Vaccine Development: Lipopolysaccharide Structural Analysis

DTIC Science & Technology

1991-02-20

Analytical instrumentation and methodology is presented for the determination of endotoxin -related structures at much improved sensitivity and... ENDOTOXIN CHARACTERIZATION BY SFC .......................... 10 III. COXIELLA BURNETII LPS CHARACTERIZATION A. EXPERIMENTAL...period for the determination of endotoxin -related structures at much improved sensitivity and specificity. Reports, and their applications, are listed in

Colorimetric Determination of pH.

ERIC Educational Resources Information Center

Tucker, Sheryl; And Others

1989-01-01

Presented is an activity in which the pH of a solution can be quantitatively measured using a spectrophotometer. The theory, experimental details, sample preparation and selection, instrumentation, and results are discussed. (CW)

On use of ZPR research reactors and associated instrumentation and measurement methods for reactor physics studies

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chauvin, J.P.; Blaise, P.; Lyoussi, A.

2015-07-01

The French atomic and alternative energies -CEA- is strongly involved in research and development programs concerning the use of nuclear energy as a clean and reliable source of energy and consequently is working on the present and future generation of reactors on various topics such as ageing plant management, optimization of the plutonium stockpile, waste management and innovative systems exploration. Core physics studies are an essential part of this comprehensive R and D effort. In particular, the Zero Power Reactor (ZPR) of CEA: EOLE, MINERVE and MASURCA play an important role in the validation of neutron (as well photon) physicsmore » calculation tools (codes and nuclear data). The experimental programs defined in the CEA's ZPR facilities aim at improving the calculation routes by reducing the uncertainties of the experimental databases. They also provide accurate data on innovative systems in terms of new materials (moderating and decoupling materials) and new concepts (ADS, ABWR, new MTR (e.g. JHR), GENIV) involving new fuels, absorbers and coolant materials. Conducting such interesting experimental R and D programs is based on determining and measuring main parameters of phenomena of interest to qualify calculation tools and nuclear data 'libraries'. Determining these parameters relies on the use of numerous and different experimental techniques using specific and appropriate instrumentation and detection tools. Main ZPR experimental programs at CEA, their objectives and challenges will be presented and discussed. Future development and perspectives regarding ZPR reactors and associated programs will be also presented. (authors)« less

PCV2 Vaccination Prevented Clinical PCVAD and Reduced PCV2 Viremia and Semen Shedding in Boars Concurrently Infected with PCV2b and Mycoplasma hyopneumoiae

USDA-ARS?s Scientific Manuscript database

Introduction. It has been determined that porcine circovirus type 2 (PCV2) DNA is shed in semen of naturally and experimentally infected boars (1). Recently, it also has been shown that PCV2 DNA present in semen is infectious in a swine bioassay model (2). However, under experimental conditions the ...

A Novel Method for Producing Light GMT Sheets by a Pneumatic Technique

NASA Astrophysics Data System (ADS)

Dai, H.-L.; Rao, Y.-N.

2015-09-01

A novel method for producing a kind of light glass-mat- reinforced thermoplastic (GMT) sheets by using a pneumatic technique is presented. The tensile and flexural properties of produced light GMT sheets, with various lengths of glass fibers and PP content, were determined experimentally. Results of the experimental investigation show that the light GMT sheets are fully suitable for engineering applications.

Determination of absorption coefficient based on laser beam thermal blooming in gas-filled tube.

PubMed

Hafizi, B; Peñano, J; Fischer, R; DiComo, G; Ting, A

2014-08-01

Thermal blooming of a laser beam propagating in a gas-filled tube is investigated both analytically and experimentally. A self-consistent formulation taking into account heating of the gas and the resultant laser beam spreading (including diffraction) is presented. The heat equation is used to determine the temperature variation while the paraxial wave equation is solved in the eikonal approximation to determine the temporal and spatial variation of the Gaussian laser spot radius, Gouy phase (longitudinal phase delay), and wavefront curvature. The analysis is benchmarked against a thermal blooming experiment in the literature using a CO₂ laser beam propagating in a tube filled with air and propane. New experimental results are presented in which a CW fiber laser (1 μm) propagates in a tube filled with nitrogen and water vapor. By matching laboratory and theoretical results, the absorption coefficient of water vapor is found to agree with calculations using MODTRAN (the MODerate-resolution atmospheric TRANsmission molecular absorption database) and HITRAN (the HIgh-resolution atmospheric TRANsmission molecular absorption database).

Experimental determination of Ramsey numbers.

PubMed

Bian, Zhengbing; Chudak, Fabian; Macready, William G; Clark, Lane; Gaitan, Frank

2013-09-27

Ramsey theory is a highly active research area in mathematics that studies the emergence of order in large disordered structures. Ramsey numbers mark the threshold at which order first appears and are extremely difficult to calculate due to their explosive rate of growth. Recently, an algorithm that can be implemented using adiabatic quantum evolution has been proposed that calculates the two-color Ramsey numbers R(m,n). Here we present results of an experimental implementation of this algorithm and show that it correctly determines the Ramsey numbers R(3,3) and R(m,2) for 4≤m≤8. The R(8,2) computation used 84 qubits of which 28 were computational qubits. This computation is the largest experimental implementation of a scientifically meaningful adiabatic evolution algorithm that has been done to date.

Experimental Determination of Ramsey Numbers

NASA Astrophysics Data System (ADS)

Bian, Zhengbing; Chudak, Fabian; Macready, William G.; Clark, Lane; Gaitan, Frank

2013-09-01

Ramsey theory is a highly active research area in mathematics that studies the emergence of order in large disordered structures. Ramsey numbers mark the threshold at which order first appears and are extremely difficult to calculate due to their explosive rate of growth. Recently, an algorithm that can be implemented using adiabatic quantum evolution has been proposed that calculates the two-color Ramsey numbers R(m,n). Here we present results of an experimental implementation of this algorithm and show that it correctly determines the Ramsey numbers R(3,3) and R(m,2) for 4≤m≤8. The R(8,2) computation used 84 qubits of which 28 were computational qubits. This computation is the largest experimental implementation of a scientifically meaningful adiabatic evolution algorithm that has been done to date.

Thermally induced transverse cracking in graphite-epoxy cross-ply laminates

NASA Technical Reports Server (NTRS)

Adams, D. S.; Bowles, D. E.; Herakovich, C. T.

1986-01-01

Thermally induced transverse cracking in T300/5208 graphite-epoxy cross-ply laminates was investigated experimentally and theoretically. The six laminate configurations studied were: 0/90(3)s, 0(2)/90(2)s, 0(3)/90s, 90/0(3)s, 90(2)/0(2)s, and 90(3)/0s. The thermal load required to initiate transverse cracking was determined experimentally and compared to a theoretical prediction. Experimental results for the accumulation of transverse cracks under cyclic thermal loading between - 250 and 250 F for up to 500 thermal cycles are presented. The calculated in situ transverse-lamina strength was determined to be at least 1.9 times the unidirectional-lamina transverse tensile strength. All laminate configurations exhibited an increase in crack density with increasing thermal cycles.

Determining the Products of Inertia for Small Scale UAVs

NASA Technical Reports Server (NTRS)

Lorenzetti, Joseph S.; Banuelos, Leonel C.; Clarke, Robert; Murillo, Oscar J.; Bowers, Albion H.

2017-01-01

Moments of inertia and products of inertia often need to be determined for aircraft. As complex bodies, their mass properties need to be determined experimentally for best accuracy. While several moment of inertia experimental techniques have been developed, there are few to determine the products of inertia. Products of inertia can be easily determined mathematically if the angle between the aircraft x body axis and principal x axis is known. This method finds the principal inclination angle by mathematically correlating the measured moments of inertia about a range of axes of the aircraft. This correlation uses a least squares error minimization of a mathematical model that describes the ellipse of inertia in the aircraft's x-z axes plane. Results from a test conducted on a small scale UAV (Unmanned Aerial Vehicle) at NASA Armstrong Flight Research Center is also presented, which is an example of the intended application of this technique.

Activation cross-sections of proton induced reactions on vanadium in the 37-65 MeV energy range

NASA Astrophysics Data System (ADS)

Ditrói, F.; Tárkányi, F.; Takács, S.; Hermanne, A.

2016-08-01

Experimental excitation functions for proton induced reactions on natural vanadium in the 37-65 MeV energy range were measured with the activation method using a stacked foil irradiation technique. By using high resolution gamma spectrometry cross-section data for the production of 51,48Cr, 48V, 48,47,46,44m,44g,43Sc and 43,42K were determined. Comparisons with the earlier published data are presented and results predicted by different theoretical codes (EMPIRE and TALYS) are included. Thick target yields were calculated from a fit to our experimental excitation curves and compared with the earlier experimental yield data. Depth distribution curves to be used for thin layer activation (TLA) are also presented.

Investigations on Torsion of the Two-Chords Single Laced Members

NASA Astrophysics Data System (ADS)

Lorkowski, Paweł; Gosowski, Bronisław

2017-06-01

The paper presents experimental and numerical studies to determine the equivalent second moment of area of the uniform torsion of the two-chord steel single laced members. The members are used as poles of railway traction network gates, and steel columns of framed buildings as well. The stiffness of uniform torsion of this kind of columns allows to the determine the critical loads of the spatial stability. The experimental studies have been realized on a single - span members with rotation arrested at their ends, loaded by a torque applied at the mid-span. The relationship between angle of rotation of the considered cross-section and the torque has been determined. Appropriate numerical model was created in the ABAQUS program, based on the finite element method. A very good compatibility has been observed between experimental and numerical studies. The equivalent second moment of area of the uniform torsion for analysed members has been determined by comparing the experimental and analytical results to those obtained from differential equation of non-uniform torsion, based on Vlasov's theory. Additionally, the parametric analyses of similar members subjected to the uniform torsion, for the richer range of cross-sections have been carried out by the means of SOFiSTiK program. The purpose of the latter was determining parametrical formulas for calculation of the second moment of area of uniform torsion.

Thermal Output of WK-Type Strain Gauges on Various Materials at Cryogenic and Elevated Temperatures

NASA Technical Reports Server (NTRS)

Kowalkowski, Matthew K.; Rivers, H. Kevin; Smith, Russell W.

1998-01-01

Strain gage apparent strain (thermal output) is one of the largest sources of error associated with the measurement of strain when temperatures and mechanical loads are varied. In this paper, experimentally determined apparent strains of WK-type strain gages, installed on both metallic and composite-laminate materials of various lay-ups and resin systems for temperatures ranging from -450 F to 230 F are presented. For the composite materials apparent strain in both the 0 ply orientation angle and the 90 ply orientation angle were measured. Metal specimens tested included: aluminum-lithium alloy (Al-LI 2195-T87), aluminum alloy (Al 2219-T87), and titanium alloy. Composite materials tested include: graphite-toughened-epoxy (IM7/997- 2), graphite-bismaleimide (IM7/5260), and graphite-K3 (IM7/K3B). The experimentally determined apparent strain data are curve fit with a fourth-order polynomial for each of the materials studied. The apparent strain data and the polynomials that are fit to the data are compared with those produced by the strain gage manufacturer, and the results and comparisons are presented. Unacceptably high errors between the manufacture's data and the experimentally determined data were observed (especially at temperatures below - 270-F).

Evolution of deformation in neutron-rich Ba isotopes up to A =150

NASA Astrophysics Data System (ADS)

Licǎ, R.; Benzoni, G.; Rodríguez, T. R.; Borge, M. J. G.; Fraile, L. M.; Mach, H.; Morales, A. I.; Madurga, M.; Sotty, C. O.; Vedia, V.; De Witte, H.; Benito, J.; Bernard, R. N.; Berry, T.; Bracco, A.; Camera, F.; Ceruti, S.; Charviakova, V.; Cieplicka-Oryńczak, N.; Costache, C.; Crespi, F. C. L.; Creswell, J.; Fernandez-Martínez, G.; Fynbo, H.; Greenlees, P. T.; Homm, I.; Huyse, M.; Jolie, J.; Karayonchev, V.; Köster, U.; Konki, J.; Kröll, T.; Kurcewicz, J.; Kurtukian-Nieto, T.; Lazarus, I.; Lund, M. V.; Mǎrginean, N.; Mǎrginean, R.; Mihai, C.; Mihai, R. E.; Negret, A.; Orduz, A.; Patyk, Z.; Pascu, S.; Pucknell, V.; Rahkila, P.; Rapisarda, E.; Regis, J. M.; Robledo, L. M.; Rotaru, F.; Saed-Samii, N.; Sánchez-Tembleque, V.; Stanoiu, M.; Tengblad, O.; Thuerauf, M.; Turturica, A.; Van Duppen, P.; Warr, N.; IDS Collaboration

2018-02-01

The occurrence of octupolar shapes in the Ba isotopic chain was recently established experimentally up to N =90 . To further extend the systematics, the evolution of shapes in the most neutron-rich members of the Z =56 isotopic chain accessible at present, Ba,150148, has been studied via β decay at the ISOLDE Decay Station. This paper reports on the first measurement of the positive- and negative-parity low-spin excited states of 150Ba and presents an extension of the β -decay scheme of 148Cs. Employing the fast timing technique, half-lives for the 21+ level in both nuclei have been determined, resulting in T1 /2=1.51 (1 ) ns for 148Ba and T1 /2=3.4 (2 ) ns for 150Ba. The systematics of low-spin states, together with the experimental determination of the B (E 2 :2+→0+) transition probabilities, indicate an increasing collectivity in Ba-150148, towards prolate deformed shapes. The experimental data are compared to symmetry conserving configuration mixing (SCCM) calculations, confirming an evolution of increasingly quadrupole deformed shapes with a definite octupolar character.

Predicted Turbine Heat Transfer for a Range of Test Conditions

NASA Technical Reports Server (NTRS)

Boyle, R. J.; Lucci, B. L.

1996-01-01

Comparisons are shown between predictions and experimental data for blade and endwall heat transfer. The comparisons of computational domain parisons are given for both vane and rotor geometries over an extensive range of Reynolds and Mach numbers. Comparisons are made with experimental data from a variety of sources. A number of turbulence models are available for predicting blade surface heat transfer, as well as aerodynamic performance. The results of an investigation to determine the turbulence model which gives the best agreement with experimental data over a wide range of test conditions are presented.

Assessing the Role of Anhydrite in the KT Mass Extinction: Hints from Shock-loading Experiments

NASA Technical Reports Server (NTRS)

Skala, R.; Lnagenhorst, F.; Hoerz, F.

2004-01-01

Various killing mechanisms have been suggested to contribute to the mass extinctions at the KT boundary, including severe, global deterioration of the atmosphere and hydrosphere due to SO(x) released from heavily shocked, sulfate-bearing target rocks. The devolatilization of anhydrite is predominantly inferred from thermodynamic considerations and lacks experimental confirmation. To date, the experimentally determined shock behavior of anhydrite is limited to solid-state effects employing X-ray diffraction methods. The present report employs additional methods to characterize experimentally shocked anhydrite.

Experimental study on the resonance frequencies of a cantilevered plate in air flow

NASA Astrophysics Data System (ADS)

Cros, Anne; Arellano Castro, Rocío F.

2016-02-01

The present experimental work focuses on the resonances exhibited by a cantilevered plate immersed in airflow. The flexible plate is clamped at its leading edge and submitted to a small, lateral harmonic displacement. Throughout this work, our two control parameters are the forcing frequency and the air velocity. We determine experimentally the evolution of the first three resonant frequencies as air velocity is increased. Our results are in agreement with the Eloy et al. (2007) [1] and Michelin and Llewellyn-Smith (2009) [2] linear theoretical predictions.

Experimental Determination of Unknown Masses and Their Positions in a Mechanical Black Box

ERIC Educational Resources Information Center

Chakrabarti, Bhupati; Pathare, Shirish; Huli, Saurabhee; Nachane, Madhura

2013-01-01

An experiment with a mechanical black box containing unknown masses is presented. The experiment involves the determination of these masses and their locations by performing some nondestructive tests. The set-ups are inexpensive and easy to fabricate. They are very useful to gain an understanding of some well-known principles of mechanics.

Effect of formulated glyphosate and adjuvant tank mixes on atomization from aerial application flat fan nozzles

USDA-ARS?s Scientific Manuscript database

This study was designed to determine if the present USDA ARS Spray Nozzle models based on water plus non-ionic surfactant spray solutions could be used to estimate spray droplet size data for different spray formulations through use of experimentally determined correction factors or if full spray fo...

A Simple Method for Determination of the Density of Granular Materials

ERIC Educational Resources Information Center

Tsutsumanova, G. G.; Kirilov, K. M.; Russev, S. C.

2012-01-01

A simple experiment using low cost equipment for the determination of the density of granular materials, without immersing them in a liquid, is presented. It is based only on the ideal gas state equation, so it is a good experimental task for undergraduate and high school students. (Contains 2 tables and 5 figures.)

Angles-only, ground-based, initial orbit determination

NASA Astrophysics Data System (ADS)

Taff, L. G.; Randall, P. M. S.; Stansfield, S. A.

1984-05-01

Over the past few years, passive, ground-based, angles-only initial orbit determination has had a thorough analytical, numerical, experimental, and creative re-examination. This report presents the numerical culmination of this effort and contains specific recommendations for which of several techniques one should use on the different subsets of high altitude artificial satellites and minor planets.

Determining the wavelength spectrum of neutrons on the NG6 beam line at NCNR

NASA Astrophysics Data System (ADS)

Ivanov, Juliet

2016-09-01

Historically, in-beam experiments and bottle experiments have been performed to determine the lifetime of a free neutron. However, these two different experimental techniques have provided conflicting results. It is crucial to precisely and accurately elucidate the neutron lifetime for Big Bang Nucleosynthesis calculations and to investigate physics beyond the Standard Model. Therefore, we aimed to understand and minimize systematic errors present in the neutron beam experiment at the NIST Center for Neutron Research (NCNR). In order to reduce the uncertainty related to wavelength dependent corrections present in previous beam experiments, the wavelength spectrum of the NCNR reactor cold neutron beam must be known. We utilized a beam chopper and lithium detector to characterize the wavelength spectrum on the NG6 beam line at the NCNR. The experimental design and techniques employed will be discussed, and our results will be presented. Future plans to utilize our findings to improve the neutron lifetime measurement at NCNR will also be described.

A new scenario-based approach to damage detection using operational modal parameter estimates

NASA Astrophysics Data System (ADS)

Hansen, J. B.; Brincker, R.; López-Aenlle, M.; Overgaard, C. F.; Kloborg, K.

2017-09-01

In this paper a vibration-based damage localization and quantification method, based on natural frequencies and mode shapes, is presented. The proposed technique is inspired by a damage assessment methodology based solely on the sensitivity of mass-normalized experimental determined mode shapes. The present method differs by being based on modal data extracted by means of Operational Modal Analysis (OMA) combined with a reasonable Finite Element (FE) representation of the test structure and implemented in a scenario-based framework. Besides a review of the basic methodology this paper addresses fundamental theoretical as well as practical considerations which are crucial to the applicability of a given vibration-based damage assessment configuration. Lastly, the technique is demonstrated on an experimental test case using automated OMA. Both the numerical study as well as the experimental test case presented in this paper are restricted to perturbations concerning mass change.

Determination of full piezoelectric complex parameters using gradient-based optimization algorithm

NASA Astrophysics Data System (ADS)

Kiyono, C. Y.; Pérez, N.; Silva, E. C. N.

2016-02-01

At present, numerical techniques allow the precise simulation of mechanical structures, but the results are limited by the knowledge of the material properties. In the case of piezoelectric ceramics, the full model determination in the linear range involves five elastic, three piezoelectric, and two dielectric complex parameters. A successful solution to obtaining piezoceramic properties consists of comparing the experimental measurement of the impedance curve and the results of a numerical model by using the finite element method (FEM). In the present work, a new systematic optimization method is proposed to adjust the full piezoelectric complex parameters in the FEM model. Once implemented, the method only requires the experimental data (impedance modulus and phase data acquired by an impedometer), material density, geometry, and initial values for the properties. This method combines a FEM routine implemented using an 8-noded axisymmetric element with a gradient-based optimization routine based on the method of moving asymptotes (MMA). The main objective of the optimization procedure is minimizing the quadratic difference between the experimental and numerical electrical conductance and resistance curves (to consider resonance and antiresonance frequencies). To assure the convergence of the optimization procedure, this work proposes restarting the optimization loop whenever the procedure ends in an undesired or an unfeasible solution. Two experimental examples using PZ27 and APC850 samples are presented to test the precision of the method and to check the dependency of the frequency range used, respectively.

Smartphones as Experimental Tools: Different Methods to Determine the Gravitational Acceleration in Classroom Physics by Using Everyday Devices

ERIC Educational Resources Information Center

Kuhn, Jochen; Vogt, Patrik

2013-01-01

New media technology becomes more and more important for our daily life as well as for teaching physics. Within the scope of our N.E.T. research project we develop experiments using New Media Experimental Tools (N.E.T.) in physics education and study their influence on students learning abilities. We want to present the possibilities e.g. of…

A Computer Simulation for Teaching Diagnosis of Secondary Ignition Problems

ERIC Educational Resources Information Center

Diedrick, Walter; Thomas, Rex

1977-01-01

Presents the methodology and findings of an experimental project to determine the viability of computer assisted as opposed to more traditional methods of instruction for teaching one phase of automotive troubleshooting. (Editor)

Ignition of metals in high pressure oxygen

NASA Technical Reports Server (NTRS)

Bransford, J. W.

1985-01-01

A description of an experimental facility used to determine the ignition and combustion characteristics of metallic materials is given. The results obtained for aluminum 6061, 302 stainless steel, and the nickel alloy - N06625 are presented.

Supercritical Fluid: Liquid, Gas, Both or Neither? A Different Approach.

ERIC Educational Resources Information Center

Meyer, Edwin F.; Meyer, Thomas P.

1986-01-01

Presents a laboratory experiment which determines critical temperature and density of carbon dioxide. Discusses critical point and provides equations to estimate liquid volume fraction. Analyzes experimental results in terms of variables. (JM)

Investigations of the possibility of determination of thermal parameters of Si and SiGe samples based on the Photo Thermal Radiometry technique

NASA Astrophysics Data System (ADS)

Chrobak, Ł.; Maliński, M.

2018-03-01

This paper presents results of investigations of the possibility of determination of thermal parameters (thermal conductivity, thermal diffusivity) of silicon and silicon germanium crystals from the frequency characteristics of the Photo Thermal Radiometry (PTR) signal. The theoretical analysis of the influence of the mentioned parameters on the PTR signal has been presented and discussed. The values of the thermal and recombination parameters have been extracted from the fittings of the theoretical to experimental data. The presented approach uses the reference Si sample whose thermal and recombination parameters are known.

Blurring out hydrogen: The dynamical structure of teflic acid

NASA Astrophysics Data System (ADS)

Herbers, S.; Obenchain, D. A.; Kraus, P.; Wachsmuth, D.; Grabow, J.-U.

2018-05-01

The microwave spectra of 10 teflic acid isotopologues were recorded in the frequency range of 3-25 GHz using supersonic jet-expansion Fourier transform microwave spectroscopy. Despite being asymmetric in its equilibrium structure, the delocalization of the hydrogen atom leads to a symmetric top vibrational ground state structure. In this work, we present the zero point structure obtained from the experimental rotational constants and an approach to determine the semi-experimental equilibrium structure aided by ab initio data. The Te-O bond length determined in the equilibrium structure is accurate to the picometer and can be used as a benchmark for computational methods treating relativistic effects.

Forming limit curves of DP600 determined in high-speed Nakajima tests and predicted by two different strain-rate-sensitive models

NASA Astrophysics Data System (ADS)

Weiß-Borkowski, Nathalie; Lian, Junhe; Camberg, Alan; Tröster, Thomas; Münstermann, Sebastian; Bleck, Wolfgang; Gese, Helmut; Richter, Helmut

2018-05-01

Determination of forming limit curves (FLC) to describe the multi-axial forming behaviour is possible via either experimental measurements or theoretical calculations. In case of theoretical determination, different models are available and some of them consider the influence of strain rate in the quasi-static and dynamic strain rate regime. Consideration of the strain rate effect is necessary as many material characteristics such as yield strength and failure strain are affected by loading speed. In addition, the start of instability and necking depends not only on the strain hardening coefficient but also on the strain rate sensitivity parameter. Therefore, the strain rate dependency of materials for both plasticity and the failure behaviour is taken into account in crash simulations for strain rates up to 1000 s-1 and FLC can be used for the description of the material's instability behaviour at multi-axial loading. In this context, due to the strain rate dependency of the material behaviour, an extrapolation of the quasi-static FLC to dynamic loading condition is not reliable. Therefore, experimental high-speed Nakajima tests or theoretical models shall be used to determine the FLC at high strain rates. In this study, two theoretical models for determination of FLC at high strain rates and results of experimental high-speed Nakajima tests for a DP600 are presented. One of the theoretical models is the numerical algorithm CRACH as part of the modular material and failure model MF GenYld+CrachFEM 4.2, which is based on an initial imperfection. Furthermore, the extended modified maximum force criterion considering the strain rate effect is also used to predict the FLC. These two models are calibrated by the quasi-static and dynamic uniaxial tensile tests and bulge tests. The predictions for the quasi-static and dynamic FLC by both models are presented and compared with the experimental results.

Hysteresis of liquid adsorption in porous media by coarse-grained Monte Carlo with direct experimental validation

NASA Astrophysics Data System (ADS)

Zeidman, Benjamin D.; Lu, Ning; Wu, David T.

2016-05-01

The effects of path-dependent wetting and drying manifest themselves in many types of physical systems, including nanomaterials, biological systems, and porous media such as soil. It is desirable to better understand how these hysteretic macroscopic properties result from a complex interplay between gasses, liquids, and solids at the pore scale. Coarse-Grained Monte Carlo (CGMC) is an appealing approach to model these phenomena in complex pore spaces, including ones determined experimentally. We present two-dimensional CGMC simulations of wetting and drying in two systems with pore spaces determined by sections from micro X-ray computed tomography: a system of randomly distributed spheres and a system of Ottawa sand. Results for the phase distribution, water uptake, and matric suction when corrected for extending to three dimensions show excellent agreement with experimental measurements on the same systems. This supports the hypothesis that CGMC can generate metastable configurations representative of experimental hysteresis and can also be used to predict hysteretic constitutive properties of particular experimental systems, given pore space images.

Hysteresis of liquid adsorption in porous media by coarse-grained Monte Carlo with direct experimental validation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zeidman, Benjamin D.; Lu, Ning; Wu, David T., E-mail: dwu@mines.edu

2016-05-07

The effects of path-dependent wetting and drying manifest themselves in many types of physical systems, including nanomaterials, biological systems, and porous media such as soil. It is desirable to better understand how these hysteretic macroscopic properties result from a complex interplay between gasses, liquids, and solids at the pore scale. Coarse-Grained Monte Carlo (CGMC) is an appealing approach to model these phenomena in complex pore spaces, including ones determined experimentally. We present two-dimensional CGMC simulations of wetting and drying in two systems with pore spaces determined by sections from micro X-ray computed tomography: a system of randomly distributed spheres andmore » a system of Ottawa sand. Results for the phase distribution, water uptake, and matric suction when corrected for extending to three dimensions show excellent agreement with experimental measurements on the same systems. This supports the hypothesis that CGMC can generate metastable configurations representative of experimental hysteresis and can also be used to predict hysteretic constitutive properties of particular experimental systems, given pore space images.« less

Experimental Validation of Strategy for the Inverse Estimation of Mechanical Properties and Coefficient of Friction in Flat Rolling

NASA Astrophysics Data System (ADS)

Yadav, Vinod; Singh, Arbind Kumar; Dixit, Uday Shanker

2017-08-01

Flat rolling is one of the most widely used metal forming processes. For proper control and optimization of the process, modelling of the process is essential. Modelling of the process requires input data about material properties and friction. In batch production mode of rolling with newer materials, it may be difficult to determine the input parameters offline. In view of it, in the present work, a methodology to determine these parameters online by the measurement of exit temperature and slip is verified experimentally. It is observed that the inverse prediction of input parameters could be done with a reasonable accuracy. It was also assessed experimentally that there is a correlation between micro-hardness and flow stress of the material; however the correlation between surface roughness and reduction is not that obvious.

Contact Forces between Single Metal Oxide Nanoparticles in Gas-Phase Applications and Processes.

PubMed

Salameh, Samir; van der Veen, Monique A; Kappl, Michael; van Ommen, J Ruud

2017-03-14

In this work we present a comprehensive experimental study to determine the contact forces between individual metal oxide nanoparticles in the gas-phase using atomic force microscopy. In addition, we determined the amount of physisorbed water for each type of particle surface. By comparing our results with mathematical models of the interaction forces, we could demonstrate that classical continuum models of van der Waals and capillary forces alone cannot sufficiently describe the experimental findings. Rather, the discrete nature of the molecules has to be considered, which leads to ordering at the interface and the occurrence of solvation forces. We demonstrate that inclusion of solvation forces in the model leads to quantitative agreement with experimental data and that tuning of the molecular order by addition of isopropanol vapor allows us to control the interaction forces between the nanoparticles.

Determination of 200 °C Isothermal Section of Al-Ag-Ga Phase Diagram by Microanalysis, X-ray Diffraction, Hardness and Electrical Conductivity Measurements

NASA Astrophysics Data System (ADS)

Premović, Milena; Tomović, Milica; Minić, Duško; Manasijević, Dragan; Živković, Dragana; Ćosović, Vladan; Grković, Vladan; Đorđević, Aleksandar

2017-04-01

Ternary Al-Ag-Ga system at 200 °C was experimentally and thermodynamically assessed. Isothermal section was extrapolated using optimized thermodynamic parameters for constitutive binary systems. Microstructure and phase composition of the selected alloy samples were analyzed using light microscopy, scanning electron microscopy combined with energy-dispersive spectrometry and x-ray powder diffraction technique. The obtained experimental results were found to be in a close agreement with the predicted phase equilibria. Hardness and electrical conductivity of the alloy samples from four vertical sections Al-Ag80Ga20, Al-Ag60Ga40, Ag-Al80Ga20 and Ag-Al60Ga40 of the ternary Al-Ag-Ga system at 200 °C were experimentally determined using Brinell method and eddy current measurements. Additionally, hardness of the individual phases present in the microstructure of the studied alloy samples was determined using Vickers microhardness test. Based on experimentally obtained results, isolines of Brinell hardness and electrical conductivity were calculated for the alloys from isothermal section of the ternary Al-Ag-Ga system at 200 °C.

Fluid Merging Viscosity Measurement (FMVM) Experiment on the International Space Station

NASA Technical Reports Server (NTRS)

Antar, Basil N.; Ethridge, Edwin; Lehman, Daniel; Kaukler, William

2007-01-01

The concept of using low gravity experimental data together with fluid dynamical numerical simulations for measuring the viscosity of highly viscous liquids was recently validated on the International Space Station (ISS). After testing the proof of concept for this method with parabolic flight experiments, an ISS experiment was proposed and later conducted onboard the ISS in July, 2004 and subsequently in May of 2005. In that experiment a series of two liquid drops were brought manually together until they touched and then were allowed to merge under the action of capillary forces alone. The merging process was recorded visually in order to measure the contact radius speed as the merging proceeded. Several liquids were tested and for each liquid several drop diameters were used. It has been shown that when the coefficient of surface tension for the liquid is known, the contact radius speed can then determine the coefficient of viscosity for that liquid. The viscosity is determined by fitting the experimental speed to theoretically calculated contact radius speed for the same experimental parameters. Experimental and numerical results will be presented in which the viscosity of different highly viscous liquids were determined, to a high degree of accuracy, using this technique.

Thoron-meso-tartaric acid system for determination of thorium

USGS Publications Warehouse

Fletcher, M.H.; Grimaldi, F.S.; Jenkins, L.B.

1957-01-01

In the spectrophotometric determination of thorium with thoron, mesotartaric acid is used as a masking reagent for zirconium. The effects of different experimental variables such as the concentrations of the reagents, time, and temperature, and the behavior of 35 ions which might be present in thorium ores are discussed. A dilution procedure is given for the direct determination of thorium in zircon (ZrSiO4) that is also generally applicable to other materials.

Effects of Hydrolysis on Determining the Solubility Product of Potassium Bitartrate

ERIC Educational Resources Information Center

McNaught, Ian J.; Peckham, Gavin D.

2009-01-01

The method given in many publications for calculating the solubility product of potassium bitartrate is wrong in principle. A way of modifying the experimental approach and calculations to overcome the problem are presented.

Method for determining optimal supercell representation of interfaces

NASA Astrophysics Data System (ADS)

Stradi, Daniele; Jelver, Line; Smidstrup, Søren; Stokbro, Kurt

2017-05-01

The geometry and structure of an interface ultimately determines the behavior of devices at the nanoscale. We present a generic method to determine the possible lattice matches between two arbitrary surfaces and to calculate the strain of the corresponding matched interface. We apply this method to explore two relevant classes of interfaces for which accurate structural measurements of the interface are available: (i) the interface between pentacene crystals and the (1 1 1) surface of gold, and (ii) the interface between the semiconductor indium-arsenide and aluminum. For both systems, we demonstrate that the presented method predicts interface geometries in good agreement with those measured experimentally, which present nontrivial matching characteristics and would be difficult to guess without relying on automated structure-searching methods.

Flow injection analysis simulations and diffusion coefficient determination by stochastic and deterministic optimization methods.

PubMed

Kucza, Witold

2013-07-25

Stochastic and deterministic simulations of dispersion in cylindrical channels on the Poiseuille flow have been presented. The random walk (stochastic) and the uniform dispersion (deterministic) models have been used for computations of flow injection analysis responses. These methods coupled with the genetic algorithm and the Levenberg-Marquardt optimization methods, respectively, have been applied for determination of diffusion coefficients. The diffusion coefficients of fluorescein sodium, potassium hexacyanoferrate and potassium dichromate have been determined by means of the presented methods and FIA responses that are available in literature. The best-fit results agree with each other and with experimental data thus validating both presented approaches. Copyright © 2013 The Author. Published by Elsevier B.V. All rights reserved.

EPR spectral investigation of radiation-induced radicals of gallic acid.

PubMed

Tuner, Hasan

2017-11-01

In the present work, spectroscopic features of the radiation-induced radicals of gallic acid compounds were investigated using electron paramagnetic resonance (EPR) spectroscopy. While un-irradiated samples presented no EPR signal, irradiated samples exhibited an EPR spectrum consisting of an intense resonance line at the center and weak lines on both sides. Detailed microwave saturation investigations were carried out to determine the origin of the experimental EPR lines. It is concluded that the two side lines of the triplet satellite originate from forbidden "spin-flip" transitions. The spectroscopic and structural features of the radiation-induced radicals were determined using EPR spectrum fittings. The experimental EPR spectra of the two gallic acid compounds were consistent with the calculated EPR spectroscopic features of the proposed radicals. It is concluded that the most probable radicals are the cyclohexadienyl-type, [Formula: see text] radicals for both compounds.

Acoustic composition sensor for cryogenic gas mixtures

NASA Technical Reports Server (NTRS)

Shakkottai, P.; Kwack, E. Y.; Luchik, T. S.; Back, L. H.

1991-01-01

An acoustic sensor useful for the determination of the composition of a gaseous binary mixture in cryogenic liquid spills has been characterized. One version of the instrument traps a known mixture of helium and nitrogen at ambient temperature in a tube which is interrogated by sonic pulses to determine the speed of sound and hence the composition. Experimental data shows that this sensor is quite accurate. The second version uses two unconfined microphones which sense sound pulses. Experimental data acquired during mixing when liquid nitrogen is poured into a vessel of gaseous helium is presented. Data during transient cooling of the tubular sensor containing nitrogen when the sensor is dipped into liquid nitrogen and during transient warm-up when the sensor is withdrawn are also presented. This sensor is being developed for use in the mixing of liquid cryogens with gas evolution in the simulation of liquid hydrogen/liquid oxygen explosion hazards.

Acoustic composition sensor for cryogenic gas mixtures

NASA Astrophysics Data System (ADS)

Shakkottai, P.; Kwack, E. Y.; Luchik, T. S.; Back, L. H.

An acoustic sensor useful for the determination of the composition of a gaseous binary mixture in cryogenic liquid spills has been characterized. One version of the instrument traps a known mixture of helium and nitrogen at ambient temperature in a tube which is interrogated by sonic pulses to determine the speed of sound and hence the composition. Experimental data shows that this sensor is quite accurate. The second version uses two unconfined microphones which sense sound pulses. Experimental data acquired during mixing when liquid nitrogen is poured into a vessel of gaseous helium is presented. Data during transient cooling of the tubular sensor containing nitrogen when the sensor is dipped into liquid nitrogen and during transient warm-up when the sensor is withdrawn are also presented. This sensor is being developed for use in the mixing of liquid cryogens with gas evolution in the simulation of liquid hydrogen/liquid oxygen explosion hazards.

The Effect of Temperature on Moisture Transport in Concrete.

PubMed

Wang, Yao; Xi, Yunping

2017-08-09

Most concrete structures and buildings are under temperature and moisture variations simultaneously. Thus, the moisture transport in concrete is driven by the moisture gradient as well as the temperature gradient. This paper presents an experimental approach for determining the effect of different temperature gradients on moisture distribution profiles in concrete. The effect of elevated temperatures under isothermal conditions on the moisture transport was also evaluated, and found not to be significant. The non-isothermal tests show that the temperature gradient accelerates the moisture transport in concrete. The part of increased moisture transfer due to the temperature gradient can be quantified by a coupling parameter D HT , which can be determined by the present test data. The test results indicated that D HT is not a constant but increases linearly with the temperature variation. A material model was developed for D HT based on the experimental results obtained in this study.

The Effect of Temperature on Moisture Transport in Concrete

PubMed Central

Wang, Yao; Xi, Yunping

2017-01-01

Most concrete structures and buildings are under temperature and moisture variations simultaneously. Thus, the moisture transport in concrete is driven by the moisture gradient as well as the temperature gradient. This paper presents an experimental approach for determining the effect of different temperature gradients on moisture distribution profiles in concrete. The effect of elevated temperatures under isothermal conditions on the moisture transport was also evaluated, and found not to be significant. The non-isothermal tests show that the temperature gradient accelerates the moisture transport in concrete. The part of increased moisture transfer due to the temperature gradient can be quantified by a coupling parameter DHT, which can be determined by the present test data. The test results indicated that DHT is not a constant but increases linearly with the temperature variation. A material model was developed for DHT based on the experimental results obtained in this study. PMID:28792460

Prediction of sonic boom at a focus

NASA Technical Reports Server (NTRS)

Plotkin, K. J.; Cantril, J. M.

1976-01-01

The behavior of sonic boom at a focus has been reviewed for the purpose of extending present sonic boom computational methods to include focal zones. The geometry of a focal zone - whether a smooth caustic, a cusped caustic, or a perfect focus to a point - determines the character of focused signatures. The seeming contradiction of various experimental data can be resolved by noting these differences. A ray acoustic analysis has been developed for quantitative determination of caustic geometry. The only reliable theory presently available for signatures at a focus is for a smooth caustic. There has been some controversy between theoretical and experimental values of a constant in the scaling law for this case. It has been found that this discrepancy can be resolved by accounting for the finite thickness of real sonic boom shock waves. These findings have been incorporated into an existing sonic boom computer program.

Electron ionization and dissociation of aliphatic amino acids

NASA Astrophysics Data System (ADS)

Papp, P.; Shchukin, P.; Kočíšek, J.; Matejčík, Š.

2012-09-01

We present experimental and theoretical study of electron ionization and dissociative ionization to the gas phase amino acids valine, leucine, and isoleucine. A crossed electron/molecular beams technique equipped with quadrupole mass analyzer has been applied to measure mass spectra and ion efficiency curves for formation of particular ions. From experimental data the ionization energies of the molecules and the appearance energies of the fragment ions were determined. Ab initio calculations (Density Functional Theory and G3MP2 methods) were performed in order to calculate the fragmentation paths and interpret the experimental data. The experimental ionization energies of parent molecules [P]+ 8.91 ± 0.05, 8.85 ± 0.05, and 8.79 ± 0.05 eV and G3MP2 ionization energies (adiabatic) of 8.89, 8.88, and 8.81 eV were determined for valine, leucine, and isoleucine, respectively, as well as the experimental and theoretical threshold energies for dissociative ionization channels. The comparison of experimental data with calculations resulted in identification of the ions as well as the neutral fragments formed in the dissociative reactions. Around 15 mass/charge ratio fragments were identified from the mass spectra by comparison of experimental appearance energies with calculated reaction enthalpies for particular dissociative reactions.

Biomedical and Human Factors Requirements for a Manned Earth-Orbiting Station

NASA Technical Reports Server (NTRS)

Reynolds, J. B.

1963-01-01

The study reported here has presented a measurement data pool for the determination of biomedical and behavioral effects of long-term exposure to weightlessness. This includes measures, techniques, equipment, and requirements in terms of weight, power, volume, time, crew activities, subsystem interfaces and experimental programs and designs, and confidence ratings for their effectiveness for determining weightlessness effects.

Quantitative Determination of Aluminum in Deodorant Brands: A Guided Inquiry Learning Experience in Quantitative Analysis Laboratory

ERIC Educational Resources Information Center

Sedwick, Victoria; Leal, Anne; Turner, Dea; Kanu, A. Bakarr

2018-01-01

The monitoring of metals in commercial products is essential for protecting public health against the hazards of metal toxicity. This article presents a guided inquiry (GI) experimental lab approach in a quantitative analysis lab class that enabled students' to determine the levels of aluminum in deodorant brands. The utility of a GI experimental…

The Strength of Shell Bodies : Theory and Practice

NASA Technical Reports Server (NTRS)

Ebner, H

1937-01-01

The monocoque form of airplane construction has introduced a number of new problems to the stress calculator and the designer. The problems for the stress calculator fall into two groups: the determination of the stress condition (shell statics) and the determination of the failing strength (shell strength). The present report summarizes the most important theoretical and experimental results on this subject.

Effect of the RC time on photocurrent transients and determination of charge carrier mobilities

NASA Astrophysics Data System (ADS)

Kniepert, Juliane; Neher, Dieter

2017-11-01

We present a closed analytical model to describe time dependent photocurrents upon pulsed illumination in the presence of an external RC circuit. In combination with numerical drift diffusion simulations, it is shown that the RC time has a severe influence on the shape of the transients. In particular, the maximum of the photocurrent is delayed due to a delayed recharging of the electrodes. This delay increases with the increasing RC constant. As a consequence, charge carrier mobilities determined from simple extrapolation of the initial photocurrent decay will be in general too small and feature a false dependence on the electric field. Here, we present a recipe to correct charge carrier mobilities determined from measured photocurrent transients by taking into account the RC time of the experimental set-up. We also demonstrate how the model can be used to more reliably determine the charge carrier mobility from experimental data of a typical polymer/fullerene organic solar cell. It is shown that further aspects like a finite rising time of the pulse generator and the current contribution of the slower charger carriers influence the shape of the transients and may lead to an additional underestimation of the transit time.

Determination of the θ23 octant in long baseline neutrino experiments within and beyond the standard model

NASA Astrophysics Data System (ADS)

Das, C. R.; Pulido, João; Maalampi, Jukka; Vihonen, Sampsa

2018-02-01

The recent data indicate that the neutrino mixing angle θ23 deviates from the maximal-mixing value of 45°, showing two nearly degenerate solutions, one in the lower octant (LO) (θ23<4 5 ° ) and one in the higher octant (HO) (θ23>4 5 ° ). We investigate, using numerical simulations, the prospects for determining the octant of θ23 in the future long baseline oscillation experiments. We present our results as contour plots on the (θ23-4 5 ° , δ )-plane, where δ is the C P phase, showing the true values of θ23 for which the octant can be experimentally determined at 3 σ , 2 σ and 1 σ confidence level. In particular, we study the impact of the possible nonunitarity of neutrino mixing on the experimental determination of θ23 in those experiments.

Determination of wall shear stress from mean velocity and Reynolds shear stress profiles

NASA Astrophysics Data System (ADS)

Volino, Ralph J.; Schultz, Michael P.

2018-03-01

An analytical method is presented for determining the Reynolds shear stress profile in steady, two-dimensional wall-bounded flows using the mean streamwise velocity. The method is then utilized with experimental data to determine the local wall shear stress. The procedure is applicable to flows on smooth and rough surfaces with arbitrary pressure gradients. It is based on the streamwise component of the boundary layer momentum equation, which is transformed into inner coordinates. The method requires velocity profiles from at least two streamwise locations, but the formulation of the momentum equation reduces the dependence on streamwise gradients. The method is verified through application to laminar flow solutions and turbulent DNS results from both zero and nonzero pressure gradient boundary layers. With strong favorable pressure gradients, the method is shown to be accurate for finding the wall shear stress in cases where the Clauser fit technique loses accuracy. The method is then applied to experimental data from the literature from zero pressure gradient studies on smooth and rough walls, and favorable and adverse pressure gradient cases on smooth walls. Data from very near the wall are not required for determination of the wall shear stress. Wall friction velocities obtained using the present method agree with those determined in the original studies, typically to within 2%.

Experiments assigned to determine the acceleration of 8000kN shear laboratory model elements

NASA Astrophysics Data System (ADS)

Budiul Berghian, A.; Vasiu, T.; Abrudean, C.

2017-01-01

In this paper presents an experimental kinetics study by measuring accelerations using a bi-axial accelerometer constructed in the basis of a miniature integrated circuit, included in the class of micro-electrical and mechanical systems - MMA6261Q on the experimental installation reduced to the 1:5 dividing rule by comparison with the shear existent in exploitation, conceived and projected at the Faculty of Engineering in Hunedoara.

Ultrafiltration membrane reactors for enzymatic resolution of amino acids: design model and optimization.

PubMed

Bódalo, A; Gómez, J L.; Gómez, E; Bastida, J; Máximo, M F.; Montiel, M C.

2001-03-08

In this paper the possibility of continuous resolution of DL-phenylalanine, catalyzed by L-aminoacylase in a ultrafiltration membrane reactor (UFMR) is presented. A simple design model, based on previous kinetic studies, has been demonstrated to be capable of describing the behavior of the experimental system. The model has been used to determine the optimal experimental conditions to carry out the asymmetrical hydrolysis of N-acetyl-DL-phenylalanine.

Molecular relaxation processes in dimethyldichlorosilane studied by vibrational spectroscopy

NASA Astrophysics Data System (ADS)

Bratu, I.; Grecu, Rodica; Iliescu, T.

1995-04-01

The paper presents the experimentally determined correlation functions ( CF) of the bands due to IR and Raman active vibrations ν asSiCl 2 and ν sSiCl 2 of dimethyldichlorosilane ( DMDCS) in pure liquid and in solutions. Both reorientational and vibrational relaxations (the last one being dominant) contribute to the profiles of these vibrational modes. Kubo-Rothschild's and Oxtoby's models compared with the experimental CF indicate an intermediate modulation regime.

An Experimental Study of the Use of Visual Illustrations Used to Complement Oral Instruction on Television.

ERIC Educational Resources Information Center

Dwyer, Francis M., Jr.

Five slide sequences, each containing 39 black-and-white slides designed to complement oral instruction, and carrying a 32 minute oral instructional unit on the heart, were presented to 269 college students in five groups through a television receiver. The purpose was twofold: to determine if redundant information presented simultaneously through…

Numerical determination of personal aerosol sampler aspiration efficiency.

PubMed

Lo Savio, Simone; Paradisi, Paolo; Tampieri, Francesco; Belosi, Franco; Morigi, Maria Pia; Agostini, Sergio

2003-04-01

In this work the determination of the aspiration efficiency of personal aerosol samplers, commonly used in occupational exposure assessment, is investigated by means of CFD techniques. Specifically, it will be described a code to calculate the particle trajectories in a given flow field. At the present state the code considers only the effects of the mean flow field on the particle motion, whereas the turbulent diffusion effects are neglected. Comparisons with experimental measurements are also given in the framework of a research contract, supported by the European Community, with several experimental contributions from the participants. The main objective of the European research is to develop a new approach to experimentation with airborne particle flows, working on a reduced scale. This methodology has the advantage of allowing real-time aerosol determination and use of small wind tunnels, with a better experimental control. In this article we describe how the methodology has been verified using computational fluid dynamics. Experimental and numerical aspiration efficiencies have been compared and the influence of gravity and turbulence intensity in full and reduced scale has been investigated. The numerical techniques described here are in agreement with previous similar research and allow at least qualitative predictions of aspiration efficiency for real samplers, taking care of orientation from the incoming air flow. The major discrepancies among predicted and experimental results may be a consequence of bounce effects, which are very difficult to eliminate also by greasing the sampler surface.

Determination of minor and trace elements concentration in kidney stones using elemental analysis techniques

NASA Astrophysics Data System (ADS)

Srivastava, Anjali

The determination of accurate material composition of a kidney stone is crucial for understanding the formation of the kidney stone as well as for preventive therapeutic strategies. Radiations probing instrumental activation analysis techniques are excellent tools for identification of involved materials present in the kidney stone. The X-ray fluorescence (XRF) and neutron activation analysis (NAA) experiments were performed and different kidney stones were analyzed. The interactions of X-ray photons and neutrons with matter are complementary in nature, resulting in distinctly different materials detection. This is the first approach to utilize combined X-ray fluorescence and neutron activation analysis for a comprehensive analysis of the kideny stones. Presently, experimental studies in conjunction with analytical techniques were used to determine the exact composition of the kidney stone. The use of open source program Python Multi-Channel Analyzer was utilized to unfold the XRF spectrum. A new type of experimental set-up was developed and utilized for XRF and NAA analysis of the kidney stone. To verify the experimental results with analytical calculation, several sets of kidney stones were analyzed using XRF and NAA technique. The elements which were identified from XRF technique are Br, Cu, Ga, Ge, Mo, Nb, Ni, Rb, Se, Sr, Y, Zr. And, by using Neutron Activation Analysis (NAA) are Au, Br, Ca, Er, Hg, I, K, Na, Pm, Sb, Sc, Sm, Tb, Yb, Zn. This thesis presents a new approach for exact detection of accurate material composition of kidney stone materials using XRF and NAA instrumental activation analysis techniques.

Experimental Method for Characterizing Electrical Steel Sheets in the Normal Direction

PubMed Central

Hihat, Nabil; Lecointe, Jean Philippe; Duchesne, Stephane; Napieralska, Ewa; Belgrand, Thierry

2010-01-01

This paper proposes an experimental method to characterise magnetic laminations in the direction normal to the sheet plane. The principle, which is based on a static excitation to avoid planar eddy currents, is explained and specific test benches are proposed. Measurements of the flux density are made with a sensor moving in and out of an air-gap. A simple analytical model is derived in order to determine the permeability in the normal direction. The experimental results for grain oriented steel sheets are presented and a comparison is provided with values obtained from literature. PMID:22163394

Experimental results for characterization of a tapered plastic optical fiber sensor based on SPR

NASA Astrophysics Data System (ADS)

Cennamo, N.; Galatus, R.; Zeni, L.

2015-05-01

The experimental results obtained with two different Plastic Optical Fiber (POF) geometries, tapered and not-tapered, for a sensor based on Surface Plasmon Resonance (SPR) are presented. SPR is used for determining the refractive index variations at the interface between a gold layer and a dielectric medium (aqueous medium). In this work SPR sensors in POF configurations, useful for bio-sensing applications, have been realized for the optimization of the sensitivity and experimentally tested. The results show as the sensitivity increases with the tapered POF configuration, when the refractive index of aqueous medium increases.

A Buoyancy-based Method of Determining Fat Levels in Drosophila.

PubMed

Hazegh, Kelsey E; Reis, Tânia

2016-11-01

Drosophila melanogaster is a key experimental system in the study of fat regulation. Numerous techniques currently exist to measure levels of stored fat in Drosophila, but most are expensive and/or laborious and have clear limitations. Here, we present a method to quickly and cheaply determine organismal fat levels in L3 Drosophila larvae. The technique relies on the differences in density between fat and lean tissues and allows for rapid detection of fat and lean phenotypes. We have verified the accuracy of this method by comparison to body fat percentage as determined by neutral lipid extraction and gas chromatography coupled with mass spectrometry (GCMS). We furthermore outline detailed protocols for the collection and synchronization of larvae as well as relevant experimental recipes. The technique presented below overcomes the major shortcomings in the most widely used lipid quantitation methods and provides a powerful way to quickly and sensitively screen L3 larvae for fat regulation phenotypes while maintaining the integrity of the larvae. This assay has wide applications for the study of metabolism and fat regulation using Drosophila.

Evaluation of passive belts for different size occupants.

DOT National Transportation Integrated Search

1980-04-01

This report presents findings of a combined analytical and experimental research program to: (1) determine the effect of independent variation of the vertical and longitudinal position of the upper anchor point of the Volkswagen Rabbit on the perfoma...

Kernel structures for Clouds

NASA Technical Reports Server (NTRS)

Spafford, Eugene H.; Mckendry, Martin S.

1986-01-01

An overview of the internal structure of the Clouds kernel was presented. An indication of how these structures will interact in the prototype Clouds implementation is given. Many specific details have yet to be determined and await experimentation with an actual working system.

Characterization of a space orbited incoherent fiber optic bundle

NASA Technical Reports Server (NTRS)

Dewalt, Stephen A.; Taylor, Edward W.

1993-01-01

The results of a study performed to determine the effects of adverse space environments on a bundle of over 1800 optical fibers orbited for 69 months are reported. Experimental results are presented on an incoherent fiber optic bundle oriented in low Earth orbit aboard the Long Duration Exposure Facility (LDEF) satellite as part of the Space Environment Effects Experiment (M0006). Measurements were performed to determine if space induced radiation effects changed the fiber bundle characteristics. Data demonstrating the success of light transmitting fibers to withstand the adverse space environment are presented.

Investigation of the Behavior of Hardening Masonry Exposed to Variable Stresses

PubMed Central

Šlivinskas, Tomas; Jonaitis, Bronius; Marčiukaitis, Jonas Gediminas

2018-01-01

This paper analyzes the behavior of masonry under variable loads during execution (construction stage). It specifies the creep coefficient for calcium silicate brick masonry, presenting the research data of masonry deformation under variable and constant long-term loads. The interaction of separate layers of composite material in masonry is introduced and the formulae for determining long-term deformations are offered. The research results of masonry’s compressive strength and deformation properties under variable and constant long-term loads are presented. These are then compared to calculated ones. According to the presented comparison, the calculated long-term deformations coincide quite well with those determined experimentally. PMID:29710802

Investigation of the Behavior of Hardening Masonry Exposed to Variable Stresses.

PubMed

Šlivinskas, Tomas; Jonaitis, Bronius; Marčiukaitis, Jonas Gediminas; Zavalis, Robertas

2018-04-28

This paper analyzes the behavior of masonry under variable loads during execution (construction stage). It specifies the creep coefficient for calcium silicate brick masonry, presenting the research data of masonry deformation under variable and constant long-term loads. The interaction of separate layers of composite material in masonry is introduced and the formulae for determining long-term deformations are offered. The research results of masonry’s compressive strength and deformation properties under variable and constant long-term loads are presented. These are then compared to calculated ones. According to the presented comparison, the calculated long-term deformations coincide quite well with those determined experimentally.

Velocity field near the jet orifice of a round jet in a crossflow

NASA Technical Reports Server (NTRS)

Fearn, R. L.; Benson, J. P.

1979-01-01

Experimentally determined velocities at selected locations near the jet orifice are presented and analyzed for a round jet in crossflow. Jet-to-crossflow velocity ratios of four and eight were studied experimentally for a round subsonic jet of air exhausting perpendicularly through a flat plate into a subsonic crosswind of the same temperature. Velocity measurements were made in cross sections to the jet plume located from one to four jet diameters from the orifice. Jet centerline and vortex properties are presented and utilized to extend the results of a previous study into the region close to the jet orifice.

New approach in the quantum statistical parton distribution

NASA Astrophysics Data System (ADS)

Sohaily, Sozha; Vaziri (Khamedi), Mohammad

2017-12-01

An attempt to find simple parton distribution functions (PDFs) based on quantum statistical approach is presented. The PDFs described by the statistical model have very interesting physical properties which help to understand the structure of partons. The longitudinal portion of distribution functions are given by applying the maximum entropy principle. An interesting and simple approach to determine the statistical variables exactly without fitting and fixing parameters is surveyed. Analytic expressions of the x-dependent PDFs are obtained in the whole x region [0, 1], and the computed distributions are consistent with the experimental observations. The agreement with experimental data, gives a robust confirm of our simple presented statistical model.

Density measurements in low pressure, weakly magnetized, RF plasmas: experimental verification of the sheath expansion effect

NASA Astrophysics Data System (ADS)

Zhang, Yunchao; Charles, Christine; Boswell, Roderick W.

2017-07-01

This experimental study shows the validity of Sheridan's method in determining plasma density in low pressure, weakly magnetized, RF plasmas using ion saturation current data measured by a planar Langmuir probe. The ion density derived from Sheridan's method which takes into account the sheath expansion around the negatively biased probe tip, presents a good consistency with the electron density measured by a cylindrical RF-compensated Langmuir probe using the Druyvesteyn theory. The ion density obtained from the simplified method which neglects the sheath expansion effect, overestimates the true density magnitude, e.g., by a factor of 3 to 12 for the present experiment.

Stability and Interaction of Coherent Structure in Supersonic Reactive Wakes

NASA Technical Reports Server (NTRS)

Menon, Suresh

1983-01-01

A theoretical formulation and analysis is presented for a study of the stability and interaction of coherent structure in reacting free shear layers. The physical problem under investigation is a premixed hydrogen-oxygen reacting shear layer in the wake of a thin flat plate. The coherent structure is modeled as a periodic disturbance and its stability is determined by the application of linearized hydrodynamic stability theory which results in a generalized eigenvalue problem for reactive flows. Detailed stability analysis of the reactive wake for neutral, symmetrical and antisymmetrical disturbance is presented. Reactive stability criteria is shown to be quite different from classical non-reactive stability. The interaction between the mean flow, coherent structure and fine-scale turbulence is theoretically formulated using the von-Kaman integral technique. Both time-averaging and conditional phase averaging are necessary to separate the three types of motion. The resulting integro-differential equations can then be solved subject to initial conditions with appropriate shape functions. In the laminar flow transition region of interest, the spatial interaction between the mean motion and coherent structure is calculated for both non-reactive and reactive conditions and compared with experimental data wherever available. The fine-scale turbulent motion determined by the application of integral analysis to the fluctuation equations. Since at present this turbulence model is still untested, turbulence is modeled in the interaction problem by a simple algebraic eddy viscosity model. The applicability of the integral turbulence model formulated here is studied parametrically by integrating these equations for the simple case of self-similar mean motion with assumed shape functions. The effect of the motion of the coherent structure is studied and very good agreement is obtained with previous experimental and theoretical works for non-reactive flow. For the reactive case, lack of experimental data made direct comparison difficult. It was determined that the growth rate of the disturbance amplitude is lower for reactive case. The results indicate that the reactive flow stability is in qualitative agreement with experimental observation.

Experimental results on the ω- and η'-nucleus potential - on the way to mesic states

NASA Astrophysics Data System (ADS)

Nanova, Mariana

2015-06-01

Different experimental approaches to determine the meson-nucleus optical potential are discussed. The experiments have been performed with the Crystal Barrel/TAPS detector system at the ELSA accelerator in Bonn and the Crystal Ball/TAPS at the MAMI accelerator in Mainz. Experimental results about the real and imaginary part of the η'- and ω-nucleus optical potential are presented. The imaginary part of the meson-nucleus optical potential is determined from the in-medium width of the meson by the measurement of the transparency ratio. Information on the real part of the optical potential is deduced from measurements of the excitation function and momentum distribution which are sensitive to the sign and depth of the potential. The results are discussed and compared to theoretical predictions. The data for both mesons are consistent with a weakly attractive potential. The formation and population of ω-nucleus and η'-nucleus bound states is additionally discussed.

Understanding the requirements of self-expandable stents for heart valve replacement: Radial force, hoop force and equilibrium.

PubMed

Cabrera, María Sol; Oomens, Cees W J; Baaijens, Frank P T

2017-04-01

A proper interpretation of the forces developed during stent crimping and deployment is of paramount importance for a better understanding of the requirements for successful heart valve replacement. The present study combines experimental and computational methods to assess the performance of a nitinol stent for tissue-engineered heart valve implantation. To validate the stent model, the mechanical response to parallel plate compression and radial crimping was evaluated experimentally. Finite element simulations showed good agreement with the experimental findings. The computational models were further used to determine the hoop force on the stent and radial force on a rigid tool during crimping and self-expansion. In addition, stent deployment against ovine and human pulmonary arteries was simulated to determine the hoop force on the stent-artery system and the equilibrium diameter for different degrees of oversizing. Copyright © 2017 The Authors. Published by Elsevier Ltd.. All rights reserved.

Comparison of experimental and calculated chiroptical spectra for chiral molecular structure determination.

PubMed

Polavarapu, Prasad L; Covington, Cody L

2014-09-01

For three different chiroptical spectroscopic methods, namely, vibrational circular dichroism (VCD), electronic circular dichroism (ECD), and Raman optical activity (ROA), the measures of similarity of the experimental spectra to the corresponding spectra predicted using quantum chemical theories are summarized. In determining the absolute configuration and/or predominant conformations of chiral molecules, these similarity measures provide numerical estimates of agreement between experimental observations and theoretical predictions. Selected applications illustrating the similarity measures for absorption, circular dichroism, and corresponding dissymmetry factor (DF) spectra, in the case of VCD and ECD, and for Raman, ROA, and circular intensity differential (CID) spectra in the case of ROA, are presented. The analysis of similarity in DF or CID spectra is considered to be much more discerning and accurate than that in absorption (or Raman) and circular dichroism (or ROA) spectra, undertaken individually. © 2014 Wiley Periodicals, Inc.

Experimental methods and transport models for drug delivery across the blood-brain barrier.

PubMed

Fu, Bingmei M

2012-06-01

The blood-brain barrier (BBB) is a dynamic barrier essential for maintaining the micro-environment of the brain. Although the special anatomical features of the BBB determine its protective role for the central nervous system (CNS) from blood-born neurotoxins, however, the BBB extremely limits the therapeutic efficacy of drugs into the CNS, which greatly hinders the treatment of major brain diseases. This review summarized the unique structures of the BBB, described a variety of in vivo and in vitro experimental methods for determining the transport properties of the BBB, e.g., the permeability of the BBB to water, ions, and solutes including nutrients, therapeutic agents and drug carriers, and presented newly developed mathematical models which quantitatively correlate the anatomical structures of the BBB with its barrier functions. Finally, on the basis of the experimental observations and the quantitative models, several strategies for drug delivery through the BBB were proposed.

Experimental Methods and Transport Models for Drug Delivery across the Blood-Brain Barrier

PubMed Central

Fu, Bingmei M

2017-01-01

The blood-brain barrier (BBB) is a dynamic barrier essential for maintaining the micro-environment of the brain. Although the special anatomical features of the BBB determine its protective role for the central nervous system (CNS) from blood-born neurotoxins, however, the BBB extremely limits the therapeutic efficacy of drugs into the CNS, which greatly hinders the treatment of major brain diseases. This review summarized the unique structures of the BBB, described a variety of in vivo and in vitro experimental methods for determining the transport properties of the BBB, e.g., the permeability of the BBB to water, ions, and solutes including nutrients, therapeutic agents and drug carriers, and presented newly developed mathematical models which quantitatively correlate the anatomical structures of the BBB with its barrier functions. Finally, on the basis of the experimental observations and the quantitative models, several strategies for drug delivery through the BBB were proposed. PMID:22201587

Theoretical and experimental studies of the current–voltage and capacitance–voltage of HEMT structures and field-effect transistors

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tarasova, E. A.; Obolenskaya, E. S., E-mail: obolensk@rf.unn.ru; Hananova, A. V.

The sensitivity of classical n{sup +}/n{sup –} GaAs and AlGaN/GaN structures with a 2D electron gas (HEMT) and field-effect transistors based on these structures to γ-neutron exposure is studied. The levels of their radiation hardness were determined. A method for experimental study of the structures on the basis of a differential analysis of their current–voltage characteristics is developed. This method makes it possible to determine the structure of the layers in which radiation-induced defects accumulate. A procedure taking into account changes in the plate area of the experimentally measured barrier-contact capacitance associated with the emergence of clusters of radiation-induced defectsmore » that form dielectric inclusions in the 2D-electron-gas layer is presented for the first time.« less

Contact Forces between Single Metal Oxide Nanoparticles in Gas-Phase Applications and Processes

PubMed Central

2017-01-01

In this work we present a comprehensive experimental study to determine the contact forces between individual metal oxide nanoparticles in the gas-phase using atomic force microscopy. In addition, we determined the amount of physisorbed water for each type of particle surface. By comparing our results with mathematical models of the interaction forces, we could demonstrate that classical continuum models of van der Waals and capillary forces alone cannot sufficiently describe the experimental findings. Rather, the discrete nature of the molecules has to be considered, which leads to ordering at the interface and the occurrence of solvation forces. We demonstrate that inclusion of solvation forces in the model leads to quantitative agreement with experimental data and that tuning of the molecular order by addition of isopropanol vapor allows us to control the interaction forces between the nanoparticles. PMID:28186771

Experimental thrust performance of a high-area-ratio rocket nozzle

NASA Technical Reports Server (NTRS)

Pavli, Albert J.; Kacynski, Kenneth J.; Smith, Tamara A.

1987-01-01

An experimental investigation was conducted to determine the thrust performance attainable from high-area-ratio rocket nozzles. A modified Rao-contoured nozzle with an expansion area of 1030 was test fired with hydrogen-oxygen propellants at altitude conditions. The nozzle was also tested as a truncated nozzle, at an expansion area ratio of 428. Thrust coefficient and thrust coefficient efficiency values are presented for each configuration at various propellant mixture ratios (oxygen/fuel). Several procedural techniques were developed permitting improved measurement of nozzle performance. The more significant of these were correcting the thrust for the aneroid effects, determining the effective chamber pressure, and referencing differential pressure transducers to a vacuum reference tank.

Experimental thrust performance of a high area-ratio rocket nozzle

NASA Technical Reports Server (NTRS)

Pavli, A. J.; Kacynski, K. J.; Smith, T. A.

1986-01-01

An experimental investigation was conducted to determine the thrust performance attainable from high-area-ratio rocket nozzles. A modified Rao-contoured nozzle with an expansion area of 1030 was test fired with hydrogen-oxygen propellants at altitude conditions. The nozzle was also tested as a truncated nozzle, at an expansion area ratio of 428. Thrust coefficient and thrust coefficient efficiency values are presented for each configuration at various propellant mixture ratios (oxygen/fuel). Several procedural techniques were developed permitting improved measurement of nozzle performance. The more significant of these were correcting the thrust for the aneroid effects, determining the effective chamber pressure, and referencing differential pressure transducers to a vacuum reference tank.

Determination of Cole-Cole parameters using only the real part of electrical impedivity measurements.

PubMed

Miranda, David A; Rivera, S A López

2008-05-01

An algorithm is presented to determine the Cole-Cole parameters of electrical impedivity using only measurements of its real part. The algorithm is based on two multi-fold direct inversion methods for the Cole-Cole and Debye equations, respectively, and a genetic algorithm for the optimization of the mean square error between experimental and calculated data. The algorithm has been developed to obtain the Cole-Cole parameters from experimental data, which were used to screen cervical intra-epithelial neoplasia. The proposed algorithm was compared with different numerical integrations of the Kramers-Kronig relation and the result shows that this algorithm is the best. A high immunity to noise was obtained.

An iterative method for near-field Fresnel region polychromatic phase contrast imaging

NASA Astrophysics Data System (ADS)

Carroll, Aidan J.; van Riessen, Grant A.; Balaur, Eugeniu; Dolbnya, Igor P.; Tran, Giang N.; Peele, Andrew G.

2017-07-01

We present an iterative method for polychromatic phase contrast imaging that is suitable for broadband illumination and which allows for the quantitative determination of the thickness of an object given the refractive index of the sample material. Experimental and simulation results suggest the iterative method provides comparable image quality and quantitative object thickness determination when compared to the analytical polychromatic transport of intensity and contrast transfer function methods. The ability of the iterative method to work over a wider range of experimental conditions means the iterative method is a suitable candidate for use with polychromatic illumination and may deliver more utility for laboratory-based x-ray sources, which typically have a broad spectrum.

Study of curved and planar frequency-selective surfaces with nonplanar illumination

NASA Technical Reports Server (NTRS)

Caroglanian, Armen; Webb, Kevin J.

1991-01-01

A locally planar technique (LPT) is investigated for determining the forward-scattered field from a generally shaped inductive frequency-selective surface (FSS) with nonplanar illumination. The results of an experimental study are presented to assess the LPT accuracy. The effects of a nonplanar incident field are determined by comparing the LPT numerical results with a series of experiments with the feed source placed at varying distances from the planar FSS. The limitations of the LPT model due to surface curvature are investigated in an experimental study of the scattered fields from a set of hyperbolic cylinders of different curvatures. From these comparisons, guidelines for applying the locally planar technique are developed.

Photoelastic Analysis of Cracked Thick Walled Cylinders

NASA Astrophysics Data System (ADS)

Pastramă, Ştefan Dan

2017-12-01

In this paper, the experimental determination of the stress intensity factor in thick walled cylinders subject to uniform internal pressure and having longitudinal non-penetrating cracks is presented. Photoelastic measurements were used together with the expressions of the stress field near the crack tip for Mode I crack extension and a specific methodology for stress intensity factor determination. Two types of longitudinal cracks - internal and external - were considered. Four plane models were manufactured and analyzed in a plane polariscope at different values of the applied internal pressure. The values of the normalized stress intensity factor were calculated and the results were compared to those reported by other authors. A good accuracy was noticed, showing the reliability of the experimental procedure.

Computation of Kinetics for the Hydrogen/Oxygen System Using the Thermodynamic Method

NASA Technical Reports Server (NTRS)

Marek, C. John

1996-01-01

A new method for predicting chemical rate constants using thermodynamics has been applied to the hydrogen/oxygen system. This method is based on using the gradient of the Gibbs free energy and a single proportionality constant D to determine the kinetic rate constants. Using this method the rate constants for any gas phase reaction can be computed from thermodynamic properties. A modified reaction set for the H/O system is determined. A11 of the third body efficiencies M are taken to be unity. Good agreement was obtained between the thermodynamic method and the experimental shock tube data. In addition, the hydrogen bromide experimental data presented in previous work is recomputed with M's of unity.

Development and Assessment of Planetary Gear Unit for Experimental Prototype of Vertical Axis Wind Turbine

NASA Astrophysics Data System (ADS)

Urbahs, A.; Urbaha, M.; Carjova, K.

2017-10-01

The theoretical calculation for development of planetary gear unit of wind turbine (WT) and its experimental tests are presented in the paper. Development of experimental prototypes from composite materials is essential to determine capability of element and its impact on feature. Two experimental scale prototypes of planetary gear unit for WT were developed for such purposes. Hall transducer, servomechanisms and optical tachometers were used to obtain results, comparison analysis of theoretical and actual data was performed as well as quality assessment of experimental prototypes of planetary gear unit. After kinematic and load analysis as well as control of rotation frequency, it is possible to declare that the unit is able to operate at designated quality. Theoretical calculations and test results obtained are used for industrial WT prototype development.

Assessment of analytical and experimental techniques utilized in conducting plume technology tests 575 and 593. [exhaust flow simulation (wind tunnel tests) of scale model Space Shuttle Orbiter

NASA Technical Reports Server (NTRS)

Baker, L. R.; Sulyma, P. R.; Tevepaugh, J. A.; Penny, M. M.

1976-01-01

Since exhaust plumes affect vehicle base environment (pressure and heat loads) and the orbiter vehicle aerodynamic control surface effectiveness, an intensive program involving detailed analytical and experimental investigations of the exhaust plume/vehicle interaction was undertaken as a pertinent part of the overall space shuttle development program. The program, called the Plume Technology program, has as its objective the determination of the criteria for simulating rocket engine (in particular, space shuttle propulsion system) plume-induced aerodynamic effects in a wind tunnel environment. The comprehensive experimental program was conducted using test facilities at NASA's Marshall Space Flight Center and Ames Research Center. A post-test examination of some of the experimental results obtained from NASA-MSFC's 14 x 14-inch trisonic wind tunnel is presented. A description is given of the test facility, simulant gas supply system, nozzle hardware, test procedure and test matrix. Analysis of exhaust plume flow fields and comparison of analytical and experimental exhaust plume data are presented.

Damage detection in composite materials using Lamb wave methods

NASA Astrophysics Data System (ADS)

Kessler, Seth S.; Spearing, S. Mark; Soutis, Constantinos

2002-04-01

Cost-effective and reliable damage detection is critical for the utilization of composite materials. This paper presents part of an experimental and analytical survey of candidate methods for in situ damage detection of composite materials. Experimental results are presented for the application of Lamb wave techniques to quasi-isotropic graphite/epoxy test specimens containing representative damage modes, including delamination, transverse ply cracks and through-holes. Linear wave scans were performed on narrow laminated specimens and sandwich beams with various cores by monitoring the transmitted waves with piezoceramic sensors. Optimal actuator and sensor configurations were devised through experimentation, and various types of driving signal were explored. These experiments provided a procedure capable of easily and accurately determining the time of flight of a Lamb wave pulse between an actuator and sensor. Lamb wave techniques provide more information about damage presence and severity than previously tested methods (frequency response techniques), and provide the possibility of determining damage location due to their local response nature. These methods may prove suitable for structural health monitoring applications since they travel long distances and can be applied with conformable piezoelectric actuators and sensors that require little power.

Calculation and experimental determination of the geometric parameters of the coatings by laser cladding

NASA Astrophysics Data System (ADS)

Birukov, V. P.; Fichkov, A. A.

2017-12-01

In the present work the experiments on laser cladding of powder Fe-B-Cr-6-2 on samples of steel 20. Metallographic studies of geometric parameters of deposited layers and the depth of the heat affected zone (HAZ). Using is the method of full factorial experiment (FFE) mathematical dependences of the geometrical sizes of the deposited layers of processing modes. Deviation of calculated values from experimental data is not more than 3%.

Preliminary Internal Performance Data for a Variable-Ejector Assembly on the XJ79-GE-1 Turbojet Engine. II; Afterburning Configurations

NASA Technical Reports Server (NTRS)

Bloomer, Harry E.; Groesbeck, Donald E.

1957-01-01

Internal performance of an XJ79-GE-1 variable ejector was experimentally determined with the primary nozzle in two representative after-burning positions. Jet-thrust and air-handling data were obtained in quiescent air for 4 selected ejector configurations over a wide range of secondary to primary airflow ratios and primary-nozzle pressure ratios. The experimental ejector data are presented in both graphical and tabulated form.

Novel chemometric strategy based on the application of artificial neural networks to crossed mixture design for the improvement of recombinant protein production in continuous culture.

PubMed

Didier, Caroline; Forno, Guillermina; Etcheverrigaray, Marina; Kratje, Ricardo; Goicoechea, Héctor

2009-09-21

The optimal blends of six compounds that should be present in culture media used in recombinant protein production were determined by means of artificial neural networks (ANN) coupled with crossed mixture experimental design. This combination constitutes a novel approach to develop a medium for cultivating genetically engineered mammalian cells. The compounds were collected in two mixtures of three elements each, and the experimental space was determined by a crossed mixture design. Empirical data from 51 experimental units were used in a multiresponse analysis to train artificial neural networks which satisfy different requirements, in order to define two new culture media (Medium 1 and Medium 2) to be used in a continuous biopharmaceutical production process. These media were tested in a bioreactor to produce a recombinant protein in CHO cells. Remarkably, for both predicted media all responses satisfied the predefined goals pursued during the analysis, except in the case of the specific growth rate (mu) observed for Medium 1. ANN analysis proved to be a suitable methodology to be used when dealing with complex experimental designs, as frequently occurs in the optimization of production processes in the biotechnology area. The present work is a new example of the use of ANN for the resolution of a complex, real life system, successfully employed in the context of a biopharmaceutical production process.

Experimental Investigation of Compressed Thin-Walled Steel Members

NASA Astrophysics Data System (ADS)

Juhás, Pavol; Juhásová Šenitková, Ingrid

2017-10-01

The paper presents fundamental information about realized experimental-theoretical research to determinate the load-carrying capacities for thin-walled compressed steel members with quasi-homogenous and hybrid cross-sections. The webs of such members are stressed in the elastic-plastic region. This continuous research joins on previous research of the first author of the paper. The aim of this research is to investigate and analyse the elastic-plastic post-critical behaviour of thin web and its interaction with flanges. The experimental program, test members and their geometrical parameters and material properties are evident from table 1 and table 2 as well as from figure 1 and figure 2. The test arrangement and failures of the test members are illustrated on Figures 3, 4 and 5. Some partial results are presented in Table 3 of the paper, too.

Fetal malformations and early embryonic gene expression response in cynomolgus monkeys maternally exposed to thalidomide

EPA Science Inventory

The present study was performed to determine experimental conditions for thalidomide induction of fetal malformations and to understand the molecular mechanisms underlying thalidomide teratogenicity in cynomolgus monkeys. Cynomolgus monkeys were orally administered (±)-thalidomid...

A Sabbatical Journey into the Microbial World.

ERIC Educational Resources Information Center

Lundgren, Linda

1991-01-01

Presents research results on photosynthetic, carbon monoxide utilizing bacteria. Discusses applications of the research and offers three sets of experimental procedures and data that students analyze to determine which bacterium from a soil sample uses carbon monoxide fastest. (Contains 21 references.) (MDH)

Optical device for thermal diffusivity determination in liquids by reflection of a thermal wave

NASA Astrophysics Data System (ADS)

Sánchez-Pérez, C.; De León-Hernández, A.; García-Cadena, C.

2017-08-01

In this work, we present a device for determination of the thermal diffusivity using the oblique reflection of a thermal wave within a solid slab that is in contact with the medium to be characterized. By using the reflection near a critical angle under the assumption that thermal waves obey Snell's law of refraction with the square root of the thermal diffusivities, the unknown thermal diffusivity is obtained by simple formulae. Experimentally, the sensor response is measured using the photothermal beam deflection technique within a slab that results in a compact device with no contact of the laser probing beam with the sample. We describe the theoretical basis and provide experimental results to validate the proposed method. We determine the thermal diffusivity of tridistilled water and glycerin solutions with an error of less than 0.5%.

Saturated liquid density of 1,1-difluoroethane(R 152a) and thermodynamic properties along the vapor-liquid coexistence curve

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sato, H.; Okada, M.; Uematsu, M.

1987-01-01

Saturated liquid densities of 1,1-difluoroethane (CH/sub 3/CHF/sub 2/) are measured at temperatures from 223 K to 363 K with the estimated uncertainty of +-0.2% by a magnetic densimetry. The experimental results are compared with the available experimental data and some correlations and equations of state. A simple correlation for the saturated liquid density is developed as a function of temperature. This correlation covers the temperature range up to the critical point which reproduces the present experimental results with the percent means deviation of 0.11%. Adding the available experimental data with respect to the vapor pressure, critical parameters, saturated vapor density,more » and the second virial coefficient to the present saturated liquid density data, the parameters of the Redlich-Kwong-Soave equation of state are determined and the thermodynamic properties along the vapor-liquid coexistence curve are derived.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Noe, F; Diadone, Isabella; Lollmann, Marc

There is a gap between kinetic experiment and simulation in their views of the dynamics of complex biomolecular systems. Whereas experiments typically reveal only a few readily discernible exponential relaxations, simulations often indicate complex multistate behavior. Here, a theoretical framework is presented that reconciles these two approaches. The central concept is dynamical fingerprints which contain peaks at the time scales of the dynamical processes involved with amplitudes determined by the experimental observable. Fingerprints can be generated from both experimental and simulation data, and their comparison by matching peaks permits assignment of structural changes present in the simulation to experimentally observedmore » relaxation processes. The approach is applied here to a test case interpreting single molecule fluorescence correlation spectroscopy experiments on a set of fluorescent peptides with molecular dynamics simulations. The peptides exhibit complex kinetics shown to be consistent with the apparent simplicity of the experimental data. Moreover, the fingerprint approach can be used to design new experiments with site-specific labels that optimally probe specific dynamical processes in the molecule under investigation.« less

Effect of Computer-Based Multimedia Presentation on Senior Secondary Students' Achievement in Agricultural Science

ERIC Educational Resources Information Center

Olori, Abiola Lateef; Igbosanu, Adekunle Olusegun

2016-01-01

The study was carried out to determine the use of computer-based multimedia presentation on Senior Secondary School Students' Achievement in Agricultural Science. The study was a quasi-experimental, pre-test, post-test control group research design type, using intact classes. A sample of eighty (80) Senior Secondary School One (SS II) students was…

Wind tunnel study of natural ventilation of building integrated photovoltaics double skin façade

NASA Astrophysics Data System (ADS)

Hudişteanu, Sebastian Valeriu; Popovici, Cătălin George; Cherecheş, Nelu-Cristian

2018-02-01

The paper presents a wind tunnel experimental analysis of a small-scale building model (1:30). The objective of the study is to determine the wind influence on the ventilation of a double skin façade channel (DSF) and the cooling effect over integrated photovoltaic panels. The tests were achieved by conceiving and implementation of an experimental program using a wind tunnel with atmospheric boundary layer. The effect of the wind over the ventilation of the horizontal channels of double skin façades is evaluated for different incident velocities. The results are generalized for the average steady state values of the velocities analysed. The experimental results put in evidence the correlation between the reference wind velocity and the dynamics of the air movement inside the double skin façade. These values are used to determine the convective heat transfer and the cooling effect of the air streams inside the channel upon the integrated photovoltaic panels. The decrease of the photovoltaic panels temperature determines a raise of 11% in efficiency and power generated.

NASA-Langley Research Center's participation in a round-robin comparison between some current crack-propagation prediction methods

NASA Technical Reports Server (NTRS)

Hudson, C. M.; Lewis, P. E.

1979-01-01

A round-robin study was conducted which evaluated and compared different methods currently in practice for predicting crack growth in surface-cracked specimens. This report describes the prediction methods used by the Fracture Mechanics Engineering Section, at NASA-Langley Research Center, and presents a comparison between predicted crack growth and crack growth observed in laboratory experiments. For tests at higher stress levels, the correlation between predicted and experimentally determined crack growth was generally quite good. For tests at lower stress levels, the predicted number of cycles to reach a given crack length was consistently higher than the experimentally determined number of cycles. This consistent overestimation of the number of cycles could have resulted from a lack of definition of crack-growth data at low values of the stress intensity range. Generally, the predicted critical flaw sizes were smaller than the experimentally determined critical flaw sizes. This underestimation probably resulted from using plane-strain fracture toughness values to predict failure rather than the more appropriate values based on maximum load.

Testing for intracycle determinism in pseudoperiodic time series.

PubMed

Coelho, Mara C S; Mendes, Eduardo M A M; Aguirre, Luis A

2008-06-01

A determinism test is proposed based on the well-known method of the surrogate data. Assuming predictability to be a signature of determinism, the proposed method checks for intracycle (e.g., short-term) determinism in the pseudoperiodic time series for which standard methods of surrogate analysis do not apply. The approach presented is composed of two steps. First, the data are preprocessed to reduce the effects of seasonal and trend components. Second, standard tests of surrogate analysis can then be used. The determinism test is applied to simulated and experimental pseudoperiodic time series and the results show the applicability of the proposed test.

The Shock and Vibration Bulletin. Part 1. Invited Papers, Submarine Shock Testing, Shock Analysis, Shock Testing

DTIC Science & Technology

1973-06-01

approximately 4. Use of a cold gas for determining was determined and presented in Figure 3. This analysis was unsteady flow characteristics and...driven by a hydraulic motor. shown experimentally that drawbar force re- Roller motion develops a high rotating force , ductions greater than one part in...of doors, a water table flow bient pressure. The interest in determining this decay time is analogy was used. With this analogy, a two-dimensional

Determination of the Secondary Bjerknes Force in Acoustic Resonators on Ground and in Microgravity Conditions

NASA Astrophysics Data System (ADS)

Castro, Luz Angelica; Hoyos, Mauricio

2016-04-01

We propose an experimental methodology to determine the secondary Bjerknes force between rigid particles. Measurements done for different particles sizes showed acoustical inter particles interactions. We use and extend the methodology presented in a previous work. The determination of this force will lead us a better understanding of the aggregation process in acoustic resonators. We report in this work, the results of two parabolic flights campaigns performed at the Airbus A300 ZERO-G (Novespace, France).

C-shaped specimen plane strain fracture toughness tests. [metallic materials

NASA Technical Reports Server (NTRS)

Buzzard, R. T.; Fisher, D. M.

1977-01-01

Test equipment, procedures, and data obtained in the evaluation of C-shaped specimens are presented. Observations reported on include: specimen preparation and dimensional measurement; modifications to the standard ASTM E 399 displacement gage, which permit punch mark gage point engagement; and a measurement device for determining the interior and exterior radii of ring segments. Load displacement ratios were determined experimentally which agreed with analytically determined coefficients for three different gage lengths on the inner surfaces of radially-cracked ring segments.

Solid State Kinetic Parameters and Chemical Mechanism of the Dehydration of CoCl2.6H2O.

ERIC Educational Resources Information Center

Ribas, Joan; And Others

1988-01-01

Presents an experimental example illustrating the most common methods for the determination of kinetic parameters. Discusses the different theories and equations to be applied and the mechanism derived from the kinetic results. (CW)

Physical modeling in geomorphology: are boundary conditions necessary?

NASA Astrophysics Data System (ADS)

Cantelli, A.

2012-12-01

Referring to the physical experimental design in geomorphology, boundary conditions are key elements that determine the quality of the results and therefore the study development. For years engineers have modeled structures, such as dams and bridges, with high precision and excellent results. Until the last decade, a great part of the physical experimental work in geomorphology has been developed with an engineer-like approach, requiring an accurate scaling analysis to determine inflow parameters and initial geometrical conditions. However, during the last decade, the way we have been approaching physical experiments has significantly changed. In particular, boundary conditions and initial conditions are considered unknown factors that need to be discovered during the experiment. This new philosophy leads to a more demanding data acquisition process but relaxes the obligation to a priori know the appropriate input and initial conditions and provides the flexibility to discover those data. Here I am going to present some practical examples of this experimental approach in deepwater geomorphology; some questions about scaling of turbidity currents and a new large experimental facility built at the Universidade Federal do Rio Grande do Sul, Brasil.

Theoretical and experimental studies relevant to interpretation of auroral emissions

NASA Technical Reports Server (NTRS)

Keffer, Charles E.

1992-01-01

The results obtained in the second year of a three year collaborative effort with MSFC are summarized. A succession of experimental studies was completed to determine the effects of the natural and induced space vehicle environment on the measurement of auroral images from space-based platforms. In addition, a global model which incorporates both auroral and dayglow emission sources is being developed to allow interpretation of measured auroral emissions. A description of work completed on these two tasks is presented.

Estimation of squeeze-film damping and inertial coefficients from experimental free-decay data

NASA Technical Reports Server (NTRS)

Roberts, J. B.; of Mechanical Engineers, London.

1987-01-01

The results are given for an experimental program concerned with a parametric identification of the damping and inertial coefficients of a cylindrical squeeze-film bearing, through an analysis of transient response data. The results enable the operating range for which a linear model of the squeeze-film is appropriate to be determined. Comparisons are made between the estimated coefficients and theoretical predictions. Presentation is by courtesy of the Council of the Institution of Mechanical Engineers, London.

Comparison of a 3-D DEM simulation with MRI data

NASA Astrophysics Data System (ADS)

Ng, Tang-Tat; Wang, Changming

2001-04-01

This paper presents a comparison of a granular material studied experimentally and numerically. Simple shear tests were performed inside the magnetic core of magnetic resonance imaging (MRI) equipment. Spherical pharmaceutical pills were used as the granular material, with each pill's centre location determined by MRI. These centre locations in the initial assembly were then used as the initial configuration in the numerical simulation using the discrete element method. The contact properties between pharmaceutical pills used in the numerical simulation were obtained experimentally. The numerical predication was compared with experimental data at both macroscopic and microscopic levels. Good agreement was found at both levels.

Measurement of total hemispherical emissivity of contaminated mirror surfaces

NASA Technical Reports Server (NTRS)

Facey, T. A.; Nonnenmacher, A. L.

1989-01-01

The effects of dust contamination on the total hemispherical emissivity (THE) of a 1.5-inch-diameter Al/MgF2-coated telescope mirror are investigated experimentally. The THE is determined by means of cooling-rate measurements in the temperature range 10-14.5 C in a vacuum of 100 ntorr or better. Photographs and drawings of the experimental setup are provided, and results for 11 dust levels are presented in tables and graphs. It is shown that dust has a significant effect on THE, but the experimental losses are only about half those predicted for perfectly black dust in perfect thermal contact with the mirror surface.

Advanced electric propulsion research, 1989

NASA Technical Reports Server (NTRS)

Wilbur, Paul J.

1990-01-01

Results of an experimental study of the characteristics of ion thruster hollow cathodes operating at high discharge currents (up to 60 A) are presented in a companion report. This work shows that ions produced near the cathode orifice can acquire sufficient energy to induce the high sputter erosion rates on cathode potential surfaces that have been observed in ion thrusters. A mechanism by which these ions could be produced is also described. A second, brief study showing how a discharge chamber model developed previously can be applied to determine optimal values for one or more discharge chamber design parameters is presented. The experimental approach being used to study the plasma potential field and charge-exchange ion production rate downstream of the accelerator grid of an ion thruster is discussed and preliminary results are presented.

Comparison of different coatings in solid-phase microextraction for the determination of organochlorine pesticides in ground water.

PubMed

Pérez-Trujillo, J P; Frías, S; Conde, J E; Rodríguez-Delgado, M A

2002-07-19

A solid-phase microextraction (SPME) procedure using three commercialised fibers (Carbowax-divinylbenzene, Carboxen-polydimethylsiloxane and divinylbenzene-Carboxen-polydimethylsiloxane) is presented for the determination of a selected group of organochlorine compounds in water samples. The extraction performances of these compounds were compared using fibers with two and three coatings. The optimal experimental procedures for the adsorption and desorption of pesticides were determined. The limits of detection with the divinylbenzene-Carboxen-polydimethylsiloxane fiber at levels below ng l(-1) were similar or lower than values presented in the literature for several of these compounds using polydimethylsiloxane fiber. The advantages of using this fiber, such as no salt addition, are discussed. Finally, the optimised procedures were applied successfully for the determination of these compounds in polluted ground water samples.

Sensorless Control of Permanent Magnet Machine for NASA Flywheel Technology Development

NASA Technical Reports Server (NTRS)

Kenny, Barbara H.; Kascak, Peter E.

2002-01-01

This paper describes the position sensorless algorithms presently used in the motor control for the NASA "in-house" development work of the flywheel energy storage system. At zero and low speeds a signal injection technique, the self-sensing method, is used to determine rotor position. At higher speeds, an open loop estimate of the back EMF of the machine is made to determine the rotor position. At start up, the rotor is set to a known position by commanding dc into one of the phase windings. Experimental results up to 52,000 rpm are presented.

Steel Fibers Reinforced Concrete Pipes - Experimental Tests and Numerical Simulation

NASA Astrophysics Data System (ADS)

Doru, Zdrenghea

2017-10-01

The paper presents in the first part a state of the art review of reinforced concrete pipes used in micro tunnelling realised through pipes jacking method and design methods for steel fibres reinforced concrete. In part two experimental tests are presented on inner pipes with diameters of 1410mm and 2200mm, and specimens (100x100x500mm) of reinforced concrete with metal fibres (35 kg / m3). In part two experimental tests are presented on pipes with inner diameters of 1410mm and 2200mm, and specimens (100x100x500mm) of reinforced concrete with steel fibres (35 kg / m3). The results obtained are analysed and are calculated residual flexural tensile strengths which characterise the post-cracking behaviour of steel fibres reinforced concrete. In the third part are presented numerical simulations of the tests of pipes and specimens. The model adopted for the pipes test was a three-dimensional model and loads considered were those obtained in experimental tests at reaching breaking forces. Tensile stresses determined were compared with mean flexural tensile strength. To validate tensile parameters of steel fibres reinforced concrete, experimental tests of the specimens were modelled with MIDAS program to reproduce the flexural breaking behaviour. To simulate post - cracking behaviour was used the method σ — ε based on the relationship stress - strain, according to RILEM TC 162-TDF. For the specimens tested were plotted F — δ diagrams, which have been superimposed for comparison with the similar diagrams of experimental tests. The comparison of experimental results with those obtained from numerical simulation leads to the following conclusions: - the maximum forces obtained by numerical calculation have higher values than the experimental values for the same tensile stresses; - forces corresponding of residual strengths have very similar values between the experimental and numerical calculations; - generally the numerical model estimates a breaking force greater than that obtained in the experimental tests. Experimental and numerical studies are used to establish the residual characteristic flexural tensile strength minimum guaranteed and limits of applicability of concrete pipes reinforced with steel fibres used in various field and loading situations.

Analysis of dynamic properties for a composite robotic arm at intermediate strain rate

NASA Astrophysics Data System (ADS)

Lin, Jin-Chein

The dynamic mechanical properties of any structure are governed by the storage moduli representing the stiffness and loss moduli representing the internal damping capacity. The dynamic mechanical behavior of a graphite epoxy composite laminate in flexural vibration has been investigated. This study presents the results of a theoretical and experimental effort to determine the dynamic properties of multilaminate composites. The effects of fiber orientation and vibration frequency for both unidirectional tape and Kevlar fabric were studied both analytically and experimentally. Measurement of storage and loss moduli were presented for laminated double cantilever beams of fiber reinforced composite with frequency range from 8 to 1230 Hz (up to 5th mode).

Semi-Empirical Modeling of SLD Physics

NASA Technical Reports Server (NTRS)

Wright, William B.; Potapczuk, Mark G.

2004-01-01

The effects of supercooled large droplets (SLD) in icing have been an area of much interest in recent years. As part of this effort, the assumptions used for ice accretion software have been reviewed. A literature search was performed to determine advances from other areas of research that could be readily incorporated. Experimental data in the SLD regime was also analyzed. A semi-empirical computational model is presented which incorporates first order physical effects of large droplet phenomena into icing software. This model has been added to the LEWICE software. Comparisons are then made to SLD experimental data that has been collected to date. Results will be presented for the comparison of water collection efficiency, ice shape and ice mass.

Structural Acoustic Response of a Shape Memory Alloy Hybrid Composite Panel (Lessons Learned)

NASA Technical Reports Server (NTRS)

Turner, Travis L.

2002-01-01

This study presents results from an effort to fabricate a shape memory alloy hybrid composite (SMAHC) panel specimen and test the structure for dynamic response and noise transmission characteristics under the action of thermal and random acoustic loads. A method for fabricating a SMAHC laminate with bi-directional SMA reinforcement is described. Glass-epoxy unidirectional prepreg tape and Nitinol ribbon comprise the material system. Thermal activation of the Nitinol actuators was achieved through resistive heating. The experimental hardware required for mechanical support of the panel/actuators and for establishing convenient electrical connectivity to the actuators is presented. Other experimental apparatus necessary for controlling the panel temperature and acquiring structural acoustic data are also described. Deficiency in the thermal control system was discovered in the process of performing the elevated temperature tests. Discussion of the experimental results focuses on determining the causes for the deficiency and establishing means for rectifying the problem.

Structural acoustic response of a shape memory alloy hybrid composite panel (lessons learned)

NASA Astrophysics Data System (ADS)

Turner, Travis L.

2002-07-01

This study presents results from an effort to fabricate a shape memory alloy hybrid composite (SMAHC) panel specimen and test the structure for dynamic response and noise transmission characteristics under the action of thermal and random acoustic loads. A method for fabricating a SMAHC laminate with bi-directional SMA reinforcement is described. Glass-epoxy unidirectional prepreg tape and Nitinol ribbon comprise the material system. Thermal activation of the Nitinol actuators was achieved through resistive heating. The experimental hardware required for mechanical support of the panel/actuators and for establishing convenient electrical connectivity to the actuators is presented. Other experimental apparatus necessary for controlling the panel temperature and acquiring structural acoustic data are also described. Deficiency in the thermal control system was discovered in the process of performing the elevated temperature tests. Discussion of the experimental results focuses on determining the causes for the deficiency and establishing means for rectifying the problem.

Crystal structure of minoxidil at low temperature and polymorph prediction.

PubMed

Martín-Islán, Africa P; Martín-Ramos, Daniel; Sainz-Díaz, C Ignacio

2008-02-01

An experimental and theoretical investigation on crystal forms of the popular and ubiquitous pharmaceutical Minoxidil is presented here. A new crystallization method is presented for Minoxidil (6-(1-piperidinyl)-2,4-pyrimidinediamide 3-oxide) in ethanol-poly(ethylene glycol), yielding crystals with good quality. The crystal structure is determined at low temperature, with a final R value of 0.035, corresponding to space group P2(1) (monoclinic) with cell dimensions a = 9.357(1) A, b = 8.231(1) A, c = 12.931(2) A, and beta = 90.353(4) degrees . Theoretical calculations of the molecular structure of Minoxidil are set forward using empirical force fields and quantum-mechanical methods. A theoretical prediction for Minoxidil crystal structure shows many possible polymorphs. The predicted crystal structures are compared with X-ray experimental data obtained in our laboratory, and the experimental crystal form is found to be one of the lowest energy polymorphs.

Grain reconstruction of porous media: application to a low-porosity Fontainebleau sandstone.

PubMed

Thovert, J F; Yousefian, F; Spanne, P; Jacquin, C G; Adler, P M

2001-06-01

The fundamental issue of reconstructing a porous medium is examined anew in this paper, thanks to a sample of low-porosity Fontainebleau sandstone that has been analyzed by computed microtomography. Various geometric properties are determined on the experimental sample. A statistical property, namely, the probability density of the covering radius, is determined. This is used in order to reconstruct a porous medium by means of a Poissonian generation of polydisperse spheres. In a second part, the properties of the real experimental sample and of the reconstructed one are compared. The most important success of the present reconstruction technique is the fact that the numerical sample percolates despite its low porosity. Moreover, other geometrical features and conductivity are found to be in good agreement.

Optimal Experiment Design for Thermal Characterization of Functionally Graded Materials

NASA Technical Reports Server (NTRS)

Cole, Kevin D.

2003-01-01

The purpose of the project was to investigate methods to accurately verify that designed , materials meet thermal specifications. The project involved heat transfer calculations and optimization studies, and no laboratory experiments were performed. One part of the research involved study of materials in which conduction heat transfer predominates. Results include techniques to choose among several experimental designs, and protocols for determining the optimum experimental conditions for determination of thermal properties. Metal foam materials were also studied in which both conduction and radiation heat transfer are present. Results of this work include procedures to optimize the design of experiments to accurately measure both conductive and radiative thermal properties. Detailed results in the form of three journal papers have been appended to this report.

Calculation of Optical Parameters of Liquid Crystals

NASA Astrophysics Data System (ADS)

Kumar, A.

2007-12-01

Validation of a modified four-parameter model describing temperature effect on liquid crystal refractive indices is being reported in the present article. This model is based upon the Vuks equation. Experimental data of ordinary and extraordinary refractive indices for two liquid crystal samples MLC-9200-000 and MLC-6608 are used to validate the above-mentioned theoretical model. Using these experimental data, birefringence, order parameter, normalized polarizabilities, and the temperature gradient of refractive indices are determined. Two methods: directly using birefringence measurements and using Haller's extrapolation procedure are adopted for the determination of order parameter. Both approches of order parameter calculation are compared. The temperature dependences of all these parameters are discussed. A close agreement between theory and experiment is obtained.

Piezo-optic tensor of crystals from quantum-mechanical calculations.

PubMed

Erba, A; Ruggiero, M T; Korter, T M; Dovesi, R

2015-10-14

An automated computational strategy is devised for the ab initio determination of the full fourth-rank piezo-optic tensor of crystals belonging to any space group of symmetry. Elastic stiffness and compliance constants are obtained as numerical first derivatives of analytical energy gradients with respect to the strain and photo-elastic constants as numerical derivatives of analytical dielectric tensor components, which are in turn computed through a Coupled-Perturbed-Hartree-Fock/Kohn-Sham approach, with respect to the strain. Both point and translation symmetries are exploited at all steps of the calculation, within the framework of periodic boundary conditions. The scheme is applied to the determination of the full set of ten symmetry-independent piezo-optic constants of calcium tungstate CaWO4, which have recently been experimentally reconstructed. Present calculations unambiguously determine the absolute sign (positive) of the π61 constant, confirm the reliability of 6 out of 10 experimentally determined constants and provide new, more accurate values for the remaining 4 constants.

Piezo-optic tensor of crystals from quantum-mechanical calculations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Erba, A., E-mail: alessandro.erba@unito.it; Dovesi, R.; Ruggiero, M. T.

2015-10-14

An automated computational strategy is devised for the ab initio determination of the full fourth-rank piezo-optic tensor of crystals belonging to any space group of symmetry. Elastic stiffness and compliance constants are obtained as numerical first derivatives of analytical energy gradients with respect to the strain and photo-elastic constants as numerical derivatives of analytical dielectric tensor components, which are in turn computed through a Coupled-Perturbed-Hartree-Fock/Kohn-Sham approach, with respect to the strain. Both point and translation symmetries are exploited at all steps of the calculation, within the framework of periodic boundary conditions. The scheme is applied to the determination of themore » full set of ten symmetry-independent piezo-optic constants of calcium tungstate CaWO{sub 4}, which have recently been experimentally reconstructed. Present calculations unambiguously determine the absolute sign (positive) of the π{sub 61} constant, confirm the reliability of 6 out of 10 experimentally determined constants and provide new, more accurate values for the remaining 4 constants.« less

Experimental determination of self-heating and self-ignition risks associated with the dusts of agricultural materials commonly stored in silos.

PubMed

Ramírez, Alvaro; García-Torrent, Javier; Tascón, Alberto

2010-03-15

Agricultural products stored in silos, and their dusts, can undergo oxidation and self-heating, increasing the risk of self-ignition and therefore of fires and explosions. The aim of the present work was to determine the thermal susceptibility (as reflected by the Maciejasz index, the temperature of the emission of flammable volatile substances and the combined information provided by the apparent activation energy and the oxidation temperature) of icing sugar, bread-making flour, maize, wheat, barley, alfalfa, and soybean dusts, using experimental methods for the characterisation of different types of coal (no standardised procedure exists for characterising the thermal susceptibility of either coal or agricultural products). In addition, the thermal stability of wheat, i.e., the risk of self-ignition determined as a function of sample volume, ignition temperature and storage time, was determined using the methods outlined in standard EN 15188:2007. The advantages and drawbacks of the different methods used are discussed. (c) 2009 Elsevier B.V. All rights reserved.

Disintegration of a Liquid Jet

NASA Technical Reports Server (NTRS)

Haenlein, A

1932-01-01

This report presents an experimental determination of the process of disintegration and atomization in its simplest form, and the influence of the physical properties of the liquid to be atomized on the disintegration of the jet. Particular attention was paid to the investigation of the process of atomization.

Recovery of rare earth elements (REEs) from uranium containing solutions using biosorption

NASA Astrophysics Data System (ADS)

Botalov, Maxim; Bunkov, Grigory; Rychkov, Vladimir; Kirillov, Evgeny; Kirillov, Sergey; Kuchta, Kerstin; Kücüker, Mehmet Ali; Atamaniuk, Iryna

2017-09-01

Batch testing and determination of appropriate biosorbent and experimental procedures for recovery of REEs from artificial solution as well as the efficiency of the process for recovery of REEs from artificial solution via biosorption are given in present research work.

Predictive Methodology for Delamination Growth in Laminated Composites Part 1: Theoretical Development and Preliminary Experimental Results

DOT National Transportation Integrated Search

1998-04-01

A methodology is presented for the prediction of delamination growth in laminated structures. The methodology is aimed at overcoming computational difficulties in the determination of energy release rate and mode mix. It also addresses the issue that...

Non-linear boundary-layer receptivity due to distributed surface roughness

NASA Technical Reports Server (NTRS)

Amer, Tahani Reffet

1995-01-01

The process by which a laminar boundary layer internalizes the external disturbances in the form of instability waves is known as boundary-layer receptivity. The objective of the present research was to determine the effect of acoustic excitation on boundary-layer receptivity for a flat plate with distributed variable-amplitude surface roughness through measurements with a hot-wire probe. Tollmien-Schlichting mode shapes due to surface roughness receptivity have also been determined, analyzed, and shown to be in agreement with theory and other experimental work. It has been shown that there is a linear relationship between the surface roughness and receptivity for certain roughness configurations with constant roughness wavelength. In addition, strong non-linear receptivity effects exist for certain surface roughness configurations over a band where the surface roughness and T-S wavelength are matched. The results from the present experiment follow the trends predicted by theory and other experimental work for linear receptivity. In addition, the results show the existence of non-linear receptivity effects for certain combinations of surface roughness elements.

An analytical-numerical approach for parameter determination of a five-parameter single-diode model of photovoltaic cells and modules

NASA Astrophysics Data System (ADS)

Hejri, Mohammad; Mokhtari, Hossein; Azizian, Mohammad Reza; Söder, Lennart

2016-04-01

Parameter extraction of the five-parameter single-diode model of solar cells and modules from experimental data is a challenging problem. These parameters are evaluated from a set of nonlinear equations that cannot be solved analytically. On the other hand, a numerical solution of such equations needs a suitable initial guess to converge to a solution. This paper presents a new set of approximate analytical solutions for the parameters of a five-parameter single-diode model of photovoltaic (PV) cells and modules. The proposed solutions provide a good initial point which guarantees numerical analysis convergence. The proposed technique needs only a few data from the PV current-voltage characteristics, i.e. open circuit voltage Voc, short circuit current Isc and maximum power point current and voltage Im; Vm making it a fast and low cost parameter determination technique. The accuracy of the presented theoretical I-V curves is verified by experimental data.

Influence of cutting data on surface quality when machining 17-4 PH stainless steel

NASA Astrophysics Data System (ADS)

Popovici, T. D.; Dijmărescu, M. R.

2017-08-01

The aim of the research presented in this paper is to analyse the cutting data influence upon surface quality for 17-4 PH stainless steel milling machining. The cutting regime parameters considered for the experiments were established using cutting regimes from experimental researches or from industrial conditions as basis, within the recommended ranges. The experimental program structure was determined by taking into account compatibility and orthogonality conditions, minimal use of material and labour. The machined surface roughness was determined by measuring the Ra roughness parameter, followed by surface profile registration in the form of graphics which were saved on a computer with MarSurf PS1Explorer software. Based on Ra roughness parameter, maximum values were extracted from these graphics and the influence charts of the cutting regime parameters upon surface roughness were traced using Microsoft Excel software. After a thorough analysis of the resulting data, relevant conclusions were drawn, presenting the interdependence between the surface roughness of the machined 17-4 PH samples and the cutting data variation.

Application of the correlation constrained multivariate curve resolution alternating least-squares method for analyte quantitation in the presence of unexpected interferences using first-order instrumental data.

PubMed

Goicoechea, Héctor C; Olivieri, Alejandro C; Tauler, Romà

2010-03-01

Correlation constrained multivariate curve resolution-alternating least-squares is shown to be a feasible method for processing first-order instrumental data and achieve analyte quantitation in the presence of unexpected interferences. Both for simulated and experimental data sets, the proposed method could correctly retrieve the analyte and interference spectral profiles and perform accurate estimations of analyte concentrations in test samples. Since no information concerning the interferences was present in calibration samples, the proposed multivariate calibration approach including the correlation constraint facilitates the achievement of the so-called second-order advantage for the analyte of interest, which is known to be present for more complex higher-order richer instrumental data. The proposed method is tested using a simulated data set and two experimental data systems, one for the determination of ascorbic acid in powder juices using UV-visible absorption spectral data, and another for the determination of tetracycline in serum samples using fluorescence emission spectroscopy.

Distribution of opiate alkaloids in brain tissue of experimental animals

PubMed Central

Pilija, Vladimir; Mimica-Dukic, Neda; Budakov, Branislav; Cvjeticanin, Stanko

2012-01-01

The present study examined regional distribution of opiate alkaloids from seized heroin in brain regions of experimental animals in order to select parts with the highest content of opiates. Their analysis should contribute to resolve causes of death due to heroin intake. The tests were performed at different time periods (5, 15, 45 and 120 min) after male and female Wistar rats were treated with seized heroin. Opiate alkaloids (codeine, morphine, acetylcodeine, 6-acetylmorphine and 3,6-diacetylmorphine) were quantitatively determined in brain regions known for their high concentration of µ-opiate receptors: cortex, brainstem, amygdala and basal ganglia, by using gas chromatography–mass spectrometry (GC–MS). The highest content of opiate alkaloids in the brain tissue of female animals was found 15 min and in male animals 45 min after treatment. The highest content of opiates was determined in the basal ganglia of the animals of both genders, indicating that this part of brain tissue presents a reliable sample for identifying and assessing contents of opiates after heroin intake. PMID:23554560

Measurements and Experimental Database Review for Laminar Flame Speed Premixed Ch4/Air Flames

NASA Astrophysics Data System (ADS)

Zubrilin, I. A.; Matveev, S. S.; Matveev, S. G.; Idrisov, D. V.

2018-01-01

Laminar flame speed (SL ) of CH4 was determined at atmospheric pressure and initial gas temperatures in range from 298 to 358 K. The heat flux method was employed to measure the flame speed in non-stretched flames. The kinetic mechanism GRI 3.0 [1] were used to simulate SL . The measurements were compared with available literature results. The data determined with the heat flux method agree with some previous burner measurements and disagree with the data from some vessel closed method and counterflow method. The GRI 3.0 mechanism was able to reproduce the present experiments. Laminar flame speed was determined at pressures range from of 1 to 20 atmospheres through mechanism GRI 3.0. Based on experimental data and calculations was obtained SL dependence on pressure and temperature. The resulting of dependence recommended use during the numerical simulation of methane combustion.

Dissociation energies of the hydrogen-bonded dimers RCN-HF (R = CH3, HCC) determined by rotational spectroscopy

NASA Astrophysics Data System (ADS)

Legon, A. C.; Millen, D. J.; North, Hazel M.

1987-03-01

The zero-point and equilibrium dissociation energies (D0 and De) of the hydrogen-bonded dimers CH3CN-HF and HCCCN-HF are determined experimentally on the basis of absolute intensity measurements of selected rotational transitions. A Stark-modulated microwave spectrometer is employed with the cooled absorption cell described by Legon et al. (1980). The results are presented in tables and analyzed. Energies determined are D0 = 26.1(0.6) kJ/mol and De = 29.0(0.9) kJ/mol for CH3CN-HF and D0 = 20.4(0.7) kJ/mol and De = 23.4(0.9) kJ/mol for HCCCN-HF. Theoretical De values calculated using the Morse potential function are found to be in much better agreement with the experimental results than those calculated with the Lennard-Jones potential function.

The experimental determination of atmospheric absorption from aircraft acoustic flight tests

NASA Technical Reports Server (NTRS)

Miller, R. L.; Oncley, P. B.

1971-01-01

A method for determining atmospheric absorption coefficients from acoustic flight test data is presented. Measurements from five series of acoustic flight tests were included in the study. The number of individual flights totaled 24: six Boeing 707 flights performed in May 1969 in connection with the turbofan nacelle modification program, eight flights from Boeing tests conducted during the same period, and 10 flights of the Boeing 747 airplane. The effects of errors in acoustic, meteorological, and aircraft performance and position measurements are discussed. Tabular data of the estimated sample variance of the data for each test are given for source directivity angles from 75 deg to 120 deg and each 1/3-octave frequency band. Graphic comparisons are made of absorption coefficients derived from ARP 866, using atmospheric profile data, with absorption coefficients determined by the experimental method described in the report.

Determination of Residual Stress in Composite Materials Using Ultrasonic Waves

NASA Technical Reports Server (NTRS)

Rokhlin, S. I.

1997-01-01

The performance of high temperature composites can be significantly affected by the presence of residual stresses. These stresses arise during cooling processes from fabrication to room temperature due to mismatch of thermal expansion coefficients between matrix and fiber materials. This effect is especially pronounced in metal matrix and intermetallic composites. It can lead to plastic deformations, matrix cracking and fiber/matrix interface debonding. In this work the feasibility of ultrasonic techniques for residual stress assessment in composites is addressed. A novel technique for absolute stress determination in orthotropic materials from angular dependencies of ultrasonic velocities is described. The technique is applicable for determination of both applied and residual stresses and does not require calibration measurements on a reference sample. The important advantage of this method is that stress is determined simultaneously with stress-dependent elastic constants and is thus decoupled from the material texture. It is demonstrated that when the principal plane stress directions coincide with acoustical axes, the angular velocity data in the plane perpendicular to the stress plane may be used to determine both stress components. When the stress is off the acoustical axes, the shear and the difference of the normal stress components may be determined from the angular dependence of group velocities in the plane of stresses. Synthetic sets of experimental data corresponding to materials with different anisotropy and stress levels are used to check the applicability of the technique. The method is also verified experimentally. A high precision ultrasonic wave transmission technique is developed to measure angular dependence of ultrasonic velocities. Examples of stress determination from experimental velocity data are given. A method is presented for determination of velocities of ultrasonic waves propagating through the composite material with residual stresses. It is based on the generalized self-consistent multiple scattering model. Calculation results for longitudinal and shear ultrasonic wave velocities propagating perpendicular to the fibers direction in SCS-6/Ti composite with and without residual stresses are presented. They show that velocity changes due to presence of stresses are of order 1%.

Optically induced metastability in Cu(In,Ga)Se 2

DOE PAGES

Jensen, S. A.; Kanevce, A.; Mansfield, L. M.; ...

2017-10-23

Cu(In,Ga)Se 2 (CIGS) is presently the most efficient thin-film photovoltaic technology with efficiencies exceeding 22%. An important factor impacting the efficiency is metastability, where material changes occur over timescales of up to weeks during light exposure. A previously proposed (V Se -V Cu ) divacancy model presents a widely accepted explanation. We present experimental evidence for the optically induced metastability transition and expand the divacancy model with first-principles calculations. Using photoluminescence excitation spectroscopy, we identify a sub-bandgap optical transition that severely deteriorates the carrier lifetime. This is in accordance with the expanded divacancy model, which predicts that states below themore » conduction band are responsible for the metastability change. We determine the density–capture cross-section product of the induced lifetime-limiting states and evaluate their impact on device performance. The experimental and theoretical findings presented can allow assessment of metastability characteristics of leading thin-film photovoltaic technologies.« less

Electron Impact Ionization Cross Sections in Rb and Cs.

NASA Astrophysics Data System (ADS)

Reddish, T. J.; Lukomski, M.; Sutton, S.; Kedzierski, W.; McConkey, J. W.; Bartschat, K.; Bartlett, P. L.; Stelbovics, A. T.; Bray, I.

2006-05-01

We present a new atom trapping technique for determining absolute, total ionisation cross sections (TICS) out of an excited atom. The novel feature of this method is in utilizing Doppler cooling of neutral atoms to determine ionisation cross sections. This fluorescence-monitoring experiment, which is a variant of the `trap loss' technique, has enabled us to obtain the experimental electron impact ionisation cross sections out of the Cs 6^2P3/2 excited state between 7 - 400 eV. New CCC, R-Matrix with Pseudo-States (RMPS), and Born approximation single ionisation cross sections (SICS) are also presented for both the ground and excited states of Cs and Rb, and compared with the available experimental data. The comparison of the results reveals the importance of the autoionisation and multiple ionisation contributions to the TICS. The autoionisation contribution appears to be substantial for ionisation out of the Cs 6^2P and Rb 5^2P excited states; ˜ 3-4 larger than the direct ionisation contribution predicted by CCC at ˜ 30-50 eV. This surprising result shows the importance of multi-electron processes in determining the ionisation cross sections of heavy alkali atoms.

Refractive-index profile and physical process determination in thick gratings in electrooptic crystals

NASA Technical Reports Server (NTRS)

Su, S. F.; Gaylord, T. K.

1976-01-01

A method for determining the refractive index profile of thick phase gratings in linear electrooptic crystals is presented. This method also determines the effective photovoltaic electric field and the relative contributions of diffusion and drift during hologram recording. The method requires only a knowledge of the modulation ratio during hologram recording and the fundamental and the higher-order diffraction efficiencies of the grating. As an illustration of the method, the refractive index profile, the effective photovoltaic field, and the relative contributions of diffusion and drift are determined from experimental measurements for a lithium niobate holographic grating.

Antioxidant Capacity: Experimental Determination by EPR Spectroscopy and Mathematical Modeling.

PubMed

Polak, Justyna; Bartoszek, Mariola; Chorążewski, Mirosław

2015-07-22

A new method of determining antioxidant capacity based on a mathematical model is presented in this paper. The model was fitted to 1000 data points of electron paramagnetic resonance (EPR) spectroscopy measurements of various food product samples such as tea, wine, juice, and herbs with Trolox equivalent antioxidant capacity (TEAC) values from 20 to 2000 μmol TE/100 mL. The proposed mathematical equation allows for a determination of TEAC of food products based on a single EPR spectroscopy measurement. The model was tested on the basis of 80 EPR spectroscopy measurements of herbs, tea, coffee, and juice samples. The proposed model works for both strong and weak antioxidants (TEAC values from 21 to 2347 μmol TE/100 mL). The determination coefficient between TEAC values obtained experimentally and TEAC values calculated with proposed mathematical equation was found to be R(2) = 0.98. Therefore, the proposed new method of TEAC determination based on a mathematical model is a good alternative to the standard EPR method due to its being fast, accurate, inexpensive, and simple to perform.

Determination of parameters of the Johnson-Cook model for the description of deformation and fracture of titanium alloys

NASA Astrophysics Data System (ADS)

Buzyurkin, A. E.; Gladky, I. L.; Kraus, E. I.

2015-03-01

Stress-strain curves of dynamic loading of VT6, OT4, and OT4-0 titanium-based alloys are constructed on the basis of experimental data, and the Johnson-Cook model parameters are determined. Results of LS-DYNA simulations of the processes of deformation and fracture of the fan casing after its high-velocity impact with a fan blade simulator are presented.

A new experimental method for determining local airloads on rotor blades in forward flight

NASA Astrophysics Data System (ADS)

Berton, E.; Maresca, C.; Favier, D.

This paper presents a new approach for determining local airloads on helicopter rotor blade sections in forward flight. The method is based on the momentum equation in which all the terms are expressed by means of the velocity field measured by a laser Doppler velocimeter. The relative magnitude of the different terms involved in the momentum and Bernoulli equations is estimated and the results are encouraging.

Numerical Simulation of Internal Heat Transfer Phenomena Occurring During De-Icing of Aircraft Components

NASA Technical Reports Server (NTRS)

DeWitt, Keneth J.

1996-01-01

An experimental study to determine the convective heat transfer coefficient from castings made from ice-roughened plates is reported. A corresponding topic, 'Measurements of the Convective Heat Transfer Coefficient from Ice Roughened Surfaces in Parallel and Accelerated Flows,' is presented.

Approaching the Limit in Atomic Spectrochemical Analysis.

ERIC Educational Resources Information Center

Hieftje, Gary M.

1982-01-01

To assess the ability of current analytical methods to approach the single-atom detection level, theoretical and experimentally determined detection levels are presented for several chemical elements. A comparison of these methods shows that the most sensitive atomic spectrochemical technique currently available is based on emission from…

Physics Notes.

ERIC Educational Resources Information Center

School Science Review, 1983

1983-01-01

Discusses the Rugby clock as a source of project material, use of ZX81 for experimental science, computer dice analog, oil recovery from reservoirs, and computer simulation of Thompson's experiment for determining e/m for an electron. Activities/procedures are provided when applicable. Also presents questions (and answers) related to time-coded…

An experimentally validated network of nine haematopoietic transcription factors reveals mechanisms of cell state stability

PubMed Central

Schütte, Judith; Wang, Huange; Antoniou, Stella; Jarratt, Andrew; Wilson, Nicola K; Riepsaame, Joey; Calero-Nieto, Fernando J; Moignard, Victoria; Basilico, Silvia; Kinston, Sarah J; Hannah, Rebecca L; Chan, Mun Chiang; Nürnberg, Sylvia T; Ouwehand, Willem H; Bonzanni, Nicola; de Bruijn, Marella FTR; Göttgens, Berthold

2016-01-01

Transcription factor (TF) networks determine cell-type identity by establishing and maintaining lineage-specific expression profiles, yet reconstruction of mammalian regulatory network models has been hampered by a lack of comprehensive functional validation of regulatory interactions. Here, we report comprehensive ChIP-Seq, transgenic and reporter gene experimental data that have allowed us to construct an experimentally validated regulatory network model for haematopoietic stem/progenitor cells (HSPCs). Model simulation coupled with subsequent experimental validation using single cell expression profiling revealed potential mechanisms for cell state stabilisation, and also how a leukaemogenic TF fusion protein perturbs key HSPC regulators. The approach presented here should help to improve our understanding of both normal physiological and disease processes. DOI: http://dx.doi.org/10.7554/eLife.11469.001 PMID:26901438

An experimental investigation of a cold jet emitting from a body of revolution into a subsonic free stream

NASA Technical Reports Server (NTRS)

Ousterhout, D. S.

1972-01-01

An experimental program was undertaken to determine the pressure distribution induced on aerodynamic bodies by a subsonic cold jet exhausting normal to the body surface and into a subsonic free stream. The investigation was limited to two bodies with single exhaust jets a flat plate at zero angle of attack with respect to the free-stream flow and a cylinder, fitted with a conical nose, with the longitudinal axis alined with the free-stream flow. Experimental data were obtained for free-stream velocity to jet velocity ratios between 0.3 and 0.5. The experimental data are presented in tabular form with appropriate graphs to indicate pressure coefficient contours, pressure coefficient decay, pitching-moment characteristics, and lift characteristics.

DaMoScope and its internet graphics for the visual control of adjusting mathematical models describing experimental data

DOE Office of Scientific and Technical Information (OSTI.GOV)

Belousov, V. I.; Ezhela, V. V.; Kuyanov, Yu. V., E-mail: Yu.Kuyanov@gmail.com

The experience of using the dynamic atlas of the experimental data and mathematical models of their description in the problems of adjusting parametric models of observable values depending on kinematic variables is presented. The functional possibilities of an image of a large number of experimental data and the models describing them are shown by examples of data and models of observable values determined by the amplitudes of elastic scattering of hadrons. The Internet implementation of an interactive tool DaMoScope and its interface with the experimental data and codes of adjusted parametric models with the parameters of the best description ofmore » data are schematically shown. The DaMoScope codes are freely available.« less

A study of the dynamic tire properties over a range of tire constructions

NASA Technical Reports Server (NTRS)

Nybakken, G. H.; Dodge, R. N.; Clark, S. K.

1973-01-01

The dynamic properties of four model aircraft tires of various construction were evaluated experimentally and compared with available theory. The experimental investigation consisted of measuring the cornering force and the self-aligning torque developed by the tires undergoing sinusoidal steering inputs while operating on a small scale, road-wheel tire testing apparatus. The force and moment data from the different tires are compared with both finite- and point-contact patch string theory predictions. In general, agreement between finite contact patch theory and experimental observation is good. A modified string theory is also presented in which coefficients for cornering force and self-aligning torque are determined separately. This theory improves the correspondence between the experimental and analytical data, particularly on tires with relatively high self-aligning torques.

Crack identification method in beam-like structures using changes in experimentally measured frequencies and Particle Swarm Optimization

NASA Astrophysics Data System (ADS)

Khatir, Samir; Dekemele, Kevin; Loccufier, Mia; Khatir, Tawfiq; Abdel Wahab, Magd

2018-02-01

In this paper, a technique is presented for the detection and localization of an open crack in beam-like structures using experimentally measured natural frequencies and the Particle Swarm Optimization (PSO) method. The technique considers the variation in local flexibility near the crack. The natural frequencies of a cracked beam are determined experimentally and numerically using the Finite Element Method (FEM). The optimization algorithm is programmed in MATLAB. The algorithm is used to estimate the location and severity of a crack by minimizing the differences between measured and calculated frequencies. The method is verified using experimentally measured data on a cantilever steel beam. The Fourier transform is adopted to improve the frequency resolution. The results demonstrate the good accuracy of the proposed technique.

An experimental and numerical study of endwall heat transfer in a turbine blade cascade including tangential heat conduction analysis

NASA Astrophysics Data System (ADS)

Ratto, Luca; Satta, Francesca; Tanda, Giovanni

2018-06-01

This paper presents an experimental and numerical investigation of heat transfer in the endwall region of a large scale turbine cascade. The steady-state liquid crystal technique has been used to obtain the map of the heat transfer coefficient for a constant heat flux boundary condition. In the presence of two- and three-dimensional flows with significant spatial variations of the heat transfer coefficient, tangential heat conduction could lead to error in the heat transfer coefficient determination, since local heat fluxes at the wall-to-fluid interface tend to differ from point to point and surface temperatures to be smoothed out, thus making the uniform-heat-flux boundary condition difficult to be perfectly achieved. For this reason, numerical simulations of flow and heat transfer in the cascade including the effect of tangential heat conduction inside the endwall have been performed. The major objective of numerical simulations was to investigate the influence of wall heat conduction on the convective heat transfer coefficient determined during a nominal iso-flux heat transfer experiment and to interpret possible differences between numerical and experimental heat transfer results. Results were presented and discussed in terms of local Nusselt number and a convenient wall heat flux function for two values of the Reynolds number (270,000 and 960,000).

Determining Off-Cycle Fuel Economy Benefits of 2-Layer HVAC Technology

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wood, Eric W; Moniot, Matthew; Jehlik, Forrest

This work presents a methodology to determine the off-cycle fuel economy benefit of a 2-Layer HVAC system which reduces ventilation and heat rejection losses of the heater core versus a vehicle using a standard system. Experimental dynamometer tests using EPA drive cycles over a broad range of ambient temperatures were conducted on a highly instrumented 2016 Lexus RX350 (3.5L, 8 speed automatic). These tests were conducted to measure differences in engine efficiency caused by changes in engine warmup due to the 2-Layer HVAC technology in use versus the technology being disabled (disabled equals fresh air-considered as the standard technology baseline).more » These experimental datasets were used to develop simplified response surface and lumped capacitance vehicle thermal models predictive of vehicle efficiency as a function of thermal state. These vehicle models were integrated into a database of measured on road testing and coupled with U.S. typical meteorological data to simulate vehicle efficiency across seasonal thermal and operational conditions for hundreds of thousands of drive cycles. Fuel economy benefits utilizing the 2-Layer HVAC technology are presented in addition to goodness of fit statistics of the modeling approach relative to the experimental test data.« less

Determination of the structural damping coefficients of six full-scale helicopter rotor blades of different materials and methods of construction

NASA Technical Reports Server (NTRS)

Gibson, Frederick W

1956-01-01

Results of an experimental investigation of the structural damping of six full-scale helicopter rotor blades, made to determine the variation of structural damping with materials and methods of construction, are presented. The damping of the blades was determined for the first three flapwise bending modes, first chordwise bending mode, and first torsion mode. The contribution of structural damping to the total damping of the blades is discussed for several aerodynamic conditions in order to point out situations where structural damping is significant.

The determination of the constitutive parameters of a medium with application to a reinforced concrete pad

NASA Technical Reports Server (NTRS)

Poggio, A. J.; Burke, G. L.; Pennock, S. T.

1995-01-01

This report describes the experimental and analytical efforts performed to determine the constitutive parameters of a reinforced concrete pad on which an aircraft (the NASA Boeing 757) was parked while its internal electromagnetic environment was measured. This concrete pad is part of the Large Electromagnetic System-Level Illuminator (LESLI) test facility at the Phillips Laboratory, Kirtland Air Force Base, New Mexico. The relative dielectric constant, conductivity, index of refraction, and reflection coefficient have been determined over the frequency range of 0 to 300 MHz and are presented.

Experimental setup for the determination of the correction factors of the neutron doseratemeters in fast neutron fields

DOE Office of Scientific and Technical Information (OSTI.GOV)

Iliescu, Elena; Bercea, Sorin; Dudu, Dorin

2013-12-16

The use of the U-120 Cyclotron of the IFIN-HH allowed to perform a testing bench with fast neutrons in order to determine the correction factors of the doseratemeters dedicated to neutron measurement. This paper deals with researchers performed in order to develop the irradiation facility testing the fast neutrons flux generated at the Cyclotron. This facility is presented, together with the results obtain in determining the correction factor for a doseratemeter dedicated to the neutron dose equivalent rate measurement.

DFT and experimental studies of the structure and vibrational spectra of curcumin

NASA Astrophysics Data System (ADS)

Kolev, Tsonko M.; Velcheva, Evelina A.; Stamboliyska, Bistra A.; Spiteller, Michael

The potential energy surface of curcumin [1,7-bis(4-hydroxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione] was explored with the DFT correlation functional B3LYP method using 6-311G* basis. The single-point calculations were performed at levels up to B3LYP/6-311++G**//B3LYP/6-311G*. All isomers were located and relative energies determined. According to the calculation the planar enol form is more stable than the nonplanar diketo form. The results of the optimized molecular structure are presented and compared with the experimental X-ray diffraction. In addition, harmonic vibrational frequencies of the molecule were evaluated theoretically using B3LYP density functional methods. The computed vibrational frequencies were used to determine the types of molecular motions associated with each of the experimental bands observed. Our vibrational data show that in both the solid state and in all studied solutions curcumin exists in the enol form.

Domain-based prediction of the human isoform interactome provides insights into the functional impact of alternative splicing.

PubMed

Ghadie, Mohamed Ali; Lambourne, Luke; Vidal, Marc; Xia, Yu

2017-08-01

Alternative splicing is known to remodel protein-protein interaction networks ("interactomes"), yet large-scale determination of isoform-specific interactions remains challenging. We present a domain-based method to predict the isoform interactome from the reference interactome. First, we construct the domain-resolved reference interactome by mapping known domain-domain interactions onto experimentally-determined interactions between reference proteins. Then, we construct the isoform interactome by predicting that an isoform loses an interaction if it loses the domain mediating the interaction. Our prediction framework is of high-quality when assessed by experimental data. The predicted human isoform interactome reveals extensive network remodeling by alternative splicing. Protein pairs interacting with different isoforms of the same gene tend to be more divergent in biological function, tissue expression, and disease phenotype than protein pairs interacting with the same isoforms. Our prediction method complements experimental efforts, and demonstrates that integrating structural domain information with interactomes provides insights into the functional impact of alternative splicing.

Domain-based prediction of the human isoform interactome provides insights into the functional impact of alternative splicing

PubMed Central

Lambourne, Luke; Vidal, Marc

2017-01-01

Alternative splicing is known to remodel protein-protein interaction networks (“interactomes”), yet large-scale determination of isoform-specific interactions remains challenging. We present a domain-based method to predict the isoform interactome from the reference interactome. First, we construct the domain-resolved reference interactome by mapping known domain-domain interactions onto experimentally-determined interactions between reference proteins. Then, we construct the isoform interactome by predicting that an isoform loses an interaction if it loses the domain mediating the interaction. Our prediction framework is of high-quality when assessed by experimental data. The predicted human isoform interactome reveals extensive network remodeling by alternative splicing. Protein pairs interacting with different isoforms of the same gene tend to be more divergent in biological function, tissue expression, and disease phenotype than protein pairs interacting with the same isoforms. Our prediction method complements experimental efforts, and demonstrates that integrating structural domain information with interactomes provides insights into the functional impact of alternative splicing. PMID:28846689

Clathrate Structure Determination by Combining Crystal Structure Prediction with Computational and Experimental 129Xe NMR Spectroscopy

PubMed Central

Selent, Marcin; Nyman, Jonas; Roukala, Juho; Ilczyszyn, Marek; Oilunkaniemi, Raija; Bygrave, Peter J.; Laitinen, Risto; Jokisaari, Jukka

2017-01-01

Abstract An approach is presented for the structure determination of clathrates using NMR spectroscopy of enclathrated xenon to select from a set of predicted crystal structures. Crystal structure prediction methods have been used to generate an ensemble of putative structures of o‐ and m‐fluorophenol, whose previously unknown clathrate structures have been studied by 129Xe NMR spectroscopy. The high sensitivity of the 129Xe chemical shift tensor to the chemical environment and shape of the crystalline cavity makes it ideal as a probe for porous materials. The experimental powder NMR spectra can be used to directly confirm or reject hypothetical crystal structures generated by computational prediction, whose chemical shift tensors have been simulated using density functional theory. For each fluorophenol isomer one predicted crystal structure was found, whose measured and computed chemical shift tensors agree within experimental and computational error margins and these are thus proposed as the true fluorophenol xenon clathrate structures. PMID:28111848

The Researches on Damage Detection Method for Truss Structures

NASA Astrophysics Data System (ADS)

Wang, Meng Hong; Cao, Xiao Nan

2018-06-01

This paper presents an effective method to detect damage in truss structures. Numerical simulation and experimental analysis were carried out on a damaged truss structure under instantaneous excitation. The ideal excitation point and appropriate hammering method were determined to extract time domain signals under two working conditions. The frequency response function and principal component analysis were used for data processing, and the angle between the frequency response function vectors was selected as a damage index to ascertain the location of a damaged bar in the truss structure. In the numerical simulation, the time domain signal of all nodes was extracted to determine the location of the damaged bar. In the experimental analysis, the time domain signal of a portion of the nodes was extracted on the basis of an optimal sensor placement method based on the node strain energy coefficient. The results of the numerical simulation and experimental analysis showed that the damage detection method based on the frequency response function and principal component analysis could locate the damaged bar accurately.

Experimental and Theoretical Reduction Potentials of Some Biologically Active ortho-Carbonyl para-Quinones.

PubMed

Martínez-Cifuentes, Maximiliano; Salazar, Ricardo; Ramírez-Rodríguez, Oney; Weiss-López, Boris; Araya-Maturana, Ramiro

2017-04-04

The rational design of quinones with specific redox properties is an issue of great interest because of their applications in pharmaceutical and material sciences. In this work, the electrochemical behavior of a series of four p -quinones was studied experimentally and theoretically. The first and second one-electron reduction potentials of the quinones were determined using cyclic voltammetry and correlated with those calculated by density functional theory (DFT) using three different functionals, BHandHLYP, M06-2x and PBE0. The differences among the experimental reduction potentials were explained in terms of structural effects on the stabilities of the formed species. DFT calculations accurately reproduced the first one-electron experimental reduction potentials with R ² higher than 0.94. The BHandHLYP functional presented the best fit to the experimental values ( R ² = 0.957), followed by M06-2x ( R ² = 0.947) and PBE0 ( R ² = 0.942).

Landscape-level impacts of livestock on the diversity of a desert grassland: preliminary results from long-term experimental studies

Treesearch

Charles G. Curtin

2005-01-01

This work is undertaken as a portion of long-term large-scale studies developed to determine how climate and disturbance (primarily fire and grazing) interact to structure desert grasslands. The results presented here are the initial grazing portions of the study. The analysis presented here indicates that following the reintroduction of cattle to the research area in...

The Effects of Concept Maps on the Academic Success and Attitudes of 11th Graders while Teaching Urinary System

ERIC Educational Resources Information Center

Akay, Sumeyye Ozbey; Kaya, Basturk; Kilic, Selda

2012-01-01

The aim of the present study is to support, enrich, and broaden the process of education using concept maps and to determine the effects of concept maps in biology classes on school success, attitude and retention of the knowledge taught. The present study was conducted as an experimental study with pre-test and post-test control groups. The…

Predicting the viscosity of solids using steady-state creep behavior of the fibrous composites semi-theoretically

NASA Astrophysics Data System (ADS)

Monfared, Vahid

A semi-analytical formulation is presented for obtaining the viscosity of solids (such as metals) using the steady state creep model of the short-fiber composites. For achieving this aim, fluid mechanics theory is used for determining the viscosity. Sometimes, obtaining the viscosity is experimentally difficult and intricate. So, the present model may be beneficial to obtain the viscosity of metals.

DEVELOPMENT AND OPTIMIZATION OF GAS-ASSISTED GRAVITY DRAINAGE (GAGD) PROCESS FOR IMPROVED LIGHT OIL RECOVERY

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dandina N. Rao; Subhash C. Ayirala; Madhav M. Kulkarni

This report describes the progress of the project ''Development and Optimization of Gas-Assisted Gravity Drainage (GAGD) Process for Improved Light Oil Recovery'' for the duration of the second project year (October 1, 2003--September 30, 2004). There are three main tasks in this research project. Task 1 is scaled physical model study of GAGD process. Task 2 is further development of vanishing interfacial tension (VIT) technique for miscibility determination. Task 3 is determination of multiphase displacement characteristics in reservoir rocks. In Section I, preliminary design of the scaled physical model using the dimensional similarity approach has been presented. Scaled experiments onmore » the current physical model have been designed to investigate the effect of Bond and capillary numbers on GAGD oil recovery. Experimental plan to study the effect of spreading coefficient and reservoir heterogeneity has been presented. Results from the GAGD experiments to study the effect of operating mode, Bond number and capillary number on GAGD oil recovery have been reported. These experiments suggest that the type of the gas does not affect the performance of GAGD in immiscible mode. The cumulative oil recovery has been observed to vary exponentially with Bond and capillary numbers, for the experiments presented in this report. A predictive model using the bundle of capillary tube approach has been developed to predict the performance of free gravity drainage process. In Section II, a mechanistic Parachor model has been proposed for improved prediction of IFT as well as to characterize the mass transfer effects for miscibility development in reservoir crude oil-solvent systems. Sensitivity studies on model results indicate that provision of a single IFT measurement in the proposed model is sufficient for reasonable IFT predictions. An attempt has been made to correlate the exponent (n) in the mechanistic model with normalized solute compositions present in both fluid phases. IFT measurements were carried out in a standard ternary liquid system of benzene, ethanol and water using drop shape analysis and capillary rise techniques. The experimental results indicate strong correlation among the three thermodynamic properties solubility, miscibility and IFT. The miscibility determined from IFT measurements for this ternary liquid system is in good agreement with phase diagram and solubility data, which clearly indicates the sound conceptual basis of VIT technique to determine fluid-fluid miscibility. Model fluid systems have been identified for VIT experimentation at elevated pressures and temperatures. Section III comprises of the experimental study aimed at evaluating the multiphase displacement characteristics of the various gas injection EOR process performances using Berea sandstone cores. During this reporting period, extensive literature review was completed to: (1) study the gravity drainage concepts, (2) identify the various factors influencing gravity stable gas injection processes, (3) identify various multiphase mechanisms and fluid dynamics operative during the GAGD process, and (4) identify important dimensionless groups governing the GAGD process performance. Furthermore, the dimensional analysis of the GAGD process, using Buckingham-Pi theorem to isolate the various dimensionless groups, as well as experimental design based on these dimensionless quantities have been completed in this reporting period. On the experimental front, recommendations from previous WAG and CGI have been used to modify the experimental protocol. This report also includes results from scaled preliminary GAGD displacements as well as the details of the planned GAGD corefloods for the next quarter. The technology transfer activities have mainly consisted of preparing technical papers, progress reports and discussions with industry personnel for possible GAGD field tests.« less

A study of the accuracy of neutrally buoyant bubbles used as flow tracers in air

NASA Technical Reports Server (NTRS)

Kerho, Michael F.

1993-01-01

Research has been performed to determine the accuracy of neutrally buoyant and near neutrally buoyant bubbles used as flow tracers in air. Theoretical, computational, and experimental results are presented to evaluate the dynamics of bubble trajectories and factors affecting their ability to trace flow-field streamlines. The equation of motion for a single bubble was obtained and evaluated using a computational scheme to determine the factors which affect a bubble's trajectory. A two-dimensional experiment was also conducted to experimentally determine bubble trajectories in the stagnation region of NACA 0012 airfoil at 0 deg angle of attack using a commercially available helium bubble generation system. Physical properties of the experimental bubble trajectories were estimated using the computational scheme. These properties included the density ratio and diameter of the individual bubbles. the helium bubble system was then used to visualize and document the flow field about a 30 deg swept semispan wing with simulated glaze ice. Results were compared to Navier-Stokes calculations and surface oil flow visualization. The theoretical and computational analysis have shown that neutrally buoyant bubbles will trace even the most complex flow patterns. Experimental analysis revealed that the use of bubbles to trace flow patterns should be limited to qualitative measurements unless care is taken to ensure neutral buoyancy. This is due to the difficulty in the production of neutrally buoyant bubbles.

Using dust as probes to determine sheath extent and structure

NASA Astrophysics Data System (ADS)

Douglass, Angela; Land, V.; Qiao, K.; Matthews, L.; Hyde, T.

2016-08-01

Two in situ experimental methods are presented in which dust particles are used to determine the extent of the sheath and gain information about the time-averaged electric force profile within a radio frequency (RF) plasma sheath. These methods are advantageous because they are not only simple and quick to carry out, but they also can be performed using standard dusty plasma experimental equipment. In the first method, dust particles are tracked as they fall through the plasma towards the lower electrode. These trajectories are then used to determine the electric force on the particle as a function of height as well as the extent of the sheath. In the second method, dust particle levitation height is measured across a wide range of RF voltages. Similarities were observed between the two experiments, but in order to understand the underlying physics behind these observations, the same conditions were replicated using a self-consistent fluid model. Through comparison of the fluid model and experimental results, it is shown that the particles exhibiting a levitation height that is independent of RF voltage indicate the sheath edge - the boundary between the quasineutral bulk plasma and the sheath. Therefore, both of these simple and inexpensive, yet effective, methods can be applied across a wide range of experimental parameters in any ground-based RF plasma chamber to gain useful information regarding the sheath, which is needed for interpretation of dusty plasma experiments.

Experimental Investigation of Reynolds Number Effects on Test Quality in a Hypersonic Expansion Tube

NASA Astrophysics Data System (ADS)

Rossmann, Tobias; Devin, Alyssa; Shi, Wen; Verhoog, Charles

2017-11-01

Reynolds number effects on test time and the temporal and spatial flow quality in a hypersonic expansion tube are explored using high-speed pressure, infrared optical, and Schlieren imaging measurements. Boundary layer models for shock tube flows are fairly well established to assist in the determination of test time and flow dimensions at typical high enthalpy test conditions. However, the application of these models needs to be more fully explored due to the unsteady expansion of turbulent boundary layers and contact regions separating dissimilar gasses present in expansion tube flows. Additionally, expansion tubes rely on the development of a steady jet with a large enough core-flow region at the exit of the acceleration tube to create a constant velocity region inside of the test section. High-speed measurements of pressure and Mach number at several locations within the expansion tube allow for the determination of an experimental x-t diagram. The comparison of the experimentally determined x-t diagram to theoretical highlights the Reynolds number dependent effects on expansion tube. Additionally, spatially resolved measurements of the Reynolds number dependent, steady core-flow in the expansion tube viewing section are shown. NSF MRI CBET #1531475, Lafayette College, McCutcheon Foundation.

Metainference: A Bayesian inference method for heterogeneous systems.

PubMed

Bonomi, Massimiliano; Camilloni, Carlo; Cavalli, Andrea; Vendruscolo, Michele

2016-01-01

Modeling a complex system is almost invariably a challenging task. The incorporation of experimental observations can be used to improve the quality of a model and thus to obtain better predictions about the behavior of the corresponding system. This approach, however, is affected by a variety of different errors, especially when a system simultaneously populates an ensemble of different states and experimental data are measured as averages over such states. To address this problem, we present a Bayesian inference method, called "metainference," that is able to deal with errors in experimental measurements and with experimental measurements averaged over multiple states. To achieve this goal, metainference models a finite sample of the distribution of models using a replica approach, in the spirit of the replica-averaging modeling based on the maximum entropy principle. To illustrate the method, we present its application to a heterogeneous model system and to the determination of an ensemble of structures corresponding to the thermal fluctuations of a protein molecule. Metainference thus provides an approach to modeling complex systems with heterogeneous components and interconverting between different states by taking into account all possible sources of errors.

A computer program for the localization of small areas in roentgenological images

NASA Technical Reports Server (NTRS)

Keller, R. A.; Baily, N. A.

1976-01-01

A method and associated algorithm are presented which allow a simple and accurate determination to be made of the location of small symmetric areas presented in roentgenological images. The method utilizes an operator to visually spot object positions but eliminates the need for critical positioning accuracy on the operator's part. The rapidity of measurement allows results to be evaluated on-line. Parameters associated with the algorithm have been analyzed, and methods to facilitate an optimum choice for any particular experimental setup are presented.

Complex optimization for big computational and experimental neutron datasets

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bao, Feng; Oak Ridge National Lab.; Archibald, Richard

Here, we present a framework to use high performance computing to determine accurate solutions to the inverse optimization problem of big experimental data against computational models. We demonstrate how image processing, mathematical regularization, and hierarchical modeling can be used to solve complex optimization problems on big data. We also demonstrate how both model and data information can be used to further increase solution accuracy of optimization by providing confidence regions for the processing and regularization algorithms. Finally, we use the framework in conjunction with the software package SIMPHONIES to analyze results from neutron scattering experiments on silicon single crystals, andmore » refine first principles calculations to better describe the experimental data.« less

Complex optimization for big computational and experimental neutron datasets

DOE PAGES

Bao, Feng; Oak Ridge National Lab.; Archibald, Richard; ...

2016-11-07

Here, we present a framework to use high performance computing to determine accurate solutions to the inverse optimization problem of big experimental data against computational models. We demonstrate how image processing, mathematical regularization, and hierarchical modeling can be used to solve complex optimization problems on big data. We also demonstrate how both model and data information can be used to further increase solution accuracy of optimization by providing confidence regions for the processing and regularization algorithms. Finally, we use the framework in conjunction with the software package SIMPHONIES to analyze results from neutron scattering experiments on silicon single crystals, andmore » refine first principles calculations to better describe the experimental data.« less

Chickpea seeds germination rational parameters optimization

NASA Astrophysics Data System (ADS)

Safonova, Yu A.; Ivliev, M. N.; Lemeshkin, A. V.

2018-05-01

The paper presents the influence of chickpea seeds bioactivation parameters on their enzymatic activity experimental results. Optimal bioactivation process modes were obtained by regression-factor analysis: process temperature - 13.6 °C, process duration - 71.5 h. It was found that in the germination process, the proteolytic, amylolytic and lipolytic enzymes activity increased, and the urease enzyme activity is reduced. The dependences of enzyme activity on chickpea seeds germination conditions were obtained by mathematical processing of experimental data. The calculated data are in good agreement with the experimental ones. This confirms the optimization efficiency based on experiments mathematical planning in order to determine the enzymatic activity of chickpea seeds germination optimal parameters of bioactivated seeds.

Characterizing Fracturing of Clay-Rich Lower Watrous Rock: From Laboratory Experiments to Nonlocal Damage-Based Simulations

NASA Astrophysics Data System (ADS)

Guy, N.; Seyedi, D. M.; Hild, F.

2018-06-01

The work presented herein aims at characterizing and modeling fracturing (i.e., initiation and propagation of cracks) in a clay-rich rock. The analysis is based on two experimental campaigns. The first one relies on a probabilistic analysis of crack initiation considering Brazilian and three-point flexural tests. The second one involves digital image correlation to characterize crack propagation. A nonlocal damage model based on stress regularization is used for the simulations. Two thresholds both based on regularized stress fields are considered. They are determined from the experimental campaigns performed on Lower Watrous rock. The results obtained with the proposed approach are favorably compared with the experimental results.

An analytical method based on multipole moment expansion to calculate the flux distribution in Gammacell-220

NASA Astrophysics Data System (ADS)

Rezaeian, P.; Ataenia, V.; Shafiei, S.

2017-12-01

In this paper, the flux of photons inside the irradiation cell of the Gammacell-220 is calculated using an analytical method based on multipole moment expansion. The flux of the photons inside the irradiation cell is introduced as the function of monopole, dipoles and quadruples in the Cartesian coordinate system. For the source distribution of the Gammacell-220, the values of the multipole moments are specified by direct integrating. To confirm the validation of the presented methods, the flux distribution inside the irradiation cell was determined utilizing MCNP simulations as well as experimental measurements. To measure the flux inside the irradiation cell, Amber dosimeters were employed. The calculated values of the flux were in agreement with the values obtained by simulations and measurements, especially in the central zones of the irradiation cell. In order to show that the present method is a good approximation to determine the flux in the irradiation cell, the values of the multipole moments were obtained by fitting the simulation and experimental data using Levenberg-Marquardt algorithm. The present method leads to reasonable results for the all source distribution even without any symmetry which makes it a powerful tool for the source load planning.

Experimental determination of the navigation error of the 4-D navigation, guidance, and control systems on the NASA B-737 airplane

NASA Technical Reports Server (NTRS)

Knox, C. E.

1978-01-01

Navigation error data from these flights are presented in a format utilizing three independent axes - horizontal, vertical, and time. The navigation position estimate error term and the autopilot flight technical error term are combined to form the total navigation error in each axis. This method of error presentation allows comparisons to be made between other 2-, 3-, or 4-D navigation systems and allows experimental or theoretical determination of the navigation error terms. Position estimate error data are presented with the navigation system position estimate based on dual DME radio updates that are smoothed with inertial velocities, dual DME radio updates that are smoothed with true airspeed and magnetic heading, and inertial velocity updates only. The normal mode of navigation with dual DME updates that are smoothed with inertial velocities resulted in a mean error of 390 m with a standard deviation of 150 m in the horizontal axis; a mean error of 1.5 m low with a standard deviation of less than 11 m in the vertical axis; and a mean error as low as 252 m with a standard deviation of 123 m in the time axis.

Base Pressure at Supersonic Speeds on Two-dimensional Airfoils and on Bodies of Revolution with and Without Fins Having Turbulent Boundary Layers

NASA Technical Reports Server (NTRS)

LOVE EUGENE S

1957-01-01

An analysis has been made of available experimental data to show the effects of most of the variables that are more predominant in determining base pressure at supersonic speeds. The analysis covers base pressures for two-dimensional airfoils and for bodies of revolution with and without stabilizing fins and is restricted to turbulent boundary layers. The present status of available experimental information is summarized as are the existing methods for predicting base pressure. A simple semiempirical method is presented for estimating base pressure. For two-dimensional bases, this method stems from an analogy established between the base-pressure phenomena and the peak pressure rise associated with the separation of the boundary layer. An analysis made for axially symmetric flow indicates that the base pressure for bodies of revolution is subject to the same analogy. Based upon the methods presented, estimations are made of such effects as Mach number, angle of attack, boattailing, fineness ratio, and fins. These estimations give fair predictions of experimental results. (author)

Orientation-controlled parallel assembly at the air-water interface

NASA Astrophysics Data System (ADS)

Park, Kwang Soon; Hao Hoo, Ji; Baskaran, Rajashree; Böhringer, Karl F.

2012-10-01

This paper presents an experimental and theoretical study with statistical analysis of a high-yield, orientation-specific fluidic self-assembly process on a preprogrammed template. We demonstrate self-assembly of thin (less than few hundred microns in thickness) parts, which is vital for many applications in miniaturized platforms but problematic for today's pick-and-place robots. The assembly proceeds row-by-row as the substrate is pulled up through an air-water interface. Experiments and analysis are presented with an emphasis on the combined effect of controlled surface waves and magnetic force. For various gap values between a magnet and Ni-patterned parts, magnetic force distributions are generated using Monte Carlo simulation and employed to predict assembly yield. An analysis of these distributions shows that a gradual decline in yield following the probability density function can be expected with degrading conditions. The experimentally determined critical magnetic force is in good agreement with a derived value from a model of competing forces acting on a part. A general set of design guidelines is also presented from the developed model and experimental data.

Spinacia oleracea L. leaf stomata harboring Cryptosporidium parvum oocysts: A potential threat for food safety

USDA-ARS?s Scientific Manuscript database

Scientific literature documents the prevalence of Cryptosporidium oocysts in irrigation waters and on fresh produce. In the present study spinach leaves were experimentally exposed to Cryptosporidium oocysts which were subsequently irrigated with clean water daily for 5 days. As determined by confoc...

AN EXPERIMENTAL ASSESSMENT OF MINIMUM MAPPING UNIT SIZE

EPA Science Inventory

Land-cover (LC) maps derived from remotely sensed data are often presented using a minimum mapping unit (MMU). The choice of a MMU that is appropriate for the projected use of a classification is important. The objective of this experiment was to determine the optimal MMU of a L...

Computer Skill Acquisition and Retention: The Effects of Computer-Aided Self-Explanation

ERIC Educational Resources Information Center

Chi, Tai-Yin

2016-01-01

This research presents an experimental study to determine to what extent computer skill learners can benefit from generating self-explanation with the aid of different computer-based visualization technologies. Self-explanation was stimulated with dynamic visualization (Screencast), static visualization (Screenshot), or verbal instructions only,…

Hypersonic research engine/aerothermodynamic integration model, experimental results. Volume 2: Mach 6 performance

NASA Technical Reports Server (NTRS)

Andrews, E. H., Jr.; Mackley, E. A.

1976-01-01

Computer program performance results of a Mach 6 hypersonic research engine during supersonic and subsonic combustion modes were presented. The combustion mode transition was successfully performed, exit surveys made, and effects of altitude, angle of attack, and inlet spike position were determined during these tests.

Production Techniques for Computer-Based Learning Material.

ERIC Educational Resources Information Center

Moonen, Jef; Schoenmaker, Jan

Experiences in the development of educational software in the Netherlands have included the use of individual and team approaches, the determination of software content and how it should be presented, and the organization of the entire development process, from experimental programs to prototype to final product. Because educational software is a…

Experimental Confirmation of Lenz's Law

ERIC Educational Resources Information Center

Mayer, V. V.; Varaksina, E. I.

2017-01-01

The paper presents a series of experiments that demonstrate the phenomenon of electromagnetic induction. These make it possible to determine the direction of the induced current and so confirm Lenz's Law. The simple experiments can be reproduced in a school laboratory and can be recommended for students' project activity.

Experimental confirmation of Lenz’s law

NASA Astrophysics Data System (ADS)

Mayer, V. V.; Varaksina, E. I.

2017-11-01

The paper presents a series of experiments that demonstrate the phenomenon of electromagnetic induction. These make it possible to determine the direction of the induced current and so confirm Lenz’s Law. The simple experiments can be reproduced in a school laboratory and can be recommended for students’ project activity.

A Feasibility Study on the Geophysical Response to Nanoparticles in the Subsurface

EPA Science Inventory

The research presented herein aims to determine if a spectral induced polarization (SIP) response exists due to nanoparticles in a saturated sand matrix. If a SIP response is realized in such an experimental setting, then it is feasible that SIP may be capable of delineating nano...

Epitope mapping of the domains of human angiotensin converting enzyme.

PubMed

Kugaevskaya, Elena V; Kolesanova, Ekaterina F; Kozin, Sergey A; Veselovsky, Alexander V; Dedinsky, Ilya R; Elisseeva, Yulia E

2006-06-01

Somatic angiotensin converting enzyme (sACE), contains in its single chain two homologous domains (called N- and C-domains), each bearing a functional zinc-dependent active site. The present study aims to define the differences between two sACE domains and to localize experimentally revealed antigenic determinants (B-epitopes) in the recently determined three-dimensional structure of testicular tACE. The predicted linear antigenic determinants of human sACE were determined by peptide scanning ("PEPSCAN") approach. Essential difference was demonstrated between locations of the epitopes in the N- and C-domains. Comparison of arrangement of epitopes in the human domains with the corresponding sequences of some mammalian sACEs enabled to classify the revealed antigenic determinants as variable or conserved areas. The location of antigenic determinants with respect to various structural elements and to functionally important sites of the human sACE C-domain was estimated. The majority of antigenic sites of the C-domain were located at the irregular elements and at the boundaries of secondary structure elements. The data show structural differences between the sACE domains. The experimentally revealed antigenic determinants were in agreement with the recently determined crystal tACE structure. New potential applications are open to successfully produce mono-specific and group-specific antipeptide antibodies.

Speckle techniques for determining stresses in moving objects

NASA Technical Reports Server (NTRS)

Murphree, E. A.; Wilson, T. F.; Ranson, W. F.; Swinson, W. F.

1978-01-01

Laser speckle interferometry is a relatively new experimental technique which shows promise of alleviating many difficult problems in experimental mechanics. The method utilizes simple high-resolution photographs of the surface which is illuminated by coherent light. The result is a real-time or permanently stored whole-field record of interference fringes which yields a map of displacements in the object. In this thesis, the time-average theory using the Fourier transform is developed to present the application of this technique to measurement of in-plane displacement induced by the vibration of an object.

Buckling behavior of composite cylinders subjected to compressive loading

NASA Technical Reports Server (NTRS)

Carri, R. L.

1973-01-01

Room temperature compressive buckling strengths of eight cylinders, four boron-epoxy and four boron-epoxy reinforced-titanium, with diameter to thickness ratios ranging between 40 and 67 are determined experimentally and compared with analytical predictions. Numerical buckling strengths are presented for Donnell's, Flugge's and Sanders' shell theories for anisotropic and orthotropic material cases. Comparison of analytical predictions with experimental results indicates good agreement and the recommended correlation factor suggested in the literature is applicable for design. For the cylinders tested, the correlation between experiment and theory ranged from 0.73 to 0.97.

The experimental studies of operating modes of a diesel-generator set at variable speed

NASA Astrophysics Data System (ADS)

Obukhov, S. G.; Plotnikov, I. A.; Surkov, M. A.; Sumarokova, L. P.

2017-02-01

A diesel generator set working at variable speed to save fuel is studied. The results of experimental studies of the operating modes of an autonomous diesel generator set are presented. Areas for regulating operating modes are determined. It is demonstrated that the transfer of the diesel generator set to variable speed of the diesel engine makes it possible to improve the energy efficiency of the autonomous generator source, as well as the environmental and ergonomic performance of the equipment as compared with general industrial analogues.

MaRIE: an experimental facility concept revolutionizing materials in extremes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Barnes, Cris W

The Matter-Radiation Interactions in Extremes (MaRIE) project intends to create an experimental facility that will revolutionize the control of materials in extremes. That control extends to extreme regimes where solid material has failed and begins to flow - the regimes of fluid dynamics and turbulent mixing. This presentation introduces the MaRIE facility concept, demonstrates examples of the science case that determine its functional requirements, and kicks-off the discussion of the decadal scientific challenges of mixing in extremes, including those MaRIE might address.

Experimental Demonstration of Frequency Regulation by Commercial Buildings – Part I: Modeling and Hierarchical Control Design

DOE PAGES

Vrettos, Evangelos; Kara, Emre C.; MacDonald, Jason; ...

2016-11-15

Here, this paper is the first part of a two-part series in which we present results from one of the first worldwide experimental demonstrations of frequency regulation in a commercial building test facility. We demonstrate that commercial buildings can track a frequency regulation signal with high accuracy and minimal occupant discomfort in a realistic environment. In addition, we show that buildings can determine the reserve capacity and baseline power a priori, and identify the optimal tradeoff between frequency regulation and energy efficiency.

Experimental investigation of a supersonic micro turbine running with hexamethyldisiloxane

NASA Astrophysics Data System (ADS)

Weiß Andreas, P.; Josef, Hauer; Tobias, Popp; Markus, Preißinger

2017-09-01

Experimentally determined efficiency characteristics of a supersonic micro turbine are discussed in the present paper. The micro turbine is a representative of a "micro-turbine-generator-construction-kit" for ORC small scale waste heat recovery. The isentropic total-to-static efficiency of the 12 kW turbine reaches an excellent design point performance of 73.4 %. Furthermore, its off-design operating behavior is very advantageous for small waste heat recovery plants: the turbine efficiency keeps a high level over a wide range of pressure ratio and rotational speed.

Photons Revisited

NASA Astrophysics Data System (ADS)

Batic, Matej; Begalli, Marcia; Han, Min Cheol; Hauf, Steffen; Hoff, Gabriela; Kim, Chan Hyeong; Kim, Han Sung; Grazia Pia, Maria; Saracco, Paolo; Weidenspointner, Georg

2014-06-01

A systematic review of methods and data for the Monte Carlo simulation of photon interactions is in progress: it concerns a wide set of theoretical modeling approaches and data libraries available for this purpose. Models and data libraries are assessed quantitatively with respect to an extensive collection of experimental measurements documented in the literature to determine their accuracy; this evaluation exploits rigorous statistical analysis methods. The computational performance of the associated modeling algorithms is evaluated as well. An overview of the assessment of photon interaction models and results of the experimental validation are presented.

Summary of experimentally determined facts concerning the behavior of the boundary layer and performance of boundary layer measurements. [considering sailing flight

NASA Technical Reports Server (NTRS)

Vanness, W.

1978-01-01

A summary report of boundary layer studies is presented. Preliminary results of experimental measurements show that: (1) A very thin layer (approximately 0.4 mm) of the boundary layer seems to be accelerated; (2) the static pressure of the outer flow does not remain exactly constant through the boundary layer; and (3) an oncoming boundary layer which is already turbulent at the suction point can again become laminar behind this point without being completely sucked off.

Spectroscopic study of bipolar nanosecond pulse gas-liquid discharge in atmospheric argon

NASA Astrophysics Data System (ADS)

Sen, WANG; Dezheng, YANG; Feng, LIU; Wenchun, WANG; Zhi, FANG

2018-07-01

Atmospheric gas-liquid discharge with argon as a working gas is presented by employed nanosecond pulse power. The discharge is presented in a glow-like mode. The discharge powers are determined to be less than 1 W, and remains almost constant when the discharge duration time increases. Bountiful active species are determined by capturing optical emission spectra, and their main generation processes are also discussed. The plasma gas temperature is calculated as 350 K by comparing the experimental spectra and the simulated ones of {{{N}}}2({{C}}{}3{{\\Pi }}{{g}}\\to {{B}}{}3{{\\Pi }}{{g}},{{Δ }}{{ν }}=-2). The time resolved vibrational and rotational temperature is researched to present the stability of discharge when pulse voltage and discharge duration vary. The electron density is determined to be 1016 cm‑3 according to the Stark broadening effect of the H α line.

Experimental determination of dynamic characteristics of the VentrAssist implantable rotary blood pump.

PubMed

Chung, Michael K H; Zhang, Nong; Tansley, Geoff D; Qian, Yi

2004-12-01

The VentrAssist implantable rotary blood pump, intended for long-term ventricular assist, is under development and is currently being tested for its rotor-dynamic stability. The pump consists of a shaftless impeller, which also acts as the rotor of the brushless DC motor. The impeller remains passively suspended in the pump cavity by hydrodynamic forces, which result from the small clearances between the outside surfaces of the impeller and the pump cavity. These small clearances range from approximately 50 microm to 230 microm in size in the version of pump reported here. This article presents experimental investigation into the dynamic characteristics of the impeller-bearing-pump housing system of the rotary blood pump for increasing pump speeds at different flow rates. The pump was mounted on a suspension system consisting of a platform and springs, where the natural frequency and damping ratio for the suspension system were determined. Real-time measurements of the impeller's displacement were performed using Hall effect sensors. A vertical disturbance force was exerted onto the pump housing, causing the impeller to be displaced in vertical direction from its dynamic equilibrium position within the pump cavity. The impeller displacement was represented by a decaying sine wave, which indicated the impeller restoring to its equilibrium position. From the decaying sine wave the natural frequency and stiffness coefficient of the system were determined. Furthermore, the logarithmic decrement method was used to determine the damping ratio and eventually the damping coefficient of the system. Results indicate that stiffness and damping coefficients increased as flow rate and pump speed increased, representing an increase in stability with these changing conditions. However, pump speed had a greater influence on the stiffness and damping coefficients than flow rate did, which was evident through dynamic analysis. Overall the experimental method presented in this article was successful in determining the dynamic characteristics of the system.

Three-dimensional FEM model of FBGs in PANDA fibers with experimentally determined model parameters

NASA Astrophysics Data System (ADS)

Lindner, Markus; Hopf, Barbara; Koch, Alexander W.; Roths, Johannes

2017-04-01

A 3D-FEM model has been developed to improve the understanding of multi-parameter sensing with Bragg gratings in attached or embedded polarization maintaining fibers. The material properties of the fiber, especially Young's modulus and Poisson's ratio of the fiber's stress applying parts, are crucial for accurate simulations, but are usually not provided by the manufacturers. A methodology is presented to determine the unknown parameters by using experimental characterizations of the fiber and iterative FEM simulations. The resulting 3D-Model is capable of describing the change in birefringence of the free fiber when exposed to longitudinal strain. In future studies the 3D-FEM model will be employed to study the interaction of PANDA fibers with the surrounding materials in which they are embedded.

Desktop chaotic systems: Intuition and visualization

NASA Technical Reports Server (NTRS)

Bright, Michelle M.; Melcher, Kevin J.; Qammar, Helen K.; Hartley, Tom T.

1993-01-01

This paper presents a dynamic study of the Wildwood Pendulum, a commercially available desktop system which exhibits a strange attractor. The purpose of studying this chaotic pendulum is twofold: to gain insight in the paradigmatic approach of modeling, simulating, and determining chaos in nonlinear systems; and to provide a desktop model of chaos as a visual tool. For this study, the nonlinear behavior of this chaotic pendulum is modeled, a computer simulation is performed, and an experimental performance is measured. An assessment of the pendulum in the phase plane shows the strange attractor. Through the use of a box-assisted correlation dimension methodology, the attractor dimension is determined for both the model and the experimental pendulum systems. Correlation dimension results indicate that the pendulum and the model are chaotic and their fractal dimensions are similar.

Crossflow Stability and Transition Experiments in Swept-Wing Flow

NASA Technical Reports Server (NTRS)

Dagenhart, J. Ray; Saric, William S.

1999-01-01

An experimental examination of crossflow instability and transition on a 45deg swept wing was conducted in the Arizona State University Unsteady Wind Tunnel. The stationary-vortex pattern and transition location are visualized by using both sublimating chemical and liquid-crystal coatings. Extensive hot-wire measurements were obtained at several measurement stations across a single vortex track. The mean and travelling wave disturbances were measured simultaneously. Stationary crossflow disturbance profiles were determined by subtracting either a reference or a span-averaged velocity profile from the mean velocity data. Mean, stationary crossflow, and traveling wave velocity data were presented as local boundary layer profiles and contour plots across a single stationary crossflow vortex track. Disturbance mode profiles and growth rates were determined. The experimental data are compared with predictions from linear stability theory.

Reliability approach to rotating-component design. [fatigue life and stress concentration

NASA Technical Reports Server (NTRS)

Kececioglu, D. B.; Lalli, V. R.

1975-01-01

A probabilistic methodology for designing rotating mechanical components using reliability to relate stress to strength is explained. The experimental test machines and data obtained for steel to verify this methodology are described. A sample mechanical rotating component design problem is solved by comparing a deterministic design method with the new design-by reliability approach. The new method shows that a smaller size and weight can be obtained for specified rotating shaft life and reliability, and uses the statistical distortion-energy theory with statistical fatigue diagrams for optimum shaft design. Statistical methods are presented for (1) determining strength distributions for steel experimentally, (2) determining a failure theory for stress variations in a rotating shaft subjected to reversed bending and steady torque, and (3) relating strength to stress by reliability.

Multiscale simulations of the early stages of the growth of graphene on copper

NASA Astrophysics Data System (ADS)

Gaillard, P.; Chanier, T.; Henrard, L.; Moskovkin, P.; Lucas, S.

2015-07-01

We have performed multiscale simulations of the growth of graphene on defect-free copper (111) in order to model the nucleation and growth of graphene flakes during chemical vapour deposition and potentially guide future experimental work. Basic activation energies for atomic surface diffusion were determined by ab initio calculations. Larger scale growth was obtained within a kinetic Monte Carlo approach (KMC) with parameters based on the ab initio results. The KMC approach counts the first and second neighbours to determine the probability of surface diffusion. We report qualitative results on the size and shape of the graphene islands as a function of deposition flux. The dominance of graphene zigzag edges for low deposition flux, also observed experimentally, is explained by its larger dynamical stability that the present model fully reproduced.

Experimental datasets on engineering properties of expansive soil treated with common salt.

PubMed

Durotoye, Taiwo O; Akinmusuru, Joseph O; Ogundipe, Kunle E

2018-06-01

Construction of highway pavements or high rise structures over the expansive soils are always problematic due to failures of volume change or swelling characteristic experienced in the water permeability of the soil. The data in this article represented summary of (Durotoye et al., 2016; Durotoye, 2016) [1], [2]. The data explored different percentages of sodium chloride as additive in stabilizing the engineering properties of expansive soil compared with other available stabilizer previously worked on. Experimental procedures carried out on expansive soil include: (Liquid limit, Plastic limit, Plasticity index, Shrinkage limit, Specific gravity Free swell index and Optimum water content) to determine the swelling parameters and (maximum dry density, California bearing ratio and unconfined compressive strength) to determine the strength parameters. The results of the experiment were presented in pie charts.

Determination of the refractive index and thickness of holographic silver halide materials by use of polarized reflectances.

PubMed

Beléndez, Augusto; Beléndez, Tarsicio; Neipp, Cristian; Pascual, Inmaculada

2002-11-10

A method to determine the refractive index and thickness of silver halide emulsions used in holography is presented. The emulsions are in the form of a layer of film deposited on a thick glass plate. The experimental reflectances of p-polarized light are measured as a function of the incident angles, and the values of refractive index, thickness, and extinction coefficient of the emulsion are obtained by using the theoretical equation for reflectance. As examples, five commercial holographic silver halide emulsions are analyzed. The procedure to obtain the measurements and the numerical analysis of the experimental data are simple, and agreement of the calculated reflectances, by use of the thickness and refractive index obtained, with the measured reflectances is satisfactory.

Fission in the landscape of heaviest elements: Some recent examples

NASA Astrophysics Data System (ADS)

Khuyagbaatar, J.; Yakushev, A.; Düllmann, Ch. E.; Ackermann, D.; Andersson, L.-L.; Block, M.; Brand, H.; Even, J.; Forsberg, U.; Hartmann, W.; Herzberg, R.-D.; Heßberger, F. P.; Hoffmann, J.; Hübner, A.; Jäger, E.; Jeppsson, J.; Kindler, B.; Kratz, J. V.; Krier, J.; Kurz, N.; Lommel, B.; Maiti, M.; Minami, S.; Rudolph, D.; Runke, J.; Sarmiento, L. G.; Schädel, M.; Schausten, B.; Steiner, J.; Heidenreich, T. Torres De; Uusitalo, J.; Wiehl, N.; Yakusheva, V.

2016-12-01

The fission process still remains a main factor that determines the stability of the atomic nucleus of heaviest elements. Fission half-lives vary over a wide range, 10-19-1024 s. Present experimental techniques for the synthesis of the superheavy elements that usually measure α-decay chains are sensitive only in a limited range of half-lives, often 10-5-103 s. In the past years, measurement techniques for very short-lived and very long-lived nuclei were significantly improved at the gas-filled recoil separator TASCA at GSI Darmstadt. Recently, several experimental studies of fission-related phenomena have successfully been performed. In this paper, results on 254-256Rf and 266Lr are presented and corresponding factors for retarding the fission process are discussed.

Experimental determination of J-Q in the two-parameter characterization of fracture

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, S.; Chiang, F.P.

1995-11-01

It is well recognized that using a single parameter to characterize crack tip deformation is no long adequate if constraint is present. Several approaches of two-parameter characterization scheme have been proposed. There are the J-T approach, the J-Q approach of Shih et al and the J-Q approach of Sharma and Aravas. The authors propose a scheme to measure the J and Q of the J-Q theory of Sharma and Aravas. They find that with the addition of Q term the experimentally measured U-field displacement component agrees well with the theoretical prediction. The agreement increases as the crack tip constraint increases.more » The results of a SEN and a CN specimen are presented.« less

Toward a computational and experimental model of a poly-epoxy surface

NASA Astrophysics Data System (ADS)

Duguet, Thomas; Bessaguet, Camille; Aufray, Maëlenn; Esvan, Jérôme; Charvillat, Cédric; Vahlas, Constantin; Lacaze-Dufaure, Corinne

2015-01-01

A model poly-epoxy surface formed by the reaction of DGEBA and EDA is studied by the combination of experiments and DFT calculations. A special synthesis protocol is presented leading to the formation of a surface that is smooth (Sa < 1 nm), chemically homogeneous, and that presents a low-defect density (0.21 μm-2), as shown by AFM characterizations. Then, XPS is used for the determination of the elemental and functional groups' surface composition. DFT allows the identification and assignment of individual bonds contributions to the experimental 1s core-level peaks. Overall, we demonstrate that such a model sample is perfectly suitable for a use as a template for the study of poly-epoxy surface functionalization.

Simulator for concurrent processing data flow architectures

NASA Technical Reports Server (NTRS)

Malekpour, Mahyar R.; Stoughton, John W.; Mielke, Roland R.

1992-01-01

A software simulator capability of simulating execution of an algorithm graph on a given system under the Algorithm to Architecture Mapping Model (ATAMM) rules is presented. ATAMM is capable of modeling the execution of large-grained algorithms on distributed data flow architectures. Investigating the behavior and determining the performance of an ATAMM based system requires the aid of software tools. The ATAMM Simulator presented is capable of determining the performance of a system without having to build a hardware prototype. Case studies are performed on four algorithms to demonstrate the capabilities of the ATAMM Simulator. Simulated results are shown to be comparable to the experimental results of the Advanced Development Model System.

Macroscopic aspects of interfacial reactions

NASA Technical Reports Server (NTRS)

Heckel, R. W.

1976-01-01

The extent of interdiffusion and formation of new phases is determined by the constitution diagram of the alloy system, the interdiffusion coefficients of the phases present, and the thermal conditions (temperature and time) associated with the bonding process and/or subsequent use of the bonded structure. In many instance, the kinetics of interdiffusion and phase formation can be predicted from known parameters using numerical methods and computer techniques. Predictions are compared with experimentally determined parameters for a variety of metallurgical alloy systems.

Characterization and prediction of residues determining protein functional specificity.

PubMed

Capra, John A; Singh, Mona

2008-07-01

Within a homologous protein family, proteins may be grouped into subtypes that share specific functions that are not common to the entire family. Often, the amino acids present in a small number of sequence positions determine each protein's particular functional specificity. Knowledge of these specificity determining positions (SDPs) aids in protein function prediction, drug design and experimental analysis. A number of sequence-based computational methods have been introduced for identifying SDPs; however, their further development and evaluation have been hindered by the limited number of known experimentally determined SDPs. We combine several bioinformatics resources to automate a process, typically undertaken manually, to build a dataset of SDPs. The resulting large dataset, which consists of SDPs in enzymes, enables us to characterize SDPs in terms of their physicochemical and evolutionary properties. It also facilitates the large-scale evaluation of sequence-based SDP prediction methods. We present a simple sequence-based SDP prediction method, GroupSim, and show that, surprisingly, it is competitive with a representative set of current methods. We also describe ConsWin, a heuristic that considers sequence conservation of neighboring amino acids, and demonstrate that it improves the performance of all methods tested on our large dataset of enzyme SDPs. Datasets and GroupSim code are available online at http://compbio.cs.princeton.edu/specificity/. Supplementary data are available at Bioinformatics online.

Hydrodynamic Radii of Intrinsically Disordered Proteins Determined from Experimental Polyproline II Propensities

PubMed Central

Tomasso, Maria E.; Tarver, Micheal J.; Devarajan, Deepa; Whitten, Steven T.

2016-01-01

The properties of disordered proteins are thought to depend on intrinsic conformational propensities for polyproline II (PP II) structure. While intrinsic PP II propensities have been measured for the common biological amino acids in short peptides, the ability of these experimentally determined propensities to quantitatively reproduce structural behavior in intrinsically disordered proteins (IDPs) has not been established. Presented here are results from molecular simulations of disordered proteins showing that the hydrodynamic radius (R h) can be predicted from experimental PP II propensities with good agreement, even when charge-based considerations are omitted. The simulations demonstrate that R h and chain propensity for PP II structure are linked via a simple power-law scaling relationship, which was tested using the experimental R h of 22 IDPs covering a wide range of peptide lengths, net charge, and sequence composition. Charge effects on R h were found to be generally weak when compared to PP II effects on R h. Results from this study indicate that the hydrodynamic dimensions of IDPs are evidence of considerable sequence-dependent backbone propensities for PP II structure that qualitatively, if not quantitatively, match conformational propensities measured in peptides. PMID:26727467

LEPER: Library of Experimental PhasE Relations

NASA Astrophysics Data System (ADS)

Davis, F.; Gordon, S.; Mukherjee, S.; Hirschmann, M.; Ghiorso, M.

2006-12-01

The Library of Experimental PhasE Relations (LEPER) seeks to compile published experimental determinations of magmatic phase equilibria and provide those data on the web with a searchable and downloadable interface. Compiled experimental data include the conditions and durations of experiments, the bulk compositions of experimental charges, and the identity, compositions and proportions of phases observed, and, where available, estimates of experimental and analytical uncertainties. Also included are metadata such as the type of experimental device, capsule material, and method(s) of quantitative analysis. The database may be of use to practicing experimentalists as well as the wider Earth science community. Experimentalists may find the data useful for planning new experiments and will easily be able to compare their results to the full body of previous experimentnal data. Geologists may use LEPER to compare rocks sampled in the field with experiments performed on similar bulk composition or with experiments that produced similar-composition product phases. Modelers may use LEPER to parameterize partial melting of various lithologies. One motivation for compiling LEPER is for calibration of updated and revised versions of MELTS, however, it is hoped that the availability of LEPER will facilitate formulation and calibration of additional thermodynamic or empirical models of magmatic phase relations and phase equilibria, geothermometers and more. Data entry for LEPER is occuring presently: As of August, 2006, >6200 experiments have been entered, chiefly from work published between 1997 and 2005. A prototype web interface has been written and beta release on the web is anticipated in Fall, 2006. Eventually, experimentalists will be able to submit their new experimental data to the database via the web. At present, the database contains only data pertaining to the phase equilibria of silicate melts, but extension to other experimental data involving other fluids or sub-solidus phase equilibria may be contemplated. Also, the data are at present limited to natural or near-natural systems, but in the future, extension to synthetic (i.e., CMAS, etc.) systems is also possible. Each would depend in part on whether there is community demand for such databases. A trace element adjunct to LEPER is presently in planning stages.

Evolution and Transport of Water in the Upper Regolith of Mars

NASA Technical Reports Server (NTRS)

Hudson, T. L.; Aharonson, O.; Schorghofer, N.; Hecht, M. H.; Bridges, N. T.; Green, J. R.

2003-01-01

Long standing theoretical predictions [1-3], as well as recent spacecraft observations [4] indicate that large quantities of ice is present in the high latitudes upper decimeters to meters of the Martian regolith. At shallower depths and warmer locations small amounts of H2O, either adsorbed or free, may be present transiently. An understanding of the evolution of water based on theoretical and experimental considerations of the processes operating at the Martian environment is required. In particular, the porosity, diffusivity, and permeability of soils and their effect on water vapor transport under Mars-like conditions have been estimated, but experimental validation of such models is lacking. Goal: Three related mechanisms may affect water transport in the upper Martian regolith. 1) diffusion along a concentration gradient under isobaric conditions, 2) diffusion along a thermal gradient, which may give rise to a concentration gradient as ice sublimes or molecules desorb from the regolith, and 3) hydraulic flow, or mass motion in response to a pressure gradient. Our combined theoretical and experimental investigation seeks to disentangle these mechanisms and determine which process(es) are dominant in the upper regolith over various timescales. A detailed one-dimensional model of the upper regolith is being created which incorporates water adsorption/ desorption, condensation, porosity, diffusivity, and permeability effects. Certain factors such as diffusivity are difficult to determine theoretically due to the wide range of intrinsic grain properties such as particle sizes, shapes, packing densities, and emergent properties such as tortuosity. An experiment is being designed which will allow us to more accurately determine diffusivity, permeability, and water desorption isotherms for regolith simulants.

Determining Kinetic Parameters for Isothermal Crystallization of Glasses

NASA Technical Reports Server (NTRS)

Ray, C. S.; Zhang, T.; Reis, S. T.; Brow, R. K.

2006-01-01

Non-isothermal crystallization techniques are frequently used to determine the kinetic parameters for crystallization in glasses. These techniques are experimentally simple and quick compared to the isothermal techniques. However, the analytical models used for non-isothermal data analysis, originally developed for describing isothermal transformation kinetics, are fundamentally flawed. The present paper describes a technique for determining the kinetic parameters for isothermal crystallization in glasses, which eliminates most of the common problems that generally make the studies of isothermal crystallization laborious and time consuming. In this technique, the volume fraction of glass that is crystallized as a function of time during an isothermal hold was determined using differential thermal analysis (DTA). The crystallization parameters for the lithium-disilicate (Li2O.2SiO2) model glass were first determined and compared to the same parameters determined by other techniques to establish the accuracy and usefulness of the present technique. This technique was then used to describe the crystallization kinetics of a complex Ca-Sr-Zn-silicate glass developed for sealing solid oxide fuel cells.

A Global Optimization Method to Calculate Water Retention Curves

NASA Astrophysics Data System (ADS)

Maggi, S.; Caputo, M. C.; Turturro, A. C.

2013-12-01

Water retention curves (WRC) have a key role for the hydraulic characterization of soils and rocks. The behaviour of the medium is defined by relating the unsaturated water content to the matric potential. The experimental determination of WRCs requires an accurate and detailed measurement of the dependence of matric potential on water content, a time-consuming and error-prone process, in particular for rocky media. A complete experimental WRC needs at least a few tens of data points, distributed more or less uniformly from full saturation to oven dryness. Since each measurement requires to wait to reach steady state conditions (i.e., between a few tens of minutes for soils and up to several hours or days for rocks or clays), the whole process can even take a few months. The experimental data are fitted to the most appropriate parametric model, such as the widely used models of Van Genuchten, Brooks and Corey and Rossi-Nimmo, to obtain the analytic WRC. We present here a new method for the determination of the parameters that best fit the models to the available experimental data. The method is based on differential evolution, an evolutionary computation algorithm particularly useful for multidimensional real-valued global optimization problems. With this method it is possible to strongly reduce the number of measurements necessary to optimize the model parameters that accurately describe the WRC of the samples, allowing to decrease the time needed to adequately characterize the medium. In the present work, we have applied our method to calculate the WRCs of sedimentary carbonatic rocks of marine origin, belonging to 'Calcarenite di Gravina' Formation (Middle Pliocene - Early Pleistocene) and coming from two different quarry districts in Southern Italy. WRC curves calculated using the Van Genuchten model by simulated annealing (dashed curve) and differential evolution (solid curve). The curves are calculated using 10 experimental data points randomly extracted from the full experimental dataset. Simulated annealing is not able to find the optimal solution with this reduced data set.

The Dendritic Cell Major Histocompatibility Complex II (MHC II) Peptidome Derives from a Variety of Processing Pathways and Includes Peptides with a Broad Spectrum of HLA-DM Sensitivity*

PubMed Central

Clement, Cristina C.; Becerra, Aniuska; Yin, Liusong; Zolla, Valerio; Huang, Liling; Merlin, Simone; Follenzi, Antonia; Shaffer, Scott A.; Stern, Lawrence J.; Santambrogio, Laura

2016-01-01

The repertoire of peptides displayed in vivo by MHC II molecules derives from a wide spectrum of proteins produced by different cell types. Although intracellular endosomal processing in dendritic cells and B cells has been characterized for a few antigens, the overall range of processing pathways responsible for generating the MHC II peptidome are currently unclear. To determine the contribution of non-endosomal processing pathways, we eluted and sequenced over 3000 HLA-DR1-bound peptides presented in vivo by dendritic cells. The processing enzymes were identified by reference to a database of experimentally determined cleavage sites and experimentally validated for four epitopes derived from complement 3, collagen II, thymosin β4, and gelsolin. We determined that self-antigens processed by tissue-specific proteases, including complement, matrix metalloproteases, caspases, and granzymes, and carried by lymph, contribute significantly to the MHC II self-peptidome presented by conventional dendritic cells in vivo. Additionally, the presented peptides exhibited a wide spectrum of binding affinity and HLA-DM susceptibility. The results indicate that the HLA-DR1-restricted self-peptidome presented under physiological conditions derives from a variety of processing pathways. Non-endosomal processing enzymes add to the number of epitopes cleaved by cathepsins, altogether generating a wider peptide repertoire. Taken together with HLA-DM-dependent and-independent loading pathways, this ensures that a broad self-peptidome is presented by dendritic cells. This work brings attention to the role of “self-recognition” as a dynamic interaction between dendritic cells and the metabolic/catabolic activities ongoing in every parenchymal organ as part of tissue growth, remodeling, and physiological apoptosis. PMID:26740625

Experimental-Numerical Comparison of the Cantilever MEMS Frequency Shift in presence of a Residual Stress Gradient.

PubMed

Ballestra, Alberto; Somà, Aurelio; Pavanello, Renato

2008-02-06

The dynamic characterization of a set of gold micro beams by electrostatic excitation in presence of residual stress gradient has been studied experimentally. A method to determine the micro-cantilever residual stress gradient by measuring the deflection and curvature and then identifying the residual stress model by means of frequency shift behaviour is presented. A comparison with different numerical FEM models and experimental results has been carried out, introducing in the model the residual stress of the structures, responsible for an initial upward curvature. Dynamic spectrum data are measured via optical interferometry and experimental frequency shift curves are obtained by increasing the dc voltage applied to the specimens. A good correspondence is pointed out between measures and numerical models so that the residual stress effect can be evaluated for different configurations.

Experimental-Numerical Comparison of the Cantilever MEMS Frequency Shift in presence of a Residual Stress Gradient

PubMed Central

Ballestra, Alberto; Somà, Aurelio; Pavanello, Renato

2008-01-01

The dynamic characterization of a set of gold micro beams by electrostatic excitation in presence of residual stress gradient has been studied experimentally. A method to determine the micro-cantilever residual stress gradient by measuring the deflection and curvature and then identifying the residual stress model by means of frequency shift behaviour is presented. A comparison with different numerical FEM models and experimental results has been carried out, introducing in the model the residual stress of the structures, responsible for an initial upward curvature. Dynamic spectrum data are measured via optical interferometry and experimental frequency shift curves are obtained by increasing the dc voltage applied to the specimens. A good correspondence is pointed out between measures and numerical models so that the residual stress effect can be evaluated for different configurations. PMID:27879733

Aeromechanical stability of a hingeless rotor in hover and forward flight: Analysis and wind tunnel tests

NASA Technical Reports Server (NTRS)

Yeager, W. T., Jr.; Hamouda, M. N. H.; Mantay, W. R.

1983-01-01

A research effort of analysis and testing was conducted to investigate the ground resonance phenomenon of a soft in-plane hingeless rotor. Experimental data were obtained using a 9 ft. (2.74 m) diameter model rotor in hover and forward flight. Eight model rotor configurations were investigated. Configuration parameters included pitch flap coupling, blade sweep and droop, and precone of the blade feathering axis. An analysis based on a comprehensive analytical model of rotorcraft aerodynamics and dynamics was used. The moving block was used to experimentally determine the regressing lead lag mode damping. Good agreement was obtained between the analysis and test. Both analysis and experiment indicated ground resonance instability in hover. An outline of the analysis, a description of the experimental model and procedures, and comparison of the analytical and experimental data are presented.

A Theory and Experiments for Detecting Shock Locations

NASA Technical Reports Server (NTRS)

Hariharan, S. I.; Johnson, D. K.; Adamovsky, G.

1994-01-01

In this paper we present a simplified one-dimensional theory for predicting locations of normal shocks in a converging diverging nozzle. The theory assumes that the flow is quasi one-dimensional and the flow is accelerated in the throat area. Optical aspects of the model consider propagation of electromagnetic fields transverse to the shock front. The theory consists of an inverse problem in which from the measured intensity it reconstructs an index of refraction profile for the shock. From this profile and the Dale-Gladstone relation, the density in the flow field is determined, thus determining the shock location. Experiments show agreement with the theory. In particular the location is determined within 10 percent of accuracy. Both the theoretical as well as the experimental results are presented to validate the procedures in this work.

Experimental determination of ice sublimation energies

NASA Astrophysics Data System (ADS)

Luna, R.; Canto, J.; Satorre, M. A.; Domingo, M.

2011-11-01

In Astrophysics, the study of ices is important due to the wide range of scenarios in which they are present. Their physical and chemical characteristics play an important role in the study of the interstellar medium (ISM). The assessment of the energy of sublimation allows us to improve our understanding of physical and/or chemical processes that take place where ices are present. The energy of sublimation E_sub is defined as the change of energy between solid and gas phase of certain molecule. This value is important to determinate other thermodynamical parameters such as the reticular energy of ionic compounds, the energy of formation in gas phase from the energy of formation in condensed phase, or to estimate the sublimation rate, which is very important in determining the evolution of surfaces of astrophysical objects.

Experimentally determined soil organic matter-water sorption coefficients for different classes of natural toxins and comparison with estimated numbers.

PubMed

Schenzel, Judith; Goss, Kai-Uwe; Schwarzenbach, René P; Bucheli, Thomas D; Droge, Steven T J

2012-06-05

Although natural toxins, such as mycotoxins or phytoestrogens are widely studied and were recently identified as micropollutants in the environment, many of their environmentally relevant physicochemical properties have not yet been determined. Here, the sorption affinity to Pahokee peat, a model sorbent for soil organic matter, was investigated for 29 mycotoxins and two phytoestrogens. Sorption coefficients (K(oc)) were determined with a dynamic HPLC-based column method using a fully aqueous mobile phase with 5 mM CaCl(2) at pH 4.5. Sorption coefficients varied from less than 10(0.7) L/kg(oc) (e.g., all type B trichothecenes) to 10(4.0) L/kg(oc) (positively charged ergot alkaloids). For the neutral compounds the experimental sorption data set was compared with predicted sorption coefficients using various models, based on molecular fragment approaches (EPISuite's KOCWIN or SPARC), poly parameter linear free energy relationship (pp-LFER) in combination with predicted descriptors, and quantum-chemical based software (COSMOtherm)). None of the available models was able to adequately predict absolute K(oc) numbers and relative differences in sorption affinity for the whole set of neutral toxins, largely because mycotoxins exhibit highly complex structures. Hence, at present, for such compounds fast and consistent experimental techniques for determining sorption coefficients, as the one used in this study, are required.

Ultrasonic Nondestructive Characterization of Porous Materials

NASA Astrophysics Data System (ADS)

Yang, Ningli

2011-12-01

Wave propagation in porous media is studied in a wide range of technological applications. In the manufacturing industry, determining porosity of materials in the manufacturing process is required for strict quality control. In the oil industry, acoustic signals and seismic surveys are used broadly to determine the physical properties of the reservoir rock which is a porous media filled with oil or gas. In porous noise control materials, a precise prediction of sound absorption with frequency and evaluation of tortuosity are necessary. Ultrasonic nondestructive methods are a very important tool for characterization of porous materials. The dissertation deals with two types of porous media: materials with relatively low and closed porosity and materials with comparatively high and open porosity. Numerical modeling, Finite Element simulations and experimental characterization are all discussed in this dissertation. First, ultrasonic scattering is used to determine the porosity in porous media with closed pores. In order get a relationship between the porosity in porous materials and ultrasonic scattering independently and to increase the sensitivity to obtain scattering information, ultrasonic imaging methods are applied and acoustic waves are focused by an acoustic lens. To verify the technique, engineered porous acrylic plates with varying porosity are measured by ultrasonic scanning and ultrasonic array sensors. Secondly, a laser based ultrasonic technique is explored for predicting the mechanical integrity and durability of cementitious materials. The technique used involves the measurement of the phase velocity of fast and slow longitudinal waves in water saturated cement paste. The slow wave velocity is related to the specimen's tortuosity. The fast wave speed is dependent on the elastic properties of porous solid. Experimental results detailing the generation and detection of fast and slow wave waves in freshly prepared and aged water-saturated cement samples with varying water-to-cement ratios are presented in the dissertation. The third part concerns the ultrasonic characterization of air-saturated porous materials. Using airborne reflected and transmitted ultrasonic experimental data, the open porosity and tortuosity value of a porous acrylic plate with graded void content and a polyimide foam are determined simultaneously. Experimental and numerical results of the method are presented.

Surface tension determination using liquid sample micromirror property

NASA Astrophysics Data System (ADS)

Hošek, Jan

2007-05-01

This paper presents an application of adaptive optics principle onto small sample of liquid surface tension measurement. The principle of experimental method devised by Ferguson (1924) is based on measurement of pressure difference across a liquid sample placed into small diameter capillary on condition of one flat meniscus of the liquid sample. Planarity or curvature radius of the capillary tip meniscus has to be measured and controlled, in order to fulfill this condition during measurement. Two different optical set-ups using liquid meniscus micromirror property are presented and its suitability for meniscus profile determination is compared. Meniscus radius optical measurement, data processing and control algorithm of the adaptive micromirror profile set are presented too. The presented adaptive optics system can be used for focal length control of microsystems based on liquid micromirrors or microlenses with long focal distances especially.

Investigation on the quasifission process by theoretical analysis of experimental data of fissionlike reaction products

NASA Astrophysics Data System (ADS)

Giardina, G.; Nasirov, A. K.; Mandaglio, G.; Curciarello, F.; De Leo, V.; Fazio, G.; Manganaro, M.; Romaniuk, M.; Saccá, C.

2011-02-01

The hindrance to complete fusion is a phenomenon presenting in the most part of the capture events in reactions with massive nuclei. This phenomenon is due to the onset of the quasifission process which competes with complete fusion during the evolution of the composed system formed at capture stage. The branching ratio between quasifission and complete fusion strongly depends from different characteristics of reacting nuclei in the entrance channel. The experimental and theoretical investigations of reaction dynamics connected with the formation of composed system is nowadays the main subject of the nuclear reactions. There is ambiguity in establishment of the reaction mechanism leading to the observed binary fissionlike fragments. The correct estimation of the fusion probability is important in planning experiments for the synthesis of superheavy elements. The experimental determination of evaporation residues only is not enough to restore the true reaction dynamics. The experimental observation of fissionlike fragments only cannot assure the correct distinguishing of products of the quasifission, fast fission, and fusion-fission processes which have overlapping in the mass (angular, kinetic energy) distributions of fragments. In this paper we consider a wide set of reactions (with different mass asymmetry and mass symmetry parameters) with the aim to explain the role played by many quantities on the reaction mechanisms. We also present the results of study of the 48Ca+249Bk reaction used to synthesize superheavy nuclei with Z = 117 by the determination of the evaporation residue cross sections and the effective fission barriers < Bf > of excited nuclei formed along the de-excitation cascade of the compound nucleus.

Expression patterns of histone deacetylases in experimental stroke and potential targets for neuroprotection.

PubMed

Chen, Yan-Ting; Zang, Xue-Feng; Pan, Jie; Zhu, Xiao-Lei; Chen, Fei; Chen, Zhi-Bin; Xu, Yun

2012-09-01

1. Histone deacetylase (HDAC) inhibitors exert neuroprotection in both cellular and animal models of ischaemic stroke. However, which HDAC isoform (or isoforms) mediates this beneficial effect has not yet been determined. 2. In the present study, gene levels of the HDAC isoforms were determined in the mouse cortex using reverse transcription-polymerase chain reaction (RT-PCR), whereas changes in the expression of individual zinc-dependent HDAC family members were evaluated by western blotting, 3, 12, 24 and 48 h after cerebral ischaemia induced by transient middle cerebral artery occlusion in male Kunming mice. 3. The HDAC isoforms HDAC1-11 were all expressed in the mouse cortex and differentially affected by cerebral ischaemia. Notably, there was a substantial increase in HDAC3, HDAC6 and HDAC11 expression during the early phases of experimental stroke, indicating their contribution to stroke pathogenesis. Furthermore, induction of HDAC3 and HDAC6 in cortical neurons by ischaemic stroke was confirmed in vivo and in vitro using double-labelled immunostaining and RT-PCR, respectively. Therefore, small hairpin (sh) RNAs were used to selectively knock down HDAC3 or HDAC6. This knockdown appreciably promoted the survival of cortical neurons subjected to oxygen and glucose deprivation. 4. The findings of the present study demonstrate the expression patterns of HDAC isoforms during experimental ischaemic stroke. Furthermore, HDAC3 and HDAC6 were identified as potential mediators in the neurotoxicity of ischaemic stroke, suggesting that specific therapeutic approaches may be considered according to HDAC subtype. © 2012 The Authors Clinical and Experimental Pharmacology and Physiology © 2012 Wiley Publishing Asia Pty Ltd.

Quantitative Rainbow Schlieren Deflectometry as a Temperature Diagnostic for Spherical Flames

NASA Technical Reports Server (NTRS)

Feikema, Douglas A.

2004-01-01

Numerical analysis and experimental results are presented to define a method for quantitatively measuring the temperature distribution of a spherical diffusion flame using Rainbow Schlieren Deflectometry in microgravity. First, a numerical analysis is completed to show the method can suitably determine temperature in the presence of spatially varying species composition. Also, a numerical forward-backward inversion calculation is presented to illustrate the types of calculations and deflections to be encountered. Lastly, a normal gravity demonstration of temperature measurement in an axisymmetric laminar, diffusion flame using Rainbow Schlieren deflectometry is presented. The method employed in this paper illustrates the necessary steps for the preliminary design of a Schlieren system. The largest deflections for the normal gravity flame considered in this paper are 7.4 x 10(-4) radians which can be accurately measured with 2 meter focal length collimating and decollimating optics. The experimental uncertainty of deflection is less than 5 x 10(-5) radians.

Investigation of practical and theoretical accuracy of wireless indoor-positioning system UBISENSE

NASA Astrophysics Data System (ADS)

Wozniak, Marek; Odziemczyk, Waldemar; Nagorski, Kamil

2013-04-01

The development of Real Time Locating Systems has become an important add-on to many existing location aware systems. While Global Navigation Satelite System has solved most of the outdoor problems, it fails to repeat this success indoors. Wireless indoor positioning systems have become very popular in recent years. One of them is UBISENSE system. This system requires to carry an identity tag that is detected by sensors, which typically use triangulation to determine location. This paper presents the results of the investigation of accuracy of tag position using precise geodetic measurements and geometric analysis. Experimental measurements were carried out on the field polygon using precise tacheometer TCRP 1201+ and complete equipment of Ubisense. Results of experimental measurements were analyzed and presented graphically using Surfer 8. The paper presents the results of the investigation the teoretical and practical positioning accuracy according to the various working conditions.

Goal Contents and Goal Contexts: Experiments with Chinese Students

ERIC Educational Resources Information Center

Wang, Ze; Hu, Xiao Yong; Guo, Yong Yu

2013-01-01

Using samples of Chinese middle school students, the 2 experimental studies presented here examined the effects of goal content and goal context on test performance, free-choice engagement, and test anxiety within the framework of self-determination theory. Students' learning goals were induced as intrinsic or extrinsic with the learning contexts…

Informing the Human Plasma Protein Binding of Environmental Chemicals by Machine Learning in the Pharmaceutical Space: Applicability Domain and Limits of Predictability

EPA Science Inventory

The free fraction of a xenobiotic in plasma (Fub) is an important determinant of chemical adsorption, distribution, metabolism, elimination, and toxicity, yet experimental plasma protein binding data is scarce for environmentally relevant chemicals. The presented work explores th...

Insight to Global Change: EOS/SAR Mission

NASA Technical Reports Server (NTRS)

1990-01-01

This video presentation describes the methods and instrumentation used to help in determining future climate changes on Earth and explains the benefits of experimentation with synthetic aperture radar (SAR). It also gives a better understanding of the burning of fossil fuels, deterioration of the biosphere and deforestation of the rain forest which causes the greenhouse effect.

Determining the Scope of English Quantifiers.

DTIC Science & Technology

1978-06-01

experimentation, the following " flashcard " mode of presentation was adopted. Each sentence was typed on a file card, and submitted to the informant to...l10leentS of section 4 are from Reinhart 1976). I suspect that my flashcard technique -- where informants read a sentence typed on a file card and paraphrase

Factors Influencing Career Choice among Police Recruits

ERIC Educational Resources Information Center

Cole, Bryan

2012-01-01

This quantitative, non-experimental study examined the career choice factors of 154 (n = 154) police recruits to determine a correlation of age group generation to the five career choice factors presented in the Sibson Reward of Work Model. Law enforcement agencies faced a shortage of viable candidates to fill vacant positions. While extensive…

Determination of the Size and Depth of Craters on the Moon

ERIC Educational Resources Information Center

Grubelnik, Vladimir; Marhl, Marko; Repnik, Robert

2018-01-01

Experimental work in the research of astronomical phenomena is often difficult or even impossible because of long-lasting processes or too distant objects and correspondingly too expensive equipment. In this paper, we present an example of observation of the Moon, which is our nearest astronomic object and therefore does not require professional…

Cognitive Processing Load as a Determinant of Stuttering: Summary of a Research Programme

ERIC Educational Resources Information Center

Bosshardt, Hans-Georg

2006-01-01

The present paper integrates the results of experimental studies in which cognitive differences between stuttering and nonstuttering adults were investigated. In a monitoring experiment it was found that persons who stutter encode semantic information more slowly than nonstuttering persons. In dual-task experiments the two groups were compared in…

Study of Personal and Social Adjustment Ability of the Disabled Pupils

ERIC Educational Resources Information Center

Ryabova, Natalia Vladimirovna; Parfyonova, Tatyana Aleksandrovna

2015-01-01

The article presents the results of experimental work aimed at studying personal and social adjustment of a child with disabilities. Analysis of domestic and foreign psychological and educational literature allowed us to determine the key concept of the study, namely "social and personal orientation", as a trait of a human's personality,…

Assessing Mentoring Culture: Faculty and Staff Perceptions, Gaps, and Strengths

ERIC Educational Resources Information Center

Sheridan, Lynn; Murdoch, Natasha Hubbard; Harder, Emily

2015-01-01

The purpose of this non-experimental, cross-sectional, descriptive research was to survey faculty and staff perceptions of mentorship in a postsecondary institution in order to determine gaps and strengths in the current mentorship environment. The anecdotal activities we present reflect our educational practice environment through the work of our…

Estimating p-n Diode Bulk Parameters, Bandgap Energy and Absolute Zero by a Simple Experiment

ERIC Educational Resources Information Center

Ocaya, R. O.; Dejene, F. B.

2007-01-01

This paper presents a straightforward but interesting experimental method for p-n diode characterization. The method differs substantially from many approaches in diode characterization by offering much tighter control over the temperature and current variables. The method allows the determination of important diode constants such as temperature…

RotCFD Software Validation - Computational and Experimental Data Comparison

NASA Technical Reports Server (NTRS)

Fernandez, Ovidio Montalvo

2014-01-01

RotCFD is a software intended to ease the design of NextGen rotorcraft. Since RotCFD is a new software still in the development process, the results need to be validated to determine the software's accuracy. The purpose of the present document is to explain one of the approaches to accomplish that goal.

Investigation of methods and equipment for compaction of composite mixtures during their granulation

NASA Astrophysics Data System (ADS)

Shkarpetkin, E. A.; Osokin, A. V.; Sabaev, V. G.

2018-03-01

The article presents the results of a literature analysis of the methods of compaction of materials, analytical and experimental research on the creation of a roller compacting device and the determination of its operation modes, which provides an efficient preliminary compaction of a composite mixture based on technogenic materials.

Habituation as a Determinant of Human Food Intake

ERIC Educational Resources Information Center

Epstein, Leonard H.; Temple, Jennifer L.; Roemmich, James N.; Bouton, Mark E.

2009-01-01

Research has shown that animals and humans habituate on a variety of behavioral and physiological responses to repeated presentations of food cues, and habituation is related to amount of food consumed and cessation of eating. The purpose of this article is to provide an overview of experimental paradigms used to study habituation, integrate a…

The Influence of Textual Cues on First Impressions of an Email Sender

ERIC Educational Resources Information Center

Marlow, Shannon L.; Lacerenza, Christina N.; Iwig, Chelsea

2018-01-01

The present study experimentally manipulated the gender of an email sender, closing salutation, and sending mode (i.e., email sent via desktop computer/laptop as compared with email sent via a mobile device) to determine if these specific cues influence first impressions of the sender's competence, professionalism, positive affect, and negative…

Data-driven design optimization for composite material characterization

Treesearch

John G. Michopoulos; John C. Hermanson; Athanasios Iliopoulos; Samuel G. Lambrakos; Tomonari Furukawa

2011-06-01

The main goal of the present paper is to demonstrate the value of design optimization beyond its use for structural shape determination in the realm of the constitutive characterization of anisotropic material systems such as polymer matrix composites with or without damage. The approaches discussed are based on the availability of massive experimental data...

Determination of the Rotational Barrier in Ethane by Vibrational Spectroscopy and Statistical Thermodynamics

ERIC Educational Resources Information Center

Ercolani, Gianfranco

2005-01-01

The finite-difference boundary-value method is a numerical method suited for the solution of the one-dimensional Schrodinger equation encountered in problems of hindered rotation. Further, the application of the method, in combination with experimental results for the evaluation of the rotational energy barrier in ethane is presented.

A comparison of experimental and theoretical results for leakage, pressure gradients, and rotordynamic coefficients for tapered annular gas seal

NASA Technical Reports Server (NTRS)

Elrod, D. A.; Childs, D. W.

1986-01-01

A brief review of current annular seal theory and a discussion of the predicted effect on stiffness of tapering the seal stator are presented. An outline of Nelson's analytical-computational method for determining rotordynamic coefficients for annular compressible-flow seals is included. Modifications to increase the maximum rotor speed of an existing air-seal test apparatus at Texas A&M University are described. Experimental results, including leakage, entrance-loss coefficients, pressure distributions, and normalized rotordynamic coefficients, are presented for four convergent-tapered, smooth-rotor, smooth-stator seals. A comparison of the test results shows that an inlet-to-exit clearance ratio of 1.5 to 2.0 provides the maximum direct stiffness, a clearance ratio of 2.5 provides the greatest stability, and a clearance ratio of 1.0 provides the least stability. The experimental results are compared to theoretical results from Nelson's analysis with good agreement. Test results for cross-coupled stiffness show less sensitivity of fluid prerotation than predicted.

Experimental analysis and constitutive modelling of steel of A-IIIN strength class

NASA Astrophysics Data System (ADS)

Kruszka, Leopold; Janiszewski, Jacek

2015-09-01

Fundamentally important is the better understanding of behaviour of new building steels under impact loadings, including plastic deformations. Results of the experimental analysis in wide range of strain rates in compression at room temperature, as well as constitutive modelling for and B500SP structural steels of new A-IIIN Polish strength class, examined dynamically by split Hopkinson pressure bar technique at high strain rates, are presented in table and graphic forms. Dynamic mechanical characteristics of compressive strength for tested building structural steel are determined as well as dynamic mechanical properties of this material are compared with 18G2-b steel of A-II strength class, including effects of the shape of tested specimens, i.e. their slenderness. The paper focuses the attention on those experimental tests, their interpretation, and constitutive semi-empirical modelling of the behaviour of tested steels based on Johnson-Cook's model. Obtained results of analyses presented here are used for designing and numerical simulations of reinforced concrete protective structures.

The analytical representation of viscoelastic material properties using optimization techniques

NASA Technical Reports Server (NTRS)

Hill, S. A.

1993-01-01

This report presents a technique to model viscoelastic material properties with a function of the form of the Prony series. Generally, the method employed to determine the function constants requires assuming values for the exponential constants of the function and then resolving the remaining constants through linear least-squares techniques. The technique presented here allows all the constants to be analytically determined through optimization techniques. This technique is employed in a computer program named PRONY and makes use of commercially available optimization tool developed by VMA Engineering, Inc. The PRONY program was utilized to compare the technique against previously determined models for solid rocket motor TP-H1148 propellant and V747-75 Viton fluoroelastomer. In both cases, the optimization technique generated functions that modeled the test data with at least an order of magnitude better correlation. This technique has demonstrated the capability to use small or large data sets and to use data sets that have uniformly or nonuniformly spaced data pairs. The reduction of experimental data to accurate mathematical models is a vital part of most scientific and engineering research. This technique of regression through optimization can be applied to other mathematical models that are difficult to fit to experimental data through traditional regression techniques.

Determination of effective loss factors in reduced SEA models

NASA Astrophysics Data System (ADS)

Chimeno Manguán, M.; Fernández de las Heras, M. J.; Roibás Millán, E.; Simón Hidalgo, F.

2017-01-01

The definition of Statistical Energy Analysis (SEA) models for large complex structures is highly conditioned by the classification of the structure elements into a set of coupled subsystems and the subsequent determination of the loss factors representing both the internal damping and the coupling between subsystems. The accurate definition of the complete system can lead to excessively large models as the size and complexity increases. This fact can also rise practical issues for the experimental determination of the loss factors. This work presents a formulation of reduced SEA models for incomplete systems defined by a set of effective loss factors. This reduced SEA model provides a feasible number of subsystems for the application of the Power Injection Method (PIM). For structures of high complexity, their components accessibility can be restricted, for instance internal equipments or panels. For these cases the use of PIM to carry out an experimental SEA analysis is not possible. New methods are presented for this case in combination with the reduced SEA models. These methods allow defining some of the model loss factors that could not be obtained through PIM. The methods are validated with a numerical analysis case and they are also applied to an actual spacecraft structure with accessibility restrictions: a solar wing in folded configuration.

A novel method for determining calibration and behavior of PVDF ultrasonic hydrophone probes in the frequency range up to 100 MHz.

PubMed

Bleeker, H J; Lewin, P A

2000-01-01

A new calibration technique for PVDF ultrasonic hydrophone probes is described. Current implementation of the technique allows determination of hydrophone frequency response between 2 and 100 MHz and is based on the comparison of theoretically predicted and experimentally determined pressure-time waveforms produced by a focused, circular source. The simulation model was derived from the time domain algorithm that solves the non linear KZK (Khokhlov-Zabolotskaya-Kuznetsov) equation describing acoustic wave propagation. The calibration technique data were experimentally verified using independent calibration procedures in the frequency range from 2 to 40 MHz using a combined time delay spectrometry and reciprocity approach or calibration data provided by the National Physical Laboratory (NPL), UK. The results of verification indicated good agreement between the results obtained using KZK and the above-mentioned independent calibration techniques from 2 to 40 MHz, with the maximum discrepancy of 18% at 30 MHz. The frequency responses obtained using different hydrophone designs, including several membrane and needle probes, are presented, and it is shown that the technique developed provides a desirable tool for independent verification of primary calibration techniques such as those based on optical interferometry. Fundamental limitations of the presented calibration method are also examined.

Experimental investigation of burning rates of pure ethanol and ethanol blended fuels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Parag, Shintre; Raghavan, Vasudevan

2009-05-15

A fundamental experimental study to determine the burning rates of ethanol and ethanol-blended fossil fuels is presented. Pure liquid ethanol or its blends with liquid fossil fuels such as gasoline or diesel, has been transpired to the surface a porous sphere using an infusion pump. Burning of the fuel takes place on the surface of the porous sphere, which is placed in an air stream blowing upwards with a uniform velocity at atmospheric pressure and temperature under normal gravity conditions. At low air velocities, when ignited, a flame envelopes the sphere. For each sphere size, air stream velocity and fuelmore » type, the fuel feed rate will vary and the same is recorded as the burning rate for that configuration. The flame stand-off distances from the sphere surface are measured by post-processing the digital image of the flame photograph using suitable imaging software. The transition velocity at which the flame moves and establishes itself at the wake region of the sphere has been determined for different diameters and fuel types. Correlations of these parameters are also presented. (author)« less

Transmission effects in unfolding electronic-vibrational electron-molecule energy-loss spectra

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang Shiyang; Khakoo, Murtadha A.; Johnson, Paul V.

2006-03-15

The results of an investigation concerning the sensitivity of conventional unfolding methods applied to electronic-vibrational electron-energy-loss spectra to the transmission efficiency of electron spectrometers are presented. This investigation was made in an effort to understand differences in the differential cross sections for excitation of low-lying electronic states determined experimentally by various groups using electronic-vibrational energy-loss spectra of N{sub 2}. In these experiments, very similar spectral unfolding methods were used, which relied on similar Franck-Condon factors. However, the overall analyses of the electron scattering spectra (by the individual groups) resulted in large differences among the differential cross sections determined from thesemore » energy-loss spectra. The transmission response of the experimental apparatus to different-energy scattered electrons has often been discussed as a key factor that caused these disagreements. The present investigation shows in contrast that the effect of transmission is smaller than that required to independently explain such differences, implying that other systematic effects are responsible for the existing differences between measurements.« less

Test benches for studying the properties of car tyres

NASA Astrophysics Data System (ADS)

Kuznetsov, N. Yu.; Fedotov, A. I.; Vlasov, V. G.

2017-12-01

The article describes the design of the measuring systems of test benches used to study the properties of elastic tyres. The bench has two autonomous systems - for testing the braking properties of elastic tyres rolling in a plane parallel way and for testing tyre slip properties. The system for testing braking properties determines experimental characteristics of elastic tyres as the following dependencies: longitudinal response vs time, braking torque vs slip, angular velocity vs slip, and longitudinal response vs slip. The system for studying tyre slip properties determines both steady (dependence of the lateral response in a contact area on the slipping angle) and non-steady characteristics (time variation of the slipping angle as a result of turning from -40 to +40 degrees) of tyre slip. The article presents the diagrams of bench tests of elastic tyres. The experimental results show metrological parameters and functional capabilities of the bench for studying tyre properties in driving and braking modes. The metrological indices of the recorded parameters of the measuring system for studying tyre properties are presented in the table.

Physical and chemical interactions at the interface between atmospheric pressure plasmas and aqueous solutions

NASA Astrophysics Data System (ADS)

Lindsay, Alexander; Byrns, Brandon; Knappe, Detlef; Graves, David; Shannon, Steven

2014-10-01

Transport and reactions of charged species, neutrals, and photons at the interface between plasmas and liquids must be better quantified. The work presented here combines theoretical and experimental investigations of conditions in the gas and liquid phases in proximity to the interface for various discharges. OES is used to determine rotational and vibrational temperatures of OH, NO, and N2+; the relationship between these temperatures that characterize the distribution of internal energy states and gas and electron kinetic temperatures is considered. The deviation of OH rotational states from equilibrium under high humidity conditions is also presented. In contradiction with findings of other groups, high energy rotational states appear to become underpopulated with increasing humidity. In the aqueous phase, concentrations of longer-lived species such as nitrate, nitrite, hydrogen peroxide, and ozone are determined using ion chromatography and colorimetric methods. Spin-traps and electron paramagnetic resonance (EPR) are investigated for characterization of short-lived aqueous radicals like OH, O2-, NO, and ONOO-. Finally, experimental results are compared to a numerical model which couples transport and reactions within and between the bulk gas and liquid phases.

Continued Development and Validation of Methods for Spheromak Simulation

NASA Astrophysics Data System (ADS)

Benedett, Thomas

2015-11-01

The HIT-SI experiment has demonstrated stable sustainment of spheromaks; determining how the underlying physics extrapolate to larger, higher-temperature regimes is of prime importance in determining the viability of the inductively-driven spheromak. It is thus prudent to develop and validate a computational model that can be used to study current results and provide an intermediate step between theory and future experiments. A zero-beta Hall-MHD model has shown good agreement with experimental data at 14.5 kHz injector operation. Experimental observations at higher frequency, where the best performance is achieved, indicate pressure effects are important and likely required to attain quantitative agreement with simulations. Efforts to extend the existing validation to high frequency (~ 36-68 kHz) using an extended MHD model implemented in the PSI-TET arbitrary-geometry 3D MHD code will be presented. Results from verification of the PSI-TET extended MHD model using the GEM magnetic reconnection challenge will also be presented along with investigation of injector configurations for future SIHI experiments using Taylor state equilibrium calculations. Work supported by DoE.

Modelling of mechanical and filtration processes near the well with regard to anisotropy

NASA Astrophysics Data System (ADS)

Karev, V. I.; Klimov, D. M.; Kovalenko, Yu F.; Ustinov, K. B.

2018-04-01

A geomechanical approach to modeling deformation and seepage is presented. Three stages of modeling are described: choice of an appropriate mechanical model and its adaptation to the case in question, experimental determination of parameters of the model, simulation of processes of seepage for particular configurations of the well. The applied model allows describing the main specific characteristics of mechanical behavior of the collector: the influence of the pore pressure on deformation; the influence of not only shear but also comprehensive stresses and pore pressure on the transition to inelastic behavior; the appearance of inelastic volumetric deformation and its nontrivial dependence on the stress state; the anisotropy of elastic, strength and seepage properties; non-obvious dependence of permeability on the stress strain state. The model unites essential characteristics of Hill’s plastic flow theory for anisotropic materials and the Drucker–Prager theory for inelastic deformation of soils. The results of experimental determination of the involved parameters obtained using true triaxial loading system for the collector of Vladimir Filanovsky field in the Caspian Sea are presented.

Simplex optimization of headspace factors for headspace gas chromatography determination of residual solvents in pharmaceutical products.

PubMed

Grodowska, Katarzyna; Parczewski, Andrzej

2013-01-01

The purpose of the present work was to find optimum conditions of headspace gas chromatography (HS-GC) determination of residual solvents which usually appear in pharmaceutical products. Two groups of solvents were taken into account in the present examination. Group I consisted of isopropanol, n-propanol, isobutanol, n-butanol and 1,4-dioxane and group II included cyclohexane, n-hexane and n-heptane. The members of the groups were selected in previous investigations in which experimental design and chemometric methods were applied. Four factors were taken into consideration in optimization which describe HS conditions: sample volume, equilibration time, equilibrium temperature and NaCl concentration in a sample. The relative GC peak area served as an optimization criterion which was considered separately for each analyte. Sequential variable size simplex optimization strategy was used and the progress of optimization was traced and visualized in various ways simultaneously. The optimum HS conditions appeared different for the groups of solvents tested, which proves that influence of experimental conditions (factors) depends on analyte properties. The optimization resulted in significant signal increase (from seven to fifteen times).

Validation and Continued Development of Methods for Spheromak Simulation

NASA Astrophysics Data System (ADS)

Benedett, Thomas

2016-10-01

The HIT-SI experiment has demonstrated stable sustainment of spheromaks. Determining how the underlying physics extrapolate to larger, higher-temperature regimes is of prime importance in determining the viability of the inductively-driven spheromak. It is thus prudent to develop and validate a computational model that can be used to study current results and study the effect of possible design choices on plasma behavior. A zero-beta Hall-MHD model has shown good agreement with experimental data at 14.5 kHz injector operation. Experimental observations at higher frequency, where the best performance is achieved, indicate pressure effects are important and likely required to attain quantitative agreement with simulations. Efforts to extend the existing validation to high frequency (36-68 kHz) using an extended MHD model implemented in the PSI-TET arbitrary-geometry 3D MHD code will be presented. An implementation of anisotropic viscosity, a feature observed to improve agreement between NIMROD simulations and experiment, will also be presented, along with investigations of flux conserver features and their impact on density control for future SIHI experiments. Work supported by DoE.

Calorimetric method for determination of {sup 51}Cr neutrino source activity

DOE Office of Scientific and Technical Information (OSTI.GOV)

Veretenkin, E. P., E-mail: veretenk@inr.ru; Gavrin, V. N.; Danshin, S. N.

Experimental study of nonstandard neutrino properties using high-intensity artificial neutrino sources requires the activity of the sources to be determined with high accuracy. In the BEST project, a calorimetric system for measurement of the activity of high-intensity (a few MCi) neutrino sources based on {sup 51}Cr with an accuracy of 0.5–1% is created. In the paper, the main factors affecting the accuracy of determining the neutrino source activity are discussed. The calorimetric system design and the calibration results using a thermal simulator of the source are presented.

Development of advanced methods for analysis of experimental data in diffusion

NASA Astrophysics Data System (ADS)

Jaques, Alonso V.

There are numerous experimental configurations and data analysis techniques for the characterization of diffusion phenomena. However, the mathematical methods for estimating diffusivities traditionally do not take into account the effects of experimental errors in the data, and often require smooth, noiseless data sets to perform the necessary analysis steps. The current methods used for data smoothing require strong assumptions which can introduce numerical "artifacts" into the data, affecting confidence in the estimated parameters. The Boltzmann-Matano method is used extensively in the determination of concentration - dependent diffusivities, D(C), in alloys. In the course of analyzing experimental data, numerical integrations and differentiations of the concentration profile are performed. These methods require smoothing of the data prior to analysis. We present here an approach to the Boltzmann-Matano method that is based on a regularization method to estimate a differentiation operation on the data, i.e., estimate the concentration gradient term, which is important in the analysis process for determining the diffusivity. This approach, therefore, has the potential to be less subjective, and in numerical simulations shows an increased accuracy in the estimated diffusion coefficients. We present a regression approach to estimate linear multicomponent diffusion coefficients that eliminates the need pre-treat or pre-condition the concentration profile. This approach fits the data to a functional form of the mathematical expression for the concentration profile, and allows us to determine the diffusivity matrix directly from the fitted parameters. Reformulation of the equation for the analytical solution is done in order to reduce the size of the problem and accelerate the convergence. The objective function for the regression can incorporate point estimations for error in the concentration, improving the statistical confidence in the estimated diffusivity matrix. Case studies are presented to demonstrate the reliability and the stability of the method. To the best of our knowledge there is no published analysis of the effects of experimental errors on the reliability of the estimates for the diffusivities. For the case of linear multicomponent diffusion, we analyze the effects of the instrument analytical spot size, positioning uncertainty, and concentration uncertainty on the resulting values of the diffusivities. These effects are studied using Monte Carlo method on simulated experimental data. Several useful scaling relationships were identified which allow more rigorous and quantitative estimates of the errors in the measured data, and are valuable for experimental design. To further analyze anomalous diffusion processes, where traditional diffusional transport equations do not hold, we explore the use of fractional calculus in analytically representing these processes is proposed. We use the fractional calculus approach for anomalous diffusion processes occurring through a finite plane sheet with one face held at a fixed concentration, the other held at zero, and the initial concentration within the sheet equal to zero. This problem is related to cases in nature where diffusion is enhanced relative to the classical process, and the order of differentiation is not necessarily a second--order differential equation. That is, differentiation is of fractional order alpha, where 1 ≤ alpha < 2. For alpha = 2, the presented solutions reduce to the classical second-order diffusion solution for the conditions studied. The solution obtained allows the analysis of permeation experiments. Frequently, hydrogen diffusion is analyzed using electrochemical permeation methods using the traditional, Fickian-based theory. Experimental evidence shows the latter analytical approach is not always appropiate, because reported data shows qualitative (and quantitative) deviation from its theoretical scaling predictions. Preliminary analysis of data shows better agreement with fractional diffusion analysis when compared to traditional square-root scaling. Although there is a large amount of work in the estimation of the diffusivity from experimental data, reported studies typically present only the analytical description for the diffusivity, without scattering. However, because these studies do not consider effects produced by instrument analysis, their direct applicability is limited. We propose alternatives to address these, and to evaluate their influence on the final resulting diffusivity values.

Experimental determination of the dynamics of an acoustically levitated sphere

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pérez, Nicolás, E-mail: nico@fisica.edu.uy; Andrade, Marco A. B.; Canetti, Rafael

2014-11-14

Levitation of solids and liquids by ultrasonic standing waves is a promising technique to manipulate materials without contact. When a small particle is introduced in certain areas of a standing wave field, the acoustic radiation force pushes the particle to the pressure node. This movement is followed by oscillations of the levitated particle. Aiming to investigate the particle oscillations in acoustic levitation, this paper presents the experimental and numerical characterization of the dynamic behavior of a levitated sphere. To obtain the experimental response, a small sphere is lifted by the acoustic radiation force. After the sphere lift, it presents amore » damped oscillatory behavior, which is recorded by a high speed camera. To model this behavior, a mass-spring-damper system is proposed. In this model, the acoustic radiation force that acts on the sphere is theoretically predicted by the Gor'kov theory and the viscous forces are modeled by two damping terms, one term proportional to the square of the velocity and another term proportional to the particle velocity. The proposed model was experimentally verified by using different values of sound pressure amplitude. The comparison between numerical and experimental results shows that the model can accurately describe the oscillatory behavior of the sphere in an acoustic levitator.« less

Experimental determination of the dynamics of an acoustically levitated sphere

NASA Astrophysics Data System (ADS)

Pérez, Nicolás; Andrade, Marco A. B.; Canetti, Rafael; Adamowski, Julio C.

2014-11-01

Levitation of solids and liquids by ultrasonic standing waves is a promising technique to manipulate materials without contact. When a small particle is introduced in certain areas of a standing wave field, the acoustic radiation force pushes the particle to the pressure node. This movement is followed by oscillations of the levitated particle. Aiming to investigate the particle oscillations in acoustic levitation, this paper presents the experimental and numerical characterization of the dynamic behavior of a levitated sphere. To obtain the experimental response, a small sphere is lifted by the acoustic radiation force. After the sphere lift, it presents a damped oscillatory behavior, which is recorded by a high speed camera. To model this behavior, a mass-spring-damper system is proposed. In this model, the acoustic radiation force that acts on the sphere is theoretically predicted by the Gor'kov theory and the viscous forces are modeled by two damping terms, one term proportional to the square of the velocity and another term proportional to the particle velocity. The proposed model was experimentally verified by using different values of sound pressure amplitude. The comparison between numerical and experimental results shows that the model can accurately describe the oscillatory behavior of the sphere in an acoustic levitator.

Quantification and scaling of multipartite entanglement in continuous variable systems.

PubMed

Adesso, Gerardo; Serafini, Alessio; Illuminati, Fabrizio

2004-11-26

We present a theoretical method to determine the multipartite entanglement between different partitions of multimode, fully or partially symmetric Gaussian states of continuous variable systems. For such states, we determine the exact expression of the logarithmic negativity and show that it coincides with that of equivalent two-mode Gaussian states. Exploiting this reduction, we demonstrate the scaling of the multipartite entanglement with the number of modes and its reliable experimental estimate by direct measurements of the global and local purities.

Development and study of a heat pipe with dielectric properties

NASA Astrophysics Data System (ADS)

Semena, M. G.; Gershuni, A. N.; Chepurnoi, A. B.

Requirements for the structural elements of heat pipes with dielectric properties are examined. To obtain information necessary for the thermal analysis of heat pipes, a study is made of the capillary-transport characteristics of a dielectric capillary structure consisting of quartz fibers; the capillary pressure and the liquid penetration coefficient are determined. The results of the study are used to develop dielectric heat pipes for the cooling of a vacuum electronic instrument. Experimentally determined characteristics of the heat pipes are presented.

Ellipsometric study of metal-organic chemically vapor deposited III-V semiconductor structures

NASA Technical Reports Server (NTRS)

Alterovitz, Samuel A.; Sekula-Moise, Patricia A.; Sieg, Robert M.; Drotos, Mark N.; Bogner, Nancy A.

1992-01-01

An ellipsometric study of MOCVD-grown layers of AlGaAs and InGaAs in thick films and strained layer complex structures is presented. It is concluded that the ternary composition of thick nonstrained layers can be accurately determined to within experimental errors using numerical algorithms. In the case of complex structures, thickness of all layers and the alloy composition of nonstrained layers can be determined simultaneously, provided that the correlations between parameters is no higher than 0.9.

CO 2 laser cutting of MDF . 1. Determination of process parameter settings

NASA Astrophysics Data System (ADS)

Lum, K. C. P.; Ng, S. L.; Black, I.

2000-02-01

This paper details an investigation into the laser processing of medium-density fibreboard (MDF). Part 1 reports on the determination of process parameter settings for the effective cutting of MDF by CO 2 laser, using an established experimental methodology developed to study the interrelationship between and effects of varying laser set-up parameters. Results are presented for both continuous wave (CW) and pulse mode (PM) cutting, and the associated cut quality effects have been commented on.

Determining the 40K radioactivity in rocks using x-ray spectrometry

NASA Astrophysics Data System (ADS)

Pilakouta, M.; Kallithrakas-Kontos, N.; Nikolaou, G.

2017-09-01

In this paper we propose an experimental method for the determination of potassium-40 (40K) radioactivity in commercial granite samples using x-ray fluorescence (XRF). The method correlates the total potassium concentration (yield) in samples deduced by XRF analysis with the radioactivity of the sample due to the 40K radionuclide. This method can be used in an undergraduate student laboratory. A brief theoretical background and description of the method, as well as some results and their interpretation, are presented.

Determination of the three-dimensional structure of oligosaccharides in the solid state from experimental 13C NMR data and ab initio chemical shift surfaces.

PubMed

Sergeyev, Ivan; Moyna, Guillermo

2005-05-02

A novel method for the determination of the three-dimensional (3D) structure of oligosaccharides in the solid state using experimental 13C NMR data is presented. The approach employs this information, combined with 13C chemical shift surfaces (CSSs) for the glycosidic bond carbons in the generation of NMR pseudopotential energy functions suitable for use as constraints in molecular modeling simulations. Application of the method to trehalose, cellobiose, and cellotetraose produces 3D models that agree remarkably well with the reported X-ray structures, with phi and psi dihedral angles that are within 10 degrees from the ones observed in the crystals. The usefulness of the approach is further demonstrated in the determination of the 3D structure of the cellohexaose, an hexasaccharide for which no X-ray data has been reported, as well as in the generation of accurate structural models for cellulose II and amylose V6.

Determination of the nuclear level densities and radiative strength function for 43 nuclei in the mass interval 28≤A≤200

NASA Astrophysics Data System (ADS)

Knezevic, David; Jovancevic, Nikola; Sukhovoj, Anatoly M.; Mitsyna, Ludmila V.; Krmar, Miodrag; Cong, Vu D.; Hambsch, Franz-Josef; Oberstedt, Stephan; Revay, Zsolt; Stieghorst, Christian; Dragic, Aleksandar

2018-03-01

The determination of nuclear level densities and radiative strength functions is one of the most important tasks in low-energy nuclear physics. Accurate experimental values of these parameters are critical for the study of the fundamental properties of nuclear structure. The step-like structure in the dependence of the level densities p on the excitation energy of nuclei Eex is observed in the two-step gamma cascade measurements for nuclei in the 28 ≤ A ≤ 200 mass region. This characteristic structure can be explained only if a co-existence of quasi-particles and phonons, as well as their interaction in a nucleus, are taken into account in the process of gamma-decay. Here we present a new improvement to the Dubna practical model for the determination of nuclear level densities and radiative strength functions. The new practical model guarantees a good description of the available intensities of the two step gamma cascades, comparable to the experimental data accuracy.

State Equation Determination of Cow Dung Biogas

NASA Astrophysics Data System (ADS)

Marzuki, A.; Wicaksono, L. B.

2017-08-01

A state function is a thermodynamic function which relates various macroscopically measurable properties of a system (state variable) describing the state of matter under a given set of physical conditions. A good understanding of a biogas state function plays a very important role in an effort to maximize biogas processes and to help predicting combation performance. This paper presents a step by step process of an experimental study aimed at determining the equation of state of cow dung biogas. The equation was derived from the data obtained from the experimental results of compressibility (κ) and expansivity (β) following the general form of gas state equation dV = βdT + κdP. In this equation, dV is gas volume variation, dT is temperature variation, and dP is pressure variation. From these results, we formulated a unique state equation from which the biogas critical temperature (Tc) and critical pressure were then determined (Tc = 266.7 K, Pc = 5096647.5 Pa).

Theoretical and experimental evidence of non-symmetric doubly localized rogue waves.

PubMed

He, Jingsong; Guo, Lijuan; Zhang, Yongshuai; Chabchoub, Amin

2014-11-08

We present determinant expressions for vector rogue wave (RW) solutions of the Manakov system, a two-component coupled nonlinear Schrödinger (NLS) equation. As a special case, we generate a family of exact and non-symmetric RW solutions of the NLS equation up to third order, localized in both space and time. The derived non-symmetric doubly localized second-order solution is generated experimentally in a water wave flume for deep-water conditions. Experimental results, confirming the characteristic non-symmetric pattern of the solution, are in very good agreement with theory as well as with numerical simulations, based on the modified NLS equation, known to model accurately the dynamics of weakly nonlinear wave packets in deep water.

Theoretical and experimental evidence of non-symmetric doubly localized rogue waves

PubMed Central

He, Jingsong; Guo, Lijuan; Zhang, Yongshuai; Chabchoub, Amin

2014-01-01

We present determinant expressions for vector rogue wave (RW) solutions of the Manakov system, a two-component coupled nonlinear Schrödinger (NLS) equation. As a special case, we generate a family of exact and non-symmetric RW solutions of the NLS equation up to third order, localized in both space and time. The derived non-symmetric doubly localized second-order solution is generated experimentally in a water wave flume for deep-water conditions. Experimental results, confirming the characteristic non-symmetric pattern of the solution, are in very good agreement with theory as well as with numerical simulations, based on the modified NLS equation, known to model accurately the dynamics of weakly nonlinear wave packets in deep water. PMID:25383023

Laboratory test methods for combustion stability properties of solid propellants

NASA Technical Reports Server (NTRS)

Strand, L. D.; Brown, R. S.

1992-01-01

An overview is presented of experimental methods for determining the combustion-stability properties of solid propellants. The methods are generally based on either the temporal response to an initial disturbance or on external methods for generating the required oscillations. The size distribution of condensed-phase combustion products are characterized by means of the experimental approaches. The 'T-burner' approach is shown to assist in the derivation of pressure-coupled driving contributions and particle damping in solid-propellant rocket motors. Other techniques examined include the rotating-valve apparatus, the impedance tube, the modulated throat-acoustic damping burner, and the magnetic flowmeter. The paper shows that experimental methods do not exist for measuring the interactions between acoustic velocity oscillations and burning propellant.

Experimental confirmation of a PDE-based approach to design of feedback controls

NASA Technical Reports Server (NTRS)

Banks, H. T.; Smith, Ralph C.; Brown, D. E.; Silcox, R. J.; Metcalf, Vern L.

1995-01-01

Issues regarding the experimental implementation of partial differential equation based controllers are discussed in this work. While the motivating application involves the reduction of vibration levels for a circular plate through excitation of surface-mounted piezoceramic patches, the general techniques described here will extend to a variety of applications. The initial step is the development of a PDE model which accurately captures the physics of the underlying process. This model is then discretized to yield a vector-valued initial value problem. Optimal control theory is used to determine continuous-time voltages to the patches, and the approximations needed to facilitate discrete time implementation are addressed. Finally, experimental results demonstrating the control of both transient and steady state vibrations through these techniques are presented.

An experimental evaluation of the performance deficit of an aircraft engine starter turbine

NASA Technical Reports Server (NTRS)

Haas, J. E.; Roelke, R. J.; Hermann, P.

1980-01-01

An experimental investigation is presented to determine the aerodynamic performance deficit of a 13.5 - centimeter-tip-diameter aircraft engine starter turbine. The two-phased evaluation comprised both the stator and the stage performance, and the experimental design is described in detail. Data obtained from the investigation of three honeycomb shrouds clearly showed that the filled honeycomb reached a total efficiency of 0.868, 8.2 points higher than the open honeycomb shroud, at design equivalent conditions of speed and blade-jet speed ratio. It was concluded that the use of an open honeycomb shroud caused the large performance deficit for the starter turbine. Further research is suggested to ascertain stator inlet boundary layer measurements.

Changes across age groups in self-choice elaboration effects on incidental memory.

PubMed

Toyota, Hiroshi; Konishi, Tomoko

2004-08-01

The present study investigated age differences in the effects of a self-choice elaboration and an experimenter-provided elaboration on incidental memory. Adults, sixth grade, and second grade subjects chose which of two sentence frames the target fit better in a self-choice elaboration condition. They then judged whether each target made sense in its sentence frame in the experimenter-provided elaboration, then did free recall tests. Only adults recalled better the targets with an image sentence with self-choice elaboration, rather than experimenter-provided elaboration. However, self-choice elaboration was far superior for the recall of targets with nonimage sentences only for second graders. Thus, the effects of self-choice elaboration were determined both by age and by type of sentence frame.

Methods for determining the internal thrust of scramjet engine modules from experimental data

NASA Technical Reports Server (NTRS)

Voland, Randall T.

1990-01-01

Methods for calculating zero-fuel internal drag of scramjet engine modules from experimental measurements are presented. These methods include two control-volume approaches, and a pressure and skin-friction integration. The three calculation techniques are applied to experimental data taken during tests of a version of the NASA parametric scramjet. The methods agree to within seven percent of the mean value of zero-fuel internal drag even though several simplifying assumptions are made in the analysis. The mean zero-fuel internal drag coefficient for this particular engine is calculated to be 0.150. The zero-fuel internal drag coefficient when combined with the change in engine axial force with and without fuel defines the internal thrust of an engine.

Computational knee ligament modeling using experimentally determined zero-load lengths.

PubMed

Bloemker, Katherine H; Guess, Trent M; Maletsky, Lorin; Dodd, Kevin

2012-01-01

This study presents a subject-specific method of determining the zero-load lengths of the cruciate and collateral ligaments in computational knee modeling. Three cadaver knees were tested in a dynamic knee simulator. The cadaver knees also underwent manual envelope of motion testing to find their passive range of motion in order to determine the zero-load lengths for each ligament bundle. Computational multibody knee models were created for each knee and model kinematics were compared to experimental kinematics for a simulated walk cycle. One-dimensional non-linear spring damper elements were used to represent cruciate and collateral ligament bundles in the knee models. This study found that knee kinematics were highly sensitive to altering of the zero-load length. The results also suggest optimal methods for defining each of the ligament bundle zero-load lengths, regardless of the subject. These results verify the importance of the zero-load length when modeling the knee joint and verify that manual envelope of motion measurements can be used to determine the passive range of motion of the knee joint. It is also believed that the method described here for determining zero-load length can be used for in vitro or in vivo subject-specific computational models.

The noncavitating performance and life of a small vane-type positive displacement pump in liquid hydrogen

NASA Technical Reports Server (NTRS)

Ulbricht, T. E.; Hemminger, J. A.

1986-01-01

The low flow rate and high head rise requirements of hydrogen/oxygen auxiliary propulsion systems make the application of centrifugal pumps difficult. Positive displacement pumps are well-suited for these flow conditions, but little is known about their performance and life characteristics in liquid hydrogen. An experimental and analytical investigation was conducted to determine the performance and life characteristics of a vane-type, positive displacement pump. In the experimental part of this effort, mass flow rate and shaft torque were determined as functions of shaft speed and pump pressure rise. Since liquid hydrogen offers little lubrication in a rubbing situation, pump life is an issue. During the life test, the pump was operated intermittently for 10 hr at the steady-state point of 0.074 lbm/sec (0.03 kg/sec) flow rate, 3000 psid (2.07 MPa) pressure rise, and 8000 rpm (838 rad/sec) shaft speed. Pump performance was monitored during the life test series and the results indicated no loss in performance. Material loss from the vanes was recorded and wear of the other components was documented. In the analytical part of this effort, a comprehensive pump performance analysis computer code, developed in-house, was used to predict pump performance. The results of the experimental investigation are presented and compared with the results of the analysis. Results of the life test are also presented.

Learning styles: The learning methods of air traffic control students

NASA Astrophysics Data System (ADS)

Jackson, Dontae L.

In the world of aviation, air traffic controllers are an integral part in the overall level of safety that is provided. With a number of controllers reaching retirement age, the Air Traffic Collegiate Training Initiative (AT-CTI) was created to provide a stronger candidate pool. However, AT-CTI Instructors have found that a number of AT-CTI students are unable to memorize types of aircraft effectively. This study focused on the basic learning styles (auditory, visual, and kinesthetic) of students and created a teaching method to try to increase memorization in AT-CTI students. The participants were asked to take a questionnaire to determine their learning style. Upon knowing their learning styles, participants attended two classroom sessions. The participants were given a presentation in the first class, and divided into a control and experimental group for the second class. The control group was given the same presentation from the first classroom session while the experimental group had a group discussion and utilized Middle Tennessee State University's Air Traffic Control simulator to learn the aircraft types. Participants took a quiz and filled out a survey, which tested the new teaching method. An appropriate statistical analysis was applied to determine if there was a significant difference between the control and experimental groups. The results showed that even though the participants felt that the method increased their learning, there was no significant difference between the two groups.

Problems in obtaining perfect images by single-particle electron cryomicroscopy of biological structures in amorphous ice.

PubMed

Henderson, Richard; McMullan, Greg

2013-02-01

Theoretical considerations together with simulations of single-particle electron cryomicroscopy images of biological assemblies in ice demonstrate that atomic structures should be obtainable from images of a few thousand asymmetric units, provided the molecular weight of the whole assembly being studied is greater than the minimum needed for accurate position and orientation determination. However, with present methods of specimen preparation and current microscope and detector technologies, many more particles are needed, and the alignment of smaller assemblies is difficult or impossible. Only larger structures, with enough signal to allow good orientation determination and with enough images to allow averaging of many hundreds of thousands or even millions of asymmetric units, have successfully produced high-resolution maps. In this review, we compare the contrast of experimental electron cryomicroscopy images of two smaller molecular assemblies, namely apoferritin and beta-galactosidase, with that expected from perfect simulated images calculated from their known X-ray structures. We show that the contrast and signal-to-noise ratio of experimental images still require significant improvement before it will be possible to realize the full potential of single-particle electron cryomicroscopy. In particular, although reasonably good orientations can be obtained for beta-galactosidase, we have been unable to obtain reliable orientation determination from experimental images of apoferritin. Simulations suggest that at least 2-fold improvement of the contrast in experimental images at ~10 Å resolution is needed and should be possible.

Experimental and modeling study of chloride ingress into concrete and reinforcement corrosion initiation

NASA Astrophysics Data System (ADS)

Yu, Hui

Effects of reinforcement and coarse aggregate on chloride ingression into concrete and reinforcement corrosion initiation have been studied with experimental and modeling (finite element method) analyses. Once specimens were fabricated and exposed to a chloride solution, various experimental techniques were employed to determine the effect of reinforcement and coarse aggregate on time-to-corrosion and chloride ingress and concentration at corrosion locations. Model analyses were performed to verify and explain the experimental results. Based upon the results, it was determined that unexpectedly higher chloride concentrations were present on the top of the rebar trace than that to the side at the same depth and an inverse concentration gradient (increasing [ Cl-] with increasing depth) occurred near the top of rebars. Also, coarse aggregate volume profile in close proximity to the rebar and spatial distribution of these aggregates, in conjunction with the physical obstruction afforded by reinforcement to chloride flow, complicates concrete sampling for Cl- intended to define the critical concentration of this species to initiate corrosion. Modeling analyses that considered cover thickness, chloride threshold concentration, reinforcement size and shape, and coarse aggregate type and percolation confirmed the experimental findings. The results, at least in part, account for the relatively wide spread in chloride corrosion threshold values reported in the literature and illustrate that more consistent chloride threshold concentrations can be acquired from mortar or paste specimens than from concrete ones.

Crossflow Stability and Transition Experiments in a Swept-Wing Flow. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Dagenhart, John Ray

1992-01-01

An experimental examination of crossflow instability and transition on a 45 degree swept wing is conducted in the Arizona State University Unsteady Wind Tunnel. The stationary-vortex pattern and transition location are visualized using both sublimating-chemical and liquid-crystal coatings. Extensive hot-wire measurements are conducted at several measurement stations across a single vortex track. The mean and travelling-wave disturbances are measured simultaneously. Stationary-crossflow disturbance profiles are determined by subtracting either a reference or a span-averaged velocity profile from the mean-velocity data. Mean, stationary-crossflow, and travelling-wave velocity data are presented as local boundary-layer profiles and as contour plots across a single stationary-crossflow vortex track. Disturbance-mode profiles and growth rates are determined. The experimental data are compared to predictions from linear stability theory.

Experimental investigation of an inversion technique for the determination of broadband duct mode amplitudes by the use of near-field sensor arrays.

PubMed

Castres, Fabrice O; Joseph, Phillip F

2007-08-01

This paper is an experimental investigation of an inverse technique for deducing the amplitudes of the modes radiated from a turbofan engine, including schemes for stablizing the solution. The detection of broadband modes generated by a laboratory-scaled fan inlet is performed using a near-field array of microphones arranged in a geodesic geometry. This array geometry is shown to allow a robust and accurate modal inversion. The sound power radiated from the fan inlet and the coherence function between different modal amplitudes are also presented. The knowledge of such modal content is useful in helping to characterize the source mechanisms of fan broadband noise generation, for determining the most appropriate mode distribution model for duct liner predictions, and for making sound power measurements of the radiated sound field.

Experimental parameters optimization of instrumental neutron activation analysis in order to determine selected elements in some industrial soils in Turkey

NASA Astrophysics Data System (ADS)

Haciyakupoglu, Sevilay; Nur Esen, Ayse; Erenturk, Sema

2014-08-01

The purpose of this study is optimization of the experimental parameters for analysis of soil matrix by instrumental neutron activation analysis and quantitative determination of barium, cerium, lanthanum, rubidium, scandium and thorium in soil samples collected from industrialized urban areas near Istanbul. Samples were irradiated in TRIGA MARK II Research Reactor of Istanbul Technical University. Two types of reference materials were used to check the accuracy of the applied method. The achieved results were found to be in compliance with certified values of the reference materials. The calculated En numbers for mentioned elements were found to be less than 1. The presented data of element concentrations in soil samples will help to trace the pollution as an impact of urbanization and industrialization, as well as providing database for future studies.

Wavelengths and energy levels for the Zn I isoelectronic sequence Sn{sup 20+} through U{sup 62+}

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brown, C.M.; Seely, J.F.; Kania, D.R.

Calculated and experimentally determined transition energies are presented for the Zn I isoelectronic sequence for the elements with atomic numbers Z = 50-92. The excitation energies were calculated for the 84 levels belonging to the 10 configurations of the type 4l4l{prime} by using the Hebrew University Lawrence Livermore Atomic Code (HULLAC). The analysis of the energy level structure along the isoelectronic sequence accounted for 20 avoided level crossings. The differences between the calculated and experimental transition energies were determined for 16 transitions, and the excitation energies of the levels belonging to the 4s4p, 4p{sup 2}, 4s4d, and 4s4f configurations weremore » derived from the semiempirically corrected transition energies. 16 refs., 3 figs., 1 tab.« less

Experimental Study of Axially Tension Cold Formed Steel Channel Members

NASA Astrophysics Data System (ADS)

Apriani, Widya; Lubis, Fadrizal; Angraini, Muthia

2017-12-01

Experimental testing is commonly used as one of the steps to determine the cause of the collapse of a building structure. The collapse of structures can be due to low quality materials. Although material samples have passed laboratory tests and the existing technical specifications have been met but there may be undetected defects and known material after failure. In this paper will be presented Experimental Testing of Axially Tension Cold Formed Steel Channel Members to determine the cause of the collapse of a building roof truss x in Pekanbaru. Test of tensile strength material cold formed channel sections was performed to obtain the main characteristics of Cold Formed steel material, namely ultimate tensile strength loads that can be held by members and the yield stress possessed by channel sections used in construction. Analysis of axially tension cold formed steel channel section presents in this paper was conducted through experimental study based on specificationsAnnualBook of ASTM Standards: Metal Test methods and Analitical Procedures, Section 3 (1991). The result of capacity loads experimental test was compared with design based on SNI 03-7971-2013standard of Indonesia for the design of cold formed steel structural members. The results of the yield stress of the material will be seen against the minimum allowable allowable stress range. After the test, the percentace of ultimate axial tension capacity theory has a result that is 16.46% larger than the ultimate axial tension capacity experimental. When compared with the load that must be borne 5.673 kN/m it can be concluded that 2 specimens do not meet. Yield stress of member has fulfilled requirement that wass bigger than 550 MPa. Based on the curve obtained ultimate axial tension capacity theory, results greater than experimental. The greatest voltage value (fu) is achieved under the same conditions as its yield stress. For this specimen with a melting voltage value fy = 571.5068 MPa has fulfilled the minimum melting point value of 550 MPa required for standard mild steel materials in accordance with the code SNI 03-7971-2013 about Cold formed steel.

Experimental Study of Axially Tension Cold Formed Steel Channel Members

NASA Astrophysics Data System (ADS)

Apriani, Widya; Lubis, Fadrizal; Angraini, Muthia

2017-12-01

Experimental testing is commonly used as one of the steps to determine the cause of the collapse of a building structure. The collapse of structures can be due to low quality materials. Although material samples have passed laboratory tests and the existing technical specifications have been met but there may be undetected defects and known material after failure. In this paper will be presented Experimental Testing of Axially Tension Cold Formed Steel Channel Members to determine the cause of the collapse of a building roof truss x in Pekanbaru. Test of tensile strength material cold formed channel sections was performed to obtain the main characteristics of Cold Formed steel material, namely ultimate tensile strength loads that can be held by members and the yield stress possessed by channel sections used in construction. Analysis of axially tension cold formed steel channel section presents in this paper was conducted through experimental study based on specificationsAnnualBook of ASTM Standards: Metal Test methods and Analitical Procedures, Section 3 (1991). The result of capacity loads experimental test was compared with design based on SNI 03-7971- 2013standard of Indonesia for the design of cold formed steel structural members. The results of the yield stress of the material will be seen against the minimum allowable allowable stress range. After the test, the percentace of ultimate axial tension capacity theory has a result that is 16.46% larger than the ultimate axial tension capacity experimental. When compared with the load that must be borne 5.673 kN/m it can be concluded that 2 specimens do not meet. Yield stress of member has fulfilled requirement that wass bigger than 550 MPa. Based on the curve obtained ultimate axial tension capacity theory, results greater than experimental. The greatest voltage value (fu) is achieved under the same conditions as its yield stress. For this specimen with a melting voltage value fy = 571.5068 MPa has fulfilled the minimum melting point value of 550 MPa required for standard mild steel materials in accordance with the code SNI 03- 7971-2013 about Cold formed steel.

ATR technique, an appropriate method for determining the degree of conversion in dental giomers

NASA Astrophysics Data System (ADS)

Prejmerean, Cristina; Prodan, Doina; Vlassa, Mihaela; Streza, Mihaela; Buruiana, Tinca; Colceriu, Loredana; Prejmerean, Vasile; Cuc, Stanca; Moldovan, Marioara

2016-12-01

Dental light-curing giomers were developed to combine the favourable properties of diacrylic resin composites (DRCs) and glass-ionomer cements (GICs) in a single material and to eliminate their inherent drawbacks. Giomers are characterized by their aesthetic appearance, high mechanical properties, adhesion to dental tissues as well as fluoride release and recharge abilities. The qualities of the giomers are greatly influenced by the level of conversion of the component resins. Infrared spectroscopy is one of the most largely used techniques for the determination of the degree of conversion in resin-based dental materials. However different results were obtained due to the performances of the used methods. The present work presents the determination of conversion degree in a series of dental copolymers and their corresponding giomers using transmission Fourier transform infrared spectroscopy (FTIR) and an attenuated total reflection technique (ATR) technique, respectively, the main aim being the study of the influence of the materials composition and of the light curing modes upon the achieved conversion in the cured giomers. Beautifil II commercial giomer was used as a control. A halogen lamp and a diode-blue LED lamp were used for the curing of the materials. The results showed that the composition of the resins greatly influenced the conversion. The highest conversions (up to 79%) were obtained in the case of the experimental giomers which contained the experimental Bis-GMA urethane analogue, followed by the Beautifil II giomer (61%) and experimental giomers based on commercial Bis-GMA (up to 50%), respectively. The resins light-cured by using the diode-blue LED lamp presented slightly higher conversions than the resins cured by halogen lamp. The study demonstrates the possibility to evaluate easily and reproducibly the conversion in light-curing composite materials with complex chemical composition and structure, particularly in the case of giomers by using the ATR technique.

Light field otoscope design for 3D in vivo imaging of the middle ear

PubMed Central

Bedard, Noah; Shope, Timothy; Hoberman, Alejandro; Haralam, Mary Ann; Shaikh, Nader; Kovačević, Jelena; Balram, Nikhil; Tošić, Ivana

2016-01-01

We present a light field digital otoscope designed to measure three-dimensional shape of the tympanic membrane. This paper describes the optical and anatomical considerations we used to develop the prototype, along with the simulation and experimental measurements of vignetting, field curvature, and lateral resolution. Using an experimental evaluation procedure, we have determined depth accuracy and depth precision of our system to be 0.05–0.07 mm and 0.21–0.44 mm, respectively. To demonstrate the application of our light field otoscope, we present the first three-dimensional reconstructions of tympanic membranes in normal and otitis media conditions, acquired from children who participated in a feasibility study at the Children’s Hospital of Pittsburgh of the University of Pittsburgh Medical Center. PMID:28101416

Experimental investigation of an axisymmetric free jet with an initially uniform velocity profile

NASA Technical Reports Server (NTRS)

Labus, T. L.; Symons, E. P.

1972-01-01

An experimental investigation was conducted to determine the flow characteristics of a circular free helium jet having an initially uniform velocity profile. Complete velocity profiles are presented at Reynolds numbers of 1027 and 4571 at 0, 3, 6, 10, 15, and 20 nozzle diameters (where possible) from the nozzle exit. Centerline velocity decay and potential core length were obtained over a range of Reynolds numbers from 155 to 5349 at distances up to and including 25 nozzle diameters from the nozzle exit. The angles of spread associated with the diffusion of the jet downstream of the nozzle are also given. Axial jet momentum flux and entrained mass flux, at various distances downstream of the nozzle, are presented as a function of the jet Reynolds number.

Exit Presentation: Infrared Thermography on Graphite/Epoxy

NASA Technical Reports Server (NTRS)

Comeaux, Kayla

2010-01-01

This slide presentation reports on the internship project that was accomplished during the summer of 2010. The objectives of the project were to: (1) Simulate Flash Thermography on Graphite/Epoxy Flat Bottom hole Specimen and thin void specimens, (2) Obtain Flash Thermography data on Graphite/Epoxy flat bottom hole specimens, (3) Compare experimental results with simulation results, Compare Flat Bottom Hole Simulation with Thin Void Simulation to create a graph to determine size of IR Thermography detected defects

Low-energy electron inelastic mean free paths for liquid water

NASA Astrophysics Data System (ADS)

Nguyen-Truong, Hieu T.

2018-04-01

We improve the Mermin–Penn algorithm (MPA) for determining the energy loss function (ELF) within the dielectric formalism. The present algorithm is applicable not only to real metals, but also to materials that have an energy gap in the excitation spectrum. Applying the improved MPA to liquid water, we show that the present algorithm is able to address the ELF overestimation at the energy gap, and the calculated results are in good agreement with experimental data.

Two Growth Modes of Graphitic Carbon Nanofibers with Herring-Bone Structure

DOE Office of Scientific and Technical Information (OSTI.GOV)

Merkulov, Igor A; Melechko, Anatoli Vasilievich; Wells, Jack C

2005-01-01

A simple mathematical model of the carbon nanofiber catalytic growth process is presented. Two major types of the fiber-catalyst interface shapes have been identified and described having qualitatively different structure in the center of a nanofiber. Presently, we discuss that the appearance of the irregular structure in the nanofiber central area is a result of curved-interface-growth kinematics. We suggest the method to determine the phenomenological parameters of the developed model from experimental data.

Two growth modes of graphitic carbon nanofibers with herring-bone structure

NASA Astrophysics Data System (ADS)

Merkulov, I. A.; Meleshko, A. V.; Wells, J. C.; Cui, H.; Merkulov, V. I.; Simpson, M. L.; Lowndes, D. H.

2005-07-01

A simple mathematical model of the carbon nanofiber catalytic growth process is presented. Two major types of the fiber-catalyst interface shapes have been identified and described having qualitatively different structure in the center of a nanofiber. Presently, we discuss that the appearance of the irregular structure in the nanofiber central area is a result of curved-interface-growth kinematics. We suggest the method to determine the phenomenological parameters of the developed model from experimental data.

Mathematical simulation of the drying of suspensions and colloidal solutions by their depressurization

NASA Astrophysics Data System (ADS)

Lashkov, V. A.; Levashko, E. I.; Safin, R. G.

2006-05-01

The heat and mass transfer in the process of drying of high-humidity materials by their depressurization has been investigated. The results of experimental investigation and mathematical simulation of the indicated process are presented. They allow one to determine the regularities of this process and predict the quality of the finished product. A technological scheme and an engineering procedure for calculating the drying of the liquid base of a soap are presented.

Neural and Behavioral Evidence for the Role of Mental Simulation in Meaning in Life

PubMed Central

Waytz, Adam; Hershfield, Hal E; Tamir, Diana I

2014-01-01

Mental simulation, the process of self-projection into alternate temporal, spatial, social, or hypothetical realities is a distinctively human capacity. Numerous lines of research also suggest that the tendency for mental simulation is associated with enhanced meaning. The present research tests this association specifically examining the relationship between two forms of simulation (temporal and spatial) and meaning in life. Study 1 uses neuroimaging to demonstrate that enhanced connectivity in the medial temporal lobe network, a subnetwork of the brain’s default network implicated in prospection and retrospection, correlates with self-reported meaning in life. Study 2 demonstrates that experimentally inducing people to think about the past or future versus the present enhances self-reported meaning in life, through the generation of more meaningful events. Study 3 demonstrates that experimentally inducing people to think specifically versus generally about the past or future enhances self-reported meaning in life. Study 4 turns to spatial simulation to demonstrate that experimentally inducing people to think specifically about an alternate spatial location (from the present) increases meaning derived from this simulation compared to thinking generally about another location or specifically about one’s present location. Study 5 demonstrates that experimentally inducing people to think about an alternate spatial location versus one’s present location enhances meaning in life, through meaning derived from this simulation. Study 6 demonstrates that simply asking people to imagine completing a measure of meaning in life in an alternate location compared to asking them to do so in their present location enhances reports of meaning. This research sheds light on an important determinant of meaning in life and suggests that undirected mental simulation benefits psychological well-being. PMID:25603379

Determination of Flaw Size and Depth From Temporal Evolution of Thermal Response

NASA Technical Reports Server (NTRS)

Winfree, William P.; Zalameda, Joseph N.; Cramer, Elliott; Howell, Patricia A.

2015-01-01

Simple methods for reducing the pulsed thermographic responses of flaws have tended to be based on either the spatial or temporal response. This independent assessment limits the accuracy of characterization. A variational approach is presented for reducing the thermographic data to produce an estimated size for a flaw that incorporates both the temporal and spatial response to improve the characterization. The size and depth are determined from both the temporal and spatial thermal response of the exterior surface above a flaw and constraints on the length of the contour surrounding the delamination. Examples of the application of the technique to simulation and experimental data acquired are presented to investigate the limitations of the technique.

Pressure Drop Across Woven Screens Under Uniform and Nonuniform Flow Conditions. [flow characteristics of water through Dutch twill and square weave fabrics

NASA Technical Reports Server (NTRS)

Ludewig, M.; Omori, S.; Rao, G. L.

1974-01-01

Tests were conducted to determine the experimental pressure drop and velocity data for water flowing through woven screens. The types of materials used are dutch twill and square weave fabrics. Pressure drop measures were made at four locations in a rectangular channel. The data are presented as change in pressure compared with the average entry velocity and the numerical relationship is determined by dividing the volumetric flow rate by the screen area open to flow. The equations of continuity and momentum are presented. A computer program listing an extension of a theoretical model and data from that computer program are included.

Determination of the effective refractive index spectrum of a quantum-well semiconductor laser diode from the measured modal gain spectrum

NASA Astrophysics Data System (ADS)

Wu, Linzhang; Tian, Wei; Gao, Feng

2004-09-01

This paper presents a self-consistent method to directly determine the effective refractive-index spectrum of a semiconductor quantum-well (QW) laser diode from the measured modal gain spectrum for a given current. The dispersion spectra of the optical waveguide confinement factor and the strongly carrier-density-dependent refractive index of the QW active layer of the test laser are also accurately obtained. The experimental result from a single QW GaInP/AlGaInP laser diode, which has 6 nm thick compressively strained Ga0.4InP active layer sandwiched by two 80 nm thick Al0.33GaInP, is presented.

A novel approach to the experimental study on methane/steam reforming kinetics using the Orthogonal Least Squares method

NASA Astrophysics Data System (ADS)

Sciazko, Anna; Komatsu, Yosuke; Brus, Grzegorz; Kimijima, Shinji; Szmyd, Janusz S.

2014-09-01

For a mathematical model based on the result of physical measurements, it becomes possible to determine their influence on the final solution and its accuracy. However, in classical approaches, the influence of different model simplifications on the reliability of the obtained results are usually not comprehensively discussed. This paper presents a novel approach to the study of methane/steam reforming kinetics based on an advanced methodology called the Orthogonal Least Squares method. The kinetics of the reforming process published earlier are divergent among themselves. To obtain the most probable values of kinetic parameters and enable direct and objective model verification, an appropriate calculation procedure needs to be proposed. The applied Generalized Least Squares (GLS) method includes all the experimental results into the mathematical model which becomes internally contradicted, as the number of equations is greater than number of unknown variables. The GLS method is adopted to select the most probable values of results and simultaneously determine the uncertainty coupled with all the variables in the system. In this paper, the evaluation of the reaction rate after the pre-determination of the reaction rate, which was made by preliminary calculation based on the obtained experimental results over a Nickel/Yttria-stabilized Zirconia catalyst, was performed.

Determining the VLF/ULF source height using phase measurements

NASA Astrophysics Data System (ADS)

Ryabov, A.; Kotik, D. S.

2012-12-01

Generation of ULF/VLF waves in the ionosphere using powerful RF facilities has been studied for the last 40 years, both theoretically and experimentally. During this time, it was proposed several mechanisms for explaining the experimental results: modulation of ionospheric currents based on thermal nonlinearity, ponderomotive mechanisms for generation both VLF and ULF signals, cubic nonlinearity, etc. According mentioned above mechanisms the VLF/ULF signal source could be located in the lower or upper ionosphere. The group velocity of signal propagation in the ionosphere is significantly smaller than speed of light. As a result the appreciable time delay of the received signals will occur at the earth surface. This time delay could be determine by measuring the phase difference between received and reference signals, which are GPS synchronized. The experiment on determining the time delay of ULF signal propagation from the ionospheric source was carried out at SURA facility in 2012 and the results are presented in this paper. The comparison with numerical simulation of the time delay using the adjusted IRI model and ionosonde data shows well agreement with the experimental observations. The work was supported by RFBR grant 11-02-00419-a and RF Ministry of education and science by state contract 16.518.11.7066.

Determination of the core temperature of a Li-ion cell during thermal runaway

NASA Astrophysics Data System (ADS)

Parhizi, M.; Ahmed, M. B.; Jain, A.

2017-12-01

Safety and performance of Li-ion cells is severely affected by thermal runaway where exothermic processes within the cell cause uncontrolled temperature rise, eventually leading to catastrophic failure. Most past experimental papers on thermal runaway only report surface temperature measurement, while the core temperature of the cell remains largely unknown. This paper presents an experimentally validated method based on thermal conduction analysis to determine the core temperature of a Li-ion cell during thermal runaway using surface temperature and chemical kinetics data. Experiments conducted on a thermal test cell show that core temperature computed using this method is in good agreement with independent thermocouple-based measurements in a wide range of experimental conditions. The validated method is used to predict core temperature as a function of time for several previously reported thermal runaway tests. In each case, the predicted peak core temperature is found to be several hundreds of degrees Celsius higher than the measured surface temperature. This shows that surface temperature alone is not sufficient for thermally characterizing the cell during thermal runaway. Besides providing key insights into the fundamental nature of thermal runaway, the ability to determine the core temperature shown here may lead to practical tools for characterizing and mitigating thermal runaway.

Sorption equilibrium, thermodynamics and pH-indicator properties of cresyl violet dye/bentonite composite system.

PubMed

Georgieva, Nedyalka; Yaneva, Zvezdelina; Dermendzhieva, Diyana

2017-09-01

The aim of the present study was to develop cresyl violet (CV)/bentonite composite system, to investigate the equilibrium sorption of the fluorescent dye on bentonite, to determine the characteristic equilibrium and thermodynamic parameters of the system by appropriate empirical isotherm models and to assess its pH-indicator properties. The absorption characteristics of CV solutions were investigated by UV/VIS spectrophotometer. Equilibrium experiments were conducted and the experimental data were modelled by six mathematical isotherm models. The analyses of the experimental data showed that bentonite exhibited significantly high capacity - 169.92 mg/g, towards CV. The encapsulation efficiency was 85%. The Langmuir, Flory-Huggins and El-Awady models best represented the experimental results. The free Gibbs energy of adsorption (ΔG o ) was calculated on the basis of the values of the equilibrium coefficients determined by the proposed models. The values of ΔG determined by the Langmuir, Temkin and Flory-Huggins models are within the range -20 to -40 kJ/mol, which indicates that the adsorption process is spontaneous and chemisorption takes place due to charge sharing or transfer from the dye molecules to the sorbent surface as a coordinate type of bond. The investigations of the obtained CV/bentonite hybrid systems for application as pH-markers showed satisfactory results.

Effect of investigator disturbance in experimental forensic entomology: succession and community composition.

PubMed

De Jong, G D; Hoback, W W

2006-06-01

Carrion insect succession studies have historically used repeated sampling of single or a few carcasses to produce data, either weighing the carcasses, removing a qualitative subsample of the fauna present, or both, on every visit over the course of decomposition and succession. This study, conducted in a set of related experimental hypotheses with two trials in a single season, investigated the effect that repeated sampling has on insect succession, determined by the number of taxa collected on each visit and by community composition. Each trial lasted at least 21 days, with daily visits on the first 14 days. Rat carcasses used in this study were all placed in the field on the same day, but then either sampled qualitatively on every visit (similar to most succession studies) or ignored until a given day of succession, when they were sampled qualitatively (a subsample) and then destructively sampled in their entirety. Carcasses sampled on every visit were in two groups: those from which only a sample of the fauna was taken and those from which a sample of fauna was taken and the carcass was weighed for biomass determination. Of the carcasses visited only once, the number of taxa in subsamples was compared to the actual number of taxa present when the carcass was destructively sampled to determine if the subsamples adequately represented the total carcass fauna. Data from the qualitative subsamples of those carcasses visited only once were also compared to data collected from carcasses that were sampled on every visit to investigate the effect of the repeated sampling. A total of 39 taxa were collected from carcasses during the study and the component taxa are discussed individually in relation to their role in succession. Number of taxa differed on only one visit between the qualitative subsamples and the actual number of taxa present, primarily because the organisms missed by the qualitative sampling were cryptic (hidden deep within body cavities) or rare (only represented by very few specimens). There were no differences discovered between number of taxa in qualitative subsamples from carcasses sampled repeatedly (with or without biomass determinations) and those sampled only a single time. Community composition differed considerably in later stages of decomposition, with disparate communities due primarily to small numbers of rare taxa. These results indicate that the methods used historically for community composition determination in experimental forensic entomology are generally adequate.

Measuring the ionization balance of gold in a low-density plasma of importance to ICF

DOE Office of Scientific and Technical Information (OSTI.GOV)

May, M; Beiersdorfer, P; Schneider, M

Charge state distributions (CSDs) have been determined in low density ({approx}10 {sup 12} cm{sup -3}) gold plasmas having either a monoenergetic beam (E{sub Beam} = 2.66, 3.53 and 4.54 keV) or experimentally simulated thermal electron distributions (T{sub e} = 2.0, 2.5 and 3.0 keV). These plasmas were created in the Livermore electron beam ion traps EBIT-I and EBIT-II. Line emission and radiative recombination features of Ni to Kr-like gold ions were recorded in the x-ray region with a crystal spectrometer and a photometrically calibrated microcalorimeter. The CSDs in the experimentally simulated thermal plasmas were inferred by fitting the observed 4f{yields}3dmore » and 5f{yields}3d lines with synthetic spectra from the Hebrew University Lawrence Livermore Atomic Code (HULLAC). Additionally, the CSDs in the beam plasmas were inferred both from fitting the line emission and fitting the radiative recombination emission to calculations from the General Relativistic Atomic Structure Program (GRASP). Despite the relatively simple atomic physics in the low density plasma, differences existed between the experimental CSDs and the simulations from several available codes (e.g. RIGEL). Our experimental CSD relied upon accurate electron impact cross sections provided by HULLAC. To determine their reliability, we have experimentally determined the cross sections for several of the n=3{yields}4 and n=3{yields}5 excitations in Ni to Ga-like Au and compared them to distorted wave calculations. Recent Au spectra recorded during experiments at the HELEN laser facility are presented and compared with those from EBIT-I and EBIT-II.« less

Measuring the Ionization Balance of Gold in a Low-Density Plasma of Importance to ICF

DOE Office of Scientific and Technical Information (OSTI.GOV)

May, M.J.; Beiersdorfer, P.; Schneider, M.

Charge state distributions (CSDs) have been determined in low density ({approx_equal}1012 cm-3) gold plasmas having either a monoenergetic beam (EBeam = 2.66, 3.53 and 4.54 keV) or experimentally simulated thermal electron distributions (Te = 2.0, 2.5 and 3.0 keV). These plasmas were created in the Livermore electron beam ion traps EBIT-I and EBIT-II. Line emission and radiative recombination features of Ni to Kr-like gold ions were recorded in the x-ray region with a crystal spectrometer and a photometrically calibrated microcalorimeter. The CSDs in the experimentally simulated thermal plasmas were inferred by fitting the observed 4f{yields}3d and 5f{yields}3d lines with syntheticmore » spectra from the Hebrew University Lawrence Livermore Atomic Code (HULLAC). Additionally, the CSDs in the beam plasmas were inferred both from fitting the line emission and fitting the radiative recombination emission to calculations from the General Relativistic Atomic Structure Program (GRASP). Despite the relatively simple atomic physics in the low density plasma, differences existed between the experimental CSDs and the simulations from several available codes (e.g. RIGEL). Our experimental CSD relied upon accurate electron impact cross sections provided by HULLAC. To determine their reliability, we have experimentally determined the cross sections for several of the n=3{yields}4 and n=3{yields}5 excitations in Ni to Ga-like Au and compared them to distorted wave calculations. Recent Au spectra recorded during experiments at the HELEN laser facility are presented and compared with those from EBIT-I and EB0011IT-.« less

Computation of transmitted and received B1 fields in magnetic resonance imaging.

PubMed

Milles, Julien; Zhu, Yue Min; Chen, Nan-Kuei; Panych, Lawrence P; Gimenez, Gérard; Guttmann, Charles R G

2006-05-01

Computation of B1 fields is a key issue for determination and correction of intensity nonuniformity in magnetic resonance images. This paper presents a new method for computing transmitted and received B1 fields. Our method combines a modified MRI acquisition protocol and an estimation technique based on the Levenberg-Marquardt algorithm and spatial filtering. It enables accurate estimation of transmitted and received B1 fields for both homogeneous and heterogeneous objects. The method is validated using numerical simulations and experimental data from phantom and human scans. The experimental results are in agreement with theoretical expectations.

The influence of distance between vehicles in platoon on aerodynamic parameters

NASA Astrophysics Data System (ADS)

Gnatowska, Renata; Sosnowski, Marcin

2018-06-01

The paper presents the results of experimental and numerical research focused on the reduction of fuel consumption of vehicles driving one after another in a so-called platoon arrangement. The aerodynamic parameters and safety issues were analyzed in order to determine the optimal distance between the vehicles in traffic conditions. The experimental research delivered the results concerning the drag and was performed for simplified model of two vehicles positioned in wind tunnel equipped with aerodynamic balance. The additional numerical analysis allowed investigating the pressure and velocity fields as well as other aerodynamics parameters of the test case.

An experimental investigation of ejector performance based upon different refrigerants

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, S.L.; Yen, J.Y.; Huang, M.C.

1998-12-31

This article experimentally compares the characteristics of different refrigerants as the working fluid in an ejector cooling system. The study covers common refrigerants including R-113, R-114, R-142b, and R-718. The critical choking conditions against the variation of condenser back pressure, the evaporator pressure, and the generator pressure are determined for each refrigerant. The results are compiled into a convenient performance curve and COP chart. These results can serve as an important reference for future design of ejector cooling systems. Finally, this paper presents a comparison of the performances of different refrigerants in an ejector cooling system.

[Practice of the use of remote telemedical consultations in "experimental area of work"].

PubMed

Kalachev, O V; Plakhov, A N; Pershin, I V; Agapitov, A A; Andreev, A I; Yakovlev, A E

2016-02-01

The article presents experimental results of telehealth technology of "medical company--military hospital--central military hospital". Requirements for the equipment, which is used for telehealth consultations and software are specified. Throughout the test were practiced emergency consultations of "physician-physician" interface, including the use of mobile video call and portable terminals of videoconference, remote diagnosis with the use of medical equipment and devices. Data transmission features and video definition are received. The authors determined main types of telecommunication equipment, which are supposed to prospective for the Armed Forces. Prospects of implementation of telecommunication technologies are shown.

Using stroboscopic flow imaging to validate large-scale computational fluid dynamics simulations

NASA Astrophysics Data System (ADS)

Laurence, Ted A.; Ly, Sonny; Fong, Erika; Shusteff, Maxim; Randles, Amanda; Gounley, John; Draeger, Erik

2017-02-01

The utility and accuracy of computational modeling often requires direct validation against experimental measurements. The work presented here is motivated by taking a combined experimental and computational approach to determine the ability of large-scale computational fluid dynamics (CFD) simulations to understand and predict the dynamics of circulating tumor cells in clinically relevant environments. We use stroboscopic light sheet fluorescence imaging to track the paths and measure the velocities of fluorescent microspheres throughout a human aorta model. Performed over complex physiologicallyrealistic 3D geometries, large data sets are acquired with microscopic resolution over macroscopic distances.

SCDFT Study of High Tc Nitride Superconductors

NASA Astrophysics Data System (ADS)

Arita, R.

Based on the density functional theory for superconductors (SCDFT), we study the pairing mechanism of the layered nitride superconductors, β-LixMNCl (M=Zr, Hf). Recently, it has been shown that SCDFT reproduces experimental superconducting transition temperatures (Tc) of conventional superconductors very accurately. Here we use SCDFT as a "litmus paper" to determine whether the system is a conventional or unconventional superconductor. We show that Tc estimated by SCDFT is less than half of the experimental Tc and its doping dependence is opposite to that observed in the experiments. The present result suggests that β- LixMNCl is not a Migdal-Eliashberg type superconductor.

Application of a Laplace transform pair model for high-energy x-ray spectral reconstruction.

PubMed

Archer, B R; Almond, P R; Wagner, L K

1985-01-01

A Laplace transform pair model, previously shown to accurately reconstruct x-ray spectra at diagnostic energies, has been applied to megavoltage energy beams. The inverse Laplace transforms of 2-, 6-, and 25-MV attenuation curves were evaluated to determine the energy spectra of these beams. The 2-MV data indicate that the model can reliably reconstruct spectra in the low megavoltage range. Experimental limitations in acquiring the 6-MV transmission data demonstrate the sensitivity of the model to systematic experimental error. The 25-MV data result in a physically realistic approximation of the present spectrum.

Development of serratiopeptidase and metronidazole based alginate microspheres for wound healing.

PubMed

Rath, G; Johal, E S; Goyal, Amit K

2011-02-01

The objective of this study was to establish an effective therapy system for wound management. The present work describes preparation of metronidazole/serratiopeptidase loaded alginate microspheres by emulsification method. In vitro characterizations like particle size analysis, % yield, % encapsulation, and in vitro release were carried out. Wound healing assessment was determined by physical, histological, and biochemical methods. Wound healing performance of experimental formulations was compared with marketed product in rabbits. Result obtained for alginate microspheres showed good loading efficiency with spherical in shape. Experimentation suggests wound healing is improved by using serratiopeptidase and metronidazole in full thickness wounds in rabbits.

A Method for Determining the Rate of Heat Transfer from a Wing or Streamline Body

NASA Technical Reports Server (NTRS)

Frick, Charles W; Mccullough, George B

1945-01-01

A method for calculating the rate of heat transfer from the surface of an airfoil or streamline body is presented. A comparison with the results of an experimental investigation indicates that the accuracy of the method is good. This method may be used to calculate the heat supply necessary for heat de-icing or in ascertaining the heat loss from the fuselage of an aircraft operating at great altitude. To illustrate the method, the total rate of heat transfer from an airfoil is calculated and compared with the experimental results.

An experiment for determining the Euler load by direct computation

NASA Technical Reports Server (NTRS)

Thurston, Gaylen A.; Stein, Peter A.

1986-01-01

A direct algorithm is presented for computing the Euler load of a column from experimental data. The method is based on exact inextensional theory for imperfect columns, which predicts two distinct deflected shapes at loads near the Euler load. The bending stiffness of the column appears in the expression for the Euler load along with the column length, therefore the experimental data allows a direct computation of bending stiffness. Experiments on graphite-epoxy columns of rectangular cross-section are reported in the paper. The bending stiffness of each composite column computed from experiment is compared with predictions from laminated plate theory.

Quantum state estimation when qubits are lost: a no-data-left-behind approach

DOE PAGES

Williams, Brian P.; Lougovski, Pavel

2017-04-06

We present an approach to Bayesian mean estimation of quantum states using hyperspherical parametrization and an experiment-specific likelihood which allows utilization of all available data, even when qubits are lost. With this method, we report the first closed-form Bayesian mean and maximum likelihood estimates for the ideal single qubit. Due to computational constraints, we utilize numerical sampling to determine the Bayesian mean estimate for a photonic two-qubit experiment in which our novel analysis reduces burdens associated with experimental asymmetries and inefficiencies. This method can be applied to quantum states of any dimension and experimental complexity.

Stresses in pin-loaded orthotropic plates using photoelasticity

NASA Technical Reports Server (NTRS)

Hyer, M. W.; Liu, D.

1984-01-01

The stresses in transparent glass-epoxy plates loaded by a steel pin through a hole were determined by photoelasticity. The stresses around the hole edge, across the net section, along the shear out line, and on the centerline below the hole for quasiisotropic, unidirectional, and angle ply plates are outlined. Stresses in an isotropic comparison specimen are also presented. Stress concentration factors for several locations around the plates are tabulated. The experimental apparatus and the experimental technique are discussed. The isochromatic and isoclinic fringe patterns for the four plates are shown. A description of the necessary photoelastic theory is appended.

Nuclear clustering and the electron screening puzzle

NASA Astrophysics Data System (ADS)

Bertulani, C. A.; Spitaleri, C.

2018-01-01

Electron screening changes appreciably the magnitude of astrophysical nuclear reactions within stars. This effect is also observed in laboratory experiments on Earth, where atomic electrons are present in the nuclear targets. Theoretical models were developed over the past 30 years and experimental measurements have been carried out to study electron screening in thermonuclear reactions. None of the theoretical models were able to explain the high values of the experimentally determined screening potentials. We explore the possibility that the "electron screening puzzle" is due to nuclear clusterization and polarization e_ects in the fusion reactions. We will discuss the supporting arguments for this scenario.

Experimental performance of a high-area-ratio rocket nozzle at high combustion chamber pressure

NASA Technical Reports Server (NTRS)

Jankovsky, Robert S.; Kazaroff, John M.; Pavli, Albert J.

1996-01-01

An experimental investigation was conducted to determine the thrust coefficient of a high-area-ratio rocket nozzle at combustion chamber pressures of 12.4 to 16.5 MPa (1800 to 2400 psia). A nozzle with a modified Rao contour and an expansion area ratio of 1025:1 was tested with hydrogen and oxygen at altitude conditions. The same nozzle, truncated to an area ratio of 440:1, was also tested. Values of thrust coefficient are presented along with characteristic exhaust velocity efficiencies, nozzle wall temperatures, and overall thruster specific impulse.

Precise measurement of the half-life of the Fermi {beta} decay of {sup 26}Al{sup m}

DOE Office of Scientific and Technical Information (OSTI.GOV)

Scott, Rebecca J.; Thompson, Maxwell N.; Rassool, Roger P.

2011-08-15

State-of-the-art signal digitization and analysis techniques have been used to measure the half-life of the Fermi {beta} decay of {sup 26}Al{sup m}. The half-life was determined to be 6347.8 {+-} 2.5 ms. This new datum contributes to the experimental testing of the conserved-vector-current hypothesis and the required unitarity of the Cabibbo-Kobayashi-Maskawa matrix: two essential components of the standard model. Detailed discussion of the experimental techniques and data analysis and a thorough investigation of the statistical and systematic uncertainties are presented.

Theory of the Trojan-Horse Method - From the Original Idea to Actual Applications

NASA Astrophysics Data System (ADS)

Typel, Stefan

2018-01-01

The origin and the main features of the Trojan-horse (TH) method are delineated starting with the original idea of Gerhard Baur. Basic theoretical considerations, general experimental conditions and possible problems are discussed. Significant steps in experimental studies towards the implementation of the TH method and the development of the theoretical description are presented. This lead to the successful application of the TH approach by Claudio Spitaleri and his group to determine low-energy cross section that are relevant for astrophysics. An outlook with possible developments in the future are given.

The behavior of a compressible turbulent boundary layer in a shock-wave-induced adverse pressure gradient. Ph.D. Thesis - Washington Univ., Seattle, Aug. 1972

NASA Technical Reports Server (NTRS)

Rose, W. C.

1973-01-01

The results of an experimental investigation of the mean- and fluctuating-flow properties of a compressible turbulent boundary layer in a shock-wave-induced adverse pressure gradient are presented. The turbulent boundary layer developed on the wall of an axially symmetric nozzle and test section whose nominal free-stream Mach number and boundary-layer thickness Reynolds number were 4 and 100,000, respectively. The adverse pressure gradient was induced by an externally generated conical shock wave. Mean and time-averaged fluctuating-flow data, including the complete experimental Reynolds stress tensor and experimental turbulent mass- and heat-transfer rates are presented for the boundary layer and external flow, upstream, within and downstream of the pressure gradient. The mean-flow data include distributions of total temperature throughout the region of interest. The turbulent mixing properties of the flow were determined experimentally with a hot-wire anemometer. The calibration of the wires and the interpretation of the data are discussed. From the results of the investigation, it is concluded that the shock-wave - boundary-layer interaction significantly alters the turbulent mixing characteristics of the boundary layer.

Prediction of Shrinkage Porosity Defect in Sand Casting Process of LM25

NASA Astrophysics Data System (ADS)

Rathod, Hardik; Dhulia, Jay K.; Maniar, Nirav P.

2017-08-01

In the present worldwide and aggressive environment, foundry commercial enterprises need to perform productively with least number of rejections and create casting parts in shortest lead time. It has become extremely difficult for foundry industries to meet demands of defects free casting and meet strict delivery schedules. The process of casting solidification is complex in nature. Prediction of shrinkage defect in metal casting is one of the critical concern in foundries and is one of the potential research areas in casting. Due to increasing pressure to improve quality and to reduce cost, it is very essential to upgrade the level of current methodology used in foundries. In the present research work, prediction methodology of shrinkage porosity defect in sand casting process of LM25 using experimentation and ANSYS is proposed. The objectives successfully achieved are prediction of shrinkage porosity distribution in Al-Si casting and determining effectiveness of investigated function for predicting shrinkage porosity by correlating results of simulating studies to those obtained experimentally. The real-time application of the research reflects from the fact that experimentation is performed on 9 different Y junctions at foundry industry and practical data obtained from experimentation are used for simulation.

Metainference: A Bayesian inference method for heterogeneous systems

PubMed Central

Bonomi, Massimiliano; Camilloni, Carlo; Cavalli, Andrea; Vendruscolo, Michele

2016-01-01

Modeling a complex system is almost invariably a challenging task. The incorporation of experimental observations can be used to improve the quality of a model and thus to obtain better predictions about the behavior of the corresponding system. This approach, however, is affected by a variety of different errors, especially when a system simultaneously populates an ensemble of different states and experimental data are measured as averages over such states. To address this problem, we present a Bayesian inference method, called “metainference,” that is able to deal with errors in experimental measurements and with experimental measurements averaged over multiple states. To achieve this goal, metainference models a finite sample of the distribution of models using a replica approach, in the spirit of the replica-averaging modeling based on the maximum entropy principle. To illustrate the method, we present its application to a heterogeneous model system and to the determination of an ensemble of structures corresponding to the thermal fluctuations of a protein molecule. Metainference thus provides an approach to modeling complex systems with heterogeneous components and interconverting between different states by taking into account all possible sources of errors. PMID:26844300

Experimental Investigation of a High Pressure Ratio Aspirated Fan Stage

NASA Technical Reports Server (NTRS)

Merchant, Ali; Kerrebrock, Jack L.; Adamczyk, John J.; Braunscheidel, Edward

2004-01-01

The experimental investigation of an aspirated fan stage designed to achieve a pressure ratio of 3.4:1 at 1500 ft/sec is presented in this paper. The low-energy viscous flow is aspirated from diffusion-limiting locations on the blades and flowpath surfaces of the stage, enabling a very high pressure ratio to be achieved in a single stage. The fan stage performance was mapped at various operating speeds from choke to stall in a compressor facility at fully simulated engine conditions. The experimentally determined stage performance, in terms of pressure ratio and corresponding inlet mass flow rate, was found to be in good agreement with the three-dimensional viscous computational prediction, and in turn close to the design intent. Stage pressure ratios exceeding 3:1 were achieved at design speed, with an aspiration flow fraction of 3.5 percent of the stage inlet mass flow. The experimental performance of the stage at various operating conditions, including detailed flowfield measurements, are presented and discussed in the context of the computational analyses. The sensitivity of the stage performance and operability to reduced aspiration flow rates at design and off design conditions are also discussed.

Inter-spin distance determination using L-band (1-2 GHz) non-adiabatic rapid sweep electron paramagnetic resonance (NARS EPR)

PubMed Central

Kittell, Aaron W.; Hustedt, Eric J.; Hyde, James S.

2014-01-01

Site-directed spin-labeling electron paramagnetic resonance (SDSL EPR) provides insight into the local structure and motion of a spin probe strategically attached to a molecule. When a second spin is introduced to the system, macromolecular information can be obtained through measurement of inter-spin distances either by continuous wave (CW) or pulsed electron double resonance (ELDOR) techniques. If both methodologies are considered, inter-spin distances of 8 to 80 Å can be experimentally determined. However, there exists a region at the upper limit of the conventional X-band (9.5 GHz) CW technique and the lower limit of the four-pulse double electron-electron resonance (DEER) experiment where neither method is particularly reliable. The work presented here utilizes L-band (1.9 GHz) in combination with non-adiabatic rapid sweep (NARS) EPR to address this opportunity by increasing the upper limit of the CW technique. Because L-band linewidths are three to seven times narrower than those at X-band, dipolar broadenings that are small relative to the X-band inhomogeneous linewidth become observable, but the signal loss due to the frequency dependence of the Boltzmann factor, has made L-band especially challenging. NARS has been shown to increase sensitivity by a factor of five, and overcomes much of this loss, making L-band distance determination more feasible [1]. Two different systems are presented and distances of 18–30 Å have been experimentally determined at physiologically relevant temperatures. Measurements are in excellent agreement with a helical model and values determined by DEER. PMID:22750251

Experimental constraints on the damp peridotite solidus and oceanic mantle potential temperature

NASA Astrophysics Data System (ADS)

Sarafian, Emily; Gaetani, Glenn A.; Hauri, Erik H.; Sarafian, Adam R.

2017-03-01

Decompression of hot mantle rock upwelling beneath oceanic spreading centers causes it to exceed the melting point (solidus), producing magmas that ascend to form basaltic crust ~6 to 7 kilometers thick. The oceanic upper mantle contains ~50 to 200 micrograms per gram of water (H2O) dissolved in nominally anhydrous minerals, which—relative to its low concentration—has a disproportionate effect on the solidus that has not been quantified experimentally. Here, we present results from an experimental determination of the peridotite solidus containing known amounts of dissolved hydrogen. Our data reveal that the H2O-undersaturated peridotite solidus is hotter than previously thought. Reconciling geophysical observations of the melting regime beneath the East Pacific Rise with our experimental results requires that existing estimates for the oceanic upper mantle potential temperature be adjusted upward by about 60°C.

In situ impulse test: an experimental and analytical evaluation of data interpretation procedures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Not Available

1975-08-01

Special experimental field testing and analytical studies were undertaken at Fort Lawton in Seattle, Washington, to study ''close-in'' wave propagation and evaluate data interpretation procedures for a new in situ impulse test. This test was developed to determine the shear wave velocity and dynamic modulus of soils underlying potential nuclear power plant sites. The test is different from conventional geophysical testing in that the velocity variation with strain is determined for each test. In general, strains between 10/sup -1/ and 10/sup -3/ percent are achieved. The experimental field work consisted of performing special tests in a large test sand fillmore » to obtain detailed ''close-in'' data. Six recording transducers were placed at various points on the energy source, while approximately 37 different transducers were installed within the soil fill, all within 7 feet of the energy source. Velocity measurements were then taken simultaneously under controlled test conditions to study shear wave propagation phenomenology and help evaluate data interpretation procedures. Typical test data are presented along with detailed descriptions of the results.« less

Probing Hotspot Conditions in Spherically Shock Compressed Matter

NASA Astrophysics Data System (ADS)

Bachmann, Benjamin; Nilsen, J.; Kritcher, A. L.; Swift, D.; Rygg, J. R.; Collins, G. W.; Divol, L.; Falcone, R. W.; Gaffney, J.; Glenzer, S. H.; Hatarik, R.; Hawreliak, J.; Khan, S.; Kraus, D.; Landen, O. L.; Masters, N.; Nagel, S. R.; Pardini, T.; Zimmerman, G.; Doeppner, T.

2015-11-01

We present results of an approach to experimentally determine the conditions in the center of a CD2 sphere that has been compressed to petapascal pressures by spherically converging shocks. By measuring the hotspot size using penumbral imaging, hotspot temperature using two-color spectroscopy, the neutron yield from DD nuclear reactions and the x-ray burn width, we infer average hotspot densities of 43 g/cm3 at 1.6 keV temperature. These conditions correspond to pressures of 4.4 petapascal (44 Gbar) in an ideal gas and 3.5 petapascal from independently performed rad.-hydro. simulations. The experimentally determined neutron yield, temperature and density constrain the EOS in a regime that exceeds previously reported pressures obtained in carbon EOS measurements by three orders of magnitude. The results show a path for constraining the EOS of matter at conditions that have been inaccessible with state-of-the-art experimental EOS techniques. This work was performed under the auspices of the U.S. DOE by LLNL under Contract DE-AC52-07NA27344 and LDRD Grant 13-ERD-073

Development of experimental techniques for the characterization of ultrashort photon pulses of extreme ultraviolet free-electron lasers

NASA Astrophysics Data System (ADS)

Düsterer, S.; Rehders, M.; Al-Shemmary, A.; Behrens, C.; Brenner, G.; Brovko, O.; DellAngela, M.; Drescher, M.; Faatz, B.; Feldhaus, J.; Frühling, U.; Gerasimova, N.; Gerken, N.; Gerth, C.; Golz, T.; Grebentsov, A.; Hass, E.; Honkavaara, K.; Kocharian, V.; Kurka, M.; Limberg, Th.; Mitzner, R.; Moshammer, R.; Plönjes, E.; Richter, M.; Rönsch-Schulenburg, J.; Rudenko, A.; Schlarb, H.; Schmidt, B.; Senftleben, A.; Schneidmiller, E. A.; Siemer, B.; Sorgenfrei, F.; Sorokin, A. A.; Stojanovic, N.; Tiedtke, K.; Treusch, R.; Vogt, M.; Wieland, M.; Wurth, W.; Wesch, S.; Yan, M.; Yurkov, M. V.; Zacharias, H.; Schreiber, S.

2014-12-01

One of the most challenging tasks for extreme ultraviolet, soft and hard x-ray free-electron laser photon diagnostics is the precise determination of the photon pulse duration, which is typically in the sub 100 fs range. Nine different methods, able to determine such ultrashort photon pulse durations, were compared experimentally at FLASH, the self-amplified spontaneous emission free-electron laser at DESY in Hamburg, in order to identify advantages and disadvantages of different methods. Radiation pulses at a wavelength of 13.5 and 24.0 nm together with the corresponding electron bunch duration were measured by indirect methods like analyzing spectral correlations, statistical fluctuations, and energy modulations of the electron bunch and also by direct methods like autocorrelation techniques, terahertz streaking, or reflectivity changes of solid state samples. In this paper, we present a comprehensive overview of the various techniques and a comparison of the individual experimental results. The information gained is of utmost importance for the future development of reliable pulse duration monitors indispensable for successful experiments with ultrashort extreme ultraviolet pulses.

Investigation of Dynamic Properties of Water-Saturated Sand by the Results of the Inverse Experiment Technique

NASA Astrophysics Data System (ADS)

Bragov, A. M.; Balandin, Vl. V.; Kotov, V. L.; Balandin, Vl. Vl.

2018-04-01

We present new experimental results on the investigation of the dynamic properties of sand soil on the basis of the inverse experiment technique using a measuring rod with a flat front-end face. A limited applicability has been shown of the method using the procedure for correcting the shape of the deformation pulse due to dispersion during its propagation in the measuring rod. Estimates of the pulse maximum have been obtained and the results of comparison of numerical calculations with experimental data are given. The sufficient accuracy in determining the drag force during the quasi-stationary stage of penetration has been established. The parameters of dynamic compressibility and resistance to shear of water-saturated sand have been determined in the course of the experimental-theoretical analysis of the maximum values of the drag force and its values at the quasi-stationary stage of penetration. It has been shown that with almost complete water saturation of sand its shear properties are reduced but remain significant in the practically important range of penetration rates.

Experimental design approach to the process parameter optimization for laser welding of martensitic stainless steels in a constrained overlap configuration

NASA Astrophysics Data System (ADS)

Khan, M. M. A.; Romoli, L.; Fiaschi, M.; Dini, G.; Sarri, F.

2011-02-01

This paper presents an experimental design approach to process parameter optimization for the laser welding of martensitic AISI 416 and AISI 440FSe stainless steels in a constrained overlap configuration in which outer shell was 0.55 mm thick. To determine the optimal laser-welding parameters, a set of mathematical models were developed relating welding parameters to each of the weld characteristics. These were validated both statistically and experimentally. The quality criteria set for the weld to determine optimal parameters were the minimization of weld width and the maximization of weld penetration depth, resistance length and shearing force. Laser power and welding speed in the range 855-930 W and 4.50-4.65 m/min, respectively, with a fiber diameter of 300 μm were identified as the optimal set of process parameters. However, the laser power and welding speed can be reduced to 800-840 W and increased to 4.75-5.37 m/min, respectively, to obtain stronger and better welds.

Studies of cosmogenic in-situ 14CO and 14CO2 produced in terrestrial and extraterrestrial samples: experimental procedures and applications

NASA Astrophysics Data System (ADS)

Lal, D.; Jull, A. J. T.

1994-06-01

We have developed an experimental procedure for quantitative extraction of cosmogenic in-situ 14C produced in terrestrial and extraterrestrial samples, in the two chemical forms 14CO and 14CO2 in which it is found to be present in these samples. The technique is based on wet digestion of the sample in vacuo with hydrofluoric acid at 60-80°C in a Kel-F® vessel. Kel-F is a homo-polymer (chlortrifluorethylene). The procedures and the digestion vessel sizes used allow convenient extraction of 14C activity from samples of 50 mg to 50 g weight. Procedure blanks were reduced considerably by the experience gained with the system, and can be reduced further. We determined that most of the in-situ 14C activity was present in the CO phase (> 60%) in the case of both terrestrial quartz and in bulk samples of meteorites, analogous to the case of in-situ production of 14C in ice. Some results of measurements of 14C activities in meteorites and in terrestrial samples are presented. The latter include several samples which have been studied earlier for in-situ 10Be (and 26Al) concentrations, and allow us to determine relative 14C and 10Be production rates in quartz.

Experimental Determination of Unsteady Forces on Contrarotating Propellers for Application to Torpedoes

DTIC Science & Technology

1981-12-01

Experimental determination of Unsteady Forces on Contrarotating Propellers in Uniform Flow ," David Taylor Naval Ship R&D Center, Ship Performance...were planned to determine the unsteady forces on contrarotating propellers in a 4-cycle wake, there were also experiments made in uniform flow to check...Subtitle) S. TYPE OF REPORT G PERIOD COVERED Experimental Determination of Unsteady Forces on

Reassessment of Atomic Mobilities in fcc Cu-Ag-Sn System Aiming at Establishment of an Atomic Mobility Database in Sn-Ag-Cu-In-Sb-Bi-Pb Solder Alloys

NASA Astrophysics Data System (ADS)

Xu, Huixia; Zhang, Lijun; Cheng, Kaiming; Chen, Weimin; Du, Yong

2017-04-01

To establish an accurate atomic mobility database in solder alloys, a reassessment of atomic mobilities in the fcc (face centered cubic) Cu-Ag-Sn system was performed as reported in the present work. The work entailed initial preparation of three fcc Cu-Sn diffusion couples, which were used to determine the composition-dependent interdiffusivities at 873 K, 923 K, and 973 K, to validate the literature data and provide new experimental data at low temperatures. Then, atomic mobilities in three boundary binaries, fcc Cu-Sn, fcc Ag-Sn, and fcc Cu-Ag, were updated based on the data for various experimental diffusivities obtained from the literature and the present work, together with the available thermodynamic database for solder alloys. Finally, based on the large number of interdiffusivities recently measured from the present authors, atomic mobilities in the fcc Cu-Ag-Sn ternary system were carefully evaluated. A comprehensive comparison between various calculated/model-predicted diffusion properties and the experimental data was used to validate the reliability of the obtained atomic mobilities in ternary fcc Cu-Ag-Sn alloys.

Stiffness analysis of glued connection of the timber-concrete structure

NASA Astrophysics Data System (ADS)

Daňková, Jana; Mec, Pavel; Majstríková, Tereza

2016-01-01

This paper presents results of experimental and mathematical analysis of stiffness characteristics of a composite timber-concrete structure. The composite timberconcrete structure presented herein is non-typical compared to similar types of building structures. The interaction between the timber and concrete part of the composite cross-section is not based on metal connecting elements, but it is ensured by a glued-in perforated mesh made of plywood. The paper presents results of experimental and mathematical analysis for material alternatives of the solution of the glued joint. The slip modulus values were determined experimentally. Data obtained from the experiment evaluated by means of regression analysis. Test results were also used as input data for the compilation of a 3D model of a composite structure by means of the 3D finite element model. On the basis of result evaluation, it can be stated that the stress-deformation behaviour at shear loading of this specific timber-concrete composite structure can be affected by the type of glue used. Parameters of the 3D model of both alternative of the structure represent well the behaviour of the composite structure and the model can be used for predicting design parameters of a building structure.

The Noble-Abel Stiffened-Gas equation of state

NASA Astrophysics Data System (ADS)

Le Métayer, Olivier; Saurel, Richard

2016-04-01

Hyperbolic two-phase flow models have shown excellent ability for the resolution of a wide range of applications ranging from interfacial flows to fluid mixtures with several velocities. These models account for waves propagation (acoustic and convective) and consist in hyperbolic systems of partial differential equations. In this context, each phase is compressible and needs an appropriate convex equation of state (EOS). The EOS must be simple enough for intensive computations as well as boundary conditions treatment. It must also be accurate, this being challenging with respect to simplicity. In the present approach, each fluid is governed by a novel EOS named "Noble Abel stiffened gas," this formulation being a significant improvement of the popular "Stiffened Gas (SG)" EOS. It is a combination of the so-called "Noble-Abel" and "stiffened gas" equations of state that adds repulsive effects to the SG formulation. The determination of the various thermodynamic functions and associated coefficients is the aim of this article. We first use thermodynamic considerations to determine the different state functions such as the specific internal energy, enthalpy, and entropy. Then we propose to determine the associated coefficients for a liquid in the presence of its vapor. The EOS parameters are determined from experimental saturation curves. Some examples of liquid-vapor fluids are examined and associated parameters are computed with the help of the present method. Comparisons between analytical and experimental saturation curves show very good agreement for wide ranges of temperature for both liquid and vapor.

An experimental computational system for materials thermal properties determination and its application for spacecraft structures testing

NASA Astrophysics Data System (ADS)

Alifanov, O. M.; Budnik, S. A.; Mikhaylov, V. V.; Nenarokomov, A. V.; Titov, D. M.; Yudin, V. M.

2007-06-01

An experimental-computational system, which is developed at the Thermal Laboratory, Department Space Systems Engineering, Moscow Aviation Institute (MAI), is presented for investigating the thermal properties of composite materials by methods of inverse heat transfer problems. The system is aimed at investigating the materials in conditions of unsteady contact and/or radiation heating over a wide range of temperature changes and heating rates in a vacuum, air and inert gas medium. The paper considers the hardware components of the system, including the experiment facility and the automated system of control, measurement, data acquisition and processing, as well as the aspects of methodical support of thermal tests. In the next part the conception and realization of a computer code for experimental data processing to estimate the thermal properties of thermal-insulating materials is given. The most promising direction in further development of methods for non-destructive composite materials using the procedure of solving inverse problems is the simultaneous determination of a combination of their thermal and radiation properties. The general method of iterative regularization is concerned with application to the estimation of materials properties (e.g., example: thermal conductivity λ(T) and heat capacity C(T)). Such problems are of great practical importance in the study of material properties used as non-destructive surface shield in objects of space engineering, power engineering, etc. In the third part the results of practical implementation of hardware and software presented in the previous two parts are given for the estimating of thermal properties of thermal-insulating materials. The main purpose of this study is to confirm the feasibility and effectiveness of the methods developed and hardware equipment for determining thermal properties of particular modern high porous materials.

Statistical baseline assessment in cardiotocography.

PubMed

Agostinelli, Angela; Braccili, Eleonora; Marchegiani, Enrico; Rosati, Riccardo; Sbrollini, Agnese; Burattini, Luca; Morettini, Micaela; Di Nardo, Francesco; Fioretti, Sandro; Burattini, Laura

2017-07-01

Cardiotocography (CTG) is the most common non-invasive diagnostic technique to evaluate fetal well-being. It consists in the recording of fetal heart rate (FHR; bpm) and maternal uterine contractions. Among the main parameters characterizing FHR, baseline (BL) is fundamental to determine fetal hypoxia and distress. In computerized applications, BL is typically computed as mean FHR±ΔFHR, with ΔFHR=8 bpm or ΔFHR=10 bpm, both values being experimentally fixed. In this context, the present work aims: to propose a statistical procedure for ΔFHR assessment; to quantitatively determine ΔFHR value by applying such procedure to clinical data; and to compare the statistically-determined ΔFHR value against the experimentally-determined ΔFHR values. To these aims, the 552 recordings of the "CTU-UHB intrapartum CTG database" from Physionet were submitted to an automatic procedure, which consisted in a FHR preprocessing phase and a statistical BL assessment. During preprocessing, FHR time series were divided into 20-min sliding windows, in which missing data were removed by linear interpolation. Only windows with a correction rate lower than 10% were further processed for BL assessment, according to which ΔFHR was computed as FHR standard deviation. Total number of accepted windows was 1192 (38.5%) over 383 recordings (69.4%) with at least an accepted window. Statistically-determined ΔFHR value was 9.7 bpm. Such value was statistically different from 8 bpm (P<;10 -19 ) but not from 10 bpm (P=0.16). Thus, ΔFHR=10 bpm is preferable over 8 bpm because both experimentally and statistically validated.

Physical–chemical determinants of coil conformations in globular proteins

PubMed Central

Perskie, Lauren L; Rose, George D

2010-01-01

We present a method with the potential to generate a library of coil segments from first principles. Proteins are built from α-helices and/or β-strands interconnected by these coil segments. Here, we investigate the conformational determinants of short coil segments, with particular emphasis on chain turns. Toward this goal, we extracted a comprehensive set of two-, three-, and four-residue turns from X-ray–elucidated proteins and classified them by conformation. A remarkably small number of unique conformers account for most of this experimentally determined set, whereas remaining members span a large number of rare conformers, many occurring only once in the entire protein database. Factors determining conformation were identified via Metropolis Monte Carlo simulations devised to test the effectiveness of various energy terms. Simulated structures were validated by comparison to experimental counterparts. After filtering rare conformers, we found that 98% of the remaining experimentally determined turn population could be reproduced by applying a hydrogen bond energy term to an exhaustively generated ensemble of clash-free conformers in which no backbone polar group lacks a hydrogen-bond partner. Further, at least 90% of longer coil segments, ranging from 5- to 20 residues, were found to be structural composites of these shorter primitives. These results are pertinent to protein structure prediction, where approaches can be divided into either empirical or ab initio methods. Empirical methods use database-derived information; ab initio methods rely on physical–chemical principles exclusively. Replacing the database-derived coil library with one generated from first principles would transform any empirically based method into its corresponding ab initio homologue. PMID:20512968

Effect of Drama Instruction Method on Students' Turkish Verbal Skills and Speech Anxiety

ERIC Educational Resources Information Center

Kardas, Mehmet Nuri; Koç, Rasit

2017-01-01

The objective of the present study is to determine the effect of the "drama" method on students' Turkish verbal skills and speech anxiety. Pretest-posttest experimental model with control group was utilized in the study. In the analysis of data obtained by Turkish Rhetorical Skills Scale (TRSS) and Speech Anxiety Scale (SAS), t-test…

Information and Communication Technologies (ICT) and Their Relation to Academic Results Indicators in State Public Universities in Mexico

ERIC Educational Resources Information Center

Arcos-Vega, José L.; Ramiro Marentes, Fabiola; Algravez Uranga, Juan J.

2017-01-01

We present an analysis regarding Information and Communication Technologies (ICT) and their relation with indicators of academic results in bachelor's degree programs offered in state public universities in Mexico. This work is non experimental, cross-sectional, and correlational. The goal is to determine significant relations between variables:…

Classical and Quantum-Mechanical State Reconstruction

ERIC Educational Resources Information Center

Khanna, F. C.; Mello, P. A.; Revzen, M.

2012-01-01

The aim of this paper is to present the subject of state reconstruction in classical and in quantum physics, a subject that deals with the experimentally acquired information that allows the determination of the physical state of a system. Our first purpose is to explain a method for retrieving a classical state in phase space, similar to that…

Metering Characteristics of Carburetors

NASA Technical Reports Server (NTRS)

Tice, Percival S; Dickinson, H C

1919-01-01

Report presents the results of an extensive experimental investigation of the performance of different types of carburetors as effecting the maintenance under all conditions of correct ratio between the weights of fuel and air. It also gives a description of the Bureau of Standards carburetor test plant, test equipment and measuring instruments used to determine the metering characteristics of carburetors.

Where and when to measure forest fire danger

Treesearch

G. Lloyd. Hayes

1944-01-01

This article presents the results of a study to determine the place, time, and number of measurements that should be made to obtain dependable ratings of "average-bad" fire conditions without an excessive number of stations or observations. The author concludes that under the conditions prevailing in the Priest River Experimental Forest in northern Idaho a...

Determination of the Heat and Mass Transfer Efficiency at the Contact Stage of a Jet-Film Facility

NASA Astrophysics Data System (ADS)

Dmitrieva, O. S.; Madyshev, I. N.; Dmitriev, A. V.

2017-05-01

A contact jet-film facility has been developed for increasing the efficiency of operation of industrial cooling towers. The results of experimental and analytical investigation of the operation of this facility, its hydraulic resistance, and of the heat and mass transfer efficiency of its contact stage are presented.

Experimental evaluation of the effect of inlet distortion on compressor blade vibrations

NASA Technical Reports Server (NTRS)

Lubomski, J. F.

1979-01-01

Compressor rotor strain gage data from an engine test conducted with an inlet screen distortion were reduced and analyzed. These data are compared to data obtained from the same engine without inlet pressure distortion to determine the net effect of the distortion on the vibratory response of the compressor blades. The results obtained are presented.

Assessment of 3D Models Used in Contours Studies

ERIC Educational Resources Information Center

Alvarez, F. J. Ayala; Parra, E. B. Blazquez; Tubio, F. Montes

2015-01-01

This paper presents an experimental research focusing on the view of first year students. The aim is to check the quality of implementing 3D models integrated in the curriculum. We search to determine students' preference between the various means facilitated in order to understand the given subject. Students have been respondents to prove the…

Acoustic performance of inlet multiple-pure-tone suppressors installed on NASA quiet engine C

NASA Technical Reports Server (NTRS)

Bloomer, H. E.; Schaefer, J. W.; Rice, E. J.; Feiler, C. E.

1977-01-01

The length of multiple-pure-tone (MPT) treatment required to reasonably suppress the MPT's produced by a supersonic tip speed fan was defined. Other suppression, broadband, and blade passing frequency, which might be accomplished were also determined. The experimental results are presented in terms of both far-field and duct acoustic data.

Correspondence between Preference Assessment Outcomes and Stimulus Reinforcer Value for Social Interactions

ERIC Educational Resources Information Center

Davis, Tonya N.; Hodges, Abby; Weston, Regan; Hogan, Emily; Padilla-Mainor, Kristen

2017-01-01

Preferred forms of social interaction were identified using a paired-stimulus format in which two 3-5 s videos of the experimenter providing the social interaction to the participant were presented. Reinforcer efficacy of the high-, medium-, and low-preferred interactions was evaluated using a progressive-ratio schedule to determine the amount of…

Burnout in the horizontal tubes of a furnace waterwall panel

NASA Astrophysics Data System (ADS)

Kamenetskii, B. Ya.

2009-08-01

An experimental study of heat transfer that occurs in tubes nonuniformly heated over the perimeter at low velocities of subcooled water flowing in them is presented. Experiments with unsteady supply of heat made it possible to determine heat fluxes under burnout conditions. Unusually low values of critical heat fluxes were obtained under such conditions.

PLANE STRAIN FRACTURE TOUGHNESS DATA FOR HANDBOOK PRESENTATION

DTIC Science & Technology

An experimental program was conducted to determine the plane strain fracture toughness (K sub IC) of the following classes of: (1) AISI Alloy Steels...4340, 4140 ); (2) 5Cr-Mo-V Steels; (3) Precipitation-Hardening Stainless Steels (17-7 PH, PH 15-7 Mo, 17-4, AM355); (4) Titanium Alloy, Ti-6Al-4V. The

Can a Multimedia Tool Help Students' Learning Performance in Complex Biology Subjects?

ERIC Educational Resources Information Center

Koseoglu, Pinar; Efendioglu, Akin

2015-01-01

The aim of the present study was to determine the effects of multimedia-based biology teaching (Mbio) and teacher-centered biology (TCbio) instruction approaches on learners' biology achievements, as well as their views towards learning approaches. During the research process, an experimental design with two groups, TCbio (n = 22) and Mbio (n =…

Acoustic-Structure Interaction in Rocket Engines: Validation Testing

NASA Technical Reports Server (NTRS)

Davis, R. Benjamin; Joji, Scott S.; Parks, Russel A.; Brown, Andrew M.

2009-01-01

While analyzing a rocket engine component, it is often necessary to account for any effects that adjacent fluids (e.g., liquid fuels or oxidizers) might have on the structural dynamics of the component. To better characterize the fully coupled fluid-structure system responses, an analytical approach that models the system as a coupled expansion of rigid wall acoustic modes and in vacuo structural modes has been proposed. The present work seeks to experimentally validate this approach. To experimentally observe well-coupled system modes, the test article and fluid cavities are designed such that the uncoupled structural frequencies are comparable to the uncoupled acoustic frequencies. The test measures the natural frequencies, mode shapes, and forced response of cylindrical test articles in contact with fluid-filled cylindrical and/or annular cavities. The test article is excited with a stinger and the fluid-loaded response is acquired using a laser-doppler vibrometer. The experimentally determined fluid-loaded natural frequencies are compared directly to the results of the analytical model. Due to the geometric configuration of the test article, the analytical model is found to be valid for natural modes with circumferential wave numbers greater than four. In the case of these modes, the natural frequencies predicted by the analytical model demonstrate excellent agreement with the experimentally determined natural frequencies.

Laser active thermography for non-destructive testing

NASA Astrophysics Data System (ADS)

Semerok, A.; Grisolia, C.; Fomichev, S. V.; Thro, P.-Y.

2013-11-01

Thermography methods have found their applications in different fields of human activity. The non-destructive feature of these methods along with the additional advantage by automated remote control and tests of nuclear installations without personnel attendance in the contaminated zone are of particular interest. Laser active pyrometry and laser lock-in thermography for in situ non-destructive characterization of micrometric layers on graphite substrates from European tokamaks were under extensive experimental and theoretical studies in CEA (France). The studies were aimed to obtain layer characterization with cross-checking the layer thermal contact coefficients determined by active laser pyrometry and lock-in thermography. The experimental installation comprised a Nd-YAG pulsed repetition rate laser (1 Hz - 10 kHz repetition rate frequency, homogeneous spot) and a home-made pyrometer system based on two pyrometers for the temperature measurements in 500 - 2600 K range. For both methods, the layer characterization was provided by the best fit of the experimental results and simulations. The layer thermal contact coefficients determined by both methods were quite comparable. Though there was no gain in the measurements accuracy, lock-in measurements have proved their advantage as being much more rapid. The obtained experimental and theoretical results are presented. Some practical applications and possible improvements of the methods are discussed.

High resolution study of strongly interacting ν3(F2)/ν1(A1) bands of MSiH4 (M = 28 , 29 , 30)

NASA Astrophysics Data System (ADS)

Ulenikov, O. N.; Gromova, O. V.; Bekhtereva, E. S.; Raspopova, N. I.; Fomchenko, A. L.; Sydow, C.; Bauerecker, S.

2017-11-01

The high resolution (0.0021-0.0025 cm-1) infrared spectra of SiH4 in natural abundance (92.23 % of 28SiH4, 4.68 % of 29SiH4, and 3.09 % of 30SiH4) were measured in the 2000-2350 cm-1 region with a Bruker IFS 120HR Fourier transform spectrometer. The 2584 transitions with Jmax. = 27 were assigned to the ν3 and ν1 bands of 28SiH4. Rotational, centrifugal distortion, tetrahedral splitting, and resonance interaction parameters for the (0010) and (1000) vibrational states were determined from the weighted fit of experimental line positions. The obtained set of parameters reproduces the initial experimental data with an accuracy close to experimental uncertainties. The results of analogous analyses of the 29SiH4 and 30SiH4 isotopologues (the numbers of assigned transitions are 811 and 986 both with Jmax. = 23) were made with the use of the isotopic substitution theory relations. A further analysis of 379 experimental ro-vibrational lines of the ν3 and ν1 bands of 28SiH4 was performed using the Hartmann-Tran profile to simulate the measured line shape and to determine experimental line intensities. The 4 effective dipole moment parameters were obtained on that basis from the weighted fit, which reproduce the initial experimental intensities of the 379 initial lines (both strong and weak) with the drms = 7.6 % (the 148 strongest lines are reproduced with the drms = 5.0 %). Analogous analyses were made for the two other isotopic species, 29SiH4, and 30SiH4. A detailed line list of transitions in the region of 2000-2350 cm-1 is presented. The half-widths of 100 ro-vibrational lines (Jup.max. = 17) are analyzed from the multi-spectrum fit, and self-pressure broadening coefficients are determined.

Elucidating Proteoform Families from Proteoform Intact-Mass and Lysine-Count Measurements

PubMed Central

2016-01-01

Proteomics is presently dominated by the “bottom-up” strategy, in which proteins are enzymatically digested into peptides for mass spectrometric identification. Although this approach is highly effective at identifying large numbers of proteins present in complex samples, the digestion into peptides renders it impossible to identify the proteoforms from which they were derived. We present here a powerful new strategy for the identification of proteoforms and the elucidation of proteoform families (groups of related proteoforms) from the experimental determination of the accurate proteoform mass and number of lysine residues contained. Accurate proteoform masses are determined by standard LC–MS analysis of undigested protein mixtures in an Orbitrap mass spectrometer, and the lysine count is determined using the NeuCode isotopic tagging method. We demonstrate the approach in analysis of the yeast proteome, revealing 8637 unique proteoforms and 1178 proteoform families. The elucidation of proteoforms and proteoform families afforded here provides an unprecedented new perspective upon proteome complexity and dynamics. PMID:26941048

Thickness determination of polymeric multilayer surface protection systems for concrete by means of pulse thermography

NASA Astrophysics Data System (ADS)

Altenburg, S. J.; Krankenhagen, R.; Bavendiek, F.

2017-02-01

For thickness determination of polymer based surface protection systems for concrete surfaces, so far only destructive measurement techniques are available. Pulse thermography appears to be well suited for non-destructive thickness evaluation in these systems. Here, we present first results of the development of a respective measurement and analysis procedure. Since surface protection systems consist of a number of layers, a model for the calculation of the surface temperature of a multi-layer structure on a semi-infinite (concrete) substrate in pulse thermography setup was developed. It considers semitransparency of the upmost layer and thermal losses at the surface. It also supports the use of an arbitrary temporal shape of the heating pulse to properly describe the measurement conditions for different heat sources. Simulations for one and three layers on the substrate are presented and first results from fitting the model to experimental data for thickness determination and verification of the model are presented.

Microstructure based simulations for prediction of flow curves and selection of process parameters for inter-critical annealing in DP steel

NASA Astrophysics Data System (ADS)

Deepu, M. J.; Farivar, H.; Prahl, U.; Phanikumar, G.

2017-04-01

Dual phase steels are versatile advanced high strength steels that are being used for sheet metal applications in automotive industry. It also has the potential for application in bulk components like gear. The inter-critical annealing in dual phase steels is one of the crucial steps that determine the mechanical properties of the material. Selection of the process parameters for inter-critical annealing, in particular, the inter-critical annealing temperature and time is important as it plays a major role in determining the volume fractions of ferrite and martensite, which in turn determines the mechanical properties. Selection of these process parameters to obtain a particular required mechanical property requires large number of experimental trials. Simulation of microstructure evolution and virtual compression/tensile testing can help in reducing the number of such experimental trials. In the present work, phase field modeling implemented in the commercial software Micress® is used to predict the microstructure evolution during inter-critical annealing. Virtual compression tests are performed on the simulated microstructure using finite element method implemented in the commercial software, to obtain the effective flow curve of the macroscopic material. The flow curves obtained by simulation are experimentally validated with physical simulation in Gleeble® and compared with that obtained using linear rule of mixture. The methodology could be used in determining the inter-critical annealing process parameters required for achieving a particular flow curve.

A parallel algorithm for nonlinear convection-diffusion equations

NASA Technical Reports Server (NTRS)

Scroggs, Jeffrey S.

1990-01-01

A parallel algorithm for the efficient solution of nonlinear time-dependent convection-diffusion equations with small parameter on the diffusion term is presented. The method is based on a physically motivated domain decomposition that is dictated by singular perturbation analysis. The analysis is used to determine regions where certain reduced equations may be solved in place of the full equation. The method is suitable for the solution of problems arising in the simulation of fluid dynamics. Experimental results for a nonlinear equation in two-dimensions are presented.

A precise determination of the HVP contribution to the muon anomalous magnetic moment from lattice QCD

NASA Astrophysics Data System (ADS)

Lehner, Christoph

2018-03-01

In this talk I present the current status of a precise first-principles calculation of the quark connected, quark disconnected, and leading QED and strong isospin-breaking contributions to the leading-order hadronic vacuum polarization by the RBC and UKQCD collaborations. The lattice data is also combined with experimental e+e- scattering data, consistency between the two datasets is checked, and a combined result with smaller error than the lattice data and e+e- scattering data individually is presented.

A Procedure for Measuring Latencies in Brain-Computer Interfaces

PubMed Central

Wilson, J. Adam; Mellinger, Jürgen; Schalk, Gerwin; Williams, Justin

2011-01-01

Brain-computer interface (BCI) systems must process neural signals with consistent timing in order to support adequate system performance. Thus, it is important to have the capability to determine whether a particular BCI configuration (i.e., hardware, software) provides adequate timing performance for a particular experiment. This report presents a method of measuring and quantifying different aspects of system timing in several typical BCI experiments across a range of settings, and presents comprehensive measures of expected overall system latency for each experimental configuration. PMID:20403781

Novel Principle of Contactless Gauge Block Calibration

PubMed Central

Buchta, Zdeněk; Řeřucha, Šimon; Mikel, Břetislav; Čížek, Martin; Lazar, Josef; Číp, Ondřej

2012-01-01

In this paper, a novel principle of contactless gauge block calibration is presented. The principle of contactless gauge block calibration combines low-coherence interferometry and laser interferometry. An experimental setup combines Dowell interferometer and Michelson interferometer to ensure a gauge block length determination with direct traceability to the primary length standard. By monitoring both gauge block sides with a digital camera gauge block 3D surface measurements are possible too. The principle presented is protected by the Czech national patent No. 302948. PMID:22737012

Novel principle of contactless gauge block calibration.

PubMed

Buchta, Zdeněk; Reřucha, Simon; Mikel, Břetislav; Cížek, Martin; Lazar, Josef; Cíp, Ondřej

2012-01-01

In this paper, a novel principle of contactless gauge block calibration is presented. The principle of contactless gauge block calibration combines low-coherence interferometry and laser interferometry. An experimental setup combines Dowell interferometer and Michelson interferometer to ensure a gauge block length determination with direct traceability to the primary length standard. By monitoring both gauge block sides with a digital camera gauge block 3D surface measurements are possible too. The principle presented is protected by the Czech national patent No. 302948.

A Flywheel Energy Storage System Demonstration for Space Applications

NASA Technical Reports Server (NTRS)

Kenny, Barbara H.; Kascak, Peter E.; Jansen, Ralph; Dever, Timothy

2003-01-01

A novel control algorithm for the charge and discharge modes of operation of a flywheel energy storage system for space applications is presented. The motor control portion of the algorithm uses sensorless field oriented control with position and speed estimates determined from a signal injection technique at low speeds and a back EMF technique at higher speeds. The charge and discharge portion of the algorithm use command feed-forward and disturbance decoupling, respectively, to achieve fast response with low gains. Simulation and experimental results are presented.

Simple model for piezoelectric ceramic/polymer 1-3 composites used in ultrasonic transducer applications.

PubMed

Chan, H W; Unsworth, J

1989-01-01

A theoretical model is presented for combining parameters of 1-3 ultrasonic composite materials in order to predict ultrasonic characteristics such as velocity, acoustic impedance, electromechanical coupling factor, and piezoelectric coefficients. Hence, the model allows the estimation of resonance frequencies of 1-3 composite transducers. This model has been extended to cover more material parameters, and they are compared to experimental results up to PZT volume fraction nu of 0.8. The model covers calculation of piezoelectric charge constants d(33) and d(31). Values are found to be in good agreement with experimental results obtained for PZT 7A/Araldite D 1-3 composites. The acoustic velocity, acoustic impedance, and electromechanical coupling factor are predicted and found to be close to the values determined experimentally.

An integrated radiation physics computer code system.

NASA Technical Reports Server (NTRS)

Steyn, J. J.; Harris, D. W.

1972-01-01

An integrated computer code system for the semi-automatic and rapid analysis of experimental and analytic problems in gamma photon and fast neutron radiation physics is presented. Such problems as the design of optimum radiation shields and radioisotope power source configurations may be studied. The system codes allow for the unfolding of complex neutron and gamma photon experimental spectra. Monte Carlo and analytic techniques are used for the theoretical prediction of radiation transport. The system includes a multichannel pulse-height analyzer scintillation and semiconductor spectrometer coupled to an on-line digital computer with appropriate peripheral equipment. The system is geometry generalized as well as self-contained with respect to material nuclear cross sections and the determination of the spectrometer response functions. Input data may be either analytic or experimental.

Benchmark of FDNS CFD Code For Direct Connect RBCC Test Data

NASA Technical Reports Server (NTRS)

Ruf, J. H.

2000-01-01

Computational Fluid Dynamics (CFD) analysis results are compared with experimental data from the Pennsylvania State University's (PSU) Propulsion Engineering Research Center (PERC) rocket based combined cycle (RBCC) rocket-ejector experiments. The PERC RBCC experimental hardware was in a direct-connect configuration in diffusion and afterburning (DAB) operation. The objective of the present work was to validate the Finite Difference Navier Stokes (FDNS) CFD code for the rocket-ejector mode internal fluid mechanics and combustion phenomena. A second objective was determine the best application procedures to use FDNS as a predictive/engineering tool. Three-dimensional CFD analysis was performed. Solution methodology and grid requirements are discussed. CFD results are compared to experimental data for static pressure, Raman Spectroscopy species distribution data and RBCC net thrust and specified impulse.

Development and Validation of a Constitutive Model for Dental Composites during the Curing Process

NASA Astrophysics Data System (ADS)

Wickham Kolstad, Lauren

Debonding is a critical failure of a dental composites used for dental restorations. Debonding of dental composites can be determined by comparing the shrinkage stress of to the debonding strength of the adhesive that bonds it to the tooth surface. It is difficult to measure shrinkage stress experimentally. In this study, finite element analysis is used to predict the stress in the composite during cure. A new constitutive law is presented that will allow composite developers to evaluate composite shrinkage stress at early stages in the material development. Shrinkage stress and shrinkage strain experimental data were gathered for three dental resins, Z250, Z350, and P90. Experimental data were used to develop a constitutive model for the Young's modulus as a function of time of the dental composite during cure. A Maxwell model, spring and dashpot in series, was used to simulate the composite. The compliance of the shrinkage stress device was also taken into account by including a spring in series with the Maxwell model. A coefficient of thermal expansion was also determined for internal loading of the composite by dividing shrinkage strain by time. Three FEA models are presented. A spring-disk model validates that the constitutive law is self-consistent. A quarter cuspal deflection model uses separate experimental data to verify that the constitutive law is valid. Finally, an axisymmetric tooth model is used to predict interfacial stresses in the composite. These stresses are compared to the debonding strength to check if the composite debonds. The new constitutive model accurately predicted cuspal deflection data. Predictions for interfacial bond stress in the tooth model compare favorably with debonding characteristics observed in practice for dental resins.

A novel method for assessment of fragmentation and beam-material interactions in helium ion radiotherapy with a miniaturized setup.

PubMed

Gallas, Raya R; Arico, Giulia; Burigo, Lucas N; Gehrke, Tim; Jakůbek, Jan; Granja, Carlos; Tureček, Daniel; Martišíková, Maria

2017-10-01

Radiotherapy with protons and carbon ions enables to deliver dose distributions of high conformation to the target. Treatment with helium ions has been suggested due to their physical and biological advantages. A reliable benchmarking of the employed physics models with experimental data is required for treatment planning. However, experimental data for helium interactions is limited, in part due to the complexity and large size of conventional experimental setups. We present a novel method for the investigation of helium interactions with matter using miniaturized instrumentation based on highly integrated pixel detectors. The versatile setup consisted of a monitoring detector in front of the PMMA phantom of varying thickness and a detector stack for investigation of outgoing particles. The ion type downstream from the phantom was determined by high-resolution pattern recognition analysis of the single particle signals in the pixelated detectors. The fractions of helium and hydrogen ions behind the used targets were determined. As expected for the stable helium nucleus, only a minor decrease of the primary ion fluence along the target depth was found. E.g. the detected fraction of hydrogen ions on axis of a 220MeV/u 4 He beam was below 6% behind 24.5cm of PMMA. Monte-Carlo simulations using Geant4 reproduce the experimental data on helium attenuation and yield of helium fragments qualitatively, but significant deviations were found for some combinations of target thickness and beam energy. The presented method is promising to contribute to the reduction of the uncertainty of treatment planning for helium ion radiotherapy. Copyright © 2017 Associazione Italiana di Fisica Medica. Published by Elsevier Ltd. All rights reserved.

Extracellular Neural Microstimulation May Activate Much Larger Regions than Expected by Simulations: A Combined Experimental and Modeling Study

PubMed Central

Joucla, Sébastien; Branchereau, Pascal; Cattaert, Daniel; Yvert, Blaise

2012-01-01

Electrical stimulation of the central nervous system has been widely used for decades for either fundamental research purposes or clinical treatment applications. Yet, very little is known regarding the spatial extent of an electrical stimulation. If pioneering experimental studies reported that activation threshold currents (TCs) increase with the square of the neuron-to-electrode distance over a few hundreds of microns, there is no evidence that this quadratic law remains valid for larger distances. Moreover, nowadays, numerical simulation approaches have supplanted experimental studies for estimating TCs. However, model predictions have not yet been validated directly with experiments within a common paradigm. Here, we present a direct comparison between experimental determination and modeling prediction of TCs up to distances of several millimeters. First, we combined patch-clamp recording and microelectrode array stimulation in whole embryonic mouse spinal cords to determine TCs. Experimental thresholds did not follow a quadratic law beyond 1 millimeter, but rather tended to remain constant for distances larger than 1 millimeter. We next built a combined finite element – compartment model of the same experimental paradigm to predict TCs. While theoretical TCs closely matched experimental TCs for distances <250 microns, they were highly overestimated for larger distances. This discrepancy remained even after modifications of the finite element model of the potential field, taking into account anisotropic, heterogeneous or dielectric properties of the tissue. In conclusion, these results show that quadratic evolution of TCs does not always hold for large distances between the electrode and the neuron and that classical models may underestimate volumes of tissue activated by electrical stimulation. PMID:22879886

An Improved Method of Predicting Extinction Coefficients for the Determination of Protein Concentration.

PubMed

Hilario, Eric C; Stern, Alan; Wang, Charlie H; Vargas, Yenny W; Morgan, Charles J; Swartz, Trevor E; Patapoff, Thomas W

2017-01-01

Concentration determination is an important method of protein characterization required in the development of protein therapeutics. There are many known methods for determining the concentration of a protein solution, but the easiest to implement in a manufacturing setting is absorption spectroscopy in the ultraviolet region. For typical proteins composed of the standard amino acids, absorption at wavelengths near 280 nm is due to the three amino acid chromophores tryptophan, tyrosine, and phenylalanine in addition to a contribution from disulfide bonds. According to the Beer-Lambert law, absorbance is proportional to concentration and path length, with the proportionality constant being the extinction coefficient. Typically the extinction coefficient of proteins is experimentally determined by measuring a solution absorbance then experimentally determining the concentration, a measurement with some inherent variability depending on the method used. In this study, extinction coefficients were calculated based on the measured absorbance of model compounds of the four amino acid chromophores. These calculated values for an unfolded protein were then compared with an experimental concentration determination based on enzymatic digestion of proteins. The experimentally determined extinction coefficient for the native proteins was consistently found to be 1.05 times the calculated value for the unfolded proteins for a wide range of proteins with good accuracy and precision under well-controlled experimental conditions. The value of 1.05 times the calculated value was termed the predicted extinction coefficient. Statistical analysis shows that the differences between predicted and experimentally determined coefficients are scattered randomly, indicating no systematic bias between the values among the proteins measured. The predicted extinction coefficient was found to be accurate and not subject to the inherent variability of experimental methods. We propose the use of a predicted extinction coefficient for determining the protein concentration of therapeutic proteins starting from early development through the lifecycle of the product. LAY ABSTRACT: Knowing the concentration of a protein in a pharmaceutical solution is important to the drug's development and posology. There are many ways to determine the concentration, but the easiest one to use in a testing lab employs absorption spectroscopy. Absorbance of ultraviolet light by a protein solution is proportional to its concentration and path length; the proportionality constant is the extinction coefficient. The extinction coefficient of a protein therapeutic is usually determined experimentally during early product development and has some inherent method variability. In this study, extinction coefficients of several proteins were calculated based on the measured absorbance of model compounds. These calculated values for an unfolded protein were then compared with experimental concentration determinations based on enzymatic digestion of the proteins. The experimentally determined extinction coefficient for the native protein was 1.05 times the calculated value for the unfolded protein with good accuracy and precision under controlled experimental conditions, so the value of 1.05 times the calculated coefficient was called the predicted extinction coefficient. Comparison of predicted and measured extinction coefficients indicated that the predicted value was very close to the experimentally determined values for the proteins. The predicted extinction coefficient was accurate and removed the variability inherent in experimental methods. © PDA, Inc. 2017.

Method for determining the octane rating of gasoline samples by observing corresponding acoustic resonances therein

DOEpatents

Sinha, Dipen N.; Anthony, Brian W.

1997-01-01

A method for determining the octane rating of gasoline samples by observing corresponding acoustic resonances therein. A direct correlation between the octane rating of gasoline and the frequency of corresponding acoustic resonances therein has been experimentally observed. Therefore, the octane rating of a gasoline sample can be directly determined through speed of sound measurements instead of by the cumbersome process of quantifying the knocking quality of the gasoline. Various receptacle geometries and construction materials may be employed. Moreover, it is anticipated that the measurements can be performed on flowing samples in pipes, thereby rendering the present method useful in refineries and distilleries.

A simplified method for determining reactive rate parameters for reaction ignition and growth in explosives

DOE Office of Scientific and Technical Information (OSTI.GOV)

Miller, P.J.

1996-07-01

A simplified method for determining the reactive rate parameters for the ignition and growth model is presented. This simplified ignition and growth (SIG) method consists of only two adjustable parameters, the ignition (I) and growth (G) rate constants. The parameters are determined by iterating these variables in DYNA2D hydrocode simulations of the failure diameter and the gap test sensitivity until the experimental values are reproduced. Examples of four widely different explosives were evaluated using the SIG model. The observed embedded gauge stress-time profiles for these explosives are compared to those calculated by the SIG equation and the results are described.

Combined Experimental and Numerical Simulations of Thermal Barrier Coated Turbine Blades Erosion

NASA Technical Reports Server (NTRS)

Hamed, Awate; Tabakoff, Widen; Swar, Rohan; Shin, Dongyun; Woggon, Nthanial; Miller, Robert

2013-01-01

A combined experimental and computational study was conducted to investigate the erosion of thermal barrier coated (TBC) blade surfaces by alumina particles ingestion in a single stage turbine. In the experimental investigation, tests of particle surface interactions were performed in specially designed tunnels to determine the erosion rates and particle restitution characteristics under different impact conditions. The experimental results show that the erosion rates increase with increased impingement angle, impact velocity and temperature. In the computational simulations, an Euler-Lagrangian two stage approach is used in obtaining numerical solutions to the three-dimensional compressible Reynolds Averaged Navier-Stokes equations and the particles equations of motion in each blade passage reference frame. User defined functions (UDF) were developed to represent experimentally-based correlations for particle surface interaction models which were employed in the three-dimensional particle trajectory simulations to determine the particle rebound characteristics after each surface impact. The experimentally based erosion UDF model was used to predict the TBC erosion rates on the turbine blade surfaces based on the computed statistical data of the particles impact locations, velocities and angles relative to the blade surface. Computational results are presented for the predicted TBC blade erosion in a single stage commercial APU turbine, for a NASA designed automotive turbine, and for the NASA turbine scaled for modern rotorcraft operating conditions. The erosion patterns in the turbines are discussed for uniform particle ingestion and for particle ingestion concentrated in the inner and outer 5 percent of the stator blade span representing the flow cooling the combustor liner.

Education in physics and the support of professional orientation of pupils

NASA Astrophysics Data System (ADS)

ŠebeÅ, Vladimír; Lapitková, Viera

2017-01-01

Authors in the article present some of the conclusions resulting from execution of a national project ITMS: 26110130549 "Support for guidance primary school pupils for vocational education and training through the development of polytechnic education aimed at developing work skills and work with talents". Authors focus on the influence of selected determinants of students' interest in Physics. Outputs linked to the increase of pupils' knowledge of physics; ways of increasing interest in physics and thus influencing the choice of secondary studies are presented based on two-year research that was realized in forms of experimental activities in newly built laboratories. Selection of physics experiments realized during lessons was determined by implementation of innovative teaching aids and information and communication technologies. The most important results that were analysed related to the research were presented.

A computer program to determine the possible daily release window for sky target experiments

NASA Technical Reports Server (NTRS)

Michaud, N. H.

1973-01-01

A computer program is presented which is designed to determine the daily release window for sky target experiments. Factors considered in the program include: (1) target illumination by the sun at release time and during the tracking period; (2) look angle elevation above local horizon from each tracking station to the target; (3) solar depression angle from the local horizon of each tracking station during the experimental period after target release; (4) lunar depression angle from the local horizon of each tracking station during the experimental period after target release; and (5) total sky background brightness as seen from each tracking station while viewing the target. Program output is produced in both graphic and data form. Output data can be plotted for a single calendar month or year. The numerical values used to generate the plots are furnished to permit a more detailed review of the computed daily release windows.

Investigation of gamma ray shielding, structural and dissolution rate properties of Bi2O3-BaO-B2O3-Na2O glass system

NASA Astrophysics Data System (ADS)

Dogra, Mridula; Singh, K. J.; Kaur, Kulwinder; Anand, Vikas; Kaur, Parminder; Singh, Prabhjot; Bajwa, B. S.

2018-03-01

In the present study, quaternary system of the composition (0.45 + x) Bi2O3-(0.25 - x) BaO-0.15 B2O3-0.15 Na2O (where 0 ≤ x ≤ 0.2 mol fraction) has been prepared by using melt-quenching technique for investigation of gamma ray shielding properties. Mass attenuation coefficients and half value layer parameters have been determined experimentally at 662 keV by using 137Cs source. It has been found that experimental results of these parameters hold good agreement with theoretical values. The density, molar volume, XRD, FTIR, Raman and UV-visible studies have been used to determine structural properties of the prepared glass samples. Dissolution rate of the samples has also been measured to check their utility as long term durable glasses.

[Determining the efficacy of a high-school life-skills' programme in Huancavelica, Peru].

PubMed

Choque-Larrauri, Raúl; Chirinos-Cáceres, Jesús Lorenzo

2009-01-01

Determining the efficacy of a life-skills' programme within the context of a school health promotion programme using teenagers from a high-school in the district of Huancavelica, Peru during school year 2006. This was non-equivalent experimental research with pre-test and post-test. The subjects consisted of 284 high school students. The variables analyzed were communication, self esteem, assertiveness, decision making, sex and age. There was a significant increase in the experimental group's communication and assertiveness skills' development. There were no significant differences in decision-making and self-esteem skills. The life-skills' programme was effective during one school year, especially in terms of learning and developing communication and assertiveness skills. However, self-esteem and decision-making skills did not present a statistically significance difference. Programme implementation must thus be redirected and the life-skills' programme should be implemented throughout all high-school years.

E. S. R. determination of atomic hydrogen distribution in oxy-fuel flames burning at atmospheric pressure

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bregeon, B.G.; Kadirgan, M.A.N.; Lamy, C.

1981-01-01

The authors have derived an experimental technique, using ESR spectroscopy, that allows this determination. A quartz burner equipped with an appropriate cooling system is placed directly in the ESR cavity. We obtained the hydrogen resonance signal and studied its variation for different positions of the flame inside the cavity. Hydrogen concentrations cannot be calculated directly from experimental data; hence we proceed indirectly to deconvoluate the resonance signal. This allows us to overcome the present severe handicap in obtaining atomic hydrogen concentrations in oxy-fuel flames from ESR measurements. Data obtained in this work, after temperature correction, give us the axial distributionmore » of hydrogen radicals for different oxy-propane and hydrogen-oxygen flames. These results show clearly that for all flames, the hydrogen radical concentration is maximum in a zone immediately above the inner cone. 13 refs.« less

Experimental validation of analytical models for a rapid determination of cycle parameters in thermoplastic injection molding

NASA Astrophysics Data System (ADS)

Pignon, Baptiste; Sobotka, Vincent; Boyard, Nicolas; Delaunay, Didier

2017-10-01

Two different analytical models were presented to determine cycle parameters of thermoplastics injection process. The aim of these models was to provide quickly a first set of data for mold temperature and cooling time. The first model is specific to amorphous polymers and the second one is dedicated to semi-crystalline polymers taking the crystallization into account. In both cases, the nature of the contact between the polymer and the mold could be considered as perfect or not (thermal contact resistance was considered). Results from models are compared with experimental data obtained with an instrumented mold for an acrylonitrile butadiene styrene (ABS) and a polypropylene (PP). Good agreements were obtained for mold temperature variation and for heat flux. In the case of the PP, the analytical crystallization times were compared with those given by a coupled model between heat transfer and crystallization kinetics.