Sample records for rate tensile tests

  1. High-rate tensile properties of Si-reduced TRIP sheet steels

    NASA Astrophysics Data System (ADS)

    Choi, Ildong; Park, Yeongdo; Son, Dongmin; Kim, Sung-Joon; Moon, Manbeen

    2010-02-01

    There have been efforts to develop Si-reduced TRIP steels to improve the wettability of Zn coatings, since the conventional CMnSi-TRIP steels suffer from poor galvanizability. In addition, for the development of potential applications of Si-reduced TRIP steels in vehicle crash management, a better understanding of high strain rate properties is required. In the present study, the effects of alloying elements, such as Cu, Al, Si, and P, on the high-rate tensile properties of Si-reduced TRIP sheet steels were investigated. Tensile tests were performed with a servo-hydraulic tensile testing machine at strain rates ranging from 10-2 to 6 × 102 s-1, and the ultimate tensile strength, elongation, strain rate sensitivity, and absorbed energy were evaluated. The retained austenite volume fractions and carbon content of the specimens were measured using neutron diffraction. The UTS was increased with Cu, Al, Si, and P alloying throughout the strain rate range, and the alloying effect on UTS was considerable with Cu and P. The effects of alloying on the microstructure were not significant. All the steels tested in this study exhibited positive strain rate sensitivity, and the m value at strain rates higher than 10 s-1 was at least two times higher than that at lower strain rates.

  2. Experimental and Numerical Study on Tensile Strength of Concrete under Different Strain Rates

    PubMed Central

    Min, Fanlu; Yao, Zhanhu; Jiang, Teng

    2014-01-01

    The dynamic characterization of concrete is fundamental to understand the material behavior in case of heavy earthquakes and dynamic events. The implementation of material constitutive law is of capital importance for the numerical simulation of the dynamic processes as those caused by earthquakes. Splitting tensile concrete specimens were tested at strain rates of 10−7 s−1 to 10−4 s−1 in an MTS material test machine. Results of tensile strength versus strain rate are presented and compared with compressive strength and existing models at similar strain rates. Dynamic increase factor versus strain rate curves for tensile strength were also evaluated and discussed. The same tensile data are compared with strength data using a thermodynamic model. Results of the tests show a significant strain rate sensitive behavior, exhibiting dynamic tensile strength increasing with strain rate. In the quasistatic strain rate regime, the existing models often underestimate the experimental results. The thermodynamic theory for the splitting tensile strength of concrete satisfactorily describes the experimental findings of strength as effect of strain rates. PMID:24883355

  3. High Strain Rate Tensile Testing of Silver Nanowires: Rate-Dependent Brittle-to-Ductile Transition.

    PubMed

    Ramachandramoorthy, Rajaprakash; Gao, Wei; Bernal, Rodrigo; Espinosa, Horacio

    2016-01-13

    The characterization of nanomaterials under high strain rates is critical to understand their suitability for dynamic applications such as nanoresonators and nanoswitches. It is also of great theoretical importance to explore nanomechanics with dynamic and rate effects. Here, we report in situ scanning electron microscope (SEM) tensile testing of bicrystalline silver nanowires at strain rates up to 2/s, which is 2 orders of magnitude higher than previously reported in the literature. The experiments are enabled by a microelectromechanical system (MEMS) with fast response time. It was identified that the nanowire plastic deformation has a small activation volume (<10b(3)), suggesting dislocation nucleation as the rate controlling mechanism. Also, a remarkable brittle-to-ductile failure mode transition was observed at a threshold strain rate of 0.2/s. Transmission electron microscopy (TEM) revealed that along the nanowire, dislocation density and spatial distribution of plastic regions increase with increasing strain rate. Furthermore, molecular dynamic (MD) simulations show that deformation mechanisms such as grain boundary migration and dislocation interactions are responsible for such ductility. Finally, the MD and experimental results were interpreted using dislocation nucleation theory. The predicted yield stress values are in agreement with the experimental results for strain rates above 0.2/s when ductility is pronounced. At low strain rates, random imperfections on the nanowire surface trigger localized plasticity, leading to a brittle-like failure.

  4. The Dynamic Tensile Behavior of Railway Wheel Steel at High Strain Rates

    NASA Astrophysics Data System (ADS)

    Jing, Lin; Han, Liangliang; Zhao, Longmao; Zhang, Ying

    2016-11-01

    The dynamic tensile tests on D1 railway wheel steel at high strain rates were conducted using a split Hopkinson tensile bar (SHTB) apparatus, compared to quasi-static tests. Three different types of specimens, which were machined from three different positions (i.e., the rim, web and hub) of a railway wheel, were prepared and examined. The rim specimens were checked to have a higher yield stress and ultimate tensile strength than those web and hub specimens under both quasi-static and dynamic loadings, and the railway wheel steel was demonstrated to be strain rate dependent in dynamic tension. The dynamic tensile fracture surfaces of all the wheel steel specimens are cup-cone-shaped morphology on a macroscopic scale and with the quasi-ductile fracture features on the microscopic scale.

  5. Interaction of heat production, strain rate and stress power in a plastically deforming body under tensile test

    NASA Technical Reports Server (NTRS)

    Paglietti, A.

    1982-01-01

    At high strain rates the heat produced by plastic deformation can give rise to a rate dependent response even if the material has rate independent constitutive equations. This effect has to be evaluated when interpreting a material test, or else it could erroneously be ascribed to viscosity. A general thermodynamic theory of tensile testing of elastic-plastic materials is given in this paper; it is valid for large strain at finite strain rates. It enables discovery of the parameters governing the thermodynamic strain rate effect, provides a method for proper interpretation of the results of the tests of dynamic plasticity, and suggests a way of planning experiments in order to detect the real contribution of viscosity.

  6. Strain Rate Sensitivity of Epoxy Resin in Tensile and Shear Loading

    NASA Technical Reports Server (NTRS)

    Gilat, Amos; Goldberg, Robert K.; Roberts, Gary D.

    2005-01-01

    The mechanical response of E-862 and PR-520 resins is investigated in tensile and shear loadings. At both types of loading the resins are tested at strain rates of about 5x10(exp 5), 2, and 450 to 700 /s. In addition, dynamic shear modulus tests are carried out at various frequencies and temperatures, and tensile stress relaxation tests are conducted at room temperature. The results show that the toughened PR-520 resin can carry higher stresses than the untoughened E-862 resin. Strain rate has a significant effect on the response of both resins. In shear both resins show a ductile response with maximum stress that is increasing with strain rate. In tension a ductile response is observed at low strain rate (approx. 5x10(exp 5) /s), and brittle response is observed at the medium and high strain rates (2, and 700 /s). The hydrostatic component of the stress in the tensile tests causes premature failure in the E-862 resin. Localized deformation develops in the PR-520 resin when loaded in shear. An internal state variable constitutive model is proposed for modeling the response of the resins. The model includes a state variable that accounts for the effect of the hydrostatic component of the stress on the deformation.

  7. Dynamic tensile fracture of mortar at ultra-high strain-rates

    NASA Astrophysics Data System (ADS)

    Erzar, B.; Buzaud, E.; Chanal, P.-Y.

    2013-12-01

    During the lifetime of a structure, concrete and mortar may be exposed to highly dynamic loadings, such as impact or explosion. The dynamic fracture at high loading rates needs to be well understood to allow an accurate modeling of this kind of event. In this work, a pulsed-power generator has been employed to conduct spalling tests on mortar samples at strain-rates ranging from 2 × 104 to 4 × 104 s-1. The ramp loading allowed identifying the strain-rate anytime during the test. A power law has been proposed to fit properly the rate-sensitivity of tensile strength of this cementitious material over a wide range of strain-rate. Moreover, a specimen has been recovered damaged but unbroken. Micro-computed tomography has been employed to study the characteristics of the damage pattern provoked by the dynamic tensile loading.

  8. Use of Slow Strain Rate Tensile Testing to Assess the Ability of Several Superalloys to Resist Environmentally-Assisted Intergranular Cracking

    NASA Technical Reports Server (NTRS)

    Gabb, Timothy P.; Telesman, Jack; Banik, Anthony; McDevitt, Erin

    2014-01-01

    Intergranular fatigue crack initiation and growth due to environmental degradation, especially at notched features, can often limit the fatigue life of disk superalloys at high temperatures. For clear comparisons, the effects of alloy composition on cracking in air needs to be understood and compared separately from variables associated with notches and cracks such as effective stress concentration, plastic flow, stress relaxation, and stress redistribution. The objective of this study was to attempt using simple tensile tests of specimens with uniform gage sections to compare the effects of varied alloy composition on environment-assisted cracking of several powder metal and cast and wrought superalloys including ME3, LSHR, Udimet 720(TradeMark) ATI 718Plus(Registered TradeMark) alloy, Haynes 282(Trademark), and Inconel 740(TradeMark) Slow and fast strain-rate tensile tests were found to be a useful tool to compare propensities for intergranular surface crack initiation and growth. The effects of composition and heat treatment on tensile fracture strain and associated failure modes were compared. Environment interactions were determined to often limit ductility, by promoting intergranular surface cracking. The response of various superalloys and heat treatments to slow strain rate tensile testing varied substantially, showing that composition and microstructure can significantly influence environmental resistance to cracking.

  9. Improved Tensile Test for Ceramics

    NASA Technical Reports Server (NTRS)

    Osiecki, R. A.

    1982-01-01

    For almost-nondestructive tensile testing of ceramics, steel rod is bonded to sample of ceramic. Assembly is then pulled apart in conventional tensile-test machine. Test destroys only shallow surface layer which can be machined away making specimen ready for other uses. Method should be useful as manufacturing inspection procedure for low-strength brittle materials.

  10. Dynamic tensile fracture of mortar at ultra-high strain-rates

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Erzar, B., E-mail: benjamin.erzar@cea.fr; Buzaud, E.; Chanal, P.-Y.

    2013-12-28

    During the lifetime of a structure, concrete and mortar may be exposed to highly dynamic loadings, such as impact or explosion. The dynamic fracture at high loading rates needs to be well understood to allow an accurate modeling of this kind of event. In this work, a pulsed-power generator has been employed to conduct spalling tests on mortar samples at strain-rates ranging from 2 × 10{sup 4} to 4 × 10{sup 4} s{sup −1}. The ramp loading allowed identifying the strain-rate anytime during the test. A power law has been proposed to fit properly the rate-sensitivity of tensile strength of thismore » cementitious material over a wide range of strain-rate. Moreover, a specimen has been recovered damaged but unbroken. Micro-computed tomography has been employed to study the characteristics of the damage pattern provoked by the dynamic tensile loading.« less

  11. Ultimate Tensile Strength as a Function of Test Rate for Various Ceramic Matrix Composites at Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Bansal, Narottam P.; Gyekenyesi, John P.

    2002-01-01

    Ultimate tensile strength of five different continuous fiber-reinforced ceramic composites, including SiC/BSAS (2D 2 types), SiC/MAS-5 (2D), SiC/SiC (2D enhanced), and C/SiC(2D) was determined as a function of test rate at I 100 to 1200 'C in air. All five composite materials exhibited a significant dependency of ultimate strength on test rate such that the ultimate strength decreased with decreasing test rate, similar to the behavior observed in many advanced monolithic ceramics at elevated temperatures. The application of the preloading technique as well as the prediction of life from one loading configuration (constant stress rate) to another (constant stress loading) for SiC/BSAS suggested that the overall macroscopic failure mechanism of the composites would be the one governed by a power-law type of damage evolution/accumulation, analogous to slow crack growth commonly observed in advanced monolithic ceramics.

  12. Manual for LDEF tensile tests

    NASA Technical Reports Server (NTRS)

    Witte, W. G., Jr.

    1985-01-01

    One of the experiments aboard the NASA Long Duration Exposure Facility (LDEF) consists of a tray of approximately one hundred tensile specimens of several candidate space structure composite materials. During the LDEF flight the materials will be subjected to the space environment and to possible contamination during launch and recovery. Tensile tests of representative samples were made before the LDEF flight to obtain baseline data. Similar tests will be made on control specimens stored on earth for the length of the LDEF flight and on recovered flight specimens. This manual codifies the details of testing, data acquisition, and handling used in obtaining the baseline data so that the same procedures and equipment will be used on the subsequent tests.

  13. Influence of strain rate and temperature on tensile properties and flow behaviour of a reduced activation ferritic-martensitic steel

    NASA Astrophysics Data System (ADS)

    Vanaja, J.; Laha, K.; Sam, Shiju; Nandagopal, M.; Panneer Selvi, S.; Mathew, M. D.; Jayakumar, T.; Rajendra Kumar, E.

    2012-05-01

    Tensile strength and flow behaviour of a Reduced Activation Ferritic-Martensitic (RAFM) steel (9Cr-1W-0.06Ta-0.22V-0.08C) have been investigated over a temperature range of 300-873 K at different strain rates. Tensile strength of the steel decreased with temperature and increased with strain rate except at intermediate temperatures. Negative strain rate sensitivity of flow stress of the steel at intermediate temperatures revealed the occurrence of dynamic strain ageing in the steel, even though no serrated flow was observed. The tensile flow behaviour of the material was well represented by the Voce strain hardening equation for all the test conditions. Temperature and strain rate dependence of the various parameters of Voce equation were interpreted with the possible deformation mechanisms. The equivalence between the saturation stress at a given strain rate in tensile test and steady state deformation rate at a given stress in creep test was found to be satisfied by the RAFM steel.

  14. Tensile testing apparatus

    NASA Technical Reports Server (NTRS)

    Blackburn, L. B.; Ellingsworth, J. R. (Inventor)

    1985-01-01

    An improved mechanical extensometer is described for use with a constant load creep test machine. The dead weight of the extensometer is counterbalanced by two pairs of weights connected through a pulley system and to rod extension and leading into the furnace where the test sample is undergoing elevated temperature (above 500 F.) tensile testing. Novel gripper surfaces, conical tip and flat surface are provided in each sampling engaging platens to reduce the grip pressure normally required for attachment of the extensometer to the specimen and reduce initial specimen bending normally associated with foil-gage metal testing.

  15. Static tensile and tensile creep testing of five ceramic fibers at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Zimmerman, Richard S.; Adams, Donald F.

    1988-01-01

    Static tensile and tensile creep testing of five ceramic fibers at elevated temperature was performed. J.P. Stevens, Co., Astroquartz 9288 glass fiber, Nippon Carbon, Ltd., (Dow Corning) Nicalon NLM-102 silicon carbide fiber, and 3M Company Nextel 312, 380, and 480 alumina/silica/boria fibers were supplied in unsized tows. Single fibers were separated from the tows and tested in static tension and tensile creep. Elevated test temperatures ranged from 400 to 1300 C and varied for each fiber. Room temperature static tension was also performed. Computer software was written to reduce all single fiber test data into engineering constants using ASTM Standard Test Method D3379-75 as a reference. A high temperature furnace was designed and built to perform the single fiber elevated temperature testing up to 1300 C. A computerized single fiber creep apparatus was designed and constructed to perform four fiber creep tests simultaneously at temperatures up to 1300 C. Computer software was written to acquire and reduce all creep data.

  16. Tensile Strength of Carbon Nanotubes Under Realistic Temperature and Strain Rate

    NASA Technical Reports Server (NTRS)

    Wei, Chen-Yu; Cho, Kyeong-Jae; Srivastava, Deepak; Biegel, Bryan (Technical Monitor)

    2002-01-01

    Strain rate and temperature dependence of the tensile strength of single-wall carbon nanotubes has been investigated with molecular dynamics simulations. The tensile failure or yield strain is found to be strongly dependent on the temperature and strain rate. A transition state theory based predictive model is developed for the tensile failure of nanotubes. Based on the parameters fitted from high-strain rate and temperature dependent molecular dynamics simulations, the model predicts that a defect free micrometer long single-wall nanotube at 300 K, stretched with a strain rate of 1%/hour, fails at about 9 plus or minus 1% tensile strain. This is in good agreement with recent experimental findings.

  17. High temperature tensile testing of ceramic composites

    NASA Technical Reports Server (NTRS)

    Gyekenyesi, John Z.; Hemann, John H.

    1988-01-01

    The various components of a high temperature tensile testing system are evaluated. The objective is the high temperature tensile testing of SiC fiber reinforced reaction bonded Si3N4 specimens at test temperatures up to 1650 C (3000 F). Testing is to be conducted in inert gases and air. Gripping fixtures, specimen configurations, furnaces, optical strain measuring systems, and temperature measurement techniques are reviewed. Advantages and disadvantages of the various techniques are also noted.

  18. Tensile Testing: A Simple Introduction

    ERIC Educational Resources Information Center

    Carr, Martin

    2006-01-01

    Tensile testing may be used to decide, say, which steel to use in various constructions. Analogous testing can be done simply in the classroom using plasticine and helps to introduce pupils to the various properties studied in materials science.

  19. Static tensile and tensile creep testing of five ceramic fibers at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Zimmerman, Richard S.; Adams, Donald F.

    1989-01-01

    Static tensile and tensile creep testing of five ceramic fibers at elevated temperature was performed. J.P. Stevens, Co., Astroquartz 9288 glass fiber; Nippon Carbon, Ltd., (Dow Corning) nicalon NLM-102 silicon carbide fiber; and 3M Company Nextel 312, 380, and 480 alumina/silica/boria fibers were supplied in unsized tows. Single fibers were separated from the tows and tested in static tension and tensile creep. Elevated test temperatures ranged from 400 C to 1300 C and varied for each fiber. Room temperature static tension was also performed. Computer software was written to reduce all single fiber test data into engineering constants using ASTM Standard Test Method D3379-75 as a reference. A high temperature furnace was designed and built to perform the single fiber elevated temperature testing up to 1300 C. A computerized single fiber creep apparatus was designed and constructed to perform four fiber creep tests simultaneously at temperatures up to 1300 C. Computer software was written to acquire and reduce all creep data.

  20. Apparatus facilitates high-temperature tensile testing in vacuum

    NASA Technical Reports Server (NTRS)

    Sikora, P. F.

    1964-01-01

    An apparutus for heating refractory materials to high temperatures during tensile testing includes a water-cooled stainless steel vacuum chamber. This contains a resistance heater consisting of a slit tube of tantalum or tungsten to enclose the tensile test rod.

  1. High-Tensile Strength Tape Versus High-Tensile Strength Suture: A Biomechanical Study.

    PubMed

    Gnandt, Ryan J; Smith, Jennifer L; Nguyen-Ta, Kim; McDonald, Lucas; LeClere, Lance E

    2016-02-01

    To determine which suture design, high-tensile strength tape or high-tensile strength suture, performed better at securing human tissue across 4 selected suture techniques commonly used in tendinous repair, by comparing the total load at failure measured during a fixed-rate longitudinal single load to failure using a biomechanical testing machine. Matched sets of tendon specimens with bony attachments were dissected from 15 human cadaveric lower extremities in a manner allowing for direct comparison testing. With the use of selected techniques (simple Mason-Allen in the patellar tendon specimens, whip stitch in the quadriceps tendon specimens, and Krackow stitch in the Achilles tendon specimens), 1 sample of each set was sutured with a 2-mm braided, nonabsorbable, high-tensile strength tape and the other with a No. 2 braided, nonabsorbable, high-tensile strength suture. A total of 120 specimens were tested. Each model was loaded to failure at a fixed longitudinal traction rate of 100 mm/min. The maximum load and failure method were recorded. In the whip stitch and the Krackow-stitch models, the high-tensile strength tape had a significantly greater mean load at failure with a difference of 181 N (P = .001) and 94 N (P = .015) respectively. No significant difference was found in the Mason-Allen and simple stitch models. Pull-through remained the most common method of failure at an overall rate of 56.7% (suture = 55%; tape = 58.3%). In biomechanical testing during a single load to failure, high-tensile strength tape performs more favorably than high-tensile strength suture, with a greater mean load to failure, in both the whip- and Krackow-stitch models. Although suture pull-through remains the most common method of failure, high-tensile strength tape requires a significantly greater load to pull-through in a whip-stitch and Krakow-stitch model. The biomechanical data obtained in the current study indicates that high-tensile strength tape may provide better repair

  2. Static tensile and tensile creep testing of four boron nitride coated ceramic fibers at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Coguill, Scott L.; Adams, Donald F.; Zimmerman, Richard S.

    1989-01-01

    Six types of uncoated ceramic fibers were static tensile and tensile creep tested at various elevated temperatures. Three types of boron nitride coated fibers were also tested. Room temperature static tensile tests were initially performed on all fibers, at gage lengths of 1, 2, and 4 inches, to determine the magnitude of end effects from the gripping system used. Tests at one elevated temperature, at gage lengths of 8 and 10 inches, were also conducted, to determine end effects at elevated temperatures. Fiber cross sectional shapes and areas were determined using scanning electron microscopy. Creep testing was typically performed for 4 hours, in an air atmosphere.

  3. Micro-tensile testing system

    DOEpatents

    Wenski, Edward G [Lenexa, KS

    2007-08-21

    A micro-tensile testing system providing a stand-alone test platform for testing and reporting physical or engineering properties of test samples of materials having thicknesses of approximately between 0.002 inch and 0.030 inch, including, for example, LiGA engineered materials. The testing system is able to perform a variety of static, dynamic, and cyclic tests. The testing system includes a rigid frame and adjustable gripping supports to minimize measurement errors due to deflection or bending under load; serrated grips for securing the extremely small test sample; high-speed laser scan micrometers for obtaining accurate results; and test software for controlling the testing procedure and reporting results.

  4. Micro-tensile testing system

    DOEpatents

    Wenski, Edward G.

    2006-01-10

    A micro-tensile testing system providing a stand-alone test platform for testing and reporting physical or engineering properties of test samples of materials having thicknesses of approximately between 0.002 inch and 0.030 inch, including, for example, LiGA engineered materials. The testing system is able to perform a variety of static, dynamic, and cyclic tests. The testing system includes a rigid frame and adjustable gripping supports to minimize measurement errors due to deflection or bending under load; serrated grips for securing the extremely small test sample; high-speed laser scan micrometers for obtaining accurate results; and test software for controlling the testing procedure and reporting results.

  5. Micro-tensile testing system

    DOEpatents

    Wenski, Edward G [Lenexa, KS

    2007-07-17

    A micro-tensile testing system providing a stand-alone test platform for testing and reporting physical or engineering properties of test samples of materials having thicknesses of approximately between 0.002 inch and 0.030 inch, including, for example, LiGA engineered materials. The testing system is able to perform a variety of static, dynamic, and cyclic tests. The testing system includes a rigid frame and adjustable gripping supports to minimize measurement errors due to deflection or bending under load; serrated grips for securing the extremely small test sample; high-speed laser scan micrometers for obtaining accurate results; and test software for controlling the testing procedure and reporting results.

  6. Tensile-Creep Test Specimen Preparation Practices of Surface Support Liners

    NASA Astrophysics Data System (ADS)

    Guner, Dogukan; Ozturk, Hasan

    2017-12-01

    Ground support has always been considered as a challenging issue in all underground operations. Many forms of support systems and supporting techniques are available in the mining/tunnelling industry. In the last two decades, a new polymer based material, Thin Spray-on Liner (TSL), has attained a place in the market as an alternative to the current areal ground support systems. Although TSL provides numerous merits and has different application purposes, the knowledge on mechanical properties and performance of this material is still limited. In laboratory studies, since tensile rupture is the most commonly observed failure mechanism in field applications, researchers have generally studied the tensile testing of TSLs with modification of American Society for Testing and Materials (ASTM) D-638 standards. For tensile creep testing, specimen preparation process also follows the ASTM standards. Two different specimen dimension types (Type I, Type IV) are widely preferred in TSL tensile testing that conform to the related standards. Moreover, molding and die cutting are commonly used specimen preparation techniques. In literature, there is a great variability of test results due to the difference in specimen preparation techniques and practices. In this study, a ductile TSL product was tested in order to investigate the effect of both specimen preparation techniques and specimen dimensions under 7-day curing time. As a result, ultimate tensile strength, tensile yield strength, tensile modulus, and elongation at break values were obtained for 4 different test series. It is concluded that Type IV specimens have higher strength values compared to Type I specimens and moulded specimens have lower results than that of prepared by using die cutter. Moreover, specimens prepared by molding techniques have scattered test results. Type IV specimens prepared by die cutter technique are suggested for preparation of tensile test and Type I specimens prepared by die cutter technique

  7. Effects of temperature, strain rate, and vacancies on tensile and fatigue behaviors of silicon-based nanotubes

    NASA Astrophysics Data System (ADS)

    Jeng, Yeau-Ren; Tsai, Ping-Chi; Fang, Te-Hua

    2005-02-01

    This paper adopts the Tersoff-Brenner many-body potential function to perform molecular dynamics simulations of the tensile and fatigue behaviors of hypothetical silicon-based tubular nanostructures at various temperatures, strain rates, and vacancy percentages. The tensile test results indicate that with a predicted Young’s modulus of approximately 60GPa , silicon nanotubes (SiNTs) are significantly less stiff than conventional carbon nanotubes. It is observed that the presence of hydrogen has a significant influence on the tensile strength of SiNTs . Additionally, the present results indicate that the tensile strength clearly decreases with increasing temperature and with decreasing strain rate. Moreover, it is shown that the majority of the mechanical properties considered in the present study decrease with an increasing vacancy percentage. Regarding the fatigue tests, this study uses a standard theoretical model to derive curves of amplitude stress versus number of cycles for the current nanotubes. The results demonstrate that the fatigue limit of SiNTs increases with a decreasing vacancy percentage and with increasing temperature.

  8. High-strain rate tensile characterization of graphite platelet reinforced vinyl ester based nanocomposites using split-Hopkinson pressure bar

    NASA Astrophysics Data System (ADS)

    Pramanik, Brahmananda

    The dynamic response of exfoliated graphite nanoplatelet (xGnP) reinforced and carboxyl terminated butadiene nitrile (CTBN) toughened vinyl ester based nanocomposites are characterized under both dynamic tensile and compressive loading. Dynamic direct tensile tests are performed applying the reverse impact Split Hopkinson Pressure Bar (SHPB) technique. The specimen geometry for tensile test is parametrically optimized by Finite Element Analysis (FEA) using ANSYS Mechanical APDLRTM. Uniform stress distribution within the specimen gage length has been verified using high-speed digital photography. The on-specimen strain gage installation is substituted by a non-contact Laser Occlusion Expansion Gage (LOEG) technique for infinitesimal dynamic tensile strain measurements. Due to very low transmitted pulse signal, an alternative approach based on incident pulse is applied for obtaining the stress-time history. Indirect tensile tests are also performed combining the conventional SHPB technique with Brazilian disk test method for evaluating cylindrical disk specimens. The cylindrical disk specimen is held snugly in between two concave end fixtures attached to the incident and transmission bars. Indirect tensile stress is estimated from the SHPB pulses, and diametrical transverse tensile strain is measured using LOEG. Failure diagnosis using high-speed digital photography validates the viability of utilizing this indirect test method for characterizing the tensile properties of the candidate vinyl ester based nanocomposite system. Also, quasi-static indirect tensile response agrees with previous investigations conducted using the traditional dog-bone specimen in quasi-static direct tensile tests. Investigation of both quasi-static and dynamic indirect tensile test responses show the strain rate effect on the tensile strength and energy absorbing capacity of the candidate materials. Finally, the conventional compressive SHPB tests are performed. It is observed that both

  9. The effect of low dose rate irradiation on the tensile properties and microstructure of austenitic stainless steel.

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Allen, T. R.; Tsai, H.; Cole, J. I.

    2002-09-17

    To assess the effects of long-term, low-dose-rate neutron exposure on mechanical strength and ductility, tensile properties were measured on 12% and 20% cold-worked Type 316 stainless steel. Samples were prepared from reactor core components retrieved from the EBR-II reactor following final shutdown. Sample locations were chosen to cover a dose range of 1-56 dpa at temperatures from 371-440 C and dose rates from 0.5-5.8 x10{sup -7} dpa/s. These dose rates are approximately an order of magnitude lower than those of typical EBR-II test sample locations. The tensile tests for the 12% CW material were performed at 380 C and 430more » C while those for the 20% CW samples were performed at 370 C. In each case, the tensile test temperature approximately matched the irradiation temperature. To help understand the tensile properties, microstructural samples with similar irradiation history were also examined. The strength and loss of work hardening increase the fastest as a function of irradiation dose for the 12% CW material irradiated at lower temperature. The decrease in ductility with increasing dose occurs more rapidly for the 12% CW material irradiated at lower temperature and the 20% cold-worked material. Post-tensile test fractography indicates that at higher dose, the 20% CW samples begin a shift in fracture mode from purely ductile to mainly small facets and slip bands, suggesting a transition toward channel fracture. The fracture for all of the 12% cold-worked samples was ductile. For both the 12% and 20% CW materials, the yield strength increases correlate with changes in void and loop density and size.« less

  10. Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling

    NASA Astrophysics Data System (ADS)

    Zinszner, Jean-Luc; Erzar, Benjamin; Forquin, Pascal

    2017-01-01

    Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 103 to 104 s-1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual-Forquin-Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones. This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'.

  11. Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling.

    PubMed

    Zinszner, Jean-Luc; Erzar, Benjamin; Forquin, Pascal

    2017-01-28

    Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 10 3 to 10 4  s -1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual-Forquin-Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones.This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'. © 2016 The Author(s).

  12. Computer-assisted recording of tensile tests for the evaluation of serrated flow

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Weinhandl, H.; Mitter, F.; Bernt, W.

    1994-12-01

    In a previous paper the authors pointed out the difficulties which arise in the evaluation of serrated flow curves when the applied tensile strain rates are just above normal''. The recording system of tensile testing machines which were built, say, twenty years ago, are not capable of recording the full size of the load drops due to the inertia of the recording pen. This handicap was then overcome by establishing correction factors which were determined from recording a small number of load drops with an oscilloscope. Modern testing machines are equipped with digital recording. The disadvantage of the common systemmore » is, however, their limited capacity, so that not enough space for data points is available. Consequently, the time intervals between data points are of the order of tenths of seconds. It will become obvious from the present results that such a time interval is too large for recording a correct serration size. This report is concerned with the recording of complete load-extension relations during tensile tests using a computer which is capable of storing the data at sufficiently small time intervals.« less

  13. Acoustic emission monitoring of tensile testing of corroded and un-corroded clad aluminum 2024-T3 and characterization of effects of corrosion on AE source events and material tensile properties

    NASA Astrophysics Data System (ADS)

    Okafor, A. Chukwujekwu; Natarajan, Shridhar

    2014-02-01

    Corrosion damage affects structural integrity and deteriorates material properties of aluminum alloys in aircraft structures. Acoustic Emission (AE) is an effective nondestructive evaluation (NDE) technique for monitoring such damages and predicting failure in large structures of an aircraft. For successful interpretation of data from AE monitoring, sources of AE and factors affecting it need to be identified. This paper presents results of AE monitoring of tensile testing of corroded and un-corroded clad Aluminum 2024-T3 test specimens, and characterization of the effects of strain-rate and corrosion damage on material tensile properties and AE source events. Effect of corrosion was studied by inducing corrosion in the test specimens by accelerated corrosion testing in a Q-Fog accelerated corrosion chamber for 12 weeks. Eight (8) masked dog-bone shaped specimens were placed in the accelerated corrosion chamber at the beginning of the test. Two (2) dog-bone shaped specimens were removed from the corrosion chamber after exposure time of 3, 6, 9, and 12 weeks respectively, and subjected to tension testing till specimen failure along with AE monitoring, as well as two (2) reference samples not exposed to corrosion. Material tensile properties (yield strength, ultimate tensile strength, toughness, and elongation) obtained from tension test and AE parameters obtained from AE monitoring were analyzed and characterized. AE parameters increase with increase in exposure period of the specimens in the corrosive environment. Aluminum 2024-T3 is an acoustically silent material during tensile deformation without any damage. Acoustic emission events increase with increase of corrosion damage and with increase in strain rate above a certain value. Thus AE is suitable for structural health monitoring of corrosion damage. Ultimate tensile strength, toughness and elongation values decrease with increase of exposure period in corrosion chamber.

  14. Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling

    PubMed Central

    Erzar, Benjamin

    2017-01-01

    Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 103 to 104 s−1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual–Forquin–Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’. PMID:27956504

  15. Strain Rate Effect on Tensile Flow Behavior and Anisotropy of a Medium-Manganese TRIP Steel

    NASA Astrophysics Data System (ADS)

    Alturk, Rakan; Hector, Louis G.; Matthew Enloe, C.; Abu-Farha, Fadi; Brown, Tyson W.

    2018-06-01

    The dependence of the plastic anisotropy on the nominal strain rate for a medium-manganese (10 wt.% Mn) transformation-induced plasticity (TRIP) steel with initial austenite volume fraction of 66% (balance ferrite) has been investigated. The material exhibited yield point elongation, propagative instabilities during hardening, and austenite transformation to α'-martensite either directly or through ɛ-martensite. Uniaxial strain rates within the range of 0.005-500 s-1 along the 0°, 45°, and 90° orientations were selected based upon their relevance to automotive applications. The plastic anisotropy ( r) and normal anisotropy ( r n) indices corresponding to each direction and strain rate were determined using strain fields obtained from stereo digital image correlation systems that enabled both quasistatic and dynamic measurements. The results provide evidence of significant, orientation-dependent strain rate effects on both the flow stress and the evolution of r and r n with strain. This has implications not only for material performance during forming but also for the development of future strain-rate-dependent anisotropic yield criteria. Since tensile data alone for the subject medium-manganese TRIP steel do not satisfactorily determine the microstructural mechanisms responsible for the macroscopic-scale behavior observed on tensile testing, additional tests that must supplement the mechanical test results presented herein are discussed.

  16. Strain Rate Effect on Tensile Flow Behavior and Anisotropy of a Medium-Manganese TRIP Steel

    NASA Astrophysics Data System (ADS)

    Alturk, Rakan; Hector, Louis G.; Matthew Enloe, C.; Abu-Farha, Fadi; Brown, Tyson W.

    2018-04-01

    The dependence of the plastic anisotropy on the nominal strain rate for a medium-manganese (10 wt.% Mn) transformation-induced plasticity (TRIP) steel with initial austenite volume fraction of 66% (balance ferrite) has been investigated. The material exhibited yield point elongation, propagative instabilities during hardening, and austenite transformation to α'-martensite either directly or through ɛ-martensite. Uniaxial strain rates within the range of 0.005-500 s-1 along the 0°, 45°, and 90° orientations were selected based upon their relevance to automotive applications. The plastic anisotropy (r) and normal anisotropy (r n) indices corresponding to each direction and strain rate were determined using strain fields obtained from stereo digital image correlation systems that enabled both quasistatic and dynamic measurements. The results provide evidence of significant, orientation-dependent strain rate effects on both the flow stress and the evolution of r and r n with strain. This has implications not only for material performance during forming but also for the development of future strain-rate-dependent anisotropic yield criteria. Since tensile data alone for the subject medium-manganese TRIP steel do not satisfactorily determine the microstructural mechanisms responsible for the macroscopic-scale behavior observed on tensile testing, additional tests that must supplement the mechanical test results presented herein are discussed.

  17. Effect of strain rate and notch geometry on tensile properties and fracture mechanism of creep strength enhanced ferritic P91 steel

    NASA Astrophysics Data System (ADS)

    Pandey, Chandan; Mahapatra, M. M.; Kumar, Pradeep; Saini, N.

    2018-01-01

    Creep strength enhanced ferritic (CSEF) P91 steel were subjected to room temperature tensile test for quasi-static (less than 10-1/s) strain rate by using the Instron Vertical Tensile Testing Machine. Effect of different type of notch geometry, notch depth and angle on mechanical properties were also considered for different strain rate. In quasi-static rates, the P91 steel showed a positive strain rate sensitivity. On the basis of tensile data, fracture toughness of P91 steel was also calculated numerically. For 1 mm notch depth (constant strain rate), notch strength and fracture toughness were found to be increased with increase in notch angle from 45° to 60° while the maximum value attained in U-type notch. Notch angle and notch depth has found a minute effect on P91 steel strength and fracture toughness. The fracture surface morphology was studied by field emission scanning electron microscopy (FESEM).

  18. Elevated Temperature Tensile Tests on DU–10Mo Rolled Foils

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Schulthess, Jason

    2014-09-01

    Tensile mechanical properties for uranium-10 wt.% molybdenum (U–10Mo) foils are required to support modeling and qualification of new monolithic fuel plate designs. It is expected that depleted uranium-10 wt% Mo (DU–10Mo) mechanical behavior is representative of the low enriched U–10Mo to be used in the actual fuel plates, therefore DU-10Mo was studied to simplify material processing, handling, and testing requirements. In this report, tensile testing of DU-10Mo fuel foils prepared using four different thermomechanical processing treatments were conducted to assess the impact of foil fabrication history on resultant tensile properties.

  19. Modified ring stretch tensile testing of Zr-1Nb cladding

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Cohen, A.B.; Majumdar, S.; Ruther, W.E.

    1998-03-01

    In a round robin effort between the US Nuclear Regulatory Commission, Institut de Protection et de Surete Nucleaire in France, and the Russian Research Centre-Kurchatov Institute, Argonne National Laboratory conducted 16 modified ring stretch tensile tests on unirradiated samples of zr-1Nb cladding, which is used in Russian VVER reactors. Test were conducted at two temperatures (25 and 400 C) and two strain rates (0.001 and 1 s{sup {minus}1}). At 25 C and 0.001 s{sup {minus}1}, the yield strength (YS), ultimate tensile strength (UTS), uniform elongation (UE), and total elongation (TE) were 201 MPa, 331 MPa, 18.2%, and 57.6%, respectively. Atmore » 400 C and 0.001 s{sup {minus}1}, the YS, UTS, UE, and TE were 109 MPa, 185 MPa, 15.4%, and 67.7%, respectively. Finally, at 400 C and 1 s{sup {minus}1}, the YS, UTS, UE, and TE were 134 MPa, 189 MPa, 18.9%, and 53.4%, respectively. The high strain rate tests at room temperature were not successful. Test results proved to be very sensitive to the amount of lubrication used on the inserts; because of the large contact area between the inserts and specimen, too little lubrication leads to significantly higher strengths and lower elongations being reported. It is also important to note that only 70 to 80% of the elongation takes place in the gauge section, depending on specimen geometry. The appropriate percentage can be estimated from a simple model or can be calculated from finite-element analysis.« less

  20. A cryogenic tensile testing apparatus for micro-samples cooled by miniature pulse tube cryocooler

    NASA Astrophysics Data System (ADS)

    Chen, L. B.; Liu, S. X.; Gu, K. X.; Zhou, Y.; Wang, J. J.

    2015-12-01

    This paper introduces a cryogenic tensile testing apparatus for micro-samples cooled by a miniature pulse tube cryocooler. At present, tensile tests are widely applied to measure the mechanical properties of materials; most of the cryogenic tensile testing apparatus are designed for samples with standard sizes, while for non-standard size samples, especially for microsamples, the tensile testing cannot be conducted. The general approach to cool down the specimens for tensile testing is by using of liquid nitrogen or liquid helium, which is not convenient: it is difficult to keep the temperature of the specimens at an arbitrary set point precisely, besides, in some occasions, liquid nitrogen, especially liquid helium, is not easily available. To overcome these limitations, a cryogenic tensile testing apparatus cooled by a high frequency pulse tube cryocooler has been designed, built and tested. The operating temperatures of the developed tensile testing apparatus cover from 20 K to room temperature with a controlling precision of ±10 mK. The apparatus configurations, the methods of operation and some cooling performance will be described in this paper.

  1. Method and apparatus for tensile testing of metal foil

    NASA Technical Reports Server (NTRS)

    Wade, O. W. (Inventor)

    1976-01-01

    A method for obtaining accurate and reproducible results in the tensile testing of metal foils in tensile testing machines is described. Before the test specimen are placed in the machine, foil side edges are worked until they are parallel and flaw free. The specimen are also aligned between and secured to grip end members. An aligning apparatus employed in the method is comprised of an alignment box with a longitudinal bottom wall and two upright side walls, first and second removable grip end members at each end of the box, and a means for securing the grip end members within the box.

  2. Novel development of the micro-tensile test at elevated temperature using a test structure with integrated micro-heater

    NASA Astrophysics Data System (ADS)

    Ang, W. C.; Kropelnicki, P.; Soe, Oak; Ling, J. H. L.; Randles, A. B.; Hum, A. J. W.; Tsai, J. M. L.; Tay, A. A. O.; Leong, K. C.; Tan, C. S.

    2012-08-01

    This paper describes the novel development of a micro-tensile testing method that allows testing at elevated temperatures. Instead of using a furnace, a titanium/platinum thin film micro-heater was fabricated on a conventional dog-bone-shaped test structure to heat up its gauge section locally. An infrared (IR) camera with 5 µm resolution was employed to verify the temperature uniformity across the gauge section of the test structure. With this micro-heater-integrated test structure, micro-tensile tests can be performed at elevated temperatures using any conventional tensile testing system without any major modification to the system. In this study, the tensile test of the single crystal silicon (SCS) thin film with (1 0 0) surface orientation and <1 1 0> tensile direction was performed at room temperature and elevated temperatures, up to 300 °C. Experimental results for Young's modulus as a function of temperature are presented. A micro-sized SCS film showed a low dependence of mechanical properties on temperature up to 300 °C.

  3. Testing Tensile and Shear Epoxy Strength at Cryogenic Temperatures

    NASA Technical Reports Server (NTRS)

    Alberts, S. J.; Doehne, C. J.; Johnson, W. L.

    2017-01-01

    This paper covers cryogenic, tensile testing and research completed on a number of epoxies used in cryogenic applications. Epoxies are used in many different applications; however, this research focused on the use of epoxy used to bond MLI standoffs to cryogenic storage tanks and the loads imparted to the tank through the MLI. To conduct testing, samples were made from bare stainless steel, aluminum and primed aluminum. Testing involved slowly cooling test samples with liquid nitrogen then applying gradually increasing tensile loads to the epoxy. The testing evaluated the strength and durability of epoxies at cryogenic temperatures and serves as a base for future testing. The results of the tests showed that some epoxies withstood the harsh conditions while others failed. The two epoxies yielding the best results were Masterbond EP29LPSP and Scotch Weld 2216. For all metal surfaces tested, both epoxies had zero failures for up to 11.81 kg of mass..

  4. Testing Tensile and Shear Epoxy Strength at Cryogenic Temperatures

    NASA Technical Reports Server (NTRS)

    Alberts, S. J.; Doehne, C. J.; Johnson, W. L.

    2017-01-01

    This paper covers cryogenic, tensile testing and research completed on a number of epoxies used in cryogenic applications. Epoxies are used in many different applications; however, this research focused on the use of epoxy used to bond MLI standoffs to cryogenic storage tanks and the loads imparted to the tank through the MLI. To conduct testing, samples were made from bare stainless steel, aluminum and primed aluminum. Testing involved slowly cooling test samples with liquid nitrogen then applying gradually increasing tensile loads to the epoxy. The testing evaluated the strength and durability of epoxies at cryogenic temperatures and serves as a base for future testing. The results of the tests showed that some epoxies withstood the harsh conditions while others failed. The two epoxies yielding the best results were Masterbond EP29LPSP and Scotch Weld 2216. For all metal surfaces tested, both epoxies had zero failures for up to 11.81 kg of mass.

  5. Dynamic Brazilian Test of Rock Under Intermediate Strain Rate: Pendulum Hammer-Driven SHPB Test and Numerical Simulation

    NASA Astrophysics Data System (ADS)

    Zhu, W. C.; Niu, L. L.; Li, S. H.; Xu, Z. H.

    2015-09-01

    The tensile strength of rock subjected to dynamic loading constitutes many engineering applications such as rock drilling and blasting. The dynamic Brazilian test of rock specimens was conducted with the split Hopkinson pressure bar (SHPB) driven by pendulum hammer, in order to determine the indirect tensile strength of rock under an intermediate strain rate ranging from 5.2 to 12.9 s-1, which is achieved when the incident bar is impacted by pendulum hammer with different velocities. The incident wave excited by pendulum hammer is triangular in shape, featuring a long rising time, and it is considered to be helpful for achieving a constant strain rate in the rock specimen. The dynamic indirect tensile strength of rock increases with strain rate. Then, the numerical simulator RFPA-Dynamics, a well-recognized software for simulating the rock failure under dynamic loading, is validated by reproducing the Brazilian test of rock when the incident stress wave retrieved at the incident bar is input as the boundary condition, and then it is employed to study the Brazilian test of rock under the higher strain rate. Based on the numerical simulation, the strain-rate dependency of tensile strength and failure pattern of the Brazilian disc specimen under the intermediate strain rate are numerically simulated, and the associated failure mechanism is clarified. It is deemed that the material heterogeneity should be a reason for the strain-rate dependency of rock.

  6. Tensile and Flexural Test on Kenaf Hybrid Composites

    NASA Astrophysics Data System (ADS)

    Salleh, Z.; Yunus, S.; Masdek, N. R. N. M.; Taib, Y. M.; Azhar, I. I. S.; Hyie, K. M.

    2018-03-01

    The widely use of synthetic materials like carbon and fiberglass in various industries such as automotive and aircraft has lead to human health and environment problems. Therefore, the use of natural fibres such as kenaf has received higher attention as reinforcement. Kenaf or the scientific name is Hibiscus Cannabinus. L is one of the group of Malvecea plant which in the early days, the application of kenaf served only rope and canvas. However, it has more advantages than synthetic materials such as; widely availaible, renewable, lightweight, non-abbrasiveness during processing, high specific strength, free from health hazard and biodegradeable. This study was carried out to investigate the effects of different arrangement of kenaf and fiberglass composites on Young’s Modulus. The material composite was hardened with polyester resin and their properties was characterized. The tensile and the flexural properties is determined using an Instron universal tensile testing machine and carried out by following ASTM D3039 for tensile and ASTM D790 for a flexural test. The experimental program was designed to correlate the flexural and tensile Young’s Modulus of kenaf and fiberglass composite under the same load condition but different arrangement of kenaf and fiberglass on the mold . The resistance to change in shape was described by the behavior and characteristic of the composite materials. The stiffness or the elastic modulus of the composite material was determined at the end of the experiment. The results obtained show that the [±90FG/0/90/90/0/±90FG] kenaf/fiberglass composite arrangement has the highest elastic value.

  7. Tensile and Creep Testing of Sanicro 25 Using Miniature Specimens

    PubMed Central

    Dymáček, Petr; Jarý, Milan; Dobeš, Ferdinand; Kloc, Luboš

    2018-01-01

    Tensile and creep properties of new austenitic steel Sanicro 25 at room temperature and operating temperature 700 °C were investigated by testing on miniature specimens. The results were correlated with testing on conventional specimens. Very good agreement of results was obtained, namely in yield and ultimate strength, as well as short-term creep properties. Although the creep rupture time was found to be systematically shorter and creep ductility lower in the miniature test, the minimum creep rates were comparable. The analysis of the fracture surfaces revealed similar ductile fracture morphology for both specimen geometries. One exception was found in a small area near the miniature specimen edge that was cut by electro discharge machining, where an influence of the steel fracture behavior at elevated temperature was identified. PMID:29337867

  8. The variability of the indirect tensile stripping test.

    DOT National Transportation Integrated Search

    1990-01-01

    The purpose of this investigation was to determine the variability of the Virginia Department of Transportation's (VDOT) indirect tensile stripping test. Five contractor labs and eight VDOT labs participated in the study. Each lab performed three rep...

  9. Impact tensile properties and strength development mechanism of glass for reinforcement fiber

    NASA Astrophysics Data System (ADS)

    Kim, T.; Oshima, K.; Kawada, H.

    2013-07-01

    In this study, impact tensile properties of E-glass were investigated by fiber bundle testing under a high strain rate. The impact tests were performed employing two types of experiments. One is the tension-type split Hopkinson pressure bar system, and the other is the universal high-speed tensile-testing machine. As the results, it was found that not only the tensile strength but also the fracture strain of E-glass fiber improved with the strain rate. The absorbed strain energy of this material significantly increased. It was also found that the degree of the strain rate dependency of E-glass fibers on the tensile strength was varied according to fiber diameter. As for the strain rate dependency of the glass fiber under tensile loading condition, change of the small crack-propagation behaviour was considered to clarify the development of the fiber strength. The tensile fiber strength was estimated by employing the numerical simulation based on the slow crack-growth model (SCG). Through the parametric study against the coefficient of the crack propagation rate, the numerical estimation value was obtained for the various testing conditions. It was concluded that the slow crack-growth behaviour in the glass fiber was an essential for the increase in the strength of this material.

  10. Effect of test temperature and strain rate on the tensile properties of high-strength, high-conductivity copper alloys

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Zinkle, S.J.; Eatherly, W.S.

    1997-04-01

    The unirradiated tensile properties of wrought GlidCop AL25 (ITER grade zero, IGO) solutionized and aged CuCrZr, and cold-worked and aged and solutionized and aged Hycon 3HP{trademark} CuNiBe have been measured over the temperature range of 20-500{degrees}C at strain rates between 4 x 10{sup {minus}4} s{sup {minus}1} and 0.06 s{sup {minus}1}. The measured room temperature electrical conductivity ranged from 64 to 90% IACS for the different alloys. All of the alloys were relatively insensitive to strain rate at room temperature, but the strain rate sensitivity of GlidCop Al25 increased significantly with increasing temperature. The CuNiBe alloys exhibited the best combination ofmore » high strength and high conductivity at room temperature. The strength of CuNiBe decreased slowly with increasing temperature. However, the ductility of CuNiBe decreased rapidly with increasing temperature due to localized deformation near grain boundaries, making these alloy heats unsuitable for typical structural applications above 300{degrees}C. The strength and uniform elongation of GlidCop Al25 decreased significantly with increasing temperature at a strain rate of 1 x 10{sup {minus}3} s{sup {minus}1}, whereas the total elongation was independent of test temperature. The strength and ductility of CuCrZr decreased slowly with increasing temperature.« less

  11. Flow and fracture behavior of aluminum alloy 6082-T6 at different tensile strain rates and triaxialities.

    PubMed

    Chen, Xuanzhen; Peng, Yong; Peng, Shan; Yao, Song; Chen, Chao; Xu, Ping

    2017-01-01

    This study aims to investigate the flow and fracture behavior of aluminum alloy 6082-T6 (AA6082-T6) at different strain rates and triaxialities. Two groups of Charpy impact tests were carried out to further investigate its dynamic impact fracture property. A series of tensile tests and numerical simulations based on finite element analysis (FEA) were performed. Experimental data on smooth specimens under various strain rates ranging from 0.0001~3400 s-1 shows that AA6082-T6 is rather insensitive to strain rates in general. However, clear rate sensitivity was observed in the range of 0.001~1 s-1 while such a characteristic is counteracted by the adiabatic heating of specimens under high strain rates. A Johnson-Cook constitutive model was proposed based on tensile tests at different strain rates. In this study, the average stress triaxiality and equivalent plastic strain at facture obtained from numerical simulations were used for the calibration of J-C fracture model. Both of the J-C constitutive model and fracture model were employed in numerical simulations and the results was compared with experimental results. The calibrated J-C fracture model exhibits higher accuracy than the J-C fracture model obtained by the common method in predicting the fracture behavior of AA6082-T6. Finally, the Scanning Electron Microscope (SEM) of fractured specimens with different initial stress triaxialities were analyzed. The magnified fractographs indicate that high initial stress triaxiality likely results in dimple fracture.

  12. Flow and fracture behavior of aluminum alloy 6082-T6 at different tensile strain rates and triaxialities

    PubMed Central

    Chen, Xuanzhen; Peng, Shan; Yao, Song; Chen, Chao; Xu, Ping

    2017-01-01

    This study aims to investigate the flow and fracture behavior of aluminum alloy 6082-T6 (AA6082-T6) at different strain rates and triaxialities. Two groups of Charpy impact tests were carried out to further investigate its dynamic impact fracture property. A series of tensile tests and numerical simulations based on finite element analysis (FEA) were performed. Experimental data on smooth specimens under various strain rates ranging from 0.0001~3400 s-1 shows that AA6082-T6 is rather insensitive to strain rates in general. However, clear rate sensitivity was observed in the range of 0.001~1 s-1 while such a characteristic is counteracted by the adiabatic heating of specimens under high strain rates. A Johnson-Cook constitutive model was proposed based on tensile tests at different strain rates. In this study, the average stress triaxiality and equivalent plastic strain at facture obtained from numerical simulations were used for the calibration of J-C fracture model. Both of the J-C constitutive model and fracture model were employed in numerical simulations and the results was compared with experimental results. The calibrated J-C fracture model exhibits higher accuracy than the J-C fracture model obtained by the common method in predicting the fracture behavior of AA6082-T6. Finally, the Scanning Electron Microscope (SEM) of fractured specimens with different initial stress triaxialities were analyzed. The magnified fractographs indicate that high initial stress triaxiality likely results in dimple fracture. PMID:28759617

  13. Constitutive modeling of the dynamic-tensile-extrusion test of PTFE

    NASA Astrophysics Data System (ADS)

    Resnyansky, A. D.; Brown, E. N.; Trujillo, C. P.; Gray, G. T.

    2017-01-01

    Use of polymers in defense, aerospace and industrial applications under extreme loading conditions makes prediction of the behavior of these materials very important. Crucial to this is knowledge of the physical damage response in association with phase transformations during loading and the ability to predict this via multi-phase simulation accounting for thermodynamical non-equilibrium and strain rate sensitivity. The current work analyzes Dynamic-Tensile-Extrusion (Dyn-Ten-Ext) experiments on polytetrafluoroethylene (PTFE). In particular, the phase transition during loading and subsequent tension are analyzed using a two-phase rate sensitive material model implemented in the CTH hydrocode. The calculations are compared with experimental high-speed photography. Deformation patterns and their link with changing loading modes are analyzed numerically and correlated to the test observations. It is concluded that the phase transformation is not as critical to the response of PTFE under Dyn-Ten-Ext loading as it is during the Taylor rod impact testing.

  14. Apparatus for tensile testing plate-type ceramic specimens

    DOEpatents

    Liu, Kenneth C.

    1993-01-01

    Apparatus for tensile testing plate-type ceramic specimens having dogbone- or T-shaped end sections without introducing bending stresses in the specimens during the application of a dynamic tensile loading on the specimens is described. A pair of elongated pull rods disposed in a side-by-side relationship are used to grip the shoulders on each T-shaped end section. The pull rods are pivotally attached to a piston-displaceable, disk-shaped member so as to be longitudinally movable with respect to one another effecting the self-alignment thereof with the shoulders on the T-shaped end sections of the specimen to compensate for shoulders being located in different longitudinal positions.

  15. Micro/nano-mechanical test system employing tensile test holder with push-to-pull transformer

    DOEpatents

    Oh, Yunje; Cyrankowski, Edward; Shan, Zhiwei; Asif, Syed Amanula Syed

    2013-05-07

    A micromachined or microelectromechanical system (MEMS) based push-to-pull mechanical transformer for tensile testing of micro-to-nanometer scale material samples including a first structure and a second structure. The second structure is coupled to the first structure by at least one flexible element that enables the second structure to be moveable relative to the first structure, wherein the second structure is disposed relative to the first structure so as to form a pulling gap between the first and second structures such that when an external pushing force is applied to and pushes the second structure in a tensile extension direction a width of the pulling gap increases so as to apply a tensile force to a test sample mounted across the pulling gap between a first sample mounting area on the first structure and a second sample mounting area on the second structure.

  16. Micro/nano-mechanical test system employing tensile test holder with push-to-pull transformer

    DOEpatents

    Oh, Yunje; Cyrankowski, Edward; Shan, Zhiwei; Syed Asif, Syed Amanula

    2014-07-29

    A micromachined or microelectromechanical system (MEMS) based push-to-pull mechanical transformer for tensile testing of micro-to-nanometer scale material samples including a first structure and a second structure. The second structure is coupled to the first structure by at least one flexible element that enables the second structure to be moveable relative to the first structure, wherein the second structure is disposed relative to the first structure so as to form a pulling gap between the first and second structures such that when an external pushing force is applied to and pushes the second structure in a tensile extension direction a width of the pulling gap increases so as to apply a tensile force to a test sample mounted across the pulling gap between a first sample mounting area on the first structure and a second sample mounting area on the second structure.

  17. Apparatus for tensile testing plate-type ceramic specimens

    DOEpatents

    Liu, K.C.

    1993-08-24

    Apparatus is described for gripping a plate-type tensile specimen having generally T-shaped end regions in a dynamic tension fatigue testing apparatus comprising an annular housing having an open-ended elongated cavity therein, a plurality of hydraulic piston means supported by the housing in a spaced array about the cavity, and a specimen-supporting plate means overlying the piston means at one end of the elongated cavity and displaceable by said piston means in a longitudinal direction with respect to the longitudinal axis of the cavity, said apparatus for gripping a flat plate-type tensile specimen comprising: a pair of elongated pull rods each having oppositely disposed first and second end regions; a pair of mounting means carried by said plate means with each mounting means for pivotally attaching the first end region of each of said pull rods in a central region of said plate means for supporting said pair of elongated pull rods in a side-by-side relationship along a common longitudinal centerline within said cavity; recess means in the second end region of each of said pull rods in adjacently disposed surface regions thereof with said recess means facing one another and each adapted to receive one side of one of the generally T-shaped end regions of the plate-type tensile specimen; and load-bearing means positionable in each of said recess means and adapted to bear against a shoulder on each side of the generally T-shaped end region of the plate-type tensile specimen when a tensile loading is applied thereon.

  18. Tensile strength and failure mechanisms of tantalum at extreme strain rates

    NASA Astrophysics Data System (ADS)

    Hahn, Eric; Fensin, Saryu; Germann, Timothy; Meyers, Marc

    Non-equilibrium molecular dynamics simulations are used to probe the tensile response of monocrystalline, bicrystalline, and nanocrystalline tantalum over six orders of magnitude of strain rate. Our analysis of the strain rate dependence of strength is extended to over nine orders of magnitude by bridging the present simulations to recent laser-driven shock experiments. Tensile strength shows a power-law dependence with strain rate over this wide range, with different relationships depending on the initial microstructure and active deformation mechanism. At high strain rates, multiple spall events occur independently and continue to occur until communication occurs by means of relaxation waves. Temperature plays a significant role in the reduction of spall strength as the initial shock required to achieve such large strain rates also contributes to temperature rise, through pressure-volume work as well as visco-plastic heating, which leads to softening and sometimes melting upon release. At ultra-high strain rates, those approaching or exceeding the atomic vibrational frequency, spall strength saturates at the ultimate cohesive strength of the material. UC Research Laboratories Grant (09-LR-06-118456-MEYM); Department of Energy NNSA/SSAP (DE-NA0002080); DOE ASCR Exascale Co-design Center for Materials in Extreme Environments.

  19. Constitutive Modeling of the Dynamic-Tensile-Extrusion Test of PTFE

    NASA Astrophysics Data System (ADS)

    Resnyansky, Anatoly; Brown, Eric; Trujillo, Carl; Gray, George

    2015-06-01

    Use of polymers in the defence, aerospace and industrial application at extreme conditions makes prediction of behaviour of these materials very important. Crucial to this is knowledge of the physical damage response in association with the phase transformations during the loading and the ability to predict this via multi-phase simulation taking the thermodynamical non-equilibrium and strain rate sensitivity into account. The current work analyses Dynamic-Tensile-Extrusion (DTE) experiments on polytetrafluoroethylene (PTFE). In particular, the phase transition during the loading with subsequent tension are analysed using a two-phase rate sensitive material model implemented in the CTH hydrocode and the calculations are compared with experimental high-speed photography. The damage patterns and their link with the change of loading modes are analysed numerically and are correlated to the test observations.

  20. Relationship between surface area for adhesion and tensile bond strength--evaluation of a micro-tensile bond test.

    PubMed

    Sano, H; Shono, T; Sonoda, H; Takatsu, T; Ciucchi, B; Carvalho, R; Pashley, D H

    1994-07-01

    The purpose of this study was to test the null hypothesis that there is no relationship between the bonded surface area of dentin and the tensile strength of adhesive materials. The enamel was removed from the occlusal surface of extracted human third molars, and the entire flat surface was covered with resin composite bonded to the dentin to form a flat resin composite crown. Twenty-four hours later, the bonded specimens were sectioned parallel to the long axis of the tooth into 10-20 thin sections whose upper part was composed of resin composite with the lower half being dentin. These small sections were trimmed using a high speed diamond bur into an hourglass shape with the narrowest portion at the bonded interface. Surface area was varied by altering the specimen thickness and width. Tensile bond strength was measured using custom-made grips in a universal testing machine. Tensile bond strength was inversely related to bonded surface area. At surface areas below 0.4 mm2, the tensile bond strengths were about 55 MPa for Clearfil Liner Bond 2 (Kuraray Co., Ltd.), 38 MPa for Scotchbond MP (3M Dental Products), and 20 MPa for Vitremer (3M Dental Products). At these small surface areas all of the bond failures were adhesive in nature. This new method permits measurement of high bond strengths without cohesive failure of dentin. It also permits multiple measurements to be made within a single tooth.

  1. Effects of Temperature and Strain Rate on Tensile Deformation Behavior of 9Cr-0.5Mo-1.8W-VNb Ferritic Heat-Resistant Steel

    NASA Astrophysics Data System (ADS)

    Guo, Xiaofeng; Weng, Xiaoxiang; Jiang, Yong; Gong, Jianming

    2017-09-01

    A series of uniaxial tensile tests were carried out at different strain rate and different temperatures to investigate the effects of temperature and strain rate on tensile deformation behavior of P92 steel. In the temperature range of 30-700 °C, the variations of flow stress, average work-hardening rate, tensile strength and ductility with temperature all show three temperature regimes. At intermediate temperature, the material exhibited the serrated flow behavior, the peak in flow stress, the maximum in average work-hardening rate, and the abnormal variations in tensile strength and ductility indicates the occurrence of DSA, whereas the sharp decrease in flow stress, average work-hardening rate as well as strength values, and the remarkable increase in ductility values with increasing temperature from 450 to 700 °C imply that dynamic recovery plays a dominant role in this regime. Additionally, for the temperature ranging from 550 to 650 °C, a significant decrease in flow stress values is observed with decreasing in strain rate. This phenomenon suggests the strain rate has a strong influence on flow stress. Based on the experimental results above, an Arrhenius-type constitutive equation is proposed to predict the flow stress.

  2. A novel tensile test method to assess texture and gaping in salmon fillets.

    PubMed

    Ashton, Thomas J; Michie, Ian; Johnston, Ian A

    2010-05-01

    A new tensile strength method was developed to quantify the force required to tear a standardized block of Atlantic salmon muscle with the aim of identifying those samples more prone to factory downgrading as a result of softness and fillet gaping. The new method effectively overcomes problems of sample attachment encountered with previous tensile strength tests. The repeatability and sensitivity and predictability of the new technique were evaluated against other common instrumental texture measurement methods. The relationship between sensory assessments of firmness and parameters from the instrumental texture methods was also determined. Data from the new method were shown to have the strongest correlations with gaping severity (r =-0.514, P < 0.001) and the highest level of repeatability of data when analyzing cold-smoked samples. The Warner Bratzler shear method gave the most repeatable data from fresh samples and had the highest correlations between fresh and smoked product from the same fish (r = 0.811, P < 0.001). A hierarchical cluster analysis placed the tensile test in the top cluster, alongside the Warner Bratzler method, demonstrating that it also yields adequate data with respect to these tests. None of the tested sensory analysis attributes showed significant relationships to mechanical tests except fillet firmness, with correlations (r) of 0.42 for cylinder probe maximum force (P = 0.005) and 0.31 for tensile work (P = 0.04). It was concluded that the tensile test method developed provides an important addition to the available tools for mechanical analysis of salmon quality, particularly with respect to the prediction of gaping during factory processing, which is a serious commercial problem. A novel, reliable method of measuring flesh tensile strength in salmon, provides data of relevance to gaping.

  3. Tensile characterisation of the aorta across quasi-static to blast loading strain rates

    NASA Astrophysics Data System (ADS)

    Magnus, Danyal; Proud, William; Haller, Antoine; Jouffroy, Apolline

    2017-06-01

    The dynamic tensile failure mechanisms of the aorta during Traumatic Aortic Injury (TAI) are poorly understood. In automotive incidents, where the aorta may be under strains of the order of 100/s, TAI is the second largest cause of mortality. In these studies, the proximal descending aorta is the most common site where rupture is observed. In particular, the transverse direction is most commonly affected due to the circumferential orientation of elastin, and hence the literature generally concentrates upon axial samples. This project extends these dynamic studies to the blast loading regime where strain-rates are of the order of 1000/s. A campaign of uniaxial tensile experiments are conducted at quasi-static, intermediate (drop-weight) and high (tensile Split-Hopkinson Pressure Bar) strain rates. In each case, murine and porcine aorta models are considered and the extent of damage assessed post-loading using histology. Experimental data will be compared against current viscoelastic models of the aorta under axial stress. Their applicability across strain rates will be discussed. Using a multi-disciplinary approach, the conditions applied to the samples replicate in vivo conditions, employing a blood simulant-filled tubular specimen surrounded by a physiological solution.

  4. High Strain Rate Testing of Welded DOP-26 Iridium

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Schneibel, J. H.; Miller, R. G.; Carmichael, C. A.

    The iridium alloy DOP-26 is used to produce Clad Vent Set cups that protect the radioactive fuel in radioisotope thermoelectric generators (RTGs) which provide electric power for spacecraft and rovers. In a previous study, the tensile properties of DOP-26 were measured over a wide range of strain rates and temperatures and reported in ORNL/TM-2007/81. While that study established the properties of the base material, the fabrication of the heat sources requires welding, and the mechanical properties of welded DOP-26 have not been extensively characterized in the past. Therefore, this study was undertaken to determine the mechanical properties of DOP-26 specimensmore » containing a transverse weld in the center of their gage sections. Tensile tests were performed at room temperature, 750, 900, and 1090°C and engineering strain rates of 1×10 -3 and 10 s -1. Room temperature testing was performed in air, while testing at elevated temperatures was performed in a vacuum better than 1×10 -4 Torr. The welded specimens had a significantly higher yield stress, by up to a factor of ~2, than the non-welded base material. The yield stress did not depend on the strain rate except at 1090°C, where it was slightly higher for the faster strain rate. The ultimate tensile stress, on the other hand, was significantly higher for the faster strain rate at temperatures of 750°C and above. At 750°C and above, the specimens deformed at 1×10 -3 s -1 showed pronounced necking resulting sometimes in perfect chisel-edge fracture. The specimens deformed at 10 s -1 exhibited this fracture behavior only at the highest test temperature, 1090°C. Fracture occurred usually in the fusion zone of the weld and was, in most cases, primarily intergranular.« less

  5. Finite Element Simulations for Investigating the Effects of Specimen Geometry in Superplastic Tensile Tests

    NASA Astrophysics Data System (ADS)

    Nazzal, Mohammad; Abu-Farha, Fadi; Curtis, Richard

    2011-08-01

    Characterizing the behavior of superplastic materials is largely based on the uniaxial tensile test; yet the unique nature of these materials requires a particularly tailored testing methodology, different to that used with conventional materials. One of the crucial testing facets is the specimen geometry, which has a great impact on the outcome of a superplastic tensile test, as a result of the associated extreme conditions. And while researchers agree that it should take a notably different form than the typical dog-bone shape; there is no universal agreement on the specimen's particular size and dimensions, as evident by the disparities in test specimens used in the various superplastic testing efforts found throughout the literature. In view of that, this article is dedicated to understanding the effects of specimen geometry on the superplastic behavior of the material during tensile testing. Deformation of the Ti6Al4V titanium alloy is FE simulated based on a multitude of specimen geometries, covering a wide range of gauge length, gauge width, grip length, and grip width values. The study provides key insights on the influences of each geometrical parameter as well as their interactions, and provides recommendations on selecting the specimen's proportions for accurate and unified tensile testing of superplastic materials.

  6. Numerical Simulation on the Dynamic Splitting Tensile Test of reinforced concrete

    NASA Astrophysics Data System (ADS)

    Zhao, Zhuan; Jia, Haokai; Jing, Lin

    2018-03-01

    The research for crack resistance was of RC was based on the split Hopkinson bar and numerical simulate software LS-DYNA3D. In the research, the difference of dynamic splitting failure modes between plane concrete and reinforced concrete were completed, and the change rule of tensile stress distribution with reinforcement ratio was studied; also the effect rule with the strain rate and the crack resistance was also discussed by the radial tensile stress time history curve of RC specimen under different loading speeds. The results shows that the reinforcement in the concrete can impede the crack extension, defer the failure time of concrete, increase the tension intensity of concrete; with strain rate of concrete increased, the crack resistance of RC increased.

  7. Extended tensile testing of welded joints of polyethylene pipes

    NASA Astrophysics Data System (ADS)

    Danzanova, E. V.; Gerasimov, A. I.; Botvin, G. V.

    2017-12-01

    The paper introduces the results of testing joints welded in the open air at low climatic temperatures (below minus 15 °C) without heated facilities. Extended tensile testing in an active medium reveals that the same quality standard of welded joints is reached when welded parts are preheated when welding is performed under conditions of low climatic temperatures, and when they are welded at permissible temperatures.

  8. A mechanical system for tensile testing of supported films at the nanoscale.

    PubMed

    Pantano, Maria F; Speranza, G; Galiotis, Costas; Pugno, Nicola M

    2018-06-27

    Standard tensile tests of materials are usually performed on freestanding specimens. However, such requirement is difficult to implement when the materials of interest are of nanoscopic dimensions due to problems related to their handling and manipulation. In the present paper, a new device is presented for tensile testing of thin nanomaterials, which allows tests to be carried out on specimens initially deposited onto a macroscopic pre-notched substrate. On loading, however, no substrate effects are introduced, allowing the films to be freely stretched. The results obtained from a variety of thin metal or polymeric films are very promising for the further development of this technique as a standard method for nanomaterial mechanical testing. © 2018 IOP Publishing Ltd.

  9. Orthodontic brackets removal under shear and tensile bond strength resistance tests - a comparative test between light sources

    NASA Astrophysics Data System (ADS)

    Silva, P. C. G.; Porto-Neto, S. T.; Lizarelli, R. F. Z.; Bagnato, V. S.

    2008-03-01

    We have investigated if a new LEDs system has enough efficient energy to promote efficient shear and tensile bonding strength resistance under standardized tests. LEDs 470 ± 10 nm can be used to photocure composite during bracket fixation. Advantages considering resistance to tensile and shear bonding strength when these systems were used are necessary to justify their clinical use. Forty eight human extracted premolars teeth and two light sources were selected, one halogen lamp and a LEDs system. Brackets for premolar were bonded through composite resin. Samples were submitted to standardized tests. A comparison between used sources under shear bonding strength test, obtained similar results; however, tensile bonding test showed distinct results: a statistical difference at a level of 1% between exposure times (40 and 60 seconds) and even to an interaction between light source and exposure time. The best result was obtained with halogen lamp use by 60 seconds, even during re-bonding; however LEDs system can be used for bonding and re-bonding brackets if power density could be increased.

  10. Assessing the Applicability of Digital Image Correlation (DIC) Technique in Tensile Testing of Fabric Composites

    DTIC Science & Technology

    2013-02-01

    glass composites and 318.51±6.77 MPa for the basalt fibers . On average, the S2 glass composite had a higher modulus of elasticity of 12.94±0.84 GPa...5. The progression of strain on the tool side of the tensile sample. 9 The results of the tensile testing for the basalt fibers are shown in...reported modulus values shown in table 1. Figure 6. Results of the tensile testing of the basalt fiber composites. 3.1.2 Results of the Line

  11. Tensile test of pressureless-sintered silicon nitride at elevated temperature

    NASA Technical Reports Server (NTRS)

    Matsusue, K.; Fujisawa, Y.; Takahara, K.

    1985-01-01

    Uniaxial tensile strength tests of pressureless sintered silicon nitride were carried out in air at temperatures ranging from room temperature up to 1600 C. Silicon nitrides containing Y2O3, Al2O3, Al2O3-MgO, or MgO-CeO2 additives were tested. The results show that the composition of the additive used influences the strength characteristics of the silicon nitride. The tensile strength rapidly decreased at temperatures above 1000 C for the materials containing MgO as the additive and above 1000 C for the material with Y2O3. When the temperature increased to as high as 1300 C, the strength decreased to about 10 percent of the room temperature strength in each case. Observations of the fracture origin and of the crack propagation on the fracture surfaces are discussed.

  12. Stress Wave Attenuation in Aluminum Alloy and Mild Steel Specimens Under SHPB Tensile Testing

    NASA Astrophysics Data System (ADS)

    Pothnis, J. R.; Ravikumar, G.; Arya, H.; Yerramalli, Chandra S.; Naik, N. K.

    2018-02-01

    Investigations on the effect of intensity of incident pressure wave applied through the striker bar on the specimen force histories and stress wave attenuation during split Hopkinson pressure bar (SHPB) tensile testing are presented. Details of the tensile SHPB along with Lagrangian x- t diagram of the setup are included. Studies were carried out on aluminum alloy 7075 T651 and IS 2062 mild steel. While testing specimens using the tensile SHPB setup, it was observed that the force calculated from the transmitter bar strain gauge was smaller than the force obtained from the incident bar strain gauge. This mismatch between the forces in the incident bar and the transmitter bar is explained on the basis of stress wave attenuation in the specimens. A methodology to obtain force histories using the strain gauges on the specimen during SHPB tensile testing is also presented. Further, scanning electron microscope images and photomicrographs are given. Correlation between the microstructure and mechanical properties is explained. Further, uncertainty analysis was conducted to ascertain the accuracy of the results.

  13. Instrumented impact and residual tensile strength testing of eight-ply carbon eopoxy specimens

    NASA Technical Reports Server (NTRS)

    Nettles, A. T.

    1990-01-01

    Instrumented drop weight impact testing was utilized to examine a puncture-type impact on thin carbon-epoxy coupons. Four different material systems with various eight-ply lay-up configurations were tested. Specimens were placed over a 10.3-mm diameter hole and impacted with a smaller tup (4.2-mm diameter) than those used in previous studies. Force-time plots as well as data on absorbed energy and residual tensile strength were gathered and examined. It was found that a critical impact energy level existed for each material tested, at which point tensile strength began to rapidly decrease with increasing impact energy.

  14. Tensile testing method for rare earth based bulk superconductors at liquid nitrogen temperature

    NASA Astrophysics Data System (ADS)

    Kasaba, K.; Katagiri, K.; Murakami, A.; Sato, G.; Sato, T.; Murakami, M.; Sakai, N.; Teshima, H.; Sawamura, M.

    2005-10-01

    Bending tests have been commonly carried out to investigate the mechanical properties of melt-processed rare earth based bulk superconductors. Tensile tests by using small specimen, however, are preferable to evaluate the detailed distribution of the mechanical properties and the intrinsic elastic modulus because no stress distributions exist in the cross-section. In this study, the tensile test method at low temperature by using specimens with the dimensions of 3 × 3 × 4 mm from Y123 and Gd123 bulks was examined. They were glued to Al alloy rods at 400 K by using epoxy resin. Tests were carried out at liquid nitrogen temperature (LNT) by using the immersion type jig. Although the bending strength in the direction perpendicular to the c-axis of the bulks at LNT is higher than that at room temperature (RT), the tensile strength at LNT was lower than that at RT. Many of specimens fractured near the interface between the specimen and the Al alloy rod at LNT. According to the finite element method analysis, it was shown that there was a peak thermal stress in the loading direction near the interface and it was significantly higher at LNT than that at RT. It was also shown that the replacement of the Al alloy rod to Ti rod of which the coefficient of thermal expansion is close to that of bulks significantly increased the tensile strength.

  15. Tensile testing of thin-film microstructures

    NASA Astrophysics Data System (ADS)

    Greek, Staffan; Johansson, Stefan A. I.

    1997-09-01

    The mechanical properties of thin film microstructures depend on size and shape and on the film manufacturing process. Hence, the test structures that are used to measure mechanical properties should have dimensions of the same order of magnitude as an application structure. The microstructures are easily monitored in a scanning electron microscope (SEM), but to be handled and tested in situ a micromanipulator was developed. The parts of the micromanipulator essential to the tests are two independently moveable tables driven by electric motors. The test structures and a testing unit are mounted on the tables. A testing unit was designed to measure force and displacement with high resolution. The testing unit consists of an arm actuated by a piezoelectric element and equipped with a probe. An optical encoder measures the movement of the arm, while strain gauges measure the force in the arm. Test structures consist typically of a released beam fixed at one end with a ring at the other. The micromanipulator is used to position the probe of the testing unit in the ring. The testing unit then executed a tensile test of the beam. Test structures of polysilicon films produced under various process conditions were used to verify the possibility of measuring Young's modulus with an accuracy of +/- 5 percent, as well as fracture strength.Young's modulus is calculated using the difference in elongation for different beam lengths. The fracture strength of the beams was evaluated with Weibull statistics.

  16. Tensile testing grips ensure uniform loading of bimetal tubing specimens

    NASA Technical Reports Server (NTRS)

    Driscol, S. D.; Hunt, V.

    1968-01-01

    Tensile testing grip uniformly distributes stresses to the internal and external tube of bimetal tubing specimens. The grip is comprised of a slotted external tube grip, a slotted internal tube grip, a machine bolt and nut, an internal grip expansion cone, and an external grip compression nut.

  17. A Microsample Tensile Test Application: Local Strength of Impact Welds Between Sheet Metals

    NASA Astrophysics Data System (ADS)

    Benzing, J. T.; He, M.; Vivek, A.; Taber, G. A.; Mills, M. J.; Daehn, G. S.

    2017-03-01

    Microsample tensile testing was conducted to evaluate the quality of impact welds created by vaporizing foil actuator welding. Tensile test samples with a gauge length of 0.6 mm were electro-discharge machined out of welds created between 1-mm-thick aluminum alloy type 6061 (AA6061) sheets and 6-mm-thick copper (Cu110) plates. Aluminum sheets were used as flyers, while copper plates acted as targets. Flyer sheets in T6 as well as T4 temper conditions were utilized to create welds. Some of the welds made with T4 temper flyers were heat treated to a T6 temper. It was found that the welds made with T4 temper flyers were slightly stronger (max. of 270 MPa) than those produced with T6 temper flyers. Generally, failure propagated in a brittle manner across the weld interface; however, elemental mapping reveals material transfer on either member of the welded system. This work proves the feasibility to apply microsample tensile testing to assess impact welding, even when conducted with flyer sheets of 1 mm or less, and provides insight that is complementary to other test methods.

  18. Modifications of system for elevated temperature tensile testing and stress-strain measurement of metal matrix composites

    NASA Technical Reports Server (NTRS)

    Diaz, J. O.

    1985-01-01

    Composites consisting of tungsten alloy wires in superalloy matrices are being studied because they offer the potential for increased strength compared to current materials used at temperatures up to at least 1093 C (2000F). Previous research at the NASA Lewis Research Center and at other laboratories in the U.S., Europe, and Japan has demonstrated laboratory feasibility for fiber reinforced superalloys (FRS). The data for the mechanical and physical properties used to evaluate candidate materials is limited and a need exists for a more detailed and complete data base. The focus of this work is to develop a test procedure to provide a more complete FRS data base to quantitatively evaluate the composite's potential for component applications. This paper will describe and discuss the equipment and procedures under development to obtain elevated temperature tensile stress-strain, strength and modulus data for the first generation of tungsten fiber reinforced superalloy composite (TFRS) materials. Tensile stress-strain tests are conducted using a constant crosshead speed tensile testing machine and a modified load-strain measuring apparatus. Elevated temperature tensile tests are performed using a resistance wound commercial furnace capable of heating test specimens up to 1093 C (2000 F). Tensile stress-strain data are obtained for hollow tubular stainless steel specimens serving as a prototype for future composite specimens.

  19. Effect of Cooling Rate and Chemical Modification on the Tensile Properties of Mg-5wt% Si Alloy

    NASA Astrophysics Data System (ADS)

    Mirshahi, Farshid; Meratian, Mahmood; Zahrani, Mohsen Mohammadi; Zahrani, Ehsan Mohammadi

    Hypereutectic Mg-Si alloys are a new class of light materials usable for aerospace and other advanced engineering applications. In this study, the effects of both cooling rate and bismuth modification on the micro structure and tensile properties of hypereutectic Mg-5wt% Si alloy were investigated. It was found that the addition of 0.5% Bi, altered the morphology of primary Mg2Si particles from bulky to polygonal shape and reduced their mean size from more than 70 μm to about 30 (am. Also, the tensile strength and elongation of the modified alloy increased about 10% and 20%, respectively, which should be ascribed to the modification of Mg2Si morphology and more uniform distribution of the primary particles. Moreover, an increase in tensile strength value with increase in cooling rate were observed which is attributed to finer micro structure of alloy in higher cooling rates. It was observed that Bi addition is significantly more effective in refining the morphology of primary Mg2Si particles than applying faster cooling rates.

  20. Dynamic Tensile Properties of Iron and Steels for a Wide Range of Strain Rates and Strain

    NASA Astrophysics Data System (ADS)

    Kojima, Nobusato; Hayashi, Hiroyuki; Yamamoto, Terumi; Mimura, Koji; Tanimura, Shinji

    The tensile stress-strain curves of iron and a variety of steels, covering a wide range of strength level, over a wide strain rate range on the order of 10-3 ~ 103 s-1, were obtained systematically by using the Sensing Block Type High Speed Material Testing System (SBTS, Saginomiya). Through intensive analysis of these results, the strain rate sensitivity of the flow stress for the large strain region, including the viscous term at high strain rates, the true fracture strength and the true fracture strain were cleared for the material group of the ferrous metals. These systematical data may be useful to develop a practical constitutive model for computer codes, including a fracture criterion for simulations of the dynamic behavior in crash worthiness studies and of work-pieces subjected to dynamic plastic working for a wide strain rate range.

  1. Microstructure and Strain Rate-Dependent Tensile Deformation Behavior of Fiber Laser-Welded Butt Joints of Dual-Phase Steels

    NASA Astrophysics Data System (ADS)

    Liu, Yang; Dong, Danyang; Han, Zhiqiang; Yang, Zhibin; Wang, Lu; Dong, Qingwei

    2018-05-01

    The microstructure and tensile deformation behavior of the fiber laser-welded similar and dissimilar dual-phase (DP) steel joints over a wide range of strain rates from 10-3 to 103 s-1 were investigated for the further applications on the lightweight design of vehicles. The high strain rate dynamic tensile deformation process and full-field strain distribution of the base metals and welded joints were examined using the digital image correlation method and high-speed photography. The strain rate effects on the stress-strain responses, tensile properties, deformation, and fracture behavior of the investigated materials were analyzed. The yield stress (YS) and ultimate tensile strength (UTS) of the dissimilar DP780/DP980 welded joints were lying in-between those of the DP780 and DP980 base metals, and all materials exhibited positive strain rate dependence on the YS and UTS. Owing to the microstructure heterogeneity, the welded joints showed relatively lower ductility in terms of total elongation (TE) than those of the corresponding base metals. The strain localization started before the maximum load was reached, and the strain localization occurred earlier during the whole deformation process with increasing strain rate. As for the dissimilar welded joint, the strain localization tended to occur in the vicinity of the lowest hardness value across the welded joint, which was in the subcritical HAZ at the DP780 side. As the strain rate increased, the typical ductile failure characteristic of the investigated materials did not change.

  2. Microstructure and Strain Rate-Dependent Tensile Deformation Behavior of Fiber Laser-Welded Butt Joints of Dual-Phase Steels

    NASA Astrophysics Data System (ADS)

    Liu, Yang; Dong, Danyang; Han, Zhiqiang; Yang, Zhibin; Wang, Lu; Dong, Qingwei

    2018-04-01

    The microstructure and tensile deformation behavior of the fiber laser-welded similar and dissimilar dual-phase (DP) steel joints over a wide range of strain rates from 10-3 to 103 s-1 were investigated for the further applications on the lightweight design of vehicles. The high strain rate dynamic tensile deformation process and full-field strain distribution of the base metals and welded joints were examined using the digital image correlation method and high-speed photography. The strain rate effects on the stress-strain responses, tensile properties, deformation, and fracture behavior of the investigated materials were analyzed. The yield stress (YS) and ultimate tensile strength (UTS) of the dissimilar DP780/DP980 welded joints were lying in-between those of the DP780 and DP980 base metals, and all materials exhibited positive strain rate dependence on the YS and UTS. Owing to the microstructure heterogeneity, the welded joints showed relatively lower ductility in terms of total elongation (TE) than those of the corresponding base metals. The strain localization started before the maximum load was reached, and the strain localization occurred earlier during the whole deformation process with increasing strain rate. As for the dissimilar welded joint, the strain localization tended to occur in the vicinity of the lowest hardness value across the welded joint, which was in the subcritical HAZ at the DP780 side. As the strain rate increased, the typical ductile failure characteristic of the investigated materials did not change.

  3. A simple cryogenic holder for tensile testing of soft biological tissues.

    PubMed

    Lepetit, J; Favier, R; Grajales, A; Skjervold, P O

    2004-04-01

    To overcome the difficulty of gripping soft biological materials for tensile test, a simple inexpensive cryogenic holder was developed which allows rapid (3 min) preparation of samples. It is made of 6 parts, built in a bakelite cloth, which is an excellent thermal isolant, and is used with rectangular (8x10(-2)x10(-2)x10(-2)m) samples. The holder with the sample inside is completely immersed in liquid nitrogen for 50 s. This duration allows the freezing of the sample ends on a 10(-2)m length and gives a very flat freezing surface throughout the sample cross section. The 6x10(-2)m central part of the sample remained at ambient temperature. Two parts of the holder help maintain the sample until its ends are vertically gripped in the tensile machine thus avoiding any sample deformation during this step. No pressure was applied on the frozen part of the sample by grips of the tensile machine and this avoids breaks in this region. The sample is fixed by adhesion forces (>1 kN) between its frozen parts and 2 pieces of the holder. The procedure has been successfully tested with bovine and salmon muscle samples and results show tensile breaks randomly distributed in the unfrozen region of the samples. Particular attention has been paid to obtain a very flat freezing surface so that the axial strain is equal throughout the sample and therefore any strain-related mechanical parameters can be accurately determined. The dimensions of the holder can be easily modified to fit other sample geometries and can be used with other biological materials.

  4. Optimization and Prediction of Ultimate Tensile Strength in Metal Active Gas Welding.

    PubMed

    Ampaiboon, Anusit; Lasunon, On-Uma; Bubphachot, Bopit

    2015-01-01

    We investigated the effect of welding parameters on ultimate tensile strength of structural steel, ST37-2, welded by Metal Active Gas welding. A fractional factorial design was used for determining the significance of six parameters: wire feed rate, welding voltage, welding speed, travel angle, tip-to-work distance, and shielded gas flow rate. A regression model to predict ultimate tensile strength was developed. Finally, we verified optimization of the process parameters experimentally. We achieved an optimum tensile strength (558 MPa) and wire feed rate, 19 m/min, had the greatest effect, followed by tip-to-work distance, 7 mm, welding speed, 200 mm/min, welding voltage, 30 V, and travel angle, 60°. Shield gas flow rate, 10 L/min, was slightly better but had little effect in the 10-20 L/min range. Tests showed that our regression model was able to predict the ultimate tensile strength within 4%.

  5. Analysis of Factors Influencing Measurement Accuracy of Al Alloy Tensile Test Results

    NASA Astrophysics Data System (ADS)

    Podgornik, Bojan; Žužek, Borut; Sedlaček, Marko; Kevorkijan, Varužan; Hostej, Boris

    2016-02-01

    In order to properly use materials in design, a complete understanding of and information on their mechanical properties, such as yield and ultimate tensile strength must be obtained. Furthermore, as the design of automotive parts is constantly pushed toward higher limits, excessive measuring uncertainty can lead to unexpected premature failure of the component, thus requiring reliable determination of material properties with low uncertainty. The aim of the present work was to evaluate the effect of different metrology factors, including the number of tested samples, specimens machining and surface quality, specimens input diameter, type of testing and human error on the tensile test results and measurement uncertainty when performed on 2xxx series Al alloy. Results show that the most significant contribution to measurement uncertainty comes from the number of samples tested, which can even exceed 1 %. Furthermore, moving from experimental laboratory conditions to very intense industrial environment further amplifies measurement uncertainty, where even if using automated systems human error cannot be neglected.

  6. High strain rate and quasi-static tensile behaviour of Ti-6Al-4V after cyclic damage

    NASA Astrophysics Data System (ADS)

    Galán López, J.; Verleysen, P.; Degrieck, J.

    2012-08-01

    It is common that energy absorbing structural elements are subjected to a number of loading cycles before a crash event. Several studies have shown that previous fatigue can significantly influence the tensile properties of some materials, and hence the behaviour of structural elements made of them. However, when the capacity of absorbing energy of engineering materials is determined, fresh material without any fatigue damage is most often used. This study investigates the effect of fatigue damage on the dynamic tensile properties of Ti-6Al-4V in thin-sheet form. Results are completed with tests at quasi-static strain rates and observations of the fracture surfaces, and compared with results obtained from other alloys and steel grades. The experiments show that the dynamic properties of Ti-6Al-4V are not affected by a number of fatigue loading cycles high enough to significantly reduce the energy absorbing capabilities of EDM machined samples.

  7. A microdynamic version of the tensile test machine

    NASA Technical Reports Server (NTRS)

    Glaser, R. J.

    1991-01-01

    Very large space structures require structural reactions to control forces associated with nanometer-level displacements; JPL has accordingly built a tensile test machine capable of mN-level force measurements and nm-level displacement measurements, with a view to the study of structural linear joining technology at the lower limit of its resolution. The tester is composed of a moving table that is supported by six flexured legs and a test specimen cantilevered off the table to ground. Three vertical legs contain piezoactuators allowing changes in length up to 200 microns while generating axial load and bending moments. Displacements between ground and table are measured by means of three laser-interferometric channels.

  8. Dynamic tensile stress-strain characteristics of carbon/epoxy laminated composites in through-thickness direction

    NASA Astrophysics Data System (ADS)

    Nakai, Kenji; Yokoyama, Takashi

    2015-09-01

    The effect of strain rate up to approximately ɛ˙ = 102/s on the tensile stress-strain properties of unidirectional and cross-ply carbon/epoxy laminated composites in the through-thickness direction is investigated. Waisted cylindrical specimens machined out of the laminated composites in the through-thickness direction are used in both static and dynamic tests. The dynamic tensile stress-strain curves up to fracture are determined using the split Hopkinson bar (SHB). The low and intermediate strain-rate tensile stress-strain relations up to fracture are measured on an Instron 5500R testing machine. It is demonstrated that the ultimate tensile strength and absorbed energy up to fracture increase significantly, while the fracture strain decreases slightly with increasing strain rate. Macro- and micro-scopic examinations reveal a marked difference in the fracture surfaces between the static and dynamic tension specimens.

  9. Design and fabrication of a micron scale free-standing specimen for uniaxial micro-tensile tests

    NASA Astrophysics Data System (ADS)

    Tang, Jun; Wang, Hong; Li, Shi Chen; Liu, Rui; Mao, Sheng Ping; Li, Xue Ping; Zhang, Cong Chun; Ding, Guifu

    2009-10-01

    This paper presents a novel design and fabrication of test chips with a nickel free-standing specimen for the micro uniaxial tensile test. To fabricate test chips on the quartz substrate significantly reduces the fabrication time, minimizes the number of steps and eliminates the effect of the wet anisotropic etching process on mechanical properties. The test chip can be gripped tightly to the test machine and aligned accurately in the pulling direction; furthermore, the approximately straight design of the specimen rather than the traditional dog-bone structure enables the strain be directly measured by a displacement sensor. Both finite-element method (FEM) analysis and experimental results indicate the reliability of the new design. The test chip can also be extended to other materials. The experimental measured Young's modulus of a thin nickel film and the ultimate tensile strength are approximately 94.5 Gpa and 1.76 Gpa, respectively. The results were substantially supported by the experiment on larger gauge specimens by a commercial dynamic mechanical analysis (DMA) instrument. These specimens were electroplated under the same conditions. The low Young's modulus and the high ultimate tensile strength might be explained by the fine grain in the electroplated structure.

  10. Grips for Lightweight Tensile Specimens

    NASA Technical Reports Server (NTRS)

    Witte, William G., Jr.; Gibson, Walter D.

    1987-01-01

    Set of grips developed for tensile testing of lightweight composite materials. Double-wedge design substantially increases gripping force and reduces slippage. Specimen held by grips made of hardened wedges. Assembly screwed into load cell in tensile-testing machine.

  11. A investigation on unixial and quasi-biaxial tensile mechanical properties of aging HTPB propellant under dynamic loading at low temperature

    NASA Astrophysics Data System (ADS)

    Duan, Leiguang; Wang, Guang; Zhang, Guoxing; Sun, Xinya; Shang, Hehao

    2018-06-01

    In order to study the uniaxial and quasi-biaxial mechanical properties of aging solid propellants under low temperature and high strain rate, stress-strain curves and tensile fracture surfaces of HTPB propellant were obtained in a wide range of temperature (-30,25 °C) and strain rates (0.4,4.0 and 14.29 s-1), respectively, by means of uniaxial and biaxial tensile tests and electron microscopy scanning on the fracture cross section. The results indicate that the quasi-biaxial tensile mechanical properties of aging HTPB propellant is same as the uniaxial tensile mechanical properties influenced distinctly by temperature and strain rate. With decreasing temperature and increasing strain rate, the mechanical properties gradually strengthen. The damage for HTPB propellant changes from "dehumidification" to grain fracture. The initial elastic modulus E and maximum tensile stress σ of the uniaxial and biaxial tensile increase gradually with decreasing temperature and increasing strain rate, and well present linear-log function relation with strain rate. The ratio of quasi-biaxial and uniaxial stretching under different loading conditions was obtained so that the researchers could predict the quasi-biaxial tensile mechanical properties of the propellant based on the uniaxial test data.

  12. Tensile properties of nicalon fiber-reinforced carbon following aerospace turbine engine testing

    NASA Astrophysics Data System (ADS)

    Pierce, J. L.; Zawada, L. P.; Srinivasan, R.

    2003-06-01

    The durability of coated Nicalon silicon carbide fiber-reinforced carbon (SiC/C) as the flap and seal exhaust nozzle components in a military aerospace turbine engine was studied. Test specimens machined from both a flap and a seal component were tested for residual strength following extended ground engine testing on a General Electric F414 afterburning turbofan engine. Although small amounts of damage to the protective exterior coating were identified on each component following engine testing, the tensile strengths were equal to the as-fabricated tensile strength of the material. Differences in strength between the two components and variability within the data sets could be traced back to the fabrication process using witness coupon test data from the manufacturer. It was also observed that test specimens machined transversely across the flap and seal components were stronger than those machined along the length. The excellent retained strength of the coated SiC/C material after extended exposure to the severe environment in the afterburner exhaust section of an aerospace turbofan engine has resulted in this material being selected as the baseline material for the F414 exhaust nozzle system.

  13. Mechanical tensile testing of titanium 15-3-3-3 and Kevlar 49 at cryogenic temperatures

    NASA Astrophysics Data System (ADS)

    James, B. L.; Martinez, R. M.; Shirron, P.; Tuttle, J.; Galassi, N. M.; McGuinness, D. S.; Puckett, D.; Francis, J. J.; Flom, Y.

    2012-06-01

    Titanium 15-3-3-3 and Kevlar 49 are highly desired materials for structural components in cryogenic applications due to their low thermal conductivity at low temperatures. Previous tests have indicated that titanium 15-3-3-3 becomes increasingly brittle as the temperature decreases. Furthermore, little is known regarding the mechanical properties of Kevlar 49 at low temperatures, most specifically its Young's modulus. This testing investigates the mechanical properties of both materials at cryogenic temperatures through cryogenic mechanical tensile testing to failure. The elongation, ultimate tensile strength, yield strength, and break strength of both materials are provided and analyzed here.

  14. Mechanical Tensile Testing of Titanium 15-3-3-3 and Kevlar 49 at Cryogenic Temperatures

    NASA Technical Reports Server (NTRS)

    James, Bryan L.; Martinez, Raul M.; Shirron, Peter; Tuttle, Jim; Galassi, Nicholas M.; Mcguinness, Daniel S.; Puckett, David; Francis, John J.; Flom, Yury

    2011-01-01

    Titanium 15-3-3-3 and Kevlar 49 are highly desired materials for structural components in cryogenic applications due to their low thennal conductivity at low temperatures. Previous tests have indicated that titanium 15-3-3-3 becomes increasingly brittle as the temperature decreases. Furthermore, little is known regarding the mechanical properties of Kevlar 49 at low temperatures, most specifically its Young's modulus. This testing investigates the mechanical properties of both materials at cryogenic temperatures through cryogenic mechanical tensile testing to failure. The elongation, ultimate tensile strength, yield strength, and break strength of both materials are provided and analyzed here.

  15. Ten deg off-axis tensile test for intralaminar shear characterization of fiber composites

    NASA Technical Reports Server (NTRS)

    Chamis, C. C.; Sinclair, J. H.

    1976-01-01

    A combined theoretical and experimental investigation was conducted to assess the suitability of the 10 deg off-axis tensile test specimen for the intralaminar shear characterization of unidirectional composites. Composite mechanics, a combined-stress failure criterion, and a finite element analysis were used to determine theoretically the stress-strain variation across the specimen width and the relative stress and strain magnitudes at the 10 deg plane. Strain gages were used to measure the strain variation across the specimen width at specimen midlength and near the end tabs. Specimens from Mod-I/epoxy, T-300/epoxy, and S-glass/epoxy were used in the experimental program. It was found that the 10 deg off-axis tensile test specimen is suitable for intralaminar shear characterization and it is recommended that it should be considered as a possible standard test specimen for such a characterization.

  16. Tensile properties of orthodontic elastomeric ligatures.

    PubMed

    Ahrari, F; Jalaly, T; Zebarjad, M

    2010-01-01

    Tensile properties of elastomeric ligatures become important when efficiency of orthodontic appliances is considered. The aim of this study was to compare tensile strength, extension to tensile strength, toughness and modulus of elasticity of elastomeric ligatures in both the as--received condition and after 28 days of immersion in the simulated oral environment. Furthermore, the changes that occurred in tensile properties of each brand of ligatures after 28 days were evaluated. Experimental-laboratory based. Elastomeric ligatures were obtained from different companies and their tensile properties were measured using Zwick testing machine in both the as-received condition and after 28 days of immersion in the simulated oral environment. The data were analyzed using independent sample t-tests, analysis of variance and Tukey tests. After 28 days, all the ligatures experienced a significant decrease in tensile strength, extension to tensile strength and toughness ( P < 0.05), whereas modulus of elasticity increased in some groups and decreased in others. There were significant differences in tensile properties of different brands of ligatures in both conditions ( P < 0.05), with the exception of modulus of elasticity after 28 days. The decrease in strength properties of elastomeric ligatures shows that they should be replaced at each appointment to reduce the risk of rupture. There are significant differences in tensile properties of different brands of ligatures, which should be considered during selection of these products.

  17. Biaxial tensile tests of the porcine ascending aorta.

    PubMed

    Deplano, Valérie; Boufi, Mourad; Boiron, Olivier; Guivier-Curien, Carine; Alimi, Yves; Bertrand, Eric

    2016-07-05

    One of the aims of this work is to develop an original custom built biaxial set-up to assess mechanical behavior of soft tissues. Stretch controlled biaxial tensile tests are performed and stereoscopic digital image correlation (SDIC) is implemented to measure the 3D components of the generated displacements. Using this experimental device, the main goal is to investigate the mechanical behavior of porcine ascending aorta in the more general context of human ascending aorta pathologies. The results highlight that (i) SDIC arrangement allows accurate assessment of displacements and so stress strain curves, (ii) porcine ascending aorta has a nearly linear and anisotropic mechanical behavior until 30% of strain, (iii) porcine ascending aorta is stiffer in the circumferential direction than in the longitudinal one, (iv) the material coefficient representing the interaction between the two loading directions is thickness dependent, (v) taking into account the variability of the samples the stress values are independent of the stretch rate in the range of values from 10(-3) to 10(-1)s(-1) and finally, (vi) unlike other segments of the aorta, 4-month-old pigs ascending aorta is definitely not a relevant model to investigate the mechanical behavior of the human ascending aorta. Copyright © 2016 Elsevier Ltd. All rights reserved.

  18. Effect of curing and silanizing on composite repair bond strength using an improved micro-tensile test method

    PubMed Central

    Eliasson, Sigfus Thor; Dahl, Jon E.

    2017-01-01

    Abstract Objectives: To evaluate the micro-tensile repair bond strength between aged and new composite, using silane and adhesives that were cured or left uncured when new composite was placed. Methods: Eighty Filtek Supreme XLT composite blocks and four control blocks were stored in water for two weeks and thermo-cycled. Sandpaper ground, etched and rinsed specimens were divided into two experimental groups: A, no further treatment and B, the surface was coated with bis-silane. Each group was divided into subgroups: (1) Adper Scotchbond Multi-Purpose, (2) Adper Scotchbond Multi-Purpose adhesive, (3) Adper Scotchbond Universal, (4) Clearfil SE Bond and (5) One Step Plus. For each adhesive group, the adhesive was (a) cured according to manufacturer’s instructions or (b) not cured before repair. The substrate blocks were repaired with Filtek Supreme XLT. After aging, they were serially sectioned, producing 1.1 × 1.1 mm square test rods. The rods were prepared for tensile testing and tensile strength calculated at fracture. Type of fracture was examined under microscope. Results: Leaving the adhesive uncured prior to composite repair placement increased the mean tensile values statistically significant for all adhesives tested, with or without silane pretreatment. Silane surface treatment improved significantly (p < 0.001) tensile strength values for all adhesives, both for the cured and uncured groups. The mean strength of the control composite was higher than the strongest repair strength (p < 0.001). Conclusions: Application of freshly made silane and a thin bonding layer, rendered higher tensile bond strength. Not curing the adhesive before composite placement increased the tensile bond strength. PMID:28642928

  19. Dependency of Shear Strength on Test Rate in SiC/BSAS Ceramic Matrix Composite at Elevated Temperature

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Bansal, Narottam P.; Gyekenyesi, John P.

    2003-01-01

    Both interlaminar and in-plane shear strengths of a unidirectional Hi-Nicalon(TM) fiber-reinforced barium strontium aluminosilicate (SiC/BSAS) composite were determined at 1100 C in air as a function of test rate using double notch shear test specimens. The composite exhibited a significant effect of test rate on shear strength, regardless of orientation which was either in interlaminar or in in-plane direction, resulting in an appreciable shear-strength degradation of about 50 percent as test rate decreased from 3.3 10(exp -1) mm/s to 3.3 10(exp -5) mm/s. The rate dependency of composite's shear strength was very similar to that of ultimate tensile strength at 1100 C observed in a similar composite (2-D SiC/BSAS) in which tensile strength decreased by about 60 percent when test rate varied from the highest (5 MPa/s) to the lowest (0.005 MPa/s). A phenomenological, power-law slow crack growth formulation was proposed and formulated to account for the rate dependency of shear strength of the composite.

  20. Tensile behaviour of geopolymer-based materials under medium and high strain rates

    NASA Astrophysics Data System (ADS)

    Menna, Costantino; Asprone, Domenico; Forni, Daniele; Roviello, Giuseppina; Ricciotti, Laura; Ferone, Claudio; Bozza, Anna; Prota, Andrea; Cadoni, Ezio

    2015-09-01

    Geopolymers are a promising class of inorganic materials typically obtained from an alluminosilicate source and an alkaline solution, and characterized by an amorphous 3-D framework structure. These materials are particularly attractive for the construction industry due to mechanical and environmental advantages they exhibit compared to conventional systems. Indeed, geopolymer-based concretes represent a challenge for the large scale uses of such a binder material and many research studies currently focus on this topic. However, the behaviour of geopolymers under high dynamic loads is rarely investigated, even though it is of a fundamental concern for the integrity/vulnerability assessment under extreme dynamic events. The present study aims to investigate the effect of high dynamic loading conditions on the tensile behaviour of different geopolymer formulations. The dynamic tests were performed under different strain rates by using a Hydro-pneumatic machine and a modified Hopkinson bar at the DynaMat laboratory of the University of Applied Sciences of Southern Switzerland. The results are processed in terms of stress-strain relationships and strength dynamic increase factor at different strain-rate levels. The dynamic increase factor was also compared with CEB recommendations. The experimental outcomes can be used to assess the constitutive laws of geopolymers under dynamic load conditions and implemented into analytical models.

  1. Mechanical Properties of Transgenic Silkworm Silk Under High Strain Rate Tensile Loading

    NASA Astrophysics Data System (ADS)

    Chu, J.-M.; Claus, B.; Chen, W.

    2017-12-01

    Studies have shown that transgenic silkworm silk may be capable of having similar properties of spider silk while being mass-producible. In this research, the tensile stress-strain response of transgenic silkworm silk fiber is systematically characterized using a quasi-static load frame and a tension Kolsky bar over a range of strain-rates between 10^{-3} and 700/s. The results show that transgenic silkworm silk tends to have higher overall ultimate stress and failure strain at high strain rate (700/s) compared to quasi-static strain rates, indicating rate sensitivity of the material. The failure strain at the high strain rate is higher than that of spider silk. However, the stress levels are significantly below that of spider silk, and far below that of high-performance fiber. Failure surfaces are examined via scanning electron microscopy and reveal that the failure modes are similar to those of spider silk.

  2. Self-Healing Nanofiber-Reinforced Polymer Composites. 1. Tensile Testing and Recovery of Mechanical Properties.

    PubMed

    Lee, Min Wook; An, Seongpil; Jo, Hong Seok; Yoon, Sam S; Yarin, Alexander L

    2015-09-09

    The present work aims at development of self-healing materials capable of partially restoring their mechanical properties under the conditions of prolonged periodic loading and unloading, which is characteristic, for example, of aerospace applications. Composite materials used in these and many other applications frequently reveal multiple defects stemming from their original inhomogeneity, which facilitates microcracking and delamination at ply interfaces. Self-healing nanofiber mats may effectively prevent such damage without compromising material integrity. Two types of core-shell nanofibers were simultaneously electrospun onto the same substrate in order to form a mutually entangled mat. The first type of core-shell fibers consisted of resin monomer (dimethylsiloxane) within the core and polyacrylonitrile within the shell. The second type of core-shell nanofibers consisted of cure (dimethyl-methyl hydrogen-siloxane) within the core and polyacrylonitrile within the shell. These mutually entangled nanofiber mats were used for tensile testing, and they were also encased in polydimethylsiloxane to form composites that were also subsequently subjected to tensile testing. During tensile tests, the nanofibers can be damaged in stretching up to the plastic regime of deformation. Then, the resin monomer and cure was released from the cores and the polydimethylsiloxane resin was polymerized, which might be expected to result in the self-healing properties of these materials. To reveal and evaluate the self-healing properties of the polyacrylonitrile-resin-cure nanofiber mats and their composites, the results were compared to the tensile test results of the monolithic polyacrylonitrile nanofiber mats or composites formed by encasing polyacrylonitrile nanofibers in a polydimethylsiloxane matrix. The latter do not possess self-healing properties, and indeed, do not recover their mechanical characteristics, in contrast to the polyacrylonitrile-resin-cure nanofiber mats and

  3. Localized strain measurements of the intervertebral disc annulus during biaxial tensile testing.

    PubMed

    Karakolis, Thomas; Callaghan, Jack P

    2015-01-01

    Both inter-lamellar and intra-lamellar failures of the annulus have been described as potential modes of disc herniation. Attempts to characterize initial lamellar failure of the annulus have involved tensile testing of small tissue samples. The purpose of this study was to evaluate a method of measuring local surface strains through image analysis of a tensile test conducted on an isolated sample of annular tissue in order to enhance future studies of intervertebral disc failure. An annulus tissue sample was biaxial strained to 10%. High-resolution images captured the tissue surface throughout testing. Three test conditions were evaluated: submerged, non-submerged and marker. Surface strains were calculated for the two non-marker conditions based on motion of virtual tracking points. Tracking algorithm parameters (grid resolution and template size) were varied to determine the effect on estimated strains. Accuracy of point tracking was assessed through a comparison of the non-marker conditions to a condition involving markers placed on tissue surface. Grid resolution had a larger effect on local strain than template size. Average local strain error ranged from 3% to 9.25% and 0.1% to 2.0%, for the non-submerged and submerged conditions, respectively. Local strain estimation has a relatively high potential for error. Submerging the tissue provided superior strain estimates.

  4. Strain transfer through film-substrate interface and surface curvature evolution during a tensile test

    NASA Astrophysics Data System (ADS)

    He, Wei; Han, Meidong; Goudeau, Philippe; Bourhis, Eric Le; Renault, Pierre-Olivier; Wang, Shibin; Li, Lin-an

    2018-03-01

    Uniaxial tensile tests on polyimide-supported thin metal films are performed to respectively study the macroscopic strain transfer through an interface and the surface curvature evolution. With a dual digital image correlation (DIC) system, the strains of the film and the substrate can be simultaneously measured in situ during the tensile test. For the true strains below 2% (far beyond the films' elastic limit), a complete longitudinal strain transfer is present irrespective of the film thickness, residual stresses and microstructure. By means of an optical surface profiler, the three-dimensional (3D) topography of film surface can be obtained during straining. As expected, the profile of the specimen center remains almost flat in the tensile direction. Nevertheless, a relatively significant curvature evolution (of the same order with the initial curvature induced by residual stresses) is observed along the transverse direction as a result of a Poisson's ratio mismatch between the film and the substrate. Furthermore, finite element method (FEM) has been performed to simulate the curvature evolution considering the geometric nonlinearity and the perfect strain transfer at the interface, which agrees well with the experimental results.

  5. Effects of alkanolamide loading on swelling, rheometric and tensile properties of chloroprene rubber compounds

    NASA Astrophysics Data System (ADS)

    Surya, I.; Ismail, H.

    2018-02-01

    The effects of Alkanolamide (ALK) addition on swelling, rheometric and tensile properties of unfilled chloroprene rubber (CR) compounds were investigated. The ALK was prepared from Refined Bleached Deodorized Palm Stearin and diethanolamine and -together with magnesium and zinc oxides- incorporated into the CR compounds. The ALK loadings were 0.5, 1.0, 1.5 and 2.0 phr. It was found that ALK enhanced the cure rate and torque difference of the CR compounds. ALK also enhanced the tensile modulus and tensile strength; especially up to a 1.5 phr loading. The swelling test proved that the 1.5 phr of ALK exhibited the highest degree of crosslink density which caused the highest in tensile modulus and tensile strength.

  6. Method and device for tensile testing of cable bundles

    DOEpatents

    Robertson, Lawrence M; Ardelean, Emil V; Goodding, James C; Babuska, Vit

    2012-10-16

    A standard tensile test device is improved to accurately measure the mechanical properties of stranded cables, ropes, and other composite structures wherein a witness is attached to the top and bottom mounting blocks holding the cable under test. The witness is comprised of two parts: a top and a bottom rod of similar diameter with the bottom rod having a smaller diameter stem on its upper end and the top rod having a hollow opening in its lower end into which the stem fits forming a witness joint. A small gap is present between the top rod and the larger diameter portion of the bottom rod. A standard extensometer is attached to the top and bottom rods of the witness spanning this small witness gap. When a force is applied to separate the mounting blocks, the gap in the witness expands the same length that the entire test specimen is stretched.

  7. Novel approach to tensile testing of micro- and nanoscale fibers

    NASA Astrophysics Data System (ADS)

    Tan, E. P. S.; Lim, C. T.

    2004-08-01

    Due to the strength and size of the micro- and nanoscale fibers, larger conventional universal testing machines are not suitable in performing stretch test of such fibers. Existing microtensile testing machines are custom-made and are complex and expensive to construct. Here, a novel method of using an existing atomic force microscope (AFM)-based nanoindenation system for the tensile testing of microscale or bundled nanoscale fibers is proposed. The microscale poly (L-lactic-co-glycolic acid) fiber (˜25 μm diameter) was used as an example to illustrate this technique. The microfiber was first attached to a nanoindenter tip and the base via a custom-made holder to ensure that the microfiber was taut and vertically aligned. The force transducer of the nanoindenter was used to measure the tensile force required to stretch the microfiber. The microfiber was stretched using the stepper motor of the AFM system. The elongation of the microfiber was measured by subtracting the elongation of the transducer spring from the total elongation of the microfiber and transducer spring. A plot of the load against elongation of the microfiber was then obtained. The stress and strain of the microfiber was measured by subtracting the elongation of the transducer spring from the total elongation of the microfiber was then obtained. The stress and strain of the microfiber was obtained by dividing the load and elongation by cross-sectional area and gauge length, respectively. With this data, the mechanical behavior of the sample at small strains can be studied. This system is able to provide a high load resolution of 80 nN and displacement resolution of 0.5 nm. However, maximum load and sample elongation is limited and handling of the sample still remains a challenge.

  8. Improved Tensile Adhesion Specimens for High Strength Epoxy Systems in Aerospace Applications

    NASA Technical Reports Server (NTRS)

    Haddock, M. Reed; McLennan, Michael L.

    2000-01-01

    An improved tensile adhesion button has been designed and tested that results in higher measured tensile adhesion strength while providing increased capability for testing high strength epoxy adhesive systems. The best attributes of two well-established tensile button designs were combined and refined into an optimized tensile button. The most significant design change to the tensile button was to improve alignment of the bonded tensile button specimens during tensile testing by changing the interface between the tensile button and the tensile test machine. The established or old button design uses a test fixture that pulls from a grooved annulus or anvil head while the new button design pulls from a threaded hole in the centerline of the button. Finite element (FE) analysis showed that asymmetric loading of the established anvil head tensile button significantly increases the stress concentration in the adhesive, causing failure at lower tensile test loads. The new tensile button was designed to eliminate asymmetric loading and eliminate misalignment sensitivity. Enhanced alignment resulted in improved tensile adhesion strength measurement up to 13.8 MPa (2000psi) over the established button design. Another design change increased the capability of the button by increasing the threaded hole diameter allowing it to test high strength epoxy systems up to 85 MPa(less than 12,000 psi). The improved tensile button can be used in button- to-button or button-to-panel configurations.

  9. Seismic, creep, and tensile testing of various epoxy bonded rebar products in hardened concrete.

    DOT National Transportation Integrated Search

    2007-02-01

    The objective of this project was to evaluate the performance of currently specified epoxy adhesive anchor systems on various epoxy-coated rebar under seismic, creep and tensile loading. Previous testing of dowel bonding materials for use in hardened...

  10. Seismic, creep, and tensile testing of various epoxy bonded rebar products in hardened concrete.

    DOT National Transportation Integrated Search

    2007-01-01

    The objective of this project was to evaluate the performance of currently specified epoxy adhesive : anchor systems on various epoxy-coated rebar under seismic, creep and tensile loading. Previous testing of : dowel bonding materials for use in hard...

  11. Seismic, creep, and tensile testing of various epoxy bonded rebar products in hardened concrete.

    DOT National Transportation Integrated Search

    2006-02-01

    The objective of this project was to evaluate the performance of currently specified epoxy adhesive : anchor systems on various epoxy-coated rebar under seismic, creep and tensile loading. Previous testing of : dowel bonding materials for use in hard...

  12. A novel approach for preparation and in situ tensile testing of silica glass membranes in the TEM

    NASA Astrophysics Data System (ADS)

    Mačković, Mirza; Przybilla, Thomas; Dieker, Christel; Herre, Patrick; Romeis, Stefan; Stara, Hana; Schrenker, Nadine; Peukert, Wolfgang; Spiecker, Erdmann

    2017-04-01

    The mechanical behavior of glasses in the micro- and/or nanometer regime increasingly gains importance in nowadays modern technology. However, suitable small scale preparation and mechanical testing approaches for a reliable assessment of the mechanical properties of glasses still remain a big challenge. In the present work, a novel approach for site-specific preparation and quantitative in situ tensile testing of thin silica glass membranes in the transmission electron microscope is presented. Thereby, advanced focused ion beam techniques are used for the preparation of nanoscale dog bone shaped silica glass specimens suitable for in situ tensile testing. Small amounts of gallium are detected on the surface of the membranes resulting from redeposition effects during the focused ion beam preparation procedure. Possible structural changes of silica glass upon irradiation with electrons and gallium ions are investigated by controlled irradiation experiments, followed by a structural analysis using Raman spectroscopy. While moderate electron beam irradiation does not alter the structure of silica glass, ion beam irradiation results in minor densification of the silica glass membranes. In situ tensile testing of membranes under electron beam irradiation results in distinctive elongations without fracture confirming the phenomenon of superplasticity. In contrast, in situ tensile testing in the absence of the electron beam reveals an elastic/plastic deformation behavior, and finally leads to fracture of the membranes. The Young’s moduli of the glass membranes pulled at beam off conditions in the TEM are comparable with values known for bulk fused silica, while the tensile strength is in the range of values reported for silica glass fibers with comparable dimensions. The impact of electron beam irradiation on the mechanical properties of silica glass membranes is further discussed. The results of the present work open new avenues for dedicated preparation and

  13. Semi-analytical and Numerical Studies on the Flattened Brazilian Splitting Test Used for Measuring the Indirect Tensile Strength of Rocks

    NASA Astrophysics Data System (ADS)

    Huang, Y. G.; Wang, L. G.; Lu, Y. L.; Chen, J. R.; Zhang, J. H.

    2015-09-01

    Based on the two-dimensional elasticity theory, this study established a mechanical model under chordally opposing distributed compressive loads, in order to perfect the theoretical foundation of the flattened Brazilian splitting test used for measuring the indirect tensile strength of rocks. The stress superposition method was used to obtain the approximate analytic solutions of stress components inside the flattened Brazilian disk. These analytic solutions were then verified through a comparison with the numerical results of the finite element method (FEM). Based on the theoretical derivation, this research carried out a contrastive study on the effect of the flattened loading angles on the stress value and stress concentration degree inside the disk. The results showed that the stress concentration degree near the loading point and the ratio of compressive/tensile stress inside the disk dramatically decreased as the flattened loading angle increased, avoiding the crushing failure near-loading point of Brazilian disk specimens. However, only the tensile stress value and the tensile region were slightly reduced with the increase of the flattened loading angle. Furthermore, this study found that the optimal flattened loading angle was 20°-30°; flattened load angles that were too large or too small made it difficult to guarantee the central tensile splitting failure principle of the Brazilian splitting test. According to the Griffith strength failure criterion, the calculative formula of the indirect tensile strength of rocks was derived theoretically. This study obtained a theoretical indirect tensile strength that closely coincided with existing and experimental results. Finally, this paper simulated the fracture evolution process of rocks under different loading angles through the use of the finite element numerical software ANSYS. The modeling results showed that the Flattened Brazilian Splitting Test using the optimal loading angle could guarantee the tensile

  14. Mechanical behavior and failure analysis of prosthetic retaining screws after long-term use in vivo. Part 3: Preload and tensile fracture load testing.

    PubMed

    Al Jabbari, Youssef S; Fournelle, Raymond; Ziebert, Gerald; Toth, Jeffrey; Iacopino, Anthony M

    2008-04-01

    The aim of this study was to determine the preload and tensile fracture load values of prosthetic retaining screws after long-term use in vivo compared to unused screws (controls). Additionally, the investigation addressed whether the preload and fracture load values of prosthetic retaining screws reported by the manufacturer become altered after long-term use in vivo. For preload testing, 10 new screws (controls) from Nobel Biocare (NB) and 73 used retaining screws [58 from NB and 15 from Sterngold (SG)] were subjected to preload testing. For tensile testing, eight controls from NB and 58 used retaining screws (46 from NB and 12 from SG) were subjected to tensile testing. Used screws for both tests were in service for 18-120 months. A custom load frame, load cell, and torque wrench setup were used for preload testing. All 83 prosthetic screws were torqued once to 10 Ncm, and the produced preload value was recorded (N) using an X-Y plotter. Tensile testing was performed on a universal testing machine and the resulting tensile fracture load value was recorded (N). Preload and tensile fracture load values were analyzed with 2-way ANOVA and Tukey post-hoc tests. There was a significant difference between preload values for screws from NB and screws from SG (p < 0.001). The preload values for gold alloy screws from NB decreased as the number of years in service increased. There was a significant difference between tensile fracture values for the three groups (gold alloy screws from NB and SG and palladium alloy screws from NB) at p < 0.001. The tensile fracture values for gold alloy screws from NB and SG decreased as the number of years in service increased. In fixed detachable hybrid prostheses, perhaps as a result of galling, the intended preload values of prosthetic retaining screws may decrease with increased in-service time. The reduction of the fracture load value may be related to the increase of in-service time; however, the actual determination of this

  15. Direct comparison of nanoindentation and tensile test results on reactor-irradiated materials

    DOE PAGES

    Krumweide, David L; Yamamoto, Takuya; Saleh, Tarik A.; ...

    2018-03-13

    Nanoindentation testing has been used for decades to assess materials on a local scale and to obtain fundamental mechanical property parameters. Nuclear materials research often faces the challenge of testing rather small samples due to the hazardous nature, limited space in reactors, and shallow ion-irradiated zones, fostering the need for small-scale mechanical testing (SSMT). As such, correlating the results from SSMT to bulk properties is particularly of interest. Here, this study compares macroscopic tensile test data (yield and flow stresses) to nanoindentation data (hardness) obtained on a number of different neutron-irradiated materials in order to understand the scaling behavior onmore » radiation-damaged samples.« less

  16. Direct comparison of nanoindentation and tensile test results on reactor-irradiated materials

    NASA Astrophysics Data System (ADS)

    Krumwiede, D. L.; Yamamoto, T.; Saleh, T. A.; Maloy, S. A.; Odette, G. R.; Hosemann, P.

    2018-06-01

    Nanoindentation testing has been used for decades to assess materials on a local scale and to obtain fundamental mechanical property parameters. Nuclear materials research often faces the challenge of testing rather small samples due to the hazardous nature, limited space in reactors, and shallow ion-irradiated zones, fostering the need for small-scale mechanical testing (SSMT). As such, correlating the results from SSMT to bulk properties is particularly of interest. This study compares macroscopic tensile test data (yield and flow stresses) to nanoindentation data (hardness) obtained on a number of different neutron-irradiated materials in order to understand the scaling behavior on radiation-damaged samples.

  17. Direct comparison of nanoindentation and tensile test results on reactor-irradiated materials

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Krumweide, David L; Yamamoto, Takuya; Saleh, Tarik A.

    Nanoindentation testing has been used for decades to assess materials on a local scale and to obtain fundamental mechanical property parameters. Nuclear materials research often faces the challenge of testing rather small samples due to the hazardous nature, limited space in reactors, and shallow ion-irradiated zones, fostering the need for small-scale mechanical testing (SSMT). As such, correlating the results from SSMT to bulk properties is particularly of interest. Here, this study compares macroscopic tensile test data (yield and flow stresses) to nanoindentation data (hardness) obtained on a number of different neutron-irradiated materials in order to understand the scaling behavior onmore » radiation-damaged samples.« less

  18. Study of austenitic stainless steel welded with low alloy steel filler metal. [tensile and impact strength tests

    NASA Technical Reports Server (NTRS)

    Burns, F. A.; Dyke, R. A., Jr.

    1979-01-01

    The tensile and impact strength properties of 316L stainless steel plate welded with low alloy steel filler metal were determined. Tests were conducted at room temperature and -100 F on standard test specimens machined from as-welded panels of various chemical compositions. No significant differences were found as the result of variations in percentage chemical composition on the impact and tensile test results. The weldments containing lower chromium and nickel as the result of dilution of parent metal from the use of the low alloy steel filler metal corroded more severely in a marine environment. The use of a protective finish, i.e., a nitrile-based paint containing aluminum powder, prevented the corrosive attack.

  19. Effect of Strengthening Mechanism on Strain-Rate Related Tensile Properties of Low-Carbon Sheet Steels for Automotive Application

    NASA Astrophysics Data System (ADS)

    Das, Anindya; Biswas, Pinaki; Tarafder, S.; Chakrabarti, D.; Sivaprasad, S.

    2018-05-01

    In order to ensure crash resistance of the steels used in automotive components, the ensile deformation behavior needs to be studied and predicted not only under quasi-static condition, but also under dynamic loading rates. In the present study, tensile tests have been performed on four different automobile grade sheet steels, namely interstitial free steel, dual-phase 600 and 800, and a carbon manganese steel over the strain rate regime of 0.001-800/s. Apart from the variation in strength (which always increased with strain rate), the effect of strengthening mechanism on strain rate sensitivity and strain hardening behavior has been evaluated. Strain rate sensitivity was found to increase at high-strain rate regime for all the steels. Contribution of solid solution hardening on strain rate sensitivity at lower plastic strains was found to be higher compared to dislocation strengthening and second-phase hardening. However, precipitation hardening coupled with solid solution hardening produced the highest strain rate sensitivity, in C-Mn-440 steel at high strain rates. Different strain-rate-sensitive models which take into account the change in yield stress and strain hardening behavior with strain rate for ductile materials were used to predict the flow behavior of these sheet steels at strain rates up to 800/s.

  20. Tensile properties of AZ11A-0 magnesium-alloy sheet under rapid-heating and constant temperature

    NASA Technical Reports Server (NTRS)

    Kurg, Ivo M

    1956-01-01

    Specimens of AZ31A-0 magnesium alloy sheet were heated to rupture at nominal rates of 0.2 F to 100 F per second under constant tensile load conditions. The data are presented and compared with the results of conventional tensile stress-strain tests at elevated temperatures after 1.2-hour exposure. A temperature-rate parameter was used to construct master curves from which stresses and temperatures for yield and rupture can be predicted under rapid-heating conditions. A comparison of the elevated-temperature tensile properties of AZ31A-0 and HK31XA-H24 magnesium-alloy sheet under both constant-temperature and rapid-heating conditions is included.

  1. A new tensile impact test for the toughness characterization of sheet material

    NASA Astrophysics Data System (ADS)

    Könemann, Markus; Lenz, David; Brinnel, Victoria; Münstermann, Sebastian

    2018-05-01

    In the past, the selection of suitable steels has been carried out primarily based on the mechanical properties of different steels. One of these properties is the resistance against crack propagation. For many constructions, this value plays an important role, because it can compare the impact toughness of different steel grades easily and gives information about the loading capacity of the specific materials. For thin sheets, impact toughness properties were usually not considered. One of the reasons for this is that the Charpy-impact test is not applicable for sheets with thicknesses below 2 mm. For a long time, this was not relevant because conventional steels had a sufficient impact toughness in a wide temperature range. However, since new multiphase steel grades with improved mechanical property exploitations are available, it turned out that impact toughness properties need to be considered during the component design phase, as the activation of the cleavage fracture mechanism is observed under challenging loading conditions. Therefore, this work aims to provide a new and practical testing procedure for sheet material or thin walled structures. The new testing procedure is based on tensile tests conducted in an impact pendulum similar to the Charpy impact hammer. A new standard geometry is provided, which enables a comparison between different steels or steel grades. A connection to the conventional Charpy test is presented using a damage mechanics model, which predicts material failure with consideration of to the stress state at various temperatures. Different specimen geometries are analysed to cover manifold stress states. A special advantage of the damage mechanics model is also the possibility to predict the materials behaviour in the transition area. To verify the method a conventional steel was tested in Charpy tests as well as in the new tensile impact test.

  2. Reliability design and assessment of a micro-probe using the results of a tensile test of a beryllium-copper alloy thin film

    NASA Astrophysics Data System (ADS)

    Park, Jun-Hyub; Shin, Myung-Soo

    2011-09-01

    This paper describes the results of tensile tests for a beryllium-copper (BeCu) alloy thin film and the application of the results to the design of a probe. The copper alloy films were fabricated by electroplating. To obtain the tensile characteristics of the film, the dog-bone type specimen was fabricated by the etching method. The tensile tests were performed with the specimen using a test machine developed by the authors. The BeCu alloy has an elastic modulus of 119 GPa and the 0.2% offset yield and ultimate tensile strengths of 1078 MPa and 1108 MPa, respectively. The design and manufacture of a smaller probe require higher pad density and smaller pad-pitch chips. It should be effective in high-frequency testing. For the design of a new micro-probe, we investigated several design parameters that may cause problems, such as the contact force and life, using the tensile properties and the design of experiment method in conjunction with finite element analysis. The optimal dimensions of the probe were found using the response surface method. The probe with optimal dimensions was manufactured by a precision press process. It was verified that the manufactured probe satisfied the life, the contact force and the over drive through the compression tests and the life tests of the probes.

  3. Direct Shear Tests of Sandstone Under Constant Normal Tensile Stress Condition Using a Simple Auxiliary Device

    NASA Astrophysics Data System (ADS)

    Cen, Duofeng; Huang, Da

    2017-06-01

    Tension-shear failure is a typical failure mode in the rock masses in unloading zones induced by excavation or river incision, etc., such as in excavation-disturbed zone of deep underground caverns and superficial rocks of high steep slopes. However, almost all the current shear failure criteria for rock are usually derived on the basis of compression-shear failure. This paper proposes a simple device for use with a servo-controlled compression-shear testing machine to conduct the tension-shear tests of cuboid rock specimens, to test the direct shear behavior of sandstone under different constant normal tensile stress conditions ( σ = -1, -1.5, -2, -2.5 and -3 MPa) as well as the uniaxial tension behavior. Generally, the fracture surface roughness decreases and the proportion of comminution areas in fracture surface increases as the change of stress state from tension to tension-shear and to compression-shear. Stepped fracture is a primary fracture pattern in the tension-shear tests. The shear stiffness, shear deformation and normal deformation (except the normal deformation for σ = -1 MPa) decrease during shearing, while the total normal deformation containing the pre-shearing portion increases as the normal tensile stress level (| σ|) goes up. Shear strength is more sensitive to the normal tensile stress than to the normal compressive stress, and the power function failure criterion (or Mohr envelope form of Hoek-Brown criterion) is examined to be the optimal criterion for the tested sandstone in the full region of tested normal stress in this study.

  4. Method and apparatus for determining tensile strength

    DOEpatents

    Ratigan, J.L.

    1982-05-28

    A method and apparatus is described for determining the statistical distribution of apparent tensile strength of rock, the size effect with respect to tensile strength, as well as apparent deformation modulus of both intact and fractured or jointed rock. The method is carried out by inserting a plug of deformable material, such as rubber, in an opening of a specimen to be tested. The deformable material is loaded by an upper and lower platen until the specimen ruptures, whereafter the tensile strength is calculated based on the parameters of the test specimen and apparatus.

  5. Method and apparatus for determining tensile strength

    DOEpatents

    Ratigan, Joe L.

    1984-01-01

    A method and apparatus for determining the statistical distribution of apparent tensile strength of rock, the size effect with respect to tensile strength, as well as apparent deformation modulus of both intact and fractured or jointed rock. The method is carried out by inserting a plug of deformable material, such as rubber, in an opening of a specimen to be tested. The deformable material is loaded by an upper and lower platen until the specimen ruptures, whereafter the tensile strength is calculated based on the parameters of the test specimen and apparatus.

  6. Design and construction of a tensile tester for the testing of simple composites

    NASA Technical Reports Server (NTRS)

    Borst, Mark A.; Spiegel, F. Xavier

    1994-01-01

    The following is a design for a tensile tester which will be used to test the tensile strength and anisotropic properties of simple composites. These simple composites are suspected to be anisotropic primarily in a single plane. When the composites undergo a tensile force, they will undergo deformation, causing movement either to the left or right. The composites are suspect due to their method of construction. Each sample has a single layer of unidirectional continuous fibers embedded in a rubbery resin. It has been well established that a serious limitation of unidirectional fiber composites is the very large in-plane anisotropy. The design presented here incorporates a single degree of freedom such that distortion (to the left or right) due to anisotropic tendencies may be measured. The device will spend the vast majority of its time in an undergraduate materials lab. As a result, ease of use and durability are valued more highly than research grade accuracy. Additional concerns focus on the fact that this machine will be built as a student project. Issues which are dealt with during this design include: specimen configuration or shape; a method of applying consistent, linear tension force; a method of gripping specimen without affecting its overall properties; a method of collecting data; repeatability of data; ease of use; ease of construction; and cost. After the device has been constructed, it will be used to test the simple composites which were fabricated in house. A comparison will be made between composites manufactured using aluminum screening as the strengthening fibers and those manufactured using fiberglass screening.

  7. Analysis of AISI 304 Tensile Strength as an Anchor Chain of Mooring System

    NASA Astrophysics Data System (ADS)

    Hamidah, I.; Wati, R.; Hamdani, R. A.

    2018-05-01

    The background of this research is the use of mild steel (i.e., St37) as anchor chain that works on the corrosive environment of seawater which is possible to decrease its tensile strength. The longer soaked in seawater, the more significant the lowering of its tensile strength. Anchor chain needs to be designed by considering its tensile strength and corrosion resistance, so it’s able to support mooring system well. The primary purpose of this research is obtaining the decreasing of stainless steel 304 (AISI 304) tensile strength which is corroded by seawater as anchor chain of the mooring system. It is also essential to obtain the lifetime of AISI304 and St37 as anchor chain with the same load, the corrosion rate of AISI 304, and St 37 in seawater. The method which was employed in this research is an experiment with four pieces of stainless steel AISI 304, and of St 37 corrosion testing samples, six pieces of stainless steel 304, and six pieces of St 37 for tensile testing samples. The result of this research shows that seawater caused stainless steel AISI 304 as anchor chain has decreased of tensile strength about 1.68 % during four weeks. Also, it indicates that AISI 304 as anchor chain has a lifetime about 130 times longer than St 37. Further, we found that the corrosion rate of stainless steel 304 in seawater is 0.2042 mpy in outstanding category, while the St 37 samples reached up to 27.0247 mpy ranked as fair category. This result recommends that AISI 304 more excellence than St 37 as anchor chain of the mooring system.

  8. Modeling the biomechanical and injury response of human liver parenchyma under tensile loading.

    PubMed

    Untaroiu, Costin D; Lu, Yuan-Chiao; Siripurapu, Sundeep K; Kemper, Andrew R

    2015-01-01

    The rapid advancement in computational power has made human finite element (FE) models one of the most efficient tools for assessing the risk of abdominal injuries in a crash event. In this study, specimen-specific FE models were employed to quantify material and failure properties of human liver parenchyma using a FE optimization approach. Uniaxial tensile tests were performed on 34 parenchyma coupon specimens prepared from two fresh human livers. Each specimen was tested to failure at one of four loading rates (0.01s(-1), 0.1s(-1), 1s(-1), and 10s(-1)) to investigate the effects of rate dependency on the biomechanical and failure response of liver parenchyma. Each test was simulated by prescribing the end displacements of specimen-specific FE models based on the corresponding test data. The parameters of a first-order Ogden material model were identified for each specimen by a FE optimization approach while simulating the pre-tear loading region. The mean material model parameters were then determined for each loading rate from the characteristic averages of the stress-strain curves, and a stochastic optimization approach was utilized to determine the standard deviations of the material model parameters. A hyperelastic material model using a tabulated formulation for rate effects showed good predictions in terms of tensile material properties of human liver parenchyma. Furthermore, the tissue tearing was numerically simulated using a cohesive zone modeling (CZM) approach. A layer of cohesive elements was added at the failure location, and the CZM parameters were identified by fitting the post-tear force-time history recorded in each test. The results show that the proposed approach is able to capture both the biomechanical and failure response, and accurately model the overall force-deflection response of liver parenchyma over a large range of tensile loadings rates. Copyright © 2014 Elsevier Ltd. All rights reserved.

  9. Tensile and Compressive Constitutive Response of 316 Stainless Steel at Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Manson, S. S.; Muralidharan, U.; Halford, G. R.

    1983-01-01

    Creep rate in compression is lower by factors of 2 to 10 than in tension if the microstructure of the two specimens is the same and are tested at equal temperatures and equal but opposite stresses. Such behavior is characteristic for monotonic creep and conditions involving cyclic creep. In the latter case creep rate in both tension and compression progressively increases from cycle to cycle, rendering questionable the possibility of expressing a time stabilized constitutive relationship. The difference in creep rates in tension and compression is considerably reduced if the tension specimen is first subjected to cycles of tensile creep (reversed by compressive plasticity), while the compression specimen is first subjected to cycles of compressive creep (reversed by tensile plasticity). In both cases, the test temperature is the same and the stresses are equal and opposite. Such reduction is a reflection of differences in microstructure of the specimens resulting from different prior mechanical history.

  10. Tensile and compressive constitutive response of 316 stainless steel at elevated temperatures

    NASA Technical Reports Server (NTRS)

    Manson, S. S.; Muralidharan, U.; Halford, G. R.

    1982-01-01

    It is demonstrated that creep rate of 316 SS is lower by factors of 2 to 10 in compression than in tension if the microstructure is the same and tests are conducted at identical temperatures and equal but opposite stresses. Such behavior was observed for both monotonic creep and conditions involving cyclic creep. In the latter case creep rate in both tension and compression progressively increases from cycle to cycle, rendering questionable the possibility of expressing a time-stabilized constitutive relationship. The difference in creep rates in tension and compression is considerably reduced if the tension specimen is first subjected to cycles of tensile creep (reversed by compressive plasticity), while the compression specimen is first subjected to cycles of compressive creep (reversed by tensile plasticity). In both cases, the test temperature is the same and the stresses are equal and opposite. Such reduction is a reflection of differences in microstructure of the specimens resulting from different prior mechanical history.

  11. The deformation behavior and microstructure evolution of duplex Mg-9Li-1Al alloy during superplasticity tensile testing

    NASA Astrophysics Data System (ADS)

    Liu, Meiduo; Zheng, Haipeng; Zhang, Tianlong; Wu, Ruizhi

    2017-12-01

    The superplastic mechanical properties and microstructure evolution of the duplex Mg-9Li-1Al alloy were investigated. The tensile testing results show that, the elongation of the as-extruded Mg-9Li-1Al alloy reaches 510% at 573 K with a strain rate of 2×10-4 s-1. During the deformation process, the strips of α phase break into equiaxed structure. This phenomenon can be attributed to a particular dynamic recrystallization, which suggests that the β phase can recrystallize in the α phase due to the small misfit degree between α phase and β phase.

  12. Computational Simulation of the High Strain Rate Tensile Response of Polymer Matrix Composites

    NASA Technical Reports Server (NTRS)

    Goldberg, Robert K.

    2002-01-01

    A research program is underway to develop strain rate dependent deformation and failure models for the analysis of polymer matrix composites subject to high strain rate impact loads. Under these types of loading conditions, the material response can be highly strain rate dependent and nonlinear. State variable constitutive equations based on a viscoplasticity approach have been developed to model the deformation of the polymer matrix. The constitutive equations are then combined with a mechanics of materials based micromechanics model which utilizes fiber substructuring to predict the effective mechanical and thermal response of the composite. To verify the analytical model, tensile stress-strain curves are predicted for a representative composite over strain rates ranging from around 1 x 10(exp -5)/sec to approximately 400/sec. The analytical predictions compare favorably to experimentally obtained values both qualitatively and quantitatively. Effective elastic and thermal constants are predicted for another composite, and compared to finite element results.

  13. Evolution of tensile design stresses for lumber

    Treesearch

    William L. Galligan; C. C. Gerhards; R. L. Ethington

    1979-01-01

    Until approximately 1965, allowable design stresses for lumber in tension were taken as equal to those assigned for bending. As interest in tensile properties increased, testing machines were designed specifically to stress lumber in tension. Research results that accumulated on tensile tests of full-size lumber suggested lower design stresses for tension than for...

  14. Tensile Properties of 17-7 PH and 12 MoV Stainless-Steel Sheet under Rapid-Heating and Constant-Temperature Conditions

    NASA Technical Reports Server (NTRS)

    Manning, Charles R., Jr.; Price, Howard L.

    1961-01-01

    Results are presented of rapid-heating tests of 17-7 PH and 12 MoV stainless-steel sheet heated to failure at temperature rates from about 1 F to 170 F per second under constant-load conditions. Yield and rupture strengths obtained from rapid-heating tests are compared with yield and tensile strengths obtained from short-time elevated-temperature tensile tests (30-minute exposure). A rate-temperature parameter was used to construct master curves from which yield and rupture stresses or temperatures can be predicted. A method for measuring strain by optical means is described.

  15. Low-energy electron effects on tensile modulus and infrared transmission properties of a polypyromellitimide film

    NASA Technical Reports Server (NTRS)

    Ferl, J. E.; Long, E. R., Jr.

    1981-01-01

    Infrared (IR) spectroscopy and tensile modulus testing were used to evaluate the importance of experimental procedure on changes in properties of pyromellitic dianhydride-p,p prime-oxydianiline film exposed to electron radiation. The radiation exposures were accelerated, approximate equivalents to the total dose expected for a 30 year mission in geosynchronous Earth orbit. The change in the tensile modulus depends more on the dose rate and the time interval between exposure and testing than on total dose. The IR data vary with both total dose and dose rate. A threshold dose rate exists below which reversible radiation effects on the IR spectra occur. Above the threshold dose rate, irreversible effects occur with the appearance of a new band. Post-irradiation and in situ IR absorption bands are significantly different. It is suggested that the electron radiation induced metastable, excites molecular states.

  16. Ultrasound transmission measurements for tensile strength evaluation of tablets.

    PubMed

    Simonaho, Simo-Pekka; Takala, T Aleksi; Kuosmanen, Marko; Ketolainen, Jarkko

    2011-05-16

    Ultrasound transmission measurements were performed to evaluate the tensile strength of tablets. Tablets consisting of one ingredient were compressed from dibasic calcium phosphate dehydrate, two grades of microcrystalline cellulose and two grades of lactose monohydrate powders. From each powder, tablets with five different tensile strengths were directly compressed. Ultrasound transmission measurements were conducted on every tablet at frequencies of 2.25 MHz, 5 MHz and 10 MHz and the speed of sound was calculated from the acquired waveforms. The tensile strength of the tablets was determined using a diametrical mechanical testing machine and compared to the calculated speed of sound values. It was found that the speed of sound increased with the tensile strength for the tested excipients. There was a good correlation between the speed of sound and tensile strength. Moreover, based on the statistical tests, the groups with different tensile strengths can be differentiated from each other by measuring the speed of sound. Thus, the ultrasound transmission measurement technique is a potentially useful method for non-destructive and fast evaluation of the tensile strength of tablets. Copyright © 2011 Elsevier B.V. All rights reserved.

  17. Tensile behavior of tungsten and tungsten-alloy wires from 1300 to 1600 K

    NASA Technical Reports Server (NTRS)

    Hee, Man Yun

    1988-01-01

    The tensile behavior of a 200-micrometer-diameter tungsten lamp (218CS-W), tungsten + 1.0 atomic percent (a/o) thoria (ST300-W), and tungsten + 0.4 a/o hafnium carbide (WHfC) wires was determined over the temperature range 1300 t0 1600 K at strain rates of 3.3 X 10 to the -2 to 3.3 X 10 to the -5/sec. Although most tests were conducted on as-drawn materials, one series of tests was undertaken on ST300-W wires in four different conditions: as-drawn and vacuum-annealed at 1535 K for 1 hr, with and without electroplating. Whereas heat treatment had no effect on tensile properties, electropolishing significantly increased both the proportional limit and ductility, but not the ultimate tensile strength. Comparison of the behavior of the three alloys indicates that the HfC-dispersed material possesses superior tensile properties. Theoretical calculations indicate that the strength/ductility advantage of WHfC is due to the resistance to recrystallization imparted by the dispersoid.

  18. Tensile Deformation Temperature Impact on Microstructure and Mechanical Properties of AISI 316LN Austenitic Stainless Steel

    NASA Astrophysics Data System (ADS)

    Xiong, Yi; He, Tiantian; Lu, Yan; Ren, Fengzhang; Volinsky, Alex A.; Cao, Wei

    2018-03-01

    Uniaxial tensile tests were conducted on AISI 316LN austenitic stainless steel from - 40 to 300 °C at a rate of 0.5 mm/min. Microstructure and mechanical properties of the deformed steel were investigated by optical, scanning and transmission electron microscopies, x-ray diffraction, and microhardness testing. The yield strength, ultimate tensile strength, elongation, and microhardness increase with the decrease in the test temperature. The tensile fracture morphology has the dimple rupture feature after low-temperature deformations and turns to a mixture of transgranular fracture and dimple fracture after high-temperature ones. The dominating deformation microstructure evolves from dislocation tangle/slip bands to large deformation twins/slip bands with temperature decrease. The deformation-induced martensite transformation can only be realized at low temperature, and its quantity increases with the decrease in the temperature.

  19. High-Temperature Tensile Behaviors of Base Metal and Electron Beam-Welded Joints of Ni-20Cr-9Mo-4Nb Superalloy

    NASA Astrophysics Data System (ADS)

    Gupta, R. K.; Anil Kumar, V.; Sukumaran, Arjun; Kumar, Vinod

    2018-05-01

    Electron beam welding of Ni-20Cr-9Mo-4Nb alloy sheets was carried out, and high-temperature tensile behaviors of base metal and weldments were studied. Tensile properties were evaluated at ambient temperature, at elevated temperatures of 625 °C to 1025 °C, and at strain rates of 0.1 to 0.001 s-1. Microstructure of the weld consisted of columnar dendritic structure and revealed epitaxial mode of solidification. Weld efficiency of 90 pct in terms of strength (UTS) was observed at ambient temperature and up to an elevated temperature of 850 °C. Reduction in strength continued with further increase of test temperature (up to 1025 °C); however, a significant improvement in pct elongation is found up to 775 °C, which was sustained even at higher test temperatures. The tensile behaviors of base metal and weldments were similar at the elevated temperatures at the respective strain rates. Strain hardening exponent `n' of the base metal and weldment was 0.519. Activation energy `Q' of base metal and EB weldments were 420 to 535 kJ mol-1 determined through isothermal tensile tests and 625 to 662 kJ mol-1 through jump-temperature tensile tests. Strain rate sensitivity `m' was low (< 0.119) for the base metal and (< 0.164) for the weldment. The δ phase was revealed in specimens annealed at 700 °C, whereas, twins and fully recrystallized grains were observed in specimens annealed at 1025 °C. Low-angle misorientation and strain localization in the welds and the HAZ during tensile testing at higher temperature and strain rates indicates subgrain formation and recrystallization. Higher elongation in the weldment (at Test temperature > 775 °C) is attributed to the presence of recrystallized grains. Up to 700 °C, the deformation is through slip, where strain hardening is predominant and effect of strain rate is minimal. Between 775 °C to 850 °C, strain hardening is counterbalanced by flow softening, where cavitation limits the deformation (predominantly at lower strain

  20. Engineering and experimental analyses of the tensile loads applied during strength testing of direct bonded orthodontic brackets.

    PubMed

    Katona, T R; Chen, J

    1994-08-01

    The stress levels within the cement layer (hence, the apparent strength) of a direct bonded orthodontic bracket depends, to a large extent, on the alignment of the tensile loads that are applied to the specimen. The purpose of this analysis was to determine how the construction of a ligature wire harness affects the alignment of the applied loads. Tensile tests conducted on a modified bracket/cement system showed large variations in the force-elongation curve profiles. An engineering model was developed to explain these deviations. The results indicate that it is virtually impossible to evenly apply tensile loads to the bracket. It was also proposed that long harnesses constructed with thin ligature wire, prestressing the harness, and lubrication may reduce some of the effects of unavoidable load-bracket misalignment.

  1. Cryogenic Temperature-Gradient Foam/Substrate Tensile Tester

    NASA Technical Reports Server (NTRS)

    Vailhe, Christophe

    2003-01-01

    The figure shows a fixture for measuring the tensile strength of the bond between an aluminum substrate and a thermally insulating polymeric foam. The specimen is meant to be representative of insulating foam on an aluminum tank that holds a cryogenic liquid. Prior to the development of this fixture, tensile tests of this type were performed on foam/substrate specimens immersed in cryogenic fluids. Because the specimens were cooled to cryogenic temperatures throughout their thicknesses, they tended to become brittle and to fracture at loads below true bond tensile strengths. The present fixture is equipped to provide a thermal gradient from cryogenic temperature at the foam/substrate interface to room temperature on the opposite foam surface. The fixture includes an upper aluminum block at room temperature and a lower aluminum block cooled to -423 F (approx. -253 C) by use of liquid helium. In preparation for a test, the metal outer surface (the lower surface) of a foam/substrate specimen is bonded to the lower block and the foam outer surface (the upper surface) of the specimen is bonded to the upper block. In comparison with the through-the-thickness cooling of immersion testing, the cryogenic-to-room-temperature thermal gradient that exists during testing on this fixture is a more realistic approximation of the operational thermal condition of sprayed insulating foam on a tank of cryogenic liquid. Hence, tensile tests performed on this fixture provide more accurate indications of operational bond tensile strengths. In addition, the introduction of the present fixture reduces the cost of testing by reducing the amount of cryogenic liquid consumed and the time needed to cool a specimen.

  2. Liquid Metal Embrittlement in Resistance Spot Welding and Hot Tensile Tests of Surface-refined TWIP Steels

    NASA Astrophysics Data System (ADS)

    Barthelmie, J.; Schram, A.; Wesling, V.

    2016-03-01

    Automotive industry strives to reduce vehicle weight and therefore fuel consumption and carbon dioxide emissions. Especially in the auto body, material light weight construction is practiced, but the occupant safety must be ensured. These requirements demand high-strength steels with good forming and crash characteristics. Such an approach is the use of high- manganese-content TWIP steels, which achieve strengths of around 1,000 MPa and fracture strains of more than 60%. Welding surface-refined TWIP steels reduces their elongation at break and produces cracks due to the contact with liquid metal and the subsequent liquid metal embrittlement (LME). The results of resistance spot welds of mixed joints of high-manganese- content steel in combination with micro-alloyed ferritic steel and hot tensile tests are presented. The influence of different welding parameters on the sensitivity to liquid metal embrittlement is investigated by means of spot welding. In a high temperature tensile testing machine, the influence of different parameters is determined regardless of the welding process. Defined strains just below or above the yield point, and at 25% of elongation at break, show the correlation between the applied strain and liquid metal crack initiation. Due to the possibility to carry out tensile tests on a wide range of temperatures, dependencies of different temperatures of the zinc coating to the steel can be identified. Furthermore, the attack time of the zinc on the base material is investigated by defined heating periods.

  3. Quasi-static and dynamic experimental studies on the tensile strength and failure pattern of concrete and mortar discs.

    PubMed

    Jin, Xiaochao; Hou, Cheng; Fan, Xueling; Lu, Chunsheng; Yang, Huawei; Shu, Xuefeng; Wang, Zhihua

    2017-11-10

    As concrete and mortar materials widely used in structural engineering may suffer dynamic loadings, studies on their mechanical properties under different strain rates are of great importance. In this paper, based on splitting tests of Brazilian discs, the tensile strength and failure pattern of concrete and mortar were investigated under quasi-static and dynamic loadings with a strain rate of 1-200 s -1 . It is shown that the quasi-static tensile strength of mortar is higher than that of concrete since coarse aggregates weaken the interface bonding strength of the latter. Numerical results confirmed that the plane stress hypothesis lead to a lower value tensile strength for the cylindrical specimens. With the increase of strain rates, dynamic tensile strengths of concrete and mortar significantly increase, and their failure patterns change form a single crack to multiple cracks and even fragment. Furthermore, a relationship between the dynamic increase factor and strain rate was established by using a linear fitting algorithm, which can be conveniently used to calculate the dynamic increase factor of concrete-like materials in engineering applications.

  4. Indirect and direct tensile behavior of Devonian oil shales

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Chong, K.P.; Chen, J.L.; Dana, G.F.

    1984-03-01

    Ultimate indirect tensile strengths of Devonian oil shales across the bedding planes is a mechanical property parameter important to predicting how oil shale will break. This is particularly important to in-situ fragmentation. The Split Cylinder Test was used to determine the indirect tensile strengths between the bedding planes. Test specimens, cored perpendicular to the bedding planes, representing oil shales of different oil yields taken from Silver Point Quad in DeKalb County, Tennessee and Friendship in Scioto County, Ohio, were subjected to the Split Cylinder Test. Linear regression equations relating ultimate tensile strength across the bedding planes to volume percent ofmore » organic matter in the rock were developed from the test data. In addition, direct tensile strengths were obtained between the bedding planes for the Tennessee oil shales. This property is important for the design of horizontal fractures in oil shales. Typical results were presented.« less

  5. Interlaboratory round robin study on axial tensile properties of SiC-SiC CMC tubular test specimens [Interlaboratory round robin study on axial tensile properties of SiC/SiC tubes

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Singh, Gyanender P.; Gonczy, Steve T.; Deck, Christian P.

    An interlaboratory round robin study was conducted on the tensile strength of SiC–SiC ceramic matrix composite (CMC) tubular test specimens at room temperature with the objective of expanding the database of mechanical properties of nuclear grade SiC–SiC and establishing the precision and bias statement for standard test method ASTM C1773. The mechanical properties statistics from the round robin study and the precision statistics and precision statement are presented herein. The data show reasonable consistency across the laboratories, indicating that the current C1773–13 ASTM standard is adequate for testing ceramic fiber reinforced ceramic matrix composite tubular test specimen. Furthermore, it wasmore » found that the distribution of ultimate tensile strength data was best described with a two–parameter Weibull distribution, while a lognormal distribution provided a good description of the distribution of proportional limit stress data.« less

  6. Interlaboratory round robin study on axial tensile properties of SiC-SiC CMC tubular test specimens [Interlaboratory round robin study on axial tensile properties of SiC/SiC tubes

    DOE PAGES

    Singh, Gyanender P.; Gonczy, Steve T.; Deck, Christian P.; ...

    2018-04-19

    An interlaboratory round robin study was conducted on the tensile strength of SiC–SiC ceramic matrix composite (CMC) tubular test specimens at room temperature with the objective of expanding the database of mechanical properties of nuclear grade SiC–SiC and establishing the precision and bias statement for standard test method ASTM C1773. The mechanical properties statistics from the round robin study and the precision statistics and precision statement are presented herein. The data show reasonable consistency across the laboratories, indicating that the current C1773–13 ASTM standard is adequate for testing ceramic fiber reinforced ceramic matrix composite tubular test specimen. Furthermore, it wasmore » found that the distribution of ultimate tensile strength data was best described with a two–parameter Weibull distribution, while a lognormal distribution provided a good description of the distribution of proportional limit stress data.« less

  7. Stiffness reductions during tensile fatigue testing of graphite/epoxy angle-ply laminates

    NASA Technical Reports Server (NTRS)

    Odom, E. M.; Adams, D. F.

    1982-01-01

    Tensile fatigue data was generated under carefully controlled test conditions. A computerized data acquisition system was used to permit the measurement of dynamic modulus without interrupting the fatigue cycling. Two different 8-ply laminate configurations, viz, + or - 45 (2s) and + or - 67.5 (2s), of a T300/5208 graphite/epoxy composite were tested. The + or - 45 (2s) laminate did exhibit some modulus decay, although there was no well-defined correlation with applied stress level or number of cycles. The + or - 67.5 (2s) laminate did not exhibit any measurable modulus decay. Secondary effects observed included a small but distinct difference between modulus as measured statically and dynamically, a slight recovery of the modulus decay after a test interruption, and a significant viscoelastic (creep) response of the + or - 45 (2s) laminate during fatigue testing.

  8. High-speed imaging on static tensile test for unidirectional CFRP

    NASA Astrophysics Data System (ADS)

    Kusano, Hideaki; Aoki, Yuichiro; Hirano, Yoshiyasu; Kondo, Yasushi; Nagao, Yosuke

    2008-11-01

    The objective of this study is to clarify the fracture mechanism of unidirectional CFRP (Carbon Fiber Reinforced Plastics) under static tensile loading. The advantages of CFRP are higher specific stiffness and strength than the metal material. The use of CFRP is increasing in not only the aerospace and rapid transit railway industries but also the sports, leisure and automotive industries. The tensile fracture mechanism of unidirectional CFRP has not been experimentally made clear because the fracture speed of unidirectional CFRP is quite high. We selected the intermediate modulus and high strength unidirectional CFRP laminate which is a typical material used in the aerospace field. The fracture process under static tensile loading was captured by a conventional high-speed camera and a new type High-Speed Video Camera HPV-1. It was found that the duration of fracture is 200 microseconds or less, then images taken by a conventional camera doesn't have enough temporal-resolution. On the other hand, results obtained by HPV-1 have higher quality where the fracture process can be clearly observed.

  9. Tensile properties of V-5Cr-5Ti alloy after exposure in air environment

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Natesan, K.; Soppet, W.K.

    1997-04-01

    Oxidation studies were conducted on V-5Cr-5Ti alloy specimens in an air environment to evaluate the oxygen uptake behavior of the alloy as a function of temperature and exposure time. The oxidation rates, calculated from parabolic kinetic measurements of thermogravimetric testing and confirmed by microscopic analysis of cross sections of exposed specimens, were 5, 17, and 27 {mu}m per year after exposure at 300, 400, and 500{degrees}C, respectively. Uniaxial tensile tests were conducted at room temperature and at 500{degrees}C on preoxidized specimens of the alloy to examine the effects of oxidation and oxygen migration on tensile strength and ductility. Correlations weremore » developed between tensile strength and ductility of the oxidized alloy and microstructural characteristics such as oxide thickness, depth of hardened layer, depth of intergranular fracture zone, and transverse crack length.« less

  10. Non-contact tensile viscoelastic characterization of microscale biological materials

    NASA Astrophysics Data System (ADS)

    Li, Yuhui; Hong, Yuan; Xu, Guang-Kui; Liu, Shaobao; Shi, Qiang; Tang, Deding; Yang, Hui; Genin, Guy M.; Lu, Tian Jian; Xu, Feng

    2018-06-01

    Many structures and materials in nature and physiology have important "meso-scale" structures at the micron length-scale whose tensile responses have proven difficult to characterize mechanically. Although techniques such as atomic force microscopy and micro- and nano-identation are mature for compression and indentation testing at the nano-scale, and standard uniaxial and shear rheometry techniques exist for the macroscale, few techniques are applicable for tensile-testing at the micrometre-scale, leaving a gap in our understanding of hierarchical biomaterials. Here, we present a novel magnetic mechanical testing (MMT) system that enables viscoelastic tensile testing at this critical length scale. The MMT system applies non-contact loading, avoiding gripping and surface interaction effects. We demonstrate application of the MMT system to the first analyses of the pure tensile responses of several native and engineered tissue systems at the mesoscale, showing the broad potential of the system for exploring micro- and meso-scale analysis of structured and hierarchical biological systems.

  11. Non-contact tensile viscoelastic characterization of microscale biological materials

    NASA Astrophysics Data System (ADS)

    Li, Yuhui; Hong, Yuan; Xu, Guang-Kui; Liu, Shaobao; Shi, Qiang; Tang, Deding; Yang, Hui; Genin, Guy M.; Lu, Tian Jian; Xu, Feng

    2018-01-01

    Many structures and materials in nature and physiology have important "meso-scale" structures at the micron length-scale whose tensile responses have proven difficult to characterize mechanically. Although techniques such as atomic force microscopy and micro- and nano-identation are mature for compression and indentation testing at the nano-scale, and standard uniaxial and shear rheometry techniques exist for the macroscale, few techniques are applicable for tensile-testing at the micrometre-scale, leaving a gap in our understanding of hierarchical biomaterials. Here, we present a novel magnetic mechanical testing (MMT) system that enables viscoelastic tensile testing at this critical length scale. The MMT system applies non-contact loading, avoiding gripping and surface interaction effects. We demonstrate application of the MMT system to the first analyses of the pure tensile responses of several native and engineered tissue systems at the mesoscale, showing the broad potential of the system for exploring micro- and meso-scale analysis of structured and hierarchical biological systems.

  12. Tensile strength of aluminium nitride films

    NASA Astrophysics Data System (ADS)

    Zong, Deng Gang; Ong, Chung Wo; Aravind, Manju; Tsang, Mei Po; Loong Choy, Chung; Lu, Deren; Ma, Dejun

    2004-11-01

    Two-layered aluminium nitride (AlN)/silicon nitride microbridges were fabricated for microbridge tests to evaluate the elastic modulus, residual stress and tensile strength of the AlN films. The silicon nitride layer was added to increase the robustness of the structure. In a microbridge test, load was applied to the centre of a microbridge and was gradually increased by a nano-indenter equipped with a wedge tip until the sample was broken, while displacement was recorded coherently. Measurements were performed on single-layered silicon nitride microbridges and two-layered AlN/silicon nitride microbridges respectively. The data were fitted to a theory to derive the elastic modulus, residual stress and tensile strength of the silicon nitride films and AlN films. For the AlN films, the three parameters were determined to be 200, 0.06 and 0.3 GPa, respectively. The values of elastic modulus obtained were consistent with those measured by conventional nano-indentation method. The tensile strength value can be used as a reference to reflect the maximum tolerable tensile stress of AlN films when they are used in micro-electromechanical devices.

  13. Fracture simulation of elastomer blended polypropylene based on elastoviscoplastic constitutive equation with craze and tensile softening law

    NASA Astrophysics Data System (ADS)

    Mae, H.

    2006-08-01

    The strong strain-rate dependence, neck propagation and craze evolution characterize the large plastic deformation and fracture behavior of polymer. In the latest study, Kobayashi, Tomii and Shizawa suggested the elastoviscoplastic constitutive equation based on craze evolution and annihilation and then applied it to the plane strain issue of polymer. In the previous study, the author applied their suggested elastoviscoplastic constitutive equation with craze effect to the three dimensional shell and then showed that the load displacement history was in good agreement with the experimental result including only microscopic crack such as crazes. For the future industrial applications, the macroscopic crack has to be taken into account. Thus, the main objective of this study is to propose the tensile softening equation and then add it to the elastoviscoplastic constitutive equation with craze effect so that the load displacement history can be roughly simulated during the macroscopic crack propagation. The tested material in this study is the elastomer blended polypropylene used in the interior and exterior of automobiles. First, the material properties are obtained based on the tensile test results at wide range of strain rates: 10 - 4-102 (1/sec). Next, the compact tension test is conducted and then the tensile softening parameters are fixed. Then, the dart impact test is carried out in order to obtain the load displacement history and also observe the macroscopic crack propagation at high strain rate. Finally, the fracture behavior is simulated and then compared with the experimental results. It is shown that the predictions of the constitutive equation with the proposed tensile softening equation are in good agreement with the experimental results for the future industrial applications.

  14. Stress transfer in microdroplet tensile test: PVC-coated and uncoated Kevlar-29 single fiber

    NASA Astrophysics Data System (ADS)

    Zhenkun, Lei; Quan, Wang; Yilan, Kang; Wei, Qiu; Xuemin, Pan

    2010-11-01

    The single fiber/microdroplet tensile test is applied for evaluating the interfacial mechanics between a fiber and a resin substrate. It is used to investigate the influence of a polymer coating on a Kevlar-29 fiber surface, specifically the stress transfer between the fiber and epoxy resin in a microdroplet. Unlike usual tests, this new test ensures a symmetrical axial stress on the embedded fiber and reduces the stress singularity that appears at the embedded fiber entry. Using a homemade loading device, symmetrical tensile tests are performed on a Kevlar-29 fiber with or without polyvinylchloride (PVC) coating, the surface of which is in contact with two epoxy resin microdroplets during curing. Raman spectra on the embedded fiber are recorded by micro-Raman Spectroscopy under different strain levels. Then they are transformed to the distributions of fiber axis stress based on the relationship between stress and Raman shift. The Raman results reveal that the fiber axial stresses increase with the applied loads, and the antisymmetric interfacial shear stresses, obtained by a straightforward balance of shear-to-axial forces argument, lead to the appearance of shear stress concentrations at a distance to the embedded fiber entry. The load is transferred from the outer fiber to the embedded fiber in the epoxy microdroplet. As is observed by scanning electronic microscopy (SEM), the existence of a flexible polymer coating on the fiber surface reduces the stress transfer efficiency.

  15. Effect of hydrogen on void initiation in tensile test of carbon steel JIS-S25C

    NASA Astrophysics Data System (ADS)

    Sugawa, S.; Tsutsumi, N.; Oda, K.

    2018-06-01

    In order to investigate the effect of hydrogen on tensile fracture mechanism of a carbon steel, tensile tests were conducted. Pre-strain specimens (0%, 5% and 10%) were used to study the effect of hydrogen content, since saturated hydrogen content in specimens increases in increasing dislocation density. The tensile strength and the yield stress of hydrogen specimens were almost the same as uncharged. In contrast, the reduction of area of hydrogen charged specimens was smaller than that of uncharged. To reveal the reasons of decrease of the reduction of area, the fracture surface and longitudinal cross section near the fracture surface were observed. On the fracture surface of uncharged specimens, only dimples were observed. On the other hand, dimples and flat fracture surface were observed on the fracture surface of hydrogen charged. On the longitudinal cross section of hydrogen charged specimens, many voids were observed compared to uncharged. From these observations, it is showed that hydrogen gives a rise to the increase of voids and the hydrogen charged specimens break without sufficient necking, thus hydrogen makes the reduction of area smaller.

  16. Device for testing closure disks at high rates of change of pressure

    DOEpatents

    Merten, Jr., Charles W.

    1993-11-09

    A device for testing the burst pressure of closure disks which provides high pressure to both sides of a disk and rapidly releases pressure from one side thereof causing a high rate of change of pressure. A hollow notched plug allows the rapid release of pressure upon rupturing. A means is also disclosed for transmitting a tensile load from a piston to a hollow notched plug and for sealing the means for transmitting load within a hole in a piston.

  17. Baseline tensile tests of composite materials for LDEF (Long Duration Exposure Facility) exposure

    NASA Technical Reports Server (NTRS)

    Witte, William G.

    1987-01-01

    Tensile specimens of five graphite fiber reinforced composite materials were tested at room temperature to provide baseline data for similar specimens exposed to the space environment in low-Earth orbit on the NASA Long Duration Exposure Facility. All specimens were 4-ply (+ or - 45 deg)s layups; at least five replicate specimens were tested for each parameter evaluated. Three epoxy-matrix materials and two polysulfone-matrix materials, several fiber volume fractions, and two sizes of specimen were evaluated. Stress-strain and Poisson's ratio-stress curves, ultimate stress, strain at failure, secant modulus at 0.004 strain, inplane shear stress-strain curves, and unidirectional shear modulus at .004 shear strain are presented.

  18. Experimental investigations on thermo mechanical behaviour of aluminium alloys subjected to tensile loading and laser irradiation

    NASA Astrophysics Data System (ADS)

    Jelani, Mohsan; Li, Zewen; Shen, Zhonghua; Sardar, Maryam; Tabassum, Aasma

    2017-05-01

    The present work reports the investigation of the thermal and mechanical behaviour of aluminium alloys under the combined action of tensile loading and laser irradiations. The two types of aluminium alloys (Al-1060 and Al-6061) are used for the experiments. The continuous wave Ytterbium fibre laser (wavelength 1080 nm) was employed as irradiation source, while tensile loading was provided by tensile testing machine. The effects of various pre-loading and laser power densities on the failure time, temperature distribution and on deformation behaviour of aluminium alloys are analysed. The experimental results represents the significant reduction in failure time and temperature for higher laser powers and for high load values, which implies that preloading may contribute a significant role in the failure of the material at elevated temperature. The reason and characterization of material failure by tensile and laser loading are explored in detail. A comparative behaviour of under tested materials is also investigated. This work suggests that, studies considering only combined loading are not enough to fully understand the mechanical behaviour of under tested materials. For complete characterization, one must consider the effect of heating as well as loading rate.

  19. Effects of conventional welding and laser welding on the tensile strength, ultimate tensile strength and surface characteristics of two cobalt-chromium alloys: a comparative study.

    PubMed

    Madhan Kumar, Seenivasan; Sethumadhava, Jayesh Raghavendra; Anand Kumar, Vaidyanathan; Manita, Grover

    2012-06-01

    The purpose of this study was to evaluate the efficacy of laser welding and conventional welding on the tensile strength and ultimate tensile strength of the cobalt-chromium alloy. Samples were prepared with two commercially available cobalt-chromium alloys (Wironium plus and Diadur alloy). The samples were sectioned and the broken fragments were joined using Conventional and Laser welding techniques. The welded joints were subjected to tensile and ultimate tensile strength testing; and scanning electron microscope to evaluate the surface characteristics at the welded site. Both on laser welding as well as on conventional welding technique, Diadur alloy samples showed lesser values when tested for tensile and ultimate tensile strength when compared to Wironium alloy samples. Under the scanning electron microscope, the laser welded joints show uniform welding and continuous molt pool all over the surface with less porosity than the conventionally welded joints. Laser welding is an advantageous method of connecting or repairing cast metal prosthetic frameworks.

  20. Fracture toughness versus micro-tensile bond strength testing of adhesive-dentin interfaces.

    PubMed

    De Munck, Jan; Luehrs, Anne-Katrin; Poitevin, André; Van Ende, Annelies; Van Meerbeek, Bart

    2013-06-01

    To assess interfacial fracture toughness of different adhesive approaches and compare to a standard micro-tensile bond-strength (μTBS) test. Chevron-notched beam fracture toughness (CNB) was measured following a modified ISO 24370 standard. Composite bars with dimensions of 3.0×4.0×25 mm were prepared, with the adhesive-dentin interface in the middle. At the adhesive-dentin interface, a chevron notch was prepared using a 0.15 mm thin diamond blade mounted in a water-cooled diamond saw. Each specimen was loaded until failure in a 4-point bend test setup and the fracture toughness was calculated according to the ISO specifications. Similarly, adhesive-dentin micro-specimens (1.0×1.0×8-10 mm) were stressed in tensile until failure to determine the μTBS. A positive correlation (r(2)=0.64) was observed between CNB and μTBS, which however was only nearly statistically significant, mainly due to the dissimilar outcome of Scotchbond Universal (3M ESPE). While few μTBS specimens failed at the adhesive-dentin interface, almost all CNB specimens failed interfacially at the notch tip. Weibull moduli for interfacial fracture toughness were much higher than for μTBS (3.8-11.5 versus 2.7-4.8, respectively), especially relevant with regard to early failures. Although the ranking of the adhesives on their bonding effectiveness tested using CNB and μTBS corresponded well, the outcome of CNB appeared more reliable and less variable. Fracture toughness measurement is however more laborious and requires specific equipment. The μTBS nevertheless appeared to remain a valid method to assess bonding effectiveness in a versatile way. Copyright © 2013 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

  1. A new laser reflectance system capable of measuring changing cross-sectional area of soft tissues during tensile testing.

    PubMed

    Pokhai, Gabriel G; Oliver, Michele L; Gordon, Karen D

    2009-09-01

    Determination of the biomechanical properties of soft tissues such as tendons and ligaments is dependent on the accurate measurement of their cross-sectional area (CSA). Measurement methods, which involve contact with the specimen, are problematic because soft tissues are easily deformed. Noncontact measurement methods are preferable in this regard, but may experience difficulty in dealing with the complex cross-sectional shapes and glistening surfaces seen in soft tissues. Additionally, existing CSA measurement systems are separated from the materials testing machine, resulting in the inability to measure CSA during testing. Furthermore, CSA measurements are usually made in a different orientation, and with a different preload, prior to testing. To overcome these problems, a noncontact laser reflectance system (LRS) was developed. Designed to fit in an Instron 8872 servohydraulic test machine, the system measures CSA by orbiting a laser transducer in a circular path around a soft tissue specimen held by tissue clamps. CSA measurements can be conducted before and during tensile testing. The system was validated using machined metallic specimens of various shapes and sizes, as well as different sizes of bovine tendons. The metallic specimens could be measured to within 4% accuracy, and the tendons to within an average error of 4.3%. Statistical analyses showed no significant differences between the measurements of the LRS and those of the casting method, an established measurement technique. The LRS was successfully used to measure the changing CSA of bovine tendons during uniaxial tensile testing. The LRS developed in this work represents a simple, quick, and accurate way of reconstructing complex cross-sectional profiles and calculating cross-sectional areas. In addition, the LRS represents the first system capable of automatically measuring changing CSA of soft tissues during tensile testing, facilitating the calculation of more accurate biomechanical properties.

  2. Tensile, Creep, and Fatigue Behaviors of 3D-Printed Acrylonitrile Butadiene Styrene

    NASA Astrophysics Data System (ADS)

    Zhang, Hanyin; Cai, Linlin; Golub, Michael; Zhang, Yi; Yang, Xuehui; Schlarman, Kate; Zhang, Jing

    2018-01-01

    Acrylonitrile butadiene styrene (ABS) is a widely used thermoplastics in 3D printing. However, there is a lack of thorough investigation of the mechanical properties of 3D-printed ABS components, including orientation-dependent tensile strength and creep fatigue properties. In this work, a systematic characterization is conducted on the mechanical properties of 3D-printed ABS components. Specifically, the effect of printing orientation on the tensile and creep properties is investigated. The results show that, in tensile tests, the 0° printing orientation has the highest Young's modulus of 1.81 GPa, and ultimate strength of 224 MPa. In the creep test, the 90° printing orientation has the lowest k value of 0.2 in the plastics creep model, suggesting 90° is the most creep resistant direction. In the fatigue test, the average cycle number under load of 30 N is 3796 cycles. The average cycle number decreases to 128 cycles when the load is 60 N. Using the Paris law, with an estimated crack size of 0.75 mm, and stress intensity factor is varied from 352 to 700 N√ m, the derived fatigue crack growth rate is 0.0341 mm/cycle. This study provides important mechanical property data that is useful for applying 3D-printed ABS in engineering applications.

  3. Device for testing closure disks at high rates of change of pressure

    DOEpatents

    Merten, C.W. Jr.

    1993-11-09

    A device is described for testing the burst pressure of closure disks which provides high pressure to both sides of a disk and rapidly releases pressure from one side thereof causing a high rate of change of pressure. A hollow notched plug allows the rapid release of pressure upon rupturing. A means is also disclosed for transmitting a tensile load from a piston to a hollow notched plug and for sealing the means for transmitting load within a hole in a piston. 5 figures.

  4. Tensile, swelling and morphological properties of bentonite-filled acrylonitrile butadiene rubber composites

    NASA Astrophysics Data System (ADS)

    Lotfi, Muhamad Nadhli Amin; Ismail, Hanafi; Othman, Nadras

    2017-10-01

    Tensile, swelling and morphological properties of bentonite filled acrylonitrile butadiene rubber (NBR/Bt) composites were studied. The experiments were conducted at room temperature by using two rolled mill, universal testing machine (INSTRON), and American Standard Testing Method (ASTM) D471 for compounding, tensile testing, and swelling test, respectively. Results obtained indicated that a better tensile strength, elongation at break and tensile modulus were recorded as compared to the pure NBR particularly up to 90 phr of Bt loading. However, swelling (%) exhibited the opposite trend where the liquid uptake by the composites was indirectly proportional with the increasing of Bt loading. Scanning electron microscopy (SEM) used on the tensile fractured surface of the NBR/Bt composites have shown that the fillers were well embedded in the NBR matrix, for Bt loading up to 90 phr. The agglomeration of fillers occurred for Bt loading exceeding 90 phr.

  5. Finite element analysis of the high strain rate testing of polymeric materials

    NASA Astrophysics Data System (ADS)

    Gorwade, C. V.; Alghamdi, A. S.; Ashcroft, I. A.; Silberschmidt, V. V.; Song, M.

    2012-08-01

    Advanced polymer materials are finding an increasing range of industrial and defence applications. Ultra-high molecular weight polymers (UHMWPE) are already used in lightweight body armour because of their good impact resistance with light weight. However, a broader use of such materials is limited by the complexity of the manufacturing processes and the lack of experimental data on their behaviour and failure evolution under high-strain rate loading conditions. The current study deals with an investigation of the internal heat generation during tensile of UHMWPE. A 3D finite element (FE) model of the tensile test is developed and validated the with experimental work. An elastic-plastic material model is used with adiabatic heat generation. The temperature and stresses obtained with FE analysis are found to be in a good agreement with the experimental results. The model can be used as a simple and cost effective tool to predict the thermo-mechanical behaviour of UHMWPE part under various loading conditions.

  6. Dynamic tensile characterization of a 4330 steel with kolsky bar techniques.

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Song, Bo; Antoun, Bonnie R.; Connelly, Kevin

    2010-08-01

    There has been increasing demand to understand the stress-strain response as well as damage and failure mechanisms of materials under impact loading condition. Dynamic tensile characterization has been an efficient approach to acquire satisfactory information of mechanical properties including damage and failure of the materials under investigation. However, in order to obtain valid experimental data, reliable tensile experimental techniques at high strain rates are required. This includes not only precise experimental apparatus but also reliable experimental procedures and comprehensive data interpretation. Kolsky bar, originally developed by Kolsky in 1949 [1] for high-rate compressive characterization of materials, has been extended formore » dynamic tensile testing since 1960 [2]. In comparison to Kolsky compression bar, the experimental design of Kolsky tension bar has been much more diversified, particularly in producing high speed tensile pulses in the bars. Moreover, instead of directly sandwiching the cylindrical specimen between the bars in Kolsky bar compression bar experiments, the specimen must be firmly attached to the bar ends in Kolsky tensile bar experiments. A common method is to thread a dumbbell specimen into the ends of the incident and transmission bars. The relatively complicated striking and specimen gripping systems in Kolsky tension bar techniques often lead to disturbance in stress wave propagation in the bars, requiring appropriate interpretation of experimental data. In this study, we employed a modified Kolsky tension bar, newly developed at Sandia National Laboratories, Livermore, CA, to explore the dynamic tensile response of a 4330-V steel. The design of the new Kolsky tension bar has been presented at 2010 SEM Annual Conference [3]. Figures 1 and 2 show the actual photograph and schematic of the Kolsky tension bar, respectively. As shown in Fig. 2, the gun barrel is directly connected to the incident bar with a coupler. The

  7. Effect of Test Specimen Shape and Size on Interlaminar Tensile Properties of Advanced Carbon-Carbon Composites

    NASA Technical Reports Server (NTRS)

    Vaughn, Wallace L.

    2015-01-01

    The interlaminar tensile strength of 1000-tow T-300 fiber ACC-6 carbon-carbon composites was measured using the method of bonding the coupons to adherends at room temperature. The size, 0.70 to 1.963 inches maximum width or radius, and shape, round or square, of the test coupons were varied to determine if the test method was sensitive to these variables. Sixteen total variations were investigated and the results modeled.

  8. On the Processing of Spalling Experiments. Part I: Identification of the Dynamic Tensile Strength of Concrete

    NASA Astrophysics Data System (ADS)

    Forquin, P.; Lukić, B.

    2017-11-01

    The spalling technique based on the use of a single Hopkinson bar put in contact with the tested sample has been widely adopted as a reliable method for obtaining the tensile response of concrete and rock-like materials at strain rates up-to 200 s- 1. However, the traditional processing method, based on the use of Novikov acoustic approach and the rear face velocity measurement, remains quite questionable due to strong approximations of this data processing method. Recently a new technique for deriving cross-sectional stress fields of a spalling sample filmed with an ultra-high speed camera and based on using the full field measurements and the virtual fields method (VFM) was proposed. In the present work, this topic is perused by performing several spalling tests on ordinary concrete at high acquisition speed of 1Mfps to accurately measure the tensile strength, Young's modulus, strain-rate at failure and stress-strain response of concrete at high strain-rate. The stress-strain curves contain more measurement points for a more reliable identification. The observed tensile stiffness is up-to 50% lower than the initial compressive stiffness and the obtained peak stress was about 20% lower than the one obtained by applying the Novikov method. In order to support this claim, numerical simulations were performed to show that the change of stiffness between compression and tension highly affects the rear-face velocity profile. This further suggests that the processing based only on the velocity "pullback" is quite sensitive and can produce an overestimate of the tensile strength in concrete and rock-like materials.

  9. Cyclic tensile response of a pre-tensioned polyurethane

    NASA Astrophysics Data System (ADS)

    Nie, Yizhou; Liao, Hangjie; Chen, Weinong W.

    2018-05-01

    In the research reported in this paper, we subject a polyurethane to uniaxial tensile loading at a quasi-static strain rate, a high strain rate and a jumping strain rate where the specimen is under quasi-static pre-tension and is further subjected to a dynamic cyclic loading using a modified Kolsky tension bar. The results obtained at the quasi-static and high strain rate clearly show that the mechanical response of this material is significantly rate sensitive. The rate-jumping experimental results show that the response of the material behavior is consistent before jumping. After jumping the stress-strain response of the material does not jump to the corresponding high-rate curve. Rather it approaches the high-rate curve asymptotically. A non-linear hyper-viscoelastic (NLHV) model, after having been calibrated by monotonic quasi-static and high-rate experimental results, was found to be capable of describing the material tensile behavior under such rate jumping conditions.

  10. Multiscale stochastic simulations for tensile testing of nanotube-based macroscopic cables.

    PubMed

    Pugno, Nicola M; Bosia, Federico; Carpinteri, Alberto

    2008-08-01

    Thousands of multiscale stochastic simulations are carried out in order to perform the first in-silico tensile tests of carbon nanotube (CNT)-based macroscopic cables with varying length. The longest treated cable is the space-elevator megacable but more realistic shorter cables are also considered in this bottom-up investigation. Different sizes, shapes, and concentrations of defects are simulated, resulting in cable macrostrengths not larger than approximately 10 GPa, which is much smaller than the theoretical nanotube strength (approximately 100 GPa). No best-fit parameters are present in the multiscale simulations: the input at level 1 is directly estimated from nanotensile tests of CNTs, whereas its output is considered as the input for the level 2, and so on up to level 5, corresponding to the megacable. Thus, five hierarchical levels are used to span lengths from that of a single nanotube (approximately 100 nm) to that of the space-elevator megacable (approximately 100 Mm).

  11. Tensile Mechanical Property of Oil Palm Empty Fruit Bunch Fiber Reinforced Epoxy Composites

    NASA Astrophysics Data System (ADS)

    Ghazilan, A. L. Ahmad; Mokhtar, H.; Shaik Dawood, M. S. I.; Aminanda, Y.; Ali, J. S. Mohamed

    2017-03-01

    Natural, short, untreated and randomly oriented oil palm empty fruit bunch fiber reinforced epoxy composites were manufactured using vacuum bagging technique with 20% fiber volume composition. The performance of the composite was evaluated as an alternative to synthetic or conventional reinforced composites. Tensile properties such as tensile strength, modulus of elasticity and Poisson’s ratio were compared to the tensile properties of pure epoxy obtained via tensile tests as per ASTM D 638 specifications using Universal Testing Machine INSTRON 5582. The tensile properties of oil palm empty fruit bunch fiber reinforced epoxy composites were lower compared to plain epoxy structure with the decrement in performances of 38% for modulus of elasticity and 61% for tensile strength.

  12. Decohesion models informed by first-principles calculations: The ab initio tensile test

    NASA Astrophysics Data System (ADS)

    Enrique, Raúl A.; Van der Ven, Anton

    2017-10-01

    Extreme deformation and homogeneous fracture can be readily studied via ab initio methods by subjecting crystals to numerical "tensile tests", where the energy of locally stable crystal configurations corresponding to elongated and fractured states are evaluated by means of density functional method calculations. The information obtained can then be used to construct traction curves of cohesive zone models in order to address fracture at the macroscopic scale. In this work, we perform an in depth analysis of traction curves and how ab initio calculations must be interpreted to rigorously parameterize an atomic scale cohesive zone model, using crystalline Ag as an example. Our analysis of traction curves reveal the existence of two qualitatively distinct decohesion criteria: (i) an energy criterion whereby the released elastic energy equals the energy cost of creating two new surfaces and (ii) an instability criterion that occurs at a higher and size independent stress than that of the energy criterion. We find that increasing the size of the simulation cell renders parts of the traction curve inaccessible to ab initio calculations involving the uniform decohesion of the crystal. We also find that the separation distance below which a crack heals is not a material parameter as has been proposed in the past. Finally, we show that a large energy barrier separates the uniformly stressed crystal from the decohered crystal, resolving a paradox predicted by a scaling law based on the energy criterion that implies that large crystals will decohere under vanishingly small stresses. This work clarifies confusion in the literature as to how a cohesive zone model is to be parameterized with ab initio "tensile tests" in the presence of internal relaxations.

  13. Effect of temperature and moisture content on tensile behaviour of false banana fibre (Ensete ventricosum)

    NASA Astrophysics Data System (ADS)

    Mizera, Cestmir; Herak, David; Hrabe, Petr; Kabutey, Abraham

    2017-07-01

    The mechanical behaviour of natural fibres as composite materials can be affected by changes in temperature and moisture content. The aim of this paper was to describe the effect of temperature and moisture content on tensile strength of false banana fibre (Ensete ventricosum) and to determine its water absorption. Samples of fibres were prepared and tested until rupture point with strain rate of 0.05 min-1 at temperature change between -20 and 220°C as well as moisture content between 10 and 90% wb. The water absorption and release of Ensete fibres at 60 and 90% relative humidity was also determined. Results showed that Ensete fibres exhibited stability of tensile strength in the temperature range from 0 to 100°C but the increase of temperature decreased statistically significantly the tensile strength. The effect of moisture content on tensile strength was not statistically significant. The equilibrium moisture content at 60% relative humidity and 25°C was determined.

  14. Experimental and Numerical Study on the Deformation Mechanism in AZ31B Mg Alloy Sheets Under Pulsed Electric-Assisted Tensile and Compressive Tests

    NASA Astrophysics Data System (ADS)

    Lee, Jinwoo; Kim, Se-Jong; Lee, Myoung-Gyu; Song, Jung Han; Choi, Seogou; Han, Heung Nam; Kim, Daeyong

    2016-06-01

    The uniaxial tensile and compressive stress-strain responses of AZ31B magnesium alloy sheet under pulsed electric current are reported. Tension and compression tests with pulsed electric current showed that flow stresses dropped instantaneously when the electric pulses were applied. Thermo-mechanical-electrical finite element analyses were also performed to investigate the effects of Joule heating and electro-plasticity on the flow responses of AZ31B sheets under electric-pulsed tension and compression tests. The proposed finite element simulations could reproduce the measured uniaxial tensile and compressive stress-strain curves under pulsed electric currents, when the temperature-dependent flow stress hardening model and thermal properties of AZ31B sheet were properly described in the simulations. In particular, the simulation results that fit best with experimental results showed that almost 100 pct of the electric current was subject to transform into Joule heating during electrically assisted tensile and compressive tests.

  15. Mechanical shear and tensile characteristics of selected biomass stems

    USDA-ARS?s Scientific Manuscript database

    Mechanical characteristics (stress and energy of tensile and shear modes) of selected biomass stems, such as big bluestem, bromegrass, and Barlow wheat were determined. A high capacity MTI-100K universal testing machine attached with standard tensile clamps and designed fabricated double-shear devic...

  16. High temperature tensile properties of V-4Cr-4Ti

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Zinkle, S.J.; Rowcliffe, A.F.; Stevens, C.O.

    Tensile tests have been performed on V-4Cr-4Ti at 750 and 800 C in order to extend the data base beyond the current limit of 700 C. From comparison with previous measurements, the yield strength is nearly constant and tensile elongations decrease slightly with increasing temperature between 300 and 800 C. The ultimate strength exhibits an apparent maximum near 600 C (attributable to dynamic strain aging) but adequate strength is maintained up to 800 C. The reduction in area measured on tensile specimens remained high ({approximately}80%) for test temperatures up to 800 C, in contrast to previous reported results.

  17. Elevated-temperature tensile and creep properties of several ferritic stainless steels

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.

    1977-01-01

    The elevated-temperature mechanical properties of several ferritic stainless steels were determined. The alloys evaluated included Armco 18SR, GE 1541, and NASA-18T-A. Tensile and creep strength properties at 1073 and 1273 K and residual room temperature tensile properties after creep testing were measured. In addition, 1273 K tensile and creep tests and residual property testing were conducted with Armco 18SR and GE 1541 which were exposed for 200 hours to a severe oxidizing environment in automotive thermal reactors. Aside from the residual tensile properties for Armco 18SR, prior exposure did not affect the mechanical properties of either alloy. The 1273 K creep strength parallel to the sheet-rolling direction was similar for all three alloys. At 1073 K, NASA-18T-A had better creep strength than either Armco 18SR or GE 1541. NASA-18T-A possesses better residual properties after creep testing than either Armco 18SR or Ge 1541.

  18. Energy absorption behavior of polyurea coatings under laser-induced dynamic tensile and mixed-mode loading

    NASA Astrophysics Data System (ADS)

    Jajam, Kailash; Lee, Jaejun; Sottos, Nancy

    2015-06-01

    Energy absorbing, lightweight, thin transparent layers/coatings are desirable in many civilian and military applications such as hurricane resistant windows, personnel face-shields, helmet liners, aircraft canopies, laser shields, blast-tolerant sandwich structures, sound and vibration damping materials to name a few. Polyurea, a class of segmented block copolymer, has attracted recent attention for its energy absorbing properties. However, most of the dynamic property characterization of polyurea is limited to tensile and split-Hopkinson-pressure-bar compression loading experiments with strain rates on the order of 102 and 104 s-1, respectively. In the present work, we report the energy absorption behavior of polyurea thin films (1 to 2 μm) subjected to laser-induced dynamic tensile and mixed-mode loading. The laser-generated high amplitude stress wave propagates through the film in short time frames (15 to 20 ns) leading to very high strain rates (107 to 108 s-1) . The substrate stress, surface velocity and fluence histories are inferred from the displacement fringe data. On comparing input and output fluences, test results indicate significant energy absorption by the polyurea films under both tensile and mixed-mode loading conditions. Microscopic examination reveals distinct changes in failure mechanisms under mixed-mode loading from that observed under pure tensile loading. Office of Naval Research MURI.

  19. Dynamic tensile characterization of a 4330-V steel with kolsky bar techniques.

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Song, Bo; Antoun, Bonnie R.; Connelly, Kevin

    2010-09-01

    There has been increasing demand to understand the stress-strain response as well as damage and failure mechanisms of materials under impact loading condition. Dynamic tensile characterization has been an efficient approach to acquire satisfactory information of mechanical properties including damage and failure of the materials under investigation. However, in order to obtain valid experimental data, reliable tensile experimental techniques at high strain rates are required. This includes not only precise experimental apparatus but also reliable experimental procedures and comprehensive data interpretation. Kolsky bar, originally developed by Kolsky in 1949 [1] for high-rate compressive characterization of materials, has been extended formore » dynamic tensile testing since 1960 [2]. In comparison to Kolsky compression bar, the experimental design of Kolsky tension bar has been much more diversified, particularly in producing high speed tensile pulses in the bars. Moreover, instead of directly sandwiching the cylindrical specimen between the bars in Kolsky bar compression bar experiments, the specimen must be firmly attached to the bar ends in Kolsky tensile bar experiments. A common method is to thread a dumbbell specimen into the ends of the incident and transmission bars. The relatively complicated striking and specimen gripping systems in Kolsky tension bar techniques often lead to disturbance in stress wave propagation in the bars, requiring appropriate interpretation of experimental data. In this study, we employed a modified Kolsky tension bar, newly developed at Sandia National Laboratories, Livermore, CA, to explore the dynamic tensile response of a 4330-V steel. The design of the new Kolsky tension bar has been presented at 2010 SEM Annual Conference [3]. Figures 1 and 2 show the actual photograph and schematic of the Kolsky tension bar, respectively. As shown in Fig. 2, the gun barrel is directly connected to the incident bar with a coupler. The

  20. Tensile experiments and SEM fractography on bovine subchondral bone.

    PubMed

    Braidotti, P; Bemporad, E; D'Alessio, T; Sciuto, S A; Stagni, L

    2000-09-01

    Subchondral bone undecalcified samples, extracted from bovine femoral heads, are subjected to a direct tensile load. The Young's modulus of each sample is determined from repeated tests within the elastic limit. In a last test, the tensile load is increased up to the specimen failure, determining the ultimate tensile strength. The investigation is performed on both dry and wet specimens. The measured Young's modulus for dry samples is 10.3+/-2.5GPa, while that of wet samples is 3.5+/-1.2GPa. The ultimate tensile strengths are 36+/-10 and 30+/-7.5MPa for dry and wet specimens, respectively. SEM micrographs of failure surfaces show characteristic lamellar bone structures, with lamellae composed of calcified collagen fibers. Rudimentary osteon-like structures are also observed. Failure surfaces of wet samples show a marked fiber pull-out, while delamination predominates in dry samples. The obtained results are interpreted on the basis of the deformation mechanisms typical of fiber-reinforced laminated composite materials.

  1. Tensile Properties and Integrity of Clean Room and Low-Modulus Disposable Nitrile Gloves: A Comparison of Two Dissimilar Glove Types

    PubMed Central

    Phalen, Robert N.; Wong, Weng kee

    2012-01-01

    Background: The selection of disposable nitrile exam gloves is complicated by (i) the availability of several types or formulations, (ii) product variability, and (iii) an inability of common quality control tests to detect small holes in the fingers. Differences in polymer formulation (e.g. filler and plasticizer/oil content) and tensile properties are expected to account for much of the observed variability in performance. Objectives: This study evaluated the tensile properties and integrity (leak failure rates) of two glove choices assumed to contain different amounts of plasticizers/oils. The primary aims were to determine if the tensile properties and integrity differed and if associations existed among these factors. Additional physical and chemical properties were evaluated. Methods: Six clean room and five low-modulus products were evaluated using the American Society for Testing and Materials Method D412 and a modified water-leak test to detect holes capable of passing a virus or chemical agent. Results: Significant differences in the leak failure rates and tensile properties existed between the two glove types (P ≤ 0.05). The clean room gloves were about three times more likely to have leak failures (chi-square; P = 0.001). No correlation was observed between leak failures and tensile properties. Solvent extract, an indication of added plasticizer/oil, was not associated with leak failures. However, gloves with a maximum modulus <4 MPa or area density (AD) <11 g cm−2 were about four times less likely to leak. Conclusions: On average, the low-modulus gloves were a better choice for protection against aqueous chemical or biological penetration. The observed variability between glove products indicated that glove selection cannot rely solely on glove type or manufacturer labeling. Measures of modulus and AD may aid in the selection process, in contrast with common measures of tensile strength and elongation at break. PMID:22201179

  2. Tensile properties and integrity of clean room and low-modulus disposable nitrile gloves: a comparison of two dissimilar glove types.

    PubMed

    Phalen, Robert N; Wong, Weng Kee

    2012-05-01

    The selection of disposable nitrile exam gloves is complicated by (i) the availability of several types or formulations, (ii) product variability, and (iii) an inability of common quality control tests to detect small holes in the fingers. Differences in polymer formulation (e.g. filler and plasticizer/oil content) and tensile properties are expected to account for much of the observed variability in performance. This study evaluated the tensile properties and integrity (leak failure rates) of two glove choices assumed to contain different amounts of plasticizers/oils. The primary aims were to determine if the tensile properties and integrity differed and if associations existed among these factors. Additional physical and chemical properties were evaluated. Six clean room and five low-modulus products were evaluated using the American Society for Testing and Materials Method D412 and a modified water-leak test to detect holes capable of passing a virus or chemical agent. Significant differences in the leak failure rates and tensile properties existed between the two glove types (P ≤ 0.05). The clean room gloves were about three times more likely to have leak failures (chi-square; P = 0.001). No correlation was observed between leak failures and tensile properties. Solvent extract, an indication of added plasticizer/oil, was not associated with leak failures. However, gloves with a maximum modulus <4 MPa or area density (AD) <11 g cm(-2) were about four times less likely to leak. On average, the low-modulus gloves were a better choice for protection against aqueous chemical or biological penetration. The observed variability between glove products indicated that glove selection cannot rely solely on glove type or manufacturer labeling. Measures of modulus and AD may aid in the selection process, in contrast with common measures of tensile strength and elongation at break.

  3. Tensile properties of interwoven hemp/PET (Polyethylene Terephthalate) epoxy hybrid composites

    NASA Astrophysics Data System (ADS)

    Ahmad, M. A. A.; Majid, M. S. A.; Ridzuan, M. J. M.; Firdaus, A. Z. A.; Amin, N. A. M.

    2017-10-01

    This paper describes the experimental investigation of the tensile properties of interwoven Hemp/PET hybrid composites. The effect of hybridization of hemp (warp) with PET fibres (weft) on tensile properties was of interest. Hemp and PET fibres were selected as the reinforcing material while epoxy resin was chosen as the matrix. The interwoven Hemp/PET fabric was used to produce hybrid composite using a vacuum infusion process. The tensile test was conducted using Universal Testing Machine in accordance to the ASTM D638. The tensile properties of the interwoven Hemp/PET hybrid composite were then compared with the neat woven hemp/epoxy composite. The results show that the strength of hemp/PET with the warp direction was increased by 8% compared to the neat woven hemp composite. This enhancement of tensile strength was due to the improved interlocking structure of interwoven Hemp/PET hybrid fabric.

  4. Tensile strength decreases and perfusion pressure of 3-holed polyamide epidural catheters increases in long-term epidural infusion.

    PubMed

    Kim, Pascal; Meyer, Urs; Schüpfer, Guido; Rukwied, Roman; Konrad, Christoph; Gerber, Helmut

    2011-01-01

    Epidural analgesia is an established method for pain management. The failure rate is 8% to 12% due to technical difficulties (catheter dislocation and/or disconnection; partial or total catheter occlusion) and management. The mechanical properties of the catheters, like tensile strength and flow rate, may also be affected by the analgesic solution and/or the tissue environment. We investigated the tensile strength and perfusion pressure of new (n=20), perioperatively (n=30), and postoperatively (n=73) used epidural catheters (20-gauge, polyamide, closed tip, 3 side holes; Perifix [B. Braun]). To prevent dislocation, epidural catheters were taped (n=5) or fixed by suture (n=68) to the skin. After removal, mechanical properties were assessed by a tensile-testing machine (INSTRON 4500), and perfusion pressure was measured at flow rates of 10, 20, and 40 mL/h. All catheters demonstrated a 2-step force transmission. Initially, a minimal increase of length could be observed at 15 N followed by an elongation of several cm at additional forces (7 N). Breakage occurred in the control group at 23.5±1.5 N compared with 22.4±1.6 N in perioperative and 22.4±1.7 N in postoperative catheters (P<0.05). Duration of catheter use had no effect on tensile strength, whereas perfusion pressure at clinically used flow rates (10 mL/h) increased significantly from 19±1.3 to 44±72 mm Hg during long-term (≥7 days) epidural analgesia (P<0.05, analysis of variance). Fixation by suture had no influence on tensile strength or perfusion pressure. Epidural catheter use significantly increases the perfusion pressure and decreases the tensile strength. Copyright © 2011 by American Society of Regional Anesthesia and Pain Medicine

  5. The Tensile Properties of Advanced Nickel-Base Disk Superalloys During Quenching Heat Treatments

    NASA Technical Reports Server (NTRS)

    Gabb, Timothy P.; Gayda, John; Kantzos, Pete T.; Biles, Tiffany; Konkel, William

    2001-01-01

    There is a need to increase the temperature capabilities of superalloy turbine disks. This would allow full utilization of higher temperature combustor and airfoil concepts under development. One approach to meet this goal is to modify the processing and chemistry of advanced alloys, while preserving the ability to use rapid cooling supersolvus heat treatments to achieve coarse grain, fine gamma prime microstructures. An important step in this effort is to understand the key high temperature tensile properties of advanced alloys as they exist during supersolvus heat treatments. This could help in projecting cracking tendencies of disks during quenches from supersolvus heat treatments. The objective of this study was to examine the tensile properties of two advanced disk superalloys during simulated quenching heat treatments. Specimens were cooled from the solution heat treatment temperatures at controlled rates, interrupted, and immediately tensile tested at various temperatures. The responses and failure modes were compared and related to the quench cracking tendencies of disk forgings.

  6. The Tensile Strength of Liquid Nitrogen

    NASA Astrophysics Data System (ADS)

    Huang, Jian

    1992-01-01

    The tensile strength of liquids has been a puzzling subject. On the one hand, the classical nucleation theory has met great success in predicting the nucleation rates of superheated liquids. On the other hand, most of reported experimental values of the tensile strength for different liquids are far below the prediction from the classical nucleation theory. In this study, homogeneous nucleation in liquid nitrogen and its tensile strength have been investigated. Different approaches for determining the pressure amplitude were studied carefully. It is shown that Raman-Nath theory, as modified by the introduction of an effective interaction length, can be used to determine the pressure amplitude in the focal plane of a focusing ultrasonic transducer. The results obtained from different diffraction orders are consistent and in good agreement with other approaches including Debye's theory and solving the KZK equation. The measurement of the tensile strength was carried out in a high pressure stainless steel dewar. A High intensity ultrasonic wave was focused into a small volume of liquid nitrogen in a short time period. A probe laser beam passes through the focal region of a concave spherical transducer with small aperture angle and the transmitted light is detected with a photodiode. The pressure amplitude at the focus is calculated based on the acoustic power radiated into the liquid. In the experiment, the electrical signal on the transducer is gated at its resonance frequency with gate widths of 20 mus to 0.2 ms and temperature range from 77 K to near 100 K. The calculated pressure amplitude is in agreement with the prediction of classical nucleation theory for the nucleation rates from 10^6 to 10^ {11} (bubbles/cm^3 sec). This work provides the experimental evidence that the validity of the classical nucleation theory can be extended to the region of the negative pressure up to -90 atm. This is only the second cryogenic liquid to reach the tensile strength

  7. Tensile strength and failure load of sutures for robotic surgery.

    PubMed

    Abiri, Ahmad; Paydar, Omeed; Tao, Anna; LaRocca, Megan; Liu, Kang; Genovese, Bradley; Candler, Robert; Grundfest, Warren S; Dutson, Erik P

    2017-08-01

    Robotic surgical platforms have seen increased use among minimally invasive gastrointestinal surgeons (von Fraunhofer et al. in J Biomed Mater Res 19(5):595-600, 1985. doi: 10.1002/jbm.820190511 ). However, these systems still suffer from lack of haptic feedback, which results in exertion of excessive force, often leading to suture failures (Barbash et al. in Ann Surg 259(1):1-6, 2014. doi: 10.1097/SLA.0b013e3182a5c8b8 ). This work catalogs tensile strength and failure load among commonly used sutures in an effort to prevent robotic surgical consoles from exceeding identified thresholds. Trials were thus conducted on common sutures varying in material type, gauge size, rate of pulling force, and method of applied force. Polydioxanone, Silk, Vicryl, and Prolene, gauges 5-0 to 1-0, were pulled till failure using a commercial mechanical testing system. 2-0 and 3-0 sutures were further tested for the effect of pull rate on failure load at rates of 50, 200, and 400 mm/min. 3-0 sutures were also pulled till failure using a da Vinci robotic surgical system in unlooped, looped, and at the needle body arrangements. Generally, Vicryl and PDS sutures had the highest mechanical strength (47-179 kN/cm 2 ), while Silk had the lowest (40-106 kN/cm 2 ). Larger diameter sutures withstand higher total force, but finer gauges consistently show higher force per unit area. The difference between material types becomes increasingly significant as the diameters decrease. Comparisons of identical suture materials and gauges show 27-50% improvement in the tensile strength over data obtained in 1985 (Ballantyne in Surg Endosc Other Interv Tech 16(10):1389-1402, 2002. doi: 10.1007/s00464-001-8283-7 ). No significant differences were observed when sutures were pulled at different rates. Reduction in suture strength appeared to be strongly affected by the technique used to manipulate the suture. Availability of suture tensile strength and failure load data will help define software safety

  8. Characterization of Damage in Triaxial Braid Composites Under Tensile Loading

    NASA Technical Reports Server (NTRS)

    Littell, Justin D.; Binienda, Wieslaw K.; Roberts, Gary D.; Goldberg, Robert K.

    2009-01-01

    Carbon fiber composites utilizing flattened, large tow yarns in woven or braided forms are being used in many aerospace applications. Their complex fiber architecture and large unit cell size present challenges in both understanding deformation processes and measuring reliable material properties. This report examines composites made using flattened 12k and 24k standard modulus carbon fiber yarns in a 0 /+60 /-60 triaxial braid architecture. Standard straight-sided tensile coupons are tested with the 0 axial braid fibers either parallel with or perpendicular to the applied tensile load (axial or transverse tensile test, respectively). Nonuniform surface strain resulting from the triaxial braid architecture is examined using photogrammetry. Local regions of high strain concentration are examined to identify where failure initiates and to determine the local strain at the time of initiation. Splitting within fiber bundles is the first failure mode observed at low to intermediate strains. For axial tensile tests splitting is primarily in the 60 bias fibers, which were oriented 60 to the applied load. At higher strains, out-of-plane deformation associated with localized delamination between fiber bundles or damage within fiber bundles is observed. For transverse tensile tests, the splitting is primarily in the 0 axial fibers, which were oriented transverse to the applied load. The initiation and accumulation of local damage causes the global transverse stress-strain curves to become nonlinear and causes failure to occur at a reduced ultimate strain. Extensive delamination at the specimen edges is also observed.

  9. Tensile properties of compressed moulded Napier/glass fibre reinforced epoxy composites

    NASA Astrophysics Data System (ADS)

    Fatinah, T. S.; Majid, M. S. Abdul; Ridzuan, M. J. M.; Hong, T. W.; Amin, N. A. M.; Afendi, M.

    2017-10-01

    This paper describes the experimental investigation of the tensile properties of compressed moulded Napier grass fibres reinforced epoxy composites. The effect of treatment 5% sodium hydroxide (NaOH) concentrated solution and hybridization of Napier with CSM E-glass fibres on tensile properties was also studied. The untreated and treated Napier fibres with 25% fibre loading were fabricated with epoxy resin by a cold press process. 7% fibre loading of CSM glass fibre was hybrid as the skin layer for 18% fibre loading of untreated Napier grass fibre. The tensile tests were conducted using Universal Testing Machine in accordance with ASTM D638. The tensile properties of the untreated Napier/epoxy composites were compared with treated Napier/epoxy and untreated Napier/CSM/epoxy composites. The results demonstrated that the tensile performance of untreated Napier fibre composites was significantly improved by both of the modification; alkali treatment and glass fibre hybridization. Napier grass fibres showed promising potentials to be used as reinforcement in the polymer based composites.

  10. Comparative evaluation of tensile strength of Gutta-percha cones with a herbal disinfectant.

    PubMed

    Mahali, Raghunandhan Raju; Dola, Binoy; Tanikonda, Rambabu; Peddireddi, Suresh

    2015-01-01

    To evaluate and compare the tensile strength values and influence of taper on the tensile strength of Gutta-percha (GP) cones after disinfection with sodium hypochlorite (SH) and Aloe vera gel (AV). Sixty GP cones of size 110, 2% taper, 60 GP cones F3 ProTaper, and 60 GP of size 30, 6% taper were obtained from sealed packs as three different groups. Experimental groups were disinfected with 5.25% SH and 90% AV gel except the control group. Tensile strengths of GP were measured using the universal testing machine. The mean tensile strength values for Group IA, IIA and IIIA are 11.8 MPa, 8.69 MPa, and 9.24 MPa, respectively. Results were subjected to statistical analysis one-way analysis of variance test and Tukey post-hoc test. 5.25% SH solutions decreased the tensile strength of GP cones whereas with 90% AV gel it was not significantly altered. Ninety percent Aloe vera gel as a disinfectant does not alter the tensile strength of GP cones.

  11. Stress Relaxation in Tensile Deformation of 304 Stainless Steel

    NASA Astrophysics Data System (ADS)

    Li, Xifeng; Li, Jiaojiao; Ding, Wei; Zhao, Shuangjun; Chen, Jun

    2017-02-01

    Improved ductility by stress relaxation has been reported in different kinds of steels. The influence of stress relaxation and its parameters on the ductility of 304 stainless steel has not been established so far. Stress relaxation behavior during tensile tests at different strain rates is studied in 304 stainless steel. It is observed that stress relaxation can obviously increase the elongation of 304 stainless steel in all cases. The elongation improvement of interrupted tension reaches to 14.9% compared with monotonic tension at 0.05 s-1. Contradicting with the published results, stress drop during stress relaxation increases with strain at all strain rates. It is related with dislocation motion velocity variation and martensitic transformation.

  12. Evaluation of the tensile strength of the human ureter - Preliminary results.

    PubMed

    Shilo, Yaniv; Pichamuthu, Joseph E; Averch, Timothy D; Vorp, David A

    2014-09-15

    Introduction: Ureteral injuries such as avulsion are directly related to mechanical damage of the ureter. Understanding the tensile strength of this tissue may assist in prevention of iatrogenic injuries. Few published studies have looked at the mechanical properties of the animal ureter, and of those none have determined the tensile strength of the human ureter. Therefore, the purpose of this work was to determine the tensile strength of the human ureter. Materials and Methods: We harvested 11 human proximal ureters from patients who were undergoing nephrectomy for either kidney tumors or non-functioning kidney. The specimens were then cut into multiple circumferentially and longitudinally-oriented tissue strips for tensile testing. Strips were uniaxially stretched to failure in a tensile testing machine. The corresponding force and displacement were recorded. Finally, stress at failure was noted as the tensile strength of the sample. Circumferential tensile strength was also compared in the proximal and distal regions of the specimens. Results: The tensile strength of the ureter in circumferential and longitudinal orientations was found to be 457.52±33.74 Ncm-2 and 902.43±122.08 Ncm-2, respectively (p<0.001). The circumferential strength in the proximal portion of the ureter was 409.89±35.13 Ncm-2 in comparison to 502.89±55.85 Ncm-2 in the distal portion (p=0.08). Conclusions: The circumferential tensile strength of the ureter was found to be significantly lower than the longitudinal strength. Circumferential tensile strength was also lower with more proximal parts of the ureter. This information may be important for the design of "intelligent" devices and simulators in order to prevent complications.

  13. Evaluation of the tensile strength of the human ureter--preliminary results.

    PubMed

    Shilo, Yaniv; Pichamuthu, Joseph E; Averch, Timothy D; Vorp, David A

    2014-12-01

    Ureteral injuries such as avulsion are directly related to mechanical damage of the ureter. Understanding the tensile strength of this tissue may assist in prevention of iatrogenic injuries. Few published studies have looked at the mechanical properties of the animal ureter and, of those, none has determined the tensile strength of the human ureter. Therefore, the purpose of this work was to determine the tensile strength of the human ureter. We harvested 11 human proximal ureters from patients who were undergoing nephrectomy for either kidney tumors or nonfunctioning kidney. The specimens were then cut into multiple circumferentially and longitudinally oriented tissue strips for tensile testing. Strips were uniaxially stretched to failure in a tensile testing machine. The corresponding force and displacement were recorded. Finally, stress at failure was noted as the tensile strength of the sample. Circumferential tensile strength was also compared in the proximal and distal regions of the specimens. The tensile strength of the ureter in circumferential and longitudinal orientations was found to be 457.52±33.74 Ncm(-2) and 902.43±122.08 Ncm(-2), respectively (P<0.001). The circumferential strength in the proximal portion of the ureter was 409.89±35.13 Ncm(-2) in comparison with 502.89±55.85 Ncm(-2) in the distal portion (P=0.08). The circumferential tensile strength of the ureter was found to be significantly lower than the longitudinal strength. Circumferential tensile strength was also lower with more proximal parts of the ureter. This information may be important for the design of "intelligent" devices and simulators to prevent complications.

  14. Static and fatigue interlaminar tensile characterization of laminated composites

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Koudela, K.L.; Strait, L.H.; Caiazzo, A.A.

    1997-12-31

    Spool and curved-beam specimens were evaluated to determine the viability of using either one or both of these configurations to characterize the static and fatigue interlaminar tensile behavior of carbon/epoxy laminates. Unidirectional curved-beam and quasi-isotropic spool specimens were fabricated, nondestructively inspected, and statically tested to failure. Tension-tension fatigue tests were conducted at 10 Hz and an R-ratio ({sigma}{sub min}/{sigma}{sub max}) equal to 0.1 for each specimen configuration. The interlaminar tensile strength of the spool specimen was 12% larger than the strength obtained using curved-beam specimens. In addition, data scatter associated with spool specimens was significantly less than the scatter associatedmore » with curved-beam specimens. The difference in data scatter was attributed to the influence of the fabrication process on the quality of the laminates tested. The fatigue limit at 0{sup 7} cycles for both specimen types was shown to be at least 40% of the average interlaminar tensile strength. Based on the results of this study, it was concluded that either the spool or the curved-beam specimens can be used to characterize the interlaminar tensile static and fatigue behavior of carbon/epoxy laminates. However, to obtain the most representative results, the test specimen configuration should be selected so that the specimen fabrication process closely simulates the actual component fabrication process.« less

  15. Low temperature neutron irradiation effects on microstructure and tensile properties of molybdenum

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Li, Meimei; Eldrup, M.; Byun, Thak Sang

    2008-01-01

    Polycrystalline molybdenum was irradiated in the hydraulic tube facility at the High Flux Isotope Reactor to doses ranging from 7.2 x 10{sup -5} to 0.28 dpa at {approx} 80 C. As-irradiated microstructure was characterized by room-temperature electrical resistivity measurements, transmission electron microscopy (TEM) and positron annihilation spectroscopy (PAS). Tensile tests were carried out between -50 and 100 C over the strain rate range 1 x 10{sup -5} to 1 x 10{sup -2} s{sup -1}. Fractography was performed by scanning electron microscopy (SEM), and the deformation microstructure was examined by TEM after tensile testing. Irradiation-induced defects became visible by TEM atmore » {approx}0.001 dpa. Both their density and mean size increased with increasing dose. Submicroscopic three-dimensional cavities were detected by PAS even at {approx}0.0001 dpa. The cavity density increased with increasing dose, while their mean size and size distribution was relatively insensitive to neutron dose. It is suggested that the formation of visible dislocation loops was predominantly a nucleation and growth process, while in-cascade vacancy clustering may be significant in Mo. Neutron irradiation reduced the temperature and strain rate dependence of the yield stress, leading to radiation softening in Mo at lower doses. Irradiation had practically no influence on the magnitude and the temperature and strain rate dependence of the plastic instability stress.« less

  16. Comparison of Tensile Damage Evolution in Ti6A14V Joints Between Laser Beam Welding and Gas Tungsten Arc Welding

    NASA Astrophysics Data System (ADS)

    Gao, Xiao-Long; Zhang, Lin-Jie; Liu, Jing; Zhang, Jian-Xun

    2014-12-01

    The present paper studied the evolution of tensile damage in joints welded using laser beam welding (LBW) and gas tungsten arc welding (TIG) under a uniaxial tensile load. The damage evolution in the LBW joints and TIG-welded joints was studied by using digital image correlation (DIC) technology and monitoring changes in Young's modulus during tensile testing. To study the mechanism of void nucleation and growth in the LBW joints and TIG-welded joints, test specimens with various amounts of plastic deformation were analyzed using a scanning electron microscope (SEM). Compared with TIG-welded joints, LBW-welded joints have a finer microstructure and higher microhardness in the fusion zone. The SEM analysis and DIC test results indicated that the critical strain of void nucleation was greater in the LBW-welded joints than in the TIG-welded joints, while the growth rate of voids was lower in the LBW-welded joints than in the TIG-welded joints. Thus, the damage ratio in the LBW joints was lower than that in the TIG-welded joints during tensile testing. This can be due to the coarser martensitic α' and the application of TC-1 welding rods in the TIG-welded joint.

  17. Tensile and burning properties of clay/phenolic/GF composite and its application

    NASA Astrophysics Data System (ADS)

    Diharjo, Kuncoro; Armunanto, V. Bram; Kristiawan, S. Adi

    2016-03-01

    Composite material has been widely used in automotive due to its properties can be improved by combining with reinforcement, like fiber and particle to enhance mechanical properties and burning resistance. This study aims to investigate the tensile and burning properties of hybrid composite combining glass fiber and clay in phenolic resin. The clay was produced from roof tile rejected by tile industries in Sokka, Kebumen, Indonesia. The composite was made using a press mold method for different number of laminates and orientation of woven-roving-glass-fiber/ WRGF (0/90 and ±45), and the total volume fraction of fiber and clay is constant 40%. The specimens were tested using universal testing machine for tensile properties and burning tests apparatus for burning resistance (time to ignite/ TTI and burning rate/ BR). The enhancing of the Clay/Penolic/GF composite can be performed by the increasing of GF laminates, and the composite with 0/90 orientation of WRGF has higher tensile strength and modulus compared to that with ±45 orientation of WRGF. Both composite with 0/90 and ±45 orientation of WRGF have similar burning resistance (TTI and BR) and the composite containing 13 laminates of WR-GF shows the best burning resistance. According to these properties, this composite has good opportunity to be applied as car body panels or other structure in industries due to save weight and high burning resistance.

  18. Insights into the effects of tensile and compressive loadings on human femur bone.

    PubMed

    Havaldar, Raviraj; Pilli, S C; Putti, B B

    2014-01-01

    Fragile fractures are most likely manifestations of fatigue damage that develop under repetitive loading conditions. Numerous microcracks disperse throughout the bone with the tensile and compressive loads. In this study, tensile and compressive load tests are performed on specimens of both the genders within 19 to 83 years of age and the failure strength is estimated. Fifty five human femur cortical samples are tested. They are divided into various age groups ranging from 19-83 years. Mechanical tests are performed on an Instron 3366 universal testing machine, according to American Society for Testing and Materials International (ASTM) standards. The results show that stress induced in the bone tissue depends on age and gender. It is observed that both tensile and compression strengths reduces as age advances. Compressive strength is more than tensile strength in both the genders. The compression and tensile strength of human femur cortical bone is estimated for both male and female subjecting in the age group of 19-83 years. The fracture toughness increases till 35 years in male and 30 years in female and reduces there after. Mechanical properties of bone are age and gender dependent.

  19. Measurement of the tensile forces during bone lengthening.

    PubMed

    Ohnishi, Isao; Kurokawa, Takahide; Sato, Wakyo; Nakamura, Kozo

    2005-05-01

    The purpose of this study was to investigate the effects of lengthening frequency on mechanical environment in limb lengthening. Tensile forces were continuously monitored using a load sensor attached to a unilateral external fixator. Twenty patients were monitored. Ten patients were with acquired femoral shortening, and five of them underwent quasi-continuous lengthening of 1440 steps per day, and the other five received step lengthening twice a day. The other 10 patients were with achondropalsia. Five of them underwent the same quasi-continuous lengthening, and the other five received the same step lengthening. The circadian change and the daily course of the tensile forces were assessed and compared between quasi-continuous lengthening and step lengthening. As for circadian change, an acute increase in the force took place simultaneously with each step of lengthening in the step-lengthening group, but very little change of the baseline force level was seen during quasi-continuous lengthening. As for daily course of the tensile force, it increased almost linearly in both lengthening frequency groups in the initial stage of lengthening. No significant difference of the average force increment rate in this phase was recognized between the quasi-continuous and step lengthening groups irrespective of the etiologies. The lengthening frequency greatly affected the circadian change of the tensile force, but did not affect the increment rate of the force in the linear phase.

  20. On the tensile strength of soil grains in Hertzian response

    NASA Astrophysics Data System (ADS)

    Nadimi, Sadegh; Fonseca, Joana

    2017-06-01

    The breakage initiation of soil grains is controlled by its tensile capacity. Despite the importance of tensile strength, it is often disregarded due to difficulties in measurement. This paper presents an experimental and numerical investigation on the effect of tensile strength on Hertzian response of a single soil grain. Hertz theory is commonly used in numerical simulation to present the contact constitutive behaviour of a purely elastic grain under normal loading. This normal force:displacement comes from stress distribution and concentration inside the grain. When the stress reaches the tensile capacity, a crack initiates. A series of numerical tests have been conducted to determine the sensitivity of Hertzian response to the selected tensile strength used as an input data. An elastic-damage constitutive model has been employed for spherical grains in a combined finite-discrete element framework. The interpretation of results was enriched by considering previous theoretical work. In addition, systematic experimental tests have been carried out on both spherical glass beads and grains of two different sands, i.e. Leighton Buzzard silica sand and coarse carbonate sand from Persian Gulf. The preliminary results suggest that lower tensile strength leads to a softer response under normal loading. The wider range of responses obtained for the carbonate sand, are believed to be related to the large variety of grain shape associated with bioclastic origin of the constituent grains.

  1. Tensile bond strength of an adhesive resin cement to different alloys having various surface treatments.

    PubMed

    Abreu, Amara; Loza, Maria A; Elias, Augusto; Mukhopadhyay, Siuli; Looney, Stephen; Rueggeberg, Frederick A

    2009-02-01

    The ability of a resin cement to bond to a restorative alloy is critical for maximal crown retention to nonideal preparations. Surface treatment and metal type may have an important role in optimizing resin-to-metal strength. The purpose of this study was to examine the effect of surface pretreatment on the tensile strength of base and noble metals bonded using a conventional resin cement. Cylindrical plastic rods (9.5 mm in diameter), cast in base (Rexillium NBF) or noble metal (IPS d.SIGN 53), were divided into rods 10 mm in length (n=10-12). Specimens were heated in a porcelain furnace to create an oxide layer. Test specimens were further subjected to airborne-particle abrasion (50-microm Al(2)O(3) particles) alone or with the application of a metal primer (Alloy Primer). Similarly treated rod ends were joined using resin cement (RelyX ARC), thermocycled (x500, 5 degrees -55 degrees C) and stored (24 hours, 37 degrees C) before debonding using a universal testing machine. Debond strength and failure site were recorded. Rank-based ANOVA for unbalanced designs was used to test for significant interaction (alpha=.050). Each pair of treatments was compared separately for each metal (Bonferroni-adjusted significance level of .0083, overall error rate for comparisons, .05). The 2 metals were compared separately for each of the 3 treatments using an adjusted significance level of .017, maintaining an overall error rate of .05. A multinomial logit model was used to describe the effect of metal type and surface pretreatment on failure site location (alpha=.05). Interaction between metal type and surface pretreatment was significant for stress values (P=.019). Metal type did not significantly affect tensile bond strength for any of the compared surface pretreatments. Metal primer significantly improved tensile bond strength for each metal type. Most failures tended to occur as either adhesive or mixed in nature. Metal primer application significantly enhanced tensile bond

  2. Improved Kolsky tension bar for high-rate tensile characterization of materials

    NASA Astrophysics Data System (ADS)

    Song, Bo; Antoun, Bonnie R.; Connelly, Kevin; Korellis, John; Lu, Wei-Yang

    2011-04-01

    A new Kolsky tension bar has been re-designed and developed at Sandia National Laboratories, CA. The new design uses the concept that a solid striker is fired to impact an end cap attached to the open end of the gun barrel to generate dynamic tensile loading. The gun barrel here serves as part of the loading device. The incident bar that is connected to the gun barrel and the transmission bar follow the design similar to the Kolsky compression bar. The bar supporting and aligning systems are the same as those in the Kolsky compression bar design described by Song et al (2009 Meas. Sci. Technol. 20 115701). Due to the connection complication among the gun barrel, bars and specimen, stress-wave propagation in the new Kolsky tension bar system is comprehensively analyzed. Based on the stress-wave analysis, the strain gage location on the incident bar needs to be carefully determined. A highly precise laser-beam measurement system is recommended to directly measure the displacement of the incident bar end. Dynamic tensile characterization of a 4330-V steel using this new Kolsky tension bar is presented as an example.

  3. Experimental Investigation of Tensile Test on Connection of Cold-formed Cut-curved Steel Section

    NASA Astrophysics Data System (ADS)

    Sani, Mohd Syahrul Hisyam Mohd; Muftah, Fadhluhartini; Rahman, Nurul Farraheeda Abdul; Fakri Muda, Mohd

    2017-08-01

    Cold-formed steel (CFS) is widely used as structural and non-structural components such as roof trusses and purlin. A CFS channel section with double intermediate web stiffener and lipped is chosen based on the broader usage in roof truss construction. CFS section is cut to form cold-formed pre-cut-curved steel section and lastly strengthened by several types of method or likely known as connection to establish the cold-formed cut-curved steel (CFCCS) section. CFCCS is proposed to be used as a top chord section in the roof truss system. The CFCCS is to resist the buckling phenomena of the roof truss structure and reduced the compression effect on the top chord. The tensile test connection of CFCCS section, especially at the flange element with eight types of connection by welding, plate with self-drilling screw and combination is investigated. The flange element is the weakest part that must be solved first other than the web element because they are being cut totally, 100% of their length for curving process. The testing is done using a universal testing machine for a tensile load. From the experiment, specimen with full welding has shown as a good result with an ultimate load of 13.37 kN and reported having 35.41% when compared with normal specimen without any of connection methods. Furthermore, the experimental result is distinguished by using Eurocode 3. The failure of a full welding specimen is due to breaking at the welding location. Additionally, all specimens with either full weld or spot weld or combination failed due to breaking on weld connection, but specimen with flange plate and self-drilling screw failed due to tilting and bearing. Finally, the full welding specimen is chosen as a good connection to perform the strengthening method of CFCCS section.

  4. Selective Laser Melting Produced Ti-6Al-4V: Post-Process Heat Treatments to Achieve Superior Tensile Properties

    PubMed Central

    Becker, Thorsten H.

    2018-01-01

    Current post-process heat treatments applied to selective laser melting produced Ti-6Al-4V do not achieve the same microstructure and therefore superior tensile behaviour of thermomechanical processed wrought Ti-6Al-4V. Due to the growing demand for selective laser melting produced parts in industry, research and development towards improved mechanical properties is ongoing. This study is aimed at developing post-process annealing strategies to improve tensile behaviour of selective laser melting produced Ti-6Al-4V parts. Optical and electron microscopy was used to study α grain morphology as a function of annealing temperature, hold time and cooling rate. Quasi-static uniaxial tensile tests were used to measure tensile behaviour of different annealed parts. It was found that elongated α’/α grains can be fragmented into equiaxial grains through applying a high temperature annealing strategy. It is shown that bi-modal microstructures achieve a superior tensile ductility to current heat treated selective laser melting produced Ti-6Al-4V samples. PMID:29342079

  5. Effect of Strain Rate on Mechanical Properties of Wrought Sintered Tungsten at Temperatures above 2500 F

    NASA Technical Reports Server (NTRS)

    Sikora, Paul F.; Hall, Robert W.

    1961-01-01

    Specimens of wrought sintered commercially pure tungsten were made from 1/8-inch swaged rods. All the specimens were recrystallized at 4050 F for 1 hour prior to testing at temperatures from 2500 to 4000 F at various strain rates from 0.002 to 20 inches per inch per minute. Results showed that, at a constant temperature, increasing the strain rate increased the ultimate tensile strength significantly. The effects of both strain rate and temperature on the ultimate tensile strength of tungsten may be correlated by the linear parameter method of Manson and Haferd and may be used to predict the ultimate tensile strength at higher temperatures, 4500 and 5000 F. As previously reported, ductility, as measured by reduction of area in a tensile test, decreases with increasing temperature above about 3000 F. Increasing the strain rate at temperatures above 3000 F increases the ductility. Fractures are generally transgranular at the higher strain rates and intergranular at the lower strain rates.

  6. The tensile properties of single sugar palm (Arenga pinnata) fibre

    NASA Astrophysics Data System (ADS)

    Bachtiar, D.; Sapuan, S. M.; Zainudin, E. S.; Khalina, A.; Dahlan, K. Z. M.

    2010-05-01

    This paper presents a brief description and characterization of the sugar palm fibres, still rare in the scientific community, compared to other natural fibres employed in polymeric composites. Sugar palm fibres are cellulose-based fibres extracted from the Arenga pinnata plant. The characterization consists of tensile test and the morphological examination. The average tensile properties results of fibres such as Young's modulus is equal to 3.69 GPa, tensile strength is equal to 190.29 MPa, and strain at failure is equal to 19.6%.

  7. Shore hardness and tensile bond strength of long-term soft denture lining materials.

    PubMed

    Kim, Bong-Jun; Yang, Hong-So; Chun, Min-Geoung; Park, Yeong-Joon

    2014-11-01

    Reduced softness and separation from the denture base are the most significant problems of long-term soft lining materials. The purpose of this study was to evaluate the durometer Shore A hardness and tensile bond strength of long-term soft denture lining materials and to investigate the correlation between these 2 properties. A group of 7 soft lining materials, 6 silicone based (Dentusil, GC Reline Soft, GC Reline Ultrasoft, Mucopren Soft, Mucosoft, Sofreliner Tough) and 1 acrylic resin based (Durabase), were evaluated for durometer Shore A hardness and tensile bond strength to heat-polymerized denture base resin (Lucitone 199). A specially designed split mold and loading assembly with a swivel connector were used for the durometer Shore A hardness test and tensile bond strength test to improve accuracy and facilitate measurement. Three specimens of each product were stored in a 37°C water bath, and durometer Shore A hardness tests were carried out after 24 hours and 28 days. A tensile bond strength test was carried out for 10 specimens of each product, which were stored in a 37°C water bath for 24 hours before the test. Repeated-measures ANOVA, the Kruskal-Wallis and Duncan multiple range tests, and the Spearman correlation were used for statistical analyses. The repeated-measures ANOVA found significant durometer Shore A hardness differences for the materials (P<.001) and the interaction effect (aging×materials) (P<.001). GC Reline Ultrasoft showed the lowest mean durometer Shore A hardness (21.30 ±0.29 for 24 hours, 34.73 ±0.47 for 28 days), and GC Reline Soft showed the highest mean durometer Shore A hardness (50.13 ±0.48 for 24 hours, 57.20 ±0.28 for 28 days). The Kruskal-Wallis test found a significant difference in the mean tensile bond strength values (P<.001). GC Reline Ultrasoft (0.82 ±0.32 MPa) and Mucopren Soft (0.96 ±0.46 MPa) had a significantly lower mean tensile bond strength (P<.05). GC Reline Soft had the highest mean tensile bond

  8. Evaluation of the histological and mechanical features of tendon healing in a rabbit model with the use of second-harmonic-generation imaging and tensile testing.

    PubMed

    Hase, E; Sato, K; Yonekura, D; Minamikawa, T; Takahashi, M; Yasui, T

    2016-11-01

    This study aimed to evaluate the histological and mechanical features of tendon healing in a rabbit model with second-harmonic-generation (SHG) imaging and tensile testing. A total of eight male Japanese white rabbits were used for this study. The flexor digitorum tendons in their right leg were sharply transected, and then were repaired by intratendinous stitching. At four weeks post-operatively, the rabbits were killed and the flexor digitorum tendons in both right and left legs were excised and used as specimens for tendon healing (n = 8) and control (n = 8), respectively. Each specimen was examined by SHG imaging, followed by tensile testing, and the results of the two testing modalities were assessed for correlation. While the SHG light intensity of the healing tendon samples was significantly lower than that of the uninjured tendon samples, 2D Fourier transform SHG images showed a clear difference in collagen fibre structure between the uninjured and the healing samples, and among the healing samples. The mean intensity of the SHG image showed a moderate correlation (R 2 = 0.37) with Young's modulus obtained from the tensile testing. Our results indicate that SHG microscopy may be a potential indicator of tendon healing.Cite this article: E. Hase, K. Sato, D. Yonekura, T. Minamikawa, M. Takahashi, T. Yasui. Evaluation of the histological and mechanical features of tendon healing in a rabbit model with the use of second-harmonic-generation imaging and tensile testing. Bone Joint Res 2016;5:577-585. DOI: 10.1302/2046-3758.511.BJR-2016-0162.R1. © 2016 Yasui et al.

  9. Investigation of the Microstructure Evolution in a Fe-17Mn-1.5Al-0.3C Steel via In Situ Synchrotron X-ray Diffraction during a Tensile Test

    PubMed Central

    Song, Wenwen; Bleck, Wolfgang

    2017-01-01

    The quantitative characterization of the microstructure evolution in high-Mn steel during deformation is of great importance to understanding its strain-hardening behavior. In the current study, in situ high-energy synchrotron X-ray diffraction was employed to characterize the microstructure evolution in a Fe-17Mn-1.5Al-0.3C steel during a tensile test. The microstructure at different engineering strain levels—in terms of ε-martensite and α’-martensite volume fractions, the stacking fault probability, and the twin fault probability—was analyzed by the Rietveld refinement method. The Fe-17Mn-1.5Al-0.3C steel exhibits a high ultimate tensile strength with a superior uniform elongation and a high strain-hardening rate. The remaining high strain-hardening rate at the strain level about 0.025 to 0.35 results from ε-martensite dominant transformation-induced-plasticity (TRIP) effect. The increase in the strain-hardening rate at the strain level around 0.35 to 0.43 is attributed to the synergetic α’-martensite dominant TRIP and twinning-induced-plasticity (TWIP) effects. An evaluation of the stacking fault energy (SFE) of the Fe-17Mn-1.5Al-0.3C steel by the synchrotron measurements shows good agreement with the thermodynamic calculation of the SFE. PMID:28946692

  10. Investigation of the Microstructure Evolution in a Fe-17Mn-1.5Al-0.3C Steel via In Situ Synchrotron X-ray Diffraction during a Tensile Test.

    PubMed

    Ma, Yan; Song, Wenwen; Bleck, Wolfgang

    2017-09-25

    The quantitative characterization of the microstructure evolution in high-Mn steel during deformation is of great importance to understanding its strain-hardening behavior. In the current study, in situ high-energy synchrotron X-ray diffraction was employed to characterize the microstructure evolution in a Fe-17Mn-1.5Al-0.3C steel during a tensile test. The microstructure at different engineering strain levels-in terms of ε-martensite and α'-martensite volume fractions, the stacking fault probability, and the twin fault probability-was analyzed by the Rietveld refinement method. The Fe-17Mn-1.5Al-0.3C steel exhibits a high ultimate tensile strength with a superior uniform elongation and a high strain-hardening rate. The remaining high strain-hardening rate at the strain level about 0.025 to 0.35 results from ε-martensite dominant transformation-induced-plasticity (TRIP) effect. The increase in the strain-hardening rate at the strain level around 0.35 to 0.43 is attributed to the synergetic α'-martensite dominant TRIP and twinning-induced-plasticity (TWIP) effects. An evaluation of the stacking fault energy (SFE) of the Fe-17Mn-1.5Al-0.3C steel by the synchrotron measurements shows good agreement with the thermodynamic calculation of the SFE.

  11. Effect of bending on the room-temperature tensile strengths of structural ceramics

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Jenkins, M.G.

    1992-01-01

    Results for nearly fifty, room-temperature tensile tests conducted on two advanced, monolithic silicon nitride ceramics are evaluated for the effects of bending and application of various Weibull statistical analyses. Two specimen gripping systems (straight collet and tapered collet) were evaluated for both success in producing gage section failures and tendency to minimize bending at failure. Specimen fabrication and grinding technique consderations are briefly reviewed and related to their effects on successful tensile tests. Ultimate tensile strengths are related to the bending measured at specimen failure and the effects of the gripping system on bending are discussed. Finally, comparisons are mademore » between the use of censored and uncensored data sample sets for determining the maximum likelihood estimates of the Weibull parameters from the tensile strength distributions.« less

  12. Effect of bending on the room-temperature tensile strengths of structural ceramics

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Jenkins, M.G.

    1992-07-01

    Results for nearly fifty, room-temperature tensile tests conducted on two advanced, monolithic silicon nitride ceramics are evaluated for the effects of bending and application of various Weibull statistical analyses. Two specimen gripping systems (straight collet and tapered collet) were evaluated for both success in producing gage section failures and tendency to minimize bending at failure. Specimen fabrication and grinding technique consderations are briefly reviewed and related to their effects on successful tensile tests. Ultimate tensile strengths are related to the bending measured at specimen failure and the effects of the gripping system on bending are discussed. Finally, comparisons are mademore » between the use of censored and uncensored data sample sets for determining the maximum likelihood estimates of the Weibull parameters from the tensile strength distributions.« less

  13. The Effect of Gap Angle on Tensile Strength of Preceramic Base Metal Solder Joints.

    PubMed

    Fattahi, Farnaz; Hashemi Ardakani, Zahra; Hashemi Ardakani, Maryam

    2015-12-01

    Soldering is a process commonly used in fabricating dental prosthesis. Since most soldered prosthesis fail at the solder joints; the joint strength is of utmost importance. The purpose of this study was to evaluate the effect of gap angle on the tensile strength of base metal solder joints. A total number of 40 Ni-Cr samples were fabricated according to ADA/ISO 9693 specifications for tensile test. Samples were cut at the midpoint of the bar, and were placed at the considered angles by employing an explicitly designed device. They were divided into 4 groups regarding the gap angle; Group C (control group) with parallel gap on steady distance of 0.2mm, Group 1: 10°, Group 2: 20°, and Group3: 30° gap angles. When soldered, the specimens were all tested for tensile strength using a universal testing machine at a cross-head speed of 0.5 mm/min with a preload of 10N. Kruskal-Wallis H test was used to compare tensile strength among the groups (p< 0.05). The mean tensile strength values obtained from the study groups were respectively 307.84, 391.50, 365.18, and 368.86 MPa. The tensile strength was not statistically different among the four groups in general (p≤ 0.490). Making the gap angular at the solder joints and the subsequent unsteady increase of the gap distance would not change the tensile strength of the joint.

  14. Determination of necking time in tensile test specimens, under high-temperature creep conditions, subjected to distribution of stresses over the cross-section

    NASA Astrophysics Data System (ADS)

    Lokoshchenko, A.; Teraud, W.

    2018-04-01

    The work describes an experimental research of creep of cylindrical tensile test specimens made of aluminum alloy D16T at a constant temperature of 400°C. The issue to be examined was the necking at different values of initial tensile stresses. The use of a developed noncontacting measuring system allowed us to see variations in the specimen shape and to estimate the true stress in various times. Based on the obtained experimental data, several criteria were proposed for describing the point of time at which the necking occurs (necking point). Calculations were carried out at various values of the parameters in these criteria. The relative interval of deformation time in which the test specimen is uniformly stretched was also determined.

  15. Effect of Root Moisture Content and Diameter on Root Tensile Properties.

    PubMed

    Yang, Yuanjun; Chen, Lihua; Li, Ning; Zhang, Qiufen

    2016-01-01

    The stabilization of slopes by vegetation has been a topical issue for many years. Root mechanical characteristics significantly influence soil reinforcement; therefore it is necessary to research into the indicators of root tensile properties. In this study, we explored the influence of root moisture content on tensile resistance and strength with different root diameters and for different tree species. Betula platyphylla, Quercus mongolica, Pinus tabulaeformis, and Larix gmelinii, the most popular tree species used for slope stabilization in the rocky mountainous areas of northern China, were used in this study. A tensile test was conducted after root samples were grouped by diameter and moisture content. The results showedthat:1) root moisture content had a significant influence on tensile properties; 2) slightly loss of root moisture content could enhance tensile strength, but too much loss of water resulted in weaker capacity for root elongation, and consequently reduced tensile strength; 3) root diameter had a strong positive correlation with tensile resistance; and4) the roots of Betula platyphylla had the best tensile properties when both diameter and moisture content being controlled. These findings improve our understanding of root tensile properties with root size and moisture, and could be useful for slope stabilization using vegetation.

  16. Effect of Root Moisture Content and Diameter on Root Tensile Properties

    PubMed Central

    Yang, Yuanjun; Chen, Lihua; Li, Ning; Zhang, Qiufen

    2016-01-01

    The stabilization of slopes by vegetation has been a topical issue for many years. Root mechanical characteristics significantly influence soil reinforcement; therefore it is necessary to research into the indicators of root tensile properties. In this study, we explored the influence of root moisture content on tensile resistance and strength with different root diameters and for different tree species. Betula platyphylla, Quercus mongolica, Pinus tabulaeformis, and Larix gmelinii, the most popular tree species used for slope stabilization in the rocky mountainous areas of northern China, were used in this study. A tensile test was conducted after root samples were grouped by diameter and moisture content. The results showedthat:1) root moisture content had a significant influence on tensile properties; 2) slightly loss of root moisture content could enhance tensile strength, but too much loss of water resulted in weaker capacity for root elongation, and consequently reduced tensile strength; 3) root diameter had a strong positive correlation with tensile resistance; and4) the roots of Betula platyphylla had the best tensile properties when both diameter and moisture content being controlled. These findings improve our understanding of root tensile properties with root size and moisture, and could be useful for slope stabilization using vegetation. PMID:27003872

  17. Ultra-high temperature tensile properties of ODS steel claddings under severe accident conditions

    NASA Astrophysics Data System (ADS)

    Yano, Y.; Tanno, T.; Oka, H.; Ohtsuka, S.; Inoue, T.; Kato, S.; Furukawa, T.; Uwaba, T.; Kaito, T.; Ukai, S.; Oono, N.; Kimura, A.; Hayashi, S.; Torimaru, T.

    2017-04-01

    Ultra-high temperature ring tensile tests were performed to investigate the tensile behavior of oxide dispersion strengthened (ODS) steel claddings and wrapper materials under severe accident conditions with temperatures ranging from room temperature to 1400 °C which is close to the melting point of core materials. The experimental results showed that the tensile strength of 9Cr-ODS steel claddings was highest in the core materials at ultra-high temperatures of 900-1200 °C, but there was significant degradation in the tensile strength of 9Cr-ODS steel claddings above 1200 °C. This degradation was attributed to grain boundary sliding deformation with γ/δ transformation, which is associated with reduced ductility. By contrast, the tensile strength of recrystallized 12Cr-ODS and FeCrAl-ODS steel claddings retained its high value above 1200 °C, unlike the other tested materials.

  18. Relationship between the tensile strengths and diameters of human umbilical cords.

    PubMed

    Fernando, D M G; Gamage, S M K; Ranmohottige, S; Weerakkody, I; Abeyruwan, H; Parakrama, H

    2018-05-01

    Mothers of alleged infanticides might claim that umbilical cord broke during precipitate delivery causing injuries detected on baby at autopsy. There is paucity of evidence regarding this possibility. The objective of the study was to determine relationship between tensile strength and diameter or weight per unit length of cord. Diameters and weights per unit length of fresh umbilical cords were determined. Tensile strengths were measured by Hounsfield Testing Machine. Relationship between tensile strength versus cord diameter and weight per unit length were analyzed. Of 122 cords, average tensile strength, diameter and weight per centimeter were 50.4 N, 7.73 mm and 6.87 g respectively. The tensile strengths were directly proportional to diameter. There was no association between tensile strength and weight per centimeter. Measurement of the diameter of cord is important during autopsy to predict tensile strength and thereby to presume whether cord could have broken by the weight of the baby. Copyright © 2018 Elsevier Ltd and Faculty of Forensic and Legal Medicine. All rights reserved.

  19. Effect of gap distance on tensile strength of preceramic base metal solder joints.

    PubMed

    Fattahi, Farnaz; Motamedi, Milad

    2011-01-01

    In order to fabricate prostheses with high accuracy and durability, soldering techniques have been introduced to clinical dentistry. However, these prostheses always fail at their solder joints. The purpose of this study was to evaluate the effect of gap distance on the tensile strength of base metal solder joints. Based on ADA/ISO 9693 specifications for tensile test, 40 specimens were fabricated from a Ni-Cr alloy and cut at the midpoint of 3-mm diameter bar and placed at desired positions by a specially designed device. The specimens were divided into four groups of 10 samples according to the desired solder gap distance: Group1: 0.1mm; Group2: 0.25mm; Group3: 0.5mm; and Group4: 0.75mm. After soldering, specimens were tested for tensile strength by a universal testing machine at a cross-head speed of 0.5mm/min with a preload of 10N. The mean tensile strength values of the groups were 162, 307.8, 206.1 and 336.7 MPa, respectively. The group with 0.75-mm gap had the highest and the group with 0.1-mm gap had the lowest tensile strength. Bonferroni test showed that Group1 and Group4 had statistically different values (P=0.023), but the differences between other groups were not sig-nificant at a significance level of 0.05. There was no direct relationship between increasing soldering gap distance and tensile strength of the solder joints.

  20. Mechanical tensile properties of the anterolateral ligament.

    PubMed

    Zens, Martin; Feucht, Matthias J; Ruhhammer, Johannes; Bernstein, Anke; Mayr, Hermann O; Südkamp, Norbert P; Woias, Peter; Niemeyer, Philipp

    2015-12-01

    In a noticeable percentage of patients anterolateral rotational instabilities (ALRI) remain after an isolated ACL reconstruction. Those instabilities may occur due to an insufficiently directed damage of anterolateral structures that is often associated with ACL ruptures. Recent publications describe an anatomical structure, termed the anterolateral ligament (ALL), and suggest that this ligament plays a significant role in the pathogenesis of ALRI of the knee joint. However, only limited knowledge about the biomechanical characteristics and tensile properties of the anterolateral ligament exists. The anterolateral ligament was dissected in four fresh-frozen human cadaveric specimens and all surrounding tissue removed. The initial length of the anterolateral ligament was measured using a digital caliper. Tensile tests with load to failure were performed using a materials testing machine. The explanted anterolateral ligaments were histologically examined to measure the cross-sectional area. The mean ultimate load to failure of the anterolateral ligament was 49.90 N (± 14.62 N) and the mean ultimate strain was 35.96% (± 4.47%). The mean length of the ligament was 33.08 mm (± 2.24) and the mean cross-sectional area was 1.54 m m (2) (± 0.48 m m (2)). Including the areal measurements the maximum tension was calculated to be 32.78 [Formula: see text] (± 4.04 [Formula: see text]). The anterolateral ligament is an anatomical structure with tensile properties that are considerably weaker compared to other peripheral structures of the knee. Knowledge of the anterolateral ligament's tensile strengths may help to better understand its function and with graft choices for reconstruction procedures.

  1. An in situ tensile tester for studying electrochemical repassivation behavior: Fabrication and challenges

    NASA Astrophysics Data System (ADS)

    Neelakantan, Lakshman; Schönberger, Bernd; Eggeler, Gunther; Hassel, Achim Walter

    2010-03-01

    An in situ tensile rig is proposed, which allows performing electrochemical (repassivation) experiments during dynamic mechanical testing of wires. Utilizing the basic components of a conventional tensile tester, a custom-made minitensile rig was designed and fabricated. The maximal force that can be measured by the force sensor is 80 N, with a sensitivity of 0.5 mV/V. The maximum travel range of the crosshead induced by the motor is 10 mm with a minimum step size of 0.5 nm. The functionality of the tensile test rig was validated by investigating Cu and shape memory NiTi wires. Wires of lengths between 40 and 50 mm with varying gauge lengths can be tested. An interface between wire and electrochemical setup (noncontact) with a smart arrangement of electrodes facilitated the electrochemical measurements during tensile loading. Preliminary results on the repassivation behavior of Al wire are reported.

  2. The dynamic properties behavior of high strength concrete under different strain rate

    NASA Astrophysics Data System (ADS)

    Abdullah, Hasballah; Husin, Saiful; Umar, Hamdani; Rizal, Samsul

    2005-04-01

    This paper present a number experimental data and numerical technique used in the dynamic behavior of high strength concrete. A testing device is presented for the experimental study of dynamic behavior material under high strain rates. The specimen is loaded by means of a high carbon steel Hopkinson pressure bar (40 mm diameter, 3000 mm long input bar and 1500 mm long out put bar) allowing for the testing of specimen diameter is large enough in relation to the size of aggregates. The other method also proposed for measuring tensile strength, the measurement method based on the superposition and concentration of tensile stress wave reflected both from the free-free ends of striking bar and the specimen bar. The compression Hopkinson bar test, the impact tensile test of high strength concrete bars are performed, together with compression static strength test. In addition, the relation between break position under finite element simulation and impact tensile strength are examined. The three-dimensional simulation of the specimen under transient loading are presented and comparisons between the experimental and numerical simulation on strain rate effects of constitutive law use in experimental are study.

  3. Tensile strength of Fe-Ni and Mg-Al nanocomposites: Molecular dynamic simulations

    NASA Astrophysics Data System (ADS)

    Pogorelko, V. V.; Mayer, A. E.

    2018-01-01

    In this work, molecular dynamic simulations of the tensile strength of Fe-Ni and Mg-Al nanocomposites in the conditions of high-rate uniaxial tension were carried out. Two different mechanisms of fracture were identified. In the case of nickel inclusion in iron matrix, the fracture begins on the interface between the inclusion and the matrix, a formed void penetrates both into the inclusion and into the matrix; presence of inclusion reduces the tensile strength. In the case of aluminum inclusion in magnesium matrix, fracture takes place into magnesium matrix and does not touch the inclusion; presence of inclusion has practically no effect on the tensile strength. Molecular dynamic simulations were carried out in a wide range of strain rates and temperatures.

  4. Calculation for tensile strength and fracture toughness of granite with three kinds of grain sizes using three-point-bending test.

    PubMed

    Yu, Miao; Wei, Chenhui; Niu, Leilei; Li, Shaohua; Yu, Yongjun

    2018-01-01

    Tensile strength and fracture toughness, important parameters of the rock for engineering applications are difficult to measure. Thus this paper selected three kinds of granite samples (grain sizes = 1.01mm, 2.12mm and 3mm), used the combined experiments of physical and numerical simulation (RFPA-DIP version) to conduct three-point-bending (3-p-b) tests with different notches and introduced the acoustic emission monitor system to analyze the fracture mechanism around the notch tips. To study the effects of grain size on the tensile strength and toughness of rock samples, a modified fracture model was established linking fictitious crack to the grain size so that the microstructure of the specimens and fictitious crack growth can be considered together. The fractal method was introduced to represent microstructure of three kinds of granites and used to determine the length of fictitious crack. It is a simple and novel method to calculate the tensile strength and fracture toughness directly. Finally, the theoretical model was verified by the comparison to the numerical experiments by calculating the nominal strength σn and maximum loads Pmax.

  5. Strain-rate behavior in tension of the tempered martensitic reduced activation steel Eurofer97

    NASA Astrophysics Data System (ADS)

    Cadoni, Ezio; Dotta, Matteo; Forni, Daniele; Spätig, Philippe

    2011-07-01

    The tensile properties of the high-chromium tempered martensitic reduced activation steel Eurofer97 were determined from tests carried out over a wide range of strain-rates on cylindrical specimens. The quasi-static tests were performed with a universal electro-mechanical machine, whereas a hydro-pneumatic machine and a JRC-split Hopkinson tensile bar apparatus were used for medium and high strain-rates respectively. This tempered martensitic stainless steel showed significant strain-rate sensitivity. The constitutive behavior was investigated within a framework of dislocations dynamics model using Kock's approach. The parameters of the model were determined and then used to predict the deformation range of the tensile deformation stability. A very good agreement between the experimental results and predictions of the model was found.

  6. Re-examination of the Present Stress State of the Atera Fault, Central Japan, Based on the Calibrated Crustal Stress Data of Hydraulic Fracturing Test by Measuring the Tensile Strength of Rocks

    NASA Astrophysics Data System (ADS)

    Yamashita, F.; Mizoguchi, K.; Fukuyama, E.; Omura, K.

    2008-12-01

    To infer the activity and physical state of intraplate faults in Japan, we re-examined the crustal stress with the hydraulic fracturing test by measuring the tensile strength of rocks. The tensile strength was measured by fracturing hollow cylindrical rock samples (inner and outer radius are 25.0-25.2 mm and 55.1-101.5 mm, respectively, length is 137.0-140.1 mm) which were obtained close to the in situ stress measurement locations by pressurizing the inner hole of the sample. Confining pressure is not applied to the samples in this test. To check the reliability and accuracy of this test, we conducted similar experiments with the standard rock sample (Inada granite) whose physical property is well known. Then, we measured the tensile strength of all available core samples including the Atera fault (at Ueno, Fukuoka, and Hatajiri), the Atotsugawa fault, and the Nojima fault (at Hirabayashi, Iwaya and Kabutoyama), in central Japan, which had been obtained by the National Research Institute for Earth Science and Disaster Prevention (NIED) by the stress measurement with the hydraulic fracturing method. The measured tensile strength data reveals that the in situ re- opening pressure, which is one of the parameters needed for the determination of the maximum in situ horizontal stress, was obviously biased. We re-estimated the re-opening pressure using the measured tensile strength and the in situ breakdown pressure, and re-calculated the in situ stress around the Atera fault. Although the past dislocation of the Atera fault has been considered to be left lateral from the geographical features around the fault, the re-estimated stress suggests that the present dislocation of the Atera fault is right lateral. And the shear stress decreases from the fault. The right lateral dislocation is also supported by the present-day horizontal crustal deformation observed by the triangular and GPS surveys by Geographical Survey Institute in Japan. Therefore, the dislocation direction

  7. Effects of Long-Term Thermal Exposure on Commercially Pure Titanium Grade 2 Elevated-Temperature Tensile Properties

    NASA Technical Reports Server (NTRS)

    Ellis, David L.

    2012-01-01

    Elevated-temperature tensile testing of commercially pure titanium (CP Ti) Grade 2 was conducted for as-received commercially produced sheet and following thermal exposure at 550 and 650 K (531 and 711 F) for times up to 5000 h. The tensile testing revealed some statistical differences between the 11 thermal treatments, but most thermal treatments were statistically equivalent. Previous data from room temperature tensile testing was combined with the new data to allow regression and development of mathematical models relating tensile properties to temperature and thermal exposure. The results indicate that thermal exposure temperature has a very small effect, whereas the thermal exposure duration has no statistically significant effects on the tensile properties. These results indicate that CP Ti Grade 2 will be thermally stable and suitable for long-duration space missions.

  8. Comparison and ranking of superelasticity of different austenite active nickel-titanium orthodontic archwires using mechanical tensile testing and correlating with its electrical resistivity

    PubMed Central

    Nagarajan, D.; Baskaranarayanan, Balashanmugam; Usha, K.; Jayanthi, M. S.; Vijjaykanth, M.

    2016-01-01

    Introduction: The application of light and continuous forces for optimum physiological response and the least damage to the tooth supporting structures should be the primary aim of an orthodontist. Nickel-titanium (NiTi) alloys with their desirable properties are one of the natural choices of the clinicians. Aim: This study was aimed to compare and rank them based on its tensile strength and electrical resistivity. Materials and Methods: The sample consisted of eight groups of 0.017 inch × 0.025 inch rectangular archwires from eight different manufacturers, and five samples from each group for tensile testing and nine samples for electrical resistivity tests were used. Data for stress at 10% strain and the initial slope were statistically analyzed with an analysis of variance and Scheffe tests with P < 0.05. The stress/strain plots of each product were ranked for superelastic behavior. The rankings of the wires tested were based primarily on the unloading curve's slope which is indicative of the magnitude of the deactivation force and secondarily on the length of the horizontal segment which is indicative of continuous forces during deactivation. For calculating the electric resistivity, the change in resistance after inducing strain in the wires was taken into account for the calculation of degree of martensite transformation and for ranking. Results: In tensile testing Ortho Organizers wires ranked first and GAC Lowland NiTi wires ranked last. For resistivity tests Ormco A wires were found superior and Morelli remained last. Conclusion: these rankings should be correlated clinically and need further studies. PMID:27829751

  9. An in situ tensile test apparatus for polymers in high pressure hydrogen

    DOE PAGES

    Alvine, Kyle J.; Kafentzis, Tyler A.; Pitman, Stan G.; ...

    2014-10-31

    Degradation of material properties by high-pressure hydrogen is an important factor in determining the safety and reliability of materials used in high-pressure hydrogen storage and delivery. Hydrogen damage mechanisms have a time dependence that is linked to hydrogen outgassing after exposure to the hydrogen atmosphere that makes ex situ measurements of mechanical properties problematic. Designing in situ measurement instruments for high-pressure hydrogen is challenging due to known hydrogen incompatibility with many metals and standard high-power motor materials like Nd. Here we detail the design and operation of a solenoid based in situ tensile tester under high-pressure hydrogen environments up tomore » 5,000 psi. Here, modulus data from high-density polyethylene (HDPE) samples tested under high-pressure hydrogen are also reported as compared to baseline measurements taken in air.« less

  10. The Effect of Gap Angle on Tensile Strength of Preceramic Base Metal Solder Joints

    PubMed Central

    Fattahi, Farnaz; Hashemi Ardakani, Zahra; Hashemi Ardakani, Maryam

    2015-01-01

    Statement of the Problem Soldering is a process commonly used in fabricating dental prosthesis. Since most soldered prosthesis fail at the solder joints; the joint strength is of utmost importance. Purpose The purpose of this study was to evaluate the effect of gap angle on the tensile strength of base metal solder joints. Materials and Method A total number of 40 Ni-Cr samples were fabricated according to ADA/ISO 9693 specifications for tensile test. Samples were cut at the midpoint of the bar, and were placed at the considered angles by employing an explicitly designed device. They were divided into 4 groups regarding the gap angle; Group C (control group) with parallel gap on steady distance of 0.2mm, Group 1: 10°, Group 2: 20°, and Group3: 30° gap angles. When soldered, the specimens were all tested for tensile strength using a universal testing machine at a cross-head speed of 0.5 mm/min with a preload of 10N. Kruskal-Wallis H test was used to compare tensile strength among the groups (p< 0.05). Results The mean tensile strength values obtained from the study groups were respectively 307.84, 391.50, 365.18, and 368.86 MPa. The tensile strength was not statistically different among the four groups in general (p≤ 0.490). Conclusion Making the gap angular at the solder joints and the subsequent unsteady increase of the gap distance would not change the tensile strength of the joint. PMID:26636118

  11. Porosity Defect Remodeling and Tensile Analysis of Cast Steel

    PubMed Central

    Sun, Linfeng; Liao, Ridong; Lu, Wei; Fu, Sibo

    2016-01-01

    Tensile properties on ASTM A216 WCB cast steel with centerline porosity defect were studied with radiographic mapping and finite element remodeling technique. Non-linear elastic and plastic behaviors dependent on porosity were mathematically described by relevant equation sets. According to the ASTM E8 tensile test standard, matrix and defect specimens were machined into two categories by two types of height. After applying radiographic inspection, defect morphologies were mapped to the mid-sections of the finite element models and the porosity fraction fields had been generated with interpolation method. ABAQUS input parameters were confirmed by trial simulations to the matrix specimen and comparison with experimental outcomes. Fine agreements of the result curves between simulations and experiments could be observed, and predicted positions of the tensile fracture were found to be in accordance with the tests. Chord modulus was used to obtain the equivalent elastic stiffness because of the non-linear features. The results showed that elongation was the most influenced term to the defect cast steel, compared with elastic stiffness and yield stress. Additional visual explanations on the tensile fracture caused by void propagation were also given by the result contours at different mechanical stages, including distributions of Mises stress and plastic strain. PMID:28787919

  12. Effect of Gap Distance on Tensile Strength of Preceramic Base Metal Solder Joints

    PubMed Central

    Fattahi, Farnaz; Motamedi, Milad

    2011-01-01

    Background and aims In order to fabricate prostheses with high accuracy and durability, soldering techniques have been introduced to clinical dentistry. However, these prostheses always fail at their solder joints. The purpose of this study was to evaluate the effect of gap distance on the tensile strength of base metal solder joints. Materials and methods Based on ADA/ISO 9693 specifications for tensile test, 40 specimens were fabricated from a Ni-Cr alloy and cut at the midpoint of 3-mm diameter bar and placed at desired positions by a specially designed device. The specimens were divided into four groups of 10 samples according to the desired solder gap distance: Group1: 0.1mm; Group2: 0.25mm; Group3: 0.5mm; and Group4: 0.75mm. After soldering, specimens were tested for tensile strength by a universal testing machine at a cross-head speed of 0.5mm/min with a preload of 10N. Results The mean tensile strength values of the groups were 162, 307.8, 206.1 and 336.7 MPa, respectively. The group with 0.75-mm gap had the highest and the group with 0.1-mm gap had the lowest tensile strength. Bonferroni test showed that Group1 and Group4 had statistically different values (P=0.023), but the differences between other groups were not sig-nificant at a significance level of 0.05. Conclusion There was no direct relationship between increasing soldering gap distance and tensile strength of the solder joints. PMID:22991610

  13. Note on performance of tapered grip tensile loading devices

    NASA Technical Reports Server (NTRS)

    Jones, M. H.; Brown, W. F., Jr.

    1975-01-01

    Alignment results are presented in terms of percent bending for a quick release, tapered grip, tensile loading device that has been proposed for testing sharply notched specimens of aluminum and magnesium alloys by a Task Group of the ASTM Committee E-24 on Fracture Testing of Metals. The results show that the bending introduced by the fixtures is strongly dependent on their relative rotational positions in respect to the loading rods which adapt them, to the tensile machine. For one set of tapered grips the highest bending was about 15%. Recommendations are made for improvement in the design of the tapered grips which should reduce the bending stresses substantially.

  14. Thermal and tensile properties of alumina filled PET nanocomposites

    NASA Astrophysics Data System (ADS)

    Nikam, Pravin N.; Deshpande, Vineeta D.

    2018-05-01

    In the present investigation, nanocomposites of poly(ethylene terephathalate)(PET) with different content (0 to 5 wt.%) of alumina nanoparticles (n-Al2O3) were prepared by melt-extrusion technique. Morphological characterization of samples was examined by transmission electron microscopy (TEM). Morphological analysis revealed that degree of dispersion of alumina nanoparticles (ANPs) was increased at lower content (i.e. upto 2 wt.%), which observed by TEM. Thermal and tensile measurements were carried out using and differential scanning calorimetry (DSC) and universal testing machine (UTM). The thermal analysis showed that the glass transition termperature (Tg), melting temperature (Tm), crystallization temperature (Tc) of PET/alumina nanocomposites (PNCs) were higher than neat PET (PET0). The heat enthalpy (ΔHm) of crystallization for PNCs was increased compared to PET0, which indicates that degree of crystallinity of PNCs also increased compared to PET0. The half-time (t0.5) of crystallization of PNCs were decreased compared to PET0 which indicates that the incorporation of ANPs nucleate the PET molecular chains and allowing the easily crystallization during nonisothermal process. The tensile analysis revealed that the tensile elastic modulus (i.e. Young's modulus) of PNCs increased almost linearly with increasing the content of ANPs while tensile elongation at break decreased nonlinearly. The tensile strength of PNCs increased with a 1 wt.% of ANPs whereas the higher content of ANPs decreased the tensile strength.

  15. Tensile properties of polyhydroxyalkanoate/polycaprolactone blends studied by rheo-optical near-infrared (NIR) spectroscopy

    NASA Astrophysics Data System (ADS)

    Nishida, Masahiro; Ogura, Takashi; Shinzawa, Hideyuki; Nishida, Masakazu; Kanematsu, Wataru

    2016-11-01

    In order to improve the mechanical properties of Polyhydroxyalkanoate (PHA), the polycaprolactone (PCL) pellet was blended with a PHA-based pellet. The effects of the mixing ratio on the tensile properties, Young's modulus, tensile strength and elongation at break, were examined using a universal testing machine. When the mixing ration of PCL increased to 50%, the elongation at break of the polymer blend increased and the gauge area of tensile test specimens whitened and became porous. In order to understand this behavior, a rheo-optical characterization technique based on near-infrared (NIR) spectroscopy was applied to the mechanical deformation of the polymer blends during static tensile tests. Two-dimensional (2D) correlation of NIR spectra was then examined. It was found from peaks of ethyl group or methyl group that PCL was preferentially deformed. The difference in the deformation behavior is thought to be the cause of the porous structure.

  16. In vitro tensile strength of luting cements on metallic substrate.

    PubMed

    Orsi, Iara A; Varoli, Fernando K; Pieroni, Carlos H P; Ferreira, Marly C C G; Borie, Eduardo

    2014-01-01

    The aim of this study was to determine the tensile strength of crowns cemented on metallic substrate with four different types of luting agents. Twenty human maxillary molars with similar diameters were selected and prepared to receive metallic core castings (Cu-Al). After cementation and preparation the cores were measured and the area of crown's portion was calculated. The teeth were divided into four groups based on the luting agent used to cement the crowns: zinc phosphate cement; glass ionomer cement; resin cement Rely X; and resin cement Panavia F. The teeth with the crowns cemented were subjected to thermocycling and later to the tensile strength test using universal testing machine with a load cell of 200 kgf and a crosshead speed of 0.5 mm/min. The load required to dislodge the crowns was recorded and converted to MPa/mm(2). Data were subjected to Kruskal-Wallis analysis with a significance level of 1%. Panavia F showed significantly higher retention in core casts (3.067 MPa/mm(2)), when compared with the other cements. Rely X showed a mean retention value of 1.877 MPa/mm(2) and the zinc phosphate cement with 1.155 MPa/mm(2). Glass ionomer cement (0.884 MPa/mm(2)) exhibited the lowest tensile strength value. Crowns cemented with Panavia F on cast metallic posts and cores presented higher tensile strength. The glass ionomer cement showed the lowest tensile strength among all the cements studied.

  17. Tensile and Torsional Structural Properties of the Native Scapholunate Ligament.

    PubMed

    Pang, Eric Quan; Douglass, Nathan; Behn, Anthony; Winterton, Matthew; Rainbow, Michael J; Kamal, Robin N

    2018-02-17

    The ideal material for reconstruction of the scapholunate interosseous ligament (SLIL) should replicate the mechanical properties of the native SLIL to recreate normal kinematics and prevent posttraumatic arthritis. The purpose of our study was to evaluate the cyclic torsional and tensile properties of the native SLIL and load to failure tensile properties of the dorsal SLIL. The SLIL bone complex was resected from 10 fresh-frozen cadavers. The scaphoid and lunate were secured in polymethylmethacrylate and mounted on a test machine that incorporated an x-y stage and universal joint, which permitted translations perpendicular to the rotation/pull axis as well as nonaxial angulations. After a 1 N preload, specimens underwent cyclic torsional testing (±0.45 N m flexion/extension at 0.5 Hz) and tensile testing (1-50 N at 1 Hz) for 500 cycles. Lastly, the dorsal 10 mm of the SLIL was isolated and displaced at 10 mm/min until failure. During intact SLIL cyclic torsional testing, the neutral zone was 29.7° ± 6.6° and the range of rotation 46.6° ± 7.1°. Stiffness in flexion and extension were 0.11 ± 0.02 and 0.12 ± 0.02 N m/deg, respectively. During cyclic tensile testing, the engagement length was 0.2 ± 0.1 mm, the mean stiffness was 276 ± 67 N/mm, and the range of displacement was 0.4 ± 0.1 mm. The dorsal SLIL displayed a 0.3 ± 0.2 mm engagement length, 240 ± 65 N/mm stiffness, peak load of 270 ± 91 N, and displacement at peak load of 1.8 ± 0.3 mm. We report the torsional properties of the SLIL. Our novel test setup allows for free rotation and translation, which reduces out-of-plane force application. This may explain our observation of greater dorsal SLIL load to failure than previous reports. By matching the natural ligament with respect to its tensile and torsional properties, we believe that reconstructions will better restore the natural kinematics of the wrist and lead to improved outcomes. Future clinical studies should aim to investigate this

  18. Analysis of Ninety Degree Flexure Tests for Characterization of Composite Transverse Tensile Strength

    NASA Technical Reports Server (NTRS)

    OBrien, T. Kevin; Krueger, Ronald

    2001-01-01

    Finite element (FE) analysis was performed on 3-point and 4-point bending test configurations of ninety degree oriented glass-epoxy and graphite-epoxy composite beams to identify deviations from beam theory predictions. Both linear and geometric non-linear analyses were performed using the ABAQUS finite element code. The 3-point and 4-point bending specimens were first modeled with two-dimensional elements. Three-dimensional finite element models were then performed for selected 4-point bending configurations to study the stress distribution across the width of the specimens and compare the results to the stresses computed from two-dimensional plane strain and plane stress analyses and the stresses from beam theory. Stresses for all configurations were analyzed at load levels corresponding to the measured transverse tensile strength of the material.

  19. Calculation for tensile strength and fracture toughness of granite with three kinds of grain sizes using three-point-bending test

    PubMed Central

    Yu, Miao; Wei, Chenhui; Niu, Leilei; Li, Shaohua; Yu, Yongjun

    2018-01-01

    Tensile strength and fracture toughness, important parameters of the rock for engineering applications are difficult to measure. Thus this paper selected three kinds of granite samples (grain sizes = 1.01mm, 2.12mm and 3mm), used the combined experiments of physical and numerical simulation (RFPA-DIP version) to conduct three-point-bending (3-p-b) tests with different notches and introduced the acoustic emission monitor system to analyze the fracture mechanism around the notch tips. To study the effects of grain size on the tensile strength and toughness of rock samples, a modified fracture model was established linking fictitious crack to the grain size so that the microstructure of the specimens and fictitious crack growth can be considered together. The fractal method was introduced to represent microstructure of three kinds of granites and used to determine the length of fictitious crack. It is a simple and novel method to calculate the tensile strength and fracture toughness directly. Finally, the theoretical model was verified by the comparison to the numerical experiments by calculating the nominal strength σn and maximum loads Pmax. PMID:29596422

  20. Self-aligning hydraulic piston assembly for tensile testing of ceramic

    DOEpatents

    Liu, Kenneth C.

    1987-01-01

    The present invention is directed to a self-aligning grip housing assembly that can transmit an uniaxial load to a tensil specimen without introducing bending stresses into the specimen. Disposed inside said grip housing assembly are a multiplicity of supporting pistons connected to a common source of pressurized oil that carry equal shares of the load applied to the specimen irregardless whether there is initial misalignment between the specimen load column assembly and housing axis.

  1. The effect of case hardening treatment on aluminum 7075 toward its hardness and tensile strength

    NASA Astrophysics Data System (ADS)

    Darsono, Febri Budi; Triyono, Teguh; Surojo, Eko

    2018-02-01

    This research was aimed at figuring out the effect of case hardening treatment on aluminum 7075 toward its hardness and tensile strength. Pack carburizing was the method used in this process. It was conducted in 2 hours of holding time in various solution heat treatment (SHT): 350°C, 400°C, 450°C, and 500° C using smoergen oven, which was then followed by quenching. Several tests to see the effect of the treatment were done before and after the treatment, namely: Vickers hardness test using HWMMT-X7, tensile test ASTM B557-84 using SANS UTM, XRD test using Rigaku Benchtop, and SEM-EDS test using JEOL JSM-6510 LA. The result showed that the hardness and tensile of aluminum 7075 before treatment were 59.1 VHN and 235.7 Mpa. After treatment, its hardness values were 94.0, 120.7, 141.3, and 145.9 VHN and the tensile strengths were 321.7, 410.0, 480.0, and 538.3 Mpa. The result showed that SHT temperature rise in pack carburizing process increased the tensile strength, while the increase of the hardness value is due to the formation of Al4C3 phase on the aluminum surface.

  2. Residual Tensile Property of Plain Woven Jute Fiber/Poly(Lactic Acid) Green Composites during Thermal Cycling

    PubMed Central

    Katogi, Hideaki; Takemura, Kenichi; Akiyama, Motoki

    2016-01-01

    This study investigated the residual tensile properties of plain woven jute fiber reinforced poly(lactic acid) (PLA) during thermal cycling. Temperature ranges of thermal cycling tests were 35–45 °C and 35–55 °C. The maximum number of cycles was 103 cycles. The quasi-static tensile tests of jute fiber, PLA, and composite were conducted after thermal cycling tests. Thermal mechanical analyses of jute fiber and PLA were conducted after thermal cycling tests. Results led to the following conclusions. For temperatures of 35–45 °C, tensile strength of composite at 103 cycles decreased 10% compared to that of composite at 0 cycles. For temperatures of 35–55 °C, tensile strength and Young’s modulus of composite at 103 cycles decreased 15% and 10%, respectively, compared to that of composite at 0 cycles. Tensile properties and the coefficient of linear expansion of PLA and jute fiber remained almost unchanged after thermal cycling tests. From observation of a fracture surface, the length of fiber pull out in the fracture surface of composite at 103 cycles was longer than that of composite at 0 cycles. Therefore, tensile properties of the composite during thermal cycling were decreased, probably because of the decrease of interfacial adhesion between the fiber and resin. PMID:28773694

  3. Tensile and flexural strength of commercially pure titanium submitted to laser and tungsten inert gas welds.

    PubMed

    Atoui, Juliana Abdallah; Felipucci, Daniela Nair Borges; Pagnano, Valéria Oliveira; Orsi, Iara Augusta; Nóbilo, Mauro Antônio de Arruda; Bezzon, Osvaldo Luiz

    2013-01-01

    This study evaluated the tensile and flexural strength of tungsten inert gas (TIG) welds in specimens made of commercially pure titanium (CP Ti) compared with laser welds. Sixty cylindrical specimens (2 mm diameter x 55 mm thick) were randomly assigned to 3 groups for each test (n=10): no welding (control), TIG welding (10 V, 36 A, 8 s) and Nd:YAG laser welding (380 V, 8 ms). The specimens were radiographed and subjected to tensile and flexural strength tests at a crosshead speed of 1.0 mm/min using a load cell of 500 kgf applied on the welded interface or at the middle point of the non-welded specimens. Tensile strength data were analyzed by ANOVA and Tukey's test, and flexural strength data by the Kruskal-Wallis test (α=0.05). Non-welded specimens presented significantly higher tensile strength (control=605.84 ± 19.83) (p=0.015) and flexural strength (control=1908.75) (p=0.000) than TIG- and laser-welded ones. There were no significant differences (p>0.05) between the welding types for neither the tensile strength test (TIG=514.90 ± 37.76; laser=515.85 ± 62.07) nor the flexural strength test (TIG=1559.66; laser=1621.64). As far as tensile and flexural strengths are concerned, TIG was similar to laser and could be suitable to replace laser welding in implant-supported rehabilitations.

  4. Comparison of Superelasticity of Nickel Titanium Orthodontic Arch wires using Mechanical Tensile Testing and Correlating with Electrical Resistivity

    PubMed Central

    Sivaraj, Aravind

    2013-01-01

    Background: Application of light and continuous forces for optimum physiological response and least damage to the tooth supporting structures should be the primary aim of the orthodontist. Nickel titanium alloys with the properties of excellent spring back, super elasticity and wide range of action is one of the natural choices for the clinicians to achieve this goal. In recent periods, various wire manufacturers have come with a variety of wires exhibiting different properties. It is the duty of the clinician to select appropriate wires during various stages of treatment for excellent results. For achieving this evaluation of the properties of these wires is essential. Materials & Methods: This study is focussed on evaluating the super elastic property of eight groups of austenite active nickel titanium wires. Eight groups of archwires bought from eight different manufacturers were studied. These wires were tested through mechanical tensile testing and electrical resistivity methods. Results: Unloading curves were carefully assessed for superelastic behaviour on deactivation. Rankings of the wires tested were based primarily upon the unloading curve’s slope Conclusion: Ortho organisers wires ranked first and superior, followed by American Orthodontics and Ormco A wires. Morelli and GAClowland NiTi wires were ranked last. It can be concluded that the performance of these wires based on rankings should be further evaluated by clinical studies. How to cite this article: Sivaraj A. Comparison of Superelasticity of Nickel Titanium Orthodontic Arch wires using Mechanical Tensile Testing and Correlating with Electrical Resistivity. J Int Oral Health 2013; 5(3):1-12. PMID:24155596

  5. Tensile and shear strength of adhesives

    NASA Technical Reports Server (NTRS)

    Stibolt, Kenneth A.

    1990-01-01

    This experiment is conducted in a freshman-level course: Introduction to Engineering Materials. There are no prerequisites for the course although students should have some knowledge of basic algebra. The objectives are to tension and shear test adhesives and to determine the tensile and shear properties of adhesives. Details of equipment of procedure are given.

  6. Simulated Space Environmental Testing on Thin Films

    NASA Technical Reports Server (NTRS)

    Russell, Dennis A.; Fogdall, Larry B.; Bohnhoff-Hlavacek, Gail; Connell, John W. (Technical Monitor)

    2000-01-01

    An exploratory program has been conducted, to irradiate some mature commercial and some experimental polymer films with radiation simulating certain Earth orbits, and to obtain data about the response of each test film's reflective and tensile properties. Protocols to conduct optimized tests were considered and developed to a "prototype" level during this program. Fifteen polymer film specimens were arranged on a specially designed test fixture. The fixture featured controlled exposure areas, and protected the ends of the samples for later gripping in tensile tests. The fixture featured controlled exposure areas, and protected the ends of the samples for later gripping in tensile tests. The fixture containing the films was installed in a clean vacuum chamber where protons, electrons and solar ultraviolet (UV) radiation could simultaneously irradiate the specimens. Near realtime UV rates were used, whereas proton and electron rates were accelerated appreciably to simulate 5 years in orbit during a two month test. Periodically, the spectral reflectance of each film was measured in situ. After the end of the irradiation, final reflectance measurements were made in situ, and solar absorptance values were derived for each specimen. These samples were then measured in air for thermal emittance and for tensile strength. Most specimens withstood the irradiation intact, but with reduced reflectance (increased solar absorptance). Thermal emittance changed slightly in several materials, as did their tensile strength and elongation at break. Conclusions are drawn about the performance of the films. Simulated testing to an expected 5 year dose of electrons and protons consistent with those expected at L2 and 0.98 AU orbits and 100 equivalent solar hours exposure.

  7. Self-aligning hydraulic piston assembly for tensile testing of ceramic

    DOEpatents

    Liu, K.C.

    1987-08-18

    The present invention is directed to a self-aligning grip housing assembly that can transmit an uniaxial load to a tensile specimen without introducing bending stresses into the specimen. Disposed inside said grip housing assembly are a multiplicity of supporting pistons connected to a common source of pressurized oil that carry equal shares of the load applied to the specimen regardless whether there is initial misalignment between the specimen load column assembly and housing axis. 4 figs.

  8. Tensile properties of the human glenoid labrum

    PubMed Central

    Smith, C D; Masouros, S D; Hill, A M; Wallace, A L; Amis, A A; Bull, A M J

    2008-01-01

    Human fresh-frozen cadaveric glenoid labrae from 16 donors were harvested and ten of these had no gross degeneration. These ten were divided into eight equal circumferential sections. Each section was cut to produce test-samples from the core layer with a cross-section of 1 × 1 mm. Tensile testing was performed within a controlled environment unit at 37 ± 1 °C and 100% relative humidity. Each test-sample was precycled to a quasi-static state to alleviate the effects of deep-freezing, prior to final testing. The tangent modulus was calculated for each test-sample before and after a 5-min period of stress relaxation and at yield. The mean elastic modulus and yield stress of the glenoid labrum were 22.8 ± 11.4 and 2.5 ± 2.1 MPa, respectively. The anterosuperior portion had a lower elastic modulus and lower yield stress than the inferior portion (both P < 0.02). The pre-stress relaxation tangent modulus was significantly lower than the post-stress relaxation tangent modulus for all portions of the labrum. The glenoid labrum has similar tensile material properties to articular cartilage. Its elastic modulus varies around its circumference. This suggests that the labrum may encounter different forces at different positions. PMID:18031481

  9. Relationship of fatigue to the tensile stiffness of asphaltic concrete : final report on phase 1, laboratory investigation.

    DOT National Transportation Integrated Search

    1972-01-01

    The correlation between asphaltic concrete tensile stiffness and fatigue life was determined in the laboratory. Constant strain fatigue tests were utilized and indirect tensile tests were selected because of their simplicity and applicability. Four a...

  10. Experimental Study On The Effect Of Micro-Cracks On Brazilian Tensile Strength

    NASA Astrophysics Data System (ADS)

    Wang, Xiangyu

    2015-12-01

    For coal mine ground control issues, it is necessary to propose a failure criteria accounting for the transversely isotropic behaviors of rocks. Hence, it is very helpful to provide experimental data for the validation of the failure criteria. In this paper, the method for preparing transversely isotropic specimens and the scheme of the Brazilian tensile strength test are presented. Results obtained from Brazilian split tests under dry and water-saturated conditions reflect the effect of the development direction β of the structural plane, such as the bedding fissure, on the tensile strength, ultimate displacement, failure mode, and the whole splitting process. The results show that the tensile strength decreases linearly with increasing β. The softening coefficient of the tensile strength shows a sinusoidal function. The values of the slope and inflection point for the curve vary at the different stages of the Brazilian test. The failure mode of the rock specimen presented in this paper generally coincides with the standard Brazilian splitting failure mode. Based on the test results, the major influencing factors for the Brazilian splitting strength are analyzed and a mathematical model for solving the Brazilian splitting strength is proposed. The findings in this paper would greatly benefit the coal mine ground control studies when the surrounding rocks of interest show severe transversely isotropic behaviors.

  11. Tensile and shear methods for measuring strength of bilayer tablets.

    PubMed

    Chang, Shao-Yu; Li, Jian-Xin; Sun, Changquan Calvin

    2017-05-15

    Both shear and tensile measurement methods have been used to quantify interfacial bonding strength of bilayer tablets. The shear method is more convenient to perform, but reproducible strength data requires careful control of the placement of tablet and contact point for shear force application. Moreover, data obtained from the shear method depend on the orientation of the bilayer tablet. Although more time-consuming to perform, the tensile method yields data that are straightforward to interpret. Thus, the tensile method is preferred in fundamental bilayer tableting research to minimize ambiguity in data interpretation. Using both shear and tensile methods, we measured the mechanical strength of bilayer tablets made of several different layer combinations of lactose and microcrystalline cellulose. We observed a good correlation between strength obtained by the tensile method and carefully conducted shear method. This suggests that the shear method may be used for routine quality test of bilayer tablets during manufacturing because of its speed and convenience, provided a protocol for careful control of the placement of the tablet interface, tablet orientation, and blade is implemented. Copyright © 2017 Elsevier B.V. All rights reserved.

  12. Tensile and creep properties of titanium-vanadium, titanium-molybdenum, and titanium-niobium alloys

    NASA Technical Reports Server (NTRS)

    Gray, H. R.

    1975-01-01

    Tensile and creep properties of experimental beta-titanium alloys were determined. Titanium-vanadium alloys had substantially greater tensile and creep strength than the titanium-niobium and titanium-molybdenum alloys tested. Specific tensile strengths of several titanium-vanadium-aluminum-silicon alloys were equivalent or superior to those of commercial titanium alloys to temperatures of 650 C. The Ti-50V-3Al-1Si alloy had the best balance of tensile strength, creep strength, and metallurgical stability. Its 500 C creep strength was far superior to that of a widely used commercial titanium alloy, Ti-6Al-4V, and almost equivalent to that of newly developed commercial titanium alloys.

  13. Scale effects on the transverse tensile strength of graphite epoxy composites

    NASA Technical Reports Server (NTRS)

    Obrien, T. Kevin; Salpekar, Satish A.

    1992-01-01

    The influence of material volume on the transverse tensile strength of AS4/3501-6 graphite epoxy composites was investigated. Tensile tests of 90 degree laminates with 3 different widths and 5 different thicknesses were conducted. A finite element analysis was performed to determine the influence of the grip on the stress distribution in the coupons and explain the tendency for the distribution of failure locations to be skewed toward the grip. Specimens were instrumented with strain gages and extensometers to insure good alignment and to measure failure strains. Data indicated that matrix dominated strength properties varied with the volume of material that was stressed, with the strength decreasing as volume increased. Transverse strength data were used in a volumetric scaling law based on Weibull statistics to predict the strength of 90 degree laminates loaded in three point bending. Comparisons were also made between transverse strength measurements and out-of-plane interlaminar tensile strength measurements from curved beam bending tests. The significance of observed scale effects on the use of tests for material screening, quality assurance, and design allowables is discussed.

  14. Constitutive Behavior Modelling of AA1100-O AT Large Strain and High Strain Rates

    NASA Astrophysics Data System (ADS)

    Testa, Gabriel; Iannitti, Gianluca; Ruggiero, Andrew; Gentile, Domenico; Bonora, Nicola

    2017-06-01

    Constitutive behavior of AA1100-O, provided as extruded bar, was investigated. Microscopic observation showed that the cross-section has a peculiar microstructure consisting in the inner core with a large grain size surrounded by an external annulus with finer grains. Low and high strain rates tensile tests were carried out at different temperature ranging from -190 ° C to 100 ° C. Constitutive behavior was modelled using a modified version of Rusinek & Klepaczko model. Parameters were calibrated on tensile test results. Tests and numerical simulations of symmetric Taylor (RoR) and dynamic tensile extrusion (DTE) tests at different impact velocities were carried out in order to validate the model under complex deformation paths.

  15. Tensile buckling of advanced turboprops

    NASA Technical Reports Server (NTRS)

    Chamis, C. C.; Aiello, R. A.

    1982-01-01

    Theoretical studies were conducted to determine analytically the tensile buckling of advanced propeller blades (turboprops) in centrifugal fields, as well as the effects of tensile buckling on other types of structural behavior, such as resonant frequencies and flutter. Theoretical studies were also conducted to establish the advantages of using high performance composite turboprops as compared to titanium. Results show that the vibration frequencies are not affected appreciably prior to 80 percent of the tensile speed. Some frequencies approach zero as the tensile buckling speed is approached. Composites provide a substantial advantage over titanium on a buckling speed to weight basis. Vibration modes change as the rotor speed is increased and substantial geometric coupling is present.

  16. Dynamic High-Temperature Tensile Characterization of an Iridium Alloy with Kolsky Tension Bar Techniques

    DOE PAGES

    Song, Bo; Nelson, Kevin; Lipinski, Ronald; ...

    2015-05-29

    In this study, conventional Kolsky tension bar techniques were modified to characterize an iridium alloy in tension at elevated strain rates and temperatures. The specimen was heated to elevated temperatures with an induction coil heater before dynamic loading; whereas, a cooling system was applied to keep the bars at room temperature during heating. A preload system was developed to generate a small pretension load in the bar system during heating in order to compensate for the effect of thermal expansion generated in the high-temperature tensile specimen. A laser system was applied to directly measure the displacements at both ends ofmore » the tensile specimen in order to calculate the strain in the specimen. A pair of high-sensitivity semiconductor strain gages was used to measure the weak transmitted force due to the low flow stress in the thin specimen at elevated temperatures. The dynamic high-temperature tensile stress–strain curves of a DOP-26 iridium alloy were experimentally obtained at two different strain rates (~1000 and 3000 s -1) and temperatures (~750 and 1030°C). The effects of strain rate and temperature on the tensile stress–strain response of the iridium alloy were determined. Finally, the iridium alloy exhibited high ductility in stress–strain response that strongly depended on strain-rate and temperature.« less

  17. Effect of Manufacturing Method to Tensile Properties of Hybrid Composite Reinforced by Natural (Agel Leaf Fiber) and Glass Fibers

    NASA Astrophysics Data System (ADS)

    Nugroho, A.; Abdurohman, K.; Kusmono; Hestiawan, H.; Jamasri

    2018-04-01

    This paper described the effect of different type of manufacturing method to tensile properties of hybrid composite woven agel leaf fiber and glass fiber as an alternative of LSU structure material. The research was done by using 3 ply of woven agel leaf fiber (ALF) and 3 ply of glass fiber (wr200) while the matrix was using unsaturated polyester. Composite manufacturing method used hand lay-up and vacuum bagging. Tensile test conducted with Tensilon universal testing machine, specimen shape and size according to standard size ASTM D 638. Based on tensile test result showed that the tensile strength of agel leaf fiber composite with unsaturated polyester matrix is 54.5 MPa by hand lay-up and 84.6 MPa with vacuum bagging method. From result of tensile test, hybrid fiber agel composite and glass fiber with unsaturated polyester matrix have potential as LSU structure.

  18. Some Effects of Nitrates on the Tensile Properties of Al 7075-T7351.

    DTIC Science & Technology

    1988-03-01

    SORNSOIG IO 8b OFFICE SYMBOL 7aRO NA10 MDFN %1% ST% RuMEN IENT, ON NME ORGAiZtION Reerh ru (if applicable) Sc. ADDRESS (City, State and ZIP Code) 7t0 ADRES...grains in products with significant grain directionality TUS Tensile Ultimate Strength TYS Tensile Yield Strength wt Weight TABLE OF CONTENTS Page...CONFIGURATION NI A- NI 6. 44. 6.0 .1 rl il i I I APPENDIX B CONTROL SETS - TENSILE TEST DATA Contents L -T C ontro ls

  19. Effect of human urine on the tensile strength of sutures used for hypospadias surgery.

    PubMed

    Kerstein, Ryan L; Sedaghati, Tina; Seifalian, Alexander M; Kang, Norbert

    2013-06-01

    Hypospadias is the most common congenital condition affecting between 1 in 250 and 300 live births. Even in experienced hands, surgery to repair this congenital defect can have a high complication rate. Wound dehiscence is reported to occur in 5% and fistula formation in 6%-40% depending on technique. The choice of suture material has been shown to affect the complication rate although there is (currently) no consensus about the best suture material to use. Ideally, the sutures used for urethroplasty should be absorbable while maintaining sufficient mechanical strength to support the wounds until they are self-supporting and able to resist urinary flow. Previous studies have compared the effects of human urine on different suture materials especially catgut. However, catgut is now banned in Europe. Our study examined the tensile and breaking strength as well as rate of degradation for four types of absorbable suture now commonly used for hypospadias repairs in the UK. We examined the effect of prolonged storage (up to 27 days) in human urine on 6/0 gauge Vicryl, Vicryl Rapide, Monocryl and polydioxanone (PDS) sutures. These four suture materials are commonly used by the senior plastic consultant surgeon (NK) for hypospadias repairs. 50 mm sections of these suture materials were stored in either urine or saline as control. At specified time points, each suture was placed in a uniaxial load testing machine to assess the stress-strain profile and the mechanical load required to break the suture was measured. Exposure to urine reduced the tensile and breaking strength of all the suture materials tested. PDS demonstrated the greatest resilience. Vicryl Rapide was the weakest suture and degraded completely by day 6. Vicryl and Monocryl had similar degradation profiles, but Vicryl retained more of its tensile strength for longer. There is a balance to be struck between the duration that a suture material must remain in any surgical wound and the risk that it causes

  20. Tensile and creep properties of the experimental oxide dispersion strengthened iron-base sheet alloy MA-956E at 1365 K

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D.

    1978-01-01

    A study of the 1365 K tensile properties, creep characteristics and residual room temperature properties after creep testing of the experimental oxide dispersion strengthened iron-base alloy MA-956E (Fe-20Cr-4.5Al-0.5Ti-0.5Y2O3) was conducted. The 1365 K tensile properties, particularly ductility, are strongly dependent on strain rate. It appears that MA-956E does not easily undergo slow plastic deformation. Rather than deform under creep loading conditions, the alloy apparently fails by a crack nucleation and growth mechanism. Fortunately, there appears to be a threshold stress below which crack nucleation and/or growth does not occur.

  1. Direct observation of the residual plastic deformation caused by a single tensile overload

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Bichler, C.; Pippan, R.

    1999-07-01

    The fatigue crack growth behavior following single tensile overloads at high stress intensity ranges in a cold-rolled austenitic steel has been studied experimentally. After tensile overloads, fatigue cracks initially accelerate, followed by significant retardation, before the growth rates return to their baseline level. The initial acceleration was attributed to an immediate reduction in near-tip closure. Scanning electron micrography and stereophotogrammetric reconstruction of the fracture surface were applied to study the residual plastic deformation caused by a single tensile overload in the mid-thickness of the specimen. The measured residual opening displacement of the crack as a function of the overload ismore » presented and compared with simple estimations. Also, free specimen surface observations of the residual plastic deformation and crack growth rate were performed. In the midsection of the specimens the striation spacing-length, i.e., the microscopic growth rates, were measured before and after the applied overload. It will be shown that the measured plasticity-induced wedges from the single overload and the observed propagation behavior support the significance of the concept of crack closure.« less

  2. 7 CFR 29.3061 - Strength (tensile).

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 2 2010-01-01 2010-01-01 false Strength (tensile). 29.3061 Section 29.3061... Type 93) § 29.3061 Strength (tensile). The stress a tobacco leaf can bear without tearing. Tensile strength is not an important element of quality in Burley tobacco. [24 FR 8771, Oct. 29, 1959. Redesignated...

  3. 7 CFR 29.3061 - Strength (tensile).

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 2 2011-01-01 2011-01-01 false Strength (tensile). 29.3061 Section 29.3061... Type 93) § 29.3061 Strength (tensile). The stress a tobacco leaf can bear without tearing. Tensile strength is not an important element of quality in Burley tobacco. [24 FR 8771, Oct. 29, 1959. Redesignated...

  4. Tensile creep behavior of polycrystalline alumina fibers

    NASA Technical Reports Server (NTRS)

    Yun, H. M.; Goldsby, J. C.

    1993-01-01

    Tensile creep studies were conducted on polycrystalline Nextel 610 and Fiber FP alumina fibers with grain sizes of 100 and 300 nm, respectively. Test conditions were temperatures from 800 to 1050 C and stresses from 60 to 1000 MPa. For both fibers, only a small primary creep portion occurred followed by steady-state creep. The stress exponents for steady-state creep of Nextel 610 and Fiber FP were found to be about 3 and 1, respectively. At lower temperatures, below 1000 C, the finer grained Nextel 610 had a much higher 0.2 percent creep strength for 100 hr than the Fiber FP; while at higher temperatures, Nextel 610 had a comparable creep strength to the Fiber FP. The stress and grain size dependencies suggest Nextel 610 and Fiber FP creep rates are due to grain boundary sliding controlled by interface reaction and Nabarro-Herring mechanisms, respectively.

  5. Tensile and bending fatigue of the adhesive interface to dentin.

    PubMed

    Belli, Renan; Baratieri, Luiz Narciso; Braem, Marc; Petschelt, Anselm; Lohbauer, Ulrich

    2010-12-01

    The aim of this study was to evaluate the fatigue limits of the dentin-composite interfaces established either with an etch-and-rinse or an one-step self-etch adhesive systems under tensile and bending configurations. Flat specimens (1.2 mm×5 mm×35 mm) were prepared using a plexiglass mold where dentin sections from human third molars were bonded to a resin composite, exhibiting the interface centrally located. Syntac Classic and G-Bond were used as adhesives and applied according to the manufacturer's instructions. The fluorochrome Rhodamine B was added to the adhesives to allow for fractographic evaluation. Tensile strength was measured in an universal testing machine and the bending strength (n=15) in a Flex machine (Flex, University of Antwerp, Belgium), respectively. Tensile (TFL) and bending fatigue limits (BFL) (n=25) were determined under wet conditions for 10(4) cycles following a staircase approach. Interface morphology and fracture mechanisms were observed using light, confocal laser scanning and scanning electron microscopy. Statistical analysis was performed using three-way ANOVA (mod LSD test, p<0.05). Tensile and bending characteristic strengths at 63.2% failure probability for Syntac were 23.8 MPa and 71.5 MPa, and 24.7 MPa and 72.3 MPa for G-Bond, respectively. Regarding the applied methods, no significant differences were detected between adhesives. However, fatigue limits for G-Bond (TFL=5.9 MPa; BFL=36.2 MPa) were significantly reduced when compared to Syntac (TFL=12.6 MPa; BFL=49.7 MPa). Fracture modes of Syntac were generally of adhesive nature, between the adhesive resin and dentin, while G-Bond showed fracture planes involving the adhesive-dentin interface and the adhesive resin. Cyclic loading under tensile and bending configurations led to a significant strength degradation, with a more pronounced fatigue limit decrease for G-Bond. The greater decrease in fracture strength was observed in the tensile configuration. Copyright © 2010

  6. EFFECT OF CONVENTIONAL AND EXPERIMENTAL GINGIVAL RETRACTION SOLUTIONS ON THE TENSILE STRENGTH AND INHIBITION OF POLYMERIZATION OF FOUR TYPES OF IMPRESSION MATERIALS

    PubMed Central

    Sábio, Sérgio; Franciscone, Paulo Afonso; Mondelli, José

    2008-01-01

    In the present study, two types of tests (tensile strength test and polymerization inhibition test) were performed to evaluate the physical and chemical properties of four impression materials [a polysulfide (Permlastic), a polyether (Impregum), a condensation silicone (Xantopren) and a polyvinylsiloxane (Aquasil)] when polymerized in contact with of one conventional (Hemostop) and two experimental (Vislin and Afrin) gingival retraction solutions. For the tensile strength test, the impression materials were mixed and packed into a steel plate with perforations that had residues of the gingival retraction solutions. After polymerization, the specimens were tested in tensile strength in a universal testing machine. For the polymerization inhibition test, specimens were obtained after taking impressions from a matrix with perforations that contained 1 drop of the gingival retraction solutions. Two independent examiners decided on whether or not impression material remnants remained unpolymerized, indicating interference of the chemical solutions. Based on the analysis of the results of both tests, the following conclusions were reached: 1. The tensile strength of the polysulfide decreased after contact with Hemostop and Afrin. 2. None of the chemical solutions inhibited the polymerization of the polysulfide; 3. The polyether presented lower tensile strength after polymerization in contact with the three gingival retraction agents; 4. The polyether had its polymerization inhibited only by Hemostop; 5. None of the chemical solutions affected the tensile strength of the condensation silicone; 6. Only Hemostop inhibited the polymerization of the condensation silicone; 7. The polyvinylsiloxane specimens polymerized in contact with Hemostop had significantly lower tensile strength; 8. Neither of the chemical solutions (Afrin and Vislin) affected the tensile strength of the polyvinylsiloxane and the condensation silicone; 9. Results of the tensile strength and polymerization

  7. Effect of conventional and experimental gingival retraction solutions on the tensile strength and inhibition of polymerization of four types of impression materials.

    PubMed

    Sábio, Sérgio; Franciscone, Paulo Afonso; Mondelli, José

    2008-01-01

    In the present study, two types of tests (tensile strength test and polymerization inhibition test) were performed to evaluate the physical and chemical properties of four impression materials [a polysulfide (Permlastic), a polyether (Impregum), a condensation silicone (Xantopren) and a polyvinylsiloxane (Aquasil)] when polymerized in contact with of one conventional (Hemostop) and two experimental (Vislin and Afrin) gingival retraction solutions. For the tensile strength test, the impression materials were mixed and packed into a steel plate with perforations that had residues of the gingival retraction solutions. After polymerization, the specimens were tested in tensile strength in a universal testing machine. For the polymerization inhibition test, specimens were obtained after taking impressions from a matrix with perforations that contained 1 drop of the gingival retraction solutions. Two independent examiners decided on whether or not impression material remnants remained unpolymerized, indicating interference of the chemical solutions. Based on the analysis of the results of both tests, the following conclusions were reached: 1. The tensile strength of the polysulfide decreased after contact with Hemostop and Afrin. 2. None of the chemical solutions inhibited the polymerization of the polysulfide; 3. The polyether presented lower tensile strength after polymerization in contact with the three gingival retraction agents; 4. The polyether had its polymerization inhibited only by Hemostop; 5. None of the chemical solutions affected the tensile strength of the condensation silicone; 6. Only Hemostop inhibited the polymerization of the condensation silicone; 7. The polyvinylsiloxane specimens polymerized in contact with Hemostop had significantly lower tensile strength; 8. Neither of the chemical solutions (Afrin and Vislin) affected the tensile strength of the polyvinylsiloxane and the condensation silicone; 9. Results of the tensile strength and polymerization

  8. Tensile and fatigue behavior of polymer composites reinforced with superelastic SMA strands

    NASA Astrophysics Data System (ADS)

    Daghash, Sherif M.; Ozbulut, Osman E.

    2018-06-01

    This study explores the use of superelastic shape memory alloy (SMA) strands, which consist of seven individual small-diameter wires, in an epoxy matrix and characterizes the tensile and fatigue responses of the developed SMA/epoxy composites. Using a vacuum assisted hand lay-up technique, twelve SMA fiber reinforced polymer (FRP) specimens were fabricated. The developed SMA-FRP composites had a fiber volume ratio of 50%. Tensile response of SMA-FRP specimens were characterized under both monotonic loading and increasing amplitude loading and unloading cycles. The degradation in superelastic properties of the developed SMA-FRP composites during fatigue loading at different strain amplitudes was investigated. The effect of loading rate on the fatigue response of SMA-FRP composites was also explored. In addition, fractured specimens were examined using the scanning electron microscopy (SEM) technique to study the failure mechanisms of the tested specimens. A good interfacial bonding between the SMA strands and epoxy matrix was observed. The developed SMA-FRP composites exhibited good superelastic behavior at different strain amplitudes up to at least 800 cycle after which significant degradation occurred.

  9. Surface orientation effects on bending properties of surgical mesh are independent of tensile properties.

    PubMed

    Simon, David D; Andrews, Sharon M; Robinson-Zeigler, Rebecca; Valdes, Thelma; Woods, Terry O

    2018-02-01

    Current mechanical testing of surgical mesh focuses primarily on tensile properties even though implanted devices are not subjected to pure tensile loads. Our objective was to determine the flexural (bending) properties of surgical mesh and determine if they correlate with mesh tensile properties. The flexural rigidity values of 11 different surgical mesh designs were determined along three textile directions (machine, cross-machine, and 45° to machine; n = 5 for each) using ASTM D1388-14 while tracking surface orientation. Tensile testing was also performed on the same specimens using ASTM D882-12. Linear regressions were performed to compare mesh flexural rigidity to mesh thickness, areal mass density, filament diameter, ultimate tensile strength, and maximum extension. Of 33 mesh specimen groups, 30 had significant differences in flexural rigidity values when comparing surface orientations (top and bottom). Flexural rigidity and mesh tensile properties also varied with textile direction (machine and cross-machine). There was no strong correlation between the flexural and tensile properties, with mesh thickness having the best overall correlation with flexural rigidity. Currently, surface orientation is not indicated on marketed surgical mesh, and a single mesh may behave differently depending on the direction of loading. The lack of correlation between flexural stiffness and tensile properties indicates the need to examine mesh bending stiffness to provide a more comprehensive understanding of surgical mesh mechanical behaviors. Further investigation is needed to determine if these flexural properties result in the surgical mesh behaving mechanically different depending on implantation direction. © 2017 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 106B: 854-862, 2018. © 2017 Wiley Periodicals, Inc.

  10. Assessment of the Tensile Properties for Single Fibers

    DTIC Science & Technology

    2018-02-01

    Approved for public release; distribution is unlimited. 14. ABSTRACT A novel experimental test method is presented to assess the tensile properties...distribution is unlimited. iii Contents List of Figures iv List of Tables v Acknowledgments vi 1. Introduction 1 2. Experimental Procedure 2 2.1 Test...fiber diameter measurements .............................. 7 Fig. 5 The coordinate system defining the experimental setup with the x- direction along

  11. Mass variation effect of teki grass (cyperus rotundus) composite against tensile strength and density

    NASA Astrophysics Data System (ADS)

    Rafiq Yanhar, Muhammad; Haris Nasution, A.

    2018-05-01

    The primary purpose of this study is to determine the tensile strength using ASTM D638 - 02a type IVB and density of teki grass (Cyperus rotundus) composite. The production process is carried out by mass variation of 2 gr, 3 gr, and 4 gr. Hand lay-up method with three repetitions is applied. Teki grass is chosen because it is easy to find and has some advantages biodegradable, harmless to health, available in large quantities, and cost-efficient. The test result showed the largest tensile strength is 21,61 MPa at 2-gram mass fiber. Fiber addition to 3 gram and 4-gram cause tensile strength decreases to 18,51 MPa and 11,65 MPa. It happens because the fibers are random and spread in all directions, so many fibers are undirectional with the tensile force. Beside that fibers addition made matrix volume reduced and a bond between fiber and matrix decreases, finally make fiber unable to hold the tensile force properly. It is recommended to use another type of ASTM D638 - 02a which has a larger narrow section like type I (13 mm) and type III (19mm) so specimens are not broken when removed from the mold, and there isn’t any decrease in tensile strength.Density test showed that fiber mass does not significantly affect the density.

  12. Comparison of Elevated Temperature Tensile Properties and Fatigue Behavior of Two Variants of a Woven SiC/SiC Composite

    NASA Technical Reports Server (NTRS)

    Kalluri, Sreeramesh; Brewer, David N.; Sreeramesh, Kalluri

    2005-01-01

    Tensile properties (elastic modulus, proportional limit strength, in-plane tensile strength, and strain at failure) of two variants of a woven SiC/SiC composite, manufactured during two separate time periods (9/99 and 1/01), were determined at 1038 and 1204 C by conducting tensile tests on specimens machined from plates. Continuous cycling fatigue tests (R = 0.05) and 20 cpm) were also conducted at the same two temperatures on specimens from both composites. In this study, average tensile properties, 95% confidence intervals associated with the tensile properties, and geometric mean fatigue lives of both composite materials are compared. The observed similarities and differences in the tensile properties are highlighted and an attempt is made to understand the relationship, if any, between the tensile properties and the fatigue behaviors of the two woven composites.

  13. Tensile Yielding of Multi-Wall Carbon Nanotube

    NASA Technical Reports Server (NTRS)

    Wei, Chenyu; Cho, Kyeongjae; Srivastava, Deepak; Parks, John W. (Technical Monitor)

    2002-01-01

    The tensile yielding of multiwall carbon nanotubes (MWCNTs) has been studied using Molecular Dynamics simulations and a Transition State Theory based model. We find a strong dependence of the yielding on the strain rate. A critical strain rate has been predicted above/below which yielding strain of a MWCNT is larger/smaller than that of the corresponding single-wall carbon nanotubes. At experimentally feasible strain rate of 1% /hour and T = 300K, the yield strain of a MWCNT is estimated to be about 3-4 % higher than that of an equivalent SWCNT (Single Wall Carbon Nanotube), in good agreement with recent experimental observations.

  14. Effect of Temperature and Deformation Rate on the Tensile Mechanical Properties of Polyimide Films

    NASA Technical Reports Server (NTRS)

    Moghazy, Samir F.; McNair, Kevin C.

    1996-01-01

    In order to study the structure-property relationships of different processed oriented polyimide films, the mechanical properties will be identified by using tensile tester Instron 4505 and structural information such as the 3-dimensional birefringence molecular symmetry axis and 3-dimensional refractive indices will be determined by using wave guide coupling techniques. The monoaxial drawing techniques utilized in this research are very useful for improving the tensile mechanical properties of aromatic polyimide films. In order to obtain high modulus/high strength polyimide films the following two techniques have been employed, cold drawing in which polyimide films are drawn at room temperature at different cross head speeds and hot drawing in which polyimide films are drawn at different temperatures and cross head speeds. In the hot drawing process the polyimide films are drawn at different temperatures until the glass transition temperature (Tg) is reached by using the environmental chamber. All of the mechanical and optical property parameters will be identified for each sample processed by both cold and hot drawing techniques.

  15. Tensile test and interface retention forces between wires and composites in lingual fixed retainers.

    PubMed

    Paolone, Maria Giacinta; Kaitsas, Roberto; Obach, Patricia; Kaitsas, Vasilios; Benedicenti, Stefano; Sorrenti, Eugenio; Barberi, Fabrizio

    2015-06-01

    In daily orthodontic clinical practice retention is very important, and lingual retainers are part of this challenge. The failure of lingual retainers may be due to many factors. The aim of this study was to assess the retention forces and mechanical behavior of different types of wires matched with different kinds of composites in lingual retainers. A tensile test was performed on cylindrical composite test specimens bonded to orthodontic wires. The specimens were constructed using four different wires: a straight wire (Remanium .016×.022″ Dentaurum), two round twisted wires (Penta One .0215″ Masel, Gold Penta Twisted .0215″ Gold N'braces) and a rectangular braided wire (D-Rect .016×.022″ Ormco); and three composites: two micro-hybrids (Micro-Hybrid Enamel Plus HFO Micerium, and Micro-Hybrid SDR U Dentsply) and a micro-nano-filled composite (Micro-Nano-Filled Transbond LR 3M). The test was performed at a speed of 10mm/min on an Inström device. The wire was fixed with a clamp. The results showed that the bonding between wires and composites in lingual fixed retainers seemed to be lowest for rectangular smooth wires and increased in round twisted and rectangular twisted wires where the bonding was so strong that the maximum tension/bond strength was greater than the ultimate tensile strength of the wire. The highest values were in rectangular twisted wires. Concerning the composites, hybrid composites had the lowest interface bonding values and broke very quickly, while the nano- and micro-composites tolerated stronger forces and displayed higher bonding values. The best results were observed with the golden twisted wire and reached 21.46 MPa with the Transbond composite. With the rectangular braided wire the retention forces were so high that the Enamel Plus composite fractured when the load exceeded 154.6 N/MPa. When the same wire was combined with the Transbond LR either the wire or the composite broke when the force exceeded 240 N. The results of this

  16. Open-source micro-tensile testers via additive manufacturing for the mechanical characterization of thin films and papers

    PubMed Central

    Scheftic, Charlie M.; Brinson, L. Catherine

    2018-01-01

    The cost of specialized scientific equipment can be high and with limited funding resources, researchers and students are often unable to access or purchase the ideal equipment for their projects. In the fields of materials science and mechanical engineering, fundamental equipment such as tensile testing devices can cost tens to hundreds of thousands of dollars. While a research lab often has access to a large-scale testing machine suitable for conventional samples, loading devices for meso- and micro-scale samples for in-situ testing with the myriad of microscopy tools are often hard to source and cost prohibitive. Open-source software has allowed for great strides in the reduction of costs associated with software development and open-source hardware and additive manufacturing have the potential to similarly reduce the costs of scientific equipment and increase the accessibility of scientific research. To investigate the feasibility of open-source hardware, a micro-tensile tester was designed with a freely accessible computer-aided design package and manufactured with a desktop 3D-printer and off-the-shelf components. To our knowledge this is one of the first demonstrations of a tensile tester with additively manufactured components for scientific research. The capabilities of the tensile tester were demonstrated by investigating the mechanical properties of Graphene Oxide (GO) paper and thin films. A 3D printed tensile tester was successfully used in conjunction with an atomic force microscope to provide one of the first quantitative measurements of GO thin film buckling under compression. The tensile tester was also used in conjunction with an atomic force microscope to observe the change in surface topology of a GO paper in response to increasing tensile strain. No significant change in surface topology was observed in contrast to prior hypotheses from the literature. Based on this result obtained with the new open source tensile stage we propose an

  17. Open-source micro-tensile testers via additive manufacturing for the mechanical characterization of thin films and papers.

    PubMed

    Nandy, Krishanu; Collinson, David W; Scheftic, Charlie M; Brinson, L Catherine

    2018-01-01

    The cost of specialized scientific equipment can be high and with limited funding resources, researchers and students are often unable to access or purchase the ideal equipment for their projects. In the fields of materials science and mechanical engineering, fundamental equipment such as tensile testing devices can cost tens to hundreds of thousands of dollars. While a research lab often has access to a large-scale testing machine suitable for conventional samples, loading devices for meso- and micro-scale samples for in-situ testing with the myriad of microscopy tools are often hard to source and cost prohibitive. Open-source software has allowed for great strides in the reduction of costs associated with software development and open-source hardware and additive manufacturing have the potential to similarly reduce the costs of scientific equipment and increase the accessibility of scientific research. To investigate the feasibility of open-source hardware, a micro-tensile tester was designed with a freely accessible computer-aided design package and manufactured with a desktop 3D-printer and off-the-shelf components. To our knowledge this is one of the first demonstrations of a tensile tester with additively manufactured components for scientific research. The capabilities of the tensile tester were demonstrated by investigating the mechanical properties of Graphene Oxide (GO) paper and thin films. A 3D printed tensile tester was successfully used in conjunction with an atomic force microscope to provide one of the first quantitative measurements of GO thin film buckling under compression. The tensile tester was also used in conjunction with an atomic force microscope to observe the change in surface topology of a GO paper in response to increasing tensile strain. No significant change in surface topology was observed in contrast to prior hypotheses from the literature. Based on this result obtained with the new open source tensile stage we propose an

  18. Preparation and tensile properties of linear low density polyethylene/rambutan peels (Nephelium chryseum Blum.) flour blends

    NASA Astrophysics Data System (ADS)

    Nadhirah, A. Ainatun.; Sam, S. T.; Noriman, N. Z.; Voon, C. H.; Samera, S. S.

    2015-05-01

    The effect of rambutan peels flour (RPF) content on the tensile properties of linear low density polyethylene filled with rambutan peel flour was studied. RPF was melt blended with linear low-density polyethylene (LLDPE). LLDPE/RPF blends were prepared by using internal mixer (brabender) at 160 °C with the flour content ranged from 0 to 15 wt%. The tensile properties were tested by using a universal testing machine (UTM) according to ASTM D638. The highest tensile strength was observed for pure LLDPE while the tensile strength LLDPE/RPF decreased gradually with the addition of rambutan peels flour content from 0% to 15%. Young's modulus of 63 µm to 250 µm rambutan peels blends with LLDPE with the fiber loading of 0 - 15 wt% increased with increasing fiber loading.

  19. Evaluation of flexural, diametral tensile, and shear bond strength of composite repairs.

    PubMed

    Imbery, T A; Gray, T; DeLatour, F; Boxx, C; Best, A M; Moon, P C

    2014-01-01

    Repairing composite restorations may be a more conservative treatment than replacing the entire restoration. The objective of this in vitro study was to determine the best repair method by measuring flexural, diametral tensile, and shear bond strength of repaired composites in which the surfaces were treated with chemical primers (Add & Bond or Silane Bond Enhancer), a bonding agent (Optibond Solo Plus [OBSP]), or mechanical retention with a bonding agent. Filtek Supreme Ultra shade B1B was placed in special molds to fabricate specimens that served to test the flexural, diametral tensile, or shear strength of the inherent resin substrate. The same molds were modified to make specimens for testing repair strength of the resin. Repairs were made immediately or after aging in deionized water at 37°C for seven days. All repair sites were finished with coarse Sof-Lex discs to simulate finishing new restorations or partially removing aged restorations. Repair surfaces were treated with one of the following: 1) phosphoric-acid etching and OBSP; 2) Add & Bond; 3) phosphoric-acid etching, Silane Bond Enhancer, and OBSP; or 4) quarter round bur, phosphoric-acid etching, and OBSP. Specimens were placed back in the original molds to fabricate specimens for diametral tensile or flexural testing or in an Ultradent jig to make specimens for shear bond testing. Composite resin in shade B5B was polymerized against the treated surfaces to make repairs. Two negative control groups for the three testing methods consisted of specimens in which repairs were made immediately or after aging without any surface treatments. Controls and experimental repairs were aged (water 37°C, 24 hours) before flexural, diametral tensile, or shear testing in an Instron Universal testing machine at a crosshead speed of 0.5 mm/min. Experimental flexural repair strengths ranged from 26.4% to 88.6% of the inherent substrate strength. Diametral tensile repair strengths ranged from 40% to 80% of the inherent

  20. Transverse and longitudinal tensile properties at 760 C of several oxide dispersion strengthened nickel-base alloys

    NASA Technical Reports Server (NTRS)

    Anglin, A. E., Jr.

    1979-01-01

    The transverse and longitudinal tensile properties of the oxide dispersion strengthened nickel-base alloys were determined at 760 C. The alloys with small amounts of gamma prime have strength levels suitable for turbine vane applications, while other highly alloyed, gamma prime strengthened superalloys have strengths typical of turbine blade materials. These alloys were produced by mechanical alloying and extrusion and the turbine blade alloys were also directionally recrystallized. Resultant grain aspect ratios varied from 1:1 to over 20:1. Longitudinal tensile strengths ranged from 285 to 1175 MPa, while longitudinal elongations were in excess of 4 percent for all alloys. Transverse tensile strengths were comparable to longitudinal strengths, but transverse ductility levels were generally less than 2 percent elongation. Tensile and yield strengths increased with increasing strain rate over the range 0.001 to 0.05 per second. Ductility in both orientations was not strain rate sensitive but could be related to grain size and grain aspect ratio.

  1. Evaluation of microtensile and tensile bond strength tests determining effects of erbium, chromium: yttrium-scandium-gallium-garnet laser pulse frequency on resin-enamel bonding.

    PubMed

    Yildirim, T; Ayar, M K; Yesilyurt, C; Kilic, S

    2016-01-01

    The aim of the present study was to compare two different bond strength test methods (tensile and microtensile) in investing the influence of erbium, chromium: yttrium-scandium-gallium-garnet (Er, Cr: YSGG) laser pulse frequency on resin-enamel bonding. One-hundred and twenty-five bovine incisors were used in the present study. Two test methods were used: Tensile bond strength (TBS; n = 20) and micro-TBS (μTBS; n = 5). Those two groups were further split into three subgroups according to Er, Cr: YSGG laser frequency (20, 35, and 50 Hz). Following adhesive procedures, microhybrid composite was placed in a custom-made bonding jig for TBS testing and incrementally for μTBS testing. TBS and μTBS tests were carried out using a universal testing machine and a microtensile tester, respectively. Analysis of TBS results showed that means were not significantly different. For μTBS, the Laser-50 Hz group showed the highest bond strength (P < 0.05), and increasing frequency significantly increased bond strength (P < 0.05). Comparing the two tests, the μTBS results showed higher means and lower standard deviations. It was demonstrated that increasing μTBS pulse frequency significantly improved immediate bond strength while TBS showed no significant effect. It can, therefore, be concluded that test method may play a significant role in determining optimum laser parameters for resin bonding.

  2. Simulation study of the effect of strain rate on the mechanical properties and tensile deformation of gold nanowire

    NASA Astrophysics Data System (ADS)

    Shi, Guo-Jie; Wang, Jin-Guo; Hou, Zhao-Yang; Wang, Zhen; Liu, Rang-Su

    2017-09-01

    The mechanical properties and deformation mechanisms of Au nanowire during the tensile processes at different strain rates are revealed by the molecular dynamics method. It is found that the Au nanowire displays three distinct types of mechanical behaviors when tensioning at low, medium and high strain rates, respectively. At the low strain rate, the stress-strain curve displays a periodic zigzag increase-decrease feature, and the plastic deformation is resulted from the slide of dislocation. The dislocations nucleate, propagate, and finally annihilate in every decreasing stages of stress, and the nanowire always can recover to FCC-ordered structure. At the medium strain rate, the stress-strain curve gently decreases during the plastic process, and the deformation is contributed from sliding and twinning. The dislocations formed in the yield stage do not fully propagate and further escape from the nanowire. At the high strain rate, the stress-strain curve wave-like oscillates during the plastic process, and the deformation is resulted from amorphization. The FCC atoms quickly transform into disordered amorphous structure in the yield stage. The relative magnitude between the loading velocity of strain and the propagation velocity of phonons determines the different deformation mechanisms. The mechanical behavior of Au nanowire is similar to Ni, Cu and Pt nanowires, but their deformation mechanisms are not completely identical with each other.

  3. Electrothermal fracturing of tensile specimens

    NASA Technical Reports Server (NTRS)

    Blinn, H. O.; Hanks, J. G.; Perkins, H. P.

    1970-01-01

    Pulling device consisting of structural tube, connecting rod, spring-loaded nuts, loading rod, heating element, and three bulkheads fractures tensile specimens. Alternate heating and cooling increases tensile loading by increments until fracturing occurs. Load cell or strain gage, applied to pulling rod, determines forces applied.

  4. Investigation of the elastic modulus, tensile and flexural strength of five skull simulant materials for impact testing of a forensic skin/skull/brain model.

    PubMed

    Falland-Cheung, Lisa; Waddell, J Neil; Chun Li, Kai; Tong, Darryl; Brunton, Paul

    2017-04-01

    Conducting in vitro research for forensic, impact and injury simulation modelling generally involves the use of a skull simulant with mechanical properties similar to those found in the human skull. For this study epoxy resin, fibre filled epoxy resin, 3D-printing filaments (PETG, PLA) and self-cure acrylic denture base resin were used to fabricate the specimens (n=20 per material group), according to ISO 527-2 IBB and ISO20795-1. Tensile and flexural testing in a universal testing machine was used to measure their tensile/flexural elastic modulus and strength. The results showed that the epoxy resin and fibre filled epoxy resin had similar tensile elastic moduli (no statistical significant difference) with lower values observed for the other materials. The fibre filled epoxy resin had a considerably higher flexural elastic modulus and strength, possibly attributed to the presence of fibres. Of the simulants tested, epoxy resin had an elastic modulus and flexural strength close to that of mean human skull values reported in the literature, and thus can be considered as a suitable skull simulant for a skin/skull/brain model for lower impact forces that do not exceed the fracture stress. For higher impact forces a 3D printing filament (PLA) may be a more suitable skull simulant material, due to its closer match to fracture stresses found in human skull bone. Influencing factors were also anisotropy, heterogeneity and viscoelasticity of human skull bone and simulant specimens. Copyright © 2017 Elsevier Ltd. All rights reserved.

  5. Comparison of interfacial properties of electrodeposited single carbon fiber/epoxy composites using tensile and compressive fragmentation tests and acoustic emission.

    PubMed

    Park, Joung-Man; Kim, Jin-Won; Yoon, Dong-Jin

    2002-03-01

    Interfacial and microfailure properties of carbon fiber/epoxy composites were evaluated using both tensile fragmentation and compressive Broutman tests with an aid of acoustic emission (AE). A monomeric and two polymeric coupling agents were applied via the electrodeposition (ED) and the dipping applications. A monomeric and a polymeric coupling agent showed significant and comparable improvements in interfacial shear strength (IFSS) compared to the untreated case under both tensile and compressive tests. Typical microfailure modes including cone-shaped fiber break, matrix cracking, and partial interlayer failure were observed under tension, whereas the diagonal slipped failure at both ends of the fractured fiber exhibited under compression. Adsorption and shear displacement mechanisms at the interface were described in terms of electrical attraction and primary and secondary bonding forces. For both the untreated and the treated cases AE distributions were separated well in tension, whereas AE distributions were rather closely overlapped in compression. It might be because of the difference in molecular failure energies and failure mechanisms between tension and compression. The maximum AE voltage for the waveform of either carbon or large-diameter basalt fiber breakages in tension exhibited much larger than that in compression. AE could provide more likely the quantitative information on the interfacial adhesion and microfailure.

  6. In vitro comparison of the tensile bond strength of denture adhesives on denture bases.

    PubMed

    Kore, Doris R; Kattadiyil, Mathew T; Hall, Dan B; Bahjri, Khaled

    2013-12-01

    With several denture adhesives available, it is important for dentists to make appropriate patient recommendations. The purpose of this study was to evaluate the tensile bond strength of denture adhesives on denture base materials at time intervals of up to 24 hours. Fixodent, Super Poligrip, Effergrip, and SeaBond denture adhesives were tested with 3 denture base materials: 2 heat-polymerized (Lucitone 199 and SR Ivocap) and 1 visible-light-polymerized (shade-stable Eclipse). Artificial saliva with mucin was used as a control. Tensile bond strength was tested in accordance with American Dental Association specifications at 5 minutes, 3 hours, 6 hours, 12 hours, and 24 hours after applying the adhesive. Maximum forces before failure were recorded in megapascals (MPa), and the data were subjected to a 2-way analysis of variance (α=.05). All 4 adhesives had greater tensile bond strength than the control. Fixodent, Super Poligrip, and SeaBond had higher tensile bond strength values than Effergrip. All adhesives had the greatest tensile bond strength at 5 minutes and the least at 24 hours. The 3 denture bases produced significantly different results with each adhesive (P<.001). Lucitone 199 with the adhesives had the greatest tensile bond strength, followed by Ivocap and Eclipse. All 4 adhesives had greater tensile bond strength than the control, and all 4 adhesives were strongest at the 5-minute interval. On all 3 types of denture bases, Effergrip produced significantly lower tensile bond strength, and Fixodent, Super Poligrip, and SeaBond produced significantly higher tensile bond strength. At 24 hours, the adhesive-base combinations with the highest tensile bond strength were Fixodent on Lucitone 199, Fixodent on Eclipse, Fixodent on Ivocap, and Super Poligrip on Ivocap. Copyright © 2013 Editorial Council for the Journal of Prosthetic Dentistry. Published by Mosby, Inc. All rights reserved.

  7. Microstructure and Tensile/Corrosion Properties Relationships of Directionally Solidified Al-Cu-Ni Alloys

    NASA Astrophysics Data System (ADS)

    Rodrigues, Adilson V.; Lima, Thiago S.; Vida, Talita A.; Brito, Crystopher; Garcia, Amauri; Cheung, Noé

    2018-03-01

    Al-Cu-Ni alloys are of scientific and technological interest due to high strength/high temperature applications, based on the reinforcement originated from the interaction between the Al-rich phase and intermetallic composites. The nature, morphology, size, volume fraction and dispersion of IMCs particles throughout the Al-rich matrix are important factors determining the resulting mechanical and chemical properties. The present work aims to evaluate the effect of the addition of 1wt%Ni into Al-5wt%Cu and Al-15wt%Cu alloys on the solidification rate, macrosegregation, microstructure features and the interrelations of such characteristics on tensile and corrosion properties. A directional solidification technique is used permitting a wide range of microstructural scales to be examined. Experimental growth laws relating the primary and secondary dendritic spacings to growth rate and solidification cooling rate are proposed, and Hall-Petch type equations are derived relating the ultimate tensile strength and elongation to the primary dendritic spacing. Considering a compromise between ultimate tensile strength and corrosion resistance of the examined alloys samples from both alloys castings it is shown that the samples having more refined microstructures are associated with the highest values of such properties.

  8. Theoretical Conversions of Different Hardness and Tensile Strength for Ductile Materials Based on Stress-Strain Curves

    NASA Astrophysics Data System (ADS)

    Chen, Hui; Cai, Li-Xun

    2018-04-01

    Based on the power-law stress-strain relation and equivalent energy principle, theoretical equations for converting between Brinell hardness (HB), Rockwell hardness (HR), and Vickers hardness (HV) were established. Combining the pre-existing relation between the tensile strength ( σ b ) and Hollomon parameters ( K, N), theoretical conversions between hardness (HB/HR/HV) and tensile strength ( σ b ) were obtained as well. In addition, to confirm the pre-existing σ b -( K, N) relation, a large number of uniaxial tensile tests were conducted in various ductile materials. Finally, to verify the theoretical conversions, plenty of statistical data listed in ASTM and ISO standards were adopted to test the robustness of the converting equations with various hardness and tensile strength. The results show that both hardness conversions and hardness-strength conversions calculated from the theoretical equations accord well with the standard data.

  9. Microstructural and strain rate effects on plastic deformation in aluminum 2219-T87

    NASA Astrophysics Data System (ADS)

    Rincon, Carlos D.

    A fundamental investigation has been conducted on the effects of microstructure and strain rate on the plastic deformation of theta-prime-strengthened 2219 aluminum. The motivation for this work is based upon a previous study which showed inhomogeneous and locally extreme work hardening in the HAZ regions in VPPA 2219-T87 butt welds. This strongly suggests that the HAZ microstructure plays a major role in the deformation and fracture process in precipitation hardened aluminum alloy 2219. Tensile specimens of the weld joint exhibited more rapid work hardening in the heat-affected-zone (HAZ) at higher strain levels. Microhardness contour maps for these welds illustrated that late stage deformation was concentrated in two crossing bands at about 45sp° to the tensile axis. The width of the deformation bands and the ultimate tensile strength seemed to be dictated by the amount of work hardening in the HAZ. In this study, three different heat treatments were used to produce samples with different particle sizes and particle spacings, but all hardened by copper aluminide precipitates of the thetasp' structure. The heat treatments were categorized as being (A) as-received T87 condition, (B) T87 condition aged at approximately 204sp°C for 3 hours and (C) T87 over-aged at 204sp°C for 7 days. Uniaxial tensile tests consisted of two sets of experiments: (1) three heat treatments (A, B, and C) at two strain rates (0.02 minsp{-1} and 0.2 minsp{-1}) and (2) three heat treatments that were interrupted at select stress-strain levels (0.8% and 2% total strain) during the tensile tests at strain rate equal to 0.02 minsp{-1} at room temperature. Furthermore, a detailed transmission electron microscopy (TEM) study demonstrates the microstructural development during tensile deformation. The Voce equation of strain-hardening provides a slightly better fit to the tensile curves than the Ludwik-Hollomon equation. At higher strains, localized areas showed strain fields around thetasp

  10. Effects of LEO Environment on Tensile Properties of PEEK Films

    NASA Astrophysics Data System (ADS)

    Nakamura, Takashi; Nakamura, Hiroshi; Shimamura, Hiroyuki

    2009-01-01

    To clarify the effects of space environment on mechanical properties of polymer, exposure experiments were conducted utilizing the International Space Station Russian Service Module. Poly-ether-ether-ketone (PEEK) films under tensile stress were exposed to low Earth orbit (LEO) environment, and reference samples were irradiated with atomic oxygen (AO), electron beam (EB), and ultraviolet light (UV) in ground facilities. By comparing the results of flight and ground tests, the degradation behavior and the influential factors in LEO were investigated. The following results were obtained. (1) UV was found to be the harshest factor in LEO on tensile properties, since it decreased elongation to 15% of pristine sample after 46-months exposure. (2) AO in LEO eroded the specimen surface with a cone-like morphology and reduced the thickness; however, it had no significant effect on tensile properties. (3) EB irradiation in LEO had no measurable effects on the material properties.

  11. Tensile strength of laser welded cobalt-chromium alloy with and without an argon atmosphere.

    PubMed

    Tartari, Anna; Clark, Robert K F; Juszczyk, Andrzej S; Radford, David R

    2010-06-01

    The tensile strength and depth of weld of two cobalt chromium alloys before and after laser welding with and without an argon gas atmosphere were investigated. Using two cobalt chromium alloys, rod shaped specimens (5 cm x 1.5 mm) were cast. Specimens were sand blasted, sectioned and welded with a pulsed Nd: YAG laser welding machine and tested in tension using an Instron universal testing machine. A statistically significant difference in tensile strength was observed between the two alloys. The tensile strength of specimens following laser welding was significantly less than the unwelded controls. Scanning electron microscopy showed that the micro-structure of the cast alloy was altered in the region of the weld. No statistically significant difference was found between specimens welded with or without an argon atmosphere.

  12. Tensile properties of V-Cr-Ti alloys after exposure in helium and low-partial-pressure oxygen environments

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Natesan, K.; Soppet, W.K.

    1997-04-01

    A test program is in progress to evaluate the effect of oxygen at low pO{sub 2} on the tensile properties of V-(4-5)wt% Cr-(4-5)wt% Ti alloys. Some of the tensile specimens were precharged with oxygen at low pO{sub 2} at 500{degrees}C and reannealed in vacuum at 500{degrees}C in environments with various pO{sub 2} levels and subsequently tensile tested at room temperature. The preliminary results indicate that both approaches are appropriate for evaluating the effect of oxygen uptake on the tensile properties of the alloys. The data showed that in the relatively short-time tests conducted thus far, the maximum engineering stress slightlymore » increased after oxygen exposure but the uniform and total elongation values exhibited significant decrease after exposure in oxygen-containing environments. The data for a specimen exposed to a helium environment were similar to those obtained in low pO{sub 2} environments.« less

  13. Microstructure, Tensile Properties, and Corrosion Behavior of Die-Cast Mg-7Al-1Ca- xSn Alloys

    NASA Astrophysics Data System (ADS)

    Wang, Feng; Dong, Haikuo; Sun, Shijie; Wang, Zhi; Mao, Pingli; Liu, Zheng

    2018-02-01

    The microstructure, tensile properties, and corrosion behavior of die-cast Mg-7Al-1Ca- xSn ( x = 0, 0.5, 1.0, and 2.0 wt.%) alloys were studied using OM, SEM/EDS, tensile test, weight loss test, and electrochemical test. The experimental results showed that Sn addition effectively refined grains and intermetallic phases and increased the amount of intermetallic phases. Meanwhile, Sn addition to the alloys suppressed the formation of the (Mg,Al)2Ca phase and resulted in the formation of the ternary CaMgSn phase and the binary Mg2Sn phase. The Mg-7Al-1Ca-0.5Sn alloy exhibited best tensile properties at room temperature, while Mg-7Al-1Ca-1.0Sn alloy exhibited best tensile properties at elevated temperature. The corrosion resistance of studied alloys was improved by the Sn addition, and the Mg-7Al-1Ca-0.5Sn alloy presented the best corrosion resistance.

  14. A novel in situ device based on a bionic piezoelectric actuator to study tensile and fatigue properties of bulk materials.

    PubMed

    Wang, Shupeng; Zhang, Zhihui; Ren, Luquan; Zhao, Hongwei; Liang, Yunhong; Zhu, Bing

    2014-06-01

    In this work, a miniaturized device based on a bionic piezoelectric actuator was developed to investigate the static tensile and dynamic fatigue properties of bulk materials. The device mainly consists of a bionic stepping piezoelectric actuator based on wedge block clamping, a pair of grippers, and a set of precise signal test system. Tensile and fatigue examinations share a set of driving system and a set of signal test system. In situ tensile and fatigue examinations under scanning electron microscope or metallographic microscope could be carried out due to the miniaturized dimensions of the device. The structure and working principle of the device were discussed and the effects of output difference between two piezoelectric stacks on the device were theoretically analyzed. The tensile and fatigue examinations on ordinary copper were carried out using this device and its feasibility was verified through the comparison tests with a commercial tensile examination instrument.

  15. Effects of static tensile load on the thermal expansion of Gr/PI composite material

    NASA Technical Reports Server (NTRS)

    Farley, G. L.

    1981-01-01

    The effect of static tensile load on the thermal expansion of Gr/PI composite material was measured for seven different laminate configurations. A computer program was developed which implements laminate theory in a piecewise linear fashion to predict the coupled nonlinear thermomechanical behavior. Static tensile load significantly affected the thermal expansion characteristics of the laminates tested. This effect is attributed to a fiber instability micromechanical behavior of the constituent materials. Analytical results correlated reasonably well with free thermal expansion tests (no load applied to the specimen). However, correlation was poor for tests with an applied load.

  16. Evaluation of tensile strength of surgical synthetic absorbable suture materials: an in vitro study

    PubMed Central

    Ranganath, V.; Nichani, Ashish Sham

    2013-01-01

    Purpose The purpose of this study was to evaluate the tensile strength of surgical synthetic absorbable sutures over a period of 14 days under simulated oral conditions. Methods Three suture materials (polyglycolic acid [PGA], polyglactin [PG] 910, and poly (glycolide-co-є-caprolactone) [PGC]) were used in 4-0 and 5-0 gauges. 210 suture samples (35 of each material and gauge) were used. All of the samples were tested preimmersion and 1 hour and 1, 3, 7, 10, and 14 days postimmersion. The tensile strength of each suture material and gauge was assessed. The point of breakage and the resorption pattern of the sutures were also assessed. Results During the first 24 hours of immersion, all 4-0 and 5-0 samples of PGA, PG 910, and PGC maintained their initial tensile strength. At baseline (preimmersion), there was a statistically significant (P<0.001) difference in the tensile strengths between the 4-0 and 5-0 gauge of PGA, PG 910, and PGC. PGA 4-0 showed the highest tensile strength until day 10. At 7 days, all the 4-0 sutures of the three materials had maintained their tensile strength with PGA 4-0 having significantly greater (P=0.003) tensile strength compared to PG. Conclusions 4-0 sutures are stronger and have greater tensile strength than 5-0 sutures. The PGA 4-0 suture showed the highest tensile strength at the end of day 10. PMID:23837127

  17. Experimental investigation of anisotropy evolution of AZ31 magnesium alloy sheets under tensile loading

    NASA Astrophysics Data System (ADS)

    Tari, D. Ghaffari; Worswick, M. J.

    2011-05-01

    Increasing demand for lighter final products has created new opportunities for the application of new light weight materials. Due to high strength to density ratio and good magnetic resistance properties, magnesium alloys are good candidates to replace steel and aluminum for same application. However, limited numbers of active slip deformation mechanisms, result in a decreased formability at room temperature. Furthermore, wrought magnesium alloys have an initial crystallographic texture, remained from the prior rolling operations, which makes them highly anisotropic. In this paper, tensile tests are performed at room temperature and 200° C at different strain rates and orientations relative to the rolling direction, including rolling, 30°, 45°, 60° and transverse orientation. The strain rates adopted for these experiments varied from 0.001 to 1.0. The testing results show the effect of temperature on the strain rate sensitivity of AZ31 sheets. The extent of deformation is continuously recorded using two separate high temperature extensometers. The results of testing show an increase in the r-values with the plastic deformation. The strain rate sensitivity of AZ31 increased as the temperature was elevated. At higher strain rates the measured r-values are larger and the slope of its evolution with the plastic strain is steeper.

  18. Effects of Sn addition on the microstructure and tensile properties of AX55 alloys

    NASA Astrophysics Data System (ADS)

    Qiu, K. Q.; Huang, P.

    2018-04-01

    The microstructures and tensile properties at both room and elevated temperatures for both the as-cast and as-aged Mg-5Al-5Ca (AX55) alloy with 0–2 wt% Sn addition were studied. The results indicate that the α-Mg dendrite is gradually refined and the interdendritic Al2Ca and Mg2Ca intermetallics become more connected with Sn addition. The as-cast AX55-1Sn alloy shows optimal ultimate tensile strength (UTS) at testing temperature from 25 to 225 °C. After T61 and T62 heat treatment, the eutectic-lamellar microstructure of the as-cast alloys tends to be spheroidized and distributed uniformly along the grain boundaries. While the alloys with higher Sn content show higher density of granulated and needle-shaped Al2Ca phases precipitated into α-Mg matrix, which results in the increase of UTS, yield strength (YS), elongation and microhardness with Sn addition. The morphology of CaMgSn phase can be improved by T62 treatment, which makes as-aged AX55-2.0Sn alloy exhibit a smaller decrease rate of the UTS at temperature up to 225 °C. The heat resistance of different heat-resistant magnesium alloys were compared and discussed by using the decrease rate of the UTS.

  19. Creep and tensile properties of several oxide-dispersion-strengthened nickel-base alloys at 1365 K

    NASA Technical Reports Server (NTRS)

    Wittenberger, J. D.

    1977-01-01

    The tensile properties at room temperature and at 1365 K and the tensile creep properties at low strain rates at 1365 K were measured for several oxide-dispersion-strengthened (ODS) alloys. The alloys examined included ODS Ni, ODS Ni-20Cr, and ODS Ni-16Cr-Al. Metallography of creep tested, large grain size ODS alloys indicated that creep of these alloys is an inhomogeneous process. All alloys appear to possess a threshold stress for creep. This threshold stress is believed to be associated with diffusional creep in the large grain size ODS alloys and normal dislocation motion in perfect single crystal (without transverse low angle boundaries) ODS alloys. Threshold stresses for large grain size ODS Ni-20Cr and Ni-16Cr-Al type alloys are dependent on the grain aspect ratio. Because of the deleterious effect of prior creep on room temperature mechanical properties of large grain size ODS alloys, it is speculated that the threshold stress may be the design limiting creep strength property.

  20. Effect of salivary pH on diametral tensile strength of glass ionomer cement coated with coating agent

    NASA Astrophysics Data System (ADS)

    Farahdillah; Triaminingsih, S.; Eriwati, Y. K.

    2017-08-01

    The aim of this study was to analyze the effect of salivary pH to diametral tensile strength of glass ionomer cement (GIC) coated with a coating agent. GIC specimens coated with varnish and nano-filled coating agent were stored in artificial saliva at pH values of 4.5, 5.5, and 7 for 24 h at 37°C, then the diametral tensile strength was tested by universal testing machine. Results showed that there was no significant difference in the diametral tensile strength of the GIC coated with varnish and nano-filled coating agent with decreasing of salivary pH (p < 0.05). It can be concluded that salivary pH does not affect the diametral tensile strength of GIC coated by varnish or nano-filled coating agent

  1. Compressive and tensile strength for concrete containing coal bottom ash

    NASA Astrophysics Data System (ADS)

    Maliki, A. I. F. Ahmad; Shahidan, S.; Ali, N.; Ramzi Hannan, N. I. R.; Zuki, S. S. Mohd; Ibrahim, M. H. W.; Azmi, M. A. Mohammad; Rahim, M. Abdul

    2017-11-01

    The increasing demand in the construction industry will lead to the depletion of materials used in construction sites such as sand. Due to this situation, coal bottom ash (CBA) was selected as a replacement for sand. CBA is a by-product of coal combustion from power plants. CBA has particles which are angular, irregular and porous with a rough surface texture. CBA also has the appearance and particle size distribution similar to river sand. Therefore, these properties of CBA make it attractive to be used as fine aggregate replacement in concrete. The objectives of this study were to determine the properties of CBA concrete and to evaluate the optimum percentage of CBA to be used in concrete as fine aggregate replacement. The CBA was collected at Tanjung Bin power plant. The mechanical experiment (compressive and tensile strength test) was conducted on CBA concrete. Before starting the mechanical experiment, cubic and cylindrical specimens with dimensions measuring 100 × 100 × 100 mm and 150 × 300 mm were produced based on the percentage of coal bottom ash in this study which is 0% as the control specimen. Meanwhile 10%, 20%, 30%, 40%, 50%, 60%, 70%, 80%, 90% and 100% of CBA were used to replace the fine aggregates. The CBA concrete samples were cured for 7 days and 28 days respectively to maintain the rate of hydration and moisture. After the experimental work was done, it can be concluded that the optimum percentage of CBA as fine aggregate is 60% for a curing period of both 7 days and 28 days with the total compressive strength of 36.4 Mpa and 46.2 Mpa respectively. However, the optimum percentage for tensile strength is at 70% CBA for a curing period of both 7 days and 28 days with a tensile strength of 3.03 MPa and 3.63 MPa respectively.

  2. Combined spectrophotometry and tensile measurements of human connective tissues: potentials and limitations.

    PubMed

    Ernstberger, Markus; Sichting, Freddy; Baselt, Tobias; Hartmann, Peter; Aust, Gabriela; Hammer, Niels

    2013-06-01

    Strain-dependent transmission data of nine iliotibial tract specimens are determined using a custom-built optical setup with a halogen light source and an industrial norm material testing machine. Polarized light microscopy and hematoxylin-eosin staining indicated that lateral contraction of collagen structures is responsible for total intensity variations during a 20-cycle preconditioning and a 5-cycle tensile test. Tensile force progress is opposite to total transmission progress. Due to dehydration, wavelength-specific radiation intensity shifting is determined during the test, primarily noticeable in a water absorption band between 1400 and 1500 nm. The results show the capability of integrating spectrophotometry technology into biomechanics for determining structural alterations of human collagen due to applied strain. Being more sensitive to drying, spectrophotometry may likely serve as a quality control in stress-strain testing of biological structures.

  3. Optimizing the tensile properties of polyvinyl alcohol hydrogel for the construction of a bioprosthetic heart valve stent.

    PubMed

    Wan, W K; Campbell, G; Zhang, Z F; Hui, A J; Boughner, D R

    2002-01-01

    Although bioprosthetic heart valves offer the benefits of a natural opening and closing, better hemodynamics, and avoidance of life-long anticoagulant therapy, they nevertheless tend to fail in 10-15 years from tears and calcification. Several authors, including the present ones, have identified the rigid stent as a factor contributing to these failures. The ultimate solution is an artificial heart valve that has mechanical properties that allow it to move in conformity with the aortic root during the cardiac cycle, has superior hemodynamics, is nonthrombogenic, will last more than 20 years, and mitigates the need for anticoagulants. We have identified a polymer, polyvinyl alcohol (PVA) hydrogel, that has mechanical properties similar to soft tissue. The purpose of this research is to match the tensile properties of PVA to the porcine aortic root and to fabricate a stent prototype for a bioprosthetic heart valve with the use of the PVA hydrogel. Specimens of 15% w/w PVA were prepared by processing through 1-6 cycles of freezing (-20 degrees C) at 0.2 degrees C/min freeze rate and thawing (+20 degrees C) at different thawing rates (0.2 degrees C/min and 1 degrees C/min), for different holding times (1 and 6 h) at -20 degrees C. Subsequently tensile tests and stress-relaxation tests were conducted on the specimens. The different holding times at -20 degrees C demonstrated no difference in the result. The slower thawing rate improved the tensile properties but did not produce significant changes on the stress-relaxation properties. The nonlinear stress-strain curve for the PVA after the fourth freeze-thaw cycle matched the porcine aortic root within the physiological pressure range. The stress-relaxation curve for PVA also approximated the shape of the aortic root. The complex geometry of an artificial heart valve stent was successfully injection molded. These results, in combination with other preliminary findings for biocompatibility and fatigue behavior, suggest

  4. Ratcheting Strain and Microstructure Evolution of AZ31B Magnesium Alloy under a Tensile-Tensile Cyclic Loading

    PubMed Central

    Wang, Denghui; Wang, Wenxian; Zhou, Jun; He, Xiuli; Dong, Peng; Zhang, Hongxia; Sun, Liyong

    2018-01-01

    In this paper, studies were conducted to investigate the deformation behavior and microstructure change in a hot-rolled AZ31B magnesium alloy during a tensile-tensile cyclic loading. The relationship between ratcheting effect and microstructure change was discussed. The ratcheting effect in the material during current tensile-tensile fatigue loading exceeds the material’s fatigue limit and the development of ratcheting strain in the material experienced three stages: initial sharp increase stage (Stage I); steady stage (Stage II); and final abrupt increase stage (Stage III). Microstructure changes in Stage I and Stage II are mainly caused by activation of basal slip system. The Extra Geometrically Necessary Dislocations (GNDs) were also calculated to discuss the relationship between the dislocation caused by the basal slip system and the ratcheting strain during the cyclic loading. In Stage III, both the basal slip and the {11−20} twins are found active during the crack propagation. The fatigue crack initiation in the AZ31B magnesium alloy is found due to the basal slip and the {11−20} tensile twins. PMID:29597278

  5. Ratcheting Strain and Microstructure Evolution of AZ31B Magnesium Alloy under a Tensile-Tensile Cyclic Loading.

    PubMed

    Yan, Zhifeng; Wang, Denghui; Wang, Wenxian; Zhou, Jun; He, Xiuli; Dong, Peng; Zhang, Hongxia; Sun, Liyong

    2018-03-28

    In this paper, studies were conducted to investigate the deformation behavior and microstructure change in a hot-rolled AZ31B magnesium alloy during a tensile-tensile cyclic loading. The relationship between ratcheting effect and microstructure change was discussed. The ratcheting effect in the material during current tensile-tensile fatigue loading exceeds the material's fatigue limit and the development of ratcheting strain in the material experienced three stages: initial sharp increase stage (Stage I); steady stage (Stage II); and final abrupt increase stage (Stage III). Microstructure changes in Stage I and Stage II are mainly caused by activation of basal slip system. The Extra Geometrically Necessary Dislocations (GNDs) were also calculated to discuss the relationship between the dislocation caused by the basal slip system and the ratcheting strain during the cyclic loading. In Stage III, both the basal slip and the {11-20} twins are found active during the crack propagation. The fatigue crack initiation in the AZ31B magnesium alloy is found due to the basal slip and the {11-20} tensile twins.

  6. Tensile and stress-rupture behavior of hafnium carbide dispersed molybdenum and tungsten base alloy wires

    NASA Technical Reports Server (NTRS)

    Yun, Hee Mann; Titran, Robert H.

    1993-01-01

    The tensile strain rate sensitivity and the stress-rupture strength of Mo-base and W-base alloy wires, 380 microns in diameter, were determined over the temperature range from 1200 K to 1600 K. Three molybdenum alloy wires; Mo + 1.1w/o hafnium carbide (MoHfC), Mo + 25w/o W + 1.1w/o hafnium carbide (MoHfC+25W) and Mo + 45w/o W + 1.1w/o hafnium carbide (MoHfC+45W), and a W + 0.4w/o hafnium carbide (WHfC) tungsten alloy wire were evaluated. The tensile strength of all wires studied was found to have a positive strain rate sensitivity. The strain rate dependency increased with increasing temperature and is associated with grain broadening of the initial fibrous structures. The hafnium carbide dispersed W-base and Mo-base alloys have superior tensile and stress-rupture properties than those without HfC. On a density compensated basis the MoHfC wires exhibit superior tensile and stress-rupture strengths to the WHfC wires up to approximately 1400 K. Addition of tungsten in the Mo-alloy wires was found to increase the long-term stress rupture strength at temperatures above 1400 K. Theoretical calculations indicate that the strength and ductility advantage of the HfC dispersed alloy wires is due to the resistance to recrystallization imparted by the dispersoid.

  7. Microscopic Characterization of Tensile and Shear Fracturing in Progressive Failure in Marble

    NASA Astrophysics Data System (ADS)

    Cheng, Yi; Wong, Louis Ngai Yuen

    2018-01-01

    Compression-induced tensile and shear fractures were reported to be the two fundamental fracture types in rock fracturing tests. This study investigates such tensile and shear fracturing process in marble specimens containing two different flaw configurations. Observations first reveal that the development of a tensile fracture is distinct from shear fracture with respect to their nucleation, propagation, and eventual formation in macroscale. Second, transgranular cracks and grain-scale spallings become increasingly abundant in shear fractures as loading increases, which is almost not observed in tensile fractures. Third, one or some dominant extensional microcracks are commonly observed in the center of tensile fractures, while such development of microcracks is almost absent in shear fractures. Microcracks are generally of a length comparable to grain size and distribute uniformly within the damage zone of the shear fracture. Fourth, the width of densely damaged zone in the shear fracture is nearly 10 times of that in the tensile fracture. Quantitative measurement on microcrack density suggests that (1) microcrack density in tensile and shear fractures display distinct characteristics with increasing loading, (2) transgranular crack density in the shear fracture decreases logarithmically with the distance away from the shear fracture center, and (3) whatever the fracture type, the anisotropy can only be observed for transgranular cracks with a large density, which partially explains why microcrack anisotropy usually tends to be unobvious until approaching peak stress in specimens undergoing brittle failure. Microcracking characteristics observed in this work likely shed light to some phenomena and conclusions generalized in seismological studies.

  8. Tensile bond strength of metal bracket bonding to glazed ceramic surfaces with different surface conditionings.

    PubMed

    Akhoundi, Ms Ahmad; Kamel, M Rahmati; Hashemi, Sh Mahmood; Imani, M

    2011-01-01

    The objective of this study was to compare the tensile bond strength of metal brackets bonding to glazed ceramic surfaces using three various surface treatments. Forty two glazed ceramic disks were assigned to three groups. In the first and second groups the specimens were etched with 9.5% hydrofluoric acid (HFA). Subsequently in first group, ceramic primer and adhesive were applied, but in second group a bonding agent alone was used. In third group, specimens were treated with 35% phosphoric acid followed by ceramic primer and adhesive application. Brackets were bonded with light cure composites. The specimens were stored in distilled water in the room temperature for 24 hours and thermocycled 500 times between 5°C and 55°C. The universal testing machine was used to test the tensile bond strength and the adhesive remenant index scores between three groups was evaluated. The data were subjected to one-way ANOVA, Tukey and Kruskal-Wallis tests respectively. The tensile bond strength was 3.69±0.52 MPa forfirst group, 2.69±0.91 MPa for second group and 3.60±0.41 MPa for third group. Group II specimens showed tensile strength values significantly different from other groups (P<0.01). In spite of limitations in laboratory studies it may be concluded that in application of Scotch bond multipurpose plus adhesive, phosphoric acid can be used instead of HFA for bonding brackets to the glazed ceramic restorations with enough tensile bond strength.

  9. A novel in situ device based on a bionic piezoelectric actuator to study tensile and fatigue properties of bulk materials

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Wang, Shupeng; Zhang, Zhihui, E-mail: zhzh@jlu.edu.cn; Ren, Luquan

    2014-06-15

    In this work, a miniaturized device based on a bionic piezoelectric actuator was developed to investigate the static tensile and dynamic fatigue properties of bulk materials. The device mainly consists of a bionic stepping piezoelectric actuator based on wedge block clamping, a pair of grippers, and a set of precise signal test system. Tensile and fatigue examinations share a set of driving system and a set of signal test system. In situ tensile and fatigue examinations under scanning electron microscope or metallographic microscope could be carried out due to the miniaturized dimensions of the device. The structure and working principlemore » of the device were discussed and the effects of output difference between two piezoelectric stacks on the device were theoretically analyzed. The tensile and fatigue examinations on ordinary copper were carried out using this device and its feasibility was verified through the comparison tests with a commercial tensile examination instrument.« less

  10. The temperature dependence of the tensile properties of thermally treated Alloy 690 tubing

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Harrod, D.L.; Gold, R.E.; Larsson, B.

    1992-12-31

    Tensile tests were run in air on full tube cross-sections of 22.23 mm OD by 1.27 mm wall thickness Alloy 690 steam generator production tubes from ten (10) heats of material at eight (8) temperatures between room temperature and 760{degrees}C. The tubing was manufactured to specification requirements consistent with the EPRI guidelines for Alloy 690 tubing. The room temperature stress-strain curves are described quite well by the Voce equation. Ductile fracture by dimpled rupture was observed at all test temperatures. The elevated temperature tensile properties are compared with design data given in the ASME Code.

  11. Fatigue crack growth in 2024-T3 aluminum under tensile and transverse shear stresses

    NASA Technical Reports Server (NTRS)

    Viz, Mark J.; Zehnder, Alan T.

    1994-01-01

    The influence of transverse shear stresses on the fatigue crack growth rate in thin 2024-T3 aluminum alloy sheets is investigated experimentally. The tests are performed on double-edge cracked sheets in cyclic tensile and torsional loading. This loading generates crack tip stress intensity factors in the same ratio as the values computed for a crack lying along a lap joint in a pressurized aircraft fuselage. The relevant fracture mechanics of cracks in thin plates along with the details of the geometrically nonlinear finite element analyses used for the test specimen calibration are developed and discussed. Preliminary fatigue crack growth data correlated using the fully coupled stress intensity factor calibration are presented and compared with fatigue crack growth data from pure delta K(sub I)fatigue tests.

  12. Experimental and Numerical Analysis of the Effects of Curing Time on Tensile Mechanical Properties of Thin Spray-on Liners

    NASA Astrophysics Data System (ADS)

    Guner, D.; Ozturk, H.

    2016-08-01

    The effects of curing time on tensile elastic material properties of thin spray-on liners (TSLs) were investigated in this study. Two different TSL products supplied by two manufacturers were tested comparatively. The "dogbone" tensile test samples that were prepared in laboratory conditions with different curing times (1, 7, 14, 21, and 28 days) were tested based on ASTM standards. It was concluded that longer curing times improves the tensile strength and the Young's Modulus of the TSLs but decreases their elongation at break. Moreover, as an additional conclusion of the testing procedure, it was observed that during the tensile tests, the common malpractice of measuring sample displacement from the grips of the loading machine with a linear variable displacement transducer versus the sample's gauge length had a major impact on modulus and deformation determination of TSLs. To our knowledge, true stress-strain curves were generated for the first time in TSL literature within this study. Numerical analyses of the laboratory tests were also conducted using Particle Flow Code in 2 Dimensions (PFC2D) in an attempt to guide TSL researchers throughout the rigorous PFC simulation process to model support behaviour of TSLs. A scaling coefficient between macro- and micro-properties of PFC was calculated which will help future TSL PFC modellers mimic their TSL behaviours for various tensile loading support scenarios.

  13. Effect of natural fiber types and sodium silicate coated on natural fiber mat/PLA composites: Tensile properties and rate of fire propagation

    NASA Astrophysics Data System (ADS)

    Thongpin, C.; Srimuk, J.; hipkam, N.; Wachirapong, P.

    2015-07-01

    In this study, 3 types of natural fibres, i.e. jute, sisal and abaca, were plain weaved to fibre mat. Before weaving, the fibres were treated with 5% NaOH to remove hemi cellulose and lignin. The weaving was performed by hand using square wooden block fit with nails for weaving using one and two types of natural fibres as weft and warp fibre to produce natural fibre mat. The fibre mat was also impregnated in sodium silicate solution extracted from rich husk ash. The pH of the solution was adjusted to pH 7 using H2SO4 before impregnation. After predetermined time, sodium silicate was gelled and deposited on the mat. The fabric mat and sodium silicate coated mat were then impregnated with PLA solution to produce prepreg. Dried pepreg was laminated with PLA sheet using compressing moulding machine to obtain natural fibre mat/PLA composite. The composite containing abaca aligned in longitudinal direction with respect to tension force enhanced Young's modulus more than 300%. Fibre mat composites with abaca aligned in longitudinal direction also showed tensile strength enhancement nearly 400% higher than neat PLA. After coating with sodium silicate, the tensile modulus of the composites was found slightly increased. The silicate coating was disadvantage on tensile strength of the composite due to the effect of sodium hydroxide solution that was used as solvent for silicate extraction from rice husk ash. However, sodium silicate could retard rate of fire propagation about 50%compare to neat PLA and about 10% reduction compared to fibre mat composites without sodium silicate coated fibre mat.

  14. Ab initio elastic properties and tensile strength of crystalline hydroxyapatite.

    PubMed

    Ching, W Y; Rulis, Paul; Misra, A

    2009-10-01

    We report elastic constant calculation and a "theoretical" tensile experiment on stoichiometric hydroxyapatite (HAP) crystal using an ab initio technique. These results compare favorably with a variety of measured data. Theoretical tensile experiments are performed on the orthorhombic cell of HAP for both uniaxial and biaxial loading. The results show considerable anisotropy in the stress-strain behavior. It is shown that the failure behavior of the perfect HAP crystal is brittle for tension along the z-axis with a maximum stress of 9.6 GPa at 10% strain. Biaxial failure envelopes from six "theoretical" loading tests show a highly anisotropic pattern. Structural analysis of the crystal under various stages of tensile strain reveals that the deformation behavior manifests itself mainly in the rotation of the PO(4) tetrahedron with concomitant movements of both the columnar and axial Ca ions. These results are discussed in the context of mechanical properties of bioceramic composites relevant to mineralized tissues.

  15. High temperature tensile behavior and microstructure of Al-SiC nanocomposite fabricated by mechanical milling and hot extrusion technique

    NASA Astrophysics Data System (ADS)

    Soltani, Mohammadreza; Atrian, Amir

    2018-02-01

    This paper investigates the high-temperature tensile behavior of Al-SiC nanocomposite reinforced with 0, 1.5, and 3 vol% SiC nano particles. To fabricate the samples, SiC nano reinforcements and aluminum (Al) powders were milled using an attritor milling and then were cold pressed and hot extruded at 500 °C. Afterward, mechanical and microstructural characteristics were studied in different temperatures. To this end, tensile and compressive tests, micro-hardness test, microscopic examinations, and XRD analysis were performed. The results showed significant improvement of mechanical properties of Al-SiC nanocomposite in room temperature including 40% of ultimate tensile strength (UTS), 36% of ultimate compressive strength (UCS), and 44% of micro-hardness. Moreover, performing tensile tests at elevated temperatures (up to 270 °C) decreased the tensile strength by about 53%, 46%, and 45% for Al-0 vol% SiC, Al-1.5 vol% SiC, and Al-3 vol% SiC, respectively. This temperature rise also enhanced the elongation by about 11% and 133% for non-reinforced Al and Al-3 vol% SiC, respectively.

  16. Tensile properties of HK31XA-H24 magnesium-alloy sheet under rapid-heating conditions and constant elevated temperatures

    NASA Technical Reports Server (NTRS)

    Gibbs, Thomas W

    1956-01-01

    Specimens of HK31XA-H24 magnesium-alloy sheet from an experimental batch were heated to failure at nominal temperature rates from 0.2 F to 100 F per second under constant-load conditions. Rapid-heating yield and rupture stresses are presented and compared with the yield and ultimate stresses from elevated-temperature tensile stress-strain tests for 1/2-hour exposure. Linear temperature-rate parameters were used to correlate rapid-heating results by constructing master curves which can be used for predicting yield stresses and temperatures and for estimating rupture stresses and temperatures.

  17. Correlation analysis of the variation of weld seam and tensile strength in laser welding of galvanized steel

    NASA Astrophysics Data System (ADS)

    Sinha, Amit Kumar; Kim, Duck Young; Ceglarek, Darek

    2013-10-01

    Many advantages of laser welding technology such as high speed and non-contact welding make the use of the technology more attractive in the automotive industry. Many studies have been conducted to search the optimal welding condition experimentally that ensure the joining quality of laser welding that relies both on welding system configuration and welding parameter specification. Both non-destructive and destructive techniques, for example, ultrasonic inspection and tensile test are widely used in practice for estimating the joining quality. Non-destructive techniques are attractive as a rapid quality testing method despite relatively low accuracy. In this paper, we examine the relationship between the variation of weld seam and tensile shear strength in the laser welding of galvanized steel in a lap joint configuration in order to investigate the potential of the variation of weld seam as a joining quality estimator. From the experimental analysis, we identify a trend in between maximum tensile shear strength and the variation of weld seam that clearly supports the fact that laser welded parts having larger variation in the weld seam usually have lower tensile strength. The discovered relationship leads us to conclude that the variation of weld seam can be used as an indirect non-destructive testing method for estimating the tensile strength of the welded parts.

  18. The role of shear and tensile failure in dynamically triggered landslides

    USGS Publications Warehouse

    Gipprich, T.L.; Snieder, R.K.; Jibson, R.W.; Kimman, W.

    2008-01-01

    Dynamic stresses generated by earthquakes can trigger landslides. Current methods of landslide analysis such as pseudo-static analysis and Newmark's method focus on the effects of earthquake accelerations on the landslide mass to characterize dynamic landslide behaviour. One limitation of these methods is their use Mohr-Coulomb failure criteria, which only accounts for shear failure, but the role of tensile failure is not accounted for. We develop a limit-equilibrium model to investigate the dynamic stresses generated by a given ground motion due to a plane wave and use this model to assess the role of shear and tensile failure in the initiation of slope instability. We do so by incorporating a modified Griffith failure envelope, which combines shear and tensile failure into a single criterion. Tests of dynamic stresses in both homogeneous and layered slopes demonstrate that two modes of failure exist, tensile failure in the uppermost meters of a slope and shear failure at greater depth. Further, we derive equations that express the dynamic stress in the near-surface in the acceleration measured at the surface. These equations are used to approximately define the depth range for each mechanism of failure. The depths at which these failure mechanisms occur suggest that shear and tensile failure might collaborate in generating slope failure. ?? 2007 The Authors Journal compilation ?? 2007 RAS.

  19. Measurement and Analysis of Ultra-Thin Austenitic Stainless Steel Sheet under Biaxial Tensile Loading and In-Plane Reverse Loading

    NASA Astrophysics Data System (ADS)

    Murakoso, Satoko; Kuwabara, Toshihiko

    Biaxial tensile tests of austenitic stainless steel sheet (SUS304) 0.2mm thick have been carried out using cruciform specimens. The specimens are loaded under linear stress paths in a servo-controlled biaxial tensile testing machine. Plastic orthotropy remained coaxial with the principal stresses throughout every experiment. The successive contours of plastic work in biaxial stress space changed their shapes progressively, exemplifying differential work hardening. The geometry of the entire family of the work contours and the directions of plastic strain rates have been precisely measured and compared with those calculated using conventional yield functions. Yld2000-2d [Barlat, F., Brem, J.C., Yoon, J.W., Chung, K., Dick, R.E., Lege, D.J., Pourboghrat, F., Choi, S.H. and Chu, E., International Journal of Plasticity, Vol. 19, (2003), pp. 1297-1319.] with an exponent of 6 was capable of reproducing the general trends of the work contours and the directions of plastic strain rates with good accuracy. Furthermore, in order to quantitatively evaluate the Bauschinger effect of the test material, in-plane tension/compression tests are conducted. It was found that the non-dimensional (σ /σu) - Δɛ /(σu/ E) curves measured during unloading almost fall on a single curve and are not affected by the amount of pre-strain, where σ is the current stress during unloading, σu is the stress immediately before unloading, Δɛ (< 0) is the total strain increment during unloading.

  20. Comparison of polymer-based temporary crown and fixed partial denture materials by diametral tensile strength.

    PubMed

    Ha, Seung-Ryong; Yang, Jae-Ho; Lee, Jai-Bong; Han, Jung-Suk; Kim, Sung-Hun

    2010-03-01

    The purpose of this study was to investigate the diametral tensile strength of polymer-based temporary crown and fixed partial denture (FPD) materials, and the change of the diametral tensile strength with time. One monomethacrylate-based temporary crown and FPD material (Trim) and three dimethacrylate-based ones (Protemp 3 Garant, Temphase, Luxtemp) were investigated. 20 specimens (ø 4 mm × 6 mm) were fabricated and randomly divided into two groups (Group I: Immediately, Group II: 1 hour) according to the measurement time after completion of mixing. Universal Testing Machine was used to load the specimens at a cross-head speed of 0.5 mm/min. The data were analyzed using one-way ANOVA, the multiple comparison Scheffe test and independent sample t test (α = 0.05). Trim showed severe permanent deformation without an obvious fracture during loading at both times. There were statistically significant differences among the dimethacrylate-based materials. The dimethacrylate-based materials presented an increase in strength from 5 minutes to 1 hour and were as follows: Protemp 3 Garant (23.16 - 37.6 MPa), Temphase (22.27 - 28.08 MPa), Luxatemp (14.46 - 20.59 MPa). Protemp 3 Garant showed the highest value. The dimethacrylate-based temporary materials tested were stronger in diametral tensile strength than the monomethacrylate-based one. The diametral tensile strength of the materials investigated increased with time.

  1. Toward predicting tensile strength of pharmaceutical tablets by ultrasound measurement in continuous manufacturing.

    PubMed

    Razavi, Sonia M; Callegari, Gerardo; Drazer, German; Cuitiño, Alberto M

    2016-06-30

    An ultrasound measurement system was employed as a non-destructive method to evaluate its reliability in predicting the tensile strength of tablets and investigate the benefits of incorporating it in a continuous line, manufacturing solid dosage forms. Tablets containing lactose, acetaminophen, and magnesium stearate were manufactured continuously and in batches. The effect of two processing parameters, compaction force and level of shear strain were examined. Young's modulus and tensile strength of tablets were obtained by ultrasound and diametrical mechanical testing, respectively. It was found that as the blend was exposed to increasing levels of shear strain, the speed of sound in the tablets decreased and the tablets became both softer and mechanically weaker. Moreover, the results indicate that two separate tablet material properties (e.g., relative density and Young's modulus) are necessary in order to predict tensile strength. A strategy for hardness prediction is proposed that uses the existing models for Young's modulus and tensile strength of porous materials. Ultrasound testing was found to be very sensitive in differentiating tablets with similar formulation but produced under different processing conditions (e.g., different level of shear strain), thus, providing a fast, and non-destructive method for hardness prediction that could be incorporated to a continuous manufacturing process. Copyright © 2016 Elsevier B.V. All rights reserved.

  2. Comparative evaluation of tensile bond strength of silicone-based denture liners after thermocycling and surface treatment.

    PubMed

    Kaur, Harsimran; Datta, Kusum

    2015-01-01

    To examine, evaluate, and compare the tensile bond strength of two silicone-based liners; one autopolymerizing and one heat cured, when treated with different chemical etchants to improve their adhesion with denture base resin. Hundred and sixty test specimens of heat-cured polymethyl methacrylate (PMMA) were fabricated; out of which 80 specimens were tested for tensile bond strength after bonding it to autopolymerizing resilient liner (Ufigel P) and rest 80 to heat-cured resilient liner (Molloplast B). Each main group was further divided into four subgroups of 20 specimens each, one to act as a control and three were subjected to surface treatment with different chemical etchants namely dichloromethane, MMA monomer, and chloroform. The two silicone-based denture liners were processed between 2 PMMA specimens (10 mm × 10 mm × 40 mm) in the space provided by a spacer of 3 mm, thermocycled (5-55°C) for 500 cycles, and then their tensile strength measurements were done in the universal testing machine. One-way ANOVA technique showed a highly significant difference in the mean tensile bond strength values for all the groups. The Student's t-test computed values of statistics for the compared groups were greater than the critical values both at 5% and at 1% levels. Surface treatment of denture base resin with chemical etchants prior to the application of silicone-based liner (Ufigel P and Molloplast-B) increased the tensile bond strength. The increase was the highest with specimens subjected to 180 s of MMA surface treatment and the lowest with control group specimens.

  3. Room Temperature Tensile Behavior and Damage Accumulation of Hi-Nicalon Reinforced SiC Matrix Composites

    NASA Technical Reports Server (NTRS)

    Morscher, G. N.; Gyekenyesi, J. Z.

    1998-01-01

    Composites consisting of woven Hi-Nicalon fibers, BN interphases, and different SiC matrices were studied in tension at room temperature. Composites with SiC matrices processed by CVI and melt infiltration were compared. Monotonic and load/unload/reload tensile hysteresis experiments were performed. A modal acoustic emission (AE) analyzer was used to monitor damage accumulation during the tensile test. Post test polishing of the tensile gage sections was performed to determine the extent of cracking. The occurrence and location of cracking could easily be determined using modal AE. The loss of modulus could also effectively be determined from the change in the velocity of sound across the sample. Finally, the stresses where cracks appear to intersect the load-bearing fibers correspond with high temperature low cycle fatigue run out stresses for these materials.

  4. Initial Tensile and Residual Forces of Pigmented Elastomeric Ligatures from Various Brands

    NASA Astrophysics Data System (ADS)

    Wichai, Wassana; Anuwongnukroh, Niwat; Dechkunakorn, Surachai; Kaypetch, Rattiporn; Tua-ngam, Peerapong

    2017-11-01

    This study aimed to investigate the initial tensile and residual forces of pigmented elastomeric ligatures (clear, pink, and metallic) from three commercial brands - Brand 1 (USA), Brand 2 (USA), and Brand 3(China). Twelve elastomeric ligatures of each brand and color were evaluated for initial tensile and residual forces after stretching for 28 days at 37°C by a Universal Testing Machine. The results showed that the highest initial tensile force was 14.78 N, 20.71 N, and 15.1 N for the metallic color of Brand-1, pink color of Brand -2, and metallic color of Brand -3, respectively. There were significant (p<0.05) differences in the initial tensile force of each brand, except clear and metallic color of Brand-1 & 3 and pink color of Brand-2 & 3. Similarly, among the pigmented ligatures from each brand, significant (p<0.05) differences were observed in the initial tensile force, except metallic color of Brand-1 & 3. Brand-3 had the highest residual force after 28 days, whereas the loss of force was 80-90% in Brand-1 & 2 and 20-30% in Brand-3. There were also significant (p<0.05) differences in the residual forces in each color and brand, except metallic color of Brand-1. In conclusion, there were significant differences in the initial tensile and residual forces among the three pigmented elastomeric ligatures of the three commercial brands.

  5. Development of Yield and Tensile Strength Design Curves for Alloy 617

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Nancy Lybeck; T. -L. Sham

    2013-10-01

    The U.S. Department of Energy Very High Temperature Reactor Program is acquiring data in preparation for developing an Alloy 617 Code Case for inclusion in the nuclear section of the American Society of Mechanical Engineers (ASME) Boiler and Pressure Vessel (B&PV) Code. A draft code case was previously developed, but effort was suspended before acceptance by ASME. As part of the draft code case effort, a database was compiled of yield and tensile strength data from tests performed in air. Yield strength and tensile strength at temperature are used to set time independent allowable stress for construction materials in B&PVmore » Code, Section III, Subsection NH. The yield and tensile strength data used for the draft code case has been augmented with additional data generated by Idaho National Laboratory and Oak Ridge National Laboratory in the U.S. and CEA in France. The standard ASME Section II procedure for generating yield and tensile strength at temperature is presented, along with alternate methods that accommodate the change in temperature trends seen at high temperatures, resulting in a more consistent design margin over the temperature range of interest.« less

  6. Sample selection, preparation methods, and the apparent tensile properties of silkworm (B. mori) cocoon silk.

    PubMed

    Reed, Emily J; Bianchini, Lindsay L; Viney, Christopher

    2012-06-01

    Reported literature values of the tensile properties of natural silk cover a wide range. While much of this inconsistency is the result of variability that is intrinsic to silk, some is also a consequence of differences in the way that silk is prepared for tensile tests. Here we explore how measured mechanical properties of Bombyx mori cocoon silk are affected by two intrinsic factors (the location from which the silk is collected within the cocoon, and the color of the silk), and two extrinsic factors (the storage conditions prior to testing, and different styles of reeling the fiber). We find that extrinsic and therefore controllable factors can affect the properties more than the intrinsic ones studied. Our results suggest that enhanced inter-laboratory collaborations, that lead to standardized sample collection, handling, and storage protocols prior to mechanical testing, would help to decrease unnecessary (and complicating) variation in reported tensile properties. Copyright © 2011 Wiley Periodicals, Inc.

  7. Strain Rate Sensitivity of Graphite/Polymer Laminate Composites

    NASA Astrophysics Data System (ADS)

    Syed, Izhar H.; Brar, N. S.

    2002-07-01

    Strain rate sensitivities of Graphite/Epoxy and Graphite/Peek laminate composites are investigated by measuring their stress-strain response at strain rates of 0.001/s, 0.1/s, and 400/s. Tension specimens of the composite laminates are fabricated in a dog-bone shape. Stress-strain data at quasi-static rates of 0.001/s and 0.1/s are obtained using a servohydraulic test system. High strain rate data are produced with a Direct Tension Split Hopkinson Bar (DTSHB). A tensile stress pulse is generated in the DTSHB by impacting a stopper flange at the end of the incident bar with an aluminum/polymeric tube launched around the incident bar. The failure (flow) tensile stress of Graphite/Epoxy increases from 240 MPa to 280±10 MPa (ɛ = 0.06) when the strain rate is raised from 0.001/s to 400/s. For Graphite/Peek, failure (flow) tension stress increases from 175 MPa at a strain rate of 0.001/s to 270±20 MPa at a strain rate of 400/s.

  8. 7 CFR 29.6040 - Strength (tensile).

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 2 2011-01-01 2011-01-01 false Strength (tensile). 29.6040 Section 29.6040 Agriculture Regulations of the Department of Agriculture AGRICULTURAL MARKETING SERVICE (Standards... REGULATIONS TOBACCO INSPECTION Standards Definitions § 29.6040 Strength (tensile). The stress a tobacco leaf...

  9. 7 CFR 29.6040 - Strength (tensile).

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 2 2010-01-01 2010-01-01 false Strength (tensile). 29.6040 Section 29.6040 Agriculture Regulations of the Department of Agriculture AGRICULTURAL MARKETING SERVICE (Standards... REGULATIONS TOBACCO INSPECTION Standards Definitions § 29.6040 Strength (tensile). The stress a tobacco leaf...

  10. Effect of oxidation agent on wood biomass in ethylene vinyl acetate conductive polymer: tensile properties, tensile fracture surface and electrical properties

    NASA Astrophysics Data System (ADS)

    Hanif, M. P. M.; Supri, A. G.; Rozyanty, A. R.; Tan, S. J.

    2017-10-01

    The wood fiber (WF) type of Pulverised Wood Filler obtained by combustion process at temperature under 700 °C for 3 hours was characterized and coated with ferric chloride (FeCl3) by ethanol solution. Both carbonized wood fiber (CWF) and carbonized wood fiber-ferric chloride (CWF-FeCl3) were used as filler in ethylene vinyl acetate (EVA) conductive polymer. The filler was coated with FeCl3 to enhance the properties of the CWF to achieve progressive mechanical and electrical properties. The CWF and CWF-FeCl3 loading were varied from 2.5 to 10.0 wt%. EVA/CWF and EVA/CWF-FeCl3 conductive polymer were processed by using Brabender Plasticoder at 160 °C with 50 rpm rotor speed for 10 min. The mechanical properties were investigated by tensile testing and the tensile fractured surface of conductive polymers was analyzed by scanning electron microscopy (SEM) analysis. Then, the electrical conductivity of conductive polymer was determined by four-point probe I-V measurement system. The EVA/CWF-FeCl3 conductive polymer showed greater electrical conductivity and tensile strength but lower elongation at break than EVA/CWF conductive polymer. SEM morphology displayed rougher surface between CWF-FeCl3 and EVA phases compared to EVA/CWF conductive polymer.

  11. Influence of crosshead speed on micro-tensile bond strength of two-step adhesive systems.

    PubMed

    Yamaguchi, Kanako; Miyazaki, Masashi; Takamizawa, Toshiki; Tsubota, Keishi; Rikuta, Akitomo

    2006-05-01

    The purpose of this study was to determine the influence of crosshead speed on the micro-tensile bond strength of two separate adhesive systems to dentin. The systems used were the Clearfil SE Bond (Kuraray Medical) and the Single Bond (3M ESPE) combined with a resin composite Clearfil AP-X (Kuraray Medical). Dentin surfaces of bovine madibular incisors were primed with self-etching primer followed by air blowing for Clearfil SE Bond, or etched with phosphoric acid followed by rinsing with distilled water for Single Bond, and adhesive was applied. The resin composite was then built up in three layers and light activated. After 24 h storage in water, specimens were sectioned and trimmed to a cross-sectional area of 1 mm(2) and subjected to a micro-tensile bond-strength test. Ten samples per test group were tested at crosshead speeds of 0.5, 1.0, 5.0 and 10.0 mm/min. Micro-tensile bond-strength values (in MPa) were calculated from the peak load at failure divided by the specimen surface area. Two-way ANOVA was performed at the 0.05 probability level. The mean dentin bond strength at different crosshead speeds ranged from 34.6 to 37.1MPa for Clearfil SE Bond and from 44.3 to 50.4 MPa for Single Bond. There was no significant difference among the same adhesive systems with the different crosshead speeds tested. The influence of the crosshead speed might be negligible when measuring micro-tensile bond strengths.

  12. Drying time of tray adhesive for adequate tensile bond strength between polyvinylsiloxane impression and tray resin material.

    PubMed

    Yi, Myong-Hee; Shim, Joon-Sung; Lee, Keun-Woo; Chung, Moon-Kyu

    2009-07-01

    Use of custom tray and tray adhesive is clinically recommended for elastomeric impression material. However there is not clear mention of drying time of tray adhesive in achieving appropriate bonding strength of tray material and impression material. This study is to investigate an appropriate drying time of tray adhesives by evaluating tensile bonding strength between two types of polyvinylsiloxane impression materials and resin tray, according to various drying time intervals of tray adhesives, and with different manufacturing company combination of impression material and tray adhesive. Adhesives used in this study were Silfix (Dentsply Caulk, Milford, Del, USA) and VPS Tray Adhesive (3M ESPE, Seefeld, Germany) and impression materials were Aquasil Ultra (monophase regular set, Dentsply Caulk, Milford, Del, USA) and Imprint II Garant (regular body, 3M ESPE, Seefeld, Germany). They were used combinations from the same manufacture and exchanged combinations of the two. The drying time was designed to air dry, 5 minutes, 10 minutes, 15 minutes, 20 minutes, and 25 minutes. Total 240 of test specimens were prepared by auto-polymerizing tray material (Instant Tray Mix, Lang, Wheeling, Il, USA) with 10 specimens in each group. The specimens were placed in the Universal Testing machine (Instron, model 3366, Instron Corp, University avenue, Nowood, MA, USA) to perform the tensile test (cross head speed 5 mm/min). The statistically efficient drying time was evaluated through ANOVA and Scheffe test. All the tests were performed at 95% confidence level. The results revealed that at least 10 minutes is needed for Silfix-Aquasil, and 15 minutes for VPS Tray Adhesive-Imprint II, to attain an appropriate tensile bonding strength. VPS Tray Adhesive-Imprint II had a superior tensile bonding strength when compared to Silfix-Aquasil over 15 minutes. Silfix-Aquasil had a superior bonding strength to VPS Tray Adhesive-Aquasil, and VPS Tray Adhesive-Imprint II had a superior tensile

  13. The Effect of Temperature on Compressive and Tensile Strengths of Commonly Used Luting Cements: An In Vitro Study

    PubMed Central

    Patil, Suneel G; Sajjan, MC Suresh; Patil, Rekha

    2015-01-01

    Background: The luting cements must withstand masticatory and parafunctional stresses in the warm and wet oral environment. Mouth temperature and the temperature of the ingested foods may induce thermal variation and plastic deformation within the cements and might affect the strength properties. The objectives of this study were to evaluate the effect of temperature on the compressive and diametral tensile strengths of two polycarboxylate, a conventional glass ionomer and a resin modified glass ionomer luting cements and, to compare the compressive strength and the diametral tensile strength of the selected luting cements at varying temperatures. Materials and Methods: In this study, standardized specimens were prepared. The temperature of the specimens was regulated prior to testing them using a universal testing machine at a crosshead speed of 1 mm/min. Six specimens each were tested at 23°C, 37°C and 50°C for both the compressive and diametral tensile strengths, for all the luting cements. Results: All the luting cements showed a marginal reduction in their compressive and diametral tensile strengths at raised temperatures. Fuji Plus was strongest in compression, followed by Fuji I > Poly F > Liv Carbo. Fuji Plus had the highest diametral tensile strength values, followed by Poly F = Fuji I = Liv Carbo, at all temperatures. Conclusion: An increase in the temperature caused no significant reduction in the compressive and diametral tensile strengths of the cements evaluated. The compressive strength of the luting cements differed significantly from one another at all temperatures. The diametral tensile strength of resin modified glass ionomers differed considerably from the other cements, whereas there was no significant difference between the other cements, at all the temperatures. PMID:25859100

  14. The effect of temperature on compressive and tensile strengths of commonly used luting cements: an in vitro study.

    PubMed

    Patil, Suneel G; Sajjan, Mc Suresh; Patil, Rekha

    2015-02-01

    The luting cements must withstand masticatory and parafunctional stresses in the warm and wet oral environment. Mouth temperature and the temperature of the ingested foods may induce thermal variation and plastic deformation within the cements and might affect the strength properties. The objectives of this study were to evaluate the effect of temperature on the compressive and diametral tensile strengths of two polycarboxylate, a conventional glass ionomer and a resin modified glass ionomer luting cements and, to compare the compressive strength and the diametral tensile strength of the selected luting cements at varying temperatures. In this study, standardized specimens were prepared. The temperature of the specimens was regulated prior to testing them using a universal testing machine at a crosshead speed of 1 mm/min. Six specimens each were tested at 23°C, 37°C and 50°C for both the compressive and diametral tensile strengths, for all the luting cements. All the luting cements showed a marginal reduction in their compressive and diametral tensile strengths at raised temperatures. Fuji Plus was strongest in compression, followed by Fuji I > Poly F > Liv Carbo. Fuji Plus had the highest diametral tensile strength values, followed by Poly F = Fuji I = Liv Carbo, at all temperatures. An increase in the temperature caused no significant reduction in the compressive and diametral tensile strengths of the cements evaluated. The compressive strength of the luting cements differed significantly from one another at all temperatures. The diametral tensile strength of resin modified glass ionomers differed considerably from the other cements, whereas there was no significant difference between the other cements, at all the temperatures.

  15. Making High-Tensile-Strength Amalgam Components

    NASA Technical Reports Server (NTRS)

    Grugel, Richard

    2008-01-01

    Structural components made of amalgams can be made to have tensile strengths much greater than previously known to be possible. Amalgams, perhaps best known for their use in dental fillings, have several useful attributes, including room-temperature fabrication, corrosion resistance, dimensional stability, and high compressive strength. However, the range of applications of amalgams has been limited by their very small tensile strengths. Now, it has been discovered that the tensile strength of an amalgam depends critically on the sizes and shapes of the particles from which it is made and, consequently, the tensile strength can be greatly increased through suitable choice of the particles. Heretofore, the powder particles used to make amalgams have been, variously, in the form of micron-sized spheroids or flakes. The tensile reinforcement contributed by the spheroids and flakes is minimal because fracture paths simply go around these particles. However, if spheroids or flakes are replaced by strands having greater lengths, then tensile reinforcement can be increased significantly. The feasibility of this concept was shown in an experiment in which electrical copper wires, serving as demonstration substitutes for copper powder particles, were triturated with gallium by use of a mortar and pestle and the resulting amalgam was compressed into a mold. The tensile strength of the amalgam specimen was then measured and found to be greater than 10(exp 4) psi (greater than about 69 MPa). Much remains to be done to optimize the properties of amalgams for various applications through suitable choice of starting constituents and modification of the trituration and molding processes. The choice of wire size and composition are expected to be especially important. Perusal of phase diagrams of metal mixtures could give insight that would enable choices of solid and liquid metal constituents. Finally, whereas heretofore, only binary alloys have been considered for amalgams

  16. A study on tensile deformation at room temperature and 650 °C in the directional solidified Ni-base superalloy GTD-111

    NASA Astrophysics Data System (ADS)

    Pauzi, AA; Ghaffar, MH Abdul; Chang, SY; Ng, GP; Husin, S.

    2017-10-01

    GTD-111 DS generally used for gas turbine blades is a high performance Ni-base superalloy. This alloy, with high volume of γ’ phase, has excellent tensile properties at high temperature. The effect of temperature on the tensile deformation of GTD-111 DS was investigated by using tensile test and microstructure evaluation of the fractured specimens. The tensile behaviour of GTD-111 DS was studied in the room temperature (RT) and 650 °C. From the yield strength results, the yield strength decreases from the average of 702.72 MPa to the average of 645.62 MPa with the increase of temperature from RT to 650 °C. The scanning electron microscope (SEM) results on fractured specimens confirmed that the tensile behaviour affected by deformation of the surface at 650 °C compared to fractured surface at RT. Based on the laboratory testing results, the correlation between tensile deformation of fractured surface and yield strength were discussed.

  17. Tensile Properties of Molybdenum and Tungsten from 2500 to 3700 F

    NASA Technical Reports Server (NTRS)

    Hall, Robert W.; Sikora, Paul F.

    1959-01-01

    Specimens of commercially pure sintered tungsten, arc-cast unalloyed molybdenum, and two arc-cast molybdenum-base alloys (one with 0.5 percent titanium, the other with 0.46 percent titanium and 0.07 percent zirconium) were fabricated from 1/2-inch-diameter rolled or swaged bars. All specimens were evaluated in short-time tensile tests in the as-received condition, and all except the molybdenum-titanium-zirconium alloy were tested after a 30-minute recrystallization anneal at 3800 F in a vacuum of approximately 0.1 micron. Results showed that the tungsten was considerably stronger than either the arc-cast unalloyed molybdenum or the molybdenum-base alloys over the 2500 to 3700 F temperature range. Recrystallization of swaged tungsten at 3800 F considerably reduced its tensile strength at 2500 F. However, above 3100 F, the as-swaged tungsten specimens recrystallized during testing, and had about the same strength as when recrystallized at 3800 F before evaluation. The ductility of molybdenum-base materials was very high at all test temperatures; the ductility of tungsten decreased sharply above about 3120 F.

  18. Tensile and Fatigue Testing and Material Hardening Model Development for 508 LAS Base Metal and 316 SS Similar Metal Weld under In-air and PWR Primary Loop Water Conditions

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Mohanty, Subhasish; Soppet, William; Majumdar, Saurin

    This report provides an update on an assessment of environmentally assisted fatigue for light water reactor components under extended service conditions. This report is a deliverable in September 2015 under the work package for environmentally assisted fatigue under DOE’s Light Water Reactor Sustainability program. In an April 2015 report we presented a baseline mechanistic finite element model of a two-loop pressurized water reactor (PWR) for systemlevel heat transfer analysis and subsequent thermal-mechanical stress analysis and fatigue life estimation under reactor thermal-mechanical cycles. In the present report, we provide tensile and fatigue test data for 508 low-alloy steel (LAS) base metal,more » 508 LAS heat-affected zone metal in 508 LAS–316 stainless steel (SS) dissimilar metal welds, and 316 SS-316 SS similar metal welds. The test was conducted under different conditions such as in air at room temperature, in air at 300 oC, and under PWR primary loop water conditions. Data are provided on materials properties related to time-independent tensile tests and time-dependent cyclic tests, such as elastic modulus, elastic and offset strain yield limit stress, and linear and nonlinear kinematic hardening model parameters. The overall objective of this report is to provide guidance to estimate tensile/fatigue hardening parameters from test data. Also, the material models and parameters reported here can directly be used in commercially available finite element codes for fatigue and ratcheting evaluation of reactor components under in-air and PWR water conditions.« less

  19. Development of an updated tensile neck injury criterion.

    PubMed

    Parr, Jeffrey C; Miller, Michael E; Schubert Kabban, Christine M; Pellettiere, Joseph A; Perry, Chris E

    2014-10-01

    Ejection neck safety remains a concern in military aviation with the growing use of helmet mounted displays (HMDs) worn for entire mission durations. The original USAF tensile neck injury criterion proposed by Carter et al. (4) is updated and an injury protection limit for tensile loading is presented to evaluate escape system and HMD safety. An existent tensile neck injury criterion was updated through the addition of newer post mortem human subject (PMHS) tensile loading and injury data and the application of Survival Analysis to account for censoring in this data. The updated risk function was constructed with a combined human subject (N = 208) and PMHS (N = 22) data set. An updated AIS 3+ tensile neck injury criterion is proposed based upon human and PMHS data. This limit is significantly more conservative than the criterion proposed by Carter in 2000, yielding a 5% risk of AIS 3+ injury at a force of 1136 N as compared to a corresponding force of 1559 N. The inclusion of recent PMHS data into the original tensile neck injury criterion results in an injury protection limit that is significantly more conservative, as recent PMHS data is substantially less censored than the PMHS data included in the earlier criterion. The updated tensile risk function developed in this work is consistent with the tensile risk function published by the Federal Aviation Administration used as the basis for their neck injury criterion for side facing aircraft seats.

  20. Effect of thermomechanical processing on the microstructure and retained austenite stability during in situ tensile testing using synchrotron x-ray diffraction of NbMoAI TRIP steel.

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Pereloma, E.; Zhang, L.; Liss, K.-D.

    2011-06-01

    In this work we compare and contrast the stability of retained austenite during tensile testing of Nb-Mo-Al transformation-induced plasticity steel subjected to different thermomechanical processing schedules. The obtained microstructures were characterised using optical metallography, transmission electron microscopy and X-ray diffraction. The transformation of retained austenite to martensite under tensile loading was observed by in-situ high energy X-ray diffraction at 1ID / APS. It has been shown that the variations in the microstructure of the steel, such as volume fractions of present phases, their morphology and dimensions, play a critical role in the strain-induced transition of retained austenite to martensite.

  1. The tensile effect on crack formation in single crystal silicon irradiated by intense pulsed ion beam

    NASA Astrophysics Data System (ADS)

    Liang, Guoying; Shen, Jie; Zhang, Jie; Zhong, Haowen; Cui, Xiaojun; Yan, Sha; Zhang, Xiaofu; Yu, Xiao; Le, Xiaoyun

    2017-10-01

    Improving antifatigue performance of silicon substrate is very important for the development of semiconductor industry. The cracking behavior of silicon under intense pulsed ion beam irradiation was studied by numerical simulation in order to understand the mechanism of induced surface peeling observed by experimental means. Using molecular dynamics simulation based on Stillinger Weber potential, tensile effect on crack growth and propagation in single crystal silicon was investigated. Simulation results reveal that stress-strain curves of single crystal silicon at a constant strain rate can be divided into three stages, which are not similar to metal stress-strain curves; different tensile load velocities induce difference of single silicon crack formation speed; the layered stress results in crack formation in single crystal silicon. It is concluded that the crack growth and propagation is more sensitive to strain rate, tensile load velocity, stress distribution in single crystal silicon.

  2. 46 CFR 164.023-13 - Production tests and inspections.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... Constant Rate of Traverse tensile testing machine, capable of initial clamp separation of ten inches and a... the acceptance testing values but not less than the performance minimums. (2) Length/weight values must be within 5 percent of the acceptance testing values but not less than the performance minimums...

  3. The tensile and fatigue properties of DIN 1.4914 martensitic stainless steel after 590 MeV proton irradiation

    NASA Astrophysics Data System (ADS)

    Marmy, P.; Victoria, M.

    1992-09-01

    Tensile and low cycle fatigue subsize specimens of DIN 1.4914 martensitic steel (MANET) have been irradiated with 590 MeV protons to doses up to 1 dpa and at temperatures between 363 and 703 K. The helium produced by spallation reactions was measured as 130 appm/dpa. A strong radiation hardening is found, which decreases as the irradiation temperature increases. The tensile elongation is reduced after irradiation, but the fracture mode is always ductile and transgranular. The radition hardening produced at low irradiation temperatures is recovered after annealing at higher temperatures. Continous softening is observed during low cycle fatigue testing. The rate of softening of the irradiated material is stonger than that of the unirradiated material and tends to reach the saturation level of the latter. The irradiation badly affects the fatigue life, particularly in the temperature domain of dynamic strain ageing between 553 and 653 K.

  4. Tensile and impact properties of General Atomics 832864 heat of V-4Cr-4Ti alloy

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Tsai, H.; Nowicki, L.J.; Gazda, J.

    A 1300-kg heat of V-4Cr-4Ti alloy was procured by General Atomics (GA) for the DIII-D radiative divertor program. To determine the mechanical properties of this alloy, tensile and Charpy tests were conducted on specimens prepared from pieces of 4.8-mm-thick as-rolled plates, a major product form for the DIII-D application. The tensile tests were conducted at three temperatures, 26, 280 and 380 C, the last two being the anticipated peak temperatures during DIII-D boronization and postvent bake-out, respectively. Results from these tests show that the tensile and impact properties of the 832864 heat are comparable to those of the other smallermore » V-(4-5)Cr-(4-5)Ti alloy heats previously developed by the US Fusion Materials Program and that scale-up of vanadium alloy production can be successfully achieved as long as reasonable process control is implemented.« less

  5. Wavelet Analysis of Acoustic Emissions during Tensile Test of Carbon Fibre Reinforced Polymer Composites

    NASA Astrophysics Data System (ADS)

    Świt, Grzegorz; Adamczak, Anna; Krampikowska, Aleksandra

    2017-10-01

    The increase of the interest in polymer composites in technology and in people’s everyday lives has been noticed in the recent years. Producing new materials with polymer matrix of particular properties that cannot be achieved by traditional construction materials contributed to high interest in fibre composite materials. However, a wider use of these materials is limited because of the lack of detailed knowledge about their properties and behaviour in various conditions of exposure under load. Mechanical degradation of polymer composites, which is caused by prolonged permanent loads, is connected with the changes of the material structure that are local or that include the whole volume of the element’s body. These changes are in the form of various types of discontinuity, including: deboning, matrix and fibers cracks and delamination. The article presents the example of the application of acoustic emission method based on the analysis of the waves through the use of wavelet analysis for the evaluation of the progress of the destructive processes and the level of the degradation of composite tapes that were subject to tensile testing.

  6. Tensile-stressed microelectromechanical apparatus and micromirrors formed therefrom

    DOEpatents

    Fleming, James G [Albuquerque, NM

    2006-05-16

    A microelectromechanical (MEM) apparatus is disclosed which includes one or more tensile-stressed actuators that are coupled through flexures to a stage on a substrate. The tensile-stressed actuators, which can be formed from tensile-stressed tungsten or silicon nitride, initially raise the stage above the substrate without any applied electrical voltage, and can then be used to control the height or tilt angle of the stage. An electrostatic actuator can also be used in combination with each tensile-stressed actuator. The MEM apparatus has applications for forming piston micromirrors or tiltable micromirrors and independently addressable arrays of such devices.

  7. 46 CFR 164.023-13 - Production tests and inspections.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... Constant Rate of Traverse tensile testing machine, capable of initial clamp separation of ten inches and a... production testing on a lot must meet the following criteria for the lot to be shipped as Coast Guard... the acceptance testing values but not less than the performance minimums. (2) Length/weight values...

  8. Finite element analysis of steel fiber-reinforced concrete (SFRC): validation of experimental tensile capacity of dog-bone specimens

    NASA Astrophysics Data System (ADS)

    Islam, Md. Mashfiqul; Chowdhury, Md. Arman; Sayeed, Md. Abu; Hossain, Elsha Al; Ahmed, Sheikh Saleh; Siddique, Ashfia

    2014-09-01

    Finite element analyses are conducted to model the tensile capacity of steel fiber-reinforced concrete (SFRC). For this purpose dog-bone specimens are casted and tested under direct and uniaxial tension. Two types of aggregates (brick and stone) are used to cast the SFRC and plain concrete. The fiber volume ratio is maintained 1.5 %. Total 8 numbers of dog-bone specimens are made and tested in a 1000-kN capacity digital universal testing machine (UTM). The strain data are gathered employing digital image correlation technique from high-definition images and high-speed video clips. Then, the strain data are synthesized with the load data obtained from the load cell of the UTM. The tensile capacity enhancement is found 182-253 % compared to control specimen to brick SFRC and in case of stone SFRC the enhancement is 157-268 %. Fibers are found to enhance the tensile capacity as well as ductile properties of concrete that ensures to prevent sudden brittle failure. The dog-bone specimens are modeled in the ANSYS 10.0 finite element platform and analyzed to model the tensile capacity of brick and stone SFRC. The SOLID65 element is used to model the SFRC as well as plain concretes by optimizing the Poisson's ratio, modulus of elasticity, tensile strength and stress-strain relationships and also failure pattern as well as failure locations. This research provides information of the tensile capacity enhancement of SFRC made of both brick and stone which will be helpful for the construction industry of Bangladesh to introduce this engineering material in earthquake design. Last of all, the finite element outputs are found to hold good agreement with the experimental tensile capacity which validates the FE modeling.

  9. Recovery of strain-hardening rate in Ni-Si alloys.

    PubMed

    Yang, C L; Zhang, Z J; Cai, T; Zhang, P; Zhang, Z F

    2015-10-21

    In this study, the recovery of strain-hardening rate (RSHR) was discovered for the first time in polycrystalline materials (Ni-Si alloys) that have only dislocation activities during tensile test. Detailed microstructure characterizations show that the activation of dislocations in the secondary slip systems during tensile deformation is the major reason for this RSHR. By taking into account other metals that also exhibit RSHR during tension, a more general mechanism for the RSHR was proposed, i.e. the occurrence of a sharp decrease of dislocation mean free path (Λ) during plastic deformation, caused by either planar defects or linear defects.

  10. Recovery of strain-hardening rate in Ni-Si alloys

    PubMed Central

    Yang, C. L.; Zhang, Z. J.; Cai, T.; Zhang, P.; Zhang, Z. F.

    2015-01-01

    In this study, the recovery of strain-hardening rate (RSHR) was discovered for the first time in polycrystalline materials (Ni-Si alloys) that have only dislocation activities during tensile test. Detailed microstructure characterizations show that the activation of dislocations in the secondary slip systems during tensile deformation is the major reason for this RSHR. By taking into account other metals that also exhibit RSHR during tension, a more general mechanism for the RSHR was proposed, i.e. the occurrence of a sharp decrease of dislocation mean free path (Λ) during plastic deformation, caused by either planar defects or linear defects. PMID:26487419

  11. Recovery of strain-hardening rate in Ni-Si alloys

    NASA Astrophysics Data System (ADS)

    Yang, C. L.; Zhang, Z. J.; Cai, T.; Zhang, P.; Zhang, Z. F.

    2015-10-01

    In this study, the recovery of strain-hardening rate (RSHR) was discovered for the first time in polycrystalline materials (Ni-Si alloys) that have only dislocation activities during tensile test. Detailed microstructure characterizations show that the activation of dislocations in the secondary slip systems during tensile deformation is the major reason for this RSHR. By taking into account other metals that also exhibit RSHR during tension, a more general mechanism for the RSHR was proposed, i.e. the occurrence of a sharp decrease of dislocation mean free path (Λ) during plastic deformation, caused by either planar defects or linear defects.

  12. Measurement error of Young’s modulus considering the gravity and thermal expansion of thin specimens for in situ tensile testing

    NASA Astrophysics Data System (ADS)

    Ma, Zhichao; Zhao, Hongwei; Ren, Luquan

    2016-06-01

    Most miniature in situ tensile devices compatible with scanning/transmission electron microscopes or optical microscopes adopt a horizontal layout. In order to analyze and calculate the measurement error of the tensile Young’s modulus, the effects of gravity and temperature changes, which would respectively lead to and intensify the bending deformation of thin specimens, are considered as influencing factors. On the basis of a decomposition method of static indeterminacy, equations of simplified deflection curves are obtained and, accordingly, the actual gage length is confirmed. By comparing the effects of uniaxial tensile load on the change of the deflection curve with gravity, the relation between the actual and directly measured tensile Young’s modulus is obtained. Furthermore, the quantitative effects of ideal gage length l o, temperature change ΔT and the density ρ of the specimen on the modulus difference and modulus ratio are calculated. Specimens with larger l o and ρ present more obvious measurement errors for Young’s modulus, but the effect of ΔT is not significant. The calculation method of Young’s modulus is particularly suitable for thin specimens.

  13. Determination of Temperature- Dependent Mechanical Properties of Carbon Composites Under Tensile and Flexural Loading

    NASA Astrophysics Data System (ADS)

    Chripunow, Andre; Kubisch, Aline; Ruder, Matthias; Forster, Andreas; Korber, Hannes

    2014-06-01

    The presented test setup utilises a custom-built furnace realising test temperatures of up to 500°C. In order to ensure always optimal test conditions the temperature cell can be exchanged depending on the mechanical tests and specimen sizes. Cells for tensile and flexural loadings had been developed. With the latter one it is possible to perform three-point-bending tests, interlaminar-shear-strength tests as well as tests to determine the interlaminar fracture toughness. In this work the effect of fibre orientation on the mechanical properties of CFRP prepreg material under tensile and flexural loads at elevated temperatures was studied. Especially the matrix dominated layups showed a rather early decay of the mechanical properties even at temperatures quite lower than Tg. An analytical model has been used to describe the temperature-dependent properties. The model shows good agreement concerning the strength whereas the proper prediction of the moduli was only possible for the matrix dominated layups.

  14. Effect of Load Rate on Ultimate Tensile Strength of Ceramic Matrix Composites at Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Gyekenyesi, John P.

    2001-01-01

    The strengths of three continuous fiber-reinforced ceramic composites, including SiC/CAS-II, SiC/MAS-5 and SiC/SiC, were determined as a function of test rate in air at 1100 to 1200 C. All three composite materials exhibited a strong dependency of strength on test rate, similar to the behavior observed in many advanced monolithic ceramics at elevated temperatures. The application of the preloading technique as well as the prediction of life from one loading configuration (constant stress-rate) to another (constant stress loading) suggested that the overall macroscopic failure mechanism of the composites would be the one governed by a power-law type of damage evolution/accumulation, analogous to slow crack growth commonly observed in advanced monolithic ceramics. It was further found that constant stress-rate testing could be used as an alternative to life prediction test methodology even for composite materials, at least for short range of lifetimes and when ultimate strength is used as the failure criterion.

  15. Statistical behavior of the tensile property of heated cotton fiber

    USDA-ARS?s Scientific Manuscript database

    The temperature dependence of the tensile property of single cotton fiber was studied in the range of 160-300°C using Favimat test, and its statistical behavior was interpreted in terms of structural changes. The tenacity of control cotton fiber was well described by the single Weibull distribution,...

  16. Length scale of the dendritic microstructure affecting tensile properties of Al-(Ag)-(Cu) alloys

    NASA Astrophysics Data System (ADS)

    Duarte, Roberto N.; Faria, Jonas D.; Brito, Crystopher; Veríssimo, Nathalia C.; Cheung, Noé; Garcia, Amauri

    2016-12-01

    The dependence of tensile properties on the length scale of the dendritic morphology of Al-Cu, Al-Ag and Al-Ag-Cu alloys is experimentally investigated. These alloys were directionally solidified (DS) under a wide range of cooling rates (Ṫ), permitting extensive microstructural scales to be examined. Experimental growth laws are proposed relating the primary dendritic arm spacing, λ1 to Ṫ and tensile properties to λ1. It is shown that the most significant effect of the scale of λ1 on the tensile properties is that of the ternary alloy, which is attributed to the more homogeneous distribution of the eutectic mixture for smaller λ1 and by the combined reinforcement roles of the intermetallics present in the ternary eutectic: Al2Cu and nonequilibrium Ag3Al.

  17. Tensile and compressive failure modes of laminated composites loaded by fatigue with different mean stress

    NASA Technical Reports Server (NTRS)

    Rotem, Assa

    1990-01-01

    Laminated composite materials tend to fail differently under tensile or compressive load. Under tension, the material accumulates cracks and fiber fractures, while under compression, the material delaminates and buckles. Tensile-compressive fatigue may cause either of these failure modes depending on the specific damage occurring in the laminate. This damage depends on the stress ratio of the fatigue loading. Analysis of the fatigue behavior of the composite laminate under tension-tension, compression-compression, and tension-compression had led to the development of a fatigue envelope presentation of the failure behavior. This envelope indicates the specific failure mode for any stress ratio and number of loading cycles. The construction of the fatigue envelope is based on the applied stress-cycles to failure (S-N) curves of both tensile-tensile and compressive-compressive fatigue. Test results are presented to verify the theoretical analysis.

  18. Effect of Steam Autoclaving on the Tensile Strength of Resin Cements Used for Bonding Two-Piece Zirconia Abutments.

    PubMed

    Fadanelli, Marcos Alexandre; Amaral, Flávia Lucisano Botelho do; Basting, Roberta Tarkany; Turssi, Cecilia Pedroso; Sotto-Maior, Bruno Salles; França, Fabiana Mantovani Gomes

    2017-04-01

    The purpose of this study was to evaluate the effects of steam autoclave sterilization on the tensile strength of two types of resin cements used to bond customized CAD/CAM zirconia abutments onto titanium bases. Forty sets of zirconia abutments cemented to screwed titanium bases of implants analogs were divided into 4 groups (n = 10). Two groups were treated with a conventional chemically activated resin cement (ML, Multilink Ivoclar Vivadent) and the other two groups with a self-adhesive dual resin cement (RelyX U200, 3M ESPE). One group from each cement was submitted to steam autoclaving. The autoclave sterilization cycle was performed after 72 hours of cementation for 15 minutes at 121°C and 2.1 Kgf/cm 2 . The samples were subjected to tensile strength testing in a universal testing machine (200 Kgf, 0.5 mm/min), from which the means and standard deviations were obtained in Newtons. Results showed (via ANOVA and Tukey's test; α = 0.05) that in the absence of steam autoclaving, no difference was observed in tensile strength between the cements tested: ML: 344.87 (93.79) and U200: 280 (92.42) (P = .314). Steam autoclaving, however, significantly increased tensile strength for the ML: 465.42 (87.87) compared to U200: 289.10 (49.02) (P < .001). Despite the significant increase in the ML samples (P = .013), autoclaving did not affect the tensile strength of the U200 samples (P > 0.05). The authors concluded that steam autoclaving increases the mean tensile strength of the chemically activated cement compared to the dual-cure self-adhesive cement. The performance of both cements evaluated was similar if the sterilization step was disconsidered.

  19. Study on the Tensile Creep Behavior of Carbon Nanotubes-Reinforced Sn-58Bi Solder Joints

    NASA Astrophysics Data System (ADS)

    Yang, Li; Liu, Haixiang; Zhang, Yaocheng

    2018-01-01

    The microstructure and tensile creep behavior of plain Sn-58Bi solder and carbon nanotubes (CNTs)-reinforced composite solder joints were investigated. The stress exponent n under different stresses and the creep activation energy Q c under different temperatures of solder joints were obtained by an empirical equation. The results reveal that the microstructure of the composite solder joint is refined and the tensile creep resistance is improved by CNTs. The improvement of creep behavior is due to the microstructural change of the composite solder joints, since the CNTs could provide more obstacles for dislocation pile-up, which enhances the values of the stress exponent and the creep activation energy. The steady-state tensile creep rates of plain solder and composite solder joints are increased with increasing temperature and applied stress. The tensile creep constitutive equations of plain solder and composite solder joints are written as \\dot{ɛ }_{s1} = 14.94( {σ /G} )^{3.7} \\exp ( { - 81444/RT} ) and \\dot{ɛ }_{s2} = 2.5( {σ /G} )^{4.38} \\exp ( { - 101582/RT} ) , respectively. The tensile creep mechanism of the solder joints is the effects of lattice diffusion determined by dislocation climbing.

  20. Effects of High and Low Temperature on the Tensile Strength of Glass Fiber Reinforced Polymer Composites

    NASA Astrophysics Data System (ADS)

    Kumarasamy, S.; Shukur Zainol Abidin, M.; Abu Bakar, M. N.; Nazida, M. S.; Mustafa, Z.; Anjang, A.

    2018-05-01

    In this paper, the tensile performance of glass fiber reinforced polymer (GFRP) composites at high and low temperature was experimentally evaluated. GFRP laminates were manufactured using the wet hand lay-up assisted by vacuum bag, which has resulted in average fibre volume fraction of 0.45. Using simultaneous heating/cooling and loading, glass fiber epoxy and polyester laminates were evaluated for their mechanical performance in static tensile loading. In the elevated temperature environment test, the tension mechanical properties; stress and modulus were reduced with increasing temperature from 25°C to 80°C. Results of low temperature environment from room temperature to a minimum temperature of -20°C, indicated that there is no considerable effect on the tensile strength, however a slight decrease of tensile modulus were observed on the GFRP laminates. The results obtained from the research highlight the structural survivability on tensile properties at low and high temperature of the GFRP laminates.

  1. Influence of Accumulative Roll Bonding on the Texture and Tensile Properties of an AZ31 Magnesium Alloy Sheets

    PubMed Central

    Džugan, Ján; Németh, Gergely; Lukáč, Pavel; Bohlen, Jan

    2018-01-01

    Deformation behaviour of rolled AZ31 sheets that were subjected to the accumulative roll bonding was investigated. Substantially refined microstructure of samples was achieved after the first and second pass through the rolling mill. Sheets texture was investigated using an X-ray diffractometer. Samples for tensile tests were cut either parallel or perpendicular to the rolling direction. Tensile tests were performed at temperatures ranging from room temperature up to 300 °C. Tensile plastic anisotropy, different from the anisotropy observed in AZ31 sheets by other authors, was observed. This anisotropy decreases with an increasing number of rolling passes and increasing deformation temperature. Grain refinement and texture are the crucial factors influencing the deformation behaviour. PMID:29303975

  2. Preparation of poly (arylene ether nitrile)/NzdFeB composite film with excellent thermal properties and tensile strength

    NASA Astrophysics Data System (ADS)

    Pan, Hai; Xu, Mingzhen; Liu, Xiaobo

    2017-12-01

    PEN/NdFeB composite films were prepared by the solution casting method. The thermal properties, fracture morphology and tensile strength of the composite films were tested by DSC, TGA, SEM and electromechanical universal testing machine, respectively. The results reveal that the composite film has good thermal properties and tensile strength. Glass-transition temperature and decomposition temperatures at weight loss of 5% ot the composite films retain at 166±1 C and 462±4 C, respectively. The composite film with 5 wt.% NdFeB has the best tensile strength value for 100.5 MPa. In addition, it was found that the NdFeB filler was well dispersed in PEN matrix by SEM analysis.

  3. Tailoring Morphology and Size of Microstructure and Tensile Properties of Sn-5.5 wt.%Sb-1 wt.%(Cu,Ag) Solder Alloys

    NASA Astrophysics Data System (ADS)

    Dias, Marcelino; Costa, Thiago A.; Soares, Thiago; Silva, Bismarck L.; Cheung, Noé; Spinelli, José E.; Garcia, Amauri

    2018-02-01

    Transient directional solidification experiments, and further optical and scanning electron microscopy analyses and tensile tests, allowed the dependence of tensile properties on the micromorphology and length scale of the dendritic/cellular matrix of ternary Sn-5.5Sb-1Ag and Sn-5.5Sb-1Cu alloys to be determined. Extensive ranges of cooling rates were obtained, which permitted specific values of cooling rate for each sample examined along the length of the casting to be attributed. Very broad microstructural length scales were revealed as well as the presence of either cells or dendrites for the Ag-containing alloy. Hereafter, microstructural spacing values such as the cellular spacing, λ c, and the primary dendritic spacing, λ 1, may be correlated with thermal solidification parameters, that is, the cooling rate and the growth rate. While, for the Cu-containing Sn-Sb alloy, the β-Sn matrix is characterized only by the presence of dendritic arrangements, the Ag-containing Sn-Sb alloy is shown to have high-velocity β-Sn cells associated with high cooling rate regions, i.e., positions closer to the bottom of the alloy casting, with the remaining positions being characterized by a complex growth of β-Sn dendrites. Minor additions of Cu and Ag increase both the yield and ultimate tensile strengths when compared with the corresponding values of the binary Sn-5.5Sb alloy, with a small reduction in ductility. This has been attributed to the homogeneous distribution of the Ag3Sn and Cu6Sn5 intermetallic particles related to smaller λ 1 characterizing the dendritic zones of the ternary Sn-Sb-(Cu,Ag) alloys. In addition, the Ag-modified Sn-Sb alloy exhibited an initial wetting angle consistent with that characterizing the binary Sn-5.5Sb alloy.

  4. Diametral tensile strength of two dental composites when immersed in ethanol, distilled water and artificial saliva.

    PubMed

    Rehman, Abdur; Amin, Faiza; Abbas, Muhammad

    2014-11-01

    To examine the effect of distilled water, artificial saliva and ethanol on the tensile strength of direct tooth-coloured restorative material. The study was conducted at Dr. Ishrat ul Ebad Khan Institute of Oral Health Sciences, Dow University of Health Sciences (DUHS), Karachi, from April 2011 to September 2012. The testing was performed at the Pakistan Council of Scientific and Industrial Research (PCSIR) laboratories. Two composite resins Filtek Z250 and Spectrum TPH were tested. Specimens (13 mm x 3 mm x 2 mm) of each material were prepared in the stainless steel mould according to the manufacturers' instructions and distributed into 3 equal groups: one immersed in distilled water, the other in artificial saliva, and the last one in ethanol for 24 hours. Tensile strength was determined after 24 hours in universal Instron Testing Machine. There were 72 specimens in all; 36 (50%) each for Filtek Z250 and Spectrum TPH. The three sub-groups in each case had 12 (33.3%) specimens. For the Filtek Z250, there was no statistically significant difference between immersion in distilled water and artificial saliva, but the ethanol group presented lower tensile strength (p<0.05). For the Spectrum TPH, samples immersed in ethanol and artificial saliva presented lower tensile strength compared to distilled water (p<0.05). The tested composite resins were affected by the immersion media and adversely affected the mechanical properties of composite resins.

  5. Impact of Gluma Desensitizer on the tensile strength of zirconia crowns bonded to dentin: an in vitro study.

    PubMed

    Stawarczyk, Bogna; Hartmann, Leonie; Hartmann, Rahel; Roos, Malgorzata; Ender, Andreas; Ozcan, Mutlu; Sailer, Irena; Hämmerle, Christoph H F

    2012-02-01

    This study tested the impact of Gluma Desensitizer on the tensile strength of zirconia crowns bonded to dentin. Human teeth were prepared and randomly divided into six groups (N = 144, n = 24 per group). For each tooth, a zirconia crown was manufactured. The zirconia crowns were cemented with: (1) Panavia21 (PAN), (2) Panavia21 combined with Gluma Desensitizer (PAN-G), (3) RelyX Unicem (RXU), (4) RelyX Unicem combined with Gluma Desensitizer (RXU-G), (5) G-Cem (GCM) and (6) G-Cem combined with Gluma Desensitizer (GCM-G). The initial tensile strength was measured in half (n = 12) of each group and the other half (n = 12) subjected to a chewing machine (1.2 Mio, 49 N, 5°C/50°C). The cemented crowns were pulled in a Universal Testing Machine (1 mm/min, Zwick Z010) until failure occurred and tensile strength was calculated. Data were analyzed with one-way and two-way ANOVA followed by a post hoc Scheffé test, t test and Kaplan-Meier analysis with a Breslow-Gehan analysis test (α = 0.05). After the chewing simulation, the self-adhesive resin cements combined with Gluma Desensitizer showed significantly higher tensile strength (RXU-G, 12.8 ± 4.3 MPa; GCM-G, 13.4 ± 6.2 MPa) than PAN (7.3 ± 1.7 MPa) and PAN-G (0.9 ± 0.6). Within the groups, PAN, PAN-G and RXU resulted in significantly lower values when compared to the initial tensile strength; the values of all other test groups were stable. In this study, self-adhesive resin cements combined with Gluma Desensitizer reached better long-term stability compared to PAN and PAN-G after chewing simulation.

  6. Effect of zirconium oxide nanoparticles addition on the optical and tensile properties of polymethyl methacrylate denture base material.

    PubMed

    Gad, Mohammed M; Abualsaud, Reem; Rahoma, Ahmed; Al-Thobity, Ahmad M; Al-Abidi, Khalid S; Akhtar, Sultan

    2018-01-01

    Polymethyl methacrylate (PMMA) is widely used for the fabrication of removable prostheses. Recently, zirconium oxide nanoparticles (nano-ZrO 2 ) have been added to improve some properties of PMMA, but their effect on the optical properties and tensile strength are neglected. The aim of this study was to investigate the effect of nano-ZrO 2 addition on the translucency and tensile strength of the PMMA denture base material. Eighty specimens (40 dumbbell-shaped and 40 discs) were prepared out of heat-polymerized acrylic resin and divided into four groups per test (n=10). The control group for each test included unreinforced acrylic, while the test groups were reinforced with 2.5, 5, and 7.5 wt% nano-ZrO 2 . Acrylic resin was mixed according to manufacturer's instructions, packed, and processed by conventional method. After polymerization, all specimens were finished, polished, and stored in distilled water at 37°C for 48±2 hours. Tensile strength (MPa) was evaluated using the universal testing machine while the specimens' translucency was examined using a spectrophotometer. Statistical analysis was carried out by SPSS using the paired sample t -test ( p ≤0.05). A scanning electron microscope was used to analyze the morphological changes and topography of the fractured surfaces. This study showed that the mean tensile strength of the PMMA in the test groups of 2.5%NZ, 5%NZ, and 7.5%NZ was significantly higher than the control group. The tensile strength increased significantly after nano-ZrO 2 addition, and the maximum increase seen was in the 7.5%NZ group. The translucency values of the experimental groups were significantly lower than those of the control group. Within the reinforced groups, the 2.5%NZ group had significantly higher translucency values when compared to the 5%NZ and 7.5%NZ groups. The addition of nano-ZrO 2 increased the tensile strength of the denture base acrylic. The increase was directly proportional to the nano-ZrO 2 concentration. The

  7. Ultra High Strain Rate Nanoindentation Testing.

    PubMed

    Sudharshan Phani, Pardhasaradhi; Oliver, Warren Carl

    2017-06-17

    Strain rate dependence of indentation hardness has been widely used to study time-dependent plasticity. However, the currently available techniques limit the range of strain rates that can be achieved during indentation testing. Recent advances in electronics have enabled nanomechanical measurements with very low noise levels (sub nanometer) at fast time constants (20 µs) and high data acquisition rates (100 KHz). These capabilities open the doors for a wide range of ultra-fast nanomechanical testing, for instance, indentation testing at very high strain rates. With an accurate dynamic model and an instrument with fast time constants, step load tests can be performed which enable access to indentation strain rates approaching ballistic levels (i.e., 4000 1/s). A novel indentation based testing technique involving a combination of step load and constant load and hold tests that enables measurement of strain rate dependence of hardness spanning over seven orders of magnitude in strain rate is presented. A simple analysis is used to calculate the equivalent uniaxial response from indentation data and compared to the conventional uniaxial data for commercial purity aluminum. Excellent agreement is found between the indentation and uniaxial data over several orders of magnitude of strain rate.

  8. Tensile properties and flow behavior analysis of modified 9Cr-1Mo steel clad tube material

    NASA Astrophysics Data System (ADS)

    Singh, Kanwarjeet; Latha, S.; Nandagopal, M.; Mathew, M. D.; Laha, K.; Jayakumar, T.

    2014-11-01

    The tensile properties and flow behavior of modified 9Cr-1Mo steel clad tube have been investigated in the framework of various constitutive equations for a wide range of temperatures (300-923 K) and strain rates (3 × 10-3 s-1, 3 × 10-4 s-1 and 3 × 10-5 s-1). The tensile flow behavior of modified 9Cr-1Mo steel clad tube was most accurately described by Voce equation. The variation of instantaneous work hardening rate (θ = dσ/dε) and σθ with stress (σ) indicated two stage behavior characterized by rapid decrease at low stresses (transient stage) followed by a gradual decrease in high stresses (Stage III). The variation of work hardening parameters and work hardening rate in terms of θ vs. σ and σθ vs. σ with temperature exhibited three distinct regimes. Rapid decrease in flow stress and work hardening parameters and rapid shift of θ vs. σ and σθ vs. σ towards low stresses with increase in temperature indicated dynamic recovery at high temperatures. Tensile properties of the material have been best predicted from Voce equation.

  9. Nanoindentation cannot accurately predict the tensile strength of graphene or other 2D materials

    NASA Astrophysics Data System (ADS)

    Han, Jihoon; Pugno, Nicola M.; Ryu, Seunghwa

    2015-09-01

    Due to the difficulty of performing uniaxial tensile testing, the strengths of graphene and its grain boundaries have been measured in experiments by nanoindentation testing. From a series of molecular dynamics simulations, we find that the strength measured in uniaxial simulation and the strength estimated from the nanoindentation fracture force can differ significantly. Fracture in tensile loading occurs simultaneously with the onset of crack nucleation near 5-7 defects, while the graphene sheets often sustain the indentation loads after the crack initiation because the sharply concentrated stress near the tip does not give rise to enough driving force for further crack propagation. Due to the concentrated stress, strength estimation is sensitive to the indenter tip position along the grain boundaries. Also, it approaches the strength of pristine graphene if the tip is located slightly away from the grain boundary line. Our findings reveal the limitations of nanoindentation testing in quantifying the strength of graphene, and show that the loading-mode-specific failure mechanism must be taken into account in designing reliable devices from graphene and other technologically important 2D materials.Due to the difficulty of performing uniaxial tensile testing, the strengths of graphene and its grain boundaries have been measured in experiments by nanoindentation testing. From a series of molecular dynamics simulations, we find that the strength measured in uniaxial simulation and the strength estimated from the nanoindentation fracture force can differ significantly. Fracture in tensile loading occurs simultaneously with the onset of crack nucleation near 5-7 defects, while the graphene sheets often sustain the indentation loads after the crack initiation because the sharply concentrated stress near the tip does not give rise to enough driving force for further crack propagation. Due to the concentrated stress, strength estimation is sensitive to the indenter tip

  10. Speckle-interferometric measurement system of 3D deformation to obtain thickness changes of thin specimen under tensile loads

    NASA Astrophysics Data System (ADS)

    Kowarsch, Robert; Zhang, Jiajun; Sguazzo, Carmen; Hartmann, Stefan; Rembe, Christian

    2017-06-01

    The analysis of materials and geometries in tensile tests and the extraction of mechanic parameters is an important field in solid mechanics. Especially the measurement of thickness changes is important to obtain accurate strain information of specimens under tensile loads. Current optical measurement methods comprising 3D digital image correlation enable thickness-change measurement only with nm-resolution. We present a phase-shifting electronic speckle-pattern interferometer in combination with speckle-correlation technique to measure the 3D deformation. The phase-shift for the interferometer is introduced by fast wavelength tuning of a visible diode laser by injection current. In a post-processing step, both measurements can be combined to reconstruct the 3D deformation. In this contribution, results of a 3Ddeformation measurement for a polymer membrane are presented. These measurements show sufficient resolution for the detection of 3D deformations of thin specimen in tensile test. In future work we address the thickness changes of thin specimen under tensile loads.

  11. Cell division plane orientation based on tensile stress in Arabidopsis thaliana

    PubMed Central

    Louveaux, Marion; Julien, Jean-Daniel; Mirabet, Vincent; Boudaoud, Arezki; Hamant, Olivier

    2016-01-01

    Cell geometry has long been proposed to play a key role in the orientation of symmetric cell division planes. In particular, the recently proposed Besson–Dumais rule generalizes Errera’s rule and predicts that cells divide along one of the local minima of plane area. However, this rule has been tested only on tissues with rather local spherical shape and homogeneous growth. Here, we tested the application of the Besson–Dumais rule to the divisions occurring in the Arabidopsis shoot apex, which contains domains with anisotropic curvature and differential growth. We found that the Besson–Dumais rule works well in the central part of the apex, but fails to account for cell division planes in the saddle-shaped boundary region. Because curvature anisotropy and differential growth prescribe directional tensile stress in that region, we tested the putative contribution of anisotropic stress fields to cell division plane orientation at the shoot apex. To do so, we compared two division rules: geometrical (new plane along the shortest path) and mechanical (new plane along maximal tension). The mechanical division rule reproduced the enrichment of long planes observed in the boundary region. Experimental perturbation of mechanical stress pattern further supported a contribution of anisotropic tensile stress in division plane orientation. Importantly, simulations of tissues growing in an isotropic stress field, and dividing along maximal tension, provided division plane distributions comparable to those obtained with the geometrical rule. We thus propose that division plane orientation by tensile stress offers a general rule for symmetric cell division in plants. PMID:27436908

  12. Tensile and compressive stress-strain behavior of heat treated boron-aluminum

    NASA Technical Reports Server (NTRS)

    Kennedy, J. M.; Tenney, D. R.; Herakovich, C. T.

    1978-01-01

    An experimental study was conducted to assess the effects of heat treatment and cyclic mechanical loading on the tensile and compressive stress-strain behavior of six boron-aluminum composites having different laminate orientations and being subjected to different heat treatments. The heat treatments were as-fabricated, T6, and T6N consisting of T6 treatment followed by cryogenic quench in liquid nitrogen prior to testing. All laminates were tested in monotonic and cyclic compression, while the tensile-test data are taken from the literature for comparison purposes. It is shown that the linear elastic range of the T6- and T6N-condition specimens is larger than that of the as-fabricated specimens, and that cyclic loading in tension or compression strain hardens the specimens and extends the linear elastic range. For laminates containing 0-deg plies, the stress-strain behavior upon unloading is found to be nonlinear, whereas the other laminates exhibit a linear behavior upon unloading. Specimens in the T6 and T6N conditions show higher strain hardening than the as-fabricated specimens.

  13. Tensile Properties and Fracture Behavior of Aluminum Alloy Foam Fabricated from Die Castings without Using Blowing Agent by Friction Stir Processing Route

    PubMed Central

    Hangai, Yoshihiko; Kamada, Hiroto; Utsunomiya, Takao; Kitahara, Soichiro; Kuwazuru, Osamu; Yoshikawa, Nobuhiro

    2014-01-01

    Al foam has been used in a wide range of applications owing to its light weight, high energy absorption and high sound insulation. One of the promising processes for fabricating Al foam involves the use of a foamable precursor. In this study, ADC12 Al foams with porosities of 67%–78% were fabricated from Al alloy die castings without using a blowing agent by the friction stir processing route. The pore structure and tensile properties of the ADC12 foams were investigated and compared with those of commercially available ALPORAS. From X-ray computed tomography (X-ray CT) observations of the pore structure of ADC12 foams, it was found that they have smaller pores with a narrower distribution than those in ALPORAS. Tensile tests on the ADC12 foams indicated that as their porosity increased, the tensile strength and tensile strain decreased, with strong relation between the porosity, tensile strength, and tensile strain. ADC12 foams exhibited brittle fracture, whereas ALPORAS exhibited ductile fracture, which is due to the nature of the Al alloy used as the base material of the foams. By image-based finite element (FE) analysis using X-ray CT images corresponding to the tensile tests on ADC12 foams, it was shown that the fracture path of ADC12 foams observed in tensile tests and the regions of high stress obtained from FE analysis correspond to each other. Therefore, it is considered that the fracture behavior of ADC12 foams in relation to their pore structure distribution can be investigated by image-based FE analysis. PMID:28788573

  14. Tensile Properties and Fracture Behavior of Aluminum Alloy Foam Fabricated from Die Castings without Using Blowing Agent by Friction Stir Processing Route.

    PubMed

    Hangai, Yoshihiko; Kamada, Hiroto; Utsunomiya, Takao; Kitahara, Soichiro; Kuwazuru, Osamu; Yoshikawa, Nobuhiro

    2014-03-21

    Al foam has been used in a wide range of applications owing to its light weight, high energy absorption and high sound insulation. One of the promising processes for fabricating Al foam involves the use of a foamable precursor. In this study, ADC12 Al foams with porosities of 67%-78% were fabricated from Al alloy die castings without using a blowing agent by the friction stir processing route. The pore structure and tensile properties of the ADC12 foams were investigated and compared with those of commercially available ALPORAS. From X-ray computed tomography (X-ray CT) observations of the pore structure of ADC12 foams, it was found that they have smaller pores with a narrower distribution than those in ALPORAS. Tensile tests on the ADC12 foams indicated that as their porosity increased, the tensile strength and tensile strain decreased, with strong relation between the porosity, tensile strength, and tensile strain. ADC12 foams exhibited brittle fracture, whereas ALPORAS exhibited ductile fracture, which is due to the nature of the Al alloy used as the base material of the foams. By image-based finite element (FE) analysis using X-ray CT images corresponding to the tensile tests on ADC12 foams, it was shown that the fracture path of ADC12 foams observed in tensile tests and the regions of high stress obtained from FE analysis correspond to each other. Therefore, it is considered that the fracture behavior of ADC12 foams in relation to their pore structure distribution can be investigated by image-based FE analysis.

  15. Tensile properties of textile composites

    NASA Technical Reports Server (NTRS)

    Avva, V. Sarma; Sadler, Robert L.; Lyon, Malcolm

    1992-01-01

    The importance of textile composite materials in aerospace structural applications has been gaining momentum in recent years. With a view to better understand the suitability of these materials in aerospace applications, an experimental program was undertaken to assess the mechanical properties of these materials. Specifically, the braided textile preforms were infiltrated with suitable polymeric matrices leading to the fabrication of composite test coupons. Evaluation of the tensile properties and the analyses of the results in the form of strength moduli, Poisson's ratio, etc., for the braided composites are presented. Based on our past experience with the textile coupons, the fabrication techniques have been modified (by incorporating glass microballoons in the matrix and/or by stabilizing the braid angle along the length of the specimen with axial fibers) to achieve enhanced mechanical properties of the textile composites. This paper outlines the preliminary experimental results obtained from testing these composites.

  16. Tensile Properties of the Deep Transverse Metatarsal Ligament in Hallux Valgus: A CONSORT-Compliant Article.

    PubMed

    Abdalbary, Sahar Ahmed; Elshaarawy, Ehab A A; Khalid, Bahaa E A

    2016-02-01

    The deep transverse metatarsal ligament (DTML) connects the neighboring2 metatarsal heads and is one of the stabilizers connecting the lateral sesamoid and second metatarsal head. In this study, we aimed to determine the tensile properties of the DTML in normal specimens and to compare these results with hallux valgus specimens. We hypothesized that the tensile properties of the DTML would be different between the 2 groups of specimens.The DTML in the first interspace was dissected from 12 fresh frozen human cadaveric specimens. Six cadavers had bilateral hallux valgus and the other 6 cadavers had normal feet. The initial length (L0) and cross-sectional area (A0) of the DTML were measured using a digital caliper, and tensile tests with load failure were performed using a material testing machine.There were significant between-groups differences in the initial length (L0) P = 0.009 and cross-sectional area (A0) of the DTML P = 0.007. There were also significant between-groups differences for maximum force (N) P = 0.004, maximum distance (mm) P = 0.005, maximum stress (N/mm) P = 0.003, and maximum strain (%) P = 0.006.The DTML is an anatomical structure for which the tensile properties differ in hallux valgus.

  17. 26 CFR 1.1274-4 - Test rate.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 26 Internal Revenue 11 2011-04-01 2011-04-01 false Test rate. 1.1274-4 Section 1.1274-4 Internal... TAXES (CONTINUED) Special Rules for Determining Capital Gains and Losses § 1.1274-4 Test rate. (a) Determination of test rate of interest—(1) In general—(i) Test rate is the 3-month rate. Except as provided in...

  18. 26 CFR 1.1274-4 - Test rate.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 26 Internal Revenue 11 2014-04-01 2014-04-01 false Test rate. 1.1274-4 Section 1.1274-4 Internal... TAXES (CONTINUED) Special Rules for Determining Capital Gains and Losses § 1.1274-4 Test rate. (a) Determination of test rate of interest—(1) In general—(i) Test rate is the 3-month rate. Except as provided in...

  19. 26 CFR 1.1274-4 - Test rate.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 26 Internal Revenue 11 2013-04-01 2013-04-01 false Test rate. 1.1274-4 Section 1.1274-4 Internal... TAXES (CONTINUED) Special Rules for Determining Capital Gains and Losses § 1.1274-4 Test rate. (a) Determination of test rate of interest—(1) In general—(i) Test rate is the 3-month rate. Except as provided in...

  20. 26 CFR 1.1274-4 - Test rate.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 26 Internal Revenue 11 2012-04-01 2012-04-01 false Test rate. 1.1274-4 Section 1.1274-4 Internal... TAXES (CONTINUED) Special Rules for Determining Capital Gains and Losses § 1.1274-4 Test rate. (a) Determination of test rate of interest—(1) In general—(i) Test rate is the 3-month rate. Except as provided in...

  1. In situ X-ray monitoring of damage accumulation in SiC/RBSN tensile specimens

    NASA Technical Reports Server (NTRS)

    Baaklini, George Y.; Bhatt, Ramkrishna T.

    1991-01-01

    The room-temperature tensile testing of silicon carbide fiber reinforced reaction-bonded silicon nitride (SiC/RBSN) composite specimens was monitored by using in-situ X-ray film radiography. Radiographic evaluation before, during, and after loading provided data on the effect of preexisting volume flaws (high density impurities, and local density variations) on the fracture behavior of composites. Results from (O)1, (O)3, (O)5, and (O)8 composite specimens showed that X-ray film radiography can monitor damage accumulations during tensile loading. Matrix cracking, fiber-matrix debonding, and fiber pullout were imaged throughout the tensile loading history of the specimens. Further, in-situ film radiography was found to be a helpful and practical technique for estimating interfacial shear strength between the SiC fiber and the RBSN matrix by the matrix crack spacing method. It is concluded that pretest, in-situ, and post-test radiography can provide for a greater understanding of ceramic matrix composite mechanical behavior, a verification of related experimental procedures, and a validation and development of related analytical models.

  2. In-situ x-ray monitoring of damage accumulation in SiC/RBSN tensile specimens

    NASA Technical Reports Server (NTRS)

    Baaklini, George Y.; Bhatt, Ramakrishna T.

    1991-01-01

    The room-temperature tensile testing of silicon carbide fiber reinforced reaction-bonded silicon nitride (SiC/RBSN) composite specimens was monitored by using in-situ x ray film radiography. Radiographic evaluation before, during, and after loading provided data on the effect of preexisting volume flaws (high density impurities, and local density variations) on the fracture behavior of composites. Results from (0)1, (0)3, (0)5, and (0)8 composite specimens, showed that x ray film radiography can monitor damage accumulations during tensile loading. Matrix cracking, fiber-matrix debonding, and fiber pullout were imaged throughout the tensile loading history of the specimens. Further, in-situ film radiography was found to be a helpful and practical technique for estimating interfacial shear strength between the SiC fiber and the RBSN matrix by the matrix crack spacing method. It is concluded that pretest, in-situ, and post-test radiography can provide for a greater understanding of ceramic matrix composite mechanical behavior, a verification of related experimental procedures, and a validation and development of related analytical models.

  3. Effects of soldering methods on tensile strength of a gold-palladium metal ceramic alloy.

    PubMed

    Ghadhanfari, Husain A; Khajah, Hasan M; Monaco, Edward A; Kim, Hyeongil

    2014-10-01

    The tensile strength obtained by conventional postceramic application soldering and laser postceramic welding may require more energy than microwave postceramic soldering, which could provide similar tensile strength values. The purpose of the study was to compare the tensile strength obtained by microwave postceramic soldering, conventional postceramic soldering, and laser postceramic welding. A gold-palladium metal ceramic alloy and gold-based solder were used in this study. Twenty-seven wax specimens were cast in gold-palladium noble metal and divided into 4 groups: laser welding with a specific postfiller noble metal, microwave soldering with a postceramic solder, conventional soldering with the same postceramic solder used in the microwave soldering group, and a nonsectioned control group. All the specimens were heat treated to simulate a normal porcelain sintering sequence. An Instron Universal Testing Machine was used to measure the tensile strength for the 4 groups. The means were analyzed statistically with 1-way ANOVA. The surface and fracture sites of the specimens were subjectively evaluated for fracture type and porosities by using a scanning electron microscope. The mean (standard deviation) ultimate tensile strength values were as follows: nonsectioned control 818 ±30 MPa, microwave 516 ±34 MPa, conventional 454 ±37 MPa, and laser weld 191 ±39 MPa. A 1-way ANOVA showed a significant difference in ultimate tensile strength among the groups (F3,23=334.5; P<.001). Follow-up multiple comparisons showed a significant difference among all the groups. Microwave soldering resulted in a higher tensile strength for gold and palladium noble metals than either conventional soldering or laser welding. Conventional soldering resulted in a higher tensile strength than laser welding. Under the experimental conditions described, either microwave or conventional postceramic soldering would appear to satisfy clinical requirements related to tensile strength

  4. Investigation of defect rate of lap laser welding of stainless steel railway vehicles car body

    NASA Astrophysics Data System (ADS)

    Wang, Hongxiao

    2015-02-01

    In order to resolve the disadvantages such as poor appearance quality, poor tightness, low efficiency of resistance spot welding of stainless steel rail vehicles, partial penetration lap laser welding process was investigated widely. But due to the limitation of processing technology, there will be local incomplete fusion in the lap laser welding seam. Defect rate is the ratio of the local incomplete fusion length to the weld seam length. The tensile shear strength under different defect rate and its effect on the car body static strength are not clear. It is necessary to find the biggest defect rate by numerical analysis of effects of different defect rates on the laser welding stainless steel rail vehicle body structure strength ,and tests of laser welding shear tensile strength.

  5. Seismic characteristics of tensile fracture growth induced by hydraulic fracturing

    NASA Astrophysics Data System (ADS)

    Eaton, D. W. S.; Van der Baan, M.; Boroumand, N.

    2014-12-01

    Hydraulic fracturing is a process of injecting high-pressure slurry into a rockmass to enhance its permeability. Variants of this process are used for unconventional oil and gas development, engineered geothermal systems and block-cave mining; similar processes occur within volcanic systems. Opening of hydraulic fractures is well documented by mineback trials and tiltmeter monitoring and is a physical requirement to accommodate the volume of injected fluid. Numerous microseismic monitoring investigations acquired in the audio-frequency band are interpreted to show a prevalence of shear-dominated failure mechanisms surrounding the tensile fracture. Moreover, the radiated seismic energy in the audio-frequency band appears to be a miniscule fraction (<< 1%) of the net injected energy, i.e., the integral of the product of fluid pressure and injection rate. We use a simple penny-shaped crack model as a predictive framework to describe seismic characteristics of tensile opening during hydraulic fracturing. This model provides a useful scaling relation that links seismic moment to effective fluid pressure within the crack. Based on downhole recordings corrected for attenuation, a significant fraction of observed microseismic events are characterized by S/P amplitude ratio < 5. Despite the relatively small aperture of the monitoring arrays, which precludes both full moment-tensor analysis and definitive identification of nodal planes or axes, this ratio provides a strong indication that observed microseismic source mechanisms have a component of tensile failure. In addition, we find some instances of periodic spectral notches that can be explained by an opening/closing failure mechanism, in which fracture propagation outpaces fluid velocity within the crack. Finally, aseismic growth of tensile fractures may be indicative of a scenario in which injected energy is consumed to create new fracture surfaces. Taken together, our observations and modeling provide evidence that

  6. Uniaxial Tensile Test for Soil.

    DTIC Science & Technology

    1987-04-01

    2.0 by 5.0 cm. This test was also performed on a horizontal specimen; however loading was applied through small metal plates that were embedded in the 6...i. enlarged ends. The specimen was supported by a bed of mercury and had two small ceramic markers mounted in the gage length that were monitored...with a cathetometer to determine displacements. It was found that most tests failed near the location of the embedded metal loading plates making their

  7. A comparison of tensile properties of polyester composites reinforced with pineapple leaf fiber and pineapple peduncle fiber

    NASA Astrophysics Data System (ADS)

    Juraidi, J. M.; Shuhairul, N.; Syed Azuan, S. A.; Intan Saffinaz Anuar, Noor

    2013-12-01

    Pineapple fiber which is rich in cellulose, relatively inexpensive, and abundantly available has the potential for polymer reinforcement. This research presents a study of the tensile properties of pineapple leaf fiber and pineapple peduncle fiber reinforced polyester composites. Composites were fabricated using leaf fiber and peduncle fiber with varying fiber length and fiber loading. Both fibers were mixed with polyester composites the various fiber volume fractions of 4, 8 and 12% and with three different fiber lengths of 10, 20 and 30 mm. The composites panels were fabricated using hand lay-out technique. The tensile test was carried out in accordance to ASTM D638. The result showed that pineapple peduncle fiber with 4% fiber volume fraction and fiber length of 30 mm give highest tensile properties. From the overall results, pineapple peduncle fiber shown the higher tensile properties compared to pineapple leaf fiber. It is found that by increasing the fiber volume fraction the tensile properties has significantly decreased but by increasing the fiber length, the tensile properties will be increased proportionally. Minitab software is used to perform the two-way ANOVA analysis to measure the significant. From the analysis done, there is a significant effect of fiber volume fraction and fiber length on the tensile properties.

  8. Mechanical Characterization of Immature Porcine Brainstem in Tension at Dynamic Strain Rates.

    PubMed

    Zhao, Hui; Yin, Zhiyong; Li, Kui; Liao, Zhikang; Xiang, Hongyi; Zhu, Feng

    2016-01-21

    Many brain injury cases involve pediatric road traffic accidents, and among these, brainstem injury causes disastrous outcomes. A thorough understanding of the tensile characterization of immature brainstem tissue is crucial in modeling traumatic brain injury sustained by children, but limited experimental data in tension is available for the immature brain tissue at dynamic strain rates. We harvested brainstem tissue from immature pigs (about 4 weeks old, and at a developmental stage similar to that of human toddlers) as a byproduct from a local slaughter house and very carefully prepared the samples. Tensile tests were performed on specimens at dynamic strain rates of 2/s, 20/s, and 100/s using a biological material instrument. The constitutive models, Fung, Ogden, Gent, and exponential function, for immature brainstem tissue material property were developed for the recorded experimental data using OriginPro 8.0 software. The t test was performed for infinitesimal shear modules. The curves of stress-versus-stretch ratio were convex in shape, and inflection points were found in all the test groups at the strain of about 2.5%. The average Lagrange stress of the immature brainstem specimen at the 30% strain at the strain rates of 2, 20, and 100/s was 273±114, 515±107, and 1121±197 Pa, respectively. The adjusted R-Square (R2) of Fung, Ogden, Gent, and exponential model was 0.820≤R2≤0.933, 0.774≤R2≤0.940, 0.650≤R2≤0.922, and 0.852≤R2≤0.981, respectively. The infinitesimal shear modulus of the strain energy functions showed a significant association with the strain rate (p<0.01). The immature brainstem is a rate-dependent material in dynamic tensile tests, and the tissue becomes stiffer with increased strain rate. The reported results may be useful in the study of brain injuries in children who sustain injuries in road traffic accidents. Further research in more detail should be performed in the future.

  9. Performance enhancement in uniaxially tensile stressed GeSn n-channel fin tunneling field-effect transistor: Impact of stress direction

    NASA Astrophysics Data System (ADS)

    Wang, Hongjuan; Han, Genquan; Jiang, Xiangwei; Liu, Yan; Zhang, Chunfu; Zhang, Jincheng; Hao, Yue

    2017-04-01

    In this work, the boosting effect on the performance of GeSn n-channel fin tunneling FET (nFinTFET) enabled by uniaxial tensile stress is investigated theoretically. As the fin rotates within the (001) plane, the uniaxial tensile stress is always along its direction. The electrical characteristics of tensile-stressed GeSn nFinTFETs with point and line tunneling modes are computed utilizing the technology computer aided design (TCAD) simulator in which the dynamic nonlocal band-to-band tunneling (BTBT) algorithm is employed. In comparison with the relaxed devices, tensile-stressed GeSn nFinTFETs achieve a substantial enhancement in band-to-band tunneling generation rate (G BTBT) and on-state current I ON owing to the reduced bandgap E G induced by the tensile stress. Performance improvement of GeSn nFinTFETs induced by tensile stress demonstrates a strong dependence on channel direction and tunneling modes. Under the same magnitude of stress, line-nFinTFETs obtain a more pronounced I ON enhancement over the transistors with point tunneling mode.

  10. Analysis of the tensile stress-strain behavior of elastomers at constant strain rates. I - Criteria for separability of the time and strain effects

    NASA Technical Reports Server (NTRS)

    Hong, S. D.; Fedors, R. F.; Schwarzl, F.; Moacanin, J.; Landel, R. F.

    1981-01-01

    A theoretical analysis of the tensile stress-strain relation of elastomers at constant strain rate is presented which shows that the time and the stress effect are separable if the experimental time scale coincides with a segment of the relaxation modulus that can be described by a single power law. It is also shown that time-strain separability is valid if the strain function is linearly proportional to the Cauchy strain, and that when time-strain separability holds, two strain-dependent quantities can be obtained experimentally. In the case where time and strain effect are not separable, superposition can be achieved only by using temperature and strain-dependent shift factors.

  11. Rate dependent strengths of some solder joints

    NASA Astrophysics Data System (ADS)

    Williamson, D. M.; Field, J. E.; Palmer, S. J. P.; Siviour, C. R.

    2007-08-01

    The shear strengths of three lead-free solder joints have been measured over the range of loading rates 10-3 to ~105 mm min-1. Binary (SnAg), ternary (SnAgCu) and quaternary (Castin: SnAgCuSb) alloys have been compared to a conventional binary SnPb solder alloy. Results show that at loading rates from 10-3 to 102 mm min-1, all four materials exhibit a linear relationship between the shear strength and the loading rate when the data are plotted on a log-log plot. At the highest loading rate of 105 mm min-1, the strengths of the binary alloys were in agreement with extrapolations made from the lower loading rate data. In contrast, the strengths of the higher order alloys were found to be significantly lower than those predicted by extrapolation. This is explained by a change in failure mechanism on the part of the higher order alloys. Similar behaviour was found in measurements of the tensile strengths of solder joints using a novel high-rate loading tensile test. Optical and electron microscopy were used to examine the microstructures of interest in conjunction with energy dispersive x-ray analysis for elemental identification. The effect of artificial aging and reflow of the solder joints is also reported.

  12. Effect of tensile pre-strain at different orientation on martensitic transformation and mechanical properties of 316L stainless steel

    NASA Astrophysics Data System (ADS)

    Wibowo, F.; Zulfi, F. R.; Korda, A. A.

    2017-01-01

    Deformation induced martensite was studied in 316L stainless steel through tensile pre-strain deformation in the rolling direction (RD) and perpendicular to the rolling direction (LT) at various %pre-strain. The experiment was carried out at various given %pre-strain, which were 0%, 4.6%, 12%, 17.4%, and 25.2% for the RD, whereas for LT were 0%, 4.6%, 12%, 18%, and 26% for LT. Changes in the microstructure and mechanical properties were observed using optical microscope, tensile testing, hardness testing, and X-ray diffraction (XRD) analysis. The experimental results showed that the volume fraction of martensite was increased as the %pre-strain increased. In the same level of deformation by tensile pre-strain, the volume of martensite for RD was higher than that with LT direction. The ultimate tensile strength (UTS), yield strength (YS), and hardness of the steel were increased proportionally with the increases in %pre-strain, while the value of elongation and toughness were decreased with the increases in %pre-strain.

  13. Microstructure, Tensile and Fatigue Properties of Al-5 wt.%Mg Alloy Manufactured by Twin Roll Strip Casting

    NASA Astrophysics Data System (ADS)

    Heo, Joon-Young; Baek, Min-Seok; Euh, Kwang-Jun; Lee, Kee-Ahn

    2018-04-01

    This study investigated the microstructure, tensile and fatigue properties of Al-5 wt.%Mg alloy manufactured by twin roll strip casting. Strips cast as a fabricated (F) specimen and a specimen heat treated (O) at 400 °C/5 h were produced and compared. In the F specimen, microstructural observation discovered clustered precipitates in the center area, while in the O specimen precipitates were relatively more evenly distributed. Al, Al6(Mn, Fe), Mg2Al3 and Mg2Si phases were observed. However, most of the Mg2Al3 phase in the heat-treated O specimen was dissolved. A room temperature tensile test measured yield strength of 177.7 MPa, ultimate tensile strength of 286.1 MPa and elongation of 11.1% in the F specimen and 167.7 MPa (YS), 301.5 MPa (UTS) and 24.6% (EL) in the O specimen. A high cycle fatigue test measured a fatigue limit of 145 MPa in the F specimen and 165 MPa in the O specimen, and the O specimen achieved greater fatigue properties in all fatigue stress conditions. The tensile and fatigue fracture surfaces of the above-mentioned specimens were observed, and this study attempted to investigate the tensile and fatigue deformation behavior of strip cast Al-5 wt.%Mg based on the findings.

  14. Tensile strength of cementing agents on the CeraOne system of dental prosthesis on implants.

    PubMed

    Montenegro, Alexandre Campos; Machado, Aldir Nascimento; Depes Gouvêa, Cresus Vinicius

    2008-12-01

    The aim of this in vitro study was to evaluate the tensile strength of titanium cylinders cemented on stainless steel abutment mock-ups by the Cerazone system. Four types of cements were used: glass ionomer, Fuji I (GC); zinc phosphate, Cimento LS (Vigodent); zinc oxide without eugenol, Rely x Temp NE (3M ESPE); and resin cement, Rely x ARC (3M ESPE). Four experimental groups were formed, each composed of 5 test specimens. Each test specimen consisted of a set of 1 cylinder and 1 stainless steel abutment mock-up. All cements tested were manipulated in accordance with manufacturers' instructions. A static load of 5 Newtons (N) for 2 minutes was used to standardize the procedure. The tensile tests were performed by a mechanical universal testing machine (EMIC DL500MF) at a crosshead speed of 0.5 mm/min. The highest bonding values resulting from the experiment were obtained by Cimento LS (21.86 MPa mean), followed by the resin cement Rely x ARC (12.95 MPa mean), Fuji I (6.89 MPa mean), and Rely x Temp NE (4.71 MPa mean). The results were subjected to analysis of variance (ANOVA) and the Student's t test. The cements differed amongst them as regards tensile strength, with the highest bonding levels recorded with zinc phosphate (Cimento LS) and the lowest with the zinc oxide without eugenol (Rely x Temp NE).

  15. 49 CFR 230.26 - Tensile strength of shell plates.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 4 2011-10-01 2011-10-01 false Tensile strength of shell plates. 230.26 Section... Appurtenances Strength of Materials § 230.26 Tensile strength of shell plates. When the tensile strength of steel or wrought-iron shell plates is not known, it shall be taken at 50,000 psi for steel and 45,000...

  16. 49 CFR 230.26 - Tensile strength of shell plates.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 4 2010-10-01 2010-10-01 false Tensile strength of shell plates. 230.26 Section... Appurtenances Strength of Materials § 230.26 Tensile strength of shell plates. When the tensile strength of steel or wrought-iron shell plates is not known, it shall be taken at 50,000 psi for steel and 45,000...

  17. Tensile Flow Behavior of Tungsten Heavy Alloys Produced by CIPing and Gelcasting Routes

    NASA Astrophysics Data System (ADS)

    Panchal, Ashutosh; Ravi Kiran, U.; Nandy, T. K.; Singh, A. K.

    2018-04-01

    Present work describes the flow behavior of tungsten heavy alloys with nominal compositions 90W-7Ni-3Fe, 93W-4.9Ni-2.1Fe, and 95W-3.5Ni-1.5Fe (wt pct) produced by CIPing and gelcasting routes. The overall microstructural features of gelcasting are finer than those of CIPing alloys. Both the grain size of W and corresponding contiguity values increase with increase in W content in the present alloys. The volume fraction of matrix phase decreases with increase in W content in both the alloys. The lattice parameter values of the matrix phase also increase with increase in W content. The yield strength (σ YS) continuously increases with increase in W content in both the alloys. The σ YS values of CIPing alloys are marginally higher than those of gelcasting at constant W. The ultimate tensile strength (σ UTS) and elongation values are maximum at intermediate W content. Present alloys exhibit two slopes in true stress-true plastic strain curves in low and high strain regimes and follow a characteristic Ludwigson relation. The two slopes are associated with two deformation mechanisms that are occurring during tensile deformation. The overall nature of differential curves of all the alloys is different and these curves contain three distinctive stages of work hardening (I, II, and III). This suggests varying deformation mechanisms during tensile testing due to different volume fractions of constituent phases. The slip is the predominant deformation mechanism of the present alloys during tensile testing.

  18. Tensile Flow Behavior of Tungsten Heavy Alloys Produced by CIPing and Gelcasting Routes

    NASA Astrophysics Data System (ADS)

    Panchal, Ashutosh; Ravi Kiran, U.; Nandy, T. K.; Singh, A. K.

    2018-06-01

    Present work describes the flow behavior of tungsten heavy alloys with nominal compositions 90W-7Ni-3Fe, 93W-4.9Ni-2.1Fe, and 95W-3.5Ni-1.5Fe (wt pct) produced by CIPing and gelcasting routes. The overall microstructural features of gelcasting are finer than those of CIPing alloys. Both the grain size of W and corresponding contiguity values increase with increase in W content in the present alloys. The volume fraction of matrix phase decreases with increase in W content in both the alloys. The lattice parameter values of the matrix phase also increase with increase in W content. The yield strength ( σ YS) continuously increases with increase in W content in both the alloys. The σ YS values of CIPing alloys are marginally higher than those of gelcasting at constant W. The ultimate tensile strength ( σ UTS) and elongation values are maximum at intermediate W content. Present alloys exhibit two slopes in true stress-true plastic strain curves in low and high strain regimes and follow a characteristic Ludwigson relation. The two slopes are associated with two deformation mechanisms that are occurring during tensile deformation. The overall nature of differential curves of all the alloys is different and these curves contain three distinctive stages of work hardening (I, II, and III). This suggests varying deformation mechanisms during tensile testing due to different volume fractions of constituent phases. The slip is the predominant deformation mechanism of the present alloys during tensile testing.

  19. Increased Tensile Strength of Carbon Nanotube Yarns and Sheets through Chemical Modification and Electron Beam Irradiation

    NASA Technical Reports Server (NTRS)

    Miller, Sandi G.; Williams, Tiffany S.; Baker, James S.; Sola, Francisco; Lebron-Colon, Marisabel; McCorkle, Linda S.; Wilmoth, Nathan G.; Gaier, James; Chen, Michelle; Meador, Michael A.

    2014-01-01

    The inherent strength of individual carbon nanotubes offers considerable opportunity for the development of advanced, lightweight composite structures. Recent work in the fabrication and application of carbon nanotube (CNT) forms such as yarns and sheets has addressed early nanocomposite limitations with respect to nanotube dispersion and loading; and has pushed the technology toward structural composite applications. However, the high tensile strength of an individual CNT has not directly translated to macro-scale CNT forms where bulk material strength is limited by inter-tube electrostatic attraction and slippage. The focus of this work was to assess post processing of CNT sheet and yarn to improve the macro-scale strength of these material forms. Both small molecule functionalization and e-beam irradiation was evaluated as a means to enhance tensile strength and Youngs modulus of the bulk CNT material. Mechanical testing results revealed a tensile strength increase in CNT sheets by 57 when functionalized, while an additional 48 increase in tensile strength was observed when functionalized sheets were irradiated; compared to unfunctionalized sheets. Similarly, small molecule functionalization increased yarn tensile strength up to 25, whereas irradiation of the functionalized yarns pushed the tensile strength to 88 beyond that of the baseline yarn.

  20. Tensile properties of the transverse carpal ligament and carpal tunnel complex.

    PubMed

    Ugbolue, Ukadike C; Gislason, Magnus K; Carter, Mark; Fogg, Quentin A; Riches, Philip E; Rowe, Philip J

    2015-08-01

    A new sophisticated method that uses video analysis techniques together with a Maillon Rapide Delta to determine the tensile properties of the transverse carpal ligament-carpal tunnel complex has been developed. Six embalmed cadaveric specimens amputated at the mid-forearm and aged (mean (SD)): 82 (6.29) years were tested. The six hands were from three males (four hands) and one female (two hands). Using trigonometry and geometry the elongation and strain of the transverse carpal ligament and carpal arch were calculated. The cross-sectional area of the transverse carpal ligament was determined. Tensile properties of the transverse carpal ligament-carpal tunnel complex and Load-Displacement data were also obtained. Descriptive statistics, one-way ANOVA together with a post-hoc analysis (Tukey) and t-tests were incorporated. A transverse carpal ligament-carpal tunnel complex novel testing method has been developed. The results suggest that there were no significant differences between the original transverse carpal ligament width and transverse carpal ligament at peak elongation (P=0.108). There were significant differences between the original carpal arch width and carpal arch width at peak elongation (P=0.002). The transverse carpal ligament failed either at the mid-substance or at their bony attachments. At maximum deformation the peak load and maximum transverse carpal ligament displacements ranged from 285.74N to 1369.66N and 7.09mm to 18.55mm respectively. The transverse carpal ligament cross-sectional area mean (SD) was 27.21 (3.41)mm(2). Using this method the results provide useful biomechanical information and data about the tensile properties of the transverse carpal ligament-carpal tunnel complex. Copyright © 2015 Elsevier Ltd. All rights reserved.

  1. Effect of zirconium oxide nanoparticles addition on the optical and tensile properties of polymethyl methacrylate denture base material

    PubMed Central

    Gad, Mohammed M; Abualsaud, Reem; Rahoma, Ahmed; Al-Thobity, Ahmad M; Al-Abidi, Khalid S; Akhtar, Sultan

    2018-01-01

    Background Polymethyl methacrylate (PMMA) is widely used for the fabrication of removable prostheses. Recently, zirconium oxide nanoparticles (nano-ZrO2) have been added to improve some properties of PMMA, but their effect on the optical properties and tensile strength are neglected. Objective The aim of this study was to investigate the effect of nano-ZrO2 addition on the translucency and tensile strength of the PMMA denture base material. Materials and methods Eighty specimens (40 dumbbell-shaped and 40 discs) were prepared out of heat-polymerized acrylic resin and divided into four groups per test (n=10). The control group for each test included unreinforced acrylic, while the test groups were reinforced with 2.5, 5, and 7.5 wt% nano-ZrO2. Acrylic resin was mixed according to manufacturer’s instructions, packed, and processed by conventional method. After polymerization, all specimens were finished, polished, and stored in distilled water at 37°C for 48±2 hours. Tensile strength (MPa) was evaluated using the universal testing machine while the specimens’ translucency was examined using a spectrophotometer. Statistical analysis was carried out by SPSS using the paired sample t-test (p≤0.05). A scanning electron microscope was used to analyze the morphological changes and topography of the fractured surfaces. Results This study showed that the mean tensile strength of the PMMA in the test groups of 2.5%NZ, 5%NZ, and 7.5%NZ was significantly higher than the control group. The tensile strength increased significantly after nano-ZrO2 addition, and the maximum increase seen was in the 7.5%NZ group. The translucency values of the experimental groups were significantly lower than those of the control group. Within the reinforced groups, the 2.5%NZ group had significantly higher translucency values when compared to the 5%NZ and 7.5%NZ groups. Conclusion The addition of nano-ZrO2 increased the tensile strength of the denture base acrylic. The increase was directly

  2. Measurement of fracture properties of concrete at high strain rates

    PubMed Central

    Cendón, D. A.; Sánchez-Gálvez, V.; Gálvez, F.

    2017-01-01

    An analysis of the spalling technique of concrete bars using the modified Hopkinson bar was carried out. A new experimental configuration is proposed adding some variations to previous works. An increased length for concrete specimens was chosen and finite-element analysis was used for designing a conic projectile to obtain a suitable triangular impulse wave. The aim of this initial work is to establish an experimental framework which allows a simple and direct analysis of concrete subjected to high strain rates. The efforts and configuration of these primary tests, as well as the selected geometry and dimensions for the different elements, have been focused to achieve a simple way of identifying the fracture position and so the tensile strength of tested specimens. This dynamic tensile strength can be easily compared with previous values published in literature giving an idea of the accuracy of the method and technique proposed and the possibility to extend it in a near future to obtain other mechanical properties such as the fracture energy. The tests were instrumented with strain gauges, accelerometers and high-speed camera in order to validate the results by different ways. Results of the dynamic tensile strength of the tested concrete are presented. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’. PMID:27956510

  3. An Experimental Study of the Influence of in-Plane Fiber Waviness on Unidirectional Laminates Tensile Properties

    NASA Astrophysics Data System (ADS)

    Zhao, Cong; Xiao, Jun; Li, Yong; Chu, Qiyi; Xu, Ting; Wang, Bendong

    2017-12-01

    As one of the most common process induced defects of automated fiber placement, in-plane fiber waviness and its influences on mechanical properties of fiber reinforced composite lack experimental studies. In this paper, a new approach to prepare the test specimen with in-plane fiber waviness is proposed in consideration of the mismatch between the current test standard and actual fiber trajectory. Based on the generation mechanism of in-plane fiber waviness during automated fiber placement, the magnitude of in-plane fiber waviness is characterized by axial compressive strain of prepreg tow. The elastic constants and tensile strength of unidirectional laminates with in-plane fiber waviness are calculated by off-axis and maximum stress theory. Experimental results show that the tensile properties infade dramatically with increasing magnitude of the waviness, in good agreement with theoretical analyses. When prepreg tow compressive strain reaches 1.2%, the longitudinal tensile modulus and strength of unidirectional laminate decreased by 25.5% and 57.7%, respectively.

  4. Interpretation of dynamic tensile behavior by austenite stability in ferrite-austenite duplex lightweight steels.

    PubMed

    Park, Jaeyeong; Jo, Min Cheol; Jeong, Hyeok Jae; Sohn, Seok Su; Kwak, Jai-Hyun; Kim, Hyoung Seop; Lee, Sunghak

    2017-11-16

    Phenomena occurring in duplex lightweight steels under dynamic loading are hardly investigated, although its understanding is essentially needed in applications of automotive steels. In this study, quasi-static and dynamic tensile properties of duplex lightweight steels were investigated by focusing on how TRIP and TWIP mechanisms were varied under the quasi-static and dynamic loading conditions. As the annealing temperature increased, the grain size and volume fraction of austenite increased, thereby gradually decreasing austenite stability. The strain-hardening rate curves displayed a multiple-stage strain-hardening behavior, which was closely related with deformation mechanisms. Under the dynamic loading, the temperature rise due to adiabatic heating raised the austenite stability, which resulted in the reduction in the TRIP amount. Though the 950 °C-annealed specimen having the lowest austenite stability showed the very low ductility and strength under the quasi-static loading, it exhibited the tensile elongation up to 54% as well as high strain-hardening rate and tensile strength (1038 MPa) due to appropriate austenite stability under dynamic loading. Since dynamic properties of the present duplex lightweight steels show the excellent strength-ductility combination as well as continuously high strain hardening, they can be sufficiently applied to automotive steel sheets demanded for stronger vehicle bodies and safety enhancement.

  5. Ab initio LDA+U prediction of the tensile properties of chromia across multiple length scales

    NASA Astrophysics Data System (ADS)

    Mosey, Nicholas J.; Carter, Emily A.

    2009-02-01

    Periodic density functional theory (DFT) and DFT+U calculations are used to evaluate various mechanical properties associated with the fracture of chromia (Cr 2O 3) along the [0 0 0 1] and [0 1 1¯ (3/2) (a/c)2 2] directions. The properties investigated include the tensile strength, elastic constants, and surface energies. The tensile strengths are evaluated using an ideal tensile test, which provides the theoretical tensile strength, and by fitting the calculated data to universal binding energy relationships (UBER), which permit the extrapolation of the calculated results to arbitrary length scales. The results demonstrate the ability of the UBER to yield a realistic estimate of the tensile strength of a 10-μm-thick sample of Cr 2O 3 using data obtained through calculations on nanoscopic systems. We predict that Cr 2O 3 will fracture most easily in the [0 1 1¯ (3/2) (a/c)2 2] direction, with a best estimate for the tensile strength of 386 MPa for a 10 μm grain, consistent with flexural strength measurements for chromia. The grain becomes considerably stronger at the nanoscale, where we predict a tensile strength along the same direction of 32.1 GPa for 1.45 nm crystallite. The results also provide insight into the origin of the direction dependence of the mechanical properties of Cr 2O 3, with the differences in the behavior along different directions being related to the number of Cr-O bonds supporting the applied tensile load. Additionally, the results shed light on various practical aspects of modeling the mechanical properties of materials with DFT+U calculations and in using UBERs to estimate the mechanical properties of materials across disparate length scales.

  6. Tensile and fatigue behavior of tungsten/copper composites

    NASA Technical Reports Server (NTRS)

    Verrilli, Michael J.; Gabb, Timothy P.; Kim, Y. S.

    1989-01-01

    Work on W/Cu unidirectional composites was initiated to study the behavior of this ductile-ductile composite system under thermomechanical fatigue and to examine the applicability of fatigue-life prediction methods for thermomechanical fatigue of this metal matrix composite. The first step was to characterize the tensile behavior of four ply, 10 vol. percent W/Cu plates at room and elevated temperatures. Fatigue tests were conducted in load control on 0 degree specimens at 260 C. The maximum cyclic stress was varied but the minimum cyclic stress was kept constant. All tests were performed in vacuum. The strain at failure increased with increasing maximum cyclic stress.

  7. Cervical Rotatory Manipulation Decreases Uniaxial Tensile Properties of Rabbit Atherosclerotic Internal Carotid Artery

    PubMed Central

    Qi, Ji; Zhang, Lei; Chen, Chao; Mondal, Shubhro; Ping, Kaike; Chen, Yili

    2017-01-01

    Objective. To investigate the effects of one of the Chinese massage therapies, cervical rotatory manipulation (CRM), on uniaxial tensile properties of rabbit atherosclerotic internal carotid artery (ICA). Methods. 40 male purebred New Zealand white rabbits were randomly divided into CRM-Model group, Non-CRM-Model group, CRM-Normal group, and Non-CRM-Normal group. After modeling (atherosclerotic model) and intervention (CRM or Non-CRM), uniaxial tensile tests were performed on the ICAs to assess the differences in tensile mechanical properties between the four groups. Results. Both CRM and modeling were the main effects affecting physiological elastic modulus (PEM) of ICA. PEM in CRM-Model group was 1.81 times as much as Non-CRM-Model group, while the value in CRM-Model group was 1.34 times as much as CRM-Normal group. Maximum elastic modulus in CRM-Model group was 1.80 times as much as CRM-Normal group. Max strains in CRM-Model group and Non-CRM-Model group were 30.98% and 28.71% lower than CRM-Normal group and Non-CRM-Normal group, respectively. However, whether treated with CRM or not, the uniaxial tensile properties of healthy ICAs were not statistically different. Conclusion. CRM may decrease the uniaxial tensile properties of rabbit arteriosclerotic ICA, but with no effect on normal group. The study will aid in the meaningful explanation of the controversy about the harmfulness of CRM and the suitable population of CRM. PMID:28303160

  8. Tensile strength and water absorption of alumina filled poly (methyl methacrylate) denture base material.

    PubMed

    Nizam, A; Mohamed, S H; Arifin, A; Mohd Ishak, Z A; Samsudin, A R

    2004-05-01

    The aim of this study was to evaluate the tensile properties and water absorption of denture base material prepared from high molecular weight poly methyl methacrylate (PMMA) and alumina (Al2O3) as particulate filler. Specimens for mechanical testing were prepared by adding composite powder to the monomer followed by hand mixing as in dental laboratory procedure. The tensile strength of the prepared denture base material was slightly higher than commercial denture base material, while the water absorption was almost the same for all formulation of denture base materials.

  9. Forming limit curves of DP600 determined in high-speed Nakajima tests and predicted by two different strain-rate-sensitive models

    NASA Astrophysics Data System (ADS)

    Weiß-Borkowski, Nathalie; Lian, Junhe; Camberg, Alan; Tröster, Thomas; Münstermann, Sebastian; Bleck, Wolfgang; Gese, Helmut; Richter, Helmut

    2018-05-01

    Determination of forming limit curves (FLC) to describe the multi-axial forming behaviour is possible via either experimental measurements or theoretical calculations. In case of theoretical determination, different models are available and some of them consider the influence of strain rate in the quasi-static and dynamic strain rate regime. Consideration of the strain rate effect is necessary as many material characteristics such as yield strength and failure strain are affected by loading speed. In addition, the start of instability and necking depends not only on the strain hardening coefficient but also on the strain rate sensitivity parameter. Therefore, the strain rate dependency of materials for both plasticity and the failure behaviour is taken into account in crash simulations for strain rates up to 1000 s-1 and FLC can be used for the description of the material's instability behaviour at multi-axial loading. In this context, due to the strain rate dependency of the material behaviour, an extrapolation of the quasi-static FLC to dynamic loading condition is not reliable. Therefore, experimental high-speed Nakajima tests or theoretical models shall be used to determine the FLC at high strain rates. In this study, two theoretical models for determination of FLC at high strain rates and results of experimental high-speed Nakajima tests for a DP600 are presented. One of the theoretical models is the numerical algorithm CRACH as part of the modular material and failure model MF GenYld+CrachFEM 4.2, which is based on an initial imperfection. Furthermore, the extended modified maximum force criterion considering the strain rate effect is also used to predict the FLC. These two models are calibrated by the quasi-static and dynamic uniaxial tensile tests and bulge tests. The predictions for the quasi-static and dynamic FLC by both models are presented and compared with the experimental results.

  10. Effects of the Electron Beam Welding Process on the Microstructure, Tensile, Fatigue and Fracture Properties of Nickel Alloy Nimonic 80A

    NASA Astrophysics Data System (ADS)

    Zhang, H.; Huang, Chongxiang; Guan, Zhongwei; Li, Jiukai; Liu, Yongjie; Chen, Ronghua; Wang, Qingyuan

    2018-01-01

    The purpose of this study was to evaluate rotary bending high-cycle fatigue properties and crack growth of Nimonic 80A-based metal and electron beam-welded joints. All the tests were performed at room temperature. Fracture surfaces under high-cycle fatigue and fatigue crack growth were observed by scanning electron microscopy. Microstructure, hardness and tensile properties were also evaluated in order to understand the effects on the fatigue results obtained. It was found that the tensile properties, hardness and high-cycle fatigue properties of the welded joint are lower than the base metal. The fracture surface of the high-cycle fatigue shows that fatigue crack initiated from the surface under the high stress amplitude and from the subsurface under the low stress amplitude. The effect of the welding process on the statistical fatigue data was studied with a special focus on probabilistic life prediction and probabilistic lifetime limits. The fatigue crack growth rate versus stress intensity factor range data were obtained from the fatigue crack growth tests. From the results, it was evident that the fatigue crack growth rates of the welded are higher than the base metal. The mechanisms and fracture modes of fatigue crack growth of welded specimens were found to be related to the stress intensity factor range ΔK. In addition, the effective fatigue crack propagation thresholds and mismatch of welded joints were described and discussed.

  11. Study of Tensile Properties and Deflection Temperature of Polypropylene/Subang Pineapple Leaf Fiber Composites

    NASA Astrophysics Data System (ADS)

    Hafizhah, R.; Juwono, A. L.; Roseno, S.

    2017-05-01

    The development of eco-friendly composites has been increasing in the past four decades because the requirement of eco-friendly materials has been increasing. Indonesia has a lot of natural fiber resources and, pineapple leaf fiber is one of those fibers. This study aimed to determine the influence of weight fraction of pineapple leaf fibers, that were grown at Subang, to the tensile properties and the deflection temperature of polypropylene/Subang pineapple leaf fiber composites. Pineapple leaf fibers were pretreated by alkalization, while polypropylene pellets, as the matrix, were extruded into sheets. Hot press method was used to fabricate the composites. The results of the tensile test and Heat Deflection Temperature (HDT) test showed that the composites that contained of 30 wt.% pineapple leaf fiber was the best composite. The values of tensile strength, modulus of elasticity and deflection temperature were (64.04 ± 3.91) MPa; (3.98 ± 0.55) GPa and (156.05 ± 1.77) °C respectively, in which increased 187.36%, 198.60%, 264.72% respectively from the pristine polypropylene. The results of the observation on the fracture surfaces showed that the failure modes were fiber breakage and matrix failure.

  12. Length-scale and strain rate-dependent mechanism of defect formation and fracture in carbon nanotubes under tensile loading

    NASA Astrophysics Data System (ADS)

    Javvaji, Brahmanandam; Raha, S.; Mahapatra, D. Roy

    2017-02-01

    Electromagnetic and thermo-mechanical forces play a major role in nanotube-based materials and devices. Under high-energy electron transport or high current densities, carbon nanotubes fail via sequential fracture. The failure sequence is governed by certain length scale and flow of current. We report a unified phenomenological model derived from molecular dynamic simulation data, which successfully captures the important physics of the complex failure process. Length-scale and strain rate-dependent defect nucleation, growth, and fracture in single-walled carbon nanotubes with diameters in the range of 0.47 to 2.03 nm and length which is about 6.17 to 26.45 nm are simulated. Nanotubes with long length and small diameter show brittle fracture, while those with short length and large diameter show transition from ductile to brittle fracture. In short nanotubes with small diameters, we observe several structural transitions like Stone-Wales defect initiation, its propagation to larger void nucleation, formation of multiple chains of atoms, conversion to monatomic chain of atoms, and finally complete fracture of the carbon nanotube. Hybridization state of carbon-carbon bonds near the end cap evolves, leading to the formation of monatomic chain in short nanotubes with small diameter. Transition from ductile to brittle fracture is also observed when strain rate exceeds a critical value. A generalized analytical model of failure is established, which correlates the defect energy during the formation of atomic chain with aspect ratio of the nanotube and strain rate. Variation in the mechanical properties such as elastic modulus, tensile strength, and fracture strain with the size and strain rate shows important implications in mitigating force fields and ways to enhance the life of electronic devices and nanomaterial conversion via fracture in manufacturing.

  13. Effect of soldering techniques and gap distance on tensile strength of soldered Ni-Cr alloy joint.

    PubMed

    Lee, Sang-Yeob; Lee, Jong-Hyuk

    2010-12-01

    The present study was intended to evaluate the effect of soldering techniques with infrared ray and gas torch under different gap distances (0.3 mm and 0.5 mm) on the tensile strength and surface porosity formation in Ni-Cr base metal alloy. Thirty five dumbbell shaped Ni-Cr alloy specimens were prepared and assigned to 5 groups according to the soldering method and the gap distance. For the soldering methods, gas torch (G group) and infrared ray (IR group) were compared and each group was subdivided by corresponding gap distance (0.3 mm: G3 and IR3, 0.5 mm: G5, IR5). Specimens of the experimental groups were sectioned in the middle with a diamond disk and embedded in solder blocks according to the predetermined distance. As a control group, 7 specimens were prepared without sectioning or soldering. After the soldering procedure, a tensile strength test was performed using universal testing machine at a crosshead speed 1 mm/min. The proportions of porosity on the fractured surface were calculated on the images acquired through the scanning electronic microscope. Every specimen of G3, G5, IR3 and IR5 was fractured on the solder joint area. However, there was no significant difference between the test groups (P > .05). There was a negative correlation between porosity formation and tensile strength in all the specimens in the test groups (P < .05). There was no significant difference in ultimate tensile strength of joints and porosity formations between the gas-oxygen torch soldering and infrared ray soldering technique or between the gap distance of 0.3 mm and 0.5 mm.

  14. Effect of denture cleansing agents on tensile and shear bond strengths of soft liners to acrylic denture base.

    PubMed

    Mahboub, Farhang; Salehsaber, Fariba; Parnia, Fereydoon; Gharekhani, Vahedeh; Kananizadeh, Yousef; Taghizadeh, Mahsa

    2017-01-01

    Background. The aim of the present study was to evaluate the effect of Corega and 2.5% sodium hypochlorite cleansing agents on the shear and tensile bond strengths of GC soft liner to denture base. Methods. A total of 144 samples (72 samples for tensile and 72 for shear bond strength evaluations) were prepared. The samples in each group were subdivided into three subgroups in terms of the cleansing agent used (2.5% sodium hypochlorite, Corega and distilled water [control group]). All the samples were stored in distilled water, during which each sample was immersed for 15 minutes daily in sodium hypochlorite or Corega solutions. After 20 days the tensile and shear bond strengths were determined using a universal testing machine. In addition, a stereomicroscope was used to evaluate fracture modes. Data were analyzed with one-way ANOVA, using SPSS 16. Results. The results of post hoc Tukey tests showed significant differences in the mean tensile and shear bond strength values between the sodium hypochlorite group with Corega and control groups (P=0.001 for comparison of tensile bond strengths between the sodium hypochlorite and control groups, and P<0.001 for the comparison of tensile bond strengths between the sodium hypochlorite and Corega groups and the shear bond strengths between the sodium hypochlorite and Corega groups, and sodium hypochlorite and control groups).The majority of failures were cohesive in the control and Corega groups and cohesive/adhesive in the sodium hypochlorite group. Conclusion. Immersion of soft liners in Corega will result in longevity of soft liners compared to immersion in sodium hypochlorite solution and sodium hypochlorite solution significantly decreased the tensile and shear bond strengths compared to the control and Corega groups.

  15. Effect of denture cleansing agents on tensile and shear bond strengths of soft liners to acrylic denture base

    PubMed Central

    Mahboub, Farhang; Salehsaber, Fariba; Parnia, Fereydoon; Gharekhani, Vahedeh; Kananizadeh, Yousef; Taghizadeh, Mahsa

    2017-01-01

    Background. The aim of the present study was to evaluate the effect of Corega and 2.5% sodium hypochlorite cleansing agents on the shear and tensile bond strengths of GC soft liner to denture base. Methods. A total of 144 samples (72 samples for tensile and 72 for shear bond strength evaluations) were prepared. The samples in each group were subdivided into three subgroups in terms of the cleansing agent used (2.5% sodium hypochlorite, Corega and distilled water [control group]). All the samples were stored in distilled water, during which each sample was immersed for 15 minutes daily in sodium hypochlorite or Corega solutions. After 20 days the tensile and shear bond strengths were determined using a universal testing machine. In addition, a stereomicroscope was used to evaluate fracture modes. Data were analyzed with one-way ANOVA, using SPSS 16. Results. The results of post hoc Tukey tests showed significant differences in the mean tensile and shear bond strength values between the sodium hypochlorite group with Corega and control groups (P=0.001 for comparison of tensile bond strengths between the sodium hypochlorite and control groups, and P<0.001 for the comparison of tensile bond strengths between the sodium hypochlorite and Corega groups and the shear bond strengths between the sodium hypochlorite and Corega groups, and sodium hypochlorite and control groups).The majority of failures were cohesive in the control and Corega groups and cohesive/adhesive in the sodium hypochlorite group. Conclusion. Immersion of soft liners in Corega will result in longevity of soft liners compared to immersion in sodium hypochlorite solution and sodium hypochlorite solution significantly decreased the tensile and shear bond strengths compared to the control and Corega groups. PMID:29184635

  16. Effect of Thermal Cycling on the Tensile Behavior of Polymer Composites Reinforced by Basalt and Carbon Fibers

    NASA Astrophysics Data System (ADS)

    Khalili, S. Mohammad Reza; Najafi, Moslem; Eslami-Farsani, Reza

    2017-01-01

    The aim of the present work was to investigate the effect of thermal cycling on the tensile behavior of three types of polymer-matrix composites — a phenolic resin reinforced with woven basalt fibers, woven carbon fibers, and hybrid basalt and carbon fibers — in an ambient environment. For this purpose, tensile tests were performed on specimens previously subjected to a certain number of thermal cycles. The ultimate tensile strength of the specimen reinforced with woven basalt fibers had by 5% after thermal cycling, but the strength of the specimen with woven carbon fibers had reduced to a value by 11% higher than that before thermal cycling.

  17. Surface, interphase and tensile properties of unsized, sized and heat treated basalt fibres

    NASA Astrophysics Data System (ADS)

    Förster, T.; Sommer, G. S.; Mäder, E.; Scheffler, C.

    2016-07-01

    Recycling of fibre reinforced polymers is in the focus of several investigations. Chemical and thermal treatments of composites are the common ways to separate the reinforcing fibres from the polymer matrices. However, most sizings on glass and basalt fibre are not designed to resist high temperatures. Hence, a heat treatment might also lead to a sizing removal, a decrease of mechanical performance and deterioration in fibre-matrix adhesion. Different basalt fibres were investigated using surface analysis methods as well as single fibre tensile tests and single fibre pull-out tests in order to reveal the possible causes of these issues. Heat treatment in air reduced the fibre tensile strength in the same level like heat treatment in nitrogen atmosphere, but it influenced the wetting capability. Re-sizing by a coupling agent slightly increased the adhesion strength and reflected a decreased post-debonding friction.

  18. Mechanical characterization of stomach tissue under uniaxial tensile action.

    PubMed

    Jia, Z G; Li, W; Zhou, Z R

    2015-02-26

    In this article, the tensile properties of gastric wall were investigated by using biomechanical test and theoretical analysis. The samples of porcine stomach strips from smaller and greater curvature of the stomach were cut in longitudinal and circumferential direction, respectively. The loading-unloading, stress relaxation, strain creep, tensile fracture tests were performed at mucosa-submucosa, serosa-muscle and intact layer, respectively. Results showed that the biomechanical properties of the porcine stomach depended on the layers, orientations and locations of the gastric wall and presented typical viscoelastic, nonlinear and anisotropic mechanical properties. During loading-unloading test, the stress of serosa-muscle layer in the longitudinal direction was 15-20% more than that in the circumferential direction at 12% stretch ratio, while it could reach about 40% for the intact layer and 50% for the mucosa-submucosa layer. The results of stress relaxation and strain creep showed that the variation degree was obviously faster in the circumferential direction than that in the longitudinal direction, and the ultimate residual values were also different for the different layers, orientations and locations. In the process of fracture test, the serosa-muscle layer fractured firstly followed by the mucosa-submucosa layer when the intact layer was tested, the longitudinal strips firstly began to fracture and the required stress value was about twice as much as that in the circumferential strips. The anisotropy and heterogeneity of mechanical characterization of the porcine stomach were related to its complicated geometry, structure and functions. The results would help us to understand the biomechanics of soft organ tissue. Copyright © 2015 Elsevier Ltd. All rights reserved.

  19. Impact tensile testing of wires

    NASA Technical Reports Server (NTRS)

    Dawson, T. H.

    1976-01-01

    The test consists of fixing one end of a wire specimen and allowing a threaded falling weight to strike the other. Assuming the dynamic stress in the wire to be a function only of its strain, energy considerations show for negligible wire inertia effects that the governing dynamic stress-strain law can be determined directly from impact energy vs. wire elongation data. Theoretical calculations are presented which show negligible wire inertia effects for ratios of wire mass to striking mass of the order of .01 or less. The test method is applied to soft copper wires and the dynamic stress-strain curve so determined is found to be about 30 percent higher than the corresponding static curve.

  20. Multifractal Approaches of the Ring Tensile Rupture Patterns of Dried Laver (Porphyra) as Affected by the Relative Humidity.

    PubMed

    Jung, Hwabin; Yoon, Won Byong

    2017-12-01

    The effect of water activity (a w ) or the relative humidity (RH) on the tensile rupture properties of dried laver (DL) associated with structures formed with phycocolloids was investigated. The morphological characteristics of tensile ruptured DL samples at various relative humidities were evaluated by multifractal analysis. The RH of the microclimate was controlled from 10% to 90% at 25 °C using supersaturated salt solutions. The sorption isotherm of DL was experimentally obtained and quantitatively analyzed using mathematical models. The monolayer moisture contents from the Guggenheim-Anderson-de Boer (GAB) model was 5.92% (w.b.). An increase in the RH resulted in increasing ring tensile stress and maintaining constant ring tensile strain up to 58% to 75% RH, whereas the ring tensile stress and the ring tensile strain rapidly decreased and increased, respectively, when the RH was higher than 75%. The general fractal dimensions and the multifractal spectra f(α) manifested that the patterns of the lowest and the highest moisture content of dried laver showed high irregularity. The different multifractal parameters obtained from the DL at various RHs well-represented the transient moment of the structures from the monolayer moisture to texture changes associated with RH. Overall, the ring tensile test and the multifractal analysis were useful tools to analyze the change of crispness of DL from its structural characteristics. In addition, the results of this study revealed that the integration and disintegration properties of DL occurred through the networks of phycocolloids at various moisture contents. Texture properties are the most important quality attributes for commercial dried laver (DL) products. The relative humidity influences the texture properties of DL during production, storage, shipping, and consuming. This study well characterized the effect of the relative humidity on the texture properties of DL using the tensile tests under microclimate

  1. Effect of Oil Application, Age, Diet, and Pigmentation on the Tensile Strength and Breaking Point of Hair.

    PubMed

    Kavitha, S; Natarajan, Karthika; Thilagavathi, G; Srinivas, C R

    2016-01-01

    Hair strength depends on various factors such as nutrition, environmental factors, sunlight, oiling, aging, conditioner, etc. To compare the tensile strength and breaking point of the hair shaft between (1) vegetarian and nonvegetarian. (2) Those who regularly apply and those who do not apply oil. (3) Pigmented and nonpigmented hair, (4) childhood and elderly. Hair fibers were mounted in tensile strength testing machine Zwick/Roell Z010 and gradual force was administered. The elongation of hair fiber in mm and the maximum force required to break the hair strand were recorded for each fiber. Elasticity of the children's hair was more than the elasticity of adult ( P = 0.05) although tensile strength in children hair was not statistically significant (>0.05). Similarly, the tensile strength was more among those who regularly consumed nonvegetarian food but the difference was not statistically significant ( P > 0.05). There was no statistically significant difference in other groups ( P > 0.05). Elasticity in children hair is statistically more than elderly hair although there is no significant change in tensile strength.

  2. Characterization the microstructure of pulsed Nd:YAG welding method in low frequencies; correlation with tensile and fracture behavior in laser-welded nitinol joints

    NASA Astrophysics Data System (ADS)

    Shojaei Zoeram, Ali; Rahmani, Aida; Asghar Akbari Mousavi, Seyed Ali

    2017-05-01

    The precise controllability of heat input in pulsed Nd:YAG welding method provided by two additional parameters, frequency and pulse duration, has made this method very promising for welding of alloys sensitive to heat input. The poor weldability of Ti-rich nitinol as a result of the formation of Ti2Ni IMC has deprived us of the unique properties of this alloy. In this study, to intensify solidification rate during welding of Ti-rich nitinol, pulsed Nd:YAG laser beam in low frequency was employed in addition to the employment of a copper substrate. Specific microstructure produced in this condition was characterized and the effects of this microstructure on tensile and fracture behavior of samples welded by two different procedures, full penetration and double-sided method with halved penetration depth for each side were investigated. The investigations revealed although the combination of low frequencies, the use of a high thermal conductor substrate and double-sided method eliminated intergranular fracture and increased tensile strength, the particular microstructure, built in the pulsed welding method in low frequencies, results to the formation of the longitudinal cracks during the first stages of tensile test at weld centerline. This degrades tensile strength of welded samples compared to base metal. The results showed samples welded in double-sided method performed much better than samples welded in full penetration mode.

  3. Effects of different types of temporary cements on the tensile strength and marginal adaptation of crowns on implants.

    PubMed

    Akashia, Ana Eliza; Francischone, Carlos Eduardo; Tokutsune, Edson; da Silva, Walter

    2002-01-01

    The aim of this study was to evaluate the influence of four different types of temporary cements, Tempbond (Kerr), Tempbond NE (Kerr), Improv (Sterioss), and Dycal (Dentsply/Caulk), on the marginal adaptation and tensile strength of prosthetic specimens cemented on replicas of CeraOne abutments. Four test groups were formed: Group 1 (G-1), Tempbond (Kerr); Group 2 (G-2), Tempbond NE (Kerr); Group 3 (G-3), Improv (Sterioss); Group 4 (G-4), Dycal (Dentsply/Caulk). For the specimens, gold cylinders (DCB 160, Nobel Biocare) adapted to stainless steel replicas of CeraOne abutments (Nobel Biocare) were utilized. The replicas on a stainless steel base were made in a special machine for implant components. The cement thicknesses for each luting agent were measured using a Measurement Comparative Microscope (Mitutoyo). The readings obtained before cementation were used as the controls (G-0). Following each group's cementation, the specimens were submitted to tensile strength tests with a Universal Testing Machine (Kratus). The results of the marginal adaptation test as reflected by cement thicknesses were: G-0 = 11.7 microm, G-1 = 35.7 microm (+/- 8.8), G-2 = 41.7 microm (+/- 9.0), G-3 = 32.6 microm (+/- 9.7) and G-4 = 38.2 microm (+/- 6.7). The tensile strength tests yielded the following values: G-1 = 58.5 N (+/- 14.8), G-2 = 51 N (+/- 8.2), G-3 = 61.8 N (+/- 17.1) and G-4 = 71.8 N (+/- 9.3). The four temporary cements tested all provided similar marginal adaptation. G-4 (Dycal) showed a higher tensile strength than G-2 (Tempbond NE).

  4. Tensile bond strength of an aged resin composite repaired with different protocols.

    PubMed

    Celik, Esra Uzer; Ergücü, Zeynep; Türkün, L Sebnem; Ercan, Utku Kürșat

    2011-08-01

    To evaluate the effect of different surface treatments and bonding procedures on the tensile bond strength (TBS) of resin composites repaired 6 months after polymerization. Resin composite sticks were aged in distilled water at 37°C for 6 months. They were divided into 12 groups (n = 10) according to the combination of surface treatment/bonding procedures [none, only bur treatment, XP Bond (XPB/Dentsply/DeTrey) with/without bur, AdheSE (A-SE/Ivoclar/Vivadent) with/without bur, Composite Primer (CP/GC) with/without bur, CP after bur and acid-etching, XPB after acid etching and CP with bur, A-SE after bur and CP]. The ultimate tensile bond strength (UTS) of the resin composites was tested in intact but aged specimens. Tensile bond strengths were tested with a universal testing machine (Shimadzu). Data were analyzed using one-way ANOVA and Duncan Multiple Comparisons tests (p < 0.05). All repaired groups showed significantly higher TBS than the group without any sureface treatment (p < 0.05). Four groups resulted in TBS similar to those of intact resin composite UTS: A-SE, A-SE with bur, A-SE after CP with bur, and XPB after acid etching+CP with bur. Bur treatment, silane primer or etch-and-rinse adhesive application alone were not successful in the repair process of aged resin composite, whereas self-etching adhesive alone showed similar performance to the intact specimens. Combined procedures generally showed better performance: A-SE with bur, A-SE after CP with bur, and XPB after acid etching +CP with bur showed TBS similar to those of the intact specimens. It was concluded that bur roughening of the surfaces and rebonding procedures were essential for repairing aged resin composites.

  5. Tensile Properties of Under-Matched Weld Joints for 950 MPa Steel.

    NASA Astrophysics Data System (ADS)

    Yamamoto, Kouji; Arakawa, Toshiaki; Akazawa, Nobuki; Yamamoto, Kousei; Matsuo, Hiroki; Nakagara, Kiyoyuki; Suita, Yoshikazu

    In welding of 950 MPa-class high tensile strength steel, preheating is crucial in order to avoid cold cracks, which, however, eventually increases welding deformations. One way to decrease welding deformations is lowering preheating temperature by using under-matched weld metal. Toyota and others clarify that although breaking elongation can decrease due to plastic constraint effect under certain conditions, static tensile of under-matched weld joints is comparable to that of base metal. However, there has still been no report about joint static tensile of under-matched weld joints applied to 950 MPa-class high tensile strength steel. In this study, we aim to research tensile strength and fatigue strength of under-matched weld joints applied to 950 MPa-class high tensile steel.

  6. Experimental Study on Tensile Properties of a Novel Porous Metal Fiber/Powder Sintered Composite Sheet

    PubMed Central

    Zou, Shuiping; Wan, Zhenping; Lu, Longsheng; Tang, Yong

    2016-01-01

    A novel porous metal fiber/powder sintered composite sheet (PMFPSCS) is developed by sintering a mixture of a porous metal fiber sintered sheet (PMFSS) and copper powders with particles of a spherical shape. The characteristics of the PMFPSCS including its microstructure, sintering density and porosity are investigated. A uniaxial tensile test is carried out to study the tensile behaviors of the PMFPSCS. The deformation and failure mechanisms of the PMFSCS are discussed. Experimental results show that the PMFPSCS successively experiences an elastic stage, hardening stage, and fracture stage under tension. The tensile strength of the PMFPSCS is determined by a reticulated skeleton of fibers and reinforcement of copper powders. With the porosity of the PMFSS increasing, the tensile strength of the PMFPSCS decreases, whereas the reinforcement of copper powders increases. At the elastic stage, the structural elastic deformation is dominant, and at the hardening stage, the plastic deformation is composed of the structural deformation and the copper fibers’ plastic deformation. The fracture of the PMFPSCS is mainly caused by the breaking of sintering joints. PMID:28773833

  7. Effects of Thermomechanical History on the Tensile Behavior of Nitinol Ribbon

    NASA Technical Reports Server (NTRS)

    Lach, Cynthia L.; Turner, Travis L.; Taminger, Karen M.; Shenoy, Ravi N.

    2002-01-01

    Shape memory alloys (SMAs) have enormous potential for a wide variety of applications. A large body of work exists on the characterization of the microstructure and stress-strain behavior of these alloys, Nitinol (NiTi) in particular. However, many attributes of these materials are yet to be fully understood. Previous work at NASA Langley Research Center (LaRC) has included fabrication of hybrid composite specimens with embedded Nitinol actuators and modeling of their thermomechanical behavior. An intensive characterization effort has been undertaken to facilitate fundamental understanding of this alloy and to promote implementation of Nitinol in aerospace applications. Previous work revealed attributes of the Nitinol ribbon that were not easily rationalized with existing data in the literature. In particular, tensile behavior at ambient temperature showed significant dependence on the thermomechanical history prior to testing. The present work is focused on characterizing differences in the microstructure of Nitinol ribbons exposed to four different thermomechanical histories and correlation of the microstructure with tensile properties. Differential scanning calorimetry (DSC) and x-ray diffraction (XRD) analysis were employed to rationalize the microstructures present after exposure to various thermomechanical histories. Three of the Nitinol ribbon conditions were reversible upon heating (in the DSC) through the reverse transformation temperature (A(sub f) to transform the microstructure to austenite. However, the prior thermomechanical conditioning for the Nitinol ribbon that reflected the entire fabrication procedure (4% thermal cycle condition) was found to have an irreversible effect on the microstructure, as it remained unchanged after repeated complete thermal cycles. Tensile tests were conducted to determine the effect of prior thermomechancal conditioning on both the tensile behavior of the Nitinol ribbons and the stress state of the microstructure. The

  8. Effect of Annealing on Microstructure, Texture and Tensile Properties of Twin-Roll Cast AZ31B

    NASA Astrophysics Data System (ADS)

    Masoumi, Mohsen; Zarandi, Faramarz; Pekguleryuz, Mihriban O.

    Twin-roll cast (TRC) AZ31 alloy (Mg-3wt.%Al-1wt.%Zn) was subjected to heat treatment at 420 °C. As a result, the intensity of the original basal texture was reduced considerably. Crystallographic orientation analysis revealed that such a change in the texture is due to particle-stimulated nucleation of new grains with random orientations. The tensile test results indicate that annealing slightly increases ultimate tensile strength (UTS), however, dramatically improves the elongation.

  9. Evaluation of Surface Roughness and Tensile Strength of Base Metal Alloys Used for Crown and Bridge on Recasting (Recycling).

    PubMed

    Agrawal, Amit; Hashmi, Syed W; Rao, Yogesh; Garg, Akanksha

    2015-07-01

    Dental casting alloys play a prominent role in the restoration of the partial dentition. Casting alloys have to survive long term in the mouth and also have the combination of structure, molecules, wear resistance and biologic compatibility. According to ADA system casting alloys were divided into three groups (wt%); high noble, Noble and predominantly base metal alloys. To evaluate the mechanical properties such as tensile strength and surface roughness of the new and recast base metal (nickel-chromium) alloys. Recasting of the base metal alloys derived from sprue and button, to make it reusable has been done. A total of 200 test specimens were fabricated using specially fabricated jig of metal and divided into two groups- 100 specimens of new alloy and 100 specimens of recast alloys, which were tested for tensile strength on universal testing machine and surface roughness on surface roughness tester. Tensile strength of new alloy showed no statistically significant difference (p-value>0.05) from recast alloy whereas new alloy had statistically significant surface roughness (Maximum and Average surface roughness) difference (p-value<0.01) as compared to recast alloy. Within the limitations of the study it is concluded that the tensile strength will not be affected by recasting of nickel-chromium alloy whereas surface roughness increases markedly.

  10. Thermal degradation and tensile strength of sansevieria trifasciata-polypropylene composites

    NASA Astrophysics Data System (ADS)

    Abral, H.; Kenedy, E.

    2015-07-01

    The paper exhibits thermal degradation and tensile strength of Sansevieria Trifasciata (ST) fibers and polypropylene (PP) composites. Thermal degradation of ST fibers PP composites was conducted by using thermogravimetry (TGA) instrument, meanwhile tensile strength of the composite was done by using tensile equipment. The results show that the thermal resistance of ST fibers PP composites was higher than that of virgin PP only. Increases in volume fraction of fibers in the composites enhance the tensile strength. Scanning Electron Microscope (SEM) observation exhibits good interface bonding between ST fibers and PP matrix.

  11. Acousto-Ultrasonic analysis of failure in ceramic matrix composite tensile specimens

    NASA Technical Reports Server (NTRS)

    Kautz, Harold E.; Chulya, Abhisak

    1993-01-01

    Three types of acousto-ultrasonic (AU) measurements, stress-wave factor (SWF), lowest antisymmetric plate mode group velocity (VS), and lowest symmetric plate mode group velocity (VL), were performed on specimens before and after tensile failure. Three different Nicalon fiber architectures with ceramic matrices were tested. These composites were categorized as 1D (unidirectional fiber orientation) SiC/CAS glass ceramic, and 2D and 3D woven SiC/SiC ceramic matrix materials. SWF was found to be degraded after tensile failure in all three material categories. VS was found to be degraded only in the 1D SiC/CAS. VL was difficult to determine on the irregular specimen surfaces but appeared unchanged on all failed specimens. 3D woven specimens with heat-treatment at high temperature exhibited degradation only in SWF.

  12. Characterization of Tensile Deformation in AZ91D Mg Alloy Castings

    NASA Astrophysics Data System (ADS)

    Űnal, Ogün; Tiryakioǧlu, Murat

    AZ91 cast Mg alloy specimens in T4 and T6 tempers have been tested in tension. True stress — true plastic strain relationship has been characterized by evaluating the fits to four constitutive equations. Moreover, work hardening behavior in both tempers has been investigated and how well the four constitutive equation can model this behavior has been tested. The effects of temper and structural quality on tensile properties and work hardening are discussed in the paper.

  13. Capturing tensile size-dependency in polymer nanofiber elasticity.

    PubMed

    Yuan, Bo; Wang, Jun; Han, Ray P S

    2015-02-01

    As the name implies, tensile size-dependency refers to the size-dependent response under uniaxial tension. It defers markedly from bending size-dependency in terms of onset and magnitude of the size-dependent response; the former begins earlier but rises to a smaller value than the latter. Experimentally, tensile size-dependent behavior is much harder to capture than its bending counterpart. This is also true in the computational effort; bending size-dependency models are more prevalent and well-developed. Indeed, many have questioned the existence of tensile size-dependency. However, recent experiments seem to support the existence of this phenomenon. Current strain gradient elasticity theories can accurately predict bending size-dependency but are unable to track tensile size-dependency. To rectify this deficiency a higher-order strain gradient elasticity model is constructed by including the second gradient of the strain into the deformation energy. Tensile experiments involving 10 wt% polycaprolactone nanofibers are performed to calibrate and verify our model. The results reveal that for the selected nanofibers, their size-dependency begins when their diameters reduce to 600 nm and below. Further, their characteristic length-scale parameter is found to be 1095.8 nm. Copyright © 2014 Elsevier Ltd. All rights reserved.

  14. Tensile Properties of Poly (N-vinyl caprolactam) Gels

    NASA Technical Reports Server (NTRS)

    Morgret, Leslie D.; Hinkley, Jeffrey A.

    2004-01-01

    N-vinyl caprolactam was copolymerized with ethylene glycol dimethacrylate using a free-radical initiator in alcohol/water solution. The resulting gels were thermally-responsive in water, undergoing an approximate fivefold reversible volume shrinkage between room temperature and ca. 50 C. Tensile testing showed that the stress-strain behavior was qualitatively different in the collapsed state above the temperature-induced transition. At the higher temperature, gels were stiffer, more ductile, and showed greater time dependence. Implications for the design of gel actuators are briefly discussed.

  15. Application of Gurson–Tvergaard–Needleman Constitutive Model to the Tensile Behavior of Reinforcing Bars with Corrosion Pits

    PubMed Central

    Xu, Yidong; Qian, Chunxiang

    2013-01-01

    Based on meso-damage mechanics and finite element analysis, the aim of this paper is to describe the feasibility of the Gurson–Tvergaard–Needleman (GTN) constitutive model in describing the tensile behavior of corroded reinforcing bars. The orthogonal test results showed that different fracture pattern and the related damage evolution process can be simulated by choosing different material parameters of GTN constitutive model. Compared with failure parameters, the two constitutive parameters are significant factors affecting the tensile strength. Both the nominal yield and ultimate tensile strength decrease markedly with the increase of constitutive parameters. Combining with the latest data and trial-and-error method, the suitable material parameters of GTN constitutive model were adopted to simulate the tensile behavior of corroded reinforcing bars in concrete under carbonation environment attack. The numerical predictions can not only agree very well with experimental measurements, but also simplify the finite element modeling process. PMID:23342140

  16. Correction to the Dynamic Tensile Strength of Ice and Ice-Silicate Mixtures (Lange & Ahrens 1983)

    NASA Astrophysics Data System (ADS)

    Stewart, S. T.; Ahrens, T. J.

    1999-03-01

    We present a correction to the Weibull parameters for ice and ice-silicate mixtures (Lange & Ahrens 1983). These parameters relate the dynamic tensile strength to the strain rate. These data are useful for continuum fracture models of ice.

  17. Post-Impact and Open Hole Tensile Of Kenaf Hybrid Composites

    NASA Astrophysics Data System (ADS)

    Yunus, S.; Salleh, Z.; Masdek, N. R. N. M.; Taib, Y. M.; Azhar, I. I. S.; Hyie, K. M.

    2018-03-01

    Nowadays, kenaf hybrid glass composites has been used for a vast field of study throughout the globe. There are several compositions and orientation of kenaf hybrid glass composites that has been studied. With regards to the study that has been done, this study will be focussing on a 90FG/0/90/90/0/90FG orientation of kenaf hybrid glass composites. Polyester resin is used as a matrix to these hybrid composites. Impacted and open hole specimens were then analyzed through tensile test. All specimens were fabricated by using the cold press hand lay-up technique. The results revealed that the hybrid composites were hardly affected by the impact up to 6J. After 6J the impacted specimens experienced a significant damage for both strength and modulus. The same goes to open hole specimens where the same trend of tensile properties were observed as impacted specimens.

  18. In vitro Comparative Evaluation of Tensile Bond Strength of 6(th), 7(th) and 8(th) Generation Dentin Bonding Agents.

    PubMed

    Kamble, Suresh S; Kandasamy, Baburajan; Thillaigovindan, Ranjani; Goyal, Nitin Kumar; Talukdar, Pratim; Seal, Mukut

    2015-05-01

    Newer dentin bonding agents were developed to improve the quality of composite restoration and to reduce time consumption in its application. The aim of the present study was to evaluate tensile bond strength of 6(th), 7(th) and 8(th) generation bonding agents by in vitro method. Selected 60 permanent teeth were assigned into 20 in each group (Group I: 6(th) generation bonding agent-Adper SE plus 3M ESPE, Group II: 7(th) generation bonding agent-G-Bond GC Corp Japan and Group III: 8(th) generation dentin adhesives-FuturaBond, DC, Voco, Germany). With high-speed diamond disc, coronal dentin was exposed, and selected dentin bonding agents were applied, followed by composite restoration. All samples were saved in saline for 24 h and tensile bond strength testing was done using a universal testing machine. The obtained data were tabulated and statistically analyzed using ANOVA test. The tensile bond strength readings for 6(th) generation bonding agent was 32.2465, for 7(th) generation was 31.6734, and for 8(th)-generation dentine bonding agent was 34.74431. The highest tensile bond strength was seen in 8(th) generation bonding agent compared to 6(th) and 7(th) generation bonding agents. From the present study it can be conclude that 8(th) generation dentine adhesive (Futura DC, Voco, Germany) resulted in highest tensile bond strength compared to 6(th) (Adper SE plus, 3M ESPE) and 7(th) generation (G-Bond) dentin bonding agents.

  19. LGM-30B, Stage II Dissected Motors Test Report,

    DTIC Science & Technology

    1980-07-01

    Relaxation Test Data (Outer Propellant) 29 Table 9, Stress Relaxation Test Data (Inner Propellant) 31 Table 10 , Cohesive Tear Energy Test Data (Outer...Outer) 45 7 Maximum Stress (Inner) 46 8Strain at Rupture (Inner) 47 9 Modulus (Inner) 48 Regression Plot, Low Rate Tensile 10 Maximum Stress (Outer...outer propellants are almost the same. H. TEAR ENERGY TEST: Data from this test period are contained in Tables 10 and 11. Sufficient valid data became

  20. Tensile Fracture of Ductile Materials. M.S. Thesis

    NASA Technical Reports Server (NTRS)

    Pai, D. M.

    1984-01-01

    For brittle materials, circular voids play an important role relative to fracture, intensifing both tensile and compressive stresses. A maximum intensified tensile stress failure criterion applies quite well to brittle materials. An attempt was made to explore the possibility of extending the approach to the tensile fracture of ductile materials. The three dimensional voids that exist in reality are modelled by circular holes in sheet metal. Mathematical relationships are sought between the shape and size of the hole, after the material is plastically deformed, and the amount of deformation induced. Then, the effect of hole shape, size and orientation on the mechanical properties is considered experimentally. The presence of the voids does not affect the ultimate tensile strength of the ductile materials because plastic flow wipes out the stress intensification caused by them. However, the shape and orientation of the defect is found to play an important role in affecting the strain at fracture.

  1. Effect of Thermal Exposure on the Tensile Properties of Aluminum Alloys for Elevated Temperature Service

    NASA Technical Reports Server (NTRS)

    Edahl, Robert A., Jr.; Domack, Marcia

    2004-01-01

    Tensile properties were evaluated for four aluminum alloys that are candidates for airframe applications on high speed transport aircraft. These alloys included the Al-Cu-Mg-Ag alloys C415 and C416 and the Al-Cu-Li-Mg-Ag alloys RX818 and ML377. The Al-Cu-Mg alloys CM001, which was used on the Concorde SST, and 1143, which was modified from the alloy used on the TU144 Russian supersonic aircraft, were tested for comparison. The alloys were subjected to thermal exposure at 200 F, 225 F and 275 F for times up to 30,000 hours. Tensile tests were performed on thermally-exposed and as-received material at -65 F, room temperature, 200 F, 225 F and 275 F. All four candidate alloys showed significant tensile property improvements over CM001 and 1143. Room temperature yield strengths of the candidate alloys were at least 20% greater than for CM001 and 1143, for both the as-received and thermally-exposed conditions. The strength levels of alloy RX818 were the highest of all materials investigated, and were 5-10% higher than for ML377, C415 and C416 for the as-received condition and after 5,000 hours thermal exposure. RX818 was removed from this study after 5,000 hours exposure due to poor fracture toughness performance observed in a parallel study. After 30,000 hours exposure at 200 F and 225 F, the alloys C415, C416 and ML377 showed minor decreases in yield strength, tensile strength and elongation when compared to the as-received properties. Reductions in tensile strength from the as-received values were up to 25% for alloys C415, C416 and ML377 after 15,000 hours exposure at 275 F.

  2. Experimental Investigations on the effect of Additive on the Tensile Properties of Fiber Glass Fabric Lamina

    NASA Astrophysics Data System (ADS)

    Nava Sai Divya, A.; Raghu Kumar, B., Dr; Lakshmi Narayana, G., Dr

    2017-09-01

    The main objective of this work is to investigate the effect of additives on tensile behaviour of fiber glass fabric at lamina level to explore an alternative skin material for the outer body of aerospace applications and machines. This experimental work investigates the effect of silica concentration in epoxy resin lapox L-12 on the tensile properties of glass fabric lamina of 4H-satin weave having 3.6 mm thickness. The lamina was prepared by using hand lay-up method and tests were conducted on it. Various tensile properties values obtained from experimentation were compared for four glass fiber lamina composites fabricated by adding the silica powder to resin bath. The effect of variations in silica concentration (0% SiO2, 5% SiO2, 10% SiO2 and 15% SiO2) on the tensile properties of prepared material revealed that maximum stiffness was obtained at 15% and yield strength at 10% SiO2 concentration in glass fiber lamina. Increasing the silica concentration beyond 10% had led to deterioration in the material properties. The experimentation that was carried out on test specimen was reasonably successful as the effect of silica powder as an additive in glass fiber lamina enhanced the mechanical properties up to certain limit. The underpinning microscopic behaviour at the source of these observations will be investigated in a follow up work.

  3. In Vitro Tensile Strength Study on Suturing Technique and Material.

    PubMed

    González-Barnadas, Albert; Camps-Font, Octavi; Espanya-Grifoll, Dunia; España-Tost, Antoni; Figueiredo, Rui; Valmaseda-Castellón, Eduard

    2017-06-01

    Suture technique and materials are important in preventing complications such as wound dehiscences. The purpose of this study was to determine the tensile strength of different suturing techniques, comparing several materials with different diameters. One hundred sixty sutures were performed using silk, e-PTFE, and 2 types of polyamide (monofilament and Supramid). Ten simple, 10 horizontal mattress, and 10 combinations of the two stitches were performed with 4-0 gauge of each material. Additionally, 10 simple sutures were performed with the 5-0 gauge of each material. The maximum tensile force resisted by each suture was recorded. When 5 mm of traction was applied, the polyamide monofilament resisted significantly better without untying or breaking compared with Supramid or silk, while the e-PTFE was superior to all the others. However, the force when e-PTFE 4-0 sutures untied or broke was lower than for either type of polyamide. The combined technique withstood a significantly higher tensile force before unknotting or breaking than did the simple and mattress stitches. The 5-0 gauges of silk and both types of polyamide showed lower tensile strengths than the 4-0 materials. Among the 5-0 sutures, Supramid showed a higher tensile strength than silk. The combined suture technique possessed greater tensile strength than did a simple or a horizontal mattress suture, and e-PTFE 4-0 withstood more traction without untying or breaking than did all the other materials, although at a lower tensile force. With the exception of e-PTFE, 4-0 sutures had greater tensile strength than did 5-0 sutures.

  4. Effect of soldering techniques and gap distance on tensile strength of soldered Ni-Cr alloy joint

    PubMed Central

    Lee, Sang-Yeob

    2010-01-01

    PURPOSE The present study was intended to evaluate the effect of soldering techniques with infrared ray and gas torch under different gap distances (0.3 mm and 0.5 mm) on the tensile strength and surface porosity formation in Ni-Cr base metal alloy. MATERIALS AND METHODS Thirty five dumbbell shaped Ni-Cr alloy specimens were prepared and assigned to 5 groups according to the soldering method and the gap distance. For the soldering methods, gas torch (G group) and infrared ray (IR group) were compared and each group was subdivided by corresponding gap distance (0.3 mm: G3 and IR3, 0.5 mm: G5, IR5). Specimens of the experimental groups were sectioned in the middle with a diamond disk and embedded in solder blocks according to the predetermined distance. As a control group, 7 specimens were prepared without sectioning or soldering. After the soldering procedure, a tensile strength test was performed using universal testing machine at a crosshead speed 1 mm/min. The proportions of porosity on the fractured surface were calculated on the images acquired through the scanning electronic microscope. RESULTS Every specimen of G3, G5, IR3 and IR5 was fractured on the solder joint area. However, there was no significant difference between the test groups (P > .05). There was a negative correlation between porosity formation and tensile strength in all the specimens in the test groups (P < .05). CONCLUSION There was no significant difference in ultimate tensile strength of joints and porosity formations between the gas-oxygen torch soldering and infrared ray soldering technique or between the gap distance of 0.3 mm and 0.5 mm. PMID:21264189

  5. Cubical Mass-Spring Model design based on a tensile deformation test and nonlinear material model.

    PubMed

    San-Vicente, Gaizka; Aguinaga, Iker; Tomás Celigüeta, Juan

    2012-02-01

    Mass-Spring Models (MSMs) are used to simulate the mechanical behavior of deformable bodies such as soft tissues in medical applications. Although they are fast to compute, they lack accuracy and their design remains still a great challenge. The major difficulties in building realistic MSMs lie on the spring stiffness estimation and the topology identification. In this work, the mechanical behavior of MSMs under tensile loads is analyzed before studying the spring stiffness estimation. In particular, the performed qualitative and quantitative analysis of the behavior of cubical MSMs shows that they have a nonlinear response similar to hyperelastic material models. According to this behavior, a new method for spring stiffness estimation valid for linear and nonlinear material models is proposed. This method adjusts the stress-strain and compressibility curves to a given reference behavior. The accuracy of the MSMs designed with this method is tested taking as reference some soft-tissue simulations based on nonlinear Finite Element Method (FEM). The obtained results show that MSMs can be designed to realistically model the behavior of hyperelastic materials such as soft tissues and can become an interesting alternative to other approaches such as nonlinear FEM.

  6. Incorporation of chlorhexidine diacetate in provisional cements: antimicrobial activity against Streptococcus mutans and the effect on tensile strength in vitro.

    PubMed

    Lewinstein, I; Zenziper, E; Block, J; Kfir, A

    2012-11-01

    To test the antibacterial capacities and tensile strengths of three commercially available provisional cements to which chlorhexidine diacetate was added and compare them to the same unmodified cements. Sixty cylindrical samples were prepared from either three noneugenol provisional cements or the same cements modified by the addition of chlorhexidine diacetate at 7.5% w/w, with a total of 360 samples. The cements tested included Tempbond NE, Rely X Temp NE and Freegenol. Forty-eight samples from each cement were aged in saline that was replaced twice a week for up to 96 days. Twelve of these samples were removed at either 1, 15, 30 or 96 days and assessed for antibacterial properties against Streptococcus mutans with an agar diffusion test. Twelve samples of each cement, with and without chlorhexidine diacetate, were also tested 7 days after the initial setting for their tensile strength using a diametrical tensile strength test applied with an Instron machine. The results were analysed using either one-way or three-way anova. The addition of chlorhexidine diacetate resulted in provisional cements with antibacterial properties that persisted through ageing in saline for up to 96 days. The addition of chlorhexidine did not reduce the diametrical strength of the cements. The addition of chlorhexidine diacetate to provisional cements rendered all three cements antibacterial against S. mutans and this activity was maintained even after prolonged ageing of the cements, without compromising their tensile strength at 7 days. © 2012 International Endodontic Journal.

  7. Tensile failure properties of the perinatal, neonatal, and pediatric cadaveric cervical spine.

    PubMed

    Luck, Jason F; Nightingale, Roger W; Song, Yin; Kait, Jason R; Loyd, Andre M; Myers, Barry S; Bass, Cameron R Dale

    2013-01-01

    Biomechanical tensile testing of perinatal, neonatal, and pediatric cadaveric cervical spines to failure. To assess the tensile failure properties of the cervical spine from birth to adulthood. Pediatric cervical spine biomechanical studies have been few due to the limited availability of pediatric cadavers. Therefore, scaled data based on human adult and juvenile animal studies have been used to augment the limited pediatric cadaver data. Despite these efforts, substantial uncertainty remains in our understanding of pediatric cervical spine biomechanics. A total of 24 cadaveric osteoligamentous head-neck complexes, 20 weeks gestation to 18 years, were sectioned into segments (occiput-C2 [O-C2], C4-C5, and C6-C7) and tested in tension to determine axial stiffness, displacement at failure, and load-to-failure. Tensile stiffness-to-failure (N/mm) increased by age (O-C2: 23-fold, neonate: 22 ± 7, 18 yr: 504; C4-C5: 7-fold, neonate: 71 ± 14, 18 yr: 509; C6-C7: 7-fold, neonate: 64 ± 17, 18 yr: 456). Load-to-failure (N) increased by age (O-C2: 13-fold, neonate: 228 ± 40, 18 yr: 2888; C4-C5: 9-fold, neonate: 207 ± 63, 18 yr: 1831; C6-C7: 10-fold, neonate: 174 ± 41, 18 yr: 1720). Normalized displacement at failure (mm/mm) decreased by age (O-C2: 6-fold, neonate: 0.34 ± 0.076, 18 yr: 0.059; C4-C5: 3-fold, neonate: 0.092 ± 0.015, 18 yr: 0.035; C6-C7: 2-fold, neonate: 0.088 ± 0.019, 18 yr: 0.037). Cervical spine tensile stiffness-to-failure and load-to-failure increased nonlinearly, whereas normalized displacement at failure decreased nonlinearly, from birth to adulthood. Pronounced ligamentous laxity observed at younger ages in the O-C2 segment quantitatively supports the prevalence of spinal cord injury without radiographic abnormality in the pediatric population. This study provides important and previously unavailable data for validating pediatric cervical spine models, for evaluating current scaling techniques and animal surrogate models, and for the development

  8. A silicon microwire under a three-dimensional anisotropic tensile stress

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Ji, Xiaoyu; Poilvert, Nicolas; Liu, Wenjun

    Three-dimensional tensile stress, or triaxial tensile stress, is difficult to achieve in a material. We present the investigation of an unusual three-dimensional anisotropic tensile stress field and its influence on the electronic properties of a single crystal silicon microwire. The microwire was created by laser heating an amorphous silicon wire deposited in a 1.7 μm silica glass capillary by high pressure chemical vapor deposition. Tensile strain arises due to the thermal expansion mismatch between silicon and silica. Synchrotron X-ray micro-beam Laue diffraction (μ-Laue) microscopy reveals that the three principal strain components are +0.47% (corresponding to a tensile stress of +0.7more » GPa) along the fiber axis and nearly isotropic +0.02% (corresponding to a tensile stress of +0.3 GPa) in the cross-sectional plane. This effect was accompanied with a reduction of 30 meV in the band gap energy of silicon, as predicted by the density-functional theory calculations and in close agreement with energy-dependent photoconductivity measurements. While silicon has been explored under many stress states, this study explores a stress state where all three principal stress components are tensile. Given the technological importance of silicon, the influence of such an unusual stress state on its electronic properties is of fundamental interest.« less

  9. Chain Ends and the Ultimate Tensile Strength of Polyethylene Fibers

    NASA Astrophysics Data System (ADS)

    O'Connor, Thomas C.; Robbins, Mark O.

    Determining the tensile yield mechanisms of oriented polymer fibers remains a challenging problem in polymer mechanics. By maximizing the alignment and crystallinity of polyethylene (PE) fibers, tensile strengths σ ~ 6 - 7 GPa have been achieved. While impressive, first-principal calculations predict carbon backbone bonds would allow strengths four times higher (σ ~ 20 GPa) before breaking. The reduction in strength is caused by crystal defects like chain ends, which allow fibers to yield by chain slip in addition to bond breaking. We use large scale molecular dynamics (MD) simulations to determine the tensile yield mechanism of orthorhombic PE crystals with finite chains spanning 102 -104 carbons in length. The yield stress σy saturates for long chains at ~ 6 . 3 GPa, agreeing well with experiments. Chains do not break but always yield by slip, after nucleation of 1D dislocations at chain ends. Dislocations are accurately described by a Frenkel-Kontorova model, parametrized by the mechanical properties of an ideal crystal. We compute a dislocation core size ξ = 25 . 24 Å and determine the high and low strain rate limits of σy. Our results suggest characterizing such 1D dislocations is an efficient method for predicting fiber strength. This research was performed within the Center for Materials in Extreme Dynamic Environments (CMEDE) under the Hopkins Extreme Materials Institute at Johns Hopkins University. Financial support was provided by Grant W911NF-12-2-0022.

  10. Effect of Strain Rate on Joint Strength and Failure Mode of Lead-Free Solder Joints

    NASA Astrophysics Data System (ADS)

    Lin, Jian; Lei, Yongping; Fu, Hanguang; Guo, Fu

    2018-03-01

    In surface mount technology, the Sn-3.0Ag-0.5Cu solder joint has a shorter impact lifetime than a traditional lead-tin solder joint. In order to improve the impact property of SnAgCu lead-free solder joints and identify the effect of silver content on tensile strength and impact property, impact experiments were conducted at various strain rates on three selected SnAgCu based solder joints. It was found that joint failure mainly occurred in the solder material with large plastic deformation under low strain rate, while joint failure occurred at the brittle intermetallic compound layer without any plastic deformation at a high strain rate. Joint strength increased with the silver content in SnAgCu alloys in static tensile tests, while the impact property of the solder joint decreased with increasing silver content. When the strain rate was low, plastic deformation occurred with failure and the tensile strength of the Sn-3.0Ag-0.5Cu solder joint was higher than that of Sn-0.3Ag-0.7Cu; when the strain rate was high, joint failure mainly occurred at the brittle interface layer and the Sn-0.3Ag-0.7Cu solder joint had a better impact resistance with a thinner intermetallic compound layer.

  11. Acoustic emission monitoring of low velocity impact damage in graphite/epoxy laminates during tensile loading

    NASA Technical Reports Server (NTRS)

    Parker, Bradford H.

    1992-01-01

    An acoustic emission (AE) system was set up in a linear location data acquisition mode to monitor the tensile loading of eight-ply quasi-isotropic graphite/epoxy specimens containing low velocity impact damage. The impact damage was induced using an instrumented drop weight tower. During impact, specimens were supported by either an aluminum plate or a membrane configuration. Cross-sectional examinations revealed that the aluminum plate configuration resulted in primarily matrix cracking and back surface fiber failure. The membrane support resulted in only matrix cracking and delamination damage. Penetrant enhanced radiography and immersion ultrasonics were used in order to assess the amount of impact damage in each tensile specimen. During tensile loading, AE reliably detected and located the damage sites which included fiber failure. All specimens with areas of fiber breakage ultimately failed at the impact site. AE did not reliably locate damage which consisted of only delaminations and matrix cracking. Specimens with this type of damage did not ultimately fail at the impact site. In summary, AE demonstrated the ability to increase the reliability of structural proof tests; however, the successful use of this technique requires extensive baseline testing.

  12. Prediction of Tensile Behavior of UHSFRC Considering the Flow Field in the Placing Dominated by Shear Flow.

    PubMed

    Moon, Joon-Shik; Kang, Su-Tae

    2018-01-26

    Considering the case of fabricating a UHSFRC (ultra-high strength fiber-reinforced concrete) beam with the method of one end placing and self-flowing to the other end, it was intended to simulate the variation of the fiber orientation distribution according to the flow distance and the variation of the resultant tensile behaviors. Then the validity of the simulation approach was shown by comparing the simulated results with experimental ones. A three-point bending test with a notched beam was adopted for the experiment and a finite element analysis was performed to obtain the simulated results for the bending test considering the flow-dependent tensile behavior of the UHSFRC. From the simulation for the fiber orientation distribution according to the flow distance, it could be found that the major change in the fiber orientation distribution took place within a short flow distance and most of the fibers became nearly aligned to the flow direction. After some flow distance, there was a not-so-remarkable variation in the fiber orientation distribution that could influence the tensile behavior of the composite. For this flow region, the consistent flexural test results, regardless of flow distance, demonstrate the reliability of the simulation.

  13. Stiff and tough: a comparative study on the tensile properties of shark skin.

    PubMed

    Creager, Shelby B; Porter, Marianne E

    2018-02-01

    In sharks, the skin is a biological composite with mineralized denticles embedded within a collagenous matrix. Swimming performance is enhanced by the dermal denticles on the skin, which have drag reducing properties produced by regional morphological variations and changes in density along the body. We used mechanical testing to quantify the effect of embedded mineralized denticles on the quasi-static tensile properties of shark skin to failure in four coastal species. We investigated regional differences in denticle density and skin properties by dissecting skin from the underlying fascia and muscle at 10 anatomical landmarks. Hourglass-shaped skin samples were extracted in the cranial to caudal orientation. Denticle density was quantified and varied significantly among both regions and species. We observed the greatest denticle densities in the cranial region of the body for the bonnethead, scalloped hammerhead, and bull sharks. Skin samples were then tested in tension until failure, stress strain curves were generated, and mechanical properties calculated. We found significant species and region effects for all three tensile mechanical properties. We report the greatest ultimate tensile strength, stiffness, and toughness near the cranial and lateral regions of the body for all 4 of the coastal species. We also report that denticle density increases with skin stiffness but decreases with toughness. Copyright © 2017 Elsevier GmbH. All rights reserved.

  14. A study on the tensile properties of silicone rubber/polypropylene fibers/silica hybrid nanocomposites.

    PubMed

    Ziraki, Sahar; Zebarjad, Seyed Mojtaba; Hadianfard, Mohammad Jafar

    2016-04-01

    Metacarpophalangeal joint implants have been usually made of silicone rubber. In the current study, silica nano particles and polypropylene fibers were added to silicone rubber to improve silicone properties. The effect of the addition of silica nano particles and polypropylene fibers on the tensile behavior of the resultant composites were investigated. Composite samples with different content of PP fibers and Silica nano particles (i. e. 0, 1 and 2wt%) as well as the hybrid composite of silicone rubber with 1wt% SiO2 and 1wt% PP fiber were prepared. Tensile tests were done at constant cross head speed. To study the body fluid effect on the mechanical properties of silicone rubber composites, samples soaked in simulated body fluid (SBF) at 37°C were also tested. The morphology of the samples were studied by scanning electron microscope. Results of analysis revealed that an increase in PP fibers and silica nano particles content to 2wt%, increases the tensile strength of silicone rubber of about 75% and 42% respectively. It was found out that the strength of the samples decreases after being soaked in simulated body fluid, though composites with PP fibers as the reinforcement showed less property degradation. Copyright © 2016 Elsevier Ltd. All rights reserved.

  15. A Simplified Micromechanical Modeling Approach to Predict the Tensile Flow Curve Behavior of Dual-Phase Steels

    NASA Astrophysics Data System (ADS)

    Nanda, Tarun; Kumar, B. Ravi; Singh, Vishal

    2017-11-01

    Micromechanical modeling is used to predict material's tensile flow curve behavior based on microstructural characteristics. This research develops a simplified micromechanical modeling approach for predicting flow curve behavior of dual-phase steels. The existing literature reports on two broad approaches for determining tensile flow curve of these steels. The modeling approach developed in this work attempts to overcome specific limitations of the existing two approaches. This approach combines dislocation-based strain-hardening method with rule of mixtures. In the first step of modeling, `dislocation-based strain-hardening method' was employed to predict tensile behavior of individual phases of ferrite and martensite. In the second step, the individual flow curves were combined using `rule of mixtures,' to obtain the composite dual-phase flow behavior. To check accuracy of proposed model, four distinct dual-phase microstructures comprising of different ferrite grain size, martensite fraction, and carbon content in martensite were processed by annealing experiments. The true stress-strain curves for various microstructures were predicted with the newly developed micromechanical model. The results of micromechanical model matched closely with those of actual tensile tests. Thus, this micromechanical modeling approach can be used to predict and optimize the tensile flow behavior of dual-phase steels.

  16. The evaluation of ordinary Portland cement concrete subject to elevated temperatures in conjunction with acoustic emission and splitting tensile test

    NASA Astrophysics Data System (ADS)

    Su, Yu-Min; Hou, Tsung-Chin; Chen, Guan-Ying; Hou, Ping-Ni

    2017-04-01

    The research objective was to evaluate Ordinary Portland Cement concrete subject to various elevated temperatures. Single OPC concrete mixture with water to cementitious (w/c) equal to 0.45 was proportioned. Concrete specimens were cast and placed in the curing tank in which water was saturated with calcium hydroxide. After ninety days of moist-cure, three elevated temperatures, namely 300, 600, and 900-°C, were carried out upon hardened concrete specimens. Furthermore, two post-damaged curing conditions were executed to recover damaged concrete specimens: one was to recure under 23°C with 50% humidity in a controlled environmental chamber and the other was to recure in the same curing tank. Acoustic emission apparatus coupled with the splitting tensile test was utilized and found able to assess damaged concrete. Before concrete subject to elevated temperatures, the development of indirect tensile strength versus displacement diagram fit well with the tendency of AE energy release. It was found there was a large amount of AE energy released when stress and displacement diagram developed about 40-50%. As such could be identified as the onset of first fracture and the plain concrete generally exhibited a quasi-brittle fracture with two major series of AE energy dissipations; however when concrete specimens were subject to elevated temperatures, the damaged concrete specimens displayed neither fracture pattern nor the "double-hump" AE energy dissipation in comparison with those of plain concrete.

  17. Time-frequency analysis of acoustic emission signals generated by the Glass Fibre Reinforced Polymer Composites during the tensile test

    NASA Astrophysics Data System (ADS)

    Świt, G.; Adamczak, A.; Krampikowska, A.

    2017-10-01

    Fibre reinforced polymer composites are currently dominating in the composite materials market. The lack of detailed knowledge about their properties and behaviour in various conditions of exposure under load significantly limits the broad possibilities of application of these materials. Occurring and accumulation of defects in material during the exploitation of the construction lead to the changes of its technical condition. The necessity to control the condition of the composite is therefore justified. For this purpose, non-destructive method of acoustic emission can be applied. This article presents an example of application of acoustic emission method based on time analysis and time-frequency analysis for the evaluation of the progress of the destructive processes and the level of degradation of glass fibre reinforced composite tapes that were subject to tensile testing.

  18. Effect of water storage and surface treatments on the tensile bond strength of IPS Empress 2 ceramic.

    PubMed

    Salvio, Luciana A; Correr-Sobrinho, Lourenço; Consani, Simonides; Sinhoreti, Mário A C; de Goes, Mario F; Knowles, Jonathan C

    2007-01-01

    The aim of this study was to evaluate the effect of water storage (24 hours and 1 year) on the tensile bond strength between the IPS Empress 2 ceramic and Variolink II resin cement under different superficial treatments. One hundred and eighty disks with diameters of 5.3 mm at the top and 7.0 mm at the bottom, and a thickness of 2.5 mm were made, embedded in resin, and randomly divided into six groups: Groups 1 and 4 = 10% hydrofluoric acid for 20 seconds; Groups 2 and 5 = sandblasting for 5 seconds with 50 microm aluminum oxide; and Groups 3 and 6 = sandblasting for 5 seconds with 100 microm aluminum oxide. Silane was applied on the treated ceramic surfaces, and the disks were bonded into pairs with adhesive resin cement. The samples of Groups 1 to 3 were stored in distilled water at 37 degrees C for 24 hours, and Groups 4 to 6 were stored for 1 year. The samples were subjected to a tensile strength test in an Instron universal testing machine at a crosshead speed of 1.0 mm/min, until failure. The data were submitted to analysis of variance and Tukey's test (5%). The means of the tensile bond strength of Groups 1, 2, and 3 (15.54 +/- 4.53, 10.60 +/- 3.32, and 7.87 +/- 2.26 MPa) for 24-hour storage time were significantly higher than those observed for the 1-year storage (Groups 4, 5, and 6: 10.10 +/- 3.17, 6.34 +/- 1.06, and 2.60 +/- 0.41 MPa). The surface treatments with 10% hydrofluoric acid (15.54 +/- 4.53 and 10.10 +/- 3.17 MPa) showed statistically higher tensile bond strengths compared with sandblasting with 50 microm(10.60 +/- 3.32 and 6.34 +/- 1.06 MPa) and 100 microm (7.87 +/- 2.26 and 2.60 +/- 0.41 MPa) aluminum oxide for the storage time 24 hours and 1 year. Storage time significantly decreased the tensile bond strength for both ceramic surface treatments. The application of 10% hydrofluoric acid resulted in stronger tensile bond strength values than those achieved with aluminum oxide.

  19. Fracture toughness, tensile and stress corrosion cracking properties of Alloy 600, Alloy 690 and their welds in water

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Brown, C.M.; Mills, W.J.

    1996-10-01

    The fracture toughness and tensile properties of Alloy 600, Alloy 690 and their welds, EN82H and EN52, were characterized in 54 and 338 C water with an elevated hydrogen content. Results were compared with air data to evaluate the effect of low and high temperature water on mechanical properties. In addition, the stress corrosion cracking (SCC) behavior of EN82H and EN52 welds was evaluated in 360 C water with high hydrogen. Elastic-plastic J{sub c} fracture toughness testing revealed that the fracture resistance of all test materials was exceptionally high in 54 and 338 C air and 338 C water, demonstratingmore » that fracture properties were essentially unaffected by the high temperature water environment. In 54 C water, however, J{sub c} values for EN82H and EN52 welds were reduced by an order of magnitude, and Alloy 690 showed a five-fold decrease in J{sub c}. Tensile properties for all test materials were essentially unaffected by the water environment, except for the total elongation for EN82H welds which was significantly reduced in 54 C water. At a strain rate of 5 x 10{sup 6} sec{sup {minus}1} in low temperature water, there appears to be sufficient time for environmental interactions to restrict ductility in EN82H welds. Constant-load testing of precracked weld specimens in 360 C water resulted in extensive intergranular SCC in EN82H welds loaded to K{sub I} levels between 35 and 55 MPa {radical}m, whereas no SCC occurred in EN52 welds under comparable test conditions.« less

  20. Effects of NaBF4 + NaF on the Tensile and Impact Properties of Al-Si-Mg-Fe Alloys

    NASA Astrophysics Data System (ADS)

    Chen, Zongning; Wang, Tongmin; Zhao, Yufei; Zheng, Yuanping; Kang, Huijun

    2015-05-01

    NaBF4 + NaF were found to play three roles, i.e., Fe-eliminator, grain refiner, and eutectic modifier, in treating A356 alloy with a high Fe content. The joint effects led to significant improvement in both tensile and impact properties of thus treated alloy. The multiple reactions between the NaBF4 + NaF and Al-Si-Mg-Fe system are suggested to form Fe2B, AlB2, and Na in the melt, as per thermodynamic analysis. The three are responsible for Fe removal, grain refinement, and eutectic modification, respectively. When NaBF4 and NaF are mixed in weight ratio of 1:1, an optimum addition rate is in the range between 1.0 and 2.0 wt pct for treating AlSi7Mg0.3Fe0.65 alloy, based on the results of tensile and impact tests. Excessive addition of the salt may deteriorate the mechanical properties of the alloy, basically owing to overmodification of Si and contamination of salt inclusions.

  1. Tensile bond strength of silicone-based soft denture liner to two chemically different denture base resins after various surface treatments.

    PubMed

    Akin, Hakan; Tugut, Faik; Guney, Umit; Kirmali, Omer; Akar, Turker

    2013-01-01

    This study evaluated the effect of various surface treatments on the tensile bond strength of a silicone-based soft denture liner to two chemically different denture base resins, heat-cured polymethyl methacrylate (PMMA), and light-activated urethane dimethacrylate or Eclipse denture base resin. PMMA test specimens were fabricated and relined with a silicone-based soft denture liner (group AC). Eclipse test specimens were prepared according to the manufacturer's recommendation. Before they were relined with a silicone-based soft denture liner, each received one of three surface treatments: untreated (control, group EC), Eclipse bonding agent applied (group EB), and laser-irradiated (group EL). Tensile bond strength tests (crosshead speed = 5 mm/min) were performed for all specimens, and the results were analyzed using the analysis of variance followed by Tukey's test (p = 0.05). Eclipse denture base and PMMA resins presented similar bond strengths to the silicone-based soft denture liner. The highest mean force was observed in group EL specimens, and the tensile bond strengths in group EL were significantly different (p < 0.05) from those in the other groups.

  2. The effects of tensile preloads on the impact response of carbon/epoxy laminates

    NASA Technical Reports Server (NTRS)

    Nettles, Alan; Daniel, Vince; Branscomb, Caleb

    1995-01-01

    The effects of tensile preloads on the tension-after-impact (TAI) strength of composite laminates of IM7/8551-7 were examined. A failure threshold curve was first determined so the most informative values for preload/impact energy combinations could be determined. The impact tests were instrumented so maximum load of impact, as well as several other parameters could be measured. The elastic response data indicate that as the tensile preload is increased, the maximum load of impact also increases. The damage data show that at low impact energies, the damage/failure is an 'all-or-nothing' event but at higher impact energies, a region of preload values exists where the coupons could sustain damage, yet not fail catastrophically.

  3. Effects of Strain Rate and Temperature on the Mechanical Properties of Medium Manganese Steels

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Rana, Radhakanta; Matlock, David K; Speer, John G

    2016-11-16

    The effects of temperature (-60 to 100 °C) and strain rate (0.002 to 0.2 s-1) on the properties of Al-alloyed 7 and 10 wt-% Mn steels containing 34.8 and 57.3 vol-% austenite respectively were evaluated by tensile tests in isothermal liquid baths. The tensile strengths of both medium Mn steels increased with a decrease in temperature owing to the decreased austenite stability with a decrease in temperature. At lower temperatures the strength of the 10MnAl steel was highest, a consequence of the higher strain hardening rate caused by more austenite transformation to martensite with deformation. The resulting properties are assessedmore » with a consideration of the effects of strain rate and deformation on adiabatic heating which was observed to be as high as 95o C.« less

  4. Effect of Incorporation of Antifungal Agents on the Ultimate Tensile Strength of Temporary Soft Denture Liners.

    PubMed

    Neppelenbroek, Karin Hermana; Lima, Jozely Francisca Mello; Hotta, Juliana; Galitesi, Lucas Lulo; Almeida, Ana Lucia Pompéia Fraga; Urban, Vanessa Migliorini

    2018-02-01

    To investigate the ultimate tensile strength of temporary soft denture liners modified by minimum inhibitory concentrations (MICs) of antifungal agents for Candida albicans biofilm (SC5314) determined in previous microbiological research. Dumbbell-shaped specimens (n = 7) with a central cross-sectional area of 6 × 3 × 33 mm were produced by Softone and Trusoft, without (control) or with incorporation of drugs in powder form at MICs for C. albicans biofilm (per g of material powder): nystatin (0.032 g), chlorhexidine diacetate (0.064 g), ketoconazole (0.128 g), miconazole (0.256 g), and itraconazole (0.256 g). After plasticization, specimens were immersed in distilled water at 37°C for 24 hours, 7 or 14 days, and then tested in tension in a universal testing machine at 40 mm/min. Data of tensile strength (MPa) and elongation percentage (%) were submitted to 3-way ANOVA and Tukey's test (α = 0.05). At the end of 14 days, the tensile strength for both materials was significantly lower in the groups modified by miconazole and itraconazole compared to the other groups (p < 0.0001), which showed no significant difference between them (p > 0.05). After 7 and 14 days in water, miconazole and itraconazole added into both materials resulted in significantly lower elongation percentages compared to the other antifungal agents and control (p < 0.0001), which were similar to each other (p > 0.05). The addition of the nystatin, chlorhexidine, and ketoconazole at MICs for C. albicans biofilm resulted in no harmful effects on the tensile strength and elongation percentage of the temporary soft denture liner materials up to 14 days. © 2017 by the American College of Prosthodontists.

  5. Evaluation of Surface Roughness and Tensile Strength of Base Metal Alloys Used for Crown and Bridge on Recasting (Recycling)

    PubMed Central

    Hashmi, Syed W.; Rao, Yogesh; Garg, Akanksha

    2015-01-01

    Background Dental casting alloys play a prominent role in the restoration of the partial dentition. Casting alloys have to survive long term in the mouth and also have the combination of structure, molecules, wear resistance and biologic compatibility. According to ADA system casting alloys were divided into three groups (wt%); high noble, Noble and predominantly base metal alloys. Aim To evaluate the mechanical properties such as tensile strength and surface roughness of the new and recast base metal (nickel-chromium) alloys. Materials and Methods Recasting of the base metal alloys derived from sprue and button, to make it reusable has been done. A total of 200 test specimens were fabricated using specially fabricated jig of metal and divided into two groups- 100 specimens of new alloy and 100 specimens of recast alloys, which were tested for tensile strength on universal testing machine and surface roughness on surface roughness tester. Results Tensile strength of new alloy showed no statistically significant difference (p-value>0.05) from recast alloy whereas new alloy had statistically significant surface roughness (Maximum and Average surface roughness) difference (p-value<0.01) as compared to recast alloy. Conclusion Within the limitations of the study it is concluded that the tensile strength will not be affected by recasting of nickel-chromium alloy whereas surface roughness increases markedly. PMID:26393194

  6. A preliminary characterization of the tensile and fatigue behavior of tungsten-fiber/Waspaloy-matrix composite

    NASA Technical Reports Server (NTRS)

    Corner, Ralph E.; Lerch, Brad A.

    1992-01-01

    A microstructural study and a preliminary characterization of the room temperature tensile and fatigue behavior of a continuous, tungsten fiber, Waspaloy-matrix composite was conducted. A heat treatment was chosen that would allow visibility of planar slip if it occurred during deformation, but would not allow growth of the reaction zone. Tensile and fatigue tests showed that the failed specimens contained transverse cracks in the fibers. The cracks that occurred in the tensile specimen were observed at the fracture surface and up to approximately 4.0 mm below the fracture surface. The crack spacing remained constant along the entire length of the cracked fibers. Conversely, the cracks that occurred in the fatigue specimen were only observed in the vicinity of the fracture surface. In instances where two fiber cracks occurred in the same plane, the matrix often necked between the two cracked fibers. Large groups of slip bands were generated in the matrix near the fiber cracks. Slip bands in the matrix of the tensile specimen were also observed in areas where there were no fiber cracks, at distances greater than 4 mm from the fracture surface. This suggests that the matrix plastically flows before fiber cracking occurs.

  7. Estimation of Ultimate Tensile Strength of dentin Using Finite Element Analysis from Endodontically Treated Tooth

    NASA Astrophysics Data System (ADS)

    Sinthaworn, S.; Puengpaiboon, U.; Warasetrattana, N.; Wanapaisarn, S.

    2018-01-01

    Endodontically treated teeth were simulated by finite element analysis in order to estimate ultimate tensile strength of dentin. Structures of the endodontically treated tooth cases are flared root canal, restored with different number of fiber posts {i.e. resin composite core without fiber post (group 1), fiber post No.3 with resin composite core (group 2) and fiber post No.3 accessory 2 fiber posts No.0 with resin composite core (group 3)}. Elastic modulus and Poisson’s ratio of materials were selected from literatures. The models were loaded by the average fracture resistances load of each groups (group 1: 361.80 N, group 2: 559.46 N, group 3: 468.48 N) at 135 degree angulation in respect to the longitudinal axis of the teeth. The stress analysis and experimental confirm that fracture zone is at dentin area. To estimate ultimate tensile strength of dentin, trial and error of ultimate tensile strength were tested to obtain factor of safety (FOS) equal to 1.00. The result reveals that ultimate tensile strength of dentin of group 1, 2, 3 are 38.89, 30.96, 37.19 MPa, respectively.

  8. Comparative evaluation of tensile bond strength and microleakage of conventional glass ionomer cement, resin modified glass ionomer cement and compomer: An in vitro study.

    PubMed

    Rekha, C Vishnu; Varma, Balagopal; Jayanthi

    2012-07-01

    The purpose of this study was to evaluate and compare the tensile bond strength and microleakage of Fuji IX GP, Fuji II LC, and compoglass and to compare bond strength with degree of microleakage exhibited by the same materials. Occlusal surfaces of 96 noncarious primary teeth were ground perpendicular to long axis of the tooth. Preparations were distributed into three groups consisting of Fuji IX GP, Fuji II LC and Compoglass. Specimens were tested for tensile bond strength by mounting them on Instron Universal Testing Machine. Ninety-six primary molars were treated with Fuji IX GP, Fuji II LC, and compoglass on box-only prepared proximal surface. Samples were thermocycled, stained with dye, sectioned, and scored for microleakage under stereomicroscope. ANOVA and Bonferrani correction test were done for comparisons. Pearson Chi-square test and regression analysis were done to assess the association between the parameters. Compoglass showed highest tensile strength and Fuji II LC showed least microleakage. There was a significant difference between the three groups in tensile strength and microleakage levels. The correlation between tensile strength and microleakage level in each group showed that there was a significant negative correlation only in Group 3. Fuji II LC and compoglass can be advocated in primary teeth because of their superior physical properties when compared with Fuji IX GP.

  9. A Study of Tensile Flow and Work-Hardening Behavior of Alloy 617

    NASA Astrophysics Data System (ADS)

    Singh, Aditya Narayan; Moitra, A.; Bhaskar, Pragna; Dasgupta, Arup; Sasikala, G.; Bhaduri, A. K.

    2018-04-01

    The simple power relationship σ = Κɛ p n satisfactorily expresses the tensile flow behavior of many metals and alloys in their uniform plastic strain regime. However, many FCC materials with low stacking fault energy have opposed such power law relationship. Alloy 617, an age-hardenable Ni-based superalloy is also observed not to obey the simple power law relationship neither in its solution-treated nor in its aged conditions. Various flow relationships were used to obtain the best fit for the tensile data, and different relationships were identified for the different aged conditions. The work-hardening rate (θ) demonstrates three distinct regions for all aged conditions, and there is an obvious change in the trend of θ versus σ. In the initial portion, θ decreases rapidly followed by a gradual increase in the second stage and again a decrease in its third stage is perceived in the Alloy 617. These three-stage characteristics are attributed to a commonly known precipitate, γ': Ni3(Ti, Al) which evolves during aging treatment and well recognized under transmission electron microscopy (TEM) observation. TEM results also reveal a slight degree of coarsening in γ' over aging. The tensile flow and the work-hardening behavior are well correlated with other microstructural evolution during the aging treatments.

  10. Mechanical properties of graphene nanoribbons under uniaxial tensile strain

    NASA Astrophysics Data System (ADS)

    Yoneyama, Kazufumi; Yamanaka, Ayaka; Okada, Susumu

    2018-03-01

    Based on the density functional theory with the generalized gradient approximation, we investigated the mechanical properties of graphene nanoribbons in terms of their edge shape under a uniaxial tensile strain. The nanoribbons with armchair and zigzag edges retain their structure under a large tensile strain, while the nanoribbons with chiral edges are fragile against the tensile strain compared with those with armchair and zigzag edges. The fracture started at the cove region, which corresponds to the border between the zigzag and armchair edges for the nanoribbons with chiral edges. For the nanoribbons with armchair edges, the fracture started at one of the cove regions at the edges. In contrast, the fracture started at the inner region of the nanoribbons with zigzag edges. The bond elongation under the tensile strain depends on the mutual arrangement of covalent bonds with respect to the strain direction.

  11. An Examination of Radiation Induced Tensile Failure of Stressed and Unstressed Polymer Films Flown on MISSE-6

    NASA Technical Reports Server (NTRS)

    Miller, Sharon K.; Sechkar, Edward A.

    2012-01-01

    Thin film polymers are used in many spacecraft applications for thermal control (multilayer insulation and sunshields), as lightweight structural members (solar array blankets, inflatable/deployable structures) and have been proposed for propulsion (solar sails). Polymers in these applications are often under a tensile load and are directly exposed to the space environment, therefore it is important to understand the effect of stress in combination with the environment on the durability of these polymer films. The purpose of the Polymer Film Tensile Experiment, flown as part of Materials International Space Station Experiment 6 (MISSE 6), was to expose a variety of polymer films to the low Earth orbital environment under both relaxed and tension conditions. This paper describes the results of post flight tensile testing of these samples.

  12. Spectroscopic analysis of radiation-generated changes in tensile properties of a polyetherimide film

    NASA Technical Reports Server (NTRS)

    Long, E. R., Jr.; Long, S. A. T.

    1985-01-01

    The effects of electron radiation on Ultem, a polyetherimide were studied for doses from 2 x 10 to the 9th power to 6 x 10 to the 9th power rad. Specimens were studied for tensile property testing and for electron paramagnetic resonance and infrared spectroscopic measurements of molecular structure. A Faraday cup design and a method for remote temperature measurement were developed. The spectroscopic data show that radiation caused dehydrogenation of methyl groups, rupture of main-chain ether linkage, and opening of imide rings, all to form radicals and indicate that the so-formed atomic hydrogen attached to phenyl radicals, but not to phenoxyl radicals, which would have formed hydroxyls. The observed decays of the radiation-generated phenoxyl, gem-dimethyl, and carbonyl radicals were interpreted as a combining of the radicals to form crosslinking. This crosslinking is the probable cause of the major reduction in the elongation of the tensile specimens after irradiation. Subsequent classical solubility tests indicate that the irradiation caused massive crosslinking.

  13. INFLUENCE OF THE FINAL TEMPERATURE OF INVESTMENT HEALTING ON THE TENSILE STRENGTH AND VICKERS HARDNESS OF CP TI AND TI-6AL-4V ALLOY

    PubMed Central

    Oliveira, Pedro César Garcia; Adabo, Gelson Luis; Ribeiro, Ricardo Faria; da Rocha, Sicknan Soares; Ávila, Fabiano Araújo; do Valle, Accácio Lins

    2007-01-01

    The aim of the work was to evaluate the influence of the temperature of investment healting on the tensile strength and Vickers hardness of CP Ti and Ti-6Al-4V alloy casting. Were obtained for the tensile strength test dumbbell rods that were invested in the Rematitan Plus investment and casting in the Discovery machine cast. Thirty specimens were obtained, fiftten to the CP Titanium and fifteen to the Ti-6Al-4V alloy, five samples to each an of the three temperatures of investment: 430°C (control group), 480°C and 530°C. The tensile test was measured by means of a universal testing machine, MTS model 810, at a strain of 1.0 mm/min. After the tensile strenght test the specimens were secctioned, embedded and polished to hardness measurements, using a Vickers tester, Micromet 2100. The means values to tensile tests to the temperatures 430°C, 480 and 530: CP Ti (486.1 – 501.16 – 498.14 –mean 495.30 MPa) and Ti-6Al-4V alloy (961.33 – 958.26 – 1005.80 – mean 975.13 MPa) while for the Vickers hardness the values were (198.06, 197.85, 202.58 – mean 199.50) and (352.95, 339.36, 344.76 – mean 345.69), respectively. The values were submitted to Analysis of Variance (ANOVA) and Tukey,s Test that indicate differences significant only between the materials, but not between the temperature, for both the materias. It was conclued that increase of the temperature of investment its not chance the tensile strength and the Vickers hardness of the CP Titanium and Ti-6Al-4V alloy. PMID:19089099

  14. Tensile bond strength of filled and unfilled adhesives to dentin.

    PubMed

    Braga, R R; Cesar, P F; Gonzaga, C C

    2000-04-01

    To determine the tensile bond strength of three filled and two unfilled adhesives applied to bovine dentin. Fragments of the labial dentin of bovine incisors were embedded in PVC cylinders with self-cure acrylic resin, and ground flat using 200 grit and 600 grit sandpaper. The following adhesive systems were tested (n=10): Prime & Bond NT, Prime & Bond NT dual cure, Prime & Bond 2.1, OptiBond Solo and Single Bond. A 3 mm-diameter bonding surface was delimited using a perforated adhesive tape. After etching with 37% phosphoric acid and adhesive application, a resin-based composite truncated cone (TPH, shade A3) was built. Tensile test was performed after 24 hrs storage in distilled water at 37 degrees C. Failure mode was accessed using a x10 magnification stereomicroscope. Weibull statistical analysis revealed significant differences in the characteristic strength between Single Bond and Prime & Bond NT dual cure, and between Single Bond and Prime & Bond 2.1. The Weibull parameter (m) was statistically similar among the five groups. Single Bond and Prime & Bond NT showed areas of dentin cohesive failure in most of the specimens. For OptiBond Solo, Prime & Bond NT dual cure and Prime & Bond 2.1 failure was predominantly adhesive.

  15. Investigation of Tensile Creep of a Normal Strength Overlay Concrete.

    PubMed

    Drexel, Martin; Theiner, Yvonne; Hofstetter, Günter

    2018-06-12

    The present contribution deals with the experimental investigation of the time-dependent behavior of a typical overlay concrete subjected to tensile stresses. The latter develop in concrete overlays, which are placed on existing concrete structures as a strengthening measure, due to the shrinkage of the young overlay concrete, which is restrained by the substrate concrete. Since the tensile stresses are reduced by creep, creep in tension is investigated on sealed and unsealed specimens, loaded at different concrete ages. The creep tests as well as the companion shrinkage tests are performed in a climatic chamber at constant temperature and constant relative humidity. Since shrinkage depends on the change of moisture content, the evolution of the mass water content is determined at the center of each specimen by means of an electrolytic resistivity-based system. Together with the experimental results for compressive creep from a previous study, a consistent set of time-dependent material data, determined for the same composition of the concrete mixture and on identical specimens, is now available. It consists of the hygral and mechanical properties, creep and shrinkage strains for both sealed and drying conditions, the respective compliance functions, and the mass water contents in sealed and unsealed, loaded and load-free specimens.

  16. High-temperature tensile-hold crack-growth behavior of HASTELLOY® X alloy compared to HAYNES® 188 and HAYNES® 230® alloys

    NASA Astrophysics Data System (ADS)

    Lee, S. Y.; Lu, Y. L.; Liaw, P. K.; Choo, H.; Thompson, S. A.; Blust, J. W.; Browning, P. F.; Bhattacharya, A. K.; Aurrecoechea, J. M.; Klarstrom, D. L.

    2008-03-01

    The creep-fatigue crack-growth tests of HASTELLOY® X alloy were carried out at the temperatures of 649°C, 816°C, and 927°C in laboratory air. The experiments were conducted under a constant stress-intensity-factor-range (Δ K) control mode with a R-ratio of 0.05. In the constant Δ K tests, a Δ K of 27.5 MPa sqrt{m} and a triangular waveform with a frequency of 0.333 Hz were used. Various tensile hold times at the maximum load were imposed to study fatigue and creep-fatigue interactions. Crack lengths were measured by a direct current potential drop method. In this paper, effects of hold time and temperature on the crack-growth rates are discussed. Furthermore, the crack-growth rates of the HASTELLOY® X alloy are compared to those of the HAYNES® 188 and HAYNES® 230® superalloys.

  17. Relationships between tensile strength, morphology and crystallinity of treated kenaf bast fibers

    NASA Astrophysics Data System (ADS)

    Sosiati, H.; Rohim, Ar; Ma`arif, Triyana, K.; Harsojo

    2013-09-01

    Surface treatments on kenaf bast fibers were carried out with steam, alkali and a combination of steam-alkali. To verify and gain an understanding of their inter-relationship, tensile strength, surface morphology and crystallinity of treated and raw fibers were characterized. Tensile strength of fibers was measured with a universal tensile machine (UTM), crystallinity was estimated using X-ray diffraction (XRD) and Fourier transformation infrared (FTIR) spectroscopy, and surface morphology was examined by scanning electron microscopy (SEM). Tensile strength of the treated fibers was higher than that of the raw fiber. Tensile strength increased after steam treatment and was further improved by alkali treatment, but slightly reduced after steam treatment followed by alkalization. Increase of concentration of alkali tended to increase tensile strength. Differences in tensile strength of the treated fibers are discussed in relation to the changes in surface morphology and crystallinity. Understanding of these relationships may provide direction towards the goal of producing better performance of natural fiber composites.

  18. Covalent Crosslinking of Carbon Nanotube Materials for Improved Tensile Strength

    NASA Technical Reports Server (NTRS)

    Baker, James S.; Miller, Sandi G.; Williams, Tiffany A.; Meador, Michael A.

    2013-01-01

    Carbon nanotubes have attracted much interest in recent years due to their exceptional mechanical properties. Currently, the tensile properties of bulk carbon nanotube-based materials (yarns, sheets, etc.) fall far short of those of the individual nanotube elements. The premature failure in these materials under tensile load has been attributed to inter-tube sliding, which requires far less force than that needed to fracture individual nanotubes.1,2 In order for nanotube materials to achieve their full potential, methods are needed to restrict this tube-tube shear and increase inter-tube forces.Our group is examining covalent crosslinking between the nanotubes as a means to increase the tensile properties of carbon nanotube materials. We are working with multi-walled carbon nanotube (MWCNT) sheet and yarn materials obtained from commercial sources. Several routes to functionalize the nanotubes have been examined including nitrene, aryl diazonium, and epoxide chemistries. The functional nanotubes were crosslinked through small molecule or polymeric bridges. Additionally, electron beam irradiation induced crosslinking of the non-functional and functional nanotube materials was conducted. For example, a nanotube sheet material containing approximately 3.5 mol amine functional groups exhibited a tensile strength of 75 MPa and a tensile modulus of 1.16 GPa, compared to 49 MPa and 0.57 GPa, respectively, for the as-received material. Electron beam irradiation (2.2x 1017 ecm2) of the same amine-functional sheet material further increased the tensile strength to 120 MPa and the modulus to 2.61 GPa. This represents approximately a 150 increase in tensile strength and a 360 increase in tensile modulus over the as-received material with only a 25 increase in material mass. Once we have optimized the nanotube crosslinking methods, the performance of these materials in polymer matrix composites will be evaluated.

  19. Study of root tensile strength of softwood and hardwood tree species: Implications for slope stability

    NASA Astrophysics Data System (ADS)

    Esmaiili, Marzieh; Abdi, Ehsan; Jafary, Mohammad; Majnounian, Baris

    2017-04-01

    Landslides are known as one of the major natural hazards and often incurring economics and human life losses. The role of tree roots in slope stability is very important, especially when human lives and infrastructure are at risk. The anchorage of roots and improvement of slope stability mainly depend on specific properties of root network systems, such as tensile strength. These properties of the roots which govern the degree of reinforcement are different among tree species. Although, many studies have been conducted about plant biotechnical properties of species, yet there is lack of knowledge on comparing root systems of softwood and hardwood tree species for similar site conditions. Therefore this study was conducted to assess the tensile strength of the root system of Picea abies (softwood species) and Fraxinus excelsior (hardwood species) planted on two forested hillslopes. To this aim, single root specimens were sampled for each species and their tensile strength were then measured in laboratory using a computer controlled Instron Universal Testing Machine. According to the results root tensile strength tends to decrease with diameter according to a power law for both species. Based on analysis of covariance (ANCOVA), a significant difference has been observed in the tensile strength between the two studied species. Also the results showed that the value of mean root tensile strength for Picea abies (19.31 ± 2.64 MPa) was much more than that of Fraxinus excelsior (16.98 ± 1.01 MPa) within all root diameter classes. The data presented in this study may expand the knowledge of biotechnical properties of Picea abies and Fraxinus excelsior, as biomaterial for soil bioengineering.

  20. Tensile strength and corrosion resistance of brazed and laser-welded cobalt-chromium alloy joints.

    PubMed

    Zupancic, Rok; Legat, Andraz; Funduk, Nenad

    2006-10-01

    The longevity of prosthodontic restorations is often limited due to the mechanical or corrosive failure occurring at the sites where segments of a metal framework are joined together. The purpose of this study was to determine which joining method offers the best properties to cobalt-chromium alloy frameworks. Brazed and 2 types of laser-welded joints were compared for their mechanical and corrosion characteristics. Sixty-eight cylindrical cobalt-chromium dental alloy specimens, 35 mm long and 2 mm in diameter, were cast. Sixteen specimens were selected for electrochemical measurements in an artificial saliva solution and divided into 4 groups (n=4). In the intact group, the specimens were left as cast. The specimens of the remaining 3 groups were sectioned at the center, perpendicular to the long-axis, and were subsequently rejoined by brazing (brazing group) or laser welding using an X- or I-shaped joint design (X laser and I laser groups, respectively). Another 16 specimens were selected for electrochemical measurements in a more acidic artificial saliva solution. These specimens were also divided into 4 groups (n=4) as described above. Electrochemical impedance spectroscopy and potentiodynamic polarization were used to assess corrosion potentials, breakdown potentials, corrosion current densities, total impedances at lowest frequency, and polarization charge-transfer resistances. The remaining 36 specimens were used for tensile testing. They were divided into 3 groups in which specimen pairs (n=6) were joined by brazing or laser welding to form 70-mm-long cylindrical rods. The tensile strength (MPa) was measured using a universal testing machine. Differences between groups were analyzed using 1-way analysis of variance (alpha=.05). The fracture surfaces and corrosion defects were examined with a scanning electron microscope. The average tensile strength of brazed joints was 792 MPa and was significantly greater (P<.05) than the tensile strength of both types of

  1. On the Interplay Between Adhesion Strength and Tensile Properties of Thermal Spray Coated Laminates—Part II: Low-Velocity Thermal Spray Coatings

    NASA Astrophysics Data System (ADS)

    Luo, Xiaotao; Smith, Gregory M.; Sampath, Sanjay

    2018-02-01

    In this two-part study, uniaxial tensile testing was used to evaluate coating/substrate bonding and compared with traditional ASTM C633 bond pull test results for thermal spray (TS) coated steel laminates. In Part I, the rationale, methodology, and applicability of the test to high-velocity TS coatings were demonstrated. In this Part II, the method was investigated for low-velocity TS processes (air plasma spray and arc spray) on equivalent materials. Ni and Ni-5wt.%Al coatings were deposited on steel substrates with three different roughness levels and tested using both uniaxial tensile and ASTM C633 methods. The results indicate the uniaxial tensile approach provides useful information about the nature of the coating/substrate bonding and goes beyond the traditional bond pull test in providing insightful information on the load sharing processes across the interface. Additionally, this proposed methodology alleviates some of the longstanding shortcomings and potentially reduces error associated with the traditional ASTM C633 test. The mechanisms governing the load transfer between the substrate and the coating were investigated, and the influence of Al in the coating material evaluated.

  2. Thermal properties of graphene under tensile stress

    NASA Astrophysics Data System (ADS)

    Herrero, Carlos P.; Ramírez, Rafael

    2018-05-01

    Thermal properties of graphene display peculiar characteristics associated to the two-dimensional nature of this crystalline membrane. These properties can be changed and tuned in the presence of applied stresses, both tensile and compressive. Here, we study graphene monolayers under tensile stress by using path-integral molecular dynamics (PIMD) simulations, which allows one to take into account quantization of vibrational modes and analyze the effect of anharmonicity on physical observables. The influence of the elastic energy due to strain in the crystalline membrane is studied for increasing tensile stress and for rising temperature (thermal expansion). We analyze the internal energy, enthalpy, and specific heat of graphene, and compare the results obtained from PIMD simulations with those given by a harmonic approximation for the vibrational modes. This approximation turns out to be precise at low temperatures, and deteriorates as temperature and pressure are increased. At low temperature, the specific heat changes as cp˜T for stress-free graphene, and evolves to a dependence cp˜T2 as the tensile stress is increased. Structural and thermodynamic properties display non-negligible quantum effects, even at temperatures higher than 300 K. Moreover, differences in the behavior of the in-plane and real areas of graphene are discussed, along with their associated properties. These differences show up clearly in the corresponding compressibility and thermal expansion coefficient.

  3. Tensile properties of candidate structural materials for high power spallation sources at high helium contents

    NASA Astrophysics Data System (ADS)

    Jung, P.; Henry, J.; Chen, J.

    2005-08-01

    Low activation 9%Cr martensitic steels EUROFER97, pure tantalum, and low carbon austenitic stainless steel 316L were homogeneously implanted with helium to concentrations up to 5000 appm at temperatures from 70 °C to 400 °C. The specimens were tensile tested at room temperature and at the respective implantation temperatures. In all materials the helium caused an increased in strength and reduction in ductility, with both changes being generally larger at lower implantation and testing temperatures. After implantation some work hardening was retained in 316L and in tantalum, while it almost completely disappeared in EUROFER97. After tensile testing, fracture surfaces were analysed by scanning electron microscopy (SEM). Implantation caused reduction of necking, but up to concentrations of 2500 appm He fracture surface still showed transgranular ductile appearance. Completely brittle intergranular fracture was observed in tantalum at 9000 appm He and is also expected for EUROFER97 at this concentration, according to previous results on similar 9%Cr steels.

  4. Accelerated Stress-Corrosion Testing

    NASA Technical Reports Server (NTRS)

    1986-01-01

    Test procedures for accelerated stress-corrosion testing of high-strength aluminum alloys faster and provide more quantitative information than traditional pass/fail tests. Method uses data from tests on specimen sets exposed to corrosive environment at several levels of applied static tensile stress for selected exposure times then subsequently tensile tested to failure. Method potentially applicable to other degrading phenomena (such as fatigue, corrosion fatigue, fretting, wear, and creep) that promote development and growth of cracklike flaws within material.

  5. Tensile Characterization of Injection-Molded Fuzzy Glass Fiber/Nylon Composite Material

    DTIC Science & Technology

    2016-05-01

    enhanced reinforcement ( CER ) in a nylon matrix. A majority of the masterbatch CER material research is focused on electromagnetic shielding applications...however, the CER system, with the CNT network fixed to the host fiber, provides a novel approach of minimizing CNT agglomeration. Tensile specimens are...injection molded with varying weight percentages of CER to evaluate effect of the reinforcement on the mechanical properties. Tension testing showed

  6. Mechanical characterization of polymers and composites with a servohydraulic high-speed tensile tester

    NASA Astrophysics Data System (ADS)

    Béguelin, Ph.; Barbezat, M.; Kausch, H. H.

    1991-12-01

    This study is concerned with the measurement of the mechanical behaviour of polymers and composites at intermediate strain rates. It illustrates with two examples, the application of a high speed servohydraulic testing machine and a newly designed optical extensometer. In the first part of the study, the dynamic nature of high speed tensile testing with servohydraulic apparatus is discussed, and a damping technique is proposed. In the second part, this technique has been applied to the measurement of the tensile properties of annealed and unannealed neat PEEK at strain rates between 3 × 10^{-2} and 2,4 × 10^2 s^{-1}. Both materials show increased yield stress and drawing stress with increasing strain rate. However, annealed specimens have been shown to exhibit superior mechanical properties. In the third part, mode I delamination tests have been performed on unidirectional IM6/PEEK composites at nominal strain rates between 1 × 10^{-6} and 8 × 10^{-1} s^{-1}. At the higher velocities the analysis is performed by means of FFT filtering. A moderate reduction in interlaminar fracture toughness was found with increasing loading rate. Cette étude aborde la mesure des propriétés mécaniques des polymères et composites soumis à des vitesses de déformation moyennes. Elle illustre au travers de deux exemples l'utilisation d'une machine d'essais servo-hydraulique à grande vitesse. Elle présente également un capteur optique d'extensométrie de conception nouvelle. Dans la première partie de l'étude, la nature vibratoire des essais de traction à vitesse élevée réalisés sur une machine servo-hydraulique est discutée, et une technique d'amortissement est proposée. Dans une deuxième partie, cette technique est appliquée à l'étude des propriétés en traction du PEEK non recuit et recuit dans le domaine des vitesses de déformation de 3 × 10^{-2} à 2,4 × 10^2 s^{-1}. Les résultats montrent un accroissement systématique de la contrainte au seuil

  7. Modelling of Dynamic Rock Fracture Process with a Rate-Dependent Combined Continuum Damage-Embedded Discontinuity Model Incorporating Microstructure

    NASA Astrophysics Data System (ADS)

    Saksala, Timo

    2016-10-01

    This paper deals with numerical modelling of rock fracture under dynamic loading. For this end, a combined continuum damage-embedded discontinuity model is applied in finite element modelling of crack propagation in rock. In this model, the strong loading rate sensitivity of rock is captured by the rate-dependent continuum scalar damage model that controls the pre-peak nonlinear hardening part of rock behaviour. The post-peak exponential softening part of the rock behaviour is governed by the embedded displacement discontinuity model describing the mode I, mode II and mixed mode fracture of rock. Rock heterogeneity is incorporated in the present approach by random description of the rock mineral texture based on the Voronoi tessellation. The model performance is demonstrated in numerical examples where the uniaxial tension and compression tests on rock are simulated. Finally, the dynamic three-point bending test of a semicircular disc is simulated in order to show that the model correctly predicts the strain rate-dependent tensile strengths as well as the failure modes of rock in this test. Special emphasis is laid on modelling the loading rate sensitivity of tensile strength of Laurentian granite.

  8. Plastic Stress-strain Relations for 75S-T6 Aluminum Alloy Subjected to Biaxial Tensile Stresses

    NASA Technical Reports Server (NTRS)

    Marin, Joseph; Ulrich, B H; Hughes, W P

    1951-01-01

    In this investigation, the material tested was a 75S-T6 aluminum alloy and the stresses were essentially biaxial and tensile. The biaxial tensile stresses were produced in a specially designed testing machine by subjecting a thin-walled tubular specimen to axial tension and internal pressure. Plastic stress-strain relations for various biaxial stress conditions were obtained using a clip-type SR-4 strain gage. Three types of tests were made: Constant-stress-ratio tests, variable-stress-ratio tests, and special tests. The constant-stress-ratio test results gave control data and showed the influence of biaxial stresses on the yield, fracture, and ultimate strength of the material. By means of the variable-stress-ratio tests, it is possible to determine whether there is any significant difference between the flow and deformation type of theory. Finally, special tests were conducted to check specific assumptions made in the theories of plastic flow. The constant-stress-ratio tests show that the deformation theory based on the octahedral, effective; or significant stress-strain relations is in approximate agreement with the test results. The variable-stress-ratio tests show that both the deformation and flow theory are in equally good agreement with the test results.

  9. A new model of reaction-driven cracking: fluid volume consumption and tensile failure during serpentinization

    NASA Astrophysics Data System (ADS)

    Eichenbaum-Pikser, J. M.; Spiegelman, M. W.; Kelemen, P. B.; Wilson, C. R.

    2013-12-01

    Reactive fluid flow plays an important role in a wide range of geodynamic processes, such as melt migration, formation of hydrous minerals on fault surfaces, and chemical weathering. These processes are governed by the complex coupling between fluid transport, reaction, and solid deformation. Reaction-driven cracking is a potentially critical feedback mechanism, by which volume change associated with chemical reaction drives fracture in the surrounding rock. It has been proposed to play a role in both serpentinization and carbonation of peridotite, motivating consideration of its application to mineral carbon sequestration. Previous studies of reactive cracking have focused on the increase in solid volume, and as such, have considered failure in compression. However, if the consumption of fluid is considered in the overall volume budget, the reaction can be net volume reducing, potentially leading to failure in tension. To explore these problems, we have formulated and solved a 2-D model of coupled porous flow, reaction kinetics, and elastic deformation using the finite element model assembler TerraFERMA (Wilson et al, G3 2013 submitted). The model is applied to the serpentinization of peridotite, which can be reasonably approximated as the transfer of a single reactive component (H2O) between fluid and solid phases, making it a simple test case to explore the process. The behavior of the system is controlled by the competition between the rate of volume consumption by the reaction, and the rate of volume replacement by fluid transport, as characterized by a nondimensional parameter χ, which depends on permeability, reaction rate, and the bulk modulus of the solid. Large values of χ correspond to fast fluid transport relative to reaction rate, resulting in a low stress, volume replacing regime. At smaller values of χ, fluid transport cannot keep up with the reaction, resulting in pore fluid under-pressure and tensile solid stresses. For the range of χ relevant

  10. Tensile strength of glass fiber posts submitted to different surface treatments.

    PubMed

    Faria, Maria Isabel A; Gomes, Érica Alves; Messias, Danielle Cristine; Silva Filho, João Manoel; Souza Filho, Celso Bernardo; Paulino, Silvana Maria

    2013-01-01

    The aim of this in vitro study was to evaluate the tensile strength of glass fiber posts submitted to different surface treatments. Forty-eight maxillary canines had their crowns sectioned and root canals endodontically treated. The roots were embedded in acrylic resin and distributed into 3 groups according to the surface treatment: Group I: the posts were treated with silane agent for 30 s and adhesive; Group II: the posts were cleaned with alcohol before treatment with silane agent and adhesive; Group III: the posts were submitted to conditioning with 37% phosphoric acid for 30 s before treatment with silane agent and adhesive. Each group was divided into 2 subgroups for adhesive polymerization or not before insertion into the canal: A - adhesive was not light cured and B - adhesive was light cured. All posts were cemented with Panavia F and the samples were subjected to tensile strength test in a universal testing machine at crosshead speed of 1 mm/min. Data were submitted to one-way ANOVA and Tukey's test at 5% significance level. There was statistically significant difference (p<0.01) only between group GIII-B and groups GI-A and GI-B. No significant difference was found among the other groups (p>0.05). It was concluded that the products used for cleaning the posts influenced the retention regardless of adhesive light curing.

  11. Effect of elevated temperature on the tensile strength of Napier/glass-epoxy hybrid reinforced composites

    NASA Astrophysics Data System (ADS)

    Ridzuan, M. J. M.; Majid, M. S. Abdul; Afendi, M.; Firdaus, A. Z. Ahmad; Azduwin, K.

    2017-11-01

    The effects of elevated temperature on the tensile strength of Napier/glass-epoxy hybrid reinforced composites and its morphology of fractured surfaces are discussed. Napier/glass-epoxy hybrid reinforced composites were fabricated by using vacuum infusion method by arranging Napier fibres in between sheets of woven glass fibres. Napier and glass fibres were laminated with estimated volume ratios were 24 and 6 vol. %, respectively. The epoxy resin was used as matrix estimated to 70 vol. %. Specimens were tested to failure under tension at a cross-head speed of 1 mm/min using Universal Testing Machine (Instron) with a load cell 100 kN at four different temperatures of RT, 40°C, 60°C and 80°C. The morphology of fractured surface of hybrid composites was investigated by field emission scanning electron microscopy. The result shows reduction in tensile strength at elevated temperatures. The increase in the temperature activates the process of diffusion, and generates critical stresses which cause the damage at first-ply or at the centre of the hybrid plate, as a result lower the tensile strength. The observation of FESEM images indicates that the fracture mode is of evolution of localized damage, from fibre/matrix debonding, matric cracking, delamination and fibre breakage.

  12. Testing Machine for Biaxial Loading

    NASA Technical Reports Server (NTRS)

    Demonet, R. J.; Reeves, R. D.

    1985-01-01

    Standard tensile-testing machine applies bending and tension simultaneously. Biaxial-loading test machine created by adding two test fixtures to commercial tensile-testing machine. Bending moment applied by substrate-deformation fixture comprising yoke and anvil block. Pneumatic tension-load fixture pulls up on bracket attached to top surface of specimen. Tension and deflection measured with transducers. Modified test apparatus originally developed to load-test Space Shuttle surface-insulation tiles and particuarly important for composite structures.

  13. Dynamic Tensile Experimental Techniques for Geomaterials: A Comprehensive Review

    NASA Astrophysics Data System (ADS)

    Heard, W.; Song, B.; Williams, B.; Martin, B.; Sparks, P.; Nie, X.

    2018-01-01

    This review article is dedicated to the Dynamic Behavior of Materials Technical Division for celebrating the 75th anniversary of the Society for Experimental Mechanics (SEM). Understanding dynamic behavior of geomaterials is critical for analyzing and solving engineering problems of various applications related to underground explosions, seismic, airblast, and penetration events. Determining the dynamic tensile response of geomaterials has been a great challenge in experiments due to the nature of relatively low tensile strength and high brittleness. Various experimental approaches have been made in the past century, especially in the most recent half century, to understand the dynamic behavior of geomaterials in tension. In this review paper, we summarized the dynamic tensile experimental techniques for geomaterials that have been developed. The major dynamic tensile experimental techniques include dynamic direct tension, dynamic split tension, and spall tension. All three of the experimental techniques are based on Hopkinson or split Hopkinson (also known as Kolsky) bar techniques and principles. Uniqueness and limitations for each experimental technique are also discussed.

  14. Carbon nanotube bundles with tensile strength over 80 GPa.

    PubMed

    Bai, Yunxiang; Zhang, Rufan; Ye, Xuan; Zhu, Zhenxing; Xie, Huanhuan; Shen, Boyuan; Cai, Dali; Liu, Bofei; Zhang, Chenxi; Jia, Zhao; Zhang, Shenli; Li, Xide; Wei, Fei

    2018-05-14

    Carbon nanotubes (CNTs) are one of the strongest known materials. When assembled into fibres, however, their strength becomes impaired by defects, impurities, random orientations and discontinuous lengths. Fabricating CNT fibres with strength reaching that of a single CNT has been an enduring challenge. Here, we demonstrate the fabrication of CNT bundles (CNTBs) that are centimetres long with tensile strength over 80 GPa using ultralong defect-free CNTs. The tensile strength of CNTBs is controlled by the Daniels effect owing to the non-uniformity of the initial strains in the components. We propose a synchronous tightening and relaxing strategy to release these non-uniform initial strains. The fabricated CNTBs, consisting of a large number of components with parallel alignment, defect-free structures, continuous lengths and uniform initial strains, exhibit a tensile strength of 80 GPa (corresponding to an engineering tensile strength of 43 GPa), which is far higher than that of any other strong fibre.

  15. Effect of implanted helium on tensile properties and hardness of 9% Cr martensitic stainless steels

    NASA Astrophysics Data System (ADS)

    Jung, P.; Henry, J.; Chen, J.; Brachet, J.-C.

    2003-05-01

    Hundred micrometer thick specimens of 9% Cr martensitic steels EM10 and T91 were homogeneously implanted with He 4 to concentrations up to 0.5 at.% at temperatures from 150 to 550 °C. The specimens were tensile tested at room temperature and at the respective implantation temperatures. Subsequently the fracture surfaces were analysed by scanning electron microscopy and some of the specimens were examined in an instrumented hardness tester. The implanted helium caused hardening and embrittlement which both increased with increasing helium content and with decreasing implantation temperature. Fracture surfaces showed intergranular brittle appearance with virtually no necking at the highest implantation doses, when implanted below 250 °C. The present tensile results can be scaled to tensile data after irradiation in spallation sources on the basis of helium content but not on displacement damage. An interpretation of this finding by microstructural examination is given in a companion paper [J. Nucl. Mater., these Proceedings].

  16. Tensile bond strength between auto-polymerized acrylic resin and acrylic denture teeth treated with MF-MA solution.

    PubMed

    Thongrakard, Ticha; Wiwatwarrapan, Chairat

    2016-08-01

    This study evaluated the effect of chemical surface treatment using methyl formate-methyl acetate (MF-MA) solution on the tensile bond strength between acrylic denture teeth and auto-polymerized acrylic resin. Seventy maxillary central incisor acrylic denture teeth for each of three different brands (Yamahachi New Ace; Major Dent; Cosmo HXL) were embedded with incisal edge downwards in auto-polymerized resin in polyethylene pipes and ground with silicone carbide paper on their ridge lap surfaces. The teeth of each brand were divided into seven groups (n=10): no surface treatment (control group), MF-MA solution at a ratio of 25:75 (v/v) for 15 seconds, 30 seconds, 60 seconds, 120 seconds, 180 seconds, and MMA for 180 seconds. Auto-polymerized acrylic resin (Unifast Trad) was applied to the ground surface and polymerized in a pressure cooker. A tensile strength test was performed with a universal testing machine. Statistical analysis of the results was performed using two-way analysis of variance (ANOVA) and post-hoc Dunnett T3 test (α=.05). The surface treatment groups had significantly higher mean tensile bond strengths compared with the control group (P<.05) when compared within the same brand. Among the surface treatment groups of each brand, there were no significantly different tensile bond strengths between the MF-MA groups and the MMA 180 second group (P>.05), except for the Yamahachi New Ace MF-MA 180-second group (P<.05). 15-second MF-MA solution can be an alternative chemical surface treatment for repairing a denture base and rebonding acrylic denture teeth with auto-polymerized acrylic resin, for both conventional and cross-linked teeth.

  17. Effect of Ca and RE additions on microstructures and tensile properties of AZ31 alloys

    NASA Astrophysics Data System (ADS)

    Fu, Li; Le, Qichi; Tang, Yan; Sun, Jingying; Jia, Yonghui; Song, Zetian

    2018-05-01

    Microstructures and tensile properties of AZ31 magnesium alloys with the same amount of Ca and RE (Gd + La) additions are investigated. The results show that Al2Ca new phases form after adding Ca elements, Al2Gd and Al11La3 new phases form after adding Gd and La elements, and formations of Al-Ca and Al-RE phases could decrease Mg17Al12 phases and refine grains. Al2Ca and Al11La3 phases are crushed into granules because of severe deformation during hot extrusion, while Al2Gd phases are not. Room temperature (TR) and 150 °C (T150°C) tensile tests results reveal that both AZ31-1.5Ca and AZ31-1.5RE as-extruded alloys exhibit superior comprehensive tensile properties when compared to AZ31 as-extruded alloy, however, AZ31-1.5Ca as-extruded alloy could be a better choice in view of the costs. Textures images of as-extruded alloys indicate that 1.5 wt% Ca and RE additions affects little on textures of AZ31 as-extruded alloy, therefore, morphologies of second phases and average grain sizes are the leading cause of tensile properties of as-extruded alloys.

  18. Dynamic Tensile Strength of Low Temperature Ice and Kuiper Belt Size Distributions

    NASA Astrophysics Data System (ADS)

    Ahrens, Thomas J.; Fat'yanov, O. V.; Engelhardt, H.; Fraser, W. C.

    2009-09-01

    We model mutual gravitationally driven impact interactions in a nearly gas-free environment of the Kuiper belt (KB) and use low-temperature (< 100 K) ice dynamic strength dependent collisional out-come (accretion vs. erosion and fragmentation) models. These lead to theoretically predictable distributions of object number density, vs. mass distributions. These derived mass distributions are comparable to the now rapidly growing KB survey data. Tensional failure of single and polycrystalline ice in the temperature range from 263 to 128 K was measured for high strain rate, c.a. 104 s-1, dynamic loading conditions. Experiments, similar to Lange and Ahrens(1991)(LA), were conducted using a gas gun launched Lexan projectile. The liquid nitrogen cooled ice target approaching KB-like temperatures was partially confined, rather than using the LA confined geometry. Another set of experiments used a drop tube projectile launcher within the 263 K Caltech Ice Laboratory and at 163 K in a liquid nitrogen cooled chamber. New experiments give tensile strengths of 7.6±1.5 MPa at 263 K and 9.1±1.5 MPa at 163 K for unconfined, free of visual initial defects and measurable imperfections ice samples. The new strengths are lower than the earlier LA data ( 17 MPa). The major differences arise from ice target assembly. LA used polycrystalline ice samples confined in annular stainless steel target rings. New measurements were partially confined, in not initially contacting concentric target rings. Later shots used unconfined configurations with ice pellets affixed to aluminum foil. Circumferential confinement is known to increase the material damage threshold upon both compression and tensile loading. Previous confinement in LA is the main cause of the above discrepancy. Present tensile strengths are only a few times higher than 0.7 - 3.0 MPa summarized in Petrovic (2003) for quasistatic tension at 10-7 to 10-3 s-1 strain rate.

  19. Effect of laser welding on the titanium ceramic tensile bond strength.

    PubMed

    Galo, Rodrigo; Ribeiro, Ricardo Faria; Rodrigues, Renata Cristina Silveira; Pagnano, Valéria de Oliveira; Mattos, Maria da Glória Chiarello de

    2011-08-01

    Titanium reacts strongly with elements, mainly oxygen at high temperature. The high temperature of titanium laser welding modifies the surface, and may interfere on the metal-ceramic tensile bond strength. The influence of laser welding on the titanium-ceramic bonding has not yet been established. The purpose of this in vitro study was to analyze the influence of laser welding applied to commercially pure titanium (CpTi) substructure on the bond strength of commercial ceramic. The influence of airborne particle abrasion (Al2O3) conditions was also studied. Forty CpTi cylindrical rods (3 mm x 60 mm) were cast and divided into 2 groups: with laser welding (L) and without laser welding (WL). Each group was divided in 4 subgroups, according to the size of the particles used in airborne particle abrasion: A - Al2O3 (250 µm); B - Al2O3 (180 µm); C - Al2O3 (110 µm); D - Al2O3 (50 µm). Ceramic rings were fused around the CpTi rods. Specimens were invested and their tensile strength was measured at fracture with a universal testing machine at a crosshead speed of 2.0 mm/min and 200 kgf load cell. Statistical analysis was carried out with analysis of variance and compared using the independent t test (p<0.05). Significant differences were found among all subgroups (p<0.05). The highest and the lowest bond strength means were recorded in subgroups WLC (52.62 MPa) and LD (24.02 MPa), respectively. Airborne particle abrasion yielded significantly lower bond strength as the Al2O3 particle size decreased. Mechanical retention decreased in the laser-welded specimens, i.e. the metal-ceramic tensile bond strength was lower.

  20. Effects of Cooling Conditions on Tensile and Charpy Impact Properties of API X80 Linepipe Steels

    NASA Astrophysics Data System (ADS)

    Han, Seung Youb; Shin, Sang Yong; Lee, Sunghak; Kim, Nack J.; Bae, Jin-Ho; Kim, Kisoo

    2010-02-01

    In this study, four API X80 linepipe steel specimens were fabricated by varying the cooling rate and finish cooling temperature, and their microstructures and crystallographic orientations were analyzed to investigate the effects of the cooling conditions on the tensile and Charpy impact properties. All the specimens consisted of acicular ferrite (AF), granular bainite (GB), and martensite-austenite (MA) constituents. The volume fraction of MA increased with an increasing cooling rate, and the volume fraction and size of MA tended to decrease with an increasing finish cooling temperature. According to the crystallographic orientation analysis data, the effective grain size and unit crack path decreased as fine ACs having a large amount of high-angle grain boundaries were homogeneously formed, thereby leading to the improvement in the Charpy impact properties. The specimen fabricated with the higher cooling rate and lower finish cooling temperature had the highest upper-shelf energy (USE) and the lowest energy transition temperature (ETT), because it contained a large amount of MA homogeneously distributed inside fine AFs, while its tensile properties remained excellent.