Characterizing Salmonella Contamination in Two Rendering Processing Plants.

PubMed

Gong, Chao; Jiang, Xiuping

2017-02-01

A microbiological investigation on Salmonella contamination was conducted in two U.S. rendering plants to investigate the potential cross-contamination of Salmonella in the rendering processing environment. Sampling locations were predetermined at the areas where Salmonella contamination may potentially occur, including raw materials receiving, crax (rendered materials before grinding process) grinding, and finished meal loading-out areas. Salmonella was either enumerated directly on xylose lysine Tergitol 4 agar plates or enriched in Rappaport-Vassiliadis and tetrathionate broths. The presumptive Salmonella isolates were confirmed using CHROMagar plating and latex agglutination testing and then characterized using pulsed-field gel electrophoresis, serotyping, and biofilm-forming determination. Among 108 samples analyzed, 79 (73%) samples were Salmonella positive after enrichment. Selected Salmonella isolates (n = 65) were assigned to 31 unique pulsed-field gel electrophoresis patterns, with 16 Salmonella serotypes, including Typhimurium and Mbandaka, identified as predominant serotypes and 10 Salmonella strains determined as strong biofilm formers. Our results indicated that the raw materials receiving area was the primary source of Salmonella and that the surfaces surrounding crax grinding and finished meal loading-out areas harbor Salmonella in biofilms that may recontaminate the finished meals. The same Salmonella serotypes found in both raw materials receiving and the finished meal loading-out areas suggested a potential of cross-contamination between different areas in the rendering processing environment.

Optimized Extraction, Preliminary Characterization, and In Vitro Antioxidant Activity of Polysaccharides from Glycyrrhiza Uralensis Fisch

PubMed Central

Chen, Jie; Li, Wan-chen; Gu, Xin-li

2017-01-01

Background This study performed optimized extraction, preliminary characterization, and in vitro antioxidant activities of polysaccharides from Glycyrrhiza uralensis Fisch. Material/Methods Three parameters (extraction temperature, ratio of water to raw material, and extraction time) were optimized for yields of G. uralensis polysaccharides (GUP) using response surface methodology with Box-Behnken design (BBD). The GUP was purified using DEAE cellulose 32-column chromatography. The main fraction obtained from G. uralensis Fisch was GUP-II, which was composed of rhamnose, arabinose, galactose, and glucose monosaccharide, was screened for antioxidant properties using DP Hand hydroxyl radical scavenging assays. In addition, immunological activity of GUP-II was determined by nitric oxide and lymphocyte proliferation assays. Results Optimization revealed maximum GUP yields with an extraction temperature of 99°C, water: raw material ratio of 15: 1, and extraction duration of 2 h. GUP-II purified from G. uralensis Fisch had good in vitro DPPH and hydroxyl radical scavenging abilities. Immunologically, GUP-II significantly stimulated NO production in RAW 264.7 macrophages, and significantly enhanced LPS-induced lymphocyte proliferation. Conclusions Extraction of GUP from G. uralensis Fisch can be optimized with respect to temperature, extraction period, and ratio of water to material, using response surface methodology. The purified product (GUP-II) possesses excellent antioxidant and immunological activities. PMID:28404983

Characterization of a wollastonite glass-ceramic material prepared using sugar cane bagasse ash (SCBA) as one of the raw materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Teixeira, Silvio R., E-mail: rainho@fct.unesp.br; Souza, Agda E.; Carvalho, Claudio L.

Glass-ceramic material prepared with sugar cane bagasse ash as one of the raw materials was characterized to determine some important properties for its application as a coating material. X-ray diffraction patterns showed that wollastonite-2M (CaSiO{sub 3}) was the major glass-ceramic phase. The Rietveld method was used to quantify the crystalline (60 wt.%) and vitreous (40 wt.%) phases in the glass-ceramic. The microstructure (determined by scanning electron microscopy) of this material had a marble appearance, showing a microporous network of elongated crystals with some areas with dendritic, feather-like ordering. Microhardness data gave a mean hardness value of 564.4 HV (Vickers-hardness), andmore » light microscopy disclosed a greenish brown colored material with a vitreous luster. - Highlights: • We studied the properties of a glass-ceramic material obtained from sugarcane ash. • This material has the appearance and hardness of natural stones. • A refining method gave information about its amorphous and crystalline phases. • This material has potential to be used as coating plates for buildings.« less

Efficient sugar release by acetic acid ethanol-based organosolv pretreatment and enzymatic saccharification.

PubMed

Zhang, Hongdan; Wu, Shubin

2014-12-03

Acetic acid ethanol-based organosolv pretreatment of sugar cane bagasse was performed to enhance enzymatic hydrolysis. The effect of different parameters (including temperature, reaction time, solvent concentration, and acid catalyst dose) on pretreatment prehydrolyzate and subsequent enzymatic digestibility was determined. During the pretreatment process, 11.83 g of xylose based on 100 g of raw material could be obtained. After the ethanol-based pretreatment, the enzymatic hydrolysis was enhanced and the highest glucose yield of 40.99 g based on 100 g of raw material could be obtained, representing 93.8% of glucose in sugar cane bagasse. The maximum total sugar yields occurred at 190 °C, 45 min, 60:40 ethanol/water, and 5% dosage of acetic acid, reaching 58.36 g (including 17.69 g of xylose and 40.67 g of glucose) based on 100 g of raw material, representing 85.4% of total sugars in raw material. Furthermore, characterization of the pretreated sugar cane bagasse using X-ray diffraction and scanning electron microscopy analyses were also developed. The results suggested that ethanol-based organosolv pretreatment could enhance enzymatic digestibilities because of the delignification and removal of xylan.

A 3-year hygiene and safety monitoring of a meat processing plant which uses raw materials of global origin.

PubMed

Manios, Stavros G; Grivokostopoulos, Nikolaos C; Bikouli, Vasiliki C; Doultsos, Dimitrios A; Zilelidou, Evangelia A; Gialitaki, Maria A; Skandamis, Panagiotis N

2015-09-16

A systematic approach in monitoring the hygiene of a meat processing plant using classical microbiological analyses combined with molecular characterization tools may assist in the safety of the final products. This study aimed: (i) to evaluate the total hygiene level and, (ii) to monitor and characterize the occurrence and spread of Salmonella spp. and Listeria monocytogenes in the environment and the final products of a meat industry that processes meat of global origin. In total, 2541 samples from the processing environment, the raw materials, and the final products were collected from a Greek meat industry in the period 2011-2013. All samples were subjected to enumeration of total viable counts (TVC), Escherichia coli (EC) and total coliforms (TCC) and the detection of Salmonella spp., while 709 of these samples were also analyzed for the presence L. monocytogenes. Pathogen isolates were serotyped and further characterized for their antibiotic resistance and subtyped by PFGE. Raw materials were identified as the primary source of contamination, while improper handling might have also favored the proliferation of the initial microbial load. The occurrence of Salmonella spp. and L. monocytogenes reached 5.5% and 26.9%, respectively. Various (apparent) cross-contamination or persistence trends were deduced based on PFGE analysis results. Salmonella isolates showed wide variation in their innate antibiotic resistance, contrary to L. monocytogenes ones, which were found susceptible to all antibiotics except for cefotaxime. The results emphasize the biodiversity of foodborne pathogens in a meat industry and may be used by meat processors to understand the spread of pathogens in the processing environment, as well as to assist the Food Business Operator (FBO) in establishing effective criteria for selection of raw materials and in improving meat safety and quality. This approach can limit the increase of microbial contamination during the processing steps observed in our study as well as the cross contamination of meat products. Copyright © 2014 Elsevier B.V. All rights reserved.

Preparation, characterization and properties of ZnO nanomaterials

NASA Astrophysics Data System (ADS)

Luo, Jiaolian; Zhang, Xiaoming; Chen, Ruxue; Wang, Xiaohui; Zhu, Ji; Wang, Xiaomin

2017-06-01

In this paper, using the hydrothermal synthesis method, NaOH, Zn(NO3)2, anhydrous ethanol, deionized water as raw material to prepare ZnO nanomaterial, and by X ray diffraction (XRD), scanning electron microscopy (SEM) and photoluminescence spectroscopy (PL) on the synthesis of nano materials, surface morphology and phase luminescence characterization. The results show that the nano materials synthesized for single-phase ZnO, belonging to the six wurtzite structure; material surface shaped, arranged evenly distributed, and were the top six party structure; ZnO nano materials synthesized with strong emission spectra, emission peak is located at 394nm.

Synthesized Li4Ti5O12 from Technical Grade Raw Material by Excess LiOH.H2O as Anode Lithium Ion Battery

NASA Astrophysics Data System (ADS)

Priyono, S.; Primasari, R. D.; Saptari, S. A.; Prihandoko, B.

2017-07-01

Li4Ti5O12 powder as anode lithium ion battery was synthesized via solid state reaction with excess LiOH.H2O. Technical grades raw materials like LiOH.H2O and TiO2 were used as starting materials. LiOH.H2O excess was varied from 0; 2.5; 5 and 7.5% to get higher optimum phases and capacity of Li4Ti5O12. All raw materials were mixed stoichiometry then followed by calcination and sintering process to get final products. The obtained products were characterized by XRD, SEM, and PSA to get properties of active materials and the electrochemical properties were done by cyclic voltametry and charge-discharge test. The XRD test showed that 5% excess have highest Li4Ti5O12 phases. All samples have same in morphology, agglomerate and same in particle size distribution. Sample with 5% excess showed good reversible process and chargedischarge test showed that increasing Li4Ti5O12 phase can improve specific capacity.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Beckley, D.A.; Stites, J. Jr.

The objective was to characterize several lots of materials used for carbon/carbon and carbon/phenol product manufacture. Volume one is organized into testing categories based on raw material of product form. Each category contains a discussion of the sampling plan, comments and observations on each test method utilized, and a summary of the results obtained each category.

RESEARCH AND DEVELOPMENT ON ADVANCED GRAPHITE MATERIALS. Final Report

DOE Office of Scientific and Technical Information (OSTI.GOV)

None

1962-04-01

A review is given of activities over the period October 15, 1960 to October 15, 1961 on a three year program for the research and development of materials, experimental techniques, and equipment for development of premium quality, reproducible graphite-base materials suitable for missile and astronautic applications. Progress is reported on research and development in the study areas of raw materials, fabrication, and material characterization and evaluation. (auth)

Correlation between thermal behavior of clays and their chemical and mineralogical composition: a review

NASA Astrophysics Data System (ADS)

Dwi Yanti, Evi; Pratiwi, I.

2018-02-01

Clay's abundance has been widely used as industrial raw materials, especially ceramic and tile industries. Utilization of these minerals needs a thermal process for producing ceramic products. Two studies conducted by Septawander et al. and Chin C et al., showed the relationship between thermal behavior of clays and their chemical and mineralogical composition. Clays are characterized by XRD analysis and thermal analysis, ranging from 1100°C to 1200°C room temperature. Specimen of raw materials of clay which is used for the thermal treatment is taken from different geological conditions and formation. In raw material, Quartz is almost present in all samples. Halloysite, montmorillonite, and feldspar are present in Tanjung Morawa raw clay. KC and MC similar kaolinite and illite are present in the samples. The research illustrates the interrelationships of clay minerals and chemical composition with their heat behavior. As the temperature of combustion increases, the sample reduces a significant weight. The minerals which have undergone a transformation phase became mullite, cristobalite or illite and quartz. Under SEM analysis, the microstructures of the samples showed irregularity in shape; changes occurred due the increase of heat.

Extraction of cellulose microcrystalline from galam wood for biopolymer

NASA Astrophysics Data System (ADS)

Ismail, Ika; Sa'adiyah, Devy; Rahajeng, Putri; Suprayitno, Abdi; Andiana, Rocky

2018-04-01

Consumption of plastic raw materials tends to increase, but until now the meet of the consumption of plastic raw are still low, even some are still imported. Nowadays, Indonesia's plastic needs are supported by petrochemicals where raw materials are still dependent abroad and petropolymer raw materials are derived from petroleum which will soon be depleted due to rising petroleum needs. Therefore, various studies have been conducted to develop natural fiber-based polymers that are biodegradable and abundant in nature. It is because the natural polymer production process is very efficient and very environmentally friendly. There have been many studies of biopolymers especially natural fiber-based polymers from plants, due to plants containing cellulose, hemicellulose and lignin. However, cellulose is the only one who has crystalline structures. Cellulose has a high crystality compared to amorphous lignin and hemicellulose. In this study, extracted cellulose as biopolymer and amplifier on composite. The cellulose is extracted from galam wood from East Kalimantan. Cellulose extraction will be obtained in nano / micro form through chemical and mechanical treatment processes. The chemical treatment of cellulose extraction is alkalinization process using NaOH solution, bleaching using NaClO2 and acid hydrolysis using sulfuric acid. After chemical treatment, ultrasonic mechanical treatment is made to make cellulose fibers into micro or nano size. Besides, cellulose results will be characterized. Characterization was performed to analyze molecules of cellulose compounds extracted from plants using Fourier Transformation Infra Red (FTIR) testing. XRD testing to analyze cellulose crystallinity. Scanning Electron Microscope (SEM) test to analyze morphology and fiber size.

Measurement Challenges for Carbon Nanotube Material

NASA Technical Reports Server (NTRS)

Sosa, Edward; Arepalli, Sivaram; Nikolaev, Pasha; Gorelik, Olga; Yowell, Leonard

2006-01-01

The advances in large scale applications of carbon nanotubes demand a reliable supply of raw and processed materials. It is imperative to have a consistent quality control of these nanomaterials to distinguish material inconsistency from the modifications induced by processing of nanotubes for any application. NASA Johnson Space Center realized this need five years back and started a program to standardize the characterization methods. The JSC team conducted two workshops (2003 and 2005) in collaboration with NIST focusing on purity and dispersion measurement issues of carbon nanotubes [1]. In 2004, the NASA-JSC protocol was developed by combining analytical techniques of SEM, TEM, UV-VIS-NIR absorption, Raman, and TGA [2]. This protocol is routinely used by several researchers across the world as a first step in characterizing raw and purified carbon nanotubes. A suggested practice guide consisting of detailed chapters on TGA, Raman, electron microscopy and NIR absorption is in the final stages and is undergoing revisions with input from the nanotube community [3]. The possible addition of other techniques such as XPS, and ICP to the existing protocol will be presented. Recent activities at ANSI and ISO towards implementing these protocols as nanotube characterization standards will be discussed.

System simulation application for determining the size of daily raw material purchases at PT XY

NASA Astrophysics Data System (ADS)

Napitupulu, H. L.

2018-02-01

Every manufacturing company needs to implement green production, including PT XY as a marine catchment processing industry in Sumatera Utara Province. The company is engaged in the processing of squid for export purposes. The company’s problem relates to the absence of a decision on the daily purchase amount of the squid. The purchase of daily raw materials in varying quantities has caused companies to face the problem of excess raw materials or otherwise the lack of raw materials. The low purchase of raw materials will result in reduced productivity, while large purchases will lead to increased cooling costs for storage of excess raw materials, as well as possible loss of damage raw material. Therefore it is necessary to determine the optimal amount of raw material purchases every day. This can be determined by applying simulation. Application of system simulations can provide the expected optimal amount of raw material purchases.

Pore structure of raw and purified HiPco single-walled carbon nanotubes

NASA Astrophysics Data System (ADS)

Cinke, Martin; Li, Jing; Chen, Bin; Cassell, Alan; Delzeit, Lance; Han, Jie; Meyyappan, M.

2002-10-01

Very high purity single-walled carbon nanotubes (SWNTs) were obtained from HiPco SWNT samples containing Fe particles by a two-step purification process. The raw and purified samples were characterized using high resolution transmission electron microscopy (HRTEM), Raman spectroscopy and thermogravimetric analysis (TGA). The purified sample consists of ˜0.4% Fe and the process does not seem to introduce any additional defects. The N 2 adsorption isotherm studies at 77 K reveal that the total surface area of the purified sample increases to 1587 m 2/g from 567 m 2/g for the raw material, which is the highest value reported for SWNTs.

Analytical methods to characterize heterogeneous raw material for thermal spray process: cored wire Inconel 625

NASA Astrophysics Data System (ADS)

Lindner, T.; Bonebeau, S.; Drehmann, R.; Grund, T.; Pawlowski, L.; Lampke, T.

2016-03-01

In wire arc spraying, the raw material needs to exhibit sufficient formability and ductility in order to be processed. By using an electrically conductive, metallic sheath, it is also possible to handle non-conductive and/or brittle materials such as ceramics. In comparison to massive wire, a cored wire has a heterogeneous material distribution. Due to this fact and the complex thermodynamic processes during wire arc spraying, it is very difficult to predict the resulting chemical composition in the coating with sufficient accuracy. An Inconel 625 cored wire was used to investigate this issue. In a comparative study, the analytical results of the raw material were compared to arc sprayed coatings and droplets, which were remelted in an arc furnace under argon atmosphere. Energy-dispersive X-ray spectroscopy (EDX) and X-ray fluorescence (XRF) analysis were used to determine the chemical composition. The phase determination was performed by X-ray diffraction (XRD). The results were related to the manufacturer specifications and evaluated in respect to differences in the chemical composition. The comparison between the feedstock powder, the remelted droplets and the thermally sprayed coatings allows to evaluate the influence of the processing methods on the resulting chemical and phase composition.

40 CFR 63.1348 - Standards for affected sources other than kilns; in-line kiln/raw mills; clinker coolers; new and...

Code of Federal Regulations, 2010 CFR

2010-07-01

... than kilns; in-line kiln/raw mills; clinker coolers; new and reconstructed raw material dryers; and raw...; in-line kiln/raw mills; clinker coolers; new and reconstructed raw material dryers; and raw and finish mills. The owner or operator of each new or existing raw material, clinker, or finished product...

The effects of gamma irradiation on diclofenac sodium, liposome and niosome ingredients for rheumatoid arthritis

PubMed Central

Turker, Selcan; Çolak, Seyda; Korkmaz, Mustafa; Kiliç, Ekrem; Özalp, Meral

2013-01-01

The use of gamma rays for the sterilization of pharmaceutical raw materials and dosage forms is an alternative method for sterilization. However, one of the major problems of the radiosterilization is the production of new radiolytic products during the irradiation process. Therefore, the principal problem in radiosterilization is to determine and to characterize these physical and chemical changes originating from high-energy radiation. Parenteral drug delivery systems were prepared and in vitro characterization, biodistribution and treatment studies were done in our previous studies. Drug delivery systems (liposomes, niosomes, lipogelosomes and niogelosomes) encapsulating diclofenac sodium (DFNa) were prepared for the treatment of rheumatoid arthritis (RA). This work complies information about the studies developed in order to find out if gamma radiation could be applied as a sterilization method to DFNa, and the raw materials as dimyristoyl phosphatidylcholine (DMPC), surfactant I [polyglyceryl-3-cethyl ether (SUR I)], dicethyl phosphate (DCP) and cholesterol (CHOL) that are used to prepare those systems. The raw materials were irradiated with different radiation doses (5, 10, 25 and 50 kGy) and physicochemical changes (organoleptic properties pH, UV and melting point), microbiological evaluation [sterility assurance level (SAL), sterility and pyrogen test] and electron spin resonance (ESR) characteristics were studied at normal (25 °C, 60% relative humidity) and accelerated (40 °C, 75% relative humidity) stability test conditions. PMID:24265902

Application of a quality by design approach to the cell culture process of monoclonal antibody production, resulting in the establishment of a design space.

PubMed

Nagashima, Hiroaki; Watari, Akiko; Shinoda, Yasuharu; Okamoto, Hiroshi; Takuma, Shinya

2013-12-01

This case study describes the application of Quality by Design elements to the process of culturing Chinese hamster ovary cells in the production of a monoclonal antibody. All steps in the cell culture process and all process parameters in each step were identified by using a cause-and-effect diagram. Prospective risk assessment using failure mode and effects analysis identified the following four potential critical process parameters in the production culture step: initial viable cell density, culture duration, pH, and temperature. These parameters and lot-to-lot variability in raw material were then evaluated by process characterization utilizing a design of experiments approach consisting of a face-centered central composite design integrated with a full factorial design. Process characterization was conducted using a scaled down model that had been qualified by comparison with large-scale production data. Multivariate regression analysis was used to establish statistical prediction models for performance indicators and quality attributes; with these, we constructed contour plots and conducted Monte Carlo simulation to clarify the design space. The statistical analyses, especially for raw materials, identified set point values, which were most robust with respect to the lot-to-lot variability of raw materials while keeping the product quality within the acceptance criteria. © 2013 Wiley Periodicals, Inc. and the American Pharmacists Association.

Solid-state evaluation and polymorphic quantification of venlafaxine hydrochloride raw materials using the Rietveld method.

PubMed

Bernardi, Larissa S; Ferreira, Fábio F; Cuffini, Silvia L; Campos, Carlos E M; Monti, Gustavo A; Kuminek, Gislaine; Oliveira, Paulo R; Cardoso, Simone G

2013-12-15

Venlafaxine hydrochloride (VEN) is an antidepressant drug widely used for the treatment of depression. The purpose of this study was to carry out the preparation and solid state characterization of the pure polymorphs (Forms 1 and 2) and the polymorphic identification and quantification of four commercially-available VEN raw materials. These two polymorphic forms were obtained from different crystallization methods and characterized by X-ray Powder Diffraction (XRPD), Diffuse Reflectance Infrared Fourier Transform (DRIFT), Raman Spectroscopy (RS), liquid and solid state Nuclear Magnetic Resonance (NMR and ssNMR) spectroscopies, Differential Scanning Calorimetry (DSC), and Scanning Electron Microscopy (SEM) techniques. The main differences were observed by DSC and XRPD and the latter was chosen as the standard technique for the identification and quantification studies in combination with the Rietveld method for the commercial raw materials (VEN1-VEN4) acquired from different manufacturers. Additionally Form 1 and Form 2 can be clearly distinguished from their (13)C ssNMR spectra. Through the analysis, it was possible to conclude that VEN1 and VEN2 were composed only of Form 1, while VEN3 and VEN4 were a mixture of Forms 1 and 2. Additionally, the Rietveld refinement was successfully applied to quantify the polymorphic ratio for VEN3 and VEN4. Copyright © 2013 Elsevier B.V. All rights reserved.

Characterization of products obtained from pyrolysis and steam gasification of wood waste, RDF, and RPF.

PubMed

Hwang, In-Hee; Kobayashi, Jun; Kawamoto, Katsuya

2014-02-01

Pyrolysis and steam gasification of woody biomass chip (WBC) obtained from construction and demolition wastes, refuse-derived fuel (RDF), and refuse paper and plastic fuel (RPF) were performed at various temperatures using a lab-scale instrument. The gas, liquid, and solid products were examined to determine their generation amounts, properties, and the carbon balance between raw material and products. The amount of product gas and its hydrogen concentration showed a considerable difference depending on pyrolysis and steam gasification at higher temperature. The reaction of steam and solid product, char, contributed to an increase in gas amount and hydrogen concentration. The amount of liquid products generated greatly depended on temperature rather than pyrolysis or steam gasification. The compositions of liquid product varied relying on raw materials used at 500°C but the polycyclic aromatic hydrocarbons became the major compounds at 900°C irrespective of the raw materials used. Almost fixed carbon (FC) of raw materials remained as solid products under pyrolysis condition whereas FC started to decompose at 700°C under steam gasification condition. For WBC, both char utilization by pyrolysis at low temperature (500°C) and syngas recovery by steam gasification at higher temperature (900°C) might be practical options. From the results of carbon balance of RDF and RPF, it was confirmed that the carbon conversion to liquid products conspicuously increased as the amount of plastic increased in the raw material. To recover feedstock from RPF, pyrolysis for oil recovery at low temperature (500°C) might be one of viable options. Steam gasification at 900°C could be an option but the method of tar reforming (e.g. catalyst utilization) should be considered. Copyright © 2013 Elsevier Ltd. All rights reserved.

Innovative hyperspectral imaging (HSI) based techniques applied to end-of-life concrete drill core characterization for optimal dismantling and materials recovery

NASA Astrophysics Data System (ADS)

Bonifazi, Giuseppe; Picone, Nicoletta; Serranti, Silvia

2015-02-01

The reduction of EOL concrete disposal in landfills, together with a lower exploitation of primary raw materials, generates a strong interest to develop, set-up and apply innovative technologies to maximize Construction and Demolition Waste (C&DW) conversion into useful secondary raw materials. Such a goal can be reached starting from a punctual in-situ efficient characterization of the objects to dismantle in order to develop demolition actions aimed to set up innovative mechanical-physical processes to recover the different materials and products to recycle. In this paper an innovative recycling-oriented characterization strategy based on HyperSpectral Imaging (HSI) is described in order to identify aggregates and mortar in drill core samples from end-of-life concrete. To reach this goal, concrete drill cores from a demolition site were systematically investigated by HSI in the short wave infrared field (1000-2500 nm). Results obtained by the adoption of the HSI approach showed as this technology can be successfully applied to analyze quality and characteristics of C&DW before dismantling and as final product to reutilise after demolition-milling-classification actions. The proposed technique and the related recognition logics, through the spectral signature detection of finite physical domains (i.e. concrete slice and/or particle) of different nature and composition, allows; i) to develop characterization procedures able to quantitatively assess end-of-life concrete compositional/textural characteristics and ii) to set up innovative sorting strategies to qualify the different materials constituting drill core samples.

Free fatty acid particles in protein formulations, part 2: contribution of polysorbate raw material.

PubMed

Siska, Christine C; Pierini, Christopher J; Lau, Hollis R; Latypov, Ramil F; Fesinmeyer, R Matthew; Litowski, Jennifer R

2015-02-01

Polysorbate 20 (PS20) is a nonionic surfactant frequently used to stabilize protein biopharmaceuticals. During the development of mAb formulations containing PS20, small clouds of particles were observed in solutions stored in vials. The degree of particle formation was dependent on PS20 concentration. The particles were characterized by reversed-phase HPLC after dissolution and labeling with the fluorescent dye 1-pyrenyldiazomethane. The analysis showed that the particles consisted of free fatty acids (FFAs), with the distribution of types consistent with those found in the PS20 raw material. Protein solutions formulated with polysorbate 80, a chemically similar nonionic surfactant, showed a substantial delay in particle formation over time compared with PS20. Multiple lots of polysorbates were evaluated for FFA levels, each exhibiting differences based on polysorbate type and lot. Polysorbates purchased in more recent years show a greater distribution and quantity of FFA and also a greater propensity to form particles. This work shows that the quality control of polysorbate raw materials could play an important role in biopharmaceutical product quality. © 2014 Wiley Periodicals, Inc. and the American Pharmacists Association.

31 CFR 560.407 - Transactions related to Iranian-origin goods.

Code of Federal Regulations, 2011 CFR

2011-07-01

... from third countries of goods containing Iranian-origin raw materials or components is not prohibited if those raw materials or components have been incorporated into manufactured products or... Iranian-origin raw materials or components are not prohibited if those raw materials or components have...

Addictive Economies: Extractive Industries and Vulnerable Localities in a Changing World Economy.

ERIC Educational Resources Information Center

Freudenburg, William R.

1992-01-01

Examines development of rural communities and regions that depend on extractive industries (involving removal of raw materials from nature). Discusses "addictive activities" in such communities characterized by rising operation costs and declining commodities' prices. Discusses community and regional characteristics contributing to…

Synthesis and characterization of activated carbon from white lotus via single step chemical activation

NASA Astrophysics Data System (ADS)

Andas, Jeyashelly; Midon, Muhammad Dzulfiqar

2017-08-01

Highly porous activated carbon was successfully fabricated from the stalk of Nymphaea odorata via single step chemical activation. ZnCl2 was used as the chemical activating agent in the activation process. The raw material was preliminary characterized using Fourier Transform Infrared (FTIR), ultimate analysis (CHNS/O Analyzer) and Scanning Electron Microscope (SEM). The percentage yield, iodine number (IN) and the textural properties of the activated carbon were optimized under the influence of several synthesizing parameters such as impregnation ratio, activation temperature and activation time using ZnCl2. High IN (750.11 mg/g - 967.16 mg/g) was obtained from Sodium thiosulphate volumetric method and represents the porosity of the synthesized materials. Reduction in several functional groups was observed in the FTIR spectrum of the synthesized activated carbon. SEM analysis of the activated carbon verified the formation of highly porous surface compared to the raw Nymphaea odorata. This study provides a facile synthesis of activated carbon from waste natural resources at benign condition.

31 CFR 560.407 - Transactions related to Iranian-origin goods.

Code of Federal Regulations, 2010 CFR

2010-07-01

... United States from third countries of goods containing Iranian-origin raw materials or components is not prohibited if those raw materials or components have been incorporated into manufactured products or... Iranian-origin raw materials or components are not prohibited if those raw materials or components have...

Effect of composition on physical properties of food powders

NASA Astrophysics Data System (ADS)

Szulc, Karolina; Lenart, Andrzej

2016-04-01

The paper presents an influence of raw material composition and technological process applied on selected physical properties of food powders. Powdered multi-component nutrients were subjected to the process of mixing, agglomeration, coating, and drying. Wetting liquids ie water and a 15% water lactose solution, were used in agglomeration and coating. The analyzed food powders were characterized by differentiated physical properties, including especially: particle size, bulk density, wettability, and dispersibility. The raw material composition of the studied nutrients exerted a statistically significant influence on their physical properties. Agglomeration as well as coating of food powders caused a significant increase in particle size, decreased bulk density, increased apparent density and porosity, and deterioration in flowability in comparison with non-agglomerated nutrients.

Recycling-oriented characterization of plastic frames and printed circuit boards from mobile phones by electronic and chemical imaging

DOE Office of Scientific and Technical Information (OSTI.GOV)

Palmieri, Roberta; Bonifazi, Giuseppe; Serranti, Silvia, E-mail: silvia.serranti@uniroma1.it

Highlights: • A recycling oriented characterization of end-of-life mobile phones was carried out. • Characterization was developed in a zero-waste-perspective, aiming to recover all the mobile phone materials. • Plastic frames and printed circuit boards were analyzed by electronic and chemical imaging. • Suitable milling/classification strategies were set up to define specialized-pre-concentrated-streams. • The proposed approach can improve the recovery of polymers, base/precious metals, rare earths and critical raw materials. - Abstract: This study characterizes the composition of plastic frames and printed circuit boards from end-of-life mobile phones. This knowledge may help define an optimal processing strategy for using thesemore » items as potential raw materials. Correct handling of such a waste is essential for its further “sustainable” recovery, especially to maximize the extraction of base, rare and precious metals, minimizing the environmental impact of the entire process chain. A combination of electronic and chemical imaging techniques was thus examined, applied and critically evaluated in order to optimize the processing, through the identification and the topological assessment of the materials of interest and their quantitative distribution. To reach this goal, end-of-life mobile phone derived wastes have been systematically characterized adopting both “traditional” (e.g. scanning electronic microscopy combined with microanalysis and Raman spectroscopy) and innovative (e.g. hyperspectral imaging in short wave infrared field) techniques, with reference to frames and printed circuit boards. Results showed as the combination of both the approaches (i.e. traditional and classical) could dramatically improve recycling strategies set up, as well as final products recovery.« less

Petro-mineralogy and geochemistry as tools of provenance analysis on archaeological pottery: Study of Inka Period ceramics from Paria, Bolivia

NASA Astrophysics Data System (ADS)

Szilágyi, V.; Gyarmati, J.; Tóth, M.; Taubald, H.; Balla, M.; Kasztovszky, Zs.; Szakmány, Gy.

2012-07-01

This paper summarized the results of comprehensive petro-mineralogical and geochemical (archeometrical) investigation of Inka Period ceramics excavated from Inka (A.D. 1438-1535) and Late Intermediate Period (A.D. 1000/1200-1438) sites of the Paria Basin (Dept. Oruro, Bolivia). Applying geological analytical techniques we observed a complex and important archaeological subject of the region and the era, the cultural-economic influence of the conquering Inkas in the provincial region of Paria appearing in the ceramic material. According to our results, continuity and changes of raw material utilization and pottery manufacturing techniques from the Late Intermediate to the Inka Period are characterized by analytical methods. The geological field survey provided efficient basis for the identification of utilized raw material sources. On the one hand, ceramic supply of both eras proved to be based almost entirely on local and near raw material sources. So, imperial handicraft applied local materials but with sophisticated imperial techniques in Paria. On the other hand, Inka Imperial and local-style vessels also show clear differences in their material which suggests that sources and techniques functioned already in the Late Intermediate Period subsisted even after the Inka conquest of the Paria Basin. Based on our geological investigations, pottery supply system of the Paria region proved to be rather complex during the Inka Period.

Effect of sintering process and additives on the properties of cordierite based ceramics

NASA Astrophysics Data System (ADS)

Rundans, M.; Sperberga, I.; Sedmale, G.; Stinkulis, G.

2013-12-01

It is possible to obtain cordierite ceramics with high temperature synthesis using both synthetic and raw natural materials. This paper discusses the possibilities to obtain cordierite ceramics, replacing part of required oxides with raw materials from various Latvian deposits of dolomite and clay. The obtained raw cordierite powders were ground in two modes (3 and 12 hours) and fired at 1200 °C. Ceramic samples were characterized by hydrostatic weighting method; crystalline phase composition was studied by XRD. Obtained samples were evaluated by their mechanical (compressive) strength and linear coefficient of thermal expansion (CTE). Thermal shock resistance was tested using water quenching method and afterwards evaluated by using ultrasonic method to test changes in Young's modulus of elasticity. Results show that increase in grinding time causes samples to densify and promote formation of cordierite crystalline phase which corresponds to increase in total compressive strength and decrease of CTE values. CTE values of samples ground for 12 hours conform to that of obtained in other researches.

Identification of plant cells in black pigments of prehistoric Spanish Levantine rock art by means of a multi-analytical approach. A new method for social identity materialization using chaîne opératoire.

PubMed

López-Montalvo, Esther; Roldán, Clodoaldo; Badal, Ernestina; Murcia-Mascarós, Sonia; Villaverde, Valentín

2017-01-01

We present a new multi-analytical approach to the characterization of black pigments in Spanish Levantine rock art. This new protocol seeks to identify the raw materials that were used, as well as reconstruct the different technical gestures and decision-making processes involved in the obtaining of these black pigments. For the first of these goals, the pictorial matter of the black figurative motifs documented at the Les Dogues rock art shelter (Ares del Maestre, Castellón, Spain) was characterized through the combination of physicochemical and archeobotanical analyses. During the first stage of our research protocol, in situ and non-destructive analyses were carried out by means of portable Energy Dispersive X-Ray Fluorescence spectrometry (EDXRF); during the second stage, samples were analyzed by Optical Microscopy (OM), Raman spectroscopy, and Scanning Electron Microscopy coupled with Energy Dispersive X-ray spectroscopy (SEM-EDX). Two major conclusions have been drawn from these analyses: first, charred plant matter has been identified as a main component of these prehistoric black pigments; and second, angiosperm and conifer charcoal was a primary raw material for pigment production, identified by means of the archaeobotanical study of plant cells. For the second goal, black charcoal pigments were replicated in the laboratory by using different raw materials and binders and by reproducing two main chaînes opératoires. The comparative study of the structure and preservation of plant tissues of both prehistoric and experimental pigments by means of SEM-EDX underlines both a complex preparation process and the use of likely pigment recipes, mixing raw material with fatty or oily binders. Finally, the formal and stylistic analysis of the motifs portrayed at Les Dogues allowed us to explore the relationship between identified stylistic phases and black charcoal pigment use, raising new archaeological questions concerning the acquisition of know-how and the transfer of traditionally learned chaînes opératoires in Spanish Levantine rock art.

Identification of plant cells in black pigments of prehistoric Spanish Levantine rock art by means of a multi-analytical approach. A new method for social identity materialization using chaîne opératoire

PubMed Central

Roldán, Clodoaldo; Badal, Ernestina; Murcia-Mascarós, Sonia; Villaverde, Valentín

2017-01-01

We present a new multi-analytical approach to the characterization of black pigments in Spanish Levantine rock art. This new protocol seeks to identify the raw materials that were used, as well as reconstruct the different technical gestures and decision-making processes involved in the obtaining of these black pigments. For the first of these goals, the pictorial matter of the black figurative motifs documented at the Les Dogues rock art shelter (Ares del Maestre, Castellón, Spain) was characterized through the combination of physicochemical and archeobotanical analyses. During the first stage of our research protocol, in situ and non-destructive analyses were carried out by means of portable Energy Dispersive X-Ray Fluorescence spectrometry (EDXRF); during the second stage, samples were analyzed by Optical Microscopy (OM), Raman spectroscopy, and Scanning Electron Microscopy coupled with Energy Dispersive X-ray spectroscopy (SEM-EDX). Two major conclusions have been drawn from these analyses: first, charred plant matter has been identified as a main component of these prehistoric black pigments; and second, angiosperm and conifer charcoal was a primary raw material for pigment production, identified by means of the archaeobotanical study of plant cells. For the second goal, black charcoal pigments were replicated in the laboratory by using different raw materials and binders and by reproducing two main chaînes opératoires. The comparative study of the structure and preservation of plant tissues of both prehistoric and experimental pigments by means of SEM-EDX underlines both a complex preparation process and the use of likely pigment recipes, mixing raw material with fatty or oily binders. Finally, the formal and stylistic analysis of the motifs portrayed at Les Dogues allowed us to explore the relationship between identified stylistic phases and black charcoal pigment use, raising new archaeological questions concerning the acquisition of know-how and the transfer of traditionally learned chaînes opératoires in Spanish Levantine rock art. PMID:28207835

Exploring application of cardanol from natural resource: Chemistry and products

USDA-ARS?s Scientific Manuscript database

Cardanol (cashew nut shell liquid, CNSL) is a renewable raw material derived from a byproduct of the cashew nut processing industry. First, two natural plasticizers derived from cardanol, cardanol acetate (CA) and epoxidated cardanol acetate (ECA), have been synthesized and characterized by 1HNMR an...

Longitudinal study on the sources of Listeria monocytogenes contamination in cold-smoked salmon and its processing environment in Italy.

PubMed

Di Ciccio, Pierluigi; Meloni, Domenico; Festino, Anna Rita; Conter, Mauro; Zanardi, Emanuela; Ghidini, Sergio; Vergara, Alberto; Mazzette, Rina; Ianieri, Adriana

2012-08-01

The aim of the present study was to investigate the sources of Listeria monocytogenes contamination in a cold smoked salmon processing environment over a period of six years (2003-2008). A total of 170 samples of raw material, semi-processed, final product and processing surfaces at different production stages were tested for the presence of L. monocytogenes. The L. monocytogenes isolates were characterized by multiplex PCR for the analysis of virulence factors and for serogrouping. The routes of contamination over the six year period were traced by PFGE. L. monocytogenes was isolated from 24% of the raw salmon samples, 14% of the semi-processed products and 12% of the final products. Among the environmental samples, 16% were positive for L. monocytogenes. Serotyping yielded three serovars: 1/2a, 1/2b, 4b, with the majority belonging to serovars 1/2a (46%) and 1/2b (39%). PFGE yielded 14 profiles: two of them were repeatedly isolated in 2005-2006 and in 2007-2008 mainly from the processing environment and final products but also from raw materials. The results of this longitudinal study highlighted that contamination of smoked salmon occurs mainly during processing rather than originating from raw materials, even if raw fish can be a contamination source of the working environment. Molecular subtyping is critical for the identification of the contamination routes of L. monocytogenes and its niches into the production plant when control strategies must be implemented with the aim to reduce its prevalence during manufacturing. Copyright © 2012 Elsevier B.V. All rights reserved.

The effectiveness of the biodegradation of raw and processed polystyrene by mealworms

NASA Astrophysics Data System (ADS)

Leluk, Karol; Hanus-Lorenz, Beata; Rybak, Justyna; Bożek, Magdalena

2017-11-01

In our studies biodegradation of four variants of polystyrene was performed. We tested: raw material (PS), processed polystyrene (PSr), building insulation material (EPS) and food packaging boxes (PSp). Materials were characterized by means melt flow ratio (MFR), shore hardness and gloss. The biochemical assessment of macromolecules (proteins, lipids and sugars) in the mealworms organisms fed with tested forms of polystyrene allowed us to set how efficient and beneficial the biodegradation of types of polystyrene is. We also evaluated the variability of bacterial community in larval guts by the use of denaturing gradient gel electrophoresis (DGGE) on the bacterial DNA of 16S rRNA genes amplified in polymerase chain reaction (PCR). The results suggest that EPS and PSp polystyrene are the most digestible for T. molitor larvae. The metabolic degradation of polystyrene is probably strictly connected with the changes in biodiversity of gut bacteria.

Characterization of Limestone as Raw Material to Hydrated Lime

NASA Astrophysics Data System (ADS)

Salem Hwidi, Rajeb; Nuraiti Tengku Izhar, Tengku; Saad, Farah Naemah Mohd

2018-03-01

In Malaysia, limestone is essentially important for the economic growth as raw materials in the industry sector. Nevertheless, a little attention was paid to the physical, chemical, mineralogical, and morphological properties of the limestone using X-ray fluorescence (X-RF), X-ray diffraction (X-RD), Fourier transform infrared spectroscopy (FTIR), and Scanning electron microscopy / energy dispersive x-ray spectroscopy (SEM-EDS) respectively. Raw materials (limestone rocks) were collected from Bukit Keteri area, Chuping, Kangar, Perlis, Malaysia. Lab crusher and lab sieved were utilized to prepare five different size of ground limestone at (75 µm, 150 µm, 225 µm, 300, and 425 µm) respectively. It is found that the main chemical composition of bulk limestone was Calcium oxide (CaO) at 97.58 wt.% and trace amount of MnO, Al2O3, and Fe2O3 at 0.02%, 0.35%, and 0.396% respectively. XRD diffractograms showed characteristic peaks of calcite and quartz. Furthermore, main FTIR absorption bands at 1,419, 874.08 and 712.20 cm-1 indicated the presence of calcite. The micrographs showed clearly the difference of samples particle size. Furthermore, EDS peaks of Ca, O, and C elements confirmed the presence of CaCO3 in the samples.

Use of grape stalk, a waste of the viticulture industry, to obtain activated carbon.

PubMed

Deiana, A C; Sardella, M F; Silva, H; Amaya, A; Tancredi, N

2009-12-15

Grape stalk is an organic waste produced in great amounts in the industrialization processes of grape. This work presents the results of studies carried out to use this waste as raw material to prepare activated carbon through the physical and chemical route. The physicochemical characterization of this material suggests the presence of unusually high levels of ashes. Metal content was determined and high levels of potassium, sodium, iron, calcium and magnesium in carbonized and raw grape stalk were exhibited. This characteristic made difficult physical activation at high temperatures. A leaching step was included before the activation with steam, and adsorbents with surface areas between 700 and 900 m(2)/g were obtained. Physical activation was also performed at lower temperatures using carbonized grape stalk without leaching, leading to the development of some grade of porosity, with an area of 412 m(2)/g. These results would indicate the catalytic effect of the minerals present in this raw material. Chemical activation using phosphoric acid as activating agent seemed to be a very efficient method as final products with BET areas between 1000 and 1500 m(2)/g were obtained.

Optimization of Parameters for Manufacture Nanopowder Bioceramics at Machine Pulverisette 6 by Taguchi and ANOVA Method

NASA Astrophysics Data System (ADS)

Van Hoten, Hendri; Gunawarman; Mulyadi, Ismet Hari; Kurniawan Mainil, Afdhal; Putra, Bismantoloa dan

2018-02-01

This research is about manufacture nanopowder Bioceramics from local materials used Ball Milling for biomedical applications. Source materials for the manufacture of medicines are plants, animal tissues, microbial structures and engineering biomaterial. The form of raw material medicines is a powder before mixed. In the case of medicines, research is to find sources of biomedical materials that will be in the nanoscale powders can be used as raw material for medicine. One of the biomedical materials that can be used as raw material for medicine is of the type of bioceramics is chicken eggshells. This research will develop methods for manufacture nanopowder material from chicken eggshells with Ball Milling using the Taguchi method and ANOVA. Eggshell milled using a variation of Milling rate on 150, 200 and 250 rpm, the time variation of 1, 2 and 3 hours and variations the grinding balls to eggshell powder weight ratio (BPR) 1: 6, 1: 8, 1: 10. Before milled with Ball Milling crushed eggshells in advance and calcinate to a temperature of 900°C. After the milled material characterization of the fine powder of eggshell using SEM to see its size. The result of this research is optimum parameter of Taguchi Design analysis that is 250 rpm milling rate, 3 hours milling time and BPR is 1: 6 with the average eggshell powder size is 1.305 μm. Milling speed, milling time and ball to powder weight of ratio have contribution successively equal to 60.82%, 30.76% and 6.64% by error equal to 1.78%.

40 CFR 63.1343 - What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker piles?

Code of Federal Regulations, 2011 CFR

2011-07-01

..., clinker coolers, raw material dryers, and open clinker piles? 63.1343 Section 63.1343 Protection of... What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker piles? (a..., clinker cooler, and raw material dryer. All dioxin D/F, HCl, and total hydrocarbon (THC) emission limits...

26 CFR 1.472-1 - Last-in, first-out inventories.

Code of Federal Regulations, 2011 CFR

2011-04-01

... may elect to have such method apply to the raw materials only (including those included in goods in... adjustments are confined to costs of the raw material in the inventory and the cost of the raw material in... that the opening inventory had 10 units of raw material, 10 units of goods in process, and 10 units of...

40 CFR 63.1343 - What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker storage...

Code of Federal Regulations, 2014 CFR

2014-07-01

..., clinker coolers, raw material dryers, and open clinker storage piles? 63.1343 Section 63.1343 Protection... Limits § 63.1343 What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker... associated with that kiln, clinker cooler, raw material dryer, and open clinker storage pile. All D/F, HCl...

40 CFR 63.1343 - What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker storage...

Code of Federal Regulations, 2013 CFR

2013-07-01

..., clinker coolers, raw material dryers, and open clinker storage piles? 63.1343 Section 63.1343 Protection... Limits § 63.1343 What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker... associated with that kiln, clinker cooler, raw material dryer, and open clinker storage pile. All D/F, HCl...

40 CFR 63.1343 - What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker piles?

Code of Federal Regulations, 2012 CFR

2012-07-01

..., clinker coolers, raw material dryers, and open clinker piles? 63.1343 Section 63.1343 Protection of... What standards apply to my kilns, clinker coolers, raw material dryers, and open clinker piles? (a..., clinker cooler, and raw material dryer. All dioxin D/F, HCl, and total hydrocarbon (THC) emission limits...

26 CFR 1.472-1 - Last-in, first-out inventories.

Code of Federal Regulations, 2014 CFR

2014-04-01

... may elect to have such method apply to the raw materials only (including those included in goods in... adjustments are confined to costs of the raw material in the inventory and the cost of the raw material in... that the opening inventory had 10 units of raw material, 10 units of goods in process, and 10 units of...

26 CFR 1.472-1 - Last-in, first-out inventories.

Code of Federal Regulations, 2013 CFR

2013-04-01

... may elect to have such method apply to the raw materials only (including those included in goods in... adjustments are confined to costs of the raw material in the inventory and the cost of the raw material in... that the opening inventory had 10 units of raw material, 10 units of goods in process, and 10 units of...

26 CFR 1.472-1 - Last-in, first-out inventories.

Code of Federal Regulations, 2012 CFR

2012-04-01

... may elect to have such method apply to the raw materials only (including those included in goods in... adjustments are confined to costs of the raw material in the inventory and the cost of the raw material in... that the opening inventory had 10 units of raw material, 10 units of goods in process, and 10 units of...

[Which one is more important, raw materials or productive technology?--a case study for quality consistency control of Gegen Qinlian decoction].

PubMed

Zhong, Wen; Chen, Sha; Zhang, Jun; Wang, Yu-Sheng; Liu, An

2016-03-01

To investigate the effect of Chinese medicine raw materials and production technology on quality consistency of Chinese patent medicines with Gegen Qinlian decoction as an example, and establish a suitable method for the quality consistency control of Chinese patent medicines. The results showed that the effect of production technology on the quality consistency was generally not more than 5%, while the effect of raw materials was even more than 30%, indicating that the effect of raw materials was much greater than that of the production technology. In this study, blend technology was used to improve the quality consistency of raw materials. As a result, the difference between the product produced by raw materials and reference groups was less than 5%, thus increasing the quality consistence of finished products. The results showed that under the current circumstances, the main factor affecting the quality consistency of Chinese patent medicines was raw materials, so we shall pay more attention to the quality of Chinese medicine's raw materials. Finally, a blend technology can improve the quality consistency of Chinese patent medicines. Copyright© by the Chinese Pharmaceutical Association.

21 CFR 1304.31 - Reports from manufacturers importing narcotic raw material.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 9 2010-04-01 2010-04-01 false Reports from manufacturers importing narcotic raw... RECORDS AND REPORTS OF REGISTRANTS Reports § 1304.31 Reports from manufacturers importing narcotic raw material. (a) Every manufacturer which imports or manufactures from narcotic raw material (opium, poppy...

21 CFR 1304.31 - Reports from manufacturers importing narcotic raw material.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 9 2011-04-01 2011-04-01 false Reports from manufacturers importing narcotic raw... RECORDS AND REPORTS OF REGISTRANTS Reports § 1304.31 Reports from manufacturers importing narcotic raw material. (a) Every manufacturer which imports or manufactures from narcotic raw material (opium, poppy...

Analyses of factors affecting nickel ferrite nanoparticles synthesis in ultrasound-assisted aqueous solution ball milling.

PubMed

Yuan, Zhuang; Chen, Zhen-hua; Chen, Ding; Kang, Zhi-tao

2015-01-01

Ball milling experiments were conducted with and without ultrasound wave assistance in deionized water using NiCO3·2Ni(OH)2·4H2O as raw materials. In the reaction process of NiFe2O4 prepared by ultrasound-assisted aqueous solution ball milling, some influencing factors including raw materials, ultrasonic frequency, ball to powder ratio and liquid level were changed. Samples were characterized by X-ray diffraction, fluorescence measurements and electroconductivity detections. The results indicate that more hydroxyl radicals and ions can be generated under the coupling effect of ultrasonic and ball milling. The fluorescence measurements and electroconductivity detections also reflect the reaction speed, allowing for optimal parameters to be determined. Copyright © 2014 Elsevier B.V. All rights reserved.

Archaeometric study of black-coated pottery from Pompeii by different analytical techniques.

PubMed

Scarpelli, Roberta; Clark, Robin J H; De Francesco, Anna Maria

2014-01-01

Complementary spectroscopic methods were used to characterize ceramic body and black coating of fine pottery found at Pompeii (Italy). This has enabled us to investigate local productions and to clarify the technological changes over the 4th-1st centuries BC. Two different groups of ceramics were originally distinguished on the basis of macroscopic observations. Optical microscopy (OM), X-ray diffraction (XRD) and X-ray fluorescence (XRF) seem to indicate the usage of the same raw materials for the production of black-coated ceramics at Pompeii for about three centuries. Raman microscopy (RM) and micro-analysis (SEM/EDS) suggest different production treatments for both raw material processing and firing practice (duration of the reducing step and the cooling rate). Copyright © 2013 Elsevier B.V. All rights reserved.

Characterization of wood plastic composites made from landfill-derived plastic and sawdust: Volatile compounds and olfactometric analysis

DOE Office of Scientific and Technical Information (OSTI.GOV)

Félix, Juliana S., E-mail: jfelix@unizar.es; Domeño, Celia, E-mail: cdomeno@unizar.es; Nerín, Cristina, E-mail: cnerin@unizar.es

Graphical abstract: This work details the characterization of VOCs of WPC, produced from residual materials which would have landfills as current destination, and evaluates their odor profile. Highlights: ► More than 140 volatile compounds were identified in raw materials and WPC products. ► Markers were related to the thermal degradation, sawdust or coupling agents. ► WPC prototype showed a characteristic odor profile of burnt, sweet and wax-like. ► Aldehydes, carboxylic acids, ketones and phenols were odor descriptors of WPC. - Abstract: Application of wood plastic composites (WPCs) obtained from recycled materials initially intended for landfill is usually limited by theirmore » composition, mainly focused on release of volatile organic compounds (VOCs) which could affect quality or human safety. The study of the VOCs released by a material is a requirement for new composite materials. Characterization and quantification of VOCs of several WPC produced with low density polyethylene (LDPE) and polyethylene/ethylene vinyl acetate (PE/EVA) films and sawdust were carried out, in each stage of production, by solid phase microextraction in headspace mode (HS-SPME) and gas chromatography–mass spectrometry (GC–MS). An odor profile was also obtained by HS-SPME and GC–MS coupled with olfactometry analysis. More than 140 compounds were observed in the raw materials and WPC samples. Some quantified compounds were considered WPC markers such as furfural, 2-methoxyphenol, N-methylphthalimide and 2,4-di-tert-butylphenol. Hexanoic acid, acetic acid, 2-methoxyphenol, acetylfuran, diacetyl, and aldehydes were the most important odorants. None of the VOCs were found to affect human safety for use of the WPC.« less

Characterization of the Resource Potential of Martian Soil using the Integrated Dust/Soil Experiment Package (IDEP)

NASA Technical Reports Server (NTRS)

Cooper, Bonnie L.; Mckay, David S.; Allen, Carlton C.; Hoffman, John H.; Gittleman, Mark E.

1997-01-01

The Integrated Dust/Soil Experiment Package (IDEP) is a suite of instruments that can detect and quantify the abundances of useful raw materials on Mars. We focus here on its capability for resource characterization in the martian soil; however, it is also capable of detecting and quantifying gases in the atmosphere. This paper describes the scientific rationale and the engineering design behind the IDEP.

29 CFR 779.333 - Goods sold for use as raw materials in other products.

Code of Federal Regulations, 2011 CFR

2011-07-01

... 29 Labor 3 2011-07-01 2011-07-01 false Goods sold for use as raw materials in other products. 779... Service Establishments Sales Not Made for Resale § 779.333 Goods sold for use as raw materials in other products. Goods are sold for resale where they are sold for use as a raw material in the production of a...

29 CFR 779.333 - Goods sold for use as raw materials in other products.

Code of Federal Regulations, 2010 CFR

2010-07-01

... 29 Labor 3 2010-07-01 2010-07-01 false Goods sold for use as raw materials in other products. 779... Service Establishments Sales Not Made for Resale § 779.333 Goods sold for use as raw materials in other products. Goods are sold for resale where they are sold for use as a raw material in the production of a...

40 CFR Table N-1 to Subpart N of... - CO2 Emission Factors for Carbonate-Based Raw Materials

Code of Federal Regulations, 2011 CFR

2011-07-01

...-Based Raw Materials N Table N-1 to Subpart N of Part 98 Protection of Environment ENVIRONMENTAL... Raw Materials Carbonate-basedraw material—mineral CO2 emission factor a Limestone—CaCO3 0.440 Dolomite... in units of metric tons of CO2 emitted per metric ton of carbonate-based raw material charged to the...

DOE Office of Scientific and Technical Information (OSTI.GOV)

Viani, Alberto, E-mail: viani@itam.cas.cz; Sotiriadis, Konstantinos; Len, Adél

Full characterization of fired-clay bricks is crucial for the improvement of process variables in manufacturing and, in case of old bricks, for restoration/replacement purposes. To this aim, five bricks produced in a plant in Czech Republic in the past have been investigated with a combination of analytical techniques in order to derive information on the firing process. An additional old brick from another brickyard was also used to study the influence of different raw materials on sample microstructure. The potential of X-ray diffraction with the Rietveld method and small angle neutron scattering technique has been exploited to describe the phasemore » transformations taking place during firing and characterize the brick microstructure. Unit-cell parameter of spinel and amount of hematite are proposed as indicators of the maximum firing temperature, although for the latter, limited to bricks produced from the same raw material. The fractal quality of the surface area of pores obtained from small angle neutron scattering is also suggested as a method to distinguish between bricks produced from different raw clays. - Highlights: • Rietveld method helps in describing microstructure and physical properties of bricks. • XRPD derived cell parameter of spinel is proposed as an indicator of firing temperature. • SANS effectively describes brick micro and nanostructure, including closed porosity. • Fractal quality of pore surface is proposed as ‘fingerprint’ of brick manufacturing.« less

40 CFR 63.1346 - Standards for new or reconstructed raw material dryers.

Code of Federal Regulations, 2010 CFR

2010-07-01

... 40 Protection of Environment 11 2010-07-01 2010-07-01 true Standards for new or reconstructed raw... Industry Emission Standards and Operating Limits § 63.1346 Standards for new or reconstructed raw material dryers. (a) New or reconstructed raw material dryers located at facilities that are major sources can not...

Leveraging “Raw Materials” as Building Blocks and Bioactive Signals in Regenerative Medicine

PubMed Central

Renth, Amanda N.

2012-01-01

Components found within the extracellular matrix (ECM) have emerged as an essential subset of biomaterials for tissue engineering scaffolds. Collagen, glycosaminoglycans, bioceramics, and ECM-based matrices are the main categories of “raw materials” used in a wide variety of tissue engineering strategies. The advantages of raw materials include their inherent ability to create a microenvironment that contains physical, chemical, and mechanical cues similar to native tissue, which prove unmatched by synthetic biomaterials alone. Moreover, these raw materials provide a head start in the regeneration of tissues by providing building blocks to be bioresorbed and incorporated into the tissue as opposed to being biodegraded into waste products and removed. This article reviews the strategies and applications of employing raw materials as components of tissue engineering constructs. Utilizing raw materials holds the potential to provide both a scaffold and a signal, perhaps even without the addition of exogenous growth factors or cytokines. Raw materials contain endogenous proteins that may also help to improve the translational success of tissue engineering solutions to progress from laboratory bench to clinical therapies. Traditionally, the tissue engineering triad has included cells, signals, and materials. Whether raw materials represent their own new paradigm or are categorized as a bridge between signals and materials, it is clear that they have emerged as a leading strategy in regenerative medicine. The common use of raw materials in commercial products as well as their growing presence in the research community speak to their potential. However, there has heretofore not been a coordinated or organized effort to classify these approaches, and as such we recommend that the use of raw materials be introduced into the collective consciousness of our field as a recognized classification of regenerative medicine strategies. PMID:22462759

Scoping Future Policy Dynamics in Raw Materials Through Scenarios Testing

NASA Astrophysics Data System (ADS)

Correia, Vitor; Keane, Christopher; Sturm, Flavius; Schimpf, Sven; Bodo, Balazs

2017-04-01

The International Raw Materials Observatory (INTRAW) project is working towards a sustainable future for the European Union in access to raw materials, from an availability, economical, and environmental framework. One of the major exercises for the INTRAW project is the evaluation of potential future scenarios for 2050 to frame economic, research, and environmental policy towards a sustainable raw materials supply. The INTRAW consortium developed three possible future scenarios that encompass defined regimes of political, economic, and technological norms. The first scenario, "Unlimited Trade," reflects a world in which free trade continues to dominate the global political and economic environment, with expectations of a growing demand for raw materials from widely distributed global growth. The "National Walls" scenario reflects a world where nationalism and economic protectionism begins to dominate, leading to stagnating economic growth and uneven dynamics in raw materials supply and demand. The final scenario, "Sustainability Alliance," examines the dynamics of a global political and economic climate that is focused on environmental and economic sustainability, leading towards increasingly towards a circular raw materials economy. These scenarios were reviewed, tested, and provided simulations of impacts with members of the Consortium and a panel of global experts on international raw materials issues which led to expected end conditions for 2050. Given the current uncertainty in global politics, these scenarios are informative to identifying likely opportunities and crises. The details of these simulations and expected responses to the research demand, technology investments, and economic components of raw materials system will be discussed.

Recent analytical developments for powder characterization

NASA Astrophysics Data System (ADS)

Brackx, E.; Pages, S.; Dugne, O.; Podor, R.

2015-07-01

Powders and divided solid materials are widely represented as finished or intermediary products in industries as widely varied as foodstuffs, cosmetics, construction, pharmaceuticals, electronic transmission, and energy. Their optimal use requires a mastery of the transformation process based on knowledge of the different phenomena concerned (sintering, chemical reactivity, purity, etc.). Their modelling and understanding need a prior acquisition of sets of data and characteristics which are more or less challenging to obtain. The goal of this study is to present the use of different physico-chemical characterization techniques adapted to uranium-containing powders analyzed either in a raw state or after a specific preparation (ionic polishing). The new developments touched on concern dimensional characterization techniques for grains and pores by image analysis, chemical surface characterization and powder chemical reactivity characterization. The examples discussed are from fabrication process materials used in the nuclear fuel cycle.

40 CFR 428.75 - Standards of performance for new sources.

Code of Federal Regulations, 2011 CFR

2011-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.26 0...— Metric units (kg/kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead...

40 CFR 428.75 - Standards of performance for new sources.

Code of Federal Regulations, 2010 CFR

2010-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.26 0...— Metric units (kg/kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead...

Study on optimum length of raw material in stainless steel high-lock nuts forging

NASA Astrophysics Data System (ADS)

Cheng, Meiwen; Liu, Fenglei; Zhao, Qingyun; Wang, Lidong

2018-04-01

Taking 302 stainless steel (1Cr18Ni9) high-lock nuts for research objects, adjusting the length of raw material, then using DEFORM software to simulate the isothermal forging process of each station and conducting the corresponding field tests to study the effects of raw material size on the stainless steel high-lock nuts forming performance. The tests show that the samples of each raw material length is basically the same as the results of the DEFORM software. When the length of the raw material is 10mm, the appearance size of the parts can meet the design requirements.

Polymer Hydrogel/Polybutadiene/Iron Oxide Nanoparticle Hybrid Actuators for the Characterization of NiTi Implants

PubMed Central

Jeličić, Aleksandra; Friedrich, Alwin; Jeremić, Katarina; Siekmeyer, Gerd; Taubert, Andreas

2009-01-01

One of the main issues with the use of nickel titanium alloy (NiTi) implants in cardiovascular implants (stents) is that these devices must be of very high quality in order to avoid subsequent operations due to failing stents. For small stents with diameters below ca. 2 mm, however, stent characterization is not straightforward. One of the main problems is that there are virtually no methods to characterize the interior of the NiTi tubes used for fabrication of these tiny stents. The current paper reports on a robust hybrid actuator for the characterization of NiTi tubes prior to stent fabrication. The method is based on a polymer/hydrogel/magnetic nanoparticle hybrid material and allows for the determination of the inner diameter at virtually all places in the raw NiTi tubes. Knowledge of the inner structure of the raw NiTi tubes is crucial to avoid regions that are not hollow or regions that are likely to fail due to defects inside the raw tube. The actuator enables close contact of a magnetic polymer film with the inner NiTi tube surface. The magnetic signal can be detected from outside and be used for a direct mapping of the tube interior. As a result, it is possible to detect critical regions prior to expensive and slow stent fabrication processes.

40 CFR 428.55 - Standards of performance for new sources.

Code of Federal Regulations, 2010 CFR

2010-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.70 0.25...— Metric units (kg/kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead...

40 CFR 428.55 - Standards of performance for new sources.

Code of Federal Regulations, 2011 CFR

2011-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.70 0.25...— Metric units (kg/kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead...

40 CFR 428.65 - Standards of performance for new sources.

Code of Federal Regulations, 2010 CFR

2010-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.42 0.0...— Metric units (kg/kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead...

40 CFR 428.65 - Standards of performance for new sources.

Code of Federal Regulations, 2011 CFR

2011-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.42 0.0...— Metric units (kg/kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead...

Natural stone muds as secondary raw materials: towards a new sustainable recovery process

NASA Astrophysics Data System (ADS)

Zichella, Lorena; Tori, Alice; Bellopede, Rossana; Marini, Paola

2016-04-01

The production of residual sludge is a topical issue, and has become essential to recover and reuse the materials, both for the economics and the environmental aspect. According to environmental EU Directives, in fact ,the stone cutting and processing should characterized by following objectives, targets and actions: the reduction of waste generated, the decreasing of use of critical raw material, the zero landfilling of sludge and decreasing in potential soil contamination, the prevention of transport of dangerous waste, the reduction of energy consumption, the zero impact on air pollution and the cost reduction . There are many industrial sector in which residual sludge have high concentrations of metals and/or elements deemed harmful and therefore hazardous waste. An important goal, for all industrial sectors, is an increase in productivity and a parallel reduction in costs. The research leads to the development of solutions with an always reduced environmental impact. The possibility to decrease the amount of required raw materials and at the same time the reduction in the amount of waste has become the aim for any industrial reality. From literature there are different approaches for the recovery of raw and secondary materials, and are often used for the purpose chemical products that separate the elements constituting the mud but at the same time make additional pollutants. The aim of the study is to find solutions that are environmentally sustainable for both industries and citizens. The present study is focused on three different Piedmont rocks: Luserna, Diorite from Traversella and Diorite from Vico, processed with three different stone machining technologies: cutting with diamond wire in quarry (blocks), in sawmill (slabs) and surface polishing. The steps are: chemical analysis, particle size analysis and mineralogical composition and characterization of the sludge obtained from the various machining operations for the recovery of the metal material by cutting and waste rock through an economical and simple method, without the use of chemical products. The technical feasibility of the use of stone mud for construction materials, and industrial mud for alloy reuse, is well known on a scientific and lab scale, but it is not industrially developed because of the wide variety of waste generated and logistic or organization difficulties of interaction among companies of different sectors. This can be realized implementing an existing plant with industrial technologies in order to valorize the product "mud", to reuse the heavy metals in the process and therefore to minimize the volume of sludge produced. A further progress to the previous researches, that is beyond the results obtained in this field, will be the identification of the best technique to eliminate the small amount of heavy metals in the mud fines. This is important because , removing all the toxic substances, the mud properties can be improved in order to be reuse in the other process as secondary raw material.

INTRAW, the EU Observatory for raw materials: fostering international cooperation and developing new opportunities

NASA Astrophysics Data System (ADS)

Correia, Victor; Allington, Ruth; Keane, Christopher

2016-04-01

A secure supply of raw materials is a European priority that extends beyond country borders and national policies. Recent European initiatives have pioneered the development of an EU strategy on raw materials emphasizing the concept of the "added value chain", which continues to pursue the three pillar strategy to: (1) ensure the fair and sustainable supply of raw materials from international markets, promoting international cooperation with developed and developing countries; (2) foster sustainable supply of raw materials from European sources, and (3) reduce consumption of primary raw materials by increasing resource efficiency and promoting recycling. This contribution presents the Horizon 2020 funded project INTRAW, the objective of which is to establish the European Union's International Observatory for Raw Materials. The creation and maintenance of the European Union's International Observatory for Raw Materials is designed to have a strong impact in two dimensions: 1. To narrow the existing gap in aspects of the raw materials knowledge infrastructure in the EU by providing a link with the same knowledge infrastructure in technologically advanced reference countries. This should contribute to the harmonization of mineral policies all over the EU, by providing data that enables evidence-based policies and appropriate, cost-effective management, planning and adaptation decisions by the public sector. This will benefit businesses, industry and society. The Observatory will also provide to policy makers in the EU and its Member States the data they need to facilitate discussion in multilateral forums. 2. To enable a better alignment of the R&I activities among the individual EU members and international cooperation countries AND between the European Union and international cooperation countries by boosting synergies with international research and innovation programmes. This way the EU's role and scientific capabilities in the raw materials area will be reinforced in the mid-term, and the conditions for sustainable access and supply of raw materials in the EU will benefit from the international cooperation. The authors will describe the key stages of the INTRAW project and explain how it aims to establish (and promote the continuation of) international cooperation at every stage of the raw materials value chain and to build a repository of information and analysis to support the development and strengthening of EU raw materials strategies. Key elements of the value chain upon which the project focuses are: industry and trade; education and outreach; and research and innovation. The roles of geoscientists in delivering the aims and objectives of INTRAW will be emphasised.

Methodology for Evaluating Raw Material Changes to RSRM Elastomeric Insulation Materials

NASA Technical Reports Server (NTRS)

Mildenhall, Scott D.; McCool, Alex (Technical Monitor)

2001-01-01

The Reusable Solid Rocket Motor (RSRM) uses asbestos and silicon dioxide filled acrylonitrile butadiene rubber (AS-NBR) as the primary internal insulation to protect the case from heat. During the course of the RSRM Program, several changes have been made to the raw materials and processing of the AS-NBR elastomeric insulation material. These changes have been primarily caused by raw materials becoming obsolete. In addition, some process changes have been implemented that were deemed necessary to improve the quality and consistency of the AS-NBR insulation material. Each change has been evaluated using unique test efforts customized to determine the potential impacts of the specific raw material or process change. Following the evaluations, the various raw material and process changes were successfully implemented with no detectable effect on the performance of the AS-NBR insulation. This paper will discuss some of the raw material and process changes evaluated, the methodology used in designing the unique test plans, and the general evaluation results. A summary of the change history of RSRM AS-NBR internal insulation is also presented.

Process to create simulated lunar agglutinate particles

NASA Technical Reports Server (NTRS)

Gustafson, Robert J. (Inventor); Gustafson, Marty A. (Inventor); White, Brant C. (Inventor)

2011-01-01

A method of creating simulated agglutinate particles by applying a heat source sufficient to partially melt a raw material is provided. The raw material is preferably any lunar soil simulant, crushed mineral, mixture of crushed minerals, or similar material, and the heat source creates localized heating of the raw material.

Characterization of calcium phosphate powders originating from Phyllacanthus imperialis and Trochidae Infundibulum concavus marine shells.

PubMed

Tămăşan, M; Ozyegin, L S; Oktar, F N; Simon, V

2013-07-01

The study reports the preparation and characterization of powders consisting of the different phases of calcium phosphates that were obtained from the naturally derived raw materials of sea-shell origins reacted with H3PO4. Species of sea origin, such as corals and nacres, attracted a special interest in bone tissue engineering area. Nacre shells are built up of calcium carbonate in aragonite form crystallized in an organic matrix. In this work two natural marine origin materials (shells of echinoderm Sputnik sea urchin - Phyllacanthus imperialis and Trochidae Infundibulum concavus mollusk) were involved in the developing powders of calcium phosphate based biomaterials (as raw materials for bone-scaffolds) by hotplate and ultrasound methods. Thermal analyses of the as-prepared materials were made for an assessment of the thermal behavior and heat treatment temperatures. Samples from both sea shells each of them prepared by the above mentioned methods were subjected to thermal treatments at 450 °C and 850 °C in order to evaluate the crystalline transformations of the calcium phosphate structures in the heating process. By X-ray diffraction analyses various calcium phosphate phases were identified. In Sputnik sea urchins originated samples were found predominantly brushite and calcite as a small secondary phase, while in Trochidae I. concavus samples mainly monetite and HA phases were identified. Thermal treatment at 850 °C resulted flat-plate whitlockite crystals - β-MgTCP [(Ca, Mg)3 (PO4)2] for both samples regardless the preparation method (ultrasound or hotplate) or the targeted Ca/P molar ratio according with XRD patterns. Scanning electron microscopy and Fourier transformed infrared spectroscopy were involved more in the characterization of these materials and the good correlations of the results of these methods were made. Copyright © 2013 Elsevier B.V. All rights reserved.

40 CFR 428.72 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.26 0.../kkg of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead 0.0017 0.0007...

40 CFR 428.52 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.70 0.25... of raw material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead 0.0017 0.0007 (c...

VERAM - Vision and Roadmap for European Raw Materials

NASA Astrophysics Data System (ADS)

Baumgarten, Wibke; Vashev, Boris

2017-04-01

The overall objective of VERAM project is to produce a Vision and Roadmap for European Raw Materials in 2050 based on raw materials research and innovation (R&I) coordination. Two leading European Technology Platforms (ETPs): ETP SMR (Sustainable Minerals Resources) and FTP (Forest Technology Platform) are joining forces to develop a common vison and roadmap with the support of ECTP (European Construction Technology Platform), represented by UNIVPM, SusChem (ETP for Sustainable Chemistry), represented by Cefic, EuMaT (Advanced Materials ETP), represented by VITO, ERAMIN 2, represented by Research Centre JUELICH and WoodWisdom Network Plus represented by the Agency for Renewable Resources (FNR). This partnership provides VERAM with expertise from downstream applications and additional knowledge on non-biotic and biotic raw materials. The project encourages capacity building as well as transfer of knowledge. It expects to provide an innovation reference point for the European Institute of Innovation & Technology (EIT) Raw Materials (formerly the KIC Raw MatTERS), to coordinate the network involved in the European Innovation Partnership (EIP) on Raw Materials Commitments and relevant proposals funded under Horizon 2020. It provides a platform for identifying gaps and complementarities and enables their bridging. VERAM will be able to advise the European Commission and Member States on future research needs and policies to stimulate innovation and assist in overcoming fragmentation in the implementing the EIP Raw Materials Strategic Implementation Plan. VERAM looks for mutually beneficial information exchange, encourages cross-fertilization between actions undertaken by different raw material industries, and expects to accelerate exploitation of breakthrough innovations. One of the main outcomes of the project is the presentation of a common long term 2050 Vision and Roadmap for relevant raw materials including metals, industrial minerals and aggregates and wood. The Vision and Roadmap have the objective of highlighting the path to achieving the European Commission's ambitious target of 80% reduction in CO2 emissions by 2050.

Potential contribution of microbial communities in technical ceramics for the improvement of rheological properties

NASA Astrophysics Data System (ADS)

Moreira, Bernardino; Miller, Ana Z.; Santos, Ricardo; Monteiro, Sílvia; Dias, Diamantino; Neves, Orquídia; Dionísio, Amélia; Saiz-Jimenez, Cesareo

2014-05-01

Several bacterial and fungal species naturally occurring in ceramic raw materials used in construction, such as Aspergillus, Penicillium and Aureobasidium, are known to produce exopolysaccharides (EPS). These polymers excreted by the cells are of widespread occurrence and may confer unique and potentially interesting properties with potential industrial uses, such as viscosity control, gelation, and flocculation, during ceramic manufacturing. In this study, the microbial communities present in clay raw materials were identified by both cultural methods and DNA-based molecular techniques in order to appraise their potential contribution to enhance the performance of technical ceramics through the use of EPS. Mineralogical identification by X- Ray Diffraction (XRD) and Fourier Transform Infrared (FTIR) spectroscopy of the clay raw materials, as well as characterization of rheological properties of ceramic slips were also performed. Microbial EPS production and its introduction into ceramic slips will be then carried out in order to evaluate their effects on the rheological properties of the ceramic slips, powders and conformed bodies. Some positive aspects related to the use of EPS are: reduction of the environmental impact caused by synthetic organic additives, reduction of production costs, as well as the costs related with operator protection systems, gaseous effluent treatments, complex landfill, among others.

40 CFR 428.103 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... not exceed— Metric units (kg/kkg of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6.96 2.90 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6... raw material) Chromium 0.0086 0.0036 English units (lb/1,000 lb of raw material) Chromium 0.0086 0...

40 CFR 428.103 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2011 CFR

2011-07-01

... not exceed— Metric units (kg/kkg of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6.96 2.90 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6... raw material) Chromium 0.0086 0.0036 English units (lb/1,000 lb of raw material) Chromium 0.0086 0...

40 CFR 428.102 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6.96 2.90 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 2.0 0.73 BOD5... units (kg/kkg of raw material) Chromium 0.0086 0.0036 English units (lb/1,000 lb of raw material...

Determination of 25-OCH3-PPD and the related substances by UPLC-MS/MS and their cytotoxic activity.

PubMed

Ding, Meng; Lu, Jingjing; Zhao, Chen; Zhang, Sainan; Zhao, Yuqing

2016-06-01

20(R)-25-methoxyl-dammarane-3β,12β,20-triol (25-OCH3-PPD) is a promising antitumor compound belonging to triterpenoid saponins isolated from radix notoginseng. A systematic research on the related impurities in raw material of 25-OCH3-PPD has not been conducted. In this study, three impurities obtained by HPLC-ELSD and characterized by (13)C NMR and MS were observed in the raw material of 25-OCH3-PPD. Cytotoxic activities of the related substances were also evaluated, of which impurity B with 25-OCH3-PPD showed synergistic inhibitory activity against BGC-823 with IC50 values of 8.33μM. Furthermore, a rapid and selective UPLC-MS/MS method was developed for simultaneous determination of the principal component and three related substances in the raw material of 25-OCH3-PPD. Multiple reaction monitoring scan mode was used for the quantification of 20(R)-25-OCH3-PPD and its three related substances. The four constituents were separated within 11min on a BEH C18 column (100 mm×2.1mm, 1.7μm) using a mobile phase comprising methanol and 0.03% formic acid water (82:18, v/v) at a flow rate of 0.2mL/min. The proposed UPLC-MS/MS method displayed acceptable levels of linearity, precision, repeatability, and accuracy. In addition, the proposed method was successfully applied for the establishment of a rational quality control standard for the raw material of 25-OCH3-PPD. Copyright © 2016 Elsevier B.V. All rights reserved.

Map of critical raw material deposits in Europe

NASA Astrophysics Data System (ADS)

Guillaume, Bertrand

2016-04-01

Map of critical raw material deposits in Europe Guillaume BERTRAND1, Daniel CASSARD1, Nikolaos ARVANITIDIS2, Gerry STANLEY3 and the EuroGeoSurvey Mineral Resources Expert Group4. 1 - Bureau de Recherches Géologiques et Minières (BRGM), Georesources Divison, 3 avenue Claude Guillemin, 45060 Orléans cedex 2, FRANCE. 2 - Sveriges Geologiska Undersökning (SGU), Box 670, SE-751 28, Uppsala, SWEDEN 3 - Geological Survey of Ireland (GSI), Beggars Bush, Haddington Road, Dublin D04 K7X4, IRELAND 4 - EuroGeoSurveys, Rue Joseph II 36-38, 1000 Brussels, BELGIUM The Critical Raw Material (CRM) Deposit Map of Europe, prepared by EuroGeoSurvey's Mineral Resources Expert Group (MREG), shows European mineral deposits from the ProMine Mineral Deposit database containing critical commodities, according to the 2014 list of critical raw materials of the European Commission. EuroGeoSurveys (EGS), The Geological Surveys of Europe, is a not-for-profit organization representing 37 National Geological Surveys and some regional Geological Surveys in Europe. It provides the European Institutions with expert, independent, balanced and practical pan-European advice and information as an aid to problem-solving, policy development, regulatory and programme formulation in areas such as natural resources, energy and geo-hazards. The EGS MREG is actively involved in contributing to policy and strategy-making processes aimed at identifying, characterizing and safeguarding resource potential, especially for critical raw materials through data provision, research, technological development and innovation. The European Union aspires to reducing the import dependency of raw materials, especially CRM, that are essential to Europe's industries. In this respect, mineral resource information, data sharing and networking by European Geological Surveys is crucial. The Strategic Implementation Plan of the European Innovation Partnership on Raw Materials highlights the need for establishing and maintaining a common interoperable EU Geological Knowledge Base. Such a Knowledge Base will support exploration for indigenous mineral resources and strengthen policy and decision making. In 2010, the European Commission identified 14 non energy non-agricultural raw materials as being critical. Criticality is based on both the scarcity of supply and the importance to European industry. This list was updated in 2014 to include 7 new commodities with one being dropped from the original list. The list now comprises: antimony, beryllium, borates, chromium, cobalt, coking coal, fluorspar, gallium, germanium, graphite, indium, magnesite, magnesium, niobium, phosphate rock, platinum group metals, light and heavy rare earth elements (separately), silicon metal and tungsten. ProMine was a European Union (EU) co-funded project, which had as its main objective the stimulation of the extractive industry to deliver new products to manufacturing industry. A major deliverable of the project was the ProMine Mineral Deposit (MD) database that contains information related to almost 13,000 mineral deposits in Europe. In order to extract data to be displayed on the CRM map of Europe, the ProMine MD database was queried for all commodities on the EC CRM list which were in the medium to super-large deposit size. Following this, the dataset was circulated to MREG in order to verify, validate and update the list.

Isolation Characterization and Fermented Research of High Producing Saccharamyces Cerevisae

NASA Astrophysics Data System (ADS)

Zhaochunhai

In order to improve to alcoholic production,this paper researched on 122 strains of yeast isolated from orchard and vegetable plot through morphology and molecular biology, screening 17 strains of Saccharomyces cerevisiae through NCBI-blast, selected four yeasts to ferment,amongof them T13 used sorghum as raw material production capacity of 12.48% (v/v).

Cellulose extraction from orange peel using sulfite digestion reagents.

PubMed

Bicu, Ioan; Mustata, Fanica

2011-11-01

Orange peel (OP) was used as raw material for cellulose extraction. Two different pulping reagents were used, sodium sulfite and sodium metabisulfite. The effect of the main process parameters, sulfite agent dosage and reaction duration, on cellulose yield was investigated. A central composite rotatable design involving two variables at five levels and response surface methodology were used for the optimization of cellulose recovery. Other two invariable parameters were reaction temperature and hydromodulus. The optimum yields, referred to the weight of double extracted OP, were 40.4% and 45.2% for sodium sulfite and sodium metabisulfite digestions, respectively. The crude celluloses were bleached with hypochlorite and oxygen. The physicochemical characterization data of these cellulose materials indicate good levels of purity, low crystallinities, good whitenesses, good water retention and moderate molecular weights. According to these specific properties the recovered celluloses could be used as fillers, water absorbents, or as raw materials for cellulose derivatives. Copyright © 2011 Elsevier Ltd. All rights reserved.

Hydrothermal pre-treatment of rapeseed straw.

PubMed

Díaz, Manuel J; Cara, Cristóbal; Ruiz, Encarnación; Romero, Inmaculada; Moya, Manuel; Castro, Eulogio

2010-04-01

As a first step for ethanol production from alternative raw materials, rapeseed straw was studied for fermentable sugar production. Liquid hot water was used as a pre-treatment method and the influence of the main pre-treatment variables was assessed. Experimental design and response surface methodology were applied using pre-treatment temperature and process time as factors. The pretreated solids were further submitted to enzymatic hydrolysis and the corresponding yields were used as pre-treatment performance evaluation. Liquid fractions obtained from pre-treatment were also characterized in terms of sugars and no-sugar composition. A mathematical model describing pre-treatment effects is proposed. Results show that enzymatic hydrolysis yields near to 100% based on pretreated materials can be achieved at 210-220 degrees C for 30-50 min, equivalent to near 70% of glucose present in the raw material. According to the mathematical model, a softer pre-treatment at 193 degrees C for 27 min results in 65% of glucose and 39% of xylose available for fermentation. Copyright 2009 Elsevier Ltd. All rights reserved.

Omics for Precious Rare Biosamples: Characterization of Ancient Human Hair by a Proteomic Approach.

PubMed

Fresnais, Margaux; Richardin, Pascale; Sepúlveda, Marcela; Leize-Wagner, Emmanuelle; Charrié-Duhaut, Armelle

2017-07-01

Omics technologies have far-reaching applications beyond clinical medicine. A case in point is the analysis of ancient hair samples. Indeed, hair is an important biological indicator that has become a material of choice in archeometry to study the ancient civilizations and their environment. Current characterization of ancient hair is based on elemental and structural analyses, but only few studies have focused on the molecular aspects of ancient hair proteins-keratins-and their conservation state. In such cases, applied extraction protocols require large amounts of raw hair, from 30 to 100 mg. In the present study, we report an optimized new proteomic approach to accurately identify archeological hair proteins, and assess their preservation state, while using a minimum of raw material. Testing and adaptation of three protocols and of nano liquid chromatography-tandem mass spectrometry (nanoLC-MS/MS) parameters were performed on modern hair. On the basis of mass spectrometry data quality, and of the required initial sample amount, the most promising workflow was selected and applied to an ancient archeological sample, dated to about 3880 years before present. Finally, and importantly, we were able to identify 11 ancient hair proteins and to visualize the preservation state of mummy's hair from only 500 μg of raw material. The results presented here pave the way for new insights into the understanding of hair protein alteration processes such as those due to aging and ecological exposures. This work could enable omics scientists to apply a proteomic approach to precious and rare samples, not only in the context of archeometrical studies but also for future applications that would require the use of very small amounts of sample.

Bioactive β-carbolines norharman and harman in traditional and novel raw materials for chicory coffee.

PubMed

Wojtowicz, Elżbieta; Zawirska-Wojtasiak, Renata; Przygoński, Krzysztof; Mildner-Szkudlarz, Sylwia

2015-05-15

The β-carboline compounds norharman and harman exhibit neuroactive activity in the human body. Chicory coffee has proved to be a source of β-carboline compounds. This study assessed the norharman and harman contents of traditional and novel raw materials for the production of chicory coffee, as well as in samples of chicory coffee with novel additives. The highest content of the β-carbolines among the traditional raw materials was recorded in roasted sugar beet (2.26 μg/g), while roasting the chicory caused a 25-fold increase in the content of norharman in this raw material (from 0.05 to 1.25 μg/g). In novel raw materials not subjected to the action of high temperature, β-carboline was not detected. Among the roasted novel raw materials, the highest contents of harman and norharman were found in artichokes. High harman levels were also recorded in roasted chokeberry. Copyright © 2014 Elsevier Ltd. All rights reserved.

Use of in vitro methods to rank surfactants for irritation potential in support of new product development.

PubMed

Casterton, P L; Potts, L F; Klein, B D

1994-08-01

11 surfactant raw materials with potential applications in light-duty liquid cleaning products were evaluated in vitro using a human skin analogue (ATS SKIN(2) Model ZK1100) for predicting cytotoxicity (MTT reduction) and inflammation [prostaglandin E(2) (PGE(2)) release]. Two of the 11 raw materials, both in the same compound family, were selected to be individually combined with each of the other nine in a 90:10 (raw:selected raw) mixture. Selection criteria were based on desired performance characteristics and low irritation potential as suggested from the individual surfactant assay data. To determine whether irritation potential was mitigated, MTT and PGE(2) scores were again determined for each of the 18 combinations with the resulting data being compared with the untreated raw material data. A plot of the data indicated that one of two selected materials may have an 'anti-irritant' effect. For raw materials with intrinsic MTT scores of less than 50 mug/ml and with the original data corrected for possible dilution effects, a statistical comparison between individual raw materials and the two sets of combinations was done using a one-sample analysis. Both cytotoxicity (MTT) and inflammation (PGE(2)) were significantly decreased by the milder of the two selected raw materials. By factoring the data into future new product decisions, this methodology has become a useful and practical tool for Amway product development.

Synopsis of utilization research on SRIC raw materials

Treesearch

John B. Crist

1983-01-01

The take-home message of this paper is this: Raw materials produced using SRIC are suitable for many reconstituted end products. Juvenility, rapid growth, and bark contents do not greatly hinder the usefulness of the raw materials. In the future, increased industrial acceptance of SRIC methods and materials should be a major thrust and is discussed.

Synthesis of adsorbent with zeolite structure from red mud and rice husk ash and its properties

NASA Astrophysics Data System (ADS)

Quyen, Dinh Thi Ngoc; Loc, Luu Cam; Ha, Huynh Ky Phuong; Nga, Dang Thi Hang; Tri, Nguyen; Van, Nguyen Thi Thuy

2017-09-01

There are many researches in the modification of red mud as adsorbent for treatment of wastewater or waste gases. Yet, most of them have to face up with a thorny problem caused by remaining alkali in red mud. In this study, the material with zeolite structure was synthesized by fusion method using red mud with the remaining alkali and rice husk ash as raw materials. It comprised alkaline fusion followed by hydrothermal treatment with step - change of synthesis temperature. The synthesized materials were characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), BET and CO2 adsorption capacity. The influences on the quality of these materialswere investigated under various calcination temperatures, calcination times and the ratios of raw materials (based on SiO2/Al2O3 ratio). The optimum reaction parameters were determined. The results depicted that the sample treated at 600 °C for 2 hours with the ratio of SiO2/Al2O3 of 1.8 had the best adsorption capacity and total specific surface area compared with the others.

7 CFR 58.735 - Quality specifications for raw materials.

Code of Federal Regulations, 2011 CFR

2011-01-01

... 7 Agriculture 3 2011-01-01 2011-01-01 false Quality specifications for raw materials. 58.735 Section 58.735 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING... specifications for raw materials. (a) Cheddar colby, washed or soaked curd, granular or stirred curd cheese...

Future Sources of Organic Raw Materials.

ERIC Educational Resources Information Center

Shapiro, Irving S.

1978-01-01

Examines the need for industrial organization, academic institutions, and national governments to agree on cooperative roles in planning the future raw materials demands of the chemical industry. Political and social concerns, as well as technical and economic considerations, are important to the raw material future of the industry. (MA)

Characterization of raw and alkali treated new natural cellulosic fiber from Coccinia grandis.L.

PubMed

Senthamaraikannan, P; Kathiresan, M

2018-04-15

The physical, chemical, tensile, crystalline, thermal, and surface morphological properties of raw and alkali treated Coccinia Grandis.L Fibers (CGFs) were characterized for the first time in this work. The results of the chemical analysis indicate that, after alkali treatment, the cellulose content of CGFs increased whereas hemicelluloses, lignin and wax contents decreased. This directly influenced the tensile strength, crystallinity index, thermal stability and the roughness of alkali-treated CGFs. The thermal stability and activation energy of the CGFs improved from 213.4 °C to 220.6 °C and 67.02 kJ/mol to 73.43 kJ/mol, respectively, due to alkali treatment. The statistical approach, Weibull distribution was adopted to analyze the tensile properties. The improved properties of the alkali treated CGF indicate that it could be an appropriate material for reinforcement in polymer composites. Copyright © 2018 Elsevier Ltd. All rights reserved.

Preparation and Characterization of Activated Carbon from Palm Kernel Shell

NASA Astrophysics Data System (ADS)

Andas, J.; Rahman, M. L. A.; Yahya, M. S. M.

2017-08-01

In this study, a high quality of activated carbon (AC) was successfully synthesized from palm kernel shell (PKS) via single step KOH activation. Several optimal conditions such as impregnation ratio and activation temperature were investigated. The prepared activated carbon under the optimum condition of impregnation ratio (1:1.5 raw/KOH) and activation temperature (800 °C) was characterized using Na2S2O3 volumetric method, CHNS/O analysis and Scanning Electron Microscope (SEM). Na2S2O3 volumetric showed an iodine number of 994.83 mgg-1 with yield % of 8.931 %. CHNS/O analysis verified an increase in C content for KOH-AC (61.10 %) in comparison to the raw PKS (47.28 %). Well-formation of porous structure was evidenced through SEM for KOH-AC. From this study, it showed a successful conversion of agricultural waste into value added porous material under benign condition.

7 CFR 58.332 - Segregation of raw material.

Code of Federal Regulations, 2010 CFR

2010-01-01

... 7 Agriculture 3 2010-01-01 2010-01-01 false Segregation of raw material. 58.332 Section 58.332 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... Procedures § 58.332 Segregation of raw material. The milk and cream received at the dairy plant shall meet...

7 CFR 58.332 - Segregation of raw material.

Code of Federal Regulations, 2011 CFR

2011-01-01

... 7 Agriculture 3 2011-01-01 2011-01-01 false Segregation of raw material. 58.332 Section 58.332 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... Procedures § 58.332 Segregation of raw material. The milk and cream received at the dairy plant shall meet...

77 FR 2662 - Airworthiness Directives; Bombardier, Inc. Airplanes

Federal Register 2010, 2011, 2012, 2013, 2014

2012-01-19

... to batches of raw material that did not meet required tensile strength. This proposed AD would..., Avox Systems Inc., revealed that the deformation was attributed to two (2) batches of raw material that... regulator on the oxygen cylinder, which was attributed to batches of raw material that did not meet required...

77 FR 31174 - Airworthiness Directives; Bombardier, Inc. Airplanes

Federal Register 2010, 2011, 2012, 2013, 2014

2012-05-25

..., which was attributed to batches of raw material that did not meet required tensile strength. This AD... the deformation was attributed to two (2) batches of raw material that did not meet the required... deformation of the pressure regulator on the oxygen cylinder, which was attributed to batches of raw material...

Influence of man-made aluminosilicate raw materials on physical and mechanical properties of building materials.

NASA Astrophysics Data System (ADS)

Volodchenko, A. A.; Lesovik, V. S.; Stoletov, A. A.; Glagolev, E. S.; Volodchenko, A. N.; Magomedov, Z. G.

2018-03-01

It has been identified that man-made aluminosilicate raw materials represented by clay rock of varied genesis can be used as energy-efficient raw materials to obtain efficient highly-hollow non-autoclaved silicate materials. A technique of structure formation in the conditions of pressureless steam treatment has been offered. Cementing compounds of non- autoclaved silicate materials based on man-made aluminosilicate raw materials possess hydraulic properties that are conditioned by the process of further formation and recrystallization of calcium silicate hydrates, which optimizes the ratio between gellike and crystalline components and densifies the cementing compound structure, which leads to improvement of performance characteristics. Increasing the performance characteristics of the obtained products is possible by changing the molding conditions. For this reason, in order to create high-density material packaging and, as a result, to increase the strength properties of the products, it is reasonable to use higher pressure, under which raw brick is formed, which will facilitate the increase of quality of highly-hollow products.

Natural manganese ore catalyst for low-temperature selective catalytic reduction of NO with NH3 in coke-oven flue gas.

PubMed

Zhu, Baozhong; Yin, Shoulai; Sun, Yunlan; Zhu, Zicheng; Li, Jiaxin

2017-11-01

Different types of manganese ore raw materials were prepared for use as catalysts, and the effects of different manganese ore raw materials and calcination temperature on the NO conversion were analyzed. The catalysts were characterized by XRF, XRD, BET, XPS, H 2 -TPR, NH 3 -TPD, and SEM techniques. The results showed that the NO conversion of calcined manganese ore with a Mn:Fe:Al:Si ratio of 1.51:1.26:0.34:1 at 450 °C reached 80% at 120 °C and 98% at 180~240 °C. The suitable proportions and better dispersibility of active ingredients, larger BET surface area, good reductibility, a lot of acid sites, contents of Mn 4+ and Fe 3+ , and surface-adsorbed oxygen played important roles in improving the NO conversion.

Upgrading nickel content of limonite nickel ore through pelletization, selective reduction and magnetic separation

NASA Astrophysics Data System (ADS)

Mayangsari, W.; Prasetyo, A. B.; Prasetiyo, Puguh

2018-04-01

Limonite nickel ore has potency to utilize as raw material for ferronickel or nickel matte, since it has low grade nickel content, thus process development is needed to find the acceptable process for upgrading nickel. The aim of this research is to determine upgrading of Ni content as result of selective reduction of limonite nickel pellet continued by magnetic separation as effect of temperature and time reduction as well as coal and CaSO4 addition. There are four steps to perform this research, such as preparation including characterization of raw ore and pelletization, selective reduction, magnetic separation and characterization of products by using AAS, XRD and SEM. Based on the result study, pellet form can upgrade 77.78% higher than powder form. Upgrading of Ni and Fe content was up to 3fold and 1.5fold respectively from raw ore used when reduced at 1100°C for 60 minutes with composition of coal and CaSO4, both 10%. The excess of CaSO4 addition caused fayalite formation. Moreover, S2 from CaSO4 also support to reach low melting point and enlardge particle size of metal formed.

PET and PVC separation with hyperspectral imagery.

PubMed

Moroni, Monica; Mei, Alessandro; Leonardi, Alessandra; Lupo, Emanuela; Marca, Floriana La

2015-01-20

Traditional plants for plastic separation in homogeneous products employ material physical properties (for instance density). Due to the small intervals of variability of different polymer properties, the output quality may not be adequate. Sensing technologies based on hyperspectral imaging have been introduced in order to classify materials and to increase the quality of recycled products, which have to comply with specific standards determined by industrial applications. This paper presents the results of the characterization of two different plastic polymers--polyethylene terephthalate (PET) and polyvinyl chloride (PVC)--in different phases of their life cycle (primary raw materials, urban and urban-assimilated waste and secondary raw materials) to show the contribution of hyperspectral sensors in the field of material recycling. This is accomplished via near-infrared (900-1700 nm) reflectance spectra extracted from hyperspectral images acquired with a two-linear-spectrometer apparatus. Results have shown that a rapid and reliable identification of PET and PVC can be achieved by using a simple two near-infrared wavelength operator coupled to an analysis of reflectance spectra. This resulted in 100% classification accuracy. A sensor based on this identification method appears suitable and inexpensive to build and provides the necessary speed and performance required by the recycling industry.

PET and PVC Separation with Hyperspectral Imagery

PubMed Central

Moroni, Monica; Mei, Alessandro; Leonardi, Alessandra; Lupo, Emanuela; La Marca, Floriana

2015-01-01

Traditional plants for plastic separation in homogeneous products employ material physical properties (for instance density). Due to the small intervals of variability of different polymer properties, the output quality may not be adequate. Sensing technologies based on hyperspectral imaging have been introduced in order to classify materials and to increase the quality of recycled products, which have to comply with specific standards determined by industrial applications. This paper presents the results of the characterization of two different plastic polymers—polyethylene terephthalate (PET) and polyvinyl chloride (PVC)—in different phases of their life cycle (primary raw materials, urban and urban-assimilated waste and secondary raw materials) to show the contribution of hyperspectral sensors in the field of material recycling. This is accomplished via near-infrared (900–1700 nm) reflectance spectra extracted from hyperspectral images acquired with a two-linear-spectrometer apparatus. Results have shown that a rapid and reliable identification of PET and PVC can be achieved by using a simple two near-infrared wavelength operator coupled to an analysis of reflectance spectra. This resulted in 100% classification accuracy. A sensor based on this identification method appears suitable and inexpensive to build and provides the necessary speed and performance required by the recycling industry. PMID:25609050

The effect of activation agent on surface morphology, density and porosity of palm shell and coconut shell activated carbon

NASA Astrophysics Data System (ADS)

Leman, A. M.; Zakaria, S.; Salleh, M. N. M.; Sunar, N. M.; Feriyanto, D.; Nazri, A. A.

2017-09-01

Activated carbon (AC) has one of the promising alternative technology for filtration and adsorption process. It inexpensive material because the sources is abundant especially in Malaysia. Main purpose of this project is to develop AC by chemical activation process to improve adsorption capacity by improving porosity of AC. AC developed via carbonization using designed burner at temperature of 650°C to 850 °C and activated by Potassium Hydroxide (KOH) in 12 hour and then dried at temperature of 300°C. Characterization and analysis is conducted by Scanning Electron Microscopy (SEM) for surface morphology analysis, Energy Dispersive Spectroscopy (EDS) for composition analysis, density and porosity analysis. Results shows that uneven surface has been observed both of AC and non-AC and also AC shows higher porosity as compared to non-AC materials. Density value of raw material has lower than AC up to 11.67% and 47.54% and porosity of raw material has higher than AC up to 31.45% and 45.69% for palm shell and coconut shell AC. It can be concluded that lower density represent higher porosity of material and higher porosity indicated higher adsorption capacity as well.

76 FR 62447 - Importer of Controlled Substances; Notice of Registration

Federal Register 2010, 2011, 2012, 2013, 2014

2011-10-07

... narcotic raw material are not appropriate. With regard to all non-Narcotic Raw Material drugs on this...-phenethyl-4-piperidine (8333)... II Phenylacetone (8501) II Opium, raw (9600) II Poppy Straw Concentrate...

Chemical analysis of raw and processed Fructus arctii by high-performance liquid chromatography/diode array detection-electrospray ionization-mass spectrometry

PubMed Central

Qin, Kunming; Liu, Qidi; Cai, Hao; Cao, Gang; Lu, Tulin; Shen, Baojia; Shu, Yachun; Cai, Baochang

2014-01-01

Background: In traditional Chinese medicine (TCM), raw and processed herbs are used to treat the different diseases. Fructus Arctii, the dried fruits of Arctium lappa l. (Compositae), is widely used in the TCM. Stir-frying is the most common processing method, which might modify the chemical compositions in Fructus Arctii. Materials and Methods: To test this hypothesis, we focused on analysis and identification of the main chemical constituents in raw and processed Fructus Arctii (PFA) by high-performance liquid chromatography/diode array detection-electrospray ionization-mass spectrometry. Results: The results indicated that there was less arctiin in stir-fried materials than in raw materials. however, there were higher levels of arctigenin in stir-fried materials than in raw materials. Conclusion: We suggest that arctiin reduced significantly following the thermal conversion of arctiin to arctigenin. In conclusion, this finding may shed some light on understanding the differences in the therapeutic values of raw versus PFA in TCM. PMID:25422559

Raw materials in the manufacture of biotechnology products: regulatory considerations.

PubMed

Cordoba-Rodriguez, Ruth

2010-01-01

The Food and Drug Administration's Pharmaceutical cGMPs for the 21st Century initiative emphasizes science and risk-based approaches in the manufacture of drugs. These approaches are reflected in the International Conference on Harmonization (ICH) guidances ICH Q8, Q9, and Q10 and encourage a comprehensive assessment of the manufacture of a biologic, including all aspects of manufacture that have the potential to affect the finished drug product. Appropriate assessment and management of raw materials are an important part of this initiative. Ideally, a raw materials program should strive to assess and minimize the risk to product quality. With this in mind, risk-assessment concepts and control strategies will be discussed and illustrated by examples, with an emphasis on the impact of raw materials on cell substrates. Finally, the life cycle of the raw material will be considered, including its potential to affect the drug product life cycle. In this framework, the supply chain and the vendor-manufacturer relationship will be explored as important parts of an adequate raw materials control strategy.

Worldwide Mycotoxins Exposure in Pig and Poultry Feed Formulations

PubMed Central

Guerre, Philippe

2016-01-01

The purpose of this review is to present information about raw materials that can be used in pig and poultry diets and the factors responsible for variations in their mycotoxin contents. The levels of mycotoxins in pig and poultry feeds are calculated based on mycotoxin contamination levels of the raw materials with different diet formulations, to highlight the important role the stage of production and the raw materials used can have on mycotoxins levels in diets. Our analysis focuses on mycotoxins for which maximum tolerated levels or regulatory guidelines exist, and for which sufficient contamination data are available. Raw materials used in feed formulation vary considerably depending on the species of animal, and the stage of production. Mycotoxins are secondary fungal metabolites whose frequency and levels also vary considerably depending on the raw materials used and on the geographic location where they were produced. Although several reviews of existing data and of the literature on worldwide mycotoxin contamination of food and feed are available, the impact of the different raw materials used on feed formulation has not been widely studied. PMID:27886128

Raw material ‘criticality’—sense or nonsense?

NASA Astrophysics Data System (ADS)

Frenzel, M.; Kullik, J.; Reuter, M. A.; Gutzmer, J.

2017-03-01

The past decade has seen a resurgence of interest in the supply security of mineral raw materials. A key to the current debate is the concept of ‘criticality’. The present article reviews the criticality concept, as well as the methodologies used in its assessment, including a critical evaluation of their validity in view of classical risk theory. Furthermore, it discusses a number of risks present in global raw materials markets that are not captured by most criticality assessments. Proposed measures for the alleviation of these risks are also presented. We find that current assessments of raw material criticality are fundamentally flawed in several ways. This is mostly due to a lack of adherence to risk theory, and highly limits their applicability. Many of the raw materials generally identified as critical are probably not critical. Still, the flaws of current assessments do not mean that the general issue of supply security can simply be ignored. Rather, it implies that new assessments are required. While the basic theoretical framework for such assessments is outlined in this review, detailed method development will require a major collaborative effort between different disciplines along the raw materials value chain. In the opinion of the authors, the greatest longer-term challenge in the raw materials sector is to stop, or counteract the effects of, the escalation of unit energy costs of production. This issue is particularly pressing due to its close link with the renewable energy transition, requiring more metal and mineral raw materials per unit energy produced. The solution to this problem will require coordinated policy action, as well as the collaboration of scientists from many different fields—with physics, as well as the materials and earth sciences in the lead.

Characterization of industrial wastes as raw materials for Emulsified Modified Bitumen (EMB) formulation

NASA Astrophysics Data System (ADS)

Najib Razali, Mohd; Isa, Syarifah Nur Ezatie Mohd; Salehan, Noor Adilah Md; Musa, Musfafikri; Aziz, Mohd Aizudin Abd; Nour, Abdurahman Hamid; Yunus, Rosli Mohd

2018-04-01

This study was conducted to characterize industrial wastes for formulation of emulsified modified bitumen (EMB) in relation to their physical characteristic and elemental composition. This analysis will give information either raw materials from industrial wastes can be used for EMB formulation. Bitumen is produced from crude oil that is extracted from the ground which categorizes the crude oil as one of the non-renewable form of product. A vast environmental problem issues arises in Malaysia cause by the excessive manufacturing activity that lead to a miss-management of industrial waste has leads to the used of industrial waste in the EMB formulation. Industrial waste such as polystyrene, polyethylene and used automotive oil can be used as alternative to formulate bitumen. Then a suitable emulsifier needs to be added to produce the final product which is EMB. The emulsifier will yield a charge depends on its properties to bind the oily bitumen with water. Physical characteristic studies were performed by thermogravimetric Analysis (TGA), differential scanning calorimetry (DSC), flash point test, density rest and moisture content test. Fourier Transform Infrared Spectroscopy (FTIR) analysis was measured to determine the material’s molecular composition and structure.

Structural characterization of lignin in the process of cooking of cornstalk with solid alkali and active oxygen.

PubMed

Yang, Qiulin; Shi, Jianbin; Lin, Lu; Zhuang, Junping; Pang, Chunsheng; Xie, Tujun; Liu, Ying

2012-05-09

A novel, efficient, and environmentally friendly technology is used in cornstalk cooking, active oxygen (O₂ and H₂O₂) cooking with solid alkali (MgO). After the cooking, the milled wood lignin in the raw material and pulp and the water-soluble and insoluble lignin in the yellow liquor were all characterized by attenuated total reflectance Fourier transform infrared spectroscopy and two-dimensional heteronuclear single-quantum coherence NMR. The results showed that the cooking procedure with solid alkali and active oxygen had a high selectivity for delignification, which could remove 85.5% of the lignin from the raw material. The syringyl (S/S'/S') units could be dissolved preferentially because of their high reactivity, and a novel guaiacyl unit with a carbonyl group (G') was generated in the cooking process. Moreover, during the cooking, the β-O-4' (A/A'/A″) structures as the main side-chain linkages in all the lignins could be partly broken and the β-O-4' (A') with a ring-conjugated structure was readily attacked by oxygen, whereas the H unit and β-5' and β-β' structures were found to stay stable without characteristic reaction.

Characterization of impurities present on Tihimatine (Hoggar) quartz, Algeria

NASA Astrophysics Data System (ADS)

Anas Boussaa, S.; Kheloufi, A.; Boutarek Zaourar, N.

2017-11-01

Many of today's advanced materials depend on quartz as a raw material. Quartz usually contains abundant inclusions, both solid and liquid, and due to the number of these inclusions and their small size, complete separation is most difficult. Typical properties of raw quartz that must be characterized are: Size and Chemical composition of inclusions, their spatial distribution, localization of isomorphic substitutional elements (e.g. Al, Fe). The aim of this study has been to test experimental methods for investigating some inclusions (impurities) present in the Tihimatine quartz from El Hoggar region deposits (southern Algeria) using X Ray Fluorescence, scanning electron microscopy, optical Microscopy with reflected and transmitted lights, infra-red spectrometer, Raman spectrometer. Despite the high concentration of SiO2 in studied quartz reaching 98%, several harmful inclusions were found and identified as hematite, anatase, muscovite, graphite, it contains: Fe, Ti, Al, K, Ca. Some fluid inclusions were found. We detect the presence of carbon dioxide and water using raman spectroscopy. The repartition of solid impurities is aleatory and not homogeneous with maximum size of 10 μm. Concerning the fluid impurities, their diameter vary between 5 and 20 μm and their repartition is aleatory.

Analysis of hard coal quality for narrow size fraction under 20 mm

NASA Astrophysics Data System (ADS)

Niedoba, Tomasz; Pięta, Paulina

2018-01-01

The paper presents the results of an analysis of hard coal quality diversion in narrow size fraction by using taxonomic methods. Raw material samples were collected in selected mines of Upper Silesian Industrial Region and they were classified according to the Polish classification as types 31, 34.2 and 35. Then, each size fraction was characterized in terms of the following properties: density, ash content, calorific content, volatile content, total sulfur content and analytical moisture. As a result of the analysis it can be stated that the best quality in the entire range of the tested size fractions was the 34.2 coking coal type. At the same time, in terms of price parameters, high quality of raw material characterised the following size fractions: 0-6.3 mm of 31 energetic coal type and 0-3.15 mm of 35 coking coal type. The methods of grouping (Ward's method) and agglomeration (k-means method) have shown that the size fraction below 10 mm was characterized by higher quality in all the analyzed hard coal types. However, the selected taxonomic methods do not make it possible to identify individual size fraction or hard coal types based on chosen parameters.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Litchfield, J.W.; Watts, R.L.; Gurwell, W.E.

A materials assessment methodology for identifying specific critical material requirements that could hinder the implementation of solar energy has been developed and demonstrated. The methodology involves an initial screening process, followed by a more detailed materials assessment. The detailed assessment considers such materials concerns and constraints as: process and production constraints, reserve and resource limitations, lack of alternative supply sources, geopolitical problems, environmental and energy concerns, time constraints, and economic constraints. Data for 55 bulk and 53 raw materials are currently available on the data base. These materials are required in the example photovoltaic systems. One photovoltaic system and thirteenmore » photovoltaic cells, ten solar heating and cooling systems, and two agricultural and industrial process heat systems have been characterized to define their engineering and bulk material requirements.« less

Renewable resources in the chemical industry--breaking away from oil?

PubMed

Nordhoff, Stefan; Höcker, Hans; Gebhardt, Henrike

2007-12-01

Rising prices for fossil-based raw materials suggest that sooner or later renewable raw materials will, in principle, become economically viable. This paper examines this widespread paradigm. Price linkages like those seen for decades particularly in connection with petrochemical raw materials are now increasingly affecting renewable raw materials. The main driving force is the competing utilisation as an energy source because both fossil-based and renewable raw materials are used primarily for heat, electrical power and mobility. As a result, prices are determined by energy utilisation. Simple observations show how prices for renewable carbon sources are becoming linked to the crude oil price. Whether the application calls for sugar, starch, virgin oils or lignocellulose, the price for the raw material rises with the oil price. Consequently, expectations regarding price trends for fossil-based energy sources can also be utilised for the valuation of alternative processes. However, this seriously calls into question the assumption that a rising crude oil price will favour the economic viability of alternative products and processes based on renewable raw materials. Conversely, it follows that these products and processes must demonstrate economic viability today. Especially in connection with new approaches in white biotechnology, it is evident that, under realistic assumptions, particularly in terms of achievable yields and the optimisation potential of the underlying processes, the route to utilisation is economically viable. This makes the paradigm mentioned at the outset at least very questionable.

Use of raw materials in the United States from 1900 through 2014

USGS Publications Warehouse

Matos, Grecia R.

2017-08-22

The economic growth of an industrialized nation such as the United States requires raw materials for construction (buildings, bridges, highways, and so forth), defense, and processing and manufacture of goods and services. Since the beginning of the 20th century, the types and quantities of raw materials used have increased and changed significantly. This fact sheet quantifies the amounts of raw materials (other than food and fuel) that have been used in the U.S. economy annually for a period of 115 years, from 1900 through 2014. It provides a broad overview of the quantity (weight) of nonfood and nonfuel materials used in the economy and illustrates the use and significance of raw nonfuel minerals in particular as building blocks of society.These data have been compiled to help the public and policymakers understand the changing annual flow of raw materials put into use in the United States. Such information can be helpful in assessing the potential effects of materials use on the environment, assessing materials’ intensity of use, and examining the role that these materials play in the economy. The data presented indicate the substitution and shift in materials usage from renewable to nonrenewable materials during the 20th century. The disaggregated quantities by commodity (not shown in this fact sheet) may be tested against supply adequacy and end of life issues.

NASA-JSC Protocol for the Characterization of Single Wall Carbon Nanotube Material Quality

NASA Technical Reports Server (NTRS)

Arepalli, Sivaram; Nikolaev, Pasha; Gorelik, Olga; Hadjiev, Victor; Holmes, William; Devivar, Rodrigo; Files, Bradley; Yowell, Leonard

2010-01-01

It is well known that the raw as well as purified single wall carbon nanotube (SWCNT) material always contain certain amount of impurities of varying composition (mostly metal catalyst and non-tubular carbon). Particular purification method also creates defects and/or functional groups in the SWCNT material and therefore affects the its dispersability in solvents (important to subsequent application development). A number of analytical characterization tools have been used successfully in the past years to assess various properties of nanotube materials, but lack of standards makes it difficult to compare these measurements across the board. In this work we report the protocol developed at NASA-JSC which standardizes measurements using TEM, SEM, TGA, Raman and UV-Vis-NIR absorption techniques. Numerical measures are established for parameters such as metal content, homogeneity, thermal stability and dispersability, to allow easy comparison of SWCNT materials. We will also report on the recent progress in quantitative measurement of non-tubular carbon impurities and a possible purity standard for SWCNT materials.

Contamination of the cement raw material in a quarry site by seawater intrusion, Darica-Turkey

NASA Astrophysics Data System (ADS)

Camur, M. Zeki; Doyuran, Vedat

2008-02-01

The open pit mining nearby shoreline is planned to be extended into below sea level in order to use additional reserves of the cement raw material (marl). The raw material is currently contaminated by seawater intrusion below a depth of 20 m up to the distance of 90 m from shoreline. Seawater intrusion related contamination of the material used for the cement production was investigated by means of diffusion process for the future two below sea level mining scenarios covering 43 years of period. According to the results, chloride concentrations higher than the tolerable limit of a cement raw material would be present in the material about 10-25 cm inward from each discontinuity surface, controlling groundwater flow, located between 170 and 300 m landward from the shoreline at below sea level mining depths of 0-30 m. The estimations suggest that total amounts of dilution required for the contaminated raw material to reduce its concentration level to the tolerance limit with uncontaminated raw material are about 113- to 124-fold for scenario I (13 years of below sea level mining after 30 years of above sea level mining) and about 126- to 138-fold for scenario II (43 years of simultaneous above and below sea level minings).

77 FR 21532 - Glycine From the People's Republic of China: Preliminary Partial Affirmative Determination of...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-04-10

... because it is producing glycine from raw materials of Indian origin and exporting such merchandise to the... find that there is no record evidence that AICO self produces glycine from Indian raw materials... exported to the United States glycine that it produced only from Indian raw materials. For a complete...

78 FR 69130 - Importer of Controlled Substances; Notice of Application: Johnson Matthey, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2013-11-18

... Concentrate (9670) II The company plans to import the listed controlled substances as raw materials, to be... requests for hearings on applications to import narcotic raw material are not appropriate. 72 FR 3417 (2007). In reference to the non-narcotic raw material, the company plans to import gram amounts to be used as...

Effect of Sintering Temperature to Physical, Magnetic Properties and Crystal Structure on Permanent Magnet BaFe12O19 Prepared From Mill Scale

NASA Astrophysics Data System (ADS)

Ramlan; Muljadi; Sardjono, Priyo; Gulo, Fakhili; Setiabudidaya, Dedi

2017-07-01

Permanent magnet of Barium hexa Ferrite with formula BaFe12O19 has been made by metallurgy powder method from raw materials : Barium carbonate (BaCO3 E-merck) and Iron Oxide (Fe2O3 from mill scale). Both of raw materials have been mixed with stoichiometry composition by using a ball mill for 24 hours. The fine powder obtained from milling process was formed by using a hydraulic press at pressure 50 MPa and continued with sintering process. The sintering temperature was varied : 1150°C, 1200°C, 1250°C and 1300°C with holding time for 1 hour. The sintered samples were characterized such as : physical properties (bulk density, porosity and shrinkage), magnetic properties (flux density, remanence, coercivity and magnetic saturation) by using VSM and crystal structure by using XRD. According characterization results show that the crystal structure of BaFe12O19 does not change after sintering process, but the grain size tends to increase. The optimum condition is achieved at temperature 1250°C, and at this condition, the sample has characterization such as : bulk density = 4.35 g/cm3, porosity = 1.03% and firing shrinkage = 11.63%, flux density = 681.1 Gauss, remanence (σr) = 20.78 emu/g, coercivity (Hc) = 2058 Oe and magnetic saturation (σs) 45.16 emu/g.

Accuracy of the raw-data-based effective atomic numbers and monochromatic CT numbers for contrast medium with a dual-energy CT technique.

PubMed

Kawahara, Daisuke; Ozawa, Shuichi; Yokomachi, Kazushi; Tanaka, Sodai; Higaki, Toru; Fujioka, Chikako; Suzuki, Tatsuhiko; Tsuneda, Masato; Nakashima, Takeo; Ohno, Yoshimi; Nagata, Yasushi

2018-02-01

To evaluate the accuracy of raw-data-based effective atomic number (Z eff ) values and monochromatic CT numbers for contrast material of varying iodine concentrations, obtained using dual-energy CT. We used a tissue characterization phantom and varying concentrations of iodinated contrast medium. A comparison between the theoretical values of Z eff and that provided by the manufacturer was performed. The measured and theoretical monochromatic CT numbers at 40-130 keV were compared. The average difference between the Z eff values of lung (inhale) inserts in the tissue characterization phantom was 81.3% and the average Z eff difference was within 8.4%. The average difference between the Z eff values of the varying concentrations of iodinated contrast medium was within 11.2%. For the varying concentrations of iodinated contrast medium, the differences between the measured and theoretical monochromatic CT values increased with decreasing monochromatic energy. The Z eff and monochromatic CT numbers in the tissue characterization phantom were reasonably accurate. The accuracy of the raw-data-based Z eff values was higher than that of image-based Z eff values in the tissue-equivalent phantom. The accuracy of Z eff values in the contrast medium was in good agreement within the maximum SD found in the iodine concentration range of clinical dynamic CT imaging. Moreover, the optimum monochromatic energy for human tissue and iodinated contrast medium was found to be 70 keV. Advances in knowledge: The accuracy of the Z eff values and monochromatic CT numbers of the contrast medium created by raw-data-based, dual-energy CT could be sufficient in clinical conditions.

Thorium and Uranium in the Rock Raw Materials Used For the Production of Building Materials

NASA Astrophysics Data System (ADS)

Pękala, Agnieszka

2017-10-01

Thorium and uranium are constant components of all soils and most minerals thereby rock raw materials. They belong to the particularly dangerous elements because of their natural radioactivity. Evaluation of the content of the radioactive elements in the rock raw materials seems to be necessary in the early stage of the raw material evaluation. The rock formations operated from deposits often are accumulated in landfills and slag heaps where the concentration of the radioactive elements can be many times higher than under natural conditions. In addition, this phenomenon may refer to buildings where rock raw materials are often the main components of the construction materials. The global control system of construction products draws particular attention to the elimination of used construction products containing excessive quantities of the natural radioactive elements. In the presented study were determined the content of thorium and uranium in rock raw materials coming from the Bełachatów lignite deposit. The Bełchatów lignite deposit extracts mainly lignite and secondary numerous accompanying minerals with the raw material importance. In the course of the field works within the framework of the carried out work has been tested 92 samples of rocks of varied petrographic composition. There were carried out analyses of the content of the radioactive elements for 50 samples of limestone of the Jurassic age, 18 samples of kaolinite clays, and 24 samples of siliceous raw materials, represented by opoka-rocks, diatomites, gaizes and clastic rocks. The measurement of content of the natural radioactive elements thorium and uranium based on measuring the frequency counts of gamma quantum, recorded separately in measuring channels. At the same time performed measurements on volume patterns radioactive: thorium and uranium. The studies were carried out in Mazar spectrometer on the powdered material. Standardly performed ten measuring cycles, after which were calculated the concentration of radioactive elements in the sample. The highest concentration of thorium and uranium has been found in the clayey raw material. Their value was respectively from 8 to 12 mg/kg for thorium and from 2.3 to 3.5 mg/kg for uranium. In carbonate sediments the content of thorium was at the level from 0.5 to 2.1 mg/kg and uranium from 0.5-2.2 mg/kg. From a group of the siliceous raw materials the diatomite had a highest concentrations of radioactive elements where the content of thorium was from 1.5 to 1.8 mg/kg and uranium from 1.3 to 1.7 mg/kg.

Characterization of functionalized multiwalled carbon nanotubes for use in an enzymatic sensor.

PubMed

Guadarrama-Fernández, Leonor; Chanona-Pérez, Jorge; Manzo-Robledo, Arturo; Calderón-Domínguez, Georgina; Martínez-Rivas, Adrián; Ortiz-López, Jaime; Vargas-García, Jorge Roberto

2014-10-01

Carbon nanotubes (CNT) have proven to be materials with great potential for the construction of biosensors. Development of fast, simple, and low cost biosensors to follow reactions in bioprocesses, or to detect food contaminants such as toxins, chemical compounds, and microorganisms, is presently an important research topic. This report includes microscopy and spectroscopy to characterize raw and chemically modified multiwall carbon nanotubes (MWCNTs) synthesized by chemical vapor deposition with the intention of using them as the active transducer in bioprocessing sensors. MWCNT were simultaneously purified and functionalized by an acid mixture involving HNO3-H2SO4 and amyloglucosidase attached onto the chemically modified MWCNT surface. A 49.0% decrease in its enzymatic activity was observed. Raw, purified, and enzyme-modified MWCNTs were analyzed by scanning and transmission electron microscopy and Raman and X-ray photoelectron spectroscopy. These studies confirmed purification and functionalization of the CNTs. Finally, cyclic voltammetry electrochemistry was used for electrical characterization of CNTs, which showed promising results that can be useful for construction of electrochemical biosensors applied to biological areas.

A membrane-integrated fermentation reactor system: its effects in reducing the amount of sub-raw materials for D-lactic acid continuous fermentation by Sporolactobacillus laevolacticus.

PubMed

Mimitsuka, Takashi; Na, Kyungsu; Morita, Ken; Sawai, Hideki; Minegishi, Shinichi; Henmi, Masahiro; Yamada, Katsushige; Shimizu, Sakayu; Yonehara, Tetsu

2012-01-01

Continuous fermentation by retaining cells with a membrane-integrated fermentation reactor (MFR) system was found to reduce the amount of supplied sub-raw material. If the amount of sub-raw material can be reduced, continuous fermentation with the MFR system should become a more attractive process for industrialization, due to decreased material costs and loads during the refinement process. Our findings indicate that the production rate decreased when the amount of the sub-raw material was reduced in batch fermentation, but did not decrease during continuous fermentation with Sporolactobacillus laevolacticus. Moreover, continuous fermentation with a reduced amount of sub-raw material resulted in a productivity of 11.2 g/L/h over 800 h. In addition, the index of industrial process applicability used in the MFR system increased by 6.3-fold as compared with the conventional membrane-based fermentation reactor previously reported, suggesting a potential for the industrialization of this D-lactic acid continuous fermentation process.

Preparation and Characterization of Mesoporous Zirconia Made by Using a Poly (methyl methacrylate) Template

NASA Astrophysics Data System (ADS)

Duan, Guorong; Zhang, Chunxiang; Li, Aimei; Yang, Xujie; Lu, Lude; Wang, Xin

2008-03-01

Superfine powders of poly (methyl methacrylate) (PMMA) have been prepared by means of an emulsion polymerization method. These have been used as templates in the synthesis of tetragonal phase mesoporous zirconia by the sol gel method, using zirconium oxychloride and oxalic acid as raw materials. The products have been characterized by infrared spectroscopy, X-ray diffraction analysis, transmission electron microscopy, N2 adsorption-desorption isotherms, and pore size distribution. The results indicate that the average pore size was found to be 3.7 nm.

75 FR 67788 - Self-Regulatory Organizations; The NASDAQ Stock Market LLC; Notice of Filing of Proposed Rule...

Federal Register 2010, 2011, 2012, 2013, 2014

2010-11-03

... Business Plan is to Purchase and Stockpile Raw Materials or Other Commodities In the case of a Company... stockpile quantities of a raw material or other commodity (``commodity stockpiling companies'' or ``CSCs... invest at least 85% of the net proceeds of the initial public offering in the raw material or other...

Management and characteristics of recycled manure solids used for bedding in Midwest freestall dairy herds.

PubMed

Husfeldt, A W; Endres, M I; Salfer, J A; Janni, K A

2012-04-01

Interest in using recycled manure solids (RMS) as a bedding material for dairy cows has grown in the US Midwest. Cost of common bedding materials has increased in recent years and availability has decreased. Information regarding the composition of RMS and its use as a bedding material for dairy cows in the Midwest is very limited. The objectives of this study were to characterize RMS as a bedding material, observe bedding management practices, document methods of obtaining RMS, and describe housing facilities. We visited 38 Midwest dairy operations bedding freestalls with RMS to collect data. Methods of obtaining RMS for bedding included separation of anaerobic digested manure, separation of raw manure, and separation of raw manure followed by mechanical drum-composting for 18 to 24 h. Average bedding moisture of unused RMS was 72.4% with a pH of 9.16. Unused samples contained (on a dry basis) 1.4% N, 44.9% C, 32.7C:N ratio, 0.44% P, 0.70% K, 76.5% neutral detergent fiber, 9.4% ash, 4.4% nonfiber carbohydrates, and 1.1% fat. Moisture was lowest for drum-composted solids before and after use as freestall bedding. After use in the stalls, digested solids had lower neutral detergent fiber content (70.5%) than drum-composted (75.0%) and separated raw (73.1%) solids. Total N content was greater in digested solids (2.0%) than in separated raw (1.7%) solids. Total bacterial populations in unused bedding were greatest in separated raw manure solids but were similar between digested and drum-composted manure solids. Drum-composted manure solids had no coliform bacteria before use as freestall bedding. After use as bedding, digested manure solids had lower total bacteria counts compared with drum-composted and separated raw manure solids, which had similar counts. Used bedding samples of digested solids contained fewer environmental streptococci than drum-composted and separated raw solids and had reduced Bacillus counts compared with separated raw solids. Coliform counts were similar for all 3 bedding sources. Addition of a mechanical blower post-separation and use of a shelter for storage were associated with reduced fresh-bedding moisture but not associated with bacterial counts. This was the first survey of herds using RMS for bedding in the Midwest. We learned that RMS was being used successfully as a source of bedding for dairy cows. For most farms in the study, somatic cell count was comparable to the average in the region and not excessively high. Copyright © 2012 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

Peculiarities of non-autoclaved lime wall materials production using clays

NASA Astrophysics Data System (ADS)

Volodchenko, A. A.; Lesovik, V. S.; Cherepanova, I. A.; Volodchenko, A. N.; Zagorodnjuk, L. H.; Elistratkin, M. Y.

2018-03-01

At present, the development and implementation of energy saving technologies for building materials production, which correspond to modern trends of «green» technologies, become ever more popular. One of the most widely spread wall materials today is a lime brick and stones. The primary raw goods used in production of such materials are quarziferous rocks. However, they have some disadvantages, including low strength index at the intermediate phase of their production, especially in case with a raw brick, which is an issue in the production of high-hollow goods due to low strength index of raw materials and the nonoptimal matrix structure. The conducted experiments confirmed the possibility to control structurization of building composites due to application of nonconventional argillous raw materials. Besides, the material and mineral composition of nonconventional clay rocks ensures the optimal microstructure thus providing for the production of efficient wall building materials via energy saving technology.

Industry trends in chip storage and handling

Treesearch

Tim McDonald; Alastair Twaddle

2000-01-01

A survey was conducted of US pulp and paper mills to characterize chip pile management trends. The survey was developed by members of the TAPPI Fiber Raw Material Supply Committee and mailed out in December of 1999. There were a total of 80 respondents to the survey. A typical mill was foudn to maintain one sofhvood and one hardwood chip pile, with maximum inventory of...

One step sintering of homogenized bauxite raw material and kinetic study

NASA Astrophysics Data System (ADS)

Gao, Chang-he; Jiang, Peng; Li, Yong; Sun, Jia-lin; Zhang, Jun-jie; Yang, Huan-ying

2016-10-01

A one-step sintering process of bauxite raw material from direct mining was completed, and the kinetics of this process was analyzed thoroughly. The results show that the sintering kinetics of bauxite raw material exhibits the liquid-phase sintering behavior. A small portion of impurities existed in the raw material act as a liquid phase. After X-ray diffraction analyses, scanning electron microscopy observations, and kinetics calculations, sintering temperature and heating duration were determined as the two major factors contributing to the sintering process and densification of bauxite ore. An elevated heating temperature and longer duration favor the densification process. The major obstacle for the densification of bauxite material is attributed to the formation of the enclosed blowhole during liquid-phase sintering.

Tracing and control of raw materials sourcing for vaccine manufacturers.

PubMed

Faretra Peysson, Laurence

2010-05-01

The control of the raw materials used to manufacture vaccines is mandatory; therefore, a very clear process must be in place to guarantee that raw materials are traced. Those who make products or supplies used in vaccine manufacture (suppliers of culture media, diagnostic tests, etc.) must apply quality systems proving that they adhere to certain standards. ISO certification, Good Manufacturing Practices for production sites and the registration of culture media with a 'Certificate of Suitability' from the European Directorate for the Quality of Medicines and Healthcare are reliable quality systems pertaining to vaccine production. Suppliers must assure that each lot of raw materials used in a product that will be used in vaccine manufacture adheres to the level of safety and traceability required. Incoming materials must be controlled in a single 'Enterprise Resource Planning' system which is used to document important information, such as the assignment of lot number, expiration date, etc. Ingredients for culture media in particular must conform to certain specifications. The specifications that need to be checked vary according to the ingredient, based on the level of risk. The way a raw material is produced is also important, and any aspect relative to cross-contamination, such as the sanitary measures used in producing and storing the raw material must be checked as well. In addition, suppliers can reduce the risk of viral contamination of raw materials by avoiding purchases in countries where a relevant outbreak is currently declared. 2010 The International Association for Biologicals. Published by Elsevier Ltd. All rights reserved.

40 CFR 428.62 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.42 0.15... material) Lead 0.0017 0.0007 English units (lb/1,000 lb of raw material) Lead 0.0017 0.0007 (c) The...

Synthesis and characterization of SBA-3, SBA-15, and SBA-1 nanostructured catalytic materials.

PubMed

Anunziata, Oscar A; Beltramone, Andrea R; Martínez, Maria L; Belon, Lizandra López

2007-11-01

A highly ordered large pore mesoporous silica molecular sieve SBA-3, SBA-15, Al-SBA-15, and SBA-1, were developed and characterized by XRD, BET, FTIR, SEM, and NMR-MAS. The catalytic materials were synthesized using different raw materials and operation conditions. These materials contain a regular arrangement of uniform channels with diameters between 1.8 and 10 nm, high specific surface area and high specific pore volume. The designed methods were effective for the synthesis, presenting each mesostructured materials, patterns of XRD and other characteristics corresponding to the reported ones in literature. The new route employed to synthesize Al-SBA-15, generates a catalyst with only aluminum in tetrahedral form, according to the data of (27)Al NMR-MAS. However, several reports indicated that the coordination of the Al atoms changes below the Si/Al ratio of 45, presenting peaks corresponding to penta and hexa-coordinated aluminum, which are absent in our samples (Si/Al = 50 and 33).

Statistical Analyses of Raw Material Data for MTM45-1/CF7442A-36% RW: CMH Cure Cycle

NASA Technical Reports Server (NTRS)

Coroneos, Rula; Pai, Shantaram, S.; Murthy, Pappu

2013-01-01

This report describes statistical characterization of physical properties of the composite material system MTM45-1/CF7442A, which has been tested and is currently being considered for use on spacecraft structures. This composite system is made of 6K plain weave graphite fibers in a highly toughened resin system. This report summarizes the distribution types and statistical details of the tests and the conditions for the experimental data generated. These distributions will be used in multivariate regression analyses to help determine material and design allowables for similar material systems and to establish a procedure for other material systems. Additionally, these distributions will be used in future probabilistic analyses of spacecraft structures. The specific properties that are characterized are the ultimate strength, modulus, and Poisson??s ratio by using a commercially available statistical package. Results are displayed using graphical and semigraphical methods and are included in the accompanying appendixes.

Oat raw materials and bakery products - amino acid composition and celiac immunoreactivity.

PubMed

Mickowska, Barbara; Litwinek, Dorota; Gambuś, Halina

2016-01-01

The aim of this study was to compare the biochemical and immunochemical properties of avenins in some special oat raw materials and additionally the possibility of using them as a raw material for the gluten-free bakery products. The compared oat raw materials were - oat flakes, commercial oat flours (including gluten-free oat flour) and residual oat flour, which is by-product of β-glucan preparation. Biochemical characteristic included amino acid compositions and SDS-PAGE profiles of extracted avenins. The immunochemical reactivity with polyclonal anti-gluten and monoclonal anti-gliadin antibodies was evaluated qualitatively and quantitatively by immunoblotting and ELISA methods. Additionally, experimental bakery products made of examined raw materials were assessed according to their suitability for the celiac patients' diet. The highest protein content was measured in the β-glucan preparation "Betaven" and gluten-free oat flour. Proteins of all materials are rich in glutamic and aspartic acid, leucine and arginine. Proportions of amino acids in avenins extracted from most of oat raw materials are similar, excluding gluten-free oat flour, which has a very low avenin content and proportions of individual amino acids are different. The SDS-PAGE protein pattern consisted of proteins with molecular weight of about 25-35 kDa. Polyclonal anti-gluten anti-body recognized all protein fractions of molecular weight higher than 20 kDa. Quantitative ELISA analysis shows that the majority of samples has a gliadin-like protein content within the range of 80-260 mg/kg, excluding gluten-free flours and corresponding bakery products. Altogether, β-glucan preparation has extremely high level of gliadin-like proteins. In the examined oat raw materials and foods the contents of immunoreactive amino acid sequences exceeded the limit of 20 mg/kg (considered as gluten-free) except for gluten-free flours (oat and  the prepared mixture) and the bakery products based on gluten-free flours. Unfortunately, the rest of oat raw materials and products cannot be considered gluten-free.

Effects of limestone petrography and calcite microstructure on OPC clinker raw meals burnability

NASA Astrophysics Data System (ADS)

Galimberti, Matteo; Marinoni, Nicoletta; Della Porta, Giovanna; Marchi, Maurizio; Dapiaggi, Monica

2017-10-01

Limestone represents the main raw material for ordinary Portland cement clinker production. In this study eight natural limestones from different geological environments were chosen to prepare raw meals for clinker manufacturing, aiming to define a parameter controlling the burnability. First, limestones were characterized by X-Ray Fluorescence, X-Ray Powder Diffraction and Optical Microscopy to assess their suitability for clinker production and their petrographic features. The average domains size and the microstrain of calcite were also determined by X-Ray Powder Diffraction line profile analysis. Then, each limestone was admixed with clay minerals to achieve the adequate chemical composition for clinker production. Raw meals were thermally threated at seven different temperatures, from 1000 to 1450 °C, to evaluate their behaviour on heating by ex situ X-Ray Powder Diffraction and to observe the final clinker morphology by Scanning Electron Microscopy. Results indicate the calcite microstrain is a reliable parameter to predict the burnability of the raw meals, in terms of calcium silicates growth and lime consumption. In particular, mixtures prepared starting from high-strained calcite exhibit a better burnability. Later, when the melt appears this correlation vanishes; however differences in the early burnability still reflect on the final clinker composition and texture.

Fluorescence of aqueous solutions of commercial humic products

NASA Astrophysics Data System (ADS)

Gosteva, O. Yu.; Izosimov, A. A.; Patsaeva, S. V.; Yuzhakov, V. I.; Yakimenko, O. S.

2012-01-01

We have studied the spectral luminescence characteristics of aqueous solutions of humic products obtained from different raw material sources, and their behavior as the excitation wavelength increases from 270 nm to 355 nm. We have identified differences in the spectral properties of industrial humic products from coalified materials, lignin-containing organic waste, and humic products from plant raw material (peat, sapropel, vermicompost). We have shown that humic products from plant raw material have spectral properties closer to those for humic substances in natural water or soil than humic products from coalified materials.

Biotechnology in Food Production and Processing

NASA Astrophysics Data System (ADS)

Knorr, Dietrich; Sinskey, Anthony J.

1985-09-01

The food processing industry is the oldest and largest industry using biotechnological processes. Further development of food products and processes based on biotechnology depends upon the improvement of existing processes, such as fermentation, immobilized biocatalyst technology, and production of additives and processing aids, as well as the development of new opportunities for food biotechnology. Improvements are needed in the characterization, safety, and quality control of food materials, in processing methods, in waste conversion and utilization processes, and in currently used food microorganism and tissue culture systems. Also needed are fundamental studies of the structure-function relationship of food materials and of the cell physiology and biochemistry of raw materials.

Characterization and quantification of N-(3-aminopropyl)-N-dodecyl-1,3-propanediamine biocide by NMR, HPLC/MS and titration techniques.

PubMed

Mondin, Andrea; Bogialli, Sara; Venzo, Alfonso; Favaro, Gabriella; Badocco, Denis; Pastore, Paolo

2014-01-01

The present paper reports the determination of the tri-amine N-(3-aminopropyl)-N-dodecyl-1,3-propanediamine (TA) present in a raw material called LONZABAC used to formulate various, widely used commercial biocides. The active principle, TA, is present in LONZABAC together with other molecules at lower concentration levels. Three independent analytical approaches, namely solution NMR spectroscopy, liquid chromatography coupled to high resolution mass spectrometry (LC/HRMS) and acid-base titration in mixed solvent, were used to overcome the problem of the non-availability of the active principle as high purity standard. NMR analysis of raw material, using a suitable internal standard, evidenced in all analyzed lots the presence of the active principle, the N-dodecyl-1,3-propanediamine (DA) and the n-dodecylamine (MA) and the absence of non-organic, NMR-inactive species. NMR peak integration led to a rough composition of the MA:DA:TA as 1:9:90. The LC/HRMS analysis allowed the accurate determination of DA and MA and confirmed in all samples the presence of the TA, which was estimated by difference: MA=1.4±0.3%, DA=11.1±0.7%, TA=87.5±1.3%. The obtained results were used to setup an easy, rapid and cheap acid-base titration method able to furnish a sufficiently accurate evaluation of the active principle both in the raw material and in diluted commercial products. For the raw material the results were: TA+MA=91.1±0.8% and DA-MA=8.9±0.8%, statistically coherent with LC/MS ones. The LC/MS approach demonstrated also its great potentialities to recognize trace of the biocide components both in environmental samples and in the formulated commercial products. Copyright © 2013 Elsevier Ltd. All rights reserved.

Definition of price in circular raw materials from the process of incineration of hazardous industrial waste in sicilian a high risk area

NASA Astrophysics Data System (ADS)

Matarazzo, Agata; Baglio, Lorenzo; Bonanno, Sandro; Fichera, Andrea; Leanza, Andrea; Russo, Gabriele; Amara, Giovanni; Amara, Giuseppe; Gigli, Carlo; Lombardo, Enrico

2018-05-01

Waste is classified (art.184, sub. 1, L.D. n.152/2006) as urban or special depending on its origin and whether it is dangerous or not, as well as the degree of danger. The reuse and recycling of materials are two of the main features that characterize the concept of the circular economy. Every firm operating in the field of the circular economy should adopt an industrial approach based on resource efficiency and the use and supply of sustainable raw materials, which can be achieved through innovative technologies, innovative methodologies and new business models. GE.S.P.I, has become a leading firm in the sector of hazardous industrial waste disposal, adding value to waste through a groundbreaking technology. The result of the process is the production of energy, as well as the creation of ash; this ash is then treated in order to separate dangerous heavy metals from the ash through the technique of eddy currents. Metals and purified ash are then put on the market. The aim of this paper is the price definition of this special waste thanks to the analysis of the specific second raw materials market. In this firm, incineration is a process where emissions are strongly controlled by innovative instruments in order to excel in the social and environmental respect. Through SWOT analysis we moreover describe how a company can turn the weaknesses of a high risk area into opportunities and value becomes a useful problem solving instrument to analyze logistic, marketing, and social responsibility, in the perspective of the optimization of eco-management material flows.

Microbiological Spoilage of Spices, Nuts, Cocoa, and Coffee

NASA Astrophysics Data System (ADS)

Pinkas, Joan M.; Battista, Karen; Morille-Hinds, Theodora

Spices, nuts, cocoa, and coffee are raw materials that may be used alone or as ingredients in the manufacture of processed food products. The control of microbiological spoilage of these raw materials at the ingredient stage will enable the food processor to better assure the production of high-quality foods with an acceptable shelf life. While this chapter is limited to four materials, many of the spoilage control procedures recommended can also be applied to other raw materials of a similar nature.

Quality assessment of baby food made of different pre-processed organic raw materials under industrial processing conditions.

PubMed

Seidel, Kathrin; Kahl, Johannes; Paoletti, Flavio; Birlouez, Ines; Busscher, Nicolaas; Kretzschmar, Ursula; Särkkä-Tirkkonen, Marjo; Seljåsen, Randi; Sinesio, Fiorella; Torp, Torfinn; Baiamonte, Irene

2015-02-01

The market for processed food is rapidly growing. The industry needs methods for "processing with care" leading to high quality products in order to meet consumers' expectations. Processing influences the quality of the finished product through various factors. In carrot baby food, these are the raw material, the pre-processing and storage treatments as well as the processing conditions. In this study, a quality assessment was performed on baby food made from different pre-processed raw materials. The experiments were carried out under industrial conditions using fresh, frozen and stored organic carrots as raw material. Statistically significant differences were found for sensory attributes among the three autoclaved puree samples (e.g. overall odour F = 90.72, p < 0.001). Samples processed from frozen carrots show increased moisture content and decrease of several chemical constituents. Biocrystallization identified changes between replications of the cooking. Pre-treatment of raw material has a significant influence on the final quality of the baby food.

Effect of Chemical Washing Pre-treatment of Empty Fruit Bunch (EFB) biochar on Characterization of Hydrogel Biochar composite as Bioadsorbent

NASA Astrophysics Data System (ADS)

Meri, N. H.; Alias, A. B.; Talib, N.; Rashid, Z. A.; Wan, W. A.; Ghani, Ab Karim

2018-05-01

Hydrogel biochar composite (HBC) is a recent interest among researchers because of the hydrophilic characteristic which can adsorb chemical fluid and showed a versatile potential as adsorbent in removing hazardous material in wastewater and gas stream. In this study, the effect of chemical washing pre-treatment by using two different type of chemical agent Hydrochloric Acid (HCL) and Hydrogen Peroxide (H2O2) was analysed and investigated. The raw EFB biochar was prepared using microwave assisted pyrolysis under 1000W for 30 min under N2 flow with 150 mL/min. To improve the adsoprtion ability, the EFB biochar has been chemical washed pre-treatment with Hydrochloric Acid (HCl) and Hydrogen Peroxide (H2O2) before polymerization process with acrylamide (AAm) as monomer, N,N’-methylenebisacrylamide (MBA) as crosslinker and ammonium persulfate (APS) as initiator. The characterization has studied by using Fourier transform infrared spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC). FTIR result shows that, the formation of Raw EFB to Hydrogel Biochar Composite (Raw EFB > EFB Biochar > Treated Biochars (HCl & H2O2) > Hydrogel Biochar Composite) have changed in functional group. For DSC result it shows that the thermal behaviour of all samples is endothermic process and have high thermal resistance.

Energy and raw material potentials of wood residue in the Pacific Coast States: a summary of a preliminary feasibility investigation.

Treesearch

John B. Grantham; Eldon Estep; John M. Pierovich; Harold Tarkow; Thomas C. Adams

1974-01-01

Results are reported of a preliminary investigation of feasibility of using wood residue to meet energy and raw material needs in the Pacific Coast States. Magnitude of needs was examined and volume of logging-residue and unused mill residue was estimated. Costs of obtaining and preprocessing logging residue for energy and pulp and particle board raw material were...

Perchlorate in Fertilizers

DTIC Science & Technology

1999-09-01

Harrington , showed that with respect to mixed water analysis containing TDS at greater 1,000 ppm, the performance of the AS-5 column is not as robust...to note, these raw test materials were heterogeneous. Regardless of mixing time and mesh quality, dividing the raw test materials for laboratory...raw test material was prepared and shipped to seven laboratories for blind analysis. The suspension was prepared by 4 mixing the solid sample with

Indonesian CPO availability analysis to support food and energy security: a system dynamic approach

NASA Astrophysics Data System (ADS)

Rahman, T.; Arkeman, Y.; Setyaningsih, D.; Saparita, R.

2017-05-01

The development of biofuels could be a solution to overcome the energy problem. One of biofuel that has the potential to be developed, namely palm oil biodiesel that is also the raw material for food. As a provider of CPO raw materials, the production of palm biodiesel could trigger competitions, from biofuels demand growth and utilization of agricultural resources. Thus, it needs to be analyzed to determine the adequency of CPO supply to fulfill the need of food and policy recomendation which sets the development of palm oil biodiesel can be synergies with food need especially for the supply of raw material CPO. To obtain the optimal policy in the synergy between the raw material of CPO for food and energy is a need to establish some policy scenarios that allow to be applied and then chosen the best policy alternative of all scenarios. The purpose of this research were to : 1) analysis the availability of CPO to meet the needs of food and energy, 2) provide policy recommendation with regard biodiesel development of food security. The model made used system dynamic method. Several scenarios that used in the model are: 1) existing condition, 2) The scenario increase biodiesel production capacity and increase land productivity, 3) reduction scenario CPO export by 30%, 4) scenario use othe raw material for biodiesel by 20%. The simulation results showed the availability of CPO raw materials would answer all needs of both food and biodiesel when there was an increase in productivity, diversification of raw materials, and also a reduction in palm oil exports. It was needed an integrated policy from upstream to downstream along with the consistency of implementation. Policy suggestions that could be considered were increased productivity through agricultural intensification, enforcement disincentive policies of CPO to exports, and development of non-CPO biodiesel raw materials and development of renewable energy.

Toxicological and chemical characterization of the process stream materials and gas combustion products of an experimental low-btu coal gasifier.

PubMed

Benson, J M; Hanson, R L; Royer, R E; Clark, C R; Henderson, R F

1984-04-01

The process gas stream of an experimental pressurized McDowell-Wellman stirred-bed low-Btu coal gasifier, and combustion products of the clean gas were characterized as to their mutagenic properties and chemical composition. Samples of aerosol droplets condensed from the gas were obtained at selected positions along the process stream using a condenser train. Mutagenicity was assessed using the Ames Salmonella mammalian microsome mutagenicity assay (TA98, with and without rat liver S9). All materials required metabolic activation to be mutagenic. Droplets condensed from gas had a specific mutagenicity of 6.7 revertants/microgram (50,000 revertants/liter of raw gas). Methylnaphthalene, phenanthrene, chrysene, and nitrogen-containing compounds were positively identified in a highly mutagenic fraction of raw gas condensate. While gas cleanup by the humidifier-tar trap system and Venturi scrubber led to only a small reduction in specific mutagenicity of the cooled process stream material (4.1 revertants/microgram), a significant overall reduction in mutagenicity was achieved (to 2200 revertants/liter) due to a substantial reduction in the concentration of material in the gas. By the end of gas cleanup, gas condensates had no detectable mutagenic activity. Condensates of combustion product gas, which contained several polycyclic aromatic compounds, had a specific mutagenicity of 1.1 revertants/microgram (4.0 revertants/liter). Results indicate that the process stream material is potentially toxic and that care should be taken to limit exposure of workers to the condensed tars during gasifier maintenance and repair and to the aerosolized tars emitted in fugitive emissions. Health risks to the general population resulting from exposure to gas combustion products are expected to be minimal.

Sector-based VOCs emission factors and source profiles for the surface coating industry in the Pearl River Delta region of China.

PubMed

Zhong, Zhuangmin; Sha, Qing'e; Zheng, Junyu; Yuan, Zibing; Gao, Zongjiang; Ou, Jiamin; Zheng, Zhuoyun; Li, Cheng; Huang, Zhijiong

2017-04-01

Accurate depiction of VOCs emission characteristics is essential for the formulation of VOCs control strategies. As one of the continuous efforts in improving VOCs emission characterization in the Pearl River Delta (PRD) region, this study targeted on surface coating industry, the most important VOCs emission sources in the PRD. Sectors in analysis included shipbuilding coating, wood furniture coating, metal surface coating, plastic surface coating, automobile coating and fabric surface coating. Sector-based field measurement was conducted to characterize VOCs emission factors and source profiles in the PRD. It was found that the raw material-based VOCs emission factors for these six sectors ranged from 0.34 to 0.58kg VOCs per kg of raw materials (kg·kg -1 ) while the emission factors based on the production yield varied from 0.59kg to 13.72t VOCs for each production manufactured. VOCs emission factors of surface coating industry were therefore preferably calculated based on raw materials with low uncertainties. Source profiles differed greatly among different sectors. Aromatic was the largest group for shipbuilding coating, wood furniture coating, metal surface coating and automobile coating while the oxygenated VOCs (OVOCs) were the most abundant in the plastic and fabric surface coating sectors. The major species of aromatic VOCs in each of these six sectors were similar, mainly toluene and m/p-xylene, while the OVOCs varied among the different sectors. VOCs profiles in the three processes of auto industry, i.e., auto coating, auto drying and auto repairing, also showed large variations. The major species in these sectors in the PRD were similar with other places but the proportions of individual compounds were different. Some special components were also detected in the PRD region. This study highlighted the importance of updating local source profiles in a comprehensive and timely manner. Copyright © 2016 Elsevier B.V. All rights reserved.

Investigation of Air-Liquid Interface Rings in Buffer Preparation Vessels: the Role of Slip Agents.

PubMed

Shi, Ting; Ding, Wei; Kessler, Donald W; De Mas, Nuria; Weaver, Douglas G; Pathirana, Charles; Martin, Russell D; Mackin, Nancy A; Casati, Michael; Miller, Scott A; Pla, Itzcoatl A

2016-01-01

Air-liquid interface rings were observed on the side walls of stainless steel buffer vessels after certain downstream buffer preparations. Those rings were resistant to regular cleaning-in-place procedures but could be removed by manual means. To investigate the root cause of this issue, multiple analytical techniques, including liquid chromatography with tandem mass spectrometry detection (LC-MS/MS), high-resolution accurate mass liquid chromatography with mass spectrometry, nuclear magnetic resonance, Fourier transform infrared spectroscopy, and scanning electron microscopy with energy-dispersive X-ray spectroscopy have been employed to characterize the chemical composition of air-liquid interface rings. The main component of air-liquid interface rings was determined to be slip agents, and the origin of the slip agents can be traced back to their presence on raw material packaging liners. Slip agents are commonly used in plastic industry as additives to reduce the coefficient of friction during the manufacturing process of thin films. To mitigate this air-liquid interface ring issue, an alternate liner with low slip agent was identified and implemented with minimal additional cost. We have also proactively tested the packaging liners of other raw materials currently used in our downstream buffer preparation to ensure slip agent levels are appropriate. Air-liquid interface rings were observed on the side walls of stainless steel buffer vessels after certain downstream buffer preparations. To investigate the root cause of this issue, multiple analytical techniques have been employed to characterize the chemical composition of air-liquid interface rings. The main components of air-liquid interface rings were determined to be slip agents, which are common additives used in the manufacturing process of thin films. The origin of the slip agents can be traced back to their presence on certain raw material packaging liners. To mitigate this air-liquid interface ring issue, an alternate liner with low slip agent was identified and implemented. © PDA, Inc. 2016.

Evaluating chemical-, mechanical-, and bio-pulping processes and their sustainability characterization using life cycle assessment

Treesearch

Tapas K. Das; Carl Houtman

2004-01-01

Pulp and paper manufacturing constitutes one of the largest industry segments in the United States in term of water and energy usage and total discharges to the environment. More than many other industries, however, this industry plays an important role in sustainable development because its chief raw material— wood fiber—is renewable. This industry provides an example...

Characterization of Low Firing Temperature Ceramic Glaze Using Phuket MSW and Soda Lime Cullet

NASA Astrophysics Data System (ADS)

Ketboonruang, P.; Jinawat, S.; Kashima, D. P.; Wasanapiarnpong, T.; Sujaridworakun, P.; Buggakuptav, W.; Traipol, N.; Jiemsirilers, S.

2011-10-01

The normal firing temperature of ceramic products is around 1200 °C. In order to reduce firing temperature, industrial wastes were utilized in ceramic glaze. Phuket municipal solid waste (MSW), soda lime cullet, and borax were used as raw materials for low firing temperature glazes. The glaze compositions were designed using a triaxial diagram. Stoneware ceramic body was glazed then fired at 1000 and 1150 °C for 15 minutes. Morphology and phase composition of glazes were analyzed by Scanning electron microscopy (SEM-EDS) and X-ray diffraction (XRD). Thermal expansion compatibility of Stoneware body and glazes were investigated using a dilatometer. Melting behaviour of selected glaze was analyzed by heating stage microscopy. Phuket MSW and Soda lime glass cullet can be used in high percentage as major raw materials for low firing temperature ceramic glaze that show good texture and vitrified at lower firing temperature without using any commercial ceramic frits. The firing temperature can be reduced up to 150 °C in this study.

Optimized extraction of polysaccharides from Cymbopogon citratus and its biological activities.

PubMed

Thangam, Ramar; Suresh, Veeraperumal; Kannan, Soundarapandian

2014-04-01

In this study the extraction of hot water soluble polysaccharides (HWSPs) from Cymbopogon citratus using hot water decoction was discussed. Response surface methodology (RSM) based on a three level, three variable central composite rotatable design (CCRD), was employed to obtain best possible combination of extraction time (X1: 30-180 min), extraction temperature (X2: 70-100 °C) and water to the raw material ratio (X3: 10-60) for maximum HWSPs extraction. The optimum extraction conditions were as follows: extraction time was around 113.81 min, extraction temperature at 99.66 °C and the ratio of water to raw material was 33.11 g/mL. Under these conditions, the experimental yield was 13.24±0.23%, which is well in close agreement with the value predicted by RSM model yield (13.19%). The basic characterization of HWSPs was determined by using the FTIR. These preliminary in vitro biological studies indicated that lemongrass polysaccharides were useful for anticancer therapy. Copyright © 2014 Elsevier B.V. All rights reserved.

Preparation and characterization of bio-composite PEEK/nHA

NASA Astrophysics Data System (ADS)

Jin, Y. S.; Bian, C. C.; Zhang, Z. Q.; Zhao, Y.; Yang, L.

2017-01-01

PEEK/nHA composite material, with excellent mechanical property as polyetheretherketone (PEEK) and biological activity as hydroxyapatite (HA), has attracted wide attention of medical experts and materials science experts. The addition of hydroxyapatite was the decisive factor for biological activity in PEEK/nHA composite. In this paper, acicular nanohydroxyapatite was prepared by chemical precipitation method with Ca(NO3)2, (NH4)2HPO4 as raw material; PEEK/nHA composite was prepared by solution blending and vacuum sintering method. The composite was characterized with FT-IR, XRD, DSC, TG and mechanical property test. Results showed that the composite has good thermal stability and compressive property when the mass ratio of PEEK to nHA is 10:3; and high nHA content can improve the biological activity of the composite, which can meet the basic requirements for bone tissue engineering scaffold.

77 FR 31388 - Importer of Controlled Substances; Notice of Application; Noramco, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2012-05-25

... material are not appropriate. 72 FR 3417 (2007). In regard to the non-narcotic raw material, any bulk... following basic classes of controlled substances: Drug Schedule Phenylacetone (8501) II Opium, raw (9600) II Poppy Straw Concentrate (9670) II Tapentadol (9780) II The company plans to import the raw Opium (9600...

40 CFR 428.105 - Standards of performance for new sources.

Code of Federal Regulations, 2011 CFR

2011-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6.96 2.90 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 2.0 0.73 BOD5... daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Chromium 0...

40 CFR 428.105 - Standards of performance for new sources.

Code of Federal Regulations, 2010 CFR

2010-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 2.0 0.73 BOD5 3.72 2.20 TSS 6.96 2.90 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 2.0 0.73 BOD5... daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material) Chromium 0...

Anisotropic nature of radially strained metal tubes

NASA Astrophysics Data System (ADS)

Strickland, Julie N.

Metal pipes are sometimes swaged by a metal cone to enlarge them, which increases the strain in the material. The amount of strain is important because it affects the burst and collapse strength. Burst strength is the amount of internal pressure that a pipe can withstand before failure, while collapse strength is the amount of external pressure that a pipe can withstand before failure. If the burst or collapse strengths are exceeded, the pipe may fracture, causing critical failure. Such an event could cost the owners and their customers millions of dollars in clean up, repair, and lost time, in addition to the potential environmental damage. Therefore, a reliable way of estimating the burst and collapse strength of strained pipe is desired and valuable. The sponsor currently rates strained pipes using the properties of raw steel, because those properties are easily measured (for example, yield strength). In the past, the engineers assumed that the metal would be work-hardened when swaged, so that yield strength would increase. However, swaging introduces anisotropic strain, which may decrease the yield strength. This study measured the yield strength of strained material in the transverse and axial direction and compared them to raw material, to determine the amount of anisotropy. This information will be used to more accurately determine burst and collapse ratings for strained pipes. More accurate ratings mean safer products, which will minimize risk for the sponsor's customers. Since the strained metal has a higher yield strength than the raw material, using the raw yield strength to calculate burst and collapse ratings is a conservative method. The metal has even higher yield strength after strain aging, which indicates that the stresses are relieved. Even with the 12% anisotropy in the strained and 9% anisotropy in the strain aged specimens, the raw yield strengths are lower and therefore more conservative. I recommend that the sponsor continue using the raw yield strength to calculate these ratings. I set out to characterize the anisotropic nature of swaged metal. As expected, the tensile tests showed a difference between the axial and transverse tensile strength. The correlation was 12% difference in yield strength in the axial and transverse directions for strained material and 9% in strained and aged material. This means that the strength of the metal in the hoop (transverse) direction is approximately 10% stronger than in the axial direction, because the metal was work hardened during the swaging process. Therefore, the metal is more likely to fail in axial tension than in burst or collapse. I presented the findings from the microstructure examination, standard tensile tests, and SEM data. All of this data supported the findings of the mini-tensile tests. This information will help engineers set burst and collapse ratings and allow material scientists to predict the anisotropic characteristics of swaged steel tubes.

Cellulose nanocrystals the next big nano-thing?

NASA Astrophysics Data System (ADS)

Postek, Michael T.; Vladar, Andras; Dagata, John; Farkas, Natalia; Ming, Bin; Sabo, Ronald; Wegner, Theodore H.; Beecher, James

2008-08-01

Biomass surrounds us from the smallest alga to the largest redwood tree. Even the largest trees owe their strength to a newly-appreciated class of nanomaterials known as cellulose nanocrystals (CNC). Cellulose, the world's most abundant natural, renewable, biodegradable polymer, occurs as whisker like microfibrils that are biosynthesized and deposited in plant material in a continuous fashion. Therefore, the basic raw materials for a future of new nanomaterials breakthroughs already abound in the environment and are available to be utilized in an array of future materials once the manufacturing processes and nanometrology are fully developed. This presentation will discuss some of the instrumentation, metrology and standards issues associated with nanomanufacturing of cellulose nanocrystals. The use of lignocellulosic fibers derived from sustainable, annually renewable resources as a reinforcing phase in polymeric matrix composites provides positive environmental benefits with respect to ultimate disposability and raw material use. Today we lack the essential metrology infrastructure that would enable the manufacture of nanotechnology-based products based on CNCs (or other new nanomaterial) to significantly impact the U.S. economy. The basic processes common to manufacturing - qualification of raw materials, continuous synthesis methods, process monitoring and control, in-line and off-line characterization of product for quality control purposes, validation by standard reference materials - are not generally in place for nanotechnology based products, and thus are barriers to innovation. One advantage presented by the study of CNCs is that, unlike other nanomaterials, at least, cellulose nanocrystal manufacturing is already a sustainable and viable bulk process. Literally tons of cellulose nanocrystals can be generated each day, producing other viable byproducts such as glucose (for alternative fuel) and gypsum (for buildings).There is an immediate need for the development of the basic manufacturing metrology infrastructure to implement fundamental best practices for manufacturing and in the determination of properties for these for nanoscale materials and the resultant products.

Ethanol Production from Traditional and Emerging Raw Materials

NASA Astrophysics Data System (ADS)

Rudolf, Andreas; Karhumaa, Kaisa; Hahn-Hägerdal, Bärbel

The ethanol industry of today utilizes raw materials rich in saccharides, such as sugar cane or sugar beets, and raw materials rich in starch, such as corn and wheat. The concern about supply of liquid transportation fuels, which has brought the crude oil price above 100 /barrel during 2006, together with the concern about global warming, have turned the interest towards large-scale ethanol production from lignocellulosic materials, such as agriculture and forestry residues. Baker's yeast Saccharomyces cerevisiae is the preferred fermenting microorganism for ethanol production because of its superior and well-documented industrial performance. Extensive work has been made to genetically improve S. cerevisiae to enable fermentation of lignocellulosic raw materials. Ethanolic fermentation processes are conducted in batch, fed-batch, or continuous mode, with or without cell recycling, the relative merit of which will be discussed.

Solutions for Critical Raw Materials under Extreme Conditions: A Review

PubMed Central

Grilli, Maria Luisa; Bellezze, Tiziano; Gamsjäger, Ernst; Rinaldi, Antonio; Novak, Pavel; Balos, Sebastian; Piticescu, Radu Robert; Ruello, Maria Letizia

2017-01-01

In Europe, many technologies with high socio-economic benefits face materials requirements that are often affected by demand-supply disruption. This paper offers an overview of critical raw materials in high value alloys and metal-matrix composites used in critical applications, such as energy, transportation and machinery manufacturing associated with extreme working conditions in terms of temperature, loading, friction, wear and corrosion. The goal is to provide perspectives about the reduction and/or substitution of selected critical raw materials: Co, W, Cr, Nb and Mg. PMID:28772645

Hydrogenated cottonseed oil as raw material for biobased materials

USDA-ARS?s Scientific Manuscript database

There has been a lot of recent interest in using vegetable oils as biodegradable and renewable raw materials for the syntheses of various biobased materials. Although most of the attention has been paid to soybean oil thus far, cottonseed oil is a viable alternative. An advantage of cottonseed oil...

Identification of Particles in Parenteral Drug Raw Materials.

PubMed

Lee, Kathryn; Lankers, Markus; Valet, Oliver

2018-04-18

Particles in drug products are not good and are therefore regulated. These particles can come from the very beginning of the manufacturing process, from the raw materials. To prevent particles, it is important to understand what they are and where they come from so the raw material quality, processing, and shipping can be improved. Thus, it is important to correctly identify particles seen in raw materials. Raw materials need to be of a certain quality with respect to physical and chemical composition, and need to have no contaminants in the form of particles which could contaminate the product or indicate the raw materials are not pure enough to make a good quality product. Particles are often seen when handling raw materials due to color, size, or shape characteristics different from those in the raw materials. Particles may appear to the eye to be very different things than they actually are, so microscope, chemical, and elemental analyses are required for accuracy in proper identification. This paper shows how using three different spectroscopy tools correctly and together can be used to identify particles from extrinsic, intrinsic, and inherent particles. Sources of materials can be humans and the environment (extrinsic), from within the process (intrinsic), and part of the formulation (inherent). Microscope versions of Raman spectroscopy, laser-induced breakdown spectroscopy (LIBS), and IR spectroscopy are excellent tools for identifying particles because they are fast and accurate techniques needing minimal sample preparation that can provide chemical composition as well as images that can be used for identification. The micro analysis capabilities allow for easy analysis of different portions of samples so multiple components can be identified and sample preparation can be reduced. Using just one of these techniques may not be sufficient to give adequate identification results so that the source of contamination can be adequately identified. The complementarity of the techniques provides the advantage of identifying various chemical and molecular components, as well as elemental and image analyses. Correct interpretation of the results from these techniques is also very important. Copyright © 2018, Parenteral Drug Association.

40 CFR 428.73 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2011 CFR

2011-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH... Average of daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material...

40 CFR 428.53 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH... Average of daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material...

40 CFR 428.63 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH... Average of daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material...

40 CFR 428.53 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2011 CFR

2011-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.70 0.25 TSS 1.28 0.64 pH... Average of daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material...

40 CFR 428.73 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.26 0.093 TSS 0.50 0.25 pH... Average of daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material...

40 CFR 428.63 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2011 CFR

2011-07-01

... consecutive days shall not exceed— Metric units (kg/kkg of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH (1) (1) English units (lb/1,000 lb of raw material) Oil and grease 0.42 0.15 TSS 0.80 0.40 pH... Average of daily values for 30 consecutive days shall not exceed— Metric units (kg/kkg of raw material...

7 CFR 58.517 - General.

Code of Federal Regulations, 2011 CFR

2011-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58.517 General. Raw materials used for manufacturing cottage cheese shall meet the following quality...

7 CFR 58.517 - General.

Code of Federal Regulations, 2010 CFR

2010-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58.517 General. Raw materials used for manufacturing cottage cheese shall meet the following quality...

40 CFR 122.23 - Concentrated animal feeding operations (applicable to State NPDES programs, see § 123.25).

Code of Federal Regulations, 2012 CFR

2012-07-01

... with any raw materials, products, or byproducts including manure, litter, feed, milk, eggs or bedding... manure handling system). (5) The term manure is defined to include manure, bedding, compost and raw... storage area, the raw materials storage area, and the waste containment areas. The animal confinement area...

40 CFR 122.23 - Concentrated animal feeding operations (applicable to State NPDES programs, see § 123.25).

Code of Federal Regulations, 2013 CFR

2013-07-01

... with any raw materials, products, or byproducts including manure, litter, feed, milk, eggs or bedding... manure handling system). (5) The term manure is defined to include manure, bedding, compost and raw... storage area, the raw materials storage area, and the waste containment areas. The animal confinement area...

40 CFR 122.23 - Concentrated animal feeding operations (applicable to State NPDES programs, see § 123.25).

Code of Federal Regulations, 2011 CFR

2011-07-01

... with any raw materials, products, or byproducts including manure, litter, feed, milk, eggs or bedding... manure handling system). (5) The term manure is defined to include manure, bedding, compost and raw... storage area, the raw materials storage area, and the waste containment areas. The animal confinement area...

40 CFR 122.23 - Concentrated animal feeding operations (applicable to State NPDES programs, see § 123.25).

Code of Federal Regulations, 2014 CFR

2014-07-01

... with any raw materials, products, or byproducts including manure, litter, feed, milk, eggs or bedding... manure handling system). (5) The term manure is defined to include manure, bedding, compost and raw... storage area, the raw materials storage area, and the waste containment areas. The animal confinement area...

Inorganic raw materials economy and provenance of chipped industry in some stone age sites of northern and central Italy.

PubMed

Bietti, Amilcare; Boschian, Giovanni; Crisci, Gino Mirocle; Danese, Ermanno; De Francesco, Anna Maria; Dini, Mario; Fontana, Federica; Giampietri, Alessandra; Grifoni, Renata; Guerreschi, Antonio; Liagre, Jérémie; Negrino, Fabio; Radi, Giovanna; Tozzi, Carlo; Tykot, Robert

2004-06-01

An opportunistic and local choice of raw materials is typically attested in the Lower and Middle Paleolithic industries throughout Italy. The quality of the raw material usually affected the flaking technology and quality of the products. In the Upper Paleolithic and the Mesolithic, raw material procurement strategies were more complex. Flint was exploited both locally, in areas where abundant outcrops of raw materials were available (such as the Lessini mountains), and in distant localities, after which it was transported or exchanged over medium/long distances. Different routes of exchange were thus followed in the various periods; good reconstruction of these routes have been provided by a study of the Garfagnana sites in Northern Tuscany, and the Mesolithic deposit of Mondeval de Sora (Dolomites). An interesting example of a Late Upper Paleolithic flint quarry and workshop were found in Abruzzo, in the San Bartolomeo shelter. The extended trade of obsidian from Lipari, Palmarola and Sardinia to the Italian Peninsula is attested in the Neolithic, with some differences concerning the age and different areas.

Characterizing the Intrinsic Fluorescence Properties of Historical Painting Materials: The Case Study of a Sixteenth-Century Mesoamerican Manuscript.

PubMed

Pottier, Fabien; Michelin, Anne; Andraud, Christine; Goubard, Fabrice; Lavédrine, Bertrand

2018-04-01

Ultraviolet visible (UV-Vis) fluorescence spectroscopy is widely used to study polychrome objects and can help to identify the nature of certain materials when they present specific fluorescent properties. However, given the complexity of the stratified and heterogeneous materials under study, the characterization of an intrinsic fluorescence related to a given constituent (a pigment or a binder composing a paint layer for example) is not straightforward, and the recorded raw data need to be corrected for a number of effects that can influence the detected spectral distribution. The application of standard correction procedures to experimental fluorescence data gathered on the polychromatic surface of the Codex Borbonicus, a 16th-century Aztec manuscript, is described. The results are confronted to an alternate new methodology that is based on the hypothesis of transparent non-scattering paint layers. This second approach allows to establish more clearly the material origin of the detected emission and to discriminate apparent fluorescence (emitted by the substrate and transmitted through the paint layers) from actual intrinsic emission generated by the coloring materials under study. The results show that most of the various emission profiles detected in the paint layers of the manuscript actually originate from a unique fluorophore (composing the substrate) and should not be used to characterize the coloring materials.

7 CFR 58.231 - General.

Code of Federal Regulations, 2011 CFR

2011-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Materials § 58.231 General. All raw materials received at the drying plant shall meet the following quality...

7 CFR 58.231 - General.

Code of Federal Regulations, 2010 CFR

2010-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Materials § 58.231 General. All raw materials received at the drying plant shall meet the following quality...

21 CFR 113.81 - Product preparation.

Code of Federal Regulations, 2011 CFR

2011-04-01

... Production and Process Controls § 113.81 Product preparation. (a) Before using raw materials and ingredients susceptible to microbiological contamination, the processor shall ensure that those materials and ingredients... by receiving the raw materials and ingredients under a supplier's guarantee that they are suitable...

Translations on Eastern Europe, Scientific Affairs, Number 604

DTIC Science & Technology

1978-10-18

economy which in the area of raw material economy may be characterized in terms of a transition from a focus on quality to the principle of...instead, existing knowledge may be reevaluated in the new economic environment in the light of the technological progress since then. In the area of...must be strengthened within industrial production processes. The Ministry of Heavy Industry has received a great deal of help in this area from

Characterization of Chemical Weapons Convention Schedule 3 Compounds by Quantitative 13C NMR Spectroscopy

DTIC Science & Technology

2007-11-01

or other pesticides, or as fumigants for rodent extermination. Additionally, they all are used as a raw material for the synthesis of other chemicals...pressure/ vacuum valve NMR sample tubes (Catalog number 528- PV-9), were purchased from Wilmad-Labglass (Buena, NJ). 2.2 Sample Preparation Hydrogen...cyanide, cyanogen chloride, and phosgene were prepared for NMR spectroscopy by condensing their respective gases into pressure/ vacuum valve NMR sample

Spore populations among bulk tank raw milk and dairy powders are significantly different.

PubMed

Miller, Rachel A; Kent, David J; Watterson, Matthew J; Boor, Kathryn J; Martin, Nicole H; Wiedmann, Martin

2015-12-01

To accommodate stringent spore limits mandated for the export of dairy powders, a more thorough understanding of the spore species present will be necessary to develop prospective strategies to identify and reduce sources (i.e., raw materials or in-plant) of contamination. We characterized 1,523 spore isolates obtained from bulk tank raw milk (n=33 farms) and samples collected from 4 different dairy powder-processing plants producing acid whey, nonfat dry milk, sweet whey, or whey protein concentrate 80. The spores isolated comprised 12 genera, at least 44 species, and 216 rpoB allelic types. Bacillus and Geobacillus represented the most commonly isolated spore genera (approximately 68.9 and 12.1%, respectively, of all spore isolates). Whereas Bacillus licheniformis was isolated from samples collected from all plants and farms, Geobacillus spp. were isolated from samples from 3 out of 4 plants and just 1 out of 33 farms. We found significant differences between the spore population isolated from bulk tank raw milk and those isolated from dairy powder plant samples, except samples from the plant producing acid whey. A comparison of spore species isolated from raw materials and finished powders showed that although certain species, such as B. licheniformis, were found in both raw and finished product samples, other species, such as Geobacillus spp. and Anoxybacillus spp., were more frequently isolated from finished powders. Importantly, we found that 8 out of 12 genera were isolated from at least 2 different spore count methods, suggesting that some spore count methods may provide redundant information if used in parallel. Together, our results suggest that (1) Bacillus and Geobacillus are the predominant spore contaminants in a variety of dairy powders, implying that future research efforts targeted at elucidating approaches to reduce levels of spores in dairy powders should focus on controlling levels of spore isolates from these genera; and (2) the spore populations isolated from bulk tank raw milk and some dairy powder products are significantly different, suggesting that targeting in-plant sources of contamination may be important for achieving low spore counts in the finished product. These data provide important insight regarding the diversity of spore populations isolated from dairy powders and bulk tank raw milk, and demonstrate that several spore genera are detected by multiple spore count methods. Copyright © 2015 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

Enhancement of efficiency of storage and processing of food raw materials using radiation technologies

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gracheva, A. Yu.; Zav’yalov, M. A.; Ilyukhina, N. V.

The work is dedicated to improvement of efficiency of storage and processing of food raw materials using radiation technologies. International practice of radiation processing of food raw materials is presented and an increase in the consumption of irradiated food products is shown. The prospects of using radiation technologies for the processing of food products in Russia are discussed. The results of studies of radiation effects on various food products and packaging film by γ radiation and accelerated electrons are presented.

Rapid bacteriological screening of cosmetic raw materials by using bioluminescence.

PubMed

Nielsen, P; Van Dellen, E

1989-01-01

Incoming cosmetic raw materials are routinely tested for microbial content. Standard plate count methods require up to 72 h. A rapid, sensitive, and inexpensive raw material screening method was developed that detects the presence of bacteria by means of ATP (bioluminescence). With a 24-h broth enrichment, the minimum bacterial ATP detection threshold of 1 cfu/g sample can be achieved using purified firefly luciferin-luciferase and an ATP releasing reagent. By using this rapid screen, microbiologically free material may be released for production within 24 h, while contaminated material undergoes further quantitative and identification testing. In order for a raw material to be validated for this method it must be evaluated for (1) a potential nonmicrobial light-contributing reaction resulting in a false positive or, (2) degradation of the ATP giving a false negative, and (3) confirmation that the raw material has not overwhelmed the buffering capacity of the enrichment broth. The key criteria for a rapid screen was the sensitivity to detect less than one colony forming unit per g product, the speed to do this within 24 h, and cost efficiency. Bioluminescence meets these criteria. With an enrichment step, it can detect less than one cfu/g sample. After the enrichment step, analysis time per sample is approximately 2 min and the cost for material and reagents is less than one dollar per sample.

Characterization and quality assessment of recycled post-consumption poly(ethylene terephthalate) (PET).

PubMed

Masmoudi, Fatma; Fenouillot, Françoise; Mehri, Afef; Jaziri, Mohamed; Ammar, Emna

2018-06-05

In the present study, the recycled post-consumption polyethylene terephthalate (PET) flakes were investigated as possible raw materials for the production of food packaging. After heating at 220 °C for 1 h, a steaming stage was conducted as a control test to assess the quality of the product. Different samples were characterized by 1 H-NMR, FT-IR, DSC/TGA analysis, viscosity index (VI), and trace metals analysis. The results showed that the recycled post-consumed PET flakes' properties were generally conform to the standard norms of PET except the color of some flakes turned to yellow. Subsequently, a complementary study was undertaken to assess whether the material could be possibly reused for food packaging. For this purpose, rheological, thermal, and mechanical characterizations were performed. The results of the comparative study between the virgin and the recycled PET flakes concluded that the PET recycling affected the rheological properties but did not have any significant effect on their thermal and mechanical characteristics. Hence, it was deduced that the post-consumed PET flakes could be reused as a packaging material except food products.

31 CFR 545.413 - Importation of goods from third countries; transshipments.

Code of Federal Regulations, 2010 CFR

2010-07-01

...; transshipments. (a) Importation into the United States from third countries of goods containing raw materials or... raw materials or components have been incorporated into manufactured products or otherwise...

Mechanical characterization of alloys in extreme conditions of high strain rates and high temperature

NASA Astrophysics Data System (ADS)

Cadoni, Ezio

2018-03-01

The aim of this paper is the description of the mechanical characterization of alloys under extreme conditions of temperature and loading. In fact, in the frame of the Cost Action CA15102 “Solutions for Critical Raw Materials Under Extreme Conditions (CRM-EXTREME)” this aspect is crucial and many industrial applications have to consider the dynamic response of materials. Indeed, for a reduction and substitution of CRMs in alloys is necessary to design the materials and understand if the new materials behave better or if the substitution or reduction badly affect their performance. For this reason, a deep knowledge of the mechanical behaviour at high strain-rates of considered materials is required. In general, machinery manufacturing industry or transport industry as well as energy industry have important dynamic phenomena that are simultaneously affected by extended strain, high strain-rate, damage and pressure, as well as conspicuous temperature gradients. The experimental results in extreme conditions of high strain rate and high temperature of an austenitic stainless steel as well as a high-chromium tempered martensitic reduced activation steel Eurofer97 are presented.

Lanthanum cerate (La2Ce2O7): hydrothermal synthesis, characterization and optical properties

NASA Astrophysics Data System (ADS)

Khademinia, Shahin; Behzad, Mahdi

2015-03-01

La2Ce2O7 nano-powders were synthesized via a hydrothermal reaction in a deionized water (S 1) and in a 2 M NaOH aqueous solution (S 2) at 180 °C for 48 h. La(NO3)3·H2O and (NH4)2Ce(NO3)6 were used in the stoichiometric 1:1 La:Ce molar ratio as raw materials. The obtained materials were crystallized in a cubic crystal structure with space group. The synthesized materials were characterized by powder X-ray diffraction technique and Fourier-transform infrared spectroscopy. To investigate the effect of the basic solution on the morphology of the obtained materials, the morphologies of the synthesized materials were studied by field emission scanning electron microscopy technique. The technique showed that the morphology of La2Ce2O7 samples changed from grain to rod-like structure in presence of the basic solution. Cell parameter refinements showed that these parameters were larger for S2 than those for S 1. Photoluminescence and ultraviolet visible spectra of the synthesized nanomaterials were also investigated.

Synthesis and electrochemical performance of cathode material Li1.2Co0.13Ni0.13Mn0.54O2 from spent lithium-ion batteries

NASA Astrophysics Data System (ADS)

Li, Li; Zhang, Xiaoxiao; Chen, Renjie; Zhao, Taolin; Lu, Jun; Wu, Feng; Amine, Khalil

2014-03-01

Li-rich layered oxide Li1.2Co0.13Ni0.13Mn0.54O2 has been successfully re-synthesized using the ascorbic acid leaching solution of spent lithium-ion batteries as the raw materials. A combination of oxalic acid co-precipitation, hydrothermal and calcination processes was applied to synthesize this material. For comparison, a fresh sample with the same composition has been also synthesized from the commercial raw materials using the same method. X-ray diffraction (XRD), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and electrochemical measurements are carried out to characterize these samples. XRD results indicate that both samples have the layered α-NaFeO2 structures with a space group of R 3 bar m. No other crystalline phase was detected by XRD. The electrochemical results show that the re-synthesized and fresh-synthesized sample can deliver discharge capacities as high as 258.8 and 264.2 mAh g-1 at the first cycle, respectively. After 50 cycles, discharge capacities of 225.1 and 228 mAh g-1 can be obtained with capacity retention of 87.0 and 86.3%, respectively. This study suggests that the leaching solution from spent lithium ion batteries can be recycled to synthesize Li-rich cathode materials with good electrochemical performance.

Hierarchical porous carbon aerogel derived from bagasse for high performance supercapacitor electrode.

PubMed

Hao, Pin; Zhao, Zhenhuan; Tian, Jian; Li, Haidong; Sang, Yuanhua; Yu, Guangwei; Cai, Huaqiang; Liu, Hong; Wong, C P; Umar, Ahmad

2014-10-21

Renewable, cost-effective and eco-friendly electrode materials have attracted much attention in the energy conversion and storage fields. Bagasse, the waste product from sugarcane that mainly contains cellulose derivatives, can be a promising candidate to manufacture supercapacitor electrode materials. This study demonstrates the fabrication and characterization of highly porous carbon aerogels by using bagasse as a raw material. Macro and mesoporous carbon was first prepared by carbonizing the freeze-dried bagasse aerogel; consequently, microporous structure was created on the walls of the mesoporous carbon by chemical activation. Interestingly, it was observed that the specific surface area, the pore size and distribution of the hierarchical porous carbon were affected by the activation temperature. In order to evaluate the ability of the hierarchical porous carbon towards the supercapacitor electrode performance, solid state symmetric supercapacitors were assembled, and a comparable high specific capacitance of 142.1 F g(-1) at a discharge current density of 0.5 A g(-1) was demonstrated. The fabricated solid state supercapacitor displayed excellent capacitance retention of 93.9% over 5000 cycles. The high energy storage ability of the hierarchical porous carbon was attributed to the specially designed pore structures, i.e., co-existence of the micropores and mesopores. This research has demonstrated that utilization of sustainable biopolymers as the raw materials for high performance supercapacitor electrode materials is an effective way to fabricate low-cost energy storage devices.

Evaluation of lunar rocks and soils for resource utilization: Detailed image analysis of raw materials and beneficiated products

NASA Technical Reports Server (NTRS)

Taylor, Lawrence A.; Chambers, John G.; Patchen, Allan; Jerde, Eric A.; Mckay, David S.; Graf, John; Oder, Robin R.

1993-01-01

The rocks and soils of the Moon will be the raw materials for fuels and construction needs at a lunar base. This includes sources of materials for the generation of hydrogen, oxygen, metals, and other potential construction materials. For most of the bulk material needs, the regolith, and its less than 1 cm fraction, the soil, will suffice. But for specific mineral resources, it may be necessary to concentrate minerals from rocks or soils, and it is not always obvious which is the more appropriate feedstock. Besides an appreciation of site geology, the mineralogy and petrography of local rocks and soils is important for consideration of the resources which can provide feedstocks of ilmenite, glass, agglutinates, anorthite, etc. In such studies, it is very time-consuming and practically impossible to correlate particle counts (the traditional method of characterizing lunar soil petrography) with accurate modal analyses and with mineral associations in multi-mineralic grains. But x ray digital imaging, using x rays characteristic of each element, makes all this possible and much more (e.g., size and shape analysis). An application of beneficiation image analysis, in use in our lab (Oxford Instr. EDS and Cameca SX-50 EMP), was demonstrated to study mineral liberation from lunar rocks and soils. Results of x ray image analysis are presented.

Competitive Advantage Market Analysis | Energy Analysis | NREL

Science.gov Websites

Study An NREL market assessment of raw and intermediate materials, equipment, and products for equipment for c-Si PV Abundant raw materials for production of moisture barrier films, glass, aluminum

7 CFR 58.322 - Cream.

Code of Federal Regulations, 2011 CFR

2011-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58... derived from raw material meeting the requirements as listed under §§ 58.132 through 58.138 of this...

7 CFR 58.322 - Cream.

Code of Federal Regulations, 2010 CFR

2010-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58... derived from raw material meeting the requirements as listed under §§ 58.132 through 58.138 of this...

40 CFR 63.1251 - Definitions.

Code of Federal Regulations, 2012 CFR

2012-07-01

... ingredient means any material that is intended to furnish pharmacological activity or other direct effect in... this section. Consumption means the quantity of all HAP raw materials entering a process in excess of... as added as a raw material, consumption includes the quantity generated in the process. Container, as...

40 CFR 63.1251 - Definitions.

Code of Federal Regulations, 2010 CFR

2010-07-01

... ingredient means any material that is intended to furnish pharmacological activity or other direct effect in... this section. Consumption means the quantity of all HAP raw materials entering a process in excess of... as added as a raw material, consumption includes the quantity generated in the process. Container, as...

40 CFR 63.1251 - Definitions.

Code of Federal Regulations, 2011 CFR

2011-07-01

... ingredient means any material that is intended to furnish pharmacological activity or other direct effect in... this section. Consumption means the quantity of all HAP raw materials entering a process in excess of... as added as a raw material, consumption includes the quantity generated in the process. Container, as...

Occurrence and characterization of Shiga toxin-producing Escherichia coli in raw meat, raw milk, and street vended juices in Bangladesh.

PubMed

Islam, Mohammad A; Mondol, Abdus S; Azmi, Ishrat J; de Boer, Enne; Beumer, Rijkelt R; Zwietering, Marcel H; Heuvelink, Annet E; Talukder, Kaisar A

2010-11-01

The major objective of this study was to investigate the prevalence of Shiga toxin (Stx)-producing Escherichia coli (STEC) in different types of food samples and to compare their genetic relatedness with STEC strains previously isolated from animal sources in Bangladesh. We investigated a total of 213 food samples, including 90 raw meat samples collected from retail butcher shops, 20 raw milk samples from domestic cattle, and 103 fresh juice samples from street vendors in Dhaka city. We found that more than 68% (n = 62) of the raw meat samples were positive for the stx gene(s); 34% (n = 21) of buffalo meats and 66% (n = 41) of beef. Approximately 10% (n = 2) of the raw milk and 8% (n = 8) of the fresh juice samples were positive for stx. We isolated STEC O157 from seven meat samples (7.8%), of which two were from buffalo meats and five from beef; and no other STEC serotypes could be isolated. We could not isolate STEC from any of the stx-positive raw milk and juice samples. The STEC O157 isolates from raw meats were positive for the stx(2), eae, katP, etpD, and enterohemorrhagic E. coli hly virulence genes, and they belonged to three different phage types: 8 (14.3%), 31 (42.8%), and 32 (42.8%). Pulsed-field gel electrophoresis (PFGE) typing revealed six distinct patterns among seven isolates of STEC O157, suggesting a heterogeneous clonal diversity. Of the six PFGE patterns, one was identical and the other two were ≥90% related to PFGE patterns of STEC O157 strains previously isolated from animal feces, indicating that raw meats are readily contaminated with fecal materials. This study represents the first survey of STEC in the food chain in Bangladesh.

Nondestructive determination of activity

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chabalier, B.

1996-08-01

Characterization and appraisal tests include the measurement of activity in raw waste and waste packages. After conditioning, variations in density, matrix composition, and geometry make evaluation of the radionuclide activity in a package destined for storage nearly impossible without measurements and with a low uncertainty. Various nondestructive measuring techniques that use ionizing radiation are employed to characterize waste packages and raw waste. Gamma spectrometry is the most widely used technique because of its simple operation and low cost. This technique is used to quantify the beta-gamma and alpha activity of gamma-emitting radionuclides as well as to check the radioactive homogeneitymore » of the waste packages. Numerous systems for directly measuring waste packages have been developed. Two types of methods may be distinguished, depending on whether results that come from the measurements are weighted by an experimentally determined corrective term or by calculation. Through the MARCO and CARACO measuring systems, a method is described that allows one to quantify the activity of the beta-gamma and alpha radionuclides contained in either a waste package or raw waste whose geometries and material compositions are more or less accurately known. This method is based on (a) measurement by gamma spectrometry of the beta-gamma and alpha activity of the gamma-emitting radionuclides contained in the waste package and (b) the application of calculated corrections; thus, the limitations imposed by reference package geometry and matrix are avoided.« less

Carbon Nanotubes for Human Space Flight

NASA Technical Reports Server (NTRS)

Scott, Carl D.; Files, Brad; Yowell, Leonard

2003-01-01

Single-wall carbon nanotubes offer the promise of a new class of revolutionary materials for space applications. The Carbon Nanotube Project at NASA Johnson Space Center has been actively researching this new technology by investigating nanotube production methods (arc, laser, and HiPCO) and gaining a comprehensive understanding of raw and purified material using a wide range of characterization techniques. After production and purification, single wall carbon nanotubes are processed into composites for the enhancement of mechanical, electrical, and thermal properties. This "cradle-to-grave" approach to nanotube composites has given our team unique insights into the impact of post-production processing and dispersion on the resulting material properties. We are applying our experience and lessons-learned to developing new approaches toward nanotube material characterization, structural composite fabrication, and are also making advances in developing thermal management materials and electrically conductive materials in various polymer-nanotube systems. Some initial work has also been conducted with the goal of using carbon nanotubes in the creation of new ceramic materials for high temperature applications in thermal protection systems. Human space flight applications such as advanced life support and fuel cell technologies are also being investigated. This discussion will focus on the variety of applications under investigation.

The properties of weft knitted fabric medical and preventive treatment action using eco-raw materials

NASA Astrophysics Data System (ADS)

Halavska, L.; Batrak, O.

2016-07-01

A new trend in the world is the clothing production using the new types of ecological raw materials application - milk, pineapple, coconut, hemp, banana, eucalyptus, clams, corn, bamboo, soya, nettle yarn. This makes it possible to create textile materials of new generation with unique antibacterial and antiseptic properties. Such materials have a positive preventive and sometimes therapeutic effect on people, and their health. Eco-raw materials clothing is able to protect the human body from the environment harmful effects: cold, heat, rain, dust, opportunely remove from underclothing layer the steam and gases, sweat; maintain in underclothing layer the necessary microclimate for normal organism functioning. Study of knitwear consumer properties, produced with eco-materials, is an urgent task of the world vector, directed on ecological environmental protection. This paper presents the research results of hygroscopicity and capillarity weft knitted fabrics, what knitted from different types of eco-raw materials: bamboo yarn, yarn containing soybean and nettle yarn. Character of influence of the liquid raising level changes depending on the experiment time and the knitting structure is revealed.

Influence of raw material properties upon critical quality attributes of continuously produced granules and tablets.

PubMed

Fonteyne, Margot; Wickström, Henrika; Peeters, Elisabeth; Vercruysse, Jurgen; Ehlers, Henrik; Peters, Björn-Hendrik; Remon, Jean Paul; Vervaet, Chris; Ketolainen, Jarkko; Sandler, Niklas; Rantanen, Jukka; Naelapää, Kaisa; De Beer, Thomas

2014-07-01

Continuous manufacturing gains more and more interest within the pharmaceutical industry. The International Conference of Harmonisation (ICH) states in its Q8 'Pharmaceutical Development' guideline that the manufacturer of pharmaceuticals should have an enhanced knowledge of the product performance over a range of raw material attributes, manufacturing process options and process parameters. This fits further into the Process Analytical Technology (PAT) and Quality by Design (QbD) framework. The present study evaluates the effect of variation in critical raw material properties on the critical quality attributes of granules and tablets, produced by a continuous from-powder-to-tablet wet granulation line. The granulation process parameters were kept constant to examine the differences in the end product quality caused by the variability of the raw materials properties only. Theophylline-Lactose-PVP (30-67.5-2.5%) was used as model formulation. Seven different grades of theophylline were granulated. Afterward, the obtained granules were tableted. Both the characteristics of granules and tablets were determined. The results show that differences in raw material properties both affect their processability and several critical quality attributes of the resulting granules and tablets. Copyright © 2014 Elsevier B.V. All rights reserved.

An integrated production-inventory model for food products adopting a general raw material procurement policy

NASA Astrophysics Data System (ADS)

Fauza, G.; Prasetyo, H.; Amanto, B. S.

2018-05-01

Studies on an integrated production-inventory model for deteriorating items have been done extensively. Most of the studies define deterioration as physical depletion of some inventories over time. This definition may not represent the deterioration characteristics of food products. The quality of food production decreases over time while the quantity remains the same. Further, in the existing models, the raw material is replenished several times (or at least once) within one production cycle. In food industries, however, a food company, for several reasons (e.g., the seasonal raw materials, discounted price, etc.) sometimes will get more benefit if it orders raw materials in a large quantity. Considering this fact, this research, therefore, is aimed at developing a more representative inventory model by (i) considering the quality losses in food and (ii) adopting a general raw material procurement policy. A mathematical model is established to represent the proposed policy in which the total profit of the system is the objective function. To evaluate the performance of the model, a numerical test was conducted. The numerical test indicates that the developed model has better performance, i.e., the total profit is 2.3% higher compared to the existing model.

The 1995 Medical Device Technology raw materials survey.

PubMed

Pearson, L S

1995-09-01

Using information supplied by manufacturers, this article reports on the use of raw materials and compounding and conversion practices in the European medical device manufacturing industry. The findings of the survey provide an indication of which materials are being used and how frequently, and the process of selecting suppliers.

Creating a Learning-Friendly Curriculum.

ERIC Educational Resources Information Center

Donovan, Michael P.

1997-01-01

Argues against a type of program evaluation of undergraduate institutions that assumes students are products. Proposes that if students are products, then students are raw materials. Discusses the philosophical problems of considering students as raw materials. (DDR)

60. INTERIOR VIEW OF THE RAW MATERIALS BUILDING, LOOKING AT ...

Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

60. INTERIOR VIEW OF THE RAW MATERIALS BUILDING, LOOKING AT THE POIDOMETER AND WEIGHING MACHINE. MAY 5, 1919. - United States Nitrate Plant No. 2, Reservation Road, Muscle Shoals, Muscle Shoals, Colbert County, AL

Sensory analysis of cosmetic powders: personal care ingredients and emulsions.

PubMed

Moussour, M; Lavarde, M; Pensé-Lhéritier, A-M; Bouton, F

2017-02-01

The powders are ingredients increasingly used in the formulation of cosmetic products for the sensory qualities they give. The objective of this study was the development of a lexicon and a referential for sensory characterization of these pure raw materials as well as formulations which contain them. Eleven expert panellists from Ecole de biologie industrielle de Cergy (France) developed a lexicon and a referential based on 12 powders of different chemical natures. The selected attributes were then used for performing a quantitative descriptive profile of two powders and an emulsion containing or not one of these two powders. A lexicon has been established through a consensus approach of the panel. It contains seven attributes that allow the evaluation of the powders in four phases: the appearance, the pickup, the application and the after-feel. This lexicon contains definitions and assessment protocols and provides references products. The quantitative descriptive profile of two powders of the same chemical nature, but different in physical quality showed significant differences in sensory level between products. These same attributes used to evaluate an emulsion containing the powder or not allowed to prove the contribution of these raw materials on the sensory specificities of the emulsion. The lexicon developed in this study can be used for assessment of other powders but also to define the quantities necessary to put in the formulation to meet the sensory characteristics of these raw materials powder. © 2016 Society of Cosmetic Scientists and the Société Française de Cosmétologie.

Raw material procurement for termite fishing tools by wild chimpanzees in the Issa valley, Western Tanzania.

PubMed

Almeida-Warren, Katarina; Sommer, Volker; Piel, Alex K; Pascual-Garrido, Alejandra

2017-10-01

Chimpanzee termite fishing has been studied for decades, yet the selective processes preceding the manufacture of fishing tools remain largely unexplored. We investigate raw material selection and potential evidence of forward planning in the chimpanzees of Issa valley, western Tanzania. Using traditional archaeological methods, we surveyed the location of plants from where chimpanzees sourced raw material to manufacture termite fishing tools, relative to targeted mounds. We measured raw material abundance to test for availability and selection. Statistics included Chi-Squared, two-tailed Wilcoxon, and Kruskall-Wallace tests. Issa chimpanzees manufactured extraction tools only from bark, despite availability of other suitable materials (e.g., twigs), and selected particular plant species as raw material sources, which they often also exploit for food. Most plants were sourced 1-16 m away from the mound, with a maximum of 33 m. The line of sight from the targeted mound was obscured for a quarter of these plants. The exclusive use of bark tools despite availability of other suitable materials indicates a possible cultural preference. The fact that Issa chimpanzees select specific plant species and travel some distance to source them suggests some degree of selectivity and, potentially, forward planning. Our results have implications for the reconstruction of early hominin behaviors, particularly with regard to the use of perishable tools, which remain archaeologically invisible. © 2017 Wiley Periodicals, Inc.

Synchrotron White Beam X-Ray Topography Characterization of LGX and SXGS Bulk Single Crystals, Thin Films and Piezoelectric Devices

DTIC Science & Technology

2007-04-27

perceived. First, high Ga2O3 content among 23 the raw materials makes the crystal cost much higher than quartz, LiNbO3 and LiTaO3. Second, more...of the ternary component system ( e.g. La2O3 - Ga2O3 - SiO2); b. small but finite evaporation of Ga2O3 from the melt 4. This non-stoichiometry in

[Characteristics of the nitrous substances in the meat of sharks and rays as a protein food raw material].

PubMed

Kizevetter, I V; Nasedkina, E A

1975-01-01

The nitrous composition of meat in 19 species of oceanic sharks and 2 species of rays were analyzed. The meat of these fish species was found to be characterized by a comparatively low protein content, whose amino acids composition proved relatively poor of essential amino acids. The meat of sharks and rays is distinguished by a high level of extractives, whose bulk includes urea and trimethylaminoxide.

Isolation and characterization of bacteriophages specific to hydrogen-sulfide-producing bacteria.

PubMed

Gong, Chao; Heringa, Spencer; Singh, Randhir; Kim, Jinkyung; Jiang, Xiuping

2013-01-01

The objectives of this study were to isolate and characterize bacteriophages specific to hydrogen-sulfide-producing bacteria (SPB) from raw animal materials, and to develop a SPB-specific bacteriophage cocktail for rendering application. Meat, chicken offal, and feather samples collected from local supermarkets and rendering processing plants were used to isolate SPB (n = 142). Bacteriophages (n = 52) specific to SPB were isolated and purified from the above samples using 18 of those isolated SPB strains as hosts. The host ranges of bacteriophages against 5 selected SPB strains (Escherichia coli, Citrobacter freundii, and Hafnia alvei) were determined. Electron microscopy observation of 9 phages selected for the phage cocktail revealed that 6 phages belonged to the family of Siphoviridae and 3 belonged to the Myoviridae family. Restriction enzyme digestion analysis with endonuclease DraI detected 6 distinguished patterns among the 9 phages. Phage treatment prevented the growth of SPB for up to 10 h with multiplicity of infection ratios of 1, 10, 100, and 1000 in tryptic soy broth at 30 °C, and extended the lag phase of SPB growth for 2 h at 22 °C with multiplicities of infection of 10, 100, and 1000. These results suggest that the selected bacteriophage cocktail has a high potential for phage application to control SPB in raw animal materials destined for the rendering process.

Green synthesis of silver nanoparticles using Stevia leaves extracts

NASA Astrophysics Data System (ADS)

Laguta, Iryna; Stavinskaya, Oksana; Kazakova, Olga; Fesenko, Tetiana; Brychka, Sergey

2018-02-01

Three extracts of Stevia rebaudiana (Bertoni) were prepared using different types of raw materials: leaves of plants grown ex situ, leaves of plants grown in vitro, callus culture formed on damaged leaves. Composition of the extracts was studied by means of high-performance liquid chromatography and laser desorption/ionization mass spectrometry; total phenol content was estimated using Folin-Ciocalteau method. Flavonoids and hydroxycinnamic acids were found to be the main groups of phenol antioxidants available in the Stevia leaves, with the amount of these compounds in the extract being dependent on the type of raw material. The reducing properties of phenol compounds identified in the extracts were characterized using quantum chemical method; flavonoids and hydroxycinnamic acids were found to have similar redox parameters. Silver nanoparticles (AgNPs) colloids were synthesized using three Stevia extracts; AgNPs size distribution were characterized by means of scanning electron microscopy. All the extracts revealed significant activity in AgNPs synthesis; the nanoparticles of predominantly spherical shape with the average sizes of 16-25 nm were formed. The reducing properties of the extracts were found to correlate with total phenol content; the activity of extracts from the leaves of plants grown ex situ and from callus culture in Ag+ ions reduction was similar to each other and exceeded the activity of extract from the leaves of plants grown in vitro.

Characterization of Listeria monocytogenes isolated from a fresh mixed sausage processing line in Pelotas-RS by PFGE

PubMed Central

von Laer, Ana Eucares; de Lima, Andréia Saldanha; Trindade, Paula dos Santos; Andriguetto, Cristiano; Destro, Maria Teresa; da Silva, Wladimir Padilha

2009-01-01

Listeria monocytogenes is a bacterium capable to adhere to the surfaces of equipment and utensils and subsequently form biofilms. It can to persist in the food processing environmental for extended periods of time being able to contaminate the final product. The aim of this study was to trace the contamination route of L. monocytogenes on a fresh mixed sausage processing line, from raw material to the final product. The isolates obtained were characterized by serotyping and molecular typing by pulsed-field gel electrophoresis (PFGE) using the restriction enzymes ApaI and AscI. L. monocytogenes was detected in 25% of the samples. The samples of raw material were not contaminated, however, the microorganism was detected in 21% of the environmental samples (food contact and non-food contact), 20.8% of the equipments, 20% of the food worker’s hands, 40% of the mass ready to packaging and in all the final products samples, demonstrating that the contamination of final product occurred during the processing and the importance of cross contamination. PFGE yielded 22 pulsotypes wich formed 7 clusters, and serotyping yielded 3 serotypes and 1 serogroup, however, the presence of serotypes 4b and 1/2b in the final product is of great concern for public health. The tracing of contamination showed that some strains are adapted and persisted in the processing environment in this industry. PMID:24031402

Sustainability evaluation of essential critical raw materials: cobalt, niobium, tungsten and rare earth elements

NASA Astrophysics Data System (ADS)

Tkaczyk, A. H.; Bartl, A.; Amato, A.; Lapkovskis, V.; Petranikova, M.

2018-05-01

The criticality of raw materials has become an important issue in recent years. As the supply of certain raw materials is essential for technologically-advanced economies, the European Commission and other international counterparts have started several initiatives to secure reliable and unhindered access to raw materials. Such efforts include the EU Raw Materials Initiative, European Innovation Partnership on Raw Materials, US Critical Materials Institute, and others. In this paper, the authors present a multi-faceted and multi-national review of the essentials for the critical raw materials (CRMs) Co, Nb, W, and rare earth elements (REEs). The selected CRMs are of specific interest as they are considered relevant for emerging technologies and will thus continue to be of increasing major economic importance. This paper presents a ‘sustainability evaluation’ for each element, including essential data about markets, applications and recycling, and possibilities for substitution have been summarized and analysed. All the presented elements are vital for the advanced materials and processes upon which modern societies rely. These elements exhibit superior importance in ‘green’ applications and products subject to severe conditions. The annual production quantities are quite low compared to common industrial metals. Of the considered CRMs, only Co and REE gross production exceed 100 000 t. At the same time, the prices are quite high, with W and Nb being in the range of 60 USD kg‑1 and some rare earth compounds costing almost 4000 USD kg‑1. Despite valiant effort, in practice some of the considered elements are de facto irreplaceable for many specialized applications, at today’s technological level. Often, substitution causes a significant loss of quality and performance. Furthermore, possible candidates for substitution may be critical themselves or available in considerably low quantities. It can be concluded that one preferred approach for the investigated elements could be the use of secondary resources derived from recycling. W exhibits the highest recycling rate (37%), whereas Co (16%), Nb (11%) and rare earths (~0%) lag behind. In order to promote recycling of these essential elements, financial incentives as well as an improvement of recycling technologies would be required.

Infrared and Raman spectroscopic methods for characterization of Taxus baccata L.--Improved taxane isolation by accelerated quality control and process surveillance.

PubMed

Gudi, Gennadi; Krähmer, Andrea; Koudous, Iraj; Strube, Jochen; Schulz, Hartwig

2015-10-01

Different yew species contain poisonous taxane alkaloids which serve as resources for semi-synthesis of anticancer drugs. The highly variable amounts of taxanes demand new methods for fast characterization of the raw plant material and the isolation of the target structures during phyto extraction. For that purpose, applicability of different vibrational spectroscopy methods in goods receipt of raw plant material and in process control was investigated and demonstrated in online tracking isolation and purification of the target taxane 10-deacetylbaccatin III (10-DAB) during solvent extraction. Applying near (NIRS) and mid infrared spectroscopy (IRS) the amount of botanical impurities in mixed samples of two different yew species (R(2)=0.993), the leave-to-wood ratio for Taxus baccata material (R(2)=0.94) and moisture in dried yew needles (R(2)=0.997) can be quantified. By partial least square analysis (PCA) needles of different Coniferales species were successfully discriminated by Attenuated Total Reflectance-Fourier-Transform Infrared Spectroscopy (ATR-FT-IR). The analytical potential of ATR-FT-IR and Fourier Transform-Raman Spectroscopy (FT-RS) in process control of extraction and purification of taxanes is demonstrated for determination of the water content in methanolic yew extracts (R(2)=0.999) and for quantification of 10-DAB (R(2)=0.98) on a highly sophisticated level. The decrease of 10-DAB in the plant tissue during extraction was successfully visualized by FT-IR imaging of thin cross sections providing new perspectives for process control and design. Copyright © 2015 Elsevier B.V. All rights reserved.

Mechanical Properties of a Newly Additive Manufactured Implant Material Based on Ti-42Nb

PubMed Central

Schulze, Christian; Weinmann, Markus; Schweigel, Christoph; Keßler, Olaf; Bader, Rainer

2018-01-01

The application of Ti-6Al-4V alloy or commercially pure titanium for additive manufacturing enables the fabrication of complex structural implants and patient-specific implant geometries. However, the difference in Young’s modulus of α + β-phase Ti alloys compared to the human bone promotes stress-shielding effects in the implant–bone interphase. The aim of the present study is the mechanical characterization of a new pre-alloyed β-phase Ti-42Nb alloy for application in additive manufacturing. The present investigation focuses on the mechanical properties of SLM-printed Ti-42Nb alloy in tensile and compression tests. In addition, the raw Ti-42Nb powder, the microstructure of the specimens prior to and after compression tests, as well as the fracture occurring in tensile tests are characterized by means of the SEM/EDX analysis. The Ti-42Nb raw powder exhibits a dendrite-like Ti-structure, which is melted layer-by-layer into a microstructure with a very homogeneous distribution of Nb and Ti during the SLM process. Tensile tests display Young’s modulus of 60.51 ± 3.92 GPa and an ultimate tensile strength of 683.17 ± 16.67 MPa, whereas, under a compressive load, a compressive strength of 1330.74 ± 53.45 MPa is observed. The combination of high mechanical strength and low elastic modulus makes Ti-42Nb an interesting material for orthopedic and dental implants. The spherical shape of the pre-alloyed material additionally allows for application in metal 3D printing, enabling the fabrication of patient-specific structural implants. PMID:29342864

Mechanical Properties of a Newly Additive Manufactured Implant Material Based on Ti-42Nb.

PubMed

Schulze, Christian; Weinmann, Markus; Schweigel, Christoph; Keßler, Olaf; Bader, Rainer

2018-01-13

The application of Ti-6Al-4V alloy or commercially pure titanium for additive manufacturing enables the fabrication of complex structural implants and patient-specific implant geometries. However, the difference in Young's modulus of α + β-phase Ti alloys compared to the human bone promotes stress-shielding effects in the implant-bone interphase. The aim of the present study is the mechanical characterization of a new pre-alloyed β-phase Ti-42Nb alloy for application in additive manufacturing. The present investigation focuses on the mechanical properties of SLM-printed Ti-42Nb alloy in tensile and compression tests. In addition, the raw Ti-42Nb powder, the microstructure of the specimens prior to and after compression tests, as well as the fracture occurring in tensile tests are characterized by means of the SEM/EDX analysis. The Ti-42Nb raw powder exhibits a dendrite-like Ti-structure, which is melted layer-by-layer into a microstructure with a very homogeneous distribution of Nb and Ti during the SLM process. Tensile tests display Young's modulus of 60.51 ± 3.92 GPa and an ultimate tensile strength of 683.17 ± 16.67 MPa, whereas, under a compressive load, a compressive strength of 1330.74 ± 53.45 MPa is observed. The combination of high mechanical strength and low elastic modulus makes Ti-42Nb an interesting material for orthopedic and dental implants. The spherical shape of the pre-alloyed material additionally allows for application in metal 3D printing, enabling the fabrication of patient-specific structural implants.

A method to characterize average cervical spine ligament response based on raw data sets for implementation into injury biomechanics models.

PubMed

Mattucci, Stephen F E; Cronin, Duane S

2015-01-01

Experimental testing on cervical spine ligaments provides important data for advanced numerical modeling and injury prediction; however, accurate characterization of individual ligament response and determination of average mechanical properties for specific ligaments has not been adequately addressed in the literature. Existing methods are limited by a number of arbitrary choices made during the curve fits that often misrepresent the characteristic shape response of the ligaments, which is important for incorporation into numerical models to produce a biofidelic response. A method was developed to represent the mechanical properties of individual ligaments using a piece-wise curve fit with first derivative continuity between adjacent regions. The method was applied to published data for cervical spine ligaments and preserved the shape response (toe, linear, and traumatic regions) up to failure, for strain rates of 0.5s(-1), 20s(-1), and 150-250s(-1), to determine the average force-displacement curves. Individual ligament coefficients of determination were 0.989 to 1.000 demonstrating excellent fit. This study produced a novel method in which a set of experimental ligament material property data exhibiting scatter was fit using a characteristic curve approach with a toe, linear, and traumatic region, as often observed in ligaments and tendons, and could be applied to other biological material data with a similar characteristic shape. The resultant average cervical spine ligament curves provide an accurate representation of the raw test data and the expected material property effects corresponding to varying deformation rates. Copyright © 2014 Elsevier Ltd. All rights reserved.

High purity silica reflective heat shield development

NASA Technical Reports Server (NTRS)

Nachtscheim, P. R.; Blome, J. C.

1976-01-01

A hyperpure vitreous silica material is being developed for use as a reflective and ablative heat shield for planetary entry. Various purity grades and forms of raw materials were evaluated along with various processing methods. Slip casting of high purity grain was selected as the best processing method, resulting in a highly reflective material in the wavelength bands of interest (the visible and ultraviolet regions). The selected material was characterized with respect to optical, mechanical and physical properties using a limited number of specimens. The process has been scaled up to produce a one-half scale heat shield (18 in. dia.) (45.72 cm) for a Jupiter entry vehicle. This work is now being extended to improve the structural safety factor of the heat shield by making hyperpure silica material tougher through the addition of silica fibers.

Incentivizing secondary raw material markets for sustainable waste management.

PubMed

Schreck, Maximilian; Wagner, Jeffrey

2017-09-01

Notwithstanding several policy initiatives in many countries over a number of years, there remains a general sense that too much municipal solid waste is generated and that too much of the waste that is generated is landfilled. There is an emerging consensus that a sustainable approach to waste management requires further development of secondary raw material markets. The purpose of this paper is to propose a theoretical economic model that focuses upon this stage of a sustainable waste management program and explores policy options that could motivate efficiency in secondary raw material markets. In particular, we show how firm profit and social welfare optimizing objectives can be reconciled in a two-product market of waste management processes: landfilling and material reclamation. Our results provide theoretical support for building out recent Circular Economy initiatives as well as for the relatively recent emergence of landfill mining as a means for procuring secondary raw materials. Copyright © 2017 Elsevier Ltd. All rights reserved.

31 CFR 538.410 - Imports of Sudanese goods from third countries; transshipments.

Code of Federal Regulations, 2010 CFR

2010-07-01

...; transshipments. (a) Importation into the United States from third countries of goods containing raw materials or components of Sudanese origin is not prohibited if those raw materials or components have been incorporated...

78 FR 69132 - Importer of Controlled Substances; Notice of Registration; Noramco, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2013-11-18

... on applications to import narcotic raw material are not appropriate. 72 FR 3417(2007). In reference to the non-narcotic raw material, any bulk manufacturer who is presently, or is applying to be...

31 CFR 538.410 - Imports of Sudanese goods from third countries; transshipments.

Code of Federal Regulations, 2011 CFR

2011-07-01

...; transshipments. (a) Importation into the United States from third countries of goods containing raw materials or components of Sudanese origin is not prohibited if those raw materials or components have been incorporated...

78 FR 51747 - Importer of Controlled Substances; Notice of Application; NORAMCO, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2013-08-21

... on applications to import narcotic raw material are not appropriate. 72 FR 3417 (2007). In reference to the non-narcotic raw material, any bulk manufacturer who is presently, or is applying to be...

The U.S. Chemical Industry, the Raw Materials It Uses

ERIC Educational Resources Information Center

Chemical and Engineering News, 1972

1972-01-01

The raw materials used by the industry are considered in this section of the annual chemical industry report, including data covering: natural gas, lead, mercury, phosphate rock, potash, salt, petroleum products including petrochemical feedstocks. (PR)

Cellulose acetate fibers prepared from different raw materials with rapid synthesis method.

PubMed

Chen, Jinghuan; Xu, Jikun; Wang, Kun; Cao, Xuefei; Sun, Runcang

2016-02-10

Transesterification is a mild process to prepare cellulose acetate (CA) as compared with the traditional method. In this study, CA fibers were produced from six cellulose raw materials based on a simple and rapid transesterification method. The properties of the CA solutions and the obtained CA fibers were investigated in detail. Results showed that all of the cellulose raw materials were esterified within 15 min, and spinning dopes could be obtained by concentrating the CA solutions via vacuum distillation. The XRD, FT-IR, (1)H, (13)C and HSQC NMR analysis confirmed the successful synthesis of CA. The degree of substitution (DS) of the obtained CA was significantly affected by the degree of polymerization (DP) of cellulose raw materials, which further influenced the viscosity of CA solutions as well as the structural, thermal and mechanical properties of the CA fibers. Copyright © 2015 Elsevier Ltd. All rights reserved.

Method of fabricating a honeycomb structure

DOEpatents

Holleran, Louis M.; Lipp, G. Daniel

1999-01-01

A method of fabricating a monolithic honeycomb structure product involves shaping a first mixture of raw materials and a binder into a green honeycomb, extruding a second mixture of raw materials and a binder into one or more green members that each define an opening extending longitudinally therethrough. The raw materials of the second mixture are compatible with the raw materials of the first mixture. The green honeycomb and member(s) are dried. The binders of the green honeycomb and member(s) are softened at the surfaces that are to be bonded. The green member(s) is inserted into the honeycomb and bonded to the honeycomb to form an assembly thereof, which is then dried and fired to form a unified monolithic honeycomb structure. The insertion is best carried out by mounting a member in the shape of a tube on a mandrel, and inserting the mandrel into the honeycomb opening to bond the tube to the honeycomb.

Method of fabricating a honeycomb structure

DOEpatents

Holleran, L.M.; Lipp, G.D.

1999-08-03

A method of fabricating a monolithic honeycomb structure product involves shaping a first mixture of raw materials and a binder into a green honeycomb, extruding a second mixture of raw materials and a binder into one or more green members that each define an opening extending longitudinally therethrough. The raw materials of the second mixture are compatible with the raw materials of the first mixture. The green honeycomb and member(s) are dried. The binders of the green honeycomb and member(s) are softened at the surfaces that are to be bonded. The green member(s) is inserted into the honeycomb and bonded to the honeycomb to form an assembly thereof, which is then dried and fired to form a unified monolithic honeycomb structure. The insertion is best carried out by mounting a member in the shape of a tube on a mandrel, and inserting the mandrel into the honeycomb opening to bond the tube to the honeycomb. 7 figs.

Theoretical backgrounds of non-tempered materials production based on new raw materials

NASA Astrophysics Data System (ADS)

Lesovik, V. S.; Volodchenko, A. A.; Glagolev, E. S.; Chernysheva, N. V.; Lashina, I. V.; Feduk, R. S.

2018-03-01

One of the trends in construction material science is development and implementation of highly effective finish materials which improve architectural exterior of cities. Silicate materials widely-used in the construction today have rather low decorative properties. Different coloring agents are used in order to produce competitive materials, but due to the peculiarities of the production, process very strict specifications are applied to them. The use of industrial wastes or variety of rock materials as coloring agents is of great interest nowadays. The article shows that clay rock can be used as raw material in production of finish materials of non-autoclaved solidification. This raw material due to its material composition actively interacts with cementing component in steam treatment at 90–95 °C with formation of cementing joints that form a firm coagulative-cristalized and crystallization structure of material providing high physic-mechanical properties of silicate goods. It is determined that energy-saving, colored finish materials with compression strength up to 16 MPa can be produced from clay rocks.

A Comparative Study of Raw and Metal Oxide Impregnated Carbon Nanotubes for the Adsorption of Hexavalent Chromium from Aqueous Solution

PubMed Central

Qureshi, Muhammad I.; Al-Baghli, Nadhir

2017-01-01

The present study reports the use of raw, iron oxide, and aluminum oxide impregnated carbon nanotubes (CNTs) for the adsorption of hexavalent chromium (Cr(VI)) ions from aqueous solution. The raw CNTs were impregnated with 1% and 10% loadings (weight %) of iron oxide and aluminum oxide nanoparticles using wet impregnation technique. The synthesized materials were characterized using scanning electron microscopy (SEM) and thermogravimetric analysis (TGA). Batch adsorption experiments were performed to assess the removal efficiency of Cr(VI) ions from water and the effects of pH, contact time, adsorbent dosage, and initial concentration of the Cr(VI) ions were investigated. Results of the study revealed that impregnated CNTs achieved significant increase in the removal efficiency of Cr(VI) ions compared to raw CNTs. In fact, both CNTs impregnated with 10% loading of iron and aluminum oxides were able to remove up to 100% of Cr(VI) ions from aqueous solution. Isotherm studies were carried out using Langmuir and Freundlich isotherm models. Adsorption kinetics of Cr(VI) ions from water was found to be well described by the pseudo-second-order model. The results suggest that metallic oxide impregnated CNTs have very good potential application in the removal of Cr(VI) ions from water resulting in better environmental protection. PMID:28487625

40 CFR 63.1345 - Emissions limits for affected sources other than kilns; in-line kiln/raw mills; clinker coolers...

Code of Federal Regulations, 2011 CFR

2011-07-01

... other than kilns; in-line kiln/raw mills; clinker coolers; new and reconstructed raw material dryers; and raw and finish mills, and open clinker piles. 63.1345 Section 63.1345 Protection of Environment... for affected sources other than kilns; in-line kiln/raw mills; clinker coolers; new and reconstructed...

Development of Product Availability Monitoring System In Production Unit In Automotive Component Industry

NASA Astrophysics Data System (ADS)

Hartono, Rachmad; Raharno, Sri; Yuwana Martawirya, Yatna; Arthaya, Bagus

2018-03-01

This paper described a methodology to monitor the availability of products in a production unit in the automotive component industry. Automotive components made are automotive components made through sheet metal working. Raw material coming into production unit in the form of pieces of plates that have a certain size. Raw materials that come stored in the warehouse. Data of raw each material in the warehouse are recorded and stored in a data base system. The material will then undergo several production processes in the production unit. When the material is taken from the warehouse, material data are also recorded and stored in a data base. The data recorded are the amount of material, material type, and date when the material is out of the warehouse. The material coming out of the warehouse is labeled with information related to the production processes that the material must pass. Material out of the warehouse is a product will be made. The products have been completed, are stored in the warehouse products. When the product is entered into the product warehouse, product data is also recorded by scanning the barcode contained on the label. By recording the condition of the product at each stage of production, we can know the availability of the product in a production unit in the form of a raw material, the product being processed and the finished product.

Xylan from corn cobs, a promising polymer for drug delivery: production and characterization.

PubMed

Oliveira, Elquio Eleamen; Silva, Acarília Eduardo; Júnior, Toshiyuki Nagashima; Gomes, Monique Christine Salgado; Aguiar, Larissa Muratori; Marcelino, Henrique Rodrigues; Araújo, Ivonete Batista; Bayer, Marc P; Ricardo, Nágila M P S; Oliveira, Anselmo Gomes; Egito, Eryvaldo Sócrates Tabosa

2010-07-01

Although many authors have reported several beneficial effects ascribed to xylan, such as inhibitory action on mutagenicity activity, antiphlogistic effects, and mitogenic and comitogenic activities, few papers have investigated a systematic study on the technological properties of this polymer. The aim of the present work was to evaluate xylan as a promise raw material for the pharmaceutical industry. The water-insoluble xylan samples were extracted from corn cobs following several steps. The obtained powered sample was analyzed by infrared and RMN spectroscopy, and characterized regarding their particle size, bulk and tap densities, compressibility index, compactability, Hausner ratio, and angle of repose. According to the results, infrared and RMN spectroscopy were shown to be able to evaluate the xylan structural conformation and composition, respectively. In addition, rheological data demonstrated that xylan powder obtained from corn cobs may be characterized as a material with low density and very cohesive flow properties. Copyright (c) 2010 Elsevier Ltd. All rights reserved.

Petrographic characterization of lunar soils: Application of x ray digital-imaging to quantitative and automated analysis

NASA Technical Reports Server (NTRS)

Higgins, Stefan J.; Patchen, Allan; Chambers, John G.; Taylor, Lawrence A.; Mckay, David S.

1994-01-01

The rocks and soils of the moon will be the raw materials for various engineering needs at a lunar base, such as sources of hydrogen, oxygen, metals, etc. The material of choice for most of the bulk needs is the regolith and its less than 1 cm fraction, the soil. For specific mineral resources it may be necessary to concentrate minerals from either rocks or soils. Therefore, quantitative characterizations of these rocks and soils are necessary in order to better define their mineral resource potential. However, using standard point-counting microscopic procedures, it is difficult to quantitatively determine mineral abundances and virtually impossible to obtain data on mineral distributions within grains. As a start to fulfilling these needs, Taylor et al. and Chambers et al. have developed a procedure for characterization of crushed lunar rocks using x ray digital imaging. The development of a similar digital imaging procedure for lunar soils as obtained from a spectrometer is described.

Isolation and characterization of lignins from wheat straw: Application as binder in lithium batteries.

PubMed

Domínguez-Robles, Juan; Sánchez, Rafael; Díaz-Carrasco, Pilar; Espinosa, Eduardo; García-Domínguez, M T; Rodríguez, Alejandro

2017-11-01

Three different lignin-rich fractions have been used as binder material for electrodes in rechargeable lithium batteries. Lignin samples were obtained through three different pulping processes; kraft, soda and organosolv pulping processes, using wheat straw as raw material. Physico-chemical characterization of three types of lignins was evaluated. Characterization has been performed using Fourier transform infrared spectroscopy (FTIR) and 31 P NMR Spectroscopy to analyse the functional groups; gel permeation chromatography (GPC) for determining molar mass distribution (MWD), and thermogravimetric analysis (TGA) to follow the thermal behaviour. Electrodes containing lignin or poly vinylidene fluoride (PVDF) were tested electrochemically. The three different lignin samples exhibited excellent performance as binder, retaining the specific capacity after 50 cycles at a current density of 100mAg -1 . These results show that lignin could be used as a low-cost and environmental binder, replacing the PVDF polymer in electrodes for energy storage applications. Copyright © 2017 Elsevier B.V. All rights reserved.

Epoxy composites based on inexpensive tire waste filler

NASA Astrophysics Data System (ADS)

Ahmetli, Gulnare; Gungor, Ahmet; Kocaman, Suheyla

2014-05-01

Tire waste (TW) was recycled as raw material for the preparation of DGEBA-type epoxy composite materials. The effects of filler amount and epoxy type on the mechanical properties of the composites were investigated. Tensile strength and Young's modulus of the composites with NPEL were generally higher than composites with NPEF. The appropriate mass level for TW in both type composites was found to be 20 wt%. The equilibrium water sorption of NPEL/TW and NPEF/TW composites for 14-day immersion was determined as 0.10 % and 0.21 %, respectively. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used for characterization of the composites.

Extraction Optimization, Purification and Physicochemical Properties of Polysaccharides from Gynura medica.

PubMed

Li, Fengwei; Gao, Jian; Xue, Feng; Yu, Xiaohong; Shao, Tao

2016-03-23

Extraction of polysaccharides from Gynura medica (GMPs) was optimized by response surface methodology (RSM). A central composition design including three parameters, namely extraction temperature (X₁), ratio of water to raw material (X₂) and extraction time (X₃), was used. The best conditions were extraction temperature of 91.7 °C, extraction time of 4.06 h and ratio of water to raw material of 29.1 mL/g. Under the optimized conditions, the yield of GMPs was 5.56%, which was similar to the predicted polysaccharides yield of 5.66%. A fraction named GMP-1 was obtained after isolation and purification by DEAE-52 and Sephadex G-100 gel chromatography, respectively. GMP-1, with a molecular weight of 401 kDa, mainly consisted of galacturonic acid (GalA), xylose (Xyl), glucose (Glu). Infrared spectroscopy was used to characterize the major functional groups of GMP-1 and the results indicated that it was an acidic polysaccharide. The antioxidant and α-glucosidase inhibitory activities of GMPs and GMP-1 were determined in vitro. The results indicated that GMPs and GMP-1 show potential for use in functional foods or medicines.

Preparation and characterization of magnesium borate for special glass

NASA Astrophysics Data System (ADS)

Dou, Lishuang; Zhong, Jianchu; Wang, Hongzhi

2010-05-01

Magnesium borate with a variety of B2O3/MgO molar ratios, which can be applied for special glass, has been prepared through the reaction of light-burned magnesia with boric acid by a hydrothermal method. The effects of the B2O3/MgO molar ratio of raw materials, reaction time, temperature and liquid to solid ratio (ml g-1) on the synthetic product are investigated. The XRD and TG-DTG analyses indicate that the prepared magnesium borate is a mixture of magnesium hexaborate hydrate and ascharite. The results show that high B2O3/MgO molar ratios of raw materials and low reaction liquid-solid ratios favour the product with a high B2O3/MgO molar ratio and vice versa. There exists free MgO in the product when the reaction temperature is below 140 °C or the reaction time is not enough, because of the incomplete reaction of magnesium oxide with boric acid. The process of fractional crystallization for the magnesium borate mixture is also discussed.

Effect of the raw materials and mixing ratio of composted wastes on the dynamic of organic matter stabilization and nitrogen availability in composts of Sub-Saharan Africa.

PubMed

Kaboré, Théodore Wind-Tinbnoma; Houot, Sabine; Hien, Edmond; Zombré, Prosper; Hien, Victor; Masse, Dominique

2010-02-01

The effect of raw materials and their proportions in initial mixtures on organic matter (OM) stabilization and nitrogen (N) availability during pit composting in Sub-Saharan Africa was assessed using biochemical fractionation and laboratory incubations to characterize composts sampled throughout the composting process. Stabilization of OM occurred more rapidly in mixtures with slaughter-house wastes, it was progressive in mixture with household refuses while tree leaves compost remained unstable. Carbon mineralization from compost samples was positively correlated to water soluble and hemicellulose-like organic fractions. Mixtures containing large proportions of household refuses reached the highest stability and total N but available N remained weak. Slaughter-house wastes in the initial mixtures made possible to reach good OM stabilization and the largest N availability. The nature of initial mixing influenced composting parameters, OM stabilization and N availability. It is suggested mixing household refuses and slaughter-house wastes with tree leaves to reach better amending and fertilizer qualities of composts.

Identification and characterization of hydrocolloid from Cordia myxa leaf.

PubMed

Samavati, Vahid; Lorestani, Mohammad; Joolazadeh, Sajjad

2014-04-01

Hot water extraction technique was employed to extract the hydrocolloid from Cordia myxa leaf (PCM). The optimal conditions for extraction of PCM were determined using response surface methodology. A Box-Behnken design (BBD) was applied to evaluate the effects of three independent variables (extraction time (X1: 1-4 h), extraction temperature (X2: 55-95 °C), and water to raw material ratio (X3: 5-30 ml/g) on the extraction yield of PCM. The content of moisture, water-soluble and water-insoluble ash, crude protein and total phenol were determined in the extracted hydrocolloid by standard methods. The maximum hydrocolloid extraction yield (9.501±0.15%) was achieved by using extraction time of 4.94 h, extraction temperature of 94.91 °C and water to raw material ratio of 21.74 ml/g. The contents of moisture, crude protein, water-soluble and water-insoluble ash and total phenol were 21.63±0.94%, 14.27±0.55%, 3.07±0.16% and 2.61±0.19 mg galic acid/g, respectively. Copyright © 2014 Elsevier B.V. All rights reserved.

FeCl3-catalyzed ethanol pretreatment of sugarcane bagasse boosts sugar yields with low enzyme loadings and short hydrolysis time.

PubMed

Zhang, Hongdan; Zhang, Shuaishuai; Yuan, Hongyou; Lyu, Gaojin; Xie, Jun

2018-02-01

An organosolv pretreatment system consisting of 60% ethanol and 0.025 mol·L -1 FeCl 3 under various temperatures was developed in this study. During the pretreatment, the highest xylose yield was 11.4 g/100 g raw material, representing 49.8% of xylose in sugarcane bagasse. Structural features of raw material and pretreated substrates were characterized to better understand how hemicellulose removal and delignification affected subsequent enzymatic hydrolysis. The 160 °C pretreated solid presented a remarkable glucose yield of 93.8% for 72 h. Furthermore, the influence of different additives on the enzymatic hydrolysis of pretreated solid was investigated. The results indicated that the addition of Tween 80 shortened hydrolysis time to 6 h and allowed a 50% reduction of enzyme loading to achieve the same level of glucose yield. This work suggested that FeCl 3 -catalyzed organosolv pretreatment could improve the enzymatic hydrolysis significantly and reduce the hydrolysis time and enzyme dosage with the addition of Tween 80. Copyright © 2017 Elsevier Ltd. All rights reserved.

75 FR 65658 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2010-10-26

... Raw Opium (9600) II Concentrate of Poppy Straw (9670) II The company plans to import narcotic raw... a manufacturer of several controlled substances that are manufactured from raw opium, poppy straw... narcotic raw material are not appropriate. As noted in a previous notice published in the Federal Register...

7 CFR 58.519 - Dairy products.

Code of Federal Regulations, 2011 CFR

2011-01-01

... Specifications for Dairy Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58.519 Dairy products. (a) Raw skim milk. All raw skim milk obtained from a secondary source... used, shall be prepared from raw milk or skim milk that meets the same quality requirements outlined...

Hardwood pallet cant quality and pallet part yields

Treesearch

Hal L. Mitchell; Marshall White; Philip Araman; Peter Hamner

2005-01-01

Raw materials are the largest cost component in pallet manufacturing. The primary raw material used to produce pallet parts are pallet cants. Therefore, pallet cant quality directly impacts pallet part processing and material costs. By knowing the quality of the cants being processed, pallet manufacturers can predict these costs and improve manufacturing efficiency....

Physicochemical of pillared clays prepared by several metal oxides

NASA Astrophysics Data System (ADS)

Rinaldi, Nino; Kristiani, Anis

2017-03-01

Natural clays could be modified by the pillarization method, called as Pillared Clays (PILCs). PILCs have been known as porous materials that can be used for many applications, one of the fields is catalysis. PILCs as two dimensional materials are interesting because their structures and textural properties can be controlled by using a metal oxide as the pillar. Different metal oxide used as the pillar causes different properties results of pillared clays. Usually, natural smectite clays/bentonites are used as a raw material. Therefore, a series of bentonite pillared by metal oxides was prepared through pillarization method. Variation of metals pillared into bentonite are aluminium, chromium, zirconium, and ferro. The physicochemical properties of catalysts were characterized by using X-ray Diffraction (XRD), Thermo Gravimetric Analysis (TGA), Brunauer-Emmett-Teller (BET) and Barret-Joyner-Halenda (BJH) analysis, and Fourier transform infrared spectroscopy (FTIR) measurement. Noteworthy characterization results showed that different metals pillared into bentonite affected physical and chemical properties, i.e. basal spacing, surface area, pore size distribution, thermal stability and acidity.

Particle Size Characterization of Water-Elutriated Libby Amphibole 2000 and RTI International Amosite

USGS Publications Warehouse

Lowers, Heather; Bern, Amy M.

2009-01-01

This report presents data on particle characterization analyzed by scanning electron microscopy on Libby amphibole collected by the U.S. Geological Survey in 2000 (LA2000) and amosite material collected by RTI International (RTI amosite). The particle characterization data were generated to support a portion of the Libby Action Plan. Prior to analysis, the raw LA2000 and RTI amosite materials were subjected to a preparation step. Each sample was water-elutriated by U.S. Environmental Protection Agency (USEPA) Office of Research and Development, Research Triangle Park using the methods generally described in another published report and then delivered to the U.S. Geological Survey, Denver Microbeam Laboratory for analysis. Data presented here represent analyses performed by the U.S. Geological Survey, Denver Microbeam Laboratory and USEPA National Enforcement Investigations Center. This report consists of two Excel spreadsheet files developed by USEPA, Region 8 Superfund Technical Assistance Unit and describe the particle size characterization of the LA2000 and RTI amosite, respectively. Multiple tabs and data entry cells exist in each spreadsheet and are defined herein.

77 FR 73426 - Glycine From the People's Republic of China: Final Partial Affirmative Determination of...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-12-10

... the Order because it is producing glycine from raw materials of Indian origin and exporting such... Order because it produced glycine from raw materials of Indian origin and exported such merchandise to...

Critical thinking: assessing the risks to the future security of supply of critical metals

NASA Astrophysics Data System (ADS)

Gunn, Gus

2015-04-01

Increasing world population, the spread of prosperity across the globe and the demands of new technologies have led to a revival of concerns about the availability of raw materials needed by society. Despite scare stories about resource depletion, physical exhaustion of minerals is considered to be unlikely. However, we do need to know which materials might be of concern so that we can develop strategies to secure adequate supplies and to mitigate the effects of supply disruption. This requirement has led to renewed interest in criticality, a term that is generally used to refer to metals and minerals of high economic importance that have a relatively high likelihood of supply disruption. The European Union (EU) developed a quantitative methodology for the assessment of criticality which led to the definition of 14 raw materials as critical to the EU economy (EC, 2010). This has succeeded in raising awareness of potential supply issues and in helping to prioritise requirements for new policies and supporting research. The EU has recently assessed a larger number of candidate materials of which 20 are now identified as critical to the EU (EC, 2014). These include metals such as indium, mostly used in flat-screen displays, antimony for flame retardants and cobalt for rechargeable batteries, alloys and a host of other products. Although there is no consensus on the methodology for criticality assessments and broad analyses at this scale are inevitably imperfect, they can, nevertheless, provide early warning of supply problems. However, in order to develop more rigorous and dynamic assessments of future availability detailed analysis of the whole life-cycle of individual metals to identify specific problems and develop appropriate solutions is required. New policies, such as the Raw Materials Initiative (2008) and the European Innovation Partnership on Raw Materials (2013), have been developed by the European Commission (EC) and are aimed at securing sustainable supplies of raw materials. These have led to major new programmes of research throughout the minerals value chain, in order to improve the raw materials knowledge base, to develop best practices and promote international collaboration. Although recycling will make an increasingly important contribution to supply, it can never meet the total requirement when demand is increasing. Therefore, new resources of primary materials, identified through geological research, will continue to be required. The availability of regional baseline datasets, comprising geological, geophysical and geochemical data, is fundamental to the identification of exploration targets. However, in order to focus exploration we also require robust mineral deposit models for the critical metals which hitherto these have been largely neglected because of their limited economic importance. For commodities such as the platinum-group metals (PGM), cobalt, niobium, indium, rare earth elements (REE) and cobalt we have some knowledge of the processes controlling their mobilisation and concentration under certain conditions although we have little understanding of the mechanisms of deposit formation elsewhere. We also need effective techniques to explore for these metals. This may involve the development of new geophysical techniques to explore on the sea-floor or beneath thick cover, or new analytical methods for the determination of these elements in exploration samples. Improved metallurgical techniques are also required for effective and energy-efficient recovery of critical metals from ores and concentrates. References European Commission (2010). Critical raw materials for the EU. Report of the Ad-hoc Working Group on Defining Critical Raw Materials. European Commission (2014). Report on Critical raw materials for the EU. Report of the Ad-hoc Working Group on Defining Critical Raw Materials.

The behavior of biogenic silica-rich rocks and volcanic tuffs as pozzolanic additives in cement

NASA Astrophysics Data System (ADS)

Fragoulis, Dimitris; Stamatakis, Michael; Anastasatou, Marianthi

2015-04-01

Cements currently produced, include a variety of pozzolanic materials, aiming for lower clinker addition and utilization of vast deposits of certain raw materials and/or mining wastes and byproducts. The major naturally occurring pozzolanic materials include glassy tuffs, zeolitic tuffs, diatomites and volcanic lavas rich in glassy phase, such as perlites. Therefore, based on the available raw materials in different locations, the cement composition might vary according to the accessibility of efficient pozzolanic materials. In the present investigation, the behavior of pozzolanic cements produced with representative samples of the aforementioned materials was studied, following the characterization of the implemented pozzolanas with respect to their chemical and mineralogical characteristics. Laboratory cements were produced by co-grinding 75% clinker, 5% gypsum and 20% pozzolana, for the same period of time (45 min). Regarding pozzolanic materials, four different types of pozzolanas were utilized namely, diatomite, perlite, zeolite tuff and glassy tuff. More specifically, two diatomite samples originated from Australia and Greece, with high and low reactive silica content respectively, two perlite samples originated from Turkey and from Milos Island, Greece, with different reactive silica contents, a zeolite tuff sample originated from Turkey and a glassy tuff sample originated from Milos Island, Greece. The above pozzolana samples, which were ground in the laboratory ball mill for cement production performed differently during grinding and that was reflected upon the specific surface area (cm2/gr) values. The perlites and the glassy tuff were the hardest to grind, whereas, the zeolite tuff and the Australian diatomite were the easiest ones. However, the exceedingly high specific surface area of the Australian diatomite renders cement difficult to transport and tricky to use for concrete manufacturing, due to the high water demand of the cement mixture. Regarding late compressive strength, the worst performing cement was the one with the lowest reactive silica content with biogenic opal-A as the only reactive pozzolana constituent. Cements produced with perlites, raw materials consisting mainly of a glassy phase, were characterized by higher strength and a rather ordinary specific surface area. Cements produced with Turkish zeolite tuff and Milos glassy tuff exhibited higher late compressive strength than those mentioned above. The highest strength was achieved by the implementation of Australian diatomite for cement production. Its 28 day strength exceeded that of the control mixture consisting of 95% clinker and 5% gypsum. That could be attributed to both, high specific surface of cement and reactive SiO2 of diatomite. Therefore, a preliminary assessment regarding late strength of pozzolanic cements could be obtained by the consideration of two main parameters, namely: specific surface area of cement and reactive silica content of pozzolana.

Waste Material Based "Terrazzo" Tiles: The Effect Of Curing Time And Extreme Environmental Conditions Over Glass Aggregate/Cement Matrix Boundary

NASA Astrophysics Data System (ADS)

Paris, E.; Radica, F.; Stabile, P.; Ansaloni, F.; Giuli, G.; Carroll, M. R.

2017-12-01

Currently, more than half of all materials extracted globally (over three billion tonnes/year in the EU only) are transformed for use in construction. Before year 2020, the EU aims to reduce the environmental impact of the construction sector by recycling or re-using large amounts of these materials, thus reducing the consumption of raw materials and helping promote the sector's economic stability. With this challenge in mind an aesthetically pleasant and fully recycled (up to 78%) pre-cast cement based tile (Terrazzo tiles) was designed by replacing raw materials with Glass Waste (GW) and Construction/Demolition Waste (CDW). Several recent studies explored the effect of the addition of GW in the manufacture of urban pavements, concluding that the use of GW can improve various phases of pavement life and structure by enhancing the structural performance, durability, environmental friendliness, and aesthetic features. In this study we extend this knowledge also to interior cement-based tiles by evaluating the technical performances of this this novel designed tile, in particular by focusing on the interface between the GW aggregates and different Portland cement based matrix at extreme environmental conditions. For this work three representative waste material based "terrazzo" tiles were selected and characterized by means of XRD and SEM imaging in order to study the boundary effect between GW aggregate and different binding materials: limestone powder, quartz powder and fine ground WG powder. A fourth additional mixture of Portland cement and CDW material was characterized. Fragments of a Limestone matrix tile were also thermally threated at -18°C and at 60°C for one week to witness the possible formation of new harmful phases at the grain-matrix boundary. Preliminary results on X-ray diffraction patterns show that 1 year after manufacture and/or thermal treatment there is no new formation of harmful phases other than the starting ones. High magnification SEM imaging further confirmed this observation also highlighting the good binding performances of a mixture composed by the 78% of recycled WG.

77 FR 34069 - Importer of Controlled Substances; Notice of Application; Research Triangle Institute

Federal Register 2010, 2011, 2012, 2013, 2014

2012-06-08

... activities. Comments and requests for hearings on applications to import narcotic raw material are not appropriate. 72 FR 3417 (2007). In regard to the non-narcotic raw material, any bulk manufacturer who is... [[Page 34072

Colour of ground beef as influenced by raw materials, addition of sodium chloride and low oxygen packaging.

PubMed

Sørheim, O; Westad, F; Larsen, H; Alvseike, O

2009-03-01

The study aimed at examining the effects of freezing of raw materials, holding time for fresh raw materials post mortem and addition of 0.5-1.0% NaCl on the colour of ground beef under low oxygen (O2) modified atmosphere storage. The samples were exposed to 0.1-3.0% O2 at 4°C for up to 10 days, and analysed for O2 concentrations, instrumental and visual colour. Residual O2 in the headspace of the packages oxidizes myoglobin and discolours the meat. Meat may have the ability to scavenge residual O2, and ground beef differs from intact muscles by having a much higher capacity for O2 consumption. In this experiment, the use of frozen/thawed raw materials and addition of NaCl both decreased the rate of O2 consumption and increased discolouration. Using raw materials from 2 days rather than 7 days post mortem greatly increased the rate of removal of O2 and improved redness. In low O2 packaging, ground beef preferably should be stored for at least 2 days in an atmosphere with less than 0.1% residual O2 to produce a purple pigment predominantly consisting of deoxymyoglobin.

Effects and detection of raw material variability on the performance of near-infrared calibration models for pharmaceutical products.

PubMed

Igne, Benoit; Shi, Zhenqi; Drennen, James K; Anderson, Carl A

2014-02-01

The impact of raw material variability on the prediction ability of a near-infrared calibration model was studied. Calibrations, developed from a quaternary mixture design comprising theophylline anhydrous, lactose monohydrate, microcrystalline cellulose, and soluble starch, were challenged by intentional variation of raw material properties. A design with two theophylline physical forms, three lactose particle sizes, and two starch manufacturers was created to test model robustness. Further challenges to the models were accomplished through environmental conditions. Along with full-spectrum partial least squares (PLS) modeling, variable selection by dynamic backward PLS and genetic algorithms was utilized in an effort to mitigate the effects of raw material variability. In addition to evaluating models based on their prediction statistics, prediction residuals were analyzed by analyses of variance and model diagnostics (Hotelling's T(2) and Q residuals). Full-spectrum models were significantly affected by lactose particle size. Models developed by selecting variables gave lower prediction errors and proved to be a good approach to limit the effect of changing raw material characteristics. Hotelling's T(2) and Q residuals provided valuable information that was not detectable when studying only prediction trends. Diagnostic statistics were demonstrated to be critical in the appropriate interpretation of the prediction of quality parameters. © 2013 Wiley Periodicals, Inc. and the American Pharmacists Association.

Materials, critical materials and clean-energy technologies

NASA Astrophysics Data System (ADS)

Eggert, R.

2017-07-01

Modern engineered materials, components and systems depend on raw materials whose properties provide essential functionality to these technologies. Some of these raw materials are subject to supply-chain risks, and such materials are known as critical materials. This paper reviews corporate, national and world perspectives on material criticality. It then narrows its focus to studies that assess "what is critical" to clean-energy technologies. The focus on supply-chain risks is not meant to be alarmist but rather to encourage attention to monitoring these risks and pursuing technological innovation to mitigate the risks.

Dynamical tests on fiber optic data taken from the riser section of a circulating fluidized bed

DOE Office of Scientific and Technical Information (OSTI.GOV)

Taylor, E.M.; Guenther, C.P.; Breault, R.W.

2007-11-01

Dynamical tests have been applied to fiber optic data taken from a cold-flow circulating fluidized bed to characterize flow conditions, identify three time and/or length scales (macro, meso, and micro), and understand the contribution these scales have on the raw data. The characteristic variable analyzed is the raw voltage signal obtained from a fiber-optic probe taken at various axial and radial positions under different loading conditions so that different flow regimes could be attained. These experiments were carried out with the bed material of 812 μm cork particles. The characterization was accomplished through analysis of the distribution of the signalmore » through the third and fourth moments of skewness and excess kurtosis. A generalization of the autocorrelation function known as the average mutual information function was analyzed by examining the function’s first minimum, identifying the point at which successive elements are no longer correlated. Further characterization was accomplished through the correlation dimension, a measure of the complexity of the attractor. Lastly, the amount of disorder of the system is described by a Kolmogorov-type entropy estimate. All six aforementioned tests were also implemented on ten levels of detail coefficients resulting from a discrete wavelet transformation of the same signal as used above. Through this analysis it is possible to identify and describe micro (particle level), meso (clustering or turbulence level), and macro (physical or dimensional level) length scales even though some literature considers these scales inseparable [6]. This investigation also used detail wavelet coefficients in conjunction with ANOVA analysis to show which scales have the most impact on the raw signal resulting from local hydrodynamic conditions.« less

Attrition of limestone by impact loading in fluidized beds

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fabrizio Scala; Fabio Montagnaro; Piero Salatino

2007-09-15

The present study addresses limestone attrition and fragmentation associated with impact loading, a process which may occur extensively in various regions of fluidized bed (FB) combustors/gasifiers, primarily the jetting region of the bottom bed, the exit region of the riser, and the cyclone. An experimental protocol for the characterization of the propensity of limestone to undergo attrition/fragmentation by impact loading is reported. The application of the protocol is demonstrated with reference to an Italian limestone whose primary fragmentation and attrition by surface wear have already been characterized in previous studies. The experimental procedure is based on the characterization of themore » amount and particle size distribution of the debris generated upon the impact of samples of sorbent particles against a target. Experiments were carried out at a range of particle impact velocities between 10 and 45 m/s, consistent with jet velocities corresponding to typical pressure drops across FB gas distributors. The protocol has been applied to either raw or preprocessed limestone samples. In particular, the effect of calcination, sulfation, and calcination/recarbonation cycles on the impact damage suffered by sorbent particles has been assessed. The measurement of particle voidage and pore size distribution by mercury intrusion was also accomplished to correlate fragmentation with the structural properties of the sorbent samples. Fragmentation by impact loading of the limestone is significant. Lime displays the largest propensity to undergo impact damage, followed by the sorbent sulfated to exhaustion, the recarbonated sorbent, and the raw limestone. Fragmentation of the raw limestone and of the sulfated lime follows a pattern typical of the failure of brittle materials. The fragmentation behavior of lime and recarbonated lime better conforms to a disintegration failure mode, with an extensive generation of very fine fragments. 27 refs., 9 figs. 1 tab.« less

Raw liquid waste treatment process

NASA Technical Reports Server (NTRS)

Humphrey, Marshall F. (Inventor)

1980-01-01

A raw sewage treatment process is disclosed in which substantially all the non-dissolved matter, which is suspended in the sewage water is first separated from the water, in which at least organic matter is dissolved. The non-dissolved material is pyrolyzed to form an activated carbon and ash material without the addition of any conditioning agents. The activated carbon and ash material is added to the water from which the non-dissolved matter was removed. The activated carbon and ash material absorbs organic matter and heavy metal ions, it is believed, are dissolved in the water and is thereafter supplied in a counter current flow direction and combined with the incoming raw sewage to facilitate the separation of the non-dissolved settleable materials from the sewage water. The used carbon and ash material together with the non-dissolved matter which was separated from the sewage water are pyrolyzed to form the activated carbon and ash material.

Raw Liquid Waste Treatment System and Process

NASA Technical Reports Server (NTRS)

Humphrey, M. F. (Inventor)

1974-01-01

A raw sewage treatment process is disclosed in which substantially all the non-dissolved matter, suspended in the sewage water is first separated from the water, in which at least organic matter remains dissolved. The non-dissolved material is pyrolyzed to form an activated carbon and ash material without the addition of any conditioning agents. The activated carbon and ash material is added to the water from which the non-dissolved matter was removed. The activated carbon and ash material adsorbs the organic matter dissolved in the water and is thereafter supplied in a counter flow direction and combined with the incoming raw sewage to at least facilitate the separation of the non-dissolved settleable materials from the sewage water. Carbon and ash material together with the non-dissolved matter which was separated from the sewage water are pyrolyzed to form the activated carbon and ash material.

Ozonation catalyzed by the raw bauxite for the degradation of 2,4,6-trichloroanisole in drinking water.

PubMed

Qi, Fei; Xu, Bingbing; Chen, Zhonglin; Ma, Jun; Sun, Dezhi; Zhang, Liqiu; Wu, Fengchang

2009-08-30

A kind of inexpensive and environmental friendly mineral, the raw bauxite has been used successfully as a catalyst combined with ozonation in the degradation of 2,4,6-trichloroanisole (TCA). The catalyst was characterized by using various analytical techniques. X-ray powder diffraction (XRD) characterization showed that the raw bauxite containing boehmite (gamma-AlOOH), kaolinite (Al(2)Si(2)O(5)(OH)(4)) and quartz (SiO(2)), and gamma-AlOOH was the major composition. The catalytic ozonation removal effectiveness of TCA was investigated under various physicochemical conditions. Both the adsorption and the single ozonation were not effective for the degradation of TCA, and the presence of the raw bauxite in ozonation enhanced the TCA removal effectiveness. Both the hydroxyl radicals (OH) scavenging experiment and R(ct) characterization confirmed that the generation of OH was accounted for the enhancement of the degradation of TCA. The generation of OH was inhibited faintly by the presence of both natural organic matters (NOMs) and alkalinity in the natural water during catalyzed ozonation with the raw bauxite. The increasing of both the bauxite dosage and the ozone dosage enhanced the removal effectiveness of TCA. The raw bauxite was an efficient green catalyst for TCA degradation in drinking water.

Characterization of Maize Grains with Different Pigmentation Investigated by Photoacoustic Spectroscopy

NASA Astrophysics Data System (ADS)

Rico Molina, R.; Hernández Aguilar, C.; Dominguez Pacheco, A.; Cruz-Orea, A.; López Bonilla, J. L.

2014-10-01

A knowledge of grains' optical parameters is of great relevance in the maize grain technology practice. Such parameters provide information about its absorption and reflectance, which in turn is related to its color. In the dough and tortilla industries, it is important to characterize this attribute of the corn kernel, as it is one of the attributes that directly affects the quality of the food product. Thus, it is important to have techniques that contribute to the characterization of this raw material. It is traditionally characterized by conventional methods, which usually destroy the grain and involve a laborious preparation of material plus they are expensive. The objective of this study was to determine the optical absorption coefficient for maize grains ( Zea mays L.) with different pigmentations by means of photoacoustic spectroscopy (PAS). The genotype A had bluish coloration and genotype B had yellowish coloration. In addition, the photoacoustic signal obtained by two methods was analyzed mathematically: the standard deviation and the first derivative; both results were compared (Fig. 1). In combination with mathematical analysis, PAS may be considered as a potential diagnostic tool for the characterization of the grains. [Figure not available: see fulltext.

The Self-Reducing Pellet Production from Organic Household Waste

NASA Astrophysics Data System (ADS)

Nogueira, Alberto; Takano, Cyro; Mourão, Marcelo; Pillihuaman, Adolfo

The organic household waste has a growing disposal problem, requiring costly disposal systems. It is necessary to find new applications for these materials; one could be the steelmaking raw material production. In this paper is studied the development of self-reducing pellets from the organic waste pyrolysis, where is generated carbon and condensable and non-condensable volatiles. Non-condensable volatiles were burned and condensable volatiles were recovered. The resulting tar was mixed with iron ore, coal powder and flux (CaO), to then be pelletized together. Compression, falls and tumbler tests were conducted to characterize the pellets before and after heat treatment and reduction processes. The reduction curve and their physical and morphological characterization were measured. The results were as was expected, the fluidized coal create sufficient adhesion that pellets earned resistance with an equivalent resistance of common pellets, showing a good feasibility of this process.

Preparation and characterization of 'green' hybrid clay-dye nanopigments

NASA Astrophysics Data System (ADS)

Kaya, Mehmet; Onganer, Yavuz; Tabak, Ahmet

2015-03-01

We obtained a low cost and abundant nanopigment material composed of Rhodamine B (Rh-B) organic dye compound and Unye bentonite (UB) clay from Turkey. The characterization of the nanopigment was investigated using scanning electron microscopy (SEM), particle size distribution, powder X-ray diffraction (PXRD), Fourier transformed infra-red spectroscopy (FT-IR) and thermal analysis techniques. According to the result of texture analyses, we showed that the particle size distribution (d: 0.5-mean distribution) of Rh-B/UB nanopigment material was around 100 nm diameter. It was also demonstrated that the samples had a particle size around nm diameter in SEM images. As seen in the PXRD and thermal analysis, there is a difference in basal spacing by 1.46° (2θ) and a higher mass loss by 7.80% in the temperature range 200-500 °C compared to the raw bentonite.

21 CFR 1303.23 - Procedure for fixing individual manufacturing quotas.

Code of Federal Regulations, 2010 CFR

2010-04-01

... economic and physical availability of raw materials for use in manufacturing and for inventory purposes, yield and stability problems, potential disruptions to production (including possible labor strikes... current inventory position, the economic and physical availability of raw materials for use in...

Use of outer planet satellites and asteroids as sources of raw materials for life support systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Molton, P.M.; Divine, T.E.

1977-01-01

Industrialization of space and other space activities depend entirely on supply of materials from the Earth. This is a high cost route for materials supply. Space industrialization will require life support systems for maintenance and operation staff and these will of necessity be of a sophisticated nature. Use of raw materials obtained by an unmanned space shuttle, initially, and by manned shuttles later could significantly reduce the cost of life support in space. These raw materials could be obtained from small asteroids and satellites, and would consist of primary nutrients. Future development of such sources is discussed, including food productionmore » in automated asteroid-based facilities. The level of technology required is available now, and should become economical within a century.« less

Graphene Oxide Directed One-Step Synthesis of Flowerlike Graphene@HKUST-1 for Enzyme-Free Detection of Hydrogen Peroxide in Biological Samples.

PubMed

Wang, Qingxiang; Yang, Yizhen; Gao, Feng; Ni, Jiancong; Zhang, Yanhui; Lin, Zhenyu

2016-11-30

A novel metal-organic framework (MOF)-based electroactive nanocomposite containing graphene fragments and HKUST-1 was synthesized via a facile one-step solvothermal method using graphene oxide (GO), benzene-1,3,5-tricarboxylic acid (BTC), and copper nitrate (Cu(NO 3 ) 2 ) as the raw materials. The morphology and structure characterization revealed that the GO could induce the transformation of HKUST-1 from octahedral structure to the hierarchical flower shape as an effective structure-directing agent. Also, it is interesting to find out that the GO was torn into small fragments to participate in the formation of HKUST-1 and then transformed into the reduction form during the solvothermal reaction process, which dramatically increased the surface area, electronic conductivity, and redox-activity of the material. Electrochemical assays showed that the synergy of graphene and HKUST-1 in the nanocomposite leaded to high electrocatalysis, fast response, and excellent selectivity toward the reduction of hydrogen peroxide (H 2 O 2 ). Based on these remarkable advantages, satisfactory results were obtained when the nanocomposite was used as a sensing material for electrochemical determination of H 2 O 2 in the complex biological samples such as human serum and living Raw 264.7 cell fluids.

Ultrasound-assisted extraction and characterization of hydrolytic and oxidative enzymes produced by solid state fermentation.

PubMed

Szabo, Orsolya Erzsebet; Csiszar, Emilia; Toth, Karolina; Szakacs, George; Koczka, Bela

2015-01-01

Ligninolytic and hydrolytic enzymes were produced with six selected fungi on flax substrate by solid state fermentation (SSF). The extracellular enzyme production of the organisms in two SSF media was evaluated by measuring the soluble protein concentration and the filter paper, endoxylanase, 1,4-β-d-glucosidase, 1,4-β-d-endoglucanase, polygalacturonase, lignin peroxidase, manganese peroxidase and laccase activities of the clear culture solutions produced by conventional extraction from the SSF materials. The SSF material of the best enzyme producer (Trichoderma virens TUB F-498) was further investigated to enhance the enzyme recovery by low frequency ultrasound treatment. Performance of both the original and ultrasound macerated crude enzyme mixtures was evaluated in degradation of the colored lignin-containing and waxy materials of raw linen fabric. Results proved that sonication (at 40%, 60% and 80% amplitudes, for 60min) did not result in reduction in the filter paper, lignin peroxidase and laccase activities of the crude enzyme solution, but has a significant positive effect on the efficiency of enzyme extraction from the SSF material. Depending on the parameters of sonication, the enzyme activities in the extracts obtained can be increased up to 129-413% of the original activities measured in the control extracts recovered by a common magnetic stirrer. Sonication also has an effect on both the enzymatic removal of the lignin-containing color materials and hydrophobic surface layer from the raw linen. Copyright © 2014 Elsevier B.V. All rights reserved.

Rambutan Seed (Nephelium Lappaceum L.) Optimization as Raw Material of High Nutrition Value Processed Food

NASA Astrophysics Data System (ADS)

Wahini, M.; Miranti, M. G.; Lukitasari, F.; Novela, L.

2018-02-01

Rambutan (Nephelium Lappaceum L.) is a plant that identical with Southeast Asian countries, in some areas of Indonesia no exception, but rambutan seed is considered as a waste. Therefore, it needs to be optimized into raw materials of food and processed with high nutritional value and has economic value. The purpose of this research were: 1) to find the best rambutan seed immersion formula; 2) to know the nutritional value of the best immersed rambutan seed; 3) to produce raw material and various processed of rambutan seed product. The research method was quasi experiment with 6 treatments and 2 factorial design, materials for immersion was NaCl and Ca(OH)2. The results showed that: 1) the best rambutan seed immersion formula was using Ca(OH)2; 2) the best rambutan seed contains 1,6 ash, 31,2 protein, 26,9 fat; 3) the best rambutan seed produce flour and processed of seasoned nuts. This research indicates that rambutan seed is very potential to be an alternative high-value raw materials.

Not Just Lumber—Using Wood in the Sustainable Future of Materials, Chemicals, and Fuels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jakes, Joseph E.; Arzola, Xavier; Bergman, Rick

Forest-derived biomaterials can play an integral role in a sustainable and renewable future. Research across a range of disciplines is required to develop the knowledge necessary to overcome the challenges of incorporating more renewable forest resources in materials, chemicals, and fuels. We focus on wood specifically because in our view, better characterization of wood as a raw material and as a feedstock will lead to its increased utilization. We first give an overview of wood structure and chemical composition and then highlight current topics in forest products research, including (1) industrial chemicals, biofuels, and energy from woody materials; (2) wood-basedmore » activated carbon and carbon nanostructures; (3) development of improved wood protection treatments; (4) massive timber construction; (5) wood as a bioinspiring material; and (6) atomic simulations of wood polymers. We conclude with a discussion of the sustainability of wood as a renewable forest resource.« less

Not Just Lumber—Using Wood in the Sustainable Future of Materials, Chemicals, and Fuels

NASA Astrophysics Data System (ADS)

Jakes, Joseph E.; Arzola, Xavier; Bergman, Rick; Ciesielski, Peter; Hunt, Christopher G.; Rahbar, Nima; Tshabalala, Mandla; Wiedenhoeft, Alex C.; Zelinka, Samuel L.

2016-09-01

Forest-derived biomaterials can play an integral role in a sustainable and renewable future. Research across a range of disciplines is required to develop the knowledge necessary to overcome the challenges of incorporating more renewable forest resources in materials, chemicals, and fuels. We focus on wood specifically because in our view, better characterization of wood as a raw material and as a feedstock will lead to its increased utilization. We first give an overview of wood structure and chemical composition and then highlight current topics in forest products research, including (1) industrial chemicals, biofuels, and energy from woody materials; (2) wood-based activated carbon and carbon nanostructures; (3) development of improved wood protection treatments; (4) massive timber construction; (5) wood as a bioinspiring material; and (6) atomic simulations of wood polymers. We conclude with a discussion of the sustainability of wood as a renewable forest resource.

Improved silicon nitride for advanced heat engines

NASA Technical Reports Server (NTRS)

Yeh, H. C.; Wimmer, J. M.

1986-01-01

Silicon nitride is a high temperature material currently under consideration for heat engine and other applications. The objective is to improve the net shape fabrication technology of Si3N4 by injection molding. This is to be accomplished by optimizing the process through a series of statistically designed matrix experiments. To provide input to the matrix experiments, a wide range of alternate materials and processing parameters was investigated throughout the whole program. The improvement in the processing is to be demonstrated by a 20 percent increase in strength and a 100 percent increase in the Weibull modulus over that of the baseline material. A full characterization of the baseline process was completed. Material properties were found to be highly dependent on each step of the process. Several important parameters identified thus far are the starting raw materials, sinter/hot isostatic pressing cycle, powder bed, mixing methods, and sintering aid levels.

Effect of the raw material type and the reaction time on the synthesis of halloysite based Zeolite Na-P1

NASA Astrophysics Data System (ADS)

Meftah, Mahdi; Oueslati, Walid; Chorfi, Nejmeddine; Ben Haj Amara, Abdesslem

Zeolites are currently one of the most important classes of inorganic materials because of their multiple applications not only as ions exchangers and molecular sieves, but also as catalysts. This works focus the synthesis and the characterization of Zeolite Na-P1 using halloysite (collected near Ain Khemouda, western Tunisia) as the starting material. Two parameters, such as the host materials type (natural or treated) and the reaction time, involved in the synthesis process are investigated. The intermediate phases and final products were characterized by X-ray diffraction, Infrared IR spectroscopy, scanning electron microscopy and high-resolution 29Si and 27Al MAS NMR. Obtained results show that the hydrothermal synthesis from natural and heated-halloysite leads to formation of homogenous Zeolite Na-P1. The difference in the crystallization/transformation time process is explained by the effect of the dissolution rate of the starting materials in sodium hydroxide solution. In the case of heated halloysite, the synthesis reaction with alkali solution occurs very readily and achieved without prior thermal activation at high temperature. The optimal conditions of Zeolite Na-P1 crystallization, from heated-halloysite, are reached at 120 °C.

21 CFR 1315.23 - Procedure for fixing individual manufacturing quotas.

Code of Federal Regulations, 2010 CFR

2010-04-01

...) The economic and physical availability of raw materials for use in manufacturing and for inventory purposes, (iv) Yield and stability problems, (v) Potential disruptions to production (including possible... cycle and current inventory position. (iii) The economic and physical availability of raw materials for...

40 CFR 63.1251 - Definitions.

Code of Federal Regulations, 2014 CFR

2014-07-01

... other direct effect in the diagnosis, cure, mitigation, treatment, or prevention of disease, or to... this section. Consumption means the quantity of all HAP raw materials entering a process in excess of... as added as a raw material, consumption includes the quantity generated in the process. Container, as...

40 CFR 63.1251 - Definitions.

Code of Federal Regulations, 2013 CFR

2013-07-01

... other direct effect in the diagnosis, cure, mitigation, treatment, or prevention of disease, or to... this section. Consumption means the quantity of all HAP raw materials entering a process in excess of... as added as a raw material, consumption includes the quantity generated in the process. Container, as...

VIEW ALONG RAW MATERIAL CONVEYOR AT RIGHT WITH CRUSHED SHELL ...

Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

VIEW ALONG RAW MATERIAL CONVEYOR AT RIGHT WITH CRUSHED SHELL CONVEYOR ABOVE. ENGINE AND RADIATOR AT LOWER LEFT. - F. & H. Benning Company Oyster Mill, 14430 Solomons Island Road (moved from 1014 Benning Road, Galesville, Anne Arundel County, Maryland), Solomons, Calvert County, MD

40 CFR 415.91 - Specialized definitions.

Code of Federal Regulations, 2010 CFR

2010-07-01

... of any raw material, intermediate product, finished product, by-product, or waste product. The term... contact with any raw material, intermediate product, finished product, by-product or waste product by... this subpart. (b) The term product shall mean hydrogen peroxide as a one hundred percent hydrogen...

Aluminium content of some processed foods, raw materials and food additives in China by inductively coupled plasma-mass spectrometry.

PubMed

Deng, Gui-Fang; Li, Ke; Ma, Jing; Liu, Fen; Dai, Jing-Jing; Li, Hua-Bin

2011-01-01

The level of aluminium in 178 processed food samples from Shenzhen city in China was evaluated using inductively coupled plasma-mass spectrometry. Some processed foods contained a concentration of up to 1226 mg/kg, which is about 12 times the Chinese food standard. To establish the main source in these foods, Al levels in the raw materials were determined. However, aluminium concentrations in raw materials were low (0.10-451.5 mg/kg). Therefore, aluminium levels in food additives used in these foods was determined and it was found that some food additives contained a high concentration of aluminium (0.005-57.4 g/kg). The results suggested that, in the interest of public health, food additives containing high concentrations of aluminium should be replaced by those containing less. This study has provided new information on aluminium levels in Chinese processed foods, raw materials and a selection of food additives.

Physico-chemical characteristics of shallot New-Superior Varieties (NSV) from Indonesia

NASA Astrophysics Data System (ADS)

Sukasih, E.; Setyadjit; Musadad, D.

2018-01-01

Shallot is one of the priority agricultural commodities to be developed in Indonesia to reduce import and to stabilize domestic supply. The efforts include the selection of varieties, seed technology, agronomy, handling and processing to extend the supply and added value. Indonesian Agency for Agricultural Research and Development (IAARD) has purified, cross-pollinated, selected and released new varieties called New Superior Varieties (NSV) to farmers. The purpose of this research was to investigate the characteristic of fresh shallot NSV by understanding its potential for raw material of processed product. A completely randomized design (CRD) of single factor of ten local varieties of shallot such as Cv. Sembrani, Cv. Kuning, Cv. Pancasona, Cv. Bima, Cv. Trisula, Cv. Pikatan, Cv. Katumi, Cv. Kramat-2, Cv. Mentes and Cv. Majalok of three replication was used to arrange the experiment. The results showed that shallot New Superior Varieties (NSV) were significant by effect the physico-chemical parameters, such as diameter, length, weight of both in main bulb and tiller bulb, fat total, carbohydrate, crude fiber, starch content, antioxidant capacity and quercetin. Of the ten varieties of shallot characterized, the largest bulbs are Cv. Sembrani i.e 5.30 ± 0.3g per bulb, the best red color for shallot peeled was Cv. Kuning. Furthermore Cv. Pancasona have the highest protein content of 4.23 ± 0.2%, Cv. Mentes have the highest functional properties of quercetin 1766.4 ± 134 ppm. Shallot varieties such as Cv. Sembrani, Cv. Bima, Cv. Kuning and Cv. Trisula suitable for use as fresh product. Shallot varieties such as Cv. Pikatan, Cv. Pancasona, Cv. Katumi and Cv. Kramat-2 are suitable as raw materials for processed products. Cv. Mentes and Cv. Majalok were potential for raw materials of functional food and pharmaceutical industries.

[Understanding and development strategy of health food containing Chinese materia medica].

PubMed

Wang, Lin-Yuan; Zhang, Jian-Jun; Wang, Chun; Wang, Jing-Xia; Zhu, Ying-Li; Wang, Jia; Gao, Xue-Min

2016-11-01

Health food containing Chinese materia medica (CMM) conforms to the development demands of the age of big health and the theory of preventive treatment. In the view of health care and improvement of resisting diseases, it plays an important role in the market. It is very necessary to have further study and discussion on health food containing CMM. First of all, by comparing, analyzing and summarizing, the health food containing CMM could be defined as the health food which is qualified in security and functionality evaluation, with the traditional Chinese medicines(TCM) within TCM standards as the main raw materials, and the formulation-composition is based on the theory of TCM. It is characterized by higher safety than medicines, stronger biological activities than common food, multiple forms, abundant raw materials and integrated supervision and management. Secondly, we discussed the research and development (R&D) strategies and rules of health food containing CMM, pointing out that the core tasks of R&D include the investigation of formula, technology and the standards of quality. The fundamental principles of declaration and production include scientificity, rationality, reality and uniformity. Three key requirements (security, functionality and controllability) in the review as well as the process management of R&D and the key-points of risks control were summarized in this paper. Finally, the dynamic trends of policies and regulations related to health food containing CMM were analyzed in the view of registration, recording, raw materials and functions, and then related suggestions were proposed. Therefore, this article will be helpful in overall understanding the health food containing CMM and play a guiding role for its research and development. Copyright© by the Chinese Pharmaceutical Association.

Comparative physicochemical and biological characterization of NIST Interim Reference Material PM2.5 and SRM 1648 in human A549 and mouse RAW264.7 cells.

PubMed

Mitkus, Robert J; Powell, Jan L; Zeisler, Rolf; Squibb, Katherine S

2013-12-01

The epidemiological association between exposure to fine particulate matter (PM2.5) and adverse health effects is well-known. Here we report the size distribution, metals content, endotoxin content, and biological activity of National Institute of Standards and Technology (NIST) Interim Reference Material (RM) PM2.5. Biological activity was measured in vitro by effects on cell viability and the release of four inflammatory immune mediators, from human A549 alveolar epithelial cells or murine RAW264.7 monocytes. A dose range covering three orders of magnitude (1-1000μg/mL) was tested, and biological activity was compared to an existing Standard Reference Material (SRM) for urban PM (NIST SRM 1648). Robust release of IL-8 and MCP-1 from A549 cells was observed in response to IRM PM2.5 exposures. Significant TNF-α, but not IL-6, secretion from RAW264.7 cells was observed in response to both IRM PM2.5 and SRM 1648 particle types. Cytokine or chemokine release at high doses often occurred in the presence of cytotoxicity, likely as a result of externalization of preformed mediator. Our results are consistent with a local cytotoxic and pro-inflammatory mechanism of response to exposure to inhaled ambient PM2.5 and reinforce the continued relevance of in vitro assays for mechanistic research in PM toxicology. Our study furthers the goal of developing reference samples of environmentally relevant particulate matter of various sizes that can be used for hypothesis testing by multiple investigators. Published by Elsevier Ltd.

Raw materials exploitation in Prehistory of Georgia: sourcing, processing and distribution

NASA Astrophysics Data System (ADS)

Tushabramishvili, Nikoloz; Oqrostsvaridze, Avthandil

2016-04-01

Study of raw materials has a big importance to understand the ecology, cognition, behavior, technology, culture of the Paleolithic human populations. Unfortunately, explorations of the sourcing, processing and distribution of stone raw materials had a less attention until the present days. The reasons of that were: incomplete knowledge of the archaeologists who are doing the late period archaeology (Bronze Age-Medieval) and who are little bit far from the Paleolithic technology and typology; Ignorance of the stone artifacts made on different kind of raw-materials, except flint and obsidians. Studies on the origin of the stone raw materials are becoming increasingly important since in our days. Interesting picture and situation have been detected on the different sites and in different regions of Georgia. In earlier stages of Middle Paleolithic of Djruchula Basin caves the number of basalt, andesite, argillite etc. raw materials are quite big. Since 130 000 a percent of the flint raw-material is increasing dramatically. Flint is an almost lonely dominated raw-material in Western Georgia during thousand years. Since approximately 50 000 ago the first obsidians brought from the South Georgia, appeared in Western Georgia. Similar situation has been detected by us in Eastern Georgia during our excavations of Ziari and Pkhoveli open-air sites. The early Lower Paleolithic layers are extremely rich by limestone artifacts while the flint raw-materials are dominated in the Middle Paleolithic layers. Study of these issues is possible to achieve across chronologies, the origins of the sources of raw-materials, the sites and regions. By merging archaeology with anthropology, geology and geography we are able to acquire outstanding insights about those populations. New approach to the Paleolithic stone materials, newly found Paleolithic quarries gave us an opportunities to try to achieve some results for understanding of the behavior of Paleolithic populations, geology and geomorphology of different regions of Georgia. References: 1. 2015. Tushabramishvili N. Ziari. Online Archaeology 8. Tbilisi, Georgia. Pp. 41-43 2. 2012. M François-Xavier Le Bourdonnec, Sébastien Nomade, Gérard Poupeau, Hervé Guillou, Nikolos Tushabramishvili, Marie-Hélène Moncel, David Pleurdeau, Tamar Agapishvili, Pierre Voinchet, Ana Mgeladze, David Lordkipanidze). Multiple origins of Bondi Cave and Ortvale Klde (NW Georgia) obsidians and human mobility in Transcaucasia during the Middle and Upper Palaeolithic. Journal of Archaeological Science xxx (2012) 1-14 3. 2011. Mercier N., Valladas H., Meignen L., Joron J. L., Tushabramishvili N., Adler D.S., Bar Yosef O. Dating the early Middle Palaeolithic Laminar Industry from Djruchula cave, Republic of Georgia. Paléorient Volume 36. Issue 36-2, pp. 163-173 4. 2010. L. Meignen&Nicholas Tushabramishvili. Djruchula Cave, on the Southern Slopes of the Great Caucasus: An Extension of the Near Eastern Middle Paleolithic Blady Phenomenon to the North. Journal of The Israel Prehistoric Society 40 (2010), 35-61 5. 2007. Tushabramishvili N.,Pleurdeau D., Moncel M.-H., Mgeladze A. Le complexe Djruchula-Koudaro au sud Caucase (Géorgie). Remarques sur les assemblages lithiques pléistocenes de Koudaro I, Tsona et Djruchula . Anthropologie • 45/1 • pp. 1-18 6. Tushabramishvili, D., 1984. Paleolit Gruzii. (Palaeolithic of Georgia). Newsletter of the Georgian State Museum 37B, 5e27

Rehabilitation of adobe buildings. Understanding different materials from Portugal

NASA Astrophysics Data System (ADS)

Costa, Cristiana; Rocha, Fernando; Velosa, Ana

2016-04-01

Earth construction is the oldest building material known, with documented cases of the use of earth bricks since Mesopotamia around 10 000 BC (Heathcote, 1995). The earth construction exists throughout the majority of the world in different cultures, and for some countries, nowadays it continues to be the main process of construction (Vega et al, 2011). Around 30% of the world's population lives in buildings made of earth materials. Earthen construction is an environmentally friendly technique with a social and cultural contribution; this advantage is increased when this type of construction is applied in developing countries where the material costs counterbalance with labour costs, and where other materials and techniques cannot be available (Ciancio et al, 2013). Studies of materials characterization are required in order to understand the composition and specific properties of the earth buildings, their heterogeneity and their degradation mechanisms. Some adobes from different buildings, ages and regions of Portugal were collected in order to characterize them (mineralogically, chemically and physically). It was possible to understand the composition of these materials and their differences. Main minerals are quartz, feldspars, calcite and phyllosilicates (mica and kaolinite). The mechanical behaviour of these materials isn't the best, but it is possible to improve it with some simple and cheap natural additives (kaolinitic soils). The characterization of these materials allows us to understand the differences between the materials from the different regions (controlled by locally available raw materials). Understanding these materials, and their properties, it is possible to formulate new ones for repair, conservation and rehabilitation works. The adobe bricks are an alternative of kiln baked bricks which has several advantages and one of the most important is that these materials are recyclable. Adobes are an excellent option for building rehabilitation, if composition is optimised.

Alternative of raw material’s suppliers using TOPSIS method in chicken slaughterhouse industry

NASA Astrophysics Data System (ADS)

Sari, R. M.; Rizkya, I.; Syahputri, K.; Anizar; Siregar, I.

2018-02-01

Chicken slaughterhouse industry is one of the fastest growing industries that depends on the freshness of raw materials. The raw materials quality arrive at the company depends heavily on the suppliers. Fresh chicken and frozen chicken meat are the main raw materials for this industry. Problems occurred by the suppliers are catering the amount of raw material needs that are not appropriate and also delay during delivery process. This condition causes disruption of the production process in the company. Therefore, it is necessary to determine the best suppliers to supply the main raw materials of fresh and frozen chicken meat on the slaughterhouse chicken industry. This study analyze the supplier’s capability by using TOPSIS method. This method use to find out the best supplier. The TOPSIS method is performed using the principle that chosen alternative must have the shortest distance from the positive solution and furthest from the ideal solution of the geometric point by using the Euclidean distance to determine the relative proximity of the optimum solution alternative. TOPSIS method found the rank of best supplier’s order is supplier A followed by supplier D, supplier B, supplier C, supplier E, supplier F, and supplier G. Based on the rank order obtained from each company, it will assist the company in prioritizing the order to the supplier with the best rank. Total supply from All suppliers are 885,994 kg per month. Based on the results of research, the top five suppliers have been sufficient to meet the needs of the company.

Synthesis and characterization of black ceramic pigments by recycling of two hazardous wastes

NASA Astrophysics Data System (ADS)

Du, Minxing; Du, Yi; Chen, Zhongtao; Li, Zhongfu; Yang, Kai; Lv, Xingjie; Feng, Yibing

2017-09-01

In this study, two different industrial wastes, namely vanadium tailing and leather sludge, were used as less expensive alternative raw materials for the synthesis of black ceramic pigments to be used in commercial glazes. The pigments were based on hematite structure (FexCr1-x)2O3 and prepared by the common solid-state reaction method, under optimal formulation and processing conditions. The synthesized pigments were characterized in typical ceramic glazes and ceramic tile bodies. Optimal color development was achieved when the Fe/Cr mole ratios were 2.0 with 40 wt% content of vanadium tailing at 1200 °C. The coloring properties were similar to those imparted by a commercial black pigment.

Development of an Assessment Method for Building Materials Under Euratom Scope.

PubMed

de With, Govert

2017-11-01

In 2013, the European Commission published its basic safety standards for protection against the dangers arising from exposure to ionizing radiation (Council Directive 2013/59/Euratom)-also known as EU-BSS. As a result, the use of raw materials with potentially elevated activity concentrations such as fly ash, phosphogypsum, and slags will now fall under EU-BSS scope when applied in building materials. In light of this new policy, a variety of tools are available to assess compliance with the 1-mSv y reference level for building materials. At the heart of these tools is a gamma-spectrometric determination of the naturally occurring radionuclides Ra, Th, and K in the material of concern. As a large number of construction products contain a certain amount of the raw material that falls under the scope of the EU regulation, this policy will lead to substantial measurement of building materials that pose little radiation risk. For this reason, a method is developed to enable assessment against the 1-mSv value not on the basis of gamma-spectrometric analysis but rather based on the product's material composition. The proposed method prescribes a maximum permitted content of raw materials with potentially elevated activity concentrations in terms of a weight percentage of the end product, where the raw materials of concern are defined as those listed in Annex XIII of the EU-BSS. The permitted content is a function of the product's surface density. Therefore, a product with a low surface density of up to 25 kg m can consist of nearly 100% raw materials with potentially elevated activity concentrations, and this percentage drops to around 15% for products with a surface density of around 500 kg m. Building materials that comply with these requirements on product composition are exempt from testing, while products that do not comply must perform regular gamma-spectrometric analysis. A full validation and testing of the method is provided. In addition, the paper discusses issues relevant for regulatory implementation.

Biotechnologies for critical raw material recovery from primary and secondary sources: R&D priorities and future perspectives.

PubMed

Hennebel, Tom; Boon, Nico; Maes, Synthia; Lenz, Markus

2015-01-25

Europe is confronted with an increasing supply risk of critical raw materials. These can be defined as materials of which the risks of supply shortage and their impacts on the economy are higher compared to most of other raw materials. Within the framework of the EU Innovation Partnership on raw materials Initiative, a list of 14 critical materials was defined, including some bulk metals, industrial minerals, the platinum group metals and rare earth elements. To tackle the supply risk challenge, innovation is required with respect to sustainable primary mining, substitution of critical metals, and urban mining. In these three categories, biometallurgy can play a crucial role. Indeed, microbe-metal interactions have been successfully applied on full scale to win materials from primary sources, but are not sufficiently explored for metal recovery or recycling. On the one hand, this article gives an overview of the microbial strategies that are currently applied on full scale for biomining; on the other hand it identifies technologies, currently developed in the laboratory, which have a perspective for large scale metal recovery and the needs and challenges on which bio-metallurgical research should focus to achieve this ambitious goal. Copyright © 2013. Published by Elsevier B.V.

Metallurgical characterization of brass objects from the Akko 1 shipwreck, Israel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ashkenazi, D., E-mail: dana@eng.tau.ac.il; Cvikel, D.; Stern, A.

2014-06-01

The Akko 1 shipwreck was a small Egyptian armed vessel or auxiliary naval brig built in the eastern Mediterranean at the beginning of the 19th century. During the underwater excavations, about 230 brass hook-and-eye closures were found, mainly in the bow area. In addition, 158 brass cases were found, mainly between midships and the aft extremity of the shipwreck. Metallurgical non-destructive and destructive characterizations of selected items were performed, including radiographic testing, XRF, lead isotope analysis, optical microscopy, SEM–EDS and microhardness tests. The hook-and-eye closures and the cases were both found to be made of binary copper–zinc alloy (about 30more » wt.% zinc). While the brass cases were made from rolled sheets, hand-made using simple tools, and joined by tin–lead soldering material, the brass hook-and-eye closures were hand-made from drawn brass wire, and manufactured from commercial drawn brass bars by a cold-working process. The lead isotope analyses suggest different provenances of the raw materials used for making the brass objects, thus the different origins of the ores may hint that the brass wire and sheet were imported to the workshops in which the objects were manufactured. - Highlights: • Brass cases and hook-and-eye closures were retrieved from the Akko 1 shipwreck. • Both types of objects were made of binary copper–zinc alloy (about 30 wt.% zinc). • The cases were hand-made from rolled sheets and joined by tin–lead soldering. • Hook-and-eye closures were made from drawn brass wire manufactured by cold-working. • Lead isotope analyses suggest that the origins of the raw material were diverse.« less

Total materials consumption; an estimation methodology and example using lead; a materials flow analysis

USGS Publications Warehouse

Biviano, Marilyn B.; Wagner, Lorie A.; Sullivan, Daniel E.

1999-01-01

Materials consumption estimates, such as apparent consumption of raw materials, can be important indicators of sustainability. Apparent consumption of raw materials does not account for material contained in manufactured products that are imported or exported and may thus under- or over-estimate total consumption of materials in the domestic economy. This report demonstrates a methodology to measure the amount of materials contained in net imports (imports minus exports), using lead as an example. The analysis presents illustrations of differences between apparent and total consumption of lead and distributes these differences into individual lead-consuming sectors.

Epoxy composites based on inexpensive tire waste filler

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ahmetli, Gulnare, E-mail: ahmetli@selcuk.edu.tr; Gungor, Ahmet, E-mail: ahmetli@selcuk.edu.tr; Kocaman, Suheyla, E-mail: ahmetli@selcuk.edu.tr

2014-05-15

Tire waste (TW) was recycled as raw material for the preparation of DGEBA-type epoxy composite materials. The effects of filler amount and epoxy type on the mechanical properties of the composites were investigated. Tensile strength and Young’s modulus of the composites with NPEL were generally higher than composites with NPEF. The appropriate mass level for TW in both type composites was found to be 20 wt%. The equilibrium water sorption of NPEL/TW and NPEF/TW composites for 14-day immersion was determined as 0.10 % and 0.21 %, respectively. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used for characterization ofmore » the composites.« less

Pulpwood production in the Northeast 1968

Treesearch

James T. Bones; Neal P. Kingsley

1969-01-01

This report is based on a canvass of all pulpmills in the Northeast that use wood-either round wood or chips-as a basic raw material for a variety of products. Mills that use woodpulp as a raw material for insulation board and hardboard were also included in the canvass. However, the canvass did not include mills that use waste paper, rags, or pulping material other...

77 FR 5846 - Importer of Controlled Substances; Notice of Registration

Federal Register 2010, 2011, 2012, 2013, 2014

2012-02-06

... import narcotic raw material are not appropriate, in accordance with 72 FR 3417 (2007). DEA has... basic classes of controlled substances: Drug Schedule Phenylacetone (8501) II Opium, raw (9600) II Poppy... to use it as a base material in the bulk manufacture of another controlled substance. No comments or...

Indonesian Politics and Economics (Selected Translations).

DTIC Science & Technology

1961-01-10

the’rise of industries to such a proportion, particularly’in England, that it brought about the " industrial revolution ".. ’ -: Surplus capital...only limited sources of raw materials. The industrial revolution , in iEngland required an inöreased supply of raw materials, and at the sam§ time the

40 CFR 63.2550 - What definitions apply to this subpart?

Code of Federal Regulations, 2012 CFR

2012-07-01

... definition of reconstruction in § 63.2. Consumption means the quantity of all HAP raw materials entering a... the process as well as added as a raw material, consumption includes the quantity generated in the... contain primarily carbon, hydrogen, and oxygen atoms. Organic peroxides means organic compounds containing...

40 CFR 63.2550 - What definitions apply to this subpart?

Code of Federal Regulations, 2014 CFR

2014-07-01

... definition of reconstruction in § 63.2. Consumption means the quantity of all HAP raw materials entering a... the process as well as added as a raw material, consumption includes the quantity generated in the... contain primarily carbon, hydrogen, and oxygen atoms. Organic peroxides means organic compounds containing...

40 CFR 63.2550 - What definitions apply to this subpart?

Code of Federal Regulations, 2011 CFR

2011-07-01

... definition of reconstruction in § 63.2. Consumption means the quantity of all HAP raw materials entering a... the process as well as added as a raw material, consumption includes the quantity generated in the... contain primarily carbon, hydrogen, and oxygen atoms. Organic peroxides means organic compounds containing...

40 CFR 63.2550 - What definitions apply to this subpart?

Code of Federal Regulations, 2013 CFR

2013-07-01

... definition of reconstruction in § 63.2. Consumption means the quantity of all HAP raw materials entering a... the process as well as added as a raw material, consumption includes the quantity generated in the... contain primarily carbon, hydrogen, and oxygen atoms. Organic peroxides means organic compounds containing...

Removal of polycyclic aromatic hydrocarbons from aqueous solution by raw and modified plant residue materials as biosorbents.

PubMed

Xi, Zemin; Chen, Baoliang

2014-04-01

Removal of polycyclic aromatic hydrocarbons (PAHs), e.g., naphthalene, acenaphthene, phenanthrene and pyrene, from aqueous solution by raw and modified plant residues was investigated to develop low cost biosorbents for organic pollutant abatement. Bamboo wood, pine wood, pine needles and pine bark were selected as plant residues, and acid hydrolysis was used as an easily modification method. The raw and modified biosorbents were characterized by elemental analysis, Fourier transform infrared spectroscopy and scanning electron microscopy. The sorption isotherms of PAHs to raw biosorbents were apparently linear, and were dominated by a partitioning process. In comparison, the isotherms of the hydrolyzed biosorbents displayed nonlinearity, which was controlled by partitioning and the specific interaction mechanism. The sorption kinetic curves of PAHs to the raw and modified plant residues fit well with the pseudo second-order kinetics model. The sorption rates were faster for the raw biosorbents than the corresponding hydrolyzed biosorbents, which was attributed to the latter having more condensed domains (i.e., exposed aromatic core). By the consumption of the amorphous cellulose component under acid hydrolysis, the sorption capability of the hydrolyzed biosorbents was notably enhanced, i.e., 6-18 fold for phenanthrene, 6-8 fold for naphthalene and pyrene and 5-8 fold for acenaphthene. The sorption coefficients (Kd) were negatively correlated with the polarity index [(O+N)/C], and positively correlated with the aromaticity of the biosorbents. For a given biosorbent, a positive linear correlation between logKoc and logKow for different PAHs was observed. Interestingly, the linear plots of logKoc-logKow were parallel for different biosorbents. These observations suggest that the raw and modified plant residues have great potential as biosorbents to remove PAHs from wastewater. Copyright © 2014 The Research Centre for Eco-Environmental Sciences, Chinese Academy of Sciences. Published by Elsevier B.V. All rights reserved.

Design of gefitinib-loaded poly (l-lactic acid) microspheres via a supercritical anti-solvent process for dry powder inhalation.

PubMed

Lin, Qing; Liu, Guijin; Zhao, Ziyi; Wei, Dongwei; Pang, Jiafeng; Jiang, Yanbin

2017-10-30

To develop a safer, more stable and potent formulation of gefitinib (GFB), micro-spheres of GFB encapsulated into poly (l-lactic acid) (PLLA) have been prepared by supercritical anti-solvent (SAS) technology in this study. Operating factors were optimized using a selected OA 16 (4 5 ) orthogonal array design, and the properties of the raw material and SAS processed samples were characterized by different methods The results show that the GFB-loaded PLLA particles prepared were spherical, having a smaller and narrower particle size compared with raw GFB. The optimal GFB-loaded PLLA sample was prepared with less aggregation, highest GFB loading (15.82%) and smaller size (D 50 =2.48μm, which meets the size of dry powder inhalers). The results of XRD and DSC indicate that GFB is encapsulated into PLLA matrix in a polymorphic form different from raw GFB. FT-IR results show that the chemical structure of GFB does not change after the SAS process. The results of in vitro release show that the optimal sample release was slower compared with raw GFB particles. Moreover, the results of in vitro anti-cancer trials show that the optimal sample had a higher cytotoxicity than raw GFB. After blending with sieved lactose, the flowability and aerosolization performance of the optimal sample for DPI were improved, with angle of repose, emitted dose and fine particles fractions from 38.4° to 23°, 63.21% to >90%, 23.37% to >30%, respectively. Copyright © 2017 Elsevier B.V. All rights reserved.

75 FR 10460 - Improving Tracing Procedures for E. coli O157:H7 Positive Raw Beef Product

Federal Register 2010, 2011, 2012, 2013, 2014

2010-03-08

... Tracing Procedures for E. coli O157:H7 Positive Raw Beef Product AGENCY: Food Safety and Inspection... Agency procedures for identifying suppliers of source material used to produce raw beef product that FSIS... that raw beef is positive for E. coli O157:H7, and whether the Agency takes the appropriate steps to...

Influence of boiling point range of feedstock on properties of derived mesophase pitch

NASA Astrophysics Data System (ADS)

Yu, Ran; Liu, Dong; Lou, Bin; Chen, Qingtai; Zhang, Yadong; Li, Zhiheng

2018-06-01

The composition of raw material was optimized by vacuum distillation. The carbonization behavior of two kinds of raw material was followed by polarizing microscope, softening point, carbon yield and solubility. Two kinds of mesophase pitch have been monitored by X-ray diffraction (XRD), Fourier transform infrared spectrometer (FTIR), elemental analysis and 1H nuclear magnetic resonance (1H-NMR). The analysis results suggested that raw material B (15wt% of A was distillated out and the residue named B) could form large domain mesophase pitch earlier. The shortened heat treat time favored the retaining of alkyl group in mesophase pitch and reduced the softening point of masophase pitch.

Sensitization to fragrance materials in Indonesian cosmetics.

PubMed

Roesyanto-Mahadi, I D; Geursen-Reitsma, A M; van Joost, T; van den Akker, T W

1990-04-01

2 different groups of patients were patch tested with 2 test series (A and B) containing extracts of fragrance raw materials, traditionally used in Indonesian cosmetics. Series A consisted of diluted extracts of commercially available Indonesian fragrances. Series B consisted of extracts prepared in our department from corresponding indigenous flowers and fruits. Group 1 consisted of 32 patients positive to fragrance-mix, of whom 8 (25%) had positive tests to 1 or more of the different extracts of fragrance raw materials. Reactions were observed to extracts of: Rosa hybrida Hort (7); Canangium odoratum Baill (5); Citrus aurantifolia Swingle (4); Jasminum sambac Ait (2). 6 of the 8 patients had reactions to 1 or more of the components of fragrance-mix: oakmoss (3); cinnamic alcohol (2), isoeugenol (1); cinnamic aldehyde (1) and geraniol (1). Group 2 consisted of 159 patients patch tested on suspicion of contact dermatitis, who were fragrance-mix negative. Only 2 (1.2%) had a positive patch test to the extracts of fragrance raw materials. Specimens taken (as is) from the flowers and citrus fruits (being the basis sources of the fragrance raw materials) were less antigenic. The use of additional test series in Indonesia to detect allergy to traditional cosmetics and perfumes merits further investigation.

77 FR 5846 - Importer of Controlled Substances; Notice of Registration

Federal Register 2010, 2011, 2012, 2013, 2014

2012-02-06

... following basic classes of controlled substances: Drug Schedule Opium, raw (9600) II Poppy Straw Concentrate (9670) II The company plans to import narcotic raw materials for manufacturing and further distribution... substances that are manufactured from opium, raw, and poppy straw concentrate. Comments and requests for...

[Discussion on research and development of new traditional Chinese medicine preparation process based on idea of QbD].

PubMed

Feng, Yi; Hong, Yan-Long; Xian, Jie-Chen; Du, Ruo-Fei; Zhao, Li-Jie; Shen, Lan

2014-09-01

Traditional processes are mostly adopted in traditional Chinese medicine (TCM) preparation production and the quality of products is mostly controlled by terminal. Potential problems of the production in the process are unpredictable and is relied on experience in most cases. Therefore, it is hard to find the key points affecting the preparation process and quality control. A pattern of research and development of traditional Chinese medicine preparation process based on the idea of Quality by Design (QbD) was proposed after introducing the latest research achievement. Basic theories of micromeritics and rheology were used to characterize the physical property of TCM raw material. TCM preparation process was designed in a more scientific and rational way by studying the correlation among enhancing physical property of raw material, preparation process and product quality of preparation. So factors affecting the quality of TCM production would be found out and problems that might occur in the pilot process could be predicted. It would be a foundation for the R&D and production of TCM preparation as well as support for the "process control" of TCMIs gradually realized in the future.

Utilization of composite membrane polyethyleneglycol-polystyrene-cellulose acetate from pineapple leaf fibers in lowering levels of methyl orange batik waste

NASA Astrophysics Data System (ADS)

Delsy, E. V. Y.; Irmanto; Kazanah, F. N.

2017-02-01

Pineapple leaves are agricultural waste from the pineapple that the fibers can be utilized as raw material in cellulose acetate membranes. First, made pineapple leaf fibers into pulp and then converted into cellulose acetate by acetylation process in four stages consisting of activation, acetylation, hydrolysis and purification. Cellulose acetate then used as the raw material to manufacture composite membrane with addition of polystyrene and poly (ethylene glycol) as porogen. Composite membrane is made using phase inversion method with dichloromethane-acetone as a solvent. The result of FTIR analysis (Fourier transform infra-red) showed that the absorption of the carbonyl group (C=O) is at 1643.10 cm-1 and acetyl group (C-O ) at 1227.01 cm-1, with a molecular weight of 8.05 x 104 g/mol and the contents (rate) of acetyl is 37.31%. PS-PEG-CA composite membrane had also been characterized by measuring the water flux values and its application to decrease methyl orange content (level) in batik waste. The results showed that the water flux value is of 25.62 L/(m2.hour), and the decrease percentage of methyl orange content in batik waste is 71.53%.

Reduction of CO2 diffuse emissions from the traditional ceramic industry by the addition of Si-Al raw material.

PubMed

González, I; Barba-Brioso, C; Campos, P; Romero, A; Galán, E

2016-09-15

The fabrication of ceramics can produce the emission of several gases, denominated exhaust gases, and also vapours resulting from firing processes, which usually contain metals and toxic substances affecting the environment and the health of workers. Especially harmful are the diffuse emissions of CO2, fluorine, chlorine and sulphur from the ceramics industry, which, in highly industrialized areas, can suppose an important emission focus of dangerous effects. Concerning CO2, factories that use carbonate-rich raw materials (>30% carbonates) can emit high concentrations of CO2 to the atmosphere. Thus, carbonate reduction or substitution with other raw materials would reduce the emissions. In this contribution, we propose the addition of Al-shales to the carbonated ceramic materials (marls) for CO2 emission reduction, also improving the quality of the products. The employed shales are inexpensive materials of large reserves in SW-Spain. The ceramic bodies prepared with the addition of selected Al-shale to marls in variable proportions resulted in a 40%-65% CO2 emission reduction. In addition, this research underlines at the same time that the use of a low-price raw material can also contribute to obtaining products with higher added value. Copyright © 2016 Elsevier Ltd. All rights reserved.

Quality assurance of herbal raw materials in supply chain: challenges and opportunities.

PubMed

Govindaraghavan, Suresh

2008-01-01

The herbal medicine industry is presently adopting modern scientific tools to substantiate the guarantee of efficacy that, in the past, rested only on anecdotal evidence derived from traditional knowledge systems. This is particularly true for the processes of identification of herbal raw materials adopting modern tools for phytochemical fingerprinting. The successful adaptation of available technologies and practices depends on an understanding of the phytochemical complexity and variability innate in biological material. It challenges the "mainstream medicinal mindset" that "tend(s) to reject …. therapies for which mechanisms of action do not fit within Newtonian, biochemical orientation" (Dumoff, 2003). The herbal medicinal industry is independently evolving its own rigid quality assurance and control systems using Good Manufacturing Practice (GMP) and Good Laboratory Practice (GLP) guidelines, but it faces unique difficulties. These include lack of Good Agricultural and Collection Practice (GACP), lack of transparency in the raw material supply chain so as to preclude the use of unsafe practices, problems in the authentication of herbal raw materials, and a general lack of understanding of the need to reduce phytochemical variability in these materials. This paper explores these difficulties and outlines strategies to overcome them, but these strategies will require coordinated international government regulations to be fully effective.

Chemical and mineralogical characterization of archaeologicam building materials from Seyitomer Hoyuk Kutahya, Turkey.

NASA Astrophysics Data System (ADS)

Bilgen, Nejat; Olgun, Asim

This paper focuses on the spectroscopic and thermal analysis of the archaeological samples of mortar and plaster from middle Bronze Age and Achaemenid period in Seyitömer Höyük. The composition of the samples was investigated using X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy and thermogravimetric thermal analysis (TG-DTA). The results showed that human used different types of raw materials in the preperation of the mortar and plaster in the Middle Bronze Age and Achaemenid period. The material used in middle Bronze Age contains muscovite whereas the material in Achaemenid period contains albite. Although, the chemical composition of the mortar and plaster used in the period were similar, the calcium content of the plaster is relatively higher than the one of the mortar indicating people's awareness of the binding properties of calcite.

Innovative Fly Ash Geopolymer-Epoxy Composites: Preparation, Microstructure and Mechanical Properties.

PubMed

Roviello, Giuseppina; Ricciotti, Laura; Tarallo, Oreste; Ferone, Claudio; Colangelo, Francesco; Roviello, Valentina; Cioffi, Raffaele

2016-06-09

The preparation and characterization of composite materials based on geopolymers obtained from fly ash and epoxy resins are reported for the first time. These materials have been prepared through a synthetic method based on the concurrent reticulation of the organic and inorganic components that allows the formation of hydrogen bonding between the phases, ensuring a very high compatibility between them. These new composites show significantly improved mechanical properties if compared to neat geopolymers with the same composition and comparable performances in respect to analogous geopolymer-based composites obtained starting from more expensive raw material such as metakaolin. The positive combination of an easy synthetic approach with the use of industrial by-products has allowed producing novel low cost aluminosilicate binders that, thanks to their thixotropicity and good adhesion against materials commonly used in building constructions, could be used within the field of sustainable building.

Innovative Fly Ash Geopolymer-Epoxy Composites: Preparation, Microstructure and Mechanical Properties

PubMed Central

Roviello, Giuseppina; Ricciotti, Laura; Tarallo, Oreste; Ferone, Claudio; Colangelo, Francesco; Roviello, Valentina; Cioffi, Raffaele

2016-01-01

The preparation and characterization of composite materials based on geopolymers obtained from fly ash and epoxy resins are reported for the first time. These materials have been prepared through a synthetic method based on the concurrent reticulation of the organic and inorganic components that allows the formation of hydrogen bonding between the phases, ensuring a very high compatibility between them. These new composites show significantly improved mechanical properties if compared to neat geopolymers with the same composition and comparable performances in respect to analogous geopolymer-based composites obtained starting from more expensive raw material such as metakaolin. The positive combination of an easy synthetic approach with the use of industrial by-products has allowed producing novel low cost aluminosilicate binders that, thanks to their thixotropicity and good adhesion against materials commonly used in building constructions, could be used within the field of sustainable building. PMID:28773582

Recycling of the product of thermal inertization of cement-asbestos for various industrial applications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gualtieri, Alessandro F., E-mail: alessandro.gualtieri@unimore.it; Giacobbe, Carlotta; Sardisco, Lorenza

Recycling of secondary raw materials is a priority of waste handling in the countries of the European community. A potentially important secondary raw material is the product of the thermal transformation of cement-asbestos, produced by prolonged annealing at 1200-1300 {sup o}C. The product is chemically comparable to a Mg-rich clinker. Previous work has assured the reliability of the transformation process. The current challenge is to find potential applications as secondary raw material. Recycling of thermally treated asbestos-containing material (named KRY.AS) in traditional ceramics has already been studied with successful results. The results presented here are the outcome of a longmore » termed project started in 2005 and devoted to the recycling of this secondary raw materials in various industrial applications. KRY.AS can be added in medium-high percentages (10-40 wt%) to commercial mixtures for the production of clay bricks, rock-wool glasses for insulation as well as Ca-based frits and glass-ceramics for the production of ceramic tiles. The secondary raw material was also used for the synthesis of two ceramic pigments; a green uvarovite-based pigment [Ca{sub 3}Cr{sub 2}(SiO{sub 4}){sub 3}] and a pink malayaite-based pigment [Ca(Sn,Cr)SiO{sub 5}]. The latter is especially interesting as a substitute for cadmium-based pigments. This work also shows that KRY.AS can replace standard fillers in polypropylene plastics without altering the properties of the final product. For each application, a description and relevant results are presented and discussed.« less

Research and development in pilot plant production of granular NPK fertilizer

NASA Astrophysics Data System (ADS)

Failaka, Muhamad Fariz; Firdausi, Nadia Zahrotul; Chairunnisa, Altway, Ali

2017-05-01

PT Pupuk Kaltim (Pupuk Kaltim) as one of the biggest fertilizer manufacturer in Indonesia, always striving to improve the product quality and achieve the optimal performance while facing the challenges of global competition NPK (Nitrogen, Phosphorus, Potassium) market. In order to continuously improve operations and processes of two units NPK compound plant, Pupuk Kaltim has successfully initiated a new facility which is referred to as a NPK pilot-scale research facility with design capacity of 30 kg/hr. This mini-plant is used to assist in the scale up of new innovations from laboratory research to better understand the effect of using new raw materials and experiment with process changes to improve quality and efficiency. The pilot installation is composed of the following main parts: mixer, screw feeder, granulator, dryer and cooler. The granulator is the equipment where NPK granules is formed by spraying appropriate steam and water onto raw materials in a rotating drum. The rotary dryer and cooler are intended for the drying process where temperature reduction and the final moisture are obtained. As a part of innovations project since 2014, the pilot plant has conducted many of experiments such as trials using Ammonium Sulfate (ZA) as a new raw material, alternative raw materials of Diammonium Phosphate (DAP), Potassium Chloride (KCl) and clay, and using a novel material of fly ash. In addition, the process engineering staff also conduct the trials of raw materials ratio so that an ideal formulation with lower cost can be obtained especially when it is applied in the existing full-scale plant.

Pulpwood - 1976

Treesearch

James T. Bones; David R. Dickson

1977-01-01

This annual report is based on a canvass of all pulpmills in the Northeast that use wood-either roundwood or plant residues-as a basic raw material. Cross-boundary shipments are traced by exchanging information with neighboring experiment stations that conduct similar canvasses. Mills that use pulpwood as a raw material in producing insulation board and hardboard were...

9 CFR 351.14 - Processes to be supervised; extent of examinations.

Code of Federal Regulations, 2011 CFR

2011-01-01

... examinations. 351.14 Section 351.14 Animals and Animal Products FOOD SAFETY AND INSPECTION SERVICE, DEPARTMENT... be at least once a month if the plant consistently handles only raw materials acceptable under § 351... consistently handles some raw materials that are acceptable, and some that are unacceptable, under § 351.3, for...

40 CFR Table N-1 to Subpart N of... - CO2 Emission Factors for Carbonate-Based Raw Materials

Code of Federal Regulations, 2014 CFR

2014-07-01

... Raw Materials Carbonate-basedraw material—mineral CO2 emission factor a Limestone—CaCO3 0.440 Dolomite—CaMg(CO3)2 0.477 Sodium carbonate/soda ash—Na2CO3 0.415 Barium carbonate—BaCO3 0.223 Potassium...

40 CFR Table N-1 to Subpart N of... - CO2 Emission Factors for Carbonate-Based Raw Materials

Code of Federal Regulations, 2012 CFR

2012-07-01

... Raw Materials Carbonate-basedraw material—mineral CO2 emission factor a Limestone—CaCO3 0.440 Dolomite—CaMg(CO3)2 0.477 Sodium carbonate/soda ash—Na2CO3 0.415 Barium carbonate—BaCO3 0.223 Potassium...

40 CFR Table N-1 to Subpart N of... - CO2 Emission Factors for Carbonate-Based Raw Materials

Code of Federal Regulations, 2013 CFR

2013-07-01

... Raw Materials Carbonate-basedraw material—mineral CO2 emission factor a Limestone—CaCO3 0.440 Dolomite—CaMg(CO3)2 0.477 Sodium carbonate/soda ash—Na2CO3 0.415 Barium carbonate—BaCO3 0.223 Potassium...

76 FR 14910 - Small Diameter Graphite Electrodes From the People's Republic of China: Initiation of Anti...

Federal Register 2010, 2011, 2012, 2013, 2014

2011-03-18

... correct grade of petroleum coke mix, and have been baked, formed, carbonized, impregnated, and graphitized... required for the production of SDGE (e.g., raw material handling, mixing, forming, baking, impregnating... production process, demonstrating how raw materials are formed, baked, impregnated (if needed), re-baked...

Characteristics and production of tantalum powders for solid-electrolyte capacitors

NASA Astrophysics Data System (ADS)

Yoon, Jae Sik; Kim, Byung Il

The effects of using K 2TaF 7 as the raw material and sodium as the reducing agent on the characteristics of tantalum powder are investigated. Batch-type metallothermic reduction (BTMR) is used to charge the reactor with the raw material and the reducing agent, and external continuous supply metallothermic reduction (ESMR) is used to supply the raw material and the reducing agent at a constant rate at the temperature of the reduction reaction. In the case of ESMR, the yield increases by several tens of percent because of the uniform reaction between the raw material and the reducing agent. It is possible to obtain a powder of over 99.5% purity. The powder particles obtained with BTMR are relatively large (4-6 μm) and have a coarse lamellar shape, while those prepared via ESMR are of uniform 1-2 μm size with a coral-like shape. Measurements of the electric properties show that the leakage current and the dielectric dissipation are low with higher reliability in ESMR than in BTMR, and the capacitance is 26,000 and 8400 CV for ESMR and in BTMR, respectively.

Fabrication and characterization of high impact hybrid matrix composites from thermoset resin and dyneema-glass fabric reinforcement

NASA Astrophysics Data System (ADS)

Patel, R. H.; Sharma, S.; Pansuriya, T.; Malgani, E. V.; Sevkani, V.

2018-05-01

Hybrid composites have been fabricated by hand lay-up technique with epoxy resin and diethylene tri amine as a hardener for high impact energy absorption with sandwich stacking of different reinforcements of dyneema and glass fabric. High impact grade composites are nowadays gaining a lot of importance in the field of high mechanical load bearing applications, ballistics and bulletproofing. The present work emphases on the fabrication and mechanical properties of the hybrid composites of cut resistant dyneema fabric along with glass fabric reinforced in the thermosetting resin. i.e. epoxy. The prime importance while fabricating such materials have been given to the processing along with selection of the raw materials. High impact resistive materials with low density and henceforth low weight have been manufactured and characterized by IZOD impact tester, UTM, Archimedes density meter and SEM. Throughout the work, satisfactory results have been obtained. Impact resistance was observed to be boosted three times as that of the reference sample of glass fabric and epoxy. The density of the hybrid composite is observed to be 25% as that of the reference sample.

Hematite Core Nanoparticles with Carbon Shell: Potential for Environmentally Friendly Production from Iron Mining Sludge

NASA Astrophysics Data System (ADS)

Stević, Dragana; Mihajlović, Dijana; Kukobat, Radovan; Hattori, Yoshiyuki; Sagisaka, Kento; Kaneko, Katsumi; Atlagić, Suzana Gotovac

2016-08-01

Hematite nanoparticles with amorphous, yet relatively uniform carbon shell, were produced based exclusively on the waste sludge from the iron mine as the raw material. The procedure for acid digestion-based purification of the sludge with the full recovery of acid vapors and the remaining non-toxic rubble is described. Synthesis of the hematite nanoparticles was performed by the arrested precipitation method with cationic surfactant. The particles were thoroughly characterized and the potential of their economical production for the battery industry is indicated.

Radioactive characterization of the main materials involved in the titanium dioxide production process and their environmental radiological impact.

PubMed

Mantero, J; Gazquez, M J; Bolivar, J P; Garcia-Tenorio, R; Vaca, F

2013-06-01

A study about the distribution of several radionuclides from the uranium and the thorium series radionuclides along the production process of a typical NORM industry devoted to the production of titanium dioxide has been performed. With this end the activity concentrations in raw materials, final product, co-products, and wastes of the production process have been determined by both gamma-ray and alpha-particle spectrometry. The main raw material used in the studied process (ilmenite) presents activity concentrations of around 300 Bq kg(-1) for Th-series radionuclides and 100 Bq kg(-1) for the U-series ones. These radionuclides in the industrial process are distributed in the different steps of the production process according mostly to the chemical behaviour of each radioelement, following different routes. As an example, most of the radium remains associated with the un-dissolved material waste, with activity concentrations around 3 kBq kg(-1) of (228)Ra and around 1 kBq kg(-1) of (226)Ra, while the final commercial products (TiO2 pigments and co-products) contain negligible amounts of radioactivity. The obtained results have allowed assessing the possible public radiological impact associated with the use of the products and co-products obtained in this type of industry, as well as the environmental radiological impact associated with the solid residues and liquid generated discharges. Copyright © 2013 Elsevier Ltd. All rights reserved.

Study on novel functional materials carboxymethyl cellulose lithium (CMC-Li) improve high-performance lithium-ion battery.

PubMed

Qiu, Lei; Shao, Ziqiang; Xiang, Pan; Wang, Daxiong; Zhou, Zhenwen; Wang, Feijun; Wang, Wenjun; Wang, Jianquan

2014-09-22

Novel cellulose derivative CMC-Li was synthesized by cotton as raw material. The mechanism of the CMC-Li modified electrode materials by electrospinning was reported. CMC-Li/lithium iron phosphate (LiFePO4, LFP) composite fiber coated with LFP and CMC-Li nanofibers was successfully obtained by electrospinning. Then, CMC-Li/LFP nano-composite fiber was carbonized under nitrogen at a high temperature formed CNF/LFP/Li (CLL) composite nanofibers as cathode material. It can increase the contents of Li+, and improving the diffusion efficiency and specific capacity. The battery with CLL as cathode material retained close to 100% of initial reversible capacity after 200 cycles at 168 mAh g(-1), which was nearly the theoretical specific capacity of LFP. The cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), X-ray diffraction (XRD) and scanning electron microscope (SEM) were characterizing material performance. The batteries have good electrochemical property, outstanding pollution-free, excellent stability. Copyright © 2014 Elsevier Ltd. All rights reserved.

77 FR 64142 - Importer of Controlled Substances, Notice of Application, Noramco, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2012-10-18

... following basic classes of controlled substances: Drug Schedule Phenylacetone (8501) II Opium, raw (9600) II Poppy Straw Concentrate (9670) II Tapentadol (9780) II The company plans to import raw Opium (9600) and... substance. Comments and requests for hearings on applications to import narcotic raw material are not...

76 FR 62447 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2011-10-07

... registration as an importer of the following basic classes of controlled substances: Drug Schedule Opium, raw (9600) II Poppy Straw Concentrate (9670) II The company plans to import narcotic raw materials for... several controlled substances that are manufactured from raw opium, poppy straw, and concentrate of poppy...

77 FR 60143 - Importer of Controlled Substances; Notice of Registration; Cody Laboratories, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2012-10-02

... importer of the following basic classes of controlled substances: Drug Schedule Opium, raw (9600) II Concentrate Poppy Straw (9670) II Tapentadol (9780) II The company plans to import narcotic raw materials for... several controlled substances that are manufactured from opium raw, and poppy straw concentrate. The...

76 FR 17967 - Importer of Controlled Substances; Notice of Registration

Federal Register 2010, 2011, 2012, 2013, 2014

2011-03-31

... basic classes of controlled substances: Drug Schedule Raw Opium (9600) II Concentrate of Poppy Straw (9670) II The company plans to import narcotic raw materials for manufacturing and further distribution... substances that are manufactured from raw opium, poppy straw, and concentrate of poppy straw. No comments or...

75 FR 32506 - Importer of Controlled Substances; Notice of Registration

Federal Register 2010, 2011, 2012, 2013, 2014

2010-06-08

... of controlled substances listed in schedule II: Drug Schedule Raw Opium (9600) II Concentrate of Poppy Straw (9670) II The company plans to import narcotic raw materials for manufacturing and further... substances that are manufactured from raw opium, poppy straw, and concentrate of poppy straw. No comments or...

Effects of mixing and covering with mature compost on gaseous emissions during composting.

PubMed

Luo, Wen Hai; Yuan, Jing; Luo, Yi Ming; Li, Guo Xue; Nghiem, Long D; Price, William E

2014-12-01

This study investigated effects of mature compost on gaseous emissions during composting using pig manure amended with corn stalks. Apart from a control treatment, three treatments were conducted with the addition of 5% (wet weight of raw materials) of mature compost: (a) mixing raw materials with mature compost at the beginning of composting; (b) covering raw materials with mature compost throughout the experimental period; and (c) covering raw materials with mature compost at the start of composting, but incorporating it into composting pile on day 6 of composting. Mature compost used for the last treatment was inoculated with 2% (wet weight) of raw materials of strain M5 (a methanotrophic bacterium) solution. During 30-d of composting, three treatments with the addition of mature compost could reduce CH4 emission by 53-64% and N2O emission by 43-71%. However, covering with mature compost throughout the experimental period increased cumulative NH3 emission by 61%, although it could reduce 34% NH3 emission in the first 3d. Inoculating strain M5 in mature compost covered on the top of composting pile within first 6d enhanced CH4 oxidation, but simultaneously increased N2O emission. In addition, mixing with mature compost could improve compost maturity. Given the operational convenience in practice, covering with mature compost and then incorporating it into composting pile is a suitable approach to mitigate gaseous emissions during composting. Copyright © 2014. Published by Elsevier Ltd.

Determination of Coenzyme Q10 Content in Raw Materials and Dietary Supplements by High-Performance Liquid Chromatography-UV: Collaborative Study

PubMed Central

Lunetta, Steven; Roman, Mark

2008-01-01

An international collaborative study was conducted of a high-performance liquid chromatographic (HPLC)-UV method for the determination of coenzyme Q10 (CoQ10, ubidecarenone) in raw materials and dietary supplements. Ten collaborating laboratories determined the total CoQ10 content in 8 blind duplicate samples. Sample materials included CoQ10 raw material and 4 finished product dietary supplements representing softgels, hardshell gelatin capsules, and chewable wafers. In addition, collaborating laboratories received a negative control and negative control spiked with CoQ10 at low and high levels to determine recovery. Materials were extracted with an acetonitrile–tetrahydrofuran–water mixture. Ferric chloride was added to the test solutions to ensure all CoQ10 was in the oxidized form. The HPLC analyses were performed on a C18 column using UV detection at 275 nm. Repeatability relative standard deviations (RSDr) ranged from 0.94 to 5.05%. Reproducibility relative standard deviations (RSDR) ranged from 3.08 to 17.1%, with HorRat values ranging from 1.26 to 5.17. Recoveries ranged from 74.0 to 115%. Based on these results, the method is recommended for Official First Action for determination of CoQ10 in raw materials and dietary supplement finished products containing CoQ10 at a concentration of >100 mg CoQ10/g test material. PMID:18727527

Determination of coenzyme Q10 content in raw materials and dietary supplements by high-performance liquid chromatography-UV: collaborative study.

PubMed

Lunetta, Steven; Roman, Mark

2008-01-01

An international collaborative study was conducted of a high-performance liquid chromatographic (HPLC)-UV method for the determination of coenzyme Q10 (CoQ10, ubidecarenone) in raw materials and dietary supplements. Ten collaborating laboratories determined the total CoQ10 content in 8 blind duplicate samples. Sample materials included CoQ10 raw material and 4 finished product dietary supplements representing softgels, hardshell gelatin capsules, and chewable wafers. In addition, collaborating laboratories received a negative control and negative control spiked with CoQ10 at low and high levels to determine recovery. Materials were extracted with an acetonitrile-tetrahydrofuran-water mixture. Ferric chloride was added to the test solutions to ensure all CoQ10 was in the oxidized form. The HPLC analyses were performed on a C18 column using UV detection at 275 nm. Repeatability relative standard deviations (RSDr) ranged from 0.94 to 5.05%. Reproducibility relative standard deviations (RSDR) ranged from 3.08 to 17.1%, with HorRat values ranging from 1.26 to 5.17. Recoveries ranged from 74.0 to 115%. Based on these results, the method is recommended for Official First Action for determination of CoQ10 in raw materials and dietary supplement finished products containing CoQ10 at a concentration of >100 mg CoQ10/g test material.

The use of foresight methods in strategic raw materials intelligence - an international review

NASA Astrophysics Data System (ADS)

Konrat Martins, Marco Antonio; Bodo, Balazs; Falck, Eberhard

2017-04-01

Foresight methods are systematic attempts to look into the longer term future of science, society, economy and technology. There is a range of tools and techniques that can be used individually or combined, most commonly classified into qualitative, quantitative or semi-quantitative methods, that follow an exploratory or normative approach. These tools can help to identify the longer term visions, orienting policy formulation and decisions, triggering actions, among other objectives. There is an identified lack of European strategic foresight knowledge in the raw materials domain. Since the European Raw Materials Initiative was launched in 2008, the EU has been attempting to overcome challenges related to the future access of non-energy and non-agricultural raw materials. In this context, the ongoing H2020 project, MICA (Mineral Intelligence Capacity Analysis, Grant Agreement No. 689648), has been launched to answer to stakeholders needs by consolidating relevant data, determining relevant methods and tools, and investigating Raw Materials Intelligence options for European mineral policy development, all tailored to fit under the umbrella of a European Raw Materials Intelligence Capacity Platform (EU-RMICP). As part of the MICA activities, an assessment of best practices and benchmarks of international raw materials foresight case studies has been carried out in order to review how EU and non-EU countries have employed foresight. A pool of 30 case studies has been collected and reviewed internationally, one third of which were selected for detailed assessment. These were classified according to their background and goals, in function of methods employed, and to the purpose of each method in the study: a total of 12 different methods were identified in these studies. For longer time frames, qualitative predictive methods such as Scenario Development have been repeatedly observed for mineral raw materials foresight studies. Substantial variations were observed in terms of use and deployment of the scenarios. Pre-defined global scenarios can be used to explore futures thinking over a given theme - a step in the process - whereas the development of specific scenarios can be the main element of the study. The former was used to consider future strategies at different levels and how different futures influence the sector, whilst the latter was preferably used as means of assessment of sector capabilities and the current readiness for future challenges. Other methods such as SWOT, STEEP (Social, Technological, Economical, Environmental and Political scanning) and Brainstorming can be observed supporting the Scenarios, helping to provide either input for its development or post-processing its outcomes towards overall objectives. The volatility of the mineral raw materials sector presents a natural inclination towards more explorative and creativity-based methods. Such methods can address the necessity of understanding how different factors may play out in the future, where critical uncertainties can dictate a range of possible futures. Therefore, having a solid backdrop for alternative paths is extremely useful for policy and decision-makers to propose actions and respond in a timely manner to the future challenges of the sector.

Green biorefinery - Industrial implementation.

PubMed

Kamm, B; Schönicke, P; Hille, Ch

2016-04-15

Oil refineries currently generate a multitude of products for almost every sphere of life at very high efficiency. However, fossil raw materials are just available in limited quantities. The development of comparable BIOREFINERIES is necessary to make a variety of competitive biological products regarding their equivalent products based on fossil raw materials. The product range of a biorefinery comprises products that can be manufactured on the basis of crude oil, as well as such products that cannot be produced on the basis of crude oil (Kamm, Gruber, & Kamm, 2011). GREEN BIOREFINERIES [GBR's] are complex systems of sustainable, environment- and resource-friendly technologies for a comprehensive material and energy use or recovery of renewable raw materials in form of green and waste biomasses from a sustainable land use as target (Kamm et al., 2009; Digman, Runge, Shinners, & Hatfield, 2013). Copyright © 2015. Published by Elsevier Ltd.

Vinasses: characterization and treatments.

PubMed

España-Gamboa, Elda; Mijangos-Cortes, Javier; Barahona-Perez, Luis; Dominguez-Maldonado, Jorge; Hernández-Zarate, G; Alzate-Gaviria, Liliana

2011-12-01

The final products of the ethanol industry are alcoholic beverages, industrial ethanol and biofuels. They are produced by the same production process, which includes fermentation and distillation of raw materials which come from plant biomass. At the end of the distillation process a waste effluent is obtained called vinasse or stillage. The direct disposal of stillages on land or in groundwater (rivers, streams or lakes), or even for the direct irrigation of crops, pollutes the environment due to their high organic contents, dissolved solids and many other compounds which are toxic or could be contaminants under certain environmental conditions. This work reviews the characterization of vinasses from different feedstock sources and the main treatments for conditioning the soluble solids of vinasses before their disposal.

The utilization of nonterrestrial materials. [resources for solar power satellite construction

NASA Technical Reports Server (NTRS)

1981-01-01

The development of research and technology programs on the user of nonterrestrial materials for space applications was considered with emphasis on the space power satellite system as a model of large space systems for which the use of nonterrestrial materials may be economically viable. Sample topics discussed include the mining of raw materials and the conversion of raw materials into useful products. These topics were considered against a background of the comparative costs of using terrestrial materials. Exploratory activities involved in the preparation of a nonterrestrial materials utilization program, and the human factors involved were also addressed. Several recommendations from the workshop are now incorporated in NASA activities.

Design of Chitosan-Grafted Carbon Nanotubes: Evaluation of How the –OH Functional Group Affects Cs+ Adsorption

PubMed Central

Yang, Shubin; Shao, Dadong; Wang, Xiangke; Hou, Guangshun; Nagatsu, Masaaki; Tan, Xiaoli; Ren, Xuemei; Yu, Jitao

2015-01-01

In order to explore the effect of –OH functional groups in Cs+ adsorption, we herein used the low temperature plasma-induced grafting method to graft chitosan onto carbon nanotubes (denoted as CTS-g-CNTs), as raw-CNTs have few functional groups and chitosan has a large number of –OH functional groups. The synthesized CTS-g-CNT composites were characterized using different techniques. The effect of –OH functional groups in the Cs+ adsorption process was evaluated by comparison of the adsorption properties of raw-CNTs with and without grafting chitosan. The variation of environmental conditions such as pH and contact time was investigated. A comparison of contaminated seawater and simulated groundwater was also evaluated. The results indicated that: (1) the adsorption of Cs+ ions was strongly dependent on pH and the competitive cations; (2) for CNT-based material, the –OH functional groups have a positive effect on Cs+ removal; (3) simulated contaminated groundwater can be used to model contaminated seawater to evaluate the adsorption property of CNTs-based material. These results showed direct observational evidence on the effect of –OH functional groups for Cs+ adsorption. Our findings are important in providing future directions to design and to choose effective material to remedy the removal of radioactive cesium from contaminated groundwater and seawater, crucial for public health and the human social environment. PMID:26006711

Applications of a synergic analytical strategy to figure out technologies in medieval glazed pottery with "negative decoration" from Italy

NASA Astrophysics Data System (ADS)

Giannossa, Lorena Carla; Acquaviva, Marianna; Laganara, Caterina; Laviano, Rocco; Mangone, Annarosa

2014-09-01

Glazed pottery with "negative decoration" samples, dating back to the twelfth to thirteenth century ad and coming from three sites along the Adriatic coast, Siponto, Egnatia and Trani (Southern Italy) were characterized from physical-chemical, mineralogical and morphological points of view. Optical microscopy, scanning electron microscopy with energy dispersive X-ray spectroscopy, inductively coupled plasma-mass spectroscopy, X-ray diffraction and micro-Raman spectroscopy investigations were carried out on ceramic bodies, pigments and glazes of the fragments. We aimed to outline the technological features, define the nature of decorations and coatings—glazes and engobes—and look for clues to hypothesize provenance. Results obtained show clear differences in raw materials and production technology between the impressed ceramic of Islamic tradition and the incised one of Byzantine tradition. Regarding the latter, evidences of a non-local origin can be found in the compositional diversity of raw materials used for the ceramic bodies of fragments decorated with spiral and pseudo-kufic motifs, which stressed the use of clays so far not recorded in Apulia. At the same time, at least in the case of Siponto, the compositional similarity of both ceramic bodies and materials used under the glaze for impressed ceramic and painted polychrome ceramics (RMR and protomaiolica), more likely local production, could suggest that both were produced in the same workshops.

Environmentally-Friendly Dense and Porous Geopolymers Using Fly Ash and Rice Husk Ash as Raw Materials

PubMed Central

Ziegler, Daniele; Formia, Alessandra; Tulliani, Jean-Marc; Palmero, Paola

2016-01-01

This paper assesses the feasibility of two industrial wastes, fly ash (FA) and rice husk ash (RHA), as raw materials for the production of geopolymeric pastes. Three typologies of samples were thus produced: (i) halloysite activated with potassium hydroxide and nanosilica, used as the reference sample (HL-S); (ii) halloysite activated with rice husk ash dissolved into KOH solution (HL-R); (iii) FA activated with the alkaline solution realized with the rice husk ash (FA-R). Dense and porous samples were produced and characterized in terms of mechanical properties and environmental impact. The flexural and compressive strength of HL-R reached about 9 and 43 MPa, respectively. On the contrary, the compressive strength of FA-R is significantly lower than the HL-R one, in spite of a comparable flexural strength being reached. However, when porous samples are concerned, FA-R shows comparable or even higher strength than HL-R. Thus, the current results show that RHA is a valuable alternative to silica nanopowder to prepare the activator solution, to be used either with calcined clay and fly ash feedstock materials. Finally, a preliminary evaluation of the global warming potential (GWP) was performed for the three investigated formulations. With the mix containing FA and RHA-based silica solution, a reduction of about 90% of GWP was achieved with respect to the values obtained for the reference formulation. PMID:28773587

Chemical modification of the cocoa shell surface using diazonium salts.

PubMed

Fioresi, Flavia; Vieillard, Julien; Bargougui, Radhouane; Bouazizi, Nabil; Fotsing, Patrick Nkuigue; Woumfo, Emmanuel Djoufac; Brun, Nicolas; Mofaddel, Nadine; Le Derf, Franck

2017-05-15

The outer portion of the cocoa bean, also known as cocoa husk or cocoa shell (CS), is an agrowaste material from the cocoa industry. Even though raw CS is used as food additive, garden mulch, and soil conditioner or even burnt for fuel, this biomass material has hardly ever been investigated for further modification. This article proposes a strategy of chemical modification of cocoa shell to add value to this natural material. The study investigates the grafting of aryl diazonium salt on cocoa shell. Different diazonium salts were grafted on the shell surface and characterized by infrared spectroscopy and scanning electronic microscopy imaging. Strategies were developed to demonstrate the spontaneous grafting of aryl diazonium salt on cocoa shell and to elucidate that lignin is mainly involved in immobilizing the phenyl layer. Copyright © 2017 Elsevier Inc. All rights reserved.

Manufacture of mold of polymeric composite water pipe reinforced charcoal

NASA Astrophysics Data System (ADS)

Zulfikar; Misdawati; Idris, M.; Nasution, F. K.; Harahap, U. N.; Simanjuntak, R. K.; Jufrizal; Pranoto, S.

2018-03-01

In general, household wastewater pipelines currently use thermoplastic pipes of Polyvinyl Chloride (PVC). This material is known to be not high heat resistant, contains hazardous chemicals (toxins), relatively inhospitable, and relatively more expensive. Therefore, researchers make innovations utilizing natural materials in the form of wood charcoal as the basic material of making the water pipe. Making this pipe requires a simple mold design that can be worked in the scale of household and intermediate industries. This research aims to produce water pipe mold with simple design, easy to do, and making time relatively short. Some considerations for molding materials are weight of mold, ease of raw material, strong, sturdy, and able to cast. Pipe molds are grouped into 4 (four) main parts, including: outer diameter pipe molding, pipe inside diameter, pipe holder, and pipe alignment control. Some materials have been tested as raw materials for outer diameter of pipes, such as wood, iron / steel, cement, and thermoset. The best results are obtained on thermoset material, where the process of disassembling is easier and the resulting mold weight is relatively lighter. For the inside diameter of the pipe is used stainless steel, because in addition to be resistant to chemical processes that occur, in this part of the mold must hold the press load due to shrinkage of raw materials of the pipe during the process of hardening (polymerization). Therefore, it needs high pressure resistant material and does not blend with the raw material of the pipe. The base of the mold is made of stainless steel material because it must be resistant to corrosion due to chemical processes. As for the adjustment of the pipe is made of ST 37 carbon steel, because its function is only as a regulator of the alignment of the pipe structure.

North Carolina Forest Resources and Industries

Treesearch

J.W. Cruikshank

1944-01-01

Dependable information on the supply of all raw materials is vital to the conduct of the war and to the success of current and future efforts at post-war planning. This economic survey of our forests which are an integral part of the Nation's reservoir of raw material is essential to a complete understanding of resource potentialities and of the industries...

Preparation of wood for energy use

Treesearch

Donald L. Sirois; Bryce J. Stokes

1985-01-01

This paper presents an overview & current sources and forms of raw materials for wood energy use and the types of machines available to convert them to the desired form for boiler fuel. Both the fuel source or raw material, and the combustion furnace will dictate the requirements for the processing system. Because of the wide range of processing equipment...

The pallet industry: a changing hardwood market

Treesearch

G.P. Dempsey; D.G. Martens

1991-01-01

From its inception during World War II, the wooden pallet industry has grown to become the Nation's largest industrial consumer of hardwood lumber products. Since most of the raw material in wooden pallets is lower grade lumber, the pallet industry's growth, efficiency, and changing raw material inputs must be of concern to the grade hardwood lumber industry...

Acoustic assessment of wood quality of raw forest materials : a path to increased profitability

Treesearch

Xiping Wang; Peter Carter; Robert J. Ross; Brian K. Brashaw

2007-01-01

Assessment of the quality of raw wood materials has become a crucial issue in the operational value chain as forestry and the wood processing industry are increasingly under economic pressure to maximize extracted value. A significant effort has been devoted toward developing robust nondestructive evaluation (NDE) technologies capable of predicting the intrinsic wood...

Pulpwood production in the Northeast - 1974

Treesearch

James T. Bones; David R. Dickson

1976-01-01

This annual report is based on a canvass of all pulpmills in the Northeast that use wood-either roundwood or plant residues-as a basic raw material for a variety of products. Cross-boundary shipments were traced by exchanging information with neighboring experiment stations that conduct similar canvasses. Mills that use pulpwood as a raw material in producing...

Pulpwood production in the Northeast - 1975

Treesearch

James T. Bones; David R. Dickson

1976-01-01

This annual report is based on a canvass of all pulpmills in the Northeast that use wood-either roundwood or plant residues-as a basic raw material for a variety of products. Cross-boundary shipments are traced by exchanging information with neighboring experiment stations that conduct similar canvasses. Mills that use pulpwood as a raw material in producing insulation...

Metabolic Noise, Vestigial Metabolites or the Raw Material of Ecological Adaptation? Opportunitistic Enzymes, Catalytic Promiscuity and the Evolution of Chemodiversity in Nature (2010 JGI User Meeting)

ScienceCinema

Noel, Joseph

2018-04-26

Joseph Noel from the Salk Institute on "Metabolic Noise, Vestigial Metabolites or the Raw Material of Ecological Adaptation? Enzymes, Catalytic Promiscuity and the Evolution of Chemodiversity in Nature" on March 26, 2010 at the 5th Annual DOE JGI User Meeting.

Navy Fact File 1984

DTIC Science & Technology

1984-10-01

Textile Fibers/Products Foods , Feeds, Beverages Industrial Supplies Value of Goods Exported ($ billions) 1958 1968 1978 $18.1 billion...character of its government, the soundness of its economy, its industrial efficiency, the development of its internal communications, the quality...decades the United States produced more raw materials than its growing industrial complex could consume. From a raw-materials-surplus-nation we

Lagrange multiplier for perishable inventory model considering warehouse capacity planning

NASA Astrophysics Data System (ADS)

Amran, Tiena Gustina; Fatima, Zenny

2017-06-01

This paper presented Lagrange Muktiplier approach for solving perishable raw material inventory planning considering warehouse capacity. A food company faced an issue of managing perishable raw materials and marinades which have limited shelf life. Another constraint to be considered was the capacity of the warehouse. Therefore, an inventory model considering shelf life and raw material warehouse capacity are needed in order to minimize the company's inventory cost. The inventory model implemented in this study was the adapted economic order quantity (EOQ) model which is optimized using Lagrange multiplier. The model and solution approach were applied to solve a case industry in a food manufacturer. The result showed that the total inventory cost decreased 2.42% after applying the proposed approach.

Carbon source in the future chemical industries

NASA Astrophysics Data System (ADS)

Hofmann, Peter; Heinrich Krauch, Carl

1982-11-01

Rising crude oil prices favour the exploitation of hitherto unutilised energy carriers and the realisation of new technologies in all sectors where carbon is used. These changed economic constraints necessitate both savings in conventional petrochemistry and a change to oil-independent carbon sources in the chemical industry. While, in coal chemistry, the synthesis and process principles of petrochemistry — fragmentation of the raw material and subsequent buildup of molecular structures — can be maintained, the raw material structure largely remains unchanged in the chemistry of renewable raw materials. This lecture is to demonstrate the structural as well as the technological and energy criteria of the chemistry of alternative carbon sources, to forecast the chances of commercial realization and to discuss some promising fields of research and development.

Synthesis and characterization of carbon nanotube from coconut shells activated carbon

NASA Astrophysics Data System (ADS)

Melati, A.; Hidayati, E.

2016-03-01

Carbon nanotubes (CNTs) have been explored in almost every single cancer treatment modality, including drug delivery, lymphatic targeted chemotherapy, photodynamic therapy, and gene therapy. They are considered as one of the most promising nanomaterial with the capability of both detecting the cancerous cells and delivering drugs or small therapeutic molecules to the cells. CNTs have unique physical and chemical properties such as high aspect ratio, ultralight weight, high mechanical strength, high electrical conductivity, and high thermal conductivity. Coconut Shell was researched as active carbon source on 500 - 600°C. These activated carbon was synthesized becomes carbon nanotube and have been proposed as a promising tool for detecting the expression of indicative biological molecules at early stage of cancer. Clinically, biomarkers cancer can be detected by CNT Biosensor. We are using pyrolysis methods combined with CVD process or Wet Chemical Process on 600°C. Our team has successfully obtained high purity, and aligned MWCNT (Multi Wall Nanotube) bundles on synthesis CNT based on coconut shells raw materials. CNTs can be used to cross the mammalian cell membrane by endocytosis or other mechanisms. SEM characterization of these materials have 179 nm bundles on phase 83° and their materials compound known by using FTIR characterization.

The cellulose resource matrix.

PubMed

Keijsers, Edwin R P; Yılmaz, Gülden; van Dam, Jan E G

2013-03-01

The emerging biobased economy is causing shifts from mineral fossil oil based resources towards renewable resources. Because of market mechanisms, current and new industries utilising renewable commodities, will attempt to secure their supply of resources. Cellulose is among these commodities, where large scale competition can be expected and already is observed for the traditional industries such as the paper industry. Cellulose and lignocellulosic raw materials (like wood and non-wood fibre crops) are being utilised in many industrial sectors. Due to the initiated transition towards biobased economy, these raw materials are intensively investigated also for new applications such as 2nd generation biofuels and 'green' chemicals and materials production (Clark, 2007; Lange, 2007; Petrus & Noordermeer, 2006; Ragauskas et al., 2006; Regalbuto, 2009). As lignocellulosic raw materials are available in variable quantities and qualities, unnecessary competition can be avoided via the choice of suitable raw materials for a target application. For example, utilisation of cellulose as carbohydrate source for ethanol production (Kabir Kazi et al., 2010) avoids the discussed competition with easier digestible carbohydrates (sugars, starch) deprived from the food supply chain. Also for cellulose use as a biopolymer several different competing markets can be distinguished. It is clear that these applications and markets will be influenced by large volume shifts. The world will have to reckon with the increase of competition and feedstock shortage (land use/biodiversity) (van Dam, de Klerk-Engels, Struik, & Rabbinge, 2005). It is of interest - in the context of sustainable development of the bioeconomy - to categorize the already available and emerging lignocellulosic resources in a matrix structure. When composing such "cellulose resource matrix" attention should be given to the quality aspects as well as to the available quantities and practical possibilities of processing the feedstock and the performance in the end-application. The cellulose resource matrix should become a practical tool for stakeholders to make choices regarding raw materials, process or market. Although there is a vast amount of scientific and economic information available on cellulose and lignocellulosic resources, the accessibility for the interested layman or entrepreneur is very difficult and the relevance of the numerous details in the larger context is limited. Translation of science to practical accessible information with modern data management and data integration tools is a challenge. Therefore, a detailed matrix structure was composed in which the different elements or entries of the matrix were identified and a tentative rough set up was made. The inventory includes current commodities and new cellulose containing and raw materials as well as exotic sources and specialties. Important chemical and physical properties of the different raw materials were identified for the use in processes and products. When available, the market data such as price and availability were recorded. Established and innovative cellulose extraction and refining processes were reviewed. The demands on the raw material for suitable processing were collected. Processing parameters known to affect the cellulose properties were listed. Current and expected emerging markets were surveyed as well as their different demands on cellulose raw materials and processes. The setting up of the cellulose matrix as a practical tool requires two steps. Firstly, the reduction of the needed data by clustering of the characteristics of raw materials, processes and markets and secondly, the building of a database that can provide the answers to the questions from stakeholders with an indicative character. This paper describes the steps taken to achieve the defined clusters of most relevant and characteristic properties. These data can be expanded where required. More detailed specification can be obtained from the background literature and handbooks. Where gaps of information are identified, the research questions can be defined that will require further investigation. Copyright © 2012 Elsevier Ltd. All rights reserved.

Characterization of the indigenous microflora in raw and pasteurized buffalo milk during storage at refrigeration temperature by high-throughput sequencing

USDA-ARS?s Scientific Manuscript database

The effect of refrigeration on bacterial communities within raw and pasteurized buffalo milk was studied using high-throughput sequencing. High quality samples of raw buffalo milk were obtained from five dairy farms in the Guangxi province of China. A sample of each milk was pasteurized, and both r...

Influence of Oxidation in Starting Material Sn on Electric Transport Properties of SnSe Single Crystals

NASA Astrophysics Data System (ADS)

Yamashita, Aichi; Ogiso, Osamu; Matsumoto, Ryo; Tanaka, Masashi; Hara, Hiroshi; Tanaka, Hiromi; Takeya, Hiroyuki; Lee, Chul-Ho; Takano, Yoshihiko

2018-06-01

We found that the electronic transport property of SnSe single crystals was sensitively affected by oxidation in raw Sn. Semiconducting SnSe single crystals were obtained by using Sn of grain form as a starting material while powder Sn resulted in metallic SnSe. X-ray photoelectron spectroscopy analysis revealed that the surfaces of raw Sn were oxidized, which volume fraction is lower in grain Sn. This indicates that the amount of oxygen in raw Sn is the key factor for the electronic transport property of SnSe.

Synthesis and characterization of a BaGdF5:Tb glass ceramic as a nanocomposite scintillator for x-ray imaging.

PubMed

Lee, Gyuhyon; Struebing, Christian; Wagner, Brent; Summers, Christopher; Ding, Yong; Bryant, Alex; Thadhani, Naresh; Shedlock, Daniel; Star-Lack, Josh; Kang, Zhitao

2016-05-20

Transparent glass ceramics with embedded light-emitting nanocrystals show great potential as low-cost nanocomposite scintillators in comparison to single crystal and transparent ceramic scintillators. In this study, cubic structure BaGdF5:Tb nanocrystals embedded in an aluminosilicate glass matrix are reported for potential high performance MeV imaging applications. Scintillator samples with systematically varied compositions were prepared by a simple conventional melt-quenching method followed by annealing. Optical, structural and scintillation properties were characterized to guide the design and optimization of selected material systems, aiming at the development of a system with higher crystal volume and larger crystal size for improved luminosity. It is observed that enhanced scintillation performance was achieved by tuning the glass matrix composition and using GdF3 in the raw materials, which served as a nucleation agent. A 26% improvement in light output was observed from a BaGdF5:Tb glass ceramic with addition of GdF3.

Thermal Curing Process Monitoring of the Composite Material Using the FBG sensor

NASA Astrophysics Data System (ADS)

Zhang, Youhong; Chang, Xinlong; Zhang, Xiaojun; He, Xiangyong

2018-03-01

The raw composite material will suffer complex chemical and morphological changes during the thermal curing process, and it is difficult to monitor the curing process and curing effect. In this paper, the FBG sensor was embedded in the raw composite material to monitor the whole curing process. The experiment results showed that the FBG sensor can monitor the resin transformation and residual deformation of the composite material, and the FBG sensor can be applied to monitor the thermal curing process of the composite structure.

Utilization of Shrimp Skin Waste (Sea Lobster) As Raw Material for the Membrane Filtration

NASA Astrophysics Data System (ADS)

Nyoman Rupiasih, Ni; Sumadiyasa, Made; Suyanto, Hery; Windari, Putri

2017-05-01

In view of the increasing littering of the sea banks by shells of crustaceans, a study was carried out to investigate the extraction and characterization of chitosan from skin waste of sea lobster i.e. ‘Bamboo Lobster’ (Panulirus versicolor). Chitosan was extracted using conventional methods such as pretreatment, demineralization, deprotienization, and deacetylation. The result showed that the degree of deacetylation of chitosan obtained is 70.02%. The FTIR spectra of the chitosan gave a characteristic of -NH2 band at 3447 cm-1 and carbonyl group band at 1655 cm-1. This chitosan has been used to prepare membrane. The chitosan membrane 2% has been prepared using phase inversion method with precipitation by solvent evaporation. The membranes were characterized by FTIR spectrophotometer, Nova 1200e using BJH method, and filtration method. The results show that thickness of the membrane is about 134 μm. The FTIR spectra show that functional groups present in the membrane are -NH, -CH, C=O, and -OH. Using BJH method obtained that the pore diameter is 3.382 nm with pore density is 8.95 x 105 pores/m3. By filtration method obtained that pure water flux (PWF) of the membrane are 386.662 and 489.627 1/m2.h at pressure 80-85 kPa and 90-100 kPa, respectively. These results show that skin waste of sea lobster was discovered as a raw material to prepare chitosan membrane. The membrane obtained is belonged to mesoporous group which may use in microfiltration process.

Analysis of waste coal from the enterprises of Kemerovo region as raw materials for production of ceramic materials

NASA Astrophysics Data System (ADS)

Stolboushkin, A. Yu; Akst, D. V.; Fomina, O. A.; Ivanov, A. I.; Syromyasov, V. A.

2017-09-01

The analysis of waste coal from mining enterprises of Kemerovo region as raw materials for production of building ceramics is given. The results of studies of material, chemical and mineralogical compositions of waste coal from Abashevskaya processing plant (Novokuznetsk) are presented. It was established that the chemical composition of waste coal refers to aluminosilicate raw materials with a high content of alumina and coloring oxides, the residual carbon content in the wastes is 12-25 %. According to the granulometric composition the waste coal is basically a sandy-dusty fraction with a small amount of clay particles (1-3 %). Additional grinding of coal waste and the introduction of a clay additive in an amount of up to 30 % are recommended. The results of the study of the mineral composition of waste coal are presented. Clay minerals are represented in the descending order by hydromuscovite, montmorillonite and kaolinite, minerals-impurities consist of quartz, feldspar fine-dispersed carbonates. The results of the investigation of ceramic-technological properties of waste coal, which belong to the group of moderately plastic low-melting raw materials, are given. As a result of a comprehensive study it was been established that with chemical, granulometric and mineralogical compositions waste coal with the reduced residual carbon can be used in the production of ceramic bricks.

Optimization of conditions for isolation of high quality chitin from shrimp processing raw byproducts using response surface methodology and its characterization.

PubMed

Nidheesh, T; Suresh, P V

2015-06-01

Chitin is one of the most abundant bioactive biopolymer on earth. It is commercially extracted from seafood processing crustacean shell byproducts by harsh thermochemical treatments. The extraction conditions, the source and pretreatment of raw material significantly affect its quality and bioactivity. In this investigation response surface methodology (RSM) has been applied to optimize and evaluate the interaction of variables for extraction of high quality chitin from shrimp processing raw byproducts. Variables such as, concentration of HCl (%, v/v) 4.5 (for wet) and 4.9 (for dry), reaction time 3 h, solid liquid ratio of HCl (w/v) 1:5.5 (for wet) and 1:7.9 (for dry) with two treatments achieved >98 % demineralization of shrimp byproduct. Variables such as, concentration of NaOH 3.6 % (w/v), reaction time 2.5 h, temperature 69.0 ± 1 °C, solid liquid ratio of NaOH 7.4 (w/v) and two treatments accomplished >98 % deproteinization of demineralized byproducts. Significant (p ≤ 0.05-0.001) interactive effects were observed between different variables. Chitin obtained in these conditions had residual content (%, w/w) of ash <0.4 and protein <0.8 and the degree of N-acetylation was >93 % with purity of >98 %. In conclusion, the optimized conditions by RSM can be applied for large scale preparation of high quality chitin from raw shrimp byproduct.

Application of Microwave Energy at Treatment of Asbestos Cement (Eternit)

NASA Astrophysics Data System (ADS)

Znamenáčková, Ingrid; Dolinská, Silvia; Lovás, Michal; Hredzák, Slavomír; Matik, Marek; Tomčová, Jana; Čablík, Vladimír

2016-10-01

Asbestos is the common name applied to a group of natural, fibrous silicate minerals, which were once one of the most popular raw materials to be used in building materials. Asbestos was mainly used for the production of assortment asbestos cement products. Today it is generally known that asbestos belongs to the group of hazardous materials and shows carcinogenic activity. It is therefore advisable to attempt to dispose of asbestos minerals in asbestos-containing materials and to convert them into a harmless material. One of methods may be microwave thermal decomposition of asbestos minerals. The research was used for old etemit roof ceiling. X-ray analysis indicated the presence of undesirable chrysotile. Its thermal destruction was carried out in a microwave oven in the power of 2500 W. In case the heating time was 15 min, X-ray analysis was confirmed chrysotile change into harmless minerals. Thermal analysis was used for characterization and the thermal behaviour of the asbestos cement sample.

Agricultural wastes as a resource of raw materials for developing low-dielectric glass-ceramics

PubMed Central

Danewalia, Satwinder Singh; Sharma, Gaurav; Thakur, Samita; Singh, K.

2016-01-01

Agricultural waste ashes are used as resource materials to synthesize new glass and glass-ceramics. The as-prepared materials are characterized using various techniques for their structural and dielectric properties to check their suitability in microelectronic applications. Sugarcane leaves ash exhibits higher content of alkali metal oxides than rice husk ash, which reduces the melting point of the components due to eutectic reactions. The addition of sugarcane leaves ash in rice husk ash promotes the glass formation. Additionally, it prevents the cristobalite phase formation. These materials are inherently porous, which is responsible for low dielectric permittivity i.e. 9 to 40. The presence of less ordered augite phase enhances the dielectric permittivity as compared to cristobalite and tridymite phases. The present glass-ceramics exhibit lower losses than similar materials synthesized using conventional minerals. The dielectric permittivity is independent to a wide range of temperature and frequency. The glass-ceramics developed with adequately devitrified phases can be used in microelectronic devices and other dielectric applications. PMID:27087123

7 CFR 58.430 - Milk.

Code of Federal Regulations, 2010 CFR

2010-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58... milk used. Such dairy products shall have originated from raw milk meeting the same requirements as...

7 CFR 58.430 - Milk.

Code of Federal Regulations, 2011 CFR

2011-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Material § 58... milk used. Such dairy products shall have originated from raw milk meeting the same requirements as...

Characterization studies for the reuse of phosphogypsum as a raw material in the civil construction industry of Brazil

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jacomino, V.M.; Canut, M.; Magalhaes Gomes, A.

NORM stands for 'naturally occurring radioactive material', which is a material that naturally contains one or more radionuclides, mainly, uranium, thorium and potassium-40, and their radioactive decay products, such as radium and radon. An example of this material is the Phosphogypsum (PG), which results from the processing of phosphate ore into phosphoric acid for fertilizer production. In order to support regulation of the reuse of phosphogypsum as a raw material of the Brazilian civil construction industry, a characterization study was performed. The physical and chemical properties of PG and natural gypsum were determinate by evaluating the results of thermal (DTAmore » and TG), X-ray fluorescence (XRF), X-ray diffraction (XRD) and laser granulometric analyses. The radioactivity concentration of each sample was measured by gamma spectrometry analyses. The results of thermal analyses demonstrated that phosphogypsum must be treated (initially heated in an electrical oven at 60 deg. C for 24 hours, then sieved and heated again at 160 deg. C for one hour) to obtain the same mineralogical properties of the gypsum used in the civil construction industry. The X- ray fluorescence analysis showed that PG and natural gypsum are similar with both being composed mainly of S, O, Ca, P and small quantities of trace elements (Ce, Ti, La, Sr, Zr, and Pr). The main crystalline compounds found in PG samples were gypsita (CaSO{sub 4}.2H{sub 2}O) and in natural gypsum were bassanite (CaSO{sub 4}.0.5H{sub 2}O). The concentration of Ra-226, Ra-228 and Pb-210 present in PG samples was 467 Bq/kg, 224 Bq/kg and 395 Bq/kg, respectively. The levels of radioactivity in natural gypsum samples were much lower (around 3 Bq/kg). The same behavior was observed for the uranium and thorium content. The results of all the analyses showed that phosphogypsum can be a viable substitute for gypsum, after certain, beneficial processes. (authors)« less

Non-Formal Education in Ethiopia: The Modern Sector. Program of Studies in Non-Formal Education. Discussion Papers. No. 6.

ERIC Educational Resources Information Center

Niehoff, Richard O.; Wilder, Bernard

Nonformal education programs operating in the modern sector in Ethiopia are described in a perspective relevant to the Ethiopian context. The modern sector is defined as those activities concerned with the manufacture of goods, extraction of raw materials, the processing of raw materials, the provision of services, and the creation and maintenance…

40 CFR 418.52 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2012 CFR

2012-07-01

... from nitric acid production in which all the raw material ammonia is in the gaseous form: [Metric units... limitations Maximum for any 1 day Average of daily values for 30 consecutive days shall not exceed— Ammonia... all the raw material ammonia is in the shipped liquid form: [Metric units, kg/kkg of product; English...

40 CFR 418.52 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2011 CFR

2011-07-01

... from nitric acid production in which all the raw material ammonia is in the gaseous form: [Metric units... limitations Maximum for any 1 day Average of daily values for 30 consecutive days shall not exceed— Ammonia... all the raw material ammonia is in the shipped liquid form: [Metric units, kg/kkg of product; English...

40 CFR 418.52 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2014 CFR

2014-07-01

... from nitric acid production in which all the raw material ammonia is in the gaseous form: [Metric units... limitations Maximum for any 1 day Average of daily values for 30 consecutive days shall not exceed— Ammonia... all the raw material ammonia is in the shipped liquid form: [Metric units, kg/kkg of product; English...

40 CFR 418.52 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2013 CFR

2013-07-01

... from nitric acid production in which all the raw material ammonia is in the gaseous form: [Metric units... limitations Maximum for any 1 day Average of daily values for 30 consecutive days shall not exceed— Ammonia... all the raw material ammonia is in the shipped liquid form: [Metric units, kg/kkg of product; English...

40 CFR 418.52 - Effluent limitations guidelines representing the degree of effluent reduction attainable by the...

Code of Federal Regulations, 2010 CFR

2010-07-01

... from nitric acid production in which all the raw material ammonia is in the gaseous form: [Metric units... limitations Maximum for any 1 day Average of daily values for 30 consecutive days shall not exceed— Ammonia... all the raw material ammonia is in the shipped liquid form: [Metric units, kg/kkg of product; English...

Catalysis: A Potential Alternative to Kraft Pulping

Treesearch

Alan W. Rudie; Peter W. Hart

2014-01-01

A thorough analysis of the kraft pulping process makes it obvious why it has dominated for over a century as an industrial process with no replacement in sight. It uses low cost raw materials, collects and regenerates over 90% of the chemicals needed in the process, is indifferent to wood raw material and good at preserving the cellulose portion of the wood which is...

Catalysis: A Potential Alternative to Kraft Pulping

Treesearch

Alan W. Rudie; Peter W. Hart

2014-01-01

A thorough analysis of the kraft pulping process makes it obvious why it has dominated for over a century as an industrial process with no replacement in sight. It uses low-cost raw materials; collects and regenerates over 90% of the chemicals needed in the process; and is indifferent to wood raw material and good at preserving the cellulose portion of the wood, the...

Pulpwood production in the Northeast 1969

Treesearch

James T. Bones; David R. Dickson

1970-01-01

This annual report is based on a canvass of all pulpmills in the Northeast that use wood-either from roundwood or plant residues-as a basic raw material for a variety of products. Mills that use pulpwood as a raw material in producing insulation board and hardboard were also included in the canvass. The production-from-roundwood statistics reported in this bulletin are...

Pulpwood production in the Northeast 1970

Treesearch

James T. Bones; David R. Dickson

1971-01-01

This annual report is based on a canvass of all pulpmills in the Northeast that use wood-either roundwood or plant residues-as a basic raw material for a variety of products. Mills that use pulpwood as a raw material in producing insulation board and hardboard were also included in the canvass. The statistics for production from roundwood reported in this bulletin are...

2. EXTERIOR VIEW, LOOKING NORTHEAST FROM THE CUPOLA (RIGHT) TO ...

Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

2. EXTERIOR VIEW, LOOKING NORTHEAST FROM THE CUPOLA (RIGHT) TO COKE BIN (LEFT), OF RAW MATERIALS YARD. FOUNDRY IRON IS FROM SCRAP, NOT BASIC ORE. RAW MATERIALS ASSEMBLED, IN PILES, FOR SMELTING ARE AUTOMOTIVE SCRAP (CENTER), STRUCTURAL STEEL AND RAILROAD RAIL (RIGHT) AND LIMESTONE (LEFT). - Stockham Pipe & Fittings Company, Grey Iron Foundry, 4000 Tenth Avenue North, Birmingham, Jefferson County, AL

Successes, shortcomings in using production wastes as raw material

NASA Astrophysics Data System (ADS)

Glushenkova, L.

1983-10-01

The economical and rational use of all forms of resources under modern conditions is a task of nationwide significance. Its urgency is caused by factors such as the progressively growing need for raw material, fuel, energy, and supplies, the limited and non-renewable nature of many minerals, and the difficult conditions of mining them and transporting them to where they are needed.

Strategy to Overcome Effect of Raw Materials on Enzymatic Process of Biodiesel from Non-edible Oils Using Candida sp. 99-125 Lipase.

PubMed

Nie, Kaili; Wang, Fang; Tan, Tianwei; Liu, Luo

2015-11-01

Non-edible oils are preferred raw materials for biodiesel production. However, the properties of raw materials significantly affect the synthesis process, leading to difficulties to design one process suitable for any kind of raw material. In this study, the composition of five typical non-edible oils was analyzed. The major difference was the content of free fatty acids, reflected from their acid values. The influence of different oils was investigated by using lipase from Candida sp. 99-125. At low lipase dosage and low water content, the conversion was found proportional to the acid value. However, by increasing the water content or lipase dosage, we observed that the conversions for all kinds of oils used in this study could exceed 80%. Time course analysis indicates that the lipase used in this study catalyzed hydrolysis followed by esterification, rather than direct transesterification. Accumulation of free fatty acids at the very beginning was necessary. A high water content facilitated the hydrolysis of oils with low acid value. This lipase showed capability to transform all the oils by controlling the water content.

Industrial bioconversion of renewable resources as an alternative to conventional chemistry.

PubMed

Willke, Th; Vorlop, K-D

2004-12-01

There are numerous possibilities for replacing chemical techniques with biotechnological methods based on renewable resources. The potential of biotechnology (products, technologies, metabolic pathways) is for the most part well known. Often the costs are still the problem. Biotechnological advances have the best chances for replacing some fine chemicals. While the raw material costs are less of a consideration here, the environmental benefit is huge, as chemical-technical processes often produce a wide range of undesirable/harmful by-products or waste. In the case of bulk chemicals (<1 US dollar/kg) the product price is affected mainly by raw material costs. As long as fossil raw materials are still relatively inexpensive, alternatives based on renewable resources cannot establish themselves. Residues and waste, which are available even at no cost in some cases, are an exception. The introduction of new technologies for the efficient use of such raw materials is currently being promoted. The utilisation of residual wood, plant parts, waste fat, and crude glycerol, for example, provides great potential. For industrial chemicals (2-4 US dollars/kg), process and recovery costs play a greater role. Here, innovative production technologies and product recovery techniques (e.g. on-line product separation) can increase competitiveness.

Optimization of formulation and processing of Moringa oleifera and spirulina complex tablets.

PubMed

Zheng, Yi; Zhu, Fan; Lin, Dan; Wu, Jun; Zhou, Yichao; Mark, Bohn

2017-01-01

Objective: To prepare a more comprehensive nutrition, more balanced proportion of natural nutritional supplement tablets with Moringa oleifera leaves and spirulina the two nutrients which have complementary natural food ingredients. Method: On the basis of research M. oleifera leaves with spirulina nutrient composition was determined on M. oleifera leaves and spirulina ratio of raw materials, and the choice of microcrystalline cellulose, sodium salt of caboxy methyl cellulose(CMC),magnesium stearate excipient, through single factor and orthogonal experiment, selecting the best formula tablets prepared by powder direct compression technology, for preparation of M. oleifera and spirulina complex tablets. Results: The best ratio of raw material for the M. oleifera leaves powder: spirulina powder was 7:3, the best raw materials for the tablet formulation was 88.5%, 8.0% microcrystalline cellulose, CMC 2.0%, stearin magnesium 1.5%, the optimum parameters for the raw material crushing 200-300 mesh particle size, moisture content of 7%, tableting pressure 40 kN. Conclusion: Through formulation and process optimization, we can prepare more comprehensive and balanced nutrition M. oleifera and spirulina complex tablets, its sheet-shaped appearance, piece weight variation, hardness, friability, disintegration and other indicators have reached the appropriate quality requirements.

Effect of synthesis route on electrical and ethanol sensing characteristics for LaFeO3-δ nanoparticles by citric sol-gel method

NASA Astrophysics Data System (ADS)

Cao, Ensi; Yang, Yuqing; Cui, Tingting; Zhang, Yongjia; Hao, Wentao; Sun, Li; Peng, Hua; Deng, Xiao

2017-01-01

LaFeO3-δ nanoparticles were prepared by citric sol-gel method with different raw material choosing and calcination process. The choosing of polyethylene glycol instead of ethylene glycol as raw material and additional pre-calcination at 400 °C rather than direct calcination at 600 °C could result in the decrease of resistance due to the reduction of activation energy Ea. Meanwhile, the choosing of ethylene glycol as raw material and additional pre-calcination leads to the enhancement of sensitivity to ethanol. Comprehensive analysis on the sensitivity and XRD, SEM, TEM, XPS results indicates that the sensing performance of LaFeO3-δ should be mainly determined by the adsorbed oxygen species on Fe ions, with certain contribution from native active oxygen. The best sensitivity of 46.1-200 ppm ethanol at prime working temperature of 112 °C is obtained by the sample using ethylene glycol as raw material with additional pre-calcination, which originates from its uniformly-sized and well-dispersed particles as well as high atomic ratio of Fe/La at surface region.

Environmental analysis of raw cork extraction in cork oak forests in southern Europe (Catalonia--Spain).

PubMed

Rives, Jesús; Fernandez-Rodriguez, Ivan; Rieradevall, Joan; Gabarrell, Xavier

2012-11-15

Cork oak grows endemically in a narrow region bordering the western Mediterranean, and especially in the Iberian Peninsula. The importance of cork agro-forestry systems lies in the fact that a natural and renewable raw material - cork - can be extracted sustainably without endangering the tree or affecting biodiversity. This paper describes an environmental analysis of the extraction of raw cork in cork oak forests in Catalonia, using data from five representative local forest exploitations. The evaluation was carried out using life cycle assessment (LCA) methodology, and all the forestry management required to obtain a tonne of raw cork was included. The aim of the study was to evaluate the environmental impacts - in terms of global warming, acidification, eutrophication, human toxicity, and so on - caused by cork extraction and determine the carbon dioxide balance of these forestry systems, with a tree lifespan of about 200 years. During the life cycle extraction of cork in Catalonia, 0.2 kg of CO(2) eq. was emitted per kg of raw cork extracted. Moreover, cork cannot be extracted without the tree, which will be fixing carbon dioxide throughout its technological useful life (200 years), despite the fact that the bark is removed periodically: every 13-14 years. If the emission from extraction and the carbon contained in the material is discounted, the carbon dioxide balance indicates that 18 kg of CO(2) are fixed per kg of raw cork extracted. Therefore, cork is a natural, renewable and local material that can replace other non-renewable materials, at local level, to reduce the environmental impacts of products, and particularly to reduce their carbon footprint. Copyright © 2012 Elsevier Ltd. All rights reserved.

Synthesis, characterization and histopathological study of a lead-based Indian traditional drug: naga bhasma.

PubMed

Singh, S K; Gautam, D N S; Kumar, M; Rai, S B

2010-01-01

The aim of the present study is to prepare and characterize Naga bhasma on structural and elemental basis to address the role of the raw materials used during the preparation, compound form of the lead bhasma, nature (crystalline/amorphous) and crystallite/particle size of the drug. The study also covers the toxicological effect of the drug on albino rats. It was found that drug contains lead in nano-crystalline (~60 nm) lead sulfide form (Pb(2+)) associated with the organic contents and different nutrient elements coming from the herbs used during the preparation. Naga bhasma prepared was found to be totally safe in histopathology study on rats at a dose of 6 mg/100 g/day. The different characterization techniques used present a role model for the quality control and standardization of such kinds of herbo-metallic medicines.

Analysis of storage possibility of raw and smoked breast meat of oat-fattened White Kołuda® goose based on their quality characteristics.

PubMed

Damaziak, K; Stelmasiak, A; Michalczuk, M; Wyrwisz, J; Moczkowska, M; Marcinkowska-Lesiak, M M; Niemiec, J; Wierzbicka, A

2016-09-01

Raw and smoked (spickgans) fillets of oat-fattened White Kołuda® goose were packed in: PET - ethylene terephthalate bags; VSP - 99% vacuum; MAP1 - 80% O2, 20% CO2; MAP2 - 70% N2, 30% O2; MAP3 - 30% O2, 40% N2, 30% CO2, and stored at a temperature of 2°C. On the day of packaging (0 d) and during storage of raw (5, 7, 10 d) and smoked fillets (5, 10, 15 d), the samples were analyzed for weight losses, physicochemical traits, and chemical composition. The study demonstrated the effect of storage time and packaging method on storage yield of raw and smoked fillets. In VSP, the raw fillets were characterized by the lowest amount of leakage, whereas spickgans were characterized by the highest storage yield and weight loss. The analysis of the effect of the modified atmosphere demonstrated the lowest weight loss of raw fillets at, simultaneously, the smallest amount of leakage in MAP1. The spickgans stored in MAP2 showed higher weight, higher yield after storage, and lower storage loss in all terms of analyses compared to MAP1 and MAP3. The greatest cooking loss at simultaneously the lowest pH values was determined for the samples stored in VSP. The WBSF values of raw fillets were decreasing along with storage time, in contrast to WBSF values of spickgans, in which case the value of this parameter increased compared to 0 d. Raw fillets stored in MAP1 and MAP3 were characterized by the most significant increase in the value of L*, by a decrease in the value of a* and an increase in that of b* parameter. Visual assessment of spickgans on 15 d of storage revealed the presence of white sediment on the surface of products, except for the samples stored in VSP. The study demonstrated the effect of storage time on the contents of protein and fat in raw fillets and on the contents of salt and fat in spickgans. © 2016 Poultry Science Association Inc.

Agaves as a raw material: recent technologies and applications.

PubMed

Narváez-Zapata, J A; Sánchez-Teyer, L F

2009-01-01

Agave plants are a valuable source of raw material due to its fibrous and complex sugar content of their leaves and core, and their bagasse waste can be use for several aims. This plant genus belongs to the Agavaceae family and until now more than 200 species have been described. A large number of Agave species are currently used as raw material in several biotechnological processes. This review shows the reported applications and patents on fields like alcoholic brewages with special reference to Tequila and Mezcal, the isolation and use of compounds such as saponins and agave fructans, and their potential biotechnological application on several human demands. The process to obtain fibers and cellulose, stock feeds, and several miscellaneous extractives are also reviewed. Some possibilities and problems of cultivation are discussed.

Using the split Hopkinson pressure bar to validate material models.

PubMed

Church, Philip; Cornish, Rory; Cullis, Ian; Gould, Peter; Lewtas, Ian

2014-08-28

This paper gives a discussion of the use of the split-Hopkinson bar with particular reference to the requirements of materials modelling at QinetiQ. This is to deploy validated material models for numerical simulations that are physically based and have as little characterization overhead as possible. In order to have confidence that the models have a wide range of applicability, this means, at most, characterizing the models at low rate and then validating them at high rate. The split Hopkinson pressure bar (SHPB) is ideal for this purpose. It is also a very useful tool for analysing material behaviour under non-shock wave loading. This means understanding the output of the test and developing techniques for reliable comparison of simulations with SHPB data. For materials other than metals comparison with an output stress v strain curve is not sufficient as the assumptions built into the classical analysis are generally violated. The method described in this paper compares the simulations with as much validation data as can be derived from deployed instrumentation including the raw strain gauge data on the input and output bars, which avoids any assumptions about stress equilibrium. One has to take into account Pochhammer-Chree oscillations and their effect on the specimen and recognize that this is itself also a valuable validation test of the material model. © 2014 The Author(s) Published by the Royal Society. All rights reserved.

Chemical, structural and combustion characteristics of carbonaceous products obtained by hydrothermal carbonization of palm empty fruit bunches.

PubMed

Parshetti, Ganesh K; Kent Hoekman, S; Balasubramanian, Rajasekhar

2013-05-01

A carbon-rich solid product, denoted as hydrochar, was synthesized by hydrothermal carbonization (HTC) of palm oil empty fruit bunch (EFB), at different pre-treatment temperatures of 150, 250 and 350 °C. The conversion of the raw biomass to its hydrochar occurred via dehydration and decarboxylation processes. The hydrochar produced at 350 °C had the maximum energy-density (>27 MJ kg(-1)) with 68.52% of raw EFB energy retained in the char. To gain a detailed insight into the chemical and structural properties, carbonaceous hydrochar materials were characterized by FE-SEM, FT-IR, XRD and Brunauer-Emmett-Teller (BET) analyses. This work also investigated the influence of hydrothermally treated hydrochars on the co-combustion characteristics of low rank Indonesian coal. Conventional thermal gravimetric analysis (TGA) parameters, kinetics and activation energy of different hydrochar and coal blends were estimated. Our results show that solid hydrochars improve the combustion of low rank coals for energy generation. Copyright © 2012 Elsevier Ltd. All rights reserved.

Preparation of fly ash based zeolite for removal of fluoride from drinking water

NASA Astrophysics Data System (ADS)

Panda, Laxmidhar; Kar, Biswabandita; Dash, Subhakanta

2018-05-01

Fluoride contamination of drinking water is a worldwide phenomenon and scientists are working relentlessly to find ways to remove fluoride from drinking water. Out of the different methods employed for removal fluoride from drinking water adsorption process is the most suitable because in this process the adsorbent is regenerated and the process is cost effective. In the present study fly ash is used as the raw material, which is treated with alkali (NaOH) to form NaP1 zeolite. This zeolite is then subjected to characterization by standard procedures. It is found that the synthesized zeolite has more crystalline character than the raw fly ash and has also more voids and channels on its surface. The surface of the synthesized zeolite is modified with calcium chloride and the same is employed for removal of fluoride under varying pH, contact time, initial concentration of fluoride, temperature and adsorbent dose etc so as to assess the suitably or otherwise of the synthesized product.

Optical-electronic system for express analysis of mineral raw materials dressability by color sorting method

NASA Astrophysics Data System (ADS)

Alekhin, Artem A.; Gorbunova, Elena V.; Chertov, Aleksandr N.; Petuhova, Darya B.

2013-04-01

Due to the depletion of solid minerals ore reserves and the involvement in the production of the poor and refractory ores a process of continuous appreciation of minerals is going. In present time at the market of enrichment equipment are well represented optical sorters of various firms. All these sorters are essentially different from each other by parameters of productivity, classes of particles sizes for processed raw, nuances of decision algorithm, as well as by color model (RGB, YUV, HSB, etc.) chosen to describe the color of separating mineral samples. At the same time there is no dressability estimation method for mineral raw materials without direct semi-industrial test on the existing type of optical sorter, as well as there is no equipment realizing mentioned dressability estimation method. It should also be note the lack of criteria for choosing of one or another manufacturer (or type) of optical sorter. A direct consequence of this situation is the "opacity" of the color sorting method and the rejection of its potential customers. The proposed solution of mentioned problems is to develop the dressability estimation method, and to create an optical-electronic system for express analysis of mineral raw materials dressability by color sorting method. This paper has the description of structure organization and operating principles of experimental model optical-electronic system for express analysis of mineral raw material. Also in this work are represented comparison results of the proposed optical-electronic system and the real color sorter.

7 CFR 58.232 - Milk.

Code of Federal Regulations, 2011 CFR

2011-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Materials § 58.232 Milk. Raw milk shall meet the requirements as outlined in §§ 58.132 through 58.138 and, unless...

7 CFR 58.232 - Milk.

Code of Federal Regulations, 2010 CFR

2010-01-01

... Plants Approved for USDA Inspection and Grading Service 1 Quality Specifications for Raw Materials § 58.232 Milk. Raw milk shall meet the requirements as outlined in §§ 58.132 through 58.138 and, unless...

40 CFR 409.21 - Specialized definitions.

Code of Federal Regulations, 2012 CFR

2012-07-01

... AND STANDARDS SUGAR PROCESSING POINT SOURCE CATEGORY Crystalline Cane Sugar Refining Subcategory § 409... raw material (raw sugar) contained within aqueous solution at the beginning of the process for production of refined cane sugar. ...

Extraterrestrial materials processing and construction

NASA Technical Reports Server (NTRS)

Criswell, D. R.

1978-01-01

Applications of available terrestrial skills to the gathering of lunar materials and the processing of raw lunar materials into industrial feed stock were investigated. The literature on lunar soils and rocks was reviewed and the chemical processes by which major oxides and chemical elements can be extracted were identified. The gathering of lunar soil by means of excavation equipment was studied in terms of terrestrial experience with strip mining operations on earth. The application of electrostatic benefication techniques was examined for use on the moon to minimize the quantity of materials requiring surface transport and to optimize the stream of raw materials to be transported off the moon for subsequent industrial use.

[Russian and foreign legal-standards bases for guaranteeing the parasitic safety of raw produce and food products].

PubMed

Lovgalev, A S

1998-01-01

The paper analyzes the standard legal and methodological assurance of the quality and safety of animal food raw materials and foodstuffs (meat, meat products, fish, shellfish, crayfish and their processing products) by the parasitic purity rates according the requirements under the Russian Federation's laws "On Sanitary and Epidemiological Well-Being of the Population", "On Protection of Consumer's Rights", "On Certification of Products and Services", those of SanPiN, such as 2.3.2.560-96 "Sanitary Requirements for the Quality and Safety of Food Raw Materials and Foodstuffs" and 3.2.569-96 "Prevention of Parasitic Diseases in the Russian Federation".

Comparative analysis of non-destructive methods to control fissile materials in large-size containers

NASA Astrophysics Data System (ADS)

Batyaev, V. F.; Sklyarov, S. V.

2017-09-01

The analysis of various non-destructive methods to control fissile materials (FM) in large-size containers filled with radioactive waste (RAW) has been carried out. The difficulty of applying passive gamma-neutron monitoring FM in large containers filled with concreted RAW is shown. Selection of an active non-destructive assay technique depends on the container contents; and in case of a concrete or iron matrix with very low activity and low activity RAW the neutron radiation method appears to be more preferable as compared with the photonuclear one. Note to the reader: the pdf file has been changed on September 22, 2017.

Mathematical modeling of heat treatment processes conserving biological activity of plant bioresources

NASA Astrophysics Data System (ADS)

Rodionova, N. S.; Popov, E. S.; Pozhidaeva, E. A.; Pynzar, S. S.; Ryaskina, L. O.

2018-05-01

The aim of this study is to develop a mathematical model of the heat exchange process of LT-processing to estimate the dynamics of temperature field changes and optimize the regime parameters, due to the non-stationarity process, the physicochemical and thermophysical properties of food systems. The application of LT-processing, based on the use of low-temperature modes in thermal culinary processing of raw materials with preliminary vacuum packaging in a polymer heat- resistant film is a promising trend in the development of technics and technology in the catering field. LT-processing application of food raw materials guarantees the preservation of biologically active substances in food environments, which are characterized by a certain thermolability, as well as extend the shelf life and high consumer characteristics of food systems that are capillary-porous bodies. When performing the mathematical modeling of the LT-processing process, the packet of symbolic mathematics “Maple” was used, as well as the mathematical packet flexPDE that uses the finite element method for modeling objects with distributed parameters. The processing of experimental results was evaluated with the help of the developed software in the programming language Python 3.4. To calculate and optimize the parameters of the LT processing process of polycomponent food systems, the differential equation of non-stationary thermal conductivity was used, the solution of which makes it possible to identify the temperature change at any point of the solid at different moments. The present study specifies data on the thermophysical characteristics of the polycomponent food system based on plant raw materials, with the help of which the physico-mathematical model of the LT- processing process has been developed. The obtained mathematical model allows defining of the dynamics of the temperature field in different sections of the LT-processed polycomponent food systems on the basis of calculating the evolution profiles of temperature fields, which enable one to analyze the efficiency of the regime parameters of heat treatment.

JPRS Report East Asia Southeast Asia

DTIC Science & Technology

1987-06-03

the Philippines and Japan experienced production problems. The Philippines lacked supplies of raw materials while Japan’s currency rose so high as...Malaysia, Saudi Arabia, Singapore Squid: Greece, Spain, the Philippines , Saudi Arabia, U.S. Clams: U.S., Canada, Malaysia, Japan, Italy, West Germany...raw material caught under joint venture fisheries enter- prises, while Thailand’s competitors like the Philippines and Taiwan remain unable to

Effect of the raw material composition of fabrics on the Limiting Oxygen Index (LOI)

NASA Technical Reports Server (NTRS)

Jeler, S.; Ceric, B.

1986-01-01

The raw material composition of fabrics is one of the most important factors for LOI value. LOI value was determined in samples of varying composition composed of cellulose, protein, and synthetic fibers and their mixtures, based on ASTM D 2863-76. Cellulose fibers and their mixtures exhibited the lowest value, while synthetic fibers had the highest LOI value.

JPRS Report, Near East and South Asia, India

DTIC Science & Technology

1992-05-13

withdrawal of the RBI import policy for capital goods, raw materials, compo- nents and industrial consumables . Also, the licensing of host of industrial ...fully capable of establishing consumer production industries and providing raw materials for it. This would also benefit India, because a huge market...which two- thirds of population depends for their livelihood, demand base for the industrial sector, especially essen- tial consumer goods is likely

DOE Office of Scientific and Technical Information (OSTI.GOV)

Venkatraman, A.; Walawender, W.P.; Fan, L.T.

The term, activated carbon, is a generic name for a family of carbonaceous materials with well-developed porosities and consequently, large adsorptive capacities. Activated carbons are increasingly being consumed worldwide for environmental applications such as separation of volatiles from bulk gases and purification of water and waste-water streams. The global annual production is estimated to be around 300 million kilograms, with a rate of increase of 7% each year. Activated carbons can be prepared from a variety of raw materials. Approximately, 60% of the activated carbons generated in the United States is produced from coal; 20%, from coconut shells; and themore » remaining 20% from wood and other sources of biomass. The pore structure and properties of activated carbons are influenced by the nature of the starting material and the initial physical and chemical conditioning as well as the process conditions involved in its manufacture. The porous structures of charcoals and activated carbons obtained by the carbonization of kernels have been characterized.« less

Hook tool manufacture in New Caledonian crows: behavioural variation and the influence of raw materials.

PubMed

Klump, Barbara C; Sugasawa, Shoko; St Clair, James J H; Rutz, Christian

2015-11-18

New Caledonian crows use a range of foraging tools, and are the only non-human species known to craft hooks. Based on a small number of observations, their manufacture of hooked stick tools has previously been described as a complex, multi-stage process. Tool behaviour is shaped by genetic predispositions, individual and social learning, and/or ecological influences, but disentangling the relative contributions of these factors remains a major research challenge. The properties of raw materials are an obvious, but largely overlooked, source of variation in tool-manufacture behaviour. We conducted experiments with wild-caught New Caledonian crows, to assess variation in their hooked stick tool making, and to investigate how raw-material properties affect the manufacture process. In Experiment 1, we showed that New Caledonian crows' manufacture of hooked stick tools can be much more variable than previously thought (85 tools by 18 subjects), and can involve two newly-discovered behaviours: 'pulling' for detaching stems and bending of the tool shaft. Crows' tool manufactures varied significantly: in the number of different action types employed; in the time spent processing the hook and bending the tool shaft; and in the structure of processing sequences. In Experiment 2, we examined the interaction of crows with raw materials of different properties, using a novel paradigm that enabled us to determine subjects' rank-ordered preferences (42 tools by 7 subjects). Plant properties influenced: the order in which crows selected stems; whether a hooked tool was manufactured; the time required to release a basic tool; and, possibly, the release technique, the number of behavioural actions, and aspects of processing behaviour. Results from Experiment 2 suggested that at least part of the natural behavioural variation observed in Experiment 1 is due to the effect of raw-material properties. Our discovery of novel manufacture behaviours indicates a plausible scenario for the evolutionary origins, and gradual refinement, of New Caledonian crows' hooked stick tool making. Furthermore, our experimental demonstration of a link between raw-material properties and aspects of tool manufacture provides an alternative hypothesis for explaining regional differences in tool behaviours observed in New Caledonian crows, and some primate species.

Phenotyping the quality of complex medium components by simple online-monitored shake flask experiments.

PubMed

Diederichs, Sylvia; Korona, Anna; Staaden, Antje; Kroutil, Wolfgang; Honda, Kohsuke; Ohtake, Hisao; Büchs, Jochen

2014-11-07

Media containing yeast extracts and other complex raw materials are widely used for the cultivation of microorganisms. However, variations in the specific nutrient composition can occur, due to differences in the complex raw material ingredients and in the production of these components. These lot-to-lot variations can affect growth rate, product yield and product quality in laboratory investigations and biopharmaceutical production processes. In the FDA's Process Analytical Technology (PAT) initiative, the control and assessment of the quality of critical raw materials is one key aspect to maintain product quality and consistency. In this study, the Respiration Activity Monitoring System (RAMOS) was used to evaluate the impact of different yeast extracts and commercial complex auto-induction medium lots on metabolic activity and product yield of four recombinant Escherichia coli variants encoding different enzymes. Under non-induced conditions, the oxygen transfer rate (OTR) of E. coli was not affected by a variation of the supplemented yeast extract lot. The comparison of E. coli cultivations under induced conditions exhibited tremendous differences in OTR profiles and volumetric activity for all investigated yeast extract lots of different suppliers as well as lots of the same supplier independent of the E. coli variant. Cultivation in the commercial auto-induction medium lots revealed the same reproducible variations. In cultivations with parallel offline analysis, the highest volumetric activity was found at different cultivation times. Only by online monitoring of the cultures, a distinct cultivation phase (e.g. glycerol depletion) could be detected and chosen for comparable and reproducible offline analysis of the yield of functional product. This work proves that cultivations conducted in complex media may be prone to significant variation in final product quality and quantity if the quality of the raw material for medium preparation is not thoroughly checked. In this study, the RAMOS technique enabled a reliable and reproducible screening and phenotyping of complex raw material lots by online measurement of the respiration activity. Consequently, complex raw material lots can efficiently be assessed if the distinct effects on culture behavior and final product quality and quantity are visualized.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sai, P.M.S.; Ahmed, J.; Krishnaiah, K.

Activated carbon is produced from coconut shell char using steam or carbon dioxide as the reacting gas in a 100 mm diameter fluidized bed reactor. The effect of process parameters such as reaction time, fluidizing velocity, particle size, static bed height, temperature of activation, fluidizing medium, and solid raw material on activation is studied. The product is characterized by determination of iodine number and BET surface area. The product obtained in the fluidized bed reactor is much superior in quality to the activated carbons produced by conventional processes. Based on the experimental observations, the optimum values of process parameters aremore » identified.« less

Influence of input material and operational performance on the physical and chemical properties of MSW compost.

PubMed

Montejo, C; Costa, C; Márquez, M C

2015-10-01

Certain controversy exists about the use of compost from MSW (municipal solid waste) and, specifically, from the organic fraction of MSW that has not been separated at the source. In this case, the final composition of MSW compost is related to the performance of the separation process in MBT (Mechanical and Biological Treatment) plants as well as the composition of raw materials and the particular features of composting systems. In an effort to investigate the quality of MSW compost, 30 samples of this product obtained from 10 different MBT plants were studied. The main physical and chemical properties were analyzed and were compared with the requirements of current legislation. The composting systems used to produce these compost samples were studied and the input materials were characterized. The results reveal that the heavy metal content in MSW compost was below the legal restrictions in all samples but one; however, in most of them the percentage of Pb was high. The fertilizing potential of MSW compost has been demonstrated by its high nutrient concentrations, particularly N, K, P, Ca and Mg. Nevertheless, here the percentage of inert impurities with a size larger than 2 mm, such as plastic or glass, was seen to be excessively high exceeding in some cases the legal limit. The source of such pollution lies in the composting inputs, OFMSW (organic fraction of MSW), which showed high percentages of improper materials such as plastic (9%) or glass (11%). Accordingly, the performance of the sorting stage for the collection of the raw material must be improved, as must the refining process, since this does not remove the necessary amounts of these impurities from the final compost. Copyright © 2015 Elsevier Ltd. All rights reserved.

Manufacturing and actuation characterization of ionic polymer metal composites with silver as electrodes

NASA Astrophysics Data System (ADS)

Pandita, Surya D.; Lim, Hyoung Tae; Yoo, Youngtai; Park, Hoon Cheol

2006-03-01

Manufacturing and characterization of ionic polymer metal composites (IPMCs) with silver as electrodes have been investigated. Tollen's reagent that contains ion Ag(NH 3) II + was used as a raw material for silver deposition on the surfaces of the polymer membrane Nafion"R". Two types of inner solvents, namely common water based electrolyte solution (LiOH 1N) and ionic liquid were used and investigated. Compared to IPMCs with platinum electrodes, silver-plated IPMCs with water electrolyte showed higher conductivity. The actuation response of silver-plated IPMCs with the water based electrolyte was faster than that of platinum IPMCs. However, the silver electrode was too brittle and severely damaged during the solvent exchange process from water to ionic liquid, resulted in high resistance and hence very low actuation behavior.

Characterization of the indigenous microflora in raw and pasteurized buffalo milk during storage at refrigeration temperature by high-throughput sequencing.

PubMed

Li, Ling; Renye, John A; Feng, Ling; Zeng, Qingkun; Tang, Yan; Huang, Li; Ren, Daxi; Yang, Pan

2016-09-01

The effect of refrigeration on bacterial communities within raw and pasteurized buffalo milk was studied using high-throughput sequencing. High-quality samples of raw buffalo milk were obtained from 3 dairy farms in the Guangxi province in southern China. Five liters of each milk sample were pasteurized (72°C; 15 s); and both raw and pasteurized milks were stored at refrigeration temperature (1-4°C) for various times with their microbial communities characterized using the Illumina Miseq platform (Novogene, Beijing, China). Results showed that both raw and pasteurized milks contained a diverse microbial population and that the populations changed over time during storage. In raw buffalo milk, Lactococcus and Streptococcus dominated the population within the first 24h; however, when stored for up to 72h the dominant bacteria were members of the Pseudomonas and Acinetobacter genera, totaling more than 60% of the community. In pasteurized buffalo milk, the microbial population shifted from a Lactococcus-dominated community (7d), to one containing more than 84% Paenibacillus by 21d of storage. To increase the shelf-life of buffalo milk and its products, raw milk needs to be refrigerated immediately after milking and throughout transport, and should be monitored for the presence of Paenibacillus. Results from this study suggest pasteurization should be performed within 24h of raw milk collection, when the number of psychrotrophic bacteria are low; however, as Paenibacillus spores are resistant to pasteurization, additional antimicrobial treatments may be required to extend shelf-life. The findings from this study are expected to aid in improving the quality and safety of raw and pasteurized buffalo milk. Copyright © 2016 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

Coliform Bacteria for Bioremediation of Waste Hydrocarbons

PubMed Central

2017-01-01

Raw, domestic sewage of Kuwait City contained about 106 ml−1 colony forming units of Enterobacter hormaechei subsp. oharae (56.6%), Klebsiella spp. (36%), and Escherichia coli (7.4%), as characterized by their 16S rRNA-gene sequences. The isolated coliforms grew successfully on a mineral medium with crude oil vapor as a sole source of carbon and energy. Those strains also grew, albeit to different degrees, on individual n-alkanes with carbon chains between C9 and C36 and on the individual aromatic hydrocarbons, toluene, naphthalene, phenanthrene, and biphenyl as sole sources of carbon and energy. These results imply that coliforms, like other hydrocarbonoclastic microorganisms, oxidize hydrocarbons to the corresponding alcohols and then to aldehydes and fatty acids which are biodegraded by β-oxidation to acetyl CoA. The latter is a well-known key intermediate in cell material and energy production. E. coli cells grown in the presence of n-hexadecane (but not in its absence) exhibited typical intracellular hydrocarbon inclusions, as revealed by transmission electron microscopy. Raw sewage samples amended with crude oil, n-hexadecane, or phenanthrene lost these hydrocarbons gradually with time. Meanwhile, the numbers of total and individual coliforms, particularly Enterobacter, increased. It was concluded that coliform bacteria in domestic sewage, probably in other environmental materials too, are effective hydrocarbon-biodegrading microorganisms. PMID:29082238

Phenolics in Primula veris L. and P. elatior (L.) Hill Raw Materials

PubMed Central

Mirgos, Małgorzata; Kosakowska, Olga; Szymborska-Sandhu, Izabela; Węglarz, Zenon

2017-01-01

Primula veris L. and Primula elatior (L.) Hill represent medicinal plants used for the production of herbal teas and preparations with antioxidant and expectorant activity. Flowers and roots of both species possess the same biological activity. In the presented study, raw materials of wild growing P. veris and P. elatior were compared in terms of the content and composition of phenolic compounds using a fast and simple HPLC-DAD method. The study showed that flowers of both species were rich in flavonoids. However, P. veris flowers were characterized with a distinctly higher content of isorhamnetin-3-O-glucoside, astragalin, and (+)-catechin, whereas P. elatior occurred to be a richer source of rutoside and isorhamnetin-3-O-rutinoside. Hyperoside was found exclusively in P. elatior flowers. Phenolic glycosides (primverin and primulaverin) were identified only in the roots. Their content was about ten times higher in P. veris in comparison with P. elatior underground organs. The obtained results clearly show that both Primula species differ distinctly in terms of the content and composition of phenolic compounds. The compounds differentiating both species to the highest degree (hyperoside, in flowers, as well as primverin and primulaverin, in the roots) may be useful chemical markers in the identification and evaluation of both species. PMID:28835753

Polycyclic Aromatic Hydrocarbons (PAHs) produced in the combustion of fatty acid alkyl esters from different feedstocks: Quantification, statistical analysis and mechanisms of formation.

PubMed

Llamas, Alberto; Al-Lal, Ana-María; García-Martínez, María-Jesús; Ortega, Marcelo F; Llamas, Juan F; Lapuerta, Magín; Canoira, Laureano

2017-05-15

Polycyclic Aromatic Hydrocarbons (PAHs) are pollutants of concern due to their carcinogenic and mutagenic activity. Their emissions are mainly related with the combustion or pyrolysis of the organic matter, such as in fossil fuels combustion. It is important to characterize PAHs in the combustions of biofuels due to their increasing importance in the actual energetic setting. There is a lot of research focused in PAHs emission due to the combustion in diesel engines; but only few of them have analyzed the effect of raw material and type of alcohol used in the transesterification process. Different raw materials (i.e. animal fat, palm, rapeseed, linseed, peanut, coconut, and soybean oils) have been used for obtaining FAME and FAEE. A method for measuring PAHs generated during combustion in a bomb calorimeter has been developed. Combustion was made at different oxygen pressures and the samples were taken from the bomb after each combustion. Samples were extracted and the PAHs amounts formed during combustion were analyzed by GC-MS. This research shows the statistical relationships among the 16 PAHs of concern, biodiesel composition and oxygen pressure during combustion. Copyright © 2017 Elsevier B.V. All rights reserved.

The Microbiome and Metabolites in Fermented Pu-erh Tea as Revealed by High-Throughput Sequencing and Quantitative Multiplex Metabolite Analysis

PubMed Central

Sulyok, Michael; Liu, Xingzhong; Rao, Mingyong

2016-01-01

Pu-erh is a tea produced in Yunnan, China by microbial fermentation of fresh Camellia sinensis leaves by two processes, the traditional raw fermentation and the faster, ripened fermentation. We characterized fungal and bacterial communities in leaves and both Pu-erhs by high-throughput, rDNA-amplicon sequencing and we characterized the profile of bioactive extrolite mycotoxins in Pu-erh teas by quantitative liquid chromatography-tandem mass spectrometry. We identified 390 fungal and 629 bacterial OTUs from leaves and both Pu-erhs. Major findings are: 1) fungal diversity drops and bacterial diversity rises due to raw or ripened fermentation, 2) fungal and bacterial community composition changes significantly between fresh leaves and both raw and ripened Pu-erh, 3) aging causes significant changes in the microbial community of raw, but not ripened, Pu-erh, and, 4) ripened and well-aged raw Pu-erh have similar microbial communities that are distinct from those of young, raw Ph-erh tea. Twenty-five toxic metabolites, mainly of fungal origin, were detected, with patulin and asperglaucide dominating and at levels supporting the Chinese custom of discarding the first preparation of Pu-erh and using the wet tea to then brew a pot for consumption. PMID:27337135

Recycling-oriented characterization of plastic frames and printed circuit boards from mobile phones by electronic and chemical imaging.

PubMed

Palmieri, Roberta; Bonifazi, Giuseppe; Serranti, Silvia

2014-11-01

This study characterizes the composition of plastic frames and printed circuit boards from end-of-life mobile phones. This knowledge may help define an optimal processing strategy for using these items as potential raw materials. Correct handling of such a waste is essential for its further "sustainable" recovery, especially to maximize the extraction of base, rare and precious metals, minimizing the environmental impact of the entire process chain. A combination of electronic and chemical imaging techniques was thus examined, applied and critically evaluated in order to optimize the processing, through the identification and the topological assessment of the materials of interest and their quantitative distribution. To reach this goal, end-of-life mobile phone derived wastes have been systematically characterized adopting both "traditional" (e.g. scanning electronic microscopy combined with microanalysis and Raman spectroscopy) and innovative (e.g. hyperspectral imaging in short wave infrared field) techniques, with reference to frames and printed circuit boards. Results showed as the combination of both the approaches (i.e. traditional and classical) could dramatically improve recycling strategies set up, as well as final products recovery. Copyright © 2014 Elsevier Ltd. All rights reserved.

Utilization of flotation wastes of copper slag as raw material in cement production.

PubMed

Alp, I; Deveci, H; Süngün, H

2008-11-30

Copper slag wastes, even if treated via processes such as flotation for metal recovery, still contain heavy metals with hazardous properties posing environmental risks for disposal. This study reports the potential use of flotation waste of a copper slag (FWCS) as iron source in the production of Portland cement clinker. The FWCS appears a suitable raw material as iron source containing >59% Fe(2)O(3) mainly in the form of fayalite (Fe(2)SiO(4)) and magnetite (Fe(3)O(4)). The clinker products obtained using the FWCS from the industrial scale trial operations over a 4-month period were characterised for the conformity of its chemical composition and the physico-mechanical performance of the resultant cement products was evaluated. The data collected for the clinker products produced using an iron ore, which is currently used as the cement raw material were also included for comparison. The results have shown that the chemical compositions of all the clinker products including those of FWCS are typical of a Portland cement clinker. The mechanical performance of the standard mortars prepared from the FWCS clinkers were found to be similar to those from the iron ore clinkers with the desired specifications for the industrial cements e.g. CEM I type cements. Furthermore, the leachability tests (TCLP and SPLP) have revealed that the mortar samples obtained from the FWCS clinkers present no environmental problems while the FWCS could act as the potential source of heavy metal contamination. These findings suggest that flotation wastes of copper slag (FWCS) can be readily utilised as cement raw material due to its availability in large quantities at low cost with the further significant benefits for waste management/environmental practices of the FWCS and the reduced production and processing costs for cement raw materials.

Identifying Major Transitions in the Evolution of Lithic Cutting Edge Production Rates

PubMed Central

Clarkson, Chris

2016-01-01

The notion that the evolution of core reduction strategies involved increasing efficiency in cutting edge production is prevalent in narratives of hominin technological evolution. Yet a number of studies comparing two different knapping technologies have found no significant differences in edge production. Using digital analysis methods we present an investigation of raw material efficiency in eight core technologies broadly representative of the long-term evolution of lithic technology. These are bipolar, multiplatform, discoidal, biface, Levallois, prismatic blade, punch blade and pressure blade production. Raw material efficiency is assessed by the ratio of cutting edge length to original core mass. We also examine which flake attributes contribute to maximising raw material efficiency, as well as compare the difference between expert and intermediate knappers in terms of cutting edge produced per gram of core. We identify a gradual increase in raw material efficiency over the broad sweep of lithic technological evolution. The results indicate that the most significant transition in efficiency likely took place with the introduction of small foliate biface, Levallois and prismatic blade knapping, all introduced in the Middle Stone Age / Middle Palaeolithic among early Homo sapiens and Neanderthals. This suggests that no difference in raw material efficiency existed between these species. With prismatic blade technology securely dated to the Middle Palaeolithic, by including the more recent punch and pressure blade technology our results dispel the notion that the transition to the Upper Palaeolithic was accompanied by an increase in efficiency. However, further increases in cutting edge efficiency are evident, with pressure blades possessing the highest efficiency in this study, indicating that late/epi-Palaeolithic and Neolithic blade technologies further increased efficiency. PMID:27936135

Incidence, populations and diversity of fungi from raw materials, final products and air of processing environment of multigrain whole meal bread.

PubMed

Santos, Juliana Lane Paixão Dos; Bernardi, Angélica Olivier; Pozza Morassi, Letícia L; Silva, Beatriz S; Copetti, Marina Venturini; S Sant'Ana, Anderson

2016-09-01

This study aimed to assess the incidence, to quantify and to assess the diversity of fungi in a multigrain whole meal bread processing plant. Two hundred and eight one (n=281) samples were analyzed, including raw materials (n=120), air samples (n=136) and multigrain breads (n=25). Among the raw materials, the whole corn flour showed the highest counts of fungi (4.8logCFU/g), followed by whole-wheat flour (3.1logCFU/g). The counts of fungi in the air of processing environment were higher in post-baking steps (oven output, cooling, slicing, packaging) than in pre-baking steps (weighing and mixer) (p<0.05). Species of fungi isolated from spoiled bread samples stored at 5, 20, 25 and 30, and 40°C corresponded mostly to Penicillium paneum and Penicillium polonicum isolated from 20 and 24% of samples, respectively. These species were also isolated from raw materials (P. paneum and P. polonicum) and air collected at different processing sampling points (P. polonicum). The high counts of filamentous fungi in raw materials and air samples in processing steps such as cooling, slicing, and packaging, suggest that contamination that may occur in these steps can be critical for the shelf life of breads. The results of this study highlight that the prevention of contamination of breads by fungal spores is still a challenge for bakery industries and that other strategies such as control of germination and growth of spoilage fungi through the development of more stable formulations have to be developed. Copyright © 2016 Elsevier Ltd. All rights reserved.

Identifying Major Transitions in the Evolution of Lithic Cutting Edge Production Rates.

PubMed

Muller, Antoine; Clarkson, Chris

2016-01-01

The notion that the evolution of core reduction strategies involved increasing efficiency in cutting edge production is prevalent in narratives of hominin technological evolution. Yet a number of studies comparing two different knapping technologies have found no significant differences in edge production. Using digital analysis methods we present an investigation of raw material efficiency in eight core technologies broadly representative of the long-term evolution of lithic technology. These are bipolar, multiplatform, discoidal, biface, Levallois, prismatic blade, punch blade and pressure blade production. Raw material efficiency is assessed by the ratio of cutting edge length to original core mass. We also examine which flake attributes contribute to maximising raw material efficiency, as well as compare the difference between expert and intermediate knappers in terms of cutting edge produced per gram of core. We identify a gradual increase in raw material efficiency over the broad sweep of lithic technological evolution. The results indicate that the most significant transition in efficiency likely took place with the introduction of small foliate biface, Levallois and prismatic blade knapping, all introduced in the Middle Stone Age / Middle Palaeolithic among early Homo sapiens and Neanderthals. This suggests that no difference in raw material efficiency existed between these species. With prismatic blade technology securely dated to the Middle Palaeolithic, by including the more recent punch and pressure blade technology our results dispel the notion that the transition to the Upper Palaeolithic was accompanied by an increase in efficiency. However, further increases in cutting edge efficiency are evident, with pressure blades possessing the highest efficiency in this study, indicating that late/epi-Palaeolithic and Neolithic blade technologies further increased efficiency.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Boussaa, S. Anas, E-mail: sabiha.anas@gmail.com; Kheloufi, A.; Kefaifi, A.

Raw materials are essential for the functioning of modern societies, and access to these raw materials is vital to the world economy. Sustainable development, both globally level, raises important new challenges associated with access and efficient use of raw materials. High purity quartz, is consider as a critical raw material and it is a rare commodity that only forms under geological conditions where a narrow set of chemical and physical parameters is fulfilled. When identified and following special beneficiation techniques, high purity quartz obtains very attractive prices and is applied in high technology sectors that currently are under rapid expansionmore » such as photovoltaic solar cells, silicon metal - oxide wafers in the semiconductor industry and long distance optical fibers that are used in communication networks. Crystalline silicon remains the principal material for photovoltaic technology. Metallurgical silicon is produced industrially by the reduction of silica with carbon in an electric arc furnace at temperatures higher than 2000 °C in the hottest parts, by a reaction that can be written ideally as: SiO{sub 2} + 2C = Si + 2CO. The aim of this study has been to test experimental methods for investigating the various physical and chemical proprieties of Hoggar quartz with different techniques: X Ray Fluorescence, infra-red spectroscopy, Scanning Electron Microscopy, Optic Microscopy, Carbon Analyzer and Vickers Hardness. The results show finally that the quartz has got good result in purity but need enrichment for the photovoltaic application.« less

Quarry waste management and recovery: first results connected to Carrara marble ravaneti (Italy)

NASA Astrophysics Data System (ADS)

Antonella Dino, Giovanna; Chiappino, Claudia; Rossetti, Piergiorgio

2017-04-01

Quarry waste (QW) represents a huge economic and environmental issue, due to loss of resources and to economic and environmental costs connected to waste management and landfilling activities. In many cases, valuable Raw Materials (RM) and Secondary Raw Materials (SRM) can be supplied by enhancing the QW recovery. In Italy large amounts of QW have been and still are dumped: such materials, if their quality (chemical, mineralogical, physical characteristics) and quantity are adequate, and if the impacts connected to their management are positive, can represent a valuable resource for SRM exploitation. Several dimension stone quarries have been and are interested by researches as for QW exploitation. Some researches show positive results, which are the basis for QW recovery (both from waste streams and from quarry dumps exploitation): a noticeable example is represented by Carrara marble waste. The Carrara quarry basin is characterized by ca. one hundred quarries for colored and white marble exploitation. The waste production can be summarized in: 80 Mm3 waste present in old quarry dumps (Ravaneti) and 3 Mm3/y of waste stream from quarrying activities. At present only 0.5 Mm3/y of QW is exploited for SRM production, causing a huge loss of resource. This has been the background for a preliminary research, on Carrara marble Ravaneti characterization, which was carried out thanks to the close cooperation between University of Torino, Società Apuana Marmi srl, and SET srl. In 2015, two QW dumping areas, Calocara and Lorano, were selected as representative for sampling activities. Three main sample categories were individuated based on granulometry (0.5-4 mm, 0-25 mm, 0-150 mm) to be characterized (size distribution, density, Atterberg limits, Los Angeles test, freezing and heat tests, flat and shape indexes, geochemistry, mineralogy). The results obtained are promising: the physical characterization shows an attitude for Carrara QW to be recovered as crushed materials for embankments and armour stone. Furthermore, the mineralogical and geochemical analyses show that these materials, being composed of nearly pure CaCO3, could find a proper application in high value products, as filler for paper, rubber, paint, plastic, etc. These data need to be confirmed by other analyses, thus a systematic characterization of QW present in the different quarry dumps is going to be programmed. R&D is strategic to solve problems connected to QW and landscape management. The cooperation between private Companies, Research Centers and Local Authorities is fundamental to reach the target, in terms of experimentation of new products (for civil works and infrastructure, building industry, agronomy, high-tech, etc.). Furthermore, if the stone industry aims at guaranteeing the systematic and convenient SRM recovery from QW, a change in exploitation and working activities has to be planned (eg. selection of the potential SRMs; dedicated stock areas for selected SRM; proper treatments depending on the kinds of reuse; treatment-activity protocols to produce each new product, etc.).

Performance and Characterization of Geopolymer Concrete Reinforced with Short Steel Fiber

NASA Astrophysics Data System (ADS)

Abdullah, M. M. A. B.; Faris, M. A.; Tahir, M. F. M.; Kadir, A. A.; Sandu, A. V.; Mat Isa, N. A. A.; Corbu, O.

2017-06-01

In the recent years, geopolymer concrete are reporting as the greener construction technology compared to conventional concrete that made up of ordinary Portland cement. Geopolymer concrete is an innovative construction material that utilized fly ash as one of waste material in coal combustion industry as a replacement for ordinary Portland cement in concrete. The uses of fly ash could reduce the carbon dioxide emission to the atmosphere, redundant of fly ash waste and costs compared to ordinary Portland cement concrete. However, the plain geopolymer concrete suffers from numerous drawbacks such as brittleness and low durability. Thus, in this study the addition of steel fiber is introduced in plain geopolymer concrete to improve its mechanical properties especially in compressive and flexural strength. Characterization of raw materials also determined by using chemical composition analysis. Short type of steel fiber is added to the mix in weight percent of 1 wt%, 3 wt%, 5 wt% and 7 wt% with fixed molarity of sodium hydroxide of 12M and solid to liquid ratio as 2.0. The addition of steel fiber showed the excellent improvement in the mechanical properties of geopolymer concrete that are determined by various methods available in the literature and compared with each other.

The effects of fabric type, fabric width and model type on the cost of unit raw material in terms of apparel

NASA Astrophysics Data System (ADS)

Bilgiç, H.; Duru Baykal, P.

2017-10-01

The cost of the fabric which is the raw material of apparel constitutes approximately the half of the total product cost. So, it is highly important that the fabric should be used with the greatest productivity. Cost analysis are of great importance in terms of competitiveness of readymade clothing and apparel sector both in national and international markets. The proximity of costs to international average and the average cost of the countries that are competitors of Turkey in clothing market is essential for Turkey to sustain its effect in textile sector. In the contrary case, the sector won’t be able to maintain its competitive capacity sustainably [1].The main cost elements of textile and apparel sector consist of raw material, labor, energy and financing [2].

Determination of Chondroitin Sulfate Content in Raw Materials and Dietary Supplements by High-Performance Liquid Chromatography with UV Detection After Enzymatic Hydrolysis: Single-Laboratory Validation First Action 2015.11.

PubMed

Brunelle, Sharon L

2016-01-01

A previously validated method for determination of chondroitin sulfate in raw materials and dietary supplements was submitted to the AOAC Expert Review Panel (ERP) for Stakeholder Panel on Dietary Supplements Set 1 Ingredients (Anthocyanins, Chondroitin, and PDE5 Inhibitors) for consideration of First Action Official Methods(SM) status. The ERP evaluated the single-laboratory validation results against AOAC Standard Method Performance Requirements 2014.009. With recoveries of 100.8-101.6% in raw materials and 105.4-105.8% in finished products and precision of 0.25-1.8% RSDr within-day and 1.6-4.72% RSDr overall, the ERP adopted the method for First Action Official Methods status and provided recommendations for achieving Final Action status.

Measurement of the isotope ratio of acetic acid in vinegar by HS-SPME-GC-TC/C-IRMS.

PubMed

Hattori, Ryota; Yamada, Keita; Shibata, Hiroki; Hirano, Satoshi; Tajima, Osamu; Yoshida, Naohiro

2010-06-23

Acetic acid is the main ingredient of vinegar, and the worth of vinegar often depends on the fermentation of raw materials. In this study, we have developed a simple and rapid method for discriminating the fermentation of the raw materials of vinegar by measuring the hydrogen and carbon isotope ratio of acetic acid using head space solid-phase microextraction (HS-SPME) combined with gas chromatography-high temperature conversion or combustion-isotope ratio mass spectrometry (GC-TC/C-IRMS). The measurement of acetic acid in vinegar by this method was possible with repeatabilities (1sigma) of +/-5.0 per thousand for hydrogen and +/-0.4 per thousand for carbon, which are sufficient to discriminate the origin of acetic acid. The fermentation of raw materials of several vinegars was evaluated by this method.

Characterisation and classification of solid wastes coming from reductive acid leaching of low-grade manganiferous ore.

PubMed

De Michelis, Ida; Ferella, Francesco; Beolchini, Francesca; Olivieri, Agostino; Vegliò, Francesco

2009-03-15

The present work was focused on the acid leaching process for manganese extraction in reducing environment to low-grade manganiferous ore that comes from Central Italy. The aim of this study was to establish optimum leaching operating conditions to reduce treatment costs of waste or, even better, to allow a waste valorisation as raw materials for other applications. Consequently, the main focus of the work was the characterization and classification of the solid wastes coming from the process carried out at different operating conditions; at the same moment the effect of process parameters on Mn extraction was also analysed. The effect of particles size on the manganese extraction in reductive acid leaching process was investigated, by using lactose as reducing agent. Particle size did not show a large influence on the Mn extraction yields in the investigated process conditions. This aspect suggests the use of the leaching waste for civil and/or environmental application: use of leaching solid wastes like filling material is to be applied, for example, for environmental restoration. The classification of the solid wastes, according to the Italian Laws about Release Test (RT), has demonstrated that the solid waste produced by leaching can be classifiable as "hazardous special waste". An improvement of solid washing let to reduce the SO(4)(2-) and an appropriate treatment is necessary to reduce the dangerousness of these solids. Possible application of ore and waste as raw materials in the ceramic industry was demonstrated not to be feasible.

Physico-chemical characterization of mortars as a tool in studying specific hydraulic components: application to the study of ancient Naxos aqueduct

NASA Astrophysics Data System (ADS)

Maravelaki-Kalaitzaki, P.; Galanos, A.; Doganis, I.; Kallithrakas-Kontos, N.

2011-07-01

Mortars and plasters from the ancient aqueduct on the island of Naxos, Greece, were studied with regard to mineralogical and chemical composition, grain size distribution, raw materials and hydraulic properties, in order to assess their characteristics and design compatible repair mortars. The authentic materials contained lime, crushed-brick, siliceous and calcitic aggregates, in different proportions according to mortar type. Crushed-bricks fired at low temperatures and lightweight volcanic aggregates contained amorphous phases, which upon reaction with lime yielded hydraulic components capable of protecting the construction from the continuous presence of water. Hydraulic calcium silicate/aluminate hydrates, the proportions and the perfect packing of the raw materials, along with the diligent application justify the longevity and durability of the studied samples. The hydraulic properties of samples were pointed out through (a) the well-established CO2/H2O ratio derived from the thermogravimetric analysis and (b) by introducing two powerful indices issued from the chemical analysis, namely CaOhydr and soluble SiO2 hydr. These indices improved the clustering of hydraulic mortars and provided better correlation between mortars, plasters and their binders. By comparing grain size distribution and hydraulicity indices it was possible to distinguish among the construction phases. Based on this study, repair mortars were formulated by hydraulic lime, siliceous sand, calcareous and crushed-brick aggregates, with the optimal water content, ensuring optimum workability and compatible appearance with the authentic ones.

Deterioration of expanded polystyrene caused by Aureobasidium pullulans var. melanogenum.

PubMed

Castiglia, Valeria C; Kuhar, Francisco

2015-01-01

An expanded-polystyrene factory located in northern Buenos Aires reported unusual dark spots causing esthetic damage in their production. A fungal strain forming black-olive colonies on extract malt agar medium was isolated from the damaged material and identified as Aureobasidium pullullans var. melanogenum. This fungus is particularly known for its capacity to produce hydrolytic enzymes and a biodegradable extracellular polysaccharide known as pullulan, which is used in the manufacture of packaging material for food and medicine. Laboratory tests were conducted to characterize its growth parameters. It was found that the organism was resistant to a wide range of pHs but did not survive at temperatures over 65°C. The proposed action plan includes drying of the material prior to packaging and disinfection of the machinery used in the manufacturing process and of the silos used for raw material storage. Copyright © 2014 Asociación Argentina de Microbiología. Publicado por Elsevier España, S.L.U. All rights reserved.

Hemp as an Agricultural Commodity

DTIC Science & Technology

2014-02-14

yarns and raw or processed spun fibers, paper, carpeting, home furnishings, construction and insulation materials, auto parts, and composites. The...interior stalk (hurd) is used in various applications such as animal bedding, raw material inputs, low-quality papers, and composites. Hemp seed and...oilcake are used in a range of foods and beverages, and can be an alternative food protein source. Oil from the crushed hemp seed is an ingredient in a

VIEW IN OPPOSITE DIRECTION AS MD1351 AND MD1352. RAW MATERIAL ...

Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

VIEW IN OPPOSITE DIRECTION AS MD-135-1 AND MD-135-2. RAW MATERIAL CONVEYOR AT LEFT DEPOSITS SHELL INTO MILLING MACHINE AT LOWER LEFT. ENGINE IS AT LOWER RIGHT AND RADIATOR AT LOWER CENTER. ROLLER SORTER IS AT TOP OF CONVEYOR. - F. & H. Benning Company Oyster Mill, 14430 Solomons Island Road (moved from 1014 Benning Road, Galesville, Anne Arundel County, Maryland), Solomons, Calvert County, MD

Behavior or Nonmetallic Materials in Shale Oil Derived Jet Fuels and in High Aromatic and High Sulfur Petroleum Fuels

DTIC Science & Technology

1978-07-01

degrades thermal stability and forms undesirable sulfur dioxide emissions . Although the original premises for controlling total sulfur may not still...eliminate corrosive trace contamination, presence of surfactants which deactivate filter/ separators, carry-over of refinery processing materials, and...increase raw vapor emissions from ground fuel handling facilities and during refueling operations. Controlling raw vapor emissions is difficult at 3

Coal gasification systems engineering and analysis. Appendix A: Coal gasification catalog

NASA Technical Reports Server (NTRS)

1980-01-01

The scope of work in preparing the Coal Gasification Data Catalog included the following subtasks: (1) candidate system subsystem definition, (2) raw materials analysis, (3) market analysis for by-products, (4) alternate products analysis, (5) preliminary integrated facility requirements. Definition of candidate systems/subsystems includes the identity of and alternates for each process unit, raw material requirements, and the cost and design drivers for each process design.

Determination of platinum in mineral raw materials by switching chronoamperometry

NASA Astrophysics Data System (ADS)

Pakrieva, E.; Oskina, Y.; Ustinova, E.

2014-08-01

The technique of platinum (IV) determination in mineral raw materials with the application of switching chronoamperometry has been offered. The graphite electrode impregnated with polyethylene was used as the working electrode. The hydrolytic precipitation method with 3% NaOH solution has been developed to separate platinum from the sample matrix. The use of switching chronoamperometry applied to the assessment of the platinum content in geological objects has been demonstrated.

The Enhanced Red Emission and Improved Thermal Stability of CaAlSiN3:Eu2+ Phosphors by Using Nano-EuB6 as Raw Material

PubMed Central

Liu, Wen-Quan; Wu, Dan; Chang, Hugejile; Duan, Ru-Xia; Wu, Wen-Jie; Amu, Guleng; Bao, Fu-Quan; Tegus, Ojiyed

2018-01-01

Synthesizing phosphors with high performance is still a necessary work for phosphor-converted white light-emitting diodes (W-LEDs). In this paper, three series of CaAlSiN3:Eu2+ (denoted as CASN:Eu2+) phosphors using Eu2O3, EuN and EuB6 as raw materials respectively are fabricated by under the alloy precursor normal pressure nitridation synthesis condition. We demonstrate that CASN:Eu2+ using nano-EuB6 as raw material shows higher emission intensity than others, which is ascribed to the increment of Eu2+ ionic content entering into the crystal lattice. An improved thermal stability can also be obtained by using nano-EuB6 due to the structurally stable status, which is assigned to the partial substitution of Eu–O (Eu–N) bonds by more covalent Eu–B ones that leads to a higher structural rigidity. In addition, the W-LEDs lamp was fabricated to explore its possible application in W-LEDs based on blue LEDs. Our results indicate that using EuB6 as raw materials can provide an effective way of enhancing the red emission and improving the thermal stability of the CASN:Eu2+ red phosphor. PMID:29370148

Provenance study of ancient Chinese Yaozhou porcelain by neutron activation analysis

NASA Astrophysics Data System (ADS)

Li, G. X.; Y Gao, Z.; Li, R. W.; Zhao, W. J.; Xie, J. Z.; Feng, S. L.; Zhuo, Z. X.; Y Fan, D.; Zhang, Y.; Cai, Z. F.; Liu, H.

2003-09-01

This paper reports our study of the provenance of ancient Chinese Yaozhou porcelain. The content of 29 elements in the Yaozhou porcelain samples was measured by neutron activation analysis (NAA). The NAA data were further analysed using fuzzy cluster analysis to obtain the trend fuzzy cluster diagrams. These samples with different glaze colour, ranging over more than 700 years, were fired in different kilns. Our analysis indicates the relatively concentrated distribution of the sources of the raw material for the Yaozhou porcelain body samples. They can be classified into two independent periods, i.e. the Tang (AD 618-907) and the Five Dynasties (AD 907-960) period, and the Song (AD 960-1279) and Jin (AD 1115-1234) period. Our analysis also indicates that the sources of the raw material for the ancient Yaozhou porcelain glaze samples are quite scattered and those for the black glaze in the Tang Dynasty are very concentrated. The sources of the raw material for the celadon glaze and the white glaze in the Tang Dynasty are widely distributed and those for the celadon glaze in the Song Dynasty are close to those of the bluish white glaze in the Jin Dynasty, and they are very concentrated. The sources of the raw material for the porcelain glazes cover those of the porcelain bodies.

Greenhouse Gas Emissions from Asphalt Pavement Construction: A Case Study in China

PubMed Central

Ma, Feng; Sha, Aimin; Lin, Ruiyu; Huang, Yue; Wang, Chao

2016-01-01

In China, the construction of asphalt pavement has a significant impact on the environment, and energy use and greenhouse gas (GHG) emissions from asphalt pavement construction have been receiving increasing attention in recent years. At present, there is no universal criterion for the evaluation of GHG emissions in asphalt pavement construction. This paper proposes to define the system boundaries for GHG emissions from asphalt pavement by using a process-based life cycle assessment method. A method for evaluating GHG emissions from asphalt pavement construction is suggested. The paper reports a case study of GHG emissions from a typical asphalt pavement construction project in China. The results show that the greenhouse gas emissions from the mixture mixing phase are the highest, and account for about 54% of the total amount. The second highest GHG emission phase is the production of raw materials. For GHG emissions of cement stabilized base/subbase, the production of raw materials emits the most, about 98%. The GHG emission for cement production alone is about 92%. The results indicate that any measures to reduce GHG emissions from asphalt pavement construction should be focused on the raw materials manufacturing stage. If the raw materials production phase is excluded, the measures to reduce GHG emissions should be aimed at the mixture mixing phase. PMID:27011196

Greenhouse Gas Emissions from Asphalt Pavement Construction: A Case Study in China.

PubMed

Ma, Feng; Sha, Aimin; Lin, Ruiyu; Huang, Yue; Wang, Chao

2016-03-22

In China, the construction of asphalt pavement has a significant impact on the environment, and energy use and greenhouse gas (GHG) emissions from asphalt pavement construction have been receiving increasing attention in recent years. At present, there is no universal criterion for the evaluation of GHG emissions in asphalt pavement construction. This paper proposes to define the system boundaries for GHG emissions from asphalt pavement by using a process-based life cycle assessment method. A method for evaluating GHG emissions from asphalt pavement construction is suggested. The paper reports a case study of GHG emissions from a typical asphalt pavement construction project in China. The results show that the greenhouse gas emissions from the mixture mixing phase are the highest, and account for about 54% of the total amount. The second highest GHG emission phase is the production of raw materials. For GHG emissions of cement stabilized base/subbase, the production of raw materials emits the most, about 98%. The GHG emission for cement production alone is about 92%. The results indicate that any measures to reduce GHG emissions from asphalt pavement construction should be focused on the raw materials manufacturing stage. If the raw materials production phase is excluded, the measures to reduce GHG emissions should be aimed at the mixture mixing phase.

76 FR 35239 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2011-06-16

... (9040) II Raw Opium (9600) II Poppy Straw (9650) II Concentrate of Poppy Straw (9670) II The company... narcotic raw material are not appropriate. As noted in a previous notice published in the Federal Register...

76 FR 25374 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2011-05-04

...), comments and requests for hearings on applications to import narcotic raw material are not appropriate. As... Schedule Raw Opium (9600) I Concentrate of Poppy Straw (9670) II The company plans to import the listed...

77 FR 19717 - Importer of Controlled Substances; Notice of Registration Mallinckrodt LLC

Federal Register 2010, 2011, 2012, 2013, 2014

2012-04-02

... raw material are not appropriate, 72 FR 3417 (2007). Regarding all other basic classes of controlled...) II Opium, raw (9600) II Poppy Straw Concentrate (9670) II The company plans to import the listed...

75 FR 36680 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2010-06-28

... requests for hearings on applications to import narcotic raw material are not appropriate. As noted in a... as an importer of the basic classes of controlled substances listed in schedule II: Drug Schedule Raw...

75 FR 22844 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2010-04-30

... narcotic raw material are not appropriate. As noted in a previous notice published in the Federal Register... Coca Leaves (9040) II Raw Opium (9600) II Poppy Straw (9650) II Concentrate of Poppy Straw (9670) II...

77 FR 24984 - Importer of Controlled Substances; Notice of Application; Rhodes Technologies

Federal Register 2010, 2011, 2012, 2013, 2014

2012-04-26

.... Comments and requests for hearings on applications to import narcotic raw material are not appropriate. 72... schedule II: Drug Schedule Opium, Raw (9600) II Poppy Straw Concentrate (9670) II The company plans to...

75 FR 53718 - Importer of Controlled Substances; Notice of Application

Federal Register 2010, 2011, 2012, 2013, 2014

2010-09-01

... 3417 (2007), comments and requests for hearings on applications to import narcotic raw material are not... Opium, raw (9600) II Poppy Straw Concentrate (9670) II The company plans to import the basic classes of...

78 FR 12101 - Importer of Controlled Substances; Notice of Application; Mallinckrodt, LLC.

Federal Register 2010, 2011, 2012, 2013, 2014

2013-02-21

... Coca Leaves (9040) II Opium, raw (9600) II Poppy Straw Concentrate (9670) II The company plans to... or coca leaves. Comments and requests for hearings on applications to import narcotic raw material...

Materials and manufacturing processes for increased life/reliability. [of turbine wheels

NASA Technical Reports Server (NTRS)

Duttweiler, R. E.

1977-01-01

Improvements in both quality and durability of disk raw material for both military and commercial engines necessitated an entirely new concept in raw material process control which imposes careful selection, screening and sampling of the basic alloy ingredients, followed by careful monitoring of the melting parameters in all phases of the vacuum melting sequence. Special care is taken to preclude solidification conditions that produce adverse levels of segregation. Melt furnaces are routinely cleaned and inspected for contamination. Ingots are also cleaned and inspected before entering the final melt step.

Use of SRIM and Garfield with Geant4 for the characterization of a hybrid 10B/3He neutron detector

NASA Astrophysics Data System (ADS)

van der Ende, B. M.; Rand, E. T.; Erlandson, A.; Li, L.

2018-06-01

This paper describes a method for more complete neutron detector characterization using Geant4's Monte Carlo methods for characterizing overall detector response rate and Garfield interfaced with SRIM for the simulation of the detector's raw pulses, as applied to a hybrid 10B/3He detector. The Geant4 models characterizing the detector's interaction with a 252Cf point source and parallel beams of mono-energetic neutrons (assuming ISO 8529 reference energy values) compare and agree well with calibrated 252Cf measurements to within 6.4%. Validated Geant4 model outputs serve as input to Garfield+SRIM calculations to provide meaningful pulse height spectra. Modifications to Garfield for this work were necessary to account for simultaneous tracking of electrons resulting from proton and triton reaction products from a single 3He neutron capture event, and it was further necessary to interface Garfield with the energy loss, range, and straggling calculations provided by SRIM. Individual raw pulses generated by Garfield+SRIM are also observed to agree well with experimentally measured raw pulses from the detector.

Exopolysaccharide production from Sclerotium glucanicum NRRL 3006 and Botryosphaeria rhodina DABAC-P82 on raw and hydrolysed starchy materials.

PubMed

Selbmann, L; Crognale, S; Petruccioli, M

2002-01-01

Evaluation of fermentative usage of raw starchy materials for exopolysaccharide (EPS) production by Sclerotium glucanicum NRRL 3006 and Botryosphaeria rhodina DABAC-P82. Non-hydrolysed corn starch, soft wheat flour, potato flour, cassava flour, sweet and industrial potato flours, and corn starch hydrolysed to different dextrose equivalent (DE) were tested in shaken culture for EPS production. Both fungal strains produced EPS on all tested materials but the production was maximum on hydrolysed corn starch (30.5 and 19.8 g l(-1) by B. rhodina and S. glucanicum on corn starch at 100 and 62 DE, respectively). Raw starchy materials as such and, in particular, partially or totally hydrolysed corn starch could be used profitably for EPS production by S. glucanicum and B. rhodina. The excellent EPS production, productivity and yield of B. rhodina DABAC-P82 when grown on 60 g l(-1) of totally hydrolysed corn starch.

A small scale lunar launcher for early lunar material utilization

NASA Technical Reports Server (NTRS)

Snow, W. R.; Kubby, J. A.; Dunbar, R. S.

1981-01-01

A system for the launching of lunar derived oxygen or raw materials into low lunar orbit or to L2 for transfer to low earth orbit is presented. The system described is a greatly simplified version of the conventional and sophisticated approach suggested by O'Neill using mass drivers with recirculating buckets. An electromagnetic accelerator is located on the lunar surface which launches 125 kg 'smart' containers of liquid oxygen or raw materials into a transfer orbit. Upon reaching apolune a kick motor is fired to circularize the orbit at 100 km altitude or L2. These containers are collected and their payloads transferred to a tanker OTV. The empty containers then have their kick motors refurbished and then are returned to the launcher site on the lunar surface for reuse. Initial launch capability is designed for about 500T of liquid oxygen delivered to low earth orbit per year with upgrading to higher levels, delivery of lunar soil for shielding, or raw materials for processing given the demand.

Lime kiln dust as a potential raw material in portland cement manufacturing

USGS Publications Warehouse

Miller, M. Michael; Callaghan, Robert M.

2004-01-01

In the United States, the manufacture of portland cement involves burning in a rotary kiln a finely ground proportional mix of raw materials. The raw material mix provides the required chemical combination of calcium, silicon, aluminum, iron, and small amounts of other ingredients. The majority of calcium is supplied in the form of calcium carbonate usually from limestone. Other sources including waste materials or byproducts from other industries can be used to supply calcium (or lime, CaO), provided they have sufficiently high CaO content, have low magnesia content (less than 5 percent), and are competitive with limestone in terms of cost and adequacy of supply. In the United States, the lime industry produces large amounts of lime kiln dust (LKD), which is collected by dust control systems. This LKD may be a supplemental source of calcium for cement plants, if the lime and cement plants are located near enough to each other to make the arrangement economical.

Deformation of metal brackets: a comparative study.

PubMed

Flores, D A; Choi, L K; Caruso, J M; Tomlinson, J L; Scott, G E; Jeiroudi, M T

1994-01-01

The purpose of this study was to determine the effect of material and design on the force and stress required to permanently deform metal brackets. Fourteen types of metal brackets were categorized according to raw material composition, slot torque degree, and wing type. Five types of raw materials, three types of slot torque degree, and four types of wing design were tested using an archwire torque test developed by Flores. An analysis of variance (ANOVA) and t-test showed that all three categories had a significant effect on the force and stress needed to permanently deform metal brackets. Of the three, raw material had the greatest effect on the amount of force. Results showed that 17-4PH and 303S had higher yield strengths and regular twin brackets had higher resistance to deformation. Also, as slot torque degree increased, brackets deformed with less force. Result confirmed that brackets requiring the greatest stress to permanently deform were made of steel with the greatest hardness.

Device fabrication, characterization, and thermal neutron detection response of LiZnP and LiZnAs semiconductor devices

NASA Astrophysics Data System (ADS)

Montag, Benjamin W.; Ugorowski, Philip B.; Nelson, Kyle A.; Edwards, Nathaniel S.; McGregor, Douglas S.

2016-11-01

Nowotny-Juza compounds continue to be explored as candidates for solid-state neutron detectors. Such a device would have greater efficiency, in a compact form, than present day gas-filled 3He and 10BF3 detectors. The 6Li(n,t)4He reaction yields a total Q-value of 4.78 MeV, larger than 10B, an energy easily identified above background radiations. Hence, devices fabricated from semiconductor compounds having either natural Li (nominally 7.5% 6Li) or enriched 6Li (usually 95% 6Li) as constituent atoms may provide a material for compact high efficiency neutron detectors. Starting material was synthesized by preparing equimolar portions of Li, Zn, and As sealed under vacuum (10-6 Torr) in quartz ampoules lined with boron nitride and subsequently reacted in a compounding furnace [1]. The raw synthesized material indicated the presence high impurity levels (material and electrical property characterizations). A static vacuum sublimation in quartz was performed to help purify the synthesized material [2,3]. Bulk crystalline samples were grown from the purified material [4,5]. Samples were cut using a diamond wire saw, and processed into devices. Bulk resistivity was determined from I-V curve measurements, ranging from 106-1011 Ω cm. Devices were characterized for sensitivity to 5.48 MeV alpha particles, 337 nm laser light, and neutron sensitivity in a thermal neutron diffracted beam at the Kansas State University TRIGA Mark II nuclear reactor. Thermal neutron reaction product charge induction was measured with a LiZnP device, and the reaction product spectral response was observed.

Development of material formula and structure property indicators for low cold-resistant characterization of Cables’ Material

NASA Astrophysics Data System (ADS)

Sun, W.; Cai, Y. G.; Feng, Y. M.; Li, Y. L.; Zhou, H. Y.; Zhou, Y.

2018-01-01

Alpine regions account for about 27.9% of total land area in China. Northeast China, Inner Mongolia, Northwest China and other regions are located in alpine regions, wherein the above regions are rich in energy. However, the low-temperature impact embrittlement temperature of traditional PVC cable materials is between -15°C and -20°C, which is far lower than actual operation requirements. Cable insulation and sheath are always damaged during cable laying in alpine regions. Therefore, it is urgent to develop low-temperature-resistant cables applicable to low-temperature environment in alpine regions, and safe and stable operation of power grids in the alpine regions can be guaranteed. In the paper, cold-resistant PVC formula systems were mainly trial-manufactured and studied. Appropriate production technologies and formulas were determined through selecting raw materials and modified materials. The low-temperature impact embrittlement temperature was adjusted below -50°C under the precondition that PVC cable materials met national standard property requirements. Cold-resistant PVC cable materials were prepared, which were characterized by excellent physical and mechanical properties, and sound extrusion process, and cold-resistant PVC cable materials can meet production requirements of low-temperature-resistant cables. Meanwhile, the prepared cold-resistant cable material was used for extruding finished product cables and trial-manufacturing sample cables. Type tests of low temperature elongation ratio, 15min withstand voltage, etc. were completed for 35kV and lower sample cables in Mohe Low-temperature Test Site. All properties were consistent with standard requirements.

Prospects of rice straw as a raw material for paper making.

PubMed

Kaur, Daljeet; Bhardwaj, Nishi Kant; Lohchab, Rajesh Kumar

2017-02-01

Pulp and paper mills are indispensable for any nation as far as the growth of the nation is concerned. Due to fast growth in population, urbanization and industrialization, the demand and consumption of paper has increased tremendously. These put high load on our natural resources and force the industry to look for alternative raw material. Rice straw is a lignocellulosic material abundantly available in wood short countries like China, India, Bangladesh, etc. and can be used as raw material for this industry. Open burning of rice straw releases noxious green house gases to the air and poses serious threats to global air chemistry and human health. So, it is a dual benefit option (for farmers and industries) to use rice straw as a raw material in pulp and paper industry. Organosolv pulping using acids are the prominent choices of researchers to convert this residue into valuable pulp but in developed countries only. Developing world favours the soda and soda-AQ processes as these are economical. As a virtue of less lignin content in comparison to wood, rice straw requires less harsh conditions for cooking and can be easily pulped. Bleaching is a crucial step of paper making but also responsible for causing water pollution. Many studies revealed that during the process more than 500 chlorinated compounds are released that are highly toxic, bioaccumulative and carcinogenic in nature. Most of the industries over the globe switch on to the elemental chlorine free short sequence bleaching methods using chlorine dioxide, hypochlorite and hydrogen peroxide. This paper presented the effective need of ecofriendly, economically reliable pulping and bleaching sequences in case of rice straw to eliminate the problems of chlorinated compounds in wastewater of paper mills. Such approach of using waste as a raw material with its environmentally safe processing for making paper can prove to be valuable towards sustainable growth. Copyright © 2016 Elsevier Ltd. All rights reserved.

ERA-MIN: The European network (ERA-NET) on non-energy raw materials

NASA Astrophysics Data System (ADS)

vidal, o.; christmann, p.; Bol, d.; Goffé, b.; Groth, m.; Kohler, e.; Persson Nelson, k.; Schumacher, k.

2012-04-01

Non-energy raw materials are vital for the EU's economy, and for the development of environmentally friendly technologies. The EU is the world's largest consumers of non-energy minerals, but it remains dependent on the importation of many metals, as its domestic production is limited to about 3% of world production. We will present the project ERA-MIN, which is an ERA-NET on the Industrial Handling of Raw Materials for European industries, financially supported by the European Commission. The main objectives of ERA-MIN are: 1) Mapping and Networking: interconnecting the members of the currently fragmented European mineral resources research area, to the aim of fostering convergence of public research programs, industry, research institutes, academia and the European Commission, 2) Coordinating: establishing a permanent mechanism for planning and coordination of the European non-energy mineral raw materials research community (ENERC). 3) Roadmapping: defining the most important scientific and technological challenges that should be supported by the EU and its state members, 4) Programming: designing a Joint European Research Programme model and implementating it into a call for proposals open to academic and industrial research. The topics of interest in ERA-MIN are the primary continental and marine resources, the secondary resources and their related technologies, substitution and material efficiency, along with transversal topics such as environmental impact, public policy support, mineral intelligence, and public education and teaching. Public scientific research is very central in the scope of the ERA-MIN activity, whose consortium is indeed lead by a public organisation of fundamental research. Thus, universities and public research organisations are warmly invited to play an active role in defining the scientific questions and challenges that shall determine the European Raw Materials Roadmap and should be addressed by joint programming at the European scale. The various levels of possible involvement in ERA-MIN for the interested stakeholders will be presented.

Textile-reinforced concrete using composite binder based on new types of mineral raw materials

NASA Astrophysics Data System (ADS)

Lesovik, V. S.; Glagolev, E. S.; Popov, D. Y.; Lesovik, G. A.; Ageeva, M. S.

2018-03-01

To determine the level of development of science, it is necessary to start with a particular stage in the development of society. At present, the purpose of building materials science is to create composites, which ensure safety of buildings and structures, including their protection against certain natural and man-made impacts. A new stage in construction materials science envisages the development of a technology for creating composites comfortable for a particular person. To implement this, a new paradigm for designing and synthesizing building materials with a new raw material base is needed. The optimization of the “human-material-habitat” system is a complex task, for the solution of which transdisciplinary approaches are required.

VERAM, for a sustainable and competitive future for EU Raw Materials

NASA Astrophysics Data System (ADS)

Mobili, A.; Tittarelli, F.; Revel, G. M.; Wall, P.

2018-03-01

The project, VERAM “Vision and Roadmap for European Raw Materials”, aims to deliver a mapping of on-going initiatives on non-food, non-energy raw materials (including metals, industrial minerals, aggregates and wood) at European, Member State, and regional levels both from the Research and Innovation (R&I), industry, and policy perspectives. Moreover, based on a comprehensive gap analysis, VERAM will propose a common long term 2050 Vision and Roadmap in coordination and cooperation with all stakeholders across the value chain. For the first time, two European Technology Platforms (ETPs) together with their corresponding European Research Area Networks (ERA-NETs) are joining forces to develop a common roadmap.

FROZEN RAW FOODS AS SKIN-TESTING MATERIALS—Further Studies of Use in Cases of Allergic Disorders

PubMed Central

Ancona, Giacomo R.; Schumacher, Irwin C.

1954-01-01

In further studies on the use of frozen raw food as skin-testing material in patients with allergic disorders, the results of previous work were confirmed in a greater number of subjects using a larger number of foods: Tests with frozen raw foods by the scratch method induce true positive reactions of a larger size and in greater frequency than the corresponding commercial extracts by either the scratch or the intracutaneous method. Storage in the frozen state for several years does not affect the antigenic potency of the materials. The frozen preparations have caused no harmful effects in the subjects, are free from irritant properties, and are not urticariogenic. PMID:13126823

Physical-Mechanical characterization of cosmetic formulations and correlation between instrumental measurements and sensorial properties.

PubMed

Calixto, L S; Maia Campos, P M B G

2017-10-01

The correct choice of raw materials in the development of cosmetic formulations is essential for obtaining stable and pleasant skin care products. Therefore, rheological, texture and sensory analyses are important to understand the behaviour and stability of the formulations. In this context, the aim of this study was to develop cosmetic formulations containing or not (vehicle) UV filters and chicory root extract, to evaluate their stability as well as to characterize their physical and texture properties and correlate them with the sensory attributes. Four formulations containing organic UV filters and chicory extract, each alone or in combination, were developed and evaluated for 180 days with a cone and plate rheometer, a texture analyzer and consumer's sensorial analysis. Thus, the data obtained were correlated to observe the different influences. The developed formulations remained stable after 180 days regarding macroscopic aspects, organoleptic characteristics and pH values. The addition of the UV filters alone and in combination with the active substance resulted in significant increases in rheology properties, viscosity and consistency. The formulation with the active ingredient showed significant decreases in the texture parameters after 180 days, mainly due to its polysaccharide inulin. All formulations obtained high scores in sensorial parameters. A strong correlation was mainly found between spreadability and work of shear, and between the texture parameters. The raw materials strongly influenced the physical, texture and sensorial parameters. Finally, the UV filters showed a greater influence on the results of the formulations than the chicory root extract. In conclusion, the association of the mentioned methods allows the correct choice of ingredients and their combinations. © 2017 Society of Cosmetic Scientists and the Société Française de Cosmétologie.

A novel raw starch digesting alpha-amylase from a newly isolated Bacillus sp. YX-1: purification and characterization.

PubMed

Liu, Xu Dong; Xu, Yan

2008-07-01

This study reports the purification and characterization of a novel raw starch digesting alpha-amylase from a newly isolated Bacillus sp. YX-1. Maximum alpha-amylase activity (53 U mL(-1)) was obtained at 45 degrees C after 44 h of incubation. The enzyme was purified using ammonium sulfate precipitation, ion exchange and gel filtration chromatography, and showed a molecular weight of 56 kDa by SDS-PAGE. This enzyme exhibited maximum activity at pH 5.0, performed stability over a broad range of pH 4.5-11.0, and was optimally active at 40-50 degrees C. The enzyme preparation had a strong digesting ability towards various raw starches and efficiently hydrolyzed raw corn starch at a concentration of 20% and pH 5.0, which were normally used in the starch industries, in a period of 12h. By analyzing its partial amino acid sequences, the enzyme was proposed to be a novel alpha-amylase.

Prevalence, isolation and characterization of Bacillus cereus strains from rice of local cultivators of Sabah, Sarawak, and Peninsular Malaysia

NASA Astrophysics Data System (ADS)

Sawei, Jelin; Sani, Norrakiah Abdullah

2016-11-01

Bacillus cereus is a spore-forming, facultative anaerobic, motile microorganism that has been identified as a causative agent of two types of gastrointestinal diseases such as emetic and diarrhea. This foodborne pathogen is found in both vegetative cells and endospores form in foods such as rice either raw or cooked. The aim of this study is to investigate and determine the prevalence, characterize and identify the isolation of vegetative cells and endospores of B. cereus in thirty varieties (n=3) of raw rice from Sabah, Sarawak and Peninsular Malaysia. A total of 90 (n=90) raw rice were examined and 84 (93.33%) samples were positive to vegetative cells of B. cereus. However, only 32 (35.56%) samples were positive for endospore cells that able to germinate after samples were heated at 75°C for 15 mins. The mean log cfu/g for vegetative cells were higher range (0.00 - 4.1533) than visible endospores (0.00 - 3.7533 mean log cfu/g). Sample of raw red rice (UKMRC9) had significantly higher contamination by both vegetative cells and endospores at p<0.05, than the other raw rice samples.

78 FR 19016 - Importer of Controlled Substances; Notice of Registration; Johnson Matthey, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2013-03-28

... Schedule Coca Leaves (9040) II Thebaine (9333) II Opium, raw (9600) II Noroxymorphone (9668) II Poppy Straw Concentrate (9670) II The company plans to import the listed controlled substances as raw materials, to be...

76 FR 51400 - Importer of Controlled Substances; Notice of Registration

Federal Register 2010, 2011, 2012, 2013, 2014

2011-08-18

... narcotic raw material are not appropriate. DEA has considered the factors in 21 U.S.C. 823(a) and 952(a... classes of controlled substances: Drug Schedule Raw Opium (9600) II Concentrate of Poppy Straw II (9670...

77 FR 55503 - Importer of Controlled Substances; Notice of Registration; Cambrex Charles City, Inc.

Federal Register 2010, 2011, 2012, 2013, 2014

2012-09-10

... hearings on applications to import narcotic raw material are not appropriate. 72 FR 3417 (2007). DEA has...-piperidine (8333).. II Phenylacetone (8501) II Opium, raw (9600) II Poppy Straw Concentrate (9670) II The...

78 FR 39337 - Importer of Controlled Substances; Notice Of Registration; Mallinckrodt, LLC.

Federal Register 2010, 2011, 2012, 2013, 2014

2013-07-01

... narcotic raw material are not appropriate, 72 FR 3417 (2007). Regarding Phenylacetone (8501), a basic class... Phenylacetone (8501) II Coca Leaves (9040) II Opium, raw (9600) II Poppy Straw Concentrate (9670) II The company...

78 FR 23594 - Importer of Controlled Substances; Notice of Application; Rhodes Technologies

Federal Register 2010, 2011, 2012, 2013, 2014

2013-04-19

... requests for hearings on applications to import narcotic raw material are not appropriate. 72 FR 3417 (2007... Schedule Opium, Raw (9600) II Poppy Straw Concentrate (9670) II The company plans to import the listed...

77 FR 24983 - Importer of Controlled Substances; Notice of Application Penick Corporation

Federal Register 2010, 2011, 2012, 2013, 2014

2012-04-26

... import narcotic raw material are not appropriate. 72 FR 3417(2007). As noted in a previous notice... Schedule Coca Leaves (9040) II Raw Opium (9600) II Poppy Straw (9650) II Concentrate of Poppy Straw (9670...

Rational preparation of waste coal mixture for production of bricks by the method of compression molding

NASA Astrophysics Data System (ADS)

Stolboushkin, A. Yu; Ivanov, A. I.; Temlyantsev, M. V.; Fomina, O. A.

2016-10-01

Rational preparation of the mixture containing technogenic raw material - waste coal for the production of wall ceramics is developed. It was established that the technology of high-quality ceramic bricks requires: grinding of raw materials to class 0.3 + 0 mm, its aggregation in the intensive mixers into granules 1-3 mm, compression molding of adobe to plastic deformation of granules, drying and firing.

Computer Vision Hardware System for Automating Rough Mills of Furniture Plants

Treesearch

Richard W. Conners; Chong T. Ng; Thomas H. Drayer; Joe G. Tront; D. Earl Kline; C.J. Gatchell

1990-01-01

The rough mill of a hardwood furniture or fixture plant is the place where dried lumber is cut into the rough parts that will be used in the rest of the manufacturing process. Approximately a third of the cost of operating the rough mill is the cost of the raw material. Hence any increase in the number of rough parts produced from a given volume of raw material can...

Increasing the Efficiency of the Recycling of Propylene—Polyethylene Raw Materials

NASA Astrophysics Data System (ADS)

Belokon', T. D.; Kurganova, Yu. A.; Bragin, D. A.; Kovalev, M. N.

2017-12-01

The problem of the recycling of plastic wastes is discussed. The polypropylene needs of the modern Russian market are analyzed. The necessity of recycling of plastic wastes is revealed, and its advantages over reclamation are substantiated. The problems of a real enterprise regarding the recycling of polypropylene—polyethylene raw materials for increasing the properties of the end product and optimizing its production are considered, and methods for their solution are proposed.

40 CFR 406.105 - Standards of performance for new sources.

Code of Federal Regulations, 2010 CFR

2010-07-01

...) EFFLUENT GUIDELINES AND STANDARDS GRAIN MILLS POINT SOURCE CATEGORY Wheat Starch and Gluten Subcategory... units (kg/kkg of raw material (wheat flour)) BOD5 3.0 1.0 TSS 3.0 1.0 pH (1) (1) English units (lb/1,000 lb of raw material (wheat flour)) BOD5 3.0 1.0 TSS 3.0 1.0 pH (1) (1) 1 Within the range 6.0 to 9.0. ...

Mitigating the risk of Zika virus contamination of raw materials and cell lines in the manufacture of biologicals.

PubMed

Zmurko, Joanna; Vasey, Douglas B; Donald, Claire L; Armstrong, Alison A; McKee, Marian L; Kohl, Alain; Clayton, Reginald F

2018-02-01

Ensuring the virological safety of biologicals is challenging due to the risk of viral contamination of raw materials and cell banks, and exposure during in-process handling to known and/or emerging viral pathogens. Viruses may contaminate raw materials and biologicals intended for human or veterinary use and remain undetected until appropriate testing measures are employed. The outbreak and expansive spread of the mosquito-borne flavivirus Zika virus (ZIKV) poses challenges to screening human- and animal -derived products used in the manufacture of biologicals. Here, we report the results of an in vitro study where detector cell lines were challenged with African and Asian lineages of ZIKV. We demonstrate that this pathogen is robustly detectable by in vitro assay, thereby providing assurance of detection of ZIKV, and in turn underpinning the robustness of in vitro virology assays in safety testing of biologicals.

A Technological Comparison of Six Processes for the Production of Reduction-Grade Alumina from Non-Bauxitic Raw Materials

NASA Astrophysics Data System (ADS)

Bengtson, K. B.

The U. S. Bureau of Mines, by means of a contract with Kaiser Engineers and with Kaiser Aluminum & Chemical Corporation as a subcontractor, has sponsored a technological and an economic evaluation of six candidate processes for the manufacture of alumina from certain U. S. raw materials other than bauxite. This paper describes each process. Flow diagrams and the total energy requirement for each process are included. Important characteristics affecting the economics of producing alumina by each process are discussed, and some presently unsolved technical problems are identified. The extraction of alumina from clay via hydrochloric acid with iron separation by solvent extraction, and the crystallization of intermediate AlCl3·6H2O through the introduction of HCl gas into the pregnant mother liquor, appears to be technically feasible and the most attractive of the six raw material/process combinations.

The effect of commercial processing on the paralytic shellfish poison (PSP) content of naturally-contaminated Acanthocardia tuberculatum L.

PubMed

Berenguer, J A; Gonzalez, L; Jimenez, I; Legarda, T M; Olmedo, J B; Burdaspal, P A

1993-01-01

A study was undertaken to determine if any reduction in contamination of Acanthocardia tuberculatum L. (Mediterranean cockle) by paralytic shellfish poisons (PSP) could be enhanced by operations carried out during the industrial canning process, allowing contaminated raw material to be commercially marketed in safe conditions for edible purposes. A general decrease in PSP levels was consistently observed when comparing raw materials and their corresponding final products, these dropping to acceptable levels. PSP levels were determined by mouse bioassay and a fluorometric method, and saxitoxin was determined by HPLC. The detoxifying effects averaged over 71.7% and 81.8% (mouse bioassay), 70.6% and 90.9% (fluorometric method), 77.9% and 83.5% (HPLC), for boiling and sterilizing operations respectively. The highest level detected in raw material was 800 micrograms/100 g by mouse bioassay.

Chemical and biotechnological processing of collagen-containing raw materials into functional components of feed suitable for production of high-quality meat from farm animals

NASA Astrophysics Data System (ADS)

Baburina, M. I.; Ivankin, A. N.; Stanovova, I. A.

2017-09-01

The process of chemical biotechnological processing of collagen-containing raw materials into functional components of feeds for effective pig rearing was studied. Protein components of feeds were obtained as a result of hydrolysis in the presence of lactic acid of the animal collagen from secondary raw materials, which comprised subcutaneous collagen (cuticle), skin and veined mass with tendons from cattle. For comparison, a method is described for preparing protein components of feeds by cultivating Lactobacillus plantarum. Analysis of the kinetic data of the conversion of a high-molecular collagen protein to an aminolyte polypeptide mixture showed the advantage of microbiological synthesis in obtaining a protein for feeds. Feed formulations have been developed to include the components obtained, and which result in high quality pork suitable for the production of quality meat products.

Economic and environmental assessment of propionic acid production by fermentation using different renewable raw materials.

PubMed

Tufvesson, Pär; Ekman, Anna; Sardari, Roya R R; Engdahl, Kristina; Tufvesson, Linda

2013-12-01

Production of propionic acid by fermentation of glycerol as a renewable resource has been suggested as a means for developing an environmentally-friendly route for this commodity chemical. However, in order to quantify the environmental benefits, life cycle assessment of the production, including raw materials, fermentation, upstream and downstream processing is required. The economic viability of the process also needs to be analysed to make sure that any environmental savings can be realised. In this study an environmental and economic assessment from cradle-to-gate has been conducted. The study highlights the need for a highly efficient bioprocess in terms of product titre (more than 100g/L and productivity more than 2g/(L · h)) in order to be sustainable. The importance of the raw materials and energy production for operating the process to minimize emissions of greenhouse gases is also shown. Copyright © 2013 Elsevier Ltd. All rights reserved.

Typification of cider brandy on the basis of cider used in its manufacture.

PubMed

Rodríguez Madrera, Roberto; Mangas Alonso, Juan J

2005-04-20

A study of typification of cider brandies on the basis of the origin of the raw material used in their manufacture was conducted using chemometric techniques (principal component analysis, linear discriminant analysis, and Bayesian analysis) together with their composition in volatile compounds, as analyzed by gas chromatography with flame ionization to detect the major volatiles and by mass spectrometric to detect the minor ones. Significant principal components computed by a double cross-validation procedure allowed the structure of the database to be visualized as a function of the raw material, that is, cider made from fresh apple juice versus cider made from apple juice concentrate. Feasible and robust discriminant rules were computed and validated by a cross-validation procedure that allowed the authors to classify fresh and concentrate cider brandies, obtaining classification hits of >92%. The most discriminating variables for typifying cider brandies according to their raw material were 1-butanol and ethyl hexanoate.

Exploiting epoxidized natural rubber latex (ENRL) as a starting raw material for latex-based products

NASA Astrophysics Data System (ADS)

Siti Nor Qamarina, M.; Fatimah Rubaizah, M. R.; Nurul Suhaira, A.; Norhanifah, M. Y.

2017-12-01

Epoxidized natural rubber latex (ENRL) is a chemically modified natural rubber latex produced from epoxidation process that involves usage of organic peracids. Conversion of the ENRL into dry rubber products has been known to exhibit many beneficial properties, however limited published works were found on diversifiying the ENRL latex-based products applications. In this preliminary work, different source of raw materials and neutralization systems were investigated. The objective was to explore possibilities in producing distinctive ENRL. Findings have demonstrated that different source of raw materials and neutralization systems influenced the typical ENRL specifications, stability behavior and particle size distribution. Morphological observations performed on these ENRL systems appeared to agree with the ENRL characteristics achieved. Since experimenting these two main factors resulted in encouraging ENRL findings, detailed work shall be further scrutinized to search for an optimum condition in producing marketable ENRL specifically for latex-based products applications.

On the usage of agricultural raw materials--energy or food? An assessment from an economics perspective.

PubMed

Lenk, Fabian; Bröring, Stefanie; Herzog, Philipp; Leker, Jens

2007-12-01

Bioenergies are promoted across the globe as the answer for global warming and the chance to reduce dependency from fossil energy sources. Despite the fact that renewable energy sources offer the opportunity to reduce CO2 emission and present a chance to increase agricultural incomes, they also come along with some drawbacks that have been mostly neglected in the current discussion. This paper seeks to build a basis for discussing the impacts of the growing subsidization of bioenergy and the resulting usage competition of agricultural raw materials between foods and energy. To assess the usage competition and the subsidization of bioenergy, this article employs a welfare economics perspective associated with an emphasize on the construct of externalities. This will help to foster the discussion on the further subsidization of bioenergy, where funding for R&D on new ways of using non-food raw materials ought to play a significant role.

Micro-structural characterization of the hydration products of bauxite-calcination-method red mud-coal gangue based cementitious materials.

PubMed

Liu, Xiaoming; Zhang, Na; Yao, Yuan; Sun, Henghu; Feng, Huan

2013-11-15

In this research, the micro-structural characterization of the hydration products of red mud-coal gangue based cementitious materials has been investigated through SEM-EDS, (27)Al MAS NMR and (29)Si MAS NMR techniques, in which the used red mud was derived from the bauxite calcination method. The results show that the red mud-coal gangue based cementitious materials mainly form fibrous C-A-S-H gel, needle-shaped/rod-like AFt in the early hydration period. With increasing of the hydration period, densification of the pastes were promoted resulting in the development of strength. EDS analysis shows that with the Ca/Si of red mud-coal gangue based cementitious materials increases, the average Ca/Si and Ca/(Si+Al) atomic ratio of C-A-S-H gel increases, while the average Al/Si atomic ratio of C-A-S-H gel decreases. MAS NMR analysis reveals that Al in the hydration products of red mud-coal gangue based cementitious materials exists in the forms of Al(IV) and Al(VI), but mainly in the form of Al(VI). Increasing the Ca/Si ratio of raw material promotes the conversion of [AlO4] to [AlO6] and inhibits the combination between [AlO4] and [SiO4] to form C-A-S-H gel. Meanwhile, the polymerization degree of [SiO4] in the hydration products declines. Published by Elsevier B.V.

Correlation between hardness and water absorption properties of Saudi kaolin and white clay geopolymer coating

NASA Astrophysics Data System (ADS)

Ramasamy, Shamala; Abdullah, Mohd Mustafa Al Bakri; Huang, Yue; Hussin, Kamarudin; Wang, Jin; Shahedan, Noor Fifinatasha

2017-09-01

Geopolymer is an uprising technology that is being studied worldwide. Geopolymer raw materials are basically aluminosilicate source materials. However, this technology is yet to infiltrate into pipelines and coating industries which initiated our research idea. The idea of creating universal geopolymer based coating material is mainly to help oil and gas industry reduce its maintenance cost. Kaolin based geopolymer paste was coated on glass reinforced epoxy (GRE) substrates which are majorly used as pipeline material in the oil and gas industry at Saudi Arabia. Kaolin and white clay was chosen as raw material to study the possibilities of utilizing underused aluminosilicate raw materials for geopolymer coating. To obtain suitable formulation, Na2SiO3/NaOH ratio was varied from 0.40 untill 0.60 while other parameters such as solid/liquid ratio and NaOH molarity were kept constant at values as per previous works. Geopolymer coated GRE substrates were then subjected to water absorption, flexural strength and hardness test to validate our findings. Water absorption is a crucial test as for coating materials which justifies the pratical usability of the coating product. Upon testing, kaolin and white clay based geopolymer coating each shows promising properties at Na2SiO3/NaOH ratio of 0.45 and 0.50 each.

Assessment of resting-state blood flow through anterior cerebral arteries using trans-cranial doppler recordings.

PubMed

Huang, Hanrui; Sejdić, Ervin

2013-12-01

Trans-cranial Doppler (TCD) recordings are used to monitor cerebral blood flow in the main cerebral arteries. The resting state is usually characterized by the mean velocity or the maximum Doppler shift frequency (an envelope signal) by insonating the middle cerebral arteries. In this study, we characterized cerebral blood flow in the anterior cerebral arteries. We analyzed both envelope signals and raw signals obtained from bilateral insonation. We recruited 20 healthy patients and conducted the data acquisition for 15 min. Features were extracted from the time domain, the frequency domain and the time-frequency domain. The results indicate that a gender-based statistical difference exists in the frequency and time-frequency domains. However, no handedness effect was found. In the time domain, information-theoretic features indicated that mutual dependence is higher in raw signals than in envelope signals. Finally, we concluded that insonation of the anterior cerebral arteries serves as a complement to middle cerebral artery studies. Additionally, investigation of the raw signals provided us with additional information that is not otherwise available from envelope signals. Use of direct trans-cranial Doppler raw data is therefore validated as a valuable method for characterizing the resting state. Copyright © 2013 World Federation for Ultrasound in Medicine & Biology. Published by Elsevier Inc. All rights reserved.

Utilization of red mud and bagasse for production of gas absorption materials

NASA Astrophysics Data System (ADS)

Thang, Nguyen Hoc; Quyen, Pham Vo Thi Ha; Nhung, Le Thuy; Phong, Dang Thanh; Tuyen, Nguyen Ngoc Kim

2018-04-01

Gas treatment or/and gas absorption is field which has more investigation from researchers. They are finding optimal solutions from catalyst or synthesized materials to obtain the best benefit for factories and community. This study would like to introduce a method to synthesis the gas absorption materials responding requirements for the process of gas treatment. More specially, raw materials used to produce the materials are industrial waste impacting negatively on the environment. In which, red mud is solid waste of Bayer process from bauxite mining which is being the hard problem to have solutions for its management and utilization, and bagasse is industrial waste of sugar factories. Both red mud and bagasse were dried, ground, and sieved and then mixed with bentonite and water for forming by wet pressing method. Continuously, the mixtures were passed processes of heat treatment at 400°C. The final samples were tested physic-chemical properties and characterized for microstructure. The productions were also tested for gas absorption capacity with data obtained very positive in comparison with others.

Metabolite Profiling and Classification of DNA-Authenticated Licorice Botanicals

PubMed Central

Simmler, Charlotte; Anderson, Jeffrey R.; Gauthier, Laura; Lankin, David C.; McAlpine, James B.; Chen, Shao-Nong; Pauli, Guido F.

2015-01-01

Raw licorice roots represent heterogeneous materials obtained from mainly three Glycyrrhiza species. G. glabra, G. uralensis, and G. inflata exhibit marked metabolite differences in terms of flavanones (Fs), chalcones (Cs), and other phenolic constituents. The principal objective of this work was to develop complementary chemometric models for the metabolite profiling, classification, and quality control of authenticated licorice. A total of 51 commercial and macroscopically verified samples were DNA authenticated. Principal component analysis and canonical discriminant analysis were performed on 1H NMR spectra and area under the curve values obtained from UHPLC-UV chromatograms, respectively. The developed chemometric models enable the identification and classification of Glycyrrhiza species according to their composition in major Fs, Cs, and species specific phenolic compounds. Further key outcomes demonstrated that DNA authentication combined with chemometric analyses enabled the characterization of mixtures, hybrids, and species outliers. This study provides a new foundation for the botanical and chemical authentication, classification, and metabolomic characterization of crude licorice botanicals and derived materials. Collectively, the proposed methods offer a comprehensive approach for the quality control of licorice as one of the most widely used botanical dietary supplements. PMID:26244884