Shear strength characteristics of mechanically biologically treated municipal solid waste (MBT-MSW) from Bangalore.

PubMed

Sivakumar Babu, G L; Lakshmikanthan, P; Santhosh, L G

2015-05-01

Strength and stiffness properties of municipal solid waste (MSW) are important in landfill design. This paper presents the results of comprehensive testing of shear strength properties of mechanically biologically treated municipal solid waste (MBT-MSW) in laboratory. Changes in shear strength of MSW as a function of unit weight and particle size were investigated by performing laboratory studies on the MSW collected from Mavallipura landfill site in Bangalore. Direct shear tests, small scale and large scale consolidated undrained and drained triaxial tests were conducted on reconstituted compost reject MSW samples. The triaxial test results showed that the MSW samples exhibited a strain-hardening behaviour and the strength of MSW increased with increase in unit weight. Consolidated drained tests showed that the mobilized shear strength of the MSW increased by 40% for a unit weight increase from 7.3kN/m(3) to 10.3kN/m(3) at 20% strain levels. The mobilized cohesion and friction angle ranged from 5 to 9kPa and 8° to 33° corresponding to a strain level of 20%. The consolidated undrained tests exhibited reduced friction angle values compared to the consolidated drained tests. The friction angle increased with increase in the unit weight from 8° to 55° in the consolidated undrained tests. Minor variations were found in the cohesion values. Relationships for strength and stiffness of MSW in terms of strength and stiffness ratios are developed and discussed. The stiffness ratio and the strength ratio of MSW were found to be 10 and 0.43. Copyright © 2015 Elsevier Ltd. All rights reserved.

A Digital Image-Based Discrete Fracture Network Model and Its Numerical Investigation of Direct Shear Tests

NASA Astrophysics Data System (ADS)

Wang, Peitao; Cai, Meifeng; Ren, Fenhua; Li, Changhong; Yang, Tianhong

2017-07-01

This paper develops a numerical approach to determine the mechanical behavior of discrete fractures network (DFN) models based on digital image processing technique and particle flow code (PFC2D). A series of direct shear tests of jointed rocks were numerically performed to study the effect of normal stress, friction coefficient and joint bond strength on the mechanical behavior of joint rock and evaluate the influence of micro-parameters on the shear properties of jointed rocks using the proposed approach. The complete shear stress-displacement curve of the DFN model under direct shear tests was presented to evaluate the failure processes of jointed rock. The results show that the peak and residual strength are sensitive to normal stress. A higher normal stress has a greater effect on the initiation and propagation of cracks. Additionally, an increase in the bond strength ratio results in an increase in the number of both shear and normal cracks. The friction coefficient was also found to have a significant influence on the shear strength and shear cracks. Increasing in the friction coefficient resulted in the decreasing in the initiation of normal cracks. The unique contribution of this paper is the proposed modeling technique to simulate the mechanical behavior of jointed rock mass based on particle mechanics approaches.

The Influence of SAND’s Gradation and Clay Content of Direct Sheart Test on Clayey Sand

NASA Astrophysics Data System (ADS)

Wibisono, Gunawan; Agus Nugroho, Soewignjo; Umam, Khairul

2018-03-01

The shear strength of clayey-sand can be affected by several factors, e.g. gradation, density, moisture content, and the percentage of clay and sand fraction. The same percentage of clay and sand fraction in clayey-sand mixtures may have different shear strengths due to those factors. This research aims to study the effect of clay content on sand that cause the change of its shear strength. Samples consisted of different clay and sand fractions were reconstituted at a certain moisture content. Sand fractions varied from well-graded to poorly-graded sand. Shear strength was measured in terms of the direct shear test. Prior to the test, surcharge loads were applied to represent overburden pressures. Shear strength results and their components (i.e. Cohesion and internal angle of friction) were correlated with physical properties of samples (i.e. grading coefficient of curvature, coefficient of uniformity, and density). Results showed that samples classified as well-graded and dense sand had higher shear strength. In the other hand, the shear strengths decreased when the mixtures became poorly-graded and less dense. The inclusion of the clay fraction increased cohesion component and decreased internal angle of friction.

Improved Bond Strength of Cyanoacrylate Adhesives Through Nanostructured Chromium Adhesion Layers

NASA Astrophysics Data System (ADS)

Gobble, Kyle; Stark, Amelia; Stagon, Stephen P.

2016-09-01

The performance of many consumer products suffers due to weak and inconsistent bonds formed to low surface energy polymer materials, such as polyolefin-based high-density polyethylene (HDPE), with adhesives, such as cyanoacrylate. In this letter, we present an industrially relevant means of increasing bond shear strength and consistency through vacuum metallization of chromium thin films and nanorods, using HDPE as a prototype material and cyanoacrylate as a prototype adhesive. For the as received HDPE surfaces, unmodified bond shear strength is shown to be only 0.20 MPa with a standard deviation of 14 %. When Cr metallization layers are added onto the HDPE at thicknesses of 50 nm or less, nanorod-structured coatings outperform continuous films and have a maximum bond shear strength of 0.96 MPa with a standard deviation of 7 %. When the metallization layer is greater than 50 nm thick, continuous films demonstrate greater performance than nanorod coatings and have a maximum shear strength of 1.03 MPa with a standard deviation of 6 %. Further, when the combination of surface roughening with P400 grit sandpaper and metallization is used, 100-nm-thick nanorod coatings show a tenfold increase in shear strength over the baseline, reaching a maximum of 2.03 MPa with a standard deviation of only 3 %. The substantial increase in shear strength through metallization, and the combination of roughening with metallization, may have wide-reaching implications in consumer products which utilize low surface energy plastics.

Shear bond strength between autopolymerizing acrylic resin and Co-Cr alloy using different primers.

PubMed

Sanohkan, Sasiwimol; Urapepon, Somchai; Harnirattisai, Choltacha; Sirisinha, Chakrit; Sunintaboon, Panya

2012-01-01

This study aimed to examine the shear bond strength between cobalt chromium alloy and autopolymerizing acrylic resin using experimental primers containing 5, 10, and 15 wt% of 4-methacryloxyethyl trimellitic anhydride or 1, 2, and 3 wt% of 3-methacryloxypropyl-trimethoxysilane comparison to 5 commercial primers (ML primers, Alloy primer, Metal/Zirconia primer, Monobond S, and Monobond plus). Sixty alloy specimens were sandblasted and treated with each primer before bonded with an acrylic resin. The control group was not primed. The shear bond strengths were tested and statistically compared. Specimens treated with commercial primers significantly increased the shear bond strength of acrylic resin to cobalt chromium alloy (p<0.05). The highest shear bond strength was found in the Alloy primer group. Among experimental group, using 10 wt% of 4-methacryloxyethyl trimellitic anhydride -or 2 wt% of 3-methacryloxypropyltrimethoxysilane enhanced highest shear bond strength. The experimental and commercial primers in this study all improved bonding of acrylic resin to cobalt chromium alloy.

In vitro evaluation of an adhesive monomer as a bonding agent for orthodontic brackets to primary teeth and nickel-chromium ion crowns.

PubMed

Ergas, R P; Hondrum, S O; Mathieu, G P; Koonce, J D

1995-01-01

The adhesive monomer, Clearfil New Bond, was used to enhance the bond strength between orthodontic brackets and primary molars, premolars, and NiCr crowns. Twenty specimens of each had this dental adhesive applied according to the manufacturer's instructions in addition to a chemically cured composite material. The remaining specimens (20 each) were bonded without the adhesive monomer. Shear bond strengths were determined using a universal testing machine. Fracture sites were examined to determine the type of bond failure. All bond strengths were significantly increased with the addition of Clearfil New Bond (P < or = 0.0001). The shear bond strength to NiCr crowns with the addition of the adhesive monomer was 7.76 kg. This is comparable to the shear bond strength observed for primary molars (8.66 kg) and premolars (8.65 kg) without adhesive monomer. The observed decrease in adhesive bond failures with the addition of Clearfil New Bond indicated a stronger shear bond strength between the tooth surface and the bracket base. Clearfil New Bond can significantly increase the shear bond strength of orthodontic brackets to both primary molars and premolars. Additionally, it was shown that orthodontic brackets can be successfully bonded to Ni-Cr crowns at strengths comparable to primary or permanent enamel.

Longitudinal shear behavior of several oxide dispersion strengthened alloys

NASA Technical Reports Server (NTRS)

Glasgow, T. K.

1978-01-01

Two commercial oxide dispersion strengthened (ODS) alloys, MA-753 and MA-754, and three experimental ODS alloys, MA-757E, MA-755E, and MA-6000E, were tested in shear at 760 C. Comparisons were made with other turbine blade and vane alloys. All of the ODS alloys exhibited less shear strength than directionally solidified Mar-M 200 = Hf or then conventionally cast B-1900. The strongest ODS alloy tested, MA-755E, was comparable in both shear and tensile strength to the lamellar directionally solidified eutectic alloy gamma/gamma prime - delta. Substantial improvements in shear resistance were found for all alloys tested when the geometry of the specimen was changed from one generating a transverse tensile stress in the shear area to one generating a transverse compressive stress. Finally, 760 C shear strength as a fraction of tensile strength was found to increase linearly with the log of the transverse tensile ductility.

Physical Modeling of Shear Behavior of Infilled Rock Joints Under CNL and CNS Boundary Conditions

NASA Astrophysics Data System (ADS)

Shrivastava, Amit Kumar; Rao, K. Seshagiri

2018-01-01

Despite their frequent natural occurrence, filled discontinuities under constant normal stiffness (CNS) boundary conditions have been studied much less systematically, perhaps because of the difficulties arising from the increased number of variable parameters. Because of the lack of reliable and realistic theoretical or empirical relations and the difficulties in obtaining and testing representative samples, engineers rely on judgment and often consider the shear strength of the infilled material itself as shear strength of rock joints. This assumption leads to uneconomical and also sometimes the unsafe design of underground structures, slopes, rock-socketed piles and foundations. To study the effect of infill on the shear behavior of rock joints, tests were performed on the modeled infilled rock joint having different joint roughness under constant normal load (CNL) and CNS boundary conditions at various initial normal stress and varying thickness of the infilled material. The test results indicate that shear strength decreases with an increase in t/ a ratio for both CNL and CNS conditions, but the reduction in shear strength is more for CNL than for CNS condition for a given initial normal stress. The detailed account of the effect of thickness of infilled material on shear and deformation behavior of infilled rock joint is discussed in this paper, and a model is proposed to predict shear strength of infilled rock joint.

The significance of relative density for particle damage in loaded and sheared gravels

NASA Astrophysics Data System (ADS)

Fityus, Stephen; Imre, Emőke

2017-06-01

For granular assemblages of strong particles, an increase in the relative density usually leads to a significant increase in shear strength, which is evident as a peak strength, accompanied by significant dilation as the peak strength is attained. This paper describes an experimental study of shearing in assemblages of weak particles, where particle breakage offsets dilation for all but the lowest of confining stresses. In such materials, prone to particle breakage, the shear strengths of loose and dense assemblages rapidly converge to similar values as confining stress increases, and any benefit of greater relative density is lost. This is attributed to the densification effect associated with the loading under a high stress prior to shearing, which is characterised by widespread particle breakage and the formation of smaller particles to occupy space between coarser ones. Interestingly, under both low and high stresses, there was a tendency for greater particle breakage in the loose samples, as a result of both shearing and compression. This result suggests that, despite the denser assemblage having its particles more rigidly constrained and less able to rearrange to avoid direct loading, the influence of greater load-spreading capacity afforded by an increased number of particle contacts in a denser sample, is more dominant in controlling breakage.

Shear strength of metal-sapphire contacts

NASA Technical Reports Server (NTRS)

Pepper, S. V.

1976-01-01

The shear strength of polycrystalline Ag, Cu, Ni, and Fe contacts on clean (0001) sapphire has been studied in ultrahigh vacuum. Both clean metal surfaces and surfaces exposed to O2, Cl2, and C2H4 were used. The results indicate that there are two sources of strength of Al2O3-metal contacts: an intrinsic one that depends on the particular clean metal in contact with Al2O3 and an additional one due to intermediate films. The shear strength of the clean metal contacts correlated directly with the free energy of oxide formation for the lowest metal oxide, in accord with the hypothesis that a chemical bond is formed between metal cations and oxygen anions in the sapphire surface. Contacts formed by metals exposed to chlorine exhibited uniformly low shear strength indicative of van der Waals bonding between chlorinated metal surfaces and sapphire. Contacts formed by metals exposed to oxygen exhibited enhanced shear strength, in accord with the hypothesis that an intermediate oxide layer increases interfacial strength.

Stiffness, strength and adhesion characterization of electrochemically deposited conjugated polymer films

PubMed Central

Qu, Jing; Ouyang, Liangqi; Kuo, Chin-chen; Martin, David C.

2015-01-01

Conjugated polymers such as poly(3,4-ethylenedioxythiphene) (PEDOT) are of interest for a variety of applications including interfaces between electronic biomedical devices and living tissue. The mechanical properties, strength, and adhesion of these materials to solid substrates are all vital for long-term applications. We have been developing methods to quantify the mechanical properties of conjugated polymer thin films. In this study the stiffness, strength and the interfacial shear strength (adhesion) of electrochemically deposited PEDOT and PEDOT-co-1,3,5-tri[2-(3,4-ethylene dioxythienyl)]-benzene (EPh) were studied. The estimated Young’s modulus of the PEDOT films was 2.6 ± 1.4 GPa, and the strain to failure was around 2%. The tensile strength was measured to be 56 ± 27 MPa. The effective interfacial shear strength was estimated with a shear-lag model by measuring the crack spacing as a function of film thickness. For PEDOT on gold/palladium-coated hydrocarbon film substrates an interfacial shear strength of 0.7 ± 0.3 MPa was determined. The addition of 5 mole% of a tri-functional EDOT crosslinker (EPh) increased the tensile strength of the films to 283 ± 67 MPa, while the strain to failure remained about the same (2%). The effective interfacial shear strength was increased to 2.4 ± 0.6 MPa. PMID:26607768

Shock induced shear strength in an HMX based plastic bonded explosive

NASA Astrophysics Data System (ADS)

Millett, J. C. F.; Taylor, P.; Appleby-Thomas, G.

2017-01-01

The shock induced mechanical response of an HMX based plastic bonded explosive (PBX) has been investigated in terms of the shear strength. Results show that shear strength increases with impact stress. However comparison with the calculated elastic response of both the PBX and pure HMX suggests that the overall mechanical response is controlled by the HMX crystals, with the near liquid like nature of the binder phase having a minimal contribution.

An experimental study on the shear strength of FRP perfobond shear connector

NASA Astrophysics Data System (ADS)

Gwon, S. C.; Kim, S. H.; Yoon, S. J.; Choi, C. W.

2018-06-01

In this study, push-out tests were conducted to investigate shear behaviour of FRP perfobond shear connector. The parameters influencing shear capacity of FRP perfobond shear connector are concrete dowel effect, shear resistance effect of the laterally reinforced FRP re- bar, and frictional effect between shear connector and concrete. The specimens were designed to consider these parameters. The specimens coated with sand to increase frictional resistance between the FRP re-bar and concrete. Based on the test results and the parameters, new equation was suggested to predict shear strength of FRP perfobond shear connectors. The predicted results and the experimental results were compared to check the feasibility of prediction.

Effect of sandblasting on surface roughness of zirconia-based ceramics and shear bond strength of veneering porcelain.

PubMed

He, Min; Zhang, Zutai; Zheng, Dongxiang; Ding, Ning; Liu, Yan

2014-01-01

This study aims to investigate the effect of sandblasting on the surface roughness of zirconia and the shear bond strength of the veneering porcelain. Pre-sintered zirconia plates were prepared and divided into four groups. Group A were not treated at all; group B were first sandblasted under 0.2 MPa pressure and then densely sintered; group C and D were sintered first, and then sandblasted under 0.2 MPa and 0.4 MPa pressures respectively. Surface roughness was measured and 3D roughness was reconstructed for the specimens, which were also analyzed with X-ray diffractometry. Finally after veneering porcelain sintering, shear bond tests were conducted. Sandblasting zirconia before sintering significantly increased surface roughness and the shear bond strength between zirconia and veneering porcelain (p<0.05). Sandblasting zirconia before sintering is a useful method to increase surface roughness and could successfully improve the bonding strength of veneering porcelain.

A Laboratory Investigation on Shear Strength Behavior of Sandy Soil: Effect of Glass Fiber and Clinker Residue Content

NASA Astrophysics Data System (ADS)

Bouaricha, Leyla; Henni, Ahmed Djafar; Lancelot, Laurent

2017-12-01

A study was undertaken to investigate the shear strength parameters of treated sands reinforced with randomly distributed glass fibers by carrying out direct shear test after seven days curing periods. Firstly, we studied the fiber content and fiber length effect on the peak shear strength on samples. The second part gives a parametric analysis on the effect of glass fiber and clinker residue content on the shear strength parameters for two types of uniform Algerian sands having different particle sizes (Chlef sand and Rass sand) with an average relative density Dr = 50%. Finally, the test results show that the combination of glass fiber and clinker residue content can effectively improve the shear strength parameters of soil in comparison with unreinforced soil. For instance, there is a significant gain for the cohesion and friction angle of reinforced sand of Chlef. Compared to unreinforced sand, the cohesion for sand reinforced with different ratios of clinker residue increased by 4.36 to 43.08 kPa for Chlef sand and by 3.1 to 28.64 kPa for Rass sand. The feature friction angles increased from 38.73° to 43.01° (+4.28°), and after the treatment, clinker residue content of soil evaluated to 5% (WRC = 5%).

Beneficial use of off-specification fly ashes to increase the shear strength and stiffness of expansive soil-rubber (ESR) mixtures.

DOT National Transportation Integrated Search

2011-07-01

The use of off-specification fly ashes to increase the shear strength and stiffness of an expansive soil-rubber (ESR) mixture is investigated systematically in this study. The off-specification fly ashes used include a high-sulfur content and a high-...

Through thickness mechanical properties of chemical vapor infiltration and nano-infiltration and transient eutectic-phase processed SiC/SiC composites

DOE PAGES

Shih, Chunghao Phillip; Katoh, Yutai; Ozawa, Kazumi; ...

2014-04-08

The through thickness (interlaminar) shear strength and trans-thickness tensile strength of three different nuclear-grade SiC/SiC composites were evaluated at room temperature by the double-notched shear and diametral compression tests, respectively. With increasing densification of the interlaminar matrix region, a transition in failure locations from interlayer to intrafiber bundle was observed, along with significant increases in the value of the interlaminar shear strength. Under trans-thickness tensile loading, cracks were found to propagate easily in the unidirectional composite. Furthermore, the 2D woven composite had a higher trans-thickness tensile strength (38 MPa) because the failure mode involved debonding, fiber pull-out and fiber failure.

Through thickness mechanical properties of chemical vapor infiltration and nano-infiltration and transient eutectic-phase processed SiC/SiC composites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shih, Chunghao Phillip; Katoh, Yutai; Ozawa, Kazumi

The through thickness (interlaminar) shear strength and trans-thickness tensile strength of three different nuclear-grade SiC/SiC composites were evaluated at room temperature by the double-notched shear and diametral compression tests, respectively. With increasing densification of the interlaminar matrix region, a transition in failure locations from interlayer to intrafiber bundle was observed, along with significant increases in the value of the interlaminar shear strength. Under trans-thickness tensile loading, cracks were found to propagate easily in the unidirectional composite. Furthermore, the 2D woven composite had a higher trans-thickness tensile strength (38 MPa) because the failure mode involved debonding, fiber pull-out and fiber failure.

Effect of Reduced Phosphoric Acid Pre-etching Times 
on Enamel Surface Characteristics and Shear Fatigue Strength Using Universal Adhesives.

PubMed

Tsujimoto, Akimasa; Fischer, Nicholas; Barkmeier, Wayne; Baruth, Andrew; Takamizawa, Toshiki; Latta, Mark; Miyazaki, Masashi

2017-01-01

To examine the effect of reduced phosphoric acid pre-etching times on enamel fatigue bond strength of universal adhesives and surface characteristics by using atomic force microscopy (AFM). Three universal adhesives were used in this study (Clearfil Universal Bond [C], G-Premio Bond [GP], Scotchbond Universal Adhesive [SU]). Four pre-etching groups were employed: enamel pre-etched with phosphoric acid and immediately rinsed with an air-water spray, and enamel pre-etched with phosphoric acid for 5, 10, or 15 s. Ground enamel was used as the control group. For the initial bond strength test, 15 specimens per etching group for each adhesive were used. For the shear fatigue test, 20 specimens per etching group for each adhesive were loaded using a sine wave at a frequency of 20 Hz for 50,000 cycles or until failure occurred. Initial shear bond strengths and fatigue shear strengths of composite adhesively bonded to ground and pre-etched enamel were determined. AFM observations of ground and pre-etched enamel were also conducted, and surface roughness as well as surface area were evaluated. The initial shear bond strengths and fatigue shear strengths of the universal adhesives in the pre-etched groups were significantly higher than those of the control group, and were not influenced by the pre-etching time. Significantly higher surface roughness and surface area of enamel surfaces in pre-etched groups were observed compared with those in the control group. While the surface area was not significantly influenced by etching time, surface roughness of the enamel surfaces in the pre-etched groups significantly increased with pre-etching time. The results of this in vitro study suggest that reduced phosphoric acid pre-etching times do not impair the fatigue bond strength of universal adhesives. Although fatigue bond strength and surface area were not influenced by phosphoric-acid etching times, surface roughness increased with increasing etching time.

Shear strength and microstructure of polydisperse packings: The effect of size span and shape of particle size distribution.

PubMed

Azéma, Emilien; Linero, Sandra; Estrada, Nicolas; Lizcano, Arcesio

2017-08-01

By means of extensive contact dynamics simulations, we analyzed the effect of particle size distribution (PSD) on the strength and microstructure of sheared granular materials composed of frictional disks. The PSDs are built by means of a normalized β function, which allows the systematic investigation of the effects of both, the size span (from almost monodisperse to highly polydisperse) and the shape of the PSD (from linear to pronouncedly curved). We show that the shear strength is independent of the size span, which substantiates previous results obtained for uniform distributions by packing fraction. Notably, the shear strength is also independent of the shape of the PSD, as shown previously for systems composed of frictionless disks. In contrast, the packing fraction increases with the size span, but decreases with more pronounced PSD curvature. At the microscale, we analyzed the connectivity and anisotropies of the contacts and forces networks. We show that the invariance of the shear strength with the PSD is due to a compensation mechanism which involves both geometrical sources of anisotropy. In particular, contact orientation anisotropy decreases with the size span and increases with PSD curvature, while the branch length anisotropy behaves inversely.

Shear Strength and Cracking Process of Non-persistent Jointed Rocks: An Extensive Experimental Investigation

NASA Astrophysics Data System (ADS)

Asadizadeh, Mostafa; Moosavi, Mahdi; Hossaini, Mohammad Farouq; Masoumi, Hossein

2018-02-01

In this paper, a number of artificial rock specimens with two parallel (stepped and coplanar) non-persistent joints were subjected to direct shearing. The effects of bridge length ( L), bridge angle ( γ), joint roughness coefficient (JRC) and normal stress ( σ n) on shear strength and cracking process of non-persistent jointed rock were studied extensively. The experimental program was designed based on Taguchi method, and the validity of the resulting data was assessed using analysis of variance. The results revealed that σ n and γ have the maximum and minimum effects on shear strength, respectively. Also, increase in L from 10 to 60 mm led to decrease in shear strength where high level of JRC profile and σ n led to the initiation of tensile cracks due to asperity interlocking. Such tensile cracks are known as "interlocking cracks" which normally initiate from the asperity and then propagate toward the specimen boundaries. Finally, the cracking process of specimens was classified into three categories, namely tensile cracking, shear cracking and combination of tension and shear or mixed mode tensile-shear cracking.

Study on shear strengthening of RC continuous T-beams using different layers of CFRP strips

DOE Office of Scientific and Technical Information (OSTI.GOV)

Alferjani, M. B. S.; Samad, A. A. Abdul; Mohamad, Noridah

2015-05-15

Carbon fiber reinforced polymer (CFRP) laminates are externally bonded to reinforced concrete (RC) members to provide additional strength such as flexural, shear, etc. However, this paper presents the results of an experimental investigation for enhancing the shear capacity of reinforced concrete (RC) continuous T- beams using different layers of CFRP wrapping schemes. A total of three concrete beams were tested and various sheet configurations and layouts were studied to determine their effects on ultimate shear strength and shear capacity of the beams. One beam was kept as control beams, while other beams were strengthened with externally bonded CFRP strips withmore » three side bonding and one or two layers of CFRP strips. From the test results, it was found that all schemes were found to be effective in enhancing the shear strength of RC beams. It was observed that the strength increases with the number of sheet layers provided the most effective strengthening for RC continuous T- beam. Beam strengthened using this scheme showed 23.21% increase in shear capacity as compared to the control beam. Two prediction models available in literature were used for computing the contribution of CFRP strips and compared with the experimental results.« less

Study of the Peak Shear Strength of a Cement-Filled Hard Rock Joint

NASA Astrophysics Data System (ADS)

She, Cheng-Xue; Sun, Fu-Ting

2018-03-01

The peak shear strength of a cement-filled hard rock joint is studied by theoretical analysis and laboratory testing. Based on the concept of the shear resistance angle, by combining the statistical method and fractal theory, three new parameters are proposed to characterize the three-dimensional joint morphology, reflecting the effects of the average roughness, multi-scale asperities and the dispersion degree of the roughness distribution. These factors are independent of the measurement scale, and they reflect the anisotropy of the joint roughness. Compressive shear tests are conducted on cement-filled joints. Because joints without cement can be considered special cement-filled joints in which the filling degree of cement is zero, they are also tested. The cement-filled granite joint fails primarily along the granite-cement interfaces. The filling degree of cement controls the joint failure and affects its mechanical behaviour. With a decrease in the filling degree of cement, the joint cohesion decreases; however, the dilatancy angle and the basic friction angle of the interface increase. As the filling degree approaches zero, the cohesion approaches zero, while the dilatancy angle and the basic friction angle increase to those of the joint without cement. A set of formulas is proposed to evaluate the peak shear strength of the joints with and without cement. The formulas are shown to be reasonable by comparison with the tested peak shear strength, and they reflect the anisotropy of the strength. This research deepens the understanding of cement-filled joints and provides a method to evaluate their peak shear strength.

Soil-roots Strength Performance of Extensive Green Roof by Using Axonopus Compressus

NASA Astrophysics Data System (ADS)

Yusoff, N. A.; Ramli, M. N.; Chik, T. N. T.; Ahmad, H.; Abdullah, M. F.; Kasmin, H.; Embong, Z.

2016-07-01

Green roof technology has been proven to provide potential environmental benefits including improved building thermal performance, removal of air pollution and reduced storm water runoff. Installation of green roof also involved soil element usage as a plant growth medium which creates several interactions between both strands. This study was carried out to investigate the soil-roots strength performance of green roof at different construction period up to 4 months. Axonopus compressus (pearl grass) was planted in a ExE test plot with a designated suitable soil medium. Direct shear test was conducted for each plot to determine the soil shear strength according to different construction period. In addition, some basic geotechnical testing also been carried out. The results showed that the shear strength of soil sample increased over different construction period of 1st, 2nd, 3rd and 4th month with average result 3.81 kPa, 5.55 kPa, 6.05 kPa and 6.48 kPa respectively. Shear strength of rooted soil samples was higher than the soil samples without roots (control sample). In conclusion, increment of soil-roots shear strength was due to root growth over the time. The soil-roots shear strength development of Axonopus compressus can be expressed in a linear equation as: y = 0.851x + 3.345, where y = shear stress and x = time.

Effect of Different Peat Size and Pre-Consolidation Pressure of Reconstituted Peat on Effective Undrained Shear Strength Properties

NASA Astrophysics Data System (ADS)

Azhar, ATS; Norhaliza, W.; Ismail, B.; Ezree, AM; Nizam, ZM

2017-08-01

Shear strength of the soil is one of the most important parameters in engineering design, especially during the pre- or post-construction periods, since it is mainly used to measure and evaluate the foundation or slope stability of soil. Peat normally known as a soil that has a very low value of shear strength, and in order to determine and understand the shear strength of the peat, it is a difficult task in geotechnical engineering due to several factors such as types of fabrics, the origin of the soil, water content, organic matter and the degree of humification. The aim of this study is to determine the effective undrained shear strength properties of reconstituted peat of different sizes. All the reconstituted peat samples were formed with the size that passed the opening sieve of 0.425 mm (

Comparison of bond strengths of ceramic brackets bonded to zirconia surfaces using different zirconia primers and a universal adhesive.

PubMed

Lee, Ji-Yeon; Ahn, Jaechan; An, Sang In; Park, Jeong-Won

2018-02-01

The aim of this study is to compare the shear bond strengths of ceramic brackets bonded to zirconia surfaces using different zirconia primers and universal adhesive. Fifty zirconia blocks (15 × 15 × 10 mm, Zpex, Tosoh Corporation) were polished with 1,000 grit sand paper and air-abraded with 50 µm Al 2 O 3 for 10 seconds (40 psi). They were divided into 5 groups: control (CO), Metal/Zirconia primer (MZ, Ivoclar Vivadent), Z-PRIME Plus (ZP, Bisco), Zirconia Liner (ZL, Sun Medical), and Scotchbond Universal adhesive (SU, 3M ESPE). Transbond XT Primer (used for CO, MZ, ZP, and ZL) and Transbond XT Paste was used for bracket bonding (Gemini clear ceramic brackets, 3M Unitek). After 24 hours at 37°C storage, specimens underwent 2,000 thermocycles, and then, shear bond strengths were measured (1 mm/min). An adhesive remnant index (ARI) score was calculated. The data were analyzed using one-way analysis of variance and the Bonferroni test ( p = 0.05). Surface treatment with primers resulted in increased shear bond strength. The SU group showed the highest shear bond strength followed by the ZP, ZL, MZ, and CO groups, in that order. The median ARI scores were as follows: CO = 0, MZ = 0, ZP = 0, ZL = 0, and SU = 3 ( p < 0.05). Within this experiment, zirconia primer can increase the shear bond strength of bracket bonding. The highest shear bond strength is observed in SU group, even when no primer is used.

Comparison of bond strengths of ceramic brackets bonded to zirconia surfaces using different zirconia primers and a universal adhesive

PubMed Central

2018-01-01

Objectives The aim of this study is to compare the shear bond strengths of ceramic brackets bonded to zirconia surfaces using different zirconia primers and universal adhesive. Materials and Methods Fifty zirconia blocks (15 × 15 × 10 mm, Zpex, Tosoh Corporation) were polished with 1,000 grit sand paper and air-abraded with 50 µm Al2O3 for 10 seconds (40 psi). They were divided into 5 groups: control (CO), Metal/Zirconia primer (MZ, Ivoclar Vivadent), Z-PRIME Plus (ZP, Bisco), Zirconia Liner (ZL, Sun Medical), and Scotchbond Universal adhesive (SU, 3M ESPE). Transbond XT Primer (used for CO, MZ, ZP, and ZL) and Transbond XT Paste was used for bracket bonding (Gemini clear ceramic brackets, 3M Unitek). After 24 hours at 37°C storage, specimens underwent 2,000 thermocycles, and then, shear bond strengths were measured (1 mm/min). An adhesive remnant index (ARI) score was calculated. The data were analyzed using one-way analysis of variance and the Bonferroni test (p = 0.05). Results Surface treatment with primers resulted in increased shear bond strength. The SU group showed the highest shear bond strength followed by the ZP, ZL, MZ, and CO groups, in that order. The median ARI scores were as follows: CO = 0, MZ = 0, ZP = 0, ZL = 0, and SU = 3 (p < 0.05). Conclusions Within this experiment, zirconia primer can increase the shear bond strength of bracket bonding. The highest shear bond strength is observed in SU group, even when no primer is used. PMID:29487838

Factors affecting the shear strength behavior of municipal solid wastes.

PubMed

Pulat, Hasan Firat; Yukselen-Aksoy, Yeliz

2017-11-01

In this study, the shear strength behavior of European (E-1), Turkey (T-1), and United States of America (U-1) average synthetic municipal solid waste (MSW) compositions were investigated. The large-scale direct shear tests were conducted using fresh and aged MSW samples collected from the Manisa Landfill. The natural samples' test results were compared with synthetic samples. The affecting factors such as ageing, waste composition, and waste type (synthetic and natural) on the shear strength of MSWs were investigated. The effect of composition was evaluated using three main and six modified synthetic MSW compositions. In addition to the synthetic fresh MSW samples, synthetic aged samples were also used. Angle of shearing resistance decreased with increasing organic content whereas cohesion intercept increased with increasing organic content. The fresh and aged wastes with higher coarse fraction lead to a higher angle of shearing resistance. The synthetic aged samples had higher internal friction angles but lower cohesion values than the synthetic fresh samples. Waste with average European composition had the highest internal friction angle as it has the highest fibrous content. On the other hand, the highest cohesion belonged to the Turkey composition, which had the highest organic matter ratio. The main differences between E-1, T-1 and U-1 samples in terms of compositions were observed. The results of this study indicated that shear strength of waste significantly depends on composition and hence a site specific evaluation is recommended. Copyright © 2017 Elsevier Ltd. All rights reserved.

Factors affecting the pullout strength of cancellous bone screws.

PubMed

Chapman, J R; Harrington, R M; Lee, K M; Anderson, P A; Tencer, A F; Kowalski, D

1996-08-01

Screws placed into cancellous bone in orthopedic surgical applications, such as fixation of fractures of the femoral neck or the lumbar spine, can be subjected to high loads. Screw pullout is a possibility, especially if low density osteoporotic bone is encountered. The overall goal of this study was to determine how screw thread geometry, tapping, and cannulation affect the holding power of screws in cancellous bone and determine whether current designs achieve maximum purchase strength. Twelve types of commercially available cannulated and noncannulated cancellous bone screws were tested for pullout strength in rigid unicellular polyurethane foams of apparent densities and shear strengths within the range reported for human cancellous bone. The experimentally derived pullout strength was compared to a predicted shear failure force of the internal threads formed in the polyurethane foam. Screws embedded in porous materials pullout by shearing the internal threads in the porous material. Experimental pullout force was highly correlated to the predicted shear failure force (slope = 1.05, R2 = 0.947) demonstrating that it is controlled by the major diameter of the screw, the length of engagement of the thread, the shear strength of the material into which the screw is embedded, and a thread shape factor (TSF) which accounts for screw thread depth and pitch. The average TSF for cannulated screws was 17 percent lower than that of noncannulated cancellous screws, and the pullout force was correspondingly less. Increasing the TSF, a result of decreasing thread pitch or increasing thread depth, increases screw purchase strength in porous materials. Tapping was found to reduce pullout force by an average of 8 percent compared with nontapped holes (p = 0.0001). Tapping in porous materials decreases screw pullout strength because the removal of material by the tap enlarges hole volume by an average of 27 percent, in effect decreasing the depth and shear area of the internal threads in the porous material.

Characterization of the porosity of human dental enamel and shear bond strength in vitro after variable etch times: initial findings using the BET method.

PubMed

Nguyen, Trang T; Miller, Arthur; Orellana, Maria F

2011-07-01

(1) To quantitatively characterize human enamel porosity and surface area in vitro before and after etching for variable etching times; and (2) to evaluate shear bond strength after variable etching times. Specifically, our goal was to identify the presence of any correlation between enamel porosity and shear bond strength. Pore surface area, pore volume, and pore size of enamel from extracted human teeth were analyzed by Brunauer-Emmett-Teller (BET) gas adsorption before and after etching for 15, 30, and 60 seconds with 37% phosphoric acid. Orthodontic brackets were bonded with Transbond to the samples with variable etch times and were subsequently applied to a single-plane lap shear testing system. Pore volume and surface area increased after etching for 15 and 30 seconds. At 60 seconds, this increase was less pronounced. On the contrary, pore size appears to decrease after etching. No correlation was found between variable etching times and shear strength. Samples etched for 15, 30, and 60 seconds all demonstrated clinically viable shear strength values. The BET adsorption method could be a valuable tool in enhancing our understanding of enamel characteristics. Our findings indicate that distinct quantitative changes in enamel pore architecture are evident after etching. Further testing with a larger sample size would have to be carried out for more definitive conclusions to be made.

Effect of Post-Braze Heat Treatment on the Microstructure and Shear Strength of Cemented Carbide and Steel Using Ag-Based Alloy

NASA Astrophysics Data System (ADS)

Winardi, Y.; Triyono; Muhayat, N.

2018-03-01

The aim of the present study was to investigate the effect temperature of heat treatment process on the interfacial microstructure and mechanical properties of cemented carbide/carbon steel single lap joint brazed using Ag based alloy filler metal. The brazing process was carried out using torch brazing. Heat treatment process was carried out in induction furnace on the temperature of 700, 725, and 750°C, for 30 minutes. Microstructural examinations and phase analysis were performed using scanning electron microscopy (SEM) equipped with energy dispersion spectrometry (EDS). Shear strength of the joints was measured by the universal testing machine. The results of the microstructural analyses of the brazed area indicate that the increase temperature of treatment lead to the increase of solid solution phase of enrichted Cu. Based on EDS test, the carbon elements spread to all brazed area, which is disseminated by base metals. Shear strength joint is increased with temperature treatment. The highest shear strength of the brazed joint was 214,14 MPa when the heated up at 725°C.

Temperature-dependent residual shear strength characteristics of smectite-bearing landslide soils

NASA Astrophysics Data System (ADS)

Shibasaki, Tatsuya; Matsuura, Sumio; Hasegawa, Yoichi

2017-02-01

This paper presents experimental investigations regarding the effect of temperature on the residual strength of landslide soils at slow-to-moderate shearing velocities. We performed ring-shear tests on 23 soil samples at temperatures of 6-29°C. The test results show that the shear strength of smectite-rich soils decreased when temperatures were relatively low. These positive temperature effects (strength losses at lower temperatures) observed for smectite-bearing soils are typical under relatively slow shearing rates. In contrast, under relatively high shearing rates, strength was gained as temperature decreased. As rheological properties of smectite suspensions are sensitive to environmental factors, such as temperature, pH, and dissolved ions, we inferred that temperature-dependent residual strengths of smectitic soils are also attributed to their specific rheological properties. Visual and scanning electron microscope observations of Ca-bentonite suggest that slickensided shear surfaces at slow shearing rates are very shiny and smooth, whereas those at moderate shearing rates are not glossy and are slightly turbulent, indicating that platy smectite particles are strongly orientated at slow velocities. The positive temperature effect is probably due to temperature-dependent microfriction that is mobilized in the parallel directions of the sheet structure of hydrous smectite particles. On the contrary, the influence of microviscous resistance, which appears in the vertical directions of the lamination, is assumed to increase at faster velocities. Our results imply that if slip-surface soils contain high fractions of smectite, decreases in ground temperature can lead to lowered shear resistance of the slip surface and trigger slow landslide movement.

The shear strength of three-dimensional capillary-porous titanium coatings for intraosseous implants.

PubMed

Kalita, V I; Komlev, D I; Komlev, V S; Radyuk, A A

2016-03-01

A plasma spraying process for the deposition of three-dimensional capillary-porous titanium coatings using a wire has been developed. In this process, two additional dc arcs are discharged between plasmatron and both the wire and the substrate, resulting in additional activation of the substrate and the particles, particularly by increasing their temperature. The shear strength of the titanium coating with 46% porosity is 120.6 MPa. A new procedure for estimating the shear strength of porous coatings has been developed. Copyright © 2015 Elsevier B.V. All rights reserved.

[Root system distribution and biomechanical characteristics of Bambusa oldhami].

PubMed

Zhou, Ben-Zhi; Xu, Sheng-Hua; An, Yan-Fei; Xu, Sheng-Hua

2014-05-01

To determine the mechanism of soil stabilizing through Bambusa oldhami root system, the vertical distribution of B. oldhami root system in soil was investigated, and the tensile strength of individual root and soil shear strength were measured in B. oldhami forest. The dry mass, length, surface area and volume of the B. oldhami root system decreased with the increasing soil depth, with more than 90% of the root system occurring in the 0-40 cm soil layer. The root class with D 1 mm occupied the highest percentage of the total in terms of root length, accounting for 79.6%, but the lowest percentage of the total in terms of root volume, accounting for 8.2%. The root class with D >2 mm was the opposite, and the root class with D= 1-2 mm stayed in between. The maximum tensile resistance of B. oldhami root, either with 12% moisture content or a saturated moisture content, increased with the increasing root diameter, while the tensile strength decreased with the increasing root diameter in accordance with power function. Tensile strength of the root, with either of the two moisture contents, was significantly different among the diameter classes, with the highest tensile strength occurring in the root with D < or = 1 mm and the lowest in the root with D > or = 2 mm. The tensile strength of root with 12% moisture content was significantly higher than that with the saturated moisture content, and less effect of moisture content on root tensile strength would occur in thicker roots. The shear strengths of B. oldhami forest soil and of bare soil both increased with the increasing soil depth. The shear strength of B. oldhami forest soil had a linear positive correlation with the root content in soil, and was significantly higher than that of bare soil. The shear strength increment in B. oldhami forest was positively correlated with the root content in soil according to an exponential function, but not related significantly with soil depth.

49 CFR 230.28 - Higher shearing strength of rivets.

Code of Federal Regulations, 2011 CFR

2011-10-01

... 49 Transportation 4 2011-10-01 2011-10-01 false Higher shearing strength of rivets. 230.28 Section... Appurtenances Strength of Materials § 230.28 Higher shearing strength of rivets. A higher shearing strength may... quality as to justify a higher allowable shearing strength. Inspection and Repair ...

49 CFR 230.28 - Higher shearing strength of rivets.

Code of Federal Regulations, 2010 CFR

2010-10-01

... 49 Transportation 4 2010-10-01 2010-10-01 false Higher shearing strength of rivets. 230.28 Section... Appurtenances Strength of Materials § 230.28 Higher shearing strength of rivets. A higher shearing strength may... quality as to justify a higher allowable shearing strength. Inspection and Repair ...

Seasonal Effects on the Relationships Between Soil Water Content, Pore Water Pressure and Shear Strength and Their Implications for Slope Stability

NASA Astrophysics Data System (ADS)

Hughes, P. N.

2015-12-01

A soil's shear resistance is mainly dependent upon the magnitude of effective stress. For small to medium height slopes (up to 10m) in clay soils the total stress acting along potential failure planes will be low, therefore the magnitude of effective stress (and hence soil shear strength) will be dominated by the pore-water pressure. The stability of slopes on this scale through periods of increased precipitation is improved by the generation of negative pore pressures (soil suctions) during preceding, warmer, drier periods. These negative pore water pressures increase the effective stress within the soil and cause a corresponding increase in shearing resistance. The relationships between soil water content and pore water pressure (soil water retention curves) are known to be hysteretic, but for the purposes of the majority of slope stability assessments in partially saturated clay soils, these are assumed to be consistent with time. Similarly, the relationship between shear strength and water content is assumed to be consistent over time. This research presents a laboratory study in which specimens of compacted Glacial Till (typical of engineered slopes within the UK) were subjected to repeated cycles of wetting and drying to simulate seasonal cycles. At predetermined water contents, measurements of soil suction were made using tensiometer and dewpoint potentiometer methods. The undrained shear strength of the specimens was then measured using triaxial strength testing equipment. Results indicate that repeated wetting and drying cycles caused a change in the soil water retention behaviour. A reduction in undrained shear strength at corresponding water contents along the wetting and drying paths was also observed. The mechanism for the change in the relationship is believed to be a deterioration in the soil physical structure due to shrink/swell induced micro-cracking. The non-stationarity of these relationships has implications for slope stability assessment.

Microbial strengthening of loose sand.

PubMed

Banagan, B L; Wertheim, B M; Roth, M J S; Caslake, L F

2010-08-01

To test whether the addition of Flavobacterium johnsoniae could increase the strength of saturated Ottawa 30 sand. A box model was built that simulates groundwater-like flow through a main sand compartment. Strength tests were performed at seven locations and at two depths, 10.8 and 20.3 cm below the top of the tank, using a vane shear device before and after the addition of bacteria. After the addition of Fl. johnsoniae, sand samples were obtained from multiple sampling ports on the vertical sides of the box model. The presence of a bacterial biofilm was confirmed by staining these sand samples with SYTO-9 and Alexa Fluor 633 and viewing with a confocal microscope. The average shear strength increases after the addition of Fl. johnsoniae were 15.2-87.5%, depending on the experimental conditions. Flavobacterium johnsoniae caused a statistically significant increase in the strength of saturated Ottawa 30 sand. Biofilm-forming bacteria can increase the shear strength of saturated sand. The addition of biofilm-forming bacteria to a building site may be an alternate method to mitigate the effects of liquefaction.

Microfluidic perfusion culture chip providing different strengths of shear stress for analysis of vascular endothelial function.

PubMed

Hattori, Koji; Munehira, Yoichi; Kobayashi, Hideki; Satoh, Taku; Sugiura, Shinji; Kanamori, Toshiyuki

2014-09-01

We developed a microfluidic perfusion cell culture chip that provides three different shear stress strengths and a large cell culture area for the analysis of vascular endothelial functions. The microfluidic network was composed of shallow flow-control channels of three different depths and deep cell culture channels. The flow-control channels with high fluidic resistances created shear stress strengths ranging from 1.0 to 10.0 dyn/cm(2) in the cell culture channels. The large surface area of the culture channels enabled cultivation of a large number (approximately 6.0 × 10(5)) of cells. We cultured human umbilical vein endothelial cells (HUVECs) and evaluated the changes in cellular morphology and gene expression in response to applied shear stress. The HUVECs were aligned in the direction of flow when exposed to a shear stress of 10.0 dyn/cm(2). Compared with conditions of no shear stress, endothelial nitric oxide synthase mRNA expression increased by 50% and thrombomodulin mRNA expression increased by 8-fold under a shear stress of 9.5 dyn/cm(2). Copyright © 2014 The Society for Biotechnology, Japan. Published by Elsevier B.V. All rights reserved.

Ross Sea Till Properties: Implications for Ice Sheet Bed Interaction

NASA Astrophysics Data System (ADS)

Halberstadt, A. R.; Anderson, J. B.; Simkins, L.; Prothro, L. O.; Bart, P. J.

2015-12-01

Since the discovery of a pervasive shearing till layer underlying Ice Stream B, the scientific community has categorized subglacial diamictons as either deformation till or lodgement till primarily based on shear strength. Deformation till is associated with streaming ice, formed through subglacial deformation of unconsolidated sediments. Lodgement till is believed to be deposited by the plastering of sediment entrained at the base of slow-flowing ice onto a rigid bed. Unfortunately, there has been a paucity of quantitative data on the spatial distribution of shear strength across the continental shelf. Cores collected from the Ross Sea on cruises NBP1502 and NBP9902 provide a rich dataset that can be used to interpret till shear strength variability. Till strengths are analyzed within the context of: (1) geologic substrate; (2) water content and other geotechnical properties; (3) ice sheet retreat history; and (4) geomorphic framework. Tills display a continuum of shear strengths rather than a bimodal distribution, suggesting that shear strength cannot be used to distinguish between lodgement and deformation till. Where the substrate below the LGM unconformity is comprised of older lithified deposits, till shear strengths are both highly variable within the till unit, as well as highly variable between cores. Conversely, where ice streams flowed across unconsolidated Plio-Pleistocene deposits, shear strengths are low and less variable within the unit and between cores. This suggests greater homogenization of cannibalized tills, and possibly a deeper pervasive shear layer. Coarser-grained tills are observed on banks and bank slopes, with finer tills in troughs. Highly variable and more poorly sorted tills are found in close proximity to sediment-based subglacial meltwater channels, attesting to a change in ice-bed interaction as subglacial water increases. Pellets (rounded sedimentary clasts of till matrix) are observed in Ross Sea cores, suggesting a history of deformation responsible for pellet formation. Till strength was measured in a variety of environments, including mega-scale lineations and grounding zone wedges; ongoing work focuses on evaluating till shear strengths within a geomorphic context. These analyses are used to re-evaluate till genesis, transport, and characterization.

An acoustic method for predicting relative strengths of cohesive sediment deposits

NASA Astrophysics Data System (ADS)

Reed, A. H.; Sanders, W. M.

2017-12-01

Cohesive sediment dynamics are fundamentally determined by sediment mineralogy, organic matter composition, ionic strength of water, and currents. These factors work to bind the cohesive sediments and to determine depositional rates. Once deposited the sediments exhibit a nonlinear response to stress and they develop increases in shear strength. Shear strength is critically important in resuspension, transport, creep, and failure predictions. Typically, shear strength is determined by point measurements, both indirectly from free-fall penetrometers or directly on cores with a shear vane. These values are then used to interpolate over larger areas. However, the remote determination of these properties would provide continuos coverage, yet it has proven difficult with sonar systems. Recently, findings from an acoustic study on cohesive sediments in a laboratory setting suggests that cohesive sediments may be differentiated using parametric acoustics; this method pulses two primary frequencies into the sediment and the resultant difference frequency is used to determine the degree of acoustic nonlinearity within the sediment. In this study, two marine clay species, kaolinite and montmorillonite, and two biopolymers, guar gum and xanthan gum were mixed to make nine different samples. The samples were evaluated in a parametric acoustic measurement tank. From the parametric acoustic measurements, the quadratic nonlinearity coefficient (beta) was determined. beta was correlated with the cation exchange capacity (CEC), an indicator of shear strength. The results indicate that increased acoustic nonlinearity correlates with increased CEC. From this work, laboratory measurements indicate that this correlation may be used evaluate geotechnical properties of cohesive sediments and may provide a means to predict sediment weakness in subaqueous environments.

Shear bond strength of resin composite bonded with two adhesives: Influence of Er: YAG laser irradiation distance

PubMed Central

Shirani, Farzaneh; Birang, Reza; Malekipour, Mohammad Reza; Hourmehr, Zahra; Kazemi, Shantia

2014-01-01

Background: Dental surfaces prepared with different Er:YAG laser distance may have different characteristics compared with those prepared with conventional instruments. The aim of this study was to investigate the effect of Er:YAG laser irradiation distance from enamel and dentin surfaces on the shear bond strength of composite with self-etch and etch and rinse bonding systems compared with conventional preparation method. Materials and Methods: Two hundred caries-free human third molars were randomly divided into twenty groups (n = 10). Ten groups were designated for enamel surface (E1-E10) and ten for dentin surface (D1-D10). Er: YAG laser (2940 nm) was used on the E1-E8 (240 mJ, 25 Hz) and D1-D8 (140 mJ, 30 Hz) groups at four different distances of 0.5 (standard), 2, 4 and 11 mm. Control groups (E9, E10, D9 and D10) were ground with medium grit diamond bur. The enamel and dentin specimens were divided into two subgroups that were bonded with either Single Bond or Clearfil SE Bond. Resin composite (Z100) was dispensed on prepared dentin and enamel. The shear bond strengths were tested using a universal testing machine. Data were analyzed by SPSS12 statistical software using three way analysis of variance, Tukey and independent t-test. P < 0.05 was considered as significant. Results: There was a significant difference between enamel and dentin substrates (P < 0.001) and between lased and un-lased groups; the un-lased group had significantly higher bond strength (P < 0.001). Shear bond strength increased significantly with an increase in the laser irradiation distance (P < 0.05) on enamel surfaces (in both bonding agent subgroups) and on dentin surfaces (in the Single Bond subgroup). Conclusion: Laser irradiation decreases shear bond strength. Irradiation distance affects shear bond strength and increasing the distance would decrease the negative effects of laser irradiation. PMID:25540665

Evaluation of bolted connections in wood-plastic composites

NASA Astrophysics Data System (ADS)

Arnandha, Yudhi; Satyarno, Iman; Awaludin, Ali; Irawati, Inggar Septia; Ihsan, Muhamad; Wijanarko, Felyx Biondy; William, Mahdinur, Fardhani, Arfiati

2017-03-01

Wood-plastic composite (WPC) is a relatively new material that consists of sawdust and plastic polymer using the extrusion process. Due to its attributes such as low water content, low maintenance, UV durability and being fungi and termite resistant. Nowadays, WPC has already been produced in Indonesia using sawdust from local wood such as Albizia (Paraserianthes falcataria) and Teak (Tectona grandis). Moreover preliminary studies about the physical and mechanical WPC board from Albizia sawdust and HDPE plastic have been carried out. Based on these studies, WPC has a high shear strength around 25-30 MPa higher than its original wood shear strength. This paper was a part of the research in evaluating WPC as potential sheathing in a shear wall system. Since still little is known about connection behavior in WPC using Indonesian local wood, this study evaluated the connection for both of these two types of wood-plastic composite. WPC board from Albizia sawdust will be projected as shear wall sheathing and WPC stud from Teak sawdust projected to be shear wall frame. For this study, the embedding strength for both WPC was determined according to ASTM D 5764 standard, using two types of bolts (stainless bolt and standard bolt) with several diameters as variation (6 mm, 8 mm, 10 and 12 mm). Hence, dowel-bearing test under fastened condition conducted accordance to ASTM D5652, hereby the yield strength then compared with the prediction yield strength from European Yield Model (EYM). According to both single and double shear connection, it can be concluded that yield strength from the EYM method tended to under-predict the 5% diameter offset yield than the actual yield strength from the test. The yield strength itself increase with the increase of bolt diameter. For single shear connection, the highest yield strength was 12 mm standard bolt around 9732 N, slightly higher than stainless bolt around 9393 N. Whereby for double shear connection, the highest yield strength was 12 mm standard bolt around 12009 N, slightly higher than stainless bolt around 12009 N. Using statistical approach ANOVA, the different type of bolt between stainless bolt and standard bolt gave an insignificant result. Both type of bolt can be used as structural connection, moreover it was recommended using a stainless bolt for outdoor purpose to reduce corrosion.

Influence of surface treatment on shear bond strength of orthodontic brackets.

PubMed

Brunharo, Ione Helena Vieira Portella; Fernandes, Daniel Jogaib; de Miranda, Mauro Sayão; Artese, Flavia

2013-01-01

The shear bond strength of orthodontic brackets bonded to micro-hybrid and micro-particulate resins under different surface treatment methods was assessed. Two hundred and eighty test samples were divided into 28 groups (n = 10), where 140 specimens were filled with Durafill micro-particulate resin and 140 with Charisma composite. In 140 samples, a coupling agent (silane) was applied. The surface treatment methods were: Phosphoric and hydrofluoric acid etching, sodium bicarbonate and aluminum oxide blasting, stone and burs. A Universal Instron Machine was used to apply an occlusal shear force directly to the resin composite bracket surface at a speed of 0.5 mm/min. The means were compared using analysis of variance and multivariate regression to assess the interaction between composites and surface treatment methods. Means and standard deviations for the groups were: Sodium bicarbonate jet 11.27 ± 2.78; burs 9.26 ± 3.01; stone 7.95 ± 3.67; aluminum oxide blasting 7.04 ± 3.21; phosphoric acid 5.82 ± 1.90; hydrofluoric acid 4.54 ± 2.87, and without treatment 2.75 ± 1.49. An increase of 1.94 MPa in shear bond strength was seen in Charisma groups. Silane agent application reduced the Charisma shear bond strength by 0.68 Mpa, but increased Durafill means for bicarbonate blasting (0.83), burs (0.98) and stone drilling (0.46). The sodium bicarbonate blasting, burs and stone drilling methods produced adequate shear bond strength and may be suitable for clinical use. The Charisma micro hybrid resin composite showed higher shear bond means than Durafill micro particle composite.

A viscoplastic shear-zone model for episodic slow slip events in oceanic subduction zones

NASA Astrophysics Data System (ADS)

Yin, A.; Meng, L.

2016-12-01

Episodic slow slip events occur widely along oceanic subduction zones at the brittle-ductile transition depths ( 20-50 km). Although efforts have been devoted to unravel their mechanical origins, it remains unclear about the physical controls on the wide range of their recurrence intervals and slip durations. In this study we present a simple mechanical model that attempts to account for the observed temporal evolution of slow slip events. In our model we assume that slow slip events occur in a viscoplastic shear zone (i.e., Bingham material), which has an upper static and a lower dynamic plastic yield strength. We further assume that the hanging wall deformation is approximated as an elastic spring. We envision the shear zone to be initially locked during forward/landward motion but is subsequently unlocked when the elastic and gravity-induced stress exceeds the static yield strength of the shear zone. This leads to backward/trenchward motion damped by viscous shear-zone deformation. As the elastic spring progressively loosens, the hanging wall velocity evolves with time and the viscous shear stress eventually reaches the dynamic yield strength. This is followed by the termination of the trenchward motion when the elastic stress is balanced by the dynamic yield strength of the shear zone and the gravity. In order to account for the zig-saw slip-history pattern of typical repeated slow slip events, we assume that the shear zone progressively strengthens after each slow slip cycle, possibly caused by dilatancy as commonly assumed or by progressive fault healing through solution-transport mechanisms. We quantify our conceptual model by obtaining simple analytical solutions. Our model results suggest that the duration of the landward motion increases with the down-dip length and the static yield strength of the shear zone, but decreases with the ambient loading velocity and the elastic modulus of the hanging wall. The duration of the backward/trenchward motion depends on the thickness, viscosity, and dynamic yield strength of the shear zone. Our model predicts a linear increase in slip with time during the landward motion and an exponential decrease in slip magnitude during the trenchward motion.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ellen M. Rabenberg; Brian J. Jaques; Bulent H. Sencer

The mechanical properties of AISI 304 stainless steel irradiated for over a decade in the Experimental Breeder Reactor (EBR-II) were measured using miniature mechanical testing methods. The shear punch method was used to evaluate the shear strengths of the neutron-irradiated steel and a correlation factor was empirically determined to predict its tensile strength. The strength of the stainless steel slightly decreased with increasing irradiation temperature, and significantly increased with increasing dose until it saturated above approximately 5 dpa. Ferromagnetic measurements were used to observe and deduce the effects of the stress-induced austenite to martensite transformation as a result of shearmore » punch testing.« less

Shear transfer capacity of reinforced concrete exposed to fire

NASA Astrophysics Data System (ADS)

Ahmad, Subhan; Bhargava, Pradeep; Chourasia, Ajay

2018-04-01

Shear transfer capacity of reinforced concrete elements is a function of concrete compressive strength and reinforcement yield strength. Exposure of concrete and steel to elevated temperature reduces their mechanical properties resulting in reduced shear transfer capacity of RC elements. The objective of present study is to find the effect of elevated temperature on shear transfer capacity of reinforced concrete. For this purpose pushoff specimens were casted using normal strength concrete. After curing, specimens were heated to 250°C and 500°C in an electric furnace. Cooled specimens were tested for shear transfer capacity in a universal testing machine. It was found that shear transfer capacity and stiffness (slope of load-slip curve) were reduced when the specimens were heated to 250°C and 500°C. Load level for the initiation of crack slip was found to be decreased as the temperature was increased. A simple analytical approach is also proposed to predict the shear transfer capacity of reinforced concrete after elevated temperature.

Influence of helium atoms on the shear behavior of the fiber/matrix interphase of SiC/SiC composite

NASA Astrophysics Data System (ADS)

Jin, Enze; Du, Shiyu; Li, Mian; Liu, Chen; He, Shihong; He, Jian; He, Heming

2016-10-01

Silicon carbide has many attractive properties and the SiC/SiC composite has been considered as a promising candidate for nuclear structural materials. Up to now, a computational investigation on the properties of SiC/SiC composite varying in the presence of nuclear fission products is still missing. In this work, the influence of He atoms on the shear behavior of the SiC/SiC interphase is investigated via Molecular Dynamics simulation following our recent paper. Calculations are carried out on three dimensional models of graphite-like PyC/SiC interphase and amorphous PyC/SiC interphase with He atoms in different regions (the SiC region, the interface region and the PyC region). In the graphite-like PyC/SiC interphase, He atoms in the SiC region have little influence on the shear strength of the material, while both the shear strength and friction strength may be enhanced when they are in the PyC region. Low concentration of He atoms in the interface region of the graphite-like PyC/SiC interphase increases the shear strength, while there is a reduction of shear strength when the He concentration is high due to the switch of sliding plane. In the amorphous PyC/SiC interphase, He atoms can cause the reduction of the shear strength regardless of the regions that He atoms are located. The presence of He atoms may significantly alter the structure of SiC/SiC in the interface region. The influence of He atoms in the interface region is the most significant, leading to evident shear strength reduction of the amorphous PyC/SiC interphase with increasing He concentration. The behaviors of the interphases at different temperatures are studied as well. The dependence of the shear strengths of the two types of interphases on temperatures is studied as well. For the graphite-like PyC/SiC interphase, it is found strongly related to the regions He atoms are located. Combining these results with our previous study on pure SiC/SiC system, we expect this work may provide new insight into the mechanism of interphase evolution when SiC/SiC is applied as nuclear materials.

Tribological properties of boron nitride synthesized by ion beam deposition

NASA Technical Reports Server (NTRS)

Miyoshi, K.; Buckley, D. H.; Spalvins, T.

1985-01-01

The adhesion and friction behavior of boron nitride films on 440 C bearing stainless steel substrates was examined. The thin films containing the boron nitride were synthesized using an ion beam extracted from a borazine plasma. Sliding friction experiments were conducted with BN in sliding contact with itself and various transition metals. It is indicated that the surfaces of atomically cleaned BN coating film contain a small amount of oxides and carbides, in addition to boron nitride. The coefficients of friction for the BN in contact with metals are related to the relative chemical activity of the metals. The more active the metal, the higher is the coefficient of friction. The adsorption of oxygen on clean metal and BN increases the shear strength of the metal - BN contact and increases the friction. The friction for BN-BN contact is a function of the shear strength of the elastic contacts. Clean BN surfaces exhibit relatively strong interfacial adhesion and high friction. The presence of adsorbates such as adventitious carbon contaminants on the BN surfaces reduces the shear strength of the contact area. In contrast, chemically adsorbed oxygen enhances the shear strength of the BN-BN contact and increases the friction.

Shear transfer in concrete reinforced with carbon fibers

NASA Astrophysics Data System (ADS)

El-Mokadem, Khaled Mounir

2001-10-01

Scope and method of study. The research started with preliminary tests and studies on the behavior and effect of carbon fibers in different water solutions and mortar/concrete mixes. The research work investigated the use of CF in the production of concrete pipes and prestressed concrete double-tee sections. The research then focused on studying the effect of using carbon fibers on the direct shear transfer of sand-lightweight reinforced concrete push-off specimens. Findings and conclusions. In general, adding carbon fibers to concrete improved its tensile characteristics but decreased its compressive strength. The decrease in compressive strength was due to the decrease in concrete density as fibers act as three-dimensional mesh that entrapped air. The decrease in compressive strength was also due to the increase in the total surface area of non-cementitious material in the concrete. Sand-lightweight reinforced concrete push-off specimens with carbon fibers had lower shear carrying capacity than those without carbon fibers for the same cement content in the concrete. Current building codes and specifications estimate the shear strength of concrete as a ratio of the compressive strength. If applying the same principals then the ratio of shear strength to compressive strength for concrete reinforced with carbon fibers is higher than that for concrete without carbon fibers.

Temperature-dependent ideal strength and stacking fault energy of fcc Ni: a first-principles study of shear deformation.

PubMed

Shang, S L; Wang, W Y; Wang, Y; Du, Y; Zhang, J X; Patel, A D; Liu, Z K

2012-04-18

Variations of energy, stress, and magnetic moment of fcc Ni as a response to shear deformation and the associated ideal shear strength (τ(IS)), intrinsic (γ(SF)) and unstable (γ(US)) stacking fault energies have been studied in terms of first-principles calculations under both the alias and affine shear regimes within the {111} slip plane along the <112> and <110> directions. It is found that (i) the intrinsic stacking fault energy γ(SF) is nearly independent of the shear deformation regimes used, albeit a slightly smaller value is predicted by pure shear (with relaxation) compared to the one from simple shear (without relaxation); (ii) the minimum ideal shear strength τ(IS) is obtained by pure alias shear of {111}<112>; and (iii) the dissociation of the 1/2[110] dislocation into two partial Shockley dislocations (1/6[211] + 1/6[121]) is observed under pure alias shear of {111}<110>. Based on the quasiharmonic approach from first-principles phonon calculations, the predicted γ(SF) has been extended to finite temperatures. In particular, using a proposed quasistatic approach on the basis of the predicted volume versus temperature relation, the temperature dependence of τ(IS) is also obtained. Both the γ(SF) and the τ(IS) of fcc Ni decrease with increasing temperature. The computed ideal shear strengths as well as the intrinsic and unstable stacking fault energies are in favorable accord with experiments and other predictions in the literature.

Shear Capacity of C-Shaped and L-Shaped Angle Shear Connectors

PubMed Central

Tahmasbi, Farzad; Maleki, Shervin; Shariati, Mahdi; Ramli Sulong, N. H.; Tahir, M. M.

2016-01-01

This paper investigates the behaviour of C-shaped and L-shaped angle shear connectors embedded in solid concrete slabs. An effective finite element model is proposed to simulate the push out tests of these shear connectors that encompass nonlinear material behaviour, large displacement and damage plasticity. The finite element models are validated against test results. Parametric studies using this nonlinear model are performed to investigate the variations in concrete strength and connector dimensions. The finite element analyses also confirm the test results that increasing the length of shear connector increases their shear strength proportionately. It is observed that the maximum stress in L-shaped angle connectors takes place in the weld attachment to the beam, whereas in the C-shaped angle connectors, it is in the attached leg. The location of maximum concrete compressive damage is rendered in each case. Finally, a new equation for prediction of the shear capacity of C-shaped angle connectors is proposed. PMID:27478894

Shear Capacity of C-Shaped and L-Shaped Angle Shear Connectors.

PubMed

Tahmasbi, Farzad; Maleki, Shervin; Shariati, Mahdi; Ramli Sulong, N H; Tahir, M M

2016-01-01

This paper investigates the behaviour of C-shaped and L-shaped angle shear connectors embedded in solid concrete slabs. An effective finite element model is proposed to simulate the push out tests of these shear connectors that encompass nonlinear material behaviour, large displacement and damage plasticity. The finite element models are validated against test results. Parametric studies using this nonlinear model are performed to investigate the variations in concrete strength and connector dimensions. The finite element analyses also confirm the test results that increasing the length of shear connector increases their shear strength proportionately. It is observed that the maximum stress in L-shaped angle connectors takes place in the weld attachment to the beam, whereas in the C-shaped angle connectors, it is in the attached leg. The location of maximum concrete compressive damage is rendered in each case. Finally, a new equation for prediction of the shear capacity of C-shaped angle connectors is proposed.

Rectangle-capped and tilted micropillar array for enhanced anisotropic anti-shearing in biomimetic adhesion

PubMed Central

Wang, Yue; Li, Xiangming; Tian, Hongmiao; Hu, Hong; Tian, Yu; Shao, Jinyou; Ding, Yucheng

2015-01-01

Dry adhesion observed in the feet of various small creatures has attracted considerable attention owing to the unique advantages such as self-cleaning, adaptability to rough surfaces along with repeatable and reversible adhesiveness. Among these advantages, for practical applications, proper detachability is critical for dry adhesives with artificial microstructures. In this study, we present a microstructured array consisting of both asymmetric rectangle-capped tip and tilted shafts, which produce an orthogonal anisotropy of the shearing strength along the long and short dimensions of the tip, with a maximum anti-shearing in the two directions along the longer dimension. Meanwhile, the tilt feature can enhance anisotropic shearing adhesion by increasing shearing strength in the forward shearing direction and decreasing strength in the reverse shearing direction along the short dimension of the tip, leading to a minimum anti-shearing in only one of the two directions along the shorter dimension of the rectangular tip. Such a microstructured adhesive with only one weak shearing direction, leading to well-controlled attachment and detachment of the adhesive, is created in our experiment by conventional double-sided exposure of a photoresist followed by a moulding process. PMID:25808338

Study on Shear Performance of Cold-formed Steel Composite Wall with New Type of stud

NASA Astrophysics Data System (ADS)

Wang, Chungang; Yue, Sizhe; Liu, Hong; Zhang, Zhuangnan

2018-03-01

The shear resistance of single oriented-strand board wall and single gypsum board wall can be improved in different degrees by increasing strength of steel. The experimental data of literatures were used, and the test specimens had been simulated and validated by ABAQUS finite element analysis. According to the research, it showed that the compressive bearing capacity of the new stud composite wall was much better than the common stud composite wall, so the establishment and research of all models had been based on the new section stud. The analysis results show that when using new type of stud the shear resistance of the single oriented-strand board wall can be improved efficiently by increasing strength of steel, but the shear resistance of the single gypsum wall can be increased little.

49 CFR 230.27 - Maximum shearing strength of rivets.

Code of Federal Regulations, 2011 CFR

2011-10-01

... 49 Transportation 4 2011-10-01 2011-10-01 false Maximum shearing strength of rivets. 230.27 Section 230.27 Transportation Other Regulations Relating to Transportation (Continued) FEDERAL RAILROAD... Appurtenances Strength of Materials § 230.27 Maximum shearing strength of rivets. The maximum shearing strength...

49 CFR 230.27 - Maximum shearing strength of rivets.

Code of Federal Regulations, 2010 CFR

2010-10-01

... 49 Transportation 4 2010-10-01 2010-10-01 false Maximum shearing strength of rivets. 230.27 Section 230.27 Transportation Other Regulations Relating to Transportation (Continued) FEDERAL RAILROAD... Appurtenances Strength of Materials § 230.27 Maximum shearing strength of rivets. The maximum shearing strength...

Design and Optimization of an Austenitic TRIP Steel for Blast and Fragment Protection

NASA Astrophysics Data System (ADS)

Feinberg, Zechariah Daniel

In light of the pervasive nature of terrorist attacks, there is a pressing need for the design and optimization of next generation materials for blast and fragment protection applications. Sadhukhan used computational tools and a systems-based approach to design TRIP-120---a fully austenitic transformation-induced plasticity (TRIP) steel. Current work more completely evaluates the mechanical properties of the prototype, optimizes the processing for high performance in tension and shear, and builds models for more predictive power of the mechanical behavior and austenite stability. Under quasi-static and dynamic tension and shear, the design exhibits high strength and high uniform ductility as a result of a strain hardening effect that arises with martensitic transformation. Significantly more martensitic transformation occurred under quasi-static loading conditions (69% in tension and 52% in shear) compared to dynamic loading conditions (13% tension and 5% in shear). Nonetheless, significant transformation occurs at high-strain rates which increases strain hardening, delays the onset of necking instability, and increases total energy absorption under adiabatic conditions. Although TRIP-120 effectively utilizes a TRIP effect to delay necking instability, a common trend of abrupt failure with limited fracture ductility was observed in tension and shear at all strain rates. Further characterization of the structure of TRIP-120 showed that an undesired grain boundary cellular reaction (η phase formation) consumed the fine dispersion of the metastable gamma' phase and limited the fracture ductility. A warm working procedure was added to the processing of TRIP-120 in order to eliminate the grain boundary cellular reaction from the structure. By eliminating η formation at the grain boundaries, warm-worked TRIP-120 exhibits a drastic improvement in the mechanical properties in tension and shear. In quasi-static tension, the optimized warm-worked TRIP-120 with an Mssigma( u.t.) of -13°C has a yield strength of 180 ksi (1241 MPa), uniform ductility of 0.303, and fracture ductility of 0.95, which corresponds to a 48% increase in yield strength, a 43% increase in uniform ductility, and a 254% increase in fracture ductility relative to the designed processing of TRIP-120. The highest performing condition of warm-worked TRIP-120 in quasi-static shear with an Mssigma( sh) of 58°C exhibits a shear yield strength of 95.1 ksi (656 MPa), shear fracture strain of 144%, and energy dissipation density of 1099 MJ/m3, which corresponds to a shear yield strength increase of 61%, a shear fracture strain increase of 55%, and an energy dissipation density increase of 76%. A wide range of austenite stabilities can be achieved by altering the heat treatment times and temperatures, which significantly alters the mechanical properties. Although performance cannot be optimized for tension and shear simultaneously, different heat treatments can be applied to warm-worked TRIP-120 to achieve high performance in tension or shear. Parametric models calibrated with three-dimensional atom probe data played a crucial role in guiding the predictive process optimization of TRIP-120. Such models have been built to provide the predictive capability of inputting warm working and aging conditions and outputting the resulting structure, austenite stability, and mechanical properties. The predictive power of computational models has helped identify processing conditions that have improved the performance of TRIP-120 in tension and shear and can be applied to future designs that optimize for adiabatic conditions.

The Magnetohydrodynamic Kelvin-Helmholtz Instability. III. The Role of Sheared Magnetic Field in Planar Flows

NASA Astrophysics Data System (ADS)

Jeong, Hyunju; Ryu, Dongsu; Jones, T. W.; Frank, Adam

2000-01-01

We have carried out simulations of the nonlinear evolution of the magnetohydrodynamic (MHD) Kelvin-Helmholtz (KH) instability for compressible fluids in 2.5 dimensions, extending our previous work by Frank et al. and Jones et al. In the present work we have simulated flows in the x-y plane in which a ``sheared'' magnetic field of uniform strength smoothly rotates across a thin velocity shear layer from the z-direction to the x-direction, aligned with the flow field. The sonic Mach number of the velocity transition is unity. Such flows containing a uniform field in the x-direction are linearly stable if the magnetic field strength is great enough that the Alfvénic Mach number MA=U0/cA<2. That limit does not apply directly to sheared magnetic fields, however, since the z-field component has almost no influence on the linear stability. Thus, if the magnetic shear layer is contained within the velocity shear layer, the KH instability may still grow, even when the field strength is quite large. So, here we consider a wide range of sheared field strengths covering Alfvénic Mach numbers, MA=142.9 to 2. We focus on dynamical evolution of fluid features, kinetic energy dissipation, and mixing of the fluid between the two layers, considering their dependence on magnetic field strength for this geometry. There are a number of differences from our earlier simulations with uniform magnetic fields in the x-y plane. For the latter, simpler case we found a clear sequence of behaviors with increasing field strength ranging from nearly hydrodynamic flows in which the instability evolves to an almost steady cat's eye vortex with enhanced dissipation, to flows in which the magnetic field disrupts the cat's eye once it forms, to, finally, flows that evolve very little before field-line stretching stabilizes the velocity shear layer. The introduction of magnetic shear can allow a cat's eye-like vortex to form, even when the field is stronger than the nominal linear instability limit given above. For strong fields that vortex is asymmetric with respect to the preliminary shear layer, however, so the subsequent dissipation is enhanced over the uniform field cases of comparable field strength. In fact, so long as the magnetic field achieves some level of dynamical importance during an eddy turnover time, the asymmetries introduced through the magnetic shear will increase flow complexity and, with that, dissipation and mixing. The degree of the fluid mixing between the two layers is strongly influenced by the magnetic field strength. Mixing of the fluid is most effective when the vortex is disrupted by magnetic tension during transient reconnection, through local chaotic behavior that follows.

The Role of Fine Sediment Content on Soil Consolidation and Debris Flows Development after Earthquake

NASA Astrophysics Data System (ADS)

Lyu, L.; Xu, M., III; Wang, Z.

2017-12-01

Fine sediment has been identified as an important factor determining the critical runoff that initiates debris flows because its contribution to shear strength through consolidation. Especially, owing to the 2008 Wenchuan earthquake in China enormous of loose sediment with different fractions of fine particles was eroded and supplied as materials for debris flows. The loose materials are gradually consolidated along with time, and therefore stronger rainfall is required to overcome the shear strength and to initiate debris flows. In this study, flume experiments were performed to explore soil consolidation and shear strength on mass failure and debris flow initiation under the conditions that different fractions of fine sediment were contained in the materials. Under the low content of fine sediment conditions (mass percentages: 0-10%), the debris flows formed with large pores and low shear strength and thus fine particles were too few to fill up the pores among the coarse particles. The consolidation rate was mostly influenced by the content of the fine particles. Consolidation of fine particles caused an increase of the shear strength and decrease of the rainfall infiltration, and therefore, debris flow initiation required stronger rainfall as the consolidation of the fine particles developed.

Influences of Shear History and Infilling on the Mechanical Characteristics and Acoustic Emissions of Joints

NASA Astrophysics Data System (ADS)

Meng, Fanzhen; Zhou, Hui; Wang, Zaiquan; Zhang, Liming; Kong, Liang; Li, Shaojun; Zhang, Chuanqing

2017-08-01

Filled joints, which are characterized by high deformability and low shear strength, are among the most critical discontinuities in rock mass and may be sheared repeatedly when subject to cyclic loading. Shear tests were carried out on tension splitting joints, with soil and granular cement mortar particles used as infillings, and the effects of the shear history on the mechanical behavior and acoustic emission (AE) of clean and filled joints were studied. The maximum strength in the subsequent shears was approximately 60% of the peak strength of the first shear for a clean joint, and the friction angle degraded from 63° to 45° after the first shear. The maximum shear strength of the filled joints was lower than 35% of the peak strength of the clean joint under the same normal stress. The change in the shear strength of filled joints with the number of shearing cycles was closely related to the transformation of the shear medium. Rolling friction occurred and the shear strength was low for the granular particle-filled joint, but the strength was elevated when the particles were crushed and sliding friction occurred. The AEs were significantly reduced during the second shear for the clean joint, and the peak AEs were mainly obtained at or near the turning point of the shear stress curve for the filled joint. The AEs were the highest for the cement particle-filled joint and lowest for the dry soil-filled joint; when subjected to repeated shears, the AEs were more complex because of the continuous changes to the shear medium. The evolution of the AEs with the shear displacement can accurately reflect the shear failure mechanism during a single shear process.

The influence of cyclic shear fatigue on the bracket-adhesive-enamel complex: an in vitro study.

PubMed

Daratsianos, Nikolaos; Musabegovic, Ena; Reimann, Susanne; Grüner, Manfred; Jäger, Andreas; Bourauel, Christoph

2013-05-01

To describe the effect of fatigue on the strength of the bracket-adhesive-enamel complex and characterize the fatigue behavior of the materials tested. Upper central incisor brackets (Discovery(®), Dentaurum) were bonded with a light-curing (Transbond XT™, 3M Unitek) and a chemically-curing adhesive (Concise™, 3M Unitek) on bovine teeth embedded in cylindrical resign bases and stored in water at 37(±2)°C for 24 (±2)h. The first 15 specimens were tested with a universal testing machine ZMART.PRO(®) (Zwick GmbH & Co. KG, Ulm, Germany) for ultimate shear bond strength according to the DIN-13990-2-standard. The remaining three groups of 20 specimens underwent fatigue staircase testing of 100, 1000 and 3000 cycles at 1Hz with a self-made testing machine. The survived specimens were subjected to shear strength testing. The fatigued specimens showed decreased shear strength with both adhesives at all cycle levels. The shear strength after fatigue for 100, 1000 and 3000 cycles was in the Concise™-groups 34.8%, 59.0%, 47.3% and in the Transbond™ XT-groups 33.6%, 23.1%, 27.3% relative to the ultimate shear strength. The fatigue life of the Concise™-groups decreased with increasing stress and Transbond™ XT showed lower fatigue ratio with no obvious trend. The specimens bonded with Transbond™ XT showed typically favorable fracture modes in contrary to Concise™. Fatigue of the bracket-adhesive-enamel complex decreased its shear strength. The staircase method can provide a standardized experimental protocol for fatigue studies, however testing at various cycle numbers is recommended. Copyright © 2013 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Standard Methods for Bolt-Bearing Testing of Textile Composites

NASA Technical Reports Server (NTRS)

Portanova, M. A.; Masters, J. E.

1995-01-01

The response of three 2-D braided materials to bolt bearing loading was evaluated using data generated by Boeing Defense and Space Group in Philadelphia, PA. Three test methods, stabilized single shear, unstabilized single shear, and double shear, were compared. In general, these textile composites were found to be sensitive to bolt bearing test methods. The stabilized single shear method yielded higher strengths than the unstabilized single shear method in all cases. The double shear test method always produced the highest strengths but these results may be somewhat misleading. It is therefore recommended that standard material comparisons be made using the stabilized single shear test method. The effects of two geometric parameters, W/D and e/D, were also studied. An evaluation of the effect of the specimen width (W) to hole diameter (D) ratio concluded that bolt bearing responses were consistent with open hole tension results. A W/D ratio of 6 or greater should be maintained. The proximity of the hole to the specimen edge significantly affected strength. In all cases, strength was improved by increasing the ratio of the distance from the hole center to the specimen edge (e) to the hole diameter (D) above 2. An e/D ratio of 3 or greater is recommended.

Ultrasonic evaluation of the strength of unidirectional graphite-polyimide composites

NASA Technical Reports Server (NTRS)

Vary, A.; Bowles, K. J.

1977-01-01

An acoustic-ultrasonic method is described that was successful in ranking unidirectional graphite-polyimide composite specimens according to variations in interlaminar shear strength. Using this method, a quantity termed the stress wave factor was determined. It was found that this factor increases directly with interlaminar shear strength. The key variables in this investigation were composite density, fiber weight fraction, and void content. The stress wave factor and other ultrasonic factors that were studied were found to provide a powerful means for nondestructive evaluation of mechanical strength properties.

The Effect of CuO Nanoparticles on Antimicrobial Effects and Shear Bond Strength of Orthodontic Adhesives

PubMed Central

Toodehzaeim, Mohammad Hossein; Zandi, Hengameh; Meshkani, Hamidreza; Hosseinzadeh Firouzabadi, Azadeh

2018-01-01

Statement of the Problem: Orthodontic appliances facilitate microbial plaque accumulation and increase the chance of white spot lesions. There is a need for new plaque control methods independent of patient's cooperation. Purpose: The aim of this study was to determine the effects of incorporating copper oxide (CuO) nanoparticles on antimicrobial properties and bond strength of orthodontic adhesive. Materials and Method: CuO nanoparticles were added to the composite transbond XT at concentrations of 0.01, 0.5 and 1 wt.%. To evaluate the antimicrobial properties of composites containing nanoparticles, the disk agar diffusion test was used. For this purpose, 10 discs from each concentration of nano-composites (totally 30 discs) and 10 discs from conventional composite (as the control group) were prepared. Then the diameter of streptococcus mutans growth inhibition around each disc was determined in blood agar medium. To evaluate the shear bond strength, with each concentration of nano-composites as well as the control group (conventional composite), 10 metal brackets were bonded to the human premolars and shear bond strength was determined using a universal testing machine. Results: Nano-composites in all three concentrations showed significant antimicrobial effect compared to the control group (p< 0.001). With increasing concentration of nanoparticles, antimicrobial effect showed an upward trend, although statistically was not significant. There was no significant difference between the shear bond strength of nano-composites compared to control group (p= 0.695). Conclusion: Incorporating CuO nanoparticles into adhesive in all three studied concentrations added antimicrobial effects to the adhesive with no adverse effects on shear bond strength. PMID:29492409

The Effect of CuO Nanoparticles on Antimicrobial Effects and Shear Bond Strength of Orthodontic Adhesives.

PubMed

Toodehzaeim, Mohammad Hossein; Zandi, Hengameh; Meshkani, Hamidreza; Hosseinzadeh Firouzabadi, Azadeh

2018-03-01

Orthodontic appliances facilitate microbial plaque accumulation and increase the chance of white spot lesions. There is a need for new plaque control methods independent of patient's cooperation. The aim of this study was to determine the effects of incorporating copper oxide (CuO) nanoparticles on antimicrobial properties and bond strength of orthodontic adhesive. CuO nanoparticles were added to the composite transbond XT at concentrations of 0.01, 0.5 and 1 wt.%. To evaluate the antimicrobial properties of composites containing nanoparticles, the disk agar diffusion test was used. For this purpose, 10 discs from each concentration of nano-composites (totally 30 discs) and 10 discs from conventional composite (as the control group) were prepared. Then the diameter of streptococcus mutans growth inhibition around each disc was determined in blood agar medium. To evaluate the shear bond strength, with each concentration of nano-composites as well as the control group (conventional composite), 10 metal brackets were bonded to the human premolars and shear bond strength was determined using a universal testing machine. Nano-composites in all three concentrations showed significant antimicrobial effect compared to the control group ( p < 0.001). With increasing concentration of nanoparticles, antimicrobial effect showed an upward trend, although statistically was not significant. There was no significant difference between the shear bond strength of nano-composites compared to control group ( p = 0.695). Incorporating CuO nanoparticles into adhesive in all three studied concentrations added antimicrobial effects to the adhesive with no adverse effects on shear bond strength.

Effects of two soft drinks on shear bond strength and adhesive remnant index of orthodontic metal brackets.

PubMed

Sajadi, Soodabeh Sadat; Eslami Amirabadi, Gholamreza; Sajadi, Sepideh

2014-07-01

Bond failure of brackets during orthodontic treatment is a common problem; which results in treatment interference, increased treatment time and prolonged clinical time for rebonding of failed brackets. The purpose of this study was to evaluate the effects of Coca-Cola and a non-alcoholic beer on the shear bond strength and adhesive remnant index (ARI) of orthodontic metal brackets in vitro. Eighty intact human premolars were divided into two experimental groups of Coca-Cola and non-alcoholic beer (Istak), and a control group of artificial saliva. Over a period of thirty days, the test groups were immersed in the respective soft drinks for 5 minutes, twice a day. For the remainder of the time, they were kept in artificial saliva at 37°C. The control group was stored in artificial saliva during the experiment. All samples were subjected to shearing forces using Universal Testing Machine. ARI was determined with a stereomicroscope at ×12 magnification. The data of shear bond strength were statistically analyzed by one-way ANOVA and Tukey's Post-Hoc test and the data of ARI scores were analyzed by Kruskal-Wallis test. No significant difference was observed in ARIs of the three groups (P≤ 0.552). The shear bond strength of Coke group was significantly lower than that of the two other groups (P≤ 0.035); but there was no significant difference between the shear bond strength of Istak and the control group (P≤ 0.999). Coca-Cola decreased the shear bond strength of orthodontic brackets.

A method to determine shear adhesive strength of fibrin sealants.

PubMed

Sierra, D H; Feldman, D S; Saltz, R; Huang, S

1992-01-01

The adhesive strength of fibrin sealants has not been rigorously evaluated to date. The adhesive strength of six different concentrations of cryoprecipitated fibrinogen as well as the commercially available fibrin tissue adhesive Tissucol was tested under controlled conditions utilizing split-thickness skin grafts as the test adherand. This test configuration permitted the modeling of bonding strength for attachment of skin grafts as well as incorporate established engineering test standards for adhesives. An increase in fibrin concentration corresponded with an increase in shear adhesive strength. No significant increases in adhesive strength were attained after 5 min of bonding for all tested concentrations, except for the commercial adhesive, which attained the adhesive strength of an equivalent concentration of cryoprecipitated adhesive after 90 min. The adhesive strength, however, was an order of magnitude less than reported values of the tensile strength of fibrin material for similar concentrations. Therefore, it is important that the surgeon use a sufficiently high fibrinogen concentration for the specific clinical indication. The method of fibrin sealant preparation and/or the compounding adjuncts appear to have an effect on the development of adhesive strength.

In-plane and Interlaminar Shear Strength of a Unidirectional Hi-nicalon Fiber-reinforced Celsian Matrix Composite

NASA Technical Reports Server (NTRS)

Uenal, O.; Bansal, N. P.

2000-01-01

In-plane and interlaminar shear strength of a unidirectional SiC fiber-reinforced (BaSr)Al2Si2O8 celsian composite were measured by the double-notch shear test method between room temperature and 1200 C. The interlaminar shear strength was lower than the in-plane shear strength at all temperatures. Stress analysis, using finite element modeling, indicated that shear stress concentration was not responsible for the observed difference in strength. Instead, the difference in layer architecture and thus, the favorable alignment of fiber-rich layers with the shear plane in the interlaminar specimens appears to be the reason for the low strength of this composite. A rapid decrease in strength was observed with temperature due to softening of the glassy phase in the material.

Comparison of shear bond strength of brackets recycled using micro sandblasting and industrial methods.

PubMed

Montero, Manuela M Haro; Vicente, Ascensión; Alfonso-Hernández, Noelia; Jiménez-López, Manuel; Bravo-González, Luis-Alberto

2015-05-01

To evaluate in vitro the shear bond strength of brackets recycled by sandblasting with aluminum oxide particles of different sizes or reconditioned industrially after successive rebonding. Eighty brackets were bonded and debonded sequentially three times. After the first debonding, brackets were divided into four groups: (group 1) sandblasting with aluminum oxide particles of 25 μ, (group 2) 50 μ, and (group 3) 110 μ, and (group 4) industrial recycling. Bond strength and adhesive material remaining on debonded bracket bases were evaluated for each successive debond. No significant differences were detected between the four groups following the first recycle (P > .05). After the second recycle, bond strength was significantly greater for the industrially recycled group than the other groups (P < .016). When shear bond strength was compared within each recycling method, the bond strength of sandblasted brackets decreased with the increase of particle size and with each recycle; for the industrially recycled group, no significant differences were detected between the three sequences (P > .016). In the evaluation of bond material remnant, the industrially recycled group left significantly less bond material after successive recycling than the other groups did (P < .016). Within each recycling method, the adhesive remnant decreased significantly after successive debond (P < .016). Industrial recycling obtained better results than sandblasting after three successive debondings. The brackets' shear bond strength decreased as the size of the aluminum oxide particle used for sandblasting increased and as recycling was repeated.

Effect of surface treatment on bond strength between an indirect composite material and a zirconia framework.

PubMed

Komine, Futoshi; Fushiki, Ryosuke; Koizuka, Mai; Taguchi, Kohei; Kamio, Shingo; Matsumura, Hideo

2012-03-01

The present study evaluated the effect of various surface treatments for zirconia ceramics on shear bond strength between an indirect composite material and zirconia ceramics. In addition, we investigated the durability of shear bond strength by using artificial aging (20,000 thermocycles). A total of 176 Katana zirconia disks were randomly divided into eight groups according to surface treatment, as follows: group CON (as-milled); group GRD (wet-ground with 600-grit silicon carbide abrasive paper); groups 0.05, 0.1, 0.2, 0.4, and 0.6 MPa (airborne-particle abrasion at 0.05, 0.1, 0.2, 0.4, and 0.6 MPa, respectively); and group HF (9.5% hydrofluoric acid etching). Shear bond strength was measured at 0 thermocycles in half the specimens after 24-h immersion. The remaining specimens were subjected to 20,000 thermocycles before shear bond strength testing. Among the eight groups, the 0.1, 0.2, 0.4, and 0.6 MPa airborne-particle abraded groups had significantly higher bond strengths before and after thermocycling. The Mann-Whitney U-test revealed no significant difference in shear bond strength between 0 and 20,000 thermocycles, except in the 0.2 MPa group (P = 0.013). From the results of this study, use of airborne-particle abrasion at a pressure of 0.1 MPa or higher increases initial and durable bond strength between an indirect composite material and zirconia ceramics.

Dynamic shear strength of S2 glass fiber reinforced polymer composites under shock compression

NASA Astrophysics Data System (ADS)

Yuan, Fuping; Tsai, Liren; Prakash, Vikas; Dandekar, Dattatraya P.; Rajendran, A. M.

2008-05-01

In the present paper, a series of plate impact shock-reshock and shock-release experiments were conducted to study the critical shear strength of a S2 glass fiber reinforced polymer (GRP) composite under shock compression levels ranging from 0.8 to 1.8 GPa. The GRP was fabricated at ARL, Aberdeen, using S2 glass woven roving in a Cycom 4102 polyester resin matrix. The experiments were conducted by using an 82.5 mm bore single-stage gas gun at Case Western Reserve University. In order to conduct shock-reshock and shock-release experiments a dual flyer plate assembly was utilized. The shock-reshock experiments were conducted by using a projectile faced with GRP and backed with a relatively high shock impedance Al 6061-T6 plate; while for the shock-release experiments the GRP was backed by a relatively lower impedance polymethyl methacrylate backup flyer plate. A multibeam velocity interferometer was used to measure the particle velocity profile at the rear surface of the target plate. By using self-consistent technique procedure described by Asay and Chabbildas [Shock Waves and High-Strain-Rate Phenomena, in Metals, edited by M. M. Myers and L. E. Murr (Plenum, New York, 1981), pp. 417-431], the critical shear strength of the GRP (2τc) was determined for impact stresses in the range of 0.8 to 1.8 GPa. The results show that the critical shear strength of the GRP is increased from 0.108 GPa to 0.682 GPa when the impact stress is increased from 0.8 to 1.8 GPa. The increase in critical shear strength may be attributed to rate-dependence and/or pressure dependent yield behavior of the GRP.

Experimental study on the strength of double shear timber connection using bamboo dowel fastener

NASA Astrophysics Data System (ADS)

Anshari, Buan; Sugiartha, Wayan; Mahmud, Fathmah; Rofaida, Aryani; Pathurrahman

2017-11-01

Utilization of timber and bamboo as building materials was very promising for now and future. As renewable resources they have high mechanical properties, lightweight, environmentally friendly and economic. Utilization of bamboo as connector was rarely published. Therefore, this study focused on utilization of non-metal material as connector in timber structure especially for beam and column. This research was conducted in the laboratory to examine the strength of double shear timber connection by using glued in rods (bamboo dowel) as connector with variation of adhesive thickness. As control specimen was used bamboo dowel Ø14 mm without adhesive in double shear connection. The results showed that the strength of double shear timber connection by using glued in rods (bamboo dowel) as connector could increased by 41% to resist axial force higher than the control one.

Lap shear strength and healing capability of self-healing adhesive containing epoxy/mercaptan microcapsules

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ghazali, Habibah; Ye, Lin; Zhang, Ming-Qiu

The aim of this work is to develop a self-healing polymeric adhesive formulation with epoxy/mercaptan microcapsules. Epoxy/mercaptan microcapsules were dispersed into a commercialize two-part epoxy adhesive for developing self-healing epoxy adhesive. The influence of different content of microcapsules on the shear strength and healing capability of epoxy adhesive were investigated using single-lap-joints with average thickness of adhesive layer of about 180 µm. This self-healing adhesive was used in bonding of 5000 series aluminum alloys adherents after mechanical and alkaline cleaning surface treatment. The adhesion strength was measured and presented as function of microcapsules loading. The results indicated that the virgin lapmore » shear strength was increased by about 26% with addition of 3 wt% of self-healing microcapsules. 12% to 28% recovery of the shear strength is achieved after self-healing depending on the microcapsules content. Scanning electron microscopy was used to study fracture surface of the joints. The self-healing adhesives exhibit recovery of both cohesion and adhesion properties with room temperature healing.« less

Behavior of Fiber Glass Bolts, Rock Bolts and Cable Bolts in Shear

NASA Astrophysics Data System (ADS)

Li, Xuwei; Aziz, Naj; Mirzaghorbanali, Ali; Nemcik, Jan

2016-07-01

This paper experimentally compares the shear behavior of fiber glass (FG) bolt, rock bolt (steel rebar bolt) and cable bolt for the bolt contribution to bolted concrete surface shear strength, and bolt failure mode. Two double shear apparatuses of different size were used for the study. The tensile strength, the shear strength and the deformation modulus of bolt control the shear behavior of a sheared bolted joint. Since the strength and deformation modulus of FG bolt, rock bolt and cable bolt obtained from uniaxial tensile tests are different, their shear behavior in reinforcing joints is accordingly different. Test results showed that the shear stiffness of FG bolted joints decreased gradually from the beginning to end, while the shear stiffness of joints reinforced by rock bolt and cable bolt decreased bi-linearly, which is clearly consistent with their tensile deformation modulus. The bolted joint shear stiffness was highly influenced by bolt pretension in the high stiffness stage for both rock bolt and cable bolt, but not in the low stiffness stage. The rock bolt contribution to joint shear strength standardised by the bolt tensile strength was the largest, followed by cable bolts, then FG bolts. Both the rock bolts and cable bolts tended to fail in tension, while FG bolts in shear due to their low shear strength and constant deformation modulus.

Study on In-mold Punching during PPS/GF Injection Molding

NASA Astrophysics Data System (ADS)

Inuzuka, Takayuki; Fujita, Akihiro; Nakai, Asami; Hamada, Hiroyuki

The influence of the punching condition on strength and the amount of shear droop was investigated to optimize the processing condition for punching in the mold during glass fiber reinforced polyphenylenesulfide (PPS/GF) injection molding. For in-mold punching part during cooling process, the tensile strength was constant because the pressure loss by the punch did not occur. The amount of the shear droop decreased in line with the increase in delay time because the rigidity of injection molded part in the mold increased when the resin was cooled. Moreover, when the resin temperature lowered more than the glass transition temperature, the amount of the shear droop was constant because the rigidity became constant. It is necessary to begin punching when the resin temperature lowers more than the glass transition temperature after holding pressure process is completed, to secure high strength and to assume 0.05 mm or less, at which level the shear droop cannot be visually recognized. The shortest delay time for PPS/GF is 8 sec. The delay time to minimize the amount of the shear droop can be guessed by analyzing the temperature change of the resin in the mold by injection molding CAE.

Elevated-Temperature Mechanical Properties of Lead-Free Sn-0.7Cu- xSiC Nanocomposite Solders

NASA Astrophysics Data System (ADS)

Mohammadi, A.; Mahmudi, R.

2018-02-01

Mechanical properties of Sn-0.7 wt.%Cu lead-free solder alloy reinforced with 0 vol.%, 1 vol.%, 2 vol.%, and 3 vol.% 100-nm SiC particles have been assessed using the shear punch testing technique in the temperature range from 25°C to 125°C. The composite materials were fabricated by the powder metallurgy route by blending, compacting, sintering, and finally extrusion. The 2 vol.% SiC-containing composite showed superior mechanical properties. In all conditions, the shear strength was adversely affected by increasing test temperature, and the 2 vol.% SiC-containing composite showed superior mechanical properties. Depending on the test temperature, the shear yield stress and ultimate shear strength increased, respectively, by 3 MPa to 4 MPa and 4 MPa to 5.5 MPa, in the composite materials. The strength enhancement was mostly attributed to the Orowan particle strengthening mechanism due to the SiC nanoparticles, and to a lesser extent to the coefficient of thermal expansion mismatch between the particles and matrix in the composite solder. A modified shear lag model was used to predict the total strengthening achieved by particle addition, based on the contribution of each of the above mechanisms.

Prediction of soil stress-strain response incorporates mobilised shear strength envelope of granitic residual soil

NASA Astrophysics Data System (ADS)

Rahman, Abdul Samad Abdul; Noor, Mohd Jamaludin Md; Ahmad, Juhaizad Bin; Sidek, Norbaya

2017-10-01

The concept of effective stress has been the principal concept in characterizing soil volume change behavior in soil mechanics, the settlement models developed using this concept have been empirical in nature. However, there remain certain unexplained soil volume change behaviors that cannot be explained using the effective stress concept, one such behaviour is the inundation settlement. Studies have begun to indicate the inevitable role of shear strength as a critical element to be incorporated in models to unravel the unexplained soil behaviours. One soil volume change model that applies the concept of effective stress and the shear strength interaction is the Rotational Multiple Yield Surface Framework (RMYSF) model. This model has been developed from the soil-strain behavior under anisotropic stress condition. Hence, the RMYSF actually measure the soil actual elasto-plastic response to stress rather than assuming it to be fully elastic or plastic as normally perceived by the industry. The frameworks measures the increase in the mobilize shear strength when the soil undergo anisotropic settlement.

Introducing biomimetic shear and ion gradients to microfluidic spinning improves silk fiber strength.

PubMed

Li, David; Jacobsen, Matthew M; Gyune Rim, Nae; Backman, Daniel; Kaplan, David L; Wong, Joyce Y

2017-05-31

Silkworm silk is an attractive biopolymer for biomedical applications due to its high mechanical strength and biocompatibility; as a result, there is increasing interest in scalable devices to spin silk and recombinant silk so as to improve and customize their properties for diverse biomedical purposes (Vepari and Kaplan 2007 Prog. Polym. Sci. 32 ). While artificial spinning of regenerated silk fibroins adds tunability to properties such as degradation rate and surface functionalization, the resulting fibers do not yet approach the mechanical strength of native silkworm silk. These drawbacks reduce the applicability and attractiveness of artificial silk (Kinahan et al 2011 Biomacromolecules 12 ). Here, we used computational fluid dynamic simulations to incorporate shear in tandem with biomimetic ion gradients by coupling a modular novel glass microfluidic device to our previous co-axial flow device. Fibers spun with this combined apparatus demonstrated a significant increase in mechanical strength compared to fibers spun with the basic apparatus alone, with a three-fold increase in Young's modulus and extensibility and a twelve-fold increase in toughness. These results thus demonstrate the critical importance of ionic milieu and shear stress in spinning strong fibers from solubilized silk fibroin.

A novel method of testing the shear strength of thick honeycomb composites

NASA Technical Reports Server (NTRS)

Hodge, A. J.; Nettles, A. T.

1991-01-01

Sandwich composites of aluminum and glass/phenolic honeycomb core were tested for shear strength before and after impact damage. The assessment of shear strength was performed in two ways; by four point bend testing of sandwich beams and by a novel double lap shear (DLS) test. This testing technique was developed so smaller specimens could be used, thus making the use of common lab scale fabrication and testing possible. The two techniques yielded similar data. The DLS test gave slightly lower shear strength values of the two methods but were closer to the supplier's values for shear strength.

Dynamic strength, particle deformation, and fracture within fluids with impact-activated microstructures

NASA Astrophysics Data System (ADS)

Petel, Oren E.; Ouellet, Simon

2017-07-01

The evolution of material strength within several dense particle suspensions impacted by a projectile is investigated and shown to be strongly dependent on the particle material in suspension. For stronger particles, such as silicon carbide, the shear strength of the fluid is shown to increase with the ballistic impact strength. For weaker particles, such as silica, the shear strength of the suspension is found to be independent of impact strength in this dynamic range of tests. A soft-capture technique is employed to collect ejecta samples of a silica-based shear thickening fluid, following a ballistic impact and penetration event. Ejecta samples that were collected from impacts at three different velocities are observed and compared to the benchmark particles using a Scanning Electron Microscope. The images show evidence of fractured and deformed silica particles recovered among the nominally 1 μm diameter monodisperse spheres. There is also evidence of particle fragments that appear to be the result of interparticle grinding. The trends observed in the shear strength estimates are interpreted with regards to the particle damage seen in the ejecta recovery experiments to develop a concept of the impact response of these fluids. The results suggest that particle slip through deformation is likely the dominant factor in limiting the transient impact strength of these fluids. Particularly, particle strength is important in the formation and collapse of dynamically jammed particle contact networks in the penetration process.

Torsional Shear Strength Tests for Glass-Ceramic Joined Silicon Carbide

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ferraris, Monica; Ventrella, Andrea; Salvo, Milena

2014-03-17

A torsion test on hour-glass-shaped samples with a full joined or a ring-shaped joined area was chosen in this study to measure shear strength of glass-ceramic joined silicon carbide. Shear strength of about 100 MPa was measured for full joined SiC with fracture completely inside their joined area. Attempts to obtain this shear strength with a ring-shaped joined area failed due to mixed mode fractures. However, full joined and ring-shaped steel hour-glasses joined by a glass-ceramic gave the same shear strength, thus suggesting that this test measures shear strength of joined components only when their fracture is completely inside theirmore » joined area.« less

Enhanced tendon-to-bone repair through adhesive films.

PubMed

Linderman, Stephen W; Golman, Mikhail; Gardner, Thomas R; Birman, Victor; Levine, William N; Genin, Guy M; Thomopoulos, Stavros

2018-04-01

Tendon-to-bone surgical repairs have unacceptably high failure rates, possibly due to their inability to recreate the load transfer mechanisms of the native enthesis. Instead of distributing load across a wide attachment footprint area, surgical repairs concentrate shear stress on a small number of suture anchor points. This motivates development of technologies that distribute shear stresses away from suture anchors and across the enthesis footprint. Here, we present predictions and proof-of-concept experiments showing that mechanically-optimized adhesive films can mimic the natural load transfer mechanisms of the healthy attachment and increase the load tolerance of a repair. Mechanical optimization, based upon a shear lag model corroborated by a finite element analysis, revealed that adhesives with relatively high strength and low stiffness can, theoretically, strengthen tendon-to-bone repairs by over 10-fold. Lap shear testing using tendon and bone planks validated the mechanical models for a range of adhesive stiffnesses and strengths. Ex vivo human supraspinatus repairs of cadaveric tissues using multipartite adhesives showed substantial increase in strength. Results suggest that adhesive-enhanced repair can improve repair strength, and motivate a search for optimal adhesives. Current surgical techniques for tendon-to-bone repair have unacceptably high failure rates, indicating that the initial repair strength is insufficient to prevent gapping or rupture. In the rotator cuff, repair techniques apply compression over the repair interface to achieve contact healing between tendon and bone, but transfer almost all force in shear across only a few points where sutures puncture the tendon. Therefore, we evaluated the ability of an adhesive film, implanted between tendon and bone, to enhance repair strength and minimize the likelihood of rupture. Mechanical models demonstrated that optimally designed adhesives would improve repair strength by over 10-fold. Experiments using idealized and clinically-relevant repairs validated these models. This work demonstrates an opportunity to dramatically improve tendon-to-bone repair strength using adhesive films with appropriate material properties. Copyright © 2018 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

A Comparison between Shear Bond Strength of VMK Master Porcelain with Three Base-metal Alloys (Ni-cr-T3, VeraBond, Super Cast) and One Noble Alloy (X-33) in Metal-ceramic Restorations

PubMed Central

Ahmadzadeh, A; Neshati, A; Mousavi, N; Epakchi, S; Dabaghi Tabriz, F; Sarbazi, AH

2013-01-01

Statement of Problem: The increase in the use of metal-ceramic restorations and a high prevalence of porcelain chipping entails introducing an alloy which is more compatible with porcelain and causes a stronger bond between the two. This study is to compare shear bond strength of three base-metal alloys and one noble alloy with the commonly used VMK Master Porcelain. Materials and Method: Three different groups of base-metal alloys (Ni-cr-T3, Super Cast, and VeraBond) and one group of noble alloy (X-33) were selected. Each group consisted of 15 alloy samples. All groups went through the casting process and change from wax pattern into metal disks. The VMK Master Porcelain was then fired on each group. All the specimens were put in the UTM; a shear force was loaded until a fracture occurred and the fracture force was consequently recorded. The data were analyzed by SPSS Version 16 and One-Way ANOVA was run to compare the shear strength between the groups. Furthermore, the groups were compared two-by-two by adopting Tukey test. Results: The findings of this study revealed shear bond strength of Ni-Cr-T3 alloy was higher than the three other alloys (94 MPa or 330 N). Super Cast alloy had the second greatest shear bond strength (80. 87Mpa or 283.87 N). Both VeraBond (69.66 MPa or 245 N) and x-33 alloys (66.53 MPa or 234 N) took the third place. Conclusion: Ni-Cr-T3 with VMK Master Porcelain has the greatest shear bond strength. Therefore, employment of this low-cost alloy is recommended in metal-ceramic restorations. PMID:24724144

Influence of the number of cycles on shear fatigue strength of resin composite bonded to enamel and dentin using dental adhesives in self-etching mode.

PubMed

Tsujimoto, Akimasa; Barkmeier, Wayne W; Erickson, Robert L; Takamizawa, Toshiki; Latta, Mark A; Miyazaki, Masashi

2018-01-30

The influence of the number of cycles on shear fatigue strength to enamel and dentin using dental adhesives in self-etch mode was investigated. A two-step self-etch adhesive and two universal adhesives were used to bond to enamel and dentin in self-etch mode. Initial shear bond strength and shear fatigue strength to enamel and dentin using the adhesive in self-etch mode were determined. Fatigue testing was used with 20 Hz frequency and cycling periods of 50,000, 100,000 and 1,000,000 cycles, or until failure occurred. For each of the cycling periods, there was no significant difference in shear fatigue strength across the cycling periods for the individual adhesives. Differences in shear fatigue strength were found between the adhesives within the cycling periods. Regardless of the adhesive used in self-etch mode for bonding to enamel or dentin, shear fatigue strength was not influenced by the number of cycles used for shear fatigue strength testing.

Effect of delayed polymerization time and bracket manipulation on orthodontic bracket bonding

NASA Astrophysics Data System (ADS)

Ponikvar, Michael J.

This study examined the effect of bracket manipulation in combination with delayed polymerization times on orthodontic bracket shear bond strength and degree of resin composite conversion. Orthodontics brackets were bonded to extracted third molars in a simulated oral environment after a set period of delayed polymerization time and bracket manipulation. After curing the bracket adhesive, each bracket underwent shear bond strength testing followed by micro-Raman spectroscopy analysis to measure the degree of conversion of the resin composite. Results demonstrated the shear bond strength and the degree of conversion of ceramic brackets did not vary over time. However, with stainless steel brackets there was a significant effect (p ≤ 0.05) of delay time on shear bond strength between the 0.5 min and 10 min bracket groups. In addition, stainless steel brackets showed significant differences related to degree of conversion over time between the 0.5 min and 5 min groups, in addition to the 0.5 min and 10 min groups. This investigation suggests that delaying bracket adhesive polymerization up to a period of 10 min then adjusting the orthodontic bracket may increase both shear bond strength and degree of conversion of stainless steel brackets while having no effect on ceramic brackets.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Samavatian, Majid, E-mail: m.samavatian@srbiau.ac.ir; Halvaee, Ayoub; Amadeh, Ahmad Ali

Joining mechanism of Ti/Al dissimilar alloys was studied during liquid state diffusion bonding process using Cu/Sn/Cu interlayer at 510 °C under vacuum of 7.5 × 10{sup −5} Torr for various bonding times. The microstructure and compositional changes in the joint zone were analyzed by scanning electron microscopy equipped with energy dispersive spectroscopy and X-ray diffraction. Microhardness and shear strength tests were also applied to study the mechanical properties of the joints. It was found that with an increase in bonding time, the elements of interlayer diffused into the parent metals and formed various intermetallic compounds at the interface. Diffusion processmore » led to the isothermal solidification and the bonding evolution in the joint zone. The results from mechanical tests showed that microhardness and shear strength values have a straight relation with bonding time so that the maximum shear strength of joint was obtained for a bond made with 60 min bonding time. - Highlights: • Liquid state diffusion bonding of Al2024 to Ti–6Al–4V was performed successfully. • Diffusion of the elements caused the formation of various intermetallics at the interface. • Microhardness and shear strength values have a straight relation with bonding time. • The maximum shear strength reached to 36 MPa in 60 min bonding time.« less

Experimental Investigation of the Peak Shear Strength Criterion Based on Three-Dimensional Surface Description

NASA Astrophysics Data System (ADS)

Liu, Quansheng; Tian, Yongchao; Ji, Peiqi; Ma, Hao

2018-04-01

The three-dimensional (3D) morphology of joints is enormously important for the shear mechanical properties of rock. In this study, three-dimensional morphology scanning tests and direct shear tests are conducted to establish a new peak shear strength criterion. The test results show that (1) surface morphology and normal stress exert significant effects on peak shear strength and distribution of the damage area. (2) The damage area is located at the steepest zone facing the shear direction; as the normal stress increases, it extends from the steepest zone toward a less steep zone. Via mechanical analysis, a new formula for the apparent dip angle is developed. The influence of the apparent dip angle and the average joint height on the potential contact area is discussed, respectively. A new peak shear strength criterion, mainly applicable to specimens under compression, is established by using new roughness parameters and taking the effects of normal stress and the rock mechanical properties into account. A comparison of this newly established model with the JRC-JCS model and the Grasselli's model shows that the new one could apparently improve the fitting effect. Compared with earlier models, the new model is simpler and more precise. All the parameters in the new model have clear physical meanings and can be directly determined from the scanned data. In addition, the indexes used in the new model are more rational.

Current-Assisted Diffusion Bonding of Extruded Ti-22Al-25Nb Alloy by Spark Plasma Sintering: Interfacial Microstructure and Mechanical Properties

NASA Astrophysics Data System (ADS)

Yang, Jianlei; Wang, Guofeng; Jiao, Xueyan; Gu, Yibin; Liu, Qing; Li, You

2018-05-01

Spark plasma sintering (SPS) technology was used to current-assisted bond extruded Ti-22Al-25Nb alloy. The effects of bonding temperature (920-980 °C) and bonding time (10-30 min) on the microstructure evolution and shear strength of this alloy were investigated systematically. The temperature distribution in the specimen during the current-assisted bonding process was also analyzed by numerical simulation. It is noted that the highest temperature was obtained at the bonding interface. As the bonding temperature and bonding time increased, the voids in the interface shrank increasingly until they vanished. A complete metallurgical bonding interface could be produced at 960 °C/20 min/10 MPa, exhibiting the highest shear strength of 269.3 MPa. In addition, the shear strength of the bonded specimen depended on its interfacial microstructure. With increased bonding temperature, the fracture mode transformed from the intergranular fracture at the bonding interface to the cleavage fracture in the substrate.

Effects of Testing Method on Stretch-Flangeability of Dual-Phase 980/1180 Steel Grades

NASA Astrophysics Data System (ADS)

Madrid, Mykal; Van Tyne, Chester J.; Sadagopan, Sriram; Pavlina, Erik J.; Hu, Jun; Clarke, Kester D.

2018-04-01

Challenging fuel economy and safety standards in the automotive industry have led to the need for materials with higher strength while maintaining levels of formability that meet component manufacturing requirements. Advanced high-strength steels, such as dual-phase steels with tensile strengths of 980 MPa and 1180 MPa, are of interest to address this need. Increasing the strength of these materials typically comes at the expense of ductility, which may result in problems when stamping parts with trimmed or sheared edges, as cracking at the sheared edge may occur at lower strains. Here, hole expansion tests were performed with different punch geometries (conical and flat-bottom) and different edge conditions (sheared and machined) to understand the effects of testing conditions on performance, and these results are discussed in terms of mechanical properties and microstructures.

Resin adhesion strengths to zirconia ceramics after primer treatment with silane coupling monomer or oligomer.

PubMed

Okada, Masahiro; Inoue, Kazusa; Irie, Masao; Taketa, Hiroaki; Torii, Yasuhiro; Matsumoto, Takuya

2017-09-26

Resin bonding to zirconia ceramics is difficult to achieve using the standard methods for conventional silica-based dental ceramics, which employ silane coupling monomers as primers. The hypothesis in this study was that a silane coupling oligomer -a condensed product of silane coupling monomers- would be a more suitable primer for zirconia. To prove this hypothesis, the shear bond strengths between a composite resin and zirconia were compared after applying either a silane coupling monomer or oligomer. The shear bond strength increased after applying a non-activated ethanol solution of the silane coupling oligomer compared with that achieved when applying the monomer. Thermal treatment of the zirconia at 110°C after application of the silane coupling agents was essential to improve the shear bond strength between the composite resin cement and zirconia.

Effects of Testing Method on Stretch-Flangeability of Dual-Phase 980/1180 Steel Grades

NASA Astrophysics Data System (ADS)

Madrid, Mykal; Van Tyne, Chester J.; Sadagopan, Sriram; Pavlina, Erik J.; Hu, Jun; Clarke, Kester D.

2018-06-01

Challenging fuel economy and safety standards in the automotive industry have led to the need for materials with higher strength while maintaining levels of formability that meet component manufacturing requirements. Advanced high-strength steels, such as dual-phase steels with tensile strengths of 980 MPa and 1180 MPa, are of interest to address this need. Increasing the strength of these materials typically comes at the expense of ductility, which may result in problems when stamping parts with trimmed or sheared edges, as cracking at the sheared edge may occur at lower strains. Here, hole expansion tests were performed with different punch geometries (conical and flat-bottom) and different edge conditions (sheared and machined) to understand the effects of testing conditions on performance, and these results are discussed in terms of mechanical properties and microstructures.

Contribution of Field Strength Gradients to the Net Vertical Current of Active Regions

NASA Astrophysics Data System (ADS)

Vemareddy, P.

2017-12-01

We examined the contribution of field strength gradients for the degree of net vertical current (NVC) neutralization in active regions (ARs). We used photospheric vector magnetic field observations of AR 11158 obtained by Helioseismic and Magnetic Imager on board SDO and Hinode. The vertical component of the electric current is decomposed into twist and shear terms. The NVC exhibits systematic evolution owing to the presence of the sheared polarity inversion line between rotating and shearing magnetic regions. We found that the sign of shear current distribution is opposite in dominant pixels (60%–65%) to that of twist current distribution, and its time profile bears no systematic trend. This result indicates that the gradient of magnetic field strength contributes to an opposite signed, though smaller in magnitude, current to that contributed by the magnetic field direction in the vertical component of the current. Consequently, the net value of the shear current is negative in both polarity regions, which when added to the net twist current reduces the direct current value in the north (B z > 0) polarity, resulting in a higher degree of NVC neutralization. We conjecture that the observed opposite signs of shear and twist currents are an indication, according to Parker, that the direct volume currents of flux tubes are canceled by their return currents, which are contributed by field strength gradients. Furthermore, with the increase of spatial resolution, we found higher values of twist, shear current distributions. However, the resolution effect is more useful in resolving the field strength gradients, and therefore suggests more contribution from shear current for the degree of NVC neutralization.

Crystallographic controls on the frictional behavior of dry and water-saturated sheet structure minerals

USGS Publications Warehouse

Moore, Diane E.; Lockner, D.A.

2004-01-01

We compare the frictional strengths of 17 sheet structure mineral powders, measured under dry and water-saturated conditions, to identify the factors that cause many of them to be relatively weak. The dry coefficient of friction ?? ranges upward from 0.2 for graphite, leveling off at 0.8 for margarite, clintonite, gibbsite, kaolinite, and lizardite. The values of ?? (dry) correlate directly with calculated (001) interlayer bond strengths of the minerals. This correlation occurs because shear becomes localized along boundary and Riedel shears and the platy minerals in them rotate into alignment with the shear planes. For those gouges with ?? (dry) < 0.8, shear occurs by breaking the interlayer bonds to form new cleavage surfaces. Where ?? (dry) = 0.8, consistent with Byerlee's law, the interlayer bonds are sufficiently strong that other frictional processes dominate. The transition in dry friction mechanisms corresponds to calculated surface energies of 2-3 J/m2. Adding water causes ?? to decrease for every mineral tested except graphite. If the minerals are separated into groups with similar crystal structures, ?? (wet) increases with increasing interlayer bond strength within each group. This relationship also holds for the swelling clay montmorillonite, whose water-saturated strength is consistent with the strengths of nonswelling clays of similar crystal structure. Water in the saturated gouges forms thin, structured films between the plate surfaces. The polar water molecules are bonded to the plate surfaces in proportion to the mineral's surface energy, and ?? (wet) reflects the stresses required to shear through the water films. Copyright 2004 by the American Geophysical Union.

An evaluation of shear bond strength of self-etch adhesive on pre-etched enamel: an in vitro study.

PubMed

Rao, Bhadra; Reddy, Satti Narayana; Mujeeb, Abdul; Mehta, Kanchan; Saritha, G

2013-11-01

To determine the shear bond strength of self-etch adhesive G-bond on pre-etched enamel. Thirty caries free human mandibular premolars extracted for orthodontic purpose were used for the study. Occlusal surfaces of all the teeth were flattened with diamond bur and a silicon carbide paper was used for surface smoothening. The thirty samples were randomly grouped into three groups. Three different etch systems were used for the composite build up: group 1 (G-bond self-etch adhesive system), group 2 (G-bond) and group 3 (Adper single bond). Light cured was applied for 10 seconds with a LED unit for composite buildup on the occlusal surface of each tooth with 8 millimeters (mm) in diameter and 3 mm in thickness. The specimens in each group were tested in shear mode using a knife-edge testing apparatus in a universal testing machine across head speed of 1 mm/ minute. Shear bond strength values in Mpa were calculated from the peak load at failure divided by the specimen surface area. The mean shear bond strength of all the groups were calculated and statistical analysis was carried out using one-way Analysis of Variance (ANOVA). The mean bond strength of group 1 is 15.5 Mpa, group 2 is 19.5 Mpa and group 3 is 20.1 Mpa. Statistical analysis was carried out between the groups using one-way ANOVA. Group 1 showed statistically significant lower bond strength when compared to groups 2 and 3. No statistical significant difference between groups 2 and 3 (p < 0.05). Self-etch adhesive G-bond showed increase in shear bond strength on pre-etched enamel.

On double shearing in frictional materials

NASA Astrophysics Data System (ADS)

Teunissen, J. A. M.

2007-01-01

This paper evaluates the mechanical behaviour of yielding frictional geomaterials. The general Double Shearing model describes this behaviour. Non-coaxiality of stress and plastic strain increments for plane strain conditions forms an important part of this model. The model is based on a micro-mechanical and macro-mechanical formulation. The stress-dilatancy theory in the model combines the mechanical behaviour on both scales.It is shown that the general Double Shearing formulation comprises other Double Shearing models. These models differ in the relation between the mobilized friction and dilatancy and in non-coaxiality. In order to describe reversible and irreversible deformations the general Double Shearing model is extended with elasticity.The failure of soil masses is controlled by shear mechanisms. These shear mechanisms are determined by the conditions along the shear band. The shear stress ratio of a shear band depends on the orientation of the stress in the shear band. There is a difference between the peak strength and the residual strength in the shear band. While peak stress depends on strength properties only, the residual strength depends upon the yield conditions and the plastic deformation mechanisms and is generally considerably lower than the maximum strength. It is shown that non-coaxial models give non-unique solutions for the shear stress ratio on the shear band. The Double Shearing model is applied to various failure problems of soils such as the direct simple shear test, the biaxial test, infinite slopes, interfaces and for the calculation of the undrained shear strength. Copyright

Strength and compressibility of returned lunar soil.

NASA Technical Reports Server (NTRS)

Carrier, W. D., III; Bromwell, L. G.; Martin, R. T.

1972-01-01

Two oedometer and three direct shear tests have been performed in vacuum on a 200 g sample of lunar soil from Apollo 12 (12001, 119). The compressibility data have been used to calculate bulk density and shear wave velocity versus depth on the lunar surface. The shear wave velocity was found to increase approximately with the one-fourth power of the depth, and the results suggest that the Apollo 14 Active Seismic Experiment may not have detected the Fra Mauro formation at a depth of 8.5 m, but only naturally consolidated lunar soil. The shear data indicate that the strength of the lunar soil sample is about 65% that of a ground basalt simulant at the same void ratio.

Importance of Tensile Strength on the Shear Behavior of Discontinuities

NASA Astrophysics Data System (ADS)

Ghazvinian, A. H.; Azinfar, M. J.; Geranmayeh Vaneghi, R.

2012-05-01

In this study, the shear behavior of discontinuities possessing two different rock wall types with distinct separate compressive strengths was investigated. The designed profiles consisted of regular artificial joints molded by five types of plaster mortars, each representing a distinct uniaxial compressive strength. The compressive strengths of plaster specimens ranged from 5.9 to 19.5 MPa. These specimens were molded considering a regular triangular asperity profile and were designed so as to achieve joint walls with different strength material combinations. The results showed that the shear behavior of discontinuities possessing different joint wall compressive strengths (DDJCS) tested under constant normal load (CNL) conditions is the same as those possessing identical joint wall strengths, but the shear strength of DDJCS is governed by minor joint wall compressive strength. In addition, it was measured that the predicted values obtained by Barton's empirical criterion are greater than the experimental results. The finding indicates that there is a correlation between the joint roughness coefficient (JRC), normal stress, and mechanical strength. It was observed that the mode of failure of asperities is either pure tensile, pure shear, or a combination of both. Therefore, Barton's strength criterion, which considers the compressive strength of joint walls, was modified by substituting the compressive strength with the tensile strength. The validity of the modified criterion was examined by the comparison of the predicted shear values with the laboratory shear test results reported by Grasselli (Ph.D. thesis n.2404, Civil Engineering Department, EPFL, Lausanne, Switzerland, 2001). These comparisons infer that the modified criterion can predict the shear strength of joints more precisely.

Effect of Nd: YAG laser irradiation on surface properties and bond strength of zirconia ceramics.

PubMed

Liu, Li; Liu, Suogang; Song, Xiaomeng; Zhu, Qingping; Zhang, Wei

2015-02-01

This study investigated the effect of neodymium-doped yttrium aluminum garnet (Nd: YAG) laser irradiation on surface properties and bond strength of zirconia ceramics. Specimens of zirconia ceramic pieces were divided into 11 groups according to surface treatments as follows: one control group (no treatment), one air abrasion group, and nine laser groups (Nd: YAG irradiation). The laser groups were divided by applying with different output power (1, 2, or 3 W) and irradiation time (30, 60, or 90 s). Following surface treatments, the morphological characteristics of ceramic pieces was observed, and the surface roughness was measured. All specimens were bonded to resin cement. After, stored in water for 24 h and additionally aged by thermocycling, the shear bond strength was measured. Dunnett's t test and one-way ANOVA were performed as the statistical analyses for the surface roughness and the shear bond strength, respectively, with α = .05. Rougher surface of the ceramics could be obtained by laser irradiation with higher output power (2 and 3 W). However, cracks and defects were also found on material surface. The shear bond strength of laser groups was not obviously increased, and it was significantly lower than that of air abrasion group. No significant differences of the shear bond strength were found among laser groups treated with different output power or irradiation time. Nd: YAG laser irradiation cannot improve the surface properties of zirconia ceramics and cannot increase the bond strength of the ceramics. Enhancing irradiation power and extending irradiation time cannot induce higher bond strength of the ceramics and may cause material defect.

Friction and wear of metals with a single-crystal abrasive grit of silicon carbide: Effect of shear strength of metal

NASA Technical Reports Server (NTRS)

Miyoshi, K.; Buckley, D. H.

1978-01-01

Sliding friction experiments were conducted with spherical, single-crystal silicon carbide riders in contact with various metals and with metal riders in contact with silicon carbide flats. Results indicate that: (1) the friction force in the plowing of metal and (2) the groove height (corresponding to the volume of the groove) are related to the shear strength of the metal. That is, they decrease linearly as the shear strength of the bulk metal increases. Grooves are formed in metals primarily from plastic deformation, with occasional metal removal. The relation between the groove width D and the load W can be expressed by W = kD, superscript n which satisfies Meyer's law.

Comparative Laboratory and Numerical Simulations of Shearing Granular Fault Gouge: Micromechanical Processes

NASA Astrophysics Data System (ADS)

Morgan, J. K.; Marone, C. J.; Guo, Y.; Anthony, J. L.; Knuth, M. W.

2004-12-01

Laboratory studies of granular shear zones have provided significant insight into fault zone processes and the mechanics of earthquakes. The micromechanisms of granular deformation are more difficult to ascertain, but have been hypothesized based on known variations in boundary conditions, particle properties and geometries, and mechanical behavior. Numerical simulations using particle dynamics methods (PDM) can offer unique views into deforming granular shear zones, revealing the precise details of granular microstructures, particle interactions, and packings, which can be correlated with macroscopic mechanical behavior. Here, we describe a collaborative program of comparative laboratory and numerical experiments of granular shear using idealized materials, i.e., glass beads, glass rods or pasta, and angular sand. Both sets of experiments are carried out under similar initial and boundary conditions in a non-fracturing stress regime. Phenomenologically, the results of the two sets of experiments are very similar. Peak friction values vary as a function of particle dimensionality (1-D vs. 2-D vs. 3-D), particle angularity, particle size and size distributions, boundary roughness, and shear zone thickness. Fluctuations in shear strength during an experiment, i.e., stick-slip events, can be correlated with distinct changes in the nature, geometries, and durability of grain bridges that support the shear zone walls. Inclined grain bridges are observed to form, and to support increasing loads, during gradual increases in assemblage strength. Collapse of an individual grain bridge leads to distinct localization of strain, generating a rapidly propagating shear surface that cuts across multiple grain bridges, accounting for the sudden drop in strength. The distribution of particle sizes within an assemblage, along with boundary roughness and its periodicity, influence the rate of formation and dissipation of grain bridges, thereby controlling friction variations during shear.

Dependency of Shear Strength on Test Rate in SiC/BSAS Ceramic Matrix Composite at Elevated Temperature

NASA Technical Reports Server (NTRS)

Choi, Sung R.; Bansal, Narottam P.; Gyekenyesi, John P.

2003-01-01

Both interlaminar and in-plane shear strengths of a unidirectional Hi-Nicalon(TM) fiber-reinforced barium strontium aluminosilicate (SiC/BSAS) composite were determined at 1100 C in air as a function of test rate using double notch shear test specimens. The composite exhibited a significant effect of test rate on shear strength, regardless of orientation which was either in interlaminar or in in-plane direction, resulting in an appreciable shear-strength degradation of about 50 percent as test rate decreased from 3.3 10(exp -1) mm/s to 3.3 10(exp -5) mm/s. The rate dependency of composite's shear strength was very similar to that of ultimate tensile strength at 1100 C observed in a similar composite (2-D SiC/BSAS) in which tensile strength decreased by about 60 percent when test rate varied from the highest (5 MPa/s) to the lowest (0.005 MPa/s). A phenomenological, power-law slow crack growth formulation was proposed and formulated to account for the rate dependency of shear strength of the composite.

Shear Bond Strength of Superficial, Intermediate and Deep Dentin In Vitro with Recent Generation Self-etching Primers and Single Nano Composite Resin.

PubMed

Singh, Kulshrest; Naik, Rajaram; Hegde, Srinidhi; Damda, Aftab

2015-01-01

This in vitro study is intended to compare the shear bond strength of recent self-etching primers to superficial, intermediate, and deep dentin levels. All teeth were sectioned at various levels and grouped randomly into two experimental groups and two control groups having three subgroups. The experimental groups consisted of two different dentin bonding system. The positive control group consisted of All Bond 2 and the negative control group was without the bonding agent. Finally, the specimens were subjected to shear bond strength study under Instron machine. The maximum shear bond strengths were noted at the time of fracture. The results were statistically analyzed. Comparing the shear bond strength values, All Bond 2 (Group III) demonstrated fairly higher bond strength values at different levels of dentin. Generally comparing All Bond 2 with the other two experimental groups revealed highly significant statistical results. In the present investigation with the fourth generation, higher mean shear bond strength values were recorded compared with the self-etching primers. When intermediate dentin shear bond strength was compared with deep dentin shear bond strength statistically significant results were found with Clearfil Liner Bond 2V, All Bond 2 and the negative control. There was a statistically significant difference in shear bond strength values both with self-etching primers and control groups (fourth generation bonding system and without bonding system) at superficial, intermediate, and deep dentin. There was a significant fall in bond strength values as one reaches deeper levels of dentin from superficial to intermediate to deep.

Microstructure and Properties of 5083 Al/1060 Al/AZ31 Composite Plate Fabricated by Explosive Welding

NASA Astrophysics Data System (ADS)

Yang, Suyuan; Bao, Jiawei

2018-03-01

A 5083 Al/1060 Al/AZ31 composite plate was fabricated by explosive welding. The microstructure and properties of the composite plate were investigated after explosive welding. The results showed that all bonding interfaces were wavy interfaces. With an increasing distance from the detonation point, the wavelength and the amplitude also increased. The EDS results indicated that a 5-μm diffusion layer was observed at the 1060 Al/AZ31 layer, including the Mg2Al3 phase. Adiabatic shear bands and twin structures were observed in AZ31. The shear bond strength of the 5083 Al/1060 Al interface was 60 MPa, and the shear bond strength of the 1060 Al/AZ31 interface was 84 MPa.

Orthodontic bracket bonding without previous adhesive priming: A meta-regression analysis.

PubMed

Altmann, Aline Segatto Pires; Degrazia, Felipe Weidenbach; Celeste, Roger Keller; Leitune, Vicente Castelo Branco; Samuel, Susana Maria Werner; Collares, Fabrício Mezzomo

2016-05-01

To determine the consensus among studies that adhesive resin application improves the bond strength of orthodontic brackets and the association of methodological variables on the influence of bond strength outcome. In vitro studies were selected to answer whether adhesive resin application increases the immediate shear bond strength of metal orthodontic brackets bonded with a photo-cured orthodontic adhesive. Studies included were those comparing a group having adhesive resin to a group without adhesive resin with the primary outcome measurement shear bond strength in MPa. A systematic electronic search was performed in PubMed and Scopus databases. Nine studies were included in the analysis. Based on the pooled data and due to a high heterogeneity among studies (I(2)  =  93.3), a meta-regression analysis was conducted. The analysis demonstrated that five experimental conditions explained 86.1% of heterogeneity and four of them had significantly affected in vitro shear bond testing. The shear bond strength of metal brackets was not significantly affected when bonded with adhesive resin, when compared to those without adhesive resin. The adhesive resin application can be set aside during metal bracket bonding to enamel regardless of the type of orthodontic adhesive used.

Bond strength of the porcelain repair system to all-ceramic copings and porcelain.

PubMed

Lee, Sang J; Cheong, Chan Wook; Wright, Robert F; Chang, Brian M

2014-02-01

The purpose of this study was to investigate the shear bond strength of the porcelain repair system on alumina and zirconia core ceramics, comparing this strength with that of veneering porcelain. Veneering ceramic (n = 12), alumina core (n = 24), and zirconia core (n = 24) blocks measuring 10 × 5 × 5 mm(3) were fabricated. Veneering ceramic blocks were used as the control. Alumina and zirconia core blocks were divided into 2 groups (n = 12 each), and a slot (2 × 2 × 4 mm(3)) filled with veneering ceramics was prepared into one of the alumina and zirconia core groups (n = 12). Followed by surface treatments of micro-abrasion with 30 μm alumina particles, etching with 35% phosphoric acid and silane primer and bond, composite resin blocks (2 × 2 × 2 mm(3)) were built up and light polymerized onto the treated surfaces by 3 configurations: (a) composite blocks bonded onto veneering ceramic surface alone, (b) composite blocks bonded onto alumina core or zirconia core surfaces, (c) a 50% surface area of the composite blocks bonded to veneering ceramics and the other 50% surface area of the composite blocks to alumina core or zirconia core surfaces. The shear bond strength of the composite to each specimen was tested by a universal testing machine at a 0.5 mm/min crosshead speed. The shear bond strength was analyzed by unpaired t-tests for within the configuration groups and ANOVA for among the different configuration groups. When the mean shear bond strength was compared within groups of the same configuration, there were no statistically significant differences. Comparison of the shear bond strength among groups of different configurations revealed statistically significant differences. The mean shear bond strength of composite onto 100% veneering ceramic surface and composite onto 50% veneering 50% all-ceramic cores was statistically higher than that of composite onto 100% all-ceramic cores; however, the differences of the shear bond strength of composite bonded only onto the veneering ceramic surface were not statistically significant from those of 50% surface area of composite bonded onto all-ceramic cores. No statistically significant differences in the bond strength of a porcelain repair system to alumina and zirconia copings were observed. Increasing the surface of veneering ceramics to a porcelain repair system improved the repair material's bond strength. © 2013 by the American College of Prosthodontists.

Effect of adsorbed chlorine and oxygen on shear strength of iron and copper junctions

NASA Technical Reports Server (NTRS)

Wheeler, D. R.

1975-01-01

Static friction experiments were performed in ultrahigh vacuum at room temperature on copper, iron, and steel contacts selectively contaminated with oxygen and chlorine in submonolayer amounts. The concentration of the adsorbates was determined with Auger electron spectroscopy and was measured relative to the saturation concentration of oxygen on iron (concentration 1.0). The coefficient of static friction decreased with increasing adsorbate concentration. It was independent of the metal and the adsorbate. The results compared satisfactorily with an extension of the junction growth theory to heterogeneous interfaces. The reduction in interfacial shear strength was measured by the ratio sub a/sub m where sub a is the shear strength of the interface with an adsorbate concentration of 1.0, and sub m is the strength of the clean metal interface. This ratio was 0.835 + or - 0.012 for all the systems tested.

Microstructural and Mechanical Properties of Hot Roll Bonded Titanium Alloy/Low Carbon Steel Plate

NASA Astrophysics Data System (ADS)

Yu, Chao; Qi, Zi-chen; Yu, Hui; Xu, Cheng; Xiao, Hong

2018-03-01

In this paper, a titanium alloy and low carbon steel were bonded via hot rolling in a vacuum, and the effect of roll bonding temperature and reduction ratio on the microstructural and mechanical properties of the plate was studied. When the bonding temperature was between 850 and 1050 °C, the shear strength of the interface increased with an increasing reduction ratio from 18 to 70%. At a bonding temperature of 950 °C and at a rolling reduction ratio of 70%, the best bonding strength was obtained, and a shear fracture occurred on the low carbon steel matrix. At 1050 °C, brittle compounds, i.e., TiC, FeTi, and Fe2Ti, formed at the interface, which decreased the bonding strength. The large reduction ratio can break up compounds at the interface and extrude fresh metal for bonding, thereby increasing the bonding strength.

Influence of Interleaved Films on the Mechanical Properties of Carbon Fiber Fabric/Polypropylene Thermoplastic Composites

PubMed Central

Kim, Jong Won; Lee, Joon Seok

2016-01-01

A laminated composite was produced using a thermoplastic prepreg by inserting an interleaved film with the same type of matrix as the prepreg during the lay-up process to improve the low interlaminar properties, which is a known weakness of laminated composites. Carbon fiber fabric (CFF) and polypropylene (PP) were used to manufacture the thermoplastic prepregs. Eight prepregs were used to produce the laminated composites. Interleaved films with different thicknesses were inserted into each prepreg. The physical properties of the composite, such as thickness, density, fiber volume fraction (Vf), and void content (Vc), were examined. The tensile strength, flexural strength, interlaminar shear strength (ILSS), impact property, and scanning electron microscopy (SEM) were used to characterize the mechanical properties. Compared to the composite without any inserted interleaved film, as the thickness of the inserted interleaved resin film was increased, Vc decreased by 51.45%. At the same time, however, the tensile strength decreased by 8.75%. Flexural strength increased by 3.79% and flexural modulus decreased by 15.02%. Interlaminar shear strength increased by 11.05% and impact strength increased by 15.38%. Fracture toughness of the laminated composite was improved due to insertion of interleaved film. PMID:28773467

Influence of Interleaved Films on the Mechanical Properties of Carbon Fiber Fabric/Polypropylene Thermoplastic Composites.

PubMed

Kim, Jong Won; Lee, Joon Seok

2016-05-06

A laminated composite was produced using a thermoplastic prepreg by inserting an interleaved film with the same type of matrix as the prepreg during the lay-up process to improve the low interlaminar properties, which is a known weakness of laminated composites. Carbon fiber fabric (CFF) and polypropylene (PP) were used to manufacture the thermoplastic prepregs. Eight prepregs were used to produce the laminated composites. Interleaved films with different thicknesses were inserted into each prepreg. The physical properties of the composite, such as thickness, density, fiber volume fraction ( V f ), and void content ( V c ), were examined. The tensile strength, flexural strength, interlaminar shear strength (ILSS), impact property, and scanning electron microscopy (SEM) were used to characterize the mechanical properties. Compared to the composite without any inserted interleaved film, as the thickness of the inserted interleaved resin film was increased, V c decreased by 51.45%. At the same time, however, the tensile strength decreased by 8.75%. Flexural strength increased by 3.79% and flexural modulus decreased by 15.02%. Interlaminar shear strength increased by 11.05% and impact strength increased by 15.38%. Fracture toughness of the laminated composite was improved due to insertion of interleaved film.

Orthodontic brackets removal under shear and tensile bond strength resistance tests - a comparative test between light sources

NASA Astrophysics Data System (ADS)

Silva, P. C. G.; Porto-Neto, S. T.; Lizarelli, R. F. Z.; Bagnato, V. S.

2008-03-01

We have investigated if a new LEDs system has enough efficient energy to promote efficient shear and tensile bonding strength resistance under standardized tests. LEDs 470 ± 10 nm can be used to photocure composite during bracket fixation. Advantages considering resistance to tensile and shear bonding strength when these systems were used are necessary to justify their clinical use. Forty eight human extracted premolars teeth and two light sources were selected, one halogen lamp and a LEDs system. Brackets for premolar were bonded through composite resin. Samples were submitted to standardized tests. A comparison between used sources under shear bonding strength test, obtained similar results; however, tensile bonding test showed distinct results: a statistical difference at a level of 1% between exposure times (40 and 60 seconds) and even to an interaction between light source and exposure time. The best result was obtained with halogen lamp use by 60 seconds, even during re-bonding; however LEDs system can be used for bonding and re-bonding brackets if power density could be increased.

Brazing Inconel 625 Using the Copper Foil

NASA Astrophysics Data System (ADS)

Chen, Wen-Shiang; Wang, Cheng-Yen; Shiue, Ren-Kae

2013-12-01

Brazing Inconel 625 (IN-625) using the copper foil has been investigated in this research. The brazed joint is composed of nanosized CrNi3 precipitates and Cr/Mo/Nb/Ni quaternary compound in the Cu/Ni-rich matrix. The copper filler 50 μm in thickness is enough for the joint filling. However, the application of Cu foil 100 μm in thickness has little effect on the shear strength of the brazed joint. The specimen brazed at 1433 K (1160 °C) for 1800 seconds demonstrates the best shear strength of 470 MPa, and its fractograph is dominated by ductile dimple fracture with sliding marks. Decreasing the brazing temperature slightly decreases the shear strength of the brazed joint due to the presence of a few isolated solidification shrinkage voids smaller than 15 μm. Increasing the brazing temperature, especially for the specimen brazed at 1473 K (1200 °C), significantly deteriorates the shear strength of the joint below 260 MPa because of coalescence of isothermal solidification shrinkage voids in the joint. The Cu foil demonstrates potential in brazing IN-625 for industrial application.

Effect of different thickness h-BN coatings on interface shear strength of quartz fiber reinforced Sisbnd Osbnd Csbnd N composite

NASA Astrophysics Data System (ADS)

Wang, Shubin; Zheng, Yu

2014-02-01

Hexagonal boron nitride (h-BN) coatings with different thickness were prepared on quartz fibers to improve mechanical properties of quartz fiber reinforced Sisbnd Osbnd Csbnd N composite. Scanning electron microscopy (SEM), push-out test and single edge notched beam (SENB) in three point bending test were employed to study morphology, interface shear strength and fracture toughness of the composite. The results showed that h-BN coatings changed the crack growth direction and weaken the interface shear strength efficiently. When the h-BN coating was 308.2 nm, the interface shear strength was about 5.2 MPa, which was about one-quarter of that of the sample without h-BN coatings. After the heating process for obtaining composite, the h-BN nanometer-sized grains would grow up to micron-sized hexagonal grains. Different thickness h-BN coatings had different structure. When the coatings were relatively thin, the hexagonal grains were single layer structure, and when the coatings were thicker, the hexagonal grains were multiple layer structure. This multiple layer interface phase would consume more power of cracks, thus interface shear strength of the composite decreased steadily with the increasing of h-BN coatings thickness. When the coating thickness was 238.8 nm, KIC reaches the peak value 3.8 MPa m1/2, which was more than two times of that of composites without h-BN coatings.

Shear bond strength of one-step self-etch adhesives: pH influence

PubMed Central

Poggio, Claudio; Beltrami, Riccardo; Scribante, Andrea; Colombo, Marco; Chiesa, Marco

2015-01-01

Background: The aim of this study was to compare the shear bond strength of four one-step self-etch adhesives with different pH values to enamel and dentin. Materials and Methods: In this in vitro study, 200 bovine permanent mandibular incisors were used. Four one-step self-etch adhesives with different pH values were tested both on enamel and on dentin: Adper™ Easy Bond Self-Etch Adhesive (pH = 0.8-1), Futurabond NR (pH=2), G-aenial Bond (pH = 1.5), Clearfil S3 Bond (pH = 2.7). After adhesive systems application, a nanohybrid composite resin was inserted into the bonded surface. The specimens were placed in a universal testing machine. The shear bond strength was performed at a cross-head speed of 1 mm/min until the sample rupture. The shear bond strength values (MPa) of the different groups were compared with analysis of variance after that Kolmogorov and Smirnov tests were applied to assess normality of distributions. P < 0.05 was considered as significant. Results: In enamel shear bond strength, the highest shear bond strength values were reported with Futurabond NR (P < 0.01); however, no significant differences were found with Clearfil S3 Bond. The others adhesive systems showed lower shear bond strength values with significant differences between them (P < 0.05). When comparing the dentin shear bond strength, the lowest shear bond strength values were reported with Clearfil S3 Bond (P < 0.05), while there were no significant differences among the other three products (P > 0.05). Conclusion: The pH values of adhesive systems did not influence significantly their shear bond strength to enamel or dentin. PMID:26005459

The Influence of Processing on Strengthening Mechanisms in Pb-Free Solder Joints

NASA Astrophysics Data System (ADS)

Mutuku, Francis; Arfaei, Babak; Cotts, Eric J.

2017-04-01

The number, and the spacing, of Ag3Sn precipitates in Sn-Ag-Cu/Cu solder joints were related to separate processing parameters. The mechanical properties of an individual solder joint were directly related to the resulting distribution of different dispersoids in the joint. As the number of Ag3Sn precipitates increased, so did solder joint strength and shear fatigue lifetime. The room-temperature shear fatigue lifetime was inversely correlated with the separation between Ag3Sn precipitates. Bi and Sb solid solution strengthening was found to result in significantly larger values of shear strength and shear fatigue lifetime for one Pb-free solder. Room-temperature shear fatigue lifetime tests were identified as a relatively straightforward, yet sensitive means to gain insight into the reliability of Sn-Ag-Cu (SAC) solder joints.

Rapid repair of severely earthquake-damaged bridge piers with flexural-shear failure mode

NASA Astrophysics Data System (ADS)

Sun, Zhiguo; Wang, Dongsheng; Du, Xiuli; Si, Bingjun

2011-12-01

An experimental study was conducted to investigate the feasibility of a proposed rapid repair technique for severely earthquake-damaged bridge piers with flexural-shear failure mode. Six circular pier specimens were first tested to severe damage in flexural-shear mode and repaired using early-strength concrete with high-fluidity and carbon fiber reinforced polymers (CFRP). After about four days, the repaired specimens were tested to failure again. The seismic behavior of the repaired specimens was evaluated and compared to the original specimens. Test results indicate that the proposed repair technique is highly effective. Both shear strength and lateral displacement of the repaired piers increased when compared to the original specimens, and the failure mechanism of the piers shifted from flexural-shear failure to ductile flexural failure. Finally, a simple design model based on the Seible formulation for post-earthquake repair design was compared to the experimental results. It is concluded that the design equation for bridge pier strengthening before an earthquake could be applicable to seismic repairs after an earthquake if the shear strength contribution of the spiral bars in the repaired piers is disregarded and 1.5 times more FRP sheets is provided.

Interlaminar shear properties of graphite fiber, high-performance resin composites

NASA Technical Reports Server (NTRS)

Needles, H. L.; Kourtides, D. A.; Fish, R. H.; Varma, D. S.

1983-01-01

Short beam testing was used to determine the shear properties of laminates consisting of T-300 and Celion 3000 and 6000 graphite fibers, in epoxy, hot melt and solvent bismaleimide, polyimide and polystyrylpyridine (PSP). Epoxy, composites showed the highest interlaminar shear strength, with values for all other resins being substantially lower. The dependence of interlaminar shear properties on the fiber-resin interfacial bond and on resin wetting characteristics and mechanical properties is investigated, and it is determined that the lower shear strength of the tested composites, by comparison with epoxy resin matrix composites, is due to their correspondingly lower interfacial bond strengths. An investigation of the effect of the wettability of carbon fiber tow on shear strength shows wetting variations among resins that are too small to account for the large shear strength property differences observed.

Shear bond strength of self-etch adhesives to enamel with additional phosphoric acid etching.

PubMed

Lührs, Anne-Katrin; Guhr, Silke; Schilke, Reinhard; Borchers, Lothar; Geurtsen, Werner; Günay, Hüsamettin

2008-01-01

This study evaluated the shear bond strength of self-etch adhesives to enamel and the effect of additional phosphoric acid etching. Seventy sound human molars were randomly divided into three test groups and one control group. The enamel surfaces of the control group (n=10) were treated with Syntac Classic (SC). Each test group was subdivided into two groups (each n=10). In half of each test group, ground enamel surfaces were coated with the self-etch adhesives AdheSe (ADH), Xeno III (XE) or Futurabond NR (FNR). In the remaining half of each test group, an additional phosphoric acid etching of the enamel surface was performed prior to applying the adhesives. The shear bond strength was measured with a universal testing machine at a crosshead speed of 1 mm/minute after storing the samples in distilled water at 37 degrees C for 24 hours. Fracture modes were determined by SEM examination. For statistical analysis, one-way ANOVA and the two-sided Dunnett Test were used (p>0.05). Additional phosphoric etching significantly increased the shear bond strength of all the examined self-etch adhesives (p<0.001). The highest shear bond strength was found for FNR after phosphoric acid etching. Without phosphoric acid etching, only FNR showed no significant differences compared to the control (SC). SEM evaluations showed mostly adhesive fractures. For all the self-etch adhesives, a slight increase in mixed fractures occurred after conditioning with phosphoric acid. An additional phosphoric acid etching of enamel should be considered when using self-etch adhesives. More clinical studies are needed to evaluate the long-term success of the examined adhesives.

SEM/XPS analysis of fractured adhesively bonded graphite fibre surface resin-rich/graphite fibre composites

NASA Technical Reports Server (NTRS)

Devilbiss, T. A.; Wightman, J. P.; Progar, D. J.

1988-01-01

Samples of graphite fiber-reinforced polyimide were fabricated allowing the resin to accumulate at the composite surface. These surface resin-rich composites were then bonded together and tested for lap shear strength both before and after thermal aging. Lap shear strength did not appear to show a significant improvement over that previously recorded for resin-poor samples and was shown to decrease with increasing aging time and temperature.

Experimental Study on Shear Strength of Unsaturated Loess Based on Different Water Content in Xining Area

NASA Astrophysics Data System (ADS)

guibo, Bao; hui, Li; yu, Zhang; wuyu, Zhang; ningshan, Jiang

2018-05-01

Today, the study of shear strength of unsaturated soils has become a hot topic in unsaturated soil mechanics research. There are any number of factors affecting the strength of unsaturated soils. Among these factors, the moisture content has the most significant effect on the shear strength. In this paper, unsaturated loess in Xining is taken as the research object, the triaxial test without consolidation and undrain is used to determine the shear strength and its parameters under the condition of different water content, then the relationship between unsaturated loess’ water content and shear strength parameters is explored, and curve fitting is performed. The relevantily approximate mathematics formulas are obtained. The study can provide strength parameter for slope stability and foundation pit support in Xining.

Processing and characterization of unidirectional thermoplastic nanocomposites

NASA Astrophysics Data System (ADS)

Narasimhan, Kameshwaran

The manufacture of continuous fibre-reinforced thermoplastic nanocomposites is discussed for the case of E-Glass reinforced polypropylene (PP) matrix and for E-Glass reinforced Polyamide-6 (Nylon-6), with and without dispersed nanoclay (montmorillonite) platelets. The E-Glass/PP nanocomposite was manufactured using pultrusion, whereas the E-Glass/Nylon-6 nanocomposite was manufactured using compression molding. Mechanical characterization of nanocomposites were performed and compared with traditional microcomposites. Compressive as well as shear strength of nanocomposites was improved by improving the yield strength of the surrounding matrix through the dispersion of nanoclay. Significant improvements were achieved in compressive strength and shear strength with relatively low nanoclay loadings. Initially, polypropylene with and without nanoclay were melt intercalated using a single-screw extruder and the pultruded nanocomposite was fabricated using extruded pre-impregnated (pre-preg) tapes. Compression tests were performed as mandated by ASTM guidelines. SEM and TEM characterization revealed presence of nanoclay in an intercalated and partially exfoliated morphology. Mechanical tests confirmed significant improvements in compressive strength (˜122% at 10% nanoclay loading) and shear strength (˜60% at 3% nanoclay loading) in modified pultruded E-Glass/PP nanocomposites in comparison with baseline properties. Uniaxial tensile tests showed a small increase in tensile strength (˜3.4%) with 3% nanoclay loading. Subsequently, E-Glass/Nylon-6 nanocomposite panels were manufactured by compression molding. Compression tests were performed according to IITRI guidelines, whereas short beam shear and uni-axial tensile tests were performed according to ASTM standards. Mechanical tests confirmed strength enhancement with nanoclay addition, with a significant improvement in compressive strength (50% at 4% nanoclay loading) and shear strength (˜36% at 4% nanoclay loading) when compared with the baseline E-Glass/Nylon-6. Uni-axial tensile tests resulted in a small increase in tensile strength (˜3.2%) with 4% nanoclay loading. Also, hygrothermal aging (50°C and 100% RH) of baseline and nanoclay modified (4%) E-Glass/Nylon-6 was studied. It was observed that the moisture diffusion process followed Fickian diffusion. E-Glass/Nylon-6 modified with 4% nanoclay loading showed improved barrier performance with a significant reduction (˜30%) in moisture uptake compared to baseline E-Glass/Nylon-6 composites. Significant improvement in mechanical properties was also observed in hygrothermally aged nanocomposite specimens when compared with the aged baseline composite.

Verification of experimental dynamic strength methods with atomistic ramp-release simulations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moore, Alexander P.; Brown, Justin L.; Lim, Hojun

Material strength and moduli can be determined from dynamic high-pressure ramp-release experiments using an indirect method of Lagrangian wave profile analysis of surface velocities. This method, termed self-consistent Lagrangian analysis (SCLA), has been difficult to calibrate and corroborate with other experimental methods. Using nonequilibrium molecular dynamics, we validate the SCLA technique by demonstrating that it accurately predicts the same bulk modulus, shear modulus, and strength as those calculated from the full stress tensor data, especially where strain rate induced relaxation effects and wave attenuation are small. We show here that introducing a hold in the loading profile at peak pressuremore » gives improved accuracy in the shear moduli and relaxation-adjusted strength by reducing the effect of wave attenuation. When rate-dependent effects coupled with wave attenuation are large, we find that Lagrangian analysis overpredicts the maximum unload wavespeed, leading to increased error in the measured dynamic shear modulus. Furthermore, these simulations provide insight into the definition of dynamic strength, as well as a plausible explanation for experimental disagreement in reported dynamic strength values.« less

Verification of experimental dynamic strength methods with atomistic ramp-release simulations

NASA Astrophysics Data System (ADS)

Moore, Alexander P.; Brown, Justin L.; Lim, Hojun; Lane, J. Matthew D.

2018-05-01

Material strength and moduli can be determined from dynamic high-pressure ramp-release experiments using an indirect method of Lagrangian wave profile analysis of surface velocities. This method, termed self-consistent Lagrangian analysis (SCLA), has been difficult to calibrate and corroborate with other experimental methods. Using nonequilibrium molecular dynamics, we validate the SCLA technique by demonstrating that it accurately predicts the same bulk modulus, shear modulus, and strength as those calculated from the full stress tensor data, especially where strain rate induced relaxation effects and wave attenuation are small. We show here that introducing a hold in the loading profile at peak pressure gives improved accuracy in the shear moduli and relaxation-adjusted strength by reducing the effect of wave attenuation. When rate-dependent effects coupled with wave attenuation are large, we find that Lagrangian analysis overpredicts the maximum unload wavespeed, leading to increased error in the measured dynamic shear modulus. These simulations provide insight into the definition of dynamic strength, as well as a plausible explanation for experimental disagreement in reported dynamic strength values.

Verification of experimental dynamic strength methods with atomistic ramp-release simulations

DOE PAGES

Moore, Alexander P.; Brown, Justin L.; Lim, Hojun; ...

2018-05-04

Material strength and moduli can be determined from dynamic high-pressure ramp-release experiments using an indirect method of Lagrangian wave profile analysis of surface velocities. This method, termed self-consistent Lagrangian analysis (SCLA), has been difficult to calibrate and corroborate with other experimental methods. Using nonequilibrium molecular dynamics, we validate the SCLA technique by demonstrating that it accurately predicts the same bulk modulus, shear modulus, and strength as those calculated from the full stress tensor data, especially where strain rate induced relaxation effects and wave attenuation are small. We show here that introducing a hold in the loading profile at peak pressuremore » gives improved accuracy in the shear moduli and relaxation-adjusted strength by reducing the effect of wave attenuation. When rate-dependent effects coupled with wave attenuation are large, we find that Lagrangian analysis overpredicts the maximum unload wavespeed, leading to increased error in the measured dynamic shear modulus. Furthermore, these simulations provide insight into the definition of dynamic strength, as well as a plausible explanation for experimental disagreement in reported dynamic strength values.« less

Effect of interfacial species on shear strength of metal-sapphire contacts

NASA Technical Reports Server (NTRS)

Pepper, S. V.

1979-01-01

The interfacial shear strength of the metal-insulator system has been studied by means of the coefficient of static friction of copper, nickel, or gold contacts on sapphire in ultrahigh vacuum. The effect on contact strength of adsorbed oxygen, nitrogen, chlorine, and carbon monoxide on the metal surfaces is reported. It was found that exposures as low as 1 L of O2 on Ni produced observable increases in contact strength, whereas exposures of 3 L of Cl2 lead to a decrease in contact strength. These results imply that submonolayer concentrations of these species at the interface of a thin Ni film on Al2O3 should affect film adhesion similarly. The atomic mechanism by which these surface or interface phases affect interfacial strength is not yet understood.

Determination of erosion thresholds and aeolian dune stabilization mechanisms via robotic shear strength measurements

NASA Astrophysics Data System (ADS)

Qian, F.; Lee, D. B.; Bodek, S.; Roberts, S.; Topping, T. T.; Robele, Y.; Koditschek, D. E.; Jerolmack, D. J.

2017-12-01

Understanding the parameters that control the spatial variation in aeolian soil erodibility is crucial to the development of sediment transport models. Currently, in-situ measurements of erodibility are time consuming and lack robustness. In an attempt to remedy this issue, we perform field and laboratory tests to determine the suitability of a novel mechanical shear strength method to assess soil erodibility. These tests can be performed quickly ( 1 minute) by a semi-autonomous robot using its direct-drive leg, while environmental controls such as soil moisture and grain size are simultaneously characterized. The robot was deployed at White Sands National Monument to delineate and understand erodibility gradients at two different scales: (1) from dry dune crest to moist interdune (distance 10s m), where we determined that shear strength increases by a factor of three with increasing soil moisture; and (2) from barren barchan dunes to vegetated and crusted parabolics downwind (distance 5 km), where we found that shear strength was enhanced by a factor of two relative to loose sand. Interestingly, shear strength varied little from carbonate-crusted dune surfaces to bio-crust covered interdunes in the downwind parabolic region, indicating that varied surface crusts contribute similarly to erosion resistance. To isolate the control of soil moisture on erodibility, we performed laboratory experiments in a sandbox. These results verify that the observed increase in soil erodibility from barchan crest to interdune at White Sands is dominated by soil moisture, and the variation in parabolic dune and barchan interdune areas results from a combination of soil moisture, bio-activity, and crust development. This study highlights that spatial variation of soil erodibility in arid environments is large enough to significantly affect sediment transport, and that probing soil erodibility with a robot has the potential to improve our understanding of this multifaceted problem.

STUDY ON CHARACTERISTICS OF RESIDUAL STRENGTH OF RC BEAMS WITH DEFECTIVE ANCHORAGES DUE TO CORROSION OF REINFORCEMENTS

NASA Astrophysics Data System (ADS)

Murakami, Yuki; Dong, Wei; Oshita, Hideki; Suzuki, Shuichi; Tsutsumi, Tomoaki

In this study, to evaluate flexural strength and shear strength with def ective anchorages due to corrosion of reinforcemen t, the bending test of the RC beams r eceived damage in the anchorage region due to corrosion was carried out. As a result, it is se ems that the residual shear strength of RC beams with defective anchorages depends on shear span ratio in addition to the anchorage performance. Furthermore, the authors propose an evaluation model for an shear strength of RC beams with defective anchorages on the basis of these experimental results and analy tical result. The value of residual shear strength calculated using this model corresponds to the test results in the past.

Weibull models of fracture strengths and fatigue behavior of dental resins in flexure and shear.

PubMed

Baran, G R; McCool, J I; Paul, D; Boberick, K; Wunder, S

1998-01-01

In estimating lifetimes of dental restorative materials, it is useful to have available data on the fatigue behavior of these materials. Current efforts at estimation include several untested assumptions related to the equivalence of flaw distributions sampled by shear, tensile, and compressive stresses. Environmental influences on material properties are not accounted for, and it is unclear if fatigue limits exist. In this study, the shear and flexural strengths of three resins used as matrices in dental restorative composite materials were characterized by Weibull parameters. It was found that shear strengths were lower than flexural strengths, liquid sorption had a profound effect on characteristic strengths, and the Weibull shape parameter obtained from shear data differed for some materials from that obtained in flexure. In shear and flexural fatigue, a power law relationship applied for up to 250,000 cycles; no fatigue limits were found, and the data thus imply only one flaw population is responsible for failure. Again, liquid sorption adversely affected strength levels in most materials (decreasing shear strengths and flexural strengths by factors of 2-3) and to a greater extent than did the degree of cure or material chemistry.

Analytical and Experimental Assessment of Seismic Vulnerability of Beam-Column Joints without Transverse Reinforcement in Concrete Buildings

NASA Astrophysics Data System (ADS)

Hassan, Wael Mohammed

Beam-column joints in concrete buildings are key components to ensure structural integrity of building performance under seismic loading. Earthquake reconnaissance has reported the substantial damage that can result from inadequate beam-column joints. In some cases, failure of older-type corner joints appears to have led to building collapse. Since the 1960s, many advances have been made to improve seismic performance of building components, including beam-column joints. New design and detailing approaches are expected to produce new construction that will perform satisfactorily during strong earthquake shaking. Much less attention has been focused on beam-column joints of older construction that may be seismically vulnerable. Concrete buildings constructed prior to developing details for ductility in the 1970s normally lack joint transverse reinforcement. The available literature concerning the performance of such joints is relatively limited, but concerns about performance exist. The current study aimed to improve understanding and assessment of seismic performance of unconfined exterior and corner beam-column joints in existing buildings. An extensive literature survey was performed, leading to development of a database of about a hundred tests. Study of the data enabled identification of the most important parameters and the effect of each parameter on the seismic performance. The available analytical models and guidelines for strength and deformability assessment of unconfined joints were surveyed and evaluated. In particular, The ASCE 41 existing building document proved to be substantially conservative in joint shear strength estimation. Upon identifying deficiencies in these models, two new joint shear strength models, a bond capacity model, and two axial capacity models designed and tailored specifically for unconfined beam-column joints were developed. The proposed models strongly correlated with previous test results. In the laboratory testing phase of the current study, four full-scale corner beam-column joint subassemblies, with slab included, were designed, built, instrumented, tested, and analyzed. The specimens were tested under unidirectional and bidirectional displacement-controlled quasi-static loading that incorporated varying axial loads that simulated overturning seismic moment effects. The axial loads varied between tension and high compression loads reaching about 50% of the column axial capacity. The test parameters were axial load level, loading history, joint aspect ratio, and beam reinforcement ratio. The test results proved that high axial load increases joint shear strength and decreases the deformability of joints failing in pure shear failure mode without beam yielding. On the contrary, high axial load did not affect the strength of joints failing in shear after significant beam yielding; however, it substantially increased their displacement ductility. Joint aspect ratio proved to be instrumental in deciding joint shear strength; that is the deeper the joint the lower the shear strength. Bidirectional loading reduced the apparent strength of the joint in the uniaxial principal axes. However, circular shear strength interaction is an appropriate approximation to predict the biaxial strength. The developed shear strength models predicted successfully the strength of test specimens. Based on the literature database investigation, the shear and axial capacity models developed and the test results of the current study, an analytical finite element component model based on a proposed joint shear stress-rotation backbone constitutive curve was developed to represent the behavior of unconfined beam-column joints in computer numerical simulations of concrete frame buildings. The proposed finite element model included the effect of axial load, mode of joint failure, joint aspect ratio and axial capacity of joint. The proposed backbone curve along with the developed joint element exhibited high accuracy in simulating the test response of the current test specimens as well as previous test joints. Finally, a parametric study was conducted to assess the axial failure vulnerability of unconfined beam-column joints based on the developed shear and axial capacity models. This parametric study compared the axial failure potential of unconfined beam-column joint with that of shear critical columns to provide a preliminary insight into the axial collapse vulnerability of older-type buildings during intense ground shaking.

Behavior of fiber reinforced mortar joints in masonry walls subjected to in-plane shear and out-of-plane bending

NASA Astrophysics Data System (ADS)

Armwood, Catherine K.

In this project, 26 fiber-reinforced mortar (FRM) mixtures are evaluated for their workability and strength characteristics. The specimens tested include two control mixtures and 24 FRMs. The mixtures were made of two types of binders; Type N Portland cement lime (Type N-PCL) and Natural Hydrated Lime 5 (NHL5); and 6 fiber types (5 synthetic fibers and one organic). When tested in flexure, the results indicate that majority of the synthetic fiber mixtures enhanced the performance of the mortar and the nano-nylon and horse hair fibers were the least effective in improving the mortar's modulus of rupture, ductility, and energy absorption. Four FRMs that improved the mortar's mechanical properties most during the flexural strength test were then used to conduct additional experiments. The FRM's compressive strength, as well as flexural and shear bond strength with clay and concrete masonry units were determined. Those four mixtures included Type N-PCL as the binder and 4 synthetic fibers. They were evaluated at a standard laboratory flow rate of 110% +/- 5% and a practical field flow rate of 130% +/- 5%. Results indicate that the use of fibers decreases the compressive strength of the mortar most of the time. However, the bond strength test results were promising: 81% of the FRM mixtures increased the flexural bond strength of the prism. The mixtures at 110 +/- 5% flow rate bonded better with concrete bricks and those ate 130+/-5% flow rate bonded better with clay bricks. The results of the shear bond strength show 50% of the FRM mixtures improved the shear bond strength. The FRM mixtures at 110+/-5% flow rate bonded with clay units provided the most improvement in shear bond strength compared to control specimen results. Along with detailed discussions and derived conclusions of these experiments, this dissertation includes recommendations for the most feasible FRM for different applications.

Strain rate effects on mechanical properties of fiber composites, part 3

NASA Technical Reports Server (NTRS)

Daniel, I. M.; Liber, T.

1976-01-01

An experimental investigation was conducted to determine the strain rate effects in fiber composites. Unidirectional composite specimens of boron/epoxy, graphite/epoxy, S-glass/epoxy and Kevlar/epoxy were tested to determine longitudinal, transverse and intralaminar (in-plane) shear properties. In the Longitudinal direction the Kevlar/epoxy shows a definite increase in both modulus and strength with strain rate. In the transverse direction, a general trend toward higher strength with strain rate is noticed. The intralaminar shear moduli and strengths of boron/epoxy and graphite/epoxy show a definite rise with strain rate.

Comparison of polyester, film-yarn composite, balloon materials subjected to shear and biaxial loading

NASA Technical Reports Server (NTRS)

Niccum, R. J.

1972-01-01

A series of candidate materials for use in large balloons was tested and their tensile and shear strength capabilities were compared. The tests were done in a cold box at -68 C (-90 F). Some of these materials were fabricated on a special machine called the flying thread loom. This machine laminates various patterns of polyester yarn to a thin polyester film. The results show that the shear strength of materials changes with the angle selected for the transverse yarns, and substantial increases in biaxial load carrying capabilities, compared to materials formerly used, are possible. The loom capabilities and the test methods are discussed.

Evaluation of shear bond strength of orthodontic brackets using trans-illumination technique with different curing profiles of LED light-curing unit in posterior teeth.

PubMed

Heravi, Farzin; Moazzami, Saied Mostafa; Ghaffari, Negin; Jalayer, Javad; Bozorgnia, Yasaman

2013-11-21

Although using light-cured composites for bonding orthodontic brackets has become increasingly popular, curing light cannot penetrate the metallic bulk of brackets and polymerization of composites is limited to the edges. Limited access and poor direct sight may be a problem in the posterior teeth. Meanwhile, effectiveness of the trans-illumination technique is questionable due to increased bucco-lingual thickness of the posterior teeth. Light-emitting diode (LED) light-curing units cause less temperature rise and lower risk to the pulpal tissue. The purpose of this study was to evaluate the clinical effectiveness of trans-illumination technique in bonding metallic brackets to premolars, using different light intensities and curing times of an LED light-curing unit. Sixty premolars were randomly divided into six groups. Bonding of brackets was done with 40- and 80-s light curing from the buccal or lingual aspect with different intensities. Shear bond strengths of brackets were measured using a universal testing machine. Data were analyzed by one-way analysis of variance test and Duncan's post hoc test. The highest shear bond belonged to group 2 (high intensity, 40 s, buccal) and the lowest belonged to group 3 (low intensity, 40 s, lingual). Bond strength means in control groups were significantly higher than those in experimental groups. In all experimental groups except group 6 (80 s, high intensity, lingual), shear bond strength was below the clinically accepted values. In clinical limitations where light curing from the same side of the bracket is not possible, doubling the curing time and increasing the light intensity during trans-illumination are recommended for achieving acceptable bond strengths.

Effect of clay content and mineralogy on frictional sliding behavior of simulated gouges: binary and ternary mixtures of quartz, illite, and montmorillonite

USGS Publications Warehouse

Tembe, Sheryl; Lockner, David A.; Wong, Teng-Fong

2010-01-01

We investigated the frictional sliding behavior of simulated quartz-clay gouges under stress conditions relevant to seismogenic depths. Conventional triaxial compression tests were conducted at 40 MPa effective normal stress on saturated saw cut samples containing binary and ternary mixtures of quartz, montmorillonite, and illite. In all cases, frictional strengths of mixtures fall between the end-members of pure quartz (strongest) and clay (weakest). The overall trend was a decrease in strength with increasing clay content. In the illite/quartz mixture the trend was nearly linear, while in the montmorillonite mixtures a sigmoidal trend with three strength regimes was noted. Microstructural observations were performed on the deformed samples to characterize the geometric attributes of shear localization within the gouge layers. Two micromechanical models were used to analyze the critical clay fractions for the two-regime transitions on the basis of clay porosity and packing of the quartz grains. The transition from regime 1 (high strength) to 2 (intermediate strength) is associated with the shift from a stress-supporting framework of quartz grains to a clay matrix embedded with disperse quartz grains, manifested by the development of P-foliation and reduction in Riedel shear angle. The transition from regime 2 (intermediate strength) to 3 (low strength) is attributed to the development of shear localization in the clay matrix, occurring only when the neighboring layers of quartz grains are separated by a critical clay thickness. Our mixture data relating strength degradation to clay content agree well with strengths of natural shear zone materials obtained from scientific deep drilling projects.

Shear bond, wettability and AFM evaluations on CO2 laser-irradiated CAD/CAM ceramic surfaces.

PubMed

El Gamal, Ahmed; Medioni, Etienne; Rocca, Jean Paul; Fornaini, Carlo; Muhammad, Omid H; Brulat-Bouchard, Nathalie

2017-05-01

The purpose of this study is to determine the CO 2 laser irradiation in comparison with sandblasting (Sb), hydrofluoric acid (Hf) and silane coupling agent (Si) on shear bond strength (SBS), roughness (Rg) and wettability (Wt) of resin cement to CAD/CAM ceramics. Sixty (CAD/CAM) ceramic discs were prepared and distributed into six different groups: group A, control lithium disilicate (Li); group B, control zirconia (Zr); group C, Li: CO 2 /HF/Si; group D, Li: HF/Si; group E, Zr: CO 2 /Sb/Si; group F, Zr: Sb/Si. Result showed significant difference between irradiated and non-irradiated in terms of shear bond strength for zirconia ceramics (p value = 0.014). Moreover, partial surface wettability for irradiated and non-irradiated ceramics. Irradiated surface demonstrated more rough surface in lithium disilicate than zirconia ceramics. CO 2 irradiation could increase shear bond strength, surface roughness and wettability for both CAD/CAM ceramics.

A Study on the Effect of Ageing and Intermetallic Compound Growth on the Shear Strength of Surface Mount Technology Solder Joints

NASA Astrophysics Data System (ADS)

Nath, Jyotishman; Mallik, Sabuj; Borah, Anil

2015-04-01

The effect of ageing and intermetallic compound formation on the surface mount solder joints and its shear strength behavior under extreme mechanical and thermal conditions have been discussed in this paper. The specimens used are solder paste (Sn3.8Ag0.7Cu), bench marker II printed circuit boards (PCB), resistors 1206 and the fabrication of solder joints makes use of conventional surface mount technology (SMT). Reflow process was carried out at a peak temperature of 250 °C and the test samples were exposed to isothermal ageing at a constant temperature of 150 °C for a period of 600 h. Shear test was conducted on the PCB's. The shear strength of the solder joints rapidly increased during isothermal ageing to a certain time period and then started decreasing. Field emission scanning electron microscopy (FESEM) micrograph of the solder joint and energy dispersive X-ray (EDX) was performed on the solder sample to verify the formation of intermetallic compounds.

Elastic Properties in Tension and Shear of High Strength Nonferrous Metals and Stainless Steel - Effect of Previous Deformation and Heat Treatment

DTIC Science & Technology

1947-03-01

FOR AERONAUTICS TECHNICAL NOTE No. 1100 ELASTIC PROPERTIES IN TENSION AND SHEAR OF HIGH STRENGTH NONFERROUS METALS AND STAINLESS STEEL - EFFECT...1100 ELASTIC PROPERTIES IN TENSION AND SHEAR OF HIGH STRENGTH NONFERROUS METALS AND STAINLESS STEEL -- EFFECT OF PREVIOUS DEFORMATION AND HEAT...temperature on the tensile and shear elastic properties of high strength nonferrous metals and stainless steels in the form of rods and tubes. The

Low Temperature Consolidation of Micro/Nanosilver Die-Attach Preforms

NASA Astrophysics Data System (ADS)

McCoppin, Jared; Reitz, Thomas L.; Miller, Ryan; Vijwani, Hema; Mukhopadhyay, Sharmila; Young, Daniel

2014-09-01

Organically passivated silver nanopowder paste-based sintering is considered a promising solution for die-attach in high temperature power and sensing electronic devices. However, oxygen requirements during burnout and inherently high shrinkage rates limit their use to small die sizes. This work reports an alternative fabrication method that resolves decomposition and shrinkage issues of the die-attach by utilizing a prestressed optimized tape cast mixture of micro- and nanosilver particles with a polypropylene carbonate binder. The effects of prestressing, micro/nanosilver bimodal distribution, and polymer content on resulting microstructure and shear strength were investigated. Prior to application as a die-attach, uniaxial compression of the tape was found to significantly decrease shrinkage and improve green strength. This pre-stressing strategy allows for a decoupling of the resulting die-attach materials properties from the pressure applied during assembly. Bimodal mixtures consisting of 1-3 μm spherical powders with nanosilver resulted in shear strengths comparable to those of pure nanosilver. Shear strength decreased as bimodal particle size increased above 5 μm. A polymer content of ˜10 wt.% polypropylene carbonate combined with prestressing was identified as optimal for maximizing die-attach shear strength while still maintaining pliability and formability. Tape casts that were prestressed to 212 MPa by uniaxially compression and formulated with 10 wt.% of polypropylene carbonate resulted in a die-attach material with a shear strength of 54 MPa when sintered. These materials were used to demonstrate void-free 25-mm2 die-attach assemblies, suggesting that tape cast micro/nanosilver materials may be a promising die-attach method for high temperature and large-area electronics devices.

Interfacial Shear Strength and Adhesive Behavior of Silk Ionomer Surfaces.

PubMed

Kim, Sunghan; Geryak, Ren D; Zhang, Shuaidi; Ma, Ruilong; Calabrese, Rossella; Kaplan, David L; Tsukruk, Vladimir V

2017-09-11

The interfacial shear strength between different layers in multilayered structures of layer-by-layer (LbL) microcapsules is a crucial mechanical property to ensure their robustness. In this work, we investigated the interfacial shear strength of modified silk fibroin ionomers utilized in LbL shells, an ionic-cationic pair with complementary ionic pairing, (SF)-poly-l-glutamic acid (Glu) and SF-poly-l-lysine (Lys), and a complementary pair with partially screened Coulombic interactions due to the presence of poly(ethylene glycol) (PEG) segments and SF-Glu/SF-Lys[PEG] pair. Shearing and adhesive behavior between these silk ionomer surfaces in the swollen state were probed at different spatial scales and pressure ranges by using functionalized atomic force microscopy (AFM) tips as well as functionalized colloidal probes. The results show that both approaches were consistent in analyzing the interfacial shear strength of LbL silk ionomers at different spatial scales from a nanoscale to a fraction of a micron. Surprisingly, the interfacial shear strength between SF-Glu and SF-Lys[PEG] pair with partially screened ionic pairing was greater than the interfacial shear strength of the SF-Glu and SF-Lys pair with a high density of complementary ionic groups. The difference in interfacial shear strength and adhesive strength is suggested to be predominantly facilitated by the interlayer hydrogen bonding of complementary amino acids and overlap of highly swollen PEG segments.

Evaluation of a conditioning method to improve core-veneer bond strength of zirconia restorations.

PubMed

Teng, Jili; Wang, Hang; Liao, Yunmao; Liang, Xing

2012-06-01

The high strength and fracture toughness of zirconia have supported its extensive application in esthetic dentistry. However, the fracturing of veneering porcelains remains one of the primary causes of failure. The purpose of this study was to evaluate, with shear bond strength testing, the effect of a simple and novel surface conditioning method on the core-veneer bond strength of a zirconia ceramic system. The shear bond strength of a zirconia core ceramic to the corresponding veneering porcelain was tested by the Schmitz-Schulmeyer method. Thirty zirconia core specimens (10 × 5 × 5 mm) were layered with a veneering porcelain (5 × 3 × 3 mm). Three different surface conditioning methods were evaluated: polishing with up to 1200 grit silicon carbide paper under water cooling, airborne-particle abrasion with 110 μm alumina particles, and modification with zirconia powder coating before sintering. A metal ceramic system was used as a control group. All specimens were subjected to shear force in a universal testing machine at a crosshead speed of 0.5 mm/min. The shear bond strength values were analyzed with 1-way ANOVA and Tukey's post hoc pairwise comparisons (α=.05). The fractured specimens were examined with a scanning electron microscope to observe the failure mode. The mean (SD) shear bond strength values in MPa were 47.02 (6.4) for modified zirconia, 36.66 (8.6) for polished zirconia, 39.14 (6.5) for airborne-particle-abraded zirconia, and 46.12 (7.1) for the control group. The mean bond strength of the control (P=.028) and modified zirconia groups (P=.014) was significantly higher than that of the polished zirconia group. The airborne-particle-abraded group was not significantly different from any other group. Scanning electron microscopy evaluation showed that cohesive fracture in the veneering porcelain was the predominant failure mode of modified zirconia, while the other groups principally fractured at the interface. Modifying the zirconia surface with powder coating could significantly increase the shear bond strength of zirconia to veneering porcelain. Copyright © 2012 The Editorial Council of the Journal of Prosthetic Dentistry. Published by Mosby, Inc. All rights reserved.

Rheology of three-dimensional packings of aggregates: microstructure and effects of nonconvexity.

PubMed

Azéma, Emilien; Radjaï, Farhang; Saint-Cyr, Baptiste; Delenne, Jean-Yves; Sornay, Philippe

2013-05-01

We use three-dimensional contact dynamics simulations to analyze the rheological properties of granular materials composed of rigid aggregates. The aggregates are made from four overlapping spheres and described by a nonconvexity parameter depending on the relative positions of the spheres. The macroscopic and microstructural properties of several sheared packings are analyzed as a function of the degree of nonconvexity of the aggregates. We find that the internal angle of friction increases with the nonconvexity. In contrast, the packing fraction first increases to a maximum value but declines as the nonconvexity increases further. At a high level of nonconvexity, the packings are looser but show a higher shear strength. At the microscopic scale, the fabric and force anisotropy, as well as the friction mobilization, are enhanced by multiple contacts between aggregates and interlocking, thus revealings the mechanical and geometrical origins of shear strength.

Characterization of undrained shear strength profiles for soft clays at six sites in Texas.

DOT National Transportation Integrated Search

2009-01-01

TxDOT frequently uses Texas Cone Penetrometer (TCP) blow counts to estimate undrained shear strength. : However, the current correlations between TCP resistance and undrained shear strength have been developed primarily for : significantly stronger s...

In vitro analysis of shear bond strength and adhesive remnant index of different metal brackets

PubMed Central

Henkin, Fernanda de Souza; de Macêdo, Érika de Oliveira Dias; Santos, Karoline da Silva; Schwarzbach, Marília; Samuel, Susana Maria Werner; Mundstock, Karina Santos

2016-01-01

ABSTRACT Introduction: There is a great variety of orthodontic brackets in the Brazilian market, and constantly evaluating them is critical for professionals to know their properties, so as to be able to choose which product best suits their clinical practice. Objectives: To evaluate the bond strength and the adhesive remnant index (ARI) of different brands of metal brackets. Material and Methods: A total of 105 bovine incisors were used, and brackets of different brands were bonded to teeth. Seven different bracket brands were tested (MorelliTM, American OrthodonticsTM, TP OrthodonticsTM, Abzil-3MTM, OrthometricTM, TecnidentTM and UNIDENTM). Twenty-four hours after bonding, shear bond strength test was performed; and after debonding, the ARI was determined by using an optical microscope at a 10-fold increase. Results: Mean shear bond strength values ranged from 3.845 ± 3.997 (MorelliTM) to 9.871 ± 5.106 MPa (TecnidentTM). The majority of the ARI index scores was 0 and 1. Conclusion: Among the evaluated brackets, the one with the lowest mean shear bond strength values was MorelliTM. General evaluation of groups indicated that a greater number of bond failure occurred at the enamel/adhesive interface. PMID:28125142

Effects of ultraviolet irradiation on the bond strength of a composite resin adhered to stainless steel crowns.

PubMed

Baeza-Robleto, Selene J; Villa-Negrete, Dulce M; García-Contreras, René; Scougall-Vílchis, Rogelio J; Guadarrama-Quiroz, Luis J; Robles-Bermeo, Norma L

2013-01-01

A technique whereby the practitioner could improve the esthetic appearance of anterior stainless steel crowns (SSC) could provide a cost-effective alternative to more expensive commercially available preveneered SSCs, which may not be uniformly available. The purpose of this study was to evaluate the effects of ultraviolet (UV) irradiation of the metal crown surface on the shear bond strength of composite resin adhered to stainless steel crowns. Seventy extracted anterior bovine teeth randomly divided into 2 groups (n=35/group), were restored with primary maxillary left central incisor SSCs. Surface roughening with a green stone was performed on the labial surfaces, and the crowns of the experimental group were exposed to UV irradiation for 80 minutes. All samples were treated with metal-composite adhesive, followed by composite opaquer. Standardized composite blocks were bonded on the treated surfaces, and the shear bond strength was tested at 1 mm/minute. The values were recorded in MPa and statistically analyzed. The mean value of shear bond strength was significantly higher for the experimental group (19.7 ± 4.3 MPa) than the control group (16.3 ± 4.5 MPa). Ultraviolet irradiation of primary tooth stainless steel crowns significantly increased the shear bond strength of composite resin adhered to the facial surface.

Drought causes substantial reductions in non-isothermal soil strength

NASA Astrophysics Data System (ADS)

Vahedifard, F.; Robinson, J. D.; Love, C. A.; AghaKouchak, A.

2016-12-01

The stability and settlement of natural slopes and engineering structures are governed primarily by the shear strength of foundation soil. Understanding soil-atmosphere interactions and their impacts on shear strength is imperative to evaluating drought impacts on the resilience of our infrastructure. This understanding is also important for assessing a variety of emerging science and engineering problems in a changing climate including analyzing existing and new infrastructures, landslides, soil carbon sequestration, land management, and managing traction and tillage in agriculture. While progress has been made in understanding shear strength response to soil moisture changes, the impacts of concurrent soil moisture and temperature changes on shear strength remain uncertain from a regional-scale perspective. Here we present a methodological framework based on various soil types, temperatures, and moistures, and surface fluxes, to quantify a non-isothermal soil shear strength. We employ a non-isothermal soil strength analysis (NISSA) to explore the extent to which elevated soil temperatures and low moistures, along with abnormal surface fluxes, during California's record-setting 2012 - 2015 drought reduced the soil's shear strength. Our results suggest that the prolonged California drought reduced the shear strength of fine-grained soil as much as 95%. In contrast, the NISSA suggests that drought impacts on coarse-grained soil were not as significant. These opposing behaviors are attributed to the existence and absence of intermolecular physico-chemical forces in fine- and coarse-grained soils, respectively. The outlined framework offers a unique avenue to explore how soil shear strength is likely to behave under extreme drought conditions.

Surface fluorination of zirconia: adhesive bond strength comparison to commercial primers.

PubMed

Piascik, Jeffrey R; Swift, Edward J; Braswell, Krista; Stoner, Brian R

2012-06-01

This study evaluated contact angle and shear bond strength of three commercial zirconia primers and compared them to a recently developed fluorination pre-treatment. Earlier investigations reported that plasma fluorinated zirconia modifies the chemical bonding structure creating a more reactive surface. Yttria-stabilized zirconia (LAVA, 3M ESPE) plates were highly polished using 3μm diamond paste (R(a) ∼200nm) prior to pretreatments. After primer and fluorination treatment, contact angles were measured to quantify surface hydrophobicity before and after ethanol clean. Additionally, simple shear bond tests were performed to measure the adhesion strength to a composite resin. Plasma fluorination produced the lowest contact angle (7.8°) and the highest shear bond strength (37.3MPa) suggesting this pretreatment facilitates a more "chemically" active surface for adhesive bonding. It is hypothesized that plasma fluorination increase hydroxylation at the surface, making it more reactive, thus allowing for covalent bonding between zirconia surface and resin cement. A strong correlation was observed between contact angle and adhesion strength for all specimens; a relationship which may help understand the frequency and modes of failures, clinically. It is also believed that this surface treatment can increase long-term viability of zirconia restorations over other adhesive techniques. Copyright © 2012 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Rock friction under variable normal stress

USGS Publications Warehouse

Kilgore, Brian D.; Beeler, Nicholas M.; Lozos, Julian C.; Oglesby, David

2017-01-01

This study is to determine the detailed response of shear strength and other fault properties to changes in normal stress at room temperature using dry initially bare rock surfaces of granite at normal stresses between 5 and 7 MPa. Rapid normal stress changes result in gradual, approximately exponential changes in shear resistance with fault slip. The characteristic length of the exponential change is similar for both increases and decreases in normal stress. In contrast, changes in fault normal displacement and the amplitude of small high-frequency elastic waves transmitted across the surface follow a two stage response consisting of a large immediate and a smaller gradual response with slip. The characteristic slip distance of the small gradual response is significantly smaller than that of shear resistance. The stability of sliding in response to large step decreases in normal stress is well predicted using the shear resistance slip length observed in step increases. Analysis of the shear resistance and slip-time histories suggest nearly immediate changes in strength occur in response to rapid changes in normal stress; these are manifested as an immediate change in slip speed. These changes in slip speed can be qualitatively accounted for using a rate-independent strength model. Collectively, the observations and model show that acceleration or deceleration in response to normal stress change depends on the size of the change, the frictional characteristics of the fault surface, and the elastic properties of the loading system.

Methane gas hydrate effect on sediment acoustic and strength properties

USGS Publications Warehouse

Winters, W.J.; Waite, W.F.; Mason, D.H.; Gilbert, L.Y.; Pecher, I.A.

2007-01-01

To improve our understanding of the interaction of methane gas hydrate with host sediment, we studied: (1) the effects of gas hydrate and ice on acoustic velocity in different sediment types, (2) effect of different hydrate formation mechanisms on measured acoustic properties (3) dependence of shear strength on pore space contents, and (4) pore pressure effects during undrained shear.A wide range in acoustic p-wave velocities (Vp) were measured in coarse-grained sediment for different pore space occupants. Vp ranged from less than 1 km/s for gas-charged sediment to 1.77–1.94 km/s for water-saturated sediment, 2.91–4.00 km/s for sediment with varying degrees of hydrate saturation, and 3.88–4.33 km/s for frozen sediment. Vp measured in fine-grained sediment containing gas hydrate was substantially lower (1.97 km/s). Acoustic models based on measured Vp indicate that hydrate which formed in high gas flux environments can cement coarse-grained sediment, whereas hydrate formed from methane dissolved in the pore fluid may not.The presence of gas hydrate and other solid pore-filling material, such as ice, increased the sediment shear strength. The magnitude of that increase is related to the amount of hydrate in the pore space and cementation characteristics between the hydrate and sediment grains. We have found, that for consolidation stresses associated with the upper several hundred meters of sub-bottom depth, pore pressures decreased during shear in coarse-grained sediment containing gas hydrate, whereas pore pressure in fine-grained sediment typically increased during shear. The presence of free gas in pore spaces damped pore pressure response during shear and reduced the strengthening effect of gas hydrate in sands.

Ignition dynamics of a laminar diffusion flame in the field of a vortex embedded in a shear flow

NASA Technical Reports Server (NTRS)

Macaraeg, Michele G.; Jackson, T. L.; Hussaini, M. Y.

1994-01-01

The role of streamwise-spanwise vorticity interactions that occur in turbulent shear flows on flame/vortex interactions is examined by means of asymptotic analysis and numerical simulation in the limit of small Mach number. An idealized model is employed to describe the interaction process. The model consists of a one-step, irreversible Arrhenius reaction between initially unmixed species occupying adjacent half-planes which are then allowed to mix and react in the presence of a streamwise vortex embedded in a shear flow. It is found that the interaction of the streamwise vortex with shear gives rise to small-scale velocity oscillations which increase in magnitude with shear strength. These oscillations give rise to regions of strong temperature gradients via viscous heating, which can lead to multiple ignition points and substantially decrease ignition times. The evolution in time of the temperature and mass-fraction fields is followed, and emphasis is placed on the ignition time and structure as a function of vortex and shear strength.

Controlling microstructure and mechanical properties of the new microelectronic interconnect alloys

NASA Astrophysics Data System (ADS)

Mutuku, Francis M.

An in-depth understanding of the physics of solidification could lead to the optimization of the properties of micro-electronic interconnects. Sn is the base material in the billions of interconnects in devices such as smart phones. These interconnects are formed by melting and solidifying a solder alloy (e.g. SnAgCu) in situ. But Sn has a low symmetry structure, Sn nucleation from the solder melt is complex and the morphology of the Sn and Sn alloys precipitates that form during solidification can vary tremendously (along with resultant mechanical properties). The effect of processing parameters on the solidification behavior, microstructure, and properties must be carefully addressed. Strong evidence adduced in this study shows that under many conditions, when cooling near eutectic SnAgCu from the melt, Ag3Sn nucleates before beta-Sn. The difficulty in the nucleation of beta-Sn provides a window of time between the nucleation of Ag3Sn precipitates and of beta-Sn solidification within which the Ag3Sn precipitate morphology can be manipulated. Thus distinct variations in precipitate number density, and inter-particle spacing were observed for different thermal histories, e.g. for different cooling rates. The average number density of Ag3Sn particles and the area of the pseudo-eutectic phase were observed to increase with increase in the Ag concentration, and with increase in the cooling rate. The shear strength and shear fatigue life increased with increase in the area fraction of the pseudo-eutectic phase. Upon aging of SnAgCu solder joints at an elevated temperature, the Ag3Sn particles coarsened, and became less effective in impeding dislocation motion. Consequently, the shear strength and shear fatigue performance degraded. On the other hand, alloys with constituents that formed solid solutions in Sn, such as small concentrations of Bi or Sb registered less degradation in both shear strength and shear fatigue life upon aging.

Interaction of monopoles, dipoles, and turbulence with a shear flow

NASA Astrophysics Data System (ADS)

Marques Rosas Fernandes, V. H.; Kamp, L. P. J.; van Heijst, G. J. F.; Clercx, H. J. H.

2016-09-01

Direct numerical simulations have been conducted to examine the evolution of eddies in the presence of large-scale shear flows. The numerical experiments consist of initial-value-problems in which monopolar and dipolar vortices as well as driven turbulence are superposed on a plane Couette or Poiseuille flow in a periodic two-dimensional channel. The evolution of the flow has been examined for different shear rates of the background flow and different widths of the channel. Results found for retro-grade and pro-grade monopolar vortices are consistent with those found in the literature. Boundary layer vorticity, however, can significantly modify the straining and erosion of monopolar vortices normally seen for unbounded domains. Dipolar vortices are shown to be much more robust coherent structures in a large-scale shear flow than monopolar eddies. An analytical model for their trajectories, which are determined by self-advection and advection and rotation by the shear flow, is presented. Turbulent kinetic energy is effectively suppressed by the shearing action of the background flow provided that the shear is linear (Couette flow) and of sufficient strength. Nonlinear shear as present in the Poiseuille flow seems to even increase the turbulence strength especially for high shear rates.

An apparatus to measure the crosscut shearing strength of roots

Treesearch

Robert R. Ziemer

1978-01-01

Loss of tree root strength after timber cutting is a principal mechanism leading to slope failure and landslides. Measurement of root shear strength changes can be useful in evaluating effects of logging on slope stability. The simple apparatus described measures shear strength directly on roots up to 50 mm diameter. Tests on live roots showed excellent correlation...

The effect of temperature, matrix alloying and substrate coatings on wettability and shear strength of Al/Al2O3 couples

NASA Astrophysics Data System (ADS)

Sobczak, N.; Ksiazek, M.; Radziwill, W.; Asthana, R.; Mikulowski, B.

2004-03-01

A fresh approach has been advanced to examine in the Al/Al2O3 system the effects of temperature, alloying of Al with Ti or Sn, and Ti and Sn coatings on the substrate, on contact angles measured using a sessile-drop test, and on interface strength measured using a modified push-off test that allows shearing of solidified droplets with less than 90 deg contact angle. In the modified test, the solidified sessile-drop samples are bisected perpendicular to the drop/Al2O3 interface at the midplane of the contact circle to obtain samples that permit bond strength measurement by stress application to the flat surface of the bisected couple. The test results show that interface strength is strongly influenced by the wetting properties; low contact angles correspond to high interface strength, which also exhibits a strong temperature dependence. An increase in the wettability test temperature led to an increase in the interface strength in the low-temperature range where contact angles were large and wettability was poor. The room-temperature shear tests conducted on thermally cycled sessile-drop test specimens revealed the effect of chemically formed interfacial oxides; a weakening of the thermally cycled Al/Al2O3 interface was caused under the following conditions: (1) slow contact heating and short contact times in the wettability test, and (2) fast contact heating and longer contact times. The addition of 6 wt pct Ti or 7 wt pct Sn to Al only marginally influenced the contact angle and interfacial shear strength. However, Al2O3 substrates having thin (<1 µm) Ti coatings yielded relatively low contact angles and high bond strength, which appears to be related to the dissolution of the coating in Al and formation of a favorable interface structure.

Effect of surface treatment methods on the shear bond strength of auto-polymerized resin to thermoplastic denture base polymer.

PubMed

Koodaryan, Roodabeh; Hafezeqoran, Ali

2016-12-01

Polyamide polymers do not provide sufficient bond strength to auto-polymerized resins for repairing fractured denture or replacing dislodged denture teeth. Limited treatment methods have been developed to improve the bond strength between auto-polymerized reline resins and polyamide denture base materials. The objective of the present study was to evaluate the effect of surface modification by acetic acid on surface characteristics and bond strength of reline resin to polyamide denture base. 84 polyamide specimens were divided into three surface treatment groups (n=28): control (N), silica-coated (S), and acid-treated (A). Two different auto-polymerized reline resins GC and Triplex resins were bonded to the samples (subgroups T and G, respectively, n=14). The specimens were subjected to shear bond strength test after they were stored in distilled water for 1 week and thermo-cycled for 5000 cycles. Data were analyzed with independent t-test, two-way analysis of variance (ANOVA), and Tukey's post hoc multiple comparison test (α=.05). The bond strength values of A and S were significantly higher than those of N ( P <.001 for both). However, statistically significant difference was not observed between group A and group S. According to the independent Student's t-test, the shear bond strength values of AT were significantly higher than those of AG ( P <.001). The surface treatment of polyamide denture base materials with acetic acid may be an efficient and cost-effective method for increasing the shear bond strength to auto-polymerized reline resin.

Novel orthodontic cement containing dimethylaminohexadecyl methacrylate with strong antibacterial capability.

PubMed

Feng, Xiaodong; Zhang, Ning; Xu, Hockin H K; Weir, Michael D; Melo, Mary Anne S; Bai, Yuxing; Zhang, Ke

2017-09-26

Orthodontic treatments increase the incidence of white spot lesions. The objectives of this study were to develop an antibacterial orthodontic cement to inhibit demineralization, and to evaluate its enamel shear bond strength and anti-biofilm properties. Novel antibacterial monomer dimethylaminohexadecyl methacrylate (DMAHDM) was synthesized and incorporated into Transbond XT at 0, 1.5 and 3% by mass. Anti-biofilm activity was assessed using a human dental plaque microcosm biofilm model. Shear bond strength and adhesive remnant index were also tested. Biofilm activity precipitously dropped when contacting orthodontic cement with DMAHDM. Orthodontic cement containing 3% DMAHDM significantly reduced biofilm metabolic activity and lactic acid production (p<0.05), and decreased biofilm colony-forming unit (CFU) by two log. Water-aging for 90 days had no adverse influence on enamel shear bond strength (p>0.1). By incorporating DMAHDM into Transbond XT for the first time, the modified orthodontic cement obtained a strong antibacterial capability without compromising the enamel bond strength.

Investigation of interfacial shear strength in a SiC fibre/Ti-24Al-11Nb composite by a fibre push-out technique

NASA Technical Reports Server (NTRS)

Eldridge, J. I.; Brindley, P. K.

1989-01-01

A fiber push-out technique applied at several sample thicknesses was used to determine both the debond shear stress and the frictional shear stress at the fiber-matrix interface at room temperautre for a unidirectional SiC fiber-reinforced T-24Al-11Nb (in at. pct) composite prepared by a powder cloth technique. The push-out technique measures the separate contributions of bond strength and friction to the mechanical shear strength at the fiber-matrix interface. It was found that the fiber-matrix bond shear strength of this material is significantly higher than the fiber-matrix frictional shear stress (119.2 and 47.8 MPa, respectively).

Tensile and shear methods for measuring strength of bilayer tablets.

PubMed

Chang, Shao-Yu; Li, Jian-Xin; Sun, Changquan Calvin

2017-05-15

Both shear and tensile measurement methods have been used to quantify interfacial bonding strength of bilayer tablets. The shear method is more convenient to perform, but reproducible strength data requires careful control of the placement of tablet and contact point for shear force application. Moreover, data obtained from the shear method depend on the orientation of the bilayer tablet. Although more time-consuming to perform, the tensile method yields data that are straightforward to interpret. Thus, the tensile method is preferred in fundamental bilayer tableting research to minimize ambiguity in data interpretation. Using both shear and tensile methods, we measured the mechanical strength of bilayer tablets made of several different layer combinations of lactose and microcrystalline cellulose. We observed a good correlation between strength obtained by the tensile method and carefully conducted shear method. This suggests that the shear method may be used for routine quality test of bilayer tablets during manufacturing because of its speed and convenience, provided a protocol for careful control of the placement of the tablet interface, tablet orientation, and blade is implemented. Copyright © 2017 Elsevier B.V. All rights reserved.

An evaluation of upgraded boron fibers in epoxy-matrix composites

NASA Technical Reports Server (NTRS)

Rhodes, T. C.; Fleck, J. N.; Meiners, K. E.

1973-01-01

An initial evaluation of upgraded boron fibers in an epoxy matrix is performed. Data generated on the program show that fiber strength does increase as a consequence of the upgrading treatment. However, the interlaninar shear strength of upgraded fiber composites is lower than that for an untreated fiber composite. In the limited tests performed, the increased fiber strength failed to translate into the composite.

Calculation Method of Lateral Strengths and Ductility Factors of Constructions with Shear Walls of Different Ductility

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yamaguchi, Nobuyoshi; Nakao, Masato; Murakami, Masahide

2008-07-08

For seismic design, ductility-related force modification factors are named R factor in Uniform Building Code of U.S, q factor in Euro Code 8 and Ds (inverse of R) factor in Japanese Building Code. These ductility-related force modification factors for each type of shear elements are appeared in those codes. Some constructions use various types of shear walls that have different ductility, especially for their retrofit or re-strengthening. In these cases, engineers puzzle the decision of force modification factors of the constructions. Solving this problem, new method to calculate lateral strengths of stories for simple shear wall systems is proposed andmore » named 'Stiffness--Potential Energy Addition Method' in this paper. This method uses two design lateral strengths for each type of shear walls in damage limit state and safety limit state. Two lateral strengths of stories in both limit states are calculated from these two design lateral strengths for each type of shear walls in both limit states. Calculated strengths have the same quality as values obtained by strength addition method using many steps of load-deformation data of shear walls. The new method to calculate ductility factors is also proposed in this paper. This method is based on the new method to calculate lateral strengths of stories. This method can solve the problem to obtain ductility factors of stories with shear walls of different ductility.« less

Shear Behavior Models of Steel Fiber Reinforced Concrete Beams Modifying Softened Truss Model Approaches.

PubMed

Hwang, Jin-Ha; Lee, Deuck Hang; Ju, Hyunjin; Kim, Kang Su; Seo, Soo-Yeon; Kang, Joo-Won

2013-10-23

Recognizing that steel fibers can supplement the brittle tensile characteristics of concrete, many studies have been conducted on the shear performance of steel fiber reinforced concrete (SFRC) members. However, previous studies were mostly focused on the shear strength and proposed empirical shear strength equations based on their experimental results. Thus, this study attempts to estimate the strains and stresses in steel fibers by considering the detailed characteristics of steel fibers in SFRC members, from which more accurate estimation on the shear behavior and strength of SFRC members is possible, and the failure mode of steel fibers can be also identified. Four shear behavior models for SFRC members have been proposed, which have been modified from the softened truss models for reinforced concrete members, and they can estimate the contribution of steel fibers to the total shear strength of the SFRC member. The performances of all the models proposed in this study were also evaluated by a large number of test results. The contribution of steel fibers to the shear strength varied from 5% to 50% according to their amount, and the most optimized volume fraction of steel fibers was estimated as 1%-1.5%, in terms of shear performance.

Structure and strength at the bonding interface of a titanium-segmented polyurethane composite through 3-(trimethoxysilyl) propyl methacrylate for artificial organs.

PubMed

Sakamoto, Harumi; Doi, Hisashi; Kobayashi, Equo; Yoneyama, Takayuki; Suzuki, Yoshiaki; Hanawa, Takao

2007-07-01

The objective of this study was to investigate the structure and strength at the bonding interface of a titanium (Ti)-segmented polyurethane (SPU) composite through (3-trimethoxysilyl) propyl methacrylate (gamma-MPS) for artificial organs. The effects of the thickness of the gamma-MPS layer on the shear bonding strength between Ti and SPU were investigated. Ti disks were immersed in various concentrations of gamma-MPS solutions for several immersion times. The depth profiles of elements and the thickness of the gamma-MPS layer were determined by glow discharge optical emission spectroscopy and ellipsometry, respectively. The bonding stress at the Ti/gamma-MPS/SPU interface was evaluated with a shear bonding test. Furthermore, the fractured surface of a Ti-SPU composite was observed by optical microscopy and characterized using X-ray photoelectron spectroscopy. Consequently, the thickness of the gamma-MPS layer was controlled by the concentration of the gamma-MPS solution and immersion time. The shear bonding stress at the interface increased with the increase of the thickness of the gamma-MPS layer. Therefore, the control of the thickness of the gamma-MPS layer is significant to increase the shear bonding stress at the Ti/gamma-MPS/SPU interface. These results are significant to create composites for artificial organs consisting of other metals and polymers. Copyright 2007 Wiley Periodicals, Inc.

Discrete element analysis of the mechanical properties of deep-sea methane hydrate-bearing soils considering interparticle bond thickness

NASA Astrophysics Data System (ADS)

Jiang, Mingjing; He, Jie; Wang, Jianfeng; Zhou, Yaping; Zhu, Fangyuan

2017-12-01

Due to increasing global energy demands, research is being conducted on the mechanical properties of methane hydrate-bearing soils (MHBSs), from which methane hydrate (MH) will be explored. This paper presents a numerical approach to study the mechanical properties of MHBSs. The relationship between the level of MH saturation and the interparticle bond thickness is first obtained by analyzing the scanning electron microscope images of MHBS samples, in which is the bridge connecting the micromechanical behavior captured by the DEM with the macroscopic properties of MHBSs. A simplified thermal-hydromechanical (THM) bond model that considers the different bond thicknesses is then proposed to describe the contact behavior between the soil particles and those incorporated into the discrete element method (DEM). Finally, a series of biaxial compression tests are carried out with different MH saturations under different effective confining pressures to analyze the mechanical properties of deep-sea MHBSs. The results of the DEM numerical simulation are also compared with the findings from triaxial compression tests. The results show that the macromechanical properties of deep-sea MHBSs can be qualitatively captured by the proposed DEM. The shear strength, cohesion, and volumetric contraction of deep-sea MHBSs increase with increasing MH saturation, although its influence on the internal friction angle is obscure. The shear strength and volumetric contraction increase with increasing effective confining pressure. The peak shear strength and the dilation of MHBSs increase as the critical bond thickness increases, while the residual deviator stress largely remains the same at a larger axial strain. With increasing the axial strain, the percentage of broken bonds increases, along with the expansion of the shear band.

Shear Fracture of Dual Phase AHSS in the Process of Stamping: Macroscopic Failure Mode and Micro-level Metallographical Observation

NASA Astrophysics Data System (ADS)

Wang, Wurong; Wei, Xicheng; Yang, Jun; Shi, Gang

2011-08-01

Due to its excellent strength and formability combinations, dual phase (DP) steels offer the potential to improve the vehicle crashworthiness performance without increasing car body weight and have been increasingly used into new vehicles. However, a new type of crack mode termed as shear fracture is accompanied with the application of these high strength DP steel sheets. With the cup drawing experiment to identify the limit drawing ratio (LDR) of three DP AHSS with strength level from 600 MPa to 1000 MPa, the study compared and categorized the macroscopic failure mode of these three types of materials. The metallographical observation along the direction of crack was conducted for the DP steels to discover the micro-level propagation mechanism of the fracture.

The effect of fusion-relevant helium levels on the mechanical properties of isotopically tailored ferritic alloys

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hankin, G.L.; Hamilton, M.L.; Gelles, D.S.

1997-04-01

The yield and maximum strengths of an irradiated series of isotopically tailored ferritic alloys were evaluated using the shear punch test. The composition of three of the alloys was Fe-12Cr-1.5Ni. Different balances of nickel isotopes were used in each alloy in order to produce different helium levels. A fourth alloy, which contained no nickel, was also irradiated. The addition of nickel at any isotopic balance to the Fe-12Cr base alloy significantly increased the shear yield and maximum strengths of the alloys, and as expected, the strength of the alloys decreased with increasing irradiation temperature. Helium itself, up to 75 appmmore » over 7 dpa appears to have little effect on the mechanical properties of the alloys.« less

Revisiting the generalized scaling law for adhesion: role of compliance and extension to progressive failure.

PubMed

Mojdehi, Ahmad R; Holmes, Douglas P; Dillard, David A

2017-10-25

A generalized scaling law, based on the classical fracture mechanics approach, is developed to predict the bond strength of adhesive systems. The proposed scaling relationship depends on the rate of change of debond area with compliance, rather than the ratio of area to compliance. This distinction can have a profound impact on the expected bond strength of systems, particularly when the failure mechanism changes or the compliance of the load train increases. Based on the classical fracture mechanics approach for rate-independent materials, the load train compliance should not affect the force capacity of the adhesive system, whereas when the area to compliance ratio is used as the scaling parameter, it directly influences the bond strength, making it necessary to distinguish compliance contributions. To verify the scaling relationship, single lap shear tests were performed for a given pressure sensitive adhesive (PSA) tape specimens with different bond areas, number of backing layers, and load train compliance. The shear lag model was used to derive closed-form relationships for the system compliance and its derivative with respect to the debond area. Digital image correlation (DIC) is implemented to verify the non-uniform shear stress distribution obtained from the shear lag model in a lap shear geometry. The results obtained from this approach could lead to a better understanding of the relationship between bond strength and the geometry and mechanical properties of adhesive systems.

Angle-Ply Weaving

NASA Technical Reports Server (NTRS)

Farley, Gary L.

1990-01-01

Bias-direction or angle-ply weaving is proposed new process for weaving fibers along bias in conventional planar fabric or in complicated three-dimensional multilayer fabric preform of fiber-reinforced composite structure. Based upon movement of racks of needles and corresponding angle yarns across fabric as fabric being formed. Fibers woven along bias increases shear stiffness and shear strength of preform, increasing value of preform as structural member.

Effect of metal primers on bond strength of resin cements to base metals.

PubMed

Fonseca, Renata Garcia; de Almeida, Juliana Gomes dos Santos Paes; Haneda, Isabella Gagliardi; Adabo, Gelson Luis

2009-04-01

A strong and durable bond between a metal framework and a resin-based luting agent is desired. Metal primers have been shown to be very effective on noble alloys. However, there is insufficient information about their effect on base metals. The purpose of this study was to evaluate the effect of metal primers on the shear bond strength of resin cements to base metals. A total of 160 cast commercially pure titanium (CP Ti) and NiCr alloy (VeraBond II) disks were embedded in a polyvinyl chloride ring, and their surfaces were smoothed with silicon carbide papers (320, 400, and 600 grit) and airborne-particle abraded with 50-mum aluminum oxide. Specimens of each metal were divided into 4 groups (n=20), which received one of the following luting techniques: (1) Panavia F, (2) Alloy Primer plus Panavia F, (3) Bistite II DC, or (4) Metaltite plus Bistite II DC. Forty minutes after preparation, all specimens were stored in distilled water at 37 degrees C for 24 hours and then thermal cycled (1000 cycles, 5-55 degrees C). After thermal cycling, the specimens were stored in 37 degrees C distilled water for an additional 24 hours or 6 months before being tested in shear mode. Data (MPa) were analyzed using 3-way ANOVA and the post hoc Tukey test (alpha=.05). Each specimen was examined under an optical microscope (x30), and the failure mode was classified as adhesive, cohesive, or a combination of these. The only significant difference between the Panavia F and Alloy Primer plus Panavia F groups occurred in the NiCr alloy at 24 hours, at which point Panavia F demonstrated superior bond strength compared to Alloy Primer plus Panavia F (P<.001). The Bistite II DC and Metaltite plus Bistite II DC groups were not significantly different. The Bistite II DC and Metaltite plus Bistite II DC groups demonstrated significantly lower bond strength to CP Ti (P<.001) than the Panavia F and Alloy Primer plus Panavia F groups, and significantly lower bond strength to NiCr alloy (P<.001) than Panavia F. The Panavia F (P<.01) and Alloy Primer plus Panavia F groups' bond strength to titanium presented a significant increase (P<.001) in shear bond strength at 6 months. In general, the groups exhibited higher shear bond strength to CP Ti than to NiCr alloy (P<.01). The failure mode was 100% adhesive for all groups. The metal primers did not promote an increase in adhesive bonding of resin cements to NiCr alloy and to CP Ti. Water storage had no adverse effect on the shear bond strength of the groups. The shear bond strengths to titanium were significantly higher than those to the NiCr alloy.

Effect of acid and laser etching on shear bond strength of conventional and resin-modified glass-ionomer cements to composite resin.

PubMed

Navimipour, Elmira Jafari; Oskoee, Siavash Savadi; Oskoee, Parnian Alizadeh; Bahari, Mahmoud; Rikhtegaran, Sahand; Ghojazadeh, Morteza

2012-03-01

Success in sandwich technique procedures can be achieved through an acceptable bond between the materials. The aim of this study was to compare the effect of 35% phosphoric acid and Er,Cr:YSGG laser on shear bond strength of conventional glass-ionomer cement (GIC) and resin-modified glass-ionomer cement (RMGIC) to composite resin in sandwich technique. Sixty-six specimens were prepared from each type of glass-ionomer cements and divided into three treatment groups as follows: without pretreatment, acid etching by 35% phosphoric acid for 15 s, and 1-W Er,Cr:YSGG laser treatment for 15 s with a 600-μm-diameter tip aligned perpendicular to the target area at a distance of 1 mm from the surface. Energy density of laser irradiation was 17.7 J/cm(2). Two specimens in each group were prepared for evaluation under a scanning electron microscope (SEM) after surface treatment and the remainder underwent bonding procedure with a bonding agent and composite resin. Then the shear bond strength was measured at a crosshead speed of 0.5 mm/min. Two-factor analysis of variance and post-hoc Tukey test showed that the cement type, surface treatment method, and the interaction of these two factors significantly affect the shear bond strength between glass-ionomer cements and composite resin (p < 0.05). Surface treatment with phosphoric acid or Er,Cr:YSGG laser increased the shear bond strength of GIC to composite resin; however, in RMGIC only laser etching resulted in significantly higher bond strength. These findings were supported by SEM results. The fracture mode was evaluated under a stereomicroscope at ×20.

Processing, thermal and mechanical behaviour of PEI/MWCNT/carbon fiber nanostructured laminate

NASA Astrophysics Data System (ADS)

Santos, L. F. P.; Ribeiro, B.; Hein, L. R. O.; Botelho, E. C.; Costa, M. L.

2017-11-01

In this work, nanostructured composites of polyetherimide (PEI) with addition of functionalized multiwall carbon nanotube (MWCNT) were processed via solution mixing. After processing, these nanocomposites were evaluated by thermogravimetry (TGA), dynamic-mechanical analysis (DMA), scanning electron microscopy (SEM) and atomic force microscopy (AFM). Subsequently, the nanocomposite was processed with carbon fibers by using hot compression molding. In order to evaluate interlaminar fracture strength, the processed laminates were mechanically evaluated by interlaminar shear strength (ILSS) and compression shear test (CST). Also, the Weibull distribution was employed to help in the statistical treatment of the data obtained from the mechanical tests. With regards to the fracture of the specimens, optical microscopy was used for the evaluation of the material. The addition of 1 wt% of MWCNT in the polymer matrix increased both thermal stability and viscoelastic behavior of the material. These improvements positively impacted the mechanical properties, generating a 16% and 58% increase in the short-beam strength and apparent interlaminar shear, respectively. In addition, it can be verified from morphological analysis of the fracture a change in the failure mode of the laminate by the incorporation of MWCNT. This behavior can be proven from CST test where there was no presence of the shear force by compression.

Parametric Study of Shear Strength of Concrete Beams Reinforced with FRP Bars

NASA Astrophysics Data System (ADS)

Thomas, Job; Ramadass, S.

2016-09-01

Fibre Reinforced Polymer (FRP) bars are being widely used as internal reinforcement in structural elements in the last decade. The corrosion resistance of FRP bars qualifies its use in severe and marine exposure conditions in structures. A total of eight concrete beams longitudinally reinforced with FRP bars were cast and tested over shear span to depth ratio of 0.5 and 1.75. The shear strength test data of 188 beams published in various literatures were also used. The model originally proposed by Indian Standard Code of practice for the prediction of shear strength of concrete beams reinforced with steel bars IS:456 (Plain and reinforced concrete, code of practice, fourth revision. Bureau of Indian Standards, New Delhi, 2000) is considered and a modification to account for the influence of the FRP bars is proposed based on regression analysis. Out of the 196 test data, 110 test data is used for the regression analysis and 86 test data is used for the validation of the model. In addition, the shear strength of 86 test data accounted for the validation is assessed using eleven models proposed by various researchers. The proposed model accounts for compressive strength of concrete ( f ck ), modulus of elasticity of FRP rebar ( E f ), longitudinal reinforcement ratio ( ρ f ), shear span to depth ratio ( a/ d) and size effect of beams. The predicted shear strength of beams using the proposed model and 11 models proposed by other researchers is compared with the corresponding experimental results. The mean of predicted shear strength to the experimental shear strength for the 86 beams accounted for the validation of the proposed model is found to be 0.93. The result of the statistical analysis indicates that the prediction based on the proposed model corroborates with the corresponding experimental data.

Coatings for graphite fibers

NASA Technical Reports Server (NTRS)

Galasso, F. S.; Scola, D. A.; Veltri, R. D.

1980-01-01

Graphite fibers released from composites during burning or an explosion caused shorting of electrical and electronic equipment. Silicon carbide, silica, silicon nitride and boron nitride were coated on graphite fibers to increase their electrical resistances. Resistances as high as three orders of magnitude higher than uncoated fiber were attained without any significant degradation of the substrate fiber. An organo-silicone approach to produce coated fibers with high electrical resistance was also used. Celion 6000 graphite fibers were coated with an organo-silicone compound, followed by hydrolysis and pyrolysis of the coating to a silica-like material. The shear and flexural strengths of composites made from high electrically resistant fibers were considerably lower than the shear and flexural strengths of composites made from the lower electrically resistant fibers. The lower shear strengths of the composites indicated that the coatings on these fibers were weaker than the coating on the fibers which were pyrolyzed at higher temperature.

Effects of Energy Density and Shielding Medium on Performance of Laser Beam Welding (LBW) Joints on SAF2205 Duplex Stainless Steel

NASA Astrophysics Data System (ADS)

Zhang, W. W.; Cong, S.; Luo, S. B.; Fang, J. H.

2018-05-01

The corrosion resistance performance of SAF2205 duplex stainless steel depends on the amount of ferrite to austenite transformation, but the ferrite content after power beam welding is always excessively high. To obtain laser beam welding joints with better mechanical and corrosion resistance performance, the effects of the energy density and shielding medium on the austenite content, hardness distribution, and shear strength were investigated. The results showed that ferrite to austenite transformation was realized with increase in the energy density. When the energy density was increased from 120 J/mm to 200 J/mm, the austenite content of the welding joint changed from 2.6% to 38.5%. Addition of nitrogen gas to the shielding medium could promote formation of austenite. When the shielding medium contained 50% and 100% nitrogen gas, the austenite content of the welding joint was 42.7% and 47.2%, respectively. The hardness and shear strength were significantly improved by increase in the energy density. However, the shielding medium had less effect on the mechanical performance. Use of the optimal welding process parameters resulted in peak hardness of 375 HV and average shear strength of 670 MPa.

[Evaluation on a demonstration project of ecological restoration of ditches at Qianwei Village of Chongming County, Shanghai].

PubMed

Zhou, Xiang-Xiang; Zhang, Li-Quan; Yuan, Lian-Qi

2008-02-01

By using biological slope-protection techniques, oxidation pond system, and zeolite treatment system, a demonstration project of ecological restoration of ditches at the Qianwei Village of Chongming County in Shanghai was implemented, and an evaluation on the project was made via a runoff simulation experiment and the measurements of the parameters soil shear strength, biodiversity, and ditch water quality. The results showed that covering the dich slopes with shrub could significantly increase soil shear strength, compactness and moisture content, and the formed vegetation had significant effects on retarding runoff and removing TSS (P < 0.05). Applying live fascines could significantly increase soil shear strength and TSS removal rate (P < 0.05), but its effects on increasing soil compactness and moisture content and retaining runoff were not significant. After the implement of the demonstration project, the total N and P concentrations in ditch water decreased significantly, habitat quality and aesthetic value of ditch slope improved, and biodiversity enhanced greatly. The integration of the biological techniques with other ecological restoration measures could stabilize ditch slope, improve ditch habitat quality, and restore the ecological environment of the ditches.

Improved Strength and Toughness of Carbon Woven Fabric Composites with Functionalized MWCNTs

PubMed Central

Soliman, Eslam; Kandil, Usama; Reda Taha, Mahmoud

2014-01-01

This investigation examines the role of carboxyl functionalized multi-walled carbon nanotubes (COOH-MWCNTs) in the on- and off-axis flexure and the shear responses of thin carbon woven fabric composite plates. The chemically functionalized COOH-MWCNTs were used to fabricate epoxy nanocomposites and, subsequently, carbon woven fabric plates to be tested on flexure and shear. In addition to the neat epoxy, three loadings of COOH-MWCNTs were examined: 0.5 wt%, 1.0 wt% and 1.5 wt% of epoxy. While no significant statistical difference in the flexure response of the on-axis specimens was observed, significant increases in the flexure strength, modulus and toughness of the off-axis specimens were observed. The average increase in flexure strength and flexure modulus with the addition of 1.5 wt% COOH-MWCNTs improved by 28% and 19%, respectively. Finite element modeling is used to demonstrate fiber domination in on-axis flexure behavior and matrix domination in off-axis flexure behavior. Furthermore, the 1.5 wt% COOH-MWCNTs increased the toughness of carbon woven composites tested on shear by 33%. Microstructural investigation using Fourier Transform Infrared Spectroscopy (FTIR) proves the existence of chemical bonds between the COOH-MWCNTs and the epoxy matrix. PMID:28788698

How geometrical constraints contribute to the weakness of mature faults

USGS Publications Warehouse

Lockner, D.A.; Byerlee, J.D.

1993-01-01

Increasing evidence that the San Andreas fault has low shear strength1 has fuelled considerable discussion regarding the role of fluid pressure in controlling fault strength. Byerlee2,3 and Rice4 have shown how fluid pressure gradients within a fault zone can produce a fault with low strength while avoiding hydraulic fracture of the surrounding rock due to excessive fluid pressure. It may not be widely realised, however, that the same analysis2-4 shows that even in the absence of fluids, the presence of a relatively soft 'gouge' layer surrounded by harder country rock can also reduce the effective shear strength of the fault. As shown most recently by Byerlee and Savage5, as the shear stress across a fault increases, the stress state within the fault zone evolves to a limiting condition in which the maximum shear stress within the fault zone is parallel to the fault, which then slips with a lower apparent coefficient of friction than the same material unconstrained by the fault. Here we confirm the importance of fault geometry in determining the apparent weakness of fault zones, by showing that the apparent friction on a sawcut granite surface can be predicted from the friction measured in intact rock, given only the geometrical constraints introduced by the fault surfaces. This link between the sliding friction of faults and the internal friction of intact rock suggests a new approach to understanding the microphysical processes that underlie friction in brittle materials.

Comparative evaluation of compressive strength, diametral tensile strength and shear bond strength of GIC type IX, chlorhexidine-incorporated GIC and triclosan-incorporated GIC: An in vitro study.

PubMed

Jaidka, Shipra; Somani, Rani; Singh, Deepti J; Shafat, Shazia

2016-04-01

To comparatively evaluate the compressive strength, diametral tensile strength, and shear bond strength of glass ionomer cement type IX, chlorhexidine-incorporated glass ionomer cement, and triclosan-incorporated glass ionomer cement. In this study, glass ionomer cement type IX was used as a control. Chlorhexidine diacetate, and triclosan were added to glass ionomer cement type IX powder, respectively, in order to obtain 0.5, 1.25, and 2.5% concentrations of the respective experimental groups. Compressive strength, diametral tensile strength, and shear bond strength were evaluated after 24 h using Instron Universal Testing Machine. The results obtained were statistically analyzed using the independent t-test, Dunnett test, and Tukey test. There was no statistical difference in the compressive strength, diametral tensile strength, and shear bond strength of glass ionomer cement type IX (control), 0.5% triclosan-glass ionomer cement, and 0.5% chlorhexidine-glass ionomer cement. The present study suggests that the compressive strength, diametral tensile strength, and shear bond strength of 0.5% triclosan-glass ionomer cement and 0.5% chlorhexidine-glass ionomer cement were similar to those of the glass ionomer cement type IX, discernibly signifying that these can be considered as viable options for use in pediatric dentistry with the additional value of antimicrobial property along with physical properties within the higher acceptable range.

Effect of metal surface topography on mechanical bonding at simulated total hip stem-cement interfaces.

PubMed

Chen, C Q; Scott, W; Barker, T M

1999-01-01

Bonding and loosening mechanisms between bone cement and joint prostheses have not been well identified. In this study, the effects of simulated hip stem surface topography on the interfacial shear strength were examined. Six different surface topographies were used. They were described by several surface characterization parameters that may directly relate to the interfacial bonding strength: average surface roughness R(a), root mean square slope R(Deltaq), correlation length beta, and fluid retention index R(ri). The shear strengths between Palacos E bone cement and stainless steel rods were measured using an Instron materials testing machine. We found that cement can "flow" into the surface microtopography and establish good contact with the metal surface. The results show that the interfacial strength increases monotonically with the increase of R(Deltaq) instead of with R(a). The relationship between interfacial strength and surface parameters shows that a metal stem with an isotropic surface texture, higher R(Deltaq), and greater R(ri) gives a higher interfacial strength. Copyright 1999 John Wiley & Sons, Inc.

In-vitro study of resin-modified glass ionomer cements for cementation of orthodontic bands. Isolation, surplus removal and humidity as factors influencing the bond strength between enamel, cement and metal.

PubMed

Liebmann, S M; Jost-Brinkmann, P G

1999-01-01

The aim of this in vitro study was to investigate different light-cured and chemically cured resin-modified glass ionomer cements used for the cementation of orthodontic bands and to analyze various factors influencing the adhesive strength between enamel, cement and stainless steel. Four resin-modified glass ionomers (Fuji Ortho LC/GC, Fuji Duet/GC, Unitek Multi-Cure Glass Ionomer Orthodontic Band Cement/3M Unitek, Vitremer/3M) and 1 compomer (Band-Lok/Reliance) were examined. Flattened and polished bovine teeth embedded in polyurethane resin were used as enamel specimens. Before cementation, 50% of the specimens were moistened with the aerosol of an inhalation device, while the rest were dried with compressed air. Stainless steel cylinders (CrNi 18 10) were perpendicularly bonded onto the polished enamel using a custom-made cementation device and immediately topped with a pressure of 0.25 MPa. The cement was isolated with either Ketac Glaze/ESPE, Fuji Coat/GC, Cacao Butter/GC, Dryfoil/Jalenko or Final Varnish/VOCO, or was left uncoated. Eight minutes after the beginning of mixing, either the surplus cement was removed with a scalpel or surplus removal was simulated with ultrasound. After 24 hours storage in a water bath at 37 degrees C and 1,000 thermocycles the shear bond strength was determined. Significant differences with respect to the shear bond strength were found among the following cements, ranking from highest to lowest: Fuji Duet, Unitek cement > Fuji Ortho LC > Vitremer > Band-Lok. The application of a barrier coating significantly increased the shear bond strength of all cements except Fuji Ortho LC. The light-cured resin Ketac Glaze proved to be the most effective barrier coating. A dry enamel surface increased the bond strength of all investigated cements except Unitek cement. The use of ultrasound led to no significant reduction in shear bond strength in comparison with surplus removal with a scalpel.

Rheological Behavior Xanthan and SlurryPro Polymer Solutions Evaluated as Shear Thinning Delivery Fluids for Subsurface Remediation

NASA Astrophysics Data System (ADS)

Zhong, L.; Oostrom, M.; Truex, M.; Vermeul, V.

2011-12-01

Shear thinning fluids can be applied as a delivery means to enhance the uniformity of remedial amendment distribution in heterogeneous aquifers, thereby to improve remediation performance. The rheological behavior of biopolymer xanthan gum and synthetic polymer SlurryPro were tested, and their influence on the amendment delivery performance was evaluated. The impact of polymer concentration, basic water chemistry, salinity (e.g., Br-, Na+, Ca2+ concentrations), remedial amendments (phosphate, sodium lactate, ethyl lactate, lactate oil, whey), sediments, and the mixing approach on the rheological properties of the polymer solutions was determined. The SlurryPro polymer lost shear-thinning properties even at relatively low solution ionic strength. However, the xanthan gum polymer maintained shear-thinning properties under most of the tested conditions, though with some loss in absolute viscosity with increasing ionic strength. Xanthan appeared to be the better candidate for enhanced amendment delivery. Increasing in xanthan concentration not only increased the solution viscosity, but also increased degree of shear thinning. Addition of salt decreased the solution viscosity and the degree of shear thinning, while the influence was diminished when the polymer concentration was higher. After reaching a critical xanthan concentration, addition of salt increased solution viscosity. The degradation of xanthan and SlurryPro in the presence of site aquifer materials and microbes was studied in batch tests in which the field sediment/water ratio was simulated. The viscosity of the polymer solutions dropped 85% or more in the first week, while the solution chemical oxygen demand (COD) decreasing occurred at a much slower rate.

The Effect of Titanium Tetrafluoride and Sodium Hypochlorite on the Shear Bond Strength of Methacrylate and Silorane Based Composite Resins: an In-Vitro Study.

PubMed

Sharafeddin, Farahnaz; Koohpeima, Fatemeh; Razazan, Nader

2017-06-01

The bond strength of composites with different adhesive systems with dentin is an important factor in long term durability of composite restorations. The effect of titanium tetrafluoride (TiF 4 ) as anti caries agent and sodium hypochlorite (NaOCl) as disinfectant on the shear bond of nanofilled and silorane based composite resins have not been investigated in previous studies. This study was conducted to determine bond strength between dentin and two composite systems, by means of shear bond test using TiF 4 and NaOCl. Middle dentin of 60 intact extracted maxillary premolar teeth were exposed by sectioning the crowns at a depth of 2mm from central groove and parallel to the occlusal surface. Standardized smear layer was created using a 600-grit silicon carbide paper and then samples were embedded in acrylic resin blocks. Then the samples were randomly divided into 6 \\groups summarized as Group I: Z350, Group II: Z350+ NaOCl, Group III: Z350+ TiF 4 , Group IV: P90, Group V: P90+ NaOCl, Group VI: P90+ TiF 4 according to manufacturer's instruction. Then samples were subjected to shear bond strength (SBS) test using universal testing machine and data were analyzed using ANOVA and Tukey tests ( p < 0.05). Application of 5% NaOCl caused a significant decrease in SBS of nanofilled composite resin ( p = 0.004), and also silorane based composite resin ( p = 0.006). Application of 4% TiF 4 caused a significant increase in SBS of silorane based composite resin ( p = 0.001). The effect of TiF 4 on nanofilled composite was not statistically significant. Using TiF 4 has a positive effect on increasing the shear bond while NaOCl has negative effect on bond strength.

Influence of caries infiltrant contamination on shear bond strength of different adhesives to dentin.

PubMed

Jia, Liuhe; Stawarczyk, Bogna; Schmidlin, Patrick R; Attin, Thomas; Wiegand, Annette

2013-03-01

To analyze whether the contamination with a caries infiltrant system impairs the adhesive performance of etch-and-rinse and self-etching adhesives on dentin. Dentin contamination with the caries infiltrant system (Icon, DMG) was simulated by applying either hydrochloric acid (15 % HCl, Icon Etch, 15 s), the resin infiltrant (Icon infiltrant, 4 min), or both prior to the application of the respective adhesives (each group n = 10). In the control groups, the etch-and-rinse adhesive (Optibond FL, Kerr) and the self-etching adhesive (iBOND Self Etch, Hereaus) were applied without former contamination with the infiltrant system. Additionally, the adhesive performance of the resin infiltrant alone was tested. Shear bond strength of a nano-hybrid composite was analyzed after thermocycling (5,000×, 5-55°C) of the specimens and analyzed by ANOVA/Scheffé post hoc tests (p < 0.05) and Weibull statistics. Failure mode was inspected under a stereomicroscope at × 25 magnification. Contamination with the resin infiltrant alone did not impair shear bond strength, while contamination with hydrochloric acid or with hydrochloric acid and the resin infiltrant reduced shear bond strength (MPa) of the adhesives (Optibond FL: 20.5 ± 3.6, iBOND Self Etch: 17.9 ± 2.6) significantly. Hydrochloric acid contamination increased the number of adhesive failures. The adhesive performance of the caries infiltrant system alone was insufficient. The contamination with the caries infiltrant system impaired the shear bond strength of conventional dental adhesives. Contamination of the caries infiltrant system on dentin should be avoided due to the detrimental effect of hydrochloric acid etching.

Stability performance and interface shear strength of geocomposite drain/soil systems

NASA Astrophysics Data System (ADS)

Othman, Maidiana; Frost, Matthew; Dixon, Neil

2018-02-01

Landfill covers are designed as impermeable caps on top of waste containment facilities after the completion of landfill operations. Geocomposite drain (GD) materials consist of a geonet or geospacer (as a drainage core) sandwiched between non-woven geotextiles that act as separators and filters. GD provides a drainage function as part of the cover system. The stability performance of landfill cover system is largely controlled by the interface shear strength mobilized between the elements of the cover. If a GD is used, the interface shear strength properties between the upper surface of the GD and the overlying soil may govern stability of the system. It is not uncommon for fine grained materials to be used as cover soils. In these cases, understanding soil softening issues at the soil interface with the non-woven geotextile is important. Such softening can be caused by capillary break behaviour and build-up of water pressures from the toe of the drain upwards into the cover soil. The interaction processes to allow water flow into a GD core through the soil-geotextile interface is very complex. This paper reports the main behaviour of in-situ interface shear strength of soil-GD using field measurements on the trial landfill cover at Bletchley, UK. The soil softening at the interface due to soaked behaviour show a reduction in interface shear strength and this aspect should be emphasized in design specifications and construction control. The results also help to increase confidence in the understanding of the implications for design of cover systems.

Analysis and Tests of Reinforced Carbon-Epoxy/Foam-Core Sandwich Panels with Cutouts

NASA Technical Reports Server (NTRS)

Baker, Donald J.; Rogers, Charles

1996-01-01

The results of a study of a low-cost structurally efficient minimum-gage shear-panel design that can be used in light helicopters are presented. The shear-panel design is based on an integrally stiffened syntactic-foam stabilized-skin with an all-bias-ply tape construction for stabilized-skin concept with an all-bias-ply tape construction for the skins. This sandwich concept is an economical way to increase the panel bending stiffness weight penalty. The panels considered in the study were designed to be buckling resistant up to 100 lbs/in. of shear load and to have an ultimate strength of 300 lbs/in. The panel concept uses unidirectional carbon-epoxy tape on a syntactic adhesive as a stiffener that is co-cured with the skin and is an effective concept for improving panel buckling strength. The panel concept also uses pultruded carbon-epoxy rods embedded in a syntactic adhesive and over-wrapped with a bias-ply carbon-epoxy tape to form a reinforcing beam which is an effective method for redistributing load around rectangular cutout. The buckling strength of the reinforced panels is 83 to 90 percent of the predicted buckling strength based on a linear buckling analysis. The maximum experimental deflection exceeds the maximum deflection predicted by a nonlinear analysis by approximately one panel thickness. The failure strength of the reinforced panels was two and a half to seven times of the buckling strength. This efficient shear-panel design concept exceeds the required ultimate strength requirement of 300 lbs/in by more than 100 percent.

Bond strength of etch-and-rinse and self-etch adhesive systems to enamel and dentin irradiated with a novel CO2 9.3 μm short-pulsed laser for dental restorative procedures.

PubMed

Rechmann, Peter; Bartolome, N; Kinsel, R; Vaderhobli, R; Rechmann, B M T

2017-12-01

The objective of this study was to evaluate the influence of CO 2 9.3 μm short-pulsed laser irradiation on the shear bond strength of composite resin to enamel and dentin. Two hundred enamel and 210 dentin samples were irradiated with a 9.3 µm carbon dioxide laser (Solea, Convergent Dental, Inc., Natick, MA) with energies which either enhanced caries resistance or were effective for ablation. OptiBond Solo Plus [OptiBondTE] (Kerr Corporation, Orange, CA) and Peak Universal Bond light-cured adhesive [PeakTE] (Ultradent Products, South Jordan, UT) were used. In addition, Scotchbond Universal [ScotchbondSE] (3M ESPE, St. Paul, MN) and Peak SE self-etching primer with Peak Universal Bond light-cured adhesive [PeakSE] (Ultradent Products) were tested. Clearfil APX (Kuraray, New York, NY) was bonded to the samples. After 24 h, a single plane shear bond test was performed. Using the caries preventive setting on enamel resulted in increased shear bond strength for all bonding agents except for self-etch PeakSE. The highest overall bond strength was seen with PeakTE (41.29 ± 6.04 MPa). Etch-and-rinse systems achieved higher bond strength values to ablated enamel than the self-etch systems did. PeakTE showed the highest shear bond strength with 35.22 ± 4.40 MPa. OptiBondTE reached 93.8% of its control value. The self-etch system PeakSE presented significantly lower bond strength. The shear bond strength to dentin ranged between 19.15 ± 3.49 MPa for OptiBondTE and 43.94 ± 6.47 MPa for PeakSE. Etch-and-rinse systems had consistently higher bond strength to CO 2 9.3 µm laser-ablated enamel. Using the maximum recommended energy for dentin ablation, the self-etch system PeakSE reached the highest bond strength (43.9 ± 6.5 MPa).

The effects of dentin and intaglio indirect ceramic optimized polymer restoration surface treatment on the shear bond strength of resin cement

NASA Astrophysics Data System (ADS)

Puspitarini, A.; Suprastiwi, E.; Usman, M.

2017-08-01

Ceramic optimized polymer (ceromer) bonds to the tooth substrate through resin cements. The bond strength between dentin, resin cement, and ceromer depends on the applied surface treatment. To analyze the effects of dentin and intaglio ceromer surface treatment on the shear bond strength self-adhesive resin cement. Forty-five dentin premolar and ceromer specimens were bonded with resin cement and divided into three groups as follows: in group 1, no treatment was applied; in group 2, dentin surface treatment was carried out with acid etching and a bonding agent; and in group 3, dentin surface treatment was carried out with acid etching, a bonding agent, and intaglio ceromer surface treatment with etching and silane. All specimens were incubated at 37 °C for 24 hours, and the shear bond strength was measured using a universal testing machine. Group 3 showed the highest shear bond strength, followed by group 2. The surface treatment of dentin and intaglio ceromer showed significantly improved shear bond strength in the group comparison. Dentin and intaglio ceromer surface treatment can improved the shear bond strength self-adhesive resin cement.

Educational Brief: Using Space for a Better Foundation on Earth Mechanics of Granular Materials

NASA Technical Reports Server (NTRS)

Dooling, Dave (Editor)

2002-01-01

Soils are three-phase composite materials that consist of soil, solid particles, and voids filled with water and/or air. Based on the particle-size distribution, they are generally classified as fine-grained (clays and plastic silts) and coarse-grained soils (nonplastic silts, sand, and gravel). Soil's resistance to external loadings is mainly derived from friction between particles and cohesion. Friction resistance is due to particles' surface-to-surface friction, interlocking, crushing, rearrangement, and dilation (or expansion) during shearing. Cohesion can be due to chemical cementation between particles, electrostatic and electromagnetic forces, and soil-water reaction and equilibrium. The basic factor responsible for the strength of coarse-grained soils is friction. Cohesion can be ignored. This educational brief focuses on measuring shear strength of sands (typical example of coarse-grained soils) where, for the same material, packing density is a main factor to be considered when one asks about the shear strength value. As the external load is applied, the soil's resistance is attained through shearing resistance, which causes the soil volume to increase (expand) or decrease (compress) depending on the initial packing density.

Failure waves in glass and ceramics under shock compression

NASA Astrophysics Data System (ADS)

Brar, N. S.

2000-04-01

The response of various types of glasses (fused silica, borosilicates, soda-lime, and lead filled) to shock wave loading, especially the failure of glass behind the shock wave through the "so called" failure wave or front, has been the subject of intense research among a number of investigators. The variations in material properties across this front include complete loss of tensile (spall) strength, loss in shear strength, reduction in acoustic impedance and opacity to light. Both the Stress and velocity history from VISAR measurements have shown that the failure front propagates at a speed of 1.5 to 2.5 mm/s, depending on the peak shock stress. The shear strength [τ=1/2(σ1-σ2)] behind the failure front, determined using embedded transverse gauges, is found to decrease to about 1 GPa for soda-lime, borosilicate, and filled glasses. Optical (high-speed photography) observations also confirm formation of this failure front. There is a general agreement among various researchers on these failure observations. However, three proposed mechanisms for the formation of failure front are based on totally different formulations. The first, due to Clifton, is based on the hypothesis of densification of glass under shock compression. Densification is followed by shear failure around inhomogeneities resulting in a phase boundary between the comminuted and the intact material. The second, proposed by Grady, involves the transfer of elastic shear strain energy to dilatant strain energy as a result of severe micro-cracking originating from impact. The third, by Espinosa and Brar, proposes that the front is created through shear micro-cracks, which nucleate and propagate from the impact face; as originally suggested by Kanel. This later mechanism is supported by the observed loss of shear strength of glass by Clifton et al. at shock stress above the threshold level. Espinosa has incorporated this mechanism in multiple-plane model and simulations predict the increase in lateral stress and an observed reduction in spall strength behind the failure front. Failure front studies, in terms of loss of shear strength, have been recently extended to alumina and SiC ceramics by Bourne et al.

Ideal strength of bcc molybdenum and niobium

NASA Astrophysics Data System (ADS)

Luo, Weidong; Roundy, D.; Cohen, Marvin L.; Morris, J. W.

2002-09-01

The behavior of bcc Mo and Nb under large strain was investigated using the ab initio pseudopotential density-functional method. We calculated the ideal shear strength for the {211}<111> and {011}<111> slip systems and the ideal tensile strength in the <100> direction, which are believed to provide the minimum shear and tensile strengths. As either material is sheared in either of the two systems, it evolves toward a stress-free tetragonal structure that defines a saddle point in the strain-energy surface. The inflection point on the path to this tetragonal ``saddle-point'' structure sets the ideal shear strength. When either material is strained in tension along <100>, it initially follows the tetragonal, ``Bain,'' path toward a stress-free fcc structure. However, before the strained crystal reaches fcc, its symmetry changes from tetragonal to orthorhombic; on continued strain it evolves toward the same tetragonal saddle point that is reached in shear. In Mo, the symmetry break occurs after the point of maximum tensile stress has been passed, so the ideal strength is associated with the fcc extremum as in W. However, a Nb crystal strained in <100> becomes orthorhombic at tensile stress below the ideal strength. The ideal tensile strength of Nb is associated with the tetragonal saddle point and is caused by failure in shear rather than tension. In dimensionless form, the ideal shear and tensile strengths of Mo (τ*=τm/G111=0.12, σ*=σm/E100=0.078) are essentially identical to those previously calculated for W. Nb is anomalous. Its dimensionless shear strength is unusually high, τ*=0.15, even though the saddle-point structure that causes it is similar to that in Mo and W, while its dimensionless tensile strength, σ*=0.079, is almost the same as that of Mo and W, even though the saddle-point structure is quite different.

EFFECT OF RADIUS OF LOADING NOSE AND SUPPORTS IN SHORT BEAM TEST FIXTURE ON FRACTURE MODE AND INTERLAMINAR SHEAR STRENGTH OF GFRP AT 77 K

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nishimura, A.

2008-03-03

A short beam test is useful to evaluate interlaminar shear strength of glass fiber reinforced plastics, especially for material selection. However, effect of test fixture configuration on interlaminar shear strength has not been clarified. This paper describes dependence of fracture mode and interlaminar shear strength on the fixture radius using the same materials and procedure. In addition, global understanding of the role of the fixture is discussed. When small loading nose and supports are used for the tests, bending fracture or translaminar fracture happens and the interlaminar shear strength would become smaller. By adopting the large radius loading nose andmore » supports (6 mm radius is recommended), it is newly recognized that some stress concentration is able to be reduced, and the interlaminar fracture tends to occur and the other fracture modes will be suppressed. The interlaminar shear strength of 2.5 mm thick GFRP plate of G-10CR is evaluated as 130-150 MPa at 77 K.« less

Interface effects on mechanical properties of particle-reinforced composites.

PubMed

Debnath, S; Ranade, R; Wunder, S L; McCool, J; Boberick, K; Baran, G

2004-09-01

Effective bonding between the filler and matrix components typically improves the mechanical properties of polymer composites containing inorganic fillers. The aim of this study was to test the hypothesis that composite flexural modulus, flexure strength, and toughness are directly proportional to filler-matrix interfacial shear strength. The resin matrix component of the experimental composite consisted of a 60:40 blend of BisGMA:TEGDMA. Two levels of photoinitiator components were used: 0.15, and 0.5%. Raman spectroscopy was used to determine degree of cure, and thermogravimetry (TGA) was used to quantify the degree of silane, rubber, or polymer attachment to silica and glass particles. Filler-matrix interfacial shear strengths were measured using a microbond test. Composites containing glass particles with various surface treatments were prepared and the modulus, flexure strength, and fracture toughness of these materials obtained using standard methods. Mechanical properties were measured on dry and soaked specimens. The interfacial strength was greatest for the 5% MPS treated silica, and it increased for polymers prepared with 0.5% initiator compared with 0.15% initiator concentrations. For the mechanical properties measured, the authors found that: (1) the flexural modulus was independent of the type of filler surface treatment, though flexural strength and toughness were highest for the silanated glass; (2) rubber at the interface, whether bonded to the filler and matrix or not, did not improve toughness; (3) less grafting of resin to silanated filler particles was observed when the initiator concentration decreased. These findings suggest that increasing the strength of the bond between filler and matrix will not result in improvements in the mechanical properties of particulate-reinforced composites in contrast to fiber-reinforced composites. Also, contraction stresses in the 0.5 vs 0.15% initiator concentration composites may be responsible for increases in interfacial shear strengths, moduli, and flexural strengths.

Shear Behavior Models of Steel Fiber Reinforced Concrete Beams Modifying Softened Truss Model Approaches

PubMed Central

Hwang, Jin-Ha; Lee, Deuck Hang; Ju, Hyunjin; Kim, Kang Su; Seo, Soo-Yeon; Kang, Joo-Won

2013-01-01

Recognizing that steel fibers can supplement the brittle tensile characteristics of concrete, many studies have been conducted on the shear performance of steel fiber reinforced concrete (SFRC) members. However, previous studies were mostly focused on the shear strength and proposed empirical shear strength equations based on their experimental results. Thus, this study attempts to estimate the strains and stresses in steel fibers by considering the detailed characteristics of steel fibers in SFRC members, from which more accurate estimation on the shear behavior and strength of SFRC members is possible, and the failure mode of steel fibers can be also identified. Four shear behavior models for SFRC members have been proposed, which have been modified from the softened truss models for reinforced concrete members, and they can estimate the contribution of steel fibers to the total shear strength of the SFRC member. The performances of all the models proposed in this study were also evaluated by a large number of test results. The contribution of steel fibers to the shear strength varied from 5% to 50% according to their amount, and the most optimized volume fraction of steel fibers was estimated as 1%–1.5%, in terms of shear performance. PMID:28788364

Flowability parameters for chopped switchgrass, wheat straw and corn stover

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chevanan, Nehru; Womac, A.R.; Bitra, V.S.P.

2009-02-01

A direct shear cell to measure the shear strength and flow properties of chopped switchgrass, wheat straw, and corn stover was designed, fabricated, and tested. Yield loci (r2=0.99) determined at pre-consolidation pressures of 3.80 kPa and 5.02 kPa indicated that chopped biomass followed Mohr-Coulomb failure. Normal stress significantly affected the displacement required for shear failure, as well as the friction coefficient values for all three chopped biomass types. Displacement at shear failure ranged from 30 to 80 mm, and depended on pre-consolidation pressure, normal stress, and particle size. Friction coefficient was inversely related to normal stress, and was highest formore » chopped corn stover. Also, chopped corn stover exhibited the highest angle of internal friction, unconfined yield strength, major consolidation strength, and cohesive strength, all of which indicated increased challenges in handling chopped corn stover. The measured angle of internal friction and cohesive strength indicated that chopped biomass cannot be handled by gravity alone. The measured angle of internal friction and cohesive strength were 43 and 0.75 kPa for chopped switchgrass; 44 and 0.49 kPa for chopped wheat straw; and 48 and 0.82 kPa for chopped corn stover. Unconfined yield strength and major consolidation strength used for characterization of bulk flow materials and design of hopper dimensions were 3.4 and 10.4 kPa for chopped switchgrass; 2.3 and 9.6 kPa for chopped wheat straw and 4.2 and 11.8 kPa for chopped corn stover. These results are useful for development of efficient handling, storage, and transportation systems for biomass in biorefineries.« less

Bond strength and microleakage of current dentin adhesives.

PubMed

Fortin, D; Swift, E J; Denehy, G E; Reinhardt, J W

1994-07-01

The purpose of this in vitro study was to evaluate shear bond strengths and microleakage of seven current-generation dentin adhesive systems. Standard box-type Class V cavity preparations were made at the cemento-enamel junction on the buccal surfaces of eighty extracted human molars. These preparations were restored using a microfill composite following application of either All-Bond 2 (Bisco), Clearfil Liner Bond (Kuraray), Gluma 2000 (Miles), Imperva Bond (Shofu), OptiBond (Kerr), Prisma Universal Bond 3 (Caulk), Scotchbond Multi-Purpose (3M), or Scotchbond Dual-Cure (3M) (control). Lingual dentin of these same teeth was exposed and polished to 600-grit. Adhesives were applied and composite was bonded to the dentin using a gelatin capsule technique. Specimens were thermocycled 500 times. Shear bond strengths were determined using a universal testing machine, and microleakage was evaluated using a standard silver nitrate staining technique. Clearfill Liner Bond and OptiBond, adhesive systems that include low-viscosity, low-modulus intermediate resins, had the highest shear bond strengths (13.3 +/- 2.3 MPa and 12.9 +/- 1.5 MPa, respectively). Along with Prisma Universal Bond 3, they also had the least microleakage at dentin margins of Class V restorations. No statistically significant correlation between shear bond strength and microleakage was observed in this study. Adhesive systems that include a low-viscosity intermediate resin produced the high bond strengths and low microleakage. Similarly, two materials with bond strengths in the intermediate range had significantly increased microleakage, and one material with a bond strength in the low end of the spectrum exhibited microleakage that was statistically greater. Thus, despite the lack of statistical correlation, there were observable trends.

Novel Composites for Wing and Fuselage Applications: Speedy Nonlinear Analysis of Postbuckled Panels in Shear (SNAPPS)

NASA Technical Reports Server (NTRS)

Sharp, Dave; Sobel, Larry

1997-01-01

A simple and rapid analysis method, consisting of a number of modular, 'strength-of-materials-type' models, is presented for predicting the nonlinear response and stiffener separation of postbuckled, flat, composite, shear panels. The analysis determines the maximum principal tensile stress in the skin surface layer under to toe. Failure is said to occur when this stress reaches the mean transverse tensile strength of the layer. The analysis methodology consists of a number of closed-form equations that can easily be used in a 'hand analysis. For expediency, they have been programmed into a preliminary design code called SNAPPS (Speedy Nonlinear Analysis of Postbuckled Panels in Shear), which rapidly predicts postbuckling response of the panel for each value of the applied shear load. SNAPPS response and failure predictions were found to agree well with test results for three panels with widely different geometries, laminates and stiffnesses. Design guidelines are given for increasing the load-carrying capacity of stiffened, composite shear panels.

Constant load and constant volume response of municipal solid waste in simple shear.

PubMed

Zekkos, Dimitrios; Fei, Xunchang

2017-05-01

Constant load and constant volume simple shear testing was conducted on relatively fresh municipal solid waste (MSW) from two landfills in the United States, one in Michigan and a second in Texas, at respective natural moisture content below field capacity. The results were assessed in terms of two failure strain criteria, at 10% and 30% shear strain, and two interpretations of effective friction angle. Overall, friction angle obtained assuming that the failure plane is horizontal and at 10% shear strain resulted in a conservative estimation of shear strength of MSW. Comparisons between constant volume and constant load simple shear testing results indicated significant differences in the shear response of MSW with the shear resistance in constant volume being lower than the shear resistance in constant load. The majority of specimens were nearly uncompacted during specimen preparation to reproduce the state of MSW in bioreactor landfills or in uncontrolled waste dumps. The specimens had identical percentage of <20mm material but the type of <20mm material was different. The <20mm fraction from Texas was finer and of high plasticity. MSW from Texas was overall weaker in both constant load and constant volume conditions compared to Michigan waste. The results of these tests suggest the possibility of significantly lower shear strength of MSW in bioreactor landfills where waste is placed with low compaction effort and constant volume, i.e., "undrained", conditions may occur. Compacted MSW specimens resulted in shear strength parameters that are higher than uncompacted specimens and closer to values reported in the literature. However, the normalized undrained shear strength in simple shear for uncompacted and compacted MSW was still higher than the normalized undrained shear strength reported in the literature for clayey and silty soils. Copyright © 2016 Elsevier Ltd. All rights reserved.

Evaluation of Rhenium Joining Methods

NASA Technical Reports Server (NTRS)

Reed, Brian D.; Morren, Sybil H.

1995-01-01

Coupons of rhenium-to-Cl03 flat plate joints, formed by explosive and diffusion bonding, were evaluated in a series of shear tests. Shear testing was conducted on as-received, thermally-cycled (100 cycles, from 21 to 1100 C), and thermally-aged (3 and 6 hrs at 1100 C) joint coupons. Shear tests were also conducted on joint coupons with rhenium and/or Cl03 electron beam welded tabs to simulate the joint's incorporation into a structure. Ultimate shear strength was used as a figure of merit to assess the effects of the thermal treatment and the electron beam welding of tabs on the joint coupons. All of the coupons survived thermal testing intact and without any visible degradation. Two different lots of as-received, explosively-bonded joint coupons had ultimate shear strengths of 281 and 310 MPa and 162 and 223 MPa, respectively. As-received, diffusion-bonded coupons had ultimate shear strengths of 199 and 348 MPa. For the most part, the thermally-treated and rhenium weld tab coupons had shear strengths slightly reduced or within the range of the as-received values. Coupons with Cl03 weld tabs experienced a significant reduction in shear strength. The degradation of strength appeared to be the result of a poor heat sink provided during the electron beam welding. The Cl03 base material could not dissipate heat as effectively as rhenium, leading to the formation of a brittle rhenium-niobium intermetallic.

The Effect of Veneer Layers on the Bending Shear Strength and Delamination of Laminated Veneer Lumber (LVL) from Oil Palm Trunk (OPT)

NASA Astrophysics Data System (ADS)

Jamaludin, M. A.; Nordin, K.; Bahari, S. A.; Ahmad, M.

2010-03-01

The aim of this study was to evaluate the effects of the number of veneer layers on the bending shear strength and delamination of Laminated Veneer Lumber (LVL) from oil palm trunk (OPT). Five (5), Six (6) and Seven (7) veneer layers of OPT LVL were manufactured. The dimension of the boards was 45 cm by 45 cm by 1.9 cm. The boards were hot pressed for 13 minutes at a pressure of 31 kgf per m2. Urea formaldehyde (UF) supplied by a local adhesive manufacturer was used as the binder for the boards. The bending shear tests consisted of the edgewise and flatwise tests, whereas the delamination test consisted of the cold and hot water boil tests. The preparation of the test specimens and tests set-up was in accordance to the Japanese Standards, JAS-1991 [1]. Six replications were used for each test. The results were analyzed by Analysis of Variance (ANOVA) using the Duncan's Multiple Range Test to test for significant differences. The results indicated that as the number of layers increased the strength also increased. All the boards passed the standard. The difference in strength between the different types of samples was significant at 95 percent confidence level. Bending shear failures were primarily in the veneers. It is possible to use the boards as light weight interior building and furniture components. Over the years, the supply of quality timber resources from the natural forest has decrease as the wood-based industry experienced rapid growth. The supply of rubberwood for the furniture industry is also decreasing as a result of increase latex price. Accordingly, OPT LVL can be an alternative or supplementary raw material for the wood-based industry.

Comparison of enamel bond fatigue durability of universal adhesives and two-step self-etch adhesives in self-etch mode.

PubMed

Tsujimoto, Akimasa; Barkmeier, Wayne W; Hosoya, Yumiko; Nojiri, Kie; Nagura, Yuko; Takamizawa, Toshiki; Latta, Mark A; Miyazaki, Masashi

2017-10-01

To comparatively evaluate universal adhesives and two-step self-etch adhesives for enamel bond fatigue durability in self-etch mode. Three universal adhesives (Clearfil Universal Bond; G-Premio Bond; Scotchbond Universal Adhesive) and three two-step self-etch adhesives (Clearfil SE Bond; Clearfil SE Bond 2; OptiBond XTR) were used. The initial shear bond strength and shear fatigue strength of the adhesive to enamel in self-etch mode were determined. The initial shear bond strengths of the universal adhesives to enamel in self-etch mode was significantly lower than those of two-step self-etch adhesives and initial shear bond strengths were not influenced by type of adhesive in each adhesive category. The shear fatigue strengths of universal adhesives to enamel in self-etch mode were significantly lower than that of Clearfil SE Bond and Clearfil SE Bond 2, but similar to that OptiBond XTR. Unlike two-step self-etch adhesives, the initial shear bond strength and shear fatigue strength of universal adhesives to enamel in self-etch mode was not influenced by the type of adhesive. This laboratory study showed that the enamel bond fatigue durability of universal adhesives was lower than Clearfil SE Bond and Clearfil SE Bond 2, similar to Optibond XTR, and was not influenced by type of adhesive, unlike two-step self-etch adhesives.

Improving the interlaminar shear strength of carbon fiber-epoxy composites through carbon fiber bromination

NASA Technical Reports Server (NTRS)

Jaworske, Donald A.; Maciag, Carolyn

1987-01-01

The use of bromine to improve the interlaminar shear strength of PAN-based carbon fibers was investigated. Composite test specimens fabicated from brominated T-300 fibers and a MY720 matrix exhibited on average a 30% improvement in ILSS over their pristine counterparts. Mass, electrical resistivity, density, contact angle, and scanning Auger microscopy results suggested a mechanism in which the bromine was covalently bonded to the surface of the fiber, and this resulted in an increased van der Waal's adhesion between fiber and matrix.

Effect of surface condition of dental zirconia ceramic (Denzir) on bonding.

PubMed

Uo, Motohiro; Sjögren, Göran; Sundh, Anders; Goto, Mitsunari; Watari, Fumio; Bergman, Maud

2006-09-01

Yttria partially stabilized zirconia (YPSZ) ceramics are suitable for dental and medical use because of their high fracture toughness and chemical durability. The purpose of this study was to examine the bonding behavior of a dental YPSZ ceramic, Denzir. After being subjected to various surface treatments, Denzir specimens were bonded to each other using an adhesive resin composite, glass ionomer, or zinc phosphate cement. Bonding strength was then determined by the shearing test. No significant differences (p>0.05) were observed between SiC- and Al2O3-blasted specimens. In all surface treatments, the shear bond strength significantly (p<0.05) increased in the order of adhesive resin composite cement > glass ionomer cement > zinc phosphate cement. Moreover, silanization with methacryloxy propyl trimethoxysilane slightly increased the bonding strength of the adhesive resin composite cement.

Effect of Oxygen Inhibition Layer of Universal Adhesives on Enamel Bond Fatigue Durability and Interfacial Characteristics With Different Etching Modes.

PubMed

Ouchi, H; Tsujimoto, A; Nojiri, K; Hirai, K; Takamizawa, T; Barkmeier, W W; Latta, M A; Miyazaki, M

The purpose of this study was to evaluate the effect of the oxygen inhibition layer of universal adhesive on enamel bond fatigue durability and interfacial characteristics with different etching modes. The three universal adhesives used were Scotchbond Universal Adhesive (3M ESPE, St Paul, MN, USA), Adhese Universal (Ivoclar Vivadent, Schaan, Lichtenstein), and G-Premio Bond (GC, Tokyo, Japan). The initial shear bond strength and shear fatigue strength to enamel was determined in the presence and absence of the oxygen inhibition layer, with and without phosphoric acid pre-etching. The water contact angle was also measured in all groups using the sessile drop method. The enamel bonding specimens with an oxygen inhibition layer showed significantly higher (p<0.05) initial shear bond strengths and shear fatigue strengths than those without, regardless of the adhesive type and etching mode. Moreover, the water contact angles on the specimens with an oxygen inhibition layer were significantly lower (p<0.05) than on those without, regardless of etching mode. The results of this study suggest that the oxygen inhibition layer of universal adhesives significantly increases the enamel bond fatigue durability and greatly changes interfacial characteristics, suggesting that the bond fatigue durability and interfacial characteristics of these adhesives strongly rely on its presence.

Microstructural Evolution and Local Mechanical Properties of Friction Stir Processed Mg-3Gd-1Zn Cast Alloy

NASA Astrophysics Data System (ADS)

Sabbaghian, M.; Mahmudi, R.

2016-05-01

Microstructural evolution, hardness, and shear strength of the cast plates of GZ31 magnesium alloy were investigated after friction stir processing (FSP). Due to severe plastic deformation and dynamic recrystallization, FSP breaks the dendrites and results in a fine homogenous structure in the stirred zone (SZ) having average grain sizes of about 4.0 and 2.5 μm in the one and two-pass FSPed plates, respectively. As a novel approach, strength of the processed plates was examined by shear punch testing in three regions of the SZ on the surface layer, namely, center line (CL), retreating side (RS), and advancing side (AS). FSP showed great potential in the enhancement of SZ ultimate shear strength from 114 to about 152 and 155 MPa in the one and two-pass FSPed materials, respectively. The same trend was observed in hardness values of the SZ, where the average hardness of the base material increased from 41 to 60 and 68 Vickers after one and two passes of FSP, respectively. The variations in the shear strength of the CL, RS, and AS zones of the SZ were about 5% for the first pass of FSP, the effect which was decreased to less than 2% after two passes of FSP.

In vitro bonding effectiveness of three different one-step self-etch adhesives with additional enamel etching.

PubMed

Batra, Charu; Nagpal, Rajni; Tyagi, Shashi Prabha; Singh, Udai Pratap; Manuja, Naveen

2014-08-01

To evaluate the effect of additional enamel etching on the shear bond strength of three self-etch adhesives. Class II box type cavities were made on extracted human molars. Teeth were randomly divided into one control group of etch and rinse adhesive and three test groups of self-etch adhesives (Clearfil S3 Bond, Futurabond NR, Xeno V). The teeth in the control group (n = 10) were treated with Adper™ Single Bond 2. The three test groups were further divided into two subgroups (n = 10): (i) self-etch adhesive was applied as per the manufacturer's instructions; (ii) additional etching of enamel surfaces was done prior to the application of self-etch adhesives. All cavities were restored with Filtek Z250. After thermocycling, shear bond strength was evaluated using a Universal testing machine. Data were analyzed using anova independent sample's 't' test and Dunnett's test. The failure modes were evaluated with a stereomicroscope at a magnification of 10×. Additional phosphoric acid etching of the enamel surface prior to the application of the adhesive system significantly increased the shear bond strength of all the examined self-etch adhesives. Additional phosphoric acid etching of enamel surface significantly improved the shear bond strength. © 2013 Wiley Publishing Asia Pty Ltd.

Slope stability improvement using low intensity field electrosmosis

NASA Astrophysics Data System (ADS)

Armillotta, Pasquale

2014-05-01

The electrosmosis technique has been introduced in the past for slope stabilization. However, its application to real cases has been scarce due to several drawbacks mostly related to the high intensity electric field needed (1.0 V/cm or higher): the rapid degradation of the electrodes, the high system management cost, the heating and cracking of the soil and the reduction of its colloidal fraction. Thanks to the introduction of new materials, the technique is currently applied to decrease the consolidation time of saturated clay soils (forcing the elimination of water), consequently improving its mechanical strength. In clay soils, the volume variation is influenced by the presence of smectites. The clay compressibility decreases with the increasing of electrolytes concentration. Soil containing smectites that have interacted with calcium showed a reduction or the absence of swelling during hydration with distilled water and a positive increase of their shear strength. The different values of pH between the anode (acid) and the cathode (basic), induced by the electrosmosis create the conditions for the precipitation of CaCO3 near the cathode. The injection of solutions containing calcium in soils and their diffusion induced by the electrosmosis, lead to calcium precipitation and consequential increase of the shear strength. The material technological advances and the laboratory experiences described in this paper, demonstrate that the use low electric field (0.1 V/cm or lower) intensity electrosmosis (LEFE in acronym) can be effective for soil dewatering and shear strength increase while reducing its adverse effect. The LEFE can be used to: reduce the potential for swelling of active clay minerals through the introduction of ions and the precipitation of hardening substances; induce the "dewatering" in cohesive soils. Several Lab activities were carried out, using custom made electrosmosis equipment. These activities can be divided in two phases: Phase 1: Carbonates were mixed to a natural soil obtaining three groups of soil samples at different carbonates level; the geotechnical characterization of each group was carried out; Phase 2: LEFE was applied to induce the precipitation of CaCO3, the reduction of the swelling potential of clay minerals and the increment of the soil shear strength. The outcomes of Phase 1 indicated that: the values of specific gravity of the grains, plasticity index (PI) and Value of Blue (VB) decrease with the increase carbonate content; the shear strength increases with the carbonates content. From the second laboratory phase, we observed: an almost constant pH values within the sample; an increment of the carbonate content after LEFE treatment regardless of its duration; this increment is particularly significant after 60 days of treatment; a reduction of the swelling potential of soil; that the water content at the end of each treatment, regardless of its duration and intensity of the electric field, shows similar values; that the values of the soil shear strength (after 60 days of LEFE treatment) are always greater than those of the natural soil (average +7%). During the LEFE treatment, the pore fluid used is water taken from the local groundwater, with pH = 7.3 and hardness of 34.6 ° F. The CaCO3 content in treated samples increases with the duration of treatment. The application of LEFE appears to be effective in increasing the carbonate content and improve mechanical strenght of the soil; further development of the research will apply the LEFE to an ideal slope model and to a real case.

Alternative Penetrometers to Measure the Near Surface Strength of Soft Seafloor Soils

DTIC Science & Technology

2011-09-30

penetrometer (CPT), standard ball penetrometer (BPT), mini-ball penetrometer (mBPT) and a shear vane ( VST ). The CPT and BPT measure electronically a...The VST records the undrained shear strength of the soil at discreet depths. In addition, Shelby tube samples were collected for triaxial and...benchmark strengths from the VST and triaxial/simple shear tests. Thus far, the VST strengths have compared favorably with the results. Results from the

Combined-load buckling behavior of metal-matrix composite sandwich panels under different thermal environments

NASA Technical Reports Server (NTRS)

Ko, William L.; Jackson, Raymond H.

1991-01-01

Combined compressive and shear buckling analysis was conducted on flat rectangular sandwich panels with the consideration of transverse shear effects of the core. The sandwich panel is fabricated with titanium honeycomb core and laminated metal matrix composite face sheets. The results show that the square panel has the highest combined load buckling strength, and that the buckling strength decreases sharply with the increases of both temperature and panel aspect ratio. The effect of layup (fiber orientation) on the buckling strength of the panels was studied in detail. The metal matrix composite sandwich panel was much more efficient than the sandwich panel with nonreinforced face sheets and had the same specific weight.

Effect of water storage on the silanization in porcelain repair strength.

PubMed

Berry, T; Barghi, N; Chung, K

1999-06-01

This study examined the long-term water storage affect of silanization on shear bond strength of composite resin to porcelain. One hundred and sixty square-shaped specimens were fabricated and sanded flat sequentially with silicone carbide papers. The specimens were then placed into four groups and 16 subgroups of 10 specimens each randomly. Four commercially available silane systems, two one-mix and two two-mix, were tested in this study. Teflon tubes with an internal diameter of 2.97 mm and 2 mm in height were filled with a dual cure composite resin (Mirage FLC), placed on the silanated surfaces and light-cured for 120 s. Specimens were stored in room temperature water and subjected to shear bond strength testing after 24 h, 1 week, 1 month and 3 month periods of immersion. An Instron Universal testing machine with a crosshead speed of 0.5 mm/min was used for the testing. The mean values of the shear bond strengths ranged from 4.38 MPa (24-h period) to 23.90 MPa (3-month period). ANOVA and Scheffe' tests were used to analyse data with confidence level at 95%. All groups recorded an increase in bond strength after one week as compared with the 24-h period (P<0.05). With the exception of a one-mix system, all systems showed significantly higher bond strength at 3 weeks as compared with the 24-h and 1-week water storage periods. In conclusion, bond strength of composite resin to porcelain resulting from silanization of porcelain increased during the experimental period. The bond strength also varied for different silanes used in this study.

Peat Soil Stabilization using Lime and Cement

NASA Astrophysics Data System (ADS)

Zambri, Nadhirah Mohd; Ghazaly, Zuhayr Md.

2018-03-01

This paper presents a study of the comparison between two additive Lime and Cement for treating peat soil in term of stabilization. Peat and organic soils are commonly known for their high compressibility, extremely soft, and low strength. The aim of this paper is to determine the drained shear strength of treated peat soil from Perlis for comparison purposes. Direct Shear Box Test was conducted to obtain the shear strength for all the disturbed peat soil samples. The quick lime and cement was mixed with peat soil in proportions of 10% and 20% of the dry weight peat soil. The experiment results showed that the addition of additives had improved the strength characteristics of peat soil by 14% increment in shear strength. In addition, the mixture of lime with peat soil yield higher result in shear strength compared to cement by 14.07% and 13.5% respectively. These findings indicate that the lime and cement is a good stabilizer for peat soil, which often experienced high amount of moisture content.

Microstructure and Mechanical Properties of Dissimilar Friction Stir Spot Welding Between St37 Steel and 304 Stainless Steel

NASA Astrophysics Data System (ADS)

Khodadadi, Ali; Shamanian, Morteza; Karimzadeh, Fathallah

2017-05-01

In the present study, St37 low-carbon steel and 304 stainless steel were welded successfully, with the thickness of 2 mm, by a friction stir spot welding process carried out at the tool dwell time of 6 s and two different tool rotational speeds of 630 and 1250 rpm. Metallographic examinations revealed four different zones including SZ and HAZ areas of St37 steel and SZ and TMAZ regions of 304 stainless steel in the weld nugget, except the base metals. X-ray diffraction and energy-dispersive x-ray spectroscopy experiments were used to investigate the possible formation of such phases as chromium carbide. Based on these experiments, no chromium carbide precipitation was found. The recrystallization of the weld nugget in the 304 steel and the phase transformations of the weld regions in the St37 steel enhanced the hardness of the weld joint. Hardness changes of joint were acceptable and approximately uniform, as compared to the resistance spot weld. In this research, it was also observed that the tensile/shear strength, as a crucial factor, was increased with the rise in the tool rotational speed. The bond length along the interface between metals, as an effective parameter to increase the tensile/shear strength, was also determined. At higher tool rotational speeds, the bond length was found to be improved, resulting in the tensile/shear strength of 6682 N. Finally, two fracture modes were specified through the fracture mode analysis of samples obtained from the tensile/shear test consisting of the shear fracture mode and the mixed shear/tensile fracture mode.

[Effects of surface treatment and adhesive application on shear bond strength between zirconia and enamel].

PubMed

Li, Yinghui; Wu, Buling; Sun, Fengyang

2013-03-01

To evaluate the effects of sandblasting and different orthodontic adhesives on shear bond strength between zirconia and enamel. Zirconia ceramic samples were designed and manufactured for 40 extracted human maxillary first premolars with CAD/CAM system. The samples were randomized into 4 groups for surface treatment with sandblasting and non-treated with adhesives of 3M Transbond XT or Jingjin dental enamel bonding resin. After 24 h of bonded fixation, the shear bond strengths were measured by universal mechanical testing machine and analyzed with factorial variance analysis. The shear bond strength was significantly higher in sandblasting group than in untreated group (P<0.05) and comparable between the two groups with the adhesives of Transbond XT and dental enamel bonding resin (P>0.05). The shear bond strength between zirconia and enamel is sufficient after sandblasting regardless of the application of either adhesive.

High-Temperature Mechanical Properties of the P/M Extruded Mg -SiCp Composites

NASA Astrophysics Data System (ADS)

Labib, F.; Mahmudi, R.; Ghasemi, H. M.

2018-03-01

In the present study, pure magnesium reinforced with 0, 5, 10 and 15 vol.% SiC particulates was successfully prepared by powder metallurgy technique before being hot extruded. The average 14 μm grain size of the composite specimens remained almost unchanged after addition of SiC particles, while their dimensional stability was improved because of the reduction in the coefficient of thermal expansion (CTE) from 28.6 × 10-6 K-1 in pure Mg to 27.3, 25.3 and 23.4 × 10-6 K-1 in the Mg-5% SiC, Mg-10% SiC and Mg-15% SiC composites, respectively. Mechanical properties of the specimens were investigated in the temperature range of 298-498 K, implementing shear punch testing and hot hardness techniques. Depending on the test temperature, addition of SiC particles to the pure Mg matrix increased shear yield stress and ultimate shear strength of the materials by 5-25 and 6-23 MPa, respectively. The shear strength improvement was mainly attributed to the CTE mismatch strengthening mechanism (9.5-25.5 MPa), and to a lesser extent (1-4.5 MPa), to the load transfer mechanism. Finally, using the modified Clyne model, the contribution of different strengthening mechanisms to the total shear strength improvement in the composites was evaluated.

Correlation of bond strength with surface roughness using a new roughness measurement technique.

PubMed

Winkler, M M; Moore, B K

1994-07-01

The correlation between shear bond strength and surface roughness was investigated using new surface measurement methods. Bonding agents and associated resin composites were applied to set amalgam after mechanically roughening its surface. Surface treatments were noe (as set against glass), 80 grit, and 600 grit abrasive paper. Surface roughness (R(a) as measured parallel and perpendicular (+) to the direction of the polishing scratches and true profile length were measured. A knife-edge was applied (rate = 2.54 mm/min) at the bonding agent/amalgam interface of each sample until failure. Coefficients of determination for mean bond strength vs either roughness (R(a), of profile length were significantly higher for measurements in parallel directions than for those measurements in (+) directions. The shear bond strength to set amalgam for a PENTA-containing adhesives system (L.D. Caulk Division) was not significantly different from that of a PENTA-free adhesive (3M Dental Products Division), even though PENTA has been reported to increase bond strength to nonprecious metals. The shear bond strength of resin composite to amalgam is correlated to surface roughness when it is measured parallel to the polishing scratches. This correlation is significantly lower when surface roughness is measured in the typical manner, perpendicular to the polishing scratches.

Mechanical properties of thermal protection system materials.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hardy, Robert Douglas; Bronowski, David R.; Lee, Moo Yul

2005-06-01

An experimental study was conducted to measure the mechanical properties of the Thermal Protection System (TPS) materials used for the Space Shuttle. Three types of TPS materials (LI-900, LI-2200, and FRCI-12) were tested in 'in-plane' and 'out-of-plane' orientations. Four types of quasi-static mechanical tests (uniaxial tension, uniaxial compression, uniaxial strain, and shear) were performed under low (10{sup -4} to 10{sup -3}/s) and intermediate (1 to 10/s) strain rate conditions. In addition, split Hopkinson pressure bar tests were conducted to obtain the strength of the materials under a relatively higher strain rate ({approx}10{sup 2} to 10{sup 3}/s) condition. In general, TPSmore » materials have higher strength and higher Young's modulus when tested in 'in-plane' than in 'through-the-thickness' orientation under compressive (unconfined and confined) and tensile stress conditions. In both stress conditions, the strength of the material increases as the strain rate increases. The rate of increase in LI-900 is relatively small compared to those for the other two TPS materials tested in this study. But, the Young's modulus appears to be insensitive to the different strain rates applied. The FRCI-12 material, designed to replace the heavier LI-2200, showed higher strengths under tensile and shear stress conditions. But, under a compressive stress condition, LI-2200 showed higher strength than FRCI-12. As far as the modulus is concerned, LI-2200 has higher Young's modulus both in compression and in tension. The shear modulus of FRCI-12 and LI-2200 fell in the same range.« less

[Evaluation of shear bond strengths of self-etching and total-etching dental adhesives to enamel and dentin].

PubMed

Yu, Ling; Liu, Jing-Ming; Wang, Xiao-Yan; Gao, Xue-Jun

2009-03-01

To evaluate the shear bond strengths of four dental adhesives in vitro. The facial surfaces of 20 human maxillary incisors were prepared to expose fresh enamel and randomly divided into four groups, in each group 5 teeth were bonded with one adhesives: group A (Clearfil Protect Bond, self-etching two steps), group B (Adper( Prompt, self-etching one step), group C (SwissTEC SL Bond, total-etching two steps), group D (Single Bond, total-etching two steps). Shear bond strengths were determined using an universal testing machine after being stored in distilled water for 24 h at 37 degrees C. The bond strengths to enamel and dentin were (25.33 +/- 2.84) and (26.07 +/- 5.56) MPa in group A, (17.08 +/- 5.13) and (17.93 +/- 4.70) MPa in group B, (33.14 +/- 6.05) and (41.92 +/- 6.25) MPa in group C, (22.51 +/- 6.25) and (21.45 +/- 7.34) MPa in group D. Group C showed the highest and group B the lowest shear bond strength to enamel and dentin among the four groups. The two-step self-etching adhesive showed comparable shear bond strength to some of the total-etching adhesives and higher shear bond strength than one-step self-etching adhesive.

Alternative Penetrometers to Measure the Near Surface Strength of Soft Seafloor Soils

DTIC Science & Technology

2010-01-01

data. The three probe types were a cone penetrometer (CPT), ball penetrometer (BPT), and a shear vane ( VST ). The CPT and BPT measure electronically a...continuous profile of tip and sleeve resistance as well as the porewater pressure during advancement. The VST records the undrained shear strength...results and are compared with the VST shear strengths as shown on Figure 5 (Specimen 1) and Figure 6 (Specimen 2). The VST strengths compare

Fan-structure waves in shear ruptures

NASA Astrophysics Data System (ADS)

Tarasov, Boris

2016-04-01

This presentation introduces a recently identified shear rupture mechanism providing a paradoxical feature of hard rocks - the possibility of shear rupture propagation through the highly confined intact rock mass at shear stress levels significantly less than frictional strength. According to the fan-mechanism the shear rupture propagation is associated with consecutive creation of small slabs in the fracture tip which, due to rotation caused by shear displacement of the fracture interfaces, form a fan-structure representing the fracture head. The fan-head combines such unique features as: extremely low shear resistance (below the frictional strength), self-sustaining stress intensification in the rupture tip (providing easy formation of new slabs), and self-unbalancing conditions in the fan-head (making the failure process inevitably spontaneous and violent). An important feature of the fan-mechanism is the fact that for the initial formation of the fan-structure an enhanced local shear stress is required, however, after completion of the fan-structure it can propagate as a dynamic wave through intact rock mass at shear stresses below the frictional strength. Paradoxically low shear strength of pristine rocks provided by the fan-mechanism determines the correspondingly low transient strength of the lithosphere, which favours generation of new earthquake faults in the intact rock mass adjoining pre-existing faults in preference to frictional stick-slip instability along these faults. The new approach reveals an alternative role of pre-existing faults in earthquake activity: they represent local stress concentrates in pristine rock adjoining the fault where special conditions for the fan-mechanism nucleation are created, while further dynamic propagation of the new fault (earthquake) occurs at low field stresses even below the frictional strength.

Composite bonding to stainless steel crowns using a new universal bonding and single-bottle systems.

PubMed

Hattan, Mohammad Ali; Pani, Sharat Chandra; Alomari, Mohammad

2013-01-01

Aim. The aim of this study is to evaluate the shear bond strength of nanocomposite to stainless steel crowns using a new universal bonding system. Material and Methods. Eighty (80) stainless steel crowns (SSCs) were divided into four groups (20 each). Packable nanocomposite was bonded to the lingual surface of the crowns in the following methods: Group A without adhesive (control group), Group B using a new universal adhesive system (Scotchbond Universal Adhesive, 3M ESPE, Seefeld, Germany), and Group C and Group D using two different brands of single-bottle adhesive systems. Shear bond strengths were calculated and the types of failure also were recorded. Results. The shear strength of Group B was significantly greater than that of other groups. No significant differences were found between the shear bond strengths of Groups C and D. The control group had significantly lower shear bond strength (P < 0.05) to composite than the groups that utilized bonding agents. Conclusion. Composites bonding to stainless steel crowns using the new universal bonding agent (Scotchbond Universal Adhesive, 3M ESPE, Seefeld, Germany) show significantly greater shear bond strengths and fewer adhesive failures when compared to traditional single-bottle systems.

Effect of Quaternary Ammonium Salt on Shear Bond Strength of Orthodontic Brackets to Enamel

PubMed Central

Ghadirian, Hannaneh; Geramy, Allahyar; Najafi, Farhood; Heidari, Soolmaz

2017-01-01

Objectives: This study sought to assess the effect of quaternary ammonium salt (QAS) on shear bond strength of orthodontic brackets to enamel. Materials and Methods: In this in vitro experimental study, 0, 10, 20 and 30% concentrations of QAS were added to Transbond XT primer. Brackets were bonded to 60 premolar teeth using the afore-mentioned adhesive mixtures, and the shear bond strength of the four groups (n=15) was measured using a universal testing machine. After debonding, the adhesive remnant index (ARI) score was determined under a stereomicroscope. Data were analyzed using one-way ANOVA. Results: The mean and standard deviation of shear bond strength of the control and 10%, 20% and 30% groups were 23.54±6.31, 21.81±2.82, 20.83±8.35 and 22.91±5.66 MPa, respectively. No significant difference was noted in shear bond strength of the groups (P=0.83). Study groups were not different in terms of ARI scores (P=0.80). Conclusions: The results showed that addition of QAS to Transbond XT primer had no adverse effect on shear bond strength of orthodontic brackets. PMID:29167688

Erosion Characteristics and Horizontal Variability for Small Erosion Depths in the Sacramento - San Joaquin River Delta, California, USA

NASA Astrophysics Data System (ADS)

Schoellhamer, D. H.; Manning, A. J.; Work, P. A.

2015-12-01

Cohesive sediment in the Sacramento-San Joaquin River Delta affects pelagic fish habitat, contaminant transport, and marsh accretion. Observations of suspended-sediment concentration in the delta indicate that about 0.05 to 0.20 kg/m2 are eroded from the bed during a tidal cycle. If erosion is horizontally uniform, the erosion depth is about 30 to 150 microns, the typical range in diameter of suspended flocs. Application of an erosion microcosm produces similarly small erosion depths. In addition, core erodibility in the microcosm calculated with a horizontally homogeneous model increases with depth, contrary to expectations for a consolidating bed, possibly because the eroding surface area increases as applied shear stress increases. Thus, field observations and microcosm experiments, combined with visual observation of horizontally varying biota and texture at the surface of sediment cores, indicate that a conceptual model of erosion that includes horizontally varying properties may be more appropriate than assuming horizontally homogeneous erosive properties. To test this hypothesis, we collected five cores and measured the horizontal variability of shear strength within each core in the top 5.08 cm with a shear vane. Small tubes built by a freshwater worm and macroalgae were observed on the surface of all cores. The shear vane was inserted into the sediment until the top of the vane was at the top of the sediment, torque was applied to the vane until the sediment failed and the vane rotated, and the corresponding dial reading in Nm was recorded. The dial reading was assumed to be proportional to the surface strength. The horizontal standard deviation of the critical shear stress was about 30% of the mean. Results of the shear vane test provide empirical evidence that surface strength of the bed varies horizontally. A numerical simulation of erosion with an areally heterogeneous bed reproduced erosion characteristics observed in the microcosm.

Temperature-dependent tensile and shear response of graphite/aluminum

NASA Technical Reports Server (NTRS)

Fujita, T.; Pindera, M. J.; Herakovich, C. T.

1987-01-01

The thermo-mechanical response of unidirectional P100 graphite fiber/6061 aluminum matrix composites was investigated at four temperatures:-150, +75, +250, and +500 F. Two types of tests, off-axis tension and losipescu shear, were used to obtain the desired properties. Good experimental-theoretical correlation was obtained for Exx, vxy, and G12. It is shown that E11 is temperature independent, but E22, v12, and G12 generally decrease with increasing temperature. Compared with rather high longitudinal strength, very low transverse strength was obtained for the graphite/aluminum. The poor transverse strength is believed to be due to the low interfacial bond strength in this material. The strength decrease significantly with increasing temperature. The tensile response at various temperatures is greatly affected by the residual stresses caused by the mismatch in the coefficients of thermal expansion of fibers and matrix. The degradation of the aluminum matrix properties at higher temperatures has a deleterious effect on composite properties. The composite has a very low coefficient of thermal expansion in the fiber direction.

Shear capacity of high-strength concrete pre-stressed girders.

DOT National Transportation Integrated Search

1998-05-01

As part of a project at the University of Minnesota to investigate the application of high-strength concrete in prestressed girders, four shear tests were performed on high-strength concrete prestressed girders.

Prediction of shear critical behavior of high-strength reinforced concrete columns using finite element methods

NASA Astrophysics Data System (ADS)

Alrasyid, Harun; Safi, Fahrudin; Iranata, Data; Chen-Ou, Yu

2017-11-01

This research shows the prediction of shear behavior of High-Strength Reinforced Concrete Columns using Finite-Element Method. The experimental data of nine half scale high-strength reinforced concrete were selected. These columns using specified concrete compressive strength of 70 MPa, specified yield strength of longitudinal and transverse reinforcement of 685 and 785 MPa, respectively. The VecTor2 finite element software was used to simulate the shear critical behavior of these columns. The combination axial compression load and monotonic loading were applied at this prediction. It is demonstrated that VecTor2 finite element software provides accurate prediction of load-deflection up to peak at applied load, but provide similar behavior at post peak load. The shear strength prediction provide by VecTor 2 are slightly conservative compare to test result.

Effect of denture cleansing agents on tensile and shear bond strengths of soft liners to acrylic denture base.

PubMed

Mahboub, Farhang; Salehsaber, Fariba; Parnia, Fereydoon; Gharekhani, Vahedeh; Kananizadeh, Yousef; Taghizadeh, Mahsa

2017-01-01

Background. The aim of the present study was to evaluate the effect of Corega and 2.5% sodium hypochlorite cleansing agents on the shear and tensile bond strengths of GC soft liner to denture base. Methods. A total of 144 samples (72 samples for tensile and 72 for shear bond strength evaluations) were prepared. The samples in each group were subdivided into three subgroups in terms of the cleansing agent used (2.5% sodium hypochlorite, Corega and distilled water [control group]). All the samples were stored in distilled water, during which each sample was immersed for 15 minutes daily in sodium hypochlorite or Corega solutions. After 20 days the tensile and shear bond strengths were determined using a universal testing machine. In addition, a stereomicroscope was used to evaluate fracture modes. Data were analyzed with one-way ANOVA, using SPSS 16. Results. The results of post hoc Tukey tests showed significant differences in the mean tensile and shear bond strength values between the sodium hypochlorite group with Corega and control groups (P=0.001 for comparison of tensile bond strengths between the sodium hypochlorite and control groups, and P<0.001 for the comparison of tensile bond strengths between the sodium hypochlorite and Corega groups and the shear bond strengths between the sodium hypochlorite and Corega groups, and sodium hypochlorite and control groups).The majority of failures were cohesive in the control and Corega groups and cohesive/adhesive in the sodium hypochlorite group. Conclusion. Immersion of soft liners in Corega will result in longevity of soft liners compared to immersion in sodium hypochlorite solution and sodium hypochlorite solution significantly decreased the tensile and shear bond strengths compared to the control and Corega groups.

Effect of denture cleansing agents on tensile and shear bond strengths of soft liners to acrylic denture base

PubMed Central

Mahboub, Farhang; Salehsaber, Fariba; Parnia, Fereydoon; Gharekhani, Vahedeh; Kananizadeh, Yousef; Taghizadeh, Mahsa

2017-01-01

Background. The aim of the present study was to evaluate the effect of Corega and 2.5% sodium hypochlorite cleansing agents on the shear and tensile bond strengths of GC soft liner to denture base. Methods. A total of 144 samples (72 samples for tensile and 72 for shear bond strength evaluations) were prepared. The samples in each group were subdivided into three subgroups in terms of the cleansing agent used (2.5% sodium hypochlorite, Corega and distilled water [control group]). All the samples were stored in distilled water, during which each sample was immersed for 15 minutes daily in sodium hypochlorite or Corega solutions. After 20 days the tensile and shear bond strengths were determined using a universal testing machine. In addition, a stereomicroscope was used to evaluate fracture modes. Data were analyzed with one-way ANOVA, using SPSS 16. Results. The results of post hoc Tukey tests showed significant differences in the mean tensile and shear bond strength values between the sodium hypochlorite group with Corega and control groups (P=0.001 for comparison of tensile bond strengths between the sodium hypochlorite and control groups, and P<0.001 for the comparison of tensile bond strengths between the sodium hypochlorite and Corega groups and the shear bond strengths between the sodium hypochlorite and Corega groups, and sodium hypochlorite and control groups).The majority of failures were cohesive in the control and Corega groups and cohesive/adhesive in the sodium hypochlorite group. Conclusion. Immersion of soft liners in Corega will result in longevity of soft liners compared to immersion in sodium hypochlorite solution and sodium hypochlorite solution significantly decreased the tensile and shear bond strengths compared to the control and Corega groups. PMID:29184635

Shear bond strengths of self-etching adhesives to caries-affected dentin on the gingival wall.

PubMed

Koyuturk, Alp Erdin; Sengun, Abdulkadir; Ozer, Fusun; Sener, Yagmur; Gokalp, Alparslan

2006-03-01

The purpose of this study was to evaluate the bonding ability of five current self-etching adhesives to caries-affected dentin on the gingival wall. Seventy extracted human molars with approximal dentin caries were employed in this study. In order to obtain caries-affected dentin on the gingival wall, grinding was performed under running water. Following which, specimens mounted in acrylic blocks and composite resins of the bonding systems were bonded to dentin with plastic rings and then debonded by shear bond strength. With Clearfil SE Bond, bonding to caries-affected dentin showed the highest bond strength. With Optibond Solo Plus Self-Etch, bonding to caries-affected dentin showed higher shear bond strength than AQ Bond, Tyrian SPE & One-Step Plus, and Prompt-L-Pop (p<0.05). Further, the bond strengths of Clearfil SE Bond and Optibond Solo Plus Self-Etch to sound dentin were higher than those of Prompt-L-Pop, AQ Bond, and Tyrian SPE & One-Step Plus (p<0.05). In conclusion, besides micromechanical interlocking through hybrid layer formation, bond strength of self-etch adhesives to dentin may be increased from additional chemical interaction between the functional monomer and residual hydroxyapatite. The results of this study confirmed that differences in bond strength among self-etching adhesives to both caries-affected and sound dentin were due to chemical composition rather than acidity.

Shear Strength of Remoulding Clay Samples Using Different Methods of Moulding

NASA Astrophysics Data System (ADS)

Norhaliza, W.; Ismail, B.; Azhar, A. T. S.; Nurul, N. J.

2016-07-01

Shear strength for clay soil was required to determine the soil stability. Clay was known as a soil with complex natural formations and very difficult to obtain undisturbed samples at the site. The aim of this paper was to determine the unconfined shear strength of remoulded clay on different methods in moulding samples which were proctor compaction, hand operated soil compacter and miniature mould methods. All the samples were remoulded with the same optimum moisture content (OMC) and density that were 18% and 1880 kg/m3 respectively. The unconfined shear strength results of remoulding clay soils for proctor compaction method was 289.56kPa with the strain 4.8%, hand operated method was 261.66kPa with the strain 4.4% and miniature mould method was 247.52kPa with the strain 3.9%. Based on the proctor compaction method, the reduction percentage of unconfined shear strength of remoulded clay soil of hand operated method was 9.66%, and for miniature mould method was 14.52%. Thus, because there was no significant difference of reduction percentage of unconfined shear strength between three different methods, so it can be concluded that remoulding clay by hand operated method and miniature mould method were accepted and suggested to perform remoulding clay samples by other future researcher. However for comparison, the hand operated method was more suitable to form remoulded clay sample in term of easiness, saving time and less energy for unconfined shear strength determination purposes.

Shear bond strength of computer-aided design and computer-aided manufacturing feldspathic and nano resin ceramics blocks cemented with three different generations of resin cement.

PubMed

Ab-Ghani, Zuryati; Jaafar, Wahyuni; Foo, Siew Fon; Ariffin, Zaihan; Mohamad, Dasmawati

2015-01-01

To evaluate the shear bond strength between the dentin substrate and computer-aided design and computer-aided manufacturing feldspathic ceramic and nano resin ceramics blocks cemented with resin cement. Sixty cuboidal blocks (5 mm × 5 mm × 5 mm) were fabricated in equal numbers from feldspathic ceramic CEREC(®) Blocs PC and nano resin ceramic Lava™ Ultimate, and randomly divided into six groups (n = 10). Each block was cemented to the dentin of 60 extracted human premolar using Variolink(®) II/Syntac Classic (multi-steps etch-and-rinse adhesive bonding), NX3 Nexus(®) (two-steps etch-and-rinse adhesive bonding) and RelyX™ U200 self-adhesive cement. All specimens were thermocycled, and shear bond strength testing was done using the universal testing machine at a crosshead speed of 1.0 mm/min. Data were analyzed using one-way ANOVA. Combination of CEREC(®) Blocs PC and Variolink(®) II showed the highest mean shear bond strength (8.71 Mpa), while the lowest of 2.06 Mpa were observed in Lava™ Ultimate and RelyX™ U200. There was no significant difference in the mean shear bond strength between different blocks. Variolink(®) II cement using multi-steps etch-and-rinse adhesive bonding provided a higher shear bond strength than the self-adhesive cement RelyX U200. The shear bond strength was not affected by the type of blocks used.

Scaling of strength and ductility in bioinspired brick and mortar composites

NASA Astrophysics Data System (ADS)

Wilbrink, David V.; Utz, Marcel; Ritchie, Robert O.; Begley, Matthew R.

2010-11-01

This paper provides scaling relationships between constituent properties and the uniaxial tensile response of synthetic "brick and mortar" composite materials inspired by nacre. The macroscopic strength and ductility (work of fracture) are predicted in terms of the brick properties (size, strength, and layout) and interface cohesive properties (e.g., maximum shear and normal stresses and separations). The results illustrate the trade-off between increasing strength and decreasing ductility with the increasing aspect ratio of the bricks. The models can be used to identify optimum mortar properties that maximize toughness for a given brick strength.

Effect of zirconia surface treatment using nitric acid-hydrofluoric acid on the shear bond strengths of resin cements

PubMed Central

Kim, Sun Jai; Shim, June Sung

2017-01-01

PURPOSE The aim of this study was to compare the surface roughness of zirconia when using Zircos E etching system (ZSAT), applying a nitric acid-hydrofluoric acid compound as a pretreatment agent, and also to compare the shear bonding strength according to different resin cements. MATERIALS AND METHODS ZSAT, air abrasion, and tribochemical silicacoating were applied on prepared 120 zirconia specimens (10 mm in diameter, 7 mm in height) using CAD/CAM. Each 12 specimens with 4 different resin cements (Panavia F 2.0, Rely X Unicem, Superbond C&B, and Hot bond) were applied to test interfacial bond strength. The statistical analysis was performed using SAS 9.1 (SAS Institute Inc., Cary, NC, USA). The results are as follows: after application of the ZSAT on the zirconia specimens, surface roughness value after 2-hour etching was higher than those after 1- and 3-hour etching on SEM images. RESULTS For Superbond C&B and Rely X Unicem, the specimens treated with ZSAT showed higher shear bond strength values than those treated with air abrasion and tribochemical silicacoating system. Regarding the failure mode of interface over cement and zirconia surface, Rely X Unicem and Hot bond showed cohesive failures and Panavia F 2.0 and Superbond C&B showed mixed failures. CONCLUSION Zircos E etching system in zirconia restoration could increase its shear bond strength. However, its long term success rate and clinical application should be further evaluated. PMID:28435615

Failure Waves in Glass and Ceramics under Shock Compression

NASA Astrophysics Data System (ADS)

Singh Brar, N.

1999-06-01

The response of various types of glasses (fused silica, borosilicates, soda-lime, and lead filled) to shock wave loading, especially the failure of glass behind the shock wave through the ``so called" failure wave or front has been the subject of intense research among a number of investigators. The variations in material properties across this front include complete loss of tensile (spall) strength, loss in shear strength, reduction in acoustic impedance, and opacity to light. Both the Stress and velocity history from VISAR measurements have shown that the failure front propagates at a speed of 1.5 to 2.5 mm/s, depending on the peak shock stress level. The shear strength [τ = 1/2(σ_x-σ_y)] behind the failure front, determined using embedded transverse gauges, is found to decrease to about 2 GPa for soda-lime, borosilicate, and filled glasses. The optical (high-speed photography) observations also confirm the formation of failure front. There is a general agreement among various researchers on these observations. However, three proposed mechanisms for the formation of failure front are based on totally different formulations. The first, due to Clifton is based on the process of nucleation of local densification due to shock compression followed by shear failure around inhomogeneities resulting in phase boundary between the comminuted from the intact material. The second, proposed by Grady involves the transfer of elastic shear strain energy to dilatant strain energy as a result of severe microcracking originating from impact face. The third, by Espinosa and Brar proposes that the front is created through shear microcracks, which nucleate and propagate from the impact face, as originally suggested by Kanel. This mechanism is incorporated in multiple-plane model and simulations predict the increase in lateral stress and an observed reduction in spall strength behind the failure front. Failure front studies, in terms of loss of shear strength, have been recently extended to alumina and SiC ceramics by Bourne et. al.

Influence of irradiation by a novel CO2 9.3-μm short-pulsed laser on sealant bond strength.

PubMed

Rechmann, P; Sherathiya, K; Kinsel, R; Vaderhobli, R; Rechmann, B M T

2017-04-01

The objective of this in vitro study was to evaluate whether irradiation of enamel with a novel CO 2 9.3-μm short-pulsed laser using energies that enhance caries resistance influences the shear bond strength of composite resin sealants to the irradiated enamel. Seventy bovine and 240 human enamel samples were irradiated with a 9.3-μm carbon dioxide laser (Solea, Convergent Dental, Inc., Natick, MA) with four different laser energies known to enhance caries resistance or ablate enamel (pulse duration from 3 μs at 1.6 mJ/pulse to 43 μs at 14.9 mJ/pulse with fluences between 3.3 and 30.4 J/cm 2 , pulse repetition rate between 4.1 and 41.3 Hz, beam diameter of 0.25 mm and 1-mm spiral pattern, and focus distance of 4-15 mm). Irradiation was performed "freehand" or using a computerized, motor-driven stage. Enamel etching was achieved with 37% phosphoric acid (Scotchbond Universal etchant, 3M ESPE, St. Paul, MN). As bonding agent, Adper Single Bond Plus was used followed by placing Z250 Filtek Supreme flowable composite resin (both 3M ESPE). After 24 h water storage, a single-plane shear bond test was performed (UltraTester, Ultradent Products, Inc., South Jordan, UT). All laser-irradiated samples showed equal or higher bond strength than non-laser-treated controls. The highest shear bond strength values were observed with the 3-μs pulse duration/0.25-mm laser pattern (mean ± SD = 31.90 ± 2.50 MPa), representing a significant 27.4% bond strength increase over the controls (25.04 ± 2.80 MPa, P ≤ 0.0001). Two other caries-preventive irradiation (3 μs/1 mm and 7 μs/0.25 mm) and one ablative pattern (23 μs/0.25 mm) achieved significantly increased bond strength compared to the controls. Bovine enamel also showed in all test groups increased shear bond strength over the controls. Computerized motor-driven stage irradiation did not show superior bond strength values over the clinically more relevant freehand irradiation. Enamel that is made caries-resistant with CO 2 9.3-μm short-pulsed laser irradiation showed at least equal or significantly higher shear bond strength to pit and fissure sealants than non-laser-irradiated enamel. The risk of a sealant failure due to CO 2 9.3-μm short-pulsed laser irradiation appears reduced. If additional laser ablation is required before placing a sealant, the CO 2 9.3-μm enamel laser-cut showed equivalent or superior bond strength to a flowable sealant.

Development and Evaluation of Stitched Sandwich Panels

NASA Technical Reports Server (NTRS)

Stanley, Larry E.; Adams, Daniel O.; Reeder, James R. (Technical Monitor)

2001-01-01

This study explored the feasibility and potential benefits provided by the addition of through-the-thickness reinforcement to sandwich structures. Through-the-thickness stitching is proposed to increase the interlaminar strength and damage tolerance of composite sandwich structures. A low-cost, out-of-autoclave processing method was developed to produce composite sandwich panels with carbon fiber face sheets, a closed-cell foam core, and through-the-thickness Kevlar stitching. The sandwich panels were stitched in a dry preform state, vacuum bagged, and infiltrated using Vacuum Assisted Resin Transfer Molding (VARTM) processing. For comparison purposes, unstitched sandwich panels were produced using the same materials and manufacturing methodology. Test panels were produced initially at the University of Utah and later at NASA Langley Research Center. Four types of mechanical tests were performed: flexural testing, flatwise tensile testing, core shear testing, and edgewise compression testing. Drop-weight impact testing followed by specimen sectioning was performed to characterize the damage resistance of stitched sandwich panels. Compression after impact (CAI) testing was performed to evaluate the damage tolerance of the sandwich panels. Results show significant increases in the flexural stiffness and strength, out-of-plane tensile strength, core shear strength, edgewise compression strength, and compression-after-impact strength of stitched sandwich structures.

Effects of dentin surface treatments on shear bond strength of glass-ionomer cements

PubMed Central

Poggio, Claudio; Beltrami, Riccardo; Scribante, Andrea; Colombo, Marco; Lombardini, Marco

2014-01-01

Summary Aim The aim of this in vitro study was to evaluate the effect of different surface treatments on shear bond strength of a conventional glass-ionomer cement (GIC) and a resin-modified glass-ionomer cement (RMGIC) to dentin. Materials and methods 80 bovine permanent incisors were used. 40 cylindrical specimens of a GIC (Fuji IX GP Extra) and 40 cylindrical specimens of a RMGIC (Fuji II LC) were attached to the dentin. The teeth were then randomly assigned to 8 groups of equal size (n=10), 4 for every type of glass-ionomer cement, corresponding to type of dentin surface treatments. Group 1: GC Cavity Conditioner; Group 2: 37% phosphoric acid gel; Group 3: Clearfil SE Bond; Group 4: no dentin conditioning (control). The specimens were placed in a universal testing machine (Model 3343, Instron Corp., Canton, Mass., USA) and subsequently tested for shear bond strength (MPa). Results ANOVA showed the presence of significant differences among the various groups. Post hoc Tukey test showed different values of shear bond strength for Fuji IX GP Extra and for Fuji II LC. The different conditioners variably influence the adhesion of the glass-ionomer cements tested. Conclusions. RMGIC shear bond to dentin was higher than GIC. The use of a Self-etch adhesive system improved the shear bond strength values of RMGIC and lowered the shear bond strength values of GIC significantly. PMID:24753797

Improved mechanical performance of PBO fiber-reinforced bismaleimide composite using mixed O2/Ar plasma

NASA Astrophysics Data System (ADS)

Liu, Dong; Chen, Ping; Yu, Qi; Ma, Keming; Ding, Zhenfeng

2014-06-01

The mixed O2/Ar plasma was employed to enhance mechanical properties of the PBO/bismaleimide composite. The interlaminar shear strength was improved to 61.6 MPa or by 38.1%, but the composite brittleness increased. The plasma gas compositions exhibited notable effects on the interfacial adhesion strength. XPS results suggested that the mixed plasma presented higher activation effects on the surface chemical compositions than pure gas plasmas and a larger number of oxygen atoms and hydrophilic groups were introduced on the fiber surface due to the synergy effect, but the synergy effect was considerably performed only within the O2 percentage range of 40-60%. The fibers surface was increasingly etched with growing the O2 contents in the plasma, deteriorating the fibers tensile strength. SEM micrographs demonstrated that the composite shear fracture changed from debonding to cohesive failure in the matrices, and the improving mechanisms were discussed.

The effect of adhesive strength of hydroxyapatite coating on the stability of hydroxyapatite-coated prostheses in vivo at the early stage of implantation

PubMed Central

Duan, Yonghong; Zhu, Shu; Guo, Fei; Zhu, Jinyu; Li, Mao; Ma, Jie

2012-01-01

Introduction With the increase in joint revision surgery after arthroplasty, defects of hydroxyapatite (HA)-coated prostheses have been observed increasingly often. These defects adversely affect the prosthetic stability in vivo. This study has analyzed the potential effect of the adhesive strength of HA coating on the stability of HA-coated prostheses in vivo after its implantation. Material and methods Sixty experimental rabbits were divided into HA- and Ti-coated groups. HA-coated prostheses were implanted into the bilateral epicondyle of rabbits femurs. Ti-coated prostheses were implanted as control. At different time points(4, 9, and 15 weeks) after implantation, bone tissue samples were fetched out respectively for histomorphometric analysis. Push-out testing was used to detect the ultimate shear strength at the bone-prosthesis interface. Scanning electron microscope (SEM) observation and energy-dispersive X-ray spectroscopy (EDX) analysis were used to observe the changes in surface composition of the prostheses after the ultimate shear strength testing. The coating adhesive strength of two kinds of coatings were also examined by scratch testing. Results Hydroxyapatite coating has an obvious advantage in facilitating osteogenesis and its plays a critical role in the stability of prostheses. However, the ultimate shear strength of HA-coated prostheses is much lower than that of Ti-coated implants (p < 0.01). Further study has demonstrated that the stability of HA-coated prostheses in vivo is affected by the relatively low adhesive strength between coating and substrate. Conclusions Obvious advantage in facilitating osteogenesis around HA-coated prostheses is not the only factor that determines the stability of prostheses in vivo. PMID:22661990

A New Stochastic Approach to Predict Peak and Residual Shear Strength of Natural Rock Discontinuities

NASA Astrophysics Data System (ADS)

Casagrande, D.; Buzzi, O.; Giacomini, A.; Lambert, C.; Fenton, G.

2018-01-01

Natural discontinuities are known to play a key role in the stability of rock masses. However, it is a non-trivial task to estimate the shear strength of large discontinuities. Because of the inherent complexity to access to the full surface of the large in situ discontinuities, researchers or engineers tend to work on small-scale specimens. As a consequence, the results are often plagued by the well-known scale effect. A new approach is here proposed to predict shear strength of discontinuities. This approach has the potential to avoid the scale effect. The rationale of the approach is as follows: a major parameter that governs the shear strength of a discontinuity within a rock mass is roughness, which can be accounted for by surveying the discontinuity surface. However, this is typically not possible for discontinuities contained within the rock mass where only traces are visible. For natural surfaces, it can be assumed that traces are, to some extent, representative of the surface. It is here proposed to use the available 2D information (from a visible trace, referred to as a seed trace) and a random field model to create a large number of synthetic surfaces (3D data sets). The shear strength of each synthetic surface can then be estimated using a semi-analytical model. By using a large number of synthetic surfaces and a Monte Carlo strategy, a meaningful shear strength distribution can be obtained. This paper presents the validation of the semi-analytical mechanistic model required to support the new approach for prediction of discontinuity shear strength. The model can predict both peak and residual shear strength. The second part of the paper lays the foundation of a random field model to support the creation of synthetic surfaces having statistical properties in line with those of the data of the seed trace. The paper concludes that it is possible to obtain a reasonable estimate of peak and residual shear strength of the discontinuities tested from the information from a single trace, without having access to the whole surface.

Comparative Study of the Shear Bond Strength of Flowable Composite in Permanent Teeth Treated with Conventional Bur and Contact or Non-Contact Er:YAG Laser

PubMed Central

Parhami, Parisa; Pourhashemi, Seyed Jalal; Ghandehari, Mehdi; Mighani, Ghasem; Chiniforush, Nasim

2014-01-01

Introduction: The aim of this study was to evaluate and compare the in vitro effect of the Erbium-Doped Yttrium Aluminum Garnet (Er:YAG) laser with different radiation distances and high-speed rotary treatment on the shear bond strength of flowable composite to enamel of human permanent posterior teeth. Methods: freshly extracted human molar teeth with no caries or other surface defects were used in this study (n=45). The teeth were randomly divided into 3 groups. Group 1: treated with non-contact Er:YAG Laser and etched with Er:YAG laser, Group 2: treated with contact Er:YAG Laser and etched with Er:YAG laser, Group 3 (control): treated with diamond fissure bur and etched with acid phosphoric 37%. Then the adhesive was applied on the surafces of the teeth and polymerized using a curing light appliance. Resin cylinders were fabricated from flowable composite. Shear bond strength was tested at a crosshead speed of 0.5 mm/min. Results: The amount of Shear Bond Strength (SBS) in the 3 treatment groups was not the same (P<0.05).The group in which enamel surfaces were treated with diamond fissure bur and etched with acid (conrtol group) had the highest mean shear bond strength (19.92±4.76) and the group in which the enamel surfaces were treated with contact Er:YAG laser and etched with Er:YAG laser had the lowest mean shear bond strength (10.89±2.89). Mann-whitney test with adjusted P-value detected significant difference in shear bond strength between the control group and the other 2 groups (P < 0.05). Conclusion: It was concluded that both contact and non-contact Er:YAG laser treatment reduced shear bond strength of flowable resin composite to enamel in comparison with conventional treatment with high speed rotary. Different Er:YAG laser distance irradiations did not influence the shear bond strength of flowable composite to enamel. PMID:25653813

Flow Strength of Shocked Aluminum in the Solid-Liquid Mixed Phase Region

NASA Astrophysics Data System (ADS)

Reinhart, William

2011-06-01

Shock waves have been used to determine material properties under high shock stresses and very-high loading rates. The determination of mechanical properties such as compressive strength under shock compression has proven to be difficult and estimates of strength have been limited to approximately 100 GPa or less in aluminum. The term ``strength'' has been used in different ways. For a Von-Mises solid, the yield strength is equal to twice the shear strength of the material and represents the maximum shear stress that can be supported before yield. Many of these concepts have been applied to materials that undergo high strain-rate dynamic deformation, as in uni-axial strain shock experiments. In shock experiments, it has been observed that the shear stress in the shocked state is not equal to the shear strength, as evidenced by elastic recompressions in reshock experiments. This has led to an assumption that there is a yield surface with maximum (loading)and minimum (unloading), shear strength yet the actual shear stress lies somewhere between these values. This work provides the first simultaneous measurements of unloading velocity and flow strength for transition of solid aluminum to the liquid phase. The investigation describes the flow strength observed in 1100 (pure), 6061-T6, and 2024 aluminum in the solid-liquid mixed phase region. Reloading and unloading techniques were utilized to provide independent data on the two unknowns (τc and τo) , so that the actual critical shear strength and the shear stress at the shock state could be estimated. Three different observations indicate a change in material response for stresses of 100 to 160 GPa; 1) release wave speed (reloading where applicable) measurements, 2) yield strength measurements, and 3) estimates of Poisson's ratio, all of which provide information on the melt process including internal consistency and/or non-equilibrium and rate-dependent melt behavior. The study investigates the strength properties in the solid region and as the material transverses the solid-mixed-liquid regime. Differences observed appear to be the product of alloying and/or microstructural composition of the aluminum. Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the United States Department of Energy's National Nuclear Security Administration under Contract DE-AC04-94AL85000.

Strengthening Effect of Incremental Shear Deformation on Ti Alloy Clad Plate with a Ni-Based Alloy Laser-Clad Layer

NASA Astrophysics Data System (ADS)

Zhao, W.; Zha, G. C.; Kong, F. X.; Wu, M. L.; Feng, X.; Gao, S. Y.

2017-05-01

A Ti-6Al-4V alloy clad plate with a Tribaloy 700 alloy laser-clad layer is subjected to incremental shear deformation, and we evaluate the structural evolution and mechanical properties of the specimens. Results indicate the significance of the incremental shear deformation on the strengthening effect. The wear resistance and Vickers hardness of the laser-clad layer are enhanced due to increased dislocation density. The incremental shear deformation can increase the bonding strength of the laser-clad layer and the corresponding substrate and can break the columnar crystals in the laser-clad layer near the interface. These phenomena suggest that shear deformation eliminates the defects on the interface of the laser-clad layer and the substrate. Substrate hardness is evidently improved, and the strengthening effect is caused by the increased dislocation density and shear deformation. This deformation can then transform the α- and β-phases in the substrate into a high-intensity ω-phase.

Surface hydrogenation regulated wrinkling and torque capability of hydrogenated graphene annulus under circular shearing.

PubMed

Li, Yinfeng; Liu, Silin; Datta, Dibakar; Li, Zhonghua

2015-11-12

Wrinkles as intrinsic topological feature have been expected to affect the electrical and mechanical properties of atomically thin graphene. Molecular dynamics simulations are adopted to investigate the wrinkling characteristics in hydrogenated graphene annulus under circular shearing at the inner edge. The amplitude of wrinkles induced by in-plane rotation around the inner edge is sensitive to hydrogenation, and increases quadratically with hydrogen coverage. The effect of hydrogenation on mechanical properties is investigated by calculating the torque capability of annular graphene with varying hydrogen coverage and inner radius. Hydrogenation-enhanced wrinkles cause the aggregation of carbon atoms towards the inner edge and contribute to the critical torque strength of annulus. Based on detailed stress distribution contours, a shear-to-tension conversion mechanism is proposed for the contribution of wrinkles on torque capacity. As a result, the graphane annulus anomalously has similar torque capacity to pristine graphene annulus. The competition between hydrogenation caused bond strength deterioration and wrinkling induced local stress state conversion leads to a U-shaped evolution of torque strength relative to the increase of hydrogen coverage from 0 to 100%. Such hydrogenation tailored topological and mechanical characteristics provides an innovative mean to develop novel graphene-based devices.

Effect of silica-palm shell carbon composite additive in enhancing the strength of the concrete in the oil-well cementing job

NASA Astrophysics Data System (ADS)

Novriansyah, A.; Mursyidah, U.; Novrianti; Putri, S. S.; Riswati, S. S.

2018-04-01

This study provides an analysis of composite additive effect to concrete’s strength in the oil-well cementing job. The composite additive is originated from the nano-sized form of silica and charcoal from palm shell waste. The quality of the concrete will be determined from its porosity, compressive strength, and shear bond strength parameters. Those parameters must be reliable base on the most respectable standards in oil and gas industry, in this study we use the standard from American Petroleum Institute (API). Six concrete samples with different concentration will be tested to obtain these parameters. The result from the test shown a decrement trend of the porosity while the concentration is increased. In contrast, the highest values of compressive strength and shear bond strength are obtained from the sample with higher additive concentration. The optimum strength was obtained in sample with 0.02% The results become clearly proven through verification by scanning electron image where the additive has successfully fill the voids in the concrete’s sample, resulting in strength enhancement of the sample.

The Shear Strength and Fracture Behavior of Sn-Ag- xSb Solder Joints with Au/Ni-P/Cu UBM

NASA Astrophysics Data System (ADS)

Lee, Hwa-Teng; Hu, Shuen-Yuan; Hong, Ting-Fu; Chen, Yin-Fa

2008-06-01

This study investigates the effects of Sb addition on the shear strength and fracture behavior of Sn-Ag-based solders with Au/Ni-P/Cu underbump metallization (UBM) substrates. Sn-3Ag- xSb ternary alloy solder joints were prepared by adding 0 wt.% to 10 wt.% Sb to a Sn-3.5Ag alloy and joining them with Au/Ni-P/Cu UBM substrates. The solder joints were isothermally stored at 150°C for up to 625 h to study their microstructure and interfacial reaction with the UBM. Single-lap shear tests were conducted to evaluate the mechanical properties, thermal resistance, and failure behavior. The results show that UBM effectively suppressed intermetallic compound (IMC) formation and growth during isothermal storage. The Sb addition helped to refine the Ag3Sn compounds, further improving the shear strength and thermal resistance of the solders. The fracture behavior evolved from solder mode toward the mixed mode and finally to the IMC mode with increasing added Sb and isothermal storage time. However, SnSb compounds were found in the solder with 10 wt.% Sb; they may cause mechanical degradation of the solder after long-term isothermal storage.

Composite Behavior of a Novel Insulated Concrete Sandwich Wall Panel Reinforced with GFRP Shear Grids: Effects of Insulation Types.

PubMed

Kim, JunHee; You, Young-Chan

2015-03-03

A full-scale experimental program was used in this study to investigate the structural behavior of novel insulated concrete sandwich wall panels (SWPs) reinforced with grid-type glass-fiber-reinforced polymer (GFRP) shear connectors. Two kinds of insulation-expanded polystyrene (EPS) and extruded polystyrene (XPS) with 100 mm thickness were incased between the two concrete wythes to meet the increasing demand for the insulation performance of building envelope. One to four GFRP shear grids were used to examine the degree of composite action of the two concrete wythes. Ten specimens of SWPs were tested under displacement control subjected to four-point concentrated loads. The test results showed that the SWPs reinforced with GFRP grids as shear connectors developed a high degree of composite action resulting in high flexural strength. The specimens with EPS foam exhibited an enhanced load-displacement behavior compared with the specimens with XPS because of the relatively stronger bond between insulation and concrete. In addition, the ultimate strength of the test results was compared to the analytical prediction with the mechanical properties of only GRFP grids. The specimens with EPS insulation presented higher strength-based composite action than the ones with XPS insulation.

Modelling the effect of shear strength on isentropic compression experiments

NASA Astrophysics Data System (ADS)

Thomson, Stuart; Howell, Peter; Ockendon, John; Ockendon, Hilary

2017-01-01

Isentropic compression experiments (ICE) are a way of obtaining equation of state information for metals undergoing violent plastic deformation. In a typical experiment, millimetre thick metal samples are subjected to pressures on the order of 10 - 102 GPa, while the yield strength of the material can be as low as 10-2 GPa. The analysis of such experiments has so far neglected the effect of shear strength, instead treating the highly plasticised metal as an inviscid compressible fluid. However making this approximation belies the basic elastic nature of a solid object. A more accurate method should strive to incorporate the small but measurable effects of shear strength. Here we present a one-dimensional mathematical model for elastoplasticity at high stress which allows for both compressibility and the shear strength of the material. In the limit of zero yield stress this model reproduces the hydrodynamic models currently used to analyse ICEs. Numerical solutions of the governing equations will then be presented for problems relevant to ICEs in order to investigate the effects of shear strength compared with a model based purely on hydrodynamics.

In situ measurements of erosion shear stress and geotechnical shear strength of the intertidal sediments of the experimental managed realignment scheme at Tollesbury, Essex, UK

NASA Astrophysics Data System (ADS)

Watts, C. W.; Tolhurst, T. J.; Black, K. S.; Whitmore, A. P.

2003-11-01

Managed realignment is one of several 'soft' engineering options which may reduce the costs of coastal defence, provide a more 'natural' response to the problem of rising sea levels and at the same time deliver environmental, specifically nature conservation, benefits. The success of this technique depends on the ability of the soils and sediments within the site to resist the erosive action of waves and tidal currents and allow sediment accretion to occur, at least at a rate equal to mean sea-level rise. Once a critical shear stress, τ0 crt exerted by the moving fluids over the bed, is exceeded erosion will occur. A cohesive strength meter (CSM) and the fall-cone method were used to gather data, in situ on the strength and stability of sediments from an experimental managed realignment site and an adjacent, established saltmarsh in south-east England. Following six years of regular tidal cover, the underlying agricultural soil appeared both very strong (mean surface shear strength, τ f=228 kPa) and highly resistant to erosion ( τ 0 crt=6.23 N m -2). During this period much of the site had been covered by sediment, and saltmarsh plants ( Salicornia europaea) had become established above the mean high water neap tide (MHWN) level. Above MHWN level (tidal cover time <15%) sediments had greater bulk densities and lower water contents which resulted in a moderate shear strength (τ f=11.6 kPa) and resistance to erosion (τ 0 crt=2.45 N m -2) . Below MHWN, where sediment accretion rates were greatest, poor consolidation resulted in very high water contents and low bulk densities. These areas were at the highest potential risk of erosion (τ 0 crt=1.5 N m -2) and had very low shear strengths (τ f=0.33 kPa) . Where sediment exceeded 25 cm depth, gullies formed allowing their banks and adjacent margins to drain faster than the surrounding sediment. This led to a significant increase in bed strength (τ f=10.8 kPa) and stability (τ 0 crt=4.3 N m -2) . These gullies were probably the early stages of the complex creek patterns characteristic of the adjacent, established saltmarsh. The established saltmarsh was rich in plants and had a well-developed (aggregated) soil structure. These soils had a moderate to high resistance to erosion (τ 0 crt=2.45 N m -2) and shear strength (τ f=25.6 kPa) . Undrained sediment shear strength, τf, obtained with the fall-cone apparatus can also provide a useful indication of critical erosion shear stress, τ0 crt . Values of τ0 crt , measured across this site were all relatively large compared with computed bed stresses arising from locally generated waves. Thus this experimental managed realignment site was found to be primarily depositional and was thus successfully achieving the twin aims of protecting the coast from erosion and extending a rich ecosystem.

Geometry of the Nojima fault at Nojima-Hirabayashi, Japan - II. Microstructures and their implications for permeability and strength

USGS Publications Warehouse

Moore, Diane E.; Lockner, D.A.; Ito, H.; Ikeda, R.; Tanaka, H.; Omura, K.

2009-01-01

Samples of damage-zone granodiorite and fault core from two drillholes into the active, strike-slip Nojima fault zone display microstructures and alteration features that explain their measured present-day strengths and permeabilities and provide insight on the evolution of these properties in the fault zone. The least deformed damage-zone rocks contain two sets of nearly perpendicular (60-90?? angles), roughly vertical fractures that are concentrated in quartz-rich areas, with one set typically dominating over the other. With increasing intensity of deformation, which corresponds generally to increasing proximity to the core, zones of heavily fragmented rock, termed microbreccia zones, develop between prominent fractures of both sets. Granodiorite adjoining intersecting microbreccia zones in the active fault strands has been repeatedly fractured and locally brecciated, accompanied by the generation of millimeter-scale voids that are partly filled with secondary minerals. Minor shear bands overprint some of the heavily deformed areas, and small-scale shear zones form from the pairing of closely spaced shear bands. Strength and permeability measurements were made on core collected from the fault within a year after a major (Kobe) earthquake. Measured strengths of the samples decrease regularly with increasing fracturing and fragmentation, such that the gouge of the fault core and completely brecciated samples from the damage zone are the weakest. Permeability increases with increasing disruption, generally reaching a peak in heavily fractured but still more or less cohesive rock at the scale of the laboratory samples. Complete loss of cohesion, as in the gouge or the interiors of large microbreccia zones, is accompanied by a reduction of permeability by 1-2 orders of magnitude below the peak values. The core samples show abundant evidence of hydrothermal alteration and mineral precipitation. Permeability is thus expected to decrease and strength to increase somewhat in active fault strands between earthquakes, as mineral deposits progressively seal fractures and fill pore spaces. ?? Birkh??user Verlag, Basel 2009.

Shear Bond Strength of Orthodontic Brackets to Tooth Enamel After Treatment With Different Tooth Bleaching Methods.

PubMed

Vahid Dastjerdi, Elahe; Khaloo, Negar; Mojahedi, Seyed Masoud; Azarsina, Mohadese

2015-11-01

Bleaching treatments decrease shear bond strength between orthodontic brackets and teeth; although definite results have not been reported in this regard. This study determined the effects of different bleaching protocols on the shear bond strength of orthodontic brackets to teeth. This experimental study was performed in Iran. Forty-eight extracted human premolars were randomly assigned into four groups. In the control group, no bleaching treatment was performed. In groups 2 - 4, the bleaching procedures were performed using carbamide peroxide 45%, carbamide peroxide 20% and diode laser, respectively. Two weeks later, brackets were bonded to teeth and thermocycled. The shear bond strengths of the brackets to the teeth were measured. Data was analyzed by one-way ANOVA and Dunnett post-hoc test. Shear bond strength of the brackets to the teeth were 10.54 ± 1.51, 6.37 ± 0.92, 7.67 ± 1.01 and 7.49 ± 1.19 MPa, in groups 1 - 4, respectively. Significant differences were found between control group and all other groups (P < 0.001); and also between groups 2 and 3 (P < 0.05). No significant differences were found between the other groups. The bleaching procedures using 20% carbamide peroxide and 45% carbamide peroxide and diode laser significantly decreased shear bond strength of brackets to the teeth. 45% carbamide peroxide had a more significant effect on bond strength compared to 20% carbamide peroxide. The difference in bond strength was not significant between laser group and either carbamide peroxide groups.

Strength Properties and Organic Carbon of Soils in the North Apalachian Region

DOE Office of Scientific and Technical Information (OSTI.GOV)

Blanco-Canqui, H; Lal, Rattan; Owen, L B.

2005-04-01

Soil strength influenced by management and soil properties controls plant growth, root development, and soil-moisture relations. The impact of textural and structural parameters on soil strength is moderated by soil organic C (SOC) concentration. Therefore, the objectives of this study were to assess differences in soil strength and SOC concentration in watersheds under long-term (>15 yr) management practices in the North Appalachian region on a predominantly Typic Hapludults on undulating slopes (>6% slope). Seven watersheds without field replication under moldboard plow (MP), chisel plow, disk with beef cattle manure (DiskM), no-till with beef cattle manure (NTm), no-till with no beefmore » cattle manure (NTnm), pasture, and forest were studied. Cone index (CI), shear strength, bulk density (b), volumetric moisture content (v), and SOC concentration were determined at the summit, backslope, and footslope landscape positions at the 0- to 10-, 10- to 20-, and 20- to 30-cm depths. The SOC concentration was slightly higher at the footslope than at the summit position in the cultivated watersheds. The b was lower at the footslope than at the summit in NTm (1.22 vs. 1.42 Mg m{sup -3}) and chisel (1.34 vs. 1.47 Mg m{sup -3}) treatments. Forest had the lowest CI (0.19 MPa), shear strength (6.11 kPa), and b (0.93 Mg m{sup -3}) and the highest SOC concentration (62.7 g kg{sup -1}), whereas MP had the highest CI (0.67 MPa), shear strength (25.5 kPa), b (1.44 Mg m{sup -3}), and the lowest SOC concentration (13.6 g kg{sup -1}) in the 0- to 10-cm depth (P < 0.01). The SOC concentration in NTm was 1.7 times higher than that in NTnm, and both no-till treatments had lower b (<1.21 Mg m{sup -3}) than MP (1.44 Mg m{sup -3}) at 0- to 10-cm depth (P < 0.01). Manuring decreased both CI and shear strength, but increased SOC concentration. The b, v, and SOC concentration were potential predictors of CI; whereas b and SOC concentration were of shear strength (r2 > 0.42; P < 0.01). Results show that landscape positions had small effect, but management, particularly manuring, had large and significant effects on soil strength and SOC concentration.« less

Volcano collapse promoted by progressive strength reduction: New data from Mount St. Helens

USGS Publications Warehouse

Reid, Mark E.; Keith, Terry E.C.; Kayen, Robert E.; Iverson, Neal R.; Iverson, Richard M.; Brien, Dianne

2010-01-01

Rock shear strength plays a fundamental role in volcano flank collapse, yet pertinent data from modern collapse surfaces are rare. Using samples collected from the inferred failure surface of the massive 1980 collapse of Mount St. Helens (MSH), we determined rock shear strength via laboratory tests designed to mimic conditions in the pre-collapse edifice. We observed that the 1980 failure shear surfaces formed primarily in pervasively shattered older dome rocks; failure was not localized in sloping volcanic strata or in weak, hydrothermally altered rocks. Our test results show that rock shear strength under large confining stresses is reduced ∼20% as a result of large quasi-static shear strain, as preceded the 1980 collapse of MSH. Using quasi-3D slope-stability modeling, we demonstrate that this mechanical weakening could have provoked edifice collapse, even in the absence of transiently elevated pore-fluid pressures or earthquake ground shaking. Progressive strength reduction could promote collapses at other volcanic edifices.

Shear strength of a three-dimensional capillary-porous titanium coating for biomedical applications

NASA Astrophysics Data System (ADS)

Kalita, V. I.; Komlev, D. I.; Radyuk, A. A.; Ivannikov, A. Yu; Alpatov, A. V.; Komlev, V. S.; Mamonov, V. I.; Sevostyanov, M. A.; Baikin, A. S.

2018-04-01

The effect of pretreatment and plasma preheating of Ti-substrate on shear strength of three-dimensional capillary porous Ti-coating was studied. After sandblasting the shear strength of the plasma sprayed coating was 200 ± 2 MPa, and after additional matting it was 68 ± 4 MPa. The use of plasma preheating of the substrates for 9 seconds decreased difference between values of the shear strength to 249 ± 17 MPa and 229 ± 16 MPa, respectively. After plasma spraying the microhardness of the surface layer of the substrate was 4.34 ± 0.35 GPa, the microhardness of the boundary between the coating and the substrate was 8.08 ± 0.45 GPa, and the microhardness of the coating was 3.48 ± 0.25 GPa. High shear strength of the coating was attributed to the activation of the substrate by means of plasma preheating and hardening of the boundary between the coating and the substrate by oxides and nitrides.

Prediction of residual shear strength of corroded reinforced concrete beams

NASA Astrophysics Data System (ADS)

Imam, Ashhad; Azad, Abul Kalam

2016-09-01

With the aim of providing experimental data on the shear capacity and behavior of corroded reinforced concrete beams that may help in the development of strength prediction models, the test results of 13 corroded and four un-corroded beams are presented. Corrosion damage was induced by accelerated corrosion induction through impressed current. Test results show that loss of shear strength of beams is mostly attributable to two important damage factors namely, the reduction in stirrups area due to corrosion and the corrosion-induced cracking of concrete cover to stirrups. Based on the test data, a method is proposed to predict the residual shear strength of corroded reinforced concrete beams in which residual shear strength is calculated first by using corrosion-reduced steel area alone, and then it is reduced by a proposed reduction factor, which collectively represents all other applicable corrosion damage factors. The method seems to yield results that are in reasonable agreement with the available test data.

In situ pore-pressure evolution during dynamic CPT measurements in soft sediments of the western Baltic Sea

NASA Astrophysics Data System (ADS)

Seifert, Annedore; Stegmann, Sylvia; Mörz, Tobias; Lange, Matthias; Wever, Thomas; Kopf, Achim

2008-08-01

We present in situ strength and pore-pressure measurements from 57 dynamic cone penetration tests in sediments of Mecklenburg ( n = 51), Eckernförde ( n = 2) and Gelting ( n = 4) bays, western Baltic Sea, characterised by thick mud layers and partially free microbial gas resulting from the degradation of organic material. In Mecklenburg and Eckernförde bays, sediment sampling by nine gravity cores served sedimentological characterisation, analyses of geotechnical properties, and laboratory shear tests. At selected localities, high-resolution echo-sounder profiles were acquired. Our aim was to deploy a dynamic cone penetrometer (CPT) to infer sediment shear strength and cohesion of the sea bottom as a function of fluid saturation. The results show very variable changes in pore pressure and sediment strength during the CPT deployments. The majority of the CPT measurements ( n = 54) show initially negative pore-pressure values during penetration, and a delayed response towards positive pressures thereafter. This so-called type B pore-pressure signal was recorded in all three bays, and is typically found in soft muds with high water contents and undrained shear strengths of 1.6-6.4 kPa. The type B signal is further affected by displacement of sediment and fluid upon penetration of the lance, skin effects during dynamic profiling, enhanced consolidation and strength of individual horizons, the presence of free gas, and a dilatory response of the sediment. In Mecklenburg Bay, the remaining small number of CPT measurements ( n = 3) show a well-defined peak in both pore pressure and cone resistance during penetration, i.e. an initial marked increase which is followed by exponential pore-pressure decay during dissipation. This so-called type A pore-pressure signal is associated with normally consolidated mud, with indurated clay layers showing significantly higher undrained shear strength (up to 19 kPa). In Eckernförde and Gelting bays pore-pressure response type B is exclusively found, while in Mecklenburg Bay types A and B were detected. Despite the striking similarities in incremental density increase and shear strength behaviour with depth, gas occurrence and subtle variations in the coarse-grained fraction cause distinct pore-pressure curves. Gaseous muds interbedded with silty and sandy layers are most common in the three bays, and the potential effect of free gas (i.e. undersaturated pore space) on in situ strength has to be explored further.

Hybrid Microcircuit Rework Procedures Evaluation.

DTIC Science & Technology

1980-08-01

replacement Task III. Polymer Attachment Rework (a) Die replacement (b) Substrate replacement Task IV. Interconnection Rework (a) Gold and aluminum ...the following conclusions: (a) Lap Shear Strength The shear strength ( aluminum to aluminum ) values ranged from a high of 4000 psi (for Ablefilm 550...bonded specimens ( aluminum to aluminum ) to 150°C for 10, 20 and 35 days prior to testing. No significant degradation of lap shear strength of any of the

Rheological Characteristics of Cement Grout and its Effect on Mechanical Properties of a Rock Fracture

NASA Astrophysics Data System (ADS)

Liu, Quansheng; Lei, Guangfeng; Peng, Xingxin; Lu, Chaobo; Wei, Lai

2018-02-01

Grouting reinforcement, which has an obvious strengthening effect on fractured rock mass, has been widely used in various fields in geotechnical engineering. The rheological properties of grout will greatly affect its diffusion radius in rock fractures, and the water-cement ratio is an important factor in determining the grouting flow patterns. The relationship between shear stress and shear rate which could reflect the grout rheological properties, the effects of water-cement ratio, and temperature on the rheological properties of grouting was studied in the laboratory. Besides, a new method for producing fractured rock specimens was proposed and solved the problem of producing natural fractured rock specimens. To investigate the influences of grouting on mechanical properties of a rock fracture, the fractured rock specimens made using the new method were reinforced by grouting on the independent designed grouting platform, and then normal and tangential mechanical tests were carried out on fractured rock specimens. The results showed that the mechanical properties of fractured rock mass are significantly improved by grouting, the peak shear strength and residual strength of rock fractures are greatly improved, and the resistance to deformation is enhanced after grouting. Normal forces affect the tangential behavior of the rock fracture, and the tangential stress strength increases with normal forces. The strength and stability of fractured rock mass are increased by grouting reinforcement.

Effect of different intracoronal bleaching methods on shear bond strength of ceramic brackets bonded to bleached enamel: An in-vitro study.

PubMed

Chauhan, Vikas; Kumar, Piush; Sharma, Payal; Shetty, Divya

2017-01-01

To investigate the effect of different intracoronal bleaching methods on the shear bond strength and site of failure of ceramic brackets. Sixty freshly extracted human maxillary incisors were randomly divided into four groups ( n = 15). Endodontic access cavity was prepared and root canals were filled, root fillings were removed 2mm apical to the cementoenamel junction, and a 2-mmthick layer of glass ionomer cement base was applied. Group 1 served as the control. Intracoronal bleaching was performed with 35% carbamide peroxide in group 2, sodium perborate in group 3, and 37.5% hydrogen peroxide in group 4. The teeth were immersed in artificial saliva for 4 weeks before bracket bonding. Ceramic brackets were bonded with composite resin and cured with LED light. After bonding, the shear bond strength of the brackets was tested with a universal testing machine. The site of bond failure was determined by modified ARI (Adhesive Remnant Index). The highest value of shear bond strength was measured in control group (18.67 ± 1.59 MPa), which was statistically significant from groups 2,3, and 4. There was no significant difference between groups 2 and 4. The lowest shear bond strength was measured in group 3. ARI scores were not significant from each other. Intracoronal bleaching significantly affected the shear bond strength of ceramic brackets even after 4 weeks of bleaching. Bleaching with sodium perborate affects shear bond strength more adversely than does bleaching with other agents like hydrogen peroxide and carbamide peroxide.

A Comparative Evaluation of Effect of Different Chemical Solvents on the Shear Bond Strength of Glass Fiber reinforced Post to Core Material

PubMed Central

Samadi, Firoza; Jaiswal, JN; Saha, Sonali

2014-01-01

ABSTRACT% Aim: To compare the effect of different chemical solvents on glass fiber reinforced posts and to study the effect of these solvents on the shear bond strength of glass fiber reinforced post to core material. Materials and methods: This study was conducted to evaluate the effect of three chemical solvents, i.e. silane coupling agent, 6% H2O2 and 37% phosphoric acid on the shear bond strength of glass fiber post to a composite resin restorative material. The changes in post surface characteristics after different treatments were also observed, using scanning electron microscopy (SEM) and shear bond strength was analyzed using universal testing machine (UTM). Results: Surface treatment with hydrogen peroxide had greatest impact on the post surface followed by 37% phosphoric acid and silane. On evaluation of the shear bond strength, 6% H2O2 exhibited the maximum shear bond strength followed in descending order by 37% phosphoric acid and silane respectively. Conclusion: The surface treatment of glass fiber post enhances the adhesion between the post and composite resin which is used as core material. Failure of a fiber post and composite resin core often occurs at the junction between the two materials. This failure process requires better characterization. How to cite this article: Sharma A, Samadi F, Jaiswal JN, Saha S. A Comparative Evaluation of Effect of Different Chemical Solvents on the Shear Bond Strength of Glass Fiber Reinforced Post to Core Material. Int J Clin Pediatr Dent 2014;7(3):192-196. PMID:25709300

Effect of smear layer thickness and pH of self-adhesive resin cements on the shear bond strength to dentin.

PubMed

Ebrahimi Chaharom, Mohammad Esmaeel; Ajami, Amir Ahmad; Bahari, Mahmoud; Rezazadeh, Haleh

2017-01-01

There are concerns in relation to the bonding efficacy of self-adhesive resin cements to dentin covered with the smear layer. This study aims to evaluate the effect of smear layer thickness and different pH values of self-adhesive resin cements on the shear bond strength to dentin. The dentin on the buccal and lingual surfaces of 48 sound human premolars were abraded with 60- and 600-grit silicon carbide papers to achieve thick and thin smear layers, respectively. The samples were divided into three groups (n = 16) based on the cement pH: Rely-X Unicem (RXU) (pH < 2); Clearfil SA Luting (CSL) (pH = 3); and Speed CEM (SPC) (pH = 4.5). In each group, composite resin blocks were bonded to the buccal and lingual surfaces. After 24 h, the shear bond strength values were measured in MPa, and the failure modes were evaluated under a stereomicroscope. Data were analyzed with two-way ANOVA and post hoc least significant difference tests (P < 0.05). Cement pH had a significant effect on the shear bond strength (P = 0.02); however, the smear layer thickness had no significant effect on the shear bond strength (P > 0.05). The cumulative effect of these variables was not significant, either (P = 0.11). The shear bond strengths of SPC and CSL self-adhesive resin cements were similar and significantly lower than that of RXU. The smear layer thickness was not a determining factor for the shear bond strength value of self-adhesive resin cements.

Comparison of the effect of different surface treatments on the bond strength of different cements with nickel chromium metal alloy: An in vitro study

PubMed Central

Kapoor, Saumya; Balakrishnan, Dhanasekar

2017-01-01

Background For success of any indirect metal restoration, a strong bond between cement and the intaglio surface of metal is imperative. The aim of this study is to evaluate and compare the effect of different surface treatment on the tensile and shear bond strength of different cements with nickel–chromium alloy. Material and Methods 120 premolars were sectioned horizontally parallel to the occlusal surface to expose the dentin. Wax patterns were fabricated for individual tooth followed by casting them in nickel chromium alloy. 60 samples were tested for tensile bond strength, and the remaining 60 for shear bond strength. The samples were divided into three groups (of 20 samples each) as per the following surface treatment: oxidation only, oxidation and sandblasting, or oxidation, sandblasting followed by application of alloy primer. Each group was subdivided into 2 subgroups of 10 samples each, according to the bonding cement i.e RM-GIC and resin cement. Samples were subjected to thermocycling procedure followed by evaluation of bond strength. Results Two-way analyses of variance (ANOVA) was performed to compare the means of tensile and shear bond strength across type of surface treatment and cement, followed by post hoc parametric analysis. For all tests ‘p’ value of less than 0.05 was considered statistically significant. Conclusions The surface treatment of oxidation and sandblasting followed by application of alloy primer offered the maximum tensile and shear bond strength for both RM GIC and resin cement. Resin cement exhibited greater tensile and shear bond strength than RM-GIC for all the three surface treatment methods. Key words:Resin cement, resin modified glass ionomer cement, oxidation, sandblasting, alloy primer, tensile bond strength, shear bond strength, universal testing machine. PMID:28828160

Aerospace Threaded Fastener Strength in Combined Shear and Tension Loading

NASA Technical Reports Server (NTRS)

Steeve, B. E.; Wingate, R. J.

2012-01-01

A test program was initiated by Marshall Space Flight Center and sponsored by the NASA Engineering and Safety Center to characterize the failure behavior of a typical high-strength aerospace threaded fastener under a range of shear to tension loading ratios for both a nut and an insert configuration where the shear plane passes through the body and threads, respectively. The testing was performed with a customized test fixture designed to test a bolt with a single shear plane at a discrete range of loading angles. The results provide data to compare against existing combined loading failure criteria and to quantify the bolt strength when the shear plane passes through the threads.

Climatological characteristics of high altitude wind shear and lapse rate layers

NASA Technical Reports Server (NTRS)

Ehernberger, L. J.; Guttman, N. B.

1981-01-01

Indications of the climatological distribution of wind shear and temperature lapse and inversion rates as observed by rawinsonde measurements over the western United States are recorded. Frequencies of the strongest shear, lapse rates, and inversion layer strengths were observed for a 1 year period of record and were tabulated for the lower troposphere, the upper troposphere, and five altitude intervals in the lower stratosphere. Selected bivariate frequencies were also tabulated. Strong wind shears, lapse rates, and inversion are observed less frequently as altitude increases from 175 millibars to 20 millibars. On a seasonal basis the frequencies were higher in winter than in summer except for minor influences due to increased tropopause altitude in summer and the stratospheric wind reversal in the spring and fall.

Behavior of Tilted Angle Shear Connectors

PubMed Central

Khorramian, Koosha; Maleki, Shervin; Shariati, Mahdi; Ramli Sulong, N. H.

2015-01-01

According to recent researches, angle shear connectors are appropriate to transfer longitudinal shear forces across the steel-concrete interface. Angle steel profile has been used in different positions as L-shaped or C-shaped shear connectors. The application of angle shear connectors in tilted positions is of interest in this study. This study investigates the behaviour of tilted-shaped angle shear connectors under monotonic loading using experimental push out tests. Eight push-out specimens are tested to investigate the effects of different angle parameters on the ultimate load capacity of connectors. Two different tilted angles of 112.5 and 135 degrees between the angle leg and steel beam are considered. In addition, angle sizes and lengths are varied. Two different failure modes were observed consisting of concrete crushing-splitting and connector fracture. By increasing the size of connector, the maximum load increased for most cases. In general, the 135 degrees tilted angle shear connectors have a higher strength and stiffness than the 112.5 degrees type. PMID:26642193

Behavior of Tilted Angle Shear Connectors.

PubMed

Khorramian, Koosha; Maleki, Shervin; Shariati, Mahdi; Ramli Sulong, N H

2015-01-01

According to recent researches, angle shear connectors are appropriate to transfer longitudinal shear forces across the steel-concrete interface. Angle steel profile has been used in different positions as L-shaped or C-shaped shear connectors. The application of angle shear connectors in tilted positions is of interest in this study. This study investigates the behaviour of tilted-shaped angle shear connectors under monotonic loading using experimental push out tests. Eight push-out specimens are tested to investigate the effects of different angle parameters on the ultimate load capacity of connectors. Two different tilted angles of 112.5 and 135 degrees between the angle leg and steel beam are considered. In addition, angle sizes and lengths are varied. Two different failure modes were observed consisting of concrete crushing-splitting and connector fracture. By increasing the size of connector, the maximum load increased for most cases. In general, the 135 degrees tilted angle shear connectors have a higher strength and stiffness than the 112.5 degrees type.

Polycrystalline elastic moduli of a high-entropy alloy at cryogenic temperatures

DOE PAGES

Haglund, A.; Koehler, M.; Catoor, D.; ...

2014-12-05

A FCC high-entropy alloy (HEA) that exhibits strong temperature dependence of strength at low homologous temperatures in sharp contrast to pure FCC metals like Ni that show weak temperature dependence is CrMnCoFeNi. In order to understand this behavior, elastic constants were determined as a function of temperature. From 300 K down to 55 K, the shear modulus (G) of the HEA changes by only 8%, increasing from 80 to 86 GPa. Moreover, this temperature dependence is weaker than that of FCC Ni, whose G increases by 12% (81–91 GPa). Therefore, the uncharacteristic temperature-dependence of the strength of the HEA ismore » not due to the temperature dependence of its shear modulus.« less

Toward predicting tensile strength of pharmaceutical tablets by ultrasound measurement in continuous manufacturing.

PubMed

Razavi, Sonia M; Callegari, Gerardo; Drazer, German; Cuitiño, Alberto M

2016-06-30

An ultrasound measurement system was employed as a non-destructive method to evaluate its reliability in predicting the tensile strength of tablets and investigate the benefits of incorporating it in a continuous line, manufacturing solid dosage forms. Tablets containing lactose, acetaminophen, and magnesium stearate were manufactured continuously and in batches. The effect of two processing parameters, compaction force and level of shear strain were examined. Young's modulus and tensile strength of tablets were obtained by ultrasound and diametrical mechanical testing, respectively. It was found that as the blend was exposed to increasing levels of shear strain, the speed of sound in the tablets decreased and the tablets became both softer and mechanically weaker. Moreover, the results indicate that two separate tablet material properties (e.g., relative density and Young's modulus) are necessary in order to predict tensile strength. A strategy for hardness prediction is proposed that uses the existing models for Young's modulus and tensile strength of porous materials. Ultrasound testing was found to be very sensitive in differentiating tablets with similar formulation but produced under different processing conditions (e.g., different level of shear strain), thus, providing a fast, and non-destructive method for hardness prediction that could be incorporated to a continuous manufacturing process. Copyright © 2016 Elsevier B.V. All rights reserved.

The modelling influence of water content to mechanical parameter of soil in analysis of slope stability

NASA Astrophysics Data System (ADS)

Gusman, M.; Nazki, A.; Putra, R. R.

2018-04-01

One of the parameters in slope stability analysis is the shear strength of the soil. Changes in soil shear strength characteristics lead to a decrease in safety factors on the slopes. This study aims to see the effect of increased moisture content on soil mechanical parameters. The case study study was conducted on the slopes of Sitinjau Lauik Kota Padang. The research method was done by laboratory analysis and simple liniear regression analysis and multiple. Based on the test soil results show that the increase in soil water content causes a decrease in cohesion values and internal shear angle. The relationship of moisture content to cohesion is described in equation Y = 55.713-0,6X with R2 = 0.842. While the relationship of water content to shear angle in soil is described in the equation Y = 38.878-0.258X with R2 = 0.915. From several simulations of soil water level improvement, calculation of safety factor (SF) of slope. The calculation results show that the increase of groundwater content is very significant affect the safety factor (SF) slope. SF slope values are in safe condition when moisture content is 50% and when it reaches maximum water content 73.74% slope safety factor value potentially for landslide.

Ultrasonic Spot Welding of a Rare-Earth Containing ZEK100 Magnesium Alloy: Effect of Welding Energy

NASA Astrophysics Data System (ADS)

Macwan, A.; Chen, D. L.

2016-04-01

Ultrasonic spot welding was used to join a low rare-earth containing ZEK100 Mg alloy at different levels of welding energy, and tensile lap shear tests were conducted to evaluate the failure strength in relation to the microstructural changes. It was observed that dynamic recrystallization occurred in the nugget zone; the grain size increased and microhardness decreased with increasing welding energy arising from the increasing interface temperature and strain rate. The weld interface experienced severe plastic deformation at a high strain rate from ~500 to ~2100 s-1 with increasing welding energy from 500 to 2000 J. A relationship between grain size and Zener-Hollomon parameter, and a Hall-Petch-type relationship between microhardness and grain size were established. The tensile lap shear strength and failure energy were observed to first increase with increasing welding energy, reach the maximum values at 1500 J, and then decrease with a further increase in the welding energy. The samples welded at a welding energy ≤1500 J exhibited an interfacial failure mode, while nugget pull-out occurred in the samples welded at a welding energy above 1500 J. The fracture surfaces showed typical shear failure. Low-temperature tests at 233 K (-40 °C) showed no significant effect on the strength and failure mode of joints welded at the optimal welding energy of 1500 J. Elevated temperature tests at 453 K (180 °C) revealed a lower failure load but a higher failure energy due to the increased deformability, and showed a mixed mode of partial interfacial failure and partial nugget pull-out.

Shear Bond Strength of Orthodontic Brackets Bonded to Zirconium Crowns

PubMed Central

Mehmeti, Blerim; Azizi, Bleron; Kelmendi, Jeta; Iljazi-Shahiqi, Donika; Alar, Željko

2017-01-01

Background An increasing demand for esthetic restorations has resulted in an increased use of all-ceramic restorations, such as zirconium. However, one of the challenges the orthodontist must be willing to face is how to increase bond strength between the brackets and various ceramic restorations.Bond strength can beaffected bybracket type, by the material that bracketsaremade of, and their base surface design or retention mode. ​ Aim: of this study was to perform a comparative analysis of the shear bond strength (SBS) of metallic and ceramic orthodontic brackets bonded to all-zirconium ceramic surfaces used for prosthetic restorations, and also to evaluate the fracture mode of these two types of orthodontic brackets. Material and methods Twenty samples/semi-crowns of all-zirconium ceramic, on which orthodontic brackets were bonded, 10 metallic and 10 ceramic polycrystalline brackets, were prepared for this research. SBS has been testedby Universal Testing Machine, with a load applied using a knife edged rod moving at a fixed rate of 1 mm/min, until failure occurred. The force required to debond the brackets was recorded in Newton, then SBS was calculated to MPa. In addition, the samples were analyzed using a digital camera magnifier to determine Adhesive Remnant Index (ARI). Statistical data were processed using t-test, and the level of significance was set at α = 0.05. Results Higher shear bond strength values were observed in metallic brackets bonded to zirconium crowns compared tothoseof ceramic brackets, with a significant difference. During the test, two of the ceramic brackets were partially or totally damaged. Conclusion Metallic brackets, compared to ceramic polycrystalline brackets, seemed tocreate stronger adhesion with all-zirconium surfaces due to their better retention mode. Also, ceramic brackets showed higher fragility during debonding. PMID:28827846

Shear Bond Strength of Orthodontic Brackets Bonded to Zirconium Crowns.

PubMed

Mehmeti, Blerim; Azizi, Bleron; Kelmendi, Jeta; Iljazi-Shahiqi, Donika; Alar, Željko; Anić-Milošević, Sandra

2017-06-01

An increasing demand for esthetic restorations has resulted in an increased use of all-ceramic restorations, such as zirconium. However, one of the challenges the orthodontist must be willing to face is how to increase bond strength between the brackets and various ceramic restorations.Bond strength can beaffected bybracket type, by the material that bracketsaremade of, and their base surface design or retention mode. ​: A im: of this study was to perform a comparative analysis of the shear bond strength (SBS) of metallic and ceramic orthodontic brackets bonded to all-zirconium ceramic surfaces used for prosthetic restorations, and also to evaluate the fracture mode of these two types of orthodontic brackets. Twenty samples/semi-crowns of all-zirconium ceramic, on which orthodontic brackets were bonded, 10 metallic and 10 ceramic polycrystalline brackets, were prepared for this research. SBS has been testedby Universal Testing Machine, with a load applied using a knife edged rod moving at a fixed rate of 1 mm/min, until failure occurred. The force required to debond the brackets was recorded in Newton, then SBS was calculated to MPa. In addition, the samples were analyzed using a digital camera magnifier to determine Adhesive Remnant Index (ARI). Statistical data were processed using t-test, and the level of significance was set at α = 0.05. Higher shear bond strength values were observed in metallic brackets bonded to zirconium crowns compared tothoseof ceramic brackets, with a significant difference. During the test, two of the ceramic brackets were partially or totally damaged. Metallic brackets, compared to ceramic polycrystalline brackets, seemed tocreate stronger adhesion with all-zirconium surfaces due to their better retention mode. Also, ceramic brackets showed higher fragility during debonding.

Comparison of shear bond strengths of conventional orthodontic composite and nano-ceramic restorative composite: an in vitro study.

PubMed

Nagar, Namit; Vaz, Anna C

2013-01-01

To compare the shear bond strength of a nano-ceramic restorative composite Ceram-X Mono(TM♦), a restorative resin with the traditional orthodontic composite Transbond XT(TM†) and to evaluate the site of bond failure using Adhesive Remnant Index. Sixty extracted human premolars were divided into two groups of 30 each. Stainless steel brackets were bonded using Transbond XT(TM†) (Group I) and Ceram-X Mono(TM♦) (Group II) according to manufacturer's protocol. Shear bond strength was measured on Universal testing machine at crosshead speed of 1 mm/minute. Adhesive Remnant Index scores were assigned to debonded brackets of each group. Data was analyzed using unpaired 't' test and Chi square test. The mean shear bond strength of Group I (Transbond XT(TM†)) was 12.89 MPa ± 2.19 and that of Group II (Ceram-X Mono(TM)) was 7.29 MPa ± 1.76. Unpaired 't' test revealed statistically significant differences amongst the shear bond strength of the samples measured. Chi-square test revealed statistically insignificant differences amongst the ARI scores of the samples measured. Ceram-X Mono(TM♦) had a lesser mean shear bond strength when compared to Transbond XT(TM†) which was statistically significant difference. However, the mean shear bond of Ceram X Mono was within the clinically acceptable range for bonding. Ceram-X Mono(TM†) and Transbond XT(TM†) showed cohesive fracture of adhesive in 72.6% and 66.6% of the specimens, respectively.

Fan-structure wave as a source of earthquake instability

NASA Astrophysics Data System (ADS)

Tarasov, Boris

2015-04-01

Today frictional shear resistance along pre-existing faults is considered to be the lower limit on rock shear strength at confined compression corresponding to the seismogenic layer. This determines the lithospheric strength and the primary earthquake mechanism associated with frictional stick-slip instability on pre-existing faults. This paper introduces a recently identified shear rupture mechanism providing a paradoxical feature of hard rocks - the possibility of shear rupture propagation through the highly confined intact rock mass at shear stress levels significantly less than frictional strength. In the new mechanism the rock failure, associated with consecutive creation of small slabs (known as 'domino-blocks') from the intact rock in the rupture tip, is driven by a fan-shaped domino structure representing the rupture head. The fan-head combines such unique features as: extremely low shear resistance (below the frictional strength), self-sustaining stress intensification in the rupture tip (providing easy formation of new domino-blocks), and self-unbalancing conditions in the fan-head (making the failure process inevitably spontaneous and violent). An important feature of the fan-mechanism is the fact that for the initial formation of the fan-structure an enhanced local shear stress is required, however, after completion of the fan-structure it can propagate as a dynamic wave through intact rock mass at shear stresses below the frictional strength. Paradoxically low shear strength of pristine rocks provided by the fan-mechanism determines the lower limit of the lithospheric strength and favours the generation of new faults in pristine rocks in preference to frictional stick-slip instability along pre-existing faults. The new approach reveals an alternative role of pre-existing faults in earthquake activity: they represent local stress concentrates in pristine rock adjoining the fault where special conditions for the fan-mechanism nucleation are created, while further dynamic propagation of the new fault (earthquake) occurs at low field stresses even below the frictional strength. However, the proximity of the pre-existing discontinuities to the area of instability caused by the fan mechanism creates the illusion of stick-slip instability on the pre-existing faults, thus concealing the real situation.

Shear bond strength in zirconia veneered ceramics using two different surface treatments prior veneering.

PubMed

Gasparić, Lana Bergman; Schauperl, Zdravko; Mehulić, Ketij

2013-03-01

Aim of the study was to assess the effect of different surface treatments on the shear bond strength (SBS) of the veneering ceramics to zirconia core. In a shear test the influence of grinding and sandblasting of the zirconia surface on bonding were assessed. Statistical analysis was performed using SPSS statistical package (version 17.0, SPSS Inc., Chicago, IL, USA) and Microsoft Office Excel 2003 (Microsoft, Seattle, WA, USA). There was a significant difference between the groups considering shear bond strength (SBS) values, i.e. ground and sandblasted samples had significantly higher SBS values than only ground samples (mean difference = -190.67; df = 10, t = -6.386, p < 0.001). The results of the present study indicate that ground and sandblasted cores are superior to ground cores, allowing significantly higher surface roughness and significantly higher shear bond strength between the core and the veneering material.

Evaluation of Effect of Zirconia Surface Treatment, Using Plasma of Argon and Silane, on the Shear Bond Strength of Two Composite Resin Cements

PubMed Central

Ramdev, Poojya; Shruthi, C S

2017-01-01

Introduction Yttria stabilised tetragonal zirconia opens new vistas for all ceramic restoration by the mechanism of transformation toughening, making it much stronger compared to all other ceramic materials. Currently, it is the most recent core material for all ceramic fixed partial dentures due to its ability to withstand high simulated masticatory loads. Problems which have been reported with zirconia restorations involve the core cement interface leading to loss of retention of the prosthesis. Different reasons which have been reported for the same include the lack of adhesion between zirconia and commonly used cements due to absence of silica phase which makes zirconia not etchable. In addition, the hydrophobic nature of zirconia causes low wettability of zirconia surface by the adhesive cements which are commonly used. Aim The purpose of this in vitro study was to compare and evaluate the effect of two pre-treatments of zirconia, using plasma of argon and silane, on the shear bond strength values of two composite resin cements to zirconia and to evaluate the failure pattern of the debonded areas using stereomicroscopic analysis. Materials and Methods Sixty zirconia discs (10 mm×2 mm) were randomly divided into three groups (n=20), following surface treatment, with airborne particle abrasion, using 110 µm Al2O3: Group I (control), Group II (plasma of argon cleaning), and Group III (application of silane primer). Each group had two subgroups based on the type of resin cement used for bonding: subgroup A; Rely X Ultimate (3M ESPE) and subgroup B; Panavia F (Kuraray). In subgroup A, Rely X universal silane primer and in subgroup B Clearfil ceramic primer was used. Shear bond strengths were determined after water storage for one day and thermocycling for 5000 cycles. Data (megapascal) were analyzed using ANOVA and Bonferroni test. Specimens were subjected to stereomicroscopic analysis, for evaluation of failure pattern. Results Group III produced the highest shear bond strength followed by Group II and Group I. Subgroup A showed higher shear bond strength than Subgroup B. Stereomicroscopic analysis showed cohesive failure in Group III, while in Group I adhesive failure was seen. Conclusion Silane primer application caused maximum increase in shear bond strength due to increased wettability. Argon plasma treatment was less effective in comparison to silane treatment. Air abrasion when used alone resulted in lower bond strength values, thereby making it necessary to use a combination of surface treatments. Rely X Ultimate cement was superior to Panavia F in terms of adhesive bonding to zirconia. PMID:28969271

Influence of Cr and W alloying on the fiber-matrix interfacial shear strength in cast and directionally solidified sapphire NiAl composites

NASA Technical Reports Server (NTRS)

Asthana, R.; Tiwari, R.; Tewari, S. N.

1995-01-01

Sapphire-reinforced NiAl matrix composites with chromium or tungsten as alloying additions were synthesized using casting and zone directional solidification (DS) techniques and characterized by a fiber pushout test as well as by microhardness measurements. The sapphire-NiAl(Cr) specimens exhibited an interlayer of Cr rich eutectic at the fiber-matrix interface and a higher interfacial shear strength compared to unalloyed sapphire-NiAl specimens processed under identical conditions. In contrast, the sapphire-NiAl(W) specimens did not show interfacial excess of tungsten rich phases, although the interfacial shear strength was high and comparable to that of sapphire-NiAl(Cr). The postdebond sliding stress was higher in sapphire-NiAl(Cr) than in sapphire-NiAl(W) due to interface enrichment with chromium particles. The matrix microhardness progressively decreased with increasing distance from the interface in both DS NiAl and NiAl(Cr) specimens. The study highlights the potential of casting and DS techniques to improve the toughness and strength of NiAl by designing dual-phase microstructures in NiAl alloys reinforced with sapphire fibers.

The influence of ceramic surface treatments on the micro-shear bond strength of composite resin to IPS Empress 2.

PubMed

Panah, Faride Gerami; Rezai, Sosan Mir Mohammad; Ahmadian, Leila

2008-07-01

An increasing demand for esthetic restorations has resulted in the development of new ceramic systems, but fracture of veneering ceramics still remains the primary cause of failure. Porcelain repair frequently involves replacement with composite resin, but the bond strength between composite resin and all-ceramic coping materials has not been studied extensively. The purpose of this study was to evaluate the influence of different ceramic surface treatments on the micro-shear bond strength of composite resin to IPS Empress 2 coping material. Sixteen 7 x 7 x 1 mm(3) lithia disilicate-based core ceramic plates were fabricated using the lost wax technique. The plates were divided into eight groups, and eight different surface treatments were performed: (1) no treatment (NT); (2) airborne-particle abrasion with 50-mum alumina particles (Al); (3) acid etching with 9.6% hydrofluoric acid for 1 min (HF); (4) silane coating (S); (5) AlHF; (6) AlS; (7) HFS; and (8) AlHFS. Then, ten composite resin cylinders (0.8-mm diameter x 0.5-mm height) were light-polymerized onto the ceramic plates in each group. Each specimen was subjected to a shear load at a crosshead speed of 0.5 mm/min until fracture occurred. The fracture sites were examined with scanning electron microscopy (SEM) to determine the location of failure during debonding and to examine the surface treatment effects. One-way analysis of variance (ANOVA) and multiple comparison (Dunnet T3) tests were used for statistical analysis of data. The mean micro-shear bond strength values (SD) in MPa were--NT: 4.10 (3.06), Al: 7.56 (4.11), HF: 14.04 (2.60), S: 14.58 (2.14), AlHF: 15.56 (3.36), AlS: 23.02 (4.17), HFS: 24.7 (4.43), AlHFS: 26.0 (3.71). ANOVA indicated the influence of surface treatment was significant (p < 0.0001). SEM analysis did not reveal entirely cohesive failure in any composite or ceramic. The micro-shear bond strength of a composite resin to IPS Empress 2 was significantly different depending on the surface treatment method. Among the investigated methods, silane coating after airborne-particle abrasion and etching was the most effective surface treatment in terms of bond strength increase.

Evaluating the shear bond strength of enamel and dentin with or without etching: A comparative study between dimethacrylate-based and silorane-based adhesives

PubMed Central

Hajizadeh, Hila; Nasseh, Atefeh; Rahmanpour, Naim

2015-01-01

Background Silorane-based composites and their specific self-etch adhesive were introduced to conquest the polymerization shrinkage of methacrylate-based composites. It has been shown that additional etching of enamel and dentin can improve the bond strength of self-etch methacrylate-based adhesives but this claim is not apparent about silorane-based adhesives. Our objective was to compare the shear bond strength (SBS) of enamel and dentin between silorane-based adhesive resin and a methacrylate-based resin with or without additional etching. Material and Methods 40 sound human premolars were prepared and divided into two groups: 1- Filtek P60 composite and Clearfil SE Bond adhesive; 2- Filtek P90 composite and Silorane adhesive. Each group divided into two subgroups: with or without additional etching. For additional etching, 37% acid phosphoric was applied before bonding procedure. A cylinder of the composite was bonded to the surface. After 24 hours storage and 500 thermo cycling between 5-55°C, shear bond strength was assessed with the cross head speed of 0.5 mm/min. Then, bonded surfaces were observed under stereomicroscope to determine the failure mode. Data were analyzed with two-way ANOVA and Fischer exact test. Results Shear bond strength of Filtek P60 composite was significantly higher than Filtek P90 composite both in enamel and dentin surfaces (P<0.05). However, additional etching had no significant effect on shear bond strength in enamel or dentin for each of the composites (P>0.05). There was no interaction between composite type and additional etching (P>0.05). Failure pattern was mainly adhesive and no significant correlation was found between failure and composite type or additional etching (P>0.05). Conclusions Shear bond strength of methacrylate-based composite was significantly higher than silorane-based composite both in enamel and dentin surfaces and additional etching had no significant effect on shear bond strength in enamel or dentin for each of the composites. The mode of failure had no meaningful relation to the type of composite and etching factor. Key words:Shear bond strength, adhesive, composite resin, silorane, methacrylate. PMID:26644830

[Influence of different porcelain surface treatment method on the bonding of metal brackets to porcelain].

PubMed

Fan, Cun-Hui; Chen, Jie; Liu, Xin-Qiang; Ma, Xin

2005-08-01

To investigate the influence of different porcelain surface treatment methods on the shear bond strength of metal brackets bonded to porcelain. 80 porcelain facets were divided randomly into two groups according to different adhesive material that was used to bond metal brackets. Adhesive material were Jing-Jin enamel adhesive and light-cured composite resin. Each group was further divided into 4 subgroups according to different surface treatment methods, which were acid etching with 37% phosphoric acid (H3PO4), acid etching with 9.6% hydrofluoric acid (HF), deglazing by grinding and silanating the porcelain surface. All specimens were stored in 37 degrees C water for 24 hours and then the shear bond strength and the porcelain fracture after debonding was determined. The porcelain surfaces after HF etching, H3PO4 etching and deglazing by grinding were examined by scanning electron microscopy respectively. The shear bond strengths in the HF etching groups, the deglazing groups and the silanating groups were much greater than that in the phosphoric etching groups (P < 0.01). Adequate orthodontic bonding strength was achieved both when bonded with light-cured composite resin after deglazing by grinding and when bonded with either of these adhesives after HF etching or surface silanating. There were no differences in the rates of porcelain fractures among groups (P > 0.05). HF etching, deglazing by grinding and silanating can all increase the shear bond strength between metal bracket and porcelain. Surface silanating of porcelain is a better surface treatment when metal brackets bonded to porcelain.

Effect of Multiple Reflow Cycles and Al2O3 Nanoparticles Reinforcement on Performance of SAC305 Lead-Free Solder Alloy

NASA Astrophysics Data System (ADS)

Tikale, Sanjay; Prabhu, K. Narayan

2018-05-01

The effect of Al2O3 nanoparticles reinforcement on melting behavior, microstructure evolution at the interface and joint shear strength of 96.5Sn3Ag0.5Cu (SAC305) lead-free solder alloy subjected to multiple reflow cycles was investigated. The reinforced SAC305 solder alloy compositions were prepared by adding Al2O3 nanoparticles in different weight fractions (0.05, 0.1, 0.3 and 0.5 wt.%) through mechanical dispersion. Cu/solder/Cu micro-lap-shear solder joint specimens were used to assess the shear strength of the solder joint. Differential scanning calorimetry was used to investigate the melting behavior of SAC305 solder nanocomposites. The solder joint interfacial microstructure was studied using scanning electron microscopy. The results showed that the increase in melting temperature (T L) and melting temperature range of the SAC305 solder alloy by addition of Al2O3 nanoparticles were not significant. In comparison with unreinforced SAC305 solder alloy, the reinforcement of 0.05-0.5 wt.% of Al2O3 nanoparticles improved the solder wettability. The addition of nanoparticles in minor quantity effectively suppressed the Cu6Sn5 IMC growth, improved the solder joint shear strength and ductility under multiple reflow cycles. However, the improvement in solder properties was less pronounced on increasing the nanoparticle content above 0.1 wt.% of the solder alloy.

FEM Modeling of In-Plane Stress Distribution in Thick Brittle Coatings/Films on Ductile Substrates Subjected to Tensile Stress to Determine Interfacial Strength.

PubMed

Wang, Kaishi; Zhang, Fangzhou; Bordia, Rajendra K

2018-03-27

The ceramic-metal interface is present in various material structures and devices that are vulnerable to failures, like cracking, which are typically due to their incompatible properties, e.g., thermal expansion mismatch. In failure of these multilayer systems, interfacial shear strength is a good measure of the robustness of interfaces, especially for planar films. There is a widely-used shear lag model and method by Agrawal and Raj to analyse and measure the interfacial shear strength of thin brittle film on ductile substrates. The use of this classical model for a type of polymer derived ceramic coatings (thickness ~18 μm) on steel substrate leads to high values of interfacial shear strength. Here, we present finite element simulations for such a coating system when it is subjected to in-plane tension. Results show that the in-plane stresses in the coating are non-uniform, i.e., varying across the thickness of the film. Therefore, they do not meet one of the basic assumptions of the classical model: uniform in-plane stress. Furthermore, effects of three significant parameters, film thickness, crack spacing, and Young's modulus, on the in-plane stress distribution have also been investigated. 'Thickness-averaged In-plane Stress' (TIS), a new failure criterion, is proposed for estimating the interfacial shear strength, which leads to a more realistic estimation of the tensile strength and interfacial shear strength of thick brittle films/coatings on ductile substrates.

FEM Modeling of In-Plane Stress Distribution in Thick Brittle Coatings/Films on Ductile Substrates Subjected to Tensile Stress to Determine Interfacial Strength

PubMed Central

Zhang, Fangzhou; Bordia, Rajendra K.

2018-01-01

The ceramic-metal interface is present in various material structures and devices that are vulnerable to failures, like cracking, which are typically due to their incompatible properties, e.g., thermal expansion mismatch. In failure of these multilayer systems, interfacial shear strength is a good measure of the robustness of interfaces, especially for planar films. There is a widely-used shear lag model and method by Agrawal and Raj to analyse and measure the interfacial shear strength of thin brittle film on ductile substrates. The use of this classical model for a type of polymer derived ceramic coatings (thickness ~18 μm) on steel substrate leads to high values of interfacial shear strength. Here, we present finite element simulations for such a coating system when it is subjected to in-plane tension. Results show that the in-plane stresses in the coating are non-uniform, i.e., varying across the thickness of the film. Therefore, they do not meet one of the basic assumptions of the classical model: uniform in-plane stress. Furthermore, effects of three significant parameters, film thickness, crack spacing, and Young’s modulus, on the in-plane stress distribution have also been investigated. ‘Thickness-averaged In-plane Stress’ (TIS), a new failure criterion, is proposed for estimating the interfacial shear strength, which leads to a more realistic estimation of the tensile strength and interfacial shear strength of thick brittle films/coatings on ductile substrates. PMID:29584647

DOE Office of Scientific and Technical Information (OSTI.GOV)

Robert Radtke

The manufacture of thermally stable diamond (TSP) cutters for drill bits used in petroleum drilling requires the brazing of two dissimilar materials--TSP diamond and tungsten carbide. The ENDURUS{trademark} thermally stable diamond cutter developed by Technology International, Inc. exhibits (1) high attachment (shear) strength, exceeding 345 MPa (50,000 psi), (2) TSP diamond impact strength increased by 36%, (3) prevents TSP fracture when drilling hard rock, and (4) maintains a sharp edge when drilling hard and abrasive rock. A novel microwave brazing (MWB) method for joining dissimilar materials has been developed. A conventional braze filler metal is combined with microwave heating whichmore » minimizes thermal residual stress between materials with dissimilar coefficients of thermal expansion. The process results in preferential heating of the lower thermal expansion diamond material, thus providing the ability to match the thermal expansion of the dissimilar material pair. Methods for brazing with both conventional and exothermic braze filler metals have been developed. Finite element modeling (FEM) assisted in the fabrication of TSP cutters controllable thermal residual stress and high shear attachment strength. Further, a unique cutter design for absorbing shock, the densification of otherwise porous TSP diamond for increased mechanical strength, and diamond ion implantation for increased diamond fracture resistance resulted in successful drill bit tests.« less

The effect of shear strength on isentropic compression experiments

NASA Astrophysics Data System (ADS)

Thomson, Stuart; Howell, Peter; Ockendon, John; Ockendon, Hilary

2015-06-01

Isentropic compression experiments (ICE) are a novel way of obtaining equation of state information for metals undergoing violent plastic deformation. In a typical experiment, millimetre thick metal samples are subjected to pressures on the order of 10 -102 GPa, while the yield strength of the material can be as low as 10-1GPa. The analysis of such experiments has so far neglected the effect of shear strength, instead treating the highly plasticised metal as an inviscid compressible fluid. However making this approximation belies the basic elastic nature of a solid object. A more accurate method should strive to incorporate the small but measurable effects of shear strength. Here we present a one-dimensional mathematical model for elastoplasticity at high stress which allows for both compressibility and the shear strength of the material. In the limit of zero yield stress this model reproduces the hydrodynamic models currently used to analyse ICEs. We will also show using a systematic asymptotic analysis that entropy changes are universally negligible in the absence of shocks. Numerical solutions of the governing equations will then be presented for problems relevant to ICEs in order to investigate the effects of shear strength over a model based purely on hydrodynamics.

Shear bond strength of metal brackets to feldspathic porcelain treated by Nd:YAG laser and hydrofluoric acid.

PubMed

Hosseini, Mohammad Hashem; Sobouti, Farhad; Etemadi, Ardavan; Chiniforush, Nasim; Shariati, Mahsa

2015-02-01

Adult orthodontic treatment requires bonding orthodontic attachment to dental restorations. Ceramics are commonly used as esthetic restorative materials for the crowns and bridges. The present study evaluated the shear bond strength of metal orthodontic brackets to the feldspathic porcelain surfaces following conditioning by different powers of neodymium-doped yttrium aluminum garnet (Nd:YAG) laser and hydrofluoric acid as a conventional method. Seventy-two glazed porcelain samples were prepared and randomly attributed to six equal groups of 12. In the conventional hydrofluoric (HF) group, the specimens were etched by 9.6% hydrofluoric acid for 4 min. In laser groups, samples were conditioned by 0.75-, 1-, 1.25-, 1.5-, and 2-W Nd:YAG laser for 10 s. Metal brackets were bonded to porcelain samples and after being stored in distilled water for 24 h, they were subjected to thermocycling for 500 cycles. The debonding was carried out by a Zwick testing machine. The data were statistically analyzed by ANOVA and Tamhane multiple comparisons tests. The mean ± SD of the shear bond strength in the laser group 0.75, 1, 1.25, 1.5, and 2 W and HF group was 2.2 ± 0.9, 4.2 ± 1.1, 4.9 ± 2.4, 7 ± 1.7, 9.6 ± 2.7, and 9.4 ± 2.5, respectively. Together with the increased power of laser, the mean shear bond strength was increased continuously and no significant differences were found between the HF group and the laser groups with power of 1.5 or 2 W. Also, there was no significant difference between all test groups in ARI scores. There was no significant difference between bond strength of laser groups with power of 1.5 and 2 W and HF-etched group. So, Nd:YAG laser with appropriate parameters can be used as an alternative method for porcelain etching.

Acoustic Emission Parameters of Three Gorges Sandstone during Shear Failure

NASA Astrophysics Data System (ADS)

Xu, Jiang; Liu, Yixin; Peng, Shoujian

2016-12-01

In this paper, an experimental investigation of sandstone samples from the Three Gorges during shear failure was conducted using acoustic emission (AE) and direct shear tests. The AE count rate, cumulative AE count, AE energy, and amplitude of the sandstone samples were determined. Then, the relationships among the AE signals and shearing behaviors of the samples were analyzed in order to detect micro-crack initiation and propagation and reflect shear failure. The results indicated that both the shear strength and displacement exhibited a logarithmic relationship with the displacement rate at peak levels of stress. In addition, the various characteristics of the AE signals were apparent in various situations. The AE signals corresponded with the shear stress under different displacement rates. As the displacement rate increased, the amount of accumulative damage to each specimen decreased, while the AE energy peaked earlier and more significantly. The cumulative AE count primarily increased during the post-peak period. Furthermore, the AE count rate and amplitude exhibited two peaks during the peak shear stress period due to crack coalescence and rock bridge breakage. These isolated cracks later formed larger fractures and eventually caused ruptures.

Shear Bond Strength of Self-etching Adhesives to Cavities Prepared by Diamond Bur or Er,Cr:YSGG Laser and Effect of Prior Acid Etching.

PubMed

Jhingan, Pulkit; Sachdev, Vinod; Sandhu, Meera; Sharma, Karan

2015-12-01

To compare and evaluate shear bond strength of self-etching adhesives bonded to cavities prepared by diamond bur or Er,Cr:YSGG laser and the effect of prior acid etching on shear bond strength. Ninety-six caries-free human premolars were selected and divided into 2 groups depending on mode of cavity preparation (48 teeth each). Cavities were prepared with Er,Cr:YSGG laser in group 1 and diamond burs in an air-turbine handpiece in group 2. Groups 1 and 2 were further subdivided into three subgroups of 8 teeth each, which were bonded with sixth- or seventh-generation adhesives with or without prior acid etching, followed by restoration of all samples with APX Flow. These samples were subjected to shear bond strength testing. In addition, the surface morphology of 24 samples each from groups 1 and 2 was evaluated using SEM. Data were analyzed using the Shapiro-Wilk test, one- and two-way ANOVA, the t-test, and the least significant difference test, which showed that the data were normally distributed (p > 0.05). The shear bond strength of adhesives in cavities prepared by Er,Cr:YSGG laser was significantly higher than in diamond bur-prepared cavities (p < 0.05). SEM analysis showed a smear-layer-free anfractuous surface on laser-ablated teeth, in contrast to conventional bur-prepared teeth. The Er,Cr:YSGG laser-ablated surface proved to be more receptive for adhesion than those prepared by diamond bur irrespective of the bonding agent used. Seventh-generation adhesives yielded higher shear bond strength than did sixth-generation adhesives. Prior acid etching decreased the shear bond strength of self-etching adhesives.

Comparative study of the shear bond strength of various veneering materials on grade II commercially pure titanium

PubMed Central

Lee, Eun-Young; Jun, Sul-Gi; Wright, Robert F.

2015-01-01

PURPOSE To compare the shear bond strength of various veneering materials to grade II commercially pure titanium (CP-Ti). MATERIALS AND METHODS Thirty specimens of CP-Ti disc with 9 mm diameter and 10 mm height were divided into three experimental groups. Each group was bonded to heat-polymerized acrylic resin (Lucitone 199), porcelain (Triceram), and indirect composite (Sinfony) with 7 mm diameter and 2 mm height. For the control group (n=10), Lucitone 199 were applied on type IV gold alloy castings. All samples were thermocycled for 5000 cycles in 5-55℃ water. The maximum shear bond strength (MPa) was measured with a Universal Testing Machine. After the shear bond strength test, the failure mode was assessed with an optic microscope and a scanning electron microscope. Statistical analysis was carried out with a Kruskal-Wallis Test and Mann-Whitney Test. RESULTS The mean shear bond strength and standard deviations for experimental groups were as follows: Ti-Lucitone 199 (12.11 ± 4.44 MPa); Ti-Triceram (11.09 ± 1.66 MPa); Ti-Sinfony (4.32 ± 0.64 MPa). All of these experimental groups showed lower shear bond strength than the control group (16.14 ± 1.89 MPa). However, there was no statistically significant difference between the Ti-Lucitone 199 group and the control group, and the Ti-Lucitone 199 group and the Ti-Triceram group. Most of the failure patterns in all experimental groups were adhesive failures. CONCLUSION The shear bond strength of veneering materials such as heat-polymerized acrylic resin, porcelain, and indirect composite to CP-Ti was compatible to that of heatpolymerized acrylic resin to cast gold alloy. PMID:25722841

Alternative Penetrometers to Measure the Near Surface Strength of Soft Seafloor Soils

DTIC Science & Technology

2011-01-01

recorded data. The three probe types were a cone penetrometer (CPT), ball penetrometer (BPT), and a shear vane ( VST ). The CPT and BPT measure...electronically a continuous profile of tip and sleeve resistance as well as the porewater pressure during advancement. The VST records the undrained shear...test results and are compared with the VST shear strengths as shown on Figure 5 (Specimen 1) and Figure 6 (Specimen 2). The VST strengths compare

Relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives.

PubMed

Nagura, Yuko; Tsujimoto, Akimasa; Barkmeier, Wayne W; Watanabe, Hidehiko; Johnson, William W; Takamizawa, Toshiki; Latta, Mark A; Miyazaki, Masashi

2018-04-01

The relationship between enamel bond fatigue durability and surface free-energy characteristics with universal adhesives was investigated. The initial shear bond strengths and shear fatigue strengths of five universal adhesives to enamel were determined with and without phosphoric acid pre-etching. The surface free-energy characteristics of adhesive-treated enamel with and without pre-etching were also determined. The initial shear bond strength and shear fatigue strength of universal adhesive to pre-etched enamel were higher than those to ground enamel. The initial shear bond strength and shear fatigue strength of universal adhesive to pre-etched enamel were material dependent, unlike those to ground enamel. The surface free-energy of the solid (γ S ) and the hydrogen-bonding force (γSh) of universal adhesive-treated enamel were different depending on the adhesive, regardless of the presence or absence of pre-etching. The bond fatigue durability of universal adhesives was higher to pre-etched enamel than to ground enamel. In addition, the bond fatigue durability to pre-etched enamel was material dependent, unlike that to ground enamel. The surface free-energy characteristics of universal adhesive-treated enamel were influenced by the adhesive type, regardless of the presence or absence of pre-etching. The surface free-energy characteristics of universal adhesive-treated enamel were related to the results of the bond fatigue durability. © 2018 Eur J Oral Sci.

[Effect of casein phosphopeptide-amorphouscalcium phosphate (CPP-ACP) treatment on the shear bond strength of orthodontic brackets after tooth bleaching].

PubMed

Lu, Jing; Ding, Xiao-jun; Yu, Xiao-ping; Gong, Yi-ming

2015-10-01

To evaluate the effect of casein phosphopeptide-amorphouscalcium phosphate (CPP-ACP) treatment on the shear bond strength of orthodontic brackets after tooth bleaching. One hundred extracted human premolars were randomly divided and treated according to 5 groups (n=20) : (1) no treatment; (2) 10% carbamide peroxide bleaching; (3) 38% hydrogen peroxide bleaching; (4)10% carbamide peroxide bleaching and CPP-ACP paste; (5)38% hydrogen peroxide bleaching and CPP-ACP paste. In all groups, the brackets were bonded using a conventional acid-etch and bond system (Transbond XT, 3M Unitek, Monrovia, Calif). The shear bond strength adhesive remnant index (ARI) of the brackets were determined and the data was analyzed by ANOVA and Bonferroni test using SPSS13.0 software package. The use of 10% carbamide peroxide and 38% hydrogen peroxide bleaching significantly decreased the shear bond strength of orthodontic brackets when compared with untreated group (P<0.05). After combination of tooth bleaching and CPP-ACP treatment, group 4 (10% carbamide peroxide bleaching + CPP-ACP) and group 5 (38% hydrogen peroxide bleaching + CPP-ACP) showed higher levels of shear bond strength than group 2 and 3; however, no significant difference was found (P>0.05). The ARI did not show any significant difference before and after CPP-ACP treatment. After tooth bleaching, CPP-ACP treatment have little influence on the shear bond strength of orthodontic brackets.

Antibacterial effect and shear bond strength of an orthodontic adhesive cement containing Galla chinensis extract

PubMed Central

WANG, LU-FEI; LUO, FENG; XUE, CHAO-RAN; DENG, MENG; CHEN, CHEN; WU, HAO

2016-01-01

Galla chinensis extract (GCE), a naturally-derived agent, has a significant inhibitory effect on cariogenic bacteria. The present study aims to evaluate the antibacterial effect and shear bond strength of an orthodontic adhesive cement containing GCE. A resin-modified glass ionomer cement incorporated GCE at five mass fractions (0, 0.1, 0.2, 0.4, and 0.8%) to prepare GCE-containing cement for analysis. For the agar diffusion test, cement specimens were placed on agar disk inoculated with Streptococcus mutans (strain ATCC 25175). Following 48 h incubation, the inhibition halo diameter was measured. To assess bacteria colonization susceptibility, S. mutans adhesion to cement specimens was detected by scanning electron microscopy (SEM) following 48 h incubation. To evaluate bond strength, a total of 50 metal brackets were bonded on premolar surfaces by using cement (10 teeth/group). Following immersion in an artificial saliva for 3 days, shear bond strength (SBS) was measured. The results demonstrated that GCE-containing samples exhibited a larger bacterial inhibition halo than control, and the inhibition zone increased as the GCE mass fraction increased. SEM analysis demonstrated that S. mutans presented a weaker adherent capacity to all GCE-containing cements compared with control, but the difference between each GCE-containing group was not significant. SBS values of each GCE-containing group exhibited no difference compared with the control. In conclusion, GCE-containing adhesive cement exhibits a promising inhibitory effect on S. mutans growth and adhesion. Without compromising bond strength, adding GCE in adhesive cement may be an attractive option for preventing white spot lesions during orthodontic treatment. PMID:27073642

Rheological structure of the lithosphere in plate boundary strike-slip fault zones

NASA Astrophysics Data System (ADS)

Chatzaras, Vasileios; Tikoff, Basil; Kruckenberg, Seth C.; Newman, Julie; Titus, Sarah J.; Withers, Anthony C.; Drury, Martyn R.

2016-04-01

How well constrained is the rheological structure of the lithosphere in plate boundary strike-slip fault systems? Further, how do lithospheric layers, with rheologically distinct behaviors, interact within the strike-slip fault zones? To address these questions, we present rheological observations from the mantle sections of two lithospheric-scale, strike-slip fault zones. Xenoliths from ˜40 km depth (970-1100 ° C) beneath the San Andreas fault system (SAF) provide critical constraints on the mechanical stratification of the lithosphere in this continental transform fault. Samples from the Bogota Peninsula shear zone (BPSZ, New Caledonia), which is an exhumed oceanic transform fault, provide insights on lateral variations in mantle strength and viscosity across the fault zone at a depth corresponding to deformation temperatures of ˜900 ° C. Olivine recrystallized grain size piezometry suggests that the shear stress in the SAF upper mantle is 5-9 MPa and in the BPSZ is 4-10 MPa. Thus, the mantle strength in both fault zones is comparable to the crustal strength (˜10 MPa) of seismogenic strike-slip faults in the SAF system. Across the BPSZ, shear stress increases from 4 MPa in the surrounding rocks to 10 MPa in the mylonites, which comprise the core of the shear zone. Further, the BPSZ is characterized by at least one order of magnitude difference in the viscosity between the mylonites (1018 Paṡs) and the surrounding rocks (1019 Paṡs). Mantle viscosity in both the BPSZ mylonites and the SAF (7.0ṡ1018-3.1ṡ1020 Paṡs) is relatively low. To explain our observations from these two strike-slip fault zones, we propose the "lithospheric feedback" model in which the upper crust and lithospheric mantle act together as an integrated system. Mantle flow controls displacement and the upper crust controls the stress magnitude in the system. Our stress data combined with data that are now available for the middle and lower crustal sections of other transcurrent fault systems support the prediction for constant shear strength (˜10 MPa) throughout the lithosphere; the stress magnitude is controlled by the shear strength of the upper crustal faults. Fault rupture in the upper crust induces displacement rate loading of the upper mantle, which in turn, causes strain localization in the mantle shear zone beneath the strike-slip fault. Such forced localization leads to higher stresses and strain rates in the shear zone compared to the surrounding rocks. Low mantle viscosity within the shear zone is critical for facilitating mantle flow, which induces widespread crustal deformation and displacement loading. The lithospheric feedback model suggests that strike-slip fault zones are not mechanically stratified in terms of shear stress, and that it is the time-dependent interaction of the different lithospheric layers - rather than their relative strengths - that governs the rheological behavior of the plate boundary, strike-slip fault zones.

The impact of chlorhexidine mouth rinse on the bond strength of polycarbonate orthodontic brackets.

PubMed

Hussein, Farouk Ahmed; Hashem, Mohammed Ibrahim; Chalisserry, Elna P; Anil, Sukumaran

2014-11-01

The purpose of the current in-vivo study was to assess the effect of using 0.12% chlorhexidine (CHX) mouth rinse, before bonding, on shear bond strength of polycarbonate brackets bonded with composite adhesive. Eighteen orthodontic patients with a mean age 21.41 ± 1.2 years, who were scheduled to have 2 or more first premolars extracted, were included in this study. Patients were referred for an oral prophylaxis program which included, in part, the use of a mouth rinse. Patients were divided into 2 groups, a test group of 9 patients who used 0.12% CHX gluconate mouth rinse twice daily and a control group of 9 patients who used a mouth rinse without CHX, but with same color. After 1 week, polycarbonate brackets were bonded to first premolars with Transbond XT composite adhesive. Premolars were extracted after 28 days and tested for shear bond strength on a universal testing machine. Student's t-test was used to compare shear bond strengths of both groups. No statistically significant difference was found in bond strengths' values between both groups. The test group (with CHX) has mean shear bond strength of 14.21 ± 2.42 MPa whereas the control group (without CHX) revealed a mean strength of 14.52 ± 2.31 MPa. The use of 0.12% CHX mouth rinse, for one week before bonding, did not affect the shear bond strength of polycarbonate brackets bonded with Transbond composite. Furthermore, these brackets showed clinically acceptable bond strength.

Comparison of the push-out shear bond strength of four types of glass ionomers when used to bond amalgam: An in vitro study

PubMed Central

Mathew, Vinod Babu; Ramachandran, S; Indira, R; Shankar, P

2011-01-01

Background: Dental amalgam is the primary direct posterior restorative material used worldwide, but it have certain shortcomings due to the lack of adhesiveness to the cavity. The introduction of the concept of bonded amalgam helped improve the use of amalgam as a restorative material. Aim: Evaluation of the comparative push-out shear bond strength of four types of conventional glass ionomers used to bond amalgam to tooth in simulated class I situations. Materials and Methods: Four chemical cure glass ionomers are used: GC Fuji I, GC Fuji II, GC Fuji III and GC Fuji VII, and are compared with unbonded amalgam. The push-out bond strength was tested using the Instron Universal Testing Machine at a crosshead speed of 0.5 mm/min. Statistical Analysis: One-way ANOVA and post hoc Bonferroni tests were used to analyze the data. Results: The results showed that the use of glass ionomer to bond amalgam resulted in an increase in the bond strength of amalgam. The Type VII glass ionomer showed the highest bond strength in comparison with the other glass ionomers. Conclusions: Conventional glass ionomer bonds to amalgam and shows a beneficial increase in the bond strength of the restoration in comparison with unbonded amalgam. PMID:22144798

Shear bond strength of orthodontic brackets and disinclusion buttons: effect of water and saliva contamination.

PubMed

Sfondrini, Maria Francesca; Fraticelli, Danilo; Gandini, Paola; Scribante, Andrea

2013-01-01

The aim of this study was to assess the effect of water and saliva contamination on the shear bond strength and failure site of orthodontic brackets and lingual buttons. 120 bovine permanent mandibular incisors were randomly divided into 6 groups of 20 specimens each. Both orthodontic brackets and disinclusion buttons were tested under three different enamel surface conditions: (a) dry, (b) water contamination, and (c) saliva contamination. Brackets and buttons were bonded to the teeth and subsequently tested using a Instron universal testing machine. Shear bond strength values and adhesive failure rate were recorded. Statistical analysis was performed using ANOVA and Tukey tests (strength values) and Chi squared test (ARI Scores). Noncontaminated enamel surfaces showed the highest bond strengths for both brackets and buttons. Under water and saliva contamination orthodontic brackets groups showed significantly lower shear strengths than disinclusion buttons groups. Significant differences in debond locations were found among the groups under the various enamel surface conditions. Water and saliva contamination of enamel during the bonding procedure lowers bond strength values, more with orthodontic brackets than with disinclusion buttons.

Mega-earthquakes rupture flat megathrusts.

PubMed

Bletery, Quentin; Thomas, Amanda M; Rempel, Alan W; Karlstrom, Leif; Sladen, Anthony; De Barros, Louis

2016-11-25

The 2004 Sumatra-Andaman and 2011 Tohoku-Oki earthquakes highlighted gaps in our understanding of mega-earthquake rupture processes and the factors controlling their global distribution: A fast convergence rate and young buoyant lithosphere are not required to produce mega-earthquakes. We calculated the curvature along the major subduction zones of the world, showing that mega-earthquakes preferentially rupture flat (low-curvature) interfaces. A simplified analytic model demonstrates that heterogeneity in shear strength increases with curvature. Shear strength on flat megathrusts is more homogeneous, and hence more likely to be exceeded simultaneously over large areas, than on highly curved faults. Copyright © 2016, American Association for the Advancement of Science.

Influence of the processing route of porcelain/Ti-6Al-4V interfaces on shear bond strength.

PubMed

Toptan, Fatih; Alves, Alexandra C; Henriques, Bruno; Souza, Júlio C M; Coelho, Rui; Silva, Filipe S; Rocha, Luís A; Ariza, Edith

2013-04-01

This study aims at evaluating the two-fold effect of initial surface conditions and dental porcelain-to-Ti-6Al-4V alloy joining processing route on the shear bond strength. Porcelain-to-Ti-6Al-4V samples were processed by conventional furnace firing (porcelain-fused-to-metal) and hot pressing. Prior to the processing, Ti-6Al-4V cylinders were prepared by three different surface treatments: polishing, alumina or silica blasting. Within the firing process, polished and alumina blasted samples were subjected to two different cooling rates: air cooling and a slower cooling rate (65°C/min). Metal/porcelain bond strength was evaluated by shear bond test. The data were analyzed using one-way ANOVA followed by Tuckey's test (p<0.05). Before and after shear bond tests, metallic surfaces and metal/ceramic interfaces were examined by Field Emission Gun Scanning Electron Microscope (FEG-SEM) equipped with Energy Dispersive X-Ray Spectroscopy (EDS). Shear bond strength values of the porcelain-to-Ti-6Al-4V alloy interfaces ranged from 27.1±8.9MPa for porcelain fused to polished samples up to 134.0±43.4MPa for porcelain fused to alumina blasted samples. According to the statistical analysis, no significant difference were found on the shear bond strength values for different cooling rates. Processing method was statistically significant only for the polished samples, and airborne particle abrasion was statistically significant only for the fired samples. The type of the blasting material did not cause a statistically significant difference on the shear bond strength values. Shear bond strength of dental porcelain to Ti-6Al-4V alloys can be significantly improved from controlled conditions of surface treatments and processing methods. Copyright © 2013 Elsevier Ltd. All rights reserved.

Shear Adhesion of Tapered Nanopillar Arrays.

PubMed

Cho, Younghyun; Minsky, Helen K; Jiang, Yijie; Yin, Kaiyang; Turner, Kevin T; Yang, Shu

2018-04-04

Tapered nanopillars with various cross sections, including cone-shaped, stepwise, and pencil-like structures (300 nm in diameter at the base of the pillars and 1.1 μm in height), are prepared from epoxy resin templated by nanoporous anodic aluminum oxide (AAO) membranes. The effect of pillar geometry on the shear adhesion behavior of these nanopillar arrays is investigated via sliding experiments in a nanoindentation system. In a previous study of arrays with the same geometry, it was shown that cone-shaped nanopillars exhibit the highest adhesion under normal loading while stepwise and pencil-like nanopillars exhibit lower normal adhesion strength due to significant deformation of the pillars that occurs with increasing indentation depth. Contrary to the previous studies, here, we show that pencil-like nanopillars exhibit the highest shear adhesion strength at all indentation depths among three types of nanopillar arrays and that the shear adhesion increases with greater indentation depth due to the higher bending stiffness and closer packing of the pencil-like nanopillar array. Finite element simulations are used to elucidate the deformation of the pillars during the sliding experiments and agree with the nanoindentation-based sliding measurements. The experiments and finite element simulations together demonstrate that the shape of the nanopillars plays a key role in shear adhesion and that the mechanism is quite different from that of adhesion under normal loading.

Tensile and shear bond strength of hard and soft denture relining materials to the conventional heat cured acrylic denture base resin: An In-vitro study.

PubMed

Lau, Mayank; Amarnath, G S; Muddugangadhar, B C; Swetha, M U; Das, Kopal Anshuraj Ashok Kumar

2014-04-01

The condition of the denture bearing tissues may be adversely affected by high stress concentration during function. Chairside Denture (Hard and Soft) reliners are used to distribute forces applied to soft tissues during function. Tensile and shear bond strength has been shown to be dependent on their chemical composition. A weak bond could harbor bacteria, promote staining and delamination of the lining material. To investigate tensile and shear bond strength of 4 different commercially available denture relining materials to conventional heat cured acrylic denture base resin. 4 mm sections in the middle of 160 Acrylic cylindrical specimens (20 mm x 8 mm) were removed, packed with test materials (Mollosil, G C Reline Soft, G C Reline Hard (Kooliner) and Ufi Gel Hard and polymerized. Specimens were divided into 8 groups of 20 each. Tensile and shear bond strength to the conventional heat cured acrylic denture base resin were examined by Instron Universal Tensile Testing Machine using the equation F=N/A (F-maximum force exerted on the specimen (Newton) and A-bonding area= 50.24 mm2). One-way ANOVA was used for multiple group comparisons followed by Bonferroni Test and Hsu's MCB for multiple pairwise comparisons to asses any significant differences between the groups. The highest mean Tensile bond strength value was obtained for Ufi Gel Hard (6.49+0.08 MPa) and lowest for G C Reline Soft (0.52+0.01 MPa). The highest mean Shear bond strength value was obtained for Ufi Gel Hard (16.19+0.1 MPa) and lowest for Mollosil (0.59+0.05 MPa). The Benferroni test showed a significant difference in the mean tensile bond strength and the mean shear bond strength when the two denture soft liners were compared as well as when the two denture hard liners were compared. Hsu's MCB implied that Ufi gel hard is better than its other closest competitors. The Tensile and Shear bond strength values of denture soft reliners were significantly lower than denture hard reliners. How to cite the article: Lau M, Amarnath GS, Muddugangadhar BC, Swetha MU, Das KA. Tensile and shear bond strength of hard and soft denture relining materials to the conventional heat cured acrylic denture base resin: An In-vitro study. J Int Oral Health 2014;6(2):55-61.

Effects of water during cure on the properties of a carbon/phenolic system

NASA Technical Reports Server (NTRS)

Penn, B. G.; Clemons, J. M.; Ledbetter, F. E., III; Daniels, J. G.; Thompson, L. M.

1984-01-01

The effects of prepreg water contamination on interlaminar shear strength, tranverse compressive strength, and longitudinal compressive strength were determined. Decreases in these properties due to water contamination were sugstantial: 28 percent for the interlaminar shear strength, 21 percent for the transverse compressive strength and 31 percent for the longitudinal compressive strength. Since voids were not detected by X-ray analysis, the most likely cause for these results is fiber-matrix debounding in the laminate.

Bond strength evaluation in adhesive joints using NDE and DIC methods

NASA Astrophysics Data System (ADS)

Poudel, Anish

Adhesive bonding of graphite epoxy composite laminates to itself or traditional metal alloys in modern aerospace and aircraft structural applications offers an excellent opportunity to use the most efficient and intelligent combination of materials available thus providing an attractive package for efficient structural designs. However, one of the major issues of adhesive bonding is the occasional formation of interfacial defects such as kissing or weak bonds in the bondline interface. Also, there are shortcomings of existing non-destructive evaluation (NDE) methods to non-destructively detect/characterize these interfacial defects and reliably predicting the bond shear strength. As a result, adhesive bonding technology is still not solely implemented in primary structures of an aircraft. Therefore, there is a greater demand for a novel NDE tool that can meet the existing aerospace requirement for adhesive bondline characterization. This research implemented a novel Acoustography ultrasonic imaging and digital image correlation (DIC) technique to detect and characterize interfacial defects in the bondline and determine bond shear strength in adhesively bonded composite-metal joints. Adhesively bonded Carbon Fiber Reinforced Plastic (CFRP) laminate and 2024-T3 Aluminum single lap shear panels subjected to various implanted kissing/weak bond defects were the primary focus of this study. Kissing/weak bonds were prepared by controlled surface contamination in the composite bonding surface and also by improperly mixing the adhesive constituent. SEM analyses were also conducted to understand the surface morphology of substrates and their interaction with the contaminants. Morphological changes were observed in the microscopic scale and the chemical analysis confirmed the stability of the contaminant at or very close to the interface. In addition, it was also demonstrated that contaminants migrated during the curing of the adhesive from CFRP substrate which caused a decrease of bond shear strength in single lap shear test samples. Through-transmission ultrasonics (TTU) Acoustography at 3.8 MHz showed promising results on the detectability of bondline defects in adhesively bonded CFRP-Al lap shear test samples. A correlation between Acoustography ultrasonic attenuation and average bond shear strength in CFRP-Al lap shear panels demonstrated that differential attenuation increased with the reduction of the bond shear strength. Similarly, optical DIC tests were conducted to identify and quantify kissing bond defects in CFRP-Al single lap shear joints. DIC results demonstrated changes in the normal strain (epsilonyy) contour map of the contaminated specimens at relatively lower load levels (15% ~ 30% of failure loads). Kissing bond regions were characterized by negative strains, and these were attributed to high compressive bending strains and the localized disbonding taking placed at the bondline interface as a result of the load application. It was also observed that contaminated samples suffered from more compressive strains (epsilonyy) compared to the baseline sample along the loading direction and they suffered from less compressive strains (epsilonxx) compared to the baseline sample perpendicular to the loading direction. This demonstrated the adverse effect of the kissing bond on the adhesive joint integrity. This was a very significant finding for the reason that hybrid ultrasonic DIC is being developed as a faster, more efficient, and more reliable NDE technique for determining bond quality and predicting bond shear strength in adhesively bonded structures.

Influence of different processing techniques on the mechanical properties of used tires in embankment construction.

PubMed

Edinçliler, Ayşe; Baykal, Gökhan; Saygili, Altug

2010-06-01

Use of the processed used tires in embankment construction is becoming an accepted way of beneficially recycling scrap tires due to shortages of natural mineral resources and increasing waste disposal costs. Using these used tires in construction requires an awareness of the properties and the limitations associated with their use. The main objective of this paper is to assess the different processing techniques on the mechanical properties of used tires-sand mixtures to improve the engineering properties of the available soil. In the first part, a literature study on the mechanical properties of the processed used tires such as tire shreds, tire chips, tire buffings and their mixtures with sand are summarized. In the second part, large-scale direct shear tests are performed to evaluate shear strength of tire crumb-sand mixtures where information is not readily available in the literature. The test results with tire crumb were compared with the other processed used tire-sand mixtures. Sand-used tire mixtures have higher shear strength than that of the sand alone and the shear strength parameters depend on the processing conditions of used tires. Three factors are found to significantly affect the mechanical properties: normal stress, processing techniques, and the used tire content. Copyright 2009. Published by Elsevier Ltd.

Composite Behavior of a Novel Insulated Concrete Sandwich Wall Panel Reinforced with GFRP Shear Grids: Effects of Insulation Types

PubMed Central

Kim, JunHee; You, Young-Chan

2015-01-01

A full-scale experimental program was used in this study to investigate the structural behavior of novel insulated concrete sandwich wall panels (SWPs) reinforced with grid-type glass-fiber-reinforced polymer (GFRP) shear connectors. Two kinds of insulation-expanded polystyrene (EPS) and extruded polystyrene (XPS) with 100 mm thickness were incased between the two concrete wythes to meet the increasing demand for the insulation performance of building envelope. One to four GFRP shear grids were used to examine the degree of composite action of the two concrete wythes. Ten specimens of SWPs were tested under displacement control subjected to four-point concentrated loads. The test results showed that the SWPs reinforced with GFRP grids as shear connectors developed a high degree of composite action resulting in high flexural strength. The specimens with EPS foam exhibited an enhanced load-displacement behavior compared with the specimens with XPS because of the relatively stronger bond between insulation and concrete. In addition, the ultimate strength of the test results was compared to the analytical prediction with the mechanical properties of only GRFP grids. The specimens with EPS insulation presented higher strength-based composite action than the ones with XPS insulation. PMID:28787978

Relationship of Interfacial Compatibility to Durability of Adhesive - Bonded Joints

DTIC Science & Technology

1981-03-01

same as BR-238, but with the nitrile rubber removed. Because the phenolic matrix resin has different binding properties to the elastomer than do the...primer, which formed phase separated rubber particles having poor mechanical linkage with the matrix resin , resulted in significant loss in shear...having good mechanical linkage with the matrix resin , resulted in good shear strength retention andsignificantly increased toughness. An adhesive

Notched Strength Allowables and Inplane Shear Strength of AS4/VRM-34 Textile Laminates

NASA Technical Reports Server (NTRS)

Grenoble, Ray W.; Johnston, William M.

2013-01-01

Notched and unnotched strength allowables were developed for a textile composite to provide input data to analytical structural models based on the Pultruded Rod Stiffened Efficient Unitized Structure (PRSEUS) concept. Filled-hole tensile strength, filled-hole compressive strength, and inplane shear strength along stitch lines have been measured. The material system evaluated in this study is based on warp-knitted preforms of AS4 carbon fibers and VRM-34 epoxy resin, which have been processed via resin infusion and oven curing. All specimens were tested in as-fabricated (dry) condition. Filled-hole strengths were evaluated with and without through-thickness stitching. The effects of scaling on filled-hole tensile strength were evaluated by testing specimens in two widths, but with identical width / hole-diameter ratios. Inplane shear specimens were stitched in two configurations, and two specimen thicknesses were tested for each stitch configuration.

Dynamic localization and shear-induced hopping of particles: A way to understand the rheology of dense colloidal dispersions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jiang, Tianying; Zukoski, Charles F., E-mail: czukoski@illinois.edu

2014-09-01

For decades, attempts have been made to understand the formation of colloidal glasses and gels by linking suspension mechanics to particle properties where details of size, shape, and spatial dependencies of pair potentials present a bewildering array of variables that can be manipulated to achieve observed properties. Despite the range of variables that control suspension properties, one consistent observation is the remarkably similarity of flow properties observed as particle properties are varied. Understanding the underlying origins of the commonality in those behaviors (e.g., shear-thinning with increasing stress, diverging zero shear rate viscosity with increasing volume fraction, development of a dynamicmore » yield stress plateau with increases in volume faction or strength of attraction, development of two characteristic relaxation times probed in linear viscoelasticity, the creation of a rubbery plateau modulus at high strain frequencies, and shear-thickening) remains a challenge. Recently, naïve mode coupling and dynamic localization theories have been developed to capture collective behavior giving rise to formation of colloidal glasses and gels. This approach characterizes suspension mechanics of strongly interacting particles in terms of sluggish long-range particle diffusion modulated by varying particle interactions and volume fraction. These theories capture the scaling of the modulus with the volume fraction and strength of interparticle attraction, the frequency dependence of the moduli at the onset of the gel/glass transition, together with the divergence of the zero shear rate viscosity and cessation of diffusivity for hard sphere systems as close packing is approached. In this study, we explore the generality of the predictions of dynamic localization theory for systems of particles composed of bimodal particle size distributions experiencing weak interactions. We find that the mechanical properties of these suspensions are well captured within the framework of dynamic localization theory and that suspension mechanics can be understood in terms of a dynamical potential barrier, the magnitude of which governs the zero shear rate viscosity, and onset of a dynamic yield stress plateau as volume fraction or strength of interaction is raised.« less

Interpretation of the human skin biotribological behaviour after tape stripping

PubMed Central

Pailler-Mattei, C.; Guerret-Piécourt, C.; Zahouani, H.; Nicoli, S.

2011-01-01

The present study deals with the modification of the human skin biotribological behaviour after tape stripping. The tape-stripping procedure consists in the sequential application and removal of adhesive tapes on the skin surface in order to remove stratum corneum (SC) layers, which electrically charges the skin surface. The skin electric charges generated by tape stripping highly change the skin friction behaviour by increasing the adhesion component of the skin friction coefficient. It has been proposed to rewrite the friction adhesion component as the sum of two terms: the first classical adhesion term depending on the intrinsic shear strength, τ0, and the second term depending on the electric shear strength, τelec. The experimental results allowed to estimate a numerical value of the electric shear strength τelec. Moreover, a plan capacitor model with a dielectric material inside was used to modelize the experimental system. This physical model permitted to evaluate the friction electric force and the electric shear strength values to calculate the skin friction coefficient after the tape stripping. The comparison between the experimental and the theoretical value of the skin friction coefficient after the tape stripping has shown the importance of the electric charges on skin biotribological behaviour. The static electric charges produced by tape stripping on the skin surface are probably able to highly modify the interaction of formulations with the skin surface and their spreading properties. This phenomenon, generally overlooked, should be taken into consideration as it could be involved in alteration of drug absorption. PMID:21227961

Interpretation of the human skin biotribological behaviour after tape stripping.

PubMed

Pailler-Mattei, C; Guerret-Piécourt, C; Zahouani, H; Nicoli, S

2011-07-06

The present study deals with the modification of the human skin biotribological behaviour after tape stripping. The tape-stripping procedure consists in the sequential application and removal of adhesive tapes on the skin surface in order to remove stratum corneum (SC) layers, which electrically charges the skin surface. The skin electric charges generated by tape stripping highly change the skin friction behaviour by increasing the adhesion component of the skin friction coefficient. It has been proposed to rewrite the friction adhesion component as the sum of two terms: the first classical adhesion term depending on the intrinsic shear strength, τ(0), and the second term depending on the electric shear strength, τ(elec). The experimental results allowed to estimate a numerical value of the electric shear strength τ(elec). Moreover, a plan capacitor model with a dielectric material inside was used to modelize the experimental system. This physical model permitted to evaluate the friction electric force and the electric shear strength values to calculate the skin friction coefficient after the tape stripping. The comparison between the experimental and the theoretical value of the skin friction coefficient after the tape stripping has shown the importance of the electric charges on skin biotribological behaviour. The static electric charges produced by tape stripping on the skin surface are probably able to highly modify the interaction of formulations with the skin surface and their spreading properties. This phenomenon, generally overlooked, should be taken into consideration as it could be involved in alteration of drug absorption.

The Role of Water in Mediating Interfacial Adhesion and Shear Strength in Graphene Oxide.

PubMed

Soler-Crespo, Rafael A; Gao, Wei; Mao, Lily; Nguyen, Hoang T; Roenbeck, Michael R; Paci, Jeffrey T; Huang, Jiaxing; Nguyen, SonBinh T; Espinosa, Horacio D

2018-06-12

Graphene oxide (GO), whose highly tunable surface chemistry enables the formation of strong interfacial hydrogen-bond networks, has garnered increasing interest in the design of devices that operate in the presence of water. For instance, previous studies have suggested that controlling GO's surface chemistry leads to enhancements in interfacial shear strength, allowing engineers to manage deformation pathways and control failure mechanisms. However, these previous reports have not explored the role of ambient humidity and only offer extensive chemical modifications to GO's surface as the main pathway to control GO's interfacial properties. Herein, through atomic force microscopy experiments on GO-GO interfaces, the adhesion energy and interfacial shear strength of GO were measured as a function of ambient humidity. Experimental evidence shows that adhesion energy and interfacial shear strength can be improved by a factor of 2-3 when GO is exposed to moderate (∼30% water weight) water content. Furthermore, complementary molecular dynamics simulations uncovered the mechanisms by which these nanomaterial interfaces achieve their properties. They reveal that the strengthening mechanism arises from the formation of strongly interacting hydrogen-bond networks, driven by the chemistry of the GO basal plane and intercalated water molecules between two GO surfaces. In summary, the methodology and findings here reported provide pathways to simultaneously optimize GO's interfacial and in-plane mechanical properties, by tailoring the chemistry of GO and accounting for water content, in engineering applications such as sensors, filtration membranes, wearable electronics, and structural materials.

Shear Bond Strength of DentStat(trademark) for Bracket Bonding to Gold, Ceramic, and Enamel

DTIC Science & Technology

2012-12-21

i Shear bond strength of DentStatTM for bracket bonding to gold, ceramic, and enamel . A THESIS Presented to the Faculty of Uniform...in the thesis manuscript entitled: ’Shear Bond Strength of DentStatTM for Bracket Bonding to Gold, Ceramic, and Enamel ’ is appropriately...Ceramic, and Enamel ’ 7. Intended publication/meeting: June 2013 8. "Required by" date: 1 July 2013 9. Date of submission for USU approval: 6 June

Bond strength comparison of 2 self-etching primers over a 3-month storage period.

PubMed

Trites, Brian; Foley, Timothy F; Banting, David

2004-12-01

The purpose of this in vitro study was to evaluate the shear-peel bond strength of 2 self-etching primer systems, Transbond Plus (3M/ Unitek, Monrovia, Calif) and First Step (Reliance Orthodontic Products, Itasca, Ill), with their respective adhesives, and compare them with a control adhesive system (Transbond XT, 3M/ Unitek) over a 3-month period. Two hundred seventy extracted human premolars were obtained and randomly divided into 9 groups of 30 teeth. Metal orthodontic brackets were bonded to the enamel, and each adhesive group was stored for 24 horrs (T1), 30 days (T2), or 3 months (T3) in deionized water at 37 degrees C. All bonded specimens were thermocycled at 10 degrees C and 50 degrees C for 24 hours before debonding. Brackets were debonded by using a shear-peel load on a testing machine at a cross-head speed of 2 mm/min. Bond failure was also evaluated. The shear-peel bond strengths of the 3 bonding systems were clinically acceptable with the possible exception of First Step at 30-day storage. Repeated measures analysis of variance showed a statistically significant (P < .0001) difference in mean bond strengths between the 3 adhesive systems. The shear-peel bond strength of the adhesives over the 3 time intervals showed statistically significant (P = .005) changes. In each group, there were statistically significant differences in shear-peel bond strength between time intervals T1-T2 and T2-T3 for Transbond Plus and T2-T3 for First Step. The change in mean shear-peel bond strength of the 3 adhesives demonstrated a consistent pattern of behavior over the 3 storage intervals. The lowest mean shear-peel bond strength values were noted at the 30-day storage. Bond failure analysis (adhesive remnant index) demonstrated mainly cohesive bond failures.

Shear Bond Strength between Fiber-Reinforced Composite and Veneering Resin Composites with Various Adhesive Resin Systems.

PubMed

AlJehani, Yousef A; Baskaradoss, Jagan K; Geevarghese, Amrita; AlShehry, Marey A; Vallittu, Pekka K

2016-07-01

The aim of this research was to evaluate the shear bond strength of different laboratory resin composites bonded to a fiber-reinforced composite substrate with some intermediate adhesive resins. Mounted test specimens of a bidirectional continuous fiber-reinforced substrate (StickNet) were randomly assigned to three equal groups. Three types of commercially available veneering resin composites - BelleGlass®, Sinfony®, and GC Gradia® were bonded to these specimens using four different adhesive resins. Half the specimens per group were stored for 24 hours; the remaining were stored for 30 days. There were 10 specimens in the test group (n). The shear bond strengths were calculated and expressed in MPa. Data were analyzed statistically, and variations in bond strength within each group were additionally evaluated by calculating the Weibull modulus. Shear bond values of those composites are influenced by the different bonding resins and different indirect composites. There was a significant difference in the shear bond strengths using different types of adhesive resins (p = 0.02) and using different veneering composites (p < 0.01). Belle-Glass® had the highest mean shear bond strength when bonded to StickNet substrate using both Prime & Bond NT and OptiBond Solo Plus. Sinfony® composite resin exhibited the lowest shear bond strength values when used with the same adhesive resins. The adhesive mode of failure was higher than cohesive with all laboratory composite resins bonded to the StickNet substructure at both storage times. Water storage had a tendency to lower the bond strengths of all laboratory composites, although the statistical differences were not significant. Within the limitations of this study, it was found that bonding of the veneering composite to bidirectional continuous fiber-reinforced substrate is influenced by the brand of the adhesive resin and veneering composite. © 2015 by the American College of Prosthodontists.

Casein phosphopeptide-amorphous calcium phosphate and shear bond strength of adhesives to primary teeth enamel.

PubMed

Farokh Gisovar, Elham; Hedayati, Nassim; Shadman, Niloofar; Shafiee, Leila

2015-02-01

CPP-ACP (Phosphopeptide-Amorphous Calcium Phosphate) has an important role in caries prevention in pediatric patients. This study was done, because of the great use of CPP-ACP and the need for restoration for teeth treated with CPP-ACP as well as the importance of shear bond strength of adhesives in the success of restorations. This study aimed to evaluate the effect of casein phosphopeptide-amorphous calcium phosphate (CPP-ACP) on shear bond strength of dental adhesives to enamel of primary teeth molars. This in vitro study was conducted on 180 extracted primary molars. They were randomly divided into 6 groups and each group was divided into 2 subgroups (treated with CPP-ACP and untreated). In subgroups with CPP-ACP, enamel was treated with CPP-ACP paste 1 h/d for 5 days. Types of adhesives that were evaluated in this study were Tetric N-Bond, AdheSE, AdheSE One F, single Bond 2, SE Bond, and Adper Prompt L-Pop. Shear bond strength was tested with a universal testing machine and mode of failure was evaluated under stereomicroscope. Data were analyzed by T test, 2-way analysis of variance (ANOVA), Tukey and Fisher exact test using SPSS18. P < 0.05 was considered as significance level. Shear bond strengths of different adhesive systems to enamel of primary teeth treated and untreated with CPP-ACP showed no significant difference (P > 0.05). Mode of failure in all groups regardless of CPP-ACP administration was mainly adhesive type. Our results indicated that CPP-ACP did not affect shear bond strength of studied adhesives to primary teeth enamel. To have a successful and durable composite restoration, having a high strength bonding is essential. Considering the wide use of CPP-ACP in preventing tooth decay and the role of adhesive shear bond strength (SBS) in success of composite restoration, we conducted the present study to evaluate the effect of CPP-ACP on the SBS of adhesives to primary teeth enamel.

Laser-Aided Ceramic Bracket Debonding: A Comprehensive Review

PubMed Central

Ghazanfari, Rezvaneh; Nokhbatolfoghahaei, Hanieh; Alikhasi, Marzieh

2016-01-01

Different techniques have been introduced for the removal of ceramic brackets. Since the early 1990s, lasers have been used experimentally for debonding ceramic brackets. The goal of this study is to give a comprehensive literature review on laser-aided ceramic bracket debonding. PubMed and Google Scholar databases were used to identify dental articles with the following combination of key words: Ceramic brackets, Debonding, and Laser. Sixteen English articles from 2004 to 2015 were selected. The selected studies were categorized according to the variables investigated including the intrapulpal temperature, shear bond strength, debonding time, enamel damage and bracket failure. Most articles reported decreased shear bond strength and debonding time following laser irradiation without any critical and irritating increase in pulpal temperature. There were no reports of bracket failure or enamel damage. Laser irradiation is an efficient way to reduce shear bond strength of ceramic bracket and debonding time. This technique is a safe way for removing ceramic bracket with minimal impact on intrapulpal temperature and enamel surface and it reduces ceramic bracket failure. PMID:27330690

Calcium phosphate compatible bone cement: Characterization, bonding properties and tissue response

NASA Astrophysics Data System (ADS)

Roemhildt, Maria Lynn

A novel, inorganic, bone cement, containing calcium phosphate, developed for implant fixation was evaluated. Setting properties were determined over a range of temperatures. The flow of the cement was greatly increased by application of vibration. Changes in the cement during hydration and aging were evaluated. Compressive strength of the cement over time was studied under simulated physiological conditions from 1 hour to 1 year after setting. After 1 day, this cement had equivalent compressive strength to commercially used PMMA cement. The strength was found to increase over 1 month and high strength was maintained up to 1 year. The shear strength of the cement-metal interface was studied in vitro using a pull-out test. Prepared specimens were stored under physiological conditions and tested at 4 hours, 24 hours, and 60 days. Comparable interfacial shear strength values were found at 4 hours, 24 hours and 60 days for the experimental cement and were not significantly different from values obtained for PMMA cement. In vivo tissue response was evaluated after cement implantation in the femoral medullary canal in canines. Tissue response and bonding at the cement-bone interface were evaluated at 2, 6, and 12 weeks. Cortical bone was found in direct contact with the OC-cement and was healthy. The strength of the cement-bone interface, measured using a push-out test, was significantly higher for the experimental cement than for commercial PMMA bone cement.

Strength characteristics of lightly solidified dredged marine clay admixed with bentonite

NASA Astrophysics Data System (ADS)

Ariffin, Syazwana Tajul; Chan, Chee-Ming

2017-11-01

Strength characteristic is a significant parameter in measuring the effect of soil improvement and effective composition of solidification. In this study, the dredged marine sediment (DMS) collected from Kuala Perlis (Malaysia) was examined to determine its strength characteristics under light cement solidification with bentonite. Dredged marine clay generally has the low shear strength and high void ratio, and consists mainly of soil particles of the fine-grained type. As a discarded geo-waste, it can be potentially treated to for reuse as a backfill material instead of being disposed of, hence reducing the negative impact on the environment. Physico-chemical parameters of the dredged sample were first determined, then solidification was carried out to improve the engineering properties by admixing ordinary Portland cement (OPC) as the binder and bentonite as a volume enhancer to the soil. The DMS was treated with the addition of 3 % and 6 % cement and bentonite within the range of 0-30 %. The specimens were cured at room temperature for 3, 7 and 14 days. The strength gain was measured by unconfined compression test and vane shear test. The laboratory test results were analyzed to establish the relationship between strength properties and solidification specifications. In summary, the strength of specimens increased with the increase of the quantity of bentonite and cement to get the effective composition of the specimen.

Effects of vegetation on runoff generation, sediment yield and soil shear strength on road-side slopes under a simulation rainfall test in the Three Gorges Reservoir Area, China.

PubMed

Liu, Yao-Jun; Wang, Tian-Wei; Cai, Chong-Fa; Li, Zhao-Xia; Cheng, Dong-Bing

2014-07-01

Vegetation recolonization has often been used to control roadside slope erosion, and in this paper, four restoration models - Natural Restoration, Grass, Grass & Shrub, Sodded Strip - were chosen to recolonize the plants on a newly built unpaved roadside slope in the Three Gorges Reservoir Area. After eight months growth, eight rainfall simulations (intensity of 90 mm h(-1) for 60 min) and in-situ soil shear strength test were then carried out to identify the impacts of vegetation on roadside slope erosion and soil shear strength. The erosion on cutslopes was higher than that on fillslopes. The runoff coefficient and soil detachment rate were significantly lower on the Grass & Shrub model (4.3% and 1.99 g m(-2) min(-1), respectively) compared with the other three, which had the highest surface cover (91.4%), aboveground biomass (1.44 kg m(-2)) and root weight density (3.94 kg m(-3)). The runoff coefficient and soil detachment rate on roadside slopes showed a logarithmic decrease with the root weight density, root length density and aboveground biomass. The soil shear strength measured before and after the rainfall was higher on Grass & Shrub (59.29 and 53.73 kPa) and decreased on Grass (46.93 and 40.48 kPa), Sodded Strip (31.20 and 18.87 kPa) and Natural Restoration (25.31 and 9.36 kPa). Negative linear correlations were found between the soil shear strength reduction and aboveground biomass, root weight density and root length density. The variation of soil shear strength reduction was closely related to the roadside slope erosion, a positive linear correlation was found between runoff coefficient and soil shear strength reduction, and a power function was shown between soil detachment rate and soil shear strength reduction. This study demonstrated that Grass and Grass & Shrub were more suitable and highly cost-effective in controlling initial period erosion of newly built low-volume unpaved road. Copyright © 2014 Elsevier B.V. All rights reserved.

Geotechnical properties of municipal solid waste at Laogang Landfill, China.

PubMed

Feng, Shi-Jin; Gao, Ke-Wei; Chen, Yi-Xin; Li, Yao; Zhang, L M; Chen, H X

2017-05-01

Landfills have been widely constructed all around the world in order to properly dispose municipal solid waste (MSW). Understanding geotechnical properties of MSW is essential for the design and operation of landfills. A comprehensive investigation of geotechnical properties of MSW at the largest landfill in China was conducted, including waste composition, unit weight, void ratio, water content, hydraulic conductivity, and shear behavior. A large-scale rigid-wall permeameter and a direct-shear apparatus were adopted to test the hydraulic conductivity and shear behavior of the MSW, respectively. The composition of the MSW varied with age. With the depth increasing from 0 to 16m, the unit weight increased from 7.2 to 12.5kN/m 3 , while the void ratio decreased from 2.5 to 1.76. The water content ranged between 30.0% and 68.9% but did not show a trend with depth. The hydraulic conductivity of the MSW ranged between 4.6×10 -4 and 6.7×10 -3 cm/s. It decreased as the dry unit weight increased and was sensitive to changes in dry unit weight in deeper layers. Displacement-hardening was observed during the whole shearing process and the shear strength increased with the normal stress, the displacement rate, and the unit weight. The friction angle and cohesion varied from (15.7°, 29.1kPa) to (21.9°, 18.3kPa) with depth increasing from 4 to 16m. The shear strength of the MSW obtained in this study was lower than the reported values in other countries, which was caused by the less fibrous materials in the specimens in this study. The results in this study will provide guidance in the design and operation of the landfills in China. Copyright © 2016 Elsevier Ltd. All rights reserved.

Diminishing friction of joint surfaces as initiating factor for destabilising permafrost rocks?

NASA Astrophysics Data System (ADS)

Funk, Daniel; Krautblatter, Michael

2010-05-01

Degrading alpine permafrost due to changing climate conditions causes instabilities in steep rock slopes. Due to a lack in process understanding, the hazard is still difficult to asses in terms of its timing, location, magnitude and frequency. Current research is focused on ice within joints which is considered to be the key-factor. Monitoring of permafrost-induced rock failure comprises monitoring of temperature and moisture in rock-joints. The effect of low temperatures on the strength of intact rock and its mechanical relevance for shear strength has not been considered yet. But this effect is signifcant since compressive and tensile strength is reduced by up to 50% and more when rock thaws (Mellor, 1973). We hypotheisze, that the thawing of permafrost in rocks reduces the shear strength of joints by facilitating the shearing/damaging of asperities due to the drop of the compressive/tensile strength of rock. We think, that decreasing surface friction, a neglected factor in stability analysis, is crucial for the onset of destabilisation of permafrost rocks. A potential rock slide within the permafrost zone in the Wetterstein Mountains (Zugspitze, Germany) is the basis for the data we use for the empirical joint model of Barton (1973) to estimate the peak shear strength of the shear plane. Parameters are the JRC (joint roughness coefficient), the JCS (joint compressive strength) and the residual friction angle (φr). The surface roughness is measured in the field with a profile gauge to create 2D-profiles of joint surfaces. Samples of rock were taken to the laboratory to measure compressive strength using a high-impact Schmidt-Hammer under air-dry, saturated and frozen conditions on weathered and unweathered surfaces. Plugs where cut out of the rock and sand blasted for shear tests under frozen and unfrozen conditions. Peak shear strength of frozen and unfrozen rocks will be calculated using Barton's model. First results show a mean decrease of compressive strength of around 40% when frozen water-saturated rock is exposed to thawing. The friction of sand-blasted rock-plugs decreases by a mean value of 32% considering degradation of rocks by freeze-thaw cycles. Surface roughness could be measured succesfully with the profile gauge and the results show a significant difference between untouched and sheared joint surfaces in the field. Here we show, that shear resistance of rock joints will be diminshed just by the thawing of intact rock. This study will help to establish a sound concept for the destabilization of rocks in permafrost and provide the data for first stability modelling. This will be crucial for predict rock instability in permafrost regions. References: Barton, N. (1973): Review of new shear strength criterion for rock jonts. Engineering Geology 7: 287-332 Mellor, M. (1973): Mechanical Properties of Rocks at Low Temperatures. 2nd International Conference on Permafrost, Yakutsk, Siberia, 334-343.

Seismic behavior of outrigger truss-wall shear connections using multiple steel angles

NASA Astrophysics Data System (ADS)

Li, Xian; Wang, Wei; Lü, Henglin; Zhang, Guangchang

2016-06-01

An experimental investigation on the seismic behavior of a type of outrigger truss-reinforced concrete wall shear connection using multiple steel angles is presented. Six large-scale shear connection models, which involved a portion of reinforced concrete wall and a shear tab welded onto a steel endplate with three steel angles, were constructed and tested under combined actions of cyclic axial load and eccentric shear. The effects of embedment lengths of steel angles, wall boundary elements, types of anchor plates, and thicknesses of endplates were investigated. The test results indicate that properly detailed connections exhibit desirable seismic behavior and fail due to the ductile fracture of steel angles. Wall boundary elements provide beneficial confinement to the concrete surrounding steel angles and thus increase the strength and stiffness of connections. Connections using whole anchor plates are prone to suffer concrete pry-out failure while connections with thin endplates have a relatively low strength and fail due to large inelastic deformations of the endplates. The current design equations proposed by Chinese Standard 04G362 and Code GB50011 significantly underestimate the capacities of the connection models. A revised design method to account for the influence of previously mentioned test parameters was developed.

The significance of nanoparticles on bond strength of polymer concrete to steel

DOE PAGES

Douba, A.; Genedy, M.; Matteo, E. N.; ...

2017-01-03

Here, polymer concrete (PC) is a commonly used material in construction due to its improved durability and good bond strength to steel substrate. PC has been suggested as a repair and seal material to restore the bond between the cement annulus and the steel casing in wells that penetrate formations under consideration for CO 2 sequestration. Nanoparticles including Multi-Walled Carbon Nano Tubes (MWCNTs), Aluminum Nanoparticles (ANPs) and Silica Nano particles (SNPs) were added to an epoxy-based PC to examine how the nanoparticles affect the bond strength of PC to a steel substrate. Slant shear tests were used to determine themore » bond strength of PC incorporating nanomaterials to steel; results reveal that PC incorporating nanomaterials has an improved bond strength to steel substrate compared with neat PC. In particular, ANPs improve the bond strength by 51% over neat PC. Local shear stresses, extracted from Finite Element (FE) analysis of the slant shear test, were found to be as much as twice the apparent/average shear/bond strength. These results suggest that the impact of nanomaterials is higher than that shown by the apparent strength. Fourier Transform Infrared (FTIR) measurements of epoxy with and without nanomaterials showed ANPs to influence curing of epoxy, which might explain the improved bond strength of PC incorporating ANPs.« less

The significance of nanoparticles on bond strength of polymer concrete to steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Douba, A.; Genedy, M.; Matteo, E. N.

Here, polymer concrete (PC) is a commonly used material in construction due to its improved durability and good bond strength to steel substrate. PC has been suggested as a repair and seal material to restore the bond between the cement annulus and the steel casing in wells that penetrate formations under consideration for CO 2 sequestration. Nanoparticles including Multi-Walled Carbon Nano Tubes (MWCNTs), Aluminum Nanoparticles (ANPs) and Silica Nano particles (SNPs) were added to an epoxy-based PC to examine how the nanoparticles affect the bond strength of PC to a steel substrate. Slant shear tests were used to determine themore » bond strength of PC incorporating nanomaterials to steel; results reveal that PC incorporating nanomaterials has an improved bond strength to steel substrate compared with neat PC. In particular, ANPs improve the bond strength by 51% over neat PC. Local shear stresses, extracted from Finite Element (FE) analysis of the slant shear test, were found to be as much as twice the apparent/average shear/bond strength. These results suggest that the impact of nanomaterials is higher than that shown by the apparent strength. Fourier Transform Infrared (FTIR) measurements of epoxy with and without nanomaterials showed ANPs to influence curing of epoxy, which might explain the improved bond strength of PC incorporating ANPs.« less

Shear-rate-dependent strength control on the dynamics of rainfall-triggered landslides, Tokushima Prefecture, Japan

USGS Publications Warehouse

Wang, G.; Suemine, A.; Schulz, W.H.

2010-01-01

A typhoon (Typhoon No. 10) attacked Shikoku Island and the Tyugoku area of Japan in 2004. This typhoon produced a new daily precipitation record of 1317 mm on Shikoku Island and triggered hundreds of landslides in Tokushima Prefecture. One catastrophic landslide was triggered in the Shiraishi area of Kisawa village, and destroyed more than 10 houses while also leaving an unstable block high on the slope. The unstable block kept moving after the event, showing accelerating and decelerating movement during and after rainfall and reaching a displacement of several meters before countermeasures were put into place. To examine the mechanism for this landsliding characteristic, samples (weathered serpentinite) were taken from the field, and their shear behaviours examined using ring shear tests. The test results revealed that the residual shear strength of the samples is positively dependent on the shear rate, which may provide an explanation for the continuous acceleratingdecelerating process of the landsliding. The roughness of the shear surface and the microstructure of the shear zone were measured and observed by laser microscope and SEM techniques in an attempt to clarify the mechanism of shear rate effect on the residual shear strength. Copyright ?? 2010 John Wiley & Sons, Ltd.

Viscoelastic properties of healthy achilles tendon are independent of isometric plantar flexion strength and cross-sectional area.

PubMed

Suydam, Stephen M; Soulas, Elizabeth M; Elliott, Dawn M; Silbernagel, Karin Gravare; Buchanan, Thomas S; Cortes, Daniel H

2015-06-01

Changes in tendon viscoelastic properties are observed after injuries and during healing as a product of altered composition and structure. Continuous Shear Wave Elastography is a new technique measuring viscoelastic properties of soft tissues using external shear waves. Tendon has not been studied with this technique, therefore, the aims of this study were to establish the range of shear and viscosity moduli in healthy Achilles tendons, determine bilateral differences of these parameters and explore correlations of viscoelasticity to plantar flexion strength and tendon area. Continuous Shear Wave Elastography was performed over the free portion of both Achilles tendons from 29 subjects. Isometric plantar flexion strength and cross sectional area were measured. The average shear and viscous moduli was 83.2 kPa and 141.0 Pa-s, respectively. No correlations existed between the shear or viscous modulus and area or strength. This indicates that viscoelastic properties can be considered novel, independent biomarkers. The shear and viscosity moduli were bilaterally equivalent (p = 0.013, 0.017) which allows determining pathologies through side-to-side deviations. The average bilateral coefficient of variation was 7.2% and 9.4% for shear and viscosity modulus, respectively. The viscoelastic properties of the Achilles tendon may provide an unbiased, non-subjective rating system of tendon recovery and optimizing treatment strategies. © 2015 Orthopaedic Research Society. Published by Wiley Periodicals, Inc.

Viscoelastic Properties of Healthy Achilles Tendon are Independent of Isometric Plantar Flexion Strength and Cross-Sectional Area

PubMed Central

Suydam, Stephen M.; Soulas, Elizabeth M.; Elliott, Dawn M.; Silbernagel, Karin Gravare; Buchanan, Thomas S.; Cortes, Daniel H.

2015-01-01

Changes in tendon viscoelastic properties are observed after injuries and during healing as a product of altered composition and structure. Continuous Shear Wave Elastography is a new technique measuring viscoelastic properties of soft tissues using external shear waves. Tendon has not been studied with this technique, therefore, the aims of this study were to establish the range of shear and viscosity moduli in healthy Achilles tendons, determine bilateral differences of these parameters and explore correlations of viscoelasticity to plantar flexion strength and tendon area. Continuous Shear Wave Elastography was performed over the free portion of both Achilles tendons from 29 subjects. Isometric plantar flexion strength and cross sectional area were measured. The average shear and viscous moduli was 83.2kPa and 141.0Pa-s, respectively. No correlations existed between the shear or viscous modulus and area or strength. This indicates that viscoelastic properties can be considered novel, independent biomarkers. The shear and viscosity moduli were bilaterally equivalent (p=0.013,0.017) which allows determining pathologies through side-to-side deviations. The average bilateral coefficient of variation was 7.2% and 9.4% for shear and viscosity modulus, respectively. The viscoelastic properties of the Achilles tendon may provide an unbiased, non-subjective rating system of tendon recovery and optimizing treatment strategies. PMID:25882209

Effects of different black mediators on the shear strength of orthodontic bracket to the enamel treated with Nd-Yag laser

NASA Astrophysics Data System (ADS)

Huang, Shun-Te; Lin, I.-Shueng; Tsai, Chi-Cheng

1995-04-01

The Nd:YAG laser has ablation, crack, and crater effects on the dental enamel through black mediators which are very similar to the acid etching effects of phosphoric acid. This study was designed for searching how the different black mediators influence the shear strengths of the brackets bound to the enamel surfaces which were treated with the Nd:YAG laser. 90 bovine enamels divided into 5 groups were painted with 5 kinds of black mediators including Chinese ink, oil ink, black ball pen, water ink and black transfer paper. The enamel surfaces painted with black mediators were then radiated by Nd:YAG laser (ADL; American Dental Laser 300dl, power: 20 pps, 87.5 mj). Orthodontic brackets were bonded to the radiated surfaces. Then the shear strengths of the brackets to the enamels were measured by Instron. The results showed that the Chinese ink group and oil ink group has the strongest shear strength, ball pen group and water ink group showed the second strength, and the transfer paper group has the lowest shear strength. In addition, scanning electronic microscope also was used to observe the topographic changes of the enamel surfaces induced by the laser ablation.

Study of the strength of molybdenum under high pressure using electromagnetically applied compression-shear ramp loading

NASA Astrophysics Data System (ADS)

Ding, Jow; Alexander, C. Scott; Asay, James

2015-06-01

MAPS (Magnetically Applied Pressure Shear) is a new technique that has the potential to study material strength under mega-bar pressures. By applying a mixed-mode pressure-shear loading and measuring the resultant material responses, the technique provides explicit and direct information on material strength under high pressure. In order to apply sufficient shear traction to the test sample, the driver must have substantial strength. Molybdenum was selected for this reason along with its good electrical conductivity. In this work, the mechanical behavior of molybdenum under MAPS loading was studied. To understand the experimental data, a viscoplasticity model with tension-compression asymmetry was also developed. Through a combination of experimental characterization, model development, and numerical simulation, many unique insights were gained on the inelastic behavior of molybdenum such as the effects of strength on the interplay between longitudinal and shear stresses, potential interaction between the magnetic field and molybdenum strength, and the possible tension-compression asymmetry of the inelastic material response. Sandia National Labs is a multi-program laboratory managed and operated by Sandia Corporation, a wholly owned subsidiary of Lockheed Martin Corp., for the U.S. Dept. of Energy's National Nuclear Security Administration under Contract DE-AC04-94AL85000.

Controlled release in transdermal pressure sensitive adhesives using organosilicate nanocomposites.

PubMed

Shaikh, Sohel; Birdi, Anil; Qutubuddin, Syed; Lakatosh, Eric; Baskaran, Harihara

2007-12-01

Polydimethyl siloxane (PDMS) based pressure sensitive adhesives (PSA) incorporating organo-clays at different loadings were fabricated via solution casting. Partially exfoliated nanocomposites were obtained for the hydroxyl terminated PDMS in ethyl acetate solvent as determined by X-ray diffraction and atomic force microscopy. Drug release studies showed that the initial burst release was substantially reduced and the drug release could be controlled by the addition of organo-clay. Shear strength and shear adhesion failure temperature (SAFT) measurements indicated substantial improvement in adhesive properties of the PSA nanocomposite adhesives. Shear strength showed more than 200% improvement at the lower clay loadings and the SAFT increased by about 21% due to the reinforcement provided by the nano-dispersed clay platelets. It was found that by optimizing the level of the organosilicate additive to the polymer matrix, superior control over drug release kinetics and simultaneous improvements in adhesive properties could be attained for a transdermal PSA formulation.

Response of Damaged and Undamaged Tailored Extension-Shear-Coupled Composite Panels

NASA Technical Reports Server (NTRS)

Baker, Donald J.

2008-01-01

The results of an analytical and experimental investigation of the response of composite I-stiffener panels with extension-shear coupling are presented. This tailored concept, when used in the panel cover skins of a tiltrotor aircraft wing has the potential for increasing the aeroelastic stability margins and improving the aircraft productivity. The extension-shear coupling is achieved by using unbalanced plus or minus 45 deg. plies in the skin. Experimental and STAGS analysis results are compared for eight I-stiffener panel specimens. The results indicate that the tailored concept would be feasible to use in the wing skin of a tiltrotor aircraft. Evaluation of specimens impacted at an energy level of 500 in.-lbs indicate a minimal loss in stiffness and less than 30 percent loss in strength. Evaluation of specimens with severed center stiffener and adjacent skin indicated a strength loss in excess of 60 percent.

Effect of Diluent on Ultra-low Temperature Curable Conductive Silver Adhesive

NASA Astrophysics Data System (ADS)

Zhou, Xingli; Wang, Likun; Liao, Qingwei; Yan, Chao; Du, Haibo; Qin, Lei

2018-03-01

The ultra-low temperature curable conductive silver adhesive needed urgently for the surface conductive treatment of piezoelectric composite material. The effect of diluent acetone on ultra-low temperature curable conductive silver adhesive were investigated for surface conductive treatment of piezoelectric composite material. In order to improve the operability and extend the life of the conductive adhesive, the diluent was added to dissolve and disperse conductive adhesive. With the increase of the content of diluent, the volume resistivity of conductive adhesive decreased at first and then increased, and the shear strength increased at first and then decreased. When the acetone content is 10%, the silver flaky bonded together, arranged the neatest, the smallest gap, the most closely connected, the surface can form a complete conductive network, and the volume resistivity is 2.37 × 10-4Ω · cm, the shear strength is 5.13MPa.

Shear strength of fillet welds in aluminum alloy 2219. [for use on the solid rocket motor and external tank

NASA Technical Reports Server (NTRS)

Lovoy, C. V.

1978-01-01

Fillet size is discussed in terms of theoretical or design dimensions versus as-welded dimensions, drawing attention to the inherent conservatism in the design load sustaining capabilities of fillet welds. Emphasis is placed on components for the solid rocket motor, external tank, and other aerospace applications. Problems associated with inspection of fillet welds are addresses and a comparison is drawn between defect counts obtained by radiographic inspection and by visual examination of the fracture plane. Fillet weld quality is related linearly to ultimate shear strength. Correlation coefficients are obtained by simple straight line regression analysis between the variables of ultimate shear strength and accumulative discontinuity summation. Shear strength allowables are found to be equivalent to 57 percent of butt weld A allowables (F sub tu.)

Blanking Method with Aid of Scrap to Reduce Tensile Residual Stress on Sheared Edge

NASA Astrophysics Data System (ADS)

Yasutomi, T.; Yonemura, S.; Yoshida, T.; Mizumura, M.; Hiwatashi, S.

2017-09-01

A simple shearing method to reduce tensile residual stress on a sheared edge is highly desired in the automotive industry because this type of stress deteriorates the fatigue property of automotive parts. In this study, the effect of a coining method with a shearing scrap material on a sheared edge was investigated. The scrap part of a sheared plate has a fracture surface shape similar to that of the product part since these parts are generated by separation of a single plate with crack propagation. Therefore, it is possible to impose plastic strain over the entire fracture surface by using the scrap part as a coining tool. Effectiveness of this method was investigated for high-tensile-strength steel. Using this method, the tensile residual stress on the sheared surface was significantly reduced and work hardening was slightly increased. The effects of shearing clearance and coining stroke were also investigated. Tensile residual stress decreased as the coining stroke increased; however, it saturated at a certain stroke. The stroke at which tensile residual stress saturated was relatively small at a large clearance. In particular, the amount of plastic deformation on fracture surface increased when coining stroke became large. These tendencies could be explained by the conditions of contact, which were investigated using finite element analysis.

Evaluation of shear bond strength of porcelain bonded to laser welded titanium surface and determination of mode of bond failure.

PubMed

Patil, Narendra P; Dandekar, Minal; Nadiger, Ramesh K; Guttal, Satyabodh S

2010-09-01

The aim of this study was to evaluate the shear bond strength of porcelain to laser welded titanium surface and to determine the mode of bond failure through scanning electron microscopy (SEM) and energy dispersive spectrophotometry (EDS). Forty five cast rectangular titanium specimens with the dimension of 10 mm x 8 mm x 1 mm were tested. Thirty specimens had a perforation of 2 mm diameter in the centre. These were randomly divided into Group A and B. The perforations in the Group B specimens were repaired by laser welding using Cp Grade II titanium wire. The remaining 15 specimens were taken as control group. All the test specimens were layered with low fusing porcelain and tested for shear bond strength. The debonded specimens were subjected to SEM and EDS. Data were analysed with 1-way analysis of variance and Student's t-test for comparison among the different groups. One-way analysis of variance (ANOVA) showed no statistically significant difference in shear bond strength values at a 5% level of confidence. The mean shear bond strength values for control group, Group A and B was 8.4 +/- 0.5 Mpa, 8.1 +/- 0.4 Mpa and 8.3 +/- 0.3 Mpa respectively. SEM/EDS analysis of the specimens showed mixed and cohesive type of bond failure. Within the limitations of the study laser welding did not have any effect on the shear bond strength of porcelain bonded to titanium.

Effect of bromelain and papain gel on enamel deproteinisation before orthodontic bracket bonding.

PubMed

Pithon, Matheus Melo; Campos, Matheus Souza; Coqueiro, Raildo da Silva

2016-05-01

To test the hypothesis that enamel surface deproteinisation with different concentrations of bromelain in association with 10% papain increases the shear bond strength (SBS) of brackets bonded with orthodontic composite and resin modified glass ionomer cement (RMGIC). Orthodontic brackets were attached according to the following protocols to 195 bovine incisors, which were acquired and divided into 13 groups: 1) Transbond XT (TXT) according to the manufacturer's recommendations; 2) Deproteinisation with 3% bromelain (BD) plus 10% papain and TXT; 3) 6% BD plus 10% Papain and TXT; 4) RMGIC, without enamel deproteinisation and without acid etching; 5) RMGIC, with 3% BD plus 10% papain and without acid etching; 6) RMGIC, with 6% BD plus 10% papain and without acid etching; 7) attachment using RMGIC following etching with polyacrylic acid; 8) 3% BD plus 10% papain, attachment using RMGIC and etching with polyacrylic acid; 9) 6% BD plus 10% papain, and attachment using RMGIC following etching with polyacrylic acid; 10) etching with 37% phosphoric acid and attachment using RMGIC; 11) 3% BD plus 10% papain, etching with 37% phosphoric acid and attachment using RMGIC; 12) 6% BD plus 10% papain, etching with 37% phosphoric acid and attachment using RMGIC; 13) deproteinisation with 2.5% sodium hypochlorite (NaOCl), etching with polyacrylic acid and RMGIC. After bonding, the brackets were removed by a universal mechanical testing machine, which recorded shear bond strength at failure. The material remaining on the tooth was assessed using the adhesive remnant index (ARI). Deproteinisation with 3% and 6% bromelain gel plus papain significantly increased the shear bond strength (p < 0.05), when acid etching was performed with phosphoric acid, followed by primer application and attachment using Transbond XT (Group 3) and when attached with RMGIC without etching. Deproteinisation with 6% bromelain gel plus papain significantly increased (p < 0.05) the ARI score only when attachment was performed using RMGIC, without etching (Group 6). Deproteinisation with bromelain associated with papain in a gel increased the shear bond strength and is recommended before orthodontic bracket attachment.

Carboxyl functionalization of carbon fibers via aryl diazonium reaction in molten urea to enhance interfacial shear strength

NASA Astrophysics Data System (ADS)

Wang, Yuwei; Meng, Linghui; Fan, Liquan; Wu, Guangshun; Ma, Lichun; Zhao, Min; Huang, Yudong

2016-01-01

Using molten urea as the solvent, carbon fibers were functionalized with carboxylic acid groups via aryl diazonium reaction in 15 min to improve their interfacial bonding with epoxy resin. The surface functionalization was quantified by X-ray photoelectron spectroscopy, which showed that the relative surface coverage of carboxylic acid groups increased from an initial percentage of 3.17-10.41%. Mechanical property test results indicated that the aryl diazonium reaction in this paper could improve the interfacial shear strength by 66%. Meanwhile, the technique did not adopt any pre-oxidation step to produce functional groups prior to grafting and was shown to maintain the tensile strength of the fibers. This methodology provided a rapid, facile and economically viable route to produce covalently functionalized carbon fibers in large quantities with an eco-friendly method.

Influence of laser structuring of PEEK, PEEK-GF30 and PEEK-CF30 surfaces on the shear bond strength to a resin cement.

PubMed

Henriques, Bruno; Fabris, Douglas; Mesquita-Guimarães, Joana; Sousa, Anne C; Hammes, Nathalia; Souza, Júlio C M; Silva, Filipe S; Fredel, Márcio C

2018-08-01

The aim of this study was to evaluate the influence of a surface conditioning technique using laser ablation and acid etching on PEEK substrate on its bonding strength to a resin cement. Cylindrical specimens of unfilled PEEK, 30% glass fiber reinforced PEEK and 30% carbon fiber reinforced PEEK were separated in four groups according to the following surface treatments: acid etching with H 2 SO 4 , laser ablation with 200 µm holes spaced 400 µm apart (D2E4), laser ablation with 200 µm holes spaced 600 µm apart (D2E6), and laser ablation (D2E4) followed by acid etching. A dual-curing resin cement (Allcem CORE) was then applied to the PEEK surface. Specimens were aged in distilled water at 37 °C for 24 h. Shear bond strength tests were performed to the fracture of the samples. Two-way ANOVA statistical analysis was performed with a significance level of 0.05. Scanning electron microscopy analysis was performed to analyse the conditioned and fracture surfaces. SEM images of the test interfaces showed that the resin cement could not flow in the holes designed by the laser ablation on the PEEK surface. The shear bond strength of PEEK to resin cement was not improved by the surface modification of the PEEK. Also, there was a statistically significant decrease in shear bond strength for unfilled PEEK specimens. On carbon or glass reinforced PEEK, the change was not significant. SEM images of the fracture surfaces revealed that the failure mode was mainly adhesive. Although laser ablation promoted the PEEK surface modification by the formation of retentive holes, the test resin cement could not thoroughly flow on the rough modified surfaces to establish an effective mechanical interlocking. That negatively affected the shear bonding strength of PEEK to the resin cement. Further studies should be carried out to increase the bonding between PEEK and resin cements. Copyright © 2018 Elsevier Ltd. All rights reserved.

Evaluation of the effect of three innovative recyling methods on the shear bond strength of stainless steel brackets-an in vitro study.

PubMed

Gupta, Neeraj; Kumar, Dilip; Palla, Aparna

2017-04-01

Orthodontists are commonly faced with the decision of what to do with debonded or inaccurately positioned brackets. An economical option to this dilemma is to recycle the brackets. Many recycling methods have been proposed, but the optimal bond strength of these recycled brackets needs further evaluation. Objectives: To evaluate and compare the effect of three recycling methods: (i) Sandblasting (ii) Sandblasting / direct flaming (iii) Sandblasting /direct flaming /acid bath solution on shear bond strength (SBS) of stainless steel brackets. Eighty human premolars were bonded with premolar stainless steel brackets as per manufacturer's instructions. The teeth were divided into 4 groups (n=20): Recycling and initial debonding was not done in Control group (Group I). After initial bonding, the brackets in the rest of the three experimental groups were debonded and recycled by following methods: (i) Sandblasting (Group II) (ii) Sandblasting /direct flaming (Group III) (iii) Sandblasting /direct flaming /acid bath solution (Group IV). Further the recycled brackets were bonded. The specimens were then subjected to testing in a Universal machine. The evaluation of the variation of the shear bond strength (SBS) among test groups was done using one-way ANOVA test and inter-experimental group comparison was done by Newman-Keuls multiple post hoc procedure. Group I (8.6510±1.3943MPa) showed the highest bond strength followed by Group II (5.0185±0.9758MPa), Group IV (2.30±0.65MPa) and Group III (2.0455± 0.6196MPa). Statistically significant variations existed in the shear bond strength (SBS) in all groups analyzed except between Group III and Group IV. The following conclusions were drawn from the study: 1. Shear bond strength of new brackets is significantly higher than the recycled brackets. 2. Brackets sandblasted with 90µm aluminium oxide particle air-abrasion showed significantly higher shear bond strength compared to direct flaming/sandblasting and direct flaming/sandblasting/acid bath solution. 3. Sandblasting with 90µm aluminium oxide particle air-abrasion is the simplest, most efficient and hence, the preferred method of recycling debonded brackets. Key words: Orthodontic bracket, recycling, shear bond strength.

Evaluation of agglutination strength by a flow-induced cell movement assay based surface plasmon resonance (SPR) technique.

PubMed

Sudprasert, Krisda; Peungthum, Patjaree; Vongsakulyanon, Apirom; Amarit, Ratthasart; Somboonkaew, Armote; Sutapun, Boonsong; Kitpoka, Pimpun; Kunakorn, Mongkol; Srikhirin, Toemsak

2015-02-07

A flow-induced cell movement assay combined with a surface plasmon resonance (SPR) technique was developed to quantify the agglutination strength, derived from the standard tube-agglutination test. Red blood cells (RBCs), based on the ABO blood group system, were specifically captured by anti-A and/or anti-B antibodies immobilized on a sensor surface. The agglutination strength corresponds to the amount of antigen-antibody interactions or the strength of RBC adhesion. Under a shear flow, the adherent RBCs were forced to move out of the region of interest with different average cell velocities (vc) depending upon the adhesion strength and wall shear stress (WSS). That is, a higher adhesion strength (higher agglutination strength) or lower WSS represents a lower vc or vice versa. In this work, the agglutination strength was derived from the vc that was calculated from the time derivative of the relative SPR signal by using a simple model of cell movement response, whose validity was verified. The vc values of different samples were correlated with their agglutination strengths at a given WSS and antibody surface density. The vc decreased as the agglutination strength increased, which can be considered as a linear regression. The coefficient of variation of the calculated vc decreased to 0.1 as vc increased to 30 μm min(-1). The sensitivity of this assay can be controlled by optimizing the antibody surface density or the WSS. This assay has the capability to resolve the antigen density of A1 and B RBCs from that of A1B RBCs.

Experimental Investigation on the Joining of Aluminum Alloy Sheets Using Improved Clinching Process.

PubMed

Chen, Chao; Zhao, Shengdun; Han, Xiaolan; Zhao, Xuzhe; Ishida, Tohru

2017-08-01

Aluminum alloy sheets have been widely used to build the thin-walled structures by mechanical clinching technology in recent years. However, there is an exterior protrusion located on the lower sheet and a pit on the upper sheet, which may restrict the application of the clinching technology in visible areas. In the present study, an improved clinched joint used to join aluminum alloy sheets was investigated by experimental method. The improved clinching process used for joining aluminum alloy evolves through four phases: (a) localized deformation; (b) drawing; (c) backward extrusion; and (d) mechanical interlock forming. A flat surface can be produced using the improved clinching process. Shearing strength, tensile strength, material flow, main geometrical parameters, and failure mode of the improved clinched joint were investigated. The sheet material was compressed to flow radially and upward using a punch, which generated a mechanical interlock by producing severe localized plastic deformation. The neck thickness and interlock of the improved clinched joint were increased by increasing the forming force, which also contributed to increase the strength of the clinched joint. The improved clinched joint can get high shearing strength and tensile strength. Three main failure modes were observed in the failure process, which were neck fracture mode, button separation mode, and mixed failure mode. The improved clinched joint has better joining quality to join aluminum alloy sheets on the thin-walled structures.

Experimental Investigation on the Joining of Aluminum Alloy Sheets Using Improved Clinching Process

PubMed Central

Chen, Chao; Zhao, Shengdun; Han, Xiaolan; Zhao, Xuzhe; Ishida, Tohru

2017-01-01

Aluminum alloy sheets have been widely used to build the thin-walled structures by mechanical clinching technology in recent years. However, there is an exterior protrusion located on the lower sheet and a pit on the upper sheet, which may restrict the application of the clinching technology in visible areas. In the present study, an improved clinched joint used to join aluminum alloy sheets was investigated by experimental method. The improved clinching process used for joining aluminum alloy evolves through four phases: (a) localized deformation; (b) drawing; (c) backward extrusion; and (d) mechanical interlock forming. A flat surface can be produced using the improved clinching process. Shearing strength, tensile strength, material flow, main geometrical parameters, and failure mode of the improved clinched joint were investigated. The sheet material was compressed to flow radially and upward using a punch, which generated a mechanical interlock by producing severe localized plastic deformation. The neck thickness and interlock of the improved clinched joint were increased by increasing the forming force, which also contributed to increase the strength of the clinched joint. The improved clinched joint can get high shearing strength and tensile strength. Three main failure modes were observed in the failure process, which were neck fracture mode, button separation mode, and mixed failure mode. The improved clinched joint has better joining quality to join aluminum alloy sheets on the thin-walled structures. PMID:28763027

A cross-shear deformation for optimizing the strength and ductility of AZ31 magnesium alloys

PubMed Central

Hamad, Kotiba; Ko, Young Gun

2016-01-01

Magnesium alloys have recently attracted great interest due their lightweight and high specific strength. However, because of their hexagonal close-packed structure, they have few active slip systems, resulting in poor ductility and high mechanical anisotropy at room temperature. In the present work, we used a cross-shear deformation imposed by a differential speed rolling (DSR) technique to improve the room temperature strength and ductility of AZ31 magnesium alloy sheets. To introduce the cross-shear deformation, the sheets were rotated 180° around their longitudinal axis between the adjacent passes of DSR. The sheets of the AZ31 alloy subjected to the cross-shear deformation showed a uniform fine microstructure (1.2 ± 0.1 μm) with weak basal textures. The fabricated sheets showed a simultaneous high ultimate tensile strength and elongation-to-failure, i.e., ~333 MPa and ~21%, respectively. These were explained based on the structural features evolved due to the cross-shear deformation by DSR. The high strength was attributed to the uniform fine microstructure, whereas the high ductility was explained based on the basal texture weakening. PMID:27406685

[Effects of different surface treatments on the zirconia-resin cement bond strength].

PubMed

Liao, Y; Liu, X Q; Chen, L; Zhou, J F; Tan, J G

2018-02-18

To evaluate the effects of different surface treatments on the shear bond strength between zirconia and resin cement. Forty zirconia discs were randomly divided into four groups (10 discs in each group) for different surface treatments: control, no surface treatment; sandblast, applied air abrasion with aluminum oxide particles; ultraviolet (UV), the zirconia sample was placed in the UV sterilizer at the bottom of the UV lamp at 10 mm, and irradiated for 48 h; cold plasma, the discs were put in the cold plasma cabinet with the cold plasma generated from the gas of He for 30 s. Specimens of all the groups were surface treated prior to cementation with Panavia F 2.0 cement. The surface morphology and contact angle of water were measured. The shear bond strengths were tested and the failure modes were examined with a stereomicroscope. Surface morphology showed no difference between the UV/cold plasma group and the control group. Sandblasted zirconia displayed an overall heterogeneous distribution of micropores. The contact angle of the control group was 64.1°±2.0°. After sandblasting, UV irradiation and cold plasma exposure, the values significantly decreased to 48.8°±2.6°, 27.1°±3.6° and 32.0°±3.3°. The values of shear bond strength of the specimens with sandblasted (14.82±2.01) MPa were higher than those with no treatment (9.41±1.07) MPa with statistically significant difference (P<0.05). The values of shear bond strength of the specimens with UV irradiation (10.02±0.64) MPa were higher than those with no treatment (9.41±1.07) MPa, but without statistically significant difference (P>0.05). The values of cold plasma group (18.34±3.05) MPa were significantly higher than those of control group (9.41±1.07) MPa, even more than those with sandblast(14.82±2.01) MPa (P<0.05). X-ray photoelectron spectroscopy (XPS) showed increase in oxygen (O) and decrease in carbon (C) elements after UV and cold plasma treatment. The surface C/O ratio also decreased after UV and cold plasma treatment. Zirconia specimens treated with UV and cold plasma could significantly improve the hydrophilicity. The surface morphology was unaffected by the UV irradiation and cold plasma treatments. The improvements of ziconia shear bond strength were slight in UV group without statistically significant difference. Cold plasma treatment significantly improved the shear bond strength between zirconia and resin cement.

The Effect on Final Bond Strength of Bracket Manipulation Subsequent To Initial Positioning

NASA Astrophysics Data System (ADS)

Beebe, David A.

The shear bond strength of light activated orthodontic adhesives varies according to the composition of the material, placement protocol, and time prior to light curing. Manipulating brackets after their initial placement on a tooth can disrupt the adhesive's polymerization and compromise final bond strength. No previous research has investigated how a specific degree of manipulation, and the amount of time elapsed prior to curing, under specific lighting conditions, affects the orthodontic adhesives shear bond strength. Victory SeriesRTM, MBT prescription, premolar (3M Unitek, Monrovia, CA) orthodontic brackets were bonded using three different adhesives to sixty (60) bicuspids and varying the time after bracket manipulation before curing. The shear bond strength was calculated for each specimen. The brackets were debonded and the same teeth were rebonded with new, identical brackets, using the same protocol and under the same conditions. The results showed a statistically significant difference between the shear bond strength of Transbond XT and Grengloo, with Transbond XT having the highest strength. There was also a statistically significance difference in bond strength between the group cured 30 seconds after manipulation and the groups manipulated at different intervals prior to curing, with the 30 second group having the highest bond strength. This study confirms that various orthodontic adhesives have different bond strengths depending on manipulation and varying times prior to curing each adhesive.

Behaviour of Cohesionless Soil Reinforced with Three Dimensional Inclusions Under Plane Strain Conditions

NASA Astrophysics Data System (ADS)

Harikumar, M.; Sankar, N.; Chandrakaran, S.

2015-09-01

Since 1969, when the concept of earth reinforcing was brought about by Henry Vidal, a large variety of materials such as steel bars, tire shreds, polypropylene, polyester, glass fibres, coir and jute fibres etc. have been widely added to soil mass randomly or in a regular, oriented manner. The conventional reinforcements in use were two dimensional or planar, in the form of strips with negligible widths or in the form of sheets. In this investigation, a novel concept of multi oriented plastic reinforcement (hexa-pods) is discussed. Direct shear tests were conducted on unreinforced and reinforced dry fine, medium and coarse sands. Detailed parametric studies with respect to the effective grain size of soil (d10), normal stress (σ) and the volume ratio of hexa-pods (Vr) were performed. It was noticed that addition of hexa-pods resulted in increase in the shear strength parameters viz. peak deviatoric stresses and increased angle of internal friction. The hexa-pods also changed the brittle behaviour of unreinforced sand samples to ductile ones. Although the peak shear stress did not show a considerable improvement, the angle of internal friction improved noticeably. Addition of a single layer of reinforcement along the shear plane also reduced the post peak loss of strength and changed the soil behavior from brittle to a ductile one.

Effect of Various Laser Surface Treatments on Repair Shear Bond Strength of Aged Silorane-Based Composite

PubMed Central

Alizadeh Oskoee, Parnian; Savadi Oskoee, Siavash; Rikhtegaran, Sahand; Pournaghi-Azar, Fatemeh; Gholizadeh, Sarah; Aleyasin, Yasaman; Kasrae, Shahin

2017-01-01

Introduction: Successful repair of composite restorations depends on a strong bond between the old composite and the repair composite. This study sought to assess the repair shear bond strength of aged silorane-based composite following surface treatment with Nd:YAG, Er,Cr:YSGG and CO2 lasers. Methods: Seventy-six Filtek silorane composite cylinders were fabricated and aged by 2 months of water storage at 37°C. The samples were randomly divided into 4 groups (n=19) of no surface treatment (group 1) and surface treatment with Er,Cr:YSGG (group 2), Nd:YAG (group 3) and CO2 (group 4) lasers. The repair composite was applied and the shear bond strength was measured. The data were analyzed using one-way analysis of variance (ANOVA) and Tukey posthoc test. Prior to the application of the repair composite, 2 samples were randomly selected from each group and topographic changes on their surfaces following laser irradiation were studied using a scanning electron microscope (SEM). Seventeen other samples were also fabricated for assessment of cohesive strength of composite. Results: The highest and the lowest mean bond strength values were 8.99 MPa and 6.69 MPa for Er,Cr:YSGG and control groups, respectively. The difference in the repair bond strength was statistically significant between the Er,Cr:YSGG and other groups. Bond strength of the control, Nd:YAG and CO2 groups was not significantly different. The SEM micrographs revealed variable degrees of ablation and surface roughness in laser-treated groups. Conclusion: Surface treatment with Er,Cr:YSGG laser significantly increase the repair bond strength of aged silorane-based composite resin. PMID:29071025

Shear joint capability versus bolt clearance

NASA Technical Reports Server (NTRS)

Lee, H. M.

1992-01-01

The results of a conservative analysis approach into the determination of shear joint strength capability for typical space-flight hardware as a function of the bolt-hole clearance specified in the design are presented. These joints are comprised of high-strength steel fasteners and abutments constructed of aluminum alloys familiar to the aerospace industry. A general analytical expression was first arrived at which relates bolt-hole clearance to the bolt shear load required to place all joint fasteners into a shear transferring position. Extension of this work allowed the analytical development of joint load capability as a function of the number of fasteners, shear strength of the bolt, bolt-hole clearance, and the desired factor of safety. Analysis results clearly indicate that a typical space-flight hardware joint can withstand significant loading when less than ideal bolt hole clearances are used in the design.

Effect of laser welding on the titanium composite tensile bond strength.

PubMed

Galo, Rodrigo; Ribeiro, Ricardo Faria; Rodrigues, Renata Cristina Silveira; Pagnano, Valéria de Oliveira; de Mattos, Maria da Glória Chiarello

2009-01-01

The aim of this study was to analyze the shear bond strength between commercially pure titanium, with and without laser welding, after airbone-particle abrasion (Al(2)O(3)) and 2 indirect composites. Sixty-four specimens were cast and divided into 2 groups with and without laser welding. Each group was divided in 4 subgroups, related to Al(2)O(3) grain size: A - 250 microm; B - 180 microm; C- 110 microm; and D - 50 microm. Composite rings were formed around the rods and light polymerized using UniXS unit. Specimens were invested and their shear bond strength at failure was measured with a universal testing machine at a crosshead speed of 2.0 mm/min. Statistical analysis was carried out with ANOVA and Tukey's test (alpha=0.05). The highest bond strength means were recorded in 250 microm group without laser welding. The lowest shear bond strength means were recorded in 50 microm group with laser welding. Statistically significant differences (p<0.05) were found between all groups. In conclusion, airborne particle abrasion yielded significantly lower bond strength as the Al(2)O(3) particle size decreased. Shear bond strength decreased in the laser welded specimens.

Shear bond strength of a new one-bottle dentin adhesive.

PubMed

Swift, E J; Bayne, S C

1997-08-01

To test the shear bond strength of a new adhesive, 3M Single Bond, to dentin surfaces containing different degrees of moisture. Two commercially available one-bottle adhesives (Prime & Bond, One-Step) and a conventional three-step system (Scotchbond Multi-Purpose Plus) were included for comparison. 120 bovine teeth were embedded in acrylic and the labial surfaces were polished to 600 grit to create standardized dentin surfaces for testing. Resin composite was bonded to dentin using a gelatin capsule technique. Four adhesive systems were evaluated with three different degrees of surface moisture (moist, wet, and overwet). Shear bond strengths of adhesives to dentin were determined using a universal testing machine and analyzed by ANOVA and Tukey's post hoc tests. Single Bond had mean shear bond strengths of 19.2, 23.2 and 20.3 MPa to moist, wet, and overwet dentin, respectively. Bond strengths of the three-component system Scotchbond Multi-Purpose Plus ranged from 23.1 to 25.3 MPa, but were not significantly higher than the values for Single Bond. Prime & Bond had bond strengths similar to those of Single Bond, but One-Step had significantly lower bond strengths (P < 0.05) in the wet and overwet conditions.

Shear Bond Strength of Orthodontic Brackets and Disinclusion Buttons: Effect of Water and Saliva Contamination

PubMed Central

Sfondrini, Maria Francesca; Fraticelli, Danilo; Gandini, Paola

2013-01-01

Purpose. The aim of this study was to assess the effect of water and saliva contamination on the shear bond strength and failure site of orthodontic brackets and lingual buttons. Materials and Methods. 120 bovine permanent mandibular incisors were randomly divided into 6 groups of 20 specimens each. Both orthodontic brackets and disinclusion buttons were tested under three different enamel surface conditions: (a) dry, (b) water contamination, and (c) saliva contamination. Brackets and buttons were bonded to the teeth and subsequently tested using a Instron universal testing machine. Shear bond strength values and adhesive failure rate were recorded. Statistical analysis was performed using ANOVA and Tukey tests (strength values) and Chi squared test (ARI Scores). Results. Noncontaminated enamel surfaces showed the highest bond strengths for both brackets and buttons. Under water and saliva contamination orthodontic brackets groups showed significantly lower shear strengths than disinclusion buttons groups. Significant differences in debond locations were found among the groups under the various enamel surface conditions. Conclusions. Water and saliva contamination of enamel during the bonding procedure lowers bond strength values, more with orthodontic brackets than with disinclusion buttons. PMID:23762825

First-principles comparative study on the interlayer adhesion and shear strength of transition-metal dichalcogenides and graphene

NASA Astrophysics Data System (ADS)

Levita, Giacomo; Molinari, Elisa; Polcar, Tomas; Righi, Maria Clelia

2015-08-01

Due to their layered structure, graphene and transition-metal dichalcogenides (TMDs) are easily sheared along the basal planes. Despite a growing attention towards their use as solid lubricants, so far no head-to-head comparison has been carried out. By means of ab initio modeling of a bilayer sliding motion, we show that graphene is characterized by a shallower potential energy landscape while more similarities are attained when considering the sliding forces; we propose that the calculated interfacial ideal shear strengths afford the most accurate information on the intrinsic sliding capability of layered materials. We also investigate the effect of an applied uniaxial load: in graphene, this introduces a limited increase in the sliding barrier while in TMDs it has a substantially different impact on the possible polytypes. The polytype presenting a parallel orientation of the layers (R 0 ) bears more similarities to graphene while that with antiparallel orientation (R 180 ) shows deep changes in the potential energy landscape and consequently a sharper increase of its sliding barrier.

Bond strengths of Scotchbond Multi-Purpose to moist dentin and enamel.

PubMed

Swift, E J; Triolo, P T

1992-12-01

This in vitro study tested the shear bond strengths of the Scotchbond Multi-Purpose adhesive system to moist and dry enamel and dentin. After the tooth was etched, the surface was either dried with compressed air or blotted with tissue paper, leaving the surface visibly moist. Primer and adhesive were applied according to the manufacturer's directions. Resin composite posts were applied, and the specimens were thermocycled. Shear bond strengths were determined using an Instron universal testing machine. For both enamel and dentin, mean shear bond strengths were higher when the surface was left visibly moist after etching. Bond strengths to moist and dry dentin were 21.8 and 17.8 MPa, respectively. Enamel bond strengths were slightly lower, with values of 17.0 and 14.2 MPa to moist and dry enamel, respectively.

Effects of oxygen plasma treatment power on Aramid fiber III/BMI composite humidity resistance properties

NASA Astrophysics Data System (ADS)

Wang, Jing; Shi, Chen; Feng, Jiayue; Long, Xi; Meng, Lingzhi; Ren, Hang

2018-01-01

The effects of oxygen plasma treatment power on Aramid Fiber III chemical structure and its reinforced bismaleimides (BMI) composite humidity resistance properties were investigated in this work. The aramid fiber III chemical structure under different plasma treatment power were measured by FTIR. The composite bending strength and interlinear shear strength with different plasma treatment power before and after absorption water were tested respectively. The composite rupture morphology was observed by SEM. The FTIR results showed that oxygen plasma treatment do not change the fiber bulk chemical structure. The composite humidity resistance of bending strength and interlinear shear strength are similar for untreated and plasma treated samples. The retention rate of composite bending strength and interlinear shear strength are about 75% and 94%, respectively. The composite rupture mode turns to be the fiber failure after water absorption.

Comparison of hydroxyapatite and dental enamel for testing shear bond strengths.

PubMed

Imthiaz, Nishat; Georgiou, George; Moles, David R; Jones, Steven P

2008-05-01

To investigate the feasibility of using artificial hydroxyapatite as a future biomimetic laboratory substitute for human enamel in orthodontic bond strength testing by comparing the shear bond strengths and nature of failure of brackets bonded to samples of hydroxyapatite and enamel. One hundred and fifty hydroxyapatite discs were prepared by compression at 20 tons and fired in a furnace at 1300 degrees C. One hundred and five enamel samples were prepared from the buccal and palatal/lingual surfaces of healthy premolars extracted for orthodontic purposes. Orthodontic brackets were bonded to each sample and these were subjected to shear bond strength testing using a custom-made jig mounted in an Instron Universal Testing Machine. The force value at bond failure was obtained, together with the nature of failure which was assessed using the Adhesive Remnant Index. The mean shear bond strength for the enamel samples was 16.62 MPa (95 per cent CI: 15.26, 17.98) and for the hydroxyapatite samples 20.83 MPa (95 per cent CI: 19.68, 21.98). The difference between the two samples was statistically significant (p < 0.001). When the nature of failure was assessed with the ARI Index, 83 per cent of the enamel samples scored 2 or 3, while 49 per cent of the hydroxyapatite samples scored 0 or 1. Hydroxyapatite was an effective biomimetic substrate for bond strength testing with a mean shear bond strength value (20.83 MPa) at the upper end of the normal range attributed to enamel (15-20 MPa). Although the difference between the shear bond strengths for hydroxyapatite and enamel was statistically significant, hydroxyapatite could be used as an alternative to enamel for comparative laboratory studies until a closer alternative is found. This would eliminate the need for extracted teeth to be collected. However, it should be used with caution for quantitative studies where true bond strengths are to be investigated.

Wind Shear Identification with the Retrieval Wind of Doppler Wearth Radar

NASA Astrophysics Data System (ADS)

Zhou, S.; Cui, Y.; Zheng, H.; Zhang, T.

2018-05-01

A new method, which based on the wind field retrieval algorithm of Volume Velocity Process (VVP), has been used to identified the intensity of wind shear occurred in a severe convection process in Guangzhou. The intensity of wind shear's strength shown that new cells would be more likely to generate in areas where the magnitude generally larger than 3.0 m/(s*km). Moreover, in the areas of potential areas of rainfall, the wind shear's strength would larger than 4.5 m/(s*km). This wind shear identify method is very helpful to forecasting severe convections' moving and developments.

Effect of adding powder on joint properties of laser penetration welding for dual phase steel and aluminum alloy

NASA Astrophysics Data System (ADS)

Zhou, D. W.; Liu, J. S.; Lu, Y. Z.; Xu, S. H.

2017-09-01

The experiments of laser penetration welding for dual phase steel and aluminum alloy were carried out, and the effect of adding Mn or Si powder on mechanical properties and microstructure of the weld was investigated. Some defects, such as spatter, inclusion, cracks and softening in heat affected zone (HAZ), can be avoided in welding joints, and the increased penetration depth is obtained by adding Mn or Si powder. The average tensile-shear strength of Si-added joint is 3.84% higher than that of Mn-added joint, and the strength of both joints exceeds that of no-added joint. In the case of adding Mn powder, small amount of liquid Al is mixed into steel molten pool, and the Al content increases in both sides of the weld, which leads to the increased weld width in aluminum molten pool. Thus, transverse area increases in jointing steel to aluminum, which is significant for the improved tensile-shear strength of joints. As far as adding Si powder is concerned, it is not the case, the enhancement of the joint properties benefits from improvement of metallurgical reaction.

Effect of EDTA and phosphoric Acid pretreatment on the bonding effectiveness of self-etch adhesives to ground enamel.

PubMed

Ibrahim, Ihab M; Elkassas, Dina W; Yousry, Mai M

2010-10-01

This in vitro study determined the effect of enamel pretreatment with phosphoric acid and ethylenediaminetetraacetic acid (EDTA) on the bond strength of strong, intermediary strong, and mild self-etching adhesive systems. Ninety sound human premolars were used. Resin composite cylinders were bonded to flat ground enamel surfaces using three self-etching adhesive systems: strong Adper Prompt L-Pop (pH=0.9-1.0), intermediary strong AdheSE (pH=1.6-1.7), and mild Frog (pH=2). Adhesive systems were applied either according to manufacturer instructions (control) or after pretreatment with either phosphoric acid or EDTA (n=10). After 24 hours, shear bond strength was tested using a universal testing machine at a cross-head speed of 0.5 mm/minute. Ultra-morphological characterization of the surface topography and resin/enamel interfaces as well as representative fractured enamel specimens were examined using scanning electron microscopy (SEM). Neither surface pretreatment statistically increased the mean shear bond strength values of either the strong or the intermediary strong self-etching adhesive systems. However, phosphoric acid pretreatment significantly increased the mean shear bond strength values of the mild self-etching adhesive system. SEM examination of enamel surface topography showed that phosphoric acid pretreatment deepened the same etching pattern of the strong and intermediary strong adhesive systems but converted the irregular etching pattern of the mild self-etching adhesive system to a regular etching pattern. SEM examination of the resin/enamel interface revealed that deepening of the etching pattern was consistent with increase in the length of resin tags. EDTA pretreatment had a negligible effect on ultra-morphological features. Use of phosphoric acid pretreatment can be beneficial with mild self-etching adhesive systems for bonding to enamel.

Effect of EDTA and Phosphoric Acid Pretreatment on the Bonding Effectiveness of Self-Etch Adhesives to Ground Enamel

PubMed Central

Ibrahim, Ihab M.; Elkassas, Dina W.; Yousry, Mai M.

2010-01-01

Objectives: This in vitro study determined the effect of enamel pretreatment with phosphoric acid and ethylenediaminetetraacetic acid (EDTA) on the bond strength of strong, intermediary strong, and mild self-etching adhesive systems. Methods: Ninety sound human premolars were used. Resin composite cylinders were bonded to flat ground enamel surfaces using three self-etching adhesive systems: strong Adper Prompt L-Pop (pH=0.9–1.0), intermediary strong AdheSE (pH=1.6–1.7), and mild Frog (pH=2). Adhesive systems were applied either according to manufacturer instructions (control) or after pretreatment with either phosphoric acid or EDTA (n=10). After 24 hours, shear bond strength was tested using a universal testing machine at a cross-head speed of 0.5 mm/minute. Ultra-morphological characterization of the surface topography and resin/enamel interfaces as well as representative fractured enamel specimens were examined using scanning electron microscopy (SEM). Results: Neither surface pretreatment statistically increased the mean shear bond strength values of either the strong or the intermediary strong self-etching adhesive systems. However, phosphoric acid pretreatment significantly increased the mean shear bond strength values of the mild self-etching adhesive system. SEM examination of enamel surface topography showed that phosphoric acid pretreatment deepened the same etching pattern of the strong and intermediary strong adhesive systems but converted the irregular etching pattern of the mild self-etching adhesive system to a regular etching pattern. SEM examination of the resin/enamel interface revealed that deepening of the etching pattern was consistent with increase in the length of resin tags. EDTA pretreatment had a negligible effect on ultra-morphological features. Conclusions: Use of phosphoric acid pretreatment can be beneficial with mild self-etching adhesive systems for bonding to enamel. PMID:20922162

Improved failure prediction in forming simulations through pre-strain mapping

NASA Astrophysics Data System (ADS)

Upadhya, Siddharth; Staupendahl, Daniel; Heuse, Martin; Tekkaya, A. Erman

2018-05-01

The sensitivity of sheared edges of advanced high strength steel (AHSS) sheets to cracking during subsequent forming operations and the difficulty to predict this failure with any degree of accuracy using conventionally used FLC based failure criteria is a major problem plaguing the manufacturing industry. A possible method that allows for an accurate prediction of edge cracks is the simulation of the shearing operation and carryover of this model into a subsequent forming simulation. But even with an efficient combination of a solid element shearing operation and a shell element forming simulation, the need for a fine mesh, and the resulting high computation time makes this approach not viable from an industry point of view. The crack sensitivity of sheared edges is due to work hardening in the shear-affected zone (SAZ). A method to predict plastic strains induced by the shearing process is to measure the hardness after shearing and calculate the ultimate tensile strength as well as the flow stress. In combination with the flow curve, the relevant strain data can be obtained. To eliminate the time-intensive shearing simulation necessary to obtain the strain data in the SAZ, a new pre-strain mapping approach is proposed. The pre-strains to be mapped are, hereby, determined from hardness values obtained in the proximity of the sheared edge. To investigate the performance of this approach the ISO/TS 16630 hole expansion test was simulated with shell elements for different materials, whereby the pre-strains were mapped onto the edge of the hole. The hole expansion ratios obtained from such pre-strain mapped simulations are in close agreement with the experimental results. Furthermore, the simulations can be carried out with no increase in computation time, making this an interesting and viable solution for predicting edge failure due to shearing.

Recycling stainless steel orthodontic brackets with Er:YAG laser - An environmental scanning electron microscope and shear bond strength study.

PubMed

Chacko, Prince K; Kodoth, Jithesh; John, Jacob; Kumar, Kishore

2013-07-01

TO DETERMINE THE EFFICIENCY OF ERBIUM: Yttrium aluminum garnet (Er:YAG) laser with Environmental Scanning Electron Microscope (ESEM) and shear bond strength analysis as a method of recycling stainless steel orthodontic brackets and compare with other methods of recycling. Eighty samples of extracted premolar teeth bonded to SS brackets were tested for rebonded shear bond strength after recycling by four methods and compared with a control group of 20 samples. These 80 samples were randomized into four groups which were recycled by four methods, namely, sandblasting, thermal method, adhesive grinding by tungsten carbide bur, and Er: YAG laser method. After recycling, ESEM and shear bond strength analysis were used to analyze the efficiency of the recycling methods. ER: YAG laser group was found to be having the greatest bond strength among the recycled brackets (8.33±2.51 followed by the sandblasting at 6.12±1.12 MPa, thermal and electropolishing at 4.44±0.95 MPa, and lastly the adhesive grinding method at 3.08±1.07 MPa. The shear bond strength of Er: YAG laser group was found to be having no statistically significant difference with that of the control group (P>0.05 and had statistical signifance with sandblasting, thermal and electropolishing and adhesive grinding groups at P>0.001. ESEM analysis showed complete removal of adhesive from the brackets recycled with Er: YAG laser which mimicked that of the control group. ER: YAG laser (2940 nm) was found to be the most efficient method for recycling, followed by the sandblasting, thermal, and the tungsten carbide methods, which had the least shear bond strength value and is not fit for clinical usage.

Surface topography and bond strengths of feldspathic porcelain prepared using various sandblasting pressures.

PubMed

Moravej-Salehi, Elham; Moravej-Salehi, Elahe; Valian, Azam

2016-11-01

The purpose of this study was to determine the bond strength of composite resin to feldspathic porcelain and its surface topography after sandblasting at different pressures. In this in vitro study, 68 porcelain disks were fabricated and randomly divided into four groups of 17. The porcelain surface in group 1 was etched with hydrofluoric acid. Groups 2, 3, and 4 were sandblasted at 2, 3 and 4 bars pressure, respectively. Surface topography of seven samples in each of the four groups was examined by a scanning electron microscope (SEM). The remaining 40 samples received the same silane agent, bonding agent, and composite resin and they were then subjected to 5000 thermal cycles and evaluated for shear bond strength. Data were analyzed using one-way anova. The mode of failure was determined using stereomicroscope and SEM. The highest shear bond strength was seen in group 4. however, statistically significant differences were not seen between the groups (P = 0.780). The most common mode of failure was cohesive in porcelain. The SEM showed different patterns of hydrofluoric acid etching and sandblasting. Increasing the sandblasting pressure increased the surface roughness of feldspathic porcelain but no difference in bond strength occurred. © 2015 Wiley Publishing Asia Pty Ltd.

Effect of yield curves and porous crush on hydrocode simulations of asteroid airburst

NASA Astrophysics Data System (ADS)

Robertson, D. K.; Mathias, D. L.

2017-03-01

Simulations of asteroid airburst are being conducted to obtain best estimates of damage areas and assess sensitivity to variables for asteroid characterization and mitigation efforts. The simulations presented here employed the ALE3D hydrocode to examine the breakup and energy deposition of asteroids entering the Earth's atmosphere, using the Chelyabinsk meteor as a test case. This paper examines the effect of increasingly complex material models on the energy deposition profile. Modeling the meteor as a rock having a single strength can reproduce airburst altitude and energy deposition reasonably well but is not representative of real rock masses (large bodies of material). Accounting for a yield curve that includes different tensile, shear, and compressive strengths shows that shear strength determines the burst altitude. Including yield curves and compaction of porous spaces in the material changes the detailed mechanics of the breakup but only has a limited effect on the burst altitude and energy deposition. Strong asteroids fail and create peak energy deposition close to the altitude at which ram dynamic pressure equals the material strength. Weak asteroids, even though they structurally fail at high altitude, require the increased pressure at lower altitude to disrupt and disperse the rubble. As a result, a wide range of weaker asteroid strengths produce peak energy deposition at a similar altitude.

Effects of Fabrication Parameters on Interface of Zirconia and Ti-6Al-4V Joints Using Zr55Cu30Al10Ni5 Amorphous Filler

NASA Astrophysics Data System (ADS)

Liu, Yuhua; Hu, Jiandong; Shen, Ping; Guo, Zuoxing; Liu, Huijie

2013-09-01

ZrO2 was brazed to Ti-6Al-4V using a Zr55Cu30Al10Ni5 (at.%) amorphous filler in a high vacuum at 1173-1273 K. The influences of brazing temperature, holding time, and cooling rate on the microstructure and shear strength of the joints were investigated. The interfacial microstructures can be characterized as ZrO2/ZrO2- x + TiO/(Zr,Ti)2(Cu,Ni)/(Zr,Ti)2(Cu,Ni,Al)/acicular Widmanstäten structure/Ti-6Al-4V. With the increase in the brazing temperature, both the thickness of the ZrO2- x + TiO layer and the content of the (Zr,Ti)2(Cu,Ni) phase decreased. However, the acicular Widmanstäten structure gradually increased. With the increase in the holding time, the (Zr,Ti)2(Cu,Ni) phase decreased, and the thickness of the (Zr,Ti)2(Cu,Ni) + (Zr,Ti)2(Cu,Ni,Al) layer decreased. In addition, cracks formed adjacent to the ZrO2 side under rapid cooling. The microstructures produced under various fabrication parameters directly influence the shear strength of the joints. When ZrO2 and Ti-6Al-4V couples were brazed at 1173 K for 10 min and then cooled at a rate of 5 K/min, the maximum shear strength of 95 MPa was obtained.

Shear localization and size-dependent strength of YCd 6 quasicrystal approximant at the micrometer length scale

DOE PAGES

Song, Gyuho; Kong, Tai; Dusoe, Keith J.; ...

2018-01-24

Mechanical properties of materials are strongly dependent of their atomic arrangement as well as the sample dimension, particularly at the micrometer length scale. Here in this study, we investigated the small-scale mechanical properties of single-crystalline YCd 6, which is a rational approximant of the icosahedral Y-Cd quasicrystal. In situ microcompression tests revealed that shear localization always occurs on {101} planes, but the shear direction is not constrained to any particular crystallographic directions. Furthermore, the yield strengths show the size dependence with a power law exponent of 0.4. Shear localization on {101} planes and size-dependent yield strength are explained in termsmore » of a large interplanar spacing between {101} planes and the energetics of shear localization process, respectively. The mechanical behavior of the icosahedral Y-Cd quasicrystal is also compared to understand the influence of translational symmetry on the shear localization process in both YCd 6 and Y-Cd quasicrystal micropillars. Finally, the results of this study will provide an important insight in a fundamental understanding of shear localization process in novel complex intermetallic compounds.« less

Shear localization and size-dependent strength of YCd 6 quasicrystal approximant at the micrometer length scale

DOE Office of Scientific and Technical Information (OSTI.GOV)

Song, Gyuho; Kong, Tai; Dusoe, Keith J.

Mechanical properties of materials are strongly dependent of their atomic arrangement as well as the sample dimension, particularly at the micrometer length scale. Here in this study, we investigated the small-scale mechanical properties of single-crystalline YCd 6, which is a rational approximant of the icosahedral Y-Cd quasicrystal. In situ microcompression tests revealed that shear localization always occurs on {101} planes, but the shear direction is not constrained to any particular crystallographic directions. Furthermore, the yield strengths show the size dependence with a power law exponent of 0.4. Shear localization on {101} planes and size-dependent yield strength are explained in termsmore » of a large interplanar spacing between {101} planes and the energetics of shear localization process, respectively. The mechanical behavior of the icosahedral Y-Cd quasicrystal is also compared to understand the influence of translational symmetry on the shear localization process in both YCd 6 and Y-Cd quasicrystal micropillars. Finally, the results of this study will provide an important insight in a fundamental understanding of shear localization process in novel complex intermetallic compounds.« less

Study on the Strength of GFRP/Stainless Steel Adhesive Joints Reinforced with Glass Mat

NASA Astrophysics Data System (ADS)

Iwasa, Masaaki

The adhesive strengths of glass fiber reinforced plastics/metal adhesive joints reinforced with glass mat under tensile shear loads and tensile loads were investigated analytically and experimentally. First, the stress singularity parameters of the bonding edges were analyzed by FEM for various types of adhesive joints reinforced with glass mat. The shear stress and normal stress distributions near the bonding edge can be expressed by two stress singularity parameters. Second, tensile shear tests were performed on taper lap joint and taper lap joint reinforced with glass mat and tensile tests were performed on T-type adhesive joint and T-type adhesive joint reinforced with glass mat. The relationships between the loads and the crosshead displacements were measured. We concluded that reinforcing adhesive joints has a greater effect on strength under tensile load than under tensile shear load. The adhesive joints strength reinforced with glass mat can be evaluated by using stress singularity parameters.

Effect of grape seed extract against biodegradation of composite resin-dentin shear bond strength

NASA Astrophysics Data System (ADS)

Generosa, D. M.; Suprastiwi, E.; Asrianti, D.

2017-08-01

This study aimed to analyze the effect of grape seed extract (GSE) on resin-dentin shear bond strength. A group of 48 dentin samples were divided into 6 groups. The six groups, each with eight specimens, included group 1 (control), group 2 (control + NaOCl 10%), group 3 (2.9% GSE application before etching), group 4 (2.9% GSE application before etching + NaOCl 10%), group 5 (2.9% GSE application after etching), and group 6 (2.9% GSE application after etching + NaOCl 10%). Shear bond strengths were measured using a universal testing machine. Statistical analysis was done with the Kruskal-Wallis test and the Mann-Whitney U test. The highest median value was in group 3, and the lowest value was in group 5. GSE can improve the shear bond strength (p = 0.002 and 0.001), but it has no effect on reducing biodegradation (p = 0.141).

Prevention of crack in stretch flanging process using hot stamping technique

NASA Astrophysics Data System (ADS)

Syafiq, Y. Mohd; Hamedon, Z.; Azila Aziz, Wan; Razlan Yusoff, Ahmad

2017-10-01

Demand for enhancing of passenger safety as well as weight reduction of automobiles has increased the use of high strength steel sheets. As a sheet metal is a lightweight having high strength is suitable for producing automotive parts such as white body panel. The stretch flanging of the high strength steel sheet is a problem due to high springback and easy to crack. This study uses three methods to stretch flange the sheets; using lubricants, shear-edge polishing and hot stamping. The effectiveness of these methods will be measured by comparing the flange length of each methods can achieved. For stretch flange with lubricant and polished sheared edge, the flange length failed to achieve the target 15 mm while hot stamping improved the formability of the sheet and preventing the occurrence of the springback and crack. Hot stamping not only improved formability of the sheet but also transformed the microstructure into martensite thus improve the hardness and the strength of the sheet after been quenched with the dies.

Development of an easy-debonding orthodontic adhesive using thermal heating.

PubMed

Tsuruoka, Takashi; Namura, Yasuhiro; Shimizu, Noriyoshi

2007-01-01

We produced experimentally a new bonding material that consisted of a mixture of a base resin (4-META/MMA-TBB resin adhesive) and thermoexpandable microcapsules for safe, easy debonding. Microcapsules in the base resin would start expansion at 80 degrees C, leading to a remarkable decrease in bond strength. Stainless steel brackets were bonded to bovine permanent mandibular incisors using bonding materials containing the microcapsules at different contents. After thermal cycling or heating, the shear bond strength of the brackets was measured. Shear bond strength of the bonding materials containing 30-40 wt% microcapsules decreased to about one-third or one-fifth that of the base resin on heating. Heating the brackets for eight seconds increased the temperature in the pulp chamber by 2 degrees C, which should not induce pulp damage. Results obtained suggested that the new bonding material should prove useful for removing brackets easily at the time of bracket debonding without any pain or enamel cracks, while maintaining the bonding strength during active orthodontic treatment.

Atomistic modeling of Mg/Nb interfaces: shear strength and interaction with lattice glide dislocations

DOE PAGES

Yadav, Satyesh Kumar; Shao, S.; Chen, Youxing; ...

2017-10-17

Here, using a newly developed embedded-atom-method potential for Mg–Nb, the semi-coherent Mg/Nb interface with the Kurdjumov–Sachs orientation relationship is studied. Atomistic simulations have been carried out to understand the shear strength of the interface, as well as the interaction between lattice glide dislocations and the interface. The interface shear mechanisms are dependent on the shear loading directions, through either interface sliding between Mg and Nb atomic layers or nucleation and gliding of Shockley partial dislocations in between the first two atomic planes in Mg at the interface. The shear strength for the Mg/Nb interface is found to be generally high,more » in the range of 0.9–1.3 GPa depending on the shear direction. As a consequence, the extents of dislocation core spread into the interface are considerably small, especially when compared to the case of other “weak” interfaces such as the Cu/Nb interface.« less

Physical and Mechanical Properties of Surface Sediments and methane hydrate-bearing sediments in the Shenhu area of South China Sea

NASA Astrophysics Data System (ADS)

Jiang, J.; Shen, Z.; Jia, Y.

2017-12-01

Methane hydrates are superior energy resources and potential predisposing factors of geohazard. With the success in China's persistent exploitation of methane hydrates in the Shenhu area of South China Sea for 60 days, there is an increasing demand for detailed knowledge of sediment properties and hazard assessment in this area. In this paper, the physical and mechanical properties of both the surface sediments and methane hydrate-bearing sediments (MHBS) in the exploitation area, the Shenhu area of South China Sea, were investigated using laboratory geotechnical experiments, and triaxial tests were carried out on remolded sediment samples using a modified triaxial apparatus. The results show that sediments in this area are mainly silt with high moisture content, high plasticity, low permeability and low shear strength. The moisture content and permeability decrease while the shear strength increases with the increasing depth. The elastic modulus and peak strength of MHBS increase with the increasing effective confining pressure and higher hydrate saturation. The cohesion increases with higher hydrate saturation while the internal friction angle is barely affected by hydrate saturation. The obtained results demonstrate clearly that methane hydrates have significant impacts on the physical and mechanical properties of sediments and there is still a wide gap in knowledge about MHBS.

Life Limiting Behavior in Interlaminar Shear of Continuous Fiber-Reinforced Ceramic Matrix Composites at Elevated Temperatures

NASA Technical Reports Server (NTRS)

Choi, Sung R.; Calomino, Anthony M.; Bansal, Narottam P.; Verrilli, Michael J.

2006-01-01

Interlaminar shear strength of four different fiber-reinforced ceramic matrix composites was determined with doublenotch shear test specimens as a function of test rate at elevated temperatures ranging from 1100 to 1316 C in air. Life limiting behavior, represented as interlaminar shear strength degradation with decreasing test rate, was significant for 2-D crossplied SiC/MAS-5 and 2-D plain-woven C/SiC composites, but insignificant for 2-D plain-woven SiC/SiC and 2-D woven Sylramic (Dow Corning, Midland, Michigan) SiC/SiC composites. A phenomenological, power-law delayed failure model was proposed to account for and to quantify the rate dependency of interlaminar shear strength of the composites. Additional stress rupture testing in interlaminar shear was conducted at elevated temperatures to validate the proposed model. The model was in good agreement with SiC/MAS-5 and C/SiC composites, but in poor to reasonable agreement with Sylramic SiC/SiC. Constant shear stress-rate testing was proposed as a possible means of life prediction testing methodology for ceramic matrix composites subjected to interlaminar shear at elevated temperatures when short lifetimes are expected.

The internal bond and shear strength of hardwood veneered particleboard composites

Treesearch

P. Chow; J.J. Janowiak; E.W. Price

1986-01-01

The effects of several accelerated aging tests and weather exposures on hardwood reconstituted structural composite panels were evaluated. The results indicated that the internal bond and shear by tension loading strength reductions of the panels were affected by the exposure test method. The ranking of the effects of various exposure tests on strength values in an...

Short communication: pre- and co-curing effect of adhesives on shear bond strengths of composite resins to primary enamel and dentine: an in vitro study.

PubMed

Viswanathan, R; Shashibhushan, K K; Subba Reddy, V V

2011-12-01

To evaluate and compare shear bond strengths of composite resins to primary enamel and dentine when the adhesives are pre-cured (light cured before the application of the resin) or co-cured (adhesive and the resin light cured together). Buccal surfaces of 80 caries-free primary molars were wet ground to create bonding surfaces on enamel and dentine and specimens mounted on acrylic blocks. Two bonding agents (Prime and Bond NT® and Xeno III®) were applied to either enamel or dentine as per manufacturer's instructions. In 40 specimens, the bonding agent was light cured immediately after the application (pre-cured). The other 40 specimens were not light cured until the composite resin application (co-cured). Resin composite cylinders were made incrementally using acrylic moulds over the adhesives and light cured. Specimens were stored in deionised water for 24 hours at room temperature. Shear bond strength was measured using an Instron universal testing machine (in MPa) and was analysed with Student's unpaired t test. Light curing the adhesive separately produced significantly higher bond strengths to primary dentine than co-curing (p<0.001). At the same time light curing the adhesive separately did not produce significantly different bond strengths to primary enamel (p>0.05). Curing sequence had no significant effect on shear bond strength of adhesives on the primary enamel. Pre-curing adhesives before curing composite resins produced greater shear bond strength to primary dentine.

Ultra-high modulus organic fiber hybrid composites

NASA Technical Reports Server (NTRS)

Champion, A. R.

1981-01-01

An experimental organic fiber, designated Fiber D, was characterized, and its performance as a reinforcement for composites was investigated. The fiber has a modulus of 172 GPa, tensile strength of 3.14 GPa, and density of 1.46 gm/cu cm. Unidirectional Fiber D/epoxy laminates containing 60 percent fiber by volume were evaluated in flexure, shear, and compression, at room temperature and 121 C in both the as fabricated condition and after humidity aging for 14 days at 95 percent RH and 82 C. A modulus of 94.1 GPa, flexure strength of 700 MPa, shear strength of 54 MPa, and compressive strength of 232 MPa were observed at room temperature. The as-fabricated composites at elevated temperature and humidity aged material at room temperature had properties 1 to 20 percent below these values. Combined humidity aging plus evaluated temperature testing resulted in even lower mechanical properties. Hybrid composite laminates of Fiber D with Fiber FP alumina or Thornel 300 graphite fiber were also evaluated and significant increases in modulus, flexure, and compressive strengths were observed.

[Effect of nano-silica coating on bonding strength of zirconia ceramics to dentin].

PubMed

Zhang, Xian-Fang; Zheng, Hu; Han, Dong-Wei

2009-04-01

To investigate the effect of silica coating by sol-gel process on bonding strength of zirconia ceramics to dentin. Blocks of sintered zirconia ceramics were cut and randomly divided into 4 groups,16 slices in each group. Each group was subject to one of the 4 kinds of surface treatment (control group, sandblasting, sandblasting +silicone, sandblasting + silica coating + silicone) and then bonded to dentin with resin cement. After preservation in 37 degrees centigrade distilled water for 24 hours, the shear bonding strength of these specimens was tested and the data was analyzed with SAS6.12 software package for analysis of variance. The surface modality of the ceramics was observed under scanning electron microscopy (SEM). The group of sandblasting+ silica coating + silicone attained the highest shear bonding strength, which was significantly different from the other groups(P=0.000);There was no significant difference between the sandblasting and sandblasting + silicone group (P=0.827), which was significantly different from the control group(P=0.001). Silica coating by sol-gel process, coupled with silicone, can significantly increase the bonding strength of zirconia ceramics to dentin.

Evaluation of an alternative technique to optimize direct bonding of orthodontic brackets to temporary crowns.

PubMed

Dias, Francilena Maria Campos Santos; Pinzan-Vercelino, Célia Regina Maio; Tavares, Rudys Rodolfo de Jesus; Gurgel, Júlio de Araújo; Bramante, Fausto Silva; Fialho, Melissa Nogueira Proença

2015-01-01

To compare shear bond strength of different direct bonding techniques of orthodontic brackets to acrylic resin surfaces. The sample comprised 64 discs of chemically activated acrylic resin (CAAR) randomly divided into four groups: discs in group 1 were bonded by means of light-cured composite resin (conventional adhesive); discs in group 2 had surfaces roughened with a diamond bur followed by conventional direct bonding by means of light-cured composite resin; discs in group 3 were bonded by means of CAAR (alternative adhesive); and discs in group 4 had surfaces roughened with a diamond bur followed by direct bonding by means of CAAR. Shear bond strength values were determined after 24 hours by means of a universal testing machine at a speed of 0.5 mm/min, and compared by analysis of variance followed by post-hoc Tukey test. Adhesive remnant index (ARI) was measured and compared among groups by means of Kruskal-Wallis and Dunn tests. Groups 3 and 4 had significantly greater shear bond strength values in comparison to groups 1 and 2. Groups 3 and 4 yielded similar results. Group 2 showed better results when compared to group 1. In ARI analyses, groups 1 and 2 predominantly exhibited a score equal to 0, whereas groups 3 and 4 predominantly exhibited a score equal to 3. Direct bonding of brackets to acrylic resin surfaces using CAAR yielded better results than light-cured composite resin. Surface preparation with diamond bur only increased shear bond strength in group 2.

A micromechanical model to explain the mechanical properties of bovine cortical bone in tension: In vitro fluoride ion effects

NASA Astrophysics Data System (ADS)

Kotha, Shiva Prasad

Bone mineral and bone organic are assumed to be a linearly elastic, brittle material. A simple micromechanical model based on the shear lag theory is developed to model the stress transfer between the mineral platelets of bone. The bone mineral platelets carry most of the applied load while the organic primarily serves to transfer load between the overlapped mineral platelets by shear. Experiments were done to elucidate the mechanism of failure in bovine cortical bone and to decrease the mineral content of control bone with in-vitro fluoride ion treatments. It was suggested that the failure at the ultrastructural level is due to the transverse failure of bonds between the collagen microfibrils in the organic matrix. However, the shear stress transfer and the axial load bearing capacity of the organic is not impaired. Hence, it is assumed that the shear strain in the matrix increases while the shear stress remains constant at the shear yield stress once the matrix starts yielding at the ends of the bone mineral. When the shear stress over the length of the mineral platelet reaches the shear yield stress, no more applied stress is carried by the bone mineral platelets while the organic matrix carries the increased axial load. The bone fails when the axial stress in the organic reaches its ultimate stress. The bone mineral is assumed to dissolve due to in-vitro fluoride ion treatments and precipitate calcium fluoride or fluoroapatite like material. The amount of dissolution is estimated based on 19F Nuclear Magnetic Resonance or a decrease in the carbonate content of bone. The dissolution of bone mineral is assumed to increase the porosity in the organic. We assume that the elastic modulus and the ultimate strength of the organic decrease due to the increased porosity. A simple empirical model is used to model the decrease in the elastic modulus. The strength is modeled to decrease based on an increase in the cross-sectional area occupied by the porosity. The precipitate is assumed to contribute to the mechanical properties of bone due to friction generated by the poisson's contraction of the organic as it carries axial loads. The resulting stress-strain curve predicted by the model resembles the stress-strain curves obtained in the experiments.

Post-thermocycling shear bond strength of a gingiva-colored indirect composite layering material to three implant framework materials.

PubMed

Komine, Futoshi; Koizuka, Mai; Fushiki, Ryosuke; Taguchi, Kohei; Kamio, Shingo; Matsumura, Hideo

2013-09-01

To evaluate shear bond strength of a gingiva-colored indirect composite to three implant framework materials, before and after thermocycling, and verify the effect of surface pre-treatment for each framework. Commercially pure titanium (CP-Ti), American Dental Association (ADA) type 4 casting gold alloy (Type IV) and zirconia ceramics (Zirconia) were assessed. For each substrate, 96 disks were divided into six groups and primed with one of the following primers: Alloy Primer (ALP), Clearfil Photo Bond (CPB), Clearfil Photo Bond with Clearfil Porcelain Bond Activator (CPB+Activator), Estenia Opaque Primer (EOP), Metal Link (MLP) and V-Primer (VPR). The specimens were then bonded to a gingiva-colored indirect composite (Ceramage Concentrate GUM-D). Shear bond strengths were measured at 0 and 20 000 thermocycles and data were analyzed with the Steel-Dwass test and Mann-Whitney U-test. Shear bond strengths were significantly lower after thermocycling, with the exception of Type IV specimens primed with CPB (p = 0.092) or MLP (p = 0.112). For CP-Ti and Zirconia specimens, priming with CPB or CPB+Activator produced significantly higher bond strengths at 0 and 20 000 thermocycles, as compared with the other groups. For Type IV specimens, priming with ALP or MLP produced higher bond strengths at 0 and 20 000 thermocycles. Shear bond strength of a gingiva-colored indirect composite to CP-Ti, gold alloy and zirconia ceramics was generally lower after thermocycling. Application of a hydrophobic phosphate monomer and polymerization initiator was effective in maintaining bond strength of CP-Ti and zirconia ceramics. Combined use of a thione monomer and phosphoric monomer enhanced the durable bond strength of gold alloy.

Shear bond strength of a new self-adhering flowable composite resin for lithium disilicate-reinforced CAD/CAM ceramic material

PubMed Central

Sancakli, Hande Sar; Sancakli, Erkan; Eren, Meltem Mert; Ozel, Sevda; Yucel, Taner; Yildiz, Esra

2014-01-01

PURPOSE The purpose of this study was to evaluate and compare the effects of different surface pretreatment techniques on the surface roughness and shear bond strength of a new self-adhering flowable composite resin for use with lithium disilicate-reinforced CAD/CAM ceramic material. MATERIALS AND METHODS A total of one hundred thirty lithium disilicate CAD/CAM ceramic plates with dimensions of 6 mm × 4 mm and 3 mm thick were prepared. Specimens were then assigned into five groups (n=26) as follows: untreated control, coating with 30 µm silica oxide particles (Cojet™ Sand), 9.6% hydrofluoric acid etching, Er:YAG laser irradiation, and grinding with a high-speed fine diamond bur. A self-adhering flowable composite resin (Vertise Flow) was applied onto the pre-treated ceramic plates using the Ultradent shear bond Teflon mold system. Surface roughness was measured by atomic force microscopy. Shear bond strength test were performed using a universal testing machine at a crosshead speed of 1 mm/min. Surface roughness data were analyzed by one-way ANOVA and the Tukey HSD tests. Shear bond strength test values were analyzed by Kruskal-Wallis and Mann-Whitney U tests at α=.05. RESULTS Hydrofluoric acid etching and grinding with high-speed fine diamond bur produced significantly higher surface roughness than the other pretreatment groups (P<.05). Hydrofluoric acid etching and silica coating yielded the highest shear bond strength values (P<.001). CONCLUSION Self-adhering flowable composite resin used as repair composite resin exhibited very low bond strength irrespective of the surface pretreatments used. PMID:25551002

Experimental shear strength of unchecked solid-sawn Douglas-fir

Treesearch

D. R. Rammer; L. A. Soltis; P. K. Lebow

This report presents experimental results of modulus of rupture and shear strength tests on unsplit, green, sawn Douglas-fir lumber. Five different size-matched specimens, ranging from nominal 2-by 4-in (standard 38- by 89-mm) to nominal 4- by 14-in (standard 95-by 343-mm), were tested in third-point bending and five-point beam shear. A total of 120 bending and 160...

Influence of surface treatments on the shear bond strength of orthodontic brackets to porcelain

NASA Astrophysics Data System (ADS)

Wang, Cong; Zeng, Jishan; Wang, Shaoan; Yang, Zheng; Huang, Qian; Chen, Pixiu; Zhou, Shujuan; Liu, Xiaoqing

2008-11-01

The purpose of this study was to investigate the effect of various surface treatments after different storage time and thermocycling on the shear bond strength of orthodontic brackets to the feldspathic porcelain surfaces. 128 disc-shaped porcelain specimens were randomly assigned to the following surface treatments: 9.6% HFA, 9.6% HFA combined with silane, 50 μ aluminum trioxide sandblasting followed by silane and application of silane after 37% phosphoric acid. Metal or ceramic brackets were bonded onto each treated porcelain facet with light cured resin. The samples were stored in 37 °C water 1 day or 7 days, thermocycled 500 times from 5 to 55 °C. The shear bond strengths were measured (1 mm/min), and statistically analyzed. The bond failure sites were classified according to ARI system. The surface of the glazed, sandblasted, hydrofluoric and phosphoric acid etched porcelain were examined with SEM. All groups achieved reasonable bond strengths to withstand the application of orthodontic forces. Water storage for 7 days caused lower shear bond strength than that of 1 day. But there is no statistically significant difference between the two groups. The mean shear bond strength provided by ceramic bracket with mechanical retention had no statistical difference with that of metal bracket. Therefore, the optimal treatment for orthodontic brackets bonding to feldspathic porcelain was to apply phosphoric acid combined with silane.

Comparison between universal adhesives and two-step self-etch adhesives in terms of dentin bond fatigue durability in self-etch mode.

PubMed

Tsujimoto, Akimasa; Barkmeier, Wayne W; Takamizawa, Toshiki; Watanabe, Hidehiko; Johnson, William W; Latta, Mark A; Miyazaki, Masashi

2017-06-01

This aim of this study was to compare universal adhesives and two-step self-etch adhesives in terms of dentin bond fatigue durability in self-etch mode. Three universal adhesives - Clearfil Universal, G-Premio Bond, and Scotchbond Universal Adhesive - and three-two-step self-etch adhesives - Clearfil SE Bond, Clearfil SE Bond 2, and OptiBond XTR - were used. The initial shear bond strength and shear fatigue strength of resin composite bonded to adhesive on dentin in self-etch mode were determined. Scanning electron microscopy observations of fracture surfaces after bond strength tests were also made. The initial shear bond strength of universal adhesives was material dependent, unlike that of two-step self-etch adhesives. The shear fatigue strength of Scotchbond Universal Adhesive was not significantly different from that of two-step self-etch adhesives, unlike the other universal adhesives. The shear fatigue strength of universal adhesives differed depending on the type of adhesive, unlike those of two-step self-etch adhesives. The results of this study encourage the continued use of two-step self-etch adhesive over some universal adhesives but suggest that changes to the composition of universal adhesives may lead to a dentin bond fatigue durability similar to that of two-step self-etch adhesives. © 2017 Eur J Oral Sci.

Design, Fabrication, and Testing of Ceramic Joints for High Temperature SiC/SiC Composites

NASA Technical Reports Server (NTRS)

Singh, Mrityunjay; Lara-Curzio, Edgar

2000-01-01

Various issues associated with the design and mechanical evaluation of joints of ceramic matrix composites are discussed. The specific case of an affordable, robust ceramic joining technology (ARCJoinT) to join silicon carbide (CG-Nicalon(sup TM)) fiber-reinforced-chemically vapor infiltrated (CVI) silicon carbide matrix composites is addressed. Experimental results are presented for the time and temperature dependence of the shear strength of these joints in air up to 1200 C. From compression testing of double-notched joint specimens with a notch separation of 4 mm, it was found that the apparent shear strength of the joints decreased from 92 MPa at room temperature to 71 MPa at 1200 C. From shear stress-rupture testing in air at 1200 C it was found that the shear strength of the joints decreased rapidly with time from an initial shear strength of 71 to 17.5 MPa after 14.3 hr. The implications of these results in relation to the expected long-term service life of these joints in applications at elevated temperatures are discussed.

Shear strength of clay and silt embankments.

DOT National Transportation Integrated Search

2009-09-01

Highway embankment is one of the most common large-scale geotechnical facilities constructed in Ohio. In the past, the design of these embankments was largely based on soil shear strength properties that had been estimated from previously published e...

[Comparison of the shear bond strength by using nano silica sol to zirconia basement and veneer porcelain].

PubMed

Wang, Si-qian; Zhang, Da-feng; Zhen, Tie-li; Yang, Jing-yuan; Lin, Ting-ting; Ma, Jian-feng

2016-04-01

To investigate the feasibility of using sol gel technique to produce thin layer nano silicon dioxide on zirconia ceramic surface and the effect of improving shear bond strength between zirconia and veneer porcelain. The presintered zirconia specimen was cut into a rectangle block piece (15 mm×10 mm×2.5 mm), a total of 40 pieces were obtained and divided into 4 groups, each group had 10 pieces. Four different treatments were used in each group respectively. Pieces in group A (control group) were only sintered at 1450°C to crystallization; pieces in group B underwent 30% nano silica sol infiltration first and then were sintered at 1450°C to crystallization; piece in group C underwent crystallization first at 1450°C, then 30% nano silica sol infiltration and were sintered at 1450°C again; pieces in group D was coated by nano silica sol and then sintered at 1450°C to crystallization; ten rectangle block pieces (12 mm×8 mm×2 mm) in group E were made. Cylinder veneers 5 mm in diameter and 4 mm in height were produced in each group and the shear bond strength was tested. Data were statistically analyzed by SPSS 19.0 software package. The shear bond strength of the 5 group specimens were: (28.12±2.95) MPa in group A, (31.09±3.94) MPa in group B, (25.60±2.45) MPa in group C, (31.75±4.90) MPa in group D, (28.67±3.95) MPa in group E, respectively. Significant differences existed between the 5 groups, and group C had significant difference compared with group B and D. CONCLUSIONS：① Use of nano silicon sol gel on presintered zirconia surface to make thin layer of nano silicon dioxide can improve the shear bond strength between zirconia and veneer; ②Using nano silicon sol gel on crystallization zirconia surface to make thin layer of nano silicon dioxide will decrease the shear bond strength between zirconia and veneer; ③ Zirconia veneer bilayer ceramic has the same shear bond strength with porcelain fused to Ni Cr alloy; ④Use of sol gel technique to produce thin layer nano silicon dioxide on zirconia ceramic surface is feasible and can improve shear bond strength between zirconia and veneer porcelain.

Effect of various commercially available mouthrinses on shear bond strength of orthodontic metal brackets: an in vitro study.

PubMed

Meeran, Nazeer Ahmed; George, Ashwin Mathew

2013-01-01

Alcohol is known to degrade and dissolve the bisphenol A glycidyl methacrylate present in the composite resin. The effect of alcohol containing mouthrinses on the shear bond strength of orthodontic metal brackets bonded with composite resin has not been verified until date and is the purpose of this study. The aims and objectives of the present study were to evaluate (1) Whether there is a significant difference in the shear bond strength of metal orthodontic brackets after the 1 year (12 h) and 2 years simulation (24 h) of mouth rinsing with 4 different commercially available mouthrinses (2 alcoholic and 2 alcohol-free mouthrinses) when compared to the control. (2) Whether alcohol containing mouthrinses have more adverse effect on the shear bond strength when compared with alcohol-free mouthrinses. (3) To assess the site of bond failure using adhesive remnant index. Experimental - laboratory based. A total of 100 upper premolars extracted for orthodontic purpose were collected immediately after extraction, cleared soft-tissue debris and blood and immediately stored in distilled water with 0.1% thymol crystals added to inhibit bacterial growth. Two alcohol containing mouthrinses and two alcohol-free mouthrinses were used and the bonded teeth were placed in the mouthrinses for a stipulated period of time (1 year simulation and 2 years simulation) and shear bond strength were tested using Lloyd Universal Testing Machine. The data were analyzed using analysis of variance and paired samples t-test. After the 1 year and 2 years simulation time, samples stored in alcohol containing mouthrinses showed lower bond strength (P < 0.05) when compared to samples stored in alcohol free mouthrinses and distilled water (control). Alcohol containing mouthrinses affect the shear bond strength of the metal orthodontic brackets bonded with composite resin (Transbond XT in the present study), more when compared with alcohol-free mouthrinses. It is, therefore, highly advisable to avoid alcohol containing mouthrinses in patients undergoing orthodontic treatment and use alcohol-free mouthrinses as adjuncts to regular oral hygiene procedures for maintaining good enamel integrity and periodontal health, without compromising the shear bond strength of the bonded metal brackets.

Casein Phosphopeptide-Amorphous Calcium Phosphate and Shear Bond Strength of Adhesives to Primary Teeth Enamel

PubMed Central

Farokh Gisovar, Elham; Hedayati, Nassim; Shadman, Niloofar; Shafiee, Leila

2015-01-01

Background: CPP-ACP (Phosphopeptide-Amorphous Calcium Phosphate) has an important role in caries prevention in pediatric patients. This study was done, because of the great use of CPP-ACP and the need for restoration for teeth treated with CPP-ACP as well as the importance of shear bond strength of adhesives in the success of restorations. Objectives: This study aimed to evaluate the effect of casein phosphopeptide-amorphous calcium phosphate (CPP-ACP) on shear bond strength of dental adhesives to enamel of primary teeth molars. Materials and Methods: This in vitro study was conducted on 180 extracted primary molars. They were randomly divided into 6 groups and each group was divided into 2 subgroups (treated with CPP-ACP and untreated). In subgroups with CPP-ACP, enamel was treated with CPP-ACP paste 1 h/d for 5 days. Types of adhesives that were evaluated in this study were Tetric N-Bond, AdheSE, AdheSE One F, single Bond 2, SE Bond, and Adper Prompt L-Pop. Shear bond strength was tested with a universal testing machine and mode of failure was evaluated under stereomicroscope. Data were analyzed by T test, 2-way analysis of variance (ANOVA), Tukey and Fisher exact test using SPSS18. P < 0.05 was considered as significance level. Results: Shear bond strengths of different adhesive systems to enamel of primary teeth treated and untreated with CPP-ACP showed no significant difference (P > 0.05). Mode of failure in all groups regardless of CPP-ACP administration was mainly adhesive type. Our results indicated that CPP-ACP did not affect shear bond strength of studied adhesives to primary teeth enamel. Conclusions: To have a successful and durable composite restoration, having a high strength bonding is essential. Considering the wide use of CPP-ACP in preventing tooth decay and the role of adhesive shear bond strength (SBS) in success of composite restoration, we conducted the present study to evaluate the effect of CPP-ACP on the SBS of adhesives to primary teeth enamel. PMID:25793113

Influence of enamel conditioning on the shear bond strength of different adhesives.

PubMed

Brauchli, Lorenz; Muscillo, Teodoro; Steineck, Markus; Wichelhaus, Andrea

2010-11-01

Phosphoric acid etching is the gold standard for enamel conditioning. However, it is possible that air abrasion or a combination of air abrasion and etching might result in enhanced adhesion. The aim of this study was to investigate the effect of different enamel conditioning methods on the bond strength of six adhesives. Three different enamel conditioning procedures (phosphoric acid etching, air abrasion, air abrasion + phosphoric acid etching) were evaluated for their influence on the shear bond strength of six different adhesives (Transbond™ XT, Cool-Bond™, Fuji Ortho LC, Ultra Band-Lok, Tetric(®) Flow, Light-Bond™). Each group consisted of 15 specimens. Shear forces were measured with a universal testing machine. The scores of the Adhesive Remnant Index (ARI) were also analyzed. There were no significant differences between phosphoric acid etching and air abrasion + phosphoric acid etching. Air abrasion as a single conditioning technique led to significantly lower shear forces. The ARI scores did not correlate with the shear strengths measured. There were greater variations in shear forces for the different adhesives than for the conditioning techniques. The highest shear forces were found for the conventional composites Transbond™ XT and Cool- Bond™ in combination with conventional etching. Air abrasion alone and in combination with phosphoric acid etching showed no advantages compared with phosphoric acid etching alone and, therefore, cannot be recommended.

Evaluation of critical shear stresses for consolidated cohesive sediment depositions by using PIV compared with field measurements

NASA Astrophysics Data System (ADS)

Harb, Gabriele; Haun, Stefan

2013-04-01

Reservoir sedimentation is a common problem today. Due to the reduced flow velocities, turbulences and bed shear stresses the transported sediment load start to settle. These depositions reduce the worldwide average storage capacity in the range of about 1% per year. However, depending on the climate conditions and the geology in the catchment area this value may vary strongly. Therefore sediment management tasks, especially the removal of already accumulated sediments, have to be developed for each reservoir separately. The critical bed shear stress is a key parameter used to evaluate the different management tasks and depend strongly on the grain size distribution of the inflowing sediments. However, depositions which contain fine particles like clay and silt increase the critical bed shear stress due to occurring cohesive forces and the use of the Shield curve for evaluating the critical shear stress is no longer valid. Additional data is required for estimating the valid critical shear stress at the reservoir bed. In this study the critical shear stress was evaluated for cohesive sediment samples, taken from two different reservoirs, in a flume in the laboratory. The sediment samples were placed in an installed double bottom in the research flume and the discharge was increased stepwise until mass erosion took place (determined by visual inspection). A 2D PIV device was used to measure the flow conditions (velocities and turbulences) over the sediment sample. The obtained values were used to calculate the bed shear stress for the specific discharge rate by the gravity method and the Reynolds stress method. The results of both methods showed good agreement in the comparison of the values, what indicates that nearly uniform flow conditions occurred in the flume. The results from this study showed that the behaviour of natural cohesive sediments depend strongly on the natural conditions as a result of physical, chemical and biological processes. In this case especially the effect of the layer structure in the sediment samples was controlling the erosion mechanism. The results of the experiments showed also that the obtained average shear stress was above most of the values found in previous conducted studies, which may be explained by consolidation effects in the reservoirs. Additional conducted vane strength measurements have been carried out in situ. The in the field obtained vane strength values were set in relation to the critical shear stresses derived by the experimental tests from the laboratory and to data from a previous conducted study to develop a new relation function. This function may be used in future studies for a rough estimation of the critical shear stress, based on in situ measured vane strength values.

Temperature-dependent residual shear strength characteristics of smectite-rich landslide soils

NASA Astrophysics Data System (ADS)

Shibasaki, Tatsuya; Matsuura, Sumio; Okamoto, Takashi

2015-04-01

On gentle clayey slopes in weathered argillaceous rock areas, there exist many landslides which repeatedly reactivate with slow movement. The slip surface soils of these landslides are sometimes composed dominantly of swelling clay mineral (smectite) which is well known to show extremely low residual friction angle. From field data monitored at landslide sites in Japan, it has become clear that some landslides with relatively shallow slip surface begin to move and become active in late autumn or early winter every year. In such cases, the triggering mechanisms of landslides have not been understood well enough, because landslide initiation and movement are not always clearly linked with rises in pore water pressures (ground water levels). In this study, we focus on the influence of seasonal variation in ground temperature on slope stability and have investigated the effect of temperature on the shear strength of slip surface soils. Undisturbed soil samples were collected by boring from the Busuno landslide in Japan. We performed box shear experiments on undisturbed slip surface soils at low temperature ranges (approximately 5-25 °C). XRD analysis revealed that these soils contain high fraction of smectite. Slickensided slip surface within test specimen was coincided with the shearing plane of the shear box and shear displacement was applied precisely along the localized slip surface. Experiments were performed under slow shearing rate condition (0.005mm/min) and the results showed that shear strength decreased with decreasing temperature. Temperature effect was rather significant on frictional angle than on cohesion. Ring shear experiments were also performed on normally-consolidated remoulded samples. Under residual strength condition, temperature-change experiments (cooling-event tests) ranging approximately from 5 to 25 °C were performed on smectite-rich landslide soils and commercial bentonites. As well as the results by box shear test, shear weakening behaviors were also recognized during cooling-event tests. Shear stress fluctuations, which were obtained by 1 Hz data sampling, showed that shear behavior characteristically changed in response to temperature conditions. Stick-slip behavior prevailed under room temperature conditions, whereas shear behavior gradually changed into stable sliding behavior as temperature decreased. SEM (Scanning Electric Microscope) observation on shear surfaces indicated that silt- and sand-size asperities in the vicinity of the shear surface influence the occurrence of stick-slip behavior. It is also characteristically noted that rod-shaped smectitic clays, here called "roll", developed on shear surfaces and are arrayed densely perpendicular to the shearing direction in a micrometer scale. We assume that these rolls are probably rotating slowly within shear zone and acting as a lubricant which affects the temperature-dependent frictional properties of the shearing plane. These experimental results show that residual strength characteristics of smectite-rich soils are sensitive to temperature conditions. Our findings imply that if slip surface soils contain a high fraction of smectite, a decrease in ground temperature can lead to lowered shear resistance of the slip surface and triggering of slow landslide movement.

Physical properties of sediment containing methane gas hydrate

USGS Publications Warehouse

Winters, W.J.; Waite, W.F.; Mason, D.H.; Gilbert, L.Y.

2005-01-01

A study conducted by the US Geological Survey (USGS) on the formation, behavior, and properties of mixtures of gas hydrate and sediment is presented. The results show that the properties of host material influence the type and quantity of hydrates formed. The presence of hydrate during mechanical shear tests affects the measured sediment pore pressure. Sediment shear strength may be increased more than 500 percent by intact hydrate, but greatly weakened if the hydrate dissociates.

The Effects of Shear Strain, Fabric, and Porosity Evolution on Elastic and Mechanical Properties of Clay-Rich Fault Gouge

NASA Astrophysics Data System (ADS)

Kenigsberg, A.; Saffer, D. M.; Riviere, J.; Marone, C.

2017-12-01

Ultrasonic/seismic waves are widely used for probing fault zone elastic and mechanical properties (gouge composition, frictional strength, density) and elastic properties (Vp, Vs, bulk and shear moduli), as it can provide insight into key processes and fault properties during shearing. These include fabric and force chain formation, porosity evolution, and fault zone stiffness, which are in turn factors in fault slip, damage, and healing. We report on a suite of direct shear experiments on synthetic fault gouge composed of 50% smectite /50% quartz at a normal stress of 25 MPa, in which we use ultrasonic wave transmission to continuously monitor compressional and shear wave velocities (Vp, Vs) up to shear strains of 25, while simultaneously measuring friction and monitoring the evolution of density and porosity. We find that wavespeeds vary with shear strain, due to fabric development and the evolution of density and porosity. The coefficient of friction peaks at μ .47 at a shear strain of .5 - 1, decreases to a steady state value of μ .43 by shear strains of 4.5- 6 and then remains rather constant to shear strains of 6 - 25, consistent with previous work. Density increases rapidly from 1.78 g/cm3 to 1.83 g/cm3 at shear strains from 0-2 (porosity decreases from 33% to 25% over that range), and then more gradually increases to a density of 2.08 g/cm3 (porosity of 21%) at a shear strain of 25. Vp increases from 2400 m/s to 2900 m/s during the onset of shear until a shear strain of 3, and then decreases to 2400-2500 by shear strain of 7-9. At shear strains above 9, Vp slowly increases as the layer becomes denser and less porous. We interpret the co-evolving changes in friction, porosity, and elastic moduli/wavespeed to reflect fabric development and alignment of clay particles as a function of shearing. More specifically, the decrease in Vp at a shear strain of 3 reflects the clay particles gradually aligning. Once the particles are aligned, the gradual increase of Vp at shear strains of 7-9 reflects near complete alignment and increased compaction and density. This interpretation is supported by SEM imaging and analysis of a suite of experiments stopped at different shear strains.

Lateral deflection contribution to settlement estimates.

DOT National Transportation Integrated Search

2014-06-01

The construction of tall embankments on soft soils requires staged construction, which leads to the : consolidation of foundation soils, an increase in their effective stress, reduction in void ratio, and gain in shear : strength. However, tall emban...

Improved adhesion performances of aramid fibers with vinyl epoxy via supercritical carbon dioxide modification

NASA Astrophysics Data System (ADS)

Qin, M. L.; Kong, H. J.; Yu, M. H.; Teng, C. Q.

2017-06-01

In this paper, aramid fibers were treated under supercritical carbon dioxide (SCCO2) with isocyanate terminated liquid nitrile rubber to improve the adhesion performances of vinyl epoxy composites. The interfacial shear strength (IFSS) of vinyl epoxy composites was investigated by micro-bond test. The results indicate that the surface modification of aramid fibers in SCCO2 was an efficient method to increase the adhesion performances between fibers and vinyl epoxy. Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and scanning electron microscopy (SEM) were adopted to investigate the surface structure and composition of aramid fibers. The flexural strength and interlaminar shear strength (ILSS) of treated aramid fibers/vinyl epoxy composites was improved by 18.1% and 28.9% compared with untreated aramid fibers, respectively. Furthermore, the fractured surfaces of the composites were observed by SEM, which showed that the interfacial adhesion of composites has been remarkably changed.

Analysis of the Shear Behavior of Stubby Y-Type Perfobond Rib Shear Connectors for a Composite Frame Structure.

PubMed

Kim, Sang-Hyo; Kim, Kun-Soo; Lee, Do-Hoon; Park, Jun-Seung; Han, Oneil

2017-11-22

Shear connectors are used in steel beam-concrete slabs of composite frame and bridge structures to transfer shear force according to design loads. The existing Y-type perfobond rib shear connectors are designed for girder slabs of composite bridges. Therefore, the rib and transverse rebars of the conventional Y-type perfobond rib shear connectors are extremely large for the composite frames of building structures. Thus, this paper proposes stubby Y-type perfobond rib shear connectors, redefining the existing connectors, for composite frames of building structures; these were used to perform push-out tests. These shear connectors have relatively small ribs compared to the conventional Y-type perfobond rib shear connectors. To confirm the shear resistance of these stubby shear connectors, we performed an experiment by using transverse rebars D13 and D16. The results indicate that these shear connectors have suitable shear strength and ductility for application in composite frame structures. The shear strengths obtained using D13 and D16 were not significantly different. However, the ductility of the shear connectors with D16 was 45.1% higher than that of the shear connectors with D13.

Shear in high strength concrete bridge girders : technical report.

DOT National Transportation Integrated Search

2013-04-01

Prestressed Concrete (PC) I-girders are used extensively as the primary superstructure components in Texas highway bridges. : A simple semi-empirical equation was developed at the University of Houston (UH) to predict the shear strength of PC I-girde...

Increasing Ti-6Al-4V brazed joint strength equal to the base metal by Ti and Zr amorphous filler alloys

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ganjeh, E., E-mail: navidganjehie@sina.kntu.ac.ir; Sarkhosh, H.; Bajgholi, M.E.

Microstructural features developed along with mechanical properties in furnace brazing of Ti-6Al-4V alloy using STEMET 1228 (Ti-26.8Zr-13Ni-13.9Cu, wt.%) and STEMET 1406 (Zr-9.7Ti-12.4Ni-11.2Cu, wt.%) amorphous filler alloys. Brazing temperatures employed were 900-950 Degree-Sign C for the titanium-based filler and 900-990 Degree-Sign C for the zirconium-based filler alloys, respectively. The brazing time durations were 600, 1200 and 1800 s. The brazed joints were evaluated by ultrasonic test, and their microstructures and phase constitutions analyzed by metallography, scanning electron microscopy and X-ray diffraction analysis. Since microstructural evolution across the furnace brazed joints primarily depends on their alloying elements such as Cu, Ni andmore » Zr along the joint. Accordingly, existence of Zr{sub 2}Cu, Ti{sub 2}Cu and (Ti,Zr){sub 2}Ni intermetallic compounds was identified in the brazed joints. The chemical composition of segregation region in the center of brazed joints was identical to virgin filler alloy content which greatly deteriorated the shear strength of the joints. Adequate brazing time (1800 s) and/or temperature (950 Degree-Sign C for Ti-based and 990 Degree-Sign C for Zr-based) resulted in an acicular Widmanstaetten microstructure throughout the entire joint section due to eutectoid reaction. This microstructure increased the shear strength of the brazed joints up to the Ti-6Al-4V tensile strength level. Consequently, Ti-6Al-4V can be furnace brazed by Ti and Zr base foils produced excellent joint strengths. - Highlights: Black-Right-Pointing-Pointer Temperature or time was the main factors of controlling braze joint strength. Black-Right-Pointing-Pointer Developing a Widmanstaetten microstructure generates equal strength to base metal. Black-Right-Pointing-Pointer Brittle intermetallic compounds like (Ti,Zr){sub 2}Ni/Cu deteriorate shear strength. Black-Right-Pointing-Pointer Ti and Zr base filler alloys were the best choice for brazing Ti-6Al-4V.« less

Effects of increasing the allowable compressive stress at release on the shear strength of prestressed concrete girders.

DOT National Transportation Integrated Search

2008-09-01

In recent years, several research projects have been conducted to study the feasibility of increasing the allowable : compressive stress in concrete at prestress transfer, currently defined as 0.60f'ci in the AASHTO LRFD Bridge : Design Specification...

Statistical Investigation of the Effect of Process Parameters on the Shear Strength of Metal Adhesive Joints

NASA Astrophysics Data System (ADS)

Rajkumar, Goribidanur Rangappa; Krishna, Munishamaih; Narasimhamurthy, Hebbale Narayanrao; Keshavamurthy, Yalanabhalli Channegowda

2017-06-01

The objective of the work was to optimize sheet metal joining parameters such as adhesive material, adhesive thickness, adhesive overlap length and surface roughness for single lap joint of aluminium sheet shear strength using robust design. An orthogonal array, main effect plot, signal-to-noise ratio and analysis of variance were employed to investigate the shear strength of the joints. The statistical result shows vinyl ester is best candidate among other two polymers viz. epoxy and polyester due to its low viscosity value compared to other two polymers. The experiment results shows that the adhesive thickness 0.6 mm, overlap length 50 mm and surface roughness 2.12 µm for obtained maximum shear strength of Al sheet joints. The ANOVA result shows one of the most significant factors is overlap length which affect joint strength in addition to adhesive thickness, adhesive material, and surface roughness. A confirmation test was carried out as the optimal combination of parameters will not match with the any of the experiments in the orthogonal array.

The effect of silver nanoparticles on composite shear bond strength to dentin with different adhesion protocols.

PubMed

Fatemeh, Koohpeima; Mohammad Javad, Mokhtari; Samaneh, Khalafi

2017-01-01

The purpose of this study was to investigate the effect of silver nanoparticles on composite shear bond strength using one etch and rinse and one self-etch adhesive systems. Silver nanoparticles were prepared. Transmission electron microscope and X-ray diffraction were used to characterize the structure of the particles. Nanoparticles were applied on exposed dentin and then different adhesives and composites were applied. All samples were tested by universal testing machine and shear bond strength was assesed. Particles with average diameter of about 20 nm and spherical shape were found. Moreover, it was shown that pretreatment by silver nanoparticles enhanced shear bond strength in both etch and rinse, and in self-etch adhesive systems (p≤0.05). Considering the positive antibacterial effects of silver nanoparticles, using them is recommended in restorative dentistry. It seems that silver nanoparticles could have positive effects on bond strength of both etch-and-rinse and self-etch adhesive systems. The best results of silver nanoparticles have been achieved with Adper Single Bond and before acid etching.

In situ consolidation of offshore petroleum well structural casings by electrokinetic methods

NASA Astrophysics Data System (ADS)

Wrixon, Robert Christopher

Offshore drilling operations encounter cement wash-out problems while setting the initial structural casing (0--200 ft depth) due to the soft, unconsolidated nature of the sea-bed. Structural casings set by alternative methods have failed in up to 50% of cases due to insufficient frictional bearing capacity. This dissertation presents a method of increasing the bearing capacity of a jet-drilled or slick-drilled casing in-situ by applying a potential difference such that the casing is anodic compared to a remote cathode. It has been shown experimentally that clayey formations will swell and stick to a simulated anodic casing by the combined electrokinetic processes of electroosmosis and electrophoresis. Any cavities around the "casing" are eliminated and the formation is flush against the metal surface, increasing bearing capacity. The formation around the "casing" dries out due to electroosmotic migration of water away from the anode, increasing the shear strength of the surrounding soil. Corrosion products at the anode can further increase the soil shear strength by a process known as electrochemical hardening. This investigation has shown that the bearing capacity of anodic casings can potentially be increased by a factor of up to 1,000% in soft clays and silty clays. The existence of an optimal level of electrokinetic consolidation, beyond which the soil shear strength begins to degrade, has been demonstrated. The difficulties of applying electrokinetic methods to saline soil environments have been addressed and the process has been shown to be successful, as long as the requisite electric field strength is maintained. The efficiency of the electrokinetic consolidation technique has been shown to be affected by the soil water content, soil mineralogy, power supplied, time of treatment and the choice of anode material. Experiments in marine sediment show that increases in bearing capacities of about 300% can be achieved at optimal treatment conditions. With likely current and power restrictions, increases of 50% to 100% are realistic. This level of increase still makes offshore electrokinetic casing consolidation a viable process, given that it is attainable quickly and at a modest power requirement and given the enormous cost of a structural casing collapse.

Effect of Graphite Concentration on Shear-Wave Speed in Gelatin-Based Tissue-Mimicking Phantoms

PubMed Central

Anderson, Pamela G.; Rouze, Ned C.; Palmeri, Mark L.

2011-01-01

Elasticity-based imaging modalities are becoming popular diagnostic tools in clinical practice. Gelatin-based, tissue mimicking phantoms that contain graphite as the acoustic scattering material are commonly used in testing and validating elasticity-imaging methods to quantify tissue stiffness. The gelatin bloom strength and concentration are used to control phantom stiffness. While it is known that graphite concentration can be modulated to control acoustic attenuation, the impact of graphite concentrationon phantom elasticity has not been characterized in these gelatin phantoms. This work investigates the impact of graphite concentration on phantom shear stiffness as characterized by shear-wave speed measurements using impulsive acoustic-radiation-force excitations. Phantom shear-wave speed increased by 0.83 (m/s)/(dB/(cm MHz)) when increasing the attenuation coefficient slope of the phantom material through increasing graphite concentration. Therefore, gelatin-phantom stiffness can be affected by the conventional ways that attenuation is modulated through graphite concentration in these phantoms. PMID:21710828

Evaluation of the effect of three innovative recyling methods on the shear bond strength of stainless steel brackets-an in vitro study

PubMed Central

Kumar, Dilip; Palla, Aparna

2017-01-01

Background Orthodontists are commonly faced with the decision of what to do with debonded or inaccurately positioned brackets. An economical option to this dilemma is to recycle the brackets. Many recycling methods have been proposed, but the optimal bond strength of these recycled brackets needs further evaluation. Objectives: To evaluate and compare the effect of three recycling methods: (i) Sandblasting (ii) Sandblasting / direct flaming (iii) Sandblasting /direct flaming /acid bath solution on shear bond strength (SBS) of stainless steel brackets. Material and Methods Eighty human premolars were bonded with premolar stainless steel brackets as per manufacturer’s instructions. The teeth were divided into 4 groups (n=20): Recycling and initial debonding was not done in Control group (Group I). After initial bonding, the brackets in the rest of the three experimental groups were debonded and recycled by following methods: (i) Sandblasting (Group II) (ii) Sandblasting /direct flaming (Group III) (iii) Sandblasting /direct flaming /acid bath solution (Group IV). Further the recycled brackets were bonded. The specimens were then subjected to testing in a Universal machine. The evaluation of the variation of the shear bond strength (SBS) among test groups was done using one-way ANOVA test and inter-experimental group comparison was done by Newman-Keuls multiple post hoc procedure. Results Group I (8.6510±1.3943MPa) showed the highest bond strength followed by Group II (5.0185±0.9758MPa), Group IV (2.30±0.65MPa) and Group III (2.0455± 0.6196MPa). Statistically significant variations existed in the shear bond strength (SBS) in all groups analyzed except between Group III and Group IV. Conclusions The following conclusions were drawn from the study: 1. Shear bond strength of new brackets is significantly higher than the recycled brackets. 2. Brackets sandblasted with 90µm aluminium oxide particle air-abrasion showed significantly higher shear bond strength compared to direct flaming/sandblasting and direct flaming/sandblasting/acid bath solution. 3. Sandblasting with 90µm aluminium oxide particle air-abrasion is the simplest, most efficient and hence, the preferred method of recycling debonded brackets. Key words:Orthodontic bracket, recycling, shear bond strength. PMID:28469821

Influence of cobalt, tantaum and tungsten on the high temperature mechanical properties of single crystal nickel-base superalloys. Ph.D. Thesis - Case Western Reserve Univ.

NASA Technical Reports Server (NTRS)

Nathal, M. V.

1984-01-01

For alloys with the baseline refractory metal level of 3 percent Ta and 10 percent W, decreases in Co level from 10 to 0 percent resulted in increased tensile strength and creep resistance. Substitution of W for Ta resulted in decreased creep life at high stresses but improved life at low stresses. Substitution of Ni for Ta caused large reductions in tensile strength and creep resistance, and corresponding increases in ductility. For these alloys with low Ta plus W totals, strength was independent of Co level. The increases in tensile strength with increases in refractory metal content were related to the increases in gamma volume fraction and solid solution hardening. Increases in strength as Co level decreased were considered to be the result of coherency strain hardening from the increased lattice mismatch. Dislocation shear through the gamma-gamma interface is considered to be the rate limiting step in the deformation process.

Testing Bonds Between Brittle And Ductile Films

NASA Technical Reports Server (NTRS)

Wheeler, Donald R.; Ohsaki, Hiroyuki

1989-01-01

Simple uniaxial strain test devised to measure intrinsic shear strength. Brittle film deposited on ductile stubstrate film, and combination stretched until brittle film cracks, then separates from substrate. Dimensions of cracked segments related in known way to tensile strength of brittle film and shear strength of bond between two films. Despite approximations and limitations of technique, tests show it yields semiquantitative measures of bond strengths, independent of mechanical properties of substrates, with results reproducible with plus or minus 6 percent.

Direct Shear Tests of Sandstone Under Constant Normal Tensile Stress Condition Using a Simple Auxiliary Device

NASA Astrophysics Data System (ADS)

Cen, Duofeng; Huang, Da

2017-06-01

Tension-shear failure is a typical failure mode in the rock masses in unloading zones induced by excavation or river incision, etc., such as in excavation-disturbed zone of deep underground caverns and superficial rocks of high steep slopes. However, almost all the current shear failure criteria for rock are usually derived on the basis of compression-shear failure. This paper proposes a simple device for use with a servo-controlled compression-shear testing machine to conduct the tension-shear tests of cuboid rock specimens, to test the direct shear behavior of sandstone under different constant normal tensile stress conditions ( σ = -1, -1.5, -2, -2.5 and -3 MPa) as well as the uniaxial tension behavior. Generally, the fracture surface roughness decreases and the proportion of comminution areas in fracture surface increases as the change of stress state from tension to tension-shear and to compression-shear. Stepped fracture is a primary fracture pattern in the tension-shear tests. The shear stiffness, shear deformation and normal deformation (except the normal deformation for σ = -1 MPa) decrease during shearing, while the total normal deformation containing the pre-shearing portion increases as the normal tensile stress level (| σ|) goes up. Shear strength is more sensitive to the normal tensile stress than to the normal compressive stress, and the power function failure criterion (or Mohr envelope form of Hoek-Brown criterion) is examined to be the optimal criterion for the tested sandstone in the full region of tested normal stress in this study.

Chemical controls on fault behavior: weakening of serpentinite sheared against quartz-bearing rocks and its significance for fault creep in the San Andreas system

USGS Publications Warehouse

Moore, Diane E.; Lockner, David A.

2013-01-01

The serpentinized ultramafic rocks found in many plate-tectonic settings commonly are juxtaposed against crustal rocks along faults, and the chemical contrast between the rock types potentially could influence the mechanical behavior of such faults. To investigate this possibility, we conducted triaxial experiments under hydrothermal conditions (200-350°C), shearing serpentinite gouge between forcing blocks of granite or quartzite. In an ultramafic chemical environment, the coefficient of friction, µ, of lizardite and antigorite serpentinite is 0.5-0.6, and µ increases with increasing temperature over the tested range. However, when either lizardite or antigorite serpentinite is sheared against granite or quartzite, strength is reduced to µ ~ 0.3, with the greatest strength reductions at the highest temperatures (temperature weakening) and slowest shearing rates (velocity strengthening). The weakening is attributed to a solution-transfer process that is promoted by the enhanced solubility of serpentine in pore fluids whose chemistry has been modified by interaction with the quartzose wall rocks. The operation of this process will promote aseismic slip (creep) along serpentinite-bearing crustal faults at otherwise seismogenic depths. During short-term experiments serpentine minerals reprecipitate in low-stress areas, whereas in longer experiments new Mg-rich phyllosilicates crystallize in response to metasomatic exchanges across the serpentinite-crustal rock contact. Long-term shear of serpentinite against crustal rocks will cause the metasomatic mineral assemblages, which may include extremely weak minerals such as saponite or talc, to play an increasingly important role in the mechanical behavior of the fault. Our results may explain the distribution of creep on faults in the San Andreas system.

Rheology of granular materials composed of crushable particles.

PubMed

Nguyen, Duc-Hanh; Azéma, Émilien; Sornay, Philippe; Radjaï, Farhang

2018-04-11

We investigate sheared granular materials composed of crushable particles by means of contact dynamics simulations and the bonded-cell model for particle breakage. Each particle is paved by irregular cells interacting via cohesive forces. In each simulation, the ratio of the internal cohesion of particles to the confining pressure, the relative cohesion, is kept constant and the packing is subjected to biaxial shearing. The particles can break into two or more fragments when the internal cohesive forces are overcome by the action of compressive force chains between particles. The particle size distribution evolves during shear as the particles continue to break. We find that the breakage process is highly inhomogeneous both in the fragment sizes and their locations inside the packing. In particular, a number of large particles never break whereas a large number of particles are fully shattered. As a result, the packing keeps the memory of its initial particle size distribution, whereas a power-law distribution is observed for particles of intermediate size due to consecutive fragmentation events whereby the memory of the initial state is lost. Due to growing polydispersity, dense shear bands are formed inside the packings and the usual dilatant behavior is reduced or cancelled. Hence, the stress-strain curve no longer passes through a peak stress, and a progressive monotonic evolution towards a pseudo-steady state is observed instead. We find that the crushing rate is controlled by the confining pressure. We also show that the shear strength of the packing is well expressed in terms of contact anisotropies and force anisotropies. The force anisotropy increases while the contact orientation anisotropy declines for increasing internal cohesion of the particles. These two effects compensate each other so that the shear strength is nearly independent of the internal cohesion of particles.

Hydraulic and mechanical behavior of landfill clay liner containing SSA in contact with leachate.

PubMed

Zhang, Qian; Lu, Haijun; Liu, Junzhu; Wang, Weiwei; Zhang, Xiong

2018-05-01

Sewage sludge ash (SSA) produced by municipal sludge can be used as a modified additive for clay liner, and improves the working performance of landfill clay liner in contact with leachate. Under the action of landfill leachate, the permeability, shear strength, phase composition, and pore structure of the modified clay are investigated through the flexible wall permeability test, triaxial shear test, thermal gravimetric and differential thermal analysis, and low-temperature nitrogen adsorption test, respectively. The hydraulic conductivity of the modified clay containing 0-5% SSA is in the range of 3.94 × 10 -8 -1.16 × 10 -7  cm/s, and the pollutant concentration of the sample without SSA was higher than others. The shear strength of the modified clay is more than that of the traditional clay liner, the cohesion rate of modified clay increases from 32.5 to 199.91 kPa, and the internal friction angle decreases from 32.5° to 15.6°. Furthermore, the weight loss rates of the samples are 15.69%, 17.92%, 18.06%, and 20.68%, respectively, when the SSA content increases from 0% to 5%. The total pore volume and average pore diameter of the modified clay decrease with the increase in the SSA content, respectively. However, the specific area of the modified clay increases with the increase in the SSA content.

Influence of wood-derived biochar on the compactibility and strength of silt loam soil

NASA Astrophysics Data System (ADS)

Ahmed, Ahmed; Gariepy, Yvan; Raghavan, Vijaya

2017-04-01

Biochar is proven to enhance soil fertility and increase crop productivity. Given that the influence of biochar on soil compaction remains unclear, selected physico-mechanical properties of soil amended with wood-derived biochar were assessed. For unamended silt loam, the bulk density, maximum bulk density, optimum moisture content, plastic limit, liquid limit, and plasticity index were 1.05 Mg m-3, 1.69 Mg m-3, 16.55, 17.1, 29.3, and 12.2%, respectively. The penetration resistance and shear strength of the unamended silt loam compacted in the standard compaction Proctor mold and at its optimum moisture content were 1800 kPa and 850 kPa, respectively. Results from amending the silt loam with 10% particle size ranges (0.5-212 μm) led to relative decreases of 18.1, 17.75, 66.66, and 97.4% in bulk density, maximum bulk density, penetration resistance, and shear strength, respectively; a 26.8% relative increase in optimum moisture content; along with absolute increases in plastic limit, liquid limit, and plasticity index of 5.3, 13.7, and 8.4%, respectively. While the biochar-amended silt loam soil was more susceptible to compaction, however, soil mechanical impedance enhanced.

Shear bond strength of different retainer wires and bonding adhesives in consideration of the pretreatment process.

PubMed

Reicheneder, Claudia; Hofrichter, Bernd; Faltermeier, Andreas; Proff, Peter; Lippold, Carsten; Kirschneck, Christian

2014-11-28

We aimed to compare the shear bond strength (SBS) of three different retainer wires and three different bonding adhesives in consideration of the pretreatment process of enamel surface sandblasting. 400 extracted bovine incisors were divided into 10 groups of 20 paired specimens each. 10 specimens of each group were pretreated by enamel sandblasting. The retainer wires Bond-A-Braid™, GAC-Wildcat®-Twistflex and everStick®ORTHO were bonded to the teeth with the adhesives Transbond™-LR, Tetric-EvoFlow™ and Stick®FLOW and then debonded measuring the SBS. While sandblasting generally increased SBS for all tested combinations, the retainer wires bonded with Transbond™-LR showed the highest SBS both with and without prior sandblasting. Significantly lower SBS were found for Tetric-EvoFlow™ that were comparable to those for everStick®ORTHO. Pretreatment of enamel surfaces by sandblasting increased the SBS of all retainer-wires. Transbond™-LR showed the best results compared to Tetric-EvoFlow™ and everStick®ORTHO, while all combinations used provided sufficient bonding strengths for clinical use.

Theoretical and Experimental Evaluation of the Bond Strength Under Peeling Loads

NASA Technical Reports Server (NTRS)

Nayeb-Hashemi, Hamid; Jawad, Oussama Cherkaoui

1997-01-01

Reliable applications of adhesively bonded joints require understanding of the stress distribution along the bond-line and the stresses that are responsible for the joint failure. To properly evaluate factors affecting peel strength, effects of defects such as voids on the stress distribution in the overlap region must be understood. In this work, the peel stress distribution in a single lap joint is derived using a strength of materials approach. The bonded joint is modeled as Euler-Bernoulli beams, bonded together with an adhesive. which is modeled as an elastic foundation which can resist both peel and shear stresses. It is found that for certain adhesive and adherend geometries and properties, a central void with the size up to 50 percent of the overlap length has negligible effect on the peak peel and shear stresses. To verify the solutions obtained from the model, the problem is solved again by using the finite element method and by treating the adherends and the adhesive as elastic materials. It is found that the model used in the analysis not only predicts the correct trend for the peel stress distribution but also gives rather surprisingly close results to that of the finite element analysis. It is also found that both shear and peel stresses can be responsible for the joint performance and when a void is introduced, both of these stresses can contribute to the joint failure as the void size increases. Acoustic emission (AE) activities of aluminum-adhesive-aluminum specimens with different void sizes were monitored. The AE ringdown counts and energy were very sensitive and decreased significantly with the void size. It was observed that the AE events were shifting towards the edge of the overlap where the maximum peeling and shearing stresses were occurring as the void size increased.

Riveting in metal airplane construction. Part II : riveting methods and equipment (concluded)

NASA Technical Reports Server (NTRS)

Pleines, Wilhelm

1930-01-01

This report includes descriptive material on rivet inspection, types of rivets and sizes. Tabular data on shearing strength of rivets at failure, ultimate shear of various rivets, tensile tests of rivet plate, and tensile strength values of riveted joints.

Effect of Different Anti-Oxidants on Shear Bond Strength of Composite Resins to Bleached Human Enamel

PubMed Central

Saladi, Hari Krishna; Bollu, Indira Priyadarshini; Burla, Devipriya; Ballullaya, Srinidhi Vishnu; Devalla, Srihari; Maroli, Sohani; Jayaprakash, Thumu

2015-01-01

Introduction The bond strength of the composite to the bleached enamel plays a very important role in the success and longevity of an aesthetic restoration. Aim The aim of this study was to compare and evaluate the effect of Aloe Vera with 10% Sodium Ascorbate on the Shear bond strength of composite resin to bleached human enamel. Materials and Methods Fifty freshly extracted human maxillary central incisors were selected and divided into 5 groups. Group I and V are unbleached and bleached controls groups respectively. Group II, III, IV served as experimental groups. The labial surfaces of groups II, III, IV, V were treated with 35% Carbamide Peroxide for 30mins. Group II specimens were subjected to delayed composite bonding. Group III and IV specimens were subjected to application of 10% Sodium Ascorbate and leaf extract of Aloe Vera following the Carbamide Peroxide bleaching respectively. Specimens were subjected to shear bond strength using universal testing machine and the results were statistically analysed using ANOVA test. Tukey (HSD) Honest Significant Difference test was used to comparatively analyse statistical differences between the groups. A p-value <0.05 is taken as statistically significant. Results The mean shear bond strength values of Group V showed significantly lower bond strengths than Groups I, II, III, IV (p-value <0.05). There was no statistically significant difference between the shear bond strength values of groups I, II, III, IV. Conclusion Treatment of the bleached enamel surface with Aloe Vera and 10% Sodium Ascorbate provided consistently better bond strength. Aloe Vera may be used as an alternative to 10% Sodium Ascorbate. PMID:26674656

The Effect of Food-Simulating Agents on the Bond Strength of Hard Chairside Reline Materials to Denture Base Resin.

PubMed

Fatemi, Farzaneh Sadat; Vojdani, Mahroo; Khaledi, Amir Ali Reza

2018-06-08

To investigate the influence of food-simulating agents on the shear bond strength between direct hard liners and denture base acrylic resin. In addition, mode of failure was evaluated. One hundred fifty cylindrical columns of denture base resin were fabricated and bonded to three types of hard reline materials (Hard GC Reline, Tokuyama Rebase II Fast, TDV Cold Liner Rebase). Specimens of each reline material were divided into five groups (n = 10) to undergo 12-day immersion in distilled water, 0.02 N citric acid aqueous solution, heptane, and 40% ethanol/water solution at 37°C. The control group was not immersed in any solution. The shear bond strength test was performed, and the failure mode was determined. Statistics were analyzed with two-way ANOVA and chi-square test (α = 0.05). Significant interaction was found between the hard liners and food simulating agents (p < 0.001). The shear bond strength of Tokuyama in 40% ethanol and TDV in heptane decreased significantly (p = 0.001, p < 0.001 respectively); however, none of the solutions could significantly affect the shear bond strength of Hard GC Reline (p = 0.208). The mixed failure mode occurred more frequently in Hard GC Reline compared with the other liners (p < 0.001) and was predominant in specimens with higher bond strength values (p = 0.012). Food simulating agents did not adversely affect the shear bond strength of Hard GC Reline; however, ethanol and heptane decreased the bond strength of Tokuyama and TDV, respectively. These findings may provide support to dentists to recommend restricted consumption of some foods and beverages for patients who have to use dentures relined with certain hard liners. © 2018 by the American College of Prosthodontists.

Influence of nano-structured alumina coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements.

PubMed

Lee, Jung-Jin; Choi, Jung-Yun; Seo, Jae-Min

2017-04-01

The purpose of this study was to evaluate the effect of nano-structured alumina surface coating on shear bond strength between Y-TZP ceramic and various dual-cured resin cements. A total of 90 disk-shaped zirconia specimens (HASS CO., Gangneung, Korea) were divided into three groups by surface treatment method: (1) airborne particle abrasion, (2) tribochemicalsilica coating, and (3) nano-structured alumina coating. Each group was categorized into three subgroups of ten specimens and bonded with three different types of dual-cured resin cements. After thermocycling, shear bond strength was measured and failure modes were observed through FE-SEM. Two-way ANOVA and the Tukey's HSD test were performed to determine the effects of surface treatment method and type of cement on bond strength ( P <.05). To confirm the correlation of surface treatment and failure mode, the Chi-square test was used. Groups treated with the nanostructured alumina coating showed significantly higher shear bond strength compared to other groups treated with airborne particle abrasion or tribochemical silica coating. Clearfil SA Luting showed a significantly higher shear bond strength compared to RelyX ARC and RelyX Unicem. The cohesive failure mode was observed to be dominant in the groups treated with nano-structured alumina coating, while the adhesive failure mode was prevalent in the groups treated with either airborne particle abrasion or tribochemical silica coating. Nano-structured alumina coating is an effective zirconia surface treatment method for enhancing the bond strength between Y-TZP ceramic and various dual-cured resin cements.

Mechanical evaluation of a tissue-engineered zone of calcification in a bone–hydrogel osteochondral construct

PubMed Central

Hollenstein, Jérôme; Terrier, Alexandre; Cory, Esther; Chen, Albert C.; Sah, Robert L.; Pioletti, Dominique P.

2016-01-01

The objective of this study was to test the hypothesis that mechanical properties of artificial osteochondral constructs can be improved by a tissue-engineered zone of calcification (teZCC) at the bone–hydrogel interface. Experimental push-off tests were performed on osteochondral constructs with or without a teZCC. In parallel, a numerical model of the osteochondral defect treatment was developed and validated against experimental results. Experimental results showed that the shear strength at the bone–hydrogel interface increased by 100% with the teZCC. Numerical predictions of the osteochondral defect treatment showed that the shear stress at the bone–hydrogel interface was reduced with the teZCC. We conclude that a teZCC in osteochondral constructs can provide two improvements. First, it increases the strength of the bone–hydrogel interface and second, it reduces the stress at this interface. PMID:23706035

Microstructure and Interfacial Shear Strength in W/(Zr55Cu30Al10Ni5)100- x Nb x Composites

NASA Astrophysics Data System (ADS)

Mahmoodan, M.; Gholamipour, R.; Mirdamadi, Sh.; Nategh, S.

2017-11-01

In the present study, (Zr55Cu30Al10Ni5)100- x Nb( x=0,1,2,3) bulk metallic glass matrix/tungsten wire composites were fabricated by a gas pressure infiltration process at temperature 950 °C for 5 min. Microstructural studies and mechanical behaviors of the materials have been investigated by scanning electron microscopy, transmission electron microscopy and pullout tests. The mechanical results showed that the interface shear strength in the composite sample with X = 2 increased more than twice compared to the composite sample with X = 0. Based on the microstructural results, the addition of two atomic percent Nb in the matrix composite causes an increase in the diffusion band thickness during the melt infiltration and change in the interface fracture mode as a result of pullout test.

Research on wall shear stress considering wall roughness when shear swirling flow vibration cementing

NASA Astrophysics Data System (ADS)

Cui, Zhihua; Ai, Chi; Feng, Fuping

2017-01-01

When shear swirling flow vibration cementing, the casing is revolving periodically and eccentrically, which leads to the annulus fluid in turbulent swirling flow state. The wall shear stress is more than that in laminar flow field when conventional cementing. The paper mainly studied the wall shear stress distribution on the borehole wall when shear swirling flow vibration cementing based on the finite volume method. At the same time, the wall roughness affected and changed the turbulent flow near the borehole wall and the wall shear stress. Based on the wall function method, the paper established boundary conditions considering the wall roughness and derived the formula of the wall shear stress. The results showed that the wall roughness significantly increases the wall shear stress. However, the larger the wall roughness, the greater the thickness of mud cake, which weakening the cementing strength. Considering the effects in a comprehensive way, it is discovered that the particle size of solid phase in drilling fluid is about 0.1 mm to get better cementing quality.

[In vitro study on shear bond strength of veneering ceramics to zirconia].

PubMed

Hu, Xiaoping; Zhu, Hongshui; Zeng, Liwei

2012-12-01

To investigate the shear bond strength between veneering ceramic and zirconia core in different all-ceramic systems. Twenty disk-shaped specimens with 8 mm in diameter and 3 mm in height for each zirconia system (Lava, Cercon, IPS e.max ZirCAD, Procera) were fabricated respectively and divided into four groups: Lava group, Cercon group, IPS e.max ZirCAD group, Procera group. For each group, 10 specimens were sintered with 1 mm corresponding veneering ceramic, while the other were sintered with 2 mm corresponding veneering ceramic respectively. The shear bond strength and fracture mode of specimens were observed and determined. The values of shear bond strength for Lava, Cercon, IPS e.max ZirCAD and Procera were (13.82 +/- 3.71), (13.24 +/- 2.09), (6.37 +/- 4.15), (5.19 +/- 5.31) MPa in the group of 1 mm thicked veneering ceramics, respectively, while the values in the group of 2mm thicked veneering ceramics were (38.77 +/- 1.69), (21.67 +/- 3.34), (12.70 +/- 4.24), (9.94 +/- 6.67) MPa. The values of Lava and Cercon groups were significantly higher than that of IPS e.max ZirCAD and Procera groups (P < 0.05). And the values of 2 mm thicked veneering ceramic group were significantly higher than that in 1 mm thicked groups (P < 0.05). Adhesive fracture between core and veneering ceramics were observed in the fracture modes of most specimens. The shear bond strength of veneering ceramic to the zirconia framework are different from the zirconia system we chose, and the thickness of veneering ceramic has a great impact on its shear bond strength.

In vitro evaluation of casein phosphopeptide-amorphous calcium phosphate effect on the shear bond strength of dental adhesives to enamel.

PubMed

Shadman, Niloofar; Ebrahimi, Shahram Farzin; Shoul, Maryam Azizi; Sattari, Hasti

2015-01-01

Casein phosphopeptide-amorphous calcium phosphate (CPP-ACP) is applied for remineralization of early caries lesions or tooth sensitivity conditions and may affect subsequent resin bonding. This in vitro study investigated the effect of CPP-ACP on the shear bond strength of dental adhesives to enamel. Sixty extracted human molar teeth were selected and randomly divided into three groups and six subgroups. Buccal or lingual surfaces of teeth were prepared to create a flat enamel surface. Adhesives used were Tetric N-Bond, AdheSE and AdheSE One F. In three subgroups, before applying adhesives, enamel surfaces were treated with Tooth Mousse CPP-ACP for one hour, rinsed and stored in 37°C temperature with 100% humidity. This procedure was repeated for 5 days and then adhesives were applied and Tetric N-Ceram composite was adhered to the enamel. This procedure was also fulfilled for the other three subgroups without CPP-ACP treatment. After 24 hour water storage, samples were tested for shear bond strength test in a universal testing machine. Failure modes were determined by stereomicroscope. Data were analyzed by t-test and one-way analysis of variance with P < 0.05 as the level of significance. In comparison between applied and non-applied CPP-ACP subgroups, there was no significant decrease in the shear bond strength to enamel only in Tetric N-Bond (P > 0.05). In non-applied CPP-ACP subgroups, there were statistically significant differences among all subgroups. Tetric N-Bond had the highest and AdheSE One F had the lowest shear bond strength. CPP-ACP application reduces the shear bond strength of AdheSE and AdheSE One F to enamel but not Tetric N-Bond.

In vitro evaluation of casein phosphopeptide-amorphous calcium phosphate effect on the shear bond strength of dental adhesives to enamel

PubMed Central

Shadman, Niloofar; Ebrahimi, Shahram Farzin; Shoul, Maryam Azizi; Sattari, Hasti

2015-01-01

Background: Casein phosphopeptide-amorphous calcium phosphate (CPP-ACP) is applied for remineralization of early caries lesions or tooth sensitivity conditions and may affect subsequent resin bonding. This in vitro study investigated the effect of CPP-ACP on the shear bond strength of dental adhesives to enamel. Materials and Methods: Sixty extracted human molar teeth were selected and randomly divided into three groups and six subgroups. Buccal or lingual surfaces of teeth were prepared to create a flat enamel surface. Adhesives used were Tetric N-Bond, AdheSE and AdheSE One F. In three subgroups, before applying adhesives, enamel surfaces were treated with Tooth Mousse CPP-ACP for one hour, rinsed and stored in 37°C temperature with 100% humidity. This procedure was repeated for 5 days and then adhesives were applied and Tetric N-Ceram composite was adhered to the enamel. This procedure was also fulfilled for the other three subgroups without CPP-ACP treatment. After 24 hour water storage, samples were tested for shear bond strength test in a universal testing machine. Failure modes were determined by stereomicroscope. Data were analyzed by t-test and one-way analysis of variance with P < 0.05 as the level of significance. Results: In comparison between applied and non-applied CPP-ACP subgroups, there was no significant decrease in the shear bond strength to enamel only in Tetric N-Bond (P > 0.05). In non-applied CPP-ACP subgroups, there were statistically significant differences among all subgroups. Tetric N-Bond had the highest and AdheSE One F had the lowest shear bond strength. Conclusion: CPP-ACP application reduces the shear bond strength of AdheSE and AdheSE One F to enamel but not Tetric N-Bond. PMID:25878683

Mechanical characterization of municipal solid waste from two waste dumps at Delhi, India.

PubMed

Ramaiah, B J; Ramana, G V; Datta, Manoj

2017-10-01

The article presents the physical and mechanical properties of the emplaced municipal solid waste (MSW) recovered from different locations of the Ghazipur and Okhla dumps both located at Delhi, India. Mechanical compressibility and shear strength of the collected MSW were evaluated using a 300×300mm direct shear (DS) shear box. Compression ratio (C c ') of MSW at these two dumps varied between 0.11 and 0.17 and is falling on the lower bound of the range (0.1-0.5) of the data reported in the literature for MSW. Low C c ' of MSW is attributed to the relatively low percentages of compressible elements such as textiles, plastics and paper, coupled with relatively high percentages of inert materials such as soil-like and gravel sized fractions. Shear strength of MSW tested is observed to be displacement dependent. The mobilized shear strength parameters i.e., the apparent cohesion intercept (c') and friction angle (ϕ') of MSW at these two dumps are best characterized by c'=13kPa and ϕ'=23° at 25mm displacement and c'=17kPa and ϕ'=34° at 55mm displacement and are in the range reported for MSW in the literature. A large database on the shear strength of MSW from 18 countries that includes: the experimental data from 277 large-scale DS tests (in-situ and laboratory) and the data from back analysis of 11 failed landfill slopes is statistically analyzed. Based on the analysis, a simple linear shear strength envelope, characterized by c'=17kPa and ϕ'=32°, is proposed for MSW for preliminary use in the absence of site-specific data for stability evaluation of the solid waste landfill under drained conditions. Copyright © 2017 Elsevier Ltd. All rights reserved.

Constitutive Behavior of Reinforced Concrete Membrane Elements under Tri-directional Shear

NASA Astrophysics Data System (ADS)

Labib, Moheb

The two-dimensional behavior of typical reinforced concrete (RC) structures has been extensively studied in the past several decades by investigating the constitutive behavior of full-scale reinforced concrete elements subjected to a bi-axial state of stress. In order to understand the true behavior of many large complex structures, the goal of this investigation is to develop new constitutive relationships for RC elements subjected to tri-directional shear stresses. Recently, additional out-of-plane jacks were installed on the panel tester at University of Houston so that concrete elements could be subjected to tri-directional shear stresses. This upgrade makes the panel tester the only one of its kind in the US that is capable of applying such combinations of stresses on full-scale reinforced concrete elements. This dissertation presents the details of the mounting and installation of the additional hydraulic jacks on the universal panel tester. The experimental program includes a series of seven reinforced concrete elements subjected to different combinations of in-plane and out-of-plane shear stresses. Increasing the applied out-of-plane shear stresses reduced the membrane shear strength of the elements. The effect of applying out-of-plane shear stresses on the in-plane shear strength was represented by modifying the softening coefficient in the compression stress strain curve of concrete struts. The modified model was able to capture the behavior and the ultimate capacity of the tested elements. The effect of the in-plane shear reinforcement ratio on the interaction between in-plane and out-of-plane shear stresses was evaluated. The model was implemented in the Finite Element package FEAP and was used to predict the ultimate capacity of many structures subjected to a combination of in-plane and out-of-plane shear stresses. The results of the analytical model were used to develop simplified design equations for members subjected to bi-directional shear loads. The applied out-of-plane shear load was resolved in two equal out-of-plane shear components to construct tri-directional shear interaction diagrams.

Deformation mechanisms of antigorite and strain localization during dehydration

NASA Astrophysics Data System (ADS)

Proctor, B.; Hirth, G.

2012-12-01

Antigorite, the high temperature and pressure serpentine polytype, is thought to exist along subduction zones between the mantle wedge and the subducting oceanic crust (e.g., Wada et al., 2008). Understanding how the rheology of antigorite changes with depth along the slab may be key to understanding seismicity along the upper plate boundary (e.g., Hacker et al., 2003). To explore this phenomenon we are conducting constant strain rate general shear experiments on antigorite-rich serpentinite at shear strain rates of 5*10^-7/s to 10^-5/s, confining pressures from 1-2 GPa and temperatures from 400-700°C. We are using microstructural observations to constrain deformation mechanisms and investigate conditions where strain localization occurs. In some experiments we employ either strain rate stepping or temperature ramping to examine the stress dependence of viscosity (i.e., determine stress exponent) and syntectonic reaction during heating. The results of our general shear experiments suggest the rheologic behavior of antigorite varies significantly with changes in temperature and pressure, similar to previous work in axial compression (e.g., Chernak and Hirth, 2010). At 400°C and 1GPa confining pressure antigorite deforms initially via steady-state ductile flow with strengths as high as 1.4 GPa at a strain rate of 10^-5/s. With increasing strain we observe weakening events that correlate with the development of shear fractures within the sample. At 2GPa pressure, the flow strength of antigorite increases to ~1.8 GPa at 10^-6/s and deformation is distributed at low strain. Strain rate stepping at these conditions suggests a very weak strain rate dependence on strength with a 5-10% change in stress for an order of magnitude strain rate step. At 700C and 1 GPa, above the thermal stability of antigorite, the steady-state strength is ~120 MPa at 10^-5/s. In these samples olivine becomes the dominant phase as antigorite progressively reacts to olivine and pyroxene. At the sample scale, strain is relatively homogeneous. However, microstructural observation indicates that deformation tends to be localized along "Riedel-like" shear zones that develop within the sample with a spacing of ~100 μm and an orientation of ~25° with respect to the sample orientation (45° from σ1). In a temperature ramp, from 400°C to 700°C at 1 GPa and 10^-5/s strain rate, the antigorite strength decreases rapidly to ~120 MPa and strain localizes within shear fractures that correlate with the onset of thermal weakening (similar to Chernak and Hirth, 2010). To a first order our finding suggest complications with the antigorite flow law established by Hilairet et al., (2007). We find that the flow law grossly underestimates the steady-state flow strength of antigorite and we question whether strain can be fully accommodated by crystal plastic deformation.

The influence of adding modified zirconium oxide-titanium dioxide nano-particles on mechanical properties of orthodontic adhesive: an in vitro study.

PubMed

Felemban, Nayef H; Ebrahim, Mohamed I

2017-01-13

The purpose of this in-vitro study was to examine the effect of incorporating different concentrations of Zirconium oxide-Titanium dioxide (ZrO2-TiO2) nanoparticles, which can have antibacterial properties, on the mechanical properties of an orthodontic adhesive. ZrO2-TiO2 (Zirconium oxide, HWNANO, Hongwu International Group Ltd, China) -Titanium dioxide, Nanoshell, USA) nanopowder were incorporated into orthodontic adhesive (Transbond XT, 3 M Unitek, Monrovia, USA) with different concentrations (0.5% weight nonofiller and 1% weight nanofiller). The size of nanoparticle was 70-80 nm for ZrO2 and less than 50 nm for TiO2. For measuring the shear bond strength of the three groups of orthodontic adhesives [Transbond (control), Transbond mixed with 0.5% weight ZrO2-TiO2, and Transbond mixed with 1% weight ZrO2-TiO2], 30 freshly extracted human first premolars were used and bonded with stainless steel metal brackets (Dentaurum®, Discovery®, Deutschland), using the 3 orthodontic adhesives and 3 M Unitek; Transbond TM Plus Self-Etching Primer (10 samples in each group). The recorded values of compressive strength and tensile strength (measured separately on 10 samples of orthodontic adhesives (add the 3 D size of sample, light cured for 40 s on both sides) of each orthodontic adhesives), as well as the shear bond strength in Mega Pascal unit (MPa) were collected and exposed to one-way analysis of variance (ANOVA) and Tukey's post-hoc tests. orthodontic adhesive with 1% weight ZrO2-TiO2 showed the highest mean compressive (73.42 ± 1.55 MPa, p: 0.003, F: 12.74), tensile strength (8.65 ± 0.74 MPa, p: 0.001, F: 68.20), and shear bond strength (20.05 ± 0.2 MPa, p: 0.001, F: 0.17). Adding ZrO2-TiO2 nanoparticle to orthodontic adhesive increased compressive strength, tensile strength, and shear bond strength in vitro, but in vivo studies and randomized clinical trials are needed to validate the present findings.

Microstructural Characteristics of High Rate Plastic Deformation in Elektron (trademark) WE43 Magnesium Alloy

DTIC Science & Technology

2012-04-01

extremely lightweight metal , weighing 30% less than aluminum, and 70% less than steel, it also has the highest strength-to-weight ratio among any of the...commonly used non- ferrous and ferrous metallic materials [2]. As magnesium is used more often in structural components, there is an increasing...mechanism of deformation in metals has been shown to be shear localization [6] [7]. The shear localization seen in high strain rate deformation is

Influence of interfacial shear strength on the mechanical properties of SiC fiber reinforced reaction-bonded silicon nitride matrix composites

NASA Technical Reports Server (NTRS)

Bhatt, Ramakrishna T.

1990-01-01

The influence of fiber/matrix interface microstructure and interfacial shear strength on the mechanical properties of a fiber-reinforced ceramic composite was evaluated. The composite consisted of approximately 30 vol percent uniaxially aligned 142 microns diameter SiC fibers (Textron SCS-6) in a reaction-bonded Si3N4 matrix (SiC/RBSN). The interface microstructure was varied by controlling the composite fabrication conditions and by heat treating the composite in an oxidizing environment. Interfacial shear strength was determined by the matrix crack spacing method. The results of microstructural examination indicate that the carbon-rich coating provided with the as-produced SiC fibers was stable in composites fabricated at 1200 C in a nitrogen or in a nitrogen plus 4 percent hydrogen mixture for 40 hr. However this coating degraded in composites fabricated at 1350 C in N2 + 4 percent H2 for 40 and 72 hr and also in composites heat treated in an oxidizing environment at 600 C for 100 hr after fabrication at 1200 C in a nitrogen. It was determined that degradation occurred by carbon removal which in turn had a strong influence on interfacial shear strength and other mechanical properties. Specifically, as the carbon coating was removed, the composite interfacial shear strength, primary elastic modulus, first matrix cracking stress, and ultimate tensile strength decreased, but the first matrix cracking strain remained nearly the same.

Improved correlation between Texas cone penetrometer blow count and undrained shear strength of soft clays.

DOT National Transportation Integrated Search

2009-01-01

The objective of this project was to develop an improved correlation between Texas Cone Penetrometer (TCP) : blow count and undrained shear strength for soft, clay soils in the upper approximately 30 feet of the ground. Subsurface : explorations were...

Controlled Release in Transdermal Pressure Sensitive Adhesives using Organosilicate Nanocomposites

PubMed Central

Shaikh, Sohel; Birdi, Anil; Qutubuddin, Syed; Lakatosh, Eric; Baskaran, Harihara

2010-01-01

Polydimethyl siloxane (PDMS) based pressure sensitive adhesives (PSA) incorporating organo-clays at different loadings were fabricated via solution casting. Partially exfoliated nanocomposites were obtained for the hydroxyl terminated PDMS in ethyl acetate solvent as determined by X-ray diffraction (XRD) and atomic force microscopy (AFM). Drug release studies showed that the initial burst release was substantially reduced and the drug release could be controlled by the addition of organo-clay. Shear strength and shear adhesion failure temperature (SAFT) measurements indicated substantial improvement in adhesive properties of the PSA nanocomposite adhesives. Shear strength showed more than 200 % improvement at the lower clay loadings and the SAFT increased by about 21% due to the reinforcement provided by the nano-dispersed clay platelets. It was found that by optimizing the level of the organosilicate additive to the polymer matrix, superior control over drug release kinetics and simultaneous improvements in adhesive properties could be attained for a transdermal PSA formulation. PMID:17786555

Process parameter effects on material removal in magnetorheological finishing of borosilicate glass.

PubMed

Miao, Chunlin; Lambropoulos, John C; Jacobs, Stephen D

2010-04-01

We investigate the effects of processing parameters on material removal for borosilicate glass. Data are collected on a magnetorheological finishing (MRF) spot taking machine (STM) with a standard aqueous magnetorheological (MR) fluid. Normal and shear forces are measured simultaneously, in situ, with a dynamic dual load cell. Shear stress is found to be independent of nanodiamond concentration, penetration depth, magnetic field strength, and the relative velocity between the part and the rotating MR fluid ribbon. Shear stress, determined primarily by the material mechanical properties, dominates removal in MRF. The addition of nanodiamond abrasives greatly enhances the material removal efficiency, with the removal rate saturating at a high abrasive concentration. The volumetric removal rate (VRR) increases with penetration depth but is insensitive to magnetic field strength. The VRR is strongly correlated with the relative velocity between the ribbon and the part, as expected by the Preston equation. A modified removal rate model for MRF offers a better estimation of MRF removal capability by including nanodiamond concentration and penetration depth.

Mechanical and thermal buckling analysis of sandwich panels under different edge conditions

NASA Technical Reports Server (NTRS)

Ko, William L.

1993-01-01

By using the Rayleigh-Ritz method of minimizing the total potential energy of a structural system, combined load (mechanical or thermal load) buckling equations are established for orthotropic rectangular sandwich panels supported under four different edge conditions. Two-dimensional buckling interaction curves and three dimensional buckling interaction surfaces are constructed for high-temperature honeycomb-core sandwich panels supported under four different edge conditions. The interaction surfaces provide easy comparison of the panel buckling strengths and the domains of symmetrical and antisymmetrical buckling associated with the different edge conditions. Thermal buckling curves of the sandwich panels also are presented. The thermal buckling conditions for the cases with and without thermal moments were found to be identical for the small deformation theory. In sandwich panels, the effect of transverse shear is quite large, and by neglecting the transverse shear effect, the buckling loads could be overpredicted considerably. Clamping of the edges could greatly increase buckling strength more in compression than in shear.

Elasticity dominates strength and failure in metallic glasses

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liu, Z. Q.; Qu, R. T.; Zhang, Z. F., E-mail: zhfzhang@imr.ac.cn

2015-01-07

Two distinct deformation mechanisms of shearing and volume dilatation are quantitatively analyzed in metallic glasses (MGs) from the fundamental thermodynamics. Their competition is deduced to intrinsically dominate the strength and failure behaviors of MGs. Both the intrinsic shear and normal strengths give rise to the critical mechanical energies to activate destabilization of amorphous structures, under pure shearing and volume dilatation, respectively, and can be determined in terms of elastic constants. By adopting an ellipse failure criterion, the strength and failure behaviors of MGs can be precisely described just according to their shear modulus and Poisson's ratio without mechanical testing. Quantitativemore » relations are established systematically and verified by experimental results. Accordingly, the real-sense non-destructive failure prediction can be achieved in various MGs. By highlighting the broad key significance of elasticity, a “composition-elasticity-property” scheme is further outlined for better understanding and controlling the mechanical properties of MGs and other glassy materials from the elastic perspectives.« less

[Comparative study of 4 types of luting cements on shear bond strength of Zirconia ceramics to dentin].

PubMed

Yin, Bao-di; Zhang, Xian-fang; Zheng, Hu; Han, Dong-wei

2010-04-01

To investigate the adequate luting cements for zirconia ceramics to dentin. Blocks of sintered zirconia ceramics were randomly divided into 4 groups with 8 slices in each. After saliva immersion,airborne-particle abraded ceramic specimens were cleaned with phosphoric acid gel(containing 35% phosphoric acid) and then bonded to dentin with these four kinds of luting cements. After preserved in 37 degrees centigrade distilled water for 24 hours, the shear bonding strength of these specimens was tested and the data was analyzed with SPSS12.0 software package. The Multilink Automix could attain the highest shear bonding strength and the 3M RelyXTM Unicem AplicapTM could attain higher shear bonding strength, which were both significantly higher than in the Tokuso Ionomer and Shofu Polycarboxylate Cement groups(P<0.05). Total etching resin luting cement is an ideal option to the bonding of zirconia ceramics and can provide a strong bonding.

Pressure and temperature dependence of shear modulus and yield strength for aluminum, copper, and tungsten under shock compression

DOE Office of Scientific and Technical Information (OSTI.GOV)

Peng Jianxiang; Jing Fuqian; Li Dahong

2005-07-01

Experimental data for the shear modulus and yield strength of shocked aluminum, copper, and tungsten were systematically analyzed. Comparisons between these data and calculations using the Steinberg-Cochran-Guinan (SCG) constitutive model [D. J. Steinberg, S. G. Cochran, and M. W. Guinan, J. Appl. Phys. 51, 1498 (1980)] indicate that the yield strength has the same dependence on pressure and temperature as the shear modulus for aluminum for shock pressures up to 50 GPa, for copper to 100 GPa, and for tungsten to 200 GPa. Therefore, the assumption of Y{sub p}{sup '}/Y{sub 0}=G{sub p}{sup '}/G{sub 0},Y{sub T}{sup '}/Y{sub 0}=G{sub T}{sup '}/G{sub 0}more » is basically acceptable for these materials, and the SCG model can be used to describe the shear modulus and yield strength of the shocked material at high pressure and temperature.« less

Shear bond strengths of an indirect composite layering material to a tribochemically silica-coated zirconia framework material.

PubMed

Iwasaki, Taro; Komine, Futoshi; Fushiki, Ryosuke; Kubochi, Kei; Shinohara, Mitsuyo; Matsumura, Hideo

2016-01-01

This study evaluated shear bond strengths of a layering indirect composite material to a zirconia framework material treated with tribochemical silica coating. Zirconia disks were divided into two groups: ZR-PRE (airborne-particle abrasion) and ZR-PLU (tribochemical silica coating). Indirect composite was bonded to zirconia treated with one of the following primers: Clearfil Ceramic Primer (CCP), Clearfil Mega Bond Primer with Clearfil Porcelain Bond Activator (MGP+Act), ESPE-Sil (SIL), Estenia Opaque Primer, MR. Bond, Super-Bond PZ Primer Liquid A with Liquid B (PZA+PZB), and Super-Bond PZ Primer Liquid B (PZB), or no treatment. Shear bond testing was performed at 0 and 20,000 thermocycles. Post-thermocycling shear bond strengths of ZR-PLU were higher than those of ZR-PRE in CCP, MGP+Act, SIL, PZA+PZB, and PZB groups. Application of silane yielded better durable bond strengths of a layering indirect composite material to a tribochemically silica-coated zirconia framework material.

Effect of surface roughness of hydroxyapatite-coated titanium on the bone-implant interface shear strength.

PubMed

Hayashi, K; Inadome, T; Tsumura, H; Nakashima, Y; Sugioka, Y

1994-11-01

We have investigated the bone-implant interface shear strength of hydroxyapatite (HA)-coated Ti-6Al-4V (HA-coating A) (roughness average, Ra = 3.4 +/- 0.5 microns) and HA-coated Ti-6Al-4V with a rougher surface (HA-coating B) (Ra = 8.4 +/- 1.8 microns). There was no significant difference between HA-coating A and HA-coating B implants with respect to the bone-implant interface shear strength as determined in push-out tests using the transcortical model in adult dogs. The bone-implant interface shear strength of bead-coated porous Ti-6Al-4V was significantly greater than that of both HA-coating A and HA-coating B implants. The failure site, as determined by scanning electron microscopy, was the coating-substrate interface, not the coating-bone interface. This indicates a need to protect the HA coating from the direct shear forces. HA coating enhances early bone growth into the porous surface of the implant. Long-term fixation should depend on bone anchoring to this porous surface. Hydroxyapatite coatings must be developed which do not obstruct the pores of the surface of the implant.

Influence of Nd:YAG laser on the bond strength of self-etching and conventional adhesive systems to dental hard tissues.

PubMed

Marimoto, A K; Cunha, L A; Yui, K C K; Huhtala, M F R L; Barcellos, D C; Prakki, A; Gonçalves, S E P

2013-01-01

The aim of this study was to investigate the influence of Nd:YAG laser on the shear bond strength to enamel and dentin of total and self-etch adhesives when the laser was applied over the adhesives, before they were photopolymerized, in an attempt to create a new bonding layer by dentin-adhesive melting. One-hundred twenty bovine incisors were ground to obtain flat surfaces. Specimens were divided into two substrate groups (n=60): substrate E (enamel) and substrate D (dentin). Each substrate group was subdivided into four groups (n=15), according to the surface treatment accomplished: X (Xeno III self-etching adhesive, control), XL (Xeno III + laser Nd:YAG irradiation at 140 mJ/10 Hz for 60 seconds + photopolymerization, experimental), S (acid etching + Single Bond conventional adhesive, Control), and SL (acid etching + Single Bond + laser Nd:YAG at 140 mJ/10 Hz for 60 seconds + photopolymerization, experimental). The bonding area was delimited with 3-mm-diameter adhesive tape for the bonding procedures. Cylinders of composite were fabricated on the bonding area using a Teflon matrix. The teeth were stored in water at 37°C/48 h and submitted to shear testing at a crosshead speed of 0.5 mm/min in a universal testing machine. Results were analyzed with three-way analysis of variance (ANOVA; substrate, adhesive, and treatment) and Tukey tests (α=0.05). ANOVA revealed significant differences for the substrate, adhesive system, and type of treatment: lased or unlased (p<0.05). The mean shear bond strength values (MPa) for the enamel groups were X=20.2 ± 5.61, XL=23.6 ± 4.92, S=20.8 ± 4.55, SL=22.1 ± 5.14 and for the dentin groups were X=14.1 ± 7.51, XL=22.2 ± 6.45, S=11.2 ± 5.77, SL=15.9 ± 3.61. For dentin, Xeno III self-etch adhesive showed significantly higher shear bond strength compared with Single Bond total-etch adhesive; Nd:YAG laser irradiation showed significantly higher shear bond strength compared with control (unlased). Nd:YAG laser application prior to photopolymerization of adhesive systems significantly increased the bond strength to dentin.

Strength of laser welded joints of polypropylene composites

NASA Astrophysics Data System (ADS)

Votrubec, V.; Hisem, P.; Vinšová, L.; Lukášová, V.

2017-11-01

This paper deals with experimental tests of laser welded polypropylene composites. Polymers, such as polypropylene, are often filled with fibres in order to increase their mechanical properties. The welding procedure can also influence material properties nearby weld joints. Therefore the strength of weld joints is lower than strength of primary materials. This effect is proved by realized shear tests. Polymer specimens were filled with 20 % and 40 % of glass fibres and all possible combinations of specimens were welded for experiments. There is also discussed influence of volume fraction of glass fibres in polypropylene on the strength of weld joint.

Effect of CPP-ACP paste with and without CO2 laser irradiation on demineralized enamel microhardness and bracket shear bond strength

PubMed Central

Farhadian, Nasrin; Rezaei-Soufi, Loghman; Jamalian, Seyed Farzad; Farhadian, Maryam; Tamasoki, Shahrzad; Malekshoar, Milad; Javanshir, Bahareh

2017-01-01

ABSTRACT Introduction: Many patients seeking orthodontic treatment already have incipient enamel lesions and should be placed under preventive treatments. The aim of this in vitro study was to evaluate the effect of CPP-ACP paste and CO2 laser irradiation on demineralized enamel microhardness and shear bond strength of orthodontic brackets. Methods: Eighty caries-free human premolars were subjected to a demineralization challenge using Streptococcus mutans. After demineralization, the samples were randomly divided into five equal experimental groups: Group 1 (control), the brackets were bonded without any surface treatment; Group 2, the enamel surfaces were treated with CPP-ACP paste for 4 minutes before bonding; Group 3, the teeth were irradiated with CO2 laser beams at a wavelength of 10.6 µm for 20 seconds. The samples in Groups 4 and 5 were treated with CO2 laser either before or through CPP-ACP application. SEM photomicrographs of a tooth from each group were taken to observe the enamel surface. The brackets were bonded to the buccal enamel using a conventional method. Shear bond strength of brackets and ARI scores were measured. Vickers microhardness was measured on the non-bonded enamel surface. Data were analyzed with ANOVA and Tukey test at the p< 0.05 level. Results: The mean shear bond strength and microhardness of the laser group were higher than those in the control group and this difference was statistically significant (p< 0.05). All groups showed a higher percentage of ARI score 4. Conclusion: CO2 laser at a wavelength of 10.6 µm significantly increased demineralized enamel microhardness and enhanced bonding to demineralized enamel. PMID:28902250

Supercritical CO2 fluid-foaming of polymers to increase porosity: a method to improve the mechanical and biocompatibility characteristics for use as a potential alternative to allografts in impaction bone grafting?

PubMed

Tayton, Edward; Purcell, M; Aarvold, A; Smith, J O; Kalra, S; Briscoe, A; Shakesheff, K; Howdle, S M; Dunlop, D G; Oreffo, R O C

2012-05-01

Disease transmission, availability and cost of allografts have resulted in significant efforts to find an alternative for use in impaction bone grafting (IBG). Recent studies identified two polymers with both structural strength and biocompatibility characteristics as potential replacements. The aim of this study was to assess whether increasing the polymer porosity further enhanced the mechanical and cellular compatibility characteristics for use as an osteogenic biomaterial alternative to allografts in IBG. Solid and porous poly(DL-lactide) (P(DL)LA) and poly(DL-lactide-co-glycolide) (P(DL)LGA) scaffolds were produced via melt processing and supercritical CO(2) foaming, and the differences characterized using scanning electron microscopy (SEM). Mechanical testing included milling and impaction, with comparisons made using a shear testing rig as well as a novel agitation test for cohesion. Cellular compatibility tests for cell number, viability, and osteogenic differentiation using WST-1 assays, fluorostaining, and ALP assays were determined following 14 day culture with skeletal stem cells. SEM showed excellent porosity throughout both of the supercritical-foam-produced polymer scaffolds, with pores between 50 and 200 μm. Shear testing showed that the porous polymers exceeded the shear strength of allograft controls (P<0.001). Agitation testing showed greater cohesion between the particles of the porous polymers (P<0.05). Cellular studies showed increased cell number, viability, and osteogenic differentiation on the porous polymers compared to solid block polymers (P<0.05). The use of supercritical CO(2) to generate porous polymeric biodegradable scaffolds significantly improves the cellular compatibility and cohesion observed compared to non-porous counterparts, without substantial loss of mechanical shear strength. These improved characteristics are critical for clinical translation as a potential osteogenic composite for use in IBG. Copyright © 2012 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Shear bond strength of veneering porcelain to zirconia: Effect of surface treatment by CNC-milling and composite layer deposition on zirconia.

PubMed

Santos, R L P; Silva, F S; Nascimento, R M; Souza, J C M; Motta, F V; Carvalho, O; Henriques, B

2016-07-01

The purpose of this study was to evaluate the shear bond strength of veneering feldspathic porcelain to zirconia substrates modified by CNC-milling process or by coating zirconia with a composite interlayer. Four types of zirconia-porcelain interface configurations were tested: RZ - porcelain bonded to rough zirconia substrate (n=16); PZ - porcelain bonded to zirconia substrate with surface holes (n=16); RZI - application of a composite interlayer between the veneering porcelain and the rough zirconia substrate (n=16); PZI - application of a composite interlayer between the porcelain and the zirconia substrate treated by CNC-milling (n=16). The composite interlayer was composed of zirconia particles reinforced porcelain (30%, vol%). The mechanical properties of the ceramic composite have been determined. The shear bond strength test was performed at 0.5mm/min using a universal testing machine. The interfaces of fractured and untested specimens were examined by FEG-SEM/EDS. Data was analyzed with Shapiro-Wilk test to test the assumption of normality. The one-way ANOVA followed by Tukey HSD multiple comparison test was used to compare shear bond strength results (α=0.05). The shear bond strength of PZ (100±15MPa) and RZI (96±11MPa) specimens were higher than that recorded for RZ (control group) specimens (89±15MPa), although not significantly (p>0.05). The highest shear bond strength values were recorded for PZI specimens (138±19MPa), yielding a significant improvement of 55% relative to RZ specimens (p<0.05). This study shows that it is possible to highly enhance the zirconia-porcelain bond strength - even by ~55% - by combining surface holes in zirconia frameworks and the application of a proper ceramic composite interlayer. Copyright © 2016 Elsevier Ltd. All rights reserved.

In vitro Assessment of Influence of Various Bleaching Protocols on the Strength of Ceramic Orthodontic Brackets bonded to Bleached Tooth Surface: A Comparative Study.

PubMed

Iska, Divya; Devanna, Raghu; Singh, Madhvi; Chitumalla, Rajkiran; Balasubramanian, Sai C Bala; Goutam, Manish

2017-12-01

Esthetics is one of the common issues because of which patients consult dental orthodontic treatment. Two ways of tooth bleaching are available these days, which includes in-office bleach and home bleach. Various bleaching protocols are available these days for treating the tooth surfaces. Hence, we planned the present study for investigating the impact of various intracoronal bleaching protocols on shear bond strength of ceramic brackets bonded to tooth surface after bleaching. The present study included assessment of 100 extracted maxillary central incisors with the integrated buccal surface. A resin block was made and individual teeth were embedded in each block. Root canal therapy procedure was performed in all the teeth, after which 2 mm short of tooth apex up to the level of cementoenamel junction, removal of the root canal filling was done. All the samples were broadly divided into four study groups with 25 samples in each group. Bleaching procedure was carried in all the samples intracoronally followed by testing of shear bond strength using universal force testing machine. Following the modified adhesive remnant index (AI), assessment of remaining adhesive on the brackets was done. All the results were compiled and analyzed by Statistical Package for the Social Sciences (SPSS) software version 17.0. In the control group, mean shear bond strength was found to be 17.9 MPa. While comparing the carbamide peroxide (CP) group with sodium perborate study group, we observed a statistically significant difference. Nonsignificant results were obtained while comparing the shear bond strength in between sodium perborate group and hydrogen peroxide (HP) group. Intracoronal bleaching does affect the shear bond strength of ceramic brackets. Sodium perborate bleaching influences shear bond strength more strongly than other bleaching agents such as CP and HP. In patients undergoing orthodontic treatment, HP is a preferred agent where bleaching has to be followed by orthodontic bonding to the tooth surface.

Simulation of cemented granular materials. I. Macroscopic stress-strain response and strain localization.

PubMed

Estrada, Nicolas; Lizcano, Arcesio; Taboada, Alfredo

2010-07-01

This is the first of two papers investigating the mechanical response of cemented granular materials by means of contact dynamics simulations. In this paper, a two-dimensional polydisperse sample with high-void ratio is constructed and then sheared in a simple shear numerical device at different confinement levels. We study the macroscopic response of the material in terms of mean and deviatoric stresses and strains. We show that the introduction of a local force scale, i.e., the tensile strength of the cemented bonds, causes the material to behave in a rigid-plastic fashion, so that a yield surface can be easily determined. This yield surface has a concave-down shape in the mean:deviatoric stress plane and it approaches a straight line, i.e., a Coulomb strength envelope, in the limit of a very dense granular material. Beyond yielding, the cemented structure gradually degrades until the material eventually behaves as a cohesionless granular material. Strain localization is also investigated, showing that the strains concentrate in a shear band whose thickness increases with the confining stress. The void ratio inside the shear band at the steady state is shown to be a material property that depends only on contact parameters.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, B.; The Peac Institute of Multiscale Sciences, Chengdu, Sichuan 610207; Wang, L.

With large-scale molecular dynamics simulations, we investigate shock response of He nanobubbles in single crystal Cu. For sufficient bubble size or internal pressure, a prismatic dislocation loop may form around a bubble in unshocked Cu. The internal He pressure helps to stabilize the bubble against plastic deformation. However, the prismatic dislocation loops may partially heal but facilitate nucleation of new shear and prismatic dislocation loops. For strong shocks, the internal pressure also impedes internal jetting, while a bubble assists local melting; a high speed jet breaks a He bubble into pieces dispersed among Cu. Near-surface He bubbles may burst andmore » form high velocity ejecta containing atoms and small fragments, while the ejecta velocities do not follow the three-dimensional Maxwell-Boltzmann distributions expected for thermal equilibrium. The biggest fragment size deceases with increasing shock strength. With a decrease in ligament thickness or an increase in He bubble size, the critical shock strength required for bubble bursting decreases, while the velocity range, space extension and average velocity component along the shock direction, increase. Small bubbles are more efficient in mass ejecting. Compared to voids and perfect single crystal Cu, He bubbles have pronounced effects on shock response including bubble/void collapse, Hugoniot elastic limit (HEL), deformation mechanisms, and surface jetting. HEL is the highest for perfect single crystal Cu with the same orientations, followed by He bubbles without pre-existing prismatic dislocation loops, and then voids. Complete void collapse and shear dislocations occur for embedded voids, as opposed to partial collapse, and shear and possibly prismatic dislocations for He bubbles. He bubbles lower the threshhold shock strength for ejecta formation, and increase ejecta velocity and ejected mass.« less

Effects of biochar amendment on geotechnical properties of landfill cover soil.

PubMed

Reddy, Krishna R; Yaghoubi, Poupak; Yukselen-Aksoy, Yeliz

2015-06-01

Biochar is a carbon-rich product obtained when plant-based biomass is heated in a closed container with little or no available oxygen. Biochar-amended soil has the potential to serve as a landfill cover material that can oxidise methane emissions for two reasons: biochar amendment can increase the methane retention time and also enhance the biological activity that can promote the methanotrophic oxidation of methane. Hydraulic conductivity, compressibility and shear strength are the most important geotechnical properties that are required for the design of effective and stable landfill cover systems, but no studies have been reported on these properties for biochar-amended landfill cover soils. This article presents physicochemical and geotechnical properties of a biochar, a landfill cover soil and biochar-amended soils. Specifically, the effects of amending 5%, 10% and 20% biochar (of different particle sizes as produced, size-20 and size-40) to soil on its physicochemical properties, such as moisture content, organic content, specific gravity and pH, as well as geotechnical properties, such as hydraulic conductivity, compressibility and shear strength, were determined from laboratory testing. Soil or biochar samples were prepared by mixing them with 20% deionised water based on dry weight. Samples of soil amended with 5%, 10% and 20% biochar (w/w) as-is or of different select sizes, were also prepared at 20% initial moisture content. The results show that the hydraulic conductivity of the soil increases, compressibility of the soil decreases and shear strength of the soil increases with an increase in the biochar amendment, and with a decrease in biochar particle size. Overall, the study revealed that biochar-amended soils can possess excellent geotechnical properties to serve as stable landfill cover materials. © The Author(s) 2015.

Influence of hydrophilic pre-treatment on resin bonding to zirconia ceramics.

PubMed

Noro, Akio; Kameyama, Atsushi; Haruyama, Akiko; Takahashi, Toshiyuki

2015-01-01

Atmospheric plasma or ultraviolet (UV) treatment alters the surface characteristics of tetragonal zirconia polycrystal (TZP), increasing its hydrophilicity by reducing the contact angle against water to zero. This suggests that such treatment would increase the wettability of bonding resin. The purpose of this study was to determine how increasing the hydrophilicity of TZP through plasma irradiation, UV treatment, or application of ceramic primer affected initial bonding with resin composites. Here, the effect of each pre-treatment on the hydrophilicity of TZP surfaces was determined by evaluating change in shear bond strength. Plasma irradiation, UV, or ceramic primer pre-treatment showed no significant effect on bonding strength between TZP surfaces and resin composites. In addition, alumina blasting yielded no significant increase in bond strength. Plasma irradiation, UV treatment, or ceramic primer pre-treatment did not lead to significant increase in bond strength between TZP and resin composites.

Evaluation of wick drain performance in Virginia soils.

DOT National Transportation Integrated Search

2003-01-01

Prefabricated vertical drains (PVD), also known as wick drains, are commonly used to accelerate the consolidation of fine-grained soils in order to reduce future settlements and increase shear strength. Various drain designs are currently on the mark...

The effect of three variables on shear bond strength when luting a resin inlay to dentin.

PubMed

Lee, Jae-Ik; Park, Sung-Ho H

2009-01-01

The current study evaluated the effects of three variables on the shear bond strength of indirect composite restorations to human dentin. The three variables examined included immediate dentin sealing (IDS), the thinning of dentin adhesives by air-blowing before cementation and light-curing the dentin adhesive before cementation. One-hundred and eighty cylinder composite inlays, 2 mm in diameter and 3 mm in length, were made using a Tescera ATL system (BISCO Inc). Tooth disks 2-mm thick were obtained from 90 freshly-extracted human premolars. Two indirect composite cylinders were assigned to a single tooth disk. The discs were randomly divided into six groups according to the luting methods. AdheSE (Ivoclar Vivadent) was used as the dentin-bonding agent (DBA) for all groups. In Groups 1, 2 and 3, the dentin was sealed with AdheSE before taking the impression. After priming, the adhesive was lightly air-blown, then light-cured. On the other hand, the dentin was not sealed before taking the impression in Groups 4, 5 and 6. Regarding the application of DBA before cementation, it was gently air-blown and light-cured before cementation in Groups 1 and 4; whereas, it was heavily air-blown and light-cured in Groups 2 and 5 and gently air-blown but not light-cured in Groups 3 and 6. Z-250 and Duo-Link were used as luting materials. After 24-hours of storage, the bonded inlays were subjected to a shear bond test. For each luting material, one-way ANOVA and Duncan's Multiple Range Test were used to compare the shear bond strength. Paired t-tests were also performed to compare the shear strength between the two luting materials. All the statistical tests were carried out at the 95% confidence level. In Z-250, the results of the shear bond strength were as follows: Group 1(14.90MPa) > Group 2(12.22MPa), Group 4(12.16MPa) Group 5(9.61MPa), Group 3(9.60MPa) Group 6(3.54MPa)(p<0.05). In Duo-Link, the following shear bond strengths were obtained: Group 1(14.65MPa) > Group 2(13.04MPa), Group 4(12.66MPa) > Group 5(10.10MPa) > Group 3(8.40MPa) > Group 6(2.88MPa) (p<0.05). The mean shear bond strength of Z-250 and Duo-Link were not statistically different with the exception of Group 5. In conclusion, the shear bond strength of the indirect composite restoration to dentin can be improved by dentin sealing with DBA before taking an impression, gently air drying and light curing the DBA before the luting procedure.

A strategy for enhancing shear strength and bending strength of FRP laminate using MWCNTs

NASA Astrophysics Data System (ADS)

Rawat, Prashant; Singh, K. K.

2016-09-01

Multi-wall carbon nanotubes (MWCNTs) promises to enhance mechanical properties exceptionally when it is doped with fiber reinforced polymer (FRP) composite. Glass fiber symmetrical laminate with eight layers of 4.0 mm thickness was fabricated by hand lay-up technique assisted by vacuum bagging method. Ply orientations for symmetrical laminate used [(0,90)/(+45,-45)/(+45,-45)/(0,90)//(90,0)/(+45,-45)/(+45,-45)/(90,0)]. MWCNTs reinforced three different samples (0 wt.%, 0.5 wt.% and 0.75 wt.% by weight) were tested on universal testing machine (UTM). Short beam strength test and inter laminar shear strength (ILSS) calculation have been done according to ASTM D2344 and ASTM D7264. UTM having maximum load capacity of 50 KN with loading rate of 0.1 mm/min to 50 mm/min was used for mechanical testing. Testing results justified that by adding 0.50 wt.% MWCNTs in symmetrical GFRP laminate can enhance inter laminar shear strength by 13.66% and bending strength by 44.22%.

A parametric study of variables that affect fiber microbuckling initiation in composite laminates. I - Analyses. II - Experiments

NASA Technical Reports Server (NTRS)

Guynn, E. G.; Ochoa, Ozden O.; Bradley, Walter L.

1992-01-01

The effects of the stacking sequence (orientation of plies adjacent to the 0-deg plies), free surfaces, fiber/matrix interfacial bond strength, initial fiber waviness, resin-rich regions, and nonlinear shear constitutive behavior of the resin on the initiation of fiber microbuckling in thermoplastic composites were investigated using nonlinear geometric and nonlinear 2D finite-element analyses. Results show that reductions in the resin shear tangent modulus, large amplitudes of the initial fiber waviness, and debonds each cause increases in the localized matrix shear strains; these increases lead in turn to premature initiation of fiber microbuckling. The numerical results are compared to experimental data obtained using three thermoplastic composite material systems: (1) commercial APC-2, (2) QUADRAX Unidirectional Interlaced Tape, and AU4U/PEEK.

Shear Strength of Stabilized Kaolin Soil Using Liquid Polymer

NASA Astrophysics Data System (ADS)

Azhar, A. T. S.; Fazlina, M. I. S.; Nizam, Z. M.; Fairus, Y. M.; Hakimi, M. N. A.; Riduan, Y.; Faizal, P.

2017-08-01

The purpose of this research is to investigate the suitability of polymer in soil stabilization by examining its strength to withstand compressive strength. Throughout this research study, manufactured polymer was used as a chemical liquid soil stabilizer. The liquid polymer was diluted using a proposed dilution factor of 1 : 3 (1 part polymer: 3 parts distilled water) to preserve the workability of the polymer in kaolin mixture. A mold with a diameter of 50 mm and a height of 100 mm was prepared. Kaolin soil was mixed with different percentages of polymer from 10%, 15%, 20%, 25%, 30% and 35% of the mass of the kaolin clay sample. Kaolin mixtures were tested after a curing period of 3 days, 7 days, 14 days and 28 days respectively. The physical properties were determined by conducting a moisture content test and Atterberg limit test which comprise of liquid limit, plastic limit and shrinkage limit. Meanwhile, the mechanical properties of the soil shear strength were identified through an unconfined compressive strength (UCS) test. Stabilized kaolin soil showed the highest compressive strength value when it was mixed with 35% of polymer compared to other percentages that marked an increment in strength which are 45.72% (3 days), 67.57% (7 days), 81.73% (14 days) and 77.84% (28 days). Hence, the most effective percentage of liquid polymer which should be used to increase the strength of kaolin soil is 35%.

Effect of low-velocity or ballistic impact damage on the strength of thin composite and aluminum shear panels

NASA Technical Reports Server (NTRS)

Farley, G. L.

1985-01-01

Impact tests were conducted on shear panels fabricated from 6061-T6 aluminum and from woven fabric prepreg of Du Pont Kevlara fiber/epoxy resin and graphite fiber/epoxy resin. The shear panels consisted of three different composite laminates and one aluminum material configuration. Three panel aspect ratios were evaluated for each material configuration. Composite panels were impacted with a 1.27-cm (0.05-in) diameter aluminum sphere at low velocities of 46 m/sec (150 ft/sec) and 67 m/sec (220 ft/sec). Ballistic impact conditions consisted of a tumbled 0.50-caliber projectile impacting loaded composite and aluminum shear panels. The results of these tests indicate that ballistic threshold load (the lowest load which will result in immediate failure upon penetration by the projectile) varied between 0.44 and 0.61 of the average failure load of undamaged panels. The residual strengths of the panels after ballistic impact varied between 0.55 and 0.75 of the average failure strength of the undamaged panels. The low velocity impacts at 67 m/sec (220 ft/sec) caused a 15 to 20 percent reduction in strength, whereas the impacts at 46 m/sec (150 ft/sec) resulted in negligible strength loss. Good agreement was obtained between the experimental failure strengths and the predicted strength with the point stress failure criterion.

An experimentally based analytical model for the shear capacity of FRP-strengthened reinforced concrete beams

NASA Astrophysics Data System (ADS)

Pellegrino, C.; Modena, C.

2008-05-01

This paper deals with the shear strengthening of Reinforced Concrete (RC) flexural members with externally bonded Fiber-Reinforced Polymers (FRPs). The interaction between an external FRP and an internal transverse steel reinforcement is not considered in actual code recommendations, but it strongly influences the efficiency of the shear strengthening rehabilitation technique and, as a consequence, the computation of interacting contributions to the nominal shear strength of beams. This circumstance is also discussed on the basis of the results of an experimental investigation of rectangular RC beams strengthened in shear with "U-jacketed" carbon FRP sheets. Based on experimental results of the present and other investigations, a new analytical model for describing the shear capacity of RC beams strengthened according to the most common schemes (side-bonded and "U-jacketed"), taking into account the interaction between steel and FRP shear strength contributions, is proposed.

In Vitro Evaluation of Shear Bond Strength of Nanocomposites to Dentin

PubMed Central

Vellanki, Vinay Kumar; Shetty, Vikram K; Kushwah, Sudhanshu; Goyal, Geeta; Chandra, S.M. Sharath

2015-01-01

Aims: To compare the shear bond strength of nanocomposites to dentin using three different types of adhesive systems; and to test few specimens under Scanning Electron Microscope (SEM) for analysing whether the bond failure is adhesive or cohesive. Materials and Methods: Sixty human premolar teeth were selected and were randomly grouped, with 20 specimens in each group: group 1 - fluoride releasing dentin bonding agent; group 2 - antibacterial containing dentin bonding agent; and group 3 - one step conventional self etch adhesive. Each group was treated with its respective bonding agents, composite resin build up was done, and shear bond strengths were tested using Instron Universal testing machine. Few of the specimens were tested under SEM. Results: The results were statistically analysed using One-way ANOVA and paired t-test. It was observed that group 3 has the highest shear bond strength followed by group 2, and then group 1. Adhesive failures and mixed failures were most frequent types of failures as seen under SEM. Conclusion: Addition of antimicrobial agent decreases the bond strength of dentin bonding agent and addition of fluoride further decreases the bond strength. From SEM results it can be concluded that the zone of failure could not be defined and also that the failure mode was independent of the dentin bonding agent used. PMID:25738077

Effect of blood contamination on shear bond strength of orthodontic brackets and disinclusion buttons.

PubMed

Sfondrini, Maria Francesca; Gatti, Sara; Scribante, Andrea

2011-07-01

Our aim was to assess the effect of blood contamination on the shear bonding strength and sites of failure of orthodontic brackets and bondable buttons. We randomly divided 160 bovine permanent mandibular incisors into 8 groups of 20 specimens each. Both orthodontic brackets (Step brackets, Leone, Sesto Fiorentino, Italy) and bondable buttons (Flat orthodontic buttons, Leone, Sesto Fiorentino, Italy) were tested on four different enamel surfaces: dry; contamination with blood before priming; after priming; and before and after priming. Brackets and buttons were bonded to the teeth and subsequently tested using a Instron universal testing machine. Shear bonding strength and the rate of adhesive failures were recorded. Data were analysed using the analysis of variance (ANOVA), Scheffè tests, and the chi-square test. Uncontaminated enamel surfaces showed the highest bonding strengths for both brackets and buttons. When they were contaminated with blood, orthodontic brackets had significantly lower shear strengths than bondable buttons (P=0.0001). There were significant differences in sites of failure among the groups for the various enamel surfaces (P=0.001). Contamination of enamel by blood during bonding lowers the strength of the bond, more so with orthodontic brackets than with bondable buttons. Copyright © 2010 The British Association of Oral and Maxillofacial Surgeons. Published by Elsevier Ltd. All rights reserved.

Influence of Hot-Etching Surface Treatment on Zirconia/Resin Shear Bond Strength

PubMed Central

Lv, Pin; Yang, Xin; Jiang, Ting

2015-01-01

This study was designed to evaluate the effect of hot-etching surface treatment on the shear bond strength between zirconia ceramics and two commercial resin cements. Ceramic cylinders (120 units; length: 2.5 mm; diameter: 4.7 mm) were randomly divided into 12 groups (n = 10) according to different surface treatments (blank control; airborne-particle-abrasion; hot-etching) and different resin cements (Panavia F2.0; Superbond C and B) and whether or not a thermal cycling fatigue test (5°–55° for 5000 cycles) was performed. Flat enamel surfaces, mounted in acrylic resin, were bonded to the zirconia discs (diameter: 4.7 mm). All specimens were subjected to shear bond strength testing using a universal testing machine with a crosshead speed of 1 mm/min. All data were statistically analyzed using one-way analysis of variance and multiple-comparison least significant difference tests (α = 0.05). Hot-etching treatment produced higher bond strengths than the other treatment with both resin cements. The shear bond strength of all groups significantly decreased after the thermal cycling test; except for the hot-etching group that was cemented with Panavia F2.0 (p < 0.05). Surface treatment of zirconia with hot-etching solution enhanced the surface roughness and bond strength between the zirconia and the resin cement. PMID:28793699

Microscopic Observations of Adiabatic Shear Bands in Three Different Steels

DTIC Science & Technology

1988-09-01

low thermal conductivity, and a high thermal softening rate. Examples include alloys of titanium. aluminum, copper , as well as steels [5-221... steels : 1 (1) an AISI 1018 cold rolled steel , (2) a high strength low alloy structural steel , and deformation in shear was impo.ed to produce shear bands...stecls: (1) an AISI 1018 cold rolled steel , (2) a high strength low alloy structural steel , and (3) an AISI 4340 VAR steel tempered

The Influence of Second-Phase Dispersions on Shear Instability and Fracture Toughness of Ultrahigh Strength 4340 Steel

DTIC Science & Technology

1989-03-01

been a success. I am deeply grateful to Professor Ronald R. Biederman entrusting me with his TEM after business hours. Special thanks to both John V...During Shear Deformation of Ultrahigh Strength Steels, Proceedings of the Thirty-fourth Sagamore Army Materials Research Conference ( 1987 ), in press. 3...Materials Science and Engineering, V.95 ( 1987 ), pp. 93-99. 14. L. Anand, Some Experimental Observations on Localized Shear Bands in Plane- Strain

Instability of subharmonic resonances in magnetogravity shear waves.

PubMed

Salhi, A; Nasraoui, S

2013-12-01

We study analytically the instability of the subharmonic resonances in magnetogravity waves excited by a (vertical) time-periodic shear for an inviscid and nondiffusive unbounded conducting fluid. Due to the fact that the magnetic potential induction is a Lagrangian invariant for magnetohydrodynamic Euler-Boussinesq equations, we show that plane-wave disturbances are governed by a four-dimensional Floquet system in which appears, among others, the parameter ɛ representing the ratio of the periodic shear amplitude to the vertical Brunt-Väisälä frequency N(3). For sufficiently small ɛ and when the magnetic field is horizontal, we perform an asymptotic analysis of the Floquet system following the method of Lebovitz and Zweibel [Astrophys. J. 609, 301 (2004)]. We determine the width and the maximal growth rate of the instability bands associated with subharmonic resonances. We show that the instability of subharmonic resonance occurring in gravity shear waves has a maximal growth rate of the form Δ(m)=(3√[3]/16)ɛ. This instability persists in the presence of magnetic fields, but its growth rate decreases as the magnetic strength increases. We also find a second instability involving a mixing of hydrodynamic and magnetic modes that occurs for all magnetic field strengths. We also elucidate the similarity between the effect of a vertical magnetic field and the effect of a vertical Coriolis force on the gravity shear waves considering axisymmetric disturbances. For both cases, plane waves are governed by a Hill equation, and, when ɛ is sufficiently small, the subharmonic instability band is determined by a Mathieu equation. We find that, when the Coriolis parameter (or the magnetic strength) exceeds N(3)/2, the instability of the subharmonic resonance vanishes.

In vivo effects of two acidic soft drinks on shear bond strength of metal orthodontic brackets with and without resin infiltration treatment.

PubMed

Hammad, Shaza M; Enan, Enas T

2013-07-01

To evaluate the in vivo effects of two acidic soft drinks (Coca-Cola and Sprite) on the shear bond strength of metal orthodontic brackets with and without resin infiltration treatment. In addition, the enamel surface was evaluated, after debonding, using a scanning electron microscope. Sixty noncarious maxillary premolars, scheduled for extraction in 30 orthodontic patients, were used. Patients were randomly divided into two groups according to the soft drink tested (Coca-Cola or Sprite). In each group, application of resin infiltration (Icon. DMG, Hamburg, Germany) was done on one side only before bonding of brackets. Patients were told to rinse their mouth with their respective soft drink at room temperature for 5 minutes, three times a day for 3 months. Shear bond strength was tested with a universal testing machine. After shearing test, a scanning electron microscope was used to evaluate enamel erosion. Statistical analysis was performed by twoway analysis of variance followed by the least significant difference test. The Coca-Cola group without resin infiltration showed the lowest resistance to shearing forces. Scanning electron micrographs of both groups after resin application showed a significant improvement compared with results without resin use, as the enamel appeared smoother and less erosive. Pretreatment with the infiltrating resin has proved to result in a significant improvement in shear bond strength, regardless of the type of soft drink consumed.

An earthquake instability model based on faults containing high fluid-pressure compartments

USGS Publications Warehouse

Lockner, D.A.; Byerlee, J.D.

1995-01-01

It has been proposed that large strike-slip faults such as the San Andreas contain water in seal-bounded compartments. Arguments based on heat flow and stress orientation suggest that in most of the compartments, the water pressure is so high that the average shear strength of the fault is less than 20 MPa. We propose a variation of this basic model in which most of the shear stress on the fault is supported by a small number of compartments where the pore pressure is relatively low. As a result, the fault gouge in these compartments is compacted and lithified and has a high undisturbed strength. When one of these locked regions fails, the system made up of the neighboring high and low pressure compartments can become unstable. Material in the high fluid pressure compartments is initially underconsolidated since the low effective confining pressure has retarded compaction. As these compartments are deformed, fluid pressure remains nearly unchanged so that they offer little resistance to shear. The low pore pressure compartments, however, are overconsolidated and dilate as they are sheared. Decompression of the pore fluid in these compartments lowers fluid pressure, increasing effective normal stress and shear strength. While this effect tends to stabilize the fault, it can be shown that this dilatancy hardening can be more than offset by displacement weakening of the fault (i.e., the drop from peak to residual strength). If the surrounding rock mass is sufficiently compliant to produce an instability, slip will propagate along the fault until the shear fracture runs into a low-stress region. Frictional heating and the accompanying increase in fluid pressure that are suggested to occur during shearing of the fault zone will act as additional destabilizers. However, significant heating occurs only after a finite amount of slip and therefore is more likely to contribute to the energetics of rupture propagation than to the initiation of the instability. We present results of a one-dimensional dynamic Burridge-Knopoff-type model to demonstrate various aspects of the fluid-assisted fault instability described above. In the numerical model, the fault is represented by a series of blocks and springs, with fault rheology expressed by static and dynamic friction. In addition, the fault surface of each block has associated with it pore pressure, porosity and permeability. All of these variables are allowed to evolve with time, resulting in a wide range of phenomena related to fluid diffusion, dilatancy, compaction and heating. These phenomena include creep events, diffusion-controlled precursors, triggered earthquakes, foreshocks, aftershocks, and multiple earthquakes. While the simulations have limitations inherent to 1-D fault models, they demonstrate that the fluid compartment model can, in principle, provide the rich assortment of phenomena that have been associated with earthquakes. ?? 1995 Birkha??user Verlag.

Comparison of the shear bond strength of self-adhesive resin cements to enamel and dentin with different protocol of application

PubMed Central

Moghaddas, Mohammad Javad; Hossainipour, Zahra; Majidinia, Sara; Ojrati, Najmeh

2017-01-01

Aim The aim of the present study was to determine the shear bond strength of self-adhesive resin cements to enamel and dentin with and without surface treatments, and compare them with conventional resin cement as the control group. Methods In this experimental study, buccal and lingual surface of the thirty sound human premolars were polished in order to obtain a flat surface of enamel (E) in buccal, and dentin (D) in lingual. Sixty feldspathic ceramic blocks (2×3×3 mm) were prepared and randomly divided into six groups (n=10). Each block was cemented to the prepared surface (30 enamel and 30 dentin surface) according to different protocol: E1 and D1; RelyX ARC as control group, E2, D2; RelyX Unicem, E3, D3; acid etching +RelyX Unicem. The specimens were termocycled and subjected to shear forces by a universal testing machine at a cross head speed of 0.5 mm/min. The mode of fracture were evaluated by stereomicroscope. Data were analyzed with descriptive statistical methods using SPSS version 15. One-way ANOVA, and post hoc Tukey tests were used to compare bond strengths between the groups with different adhesives at α=0.05. Results Statistical analysis showed no significant differences within the enamel subgroups, but there were significant differences within the dentinal subgroups, and statistically significant differences were found between the groups D1and D3 (p=0.02). Comparison between similar enamel and dentinal subgroups showed that there was a significant difference just between the subgroups E3 and D3 (p=0.01). Conclusion Elective etching of enamel did not lead to significant increase in the shear bond strength of RelyX Unicem in comparison to RelyX ARC. On the other hand, elective etching of dentin reduces the bond strength of RelyX Unicem with the dentin. PMID:28979732

Comparison of the shear bond strength of self-adhesive resin cements to enamel and dentin with different protocol of application.

PubMed

Moghaddas, Mohammad Javad; Hossainipour, Zahra; Majidinia, Sara; Ojrati, Najmeh

2017-08-01

The aim of the present study was to determine the shear bond strength of self-adhesive resin cements to enamel and dentin with and without surface treatments, and compare them with conventional resin cement as the control group. In this experimental study, buccal and lingual surface of the thirty sound human premolars were polished in order to obtain a flat surface of enamel (E) in buccal, and dentin (D) in lingual. Sixty feldspathic ceramic blocks (2×3×3 mm) were prepared and randomly divided into six groups (n=10). Each block was cemented to the prepared surface (30 enamel and 30 dentin surface) according to different protocol: E1 and D1; RelyX ARC as control group, E2, D2; RelyX Unicem, E3, D3; acid etching +RelyX Unicem. The specimens were termocycled and subjected to shear forces by a universal testing machine at a cross head speed of 0.5 mm/min. The mode of fracture were evaluated by stereomicroscope. Data were analyzed with descriptive statistical methods using SPSS version 15. One-way ANOVA, and post hoc Tukey tests were used to compare bond strengths between the groups with different adhesives at α=0.05. Statistical analysis showed no significant differences within the enamel subgroups, but there were significant differences within the dentinal subgroups, and statistically significant differences were found between the groups D1and D3 (p=0.02). Comparison between similar enamel and dentinal subgroups showed that there was a significant difference just between the subgroups E3 and D3 (p=0.01). Elective etching of enamel did not lead to significant increase in the shear bond strength of RelyX Unicem in comparison to RelyX ARC. On the other hand, elective etching of dentin reduces the bond strength of RelyX Unicem with the dentin.

An evaluation of fatigue limit of notched specimen of a C/C composite

NASA Astrophysics Data System (ADS)

Makabe, C.; Fujikawa, M.; Ferdous, M. S.

2018-06-01

The fatigue strengths in notched specimens of carbon fiber reinforced carbon composites (C/C composites) were investigated. The fatigue limit was measured by S-N curves and load increase tests. The value of fatigue limit obtained by those methods was almost the same. Slits of several sizes were cut on both sides of a test section, and different sizes of slit length were chosen. Also, specimens with blunt-notches were used to compare the fatigue strength. The weakest fatigue limit was obtained in the case of specimens with blunt-notches. However, the stress concentration factor of those is smaller than that of slit specimens. The relationships between fatigue strengths and specimen shapes were analyzed by stress distribution. The effect of slit configuration on fatigue strength was then discussed regarding the experimental consequences. Consequently, it was discussed that the fatigue strength of the present specimens was determined depending on the damage conditions in the vicinity of the notch and on the crack initiation behavior. It is expected that the tendency of the S-N curve and fatigue limit was related to the shear damage and shear mode of the crack growth.

Comparison of shear test methods for evaluating the bond strength of resin cement to zirconia ceramic.

PubMed

Kim, Jae-Hoon; Chae, Soyeon; Lee, Yunhee; Han, Geum-Jun; Cho, Byeong-Hoon

2014-11-01

This study compared the sensitivity of three shear test methods for measuring the shear bond strength (SBS) of resin cement to zirconia ceramic and evaluated the effects of surface treatment methods on the bonding. Polished zirconia ceramic (Cercon base, DeguDent) discs were randomly divided into four surface treatment groups: no treatment (C), airborne-particle abrasion (A), conditioning with Alloy primer (Kuraray Medical Co.) (P) and conditioning with Alloy primer after airborne-particle abrasion (AP). The bond strengths of the resin cement (Multilink N, Ivoclar Vivadent) to the zirconia specimens of each surface treatment group were determined by three SBS test methods: the conventional SBS test with direct filling of the mold (Ø 4 mm × 3 mm) with resin cement (Method 1), the conventional SBS test with cementation of composite cylinders (Ø 4 mm × 3 mm) using resin cement (Method 2) and the microshear bond strength (μSBS) test with cementation of composite cylinders (Ø 0.8 mm × 1 mm) using resin cement (Method 3). Both the test method and the surface treatment significantly influenced the SBS values. In Method 3, as the SBS values increased, the coefficients of variation decreased and the Weibull parameters increased. The AP groups showed the highest SBS in all of the test methods. Only in Method 3 did the P group show a higher SBS than the A group. The μSBS test was more sensitive to differentiating the effects of surface treatment methods than the conventional SBS tests. Primer conditioning was a stronger contributing factor for the resin bond to zirconia ceramic than was airborne-particle abrasion.

Influence of nanoclay on interlaminar shear strength and fracture toughness of glass fiber reinforced nanocomposites

NASA Astrophysics Data System (ADS)

Senthil Kumar, M. S.; Chithirai Pon Selvan, M.; Sampath, P. S.; Raja, K.; Balasundaram, K.

2018-04-01

Multilayer glass fiber reinforced polymer (GFRP) laminates filled with nanoclay was manufactured with compression moulding machine. In the present work, five kinds of nanoclay (Cloisite 25A) loadings viz. 2, 4, 6, 8 and 10% on weight basis of epoxy resin were employed to modify the interlaminar shear strength (ILSS), critical energy release rate (GIc) and impact energy properties of GFRP laminates. Experimental results obtained from ILSS test on clay filled GFRP confirm that the superior strength was attained at low clay content of 155.10 MPa. Furthermore, the mode I interlaminar fracture toughness test conducted on DCB specimens revealed that the commanding improvement of GIc was obtained at 2 wt.% clay content level. On the other hand, both ILSS and fracture toughness was getting reduced at higher clay loadings. At last, the impact strength of the test samples was investigated by using Izod impact test apparatus and observed that the impact energy was increased by 44.39% for 2 wt.% and followed by 24.87% for 4 wt.% clay loadings.

Interfacial crystalline structures in injection over-molded polypropylene and bond strength.

PubMed

Yan, Bowen; Wu, Hong; Jiang, Genjie; Guo, Shaoyun; Huang, Jian

2010-11-01

This paper describes interfacial crystalline structures found in injection overmolded polypropylene components and the relationship of these structures to bond strength between the components. The combined effects of the development of hierarchical gradient structures and the particular thermomechanical environment near the interface on the interfacial crystalline structures were investigated in detail by PLM, SEM, DSC, WAXD, and infrared dichroism spectroscopy. The experimental results showed that during molding there was competitive formation of interfacial crystalline structures consisted of "shish-kebab" layer (SKL) and a transcrystalline layers (TCL). Variation in shear stress (controlled by injection pressure and injection speed) plays an important role in the formation of the SKL. The formation of TCL is influenced by the thermal environment, namely melt temperature and mold temperature. Increasing within certain limits, interfacial temperature and the thermal gradient near the interface promotes β-iPP growth. The relationship between interfacial crystalline structures and interfacial bond strength was established by lap shear measurement. The interfacial bond strength is improved by enhancing the formation of TCL, but reduced if SKL predominates.

Application of continuous normal-lognormal bivariate density functions in a sensitivity analysis of municipal solid waste landfill.

PubMed

Petrovic, Igor; Hip, Ivan; Fredlund, Murray D

2016-09-01

The variability of untreated municipal solid waste (MSW) shear strength parameters, namely cohesion and shear friction angle, with respect to waste stability problems, is of primary concern due to the strong heterogeneity of MSW. A large number of municipal solid waste (MSW) shear strength parameters (friction angle and cohesion) were collected from published literature and analyzed. The basic statistical analysis has shown that the central tendency of both shear strength parameters fits reasonably well within the ranges of recommended values proposed by different authors. In addition, it was established that the correlation between shear friction angle and cohesion is not strong but it still remained significant. Through use of a distribution fitting method it was found that the shear friction angle could be adjusted to a normal probability density function while cohesion follows the log-normal density function. The continuous normal-lognormal bivariate density function was therefore selected as an adequate model to ascertain rational boundary values ("confidence interval") for MSW shear strength parameters. It was concluded that a curve with a 70% confidence level generates a "confidence interval" within the reasonable limits. With respect to the decomposition stage of the waste material, three different ranges of appropriate shear strength parameters were indicated. Defined parameters were then used as input parameters for an Alternative Point Estimated Method (APEM) stability analysis on a real case scenario of the Jakusevec landfill. The Jakusevec landfill is the disposal site of the capital of Croatia - Zagreb. The analysis shows that in the case of a dry landfill the most significant factor influencing the safety factor was the shear friction angle of old, decomposed waste material, while in the case of a landfill with significant leachate level the most significant factor influencing the safety factor was the cohesion of old, decomposed waste material. The analysis also showed that a satisfactory level of performance with a small probability of failure was produced for the standard practice design of waste landfills as well as an analysis scenario immediately after the landfill closure. Copyright © 2015 Elsevier Ltd. All rights reserved.

Rheological Behavior of Xanthan Gum Solution Related to Shear Thinning Fluid Delivery for Subsurface Remediation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhong, Lirong; Oostrom, Martinus; Truex, Michael J.

Xanthan gum, a biopolymer, forms shear thinning fluids which can be used as delivery media to improve the distribution of remedial amendments injected into heterogeneous subsurface environments. The rheological behavior of the shear thinning solution needs to be known to develop an appropriate design for field injection. In this study, the rheological properties of xanthan gum solutions were obtained under various chemical and environmental conditions relevant to delivery of remedial amendments to groundwater. Higher xanthan concentration raised the absolute solution viscosity and increased the degree of shear thinning. Addition of remedial amendments (e.g., phosphate, sodium lactate, ethyl lactate) caused themore » dynamic viscosity of xanthan gum to decrease, but the solutions maintained shear-thinning properties. Use of simple salt (e.g. Na+, Ca2+) to increase the solution ionic strength also decreased the dynamic viscosity of xanthan and the degree of shear thinning, although the effect is a function of xanthan gum concentration and diminished as the xanthan gum concentration was increased. At high xanthan concentration, addition of salt to the solution increased dynamic viscosity. In the absence of sediments, xanthan gum solutions maintain their viscosity properties for months. However, xanthan gum solutions were shown to lose dynamic viscosity over a period of days to weeks when contacted with saturated site sediment. Loss of viscosity is attributed to physical and biodegradation processes.« less

Influence of hydraulic hysteresis on the mechanical behavior of unsaturated soils and interfaces

NASA Astrophysics Data System (ADS)

Khoury, Charbel N.

Unsaturated soils are commonly widespread around the world, especially at shallow depths from the surface. The mechanical behavior of this near surface soil is influenced by the seasonal variations such as rainfall or drought, which in turn may have a detrimental effect on many structures (e.g. retaining walls, shallow foundations, mechanically stabilized earth walls, soil slopes, and pavements) in contact with it. Thus, in order to better understand this behavior, it is crucial to study the complex relationship between soil moisture content and matric suction (a stress state variable defined as pore air pressure minus pore water pressure) known as the Soil Water Characteristic Curve (SWCC). In addition, the influence of hydraulic hysteresis on the behavior of unsaturated soils, soil-structure interaction (i.e. rough and smooth steel interfaces, soil-geotextile interfaces) and pavement subgrade (depicted herein mainly by resilient modulus, Mr) was also studied. To this end, suction-controlled direct shear tests were performed on soils, rough and smooth steel interfaces and geotextile interface under drying (D) and wetting after drying (DW). The shearing behavior is examined in terms of the two stress state variables, matric suction and net normal stress. Results along the D and DW paths indicated that peak shear strength increased with suction and net normal stress; while in general, the post peak shear strength was not influenced by suction for rough interfaces and no consistent trend was observed for soils and soil-geotextiles interfaces. Contrary to saturated soils, results during shearing at higher suction values (i.e. 25 kPa and above) showed a decrease in water content eventhough the sample exhibited dilation. A behavior postulated to be related to disruption of menisci and/or non-uniformity of pore size which results in an increase in localized pore water pressures. Interestingly, wetting after drying (DW) test results showed higher peak and post peak shear strength than that of the drying (D) tests. This is believed to be the result of many factors such as: (1) cyclic suction stress loading, (2) water content (less on wetting than drying), and (3) type of soil. The cyclic suction loading may have induced irrecoverable plastic strains, resulting in stiffer samples for wetting tests as compared to drying. Additionally, water may be acting as a lubricant and thus resulting in lower shear strength for test samples D with higher water contents than DW samples. Furthermore, various shear strength models were investigated for their applicability to the experimental data. Models were proposed for the prediction of shear strength with suction based on the SWCC. The models are able to predict the shear strength of unsaturated soil and interfaces due to drying and wetting (i.e. hydraulic hysteresis) by relating directly to the SWCC. The proposed models were used and partly validated by predicting different test results from the literature. In addition, an existing elastoplastic constitutive model was investigated and validated by comparing the predicted and experimental (stress-displacement, volume change behavior) results obtained from rough and geotextile interface tests. This study also explores the effect of hydraulic hysteresis on the resilient modulus (Mr) of subgrade soils. Suction-controlled Mr tests were performed on compacted samples along the primary drying, wetting, secondary drying and wetting paths. Two test types were performed to check the effect of cyclic deviatoric stress loading on the results. First, M r tests were performed on the same sample at each suction (i.e. 25, 50, 75, 100 kPa) value along all the paths (drying, wetting etc.). A relationship between resilient modulus (Mr) and matric suction was obtained and identified as the resilient modulus characteristic curve (MRCC). MRCC results indicated that Mr increased with suction along the drying curve. On the other hand, results on the primary wetting indicated higher Mr than that of the primary drying and the secondary drying. The second type of test was performed at selected suction without subjecting the sample to previous Mr tests. Results indicated that Mr compared favorably with the other type of test (i.e. with previous M r testing), which indicates that the cyclic deviatoric stress loading influence was not as significant as the hydraulic hysteresis (i.e. cyclic suction stress loading). A new model to predict the MRCC results during drying and wetting (i.e., hydraulic hysteresis) is proposed based on the SWCC hysteresis. The model predicted favorably the drying and then the wetting results using the SWCC at all stress levels. (Abstract shortened by UMI.)

Cholesteric-nematic transitions induced by a shear flow and a magnetic field

NASA Astrophysics Data System (ADS)

Zakhlevnykh, A. N.; Makarov, D. V.; Novikov, A. A.

2017-10-01

The untwisting of the helical structure of a cholesteric liquid crystal under the action of a magnetic field and a shear flow has been studied theoretically. Both factors can induce the cholesteric-nematic transition independently; however, the difference in the orienting actions of the magnetic field and the shear flow leads to competition between magnetic and hydrodynamic mechanisms of influence on the cholesteric liquid crystal. We have analyzed different orientations of the magnetic field relative to the direction of the flow in the shear plane. In a number of limiting cases, the analytic dependences are obtained for the pitch of the cholesteric helix deformed by the shear flow. The phase diagrams of the cholesteric-nematic transitions and the pitch of the cholesteric helix are calculated for different values of the magnetic field strength and the angle of orientation, the flow velocity gradient, and the reactive parameter. It is shown that the magnetic field stabilizes the orientation of the director in the shear flow and expands the boundaries of orientability of cholesterics. It has been established that the shear flow shifts the critical magnetic field strength of the transition. It is shown that a sequence of reentrant orientational cholesteric-nematic-cholesteric transitions can be induced by rotating the magnetic field in certain intervals of its strength and shear flow velocity gradients.

Investigation of the behavior of asphalt tack coat interface layer.

DOT National Transportation Integrated Search

2005-08-04

Asphalt tack coat is a light application of asphalt, usually asphalt diluted with water. It ensures a bond between the surface being paved and the overlying course by providing increased shear strength between two interfaces. Normally hot asphalt cem...

Turbulent Mixing in Gravity Currents with Transverse Shear

NASA Astrophysics Data System (ADS)

White, Brian; Helfrich, Karl; Scotti, Alberto

2010-11-01

A parallel flow with horizontal shear and horizontal density gradient undergoes an intensification of the shear by gravitational tilting and stretching, rapidly breaking down into turbulence. Such flows have the potential for substantial mixing in estuaries and the coastal ocean. We present high-resolution numerical results for the mixing efficiency of these flows, which can be viewed as gravity currents with transverse shear, and contrast them with the well-studied case of stably stratified, homogeneous turbulence (uniform vertical density and velocity gradients). For a sheared gravity current, the buoyancy flux, turbulent Reynolds stress, and dissipation are well out of equilibrium. The total kinetic energy first increases as potential energy is transferred to the gravity current, but rapidly decays once turbulence sets in. Despite the non-equilibrium character, mixing efficiencies are slightly higher but qualitatively similar to homogeneous stratified turbulence. Efficiency decreases in the highly energetic regime where the dissipation rate is large compared with viscosity and stratification, ɛ/(νN^2)>100, further declining as turbulence decays and kinetic energy dissipation dominates the buoyancy flux. In general, the mixing rate, parameterized by a turbulent eddy diffusivity, increases with the strength of the transverse shear.

Tensile and shear loading of four fcc high-entropy alloys: A first-principles study

NASA Astrophysics Data System (ADS)

Li, Xiaoqing; Schönecker, Stephan; Li, Wei; Varga, Lajos K.; Irving, Douglas L.; Vitos, Levente

2018-03-01

Ab initio density-functional calculations are used to investigate the response of four face-centered-cubic (fcc) high-entropy alloys (HEAs) to tensile and shear loading. The ideal tensile and shear strengths (ITS and ISS) of the HEAs are studied by employing first-principles alloy theory formulated within the exact muffin-tin orbital method in combination with the coherent-potential approximation. We benchmark the computational accuracy against literature data by studying the ITS under uniaxial [110] tensile loading and the ISS for the [11 2 ¯] (111 ) shear deformation of pure fcc Ni and Al. For the HEAs, we uncover the alloying effect on the ITS and ISS. Under shear loading, relaxation reduces the ISS by ˜50 % for all considered HEAs. We demonstrate that the dimensionless tensile and shear strengths are significantly overestimated by adopting two widely used empirical models in comparison with our ab initio calculations. In addition, our predicted relationship between the dimensionless shear strength and shear instability are in line with the modified Frenkel model. Using the computed ISS, we derive the half-width of the dislocation core for the present HEAs. Employing the ratio of ITS to ISS, we discuss the intrinsic ductility of HEAs and compare it with a common empirical criterion. We observe a strong linear correlation between the shear instability and the ratio of ITS to ISS, whereas a weak positive correlation is found in the case of the empirical criterion.

The effects of silver coating on friction coefficient and shear bond strength of steel orthodontic brackets.

PubMed

Arash, Valiollah; Anoush, Keivan; Rabiee, Sayed Mahmood; Rahmatei, Manuchehr; Tavanafar, Saeid

2015-01-01

Aims of the present study was to measure frictional resistance between silver coated brackets and different types of arch wires, and shear bond strength of these brackets to the tooth. In an experimental clinical research 28 orthodontic brackets (standard, 22 slots) were coated with silver ions using electroplate method. Six brackets (coated: 3, uncoated: 3) were evaluated with Scanning Electron Microscopy and Atomic Force Microscopy. The amount of friction in 15 coated brackets was measured with three different kinds of arch wires (0.019 × 0.025-in stainless steel [SS], 0.018-in stainless steel [SS], 0.018-in Nickel-Titanium [Ni-Ti]) and compared with 15 uncoated steel brackets. In addition, shear bond strength values were compared between 10 brackets with silver coating and 10 regular brackets. Universal testing machine was used to measure shear bond strength and the amount of friction between the wires and brackets. SPSS 18 was used for data analysis with t-test. SEM and AFM results showed deposition of a uniform layer of silver, measuring 8-10 μm in thickness on bracket surfaces. Silver coating led to higher frictional forces in all the three types of arch wires, which was statistically significant in 0.019 × 0.025-in SS and 0.018-in Ni-Ti, but it did not change the shear bond strength significantly. Silver coating with electroplating method did not affect the bond strength of the bracket to enamel; in addition, it was not an effective method for decreasing friction in sliding mechanics. © Wiley Periodicals, Inc.

Influence of Temperature on Frictional Strength and Healing Properties of Water Saturated Granular Fault Gouges During Dynamic Slip Instabilities

NASA Astrophysics Data System (ADS)

Scuderi, M.; Marone, C.

2012-12-01

The seismic potential of faults, as well as mechanical strength and frictional instability are controlled by the evolution of the real contact area within the fault gouge. Fault gouge is characterized by granular and clay rich material, as the result of continuous wear produced by dynamic or quasi-static slip along the fault plane. In this context, water and thermally-activated physicochemical reactions play a fundamental role in controlling the evolution of friction, via asperity contact properties and processes including hydrolytic weakening, adsorption/desorption, and/or intergranular pressure-solution (IPS). To investigate the role of granular processes and temperature in faulting, we performed shear experiments in water-saturated simulated gouges. We sheared layers of synthetic fault gouge composed of soda-lime glass beads (dia. 105-149 mm) in a double direct shear configuration within a true-triaxial pressure vessel under controlled fluid pressure using DI water. Effective normal stress (σn) was kept constant during shear at 5 MPa, and layer thickness was constantly monitored via a DCDT attached to the ram. Shear stress (τ) was applied via a constant shear displacement rate at layers boundaries. We performed velocity step experiments, during which shearing velocity was increased stepwise from 0.3 to 300 μm/s, and slide-hold-slide tests, with hold times from 1 to 1000 s. During each experiment temperature was kept constant at values of 25, 50 and 75C. Our experiments were conducted in a stick-slip sliding regime. At the end of each run, simulated gouge layers were carefully collected and impregnated with epoxy resin for SEM analysis. For all experiments, stress drop (Δτ) decreases roughly linearly with the log of velocity. With increasing temperature Δτ increases and the velocity dependence varies. Frictional healing is characterized by β = 0.023 change in friction per decade at T = 25C, increasing to β = 0.037 at T = 50C. We find that maximum friction (μmax) increases with increasing temperature, as well as the amount of pre-seismic slip and the corresponding layers dilation. In agreement with previous studies, our data suggest that in water saturated simulated gouges, solid-fluid chemical reactions are enhanced by increasing temperature, which may induce plastic flow and/or intergranular pressure solution at grain junction, controlling μmax, stress drop magnitude and frictional healing. Future work will consider the connection between the observed mechanical behavior and the evolution of grain contact properties.

Food waste impact on municipal solid waste angle of internal friction.

PubMed

Cho, Young Min; Ko, Jae Hac; Chi, Liqun; Townsend, Timothy G

2011-01-01

The impact of food waste content on the municipal solid waste (MSW) friction angle was studied. Using reconstituted fresh MSW specimens with different food waste content (0%, 40%, 58%, and 80%), 48 small-scale (100-mm-diameter) direct shear tests and 12 large-scale (430 mm × 430 mm) direct shear tests were performed. A stress-controlled large-scale direct shear test device allowing approximately 170-mm sample horizontal displacement was designed and used. At both testing scales, the mobilized internal friction angle of MSW decreased considerably as food waste content increased. As food waste content increased from 0% to 40% and from 40% to 80%, the mobilized internal friction angles (estimated using the mobilized peak (ultimate) shear strengths of the small-scale direct shear tests) decreased from 39° to 31° and from 31° to 7°, respectively, while those of large-scale tests decreased from 36° to 26° and from 26° to 15°, respectively. Most friction angle measurements produced in this study fell within the range of those previously reported for MSW. Copyright © 2010 Elsevier Ltd. All rights reserved.

Poromechanics of stick-slip frictional sliding and strength recovery on tectonic faults

DOE PAGES

Scuderi, Marco M.; Carpenter, Brett M.; Johnson, Paul A.; ...

2015-10-22

Pore fluids influence many aspects of tectonic faulting including frictional strength aseismic creep and effective stress during the seismic cycle. But, the role of pore fluid pressure during earthquake nucleation and dynamic rupture remains poorly understood. Here we report on the evolution of pore fluid pressure and porosity during laboratory stick-slip events as an analog for the seismic cycle. We sheared layers of simulated fault gouge consisting of glass beads in a double-direct shear configuration under true triaxial stresses using drained and undrained fluid conditions and effective normal stress of 5–10 MPa. Shear stress was applied via a constant displacementmore » rate, which we varied in velocity step tests from 0.1 to 30 µm/s. Here, we observe net pore pressure increases, or compaction, during dynamic failure and pore pressure decreases, or dilation, during the interseismic period, depending on fluid boundary conditions. In some cases, a brief period of dilation is attendant with the onset of dynamic stick slip. Our data show that time-dependent strengthening and dynamic stress drop increase with effective normal stress and vary with fluid conditions. For undrained conditions, dilation and preseismic slip are directly related to pore fluid depressurization; they increase with effective normal stress and recurrence time. Microstructural observations confirm the role of water-activated contact growth and shear-driven elastoplastic processes at grain junctions. These results indicate that physicochemical processes acting at grain junctions together with fluid pressure changes dictate stick-slip stress drop and interseismic creep rates and thus play a key role in earthquake nucleation and rupture propagation.« less

Fracture surface analysis in composite and titanium bonding: Part 1: Titanium bonding

NASA Technical Reports Server (NTRS)

Sanderson, K. A.; Wightman, J. P.

1985-01-01

Fractured lap shear Ti 6-4 adherends bonded with polyphenyquinoxaline (PPQ) and polysulfone were analyzed. The effects of adherend pretreatment, stress level, thermal aging, anodizing voltage, and modified adhesive of Ti 6-4 adherend bonded with PPQ on lap shear strength were studied. The effect of adherend pretreatment on lap shear strength was investigated for PS samples. Results of scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) used to study the surface topography and surface composition are also discussed.

True Triaxial Strength and Failure Modes of Cubic Rock Specimens with Unloading the Minor Principal Stress

NASA Astrophysics Data System (ADS)

Li, Xibing; Du, Kun; Li, Diyuan

2015-11-01

True triaxial tests have been carried out on granite, sandstone and cement mortar using cubic specimens with the process of unloading the minor principal stress. The strengths and failure modes of the three rock materials are studied in the processes of unloading σ 3 and loading σ 1 by the newly developed true triaxial test system under different σ 2, aiming to study the mechanical responses of the rock in underground excavation at depth. It shows that the rock strength increases with the raising of the intermediate principal stress σ 2 when σ 3 is unloaded to zero. The true triaxial strength criterion by the power-law relationship can be used to fit the testing data. The "best-fitting" material parameters A and n ( A > 1.4 and n < 1.0) are almost located in the same range as expected by Al-Ajmi and Zimmerman (Int J Rock Mech Min Sci 563 42(3):431-439, 2005). It indicates that the end effect caused by the height-to-width ratio of the cubic specimens will not significantly affect the testing results under true triaxial tests. Both the strength and failure modes of cubic rock specimens under true triaxial unloading condition are affected by the intermediate principal stress. When σ 2 increases to a critical value for the strong and hard rocks (R4, R5 and R6), the rock failure mode may change from shear to slabbing. However, for medium strong and weak rocks (R3 and R2), even with a relatively high intermediate principal stress, they tend to fail in shear after a large amount of plastic deformation. The maximum extension strain criterion Stacey (Int J Rock Mech Min Sci Geomech Abstr 651 18(6):469-474, 1981) can be used to explain the change of failure mode from shear to slabbing for strong and hard rocks under true triaxial unloading test condition.

Protein unfolding versus β-sheet separation in spider silk nanocrystals

NASA Astrophysics Data System (ADS)

Alam, Parvez

2014-03-01

In this communication a mechanism for spider silk strain hardening is proposed. Shear failure of β-sheet nanocrystals is the first failure mode that gives rise to the creation of smaller nanocrystals, which are of higher strength and stiffness. β-sheet unfolding requires more energy than nanocrystal separation in a shear mode of failure. As a result, unfolding occurs after the nanocrystals separate in shear. β-sheet unfolding yields a secondary strain hardening effect once the β-sheet conformation is geometrically stable and acts like a unidirectional fibre in a fibre reinforced composite. The mechanism suggested herein is based on molecular dynamics calculations of residual inter-β-sheet separation strengths against residual intra-β-sheet unfolding strengths.