Comparison of metal ion release from different bracket archwire combinations: an in vitro study.

PubMed

Karnam, Srinivas Kumar; Reddy, A Naveen; Manjith, C M

2012-05-01

The metal ion released from the orthodontic appliance may cause allergic reactions particularly nickel and chromium ions. Hence, this study was undertaken to determine the amount of nickel, chromium, copper, cobalt and iron ions released from simulated orthodontic appliance made of new archwires and brackets. Sixty sets of new archwire, band material, brackets and ligature wires were prepared simulating fixed orthodontic appliance. These sets were divided into four groups of fifteen samples each. Group 1: Stainless steel rectangular archwires. Group 2: Rectangular NiTi archwires. Group 3: Rectangular copper NiTi archwires. Group 4: Rectangular elgiloy archwires. These appliances were immersed in 50 ml of artificial saliva solution and stored in polypropylene bottles in the incubator to simulate oral conditions. After 90 days the solution were tested for nickel, chromium, copper, cobalt and iron ions using atomic absorption spectrophotometer. Results showed that high levels of nickel ions were released from all four groups, compared to all other ions, followed by release of iron ion levels. There is no significant difference in the levels of all metal ions released in the different groups. The study confirms that the use of newer brackets and newer archwires confirms the negligible release of metal ions from the orthodontic appliance. The measurable amount of metals, released from orthodontic appliances in artificial saliva, was significantly below the average dietary intake and did not reach toxic concentrations.

Pulsed eddy current differential probe to detect the defects in a stainless steel pipe

NASA Astrophysics Data System (ADS)

Angani, C. S.; Park, D. G.; Kim, C. G.; Leela, P.; Kishore, M.; Cheong, Y. M.

2011-04-01

Pulsed eddy current (PEC) is an electromagnetic nondestructive technique widely used to detect and quantify the flaws in conducting materials. In the present study a differential Hall-sensor probe which is used in the PEC system has been fabricated for the detection of defects in stainless steel pipelines. The differential probe has an exciting coil with two Hall-sensors. A stainless steel test sample with electrical discharge machining (EDM) notches under different depths of 1-5 mm was made and the sample was laminated by plastic insulation having uniform thickness to simulate the pipelines in nuclear power plants (NPPs). The driving coil in the probe is excited by a rectangular current pulse and the resultant response, which is the difference of the two Hall-sensors, has been detected as the PEC probe signal. The discriminating time domain features of the detected pulse such as peak value and time to zero are used to interpret the experimental results with the defects in the test sample. A feature extraction technique such as spectral power density has been devised to infer the PEC response.

An in vitro investigation on friction generated by ceramic brackets.

PubMed

Tecco, Simona; Teté, Stefano; Festa, Mario; Festa, Felice

2010-01-01

To compare friction (F) of conventional and ceramic brackets (0.022-inch slot) using a model that tests the sliding of the archwire through 10 aligned brackets. Polycrystalline alumina brackets (PCAs), PCA brackets with a stainless steel slot (PCA-M), and monocrystalline sapphire brackets (MCS) were tested under elastic ligatures using various archwires in dry and wet (saliva) states. Conventional stainless steel brackets were used as controls. In both dry and wet states, PCA and MCS brackets expressed a statistically significant higher F value with respect to stainless steel and PCA-M brackets when combined with the rectangular archwires (P<.01). PCA brackets showed significantly higher friction than MCS brackets (P<.01) when coupled with 0.014 x 0.025-inch nickel-titanium (Ni-Ti) archwire. SEM analysis showed differences in the surfaces among stainless steel, MCS, PCA-M, and PCA brackets. In the wet state, the mean F values were generally higher than in the dry state. PCA brackets showed significantly higher F than MCS brackets only when combined with 0.014 x 0.025-inch Ni-Ti archwires. Thus, in this study, a 10 aligned-brackets study model showed similar results when compared to a single bracket system except for friction level with 0.014 × 0.025-inch Ni-Ti archwires. © 2011 BY QUINTESSENCE PUBLISHING CO, INC.

Test program to demonstrate the stability of hydrazine in propellant tanks

NASA Technical Reports Server (NTRS)

Moran, C. M.; Sutton, D.

1983-01-01

The suitability of stainless steels and Inconel for long-term hydrazine propellant-storage tanks is investigated. Rectangular coupon samples cut from propellent tanks were sealed with a measured amount of hydrazine in glass capsules, stored at 43 or 60 C, and removed after 6 to 24 months, when corrosion of the coupon and decomposition of the hydrazine was determined, and SEM and electron spectroscopy were performed on some coupons. Corrosion was found to be unmeasurably low for all the coupons, and hydrazine decomposition produced less than 1.0 cu cm of gas per sq cm of wetted surface per year, except in those few cases when catalysis or contamination were detected. Especially good stability was observed for type 304L stainless steel. The decomposition rates determined in the coupon tests are confirmed by preliminary results of actual tank storage trials.

Laboratory glassware rack for seismic safety

NASA Technical Reports Server (NTRS)

Cohen, M. M. (Inventor)

1985-01-01

A rack for laboratory bottles and jars for chemicals and medicines has been designed to provide the maximum strength and security to the glassware in the event of a significant earthquake. The rack preferably is rectangular and may be made of a variety of chemically resistant materials including polypropylene, polycarbonate, and stainless steel. It comprises a first plurality of parallel vertical walls, and a second plurality of parallel vertical walls, perpendicular to the first. These intersecting vertical walls comprise a self-supporting structure without a bottom which sits on four legs. The top surface of the rack is formed by the top edges of all the vertical walls, which are not parallel but are skewed in three dimensions. These top edges form a grid matrix having a number of intersections of the vertical walls which define a number of rectangular compartments having varying widths and lengths and varying heights.

Comparison of the frictional characteristics of aesthetic orthodontic brackets measured using a modified in vitro technique

PubMed Central

Arici, Nursel

2015-01-01

Objective The coefficients of friction (COFs) of aesthetic ceramic and stainless steel brackets used in conjunction with stainless steel archwires were investigated using a modified linear tribometer and special computer software, and the effects of the bracket slot size (0.018 inches [in] or 0.022 in) and materials (ceramic or metal) on the COF were determined. Methods Four types of ceramic (one with a stainless steel slot) and one conventional stainless steel bracket were tested with two types of archwire sizes: a 0.017 × 0.025-in wire in the 0.018-in slots and a 0.019 × 0.025-in wire in the 0.022-in slot brackets. For pairwise comparisons between the 0.018-in and 0.022-in slot sizes in the same bracket, an independent sample t-test was used. One-way and two-way analysis of variance (ANOVA) and Tukey's post-hoc test at the 95% confidence level (α = 0.05) were also used for statistical analyses. Results There were significant differences between the 0.022-in and 0.018-in slot sizes for the same brand of bracket. ANOVA also showed that both slot size and bracket slot material had significant effects on COF values (p < 0.001). The ceramic bracket with a 0.022-in stainless steel slot showed the lowest mean COF (µ = 0.18), followed by the conventional stainless steel bracket with a 0.022-in slot (µ = 0.21). The monocrystalline alumina ceramic bracket with a 0.018-in slot had the highest COF (µ = 0.85). Conclusions Brackets with stainless steel slots exhibit lower COFs than ceramic slot brackets. All brackets show lower COFs as the slot size increases. PMID:25667915

Effect of Barrel Material on Critical Current Measurements of High-Jc RRP Nb3Sn Wires

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ghosh, A.

Nb{sub 3}Sn strands extracted from a 20-strand rectangular Rutherford cable were reacted on either stainless steel or Ti-alloy barrels and the critical current, I{sub c}, in the field range of 8-11.5 T was measured on ITER-type barrels made from Ti-6Al-4V alloy, 304 stainless steel and G-10. Measurements on the 'standard' Ti-alloy barrel using the test procedure employed at BNL are shown to reproduce I{sub c} for extracted strands to {+-}2%. The I{sub c} data for the sample mounted on the 'standard' Ti-alloy are fit to the deviatoric strain scaling model developed for Nb{sub 3}Sn by the University of Twente groupmore » using an arbitrary pre-strain. Using the parameters for this fit, the I{sub c} data for the other barrels are fitted by only adjusting the strain. Using this procedure, the strain difference due to the barrel material is determined. Assuming a thermal pre-strain of -0.2% for the sample measured on the Ti-alloy barrel, the use of stainless steel barrel increases the compressive strain by -0.07%, that of G-10 by -0.10%. With the wire soldered to the stainless steel barrel, the strain increases to -0.15%. Details of this study are presented.« less

Variation in flexural properties of photo-pultruded composite archwires: analyses of round and rectangular profiles.

PubMed

Fallis, D W; Kusy, R P

2000-11-01

Prototype continuous, unidirectional, fiber-reinforced composite archwires were manufactured into round and rectangular profiles utilizing a photo-pultrusion process. Both 0.022 inch (0.56 mm) diameter and 0.021 x 0.028 inch (0.53 x 0.71 mm) rectangular composites were formed utilizing commercially available S2-glass reinforcement within a polymeric matrix. Reinforcement was varied according to the number, denier and twists per inch (TPI) of four S2-glass yarns to volume levels of 32-74% for round and 41-61% for rectangular profiles. Cross-sectional geometry was evaluated via light microscopy to determine loading characteristics; whereas two flexural properties (the elastic moduli and flexural strengths) were determined by 3-point bending tests. Morphological evaluation of samples revealed that as the TPI increased from 1 to 8, the yarns were more separated from one another and distributed more peripherally within a profile. For round and rectangular profiles utilizing 1 TPI fibers, moduli increased with fiber content approaching theoretical values. For round profiles utilizing 1 TPI and 4 TPI fibers, flexural strengths increased until the loading geometry was optimized. In contrast, the flexural strengths of composites that were pultruded with 8 TPI fibers were not improved at any loading level. Doubling the denier of the yarn, without altering the loading, increased both the moduli and flexural strengths in rectangular samples; whereas, the increases observed in round samples were not statistically significant. At optimal loading the maximum mean moduli and strengths equaled 53.6 +/- 2.0 and 1.36 +/- 0.17 GPa for round wire and equaled 45.7 +/- 0.8 and 1.40 +/- 0.05 GPa for rectangular wires, respectively. These moduli were midway between that of martensitic NiTi (33.4 GPa) and beta-titanium (72.4 GPa), and produced about one-quarter the force of a stainless steel wire per unit of activation. Values of strengths placed this composite material in the range of published values for beta-titanium wires (1.3-1.5 GPa). Copyright 2000 Kluwer Academic Publishers

Laser Surface Hardening of Groove Edges

NASA Astrophysics Data System (ADS)

Hussain, A.; Hamdani, A. H.; Akhter, R.; Aslam, M.

2013-06-01

Surface hardening of groove-edges made of 3Cr13 Stainless Steel has been carried out using 500 W CO2 laser with a rectangular beam of 2.5×3 mm2. The processing speed was varied from 150-500 mm/min. It was seen that the hardened depth increases with increase in laser interaction time. A maximum hardened depth of around 1mm was achieved. The microhardness of the transformed zone was 2.5 times the hardness of base metal. The XRD's and microstructural analysis were also reported.

Elastic and plastic buckling of simply supported solid-core sandwich plates in compression

NASA Technical Reports Server (NTRS)

Seide, Paul; Stowell, Elbridge Z

1950-01-01

A solution is presented for the problem of the compressive buckling of simply supported, flat, rectangular, solid-core sandwich plates stressed either in the elastic range or in the plastic range. Charts for the analysis of long sandwich plates are presented for plates having face materials of 24s-t3 aluminum alloy, 76s-t6 alclad aluminum alloy, and stainless steel. A comparison of computed and experimental buckling stresses of square solid-core sandwich plates indicates fair agreement between theory and experiment.

Orthodontic Bracket Manufacturing Tolerances and Dimensional Differences between Select Self-Ligating Brackets

PubMed Central

Major, Thomas W.; Carey, Jason P.; Nobes, David S.; Major, Paul W.

2010-01-01

In all manufacturing processes there are tolerances; however, orthodontic bracket manufacturers seldom state the slot dimensional tolerances. This experiment develops a novel method of analyzing slot profile dimensions using photographs of the slot. Five points are selected along each wall, and lines are fitted to define a trapezoidal slot shape. This investigation measures slot height at the slot's top and bottom, angles between walls, slot taper, and the linearity of each wall. Slot dimensions for 30 upper right central incisor self-ligating stainless steel brackets from three manufacturers were evaluated. Speed brackets have a slot height 2% smaller than the nominal 0.559 mm size and have a slightly convergent taper. In-Ovation brackets have a divergent taper at an average angle of 1.47 degrees. In-Ovation is closest to the nominal value of slot height at the slot base and has the smallest manufacturing tolerances. Damon Q brackets are the most rectangular in shape, with nearly 90-degree corners between the slot bottom and walls. Damon slot height is on average 3% oversized. PMID:20981299

Simulation and experiment for the inspection of stainless steel bolts in servicing using an ultrasonic phased array

NASA Astrophysics Data System (ADS)

Chen, Jinzhong; He, Renyang; Kang, Xiaowei; Yang, Xuyun

2015-10-01

The non-destructive testing of small-sized (M12-M20) stainless steel bolts in servicing is always a technical problem. This article focuses on the simulation and experimental research of stainless steel bolts with an artificial defect reflector using ultrasonic phased array inspection. Based on the observation of the sound field distribution of stainless steel bolts in ultrasonic phased array as well as simulation modelling and analysis of the phased array probes' detection effects with various defect sizes, different artificial defect reflectors of M16 stainless steel bolts are machined in reference to the simulation results. Next, those bolts are tested using a 10-wafer phased array probe with 5 MHz. The test results finally prove that ultrasonic phased array can detect 1-mm cracks in diameter with different depths of M16 stainless steel bolts and a metal loss of Φ1 mm of through-hole bolts, which provides technical support for future non-destructive testing of stainless steel bolts in servicing.

Two-step fabrication of single-layer rectangular SnSe flakes

NASA Astrophysics Data System (ADS)

Jiang, Jizhou; Wong, Calvin Pei Yu; Zou, Jing; Li, Shisheng; Wang, Qixing; Chen, Jianyi; Qi, Dianyu; Wang, Hongyu; Eda, Goki; Chua, Daniel H. C.; Shi, Yumeng; Zhang, Wenjing; Thye Shen Wee, Andrew

2017-06-01

Recent findings about ultrahigh thermoelectric performances in SnSe single crystals have stimulated research on this binary semiconductor material. Furthermore, single-layer SnSe is an interesting analogue of phosphorene, with potential applications in two-dimensional (2D) nanoelectronics. Although significant advances in the synthesis of SnSe nanocrystals have been made, fabrication of well-defined large-sized single-layer SnSe flakes in a facile way still remains a challenge. The growth of single-layer rectangular SnSe flakes with a thickness of ~6.8 Å and lateral dimensions of about 30 µm  ×  50 µm is demonstrated by a two-step synthesis method, where bulk rectangular SnSe flakes were synthesized first by a vapor transport deposition method followed by a nitrogen etching technique to fabricate single-layer rectangular SnSe flakes in an atmospheric pressure system. The as-obtained rectangular SnSe flakes exhibited a pure crystalline phase oriented along the a-axis direction. Field-effect transistor devices fabricated on individual single-layer rectangular SnSe flakes using gold electrodes exhibited p-doped ambipolar behavior and a hole mobility of about 0.16 cm2 V-1 s-1. This two-step fabrication method can be helpful for growing other similar 2D large-sized single-layer materials.

Biocompatibility of 17-4 PH stainless steel foam for implant applications.

PubMed

Mutlu, Ilven; Oktay, Enver

2011-01-01

In this study, biocompatibility of 17-4 PH stainless steel foam for biomedical implant applications was investigated. 17-4 PH stainless steel foams having porosities in the range of 40-82% with an average pore size of around 600 μm were produced by space holder-sintering technique. Sintered foams were precipitation hardened for times of 1-6 h at temperatures between 450-570 °C. Compressive yield strength and Young's modulus of aged stainless steel foams were observed to vary between 80-130 MPa and 0.73-1.54 GPa, respectively. Pore morphology, pore size and the mechanical properties of the 17-4 PH stainless steel foams were close to cancellous bone. In vitro evaluations of cytotoxicity of the foams were investigated by XTT and MTT assays and showed sufficient biocompatibility. Surface roughness parameters of the stainless steel foams were also determined to characterize the foams.

Effect of the computational domain size and shape on the self-diffusion coefficient in a Lennard-Jones liquid.

PubMed

Kikugawa, Gota; Ando, Shotaro; Suzuki, Jo; Naruke, Yoichi; Nakano, Takeo; Ohara, Taku

2015-01-14

In the present study, molecular dynamics (MD) simulations on the monatomic Lennard-Jones liquid in a periodic boundary system were performed in order to elucidate the effect of the computational domain size and shape on the self-diffusion coefficient measured by the system. So far, the system size dependence in cubic computational domains has been intensively investigated and these studies showed that the diffusion coefficient depends linearly on the inverse of the system size, which is theoretically predicted based on the hydrodynamic interaction. We examined the system size effect not only in the cubic cell systems but also in rectangular cell systems which were created by changing one side length of the cubic cell with the system density kept constant. As a result, the diffusion coefficient in the direction perpendicular to the long side of the rectangular cell significantly increases more or less linearly with the side length. On the other hand, the diffusion coefficient in the direction along the long side is almost constant or slightly decreases. Consequently, anisotropy of the diffusion coefficient emerges in a rectangular cell with periodic boundary conditions even in a bulk liquid simulation. This unexpected result is of critical importance because rectangular fluid systems confined in nanospace, which are present in realistic nanoscale technologies, have been widely studied in recent MD simulations. In order to elucidate the underlying mechanism for this serious system shape effect on the diffusion property, the correlation structures of particle velocities were examined.

A comparative study of frictional force in self-ligating brackets according to the bracket-archwire angulation, bracket material, and wire type

PubMed Central

Lee, Souk Min

2015-01-01

Objective This study aimed to compare the frictional force (FR) in self-ligating brackets among different bracket-archwire angles, bracket materials, and archwire types. Methods Passive and active metal self-ligating brackets and active ceramic self-ligating brackets were included as experimental groups, while conventional twin metal brackets served as a control group. All brackets were maxillary premolar brackets with 0.022 inch [in] slots and a -7° torque. The orthodontic wires used included 0.018 round and 0.019 × 0.025 in rectangular stainless steel wires. The FR was measured at 0°, 5°, and 10° angulations as the wire was drawn through the bracket slots after attaching brackets from each group to the universal testing machine. Static and kinetic FRs were also measured. Results The passive self-ligating brackets generated a lower FR than all the other brackets. Static and kinetic FRs generally increased with an increase in the bracket-archwire angulation, and the rectangular wire caused significantly higher static and kinetic FRs than the round wire (p < 0.001). The metal passive self-ligating brackets exhibited the lowest static FR at the 0° angulation and a lower increase in static and kinetic FRs with an increase in bracket-archwire angulation than the other brackets, while the conventional twin brackets showed a greater increase than all three experimental brackets. Conclusions The passive self-ligating brackets showed the lowest FR in this study. Self-ligating brackets can generate varying FRs in vitro according to the wire size, surface characteristics, and bracket-archwire angulation. PMID:25667913

Microstructural Study of 17-4PH Stainless Steel after Plasma-Transferred Arc Welding.

PubMed

Deng, Dewei; Chen, Rui; Sun, Qi; Li, Xiaona

2015-01-29

The improvement of the surface qualities and surface hardening of precipitation hardened martensitic stainless steel 17-4PH was achieved by the plasma-transferred arc welding (PTAW) process deposited with Co-based alloy. The microstructure of the heat affected zone (HAZ) and base metal were characterized by optical microscope (OM), scanning electron microscope (SEM) and transmission electron microscope (TEM). The results show that there are obvious microstructural differences between the base metal and HAZ. For example, base material is transformed from lath martensite to austenite due to the heateffect of the welding process. On the other hand, the precipitate in the matrix (bar-like shape Cr₇C₃ phase with a width of about one hundred nanometres and a length of hundreds of nanometres) grows to a rectangular appearance with a width of about two hundred nanometres and a length of about one micron. Stacking fault could also be observed in the Cr₇C₃ after PTAW. The above means that welding can obviously improve the surface qualities.

Analytical Model of Advection and Erosion in a Rectangular Channel

NASA Astrophysics Data System (ADS)

Kaufman, Miron

2007-03-01

We consider the Boussinesq pressure driven creeping flow in a rectangular channel. We assume a particle to be made of primary fragments bound together. Particles are advected by the flow and they erode because of the shear stresses imparted by the fluid. The time evolution of the numbers of particles of different sizes is described by the Bateman equations of nuclear radioactivity. We find, by solving these differential equations, the numbers of particles of each possible size as functions of time.

Nanoparticle Treated Stainless Steel Filters for Metal Vapor Sequestration

NASA Astrophysics Data System (ADS)

Murph, Simona E. Hunyadi; Larsen, George K.; Korinko, Paul; Coopersmith, Kaitlin J.; Summer, Ansley J.; Lewis, Rebecca

2017-02-01

The ability to sequester vapor phase radioactive compounds during industrial processes reduces the exposure of workers and the environment to dangerous radioactive materials. Nanomaterials have a lot of potential in this area because they typically demonstrate size- and shape-dependent properties with higher reactivity than bulk. This is due to the increased surface area-to-volume ratio and quantum size effects. In this report, we developed a gold nanomaterial-treated stainless steel filter, namely wools and coupons, that can be efficiently used for zinc vapor sequestration. Without nanoparticle modification, stainless steel coupons do not react or alloy with Zn. Gold nanomaterials were grown onto various stainless steel filters using solution chemistry that is amenable to scaling up. Materials were characterized by electron microscopy, inductively coupled plasma mass spectroscopy and dynamic light scattering before and after exposure to zinc vapors. X-ray diffraction, high-resolution transmission electron microscopy, energy dispersive x-ray spectroscopy mapping and ultraviolet-visible spectroscopy confirm the formation of gold-zinc alloys after Zn vapor exposure. The effect of surface topography on nanoparticle morphology, size and loading density were also investigated, and stainless steel surface defects were found to have an impact on the Au NP growth and subsequently Zn sequestration.

[Counting colonies of micro-organisms on solid media (author's transl)].

PubMed

Stonebrink, B

1978-11-01

The base of the system consists in a stainless steel cup with a shallow recess into which about 3 ml. of fluid agar medium may be poured, which produces a flat rectangular surface of about 8.65 sq. cm. after solidification. In the majority of cases, inoculation was performed by flooding the medium with a diluted suspension of micro-organisms. The cups were then put upright and carried over into a centrifuge tube which was closed with a rubber stopper. After the required incubation period, the colonies were counted, if necessary, using a specially developed colony counter connected to an electromechanical counting relay. Dilutions were prepared in screw capped bottles of various sizes. Pipettes were used only with connected "Volac" pipette holders. Cleaning and sterilisation could be done in an efficient and reliable way. In addition to the above method, the cups containing media may also be used for: impression counts, examination of fluids by immersion, inoculation by swabs or wire loops, studying air pollution. the system requires a rather large investment, but the daily cost and quantities of material used are small. The underlying study of the literature and the discussion of statistical methods used are available to the interested reader.

Development of Duplex Stainless Steels by Field-Assisted Hot Pressing: Influence of the Particle Size and Morphology of the Powders on the Final Mechanical Properties

NASA Astrophysics Data System (ADS)

García-Junceda, A.; Rincón, M.; Torralba, J. M.

2018-01-01

The feasibility of processing duplex stainless steels with promising properties using a powder metallurgical route, including the consolidation by field-assisted hot pressing, is assessed in this investigation. The influence of the particle size and morphology of the raw austenitic and ferritic powders on the final microstructure and properties is also evaluated for an austenitic content of 60 wt pct. In addition, the properties of a new microconstituent generated between the initial constituents are analyzed. The maximum sintered density (98.9 pct) and the best mechanical behavior, in terms of elastic modulus, nanohardness, yield strength, ultimate tensile strength, and ductility, are reached by the duplex stainless steel processed with austenitic and ferritic gas atomized stainless steel powders.

Computer code for the prediction of nozzle admittance

NASA Technical Reports Server (NTRS)

Nguyen, Thong V.

1988-01-01

A procedure which can accurately characterize injector designs for large thrust (0.5 to 1.5 million pounds), high pressure (500 to 3000 psia) LOX/hydrocarbon engines is currently under development. In this procedure, a rectangular cross-sectional combustion chamber is to be used to simulate the lower traverse frequency modes of the large scale chamber. The chamber will be sized so that the first width mode of the rectangular chamber corresponds to the first tangential mode of the full-scale chamber. Test data to be obtained from the rectangular chamber will be used to assess the full scale engine stability. This requires the development of combustion stability models for rectangular chambers. As part of the combustion stability model development, a computer code, NOAD based on existing theory was developed to calculate the nozzle admittances for both rectangular and axisymmetric nozzles. This code is detailed.

Study of the Effects of Centrifugal Instabilities on Flow in a 40 to 1 Aspect Ratio Rectangular Curved Channel, for Dean Numbers from 35 to Fully Turbulent Conditions

DTIC Science & Technology

1990-12-01

is constructed from stainless steel hypodermic tubing with inner and outer diameters of 0.203 mm and 0.406 mm. The five tubes were first joined by...for all channels is 256 kHz. A schematic diagram of the measurement process [Ref. 25] is given in Figure 78, and is also described below. The analog...and smoke rake. Combustion takes place inside a 40.64 cm long, 6.27 cm inside diameter (2.5 inch schedule 40) steel pipe. Inside this chamber, smoke is

Experimental investigation of the two-phase flow regimes and pressure drop in horizontal mini-size rectangular test section

NASA Astrophysics Data System (ADS)

Elazhary, Amr Mohamed; Soliman, Hassan M.

2012-10-01

An experimental study was conducted in order to investigate two-phase flow regimes and fully developed pressure drop in a mini-size, horizontal rectangular channel. The test section was machined in the form of an impacting tee junction in an acrylic block (in order to facilitate visualization) with a rectangular cross-section of 1.87-mm height on 20-mm width on the inlet and outlet sides. Pressure drop measurement and flow regime identification were performed on all three sides of the junction. Air-water mixtures at 200 kPa (abs) and room temperature were used as the test fluids. Four flow regimes were identified visually: bubbly, plug, churn, and annular over the ranges of gas and liquid superficial velocities of 0.04 ≤ JG ≤ 10 m/s and 0.02 ≤ JL ≤ 0.7 m/s, respectively, and a flow regime map was developed. Accuracy of the pressure-measurement technique was validated with single-phase, laminar and turbulent, fully developed data. Two-phase experiments were conducted for eight different inlet conditions and various mass splits at the junction. Comparisons were conducted between the present data and former correlations for the fully developed two-phase pressure drop in rectangular channels with similar sizes. Wide deviations were found among these correlations, and the correlations that agreed best with the present data were identified.

Nanoparticle treated stainless steel filters for metal vapor sequestration

DOE PAGES

Murph, Simona E. Hunyadi; Larsen, George K.; Korinko, Paul; ...

2016-12-07

The ability to sequester vapor phase radioactive compounds during industrial processes reduces the exposure of workers and the environment to dangerous radioactive materials. Nanomaterials have a lot of potential in this area because they typically demonstrate size- and shape-dependent properties with higher reactivity than bulk. This is due to the increased surface area-to-volume ratio and quantum size effects. In this report, we developed a gold nanomaterial-treated stainless steel filter, namely wools and coupons, that can be efficiently used for zinc vapor sequestration. Without nanoparticle modification, stainless steel coupons do not react or alloy with Zn. Gold nanomaterials were grown ontomore » various stainless steel filters using solution chemistry that is amenable to scaling up. Materials were characterized by electron microscopy, inductively coupled plasma mass spectroscopy and dynamic light scattering before and after exposure to zinc vapors. X-ray diffraction, high-resolution transmission electron microscopy, energy dispersive x-ray spectroscopy mapping and ultraviolet-visible spectroscopy confirm the formation of gold-zinc alloys after Zn vapor exposure. Furthermore, the effect of surface topography on nanoparticle morphology, size and loading density were also investigated, and stainless steel surface defects were found to have an impact on the Au NP growth and subsequently Zn sequestration.« less

Nanoparticle treated stainless steel filters for metal vapor sequestration

DOE Office of Scientific and Technical Information (OSTI.GOV)

Murph, Simona E. Hunyadi; Larsen, George K.; Korinko, Paul

The ability to sequester vapor phase radioactive compounds during industrial processes reduces the exposure of workers and the environment to dangerous radioactive materials. Nanomaterials have a lot of potential in this area because they typically demonstrate size- and shape-dependent properties with higher reactivity than bulk. This is due to the increased surface area-to-volume ratio and quantum size effects. In this report, we developed a gold nanomaterial-treated stainless steel filter, namely wools and coupons, that can be efficiently used for zinc vapor sequestration. Without nanoparticle modification, stainless steel coupons do not react or alloy with Zn. Gold nanomaterials were grown ontomore » various stainless steel filters using solution chemistry that is amenable to scaling up. Materials were characterized by electron microscopy, inductively coupled plasma mass spectroscopy and dynamic light scattering before and after exposure to zinc vapors. X-ray diffraction, high-resolution transmission electron microscopy, energy dispersive x-ray spectroscopy mapping and ultraviolet-visible spectroscopy confirm the formation of gold-zinc alloys after Zn vapor exposure. Furthermore, the effect of surface topography on nanoparticle morphology, size and loading density were also investigated, and stainless steel surface defects were found to have an impact on the Au NP growth and subsequently Zn sequestration.« less

Unpinning of spiral waves from rectangular obstacles by stimulated wave trains

NASA Astrophysics Data System (ADS)

Ponboonjaroenchai, Benjamas; Srithamma, Panatda; Kumchaiseemak, Nakorn; Sutthiopad, Malee; Müller, Stefan C.; Luengviriya, Chaiya; Luengviriya, Jiraporn

2017-09-01

Pinned spiral waves are exhibited in many excitable media. In cardiology, lengthened tachycardia correspond to propagating action potential in forms of spiral waves pinned to anatomical obstacles including veins and scares. Thus, elimination such waves is important particularly in medical treatments. We present study of unpinning of a spiral wave by a wave train initiated by periodic stimuli at a given location. The spiral wave is forced to leave the rectangular obstacle when the period of the wave train is shorter than a threshold Tunpin. For small obstacles, Tunpin decreases when the obstacle size is increased. Furthermore, Tunpin depends on the obstacle orientation with respect to the wave train propagation. For large obstacles, Tunpin is independent to the obstacle size. It implies that the orientation of the obstacle plays an important role in the unpinning of the spiral wave, especially for small rectangular obstacles.

Microstructural Study of 17-4PH Stainless Steel after Plasma-Transferred Arc Welding

PubMed Central

Deng, Dewei; Chen, Rui; Sun, Qi; Li, Xiaona

2015-01-01

The improvement of the surface qualities and surface hardening of precipitation hardened martensitic stainless steel 17-4PH was achieved by the plasma-transferred arc welding (PTAW) process deposited with Co-based alloy. The microstructure of the heat affected zone (HAZ) and base metal were characterized by optical microscope (OM), scanning electron microscope (SEM) and transmission electron microscope (TEM). The results show that there are obvious microstructural differences between the base metal and HAZ. For example, base material is transformed from lath martensite to austenite due to the heateffect of the welding process. On the other hand, the precipitate in the matrix (bar-like shape Cr7C3 phase with a width of about one hundred nanometres and a length of hundreds of nanometres) grows to a rectangular appearance with a width of about two hundred nanometres and a length of about one micron. Stacking fault could also be observed in the Cr7C3 after PTAW. The above means that welding can obviously improve the surface qualities. PMID:28787947

Study on optimum length of raw material in stainless steel high-lock nuts forging

NASA Astrophysics Data System (ADS)

Cheng, Meiwen; Liu, Fenglei; Zhao, Qingyun; Wang, Lidong

2018-04-01

Taking 302 stainless steel (1Cr18Ni9) high-lock nuts for research objects, adjusting the length of raw material, then using DEFORM software to simulate the isothermal forging process of each station and conducting the corresponding field tests to study the effects of raw material size on the stainless steel high-lock nuts forming performance. The tests show that the samples of each raw material length is basically the same as the results of the DEFORM software. When the length of the raw material is 10mm, the appearance size of the parts can meet the design requirements.

Numerical evaluation of the surface deformation of elastic solids subjected to a hertzian contact stress

NASA Technical Reports Server (NTRS)

Hamrock, B. J.; Dowson, D.

1974-01-01

The elastic deformation of two ellipsoidal solids in contact and subjected to Hertzian stress distribution was evaluated numerically as part of a general study of the elastic deformation of such solids in elastohydrodynamic contacts. In the analysis the contact zone was divided into equal rectangular areas, and it was assumed that a uniform pressure is applied over each rectangular area. The influence of the size of the rectangular area upon accuracy was also studied. The results indicate the distance from the center of the contact at which elastic deformation becomes insignificant.

Simulation of multipactor on the rectangular grooved dielectric surface

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cai, Libing; Wang, Jianguo, E-mail: wanguiuc@mail.xjtu.edu.cn; Northwest Institute of Nuclear Technology, Xi'an, Shaanxi 710024

2015-11-15

Multipactor discharge on the rectangular grooved dielectric surface is simulated self-consistently by using a two-and-a-half dimensional (2.5 D) electrostatic particle-in-cell (PIC) code. Compared with the electromagnetic PIC code, the former can give much more accurate solution for the space charge field caused by the multipactor electrons and the deposited surface charge. According to the rectangular groove width and height, the multipactor can be divided into four models, the spatial distributions of the multipactor electrons and the space charge fields are presented for these models. It shows that the rectangular groove in different models gives very different suppression effect on themore » multipactor, effective and efficient suppression on the multipactor can only be reached with a proper groove size.« less

Effect of ultrafine grain on tensile behaviour and corrosion resistance of the duplex stainless steel.

PubMed

Jinlong, Lv; Tongxiang, Liang; Chen, Wang; Limin, Dong

2016-05-01

The ultrafine grained 2205 duplex stainless steel was obtained by cold rolling and annealing. The tensile properties were investigated at room temperature. Comparing with coarse grained stainless steel, ultrafine grained sample showed higher strength and plasticity. In addition, grain size changed deformation orientation. The strain induced α'-martensite was observed in coarse grained 2205 duplex stainless steel with large strain. However, the grain refinement inhibited the transformation of α'-martensite;nevertheless, more deformation twins improved the strength and plasticity of ultrafine grained 2205 duplex stainless steel. In addition, the grain refinement improved corrosion resistance of the 2205 duplex stainless steel in sodium chloride solution. Copyright © 2016 Elsevier B.V. All rights reserved.

Fatigue crack propagation behavior of stainless steel welds

NASA Astrophysics Data System (ADS)

Kusko, Chad S.

The fatigue crack propagation behavior of austenitic and duplex stainless steel base and weld metals has been investigated using various fatigue crack growth test procedures, ferrite measurement techniques, light optical microscopy, stereomicroscopy, scanning electron microscopy, and optical profilometry. The compliance offset method has been incorporated to measure crack closure during testing in order to determine a stress ratio at which such closure is overcome. Based on this method, an empirically determined stress ratio of 0.60 has been shown to be very successful in overcoming crack closure for all da/dN for gas metal arc and laser welds. This empirically-determined stress ratio of 0.60 has been applied to testing of stainless steel base metal and weld metal to understand the influence of microstructure. Regarding the base metal investigation, for 316L and AL6XN base metals, grain size and grain plus twin size have been shown to influence resulting crack growth behavior. The cyclic plastic zone size model has been applied to accurately model crack growth behavior for austenitic stainless steels when the average grain plus twin size is considered. Additionally, the effect of the tortuous crack paths observed for the larger grain size base metals can be explained by a literature model for crack deflection. Constant Delta K testing has been used to characterize the crack growth behavior across various regions of the gas metal arc and laser welds at the empirically determined stress ratio of 0.60. Despite an extensive range of stainless steel weld metal FN and delta-ferrite morphologies, neither delta-ferrite morphology significantly influence the room temperature crack growth behavior. However, variations in weld metal da/dN can be explained by local surface roughness resulting from large columnar grains and tortuous crack paths in the weld metal.

Shear flow control of cold and heated rectangular jets by mechanical tabs. Volume 1: Results and discussion

NASA Technical Reports Server (NTRS)

Brown, W. H.; Ahuja, K. K.

1989-01-01

The effects of mechanical protrusions on the jet mixing characteristics of rectangular nozzles for heated and unheated subsonic and supersonic jet plumes were studied. The characteristics of a rectangular nozzle of aspect ratio 4 without the mechanical protrusions were first investigated. Intrusive probes were used to make the flow measurements. Possible errors introduced by intrusive probes in making shear flow measurements were also examined. Several scaled sizes of mechanical tabs were then tested, configured around the perimeter of the rectangular jet. Both the number and the location of the tabs were varied. From this, the best configuration was selected. The conclusions derived were: (1) intrusive probes can produce significant errors in the measurements of the velocity of jets if they are large in diameter and penetrate beyond the jet center; (2) rectangular jets without tabs, compared to circular jets of the same exit area, provide faster jet mixing; and (3) further mixing enhancement is possible by using mechanical tabs.

Scattered acoustic field above a grating of parallel rectangular cavities

NASA Astrophysics Data System (ADS)

Khanfir, A.; Faiz, A.; Ducourneau, J.; Chatillon, J.; Skali Lami, S.

2013-02-01

The aim of this research project was to predict the sound pressure above a wall facing composed of N parallel rectangular cavities. The diffracted acoustic field is processed by generalizing the Kobayashi Potential (KP) method used for determining the electromagnetic field diffracted by a rectangular cavity set in a thick screen. This model enables the diffracted field to be expressed in modal form. Modal amplitudes are subsequently calculated using matrix equations obtained by enforcing boundary conditions. Solving these equations allows the determination of the total reflected acoustic field above the wall facing. This model was compared with experimental results obtained in a semi-anechoic room for a single cavity, a periodic array of three rectangular cavities and an aperiodic grating of nine rectangular cavities of different size and spacing. These facings were insonified by an incident spherical acoustic field, which was decomposed into plane waves. The validity of this model is supported by the agreement between the numerical and experimental results observed.

Dependence of charge transfer phenomena during solid-air two-phase flow on particle disperser

NASA Astrophysics Data System (ADS)

Tanoue, Ken-ichiro; Suedomi, Yuuki; Honda, Hirotaka; Furutani, Satoshi; Nishimura, Tatsuo; Masuda, Hiroaki

2012-12-01

An experimental investigation of the tribo-electrification of particles has been conducted during solid-air two-phase turbulent flow. The current induced in a metal plate by the impact of polymethylmethacrylate (PMMA) particles in a high-speed air flow was measured for two different plate materials. The results indicated that the contact potential difference between the particles and a stainless steel plate was positive, while for a nickel plate it was negative. These results agreed with theoretical contact charge transfer even if not only the particle size but also the kind of metal plate was changed. The specific charge of the PMMA particles during solid-air two-phase flow using an ejector, a stainless steel branch pipe, and a stainless steel straight pipe was measured using a Faraday cage. Although the charge was negative in the ejector, the particles had a positive specific charge at the outlet of the branch pipe, and this positive charge increased in the straight pipe. The charge decay along the flow direction could be reproduced by the charging and relaxation theory. However, the proportional coefficients in the theory changed with the particle size and air velocity. Therefore, an unexpected charge transfer occurred between the ejector and the branch pipe, which could not be explained solely by the contact potential difference. In the ejector, an electrical current in air might have been produced by self-discharge of particles with excess charge between the nickel diffuser in the ejector and the stainless steel nozzle or the stainless steel pipe due to a reversal in the contact potential difference between the PMMA and the stainless steel. The sign of the current depended on the particle size, possibly because the position where the particles impacted depended on their size. When dual coaxial glass pipes were used as a particle disperser, the specific charge of the PMMA particles became more positive along the particle flow direction due to the contact potential difference between the PMMA and the stainless steel. Furthermore, the current in air using the dual coaxial glass pipes was less than that using the ejector.

Shear flow control of cold and heated rectangular jets by mechanical tabs. Volume 2: Tabulated data

NASA Technical Reports Server (NTRS)

Brown, W. H.; Ahuja, K. K.

1989-01-01

The effects of mechanical protrusions on the jet mixing characteristics of rectangular nozzles for heated and unheated subsonic and supersonic jet plumes were studied. The characteristics of a rectangular nozzle of aspect ratio 4 without the mechanical protrusions were first investigated. Intrusive probes were used to make the flow measurements. Possible errors introduced by intrusive probes in making shear flow measurements were also examined. Several scaled sizes of mechanical tabs were then tested, configured around the perimeter of the rectangular jet. Both the number and the location of the tabs were varied. From this, the best configuration was selected. This volume contains tabulated data for each of the data runs cited in Volume 1. Baseline characteristics, mixing modifications (subsonic and supersonic, heated and unheated) and miscellaneous charts are included.

Novel single-cell mega-size chambers for electrochemical etching of panorama position-sensitive polycarbonate ion image detectors

NASA Astrophysics Data System (ADS)

Sohrabi, Mehdi

2017-11-01

A novel development is made here by inventing panorama single-cell mega-size electrochemical etching (MS-ECE) chamber systems for processing panorama position-sensitive mega-size polycarbonate ion image detectors (MS-PCIDs) of potential for many neutron and ion detection applications in particular hydrogen ions or proton tracks and images detected for the first time in polycarbonates in this study. The MS-PCID is simply a large polycarbonate sheet of a desired size. The single-cell MS-ECE invented consists of two large equally sized transparent Plexiglas sheets as chamber walls holding a MS-PCID and the ECE chamber components tightly together. One wall has a large flat stainless steel electrode (dry cell) attached to it which is directly in contact with the MS-PCID and the other wall has a rod electrode with two holes to facilitate feeding and draining out the etching solution from the wet cell. A silicon rubber washer plays the role of the wet cell to hold the etchant and the electrical insulator to isolate the dry cell from the wet cell. A simple 50 Hz-HV home-made generator provides an adequate field strength through the two electrodes across the MS-ECE chamber. Two panorama single-cell MS-ECE chamber systems (circular and rectangular shapes) constructed were efficiently applied to processing the MS-PCIDs for 4π ion emission image detection of different gases in particular hydrogen ions or protons in a 3.5 kJ plasma focus device (PFD as uniquely observed by the unaided eyes). The panorama MS-PCID/MS-ECE image detection systems invented are novel with high potential for many applications in particular as applied to 4π panorama ion emission angular distribution image detection studies in PFD space, some results of which are presented and discussed.

Novel single-cell mega-size chambers for electrochemical etching of panorama position-sensitive polycarbonate ion image detectors.

PubMed

Sohrabi, Mehdi

2017-11-01

A novel development is made here by inventing panorama single-cell mega-size electrochemical etching (MS-ECE) chamber systems for processing panorama position-sensitive mega-size polycarbonate ion image detectors (MS-PCIDs) of potential for many neutron and ion detection applications in particular hydrogen ions or proton tracks and images detected for the first time in polycarbonates in this study. The MS-PCID is simply a large polycarbonate sheet of a desired size. The single-cell MS-ECE invented consists of two large equally sized transparent Plexiglas sheets as chamber walls holding a MS-PCID and the ECE chamber components tightly together. One wall has a large flat stainless steel electrode (dry cell) attached to it which is directly in contact with the MS-PCID and the other wall has a rod electrode with two holes to facilitate feeding and draining out the etching solution from the wet cell. A silicon rubber washer plays the role of the wet cell to hold the etchant and the electrical insulator to isolate the dry cell from the wet cell. A simple 50 Hz-HV home-made generator provides an adequate field strength through the two electrodes across the MS-ECE chamber. Two panorama single-cell MS-ECE chamber systems (circular and rectangular shapes) constructed were efficiently applied to processing the MS-PCIDs for 4π ion emission image detection of different gases in particular hydrogen ions or protons in a 3.5 kJ plasma focus device (PFD as uniquely observed by the unaided eyes). The panorama MS-PCID/MS-ECE image detection systems invented are novel with high potential for many applications in particular as applied to 4π panorama ion emission angular distribution image detection studies in PFD space, some results of which are presented and discussed.

Jamming/flowing transition of non-Brownian particles suspended in a iso-density fluid flowing in a 2D rectangular duct

NASA Astrophysics Data System (ADS)

Burel, Maxym; Martin, Sylvain; Bonnefoy, Olivier

2017-06-01

We present the results of an experimental study on the jamming/flowing transition. A suspension of neutrally buoyant large particles flows in an horizontal rectangular duct, where an artificial restriction triggers jamming. We show that the avalanche distribution size is exponential, that is memoryless. We further demonstrate that the avalanche size diverges when the restriction size approaches a critical value and that this divergence is well described by a power law. The parameters (critical opening size and divergence velocity) are compared to literature values and show a strong similarity with others systems. Another result of this paper is the study of the influence of the particle morphology. We show that, for a moderate restriction size, the dead-zone formed right upstream of the restriction is larger for angular particles but, paradoxically, that the avalanche size is larger for polyhedra compared to spheres by at least one order of magnitude.

Trade off between variable and fixed size normalization in orthogonal polynomials based iris recognition system.

PubMed

Krishnamoorthi, R; Anna Poorani, G

2016-01-01

Iris normalization is an important stage in any iris biometric, as it has a propensity to trim down the consequences of iris distortion. To indemnify the variation in size of the iris owing to the action of stretching or enlarging the pupil in iris acquisition process and camera to eyeball distance, two normalization schemes has been proposed in this work. In the first method, the iris region of interest is normalized by converting the iris into the variable size rectangular model in order to avoid the under samples near the limbus border. In the second method, the iris region of interest is normalized by converting the iris region into a fixed size rectangular model in order to avoid the dimensional discrepancies between the eye images. The performance of the proposed normalization methods is evaluated with orthogonal polynomials based iris recognition in terms of FAR, FRR, GAR, CRR and EER.

Size-separated particle fractions of stainless steel welding fume particles - A multi-analytical characterization focusing on surface oxide speciation and release of hexavalent chromium.

PubMed

Mei, N; Belleville, L; Cha, Y; Olofsson, U; Odnevall Wallinder, I; Persson, K-A; Hedberg, Y S

2018-01-15

Welding fume of stainless steels is potentially health hazardous. The aim of this study was to investigate the manganese (Mn) and chromium (Cr) speciation of welding fume particles and their extent of metal release relevant for an inhalation scenario, as a function of particle size, welding method (manual metal arc welding, metal arc welding using an active shielding gas), different electrodes (solid wires and flux-cored wires) and shielding gases, and base alloy (austenitic AISI 304L and duplex stainless steel LDX2101). Metal release investigations were performed in phosphate buffered saline (PBS), pH 7.3, 37°, 24h. The particles were characterized by means of microscopic, spectroscopic, and electroanalytical methods. Cr was predominantly released from particles of the welding fume when exposed in PBS [3-96% of the total amount of Cr, of which up to 70% as Cr(VI)], followed by Mn, nickel, and iron. Duplex stainless steel welded with a flux-cored wire generated a welding fume that released most Cr(VI). Nano-sized particles released a significantly higher amount of nickel compared with micron-sized particle fractions. The welding fume did not contain any solitary known chromate compounds, but multi-elemental highly oxidized oxide(s) (iron, Cr, and Mn, possibly bismuth and silicon). Copyright © 2017 The Authors. Published by Elsevier B.V. All rights reserved.

On solving three-dimensional open-dimension rectangular packing problems

NASA Astrophysics Data System (ADS)

Junqueira, Leonardo; Morabito, Reinaldo

2017-05-01

In this article, a recently proposed three-dimensional open-dimension rectangular packing problem is considered, in which the objective is to find a minimal volume rectangular container that packs a set of rectangular boxes. The literature has tackled small-sized instances of this problem by means of optimization solvers, position-free mixed-integer programming (MIP) formulations and piecewise linearization approaches. In this study, the problem is alternatively addressed by means of grid-based position MIP formulations, whereas still considering optimization solvers and the same piecewise linearization techniques. A comparison of the computational performance of both models is then presented, when tested with benchmark problem instances and with new instances, and it is shown that the grid-based position MIP formulation can be competitive, depending on the characteristics of the instances. The grid-based position MIP formulation is also embedded with real-world practical constraints, such as cargo stability, and results are additionally presented.

Relativistic energy-dispersion relations of 2D rectangular lattices

NASA Astrophysics Data System (ADS)

Ata, Engin; Demirhan, Doğan; Büyükkılıç, Fevzi

2017-04-01

An exactly solvable relativistic approach based on inseparable periodic well potentials is developed to obtain energy-dispersion relations of spin states of a single-electron in two-dimensional (2D) rectangular lattices. Commutation of axes transfer matrices is exploited to find energy dependencies of the wave vector components. From the trace of the lattice transfer matrix, energy-dispersion relations of conductance and valence states are obtained in transcendental form. Graphical solutions of relativistic and nonrelativistic transcendental energy-dispersion relations are plotted to compare how lattice parameters V0, core and interstitial size of the rectangular lattice affects to the energy-band structures in a situation core and interstitial diagonals are of equal slope.

A Theoretical Investigation of the Input Characteristics of a Rectangular Cavity-Backed Slot Antenna

NASA Technical Reports Server (NTRS)

Cockrell, C. R.

1975-01-01

Equations which represent the magnetic and electric stored energies are derived for an infinite section of rectangular waveguide and a rectangular cavity. These representations which are referred to as being physically observable are obtained by considering the difference in the volume integrals appearing in the complex Poynting theorem. It is shown that the physically observable stored energies are determined by the field components that vanish in a reference plane outside the aperture. These physically observable representations are used to compute the input admittance of a rectangular cavity-backed slot antenna in which a single propagating wave is assumed to exist in the cavity. The slot is excited by a voltage source connected across its center; a sinusoidal distribution is assumed in the slot. Input-admittance calculations are compared with measured data. In addition, input-admittance curves as a function of electrical slot length are presented for several size cavities. For the rectangular cavity backed slot antenna, the quality factor and relative bandwidth were computed independently by using these energy relationships. It is shown that the asymptotic relationship which is usually assumed to exist between the quality bandwidth and the reciprocal of relative bandwidth is equally valid for the rectangular cavity backed slot antenna.

A low profile rectangular patch microstrip antenna for dual-band operation of wireless communication system

NASA Astrophysics Data System (ADS)

Rambe, A. H.; Abdillah, K.

2018-02-01

This paper discussed a low profile rectangular patch microstrip antenna design working on dual-band 1.8 GHz and 2.4 GHz. Dual-band characteristic is achieved by using inset-feed point and slot size adjustment. The designed antenna was printed on a FR4 substrate with relative permittivity of 4.4 and a thickness of 1.6 mm with patch size 40 x 29 mm. The measurement results show that the realized antenna successfully working on dual-band, achieving bandwidth of 45 MHz and 95 MHz, gain of 4.08 dBi and 5.79 dBi for 1.8 GHz and 2.4 GHz subsequently.

Experimental investigations on sodium-filled heat pipes

NASA Technical Reports Server (NTRS)

Dorner, S.; Reiss, F.; Schretzmann, K.

1977-01-01

The possibilities of producing heat pipes and, especially, the necessary capillary structures are discussed. Several types of heat pipes were made from stainless steel and tested at temperatures between 400 and 1055 deg C. The thermal power was determined by a calorimeter. Results indicate: bubble-free evaporation of sodium from rectangular open chennels is possible with a heat flux of more than 1,940 W/sq cm at 1055 C. The temperature drop along the tube could be measured only at low temperatures. A subdivided heat pipe worked against the gravitational field. A heat pipe with a capillary structure made of a rolled screen was supported by rings and bars operated at 250 W/sq cm heat flux in the evaporating region.

Cost and Performance Report: Innovative Welding Technologies Using Silicon Additives to Control Hazardous Air Pollutant (HAP) Emissions

DTIC Science & Technology

2013-08-30

turntable inside the hood to maintain a constant weld speed, while the ER308L stainless steel wire were fed by the welding gun. Figure 2. Fume chamber...size distribution, density and specific surface area of welding fumes from SMAW and GMAW mild- steel and stainless - steel consumables, American...shipyards. It uses mild or stainless steel filler material to join pieces of metal. The intense energy expended in the welding process results in the

Effects of deformation-induced martensite and grain size on ductile-to-brittle transition behavior of austenitic 18Cr-10Mn-N stainless steels

NASA Astrophysics Data System (ADS)

Hwang, Byoungchul; Lee, Tae-Ho; Kim, Sung-Joon

2010-12-01

Effects of deformation-induced martensite and grain size on ductile-to-brittle transition behavior of austenitic 18Cr-10Mn-(0.3˜0.6)N stainless steels with different alloying elements were investigated by means of Charpy impact tests and microstructural analyses. The steels all exhibited ductile-to-brittle transition behavior due to unusual brittle fracture at low temperatures despite having a face-centered cubic structure. The ductileto-brittle transition temperature (DBTT) obtained from Chapry impact tests did not coincide with that predicted by an empirical equation depending on N content in austenitic Cr-Mn-N stainless steels. Furthermore, a decrease of grain size was not effective in terms of lowering DBTT. Electron back-scattered diffraction and transmission electron microscopy analyses of the cross-sectional area of the fracture surface showed that some austenites with lower stability could be transformed to α'-martensite by localized plastic deformation near the fracture surface. Based on these results, it was suggested that when austenitic 18Cr-10Mn-N stainless steels have limited Ni, Mo, and N content, the deterioration of austenite stability promotes the formation of deformation-induced martensite and thus increases DBTT by substantially decreasing low-temperature toughness.

Boiling Visualization and Critical Heat Flux Phenomena In Narrow Rectangular Gap

DOE Office of Scientific and Technical Information (OSTI.GOV)

J. J. Kim; Y. H. Kim; S. J. Kim

2004-12-01

An experimental study was performed to investifate the pool boling critical hear flux (CHF) on one-dimensional inclined rectangular channels with narrow gaps by changing the orientation of a copper test heater assembly. In a pool of saturated water at atmospheric pressure, the test parameters include the gap sizes of 1,2,5, and 10 mm, andthe surface orientation angles from the downward facing position (180 degrees) to the vertical position (90 degress) respectively.

One-dimensional acoustic standing waves in rectangular channels for flow cytometry.

PubMed

Austin Suthanthiraraj, Pearlson P; Piyasena, Menake E; Woods, Travis A; Naivar, Mark A; Lόpez, Gabriel P; Graves, Steven W

2012-07-01

Flow cytometry has become a powerful analytical tool for applications ranging from blood diagnostics to high throughput screening of molecular assemblies on microsphere arrays. However, instrument size, expense, throughput, and consumable use limit its use in resource poor areas of the world, as a component in environmental monitoring, and for detection of very rare cell populations. For these reasons, new technologies to improve the size and cost-to-performance ratio of flow cytometry are required. One such technology is the use of acoustic standing waves that efficiently concentrate cells and particles to the center of flow channels for analysis. The simplest form of this method uses one-dimensional acoustic standing waves to focus particles in rectangular channels. We have developed one-dimensional acoustic focusing flow channels that can be fabricated in simple capillary devices or easily microfabricated using photolithography and deep reactive ion etching. Image and video analysis demonstrates that these channels precisely focus single flowing streams of particles and cells for traditional flow cytometry analysis. Additionally, use of standing waves with increasing harmonics and in parallel microfabricated channels is shown to effectively create many parallel focused streams. Furthermore, we present the fabrication of an inexpensive optical platform for flow cytometry in rectangular channels and use of the system to provide precise analysis. The simplicity and low-cost of the acoustic focusing devices developed here promise to be effective for flow cytometers that have reduced size, cost, and consumable use. Finally, the straightforward path to parallel flow streams using one-dimensional multinode acoustic focusing, indicates that simple acoustic focusing in rectangular channels may also have a prominent role in high-throughput flow cytometry. Copyright © 2012 Elsevier Inc. All rights reserved.

Development of nano/sub-micron grain structures in metastable austenitic stainless steels

NASA Astrophysics Data System (ADS)

Rajasekhara, Shreyas

2007-12-01

This dissertation is a part of a collaborative work between the University of Texas, Austin-Texas, the University of Oulu, Oulu-Finland, and Outokumpu Stainless Oy, Tornio-Finland, to develop commercial austenitic stainless steels with high strength and ductility. The idea behind this work involves cold-rolling a commercial metastable austenitic stainless steel - AISI 301LN stainless steel to produce strain-induced martensite, followed by an annealing treatment to generate nano/sub-micron grained austenite. AISI 301LN stainless steel sheets are cold-rolled to 63% reduction and subsequently annealed at 600°C, 700°C, 800°C, 900°C and 1000°C for 1, 10 and 100 seconds. The samples are analyzed by X-Ray diffraction, SQUID, transmission electron microscopy, and tensile testing to fundamentally understand the microstructural evolution, the mechanism for the martensite → austenite reversion, the formation of nano/sub-micron austenite grains, and the relationship between the microstructure and the strength obtained in this stainless steel. The results show that cold-rolled AISI 301LN stainless steel consist of dislocation-cell martensite, heavily deformed lath-martensite and austenite shear bands. Subsequent annealing at 600°C for short durations of 1 and 10 seconds leads to negligible martensite to austenite reversion. These 600°C samples exhibit a similar microstructure to the cold-rolled sample. However, for samples annealed at 600°C for 100 seconds and those annealed at higher temperatures (700°C, 800°C, 900°C and 1000°C) exhibit equiaxed austenitic grains of sizes 0.2mum-10mum and secondary phase precipitates. The microstructural analysis also reveals that the martensite → austenite reversion occurs via a diffusion-type reversion mechanism. In this regard, a generalized form of Avrami's equation is used to model the kinetics of martensite → austenite phase reversion. The results from the model agree reasonably well with the experiments. Furthermore, the activation energy for grain growth in nano/sub-micron grained AISI 301LN stainless steel is found to be ˜ 205kJ/mol, which is comparable to values observed in coarse grained commercial stainless steels (AISI 304, 316). However, the driving force for grain growth in nano/sub-micron grained AISI 301LN stainless steel is considerably higher when compared to other stainless steels. Finally, the average grain sizes in AISI 301LN stainless steels are related to the mechanical properties obtained, through the Hall-Petch relationship.

Effects of intraoral aging of arch-wires on frictional forces: An ex vivo study.

PubMed

Kumar, Avinash; Khanam, Arifa; Ghafoor, Hajra

2016-01-01

Archwires act as gears to move teeth with light, continuous forces. However, the intraoral use of orthodontic archwires is liable to surface deposits which alter the mechanical properties of archwires, causing an increase in the friction coefficient. To evaluate the surface changes of the stainless steel archwires after 6 weeks of intraoral use and its influence on frictional resistance during sliding mechanics. As-received rectangular 0.019" × 0.025" stainless steel orthodontic archwires (control) were compared with the archwires retrieved after the final phase of leveling and alignment stage of orthodontic treatment collected after 6 weeks of intraoral exposure (test samples) from 10 patients undergoing treatment. The control and test samples were used to evaluate surface debris using Scanning Electron Microscopy, surface roughness was assessed using Atomic Force Microscope and frictional forces were measured using Instron Universal Testing Machine in the buccal inter-bracket region that slides through the molar tube for space closure. Unpaired t -test and Pearson correlation tests were used for statistical analysis ( P < 0.05 level of significance). Significant increase was observed in the level of debris ( P = 0.0001), surface roughness ( P = 0.0001), and friction resistance ( P = 0.001) of orthodontic archwires after their intraoral exposure. Significant positive correlations ( P < 0.05) were also observed between these three variables. Stainless steel test archwires showed a significant increase in the degree of debris and surface roughness, increasing the frictional forces between the archwire-bracket interfaces which would considerably reduce the normal orthodontic forces. Thus, continuing the same archwire after levelling and alignment for space closure is not recommended.

Comparative study of friction between metallic and conventional interactive self-ligating brackets in different alignment conditions.

PubMed

Jakob, Sérgio Ricardo; Matheus, Davison; Jimenez-Pellegrin, Maria Cristina; Turssi, Cecília Pedroso; Amaral, Flávia Lucisano Botelho

2014-01-01

The aim of this study was to compare the friction between three bracket models: conventional stainless steel (Ovation, Dentsply GAC), self-ligating ceramic (In-Ovation, Denstply GAC) and self-ligating stainless steel brackets (In-Ovation R, Dentsply GAC). Five brackets were used for each model. They were bonded to an aluminum prototype that allowed the simulation of four misalignment situations (n = 10). Three of these situations occured at the initial phase (in which a 0.016-in nickel-titanium wire was used): 1. horizontal; 2. vertical; and 3. simultaneous horizontal/vertical. One of the situations occurred at the final treatment phase: 4. no misalignment (in which a 0.019 x 0.025-inch stainless steel rectangular wire was used). The wires slipped through the brackets and friction was measured by a Universal Testing Machine. Analysis of variance followed by Tukey's Test for multiple comparisons (α = 0.05) were applied to assess the results. Significant interaction (p < 0.01) among groups was found. For the tests that simulated initial alignment, Ovation® bracket produced the highest friction. The two self-ligating models resulted in lower and similar values, except for the horizontal situation, in which In-Ovation C® showed lower friction, which was similar to the In-Ovation R® metallic model. For the no misalignment situation, the same results were observed. The self-ligating system was superior to the conventional one due to producing less friction. With regard to the material used for manufacturing the brackets, the In-Ovation C® ceramic model showed less friction than the metallic ones.

Characterization of 17-4 PH stainless steel foam for biomedical applications in simulated body fluid and artificial saliva environments.

PubMed

Mutlu, Ilven; Oktay, Enver

2013-04-01

Highly porous 17-4 PH stainless steel foam for biomedical applications was produced by space holder technique. Metal release and weight loss from 17-4 PH stainless steel foams was investigated in simulated body fluid and artificial saliva environments by static immersion tests. Inductively coupled plasma-mass spectrometer was employed to measure the concentrations of various metal ions released from the 17-4 PH stainless steel foams into simulated body fluids and artificial saliva. Effect of immersion time and pH value on metal release and weight loss in simulated body fluid and artificial saliva were determined. Pore morphology, pore size and mechanical properties of the 17-4 PH stainless steel foams were close to human cancellous bone. Copyright © 2012 Elsevier B.V. All rights reserved.

Rectangular Microstrip Antenna with Slot Embedded Geometry

NASA Astrophysics Data System (ADS)

Ambresh, P. A.; Hadalgi, P. M.; Hunagund, P. V.; Sujata, A. A.

2014-09-01

In this paper, a novel design that improves the performance of conventional rectangular microstrip antenna is discussed. Design adopts basic techniques such as probe feeding technique with rectangular inverted patch structure as superstrate, air filled dielectric medium as substrate and slot embedded patch. Prototype of the proposed antenna has been fabricated and various antenna performance parameters such as impedance bandwidth, return loss, radiation pattern and antenna gain are considered for Electromagnetic-study. The antennas are designed for the wireless application operating in the frequency range of 3.3 GHz to 3.6 GHz, and UK based fixed satellite service application (3 GHz to 4 GHz), and are named as single inverted patch conventional rectangular microstrip antenna (SIP-CRMSA) and slots embedded inverted patch rectangular microstrip antenna (SEIP-RMSA), respectively. Measurement outcomes for SEIP-RMSA1 and SEIP-RMSA2 showed the satisfactory performance with an achievable impedance bandwidth of 260 MHz (7 %) and 250 MHz (6.72 %), with return loss (RL) of -11.06 dB and -17.98 dB, achieved gain of 8.17 dB and 5.17 dB with 10% and 8% size reduction in comparison with the conventional patch antenna.

Influence of surface rectangular defect winding layer on burst pressure of CNG-II composite cylinder

NASA Astrophysics Data System (ADS)

You, H. X.; Peng, L.; Zhao, C.; Ma, K.; Zhang, S.

2018-01-01

To study the influence of composite materials’ surface defect on the burst pressure of CNG-II composite cylinder, the surface defect was simplified as a rectangular slot of certain size on the basis of actually investigating the shape of cylinder’s surface defect. A CNG-II composite cylinder with a rectangular slot defect (2mm in depth) was used for burst test, and the numerical simulation software ANSYS was used to calculate its burst pressure. Through comparison between the burst pressure in the test and the numerical analysis result, the correctness of the numerical analysis method was verified. On this basis, the numerical analysis method was conducted for composite cylinders with surface defect in other depth. The result showed that surface defect in the form of rectangular slot had no significant effect on the liner stress of composite cylinder. Instead, it had a great influence on the stress of fiber-wrapped layer. The burst pressure of the composite cylinder decreased as the defect depth increasing. The hoop stress at the bottom of the defect in the shape of rectangular slot exceeded the maximum of the composite materials’ tensile strength, which could result in the burst pressure of composite cylinders decreasing.

Strength of Rectangular Flat Plates Under Edge Compression

NASA Technical Reports Server (NTRS)

Schuman, Louis; Back, Goldie

1931-01-01

Flat rectangular plates of duralumin, stainless iron, monel metal, and nickel were tested under loads applied at two opposite edges and acting in the plane of the plate. The edges parallel to the direction of loading were supported in V grooves. The plates were all 24 inches long and varied in width from 4 to 24 inches by steps of 4 inches, and in thickness from 0.015 to 0.095 inch by steps of approximately 0.015 inch. There were also a few 1, 2, 3, and 6 inch wide specimens. The loads were applied in the testing machine at the center of a bar which rested along the top of the plate. Load was applied until the plate failed to take any more load. The tests show that the loads carried by the plates generally reached a maximum for the 8 or 12 inch width and that there was relatively small drop in load for the greater widths. Deflection and set measurement perpendicular to the plane of the plate were taken and the form of the buckle determined. The number of buckles were found to correspond in general to that predicted by the theory of buckling of a plate uniformly loaded at two opposite edges and simply supported at the edges.

Digital Laser Speckle Technologies in Measuring Blood Flow in Biotissues and the Stressed-Strained State of the Maxillodental System

NASA Astrophysics Data System (ADS)

Rubnikovich, S. P.; Denisova, Yu. A.; Fomin, N. A.

2017-11-01

A method has been developed for estimating the stressed-strained state in the ″orthodontic apparatus-dentin″ system with the use of laser-optical diagnostics based on speckle photography. We have determined the indices of the stressed-strained state in the ″orthodontic apparatus-dentin″ system depending on the composition and form of the orthodontic arch cross section. We have determined the optimum indices of the stressed-strained state of orthodontic arches in patients with periodontium diseases in combination with maxillodental anomalies and deformations, to which the following arches correspond: from copper-nickel-titanium (CuNiTi) alloy with circular (0.012″, 0.013″, 0.014″, 0.016″, 0.018″), and rectangular (0.014 × 0.025″, 0.016 × 0.025″) cross sections, from titanium-molybdenum alloy (TMA) with a rectangular cross section (0.016 × 0.025″), and from stainless steel (SS) with a circular (0.016″, 0.018″) cross section. Direct correlation has been established between indices of the stressed-strained state in the ″orthodontic apparatus-dentin″ system and the periodontium capillary pressure (r = 0.78, p < 0.05), as well as inverse strong correlation with the periodontium microcirculation intensity (r = -0.88, p < 0.05).

Fatigue life characterization for piezoelectric macrofiber composites

NASA Astrophysics Data System (ADS)

Henslee, Isaac A.; Miller, David A.; Tempero, Tyler

2012-10-01

In an effort to aid the investigation into lightweight and reliable materials for actuator design, a study was developed to characterize the temperature-dependent lifetime performance of a piezoelectric macrofiber composite (MFC). MFCs are thin rectangular patches of polyimide film, epoxy and a single layer of rectangular lead zirconium titanate (PZT) fibers. In this study, the useful life of the MFC is characterized to determine the effect of temperature on the performance of the composite as it is fatigued by cyclic piezoelectric excitation. The test specimen consists of the MFC laminated to a cantilevered stainless steel beam. Beam strain and tip displacement measurements are used as a basis for determining the performance of the MFC as it is cyclically actuated under various operating temperatures. The temperature of the beam laminate is held constant and then cycled to failure, or 250 million cycles, in order to determine the useful life of the MFC over a temperature range from - 15 to 145 °C. The results of the experiments show a strong temperature dependence of the operational life for the MFC. Damage inside the composite was identified through in situ visual inspection and during post-test microstructural observation; however, no degradation in operational performance was identified as it was cyclically actuated up to the point of failure, regardless of temperature or actuation cycle number.

From micro- to nano-scale molding of metals : size effect during molding of single crystal Al with rectangular strip punches.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, K.; Meng, W. J.; Mei, F.

2011-02-01

A single crystal Al specimen was molded at room temperature with long, rectangular, strip diamond punches. Quantitative molding response curves were obtained at a series of punch widths, ranging from 5 {micro}m to 550 nm. A significant size effect was observed, manifesting itself in terms of significantly increasing characteristic molding pressure as the punch width decreases to 1.5 {micro}m and below. A detailed comparison of the present strip punch molding results was made with Berkovich pyramidal indentation on the same single crystal Al specimen. The comparison reveals distinctly different dependence of the characteristic pressure on corresponding characteristic length. The presentmore » results show the feasibility of micro-/nano-scale compression molding as a micro-/nano-fabrication technique, and offer an experimental test case for size-dependent plasticity theories.« less

Nonlinear Dynamical Model of a Soft Viscoelastic Dielectric Elastomer

NASA Astrophysics Data System (ADS)

Zhang, Junshi; Chen, Hualing; Li, Dichen

2017-12-01

Actuated by alternating stimulation, dielectric elastomers (DEs) show a behavior of complicated nonlinear vibration, implying a potential application as dynamic electromechanical actuators. As is well known, for a vibrational system, including the DE system, the dynamic properties are significantly affected by the geometrical sizes. In this article, a nonlinear dynamical model is deduced to investigate the geometrical effects on dynamic properties of viscoelastic DEs. The DEs with square and arbitrary rectangular geometries are considered, respectively. Besides, the effects of tensile forces on dynamic performances of rectangular DEs with comparably small and large geometrical sizes are explored. Phase paths and Poincaré maps are utilized to detect the periodicity of the nonlinear vibrations of DEs. The resonance characteristics of DEs incorporating geometrical effects are also investigated. The results indicate that the dynamic properties of DEs, including deformation response, vibrational periodicity, and resonance, are tuned when the geometrical sizes vary.

Elaboration of austenitic stainless steel samples with bimodal grain size distributions and investigation of their mechanical behavior

NASA Astrophysics Data System (ADS)

Flipon, B.; de la Cruz, L. Garcia; Hug, E.; Keller, C.; Barbe, F.

2017-10-01

Samples of 316L austenitic stainless steel with bimodal grain size distributions are elaborated using two distinct routes. The first one is based on powder metallurgy using spark plasma sintering of two powders with different particle sizes. The second route applies the reverse-annealing method: it consists in inducing martensitic phase transformation by plastic strain and further annealing in order to obtain two austenitic grain populations with different sizes. Microstructural analy ses reveal that both methods are suitable to generate significative grain size contrast and to control this contrast according to the elaboration conditions. Mechanical properties under tension are then characterized for different grain size distributions. Crystal plasticity finite element modelling is further applied in a configuration of bimodal distribution to analyse the role played by coarse grains within a matrix of fine grains, considering not only their volume fraction but also their spatial arrangement.

Industrial Implementation of Environmentally Friendly Nanometal Electroplating Process for Chromium and Copper Beryllium Replacement using Low Cost Pulse Current Power Supplies

DTIC Science & Technology

2014-09-10

Cr-Mo, and stainless steel have to some extent found acceptance in various military and commercial CuBe-replacement roles. 1.1.2 Proposed...including low and high strength steels , stainless steel , Inconel and nickel. Figure 4-8 Activation line used to prepare components for nCoP plating...size up to a maximum thickness of 0.012”, can be produced in the tank by electroforming onto a flat stainless steel mandrel and subsequently

Persistence of deposited metals in the lungs after stainless steel and mild steel welding fume inhalation in rats.

PubMed

Antonini, James M; Roberts, Jenny R; Stone, Samuel; Chen, Bean T; Schwegler-Berry, Diane; Chapman, Rebecca; Zeidler-Erdely, Patti C; Andrews, Ronnee N; Frazer, David G

2011-05-01

Welding generates complex metal fumes that vary in composition. The objectives of this study were to compare the persistence of deposited metals and the inflammatory potential of stainless and mild steel welding fumes, the two most common fumes used in US industry. Sprague-Dawley rats were exposed to 40 mg/m(3) of stainless or mild steel welding fumes for 3 h/day for 3 days. Controls were exposed to filtered air. Generated fume was collected, and particle size and elemental composition were determined. Bronchoalveolar lavage was done on days 0, 8, 21, and 42 after the last exposure to assess lung injury/inflammation and to recover lung phagocytes. Non-lavaged lung samples were analyzed for total and specific metal content as a measure of metal persistence. Both welding fumes were similar in particle morphology and size. Following was the chemical composition of the fumes-stainless steel: 57% Fe, 20% Cr, 14% Mn, and 9% Ni; mild steel: 83% Fe and 15% Mn. There was no effect of the mild steel fume on lung injury/inflammation at any time point compared to air control. Lung injury and inflammation were significantly elevated at 8 and 21 days after exposure to the stainless steel fume compared to control. Stainless steel fume exposure was associated with greater recovery of welding fume-laden macrophages from the lungs at all time points compared with the mild steel fume. A higher concentration of total metal was observed in the lungs of the stainless steel welding fume at all time points compared with the mild steel fume. The specific metals present in the two fumes were cleared from the lungs at different rates. The potentially more toxic metals (e.g., Mn, Cr) present in the stainless steel fume were cleared from the lungs more quickly than Fe, likely increasing their translocation from the respiratory system to other organs.

Characterization of 17-4PH stainless steel powders produced by supersonic gas atomization

NASA Astrophysics Data System (ADS)

Zhao, Xin-Ming; Xu, Jun; Zhu, Xue-Xin; Zhang, Shao-Ming; Zhao, Wen-Dong; Yuan, Guo-Liang

2012-01-01

17-4PH stainless steel powders were prepared using a supersonic nozzle in a close-coupled gas atomization system. The characteristics of powder particles were carried out by means of a laser particle size analyzer, scanning electron microscopy (SEM), and the X-ray diffraction (XRD) technique. The results show that the mass median particle diameter is about 19.15 μm. Three main types of surface microstructures are observed in the powders: well-developed dendrite, cellular, and cellular dendrite structure. The XRD measurements show that, as the particle size decreases, the amount of fcc phase gradually decreases and that of bcc phase increases. The cooling rate is inversely related to the particle size, i.e., it decreases with an increase in particle size.

Rectangular pulsed LD pumped saturable output coupler (SOC) Q-switched microchip laser

NASA Astrophysics Data System (ADS)

Wang, Yan-biao; Wang, Sha; Feng, Guo-ying; Zhou, Shou-huan

2017-02-01

We studied the cw LD and rectangular pulsed LD pumped saturable output coupler (SOC) passively Q-switched Nd:YVO4 transmission microchip laser experimentally. We demonstrated that the SOC passively Q-switched Nd:YVO4 transmission microchip laser pumped by a highly stabilized narrow bandwidth pulsed LD has a much lower timing jitter than pumped by a continuous wave (CW) LD, especially at low output frequency regime. By changing the pump beam size in the rectangular shape pulsed pump scheme, the output frequency can be achieved from 333.3 kHz to 71.4 kHz, while the relative timing jitter decreased from 0.09865% to 0.03115% accordingly. Additionally, the microchip laser has a good stability of output power, the power fluctuation below 2%.

Computed Tomographic Evaluation of K3 Rotary and Stainless Steel K File Instrumentation in Primary Teeth

PubMed Central

Kavitha, Swaminathan; Thomas, Eapen; Anadhan, Vasanthakumari; Vijayakumar, Rajendran

2016-01-01

Introduction The intention of root canal preparation is to reduce infected content and create a root canal shape allowing for a well condensed root filling. Therefore, it is not necessary to remove excessive dentine for successful root canal preparation and concern must be taken not to over instrument as perforations can occur in the thin dentinal walls of primary molars. Aim This study was done to evaluate the time preparation, the risk of lateral perforation and dentine removal of the stainless steel K file and K3 rotary instrumentation in primary teeth. Materials and Methods Seventy-five primary molars were selected and divided into three groups. Using spiral computed tomography the teeth were scanned before instrumentation. Teeth were prepared using a stainless steel K file for manual technique. All the canals were prepared up to file size 35. In K3 rotary files (.02 taper) instrumentation was done up to 35 size file. In K3 rotary files (.04 taper) the instrumentation was done up to 25 size file and simultaneously the instrumentation time was recorded. The instrumented teeth were once again scanned and the images were compared with the images of the uninstrumented canals. Statistical Analysis Data was statistically analysed using Kruskal Wallis One-way ANOVA, Mann-Whitney U-Test and Pearson’s Chi-square Test. Results K3 rotary files (.02 taper) removed a significantly less amount of dentine, required less instrumentation time than a stainless steel K file. Conclusion K3 files (.02 taper) generated less dentine removal than the stainless steel K file and K3 files (.04 taper). K3 rotary files (.02 taper) were more effective for root canal instrumentation in primary teeth. PMID:26894166

Orthodontic archwire composition and phase analyses by neutron spectroscopy.

PubMed

Tian, Kun V; Festa, Giulia; Basoli, Francesco; Laganà, Giuseppina; Scherillo, Antonella; Andreani, Carla; Bollero, Patrizio; Licoccia, Silvia; Senesi, Roberto; Cozza, Paola

2017-05-31

Quantitative metallurgical and phase analyses employing neutron diffraction technique were conducted on two as-received commercial rectangular austenitic stainless steel orthodontic archwires, G&H and Azdent, 0.43×0.64 mm (0.017×0.025 inch). Results showed a bi-phase structure containing martensitic phase (45.67% for G&H and 6.62% for Azdent) in addition to the expected metastable austenite. The former may be a strain-induced phase-transformation arising during the cold working process of wire fabrication. Further neutron resonance capture analysis determinations provided atomic and isotopic compositions, including alloying elements in each sample, complementary to the results of traditional energy dispersive X-ray spectroscopy. Together, these results assist in relating commercial alloying recipes and processing histories with mechanical performance, strength and ductility in particular.

Effect of irradiation temperature on microstructural changes in self-ion irradiated austenitic stainless steel

NASA Astrophysics Data System (ADS)

Jin, Hyung-Ha; Ko, Eunsol; Lim, Sangyeob; Kwon, Junhyun; Shin, Chansun

2017-09-01

We investigated the microstructural and hardness changes in austenitic stainless steel after Fe ion irradiation at 400, 300, and 200 °C using transmission electron microscopy (TEM) and nanoindentation. The size of the Frank loops increased and the density decreased with increasing irradiation temperature. Radiation-induced segregation (RIS) was detected across high-angle grain boundaries, and the degree of RIS increases with increasing irradiation temperature. Ni-Si clusters were observed using high-resolution TEM in the sample irradiated at 400 °C. The results of this work are compared with the literature data of self-ion and proton irradiation at comparable temperatures and damage levels on stainless steels with a similar material composition with this study. Despite the differences in dose rate, alloy composition and incident ion energy, the irradiation temperature dependence of RIS and the size and density of radiation defects followed the same trends, and were very comparable in magnitude.

Development of Metal Plate with Internal Structure Utilizing the Metal Injection Molding (MIM) Process.

PubMed

Shin, Kwangho; Heo, Youngmoo; Park, Hyungpil; Chang, Sungho; Rhee, Byungohk

2013-12-12

In this study, we focus on making a double-sided metal plate with an internal structure, such as honeycomb. The stainless steel powder was used in the metal injection molding (MIM) process. The preliminary studies were carried out for the measurement of the viscosity of the stainless steel feedstock and for the prediction of the filling behavior through Computer Aided Engineering (CAE) simulation. PE (high density polyethylene (HDPE) and low density polyethylene (LDPE)) and polypropylene (PP) resins were used to make the sacrificed insert with a honeycomb structure using a plastic injection molding process. Additionally, these sacrificed insert parts were inserted in the metal injection mold, and the metal injection molding process was carried out to build a green part with rectangular shape. Subsequently, debinding and sintering processes were adopted to remove the sacrificed polymer insert. The insert had a suitable rigidity that was able to endure the filling pressure. The core shift analysis was conducted to predict the deformation of the insert part. The 17-4PH feedstock with a low melting temperature was applied. The glass transition temperature of the sacrificed polymer insert would be of a high grade, and this insert should be maintained during the MIM process. Through these processes, a square metal plate with a honeycomb structure was made.

Development of Metal Plate with Internal Structure Utilizing the Metal Injection Molding (MIM) Process

PubMed Central

Shin, Kwangho; Heo, Youngmoo; Park, Hyungpil; Chang, Sungho; Rhee, Byungohk

2013-01-01

In this study, we focus on making a double-sided metal plate with an internal structure, such as honeycomb. The stainless steel powder was used in the metal injection molding (MIM) process. The preliminary studies were carried out for the measurement of the viscosity of the stainless steel feedstock and for the prediction of the filling behavior through Computer Aided Engineering (CAE) simulation. PE (high density polyethylene (HDPE) and low density polyethylene (LDPE)) and polypropylene (PP) resins were used to make the sacrificed insert with a honeycomb structure using a plastic injection molding process. Additionally, these sacrificed insert parts were inserted in the metal injection mold, and the metal injection molding process was carried out to build a green part with rectangular shape. Subsequently, debinding and sintering processes were adopted to remove the sacrificed polymer insert. The insert had a suitable rigidity that was able to endure the filling pressure. The core shift analysis was conducted to predict the deformation of the insert part. The 17-4PH feedstock with a low melting temperature was applied. The glass transition temperature of the sacrificed polymer insert would be of a high grade, and this insert should be maintained during the MIM process. Through these processes, a square metal plate with a honeycomb structure was made. PMID:28788427

Evaluation of force released by deflection of orthodontic wires in conventional and self-ligating brackets.

PubMed

Higa, Rodrigo Hitoshi; Semenara, Nayara Thiago; Henriques, José Fernando Castanha; Janson, Guilherme; Sathler, Renata; Fernandes, Thais Maria Freire

2016-01-01

The aim of the study was to evaluate deflection forces of rectangular orthodontic wires in conventional (MorelliTM), active (In-Ovation RTM) and passive (Damon 3MXTM) self-ligating brackets. Two brands of stainless steel and nickel-titanium (NiTi) wires (MorelliTM and GACTM), in addition to OrmcoTM copper-nickel-titanium wires were used. Specimens were assembled in a clinical simulation device especially designed for this study and tested in an Instron universal testing machine. For the testing procedures, an acrylic structure representative of the maxillary right central incisor was lingually moved in activations of 0 to 1 mm, with readings of the force released by deflection in unloading of 0.5, 0.8 and 1 mm at a constant speed of 2 mm/min. Inter-bracket forces with stainless steel, NiTi and CuNiTi were individually compared by two-way ANOVA, followed by Tukey's tests. Results showed that there were lower forces in conventional brackets, followed by active and passive self-ligating brackets. Within the brands, only for NiTi wires, the MorelliTM brand presented higher forces than GACTM wires. Bracket systems provide different degrees of deflection force, with self-ligating brackets showing the highest forces.

Thermal Plasma Spheroidization of High-Nitrogen Stainless Steel Powder Alloys Synthesized by Mechanical Alloying

NASA Astrophysics Data System (ADS)

Razumov, Nikolay G.; Popovich, Anatoly A.; Wang, QingSheng

2018-03-01

This paper presents the results of experimental studies on the treatment of Fe-23Cr-11Mn-1N high-nitrogen stainless steel powder alloys, synthesized by the mechanical alloying (MA) of elemental powders in the flow of a thermal plasma. Fe-23Cr-11Mn-1N high-nitrogen stainless steel powder alloys were prepared by MA in the attritor under an argon atmosphere. For spheroidization of Fe-23Cr-11Mn-1N high-nitrogen stainless steel powder alloys, the TekSphero 15 plant manufactured by Tekna Plasma Systems Inc was used. The studies have shown the possibility of obtaining Fe-23Cr-11Mn-1N high-nitrogen spherical powders steel alloys from the powder obtained by MA. According to the results of a series of experiments, it was found that the results of plasma spheroidization of powders essentially depend on the size of the fraction due to some difference in the particle shape and flowability, and on the gas regime of the plasma torch. It is established that during the plasma spheroidization process, some of the nitrogen leaves the alloy. The loss rate of nitrogen depends on the size of the initial particles.

Comparative study of friction between metallic and conventional interactive self-ligating brackets in different alignment conditions

PubMed Central

Jakob, Sérgio Ricardo; Matheus, Davison; Jimenez-Pellegrin, Maria Cristina; Turssi, Cecília Pedroso; do Amaral, Flávia Lucisano Botelho

2014-01-01

Objective The aim of this study was to compare the friction between three bracket models: conventional stainless steel (Ovation, Dentsply GAC), self-ligating ceramic (In-Ovation, Denstply GAC) and self-ligating stainless steel brackets (In-Ovation R, Dentsply GAC). Methods Five brackets were used for each model. They were bonded to an aluminum prototype that allowed the simulation of four misalignment situations (n = 10). Three of these situations occurred at the initial phase (in which a 0.016-in nickel-titanium wire was used): 1. horizontal; 2. vertical; and 3. simultaneous horizontal/vertical. One of the situations occurred at the final treatment phase: 4. no misalignment (in which a 0.019 x 0.025-inch stainless steel rectangular wire was used). The wires slipped through the brackets and friction was measured by a Universal Testing Machine. Results Analysis of variance followed by Tukey's Test for multiple comparisons (α = 0.05) were applied to assess the results. Significant interaction (p < 0.01) among groups was found. For the tests that simulated initial alignment, Ovation® bracket produced the highest friction. The two self-ligating models resulted in lower and similar values, except for the horizontal situation, in which In-Ovation C® showed lower friction, which was similar to the In-Ovation R® metallic model. For the no misalignment situation, the same results were observed. Conclusion The self-ligating system was superior to the conventional one due to producing less friction. With regard to the material used for manufacturing the brackets, the In-Ovation C® ceramic model showed less friction than the metallic ones. PMID:25162570

Impact of different rectangular wires on torsional expression of different sizes of buccal tube.

PubMed

Ajami, Shabnam; Boroujeni, Afshar-Rasti

2018-01-01

Torsions in rectangular wires are the essential part of corrections in the finishing stage of treatment. Moreover the greatest amounts of torques are applied in the molar areas. a clinically effective moment is between 5 and 20 Nmm. In this study we have decided to evaluate the impact of different tube sizes and different dimensions of wires with different modulus of elasticities on the amount torsional bond strength of molar tubes. 60 human impacted molar teeth were collected. A buccal tube was bonded on the buccal surface of all the samples by using light cured adhesive resin. After that, the teeth were mounted in a hard acrylic block. According to the size of buccal tube and the rectangular wires to be tested 4 groups will be designed. Torsional force was applied by instron machine. The torque angle at 5Nmm and at 20Nmm point will be calculated: which means, how many degrees of torque is required to reach the maximum 20Nmm moment from the minimum 5Nmm.One-way ANOVA was used to compare torque angle in all of the groups. The least amount of clinically significant angle was 2.2 ᵒ in the 0.017×0.025 SS and the largest amount of it was 23.7 ᵒ in the 0.017×0.025 TMA in 0.018×0.025 slot molar tube. But, this angle was 19.9 ᵒand 13.6 ᵒ in 0.019×0.025 SS and 0.019×0.025 TMA archwire in 0.022×0.028 molar tube. The 0.017×0.025 SS archwire in 0.018×0.025 molar tube had the lowest clinically significant angle. The largest amount was seen in group 0.017×0.025 TMA in 0.018×0.025 slot molar tube. Key words: Torsional efficacy, rectangular wires, buccal tubes, torque angle.

Impact of different rectangular wires on torsional expression of different sizes of buccal tube

PubMed Central

Boroujeni, Afshar-Rasti

2018-01-01

Background Torsions in rectangular wires are the essential part of corrections in the finishing stage of treatment. Moreover the greatest amounts of torques are applied in the molar areas. a clinically effective moment is between 5 and 20 Nmm. In this study we have decided to evaluate the impact of different tube sizes and different dimensions of wires with different modulus of elasticities on the amount torsional bond strength of molar tubes. Material and Methods 60 human impacted molar teeth were collected. A buccal tube was bonded on the buccal surface of all the samples by using light cured adhesive resin. After that, the teeth were mounted in a hard acrylic block. According to the size of buccal tube and the rectangular wires to be tested 4 groups will be designed. Torsional force was applied by instron machine. The torque angle at 5Nmm and at 20Nmm point will be calculated: which means, how many degrees of torque is required to reach the maximum 20Nmm moment from the minimum 5Nmm.One-way ANOVA was used to compare torque angle in all of the groups. Results The least amount of clinically significant angle was 2.2 ᵒ in the 0.017×0.025 SS and the largest amount of it was 23.7 ᵒ in the 0.017×0.025 TMA in 0.018×0.025 slot molar tube. But, this angle was 19.9 ᵒand 13.6 ᵒ in 0.019×0.025 SS and 0.019×0.025 TMA archwire in 0.022×0.028 molar tube. Conclusions The 0.017×0.025 SS archwire in 0.018×0.025 molar tube had the lowest clinically significant angle. The largest amount was seen in group 0.017×0.025 TMA in 0.018×0.025 slot molar tube. Key words: Torsional efficacy, rectangular wires, buccal tubes, torque angle. PMID:29670712

NOVEL CHAMBER DESIGN FOR AN IN-VACUUM CRYO-COOLED MINI-GAP UNDULATOR.

DOE Office of Scientific and Technical Information (OSTI.GOV)

HU, J.-P.; FOERSTER, C.L.; SKARITKA, J.R.

2006-05-24

A stainless steel, Ultra-High Vacuum (UHV) chamber, featuring a large vertical rectangular port (53''W by 16''H), has been fabricated to house the one-meter magnet assembly of a newly installed undulator insertion device for beamline X-25 at the National Synchrotron Light Source. To achieve UHV, the new chamber is equipped with a differential ion pump, NEG pump, nude ion gauge, residual gas analyzer, and an all metal roughing valve. Temperature of the magnet assembly is maintained below 90 C during vacuum bake. The large rectangular port cover is sealed to the main flange of the chamber using a one-piece flat aluminummore » gasket and special sealing surfaces developed exclusively by Nor-Cal Products, Inc. The large flange provides easy access to the gap of the installed magnet girders for in situ magnetic measurements and shimming. Special window ports were designed into the cover and chamber for manipulation of optical micrometers external to the chamber to provide precise measurements of the in-vacuum magnet gap. The vacuum chamber assembly features independently vacuum-isolated feedthroughs that can be used for either water-or-cryogenic refrigeration-cooling of the monolithic magnet girders. This would allow for cryogenic-cooled permanent magnet operation and has been successfully tested within temperature range of +100 C to -150 C. Details of the undulator assembly for beamline X-25 is described in the paper.« less

Industrial ion source technology

NASA Technical Reports Server (NTRS)

Kaufman, H. R.; Robinson, R. S.

1979-01-01

In reactive ion etching of Si, varying amounts of O2 were added to the CF4 background. The experimental results indicated an etch rate less than that for Ar up to an O2 partial pressure of about .00006 Torr. Above this O2 pressure, the etch rate with CF4 exceeded that with Ar alone. For comparison the random arrival rate of O2 was approximately equal to the ion arrival rate at a partial pressure of about .00002 Torr. There were also ion source and ion pressure gauge maintenance problems as a result of the use of CF4. Large scale (4 sq cm) texturing of Si was accomplished using both Cu and stainless steel seed. The most effective seeding method for this texturing was to surround the sample with large inclined planes. Designing, fabricating, and testing a 200 sq cm rectangular beam ion source was emphasized. The design current density was 6 mA/sq cm with 500 eV argon ions, although power supply limitations permitted operation to only 2 mA/sq cm. The use of multiple rectangular beam ion sources for continuous processing of wider areas than would be possible with a single source was also studied. In all cases investigated, the most uniform coverage was obtained with 0 to 2 cm beam overlay. The maximum departure from uniform processing at optimum beam overlap was found to be +15%.

Fabrication of stainless steel clad tubing. [gas pressure bonding

NASA Technical Reports Server (NTRS)

Kovach, C. W.

1978-01-01

The feasibility of producing stainless steel clad carbon steel tubing by a gas pressure bonding process was evaluated. Such a tube product could provide substantial chromium savings over monolithic stainless tubing in the event of a serious chromium shortage. The process consists of the initial assembly of three component tubesets from conventionally produced tubing, the formation of a strong metallurgical bond between the three components by gas pressure bonding, and conventional cold draw and anneal processing to final size. The quality of the tubes produced was excellent from the standpoint of bond strength, mechanical, and forming properties. The only significant quality problem encountered was carburization of the stainless clad by the carbon steel core which can be overcome by further refinement through at least three different approaches. The estimated cost of clad tubing produced by this process is greater than that for monolithic stainless tubing, but not so high as to make the process impractical as a chromium conservation method.

Influence of Size on the Microstructure and Mechanical Properties of an AISI 304L Stainless Steel—A Comparison between Bulk and Fibers

PubMed Central

Baldenebro-Lopez, Francisco J.; Gomez-Esparza, Cynthia D.; Corral-Higuera, Ramon; Arredondo-Rea, Susana P.; Pellegrini-Cervantes, Manuel J.; Ledezma-Sillas, Jose E.; Martinez-Sanchez, Roberto; Herrera-Ramirez, Jose M.

2015-01-01

In this work, the mechanical properties and microstructural features of an AISI 304L stainless steel in two presentations, bulk and fibers, were systematically studied in order to establish the relationship among microstructure, mechanical properties, manufacturing process and effect on sample size. The microstructure was analyzed by XRD, SEM and TEM techniques. The strength, Young’s modulus and elongation of the samples were determined by tensile tests, while the hardness was measured by Vickers microhardness and nanoindentation tests. The materials have been observed to possess different mechanical and microstructural properties, which are compared and discussed. PMID:28787949

Rectification of depth measurement using pulsed thermography with logarithmic peak second derivative method

NASA Astrophysics Data System (ADS)

Li, Xiaoli; Zeng, Zhi; Shen, Jingling; Zhang, Cunlin; Zhao, Yuejin

2018-03-01

Logarithmic peak second derivative (LPSD) method is the most popular method for depth prediction in pulsed thermography. It is widely accepted that this method is independent of defect size. The theoretical model for LPSD method is based on the one-dimensional solution of heat conduction without considering the effect of defect size. When a decay term considering defect aspect ratio is introduced into the solution to correct the three-dimensional thermal diffusion effect, we found that LPSD method is affected by defect size by analytical model. Furthermore, we constructed the relation between the characteristic time of LPSD method and defect aspect ratio, which was verified with the experimental results of stainless steel and glass fiber reinforced plate (GFRP) samples. We also proposed an improved LPSD method for depth prediction when the effect of defect size was considered, and the rectification results of stainless steel and GFRP samples were presented and discussed.

Performance of engine-driven rotary endodontic instruments with a superimposed bending deflection: V. Gates Glidden and Peeso drills.

PubMed

Brantley, W A; Luebke, N H; Luebke, F L; Mitchell, J C

1994-05-01

A laboratory study was performed on Gates Glidden and Peeso drills to determine the incidence of shaft fracture when a bending deflection was superimposed on the rotating drills. Samples of sizes #1 to #6 stainless steel Gates Glidden drills, sizes #1 to #6 stainless steel and carbon steel-type P Peeso drills, and sizes #009 to #023 carbon steel-type B-1 Peeso drills from each of two manufacturers were evaluated with a unique apparatus that applied a 2-mm bending deflection while rotating the instruments. The apparatus did not restrict movement of the bur head during rotation. The test drills were rotated at 2500, 4000, and 7000 revolutions per minute, and the number of revolutions at failure was recorded. Scanning electron microscopic observations established that the stainless steel Gates Glidden and Peeso drills failed by ductile fracture, whereas the carbon steel Peeso drills failed by brittle fracture. Instrument fracture was always near the handpiece shank with this test, and the length of the fractured drills was measured from the working tip. It is recommended that this additional test be adopted to determine fatigue properties of engine-driven rotary endodontic instruments in establishing international performance standards.

Precipitation-Induced Changes in Microstrain and Its Relation with Hardness and Tempering Parameter in 17-4 PH Stainless Steel

NASA Astrophysics Data System (ADS)

Mahadevan, S.; Manojkumar, R.; Jayakumar, T.; Das, C. R.; Rao, B. P. C.

2016-06-01

17-4 PH (precipitation hardening) stainless steel is a soft martensitic stainless steel strengthened by aging at appropriate temperature for sufficient duration. Precipitation of copper particles in the martensitic matrix during aging causes coherency strains which improves the mechanical properties, namely hardness and strength of the matrix. The contributions to X-ray diffraction (XRD) profile broadening due to coherency strains caused by precipitation and crystallite size changes due to aging are separated and quantified using the modified Williamson-Hall approach. The estimated normalized mean square strain and crystallite size are used to explain the observed changes in hardness. Microstructural changes observed in secondary electron images are in qualitative agreement with crystallite size changes estimated from XRD profile analysis. The precipitation kinetics in the age-hardening regime and overaged regime are studied from hardness changes and they follow the Avrami kinetics and Wilson's model, respectively. In overaged condition, the hardness changes are linearly correlated to the tempering parameter (also known as Larson-Miller parameter). Similar linear variation is observed between the normalized mean square strain (determined from XRD line profile analysis) and the tempering parameter, in the incoherent regime which is beyond peak microstrain conditions.

Ultrasonic liquid-level detector for varying temperature and pressure environments

DOEpatents

Anderson, R.L.; Miller, G.N.

1981-10-26

An ultrasonic liquid level detector for use in varying temperature and pressure environments, such as a pressurized water nuclear reactor vessel, is provided. The detector employs ultrasonic extensional and torsional waves launched in a multiplexed alternating sequence into a common sensor. The sensor is a rectangular cross section stainless steel rod which extends into the liquid medium whose level is to be detected. The sensor temperature derived from the extensional wave velocity measurements is used to compensate for the temperature dependence of the torsional wave velocity measurements which are also level dependent. The torsional wave velocity measurements of a multiple reflection sensor then provide a measurement of liquid level over a range of several meters with a small uncertainty over a temperature range of 20 to 250/sup 0/C and pressures up to 15 MPa.

Numerical simulation for the magnetic force distribution in electromagnetic forming of small size flat sheet

NASA Astrophysics Data System (ADS)

Chen, Xiaowei; Wang, Wenping; Wan, Min

2013-12-01

It is essential to calculate magnetic force in the process of studying electromagnetic flat sheet forming. Calculating magnetic force is the basis of analyzing the sheet deformation and optimizing technical parameters. Magnetic force distribution on the sheet can be obtained by numerical simulation of electromagnetic field. In contrast to other computing methods, the method of numerical simulation has some significant advantages, such as higher calculation accuracy, easier using and other advantages. In this paper, in order to study of magnetic force distribution on the small size flat sheet in electromagnetic forming when flat round spiral coil, flat rectangular spiral coil and uniform pressure coil are adopted, the 3D finite element models are established by software ANSYS/EMAG. The magnetic force distribution on the sheet are analyzed when the plane geometries of sheet are equal or less than the coil geometries under fixed discharge impulse. The results showed that when the physical dimensions of sheet are less than the corresponding dimensions of the coil, the variation of induced current channel width on the sheet will cause induced current crowding effect that seriously influence the magnetic force distribution, and the degree of inhomogeneity of magnetic force distribution is increase nearly linearly with the variation of induced current channel width; the small size uniform pressure coil will produce approximately uniform magnetic force distribution on the sheet, but the coil is easy to early failure; the desirable magnetic force distribution can be achieved when the unilateral placed flat rectangular spiral coil is adopted, and this program can be take as preferred one, because the longevity of flat rectangular spiral coil is longer than the working life of small size uniform pressure coil.

Effect of electromagnetic interaction during fusion welding of AISI 2205 duplex stainless steel on the corrosion resistance

NASA Astrophysics Data System (ADS)

García-Rentería, M. A.; López-Morelos, V. H.; González-Sánchez, J.; García-Hernández, R.; Dzib-Pérez, L.; Curiel-López, F. F.

2017-02-01

The effect of electromagnetic interaction of low intensity (EMILI) applied during fusion welding of AISI 2205 duplex stainless steel on the resistance to localised corrosion in natural seawater was investigated. The heat affected zone (HAZ) of samples welded under EMILI showed a higher temperature for pitting initiation and lower dissolution under anodic polarisation in chloride containing solutions than samples welded without EMILI. The EMILI assisted welding process developed in the present work enhanced the resistance to localised corrosion due to a modification on the microstructural evolution in the HAZ and the fusion zone during the thermal cycle involved in fusion welding. The application of EMILI reduced the size of the HAZ, limited coarsening of the ferrite grains and promoted regeneration of austenite in this zone, inducing a homogeneous passive condition of the surface. EMILI can be applied during fusion welding of structural or functional components of diverse size manufactured with duplex stainless steel designed to withstand aggressive environments such as natural seawater or marine atmospheres.

Cultural differences in room size perception

PubMed Central

Bülthoff, Heinrich H.; de la Rosa, Stephan; Dodds, Trevor J.

2017-01-01

Cultural differences in spatial perception have been little investigated, which gives rise to the impression that spatial cognitive processes might be universal. Contrary to this idea, we demonstrate cultural differences in spatial volume perception of computer generated rooms between Germans and South Koreans. We used a psychophysical task in which participants had to judge whether a rectangular room was larger or smaller than a square room of reference. We systematically varied the room rectangularity (depth to width aspect ratio) and the viewpoint (middle of the short wall vs. long wall) from which the room was viewed. South Koreans were significantly less biased by room rectangularity and viewpoint than their German counterparts. These results are in line with previous notions of general cognitive processing strategies being more context dependent in East Asian societies than Western ones. We point to the necessity of considering culturally-specific cognitive processing strategies in visual spatial cognition research. PMID:28426729

Two new species of Parasaveljevia Wieser, 1953 (Thoracostomopsidae, Nematoda) from Argentinean coasts (Chubut, Argentina).

PubMed

Pastor, Catalina; Lo Russo, Virginia; Villares, Gabriela

2015-10-06

Two new Parasavaljevia species are described, one from Puerto Madryn, and one from El Límite beach, San Jorge Gulf, Chubut Province, Argentina. The two species are characterised by a combination of characters. Parasavaljevia uncinoa n. sp. is characterised by having a long rectangular cirrus, positioned at the level of the inner labial setae, rectangular mandibles with prominent lateral hooks bearing denticles in three lines of nine each, and six cephalic setae of the same length, inserted at the anterior end of a small head capsule. Parasavaljevia limitense n. sp. is characterized by having a cirrus posterior positioned, between the labial and cephalic setae, rectangular-arched mandibles bearing denticles in five lines of ten each in a gradient of sizes; a small buccal cavity, small cephalic capsule and abundant cervical setae (4+10). An emendation of the genus diagnosis and a new key are given and discussed.

Resonant frequency function of thickness-shear vibrations of rectangular crystal plates.

PubMed

Wang, Ji; Yang, Lijun; Pan, Qiaoqiao; Chao, Min-Chiang; Du, Jianke

2011-05-01

The resonant frequencies of thickness-shear vibrations of quartz crystal plates in rectangular and circular shapes are always required in the design and manufacturing of quartz crystal resonators. As the size of quartz crystal resonators shrinks, for rectangular plates we must consider effects of both length and width for the precise calculation of resonant frequency. Starting from the three-dimensional equations of wave propagation in finite crystal plates and the general expression of vibration modes, we obtained the relations between frequency and wavenumbers. By satisfying the major boundary conditions of the dominant thickness-shear mode, three wavenumber solutions are obtained and the frequency equation is constructed. It is shown the resonant frequency of thickness-shear mode is a second-order polynomial of aspect ratios. This conforms to known results in the simplest form and is applicable to further analytical and experimental studies of the frequency equation of quartz crystal resonators.

Metal release from stainless steel particles in vitro-influence of particle size.

PubMed

Midander, K; Pan, J; Wallinder, I Odnevall; Leygraf, C

2007-01-01

Human inhalation of airborne metallic particles is important for health risk assessment. To study interactions between metallic particles and the human body, metal release measurements of stainless steel powder particles were performed in two synthetic biological media simulating lung-like environments. Particle size and media strongly influence the metal release process. The release rate of Fe is enhanced compared with Cr and Ni. In artificial lysosomal fluid (ALF, pH 4.5), the accumulated amounts of released metal per particle loading increase drastically with decreasing particle size. The release rate of Fe per unit surface area increases with decreasing particle size. Compared with massive sheet metal, fine powder particles (<4 microm) show similar release rates of Cr and Ni, but a higher release rate of Fe. Release rates in Gamble's solution (pH 7.4), for all powders investigated, are significantly lower compared to ALF. No clear trend is seen related to particle size in Gamble's solution.

Effects of Ce on Inclusions, Microstructure, Mechanical Properties, and Corrosion Behavior of AISI 202 Stainless Steel

NASA Astrophysics Data System (ADS)

Cai, Guojun; Li, Changsheng

2015-10-01

The sizes and morphologies of nonmetallic inclusions, microhardness, tensile strength, and Charpy impact toughness in AISI 202 stainless steel with different Ce contents were synthetically analyzed by means of SEM, TEM, microhardness tester, and tensile and Charpy impact tests. Effects of Ce addition on the corrosion behavior were investigated in 5 wt.% H2SO4 solution for different periods of time through measuring AC impedance. The EIS measurements indicate that the steels with Ce addition exhibit higher R p values than those without Ce, which illustrates the relative resistance to uniform corrosion is accompanied by an increasing Ce addition. Ce addition to AISI 202 stainless steel improves its uniform corrosion resistance owing to metamorphic inclusions and the improvement of electrode potential in matrix. Upon increasing Ce addition, the indentation morphology of samples transfers from sink-in types to pile-up types, explaining good machinability of steels containing Ce. It is witnessed from the fracture mode that Ce refines the grain size of steels, significantly increasing the strength; in the meantime, its plasticity is improved, thereby solving the contradiction between the strength and the plasticity of steels. It is concluded that AISI 202 stainless steel with 0.016 wt.% Ce addition in the mass fraction has the best mechanical properties and the uniform corrosion resistance.

Effects of Grain Size on Ultrasonic Attenuation in Type 316L Stainless Steel

PubMed Central

Wan, Tao; Wakui, Takashi; Futakawa, Masatoshi; Obayashi, Hironari

2017-01-01

A lead bismuth eutectic (LBE) spallation target will be installed in the Target Test Facility (TEF-T) in the Japan Proton Accelerator Research Complex (J-PARC). The spallation target vessel filled with LBE is made of type 316L stainless steel. However, various damages, such as erosion/corrosion damage and liquid metal embrittlement caused by contact with flowing LBE at high temperature, and irradiation hardening caused by protons and neutrons, may be inflicted on the target vessel, which will deteriorate the steel and might break the vessel. To monitor the target vessel for prevention of an accident, an ultrasonic technique has been proposed to establish off-line evaluation for estimating vessel material status during the target maintenance period. Basic R&D must be carried out to clarify the dependency of ultrasonic wave propagation behavior on material microstructures and obtain fundamental knowledge. As a first step, ultrasonic waves scattered by the grains of type 316L stainless steel are investigated using new experimental and numerical approaches in the present study. The results show that the grain size can be evaluated exactly and quantitatively by calculating the attenuation coefficient of the ultrasonic waves scattered by the grains. The results also show that the scattering regimes of ultrasonic waves depend heavily on the ratio of wavelength to average grain size, and are dominated by grains of extraordinarily large size along the wave propagation path. PMID:28773115

Processing of fine grained AISI 304L austenitic stainless steel by cold rolling and high-temperature short-term annealing

NASA Astrophysics Data System (ADS)

Naghizadeh, Meysam; Mirzadeh, Hamed

2018-05-01

An advanced thermomechanical process based on the formation and reversion of deformation-induced martensite was used to refine the grain size and enhance the hardness of an AISI 304L austenitic stainless steel. Both low and high reversion annealing temperatures and also the repetition of the whole thermomechanical cycle were considered. While a microstructure with average austenite grain size of a few micrometers was achieved based on cold rolling and high-temperature short-term annealing, an extreme grain refinement up to submicrometer regime was obtained by cold rolling followed by low-temperature long-term annealing. However, the required annealing time was found to be much longer, which negates its appropriateness for industrial production. While a magnificent grain refinement was achieved by one pass of the high-temperature thermomechanical process, the reduction in grain size was negligible by the repetition of the whole cycle. It was found that the hardness of the thermomechanically processed material is much higher than that of the as-received material. The results of the present work were shown to be compatible with the general trend of grain size dependence of hardness for AISI 304L stainless steel based on the Hall-Petch relationship. The results were also discussed based on the X-ray evaluation of dislocation density by modified Williamson-Hall plots.

Ensemble Empirical Mode Decomposition based methodology for ultrasonic testing of coarse grain austenitic stainless steels.

PubMed

Sharma, Govind K; Kumar, Anish; Jayakumar, T; Purnachandra Rao, B; Mariyappa, N

2015-03-01

A signal processing methodology is proposed in this paper for effective reconstruction of ultrasonic signals in coarse grained high scattering austenitic stainless steel. The proposed methodology is comprised of the Ensemble Empirical Mode Decomposition (EEMD) processing of ultrasonic signals and application of signal minimisation algorithm on selected Intrinsic Mode Functions (IMFs) obtained by EEMD. The methodology is applied to ultrasonic signals obtained from austenitic stainless steel specimens of different grain size, with and without defects. The influence of probe frequency and data length of a signal on EEMD decomposition is also investigated. For a particular sampling rate and probe frequency, the same range of IMFs can be used to reconstruct the ultrasonic signal, irrespective of the grain size in the range of 30-210 μm investigated in this study. This methodology is successfully employed for detection of defects in a 50mm thick coarse grain austenitic stainless steel specimens. Signal to noise ratio improvement of better than 15 dB is observed for the ultrasonic signal obtained from a 25 mm deep flat bottom hole in 200 μm grain size specimen. For ultrasonic signals obtained from defects at different depths, a minimum of 7 dB extra enhancement in SNR is achieved as compared to the sum of selected IMF approach. The application of minimisation algorithm with EEMD processed signal in the proposed methodology proves to be effective for adaptive signal reconstruction with improved signal to noise ratio. This methodology was further employed for successful imaging of defects in a B-scan. Copyright © 2014. Published by Elsevier B.V.

Acoustic Measurements of Rectangular Nozzles with Bevel

NASA Technical Reports Server (NTRS)

Bridges, James E.

2012-01-01

A series of convergent rectangular nozzles of aspect ratios 2:1, 4:1, and 8:1 were constructed with uniform exit velocity profiles. Additional nozzles were constructed that extended the wide lip on one side of these nozzles to form beveled nozzles. Far-field acoustic measurements were made and analyzed, and the results presented. The impact of aspect ratio on jet noise was similar to that of enhanced mixing devices: reduction in aft, peak frequency noise with an increase in broadside, high frequency noise. Azimuthally, it was found that rectangular jets produced more noise directed away from their wide sides than from their narrow sides. The azimuthal dependence decreased at aft angles where noise decreased. The effect of temperature, keeping acoustic Mach number constant, was minimal. Since most installations would have the observer on the wide size of the nozzle, the increased high frequency noise has a deleterious impact on the observer. Extending one wide side of the rectangular nozzle, evocative of an aft deck in an installed propulsion system, increased the noise of the jet with increasing length. The impact of both aspect ratio and bevel length were relatively well behaved, allowing a simple bilinear model to be constructed relative to a simple round jet.

Axion searches with microwave filters: the RADES project

NASA Astrophysics Data System (ADS)

Álvarez Melcón, Alejandro; Arguedas Cuendis, Sergio; Cogollos, Cristian; Díaz-Morcillo, Alejandro; Döbrich, Babette; Gallego, Juan Daniel; Gimeno, Benito; Irastorza, Igor G.; José Lozano-Guerrero, Antonio; Malbrunot, Chloé; Navarro, Pablo; Peña Garay, Carlos; Redondo, Javier; Vafeiadis, Theodoros; Wuensch, Walter

2018-05-01

We propose, design and construct a variant of the conventional axion haloscope concept that could be competitive in the search for dark matter axions of masses in the decade 10–100 μeV. Theses masses are located somewhat above the mass range in which existing experiments have reached sensitivity to benchmark QCD axion models. Our haloscope consists of an array of small microwave cavities connected by rectangular irises, in an arrangement commonly used in radio-frequency filters. The size of the unit cavity determines the main resonant frequency, while the possibility to connect a large number of cavities allows to reach large detection volumes. We develop the theoretical framework of the detection concept, and present design prescriptions to optimize detection capabilities. We describe the design and realization of a first small-scale prototype of this concept, called Relic Axion Detector Exploratory Setup (RADES). It consists of a copper-coated stainless steel five-cavities microwave filter with the detecting mode operating at around 8.4 GHz. This structure has been electromagnetically characterized at 2 K and 298 K, and it is now placed in ultra-high vacuum in one of the twin-bores of the 9 T CAST dipole magnet at CERN. We describe the data acquisition system developed for relic axion detection, and present preliminary results of the electromagnetic properties of the microwave filter, which show the potential of filters to reach QCD axion window sensitivity at X-band frequencies.

Optimization of Dimensional accuracy in plasma arc cutting process employing parametric modelling approach

NASA Astrophysics Data System (ADS)

Naik, Deepak kumar; Maity, K. P.

2018-03-01

Plasma arc cutting (PAC) is a high temperature thermal cutting process employed for the cutting of extensively high strength material which are difficult to cut through any other manufacturing process. This process involves high energized plasma arc to cut any conducting material with better dimensional accuracy in lesser time. This research work presents the effect of process parameter on to the dimensional accuracy of PAC process. The input process parameters were selected as arc voltage, standoff distance and cutting speed. A rectangular plate of 304L stainless steel of 10 mm thickness was taken for the experiment as a workpiece. Stainless steel is very extensively used material in manufacturing industries. Linear dimension were measured following Taguchi’s L16 orthogonal array design approach. Three levels were selected to conduct the experiment for each of the process parameter. In all experiments, clockwise cut direction was followed. The result obtained thorough measurement is further analyzed. Analysis of variance (ANOVA) and Analysis of means (ANOM) were performed to evaluate the effect of each process parameter. ANOVA analysis reveals the effect of input process parameter upon leaner dimension in X axis. The results of the work shows that the optimal setting of process parameter values for the leaner dimension on the X axis. The result of the investigations clearly show that the specific range of input process parameter achieved the improved machinability.

Low gamma counting for measuring NORM/TENORM with a radon reducing system

NASA Astrophysics Data System (ADS)

Paschoa, Anselmo S.

2001-06-01

A detection system for counting low levels of gamma radiation was built by upgrading an existing rectangular chamber made of 18 metric tonne of steel fabricated before World War II. The internal walls, the ceiling, and the floor of the chamber are covered with copper sheets. The new detection system consists of a stainless steel hollow cylinder with variable circular apertures in the cylindrical wall and in the base, to allow introduction of a NaI (Tl) crystal, or alternatively, a HPGe detector in its interior. This counting system is mounted inside the larger chamber, which in turn is located in a subsurface air-conditioned room. The access to the subsurface room is made from a larger entrance room through a tunnel plus a glass anteroom to decrease the air-exchange rate. Both sample and detector are housed inside the stainless steel cylinder. This cylinder is filled with hyper pure nitrogen gas, before counting a sample, to prevent radon coming into contact with the detector surface. As a consequence, the contribution of the 214Bi photopeaks to the background gamma spectra is minimized. The reduction of the gamma radiation background near the detector facilitates measurement of naturally occurring radioactive materials (NORM), and/or technologically enhanced NORM (TENORM), which are usually at concentration levels only slightly higher than those typically found in the natural radioactive background.

Investigation of holder pressure and size effects in micro deep drawing of rectangular work pieces driven by piezoelectric actuator.

PubMed

Aminzahed, Iman; Mashhadi, Mahmoud Mosavi; Sereshk, Mohammad Reza Vaziri

2017-02-01

Micro forming is a manufacturing process to fabricate micro parts with high quality and a cost effective manner. Deep drawing could be a favorable method for production of complicated parts in macro and micro sizes. In this paper piezoelectric actuator is used as a novel approach in the field of micro manufacturing. Also, in current work, investigations are conducted with four rectangular punches and blanks with various thicknesses. Blank holder pressure effects on thickness distributions, punch force, and springback are studied. According to the results of this work, increasing of blank holder pressure in scaled deep drawing, in contrast to thickness of drawn part, leads to decrease in the punch forces and springback. Furthermore, it is shown that in micro deep drawing, the effects of holder pressure on mentioned parameters can be ignored. Copyright © 2016 Elsevier B.V. All rights reserved.

Comparison of Geometric Design of a Brand of Stainless Steel K-Files: An In Vitro Study.

PubMed

Saeedullah, Maryam; Husain, Syed Wilayat

2018-04-01

The purpose of this experimental study was to determine the diametric variations of a brand of handheld stainless-steel K-files, acquired from different countries, in accordance with the available standards. 20 Mani stainless-steel K-files of identical size (ISO#25) were acquired from Pakistan and were designated as Group A while 20 Mani K-files were purchased from London, UK and designated as Group B. Files were assessed using profile projector Nikon B 24V. Data was statistically compared with ISO 3630:1 and ADA 101 by one sample T test. Significant difference was found between Groups A and B. Average discrepancy of Group A fell within the tolerance limit while that of Group B exceeded the limit. Findings in this study call attention towards adherence to the dimensional standards of stainless-steel endodontic files.

A user guide for the sign sizing program

Treesearch

Donna Sheehy; Kurt Krueger

1999-01-01

This user guide explains how to use the Forest Service Sign Sizing program. The program calculates the length and height of a rectangular sign panel for road and trail guide signs. Variable text messages and directional arrows can be mocked up using U.S. Federal Highway Administration standards. Users can make text or other changes and quickly determine the effect on...

Effect of plasma arc welding variables on fusion zone grain size and hardness of AISI 321 austenitic stainless steel

NASA Astrophysics Data System (ADS)

Kondapalli, S. P.

2017-12-01

In the present work, pulsed current microplasma arc welding is carried out on AISI 321 austenitic stainless steel of 0.3 mm thickness. Peak current, Base current, Pulse rate and Pulse width are chosen as the input variables, whereas grain size and hardness are considered as output responses. Response surface method is adopted by using Box-Behnken Design, and in total 27 experiments are performed. Empirical relation between input and output response is developed using statistical software and analysis of variance (ANOVA) at 95% confidence level to check the adequacy. The main effect and interaction effect of input variables on output response are also studied.

Improving hydro-formability of stainless steel tubes by tube channel pressing

NASA Astrophysics Data System (ADS)

Kitano, Y.; Yuasa, M.; Miyamoto, H.; Farshidi, M. H.; Bagherpour, E.

2017-05-01

Tube channel pressing (TCP), which is one of the severe plastic deformation (SPD) technologies to refine grain size into submicron size for tubular materials, have been applied to ferritic stainless steel tubes for one pass, in order to alleviate ridging and enhance the hydro-formability. It was found that grain-scale shear bands were introduced by one-pass TCP, and texture and microstructure was successfully modified by promoting recrystallization of deformation microstructure, which is otherwise hard-to-recrystallize, in the post-TCP annealing. Elongation to failure, strain-hardening exponent (n-value) and Lankford values of both longitudinal and circumferential directions increased in comparison to with the tube fabricated by conventional process.

Excitation of a Parallel Plate Waveguide by an Array of Rectangular Waveguides

NASA Technical Reports Server (NTRS)

Rengarajan, Sembiam

2011-01-01

This work addresses the problem of excitation of a parallel plate waveguide by an array of rectangular waveguides that arises in applications such as the continuous transverse stub (CTS) antenna and dual-polarized parabolic cylindrical reflector antennas excited by a scanning line source. In order to design the junction region between the parallel plate waveguide and the linear array of rectangular waveguides, waveguide sizes have to be chosen so that the input match is adequate for the range of scan angles for both polarizations. Electromagnetic wave scattered by the junction of a parallel plate waveguide by an array of rectangular waveguides is analyzed by formulating coupled integral equations for the aperture electric field at the junction. The integral equations are solved by the method of moments. In order to make the computational process efficient and accurate, the method of weighted averaging was used to evaluate rapidly oscillating integrals encountered in the moment matrix. In addition, the real axis spectral integral is evaluated in a deformed contour for speed and accuracy. The MoM results for a large finite array have been validated by comparing its reflection coefficients with corresponding results for an infinite array generated by the commercial finite element code, HFSS. Once the aperture electric field is determined by MoM, the input reflection coefficients at each waveguide port, and coupling for each polarization over the range of useful scan angles, are easily obtained. Results for the input impedance and coupling characteristics for both the vertical and horizontal polarizations are presented over a range of scan angles. It is shown that the scan range is limited to about 35 for both polarizations and therefore the optimum waveguide is a square of size equal to about 0.62 free space wavelength.

Investigation of imaging properties for submillimeter rectangular pinholes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Xia, Dan, E-mail: dxia@uchicago.edu; Moore, Stephen C., E-mail: scmoore@bwh.harvard.edu, E-mail: miaepark@bwh.harvard.edu, E-mail: mcervo@bwh.harvard.edu; Park, Mi-Ae, E-mail: scmoore@bwh.harvard.edu, E-mail: miaepark@bwh.harvard.edu, E-mail: mcervo@bwh.harvard.edu

Purpose: Recently, a multipinhole collimator with inserts that have both rectangular apertures and rectangular fields of view (FOVs) has been proposed for SPECT imaging since it can tile the projection onto the detector efficiently and the FOVs in transverse and axial directions become separable. The purpose of this study is to investigate the image properties of rectangular-aperture pinholes with submillimeter apertures sizes. Methods: In this work, the authors have conducted sensitivity and FOV experiments for 18 replicates of a prototype insert fabricated in platinum/iridium (Pt/Ir) alloy with submillimeter square-apertures. A sin{sup q}θ fit to the experimental sensitivity has been performedmore » for these inserts. For the FOV measurement, the authors have proposed a new formula to calculate the projection intensity of a flood image on the detector, taking into account the penumbra effect. By fitting this formula to the measured projection data, the authors obtained the acceptance angles. Results: The mean (standard deviation) of fitted sensitivity exponents q and effective edge lengths w{sub e} were, respectively, 10.8 (1.8) and 0.38 mm (0.02 mm), which were close to the values, 7.84 and 0.396 mm, obtained from Monte Carlo calculations using the parameters of the designed inserts. For the FOV measurement, the mean (standard deviation) of the transverse and axial acceptances were 35.0° (1.2°) and 30.5° (1.6°), which are in good agreement with the designed values (34.3° and 29.9°). Conclusions: These results showed that the physical properties of the fabricated inserts with submillimeter aperture size matched our design well.« less

Comparison of wing-span averaging effects on lift, rolling moment, and bending moment for two span load distributions and for two turbulence representations

NASA Technical Reports Server (NTRS)

Lichtenstein, J. H.

1978-01-01

An analytical method of computing the averaging effect of wing-span size on the loading of a wing induced by random turbulence was adapted for use on a digital electronic computer. The turbulence input was assumed to have a Dryden power spectral density. The computations were made for lift, rolling moment, and bending moment for two span load distributions, rectangular and elliptic. Data are presented to show the wing-span averaging effect for wing-span ratios encompassing current airplane sizes. The rectangular wing-span loading showed a slightly greater averaging effect than did the elliptic loading. In the frequency range most bothersome to airplane passengers, the wing-span averaging effect can reduce the normal lift load, and thus the acceleration, by about 7 percent for a typical medium-sized transport. Some calculations were made to evaluate the effect of using a Von Karman turbulence representation. These results showed that using the Von Karman representation generally resulted in a span averaging effect about 3 percent larger.

A Comparison between heat transfer performance of rectangular and semicircular tubes considering boundary effects on Brownian motions in the presence of Ag / water nanofluids: Applicable in the design of cooling system of photovoltaic cells

PubMed Central

Aberoumand, Sadegh

2017-01-01

The present study aims to experimentally investigate heat transfer performance of rectangular and semicircular tubes in the presence of Ag / water nanofluids. The nanoparticles of Ag (silver) were used in seven different volume concentrations of 0.03%, 0.07%, 0.1%, 0.2%, 0.4%, 1% and 2%. The experiment was conducted in relatively low Reynolds numbers of 301 to 740. A heater with the power of 200 W was used to keep the outer surface of the tubes under a constant heat flux condition. In addition, the rectangular tube has been designed within the same length as the semicircular one and also within the same hydraulic diameter. Moreover, the average nanoparticles size was 20 nm. The outcome results of the present empirical work indicate that, for all the examined Reynolds numbers, the semicircular tube has higher convective heat transfer coefficient for all the utilized volume concentrations of Ag nanoparticles. The possible reasons behind this advantage are discussed through the present work mainly by taking the boundary effect on Brownian motions into account. Coming to this point that the conventional design for cooling system of photovoltaic cells is a heat sink with the rectangular graves, it is discussed that using a semicircular design may have the advantage over the rectangular one in convective heat transfer coefficient enhancement and hence a better cooling performance for these solar cells. PMID:28753603

A Comparison between heat transfer performance of rectangular and semicircular tubes considering boundary effects on Brownian motions in the presence of Ag / water nanofluids: Applicable in the design of cooling system of photovoltaic cells.

PubMed

Jafarimoghaddam, Amin; Aberoumand, Sadegh

2017-01-01

The present study aims to experimentally investigate heat transfer performance of rectangular and semicircular tubes in the presence of Ag / water nanofluids. The nanoparticles of Ag (silver) were used in seven different volume concentrations of 0.03%, 0.07%, 0.1%, 0.2%, 0.4%, 1% and 2%. The experiment was conducted in relatively low Reynolds numbers of 301 to 740. A heater with the power of 200 W was used to keep the outer surface of the tubes under a constant heat flux condition. In addition, the rectangular tube has been designed within the same length as the semicircular one and also within the same hydraulic diameter. Moreover, the average nanoparticles size was 20 nm. The outcome results of the present empirical work indicate that, for all the examined Reynolds numbers, the semicircular tube has higher convective heat transfer coefficient for all the utilized volume concentrations of Ag nanoparticles. The possible reasons behind this advantage are discussed through the present work mainly by taking the boundary effect on Brownian motions into account. Coming to this point that the conventional design for cooling system of photovoltaic cells is a heat sink with the rectangular graves, it is discussed that using a semicircular design may have the advantage over the rectangular one in convective heat transfer coefficient enhancement and hence a better cooling performance for these solar cells.

Immobilization and release of copper species from a microstructured polypyrrole matrix.

PubMed

González, M B; Brugnoni, L I; Flamini, D O; Quinzani, L M; Saidman, S B

2017-01-01

Copper species immobilization in hollow rectangular-sectioned microtubes of polypyrrole (PPy) electrosynthesized on 316L stainless steel was carried out using two different methods. One of them involved the immobilization after the PPy electropolymerization and the other one during the electrosynthesis process. The electrodes modified with copper species were rotated at different speeds in well water under open-circuit potential conditions. The release of copper species from the PPy matrix and the antibacterial activity against Escherichia coli were analyzed. The obtained results demonstrate that the amount of copper species released as well as the bactericidal effects against E. coli increases with rotation speed. The PPy coating modified with copper species after the electropolymerization reaction exhibited the best performance in terms of antibacterial activity and corrosion protection. These electrodes were tested in a lab-scale continuous flow system for well water disinfection.

Analysis of the velocity distribution in different types of ventilation system ducts

NASA Astrophysics Data System (ADS)

Peszyński, Kazimierz; Olszewski, Lukasz; Smyk, Emil; Perczyński, Daniel

2018-06-01

The paper presents the results obtained during the preliminary studies of circular and rectangular ducts before testing the properties elements (elbows, tees, etc.)of rectangular with rounded corners ducts. The fundamental problem of the studies was to determine the flow rate in the ventilation duct. Due to the size of the channel it was decided to determine the flow rate based on the integration of flow velocity over the considered cross-section. This method requires knowledge of the velocity distribution in the cross section. Approximation of the measured actual profile by the classic and modified Prandtl power-law velocity profile was analysed.

Tensile Fracture Behavior of 316L Austenitic Stainless Steel Manufactured by Hot Isostatic Pressing

NASA Astrophysics Data System (ADS)

Cooper, A. J.; Brayshaw, W. J.; Sherry, A. H.

2018-02-01

Herein we investigate how the oxygen content in hot isostatically pressed (HIP'd) 316L stainless steel affects the mechanical properties and tensile fracture behavior. This work follows on from previous studies, which aimed to understand the effect of oxygen content on the Charpy impact toughness of HIP'd steel. We expand on the work by performing room-temperature tensile testing on different heats of 316L stainless steel, which contain different levels of interstitial elements (carbon and nitrogen) as well as oxygen in the bulk material. Throughout the work we repeat the experiments on conventionally forged 316L steel as a reference material. The analysis of the work indicates that oxygen does not contribute to a measureable solution strengthening mechanism, as is the case with carbon and nitrogen in austenitic stainless steels (Werner in Mater Sci Eng A 101:93-98, 1988). Neither does oxygen, in the form of oxide inclusions, contribute to precipitation hardening due to the size and spacing of particles. However, the oxide particles do influence fracture behavior; fractography of the failed tension test specimens indicates that the average ductile dimple size is related to the oxygen content in the bulk material, the results of which support an on-going hypothesis relating oxygen content in HIP'd steels to their fracture mechanisms by providing additional sites for the initiation of ductile damage in the form of voids.

[The long-term fracture resistance of orthodontic nickel-titanium wires].

PubMed

Drescher, D; Bourauel, C; Sonneborn, W; Schmuth, G P

1994-01-01

This study reports on the long-term fracture resistance of orthodontic nickel titanium wires, a material property that has not been investigated thoroughly, yet. A computer-controlled apparatus was designed to perform long-term bending tests. The investigated material comprised 9 nickel titanium wires (dimensions 0.016", round and 0.016" x 0.022", rectangular) as well as a stainless steel and a beta-titanium wire that were included as reference. Compared with the steel wire, the nickel titanium wires exhibited 2- to 5-fold higher yield forces in bending. At a specified deflection angle, the generated bending forces of the nickel titanium wires reached one half to one fourth of the values of steel. The fracture resistance under longterm loading was determined using the Wöhler-method. After 10(5) loadings, 0.016" nickel titanium wires were subject to break failure, if forces exceed values greater than 1.2 to 3.1 N. Steel and TMA wires could be loaded with forces of up to 4.4 and 3.7 N, respectively. The 0.016" x 0.022"-rectangular wires allowed forces of approximately twice this magnitude. Elastic fatigue of the superelastic specimens "Memorywire", "Rematitan Lite", and "Sentalloy medium" showed up as hardening of the wire by up to 70%. Material degradation lead to a severe deformation of the hysteresis loop and to plastic deformation. Work-hardened martensitic NiTi wires did not show these effects to this extent.

Morphologically controlled synthesis of ferric oxide nano/micro particles and their catalytic application in dry and wet media: a new approach.

PubMed

Janjua, Muhammad Ramzan Saeed Ashraf; Jamil, Saba; Jahan, Nazish; Khan, Shanza Rauf; Mirza, Saima

2017-05-31

Morphologically controlled synthesis of ferric oxide nano/micro particles has been carried out by using solvothermal route. Structural characterization displays that the predominant morphologies are porous hollow spheres, microspheres, micro rectangular platelets, octahedral and irregular shaped particles. It is also observed that solvent has significant effect on morphology such as shape and size of the particles. All the morphologies obtained by using different solvents are nearly uniform with narrow size distribution range. The values of full width at half maxima (FWHM) of all the products were calculated to compare their size distribution. The FWHM value varies with size of the particles for example small size particles show polydispersity whereas large size particles have shown monodispersity. The size of particles increases with decrease in polarity of the solvent whereas their shape changes from spherical to rectangular/irregular with decrease in polarity of the solvent. The catalytic activities of all the products were investigated for both dry and wet processes such as thermal decomposition of ammonium per chlorate (AP) and reduction of 4-nitrophenol in aqueous media. The results indicate that each product has a tendency to act as a catalyst. The porous hollow spheres decrease the thermal decomposition temperature of AP by 140 °C and octahedral Fe 3 O 4 particles decrease the decomposition temperature by 30 °C. The value of apparent rate constant (k app ) of reduction of 4-NP has also been calculated.

UNS S31603 Stainless Steel Tungsten Inert Gas Welds Made with Microparticle and Nanoparticle Oxides

PubMed Central

Tseng, Kuang-Hung; Lin, Po-Yu

2014-01-01

The purpose of this study was to investigate the difference between tungsten inert gas (TIG) welding of austenitic stainless steel assisted by microparticle oxides and that assisted by nanoparticle oxides. SiO2 and Al2O3 were used to investigate the effects of the thermal stability and the particle size of the activated compounds on the surface appearance, geometric shape, angular distortion, delta ferrite content and Vickers hardness of the UNS S31603 stainless steel TIG weld. The results show that the use of SiO2 leads to a satisfactory surface appearance compared to that of the TIG weld made with Al2O3. The surface appearance of the TIG weld made with nanoparticle oxide has less flux slag compared with the one made with microparticle oxide of the same type. Compared with microparticle SiO2, the TIG welding with nanoparticle SiO2 has the potential benefits of high joint penetration and less angular distortion in the resulting weldment. The TIG welding with nanoparticle Al2O3 does not result in a significant increase in the penetration or reduction of distortion. The TIG welding with microparticle or nanoparticle SiO2 uses a heat source with higher power density, resulting in a higher ferrite content and hardness of the stainless steel weld metal. In contrast, microparticle or nanoparticle Al2O3 results in no significant difference in metallurgical properties compared to that of the C-TIG weld metal. Compared with oxide particle size, the thermal stability of the oxide plays a significant role in enhancing the joint penetration capability of the weld, for the UNS S31603 stainless steel TIG welds made with activated oxides. PMID:28788704

UNS S31603 Stainless Steel Tungsten Inert Gas Welds Made with Microparticle and Nanoparticle Oxides.

PubMed

Tseng, Kuang-Hung; Lin, Po-Yu

2014-06-20

The purpose of this study was to investigate the difference between tungsten inert gas (TIG) welding of austenitic stainless steel assisted by microparticle oxides and that assisted by nanoparticle oxides. SiO₂ and Al₂O₃ were used to investigate the effects of the thermal stability and the particle size of the activated compounds on the surface appearance, geometric shape, angular distortion, delta ferrite content and Vickers hardness of the UNS S31603 stainless steel TIG weld. The results show that the use of SiO₂ leads to a satisfactory surface appearance compared to that of the TIG weld made with Al₂O₃. The surface appearance of the TIG weld made with nanoparticle oxide has less flux slag compared with the one made with microparticle oxide of the same type. Compared with microparticle SiO₂, the TIG welding with nanoparticle SiO₂ has the potential benefits of high joint penetration and less angular distortion in the resulting weldment. The TIG welding with nanoparticle Al₂O₃ does not result in a significant increase in the penetration or reduction of distortion. The TIG welding with microparticle or nanoparticle SiO₂ uses a heat source with higher power density, resulting in a higher ferrite content and hardness of the stainless steel weld metal. In contrast, microparticle or nanoparticle Al₂O₃ results in no significant difference in metallurgical properties compared to that of the C-TIG weld metal. Compared with oxide particle size, the thermal stability of the oxide plays a significant role in enhancing the joint penetration capability of the weld, for the UNS S31603 stainless steel TIG welds made with activated oxides.

High Temperature Degradation of 5250-4 Polymer Resin

DTIC Science & Technology

2007-06-01

fragments. The pieces were then repeatedly crushed between two stainless steel plates with a Wabash 30 Ton Press. After this process, the pieces...the BMI powder. Two stainless steel ASTM test sieves, with mesh sizes of 45 and 90 µm, were used to collect only the powder in the 45 to 90 µm range...The o,o’-diallylbisphenol A ( BPA ) monomer in Figure 1 is not a bismaleimide, but it is often used in BMI polymers to make otherwise brittle BMIs

Multipurpose Sediment Passive Sampler with Improved Tissue Mimicry to Measure the Bioavailable Fraction

DTIC Science & Technology

2016-11-01

sieved to a 35-60 mesh particle size (250-500 μm) for testing. Sampler construction. Media (500 mg) was placed in 150 mesh stainless steel which...ASP400P), and 5% kaolin clay (ASP900) by weight into a cement mixer. The sediment was mixed for 1.5 hr to 10 ensure homogeneity. This resulted in...fabricated using stainless steel mesh and 500 mg of the identified media blend. A manufacturing space and process was established for Osorb enhanced

Dilatometry Analysis of Dissolution of Cr-Rich Carbides in Martensitic Stainless Steels

NASA Astrophysics Data System (ADS)

Huang, Qiuliang; Volkova, Olena; Biermann, Horst; Mola, Javad

2017-12-01

The dissolution of Cr-rich carbides formed in the martensitic constituent of a 13 pct Cr stainless steel was studied by dilatometry and correlative electron channeling contrast examinations. The dissolution of carbides subsequent to the martensite reversion to austenite was associated with a net volume expansion which in turn increased the dilatometry-based apparent coefficient of thermal expansion (CTEa) during continuous heating. The effects of carbides fraction and size on the CTEa variations during carbides dissolution are discussed.

Immobilization of mesoporous silica particles on stainless steel plates

NASA Astrophysics Data System (ADS)

Pasqua, Luigi; Morra, Marco

2017-03-01

A preliminary study aimed to the nano-engineering of stainless steel surface is presented. Aminopropyl-functionalized mesoporous silica is covalently and electrostatically anchored on the surface of stainless steel plates. The anchoring is carried out through the use of a nanometric spacer, and two different spacers are proposed (both below 2 nm in size). The first sample is obtained by anchoring to the stainless steel amino functionalized, a glutaryl dichloride spacer. This specie forms an amide linkage with the amino group while the unreacted acyl groups undergo hydrolysis giving a free carboxylic group. The so-obtained functionalized stainless steel plate is used as substrate for anchoring derivatized mesoporous silica particles. The second sample is prepared using 2-bromo-methyl propionic acid as spacer (BMPA). Successively, the carboxylic group of propionic acid is condensed to the aminopropyl derivatization on the external surface of the mesoporous silica particle through covalent bond. In both cases, a continuous deposition (coating thickness is around 10 μm) is obtained, in fact, XPS data do not reveal the metal elements constituting the plate. The nano-engineering of metal surfaces can represent an intriguing opportunity for producing long-term drug release or biomimetic surface.

Laser-assisted electrochemical micromachining of mould cavity on the stainless steel surface

NASA Astrophysics Data System (ADS)

Li, Xiaohai; Wang, Shuming; Wang, Dong; Tong, Han

2018-02-01

In order to fabricate the micro mould cavities with complex structures on 304 stainless steel, laser-assisted electrochemical micromachining (EMM) based on surface modification by fiber laser masking was studied,and a new device of laser-assisted EMM was developed. Laser marking on the surface of 304 stainless steel can first be realized by fiber laser heating scanning. Through analysis of X ray diffraction analysis (XRD), metal oxide layer with predefined pattern can be formed by laser marking, and phase transformation can also occur on the 304 stainless steel surface, which produce the laser masking layer with corrosion resistance. The stainless steel surface with laser masking layer is subsequently etched by EMM, the laser masking layer severs as the temporary protective layer without relying on lithography mask, the fabrication of formed electrodes is also avoided, so micro pattern cavities can fast be fabricated. The impacts on machining accuracy during EMM with laser masking were discussed to optimize machining parameters, such as machining voltage, electrolyte concentration, duty cycle of pulse power supply and electrode gap size, the typical mould cavities 23μm deep were fabricated under the optimized parameters.

Root canal shaping with manual stainless steel files and rotary Ni-Ti files performed by students.

PubMed

Sonntag, D; Guntermann, A; Kim, S K; Stachniss, V

2003-04-01

To investigate root canal shaping with manual stainless steel files and rotary Ni-Ti files by students. Two hundred and ten simulated root canals with the same geometrical shape and size in acrylic resin blocks were prepared by 21 undergraduate dental students with manual stainless steel files using a stepback technique or with rotary Ni-Ti files in crown-down technique. Preparation length, canal shape, incidence of fracture and preparation time were investigated. Zips and elbows occurred significantly (P < 0.001) less frequently with rotary than with manual preparation. The correct preparation length was achieved significantly (P < 0.05) more often with rotary Ni-Ti files than with manual stainless steel files. Fractures occurred significantly (P < 0.05) less frequently with hand instrumentation. The mean time required for manual preparation was significantly (P < 0.001) longer than that required for rotary preparation. Prior experience with a hand preparation technique was not reflected in an improved quality of the subsequent engine-driven preparation. Inexperienced operators achieved better canal preparations with rotary Ni-Ti instruments than with manual stainless steel files. However, rotary preparation was associated with significantly more fractures.

In vitro analysis of the marginal adaptation and discrepancy of stainless steel crowns

PubMed Central

Mulder, Riaan; Medhat, Rasha; Mohamed, Nadia

2018-01-01

Abstract Aim: The purpose of the study was to assess the marginal adaptation and discrepancy of SSC’s. Differences in adaptation and discrepancy between the four surfaces (mesial, lingual, distal, and buccal) were evaluated. Methods: The placement of stainless steel crowns were completed on a phantom head in accordance with the clinical technique. The ideal tooth preparation was made and this ‘master tooth’ duplicated to achieve a sample size of 15. The stainless steel crowns were placed, trimmed, and cemented as per the clinical technique. The cemented stainless crowns were analyzed under 100× stereomicroscope magnification. The marginal adaptation and discrepancy of each specimen was measured every 2 µm. Results: All the specimens showed marginal adaptation and discrepancy. The lingual margin had a significantly better adaptation (p < .0001) over the other surfaces. The buccal surface was the only surface that had an appropriate supra-CEJ level with a significance of p < .0001. Conclusion: The marginal discrepancies occur during the trimming procedure and assessment of the gingival approximation of the SSC margin. The inspection of stainless steel crown adaptation and discrepancy is an essential clinical step. PMID:29536024

Analysis and characterization of microwave plasma generated with rectangular all-dielectric resonators

NASA Astrophysics Data System (ADS)

Kourtzanidis, K.; Raja, L. L.

2017-04-01

We report on a computational modeling study of small scale plasma discharge formation with rectangular dielectric resonators (DR). An array of rectangular dielectric slabs, separated by a gap of millimeter dimensions is used to provide resonant response when illuminated by an incident wave of 1.26 GHz. A coupled electromagnetic (EM) wave-plasma model is used to describe the breakdown, early response and steady state of the argon discharge. We characterize the plasma generation with respect to the input power, background gas pressure and gap size. It is found that the plasma discharge is generated mainly inside the gaps between the DR at positions that correspond to the antinodes of the resonant enhanced electric field pattern. The enhancement of the electric field inside the gaps is due to a combination of leaking and displacement current radiation from the DR. The plasma is sustained in over-critical densities due to the large skin depth with respect to the gap and plasma size. Electron densities are calculated in the order of {10}18{--}{10}19 {{{m}}}-3 for a gas pressure of 10 Torr, while they exceed 1020 {{{m}}}-3 in atmospheric conditions. Increase of input power leads to more intense ionization and thus faster plasma formation and results to a more symmetric plasma pattern. For low background gas pressure the discharge is diffusive and extends away from the gap region while in high pressure it is constricted inside the gap. An optimal gap size can be found to provide maximum EM energy transfer to the plasma. This fact demonstrates that the gap size dictates to a certain extent the resonant frequency and the Q-factor of the dielectric array and the breakdown fields can not be determined in a straight-forward way but they are functions of the resonators geometry and incident field frequency.

Adaptive wavefront sensor based on the Talbot phenomenon.

PubMed

Podanchuk, Dmytro V; Goloborodko, Andrey A; Kotov, Myhailo M; Kovalenko, Andrey V; Kurashov, Vitalij N; Dan'ko, Volodymyr P

2016-04-20

A new adaptive method of wavefront sensing is proposed and demonstrated. The method is based on the Talbot self-imaging effect, which is observed in an illuminating light beam with strong second-order aberration. Compensation of defocus and astigmatism is achieved with an appropriate choice of size of the rectangular unit cell of the diffraction grating, which is performed iteratively. A liquid-crystal spatial light modulator is used for this purpose. Self-imaging of rectangular grating in the astigmatic light beam is demonstrated experimentally. High-order aberrations are detected with respect to the compensated second-order aberration. The comparative results of wavefront sensing with a Shack-Hartmann sensor and the proposed sensor are adduced.

Critical heat flux for free convection boiling in thin rectangular channels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cheng, Lap Y.; Tichler, P.R.

A review of the experimental data on free convection boiling critical heat flux (CHF) in vertical rectangular channels reveals three mechanisms of burnout. They are the pool boiling limit, the circulation limit, and the flooding limit associated with a transition in flow regime from churn to annular flow. The dominance of a particular mechanism depends on the dimensions of the channel. Analytical models were developed for each free convection boiling limit. Limited agreement with data is observed. A CHF correlation, which is valid for a wide range of gap sizes, was constructed from the CHFs calculated according to the threemore » mechanisms of burnout. 17 refs., 7 figs.« less

Size of metallic and polyethylene debris particles in failed cemented total hip replacements

NASA Technical Reports Server (NTRS)

Lee, J. M.; Salvati, E. A.; Betts, F.; DiCarlo, E. F.; Doty, S. B.; Bullough, P. G.

1992-01-01

Reports of differing failure rates of total hip prostheses made of various metals prompted us to measure the size of metallic and polyethylene particulate debris around failed cemented arthroplasties. We used an isolation method, in which metallic debris was extracted from the tissues, and a non-isolation method of routine preparation for light and electron microscopy. Specimens were taken from 30 cases in which the femoral component was of titanium alloy (10), cobalt-chrome alloy (10), or stainless steel (10). The mean size of metallic particles with the isolation method was 0.8 to 1.0 microns by 1.5 to 1.8 microns. The non-isolation method gave a significantly smaller mean size of 0.3 to 0.4 microns by 0.6 to 0.7 microns. For each technique the particle sizes of the three metals were similar. The mean size of polyethylene particles was 2 to 4 microns by 8 to 13 microns. They were larger in tissue retrieved from failed titanium-alloy implants than from cobalt-chrome and stainless-steel implants. Our results suggest that factors other than the size of the metal particles, such as the constituents of the alloy, and the amount and speed of generation of debris, may be more important in the failure of hip replacements.

A New Maraging Stainless Steel with Excellent Strength-Toughness-Corrosion Synergy.

PubMed

Tian, Jialong; Wang, Wei; Babar Shahzad, M; Yan, Wei; Shan, Yiyin; Jiang, Zhouhua; Yang, Ke

2017-11-10

A new maraging stainless steel with superior strength-toughness-corrosion synergy has been developed based on an innovative concept of alloy design. The high strength-toughness combination is achieved by forming dispersive nano-sized intermetallic compounds in the soft lath martensitic matrix with a slight amount of residual austenite. The good corrosion resistance is guaranteed by exactly controlling the Co content based on understanding the synergistic effect between Co and Cr. The fine structure characteristics of two dominant strengthening precipitations including Ni₃Ti and Mo-rich phases were finely characterized associated with transmission electron microscope (TEM) and atom probe tomography (APT) analyses. The relationship among microstructure, strength and toughness is discussed. The precipitation mechanism of different precipitates in the new maraging stainless steel is revealed based on the APT analysis.

Evaluation of Giga-cycle Fatigue Properties of Austenitic Stainless Steels Using Ultrasonic Fatigue Test

NASA Astrophysics Data System (ADS)

Takahashi, Kyouhei; Ogawa, Takeshi

Ultrasonic fatigue tests have been performed in austenitic stainless steel, SUS316NG, in order to investigate giga-cycle fatigue strength of pre-strained materials, i.e. 5, 10 and 20% tensile pre-strains and -20% compressive pre-strain. The pre-strains were applied before specimen machining. The austenitic stainless steels are known to exhibit remarkable self-heating during the fatigue experiment. Therefore, heat radiation method was established by setting fatigue specimens in a low temperature chamber at about -100°C. The self-heating was controlled by intermittent loading condition, which enabled us to maintain the test section of the specimens at about room temperature. The results revealed that the fatigue strength increased with increasing pre-strain levels. Fish-eye fracture was observed for -20% pre-strained specimen fractured at 4.11×107 cycles, while the other specimens exhibited ordinary fatigue fracture surface originated from stage I facet on the specimen surface. The increase in fatigue limit was predicted by Vickers hardness, HV, which depended on the size of indented region. The prediction was successful using HV values obtained by the size of the indented region similar to those of the stage I facets.

SU-G-BRC-17: Using Generalized Mean for Equivalent Square Estimation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhou, S; Fan, Q; Lei, Y

Purpose: Equivalent Square (ES) is a widely used concept in radiotherapy. It enables us to determine many important quantities for a rectangular treatment field, without measurement, based on the corresponding values from its ES field. In this study, we propose a Generalized Mean (GM) type ES formula and compare it with other established formulae using benchmark datasets. Methods: Our GM approach is expressed as ES=(w•fx^α+(1-w)•fy^α)^(1/α), where fx, fy, α, and w represent field sizes, power index, and a weighting factor, respectively. When α=−1 it reduces to well-known Sterling type ES formulae. In our study, α and w are determined throughmore » least-square-fitting. Akaike Information Criterion (AIC) was used to benchmark the performance of each formula. BJR (Supplement 17) ES field table for X-ray PDDs and open field output factor tables in Varian TrueBeam representative dataset were used for validation. Results: Switching from α=−1 to α=−1.25, a 20% reduction in standard deviation of residual error in ES estimation was achieved for the BJR dataset. The maximum relative residual error was reduced from ∼3% (in Sterling formula) or ∼2% (in Vadash/Bjarngard formula) down to ∼1% in GM formula for open fields of all energies and at rectangular field sizes from 3cm to 40cm in the Varian dataset. The improvement of the GM over the Sterling type ES formulae is particularly noticeable for very elongated rectangular fields with short width. AIC analysis confirmed the superior performance of the GM formula after taking into account the expanded parameter space. Conclusion: The GM significantly outperforms Sterling type formulae at slightly increased computational cost. The GM calculation may nullify the requirement of data measurement for many rectangular fields and hence shorten the Linac commissioning process. Improved dose calculation accuracy is also expected by adopting the GM formula into treatment planning and secondary MU check systems.« less

The Effects of Specimen Geometry and Size on the Dynamic Failure of Aluminum Alloy 2219-T8 Under Impact Loading

NASA Astrophysics Data System (ADS)

Bolling, Denzell Tamarcus

A significant amount of research has been devoted to the characterization of new engineering materials. Searching for new alloys which may improve weight, ultimate strength, or fatigue life are just a few of the reasons why researchers study different materials. In support of that mission this study focuses on the effects of specimen geometry and size on the dynamic failure of AA2219 aluminum alloy subjected to impact loading. Using the Split Hopkinson Pressure Bar (SHPB) system different geometric samples including cubic, rectangular, cylindrical, and frustum samples are loaded at different strain rates ranging from 1000s-1 to 6000s-1. The deformation properties, including the potential for the formation of adiabatic shear bands, of the different geometries are compared. Overall the cubic geometry achieves the highest critical strain and the maximum stress values at low strain rates and the rectangular geometry has the highest critical strain and the maximum stress at high strain rates. The frustum geometry type consistently achieves the lowest the maximum stress value compared to the other geometries under equal strain rates. All sample types clearly indicated susceptibility to strain localization at different locations within the sample geometry. Micrograph analysis indicated that adiabatic shear band geometry was influenced by sample geometry, and that specimens with a circular cross section are more susceptible to shear band formation than specimens with a rectangular cross section.

Nano/ultrafine grained austenitic stainless steel through the formation and reversion of deformation-induced martensite: Mechanisms, microstructures, mechanical properties, and TRIP effect

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shirdel, M., E-mail: mshirdel1989@ut.ac.ir; Mirzadeh, H., E-mail: hmirzadeh@ut.ac.ir; Advanced Metalforming and Thermomechanical Processing Laboratory, School of Metallurgy and Materials Engineering, University of Tehran, Tehran

A comprehensive study was carried out on the strain-induced martensitic transformation, its reversion to austenite, the resultant grain refinement, and the enhancement of strength and strain-hardening ability through the transformation-induced plasticity (TRIP) effect in a commercial austenitic 304L stainless steel with emphasis on the mechanisms and the microstructural evolution. A straightforward magnetic measurement device, which is based on the measurement of the saturation magnetization, for evaluating the amount of strain-induced martensite after cold rolling and reversion annealing in metastable austenitic stainless steels was used, which its results were in good consistency with those of the X-ray diffraction (XRD) method. Amore » new parameter called the effective reduction in thickness was introduced, which corresponds to the reasonable upper bound on the obtainable martensite fraction based on the saturation in the martensitic transformation. By means of thermodynamics calculations, the reversion mechanisms were estimated and subsequently validated by experimental results. The signs of thermal martensitic transformation at cooling stage after reversion at 850 °C were found, which was attributed to the rise in the martensite start temperature due to the carbide precipitation. After the reversion treatment, the average grain sizes were around 500 nm and the nanometric grains of the size of ~ 65 nm were also detected. The intense grain refinement led to the enhanced mechanical properties and observation of the change in the work-hardening capacity and TRIP effect behavior. A practical map as a guidance for grain refining and characterizing the stability against grain growth was proposed, which shows the limitation of the reversion mechanism for refinement of grain size. - Graphical abstract: Display Omitted - Highlights: • Nano/ultrafine grained austenitic stainless steel through martensite treatment • A parameter descriptive of a reasonable upper bound on the obtainable martensite • Characterization of martensite by virtue of a new developed magnetic device • Investigation of mechanical properties and TRIP effect and the effect of grain size.« less

Flow regimes of adiabatic gas-liquid two-phase under rolling conditions

NASA Astrophysics Data System (ADS)

Yan, Chaoxing; Yan, Changqi; Sun, Licheng; Xing, Dianchuan; Wang, Yang; Tian, Daogui

2013-07-01

Characteristics of adiabatic air/water two-phase flow regimes under vertical and rolling motion conditions were investigated experimentally. Test sections are two rectangular ducts with the gaps of 1.41 and 10 mm, respectively, and a circular tube with 25 mm diameter. Flow regimes were recorded by a high speed CCD-camera and were identified by examining the video images. The experimental results indicate that the characteristics of flow patterns in 10 mm wide rectangular duct under vertical condition are very similar to those in circular tube, but different from the 1.41 mm wide rectangular duct. Channel size has a significant influence on flow pattern transition, boundary of which in rectangular channels tends asymptotically towards that in the circular tube with increasing the width of narrow side. Flow patterns in rolling channels are similar to each other, nevertheless, the effect of rolling motion on flow pattern transition are significantly various. Due to the remarkable influences of the friction shear stress and surface tension in the narrow gap duct, detailed flow pattern maps of which under vertical and rolling conditions are indistinguishable. While for the circular tube with 25 mm diameter, the transition from bubbly to slug flow occurs at a higher superficial liquid velocity and the churn flow covers more area on the flow regime map as the rolling period decreases.

Oxide particle size distribution from shearing irradiated and unirradiated LWR fuels in Zircaloy and stainless steel cladding: significance for risk assessment

DOE Office of Scientific and Technical Information (OSTI.GOV)

Davis, W. Jr.; West, G.A.; Stacy, R.G.

1979-03-22

Sieve fractionation was performed with oxide particles dislodged during shearing of unirradiated or irradiated fuel bundles or single rods of UO/sub 2/ or 96 to 97% ThO/sub 2/--3 to 4% UO/sub 2/. Analyses of these data by nonlinear least-squares techniques demonstrated that the particle size distribution is lognormal. Variables involved in the numerical analyses include lognormal median size, lognormal standard deviation, and shear cut length. Sieve-fractionation data are presented for unirradiated bundles of stainless-steel-clad or Zircaloy-2-clad UO/sub 2/ or ThO/sub 2/--UO/sub 2/ sheared into lengths from 0.5 to 2.0 in. Data are also presented for irradiated single rods (sheared intomore » lengths of 0.25 to 2.0 in.) of Zircaloy-2-clad UO/sub 2/ from BWRs and of Zircaloy-4-clad UO/sub 2/ from PWRs. Median particle sizes of UO/sub 2/ from shearing irradiated stainless-steel-clad fuel ranged from 103 to 182 ..mu..m; particle sizes of ThO/sub 2/--UO/sub 2/, under these same conditions, ranged from 137 to 202 ..mu..m. Similarly, median particle sizes of UO/sub 2/ from shearing unirradiated Zircaloy-2-clad fuel ranged from 230 to 957 ..mu..m. Irradiation levels of fuels from reactors ranged from 9,000 to 28,000 MWd/MTU. In general, particle sizes from shearing these irradiated fuels are larger than those from the unirradiated fuels; however, unirradiated fuel from vendors was not available for performing comparative shearing experiments. In addition, variations in particle size parameters pertaining to samples of a single vendor varied as much as those between different vendors. The fraction of fuel dislodged from the cladding is nearly proportional to the reciprocal of the shear cut length, until the cut length attains some minimum value below which all fuel is dislodged. Particles of fuel are generally elongated with a long-to-short axis ratio usually less than 3. Using parameters of the lognormal distribution estimates can be made of fractions of dislodged fuel having dimensions less than specified values.« less

Near-Field Microwave Detection of Corrosion Precursor Pitting under Thin Dielectric Coatings in Metallic Substrate

NASA Astrophysics Data System (ADS)

Hughes, D.; Zoughi, R.; Austin, R.; Wood, N.; Engelbart, R.

2003-03-01

Detection of corrosion precursor pitting on metallic surfaces under various coatings and on bare metal is of keen interest in evaluation of aircraft fuselage. Near-field microwave nondestructive testing methods, utilizing open-ended rectangular waveguides and coaxial probes, have been used extensively for detection of surface flaws in metals, both on bare metal and under a dielectric coating. This paper presents the preliminary results of using microwave techniques to detect corrosion precursor pitting under paint and primer, applique and on bare metal. Machined pits of 500 μm diameter were detected using open-ended rectangular waveguides at V-Band under paint and primer and applique, and on bare metal. Using coaxial probes, machined pits with diameters down to 150 μm on bare metal were also detected. Relative pit size and density were shown on a corrosion-pitted sample using open-ended rectangular waveguides at frequencies of 35 GHz to 70 GHz. The use of Boeing's MAUS™ scanning systems provided improved results by alleviating standoff variation and scanning artifact. Typical results of this investigation are also presented.

Polyomino Problems to Confuse Computers

ERIC Educational Resources Information Center

Coffin, Stewart

2009-01-01

Computers are very good at solving certain types combinatorial problems, such as fitting sets of polyomino pieces into square or rectangular trays of a given size. However, most puzzle-solving programs now in use assume orthogonal arrangements. When one departs from the usual square grid layout, complications arise. The author--using a computer,…

Comparison of torsional stability of 2 types of split crimpable surgical hooks with soldered brass surgical hooks.

PubMed

O'Bannon, Shawn P; Dunn, William J; Lenk, Jason S

2006-10-01

The purpose of this in-vitro study was to compare the torsional stability of split crimpable surgical hooks and soldered brass surgical hooks on a rectangular stabilizing archwire. Coated split crimpable hooks (Never-Slip Grip, TP Orthodontics, LaPorte, Ind), ribbed crimpable hooks (TP Orthodontics), and .032-in brass soldered hooks/notched electrodes (Ormco/Sybron Dental Specialties, Orange, Calif) were attached to a 0.019 x 0.025-in stainless steel archwire. The archwire/hook attachment assembly was secured into a dual contact jig and statically mounted to the base of a universal testing machine. The hooks were engaged by a wire loop attached to the upper load cell of the machine, which pulled the wire until the hook was torsionally displaced from the archwire. The mean forces, measured in newtons (N), required to dislodge the hooks were as follows: soldered brass surgical hooks (51.3 +/- 5.2 N), coated split crimpable hooks (49.9 +/- 6.6 N), and ribbed split crimpable hooks (31.3 +/- 5.4 N). Data were analyzed with 1-way ANOVA and Tukey HSD post-hoc tests at alpha = .05. Ribbed split crimpable hooks provided significantly less resistance to torsional displacement than the other types of hooks (P <001). There was no difference between coated split crimpable hooks and soldered brass surgical hooks (P >05). Under the conditions of this study, the results suggest that soldered brass surgical hooks and coated split crimpable hook attachments provide more stability to torsional dislodgement from a rectangular stabilizing archwire than ribbed split crimpable hooks.

Revisiting the Fundamental Analytical Solutions of Heat and Mass Transfer: The Kernel of Multirate and Multidimensional Diffusion

NASA Astrophysics Data System (ADS)

Zhou, Quanlin; Oldenburg, Curtis M.; Rutqvist, Jonny; Birkholzer, Jens T.

2017-11-01

There are two types of analytical solutions of temperature/concentration in and heat/mass transfer through boundaries of regularly shaped 1-D, 2-D, and 3-D blocks. These infinite-series solutions with either error functions or exponentials exhibit highly irregular but complementary convergence at different dimensionless times, td. In this paper, approximate solutions were developed by combining the error-function-series solutions for early times and the exponential-series solutions for late times and by using time partitioning at the switchover time, td0. The combined solutions contain either the leading term of both series for normal-accuracy approximations (with less than 0.003 relative error) or the first two terms for high-accuracy approximations (with less than 10-7 relative error) for 1-D isotropic (spheres, cylinders, slabs) and 2-D/3-D rectangular blocks (squares, cubes, rectangles, and rectangular parallelepipeds). This rapid and uniform convergence for rectangular blocks was achieved by employing the same time partitioning with individual dimensionless times for different directions and the product of their combined 1-D slab solutions. The switchover dimensionless time was determined to minimize the maximum approximation errors. Furthermore, the analytical solutions of first-order heat/mass flux for 2-D/3-D rectangular blocks were derived for normal-accuracy approximations. These flux equations contain the early-time solution with a three-term polynomial in √td and the late-time solution with the limited-term exponentials for rectangular blocks. The heat/mass flux equations and the combined temperature/concentration solutions form the ultimate kernel for fast simulations of multirate and multidimensional heat/mass transfer in porous/fractured media with millions of low-permeability blocks of varying shapes and sizes.

Revisiting the Fundamental Analytical Solutions of Heat and Mass Transfer: The Kernel of Multirate and Multidimensional Diffusion

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhou, Quanlin; Oldenburg, Curtis M.; Rutqvist, Jonny

There are two types of analytical solutions of temperature/concentration in and heat/mass transfer through boundaries of regularly shaped 1D, 2D, and 3D blocks. These infinite-series solutions with either error functions or exponentials exhibit highly irregular but complementary convergence at different dimensionless times, t d0. In this paper, approximate solutions were developed by combining the error-function-series solutions for early times and the exponential-series solutions for late times and by using time partitioning at the switchover time, t d0. The combined solutions contain either the leading term of both series for normal-accuracy approximations (with less than 0.003 relative error) or the firstmore » two terms for high-accuracy approximations (with less than 10-7 relative error) for 1D isotropic (spheres, cylinders, slabs) and 2D/3D rectangular blocks (squares, cubes, rectangles, and rectangular parallelepipeds). This rapid and uniform convergence for rectangular blocks was achieved by employing the same time partitioning with individual dimensionless times for different directions and the product of their combined 1D slab solutions. The switchover dimensionless time was determined to minimize the maximum approximation errors. Furthermore, the analytical solutions of first-order heat/mass flux for 2D/3D rectangular blocks were derived for normal-accuracy approximations. These flux equations contain the early-time solution with a three-term polynomial in √td and the late-time solution with the limited-term exponentials for rectangular blocks. The heat/mass flux equations and the combined temperature/concentration solutions form the ultimate kernel for fast simulations of multirate and multidimensional heat/mass transfer in porous/fractured media with millions of low-permeability blocks of varying shapes and sizes.« less

Revisiting the Fundamental Analytical Solutions of Heat and Mass Transfer: The Kernel of Multirate and Multidimensional Diffusion

DOE PAGES

Zhou, Quanlin; Oldenburg, Curtis M.; Rutqvist, Jonny; ...

2017-10-24

There are two types of analytical solutions of temperature/concentration in and heat/mass transfer through boundaries of regularly shaped 1D, 2D, and 3D blocks. These infinite-series solutions with either error functions or exponentials exhibit highly irregular but complementary convergence at different dimensionless times, t d0. In this paper, approximate solutions were developed by combining the error-function-series solutions for early times and the exponential-series solutions for late times and by using time partitioning at the switchover time, t d0. The combined solutions contain either the leading term of both series for normal-accuracy approximations (with less than 0.003 relative error) or the firstmore » two terms for high-accuracy approximations (with less than 10-7 relative error) for 1D isotropic (spheres, cylinders, slabs) and 2D/3D rectangular blocks (squares, cubes, rectangles, and rectangular parallelepipeds). This rapid and uniform convergence for rectangular blocks was achieved by employing the same time partitioning with individual dimensionless times for different directions and the product of their combined 1D slab solutions. The switchover dimensionless time was determined to minimize the maximum approximation errors. Furthermore, the analytical solutions of first-order heat/mass flux for 2D/3D rectangular blocks were derived for normal-accuracy approximations. These flux equations contain the early-time solution with a three-term polynomial in √td and the late-time solution with the limited-term exponentials for rectangular blocks. The heat/mass flux equations and the combined temperature/concentration solutions form the ultimate kernel for fast simulations of multirate and multidimensional heat/mass transfer in porous/fractured media with millions of low-permeability blocks of varying shapes and sizes.« less

A New Maraging Stainless Steel with Excellent Strength–Toughness–Corrosion Synergy

PubMed Central

Tian, Jialong; Wang, Wei; Babar Shahzad, M.; Yan, Wei; Shan, Yiyin; Jiang, Zhouhua; Yang, Ke

2017-01-01

A new maraging stainless steel with superior strength–toughness–corrosion synergy has been developed based on an innovative concept of alloy design. The high strength–toughness combination is achieved by forming dispersive nano-sized intermetallic compounds in the soft lath martensitic matrix with a slight amount of residual austenite. The good corrosion resistance is guaranteed by exactly controlling the Co content based on understanding the synergistic effect between Co and Cr. The fine structure characteristics of two dominant strengthening precipitations including Ni3Ti and Mo-rich phases were finely characterized associated with transmission electron microscope (TEM) and atom probe tomography (APT) analyses. The relationship among microstructure, strength and toughness is discussed. The precipitation mechanism of different precipitates in the new maraging stainless steel is revealed based on the APT analysis. PMID:29125550

Positron annihilation lifetime measurements of austenitic stainless and ferritic/martensitic steels irradiated in the SINQ target irradiation program

NASA Astrophysics Data System (ADS)

Sato, K.; Xu, Q.; Yoshiie, T.; Dai, Y.; Kikuchi, K.

2012-12-01

Titanium-doped austenitic stainless steel (JPCA) and reduced activated ferritic/martensitic steel (F82H) irradiated with high-energy protons and spallation neutrons were investigated by positron annihilation lifetime measurements. Subnanometer-sized (<˜0.8 nm) helium bubbles, which cannot be observed by transmission electron microscopy, were detected by positron annihilation lifetime measurements for the first time. For the F82H steel, the positron annihilation lifetime of the bubbles decreased with increasing irradiation dose and annealing temperature because the bubbles absorb additional He atoms. In the case of JPCA steel, the positron annihilation lifetime increased with increasing annealing temperature above 773 K, in which case the dissociation of complexes of vacancy clusters with He atoms and the growth of He bubbles was detected. He bubble size and density were also discussed.

Abnormal grain growth in AISI 304L stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shirdel, M., E-mail: mshirdel1989@ut.ac.ir; Mirzadeh, H., E-mail: hmirzadeh@ut.ac.ir; Advanced Metalforming and Thermomechanical Processing Laboratory, School of Metallurgy and Materials Engineering, University of Tehran, Tehran

2014-11-15

The microstructural evolution during abnormal grain growth (secondary recrystallization) in 304L stainless steel was studied in a wide range of annealing temperatures and times. At relatively low temperatures, the grain growth mode was identified as normal. However, at homologous temperatures between 0.65 (850 °C) and 0.7 (900 °C), the observed transition in grain growth mode from normal to abnormal, which was also evident from the bimodality in grain size distribution histograms, was detected to be caused by the dissolution/coarsening of carbides. The microstructural features such as dispersed carbides were characterized by optical metallography, X-ray diffraction, scanning electron microscopy, energy dispersivemore » X-ray analysis, and microhardness. Continued annealing to a long time led to the completion of secondary recrystallization and the subsequent reappearance of normal growth mode. Another instance of abnormal grain growth was observed at homologous temperatures higher than 0.8, which may be attributed to the grain boundary faceting/defaceting phenomenon. It was also found that when the size of abnormal grains reached a critical value, their size will not change too much and the grain growth behavior becomes practically stagnant. - Highlights: • Abnormal grain growth (secondary recrystallization) in AISI 304L stainless steel • Exaggerated grain growth due to dissolution/coarsening of carbides • The enrichment of carbide particles by titanium • Abnormal grain growth due to grain boundary faceting at very high temperatures • The stagnancy of abnormal grain growth by annealing beyond a critical time.« less

Biomaterial Studies on AISI 316L Stainless Steel after Magnetoelectropolishing

PubMed Central

Hryniewicz, Tadeusz; Rokosz, Krzysztof; Filippi, Massimiliano

2009-01-01

The polarisation characteristics of the electropolishing process in a magnetic field (MEP – magnetoelectropolishing), in comparison with those obtained under standard/conventional process (EP) conditions, have been obtained. The occurrence of an EP plateau has been observed in view of the optimization of MEP process. Up-to-date stainless steel surface studies always indicated some amount of free-metal atoms apart from the detected oxides and hydroxides. Such a morphology of the surface film usually affects the thermodynamic stability and corrosion resistance of surface oxide layer and is one of the most important features of stainless steels. With this new MEP process we can improve metal surface properties by making the stainless steel more resistant to halides encountered in a variety of environments. Furthermore, in this paper the stainless steel surface film study results have been presented. The results of the corrosion research carried out by the authors on the behaviour of the most commonly used material − medical grade AISI 316L stainless steel both in Ringer’s body fluid and in aqueous 3% NaCl solution have been investigated and presented earlier elsewhere, though some of these results, concerning the EIS Nyquist plots and polarization curves are also revealed herein. In this paper an attempt to explain this peculiar performance of 316L stainless steel has been undertaken. The SEM studies, Auger electron spectroscopy (AES) and X-ray photoelectron spectroscopy (XPS) were performed on 316L samples after three treatments: MP – abrasive polishing (800 grit size), EP – conventional electrolytic polishing, and MEP – magnetoelectropolishing. It has been found that the proposed magnetoelectropolishing (MEP) process considerably modifies the morphology and the composition of the surface film, thus leading to improved corrosion resistance of the studied 316L SS.

Flexibility and torsional behaviour of rotary nickel-titanium PathFile, RaCe ISO 10, Scout RaCe and stainless steel K-File hand instruments.

PubMed

Nakagawa, R K L; Alves, J L; Buono, V T L; Bahia, M G A

2014-03-01

To assess and compare the flexibility and torsional resistance of PathFile, RaCe ISO 10 and Scout RaCe instruments in relation to stainless steel K-File hand instruments. Rotary PathFile (sizes 13, 16 and 19; .02 taper), Race ISO 10 (size 10; 0.02, 0.04 and 0.06 tapers), Scout RaCe (sizes 10, 15 and 20; 0.02 taper) and hand K-File (sizes 10, 15 and 20; 0.02 taper) instruments were evaluated. Alloy chemical composition, phases present and transformation temperatures were determined for the NiTi instruments. For all instruments, diameters at each millimetre from the tip as well as cross-sectional areas at 3 mm from the tip were measured based on ANSI/ADA Specification No. 101 using image analysis software. Resistance to bending and torsional resistance were determined according to specification ISO 3630-1. Vickers microhardness measurements were also taken in all instruments to assess their strength. Data were analysed using analysis of variance (α = 0.05). The alloys used in the manufacture of the three types of NiTi instruments had approximately the same chemical composition, but the PathFile instruments had a higher Af transformation temperature and contained a small amount of B19' martensite. All instruments had diameter values within the standard tolerance. The bending and torsional resistance values were significantly increased relative to the instrument diameter and cross-sectional area. PathFile instruments were the most flexible and the least torque resistant, whilst the stainless steel instruments were the least flexible although they were more torque resistant than the NiTi instruments. © 2013 International Endodontic Journal. Published by John Wiley & Sons Ltd.

Pressure drop and He II flow through fine mesh screens

NASA Astrophysics Data System (ADS)

Maddocks, J. R.; van Sciver, S. W.

1989-05-01

Fluid acquisition systems for He II transfer devices will utilize gallery arms to ensure that the fluid encounters the pump inlet. In near term experiments such as Superfluid Helium on Orbit Transfer (SHOOT), the preferred configuration consists of several rectangular channels which have one side made from a Dutch weave stainless steel screen having 325 x 2300 wires per inch. The effective pore diameter for this screen is about 5 microns. The present paper reports on measurements of pressure drop across a screen when it is subjected to a flow of liquid helium. The experiment measures the time rate of change of the level in two different helium reservoirs connected by a screen-blocked channel. Results with normal helium are compared with predictions based on the Armour-Cannon (1968) equations. The He II data show considerable deviation from the classical result. A discussion of the He II pressure drop results in terms of two fluid hydrodynamics is included.

Pressure drop and He II flow through fine mesh screens

NASA Technical Reports Server (NTRS)

Maddocks, J. R.; Van Sciver, S. W.

1989-01-01

Fluid acquisition systems for He II transfer devices will utilize gallery arms to ensure that the fluid encounters the pump inlet. In near term experiments such as Superfluid Helium on Orbit Transfer (SHOOT), the preferred configuration consists of several rectangular channels which have one side made from a Dutch weave stainless steel screen having 325 x 2300 wires per inch. The effective pore diameter for this screen is about 5 microns. The present paper reports on measurements of pressure drop across a screen when it is subjected to a flow of liquid helium. The experiment measures the time rate of change of the level in two different helium reservoirs connected by a screen-blocked channel. Results with normal helium are compared with predictions based on the Armour-Cannon (1968) equations. The He II data show considerable deviation from the classical result. A discussion of the He II pressure drop results in terms of two fluid hydrodynamics is included.

Area of Lattice Polygons

ERIC Educational Resources Information Center

Scott, Paul

2006-01-01

A lattice is a (rectangular) grid of points, usually pictured as occurring at the intersections of two orthogonal sets of parallel, equally spaced lines. Polygons that have lattice points as vertices are called lattice polygons. It is clear that lattice polygons come in various shapes and sizes. A very small lattice triangle may cover just 3…

Numerical approximations of the mean absorption cross-section of a variety of randomly oriented microalgal shapes.

PubMed

Baird, Mark E

2003-10-01

The size, shape, and absorption coefficient of a microalgal cell determines, to a first order approximation, the rate at which light is absorbed by the cell. The rate of absorption determines the maximum amount of energy available for photosynthesis, and can be used to calculate the attenuation of light through the water column, including the effect of packaging pigments within discrete particles. In this paper, numerical approximations are made of the mean absorption cross-section of randomly oriented cells, aA. The shapes investigated are spheroids, rectangular prisms with a square base, cylinders, cones and double cones with aspect ratios of 0.25, 0.5, 1, 2, and 4. The results of the numerical simulations are fitted to a modified sigmoid curve, and take advantage of three analytical solutions. The results are presented in a non-dimensionalised format and are independent of size. A simple approximation using a rectangular hyperbolic curve is also given, and an approach for obtaining the upper and lower bounds of aA for more complex shapes is outlined.

Experimental Stress Analysis of Stiffened Cylinders with Cutouts : Pure Bending

NASA Technical Reports Server (NTRS)

Schlechte, Floyd R; Rosecrans, Richard

1954-01-01

Bending tests were made on a cylindrical semimonocoque shell of circular cross section. The cylinder was tested without a cutout and then with a rectangular cutout which was successively enlarged through six sizes varying from 30 degrees to 130 degrees in circumference and from 1 to 2 bays in length. Strain measurements were made with resistance-type wire strain gages near the cutout on the stringers, the skin, and the rings for each size of cutout, and the stresses obtained are presented in tables. (author)

Effect of Coulomb interaction on chemical potential of metal film

NASA Astrophysics Data System (ADS)

Kostrobij, P. P.; Markovych, B. M.

2018-07-01

The chemical potential of a metal film within the jellium model taking into account the Coulomb interaction between electrons is calculated. The surface potential is modelled as the infinite rectangular potential well. The behaviour of the chemical potential as a function of the film thickness is studied, the quantum size effect for this quantity is analysed. It is shown that taking into account the Coulomb interaction leads to a significant decrease of the chemical potential and to an enhancement of the quantum size effect.

Preparation of Porous Stainless Steel Hollow-Fibers through Multi-Modal Particle Size Sintering towards Pore Engineering

PubMed Central

Allioux, Francois-Marie; Etxeberria Benavides, Miren

2017-01-01

The sintering of metal powders is an efficient and versatile technique to fabricate porous metal elements such as filters, diffusers, and membranes. Neck formation between particles is, however, critical to tune the porosity and optimize mass transfer in order to minimize the densification process. In this work, macro-porous stainless steel (SS) hollow-fibers (HFs) were fabricated by the extrusion and sintering of a dope comprised, for the first time, of a bimodal mixture of SS powders. The SS particles of different sizes and shapes were mixed to increase the neck formation between the particles and control the densification process of the structure during sintering. The sintered HFs from particles of two different sizes were shown to be more mechanically stable at lower sintering temperature due to the increased neck area of the small particles sintered to the large ones. In addition, the sintered HFs made from particles of 10 and 44 μm showed a smaller average pore size (<1 μm) as compared to the micron-size pores of sintered HFs made from particles of 10 μm only and those of 10 and 20 μm. The novel HFs could be used in a range of applications, from filtration modules to electrochemical membrane reactors. PMID:28777352

Grain boundary engineering for structure materials of nuclear reactors

NASA Astrophysics Data System (ADS)

Tan, L.; Allen, T. R.; Busby, J. T.

2013-10-01

Grain boundary engineering (GBE), primarily implemented by thermomechanical processing, is an effective and economical method of enhancing the properties of polycrystalline materials. Among the factors affecting grain boundary character distribution, literature data showed definitive effect of grain size and texture. GBE is more effective for austenitic stainless steels and Ni-base alloys compared to other structural materials of nuclear reactors, such as refractory metals, ferritic and ferritic-martensitic steels, and Zr alloys. GBE has shown beneficial effects on improving the strength, creep strength, and resistance to stress corrosion cracking and oxidation of austenitic stainless steels and Ni-base alloys.

Thermal conductivity of austenitic stainless steel, SRM 735, from 5 to 280 K

NASA Technical Reports Server (NTRS)

Hust, J. G.; Sparks, L. L.

1972-01-01

Thermal conductivity and electrical resistivity measurements were conducted on two lots of an austenitic stainless steel. Electrical resistivity measurements were performed on the second lot, both before and after the material was hot-swaged and reannealed to a size 1/10 the original diameter. These measurements indicate that this steel can be swaged and reannealed without an appreciable change in thermal conductivity. Electrical resistivity measurements as well as direct thermal conductivity measurements on several specimens from both lots indicate a material variability in these lots of less than 1% in thermal conductivity.

In vitro electrochemical corrosion and cell viability studies on nickel-free stainless steel orthopedic implants.

PubMed

Salahinejad, Erfan; Hadianfard, Mohammad Jafar; Macdonald, Digby Donald; Sharifi-Asl, Samin; Mozafari, Masoud; Walker, Kenneth J; Rad, Armin Tahmasbi; Madihally, Sundararajan V; Tayebi, Lobat

2013-01-01

The corrosion and cell viability behaviors of nanostructured, nickel-free stainless steel implants were studied and compared with AISI 316L. The electrochemical studies were conducted by potentiodynamic polarization and electrochemical impedance spectroscopic measurements in a simulated body fluid. Cytocompatibility was also evaluated by the adhesion behavior of adult human stem cells on the surface of the samples. According to the results, the electrochemical behavior is affected by a compromise among the specimen's structural characteristics, comprising composition, density, and grain size. The cell viability is interpreted by considering the results of the electrochemical impedance spectroscopic experiments.

Weld pool development during GTA and laser beam welding of Type 304 stainless steel; Part II-experimental correlation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zacharia, T.; David, S.A.; Vitek, J.M.

1989-12-01

In part I of the paper, the results of the heat flow and the fluid flow analysis were presented. Here, in Part II of the paper, predictions of the computational model are verified by comparing the numerically predicted and experimentally observed fusion zone size and shape. Stationary gas tungsten arc and laser beam welds were made on Type 304 stainless steel for different times to provide a variety of solidification conditions such as cooling rate and temperature gradient. Calculated temperatures and cooling rates are correlated with the experimentally observed fusion zone structure. In addition, the effect of sulfur on GTAmore » weld penetration was quantitatively evaluated by considering two heats of 304 stainless steel containing 90 and 240 ppm sulfur. Sulfur, as expected, increased the depth/width ratio by altering the surface tension gradient driven flow in the weld pool.« less

Effects of drilling variables on burr properties

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gillespie, L.K.

1976-09-01

An investigation utilizing 303Se stainless steel, 17-4PH stainless steel, 1018 steel, and 6061-T6 aluminum was conducted to determine the influence of drilling variables in controlling burr size to minimize burr-removal cost and improve the quality and reliability of parts for small precision mechanisms. Burr thickness can be minimized by reducing feedrate and cutting velocity, and by using drills having high helix angles. High helix angles reduce burr thickness, length, and radius, while most other variables reduce only one of these properties. Radial-lip drills minimize burrs from 303Se stainless steel when large numbers of holes are drilled; this material stretches 10more » percent before drill-breakthrough. Entrance burrs can be minimized by the use of subland drills at a greatly increased tool cost. Backup-rods used in cross-drilled holes may be difficult to remove and may scratch the hole walls.« less

Fabrication of a Flexible Micro Temperature Sensor for Micro Reformer Applications

PubMed Central

Lee, Chi-Yuan; Lin, Chien-Hen; Lo, Yi-Man

2011-01-01

Micro reformers still face obstacles in minimizing their size, decreasing the concentration of CO, conversion efficiency and the feasibility of integrated fabrication with fuel cells. By using a micro temperature sensor fabricated on a stainless steel-based micro reformer, this work attempts to measure the inner temperature and increase the conversion efficiency. Micro temperature sensors on a stainless steel substrate are fabricated using micro-electro-mechanical systems (MEMS) and then placed separately inside the micro reformer. Micro temperature sensors are characterized by their higher accuracy and sensitivity than those of a conventional thermocouple. To the best of our knowledge, micro temperature sensors have not been embedded before in micro reformers and commercial products, therefore, this work presents a novel approach to integrating micro temperature sensors in a stainless steel-based micro reformer in order to evaluate inner local temperature distributions and enhance reformer performance. PMID:22163817

Galvanic corrosion behavior of orthodontic archwire alloys coupled to bracket alloys.

PubMed

Iijima, Masahiro; Endo, Kazuhiko; Yuasa, Toshihiro; Ohno, Hiroki; Hayashi, Kazuo; Kakizaki, Mitsugi; Mizoguchi, Itaru

2006-07-01

The purpose of this study was to provide a quantitative assessment of galvanic corrosion behavior of orthodontic archwire alloys coupled to orthodontic bracket alloys in 0.9% NaCl solution and to study the effect of surface area ratios. Two common bracket alloys, stainless steels and titanium, and four common wire alloys, nickel-titanium (NiTi) alloy, beta-titanium (beta-Ti) alloy, stainless steel, and cobalt-chromium-nickel alloy, were used. Three different area ratios, 1:1, 1:2.35, and 1:3.64, were used; two of them assumed that the multibracket appliances consists of 14 brackets and 0.016 inch of round archwire or 0.016 x 0.022 inch of rectangular archwire. The galvanic current was measured for 3 successive days using zero-impedance ammeter. When the NiTi alloy was coupled with Ti (1:1, 1:2.35, and 1:3.64 of the surface area ratio) or beta-Ti alloy was coupled with Ti (1:2.35 and 1:3.64 of the surface area ratio), Ti initially was the anode and corroded. However, the polarity reversed in 1 hour, resulting in corrosion of the NiTi or beta-Ti. The NiTi alloy coupled with SUS 304 or Ti exhibited a relatively large galvanic current density even after 72 hours. It is suggested that coupling SUS 304-NiTi and Ti-NiTi may remarkably accelerate the corrosion of NiTi alloy, which serves as the anode. The different anode-cathode area ratios used in this study had little effect on galvanic corrosion behavior.

Structure and mechanical properties of as-received and heat-treated stainless steel orthodontic wires.

PubMed

Khier, S E; Brantley, W A; Fournelle, R A

1988-03-01

A combination of x-ray diffraction analysis with mechanical testing in tension and bending has been used to investigate the metallurgical structures and mechanical properties for as-received and heat-treated stainless steel orthodontic wires. Two different proprietary wire types were selected, having a wide range in cross-sectional dimensions: 0.016-, 0.030-, and 0.050- or 0.051-inch diameters, and 0.017 X 0.025-inch rectangular specimens. Heat treatments were performed for 10 minutes in air at temperatures of 700 degrees, 900 degrees, and 1100 degrees F. The x-ray diffraction patterns showed that the as-received 0.016-inch diameter and 0.017 X 0.025-inch wires of both proprietary types consisted of a two-phase structure containing a martensitic phase along with the austenitic phase. This duplex structure was converted entirely to austenite with heat treatment for one wire type, but persisted after heat treatment for the other wire type. The largest diameter, 0.050- or 0.051-inch, wires of both types were single-phase austenitic structure for both the as-received and heat-treated conditions. Evidence of substantial preferred crystallographic orientation or texturing in these orthodontic wires was also found by x-ray diffraction. As in our previous studies, the modulus of elasticity in bending was significantly less than the value obtained in tension for only the smaller cross-sectional wires. The 0.05 radian flexural yield strength correlated more closely with the 0.2% offset yield strength in tension than with the yield strength for 0.05% and 0.1% permanent offsets.

Loss of 3-D shape constancy in interior spaces: the basis of the Ames-room illusion.

PubMed

Dorward, F M; Day, R H

1997-01-01

The apparently rectangular form of the irregularly shaped Ames room is explained in terms of a loss of interior 3-D shape constancy consequent on viewing the room with one eye through a small specifically positioned aperture. In the absence of retinal disparity and motion parallax the appearance of the room is held to shift markedly toward the rectangular dimensions of its retinal image. Three experiments designed to test this explanation with a miniature (one-tenth size) version of the Ames room No 1 with the matched 2-D shape of the back wall and as an index of interior 3-D shape are reported. The experiments showed that interior constancy was almost fully restored with binocular viewing of the room (experiment 1). The effect with a 'skeletal' version of the room was about the same as that with the conventional version and was clearly evident when the back wall or its frame version was presented alone (experiment 2), and it varied according to whether the interior perspective corresponded with that of the Ames or a rectangular room (experiment 3). Experiment 3 also showed that a rectangular room is significantly distorted when the interior perspective accords with that of the Ames room. These outcomes are construed as supporting the loss-of-constancy explanation and as showing that the Ames-room effect is one of a class of illusions attributable to the absence of stimulus correlates that normally sustain visual shape constancy.

Identification, amounts, and kinetics of extraction of C-glucosidic ellagitannins during wine aging in oak barrels or in stainless steel tanks with oak chips.

PubMed

Jourdes, Michaël; Michel, Julien; Saucier, Cédric; Quideau, Stéphane; Teissedre, Pierre-Louis

2011-09-01

The C-glucosidic ellagitannins are found in wine as a result of its aging in oak barrels or in stainless steel tanks with oak chips. Once dissolved in this slightly acidic solution, the C-glucosidic ellagitannins vescalagin can react with nucleophilic entities present in red wine, such as ethanol, catechin, and epicatechin, to generate condensed hybrid products such as the β-1-O-ethylvescalagin and the flavano-ellagitannins (acutissimin A/B and epiacutissimin A/B), respectively. During this study, we first monitored the extraction kinetic and the evolution of the eight major oak-derived C-glucosidic ellagitannins in red wines aged in oak barrels or in stainless steel tank with oak chips. Their extraction rates appeared to be faster during red wine aging in stainless steel tanks with oak chips. However, their overall concentrations in wines were found higher in the wine aged in barrels. The formation rates of the vescalagin-coupled derivatives were also estimated for the first time under both red wine aging conditions (i.e., oak barrels or stainless steel tanks with oak chips). As observed for the oak-native C-glucosidic ellagitannins, the concentrations of these vescalagin derivatives were higher in the red wine aged in oak barrels than in stainless steel tanks with oak chips. Despite these differences, their relative composition was similar under both red wine aging conditions. Finally, the impact of the oak chips size and toasting level on the C-glucosidic ellagitannins concentration in wine was also investigated.

Influence of Deposition Conditions on Fatigue Properties of Martensitic Stainless Steel with Tin Film Coated by Arc Ion Plating Method

NASA Astrophysics Data System (ADS)

Fukui, Satoshi; Yonekura, Daisuke; Murakami, Ri-Ichi

The surface properties like roughness etc. strongly influence the fatigue strength of high-tensile steel. To investigate the effect of surface condition and TiN coating on the fatigue strength of high-strength steel, four-point bending fatigue tests were carried out for martensitic stainless steel with TiN film coated using arc ion plating (AIP) method. This study, using samples that had been polished under several size of grind particle, examines the influence of pre-coating treatment on fatigue properties. A 2-µm-thick TiN film was deposited onto the substrate under three kinds of polishing condition. The difference of the hardness originated in the residual stress or thin deformation layer where the difference of the size of grinding particle of the surface polishing. And it leads the transformation of the interface of the substrate and the TiN film and improves fatigue limit.

Hydrophobic and porous cellulose nanofibrous screen for efficient particulate matter (PM2.5) blocking

NASA Astrophysics Data System (ADS)

Chen, Liping; Guo, Yi; Peng, Xinsheng

2017-10-01

Particulate matter (PM2.5) pollution in air seriously affects public health. However, both bulk thickness and the accumulation of PM particles typically lead to a quick decline in the air permeability and large pressure drops of the conventional air clean membranes. In this work, we choose cellulose nanofibers (CNFs, a low cost, biodegradable and sustainable material) to form a hydrophobic and porous CNF thin layer on a stainless steel screen (300 mesh with pore size of 48 µm) through a simple filtration-assisted gelation process and subsequent polydimethylsiloxane modification. The prepared hydrophobic CNFs/stainless steel screen demonstrates highly efficient PM2.5 blocking based on size-sieving effect, fast air permeability and long-term durability under natural ventilation conditions in the relative humidity range from 45% to 93%. This technique holds great potential for indoor PM2.5 blocking under natural ventilation conditions.

Quantum-confinement effects on conduction band structure of rectangular cross-sectional GaAs nanowires

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tanaka, H., E-mail: tanaka@semicon.kuee.kyoto-u.ac.jp; Morioka, N.; Mori, S.

2014-02-07

The conduction band structure and electron effective mass of GaAs nanowires with various cross-sectional shapes and orientations were calculated by two methods, a tight-binding method and an effective mass equation taking the bulk full-band structure into account. The effective mass of nanowires increases as the cross-sectional size decreases, and this increase in effective mass depends on the orientations and substrate faces of nanowires. Among [001], [110], and [111]-oriented rectangular cross-sectional GaAs nanowires, [110]-oriented nanowires with wider width along the [001] direction showed the lightest effective mass. This dependence originates from the anisotropy of the Γ valley of bulk GaAs. Themore » relationship between effective mass and bulk band structure is discussed.« less

Friction behavior of self-ligating and conventional brackets with different ligature systems.

PubMed

Szczupakowski, Alexandra; Reimann, Susanne; Dirk, Cornelius; Keilig, Ludger; Weber, Anna; Jäger, Andreas; Bourauel, Christoph

2016-07-01

Self-ligating brackets are widely believed to offer better clinical efficiency and, in particular, less friction. Thus, the goal of this in vitro investigation was to assess the friction behavior of different bracket/archwire/ligature combinations during simulated canine retraction. An important aspect of this work was to determine whether conventional bracket systems behave differently in passive or active self-ligating brackets used with a Slide™ ligature, an elastic ligature, or a steel ligature. Three conventional (Contour, Class One; Discovery(®), Dentaurum; Mystique MB, GAC) and six self-ligating (Carriere SL, Class One; Clarity™ SL, 3M Unitek; Damon3, Ormco; In-Ovation(®) C, GAC; Speed Appliance, Speed System™; QuicKlear(®), Forestadent(®)) bracket systems were analyzed. All brackets featured a 0.022″ slot (0.56 mm). Each conventional system was tested with a steel ligature (0.25 mm; Remanium(®), Dentaurum), an elastic ligature (1.3 mm in diameter; Dentalastics, Dentaurum), and a modified elastic ligature (Slide™; Leone(®)). Each combination was used with four archwires, including rectangular stainless steel (0.46 × 0.64 mm, 0.018 × 0.025″, Dentaurum), rectangular nickel-titanium with Teflon coating (0.46 × 0.64 mm, 0.018 × 0.025″, Forestadent(®)), round coaxial nickel-titanium (0.46 mm, 0.018″, Speed), and half-round/half-square (D-profile) stainless steel (0.46 mm, 0.018″, Speed). In the orthodontic measurement and simulation system (OMSS), retraction of a canine was simulated on a Frasaco model replicated in resin. Based on the force systems, the respective friction values were determined. For each combination of materials, five brackets of the same type were tested and five single measurements performed. Friction values were found to vary distinctly with the different combinations, modifiers being the ligature systems and the archwire types. Any significant friction differences between the steel-ligated, Slide™-ligated, and self-ligated brackets were sporadic. All three systems were associated with average friction values of 40 %. Active self-ligating brackets and elastic-ligated conventional brackets, by contrast, generally differed significantly from the three above-mentioned bracket systems and showed distinctly higher friction values averaging 59 and 67 %, respectively. While passive self-ligating bracket systems have frequently been touted as advantageous in the literature, they should not be regarded as the only favorable system. Steel-ligated and Slide™-ligated conventional bracket systems are capable of offering similar friction performance.

Evaluation of vacuum filter sock surface sample collection method for Bacillus spores from porous and non-porous surfaces.

PubMed

Brown, Gary S; Betty, Rita G; Brockmann, John E; Lucero, Daniel A; Souza, Caroline A; Walsh, Kathryn S; Boucher, Raymond M; Tezak, Matthew S; Wilson, Mollye C

2007-07-01

Vacuum filter socks were evaluated for recovery efficiency of powdered Bacillus atrophaeus spores from two non-porous surfaces, stainless steel and painted wallboard and two porous surfaces, carpet and bare concrete. Two surface coupons were positioned side-by-side and seeded with aerosolized Bacillus atrophaeus spores. One of the surfaces, a stainless steel reference coupon, was sized to fit into a sample vial for direct spore removal, while the other surface, a sample surface coupon, was sized for a vacuum collection application. Deposited spore material was directly removed from the reference coupon surface and cultured for enumeration of colony forming units (CFU), while deposited spore material was collected from the sample coupon using the vacuum filter sock method, extracted by sonication and cultured for enumeration. Recovery efficiency, which is a measure of overall transfer effectiveness from the surface to culture, was calculated as the number of CFU enumerated from the filter sock sample per unit area relative to the number of CFU enumerated from the co-located reference coupon per unit area. The observed mean filter sock recovery efficiency from stainless steel was 0.29 (SD = 0.14, n = 36), from painted wallboard was 0.25 (SD = 0.15, n = 36), from carpet was 0.28 (SD = 0.13, n = 40) and from bare concrete was 0.19 (SD = 0.14, n = 44). Vacuum filter sock recovery quantitative limits of detection were estimated at 105 CFU m(-2) from stainless steel and carpet, 120 CFU m(-2) from painted wallboard and 160 CFU m(-2) from bare concrete. The method recovery efficiency and limits of detection established in this work provide useful guidance for the planning of incident response environmental sampling for biological agents such as Bacillus anthracis.

Jetting of a shear banding fluid in rectangular ducts

PubMed Central

Salipante, Paul F.; Little, Charles A. E.; Hudson, Steven D.

2017-01-01

Non-Newtonian fluids are susceptible to flow instabilities such as shear banding, in which the fluid may exhibit a markedly discontinuous viscosity at a critical stress. Here we report the characteristics and causes of a jetting flow instability of shear banding wormlike micelle solutions in microfluidic channels with rectangular cross sections over an intermediate volumetric flow regime. Particle-tracking methods are used to measure the three-dimensional flow field in channels of differing aspect ratios, sizes, and wall materials. When jetting occurs, it is self-contained within a portion of the channel where the flow velocity is greater than the surroundings. We observe that the instability forms in channels with aspect ratio greater than 5, and that the location of the high-velocity jet appears to be sensitive to stress localizations. Jetting is not observed in a lower concentration solution without shear banding. Simulations using the Johnson-Segalman viscoelastic model show a qualitatively similar behavior to the experimental observations and indicate that compressive normal stresses in the cross-stream directions support the development of the jetting flow. Our results show that nonuniform flow of shear thinning fluids can develop across the wide dimension in rectangular microfluidic channels, with implications for microfluidic rheometry. PMID:28691108

A functional analysis of photo-object matching skills of severely retarded adolescents.

PubMed

Dixon, L S

1981-01-01

Matching-to-sample procedures were used to assess picture representation skills of severely retarded, nonverbal adolescents. Identity matching within the classes of objects and life-size, full-color photos of the objects was first used to assess visual discrimination, a necessary condition for picture representation. Picture representation was then assessed through photo-object matching tasks. Five students demonstrated visual discrimination (identity matching) within the two classes of photos and the objects. Only one student demonstrated photo-object matching. The results of the four students who failed to demonstrate photo-object matching suggested that physical properties of photos (flat, rectangular) and depth dimensions of objects may exert more control over matching than the similarities of the objects and images within the photos. An analysis of figure-ground variables was conducted to provide an empirical basis for program development in the use of pictures. In one series of tests, rectangular shape and background were removed by cutting out the figures in the photos. The edge shape of the photo and the edge shape of the image were then identical. The results suggest that photo-object matching may be facilitated by using cut-out figures rather than the complete rectangular photo.

Effect of post-curing treatment on mechanical properties of composite resins.

PubMed

Almeida-Chetti, Verónica A; Macchi, Ricardo L; Iglesias, María E

2014-01-01

The aim of this study is to assess the effect of additional curing procedures on the flexural strength and modulus of elasticity of indirect and direct composite materials. Twenty-four rectangular prism-shaped 2 mm x 2 mm x 25 mm samples of Belleglass, Premisa (Kerr), Adoro and Heliomolar (Ivoclar Vivadent) were prepared. Each composite was packed in an ad-hoc stainless steel device with a TeflonR instrument. A mylar strip and a glass slab were placed on top to obtain a flat surface. Polymerization was activated for 20 seconds with a halogen unit (Astralis 10, Ivoclar - Vivadent) with soft start regime and an output with a 350 to 1200 mw/cm2 range at four different points according to the diameter of the end of the guide. The specimens obtained were then randomly divided into two different groups: with and without additional treatment. In the group with additional treatment, the samples adorro were submitted to 25 minutes in Lumamat 100 (Ivoclar Vivadent) and the rest to 20 minutes in BelleGlass HP (Kerr). After the curing procedures, all samples were treated with sandpapers of decreasing grain size under water flow, and stored in distilled water for 24 h. Flexural strength was measured according to the ISO 404920 recommendations and elastic modulus was determined following the procedures of ANSI/ADA standard No. 27. Statistical differences were found among the different materials and curing procedures employed (P<0.01). The elastic modulus was significantly higher after the additional curing treatment for all materials except Premisa. Further work is needed to determine the association between the actual monomers present in the matrix and the effect of additional curing processes on the mechanical properties of both direct and indirect composites, and its clinical relevance.

Effect of heat input on the microstructure, residual stresses and corrosion resistance of 304L austenitic stainless steel weldments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Unnikrishnan, Rahul, E-mail: rahulunnikrishnannair@gmail.com; Idury, K.S.N. Satish, E-mail: satishidury@gmail.com; Ismail, T.P., E-mail: tpisma@gmail.com

Austenitic stainless steels are widely used in high performance pressure vessels, nuclear, chemical, process and medical industry due to their very good corrosion resistance and superior mechanical properties. However, austenitic stainless steels are prone to sensitization when subjected to higher temperatures (673 K to 1173 K) during the manufacturing process (e.g. welding) and/or certain applications (e.g. pressure vessels). During sensitization, chromium in the matrix precipitates out as carbides and intermetallic compounds (sigma, chi and Laves phases) decreasing the corrosion resistance and mechanical properties. In the present investigation, 304L austenitic stainless steel was subjected to different heat inputs by shielded metalmore » arc welding process using a standard 308L electrode. The microstructural developments were characterized by using optical microscopy and electron backscattered diffraction, while the residual stresses were measured by X-ray diffraction using the sin{sup 2}ψ method. It was observed that even at the highest heat input, shielded metal arc welding process does not result in significant precipitation of carbides or intermetallic phases. The ferrite content and grain size increased with increase in heat input. The grain size variation in the fusion zone/heat affected zone was not effectively captured by optical microscopy. This study shows that electron backscattered diffraction is necessary to bring out changes in the grain size quantitatively in the fusion zone/heat affected zone as it can consider twin boundaries as a part of grain in the calculation of grain size. The residual stresses were compressive in nature for the lowest heat input, while they were tensile at the highest heat input near the weld bead. The significant feature of the welded region and the base metal was the presence of a very strong texture. The texture in the heat affected zone was almost random. - Highlights: • Effect of heat input on microstructure, residual stresses and corrosion is studied. • HAZ and width of dendrite in the welded region increase with heat input. • Residual stresses are tensile near the welded region after the highest heat input. • Welded region has the highest pit density after highest heat input. • Dendrites and δ-ferrite were highly oriented in the welded region.« less

Effect of Cyclic Thermal Process on Ultrafine Grain Formation in AISI 304L Austenitic Stainless Steel

NASA Astrophysics Data System (ADS)

Ravi Kumar, B.; Mahato, B.; Sharma, Sailaja; Sahu, J. K.

2009-12-01

As-received hot-rolled commercial grade AISI 304L austenitic stainless steel plates were solution treated at 1060 °C to achieve chemical homogeneity. Microstructural characterization of the solution-treated material revealed polygonal grains of about 85- μm size along with annealing twins. The solution-treated plates were heavily cold rolled to about 90 pct of reduction in thickness. Cold-rolled specimens were then subjected to thermal cycles at various temperatures between 750 °C and 925 °C. X-ray diffraction showed about 24.2 pct of strain-induced martensite formation due to cold rolling of austenitic stainless steel. Strain-induced martensite formed during cold rolling reverted to austenite by the cyclic thermal process. The microstructural study by transmission electron microscope of the material after the cyclic thermal process showed formation of nanostructure or ultrafine grain austenite. The tensile testing of the ultrafine-grained austenitic stainless steel showed a yield strength 4 to 6 times higher in comparison to its coarse-grained counterpart. However, it demonstrated very poor ductility due to inadequate strain hardenability. The poor strain hardenability was correlated with the formation of strain-induced martensite in this steel grade.

Physical properties and microstructure study of stainless steel 316L alloy fabricated by selective laser melting

NASA Astrophysics Data System (ADS)

Islam, Nurul Kamariah Md Saiful; Harun, Wan Sharuzi Wan; Ghani, Saiful Anwar Che; Omar, Mohd Asnawi; Ramli, Mohd Hazlen; Ismail, Muhammad Hussain

2017-12-01

Selective Laser Melting (SLM) demonstrates the 21st century's manufacturing infrastructure in which powdered raw material is melted by a high energy focused laser, and built up layer-by-layer until it forms three-dimensional metal parts. SLM process involves a variation of process parameters which affects the final material properties. 316L stainless steel compacts through the manipulation of building orientation and powder layer thickness parameters were manufactured by SLM. The effect of the manipulated parameters on the relative density and dimensional accuracy of the 316L stainless steel compacts, which were in the as-build condition, were experimented and analysed. The relationship between the microstructures and the physical properties of fabricated 316L stainless steel compacts was investigated in this study. The results revealed that 90° building orientation has higher relative density and dimensional accuracy than 0° building orientation. Building orientation was found to give more significant effect in terms of dimensional accuracy, and relative density of SLM compacts compare to build layer thickness. Nevertheless, the existence of large number and sizes of pores greatly influences the low performances of the density.

The effect of high pressure torsion on structural refinement and mechanical properties of an austenitic stainless steel.

PubMed

Krawczynska, Agnieszka Teresa; Lewandowska, Malgorzata; Pippan, Reinhard; Kurzydlowski, Krzysztof Jan

2013-05-01

In the present study, the high pressure torsion (HPT) was used to refine the grain structure down to the nanometer scale in an austenitic stainless steel. The principles of HPT lay on torsional deformation under simultaneous high pressure of the specimen, which results in substantial reduction in the grain size. Disks of the 316LVM austenitic stainless steel of 10 mm in diameter were subjected to equivalent strains epsilon of 32 at RT and 450 degrees C under the pressure of 4 GPa. Furthermore, two-stage HPT processes, i.e., deformation at room temperature followed by deformation at 450 degrees C, were performed. The resulting microstructures were investigated in TEM observations. The mechanical properties were measured in terms of the microhardness and in tensile tests. HPT performed at two-stage conditions (firstly at RT next at 450 degrees C) gives similar values of microhardness to the ones obtained after deforming only at 450 degrees C but performed to higher values of the overall equivalent strain epsilon. The effect of high pressure torsion on structural refinement and mechanical properties of an austenitic stainless steel was evaluated.

Generalization in Place Learning and Geometry Knowledge in Rats

ERIC Educational Resources Information Center

Tommasi, Luca; Thinus-Blanc, Catherine

2004-01-01

Rats were trained to search for a food reward hidden under sawdust in the center of a square-shaped enclosure designed to force orientation on the basis of the overall geometry of the environment. They were then tested in a number of enclosures differing in shape and in size (rectangular-, double-side square-, and equilateral triangle-shaped…

16 CFR 309.21 - Labeling requirements for used covered vehicles.

Code of Federal Regulations, 2010 CFR

2010-01-01

... visible surface of each such vehicle. (b) Layout. Figure 6 of appendix A is the prototype label that... consistent with the prototype label. The label required by this section is one-sided and rectangular in shape... label. Specific type sizes and faces to be used are indicated on the prototype label (Figure 6 of...

2015 Accomplishments-Tritium aging studies on stainless steel. Effects of hydrogen isotopes, crack orientation, and specimen geometry on fracture toughness

DOE Office of Scientific and Technical Information (OSTI.GOV)

Morgan, Michael J.

This study reports on the effects of hydrogen isotopes, crack orientation, and specimen geometry on the fracture toughness of stainless steels. Fracture toughness variability was investigated for Type 21-6-9 stainless steel using the 7K0004 forging. Fracture toughness specimens were cut from the forging in two different geometric configurations: arc shape and disc shape. The fracture toughness properties were measured at ambient temperature before and after exposure to hydrogen gas and compared to prior studies. There are three main conclusions that can be drawn from the results. First, the fracture toughness properties of actual reservoir forgings and contemporary heats of steelmore » are much higher than those measured in earlier studies that used heats of steel from the 1980s and 1990s and forward extruded forgings which were designed to simulate reservoir microstructures. This is true for as-forged heats as well as forged heats exposed to hydrogen gas. Secondly, the study confirms the well-known observation that cracks oriented parallel to the forging grain flow will propagate easier than those oriented perpendicular to the grain flow. However, what was not known, but is shown here, is that this effect is more pronounced, particularly after hydrogen exposures, when the forging is given a larger upset. In brick forgings, which have a relatively low amount of upset, the fracture toughness variation with specimen orientation is less than 5%; whereas, in cup forgings, the fracture toughness is about 20% lower than that forging to show how specimen geometry affects fracture toughness values. The American Society for Testing Materials (ASTM) specifies minimum specimen section sizes for valid fracture toughness values. However, sub-size specimens have long been used to study tritium effects because of the physical limitation of diffusing hydrogen isotopes into stainless steel at mild temperatures so as to not disturb the underlying forged microstructure. This study shows that fracture toughness values of larger specimens are higher and more representative of the material’s fracture behavior in a fully constrained tritium reservoir. The toughness properties measured for sub-size specimens were about 65-75% of the values for larger specimens. While the data from sub-size specimens are conservative, they may be overly so. The fracture toughness properties from sub-size specimens are valuable in that they can be used for tritium effects studies and show the same trends and alloy differences as those seen from larger specimen data. Additional work is planned, including finite element modeling, to see if sub-size specimen data could be adjusted in some way to be more closely aligned with the actual material behavior in a fully constrained pressure vessel.« less

In Vitro Electrochemical Corrosion and Cell Viability Studies on Nickel-Free Stainless Steel Orthopedic Implants

PubMed Central

Salahinejad, Erfan; Hadianfard, Mohammad Jafar; Macdonald, Digby Donald; Sharifi-Asl, Samin; Mozafari, Masoud; Walker, Kenneth J.; Rad, Armin Tahmasbi; Madihally, Sundararajan V.; Tayebi, Lobat

2013-01-01

The corrosion and cell viability behaviors of nanostructured, nickel-free stainless steel implants were studied and compared with AISI 316L. The electrochemical studies were conducted by potentiodynamic polarization and electrochemical impedance spectroscopic measurements in a simulated body fluid. Cytocompatibility was also evaluated by the adhesion behavior of adult human stem cells on the surface of the samples. According to the results, the electrochemical behavior is affected by a compromise among the specimen's structural characteristics, comprising composition, density, and grain size. The cell viability is interpreted by considering the results of the electrochemical impedance spectroscopic experiments. PMID:23630603

Comparison of stainless and mild steel welding fumes in generation of reactive oxygen species.

PubMed

Leonard, Stephen S; Chen, Bean T; Stone, Samuel G; Schwegler-Berry, Diane; Kenyon, Allison J; Frazer, David; Antonini, James M

2010-11-03

Welding fumes consist of a wide range of complex metal oxide particles which can be deposited in all regions of the respiratory tract. The welding aerosol is not homogeneous and is generated mostly from the electrode/wire. Over 390,000 welders were reported in the U.S. in 2008 while over 1 million full-time welders were working worldwide. Many health effects are presently under investigation from exposure to welding fumes. Welding fume pulmonary effects have been associated with bronchitis, metal fume fever, cancer and functional changes in the lung. Our investigation focused on the generation of free radicals and reactive oxygen species from stainless and mild steel welding fumes generated by a gas metal arc robotic welder. An inhalation exposure chamber located at NIOSH was used to collect the welding fume particles. Our results show that hydroxyl radicals (.OH) were generated from reactions with H2O2 and after exposure to cells. Catalase reduced the generation of .OH from exposed cells indicating the involvement of H2O2. The welding fume suspension also showed the ability to cause lipid peroxidation, effect O2 consumption, induce H2O2 generation in cells, and cause DNA damage. Increase in oxidative damage observed in the cellular exposures correlated well with .OH generation in size and type of welding fumes, indicating the influence of metal type and transition state on radical production as well as associated damage. Our results demonstrate that both types of welding fumes are able to generate ROS and ROS-related damage over a range of particle sizes; however, the stainless steel fumes consistently showed a significantly higher reactivity and radical generation capacity. The chemical composition of the steel had a significant impact on the ROS generation capacity with the stainless steel containing Cr and Ni causing more damage than the mild steel. Our results suggest that welding fumes may cause acute lung injury. Since type of fume generated, particle size, and elapsed time after generation of the welding exposure are significant factors in radical generation and particle deposition these factors should be considered when developing protective strategies.

Comparison of stainless and mild steel welding fumes in generation of reactive oxygen species

PubMed Central

2010-01-01

Background Welding fumes consist of a wide range of complex metal oxide particles which can be deposited in all regions of the respiratory tract. The welding aerosol is not homogeneous and is generated mostly from the electrode/wire. Over 390,000 welders were reported in the U.S. in 2008 while over 1 million full-time welders were working worldwide. Many health effects are presently under investigation from exposure to welding fumes. Welding fume pulmonary effects have been associated with bronchitis, metal fume fever, cancer and functional changes in the lung. Our investigation focused on the generation of free radicals and reactive oxygen species from stainless and mild steel welding fumes generated by a gas metal arc robotic welder. An inhalation exposure chamber located at NIOSH was used to collect the welding fume particles. Results Our results show that hydroxyl radicals (.OH) were generated from reactions with H2O2 and after exposure to cells. Catalase reduced the generation of .OH from exposed cells indicating the involvement of H2O2. The welding fume suspension also showed the ability to cause lipid peroxidation, effect O2 consumption, induce H2O2 generation in cells, and cause DNA damage. Conclusion Increase in oxidative damage observed in the cellular exposures correlated well with .OH generation in size and type of welding fumes, indicating the influence of metal type and transition state on radical production as well as associated damage. Our results demonstrate that both types of welding fumes are able to generate ROS and ROS-related damage over a range of particle sizes; however, the stainless steel fumes consistently showed a significantly higher reactivity and radical generation capacity. The chemical composition of the steel had a significant impact on the ROS generation capacity with the stainless steel containing Cr and Ni causing more damage than the mild steel. Our results suggest that welding fumes may cause acute lung injury. Since type of fume generated, particle size, and elapsed time after generation of the welding exposure are significant factors in radical generation and particle deposition these factors should be considered when developing protective strategies. PMID:21047424

Proposed method for determining the thickness of glass in solar collector panels

NASA Technical Reports Server (NTRS)

Moore, D. M.

1980-01-01

An analytical method was developed for determining the minimum thickness for simply supported, rectangular glass plates subjected to uniform normal pressure environmental loads such as wind, earthquake, snow, and deadweight. The method consists of comparing an analytical prediction of the stress in the glass panel to a glass breakage stress determined from fracture mechanics considerations. Based on extensive analysis using the nonlinear finite element structural analysis program ARGUS, design curves for the structural analysis of simply supported rectangular plates were developed. These curves yield the center deflection, center stress and corner stress as a function of a dimensionless parameter describing the load intensity. A method of estimating the glass breakage stress as a function of a specified failure rate, degree of glass temper, design life, load duration time, and panel size is also presented.

Development of digital rectangular phantoms for quality controls of medical primary monitors in RIS-PACS systems

NASA Astrophysics Data System (ADS)

Mattacchioni, A.; Cristianini, M.; Lo Bosco, A.

2013-03-01

The purpose of this paper is to project digital rectangular phantoms, Di.Recta Multipurpose Phantoms (Di.Recta MP) for quality controls of primary high resolution medical monitors. The first approach for the monitors quality evaluation is represented by AAPM tests using multipurpose TG-18- CQ phantoms. The TG18-QC patterns are available in two sizes: 1024x1024 and 2048x2048 and the use of these phantoms requires a correct monitor setup. The study demonstrates that this type of phantoms is suitable for CRT monitors with adequate settings procedures. In the second step LCD monitors are analysed. Different types of primary monitors are included in a range between 2 and 5 Mp. The difference between the resolution of monitors and phantoms does not allow a complete analysis of the entire system, just moving phantoms in different positions. Of course, the analysis of images in the peripheral regions of medical monitors can not be neglected, especially because of the possible legal implications. A simpler analysis of these areas can be done through the use of rectangular phantoms in place of square ones. Furthermore, because of different technology, also different analysis patches are necessary for these types of monitors. Therefore, there are proposed digital rectangular phantoms, Di.Recta MP, compatible with the spatial resolution of most of commercial monitors. These phantoms are designed to simulate typical radiological conditions to determine the presence of significant defects using appropriate patches such as luminance, contrast, noise patterns. Finally a preliminary study of dedicate Di.Recta MP are proposed for LED monitors.

A Analysis of the Low Frequency Sound Field in Non-Rectangular Enclosures Using the Finite Element Method.

NASA Astrophysics Data System (ADS)

Geddes, Earl Russell

The details of the low frequency sound field for a rectangular room can be studied by the use of an established analytic technique--separation of variables. The solution is straightforward and the results are well-known. A non -rectangular room has boundary conditions which are not separable and therefore other solution techniques must be used. This study shows that the finite element method can be adapted for use in the study of sound fields in arbitrary shaped enclosures. The finite element acoustics problem is formulated and the modification of a standard program, which is necessary for solving acoustic field problems, is examined. The solution of the semi-non-rectangular room problem (one where the floor and ceiling remain parallel) is carried out by a combined finite element/separation of variables approach. The solution results are used to construct the Green's function for the low frequency sound field in five rooms (or data cases): (1) a rectangular (Louden) room; (2) The smallest wall of the Louden room canted 20 degrees from normal; (3) The largest wall of the Louden room canted 20 degrees from normal; (4) both the largest and the smallest walls are canted 20 degrees; and (5) a five-sided room variation of Case 4. Case 1, the rectangular room was calculated using both the finite element method and the separation of variables technique. The results for the two methods are compared in order to access the accuracy of the finite element method models. The modal damping coefficient are calculated and the results examined. The statistics of the source and receiver average normalized RMS P('2) responses in the 80 Hz, 100 Hz, and 125 Hz one-third octave bands are developed. The receiver averaged pressure response is developed to determine the effect of the source locations on the response. Twelve source locations are examined and the results tabulated for comparison. The effect of a finite sized source is looked at briefly. Finally, the standard deviation of the spatial pressure response is studied. The results for this characteristic show that it not significantly different in any of the rooms. The conclusions of the study are that only the frequency variations of the pressure response are affected by a room's shape. Further, in general, the simplest modification of a rectangular room (i.e., changing the angle of only one of the smallest walls), produces the most pronounced decrease of the pressure response variations in the low frequency region.

High-speed fiber laser cutting of thick stainless steel for dismantling tasks

NASA Astrophysics Data System (ADS)

Shin, Jae Sung; Oh, Seong Yong; Park, Hyunmin; Chung, Chin-Man; Seon, Sangwoo; Kim, Taek-Soo; Lee, Lim; Choi, Byung-Seon; Moon, Jei-Kwon

2017-09-01

A high-speed fiber laser cutting technology of thick steels for dismantling tasks was achieved using a 6-kW fiber laser system. At first, a new cutting head for efficient cutting of thick steels was developed, which was composed by a collimator with a focal length of 160 mm and mirror-type focusing objects with a long focal length of 600 mm. The long focal length of the focusing object made it possible for the beam size to be small through the thick cutting material and the cutting efficiency was expected to increase compared with the short focal length. In addition, folding the beam facilitated the compact cutting head with a size of 160 mm (width) × 80 mm (height) × 640 mm (length) and a weight of 6.9 kg. In the cutting experiment, the laser beam was delivered to the cutting head by a 25-m long process fiber with a core diameter of 100 μm. The cutting performances were studied against the thicknesses of stainless steel plates. A maximum cutting speed of 72 mm/min was obtained for the 60-mm thick stainless steel plate cutting and the cut specimen showed an excellent kerf shape and a narrow kerf width. To the best of our knowledge, this cutting speed was higher than other previously reported results when cutting with a 6-kW laser power.

Mechanical and histological analysis of bone-pedicle screw interface in vivo: titanium versus stainless steel.

PubMed

Sun, C; Huang, G; Christensen, F B; Dalstra, M; Overgaard, S; Bünger, C

1999-05-01

To investigate the differences in bone interface between titanium and stainless steel pedicle screws in the lumbar spine. Eighteen adult mini-pigs that underwent total laminectomy, posterolateral spinal fusion (L4-L5) were randomly selected to receive stainless steel (9) or titanium pedicle screw devices (9). In both groups, the devices were CCD (Sofamore Danek) type with the same size and shape. The postoperative observation time was 3 months. Screws from L4 were harvested along their long axis of pedicle for histomorphometric study. Bone-screw interface and bone volume from thread were examined using linear intercept techniques. Mechanical testing (torsional test and pull-out test) was performed on the screws from L5. The titanium screw group had a significantly higher maximum torque (P < 0.05) and angle related stiffness (P < 0.05) measured by torsional test. In the pull-out tests, no differences were found between the two groups in relation to the maximum load, stiffness and energy to failure. Direct bone contact with the screw in percentage was 29.4% for stainless steel and 43.8% for titanium (P < 0.05). No differences in the bone purchase between the vertebral body part and pedicle part were found. Pedicle screws made of titanium have a better bone-screw interface binding than screws made of stainless steel. Torsional tests are more informative for bone-screw interface study. Pull-out tests seem less valuable when comparing bone purchase of screws made from different materials.

Development of Nanofluids as Lubricant to Study Friction and Wear Behavior of Stainless Steels

NASA Astrophysics Data System (ADS)

Sahoo, Rashmi Ranjan; Bhattacharjee, Santu; Das, Tuhin

A number of nanofluids have been prepared to study the effect of lubrication properties of nanofluids on stainless steels taking Kaolin and Boron Nitride (BN) as the lubricant particles and Sodium Dodecyl Sulfate (SDS), Cetyl Trimethyl Ammonium Bromide (CTAB), Sodium Hexa Meta Phosphate (SHMP) as dispersants in the same liquid medium i.e. water. A pin on disc tribometer is being used to access the tribological behaviour of the prepared nanofluids. The particle size of these particle dispersions are examined with a nanoparticle size analyzer. It has been found that the use of dispersants significantly control the particle size and tribological behavior of the nanofluids as for Boron Nitride particle with Sodium Dodecyl Sulfate (SDS) as dispersant has got a very low value of coefficient of friction being equal to 0.142 while without dispersant the value is 0.498. Similarly, in case of Kaolin water with SDS as dispersant the value of coefficient of friction obtained is 0.161 and without dispersant it is 0.333. Sodium Dodecyl Sulfate (SDS) as dispersant has resulted a very low coefficient of friction compared to other dispersants tested even though it doesn’t always assure a least particle size. The role of SDS in yielding the lowest friction has pursued significant attention for further investigation.

Spheroidization by Plasma Processing and Characterization of Stainless Steel Powder for 3D Printing

NASA Astrophysics Data System (ADS)

Ji, Lina; Wang, Changzhen; Wu, Wenjie; Tan, Chao; Wang, Guoyu; Duan, Xuan-Ming

2017-10-01

Stainless steel 316L (SS 316L) powder was spheroidized by plasma processing to improve its suitability for powder 3D printing. The obtained spheroidized (sphero) powder was characterized in terms of its crystalline phases, elemental composition, morphology, particle size and distribution, light absorption, and flow properties. The elemental composition of the sphero powder met the Chinese standard for SS 316L except for its Si content. The volume fraction of ferrite increased after plasma processing. Furthermore, plasma processing was shown to not only reduce the mean size of the particles in the size range of 10 to 100 μm but also generate particles in the size range of 0.1 to 10 μm. The smaller particles filled the voids among larger particles, increasing the powder density. The light absorption was also increased owing to enhanced internal reflection. Although the basic flow energy decreased after plasma processing, the flow function (FF) value was smaller for the sphero powder, indicating a lower flowability of the sphero powder. However, the density of SS 316L pieces printed with commercial and sphero powders was 98.76 pct and 98.16 pct of the SS 316L bulk density, respectively, indicating the suitability of the sphero powder for 3D printing despite an FF below 10.

76 FR 9547 - Light-Walled Rectangular Pipe and Tube From Mexico; Final Results of Antidumping Duty...

Federal Register 2010, 2011, 2012, 2013, 2014

2011-02-18

... DEPARTMENT OF COMMERCE International Trade Administration [A-201-836] Light-Walled Rectangular... preliminary results of the administrative review of the antidumping duty order on light-walled rectangular... light-walled rectangular pipe and tube from Mexico. See Light-Walled Rectangular Pipe and Tube From...

A thermocouple thermode for small animals

NASA Technical Reports Server (NTRS)

Williams, B. A.

1972-01-01

Thermode composed of two thin-walled stainless steel hypodermic needles and cooper-constantan thermocouple or small thermistor to indicate temperature at point of perfusion is used to measure brain temperature in animals. Because of relatively small size of thermode, structural damage to brain is minimized.

Receive Mode Analysis and Design of Microstrip Reflectarrays

NASA Technical Reports Server (NTRS)

Rengarajan, Sembiam

2011-01-01

Traditionally microstrip or printed reflectarrays are designed using the transmit mode technique. In this method, the size of each printed element is chosen so as to provide the required value of the reflection phase such that a collimated beam results along a given direction. The reflection phase of each printed element is approximated using an infinite array model. The infinite array model is an excellent engineering approximation for a large microstrip array since the size or orientation of elements exhibits a slow spatial variation. In this model, the reflection phase from a given printed element is approximated by that of an infinite array of elements of the same size and orientation when illuminated by a local plane wave. Thus the reflection phase is a function of the size (or orientation) of the element, the elevation and azimuth angles of incidence of a local plane wave, and polarization. Typically, one computes the reflection phase of the infinite array as a function of several parameters such as size/orientation, elevation and azimuth angles of incidence, and in some cases for vertical and horizontal polarization. The design requires the selection of the size/orientation of the printed element to realize the required phase by interpolating or curve fitting all the computed data. This is a substantially complicated problem, especially in applications requiring a computationally intensive commercial code to determine the reflection phase. In dual polarization applications requiring rectangular patches, one needs to determine the reflection phase as a function of five parameters (dimensions of the rectangular patch, elevation and azimuth angles of incidence, and polarization). This is an extremely complex problem. The new method employs the reciprocity principle and reaction concept, two well-known concepts in electromagnetics to derive the receive mode analysis and design techniques. In the "receive mode design" technique, the reflection phase is computed for a plane wave incident on the reflectarray from the direction of the beam peak. In antenna applications with a single collimated beam, this method is extremely simple since all printed elements see the same angles of incidence. Thus the number of parameters is reduced by two when compared to the transmit mode design. The reflection phase computation as a function of five parameters in the rectangular patch array discussed previously is reduced to a computational problem with three parameters in the receive mode. Furthermore, if the beam peak is in the broadside direction, the receive mode design is polarization independent and the reflection phase computation is a function of two parameters only. For a square patch array, it is a function of the size, one parameter only, thus making it extremely simple.

Wider-Opening Dewar Flasks for Cryogenic Storage

NASA Technical Reports Server (NTRS)

Ruemmele, Warren P.; Manry, John; Stafford, Kristin; Bue, Grant; Krejci, John; Evernden, Bent

2010-01-01

Dewar flasks have been proposed as containers for relatively long-term (25 days) storage of perishable scientific samples or other perishable objects at a temperature of 175 C. The refrigeration would be maintained through slow boiling of liquid nitrogen (LN2). For the purposes of the application for which these containers were proposed, (1) the neck openings of commercial off-the-shelf (COTS) Dewar flasks are too small for most NASA samples; (2) the round shapes of the COTS containers give rise to unacceptably low efficiency of packing in rectangular cargo compartments; and (3) the COTS containers include metal structures that are too thermally conductive, such that they cannot, without exceeding size and weight limits, hold enough LN2 for the required long-term-storage. In comparison with COTS Dewar flasks, the proposed containers would be rectangular, yet would satisfy the long-term storage requirement without exceeding size and weight limits; would have larger neck openings; and would have greater sample volumes, leading to a packing efficiency of about double the sample volume as a fraction of total volume. The proposed containers would be made partly of aerospace- type composite materials and would include vacuum walls, multilayer insulation, and aerogel insulation.

Reduction of the discretization stencil of direct forcing immersed boundary methods on rectangular cells: The ghost node shifting method

NASA Astrophysics Data System (ADS)

Picot, Joris; Glockner, Stéphane

2018-07-01

We present an analytical study of discretization stencils for the Poisson problem and the incompressible Navier-Stokes problem when used with some direct forcing immersed boundary methods. This study uses, but is not limited to, second-order discretization and Ghost-Cell Finite-Difference methods. We show that the stencil size increases with the aspect ratio of rectangular cells, which is undesirable as it breaks assumptions of some linear system solvers. To circumvent this drawback, a modification of the Ghost-Cell Finite-Difference methods is proposed to reduce the size of the discretization stencil to the one observed for square cells, i.e. with an aspect ratio equal to one. Numerical results validate this proposed method in terms of accuracy and convergence, for the Poisson problem and both Dirichlet and Neumann boundary conditions. An improvement on error levels is also observed. In addition, we show that the application of the chosen Ghost-Cell Finite-Difference methods to the Navier-Stokes problem, discretized by a pressure-correction method, requires an additional interpolation step. This extra step is implemented and validated through well known test cases of the Navier-Stokes equations.

Factors that affect micro-tooling features created by direct printing approach

NASA Astrophysics Data System (ADS)

Kumbhani, Mayur N.

Current market required faster pace production of smaller, better, and improved products in shorter amount of time. Traditional high-rate manufacturing process such as hot embossing, injection molding, compression molding, etc. use tooling to replicate feature on a products. Miniaturization of many product in the field of biomedical, electronics, optical, and microfluidic is occurring on a daily bases. There is a constant need to produce cheaper, and faster tooling, which can be utilize by existing manufacturing processes. Traditionally, in order to manufacture micron size tooling features processes such as micro-machining, Electrical Discharge Machining (EDM), etc. are utilized. Due to a higher difficulty to produce smaller size features, and longer production cycle time, various additive manufacturing approaches are proposed, e.g. selective laser sintering (SLS), inkjet printing (3DP), fused deposition modeling (FDM), etc. were proposed. Most of these approaches can produce net shaped products from different materials such as metal, ceramic, or polymers. Several attempts were made to produce tooling features using additive manufacturing approaches. Most of these produced tooling were not cost effective, and the life cycle of these tooling was reported short. In this research, a method to produce tooling features using direct printing approach, where highly filled feedstock was dispensed on a substrate. This research evaluated different natural binders, such as guar gum, xanthan gum, and sodium carboxymethyl cellulose (NaCMC) and their combinations were evaluated. The best binder combination was then use to evaluate effect of different metal (316L stainless steel (3 mum), 316 stainless steel (45 mum), and 304 stainless steel (45 mum)) particle size on feature quality. Finally, the effect of direct printing process variables such as dispensing tip internal diameter (500 mum, and 333 mum) at different printing speeds were evaluated.

A Model of Post-Traumatic Epilepsy After Penetrating Brain Injuries: Effect of Lesion Size and Metal Fragments

PubMed Central

Kendirli, M. Tansel; Rose, Dominique T.; Bertram, Edward H.

2014-01-01

Objective Penetrating brain injury (PBI) has the highest risk for inducing post-traumatic epilepsy and retained foreign materials such as bullet fragments carry the greatest risk. This study examines the potential contribution of copper, a major component of bullets, to the development of epilepsy following PBI. Methods Anesthetized adult male rats received a penetrating injury from the dorsal cortex to the ventral hippocampus from a high speed small bit drill. In one group of animals, copper wire was inserted into the lesion. Control animals had only the lesion or the lesion plus stainless steel wire (biologically inert foreign body). From 6 to up to 11 months following the injury the rats were monitored intermittently for the development of epilepsy with video-EEG. A separate set of animals was examined for possible acute seizures in the week following the injury. Results 22 of the 23 animals with copper wire developed chronic epilepsy compared to 3 of the 20 control rats (lesion and lesion with stainless steel). Copper was associated with more extensive injury. The control rats with epilepsy had larger lesions. In the acute injury group, there was no difference in the incidence of seizures (83% lesion plus stainless steel, 70% lesion plus copper). Conclusions Copper increases the risk for epilepsy and may increase damage over time, but there were no differences between the groups in the incidence of acute post-injury seizures. Lesion size may contribute to epilepsy development in lesion only animals. Copper maybe an independent risk factor for the development of epilepsy and possible secondary injury, but lesion size also contributes to the development of epilepsy. The consequences of prolonged exposure of the brain to copper observed in these animals may have clinical implications that require further evaluation. PMID:25470332

Natural Crack Sizing Based on Eddy Current Image and Electromagnetic Field Analyses

DOE Office of Scientific and Technical Information (OSTI.GOV)

Endo, H.; Uchimoto, T.; Takagi, T.

2006-03-06

An eddy current testing (ECT) system with multi-coil type probes is applied to size up cracks fabricated on austenite stainless plates. We have developed muti-channel ECT system to produce data as digital images. The probes consist of transmit-receive type sensors as elements to classify crack directions, working as two scan direction modes simultaneously. Template matching applied to the ECT images determines regions of interest in sizing up cracks. Finite element based inversion sizes up the crack depth from the measured ECT signal. The present paper demonstrates this approach for fatigue crack and stress corrosion cracking.

Mechanical Properties and Microstructure of Dissimilar Friction Stir Welds of 11Cr-Ferritic/Martensitic Steel to 316 Stainless Steel

NASA Astrophysics Data System (ADS)

Sato, Yutaka S.; Kokawa, Hiroyuki; Fujii, Hiromichi T.; Yano, Yasuhide; Sekio, Yoshihiro

2015-12-01

Dissimilar joints between ferritic and austenitic steels are of interest for selected applications in next generation fast reactors. In this study, dissimilar friction-stir welding of an 11 pct Cr ferritic/martensitic steel to a 316 austenitic stainless steel was attempted and the mechanical properties and microstructure of the resulting welds were examined. Friction-stir welding produces a stir zone without macroscopic weld-defects, but the two dissimilar steels are not intermixed. The two dissimilar steels are interleaved along a sharp zigzagging interface in the stir zone. During small-sized tensile testing of the stir zone, this sharp interface did not act as a fracture site. Furthermore, the microstructure of the stir zone was refined in both the ferritic/martensitic steel and the 316 stainless steel resulting in improved mechanical properties over the adjacent base material regions. This study demonstrates that friction-stir welding can produce welds between dissimilar steels that contain no macroscopic weld-defects and display suitable mechanical properties.

Bio-Environment-Induced Degradation and Failure of Internal Fixation Implants.

PubMed

Zhou, Yan; Perkins, Luke A; Wang, Guodong; Zhou, Dongsheng; Liang, Hong

2015-10-15

Internal fixations provide fast healing but their failure remains problematic to patients. Here, we report an experimental study in failure of three typical cases of metals: a bent intramedullary stainless steel nail, a broken exterior pure Ti plate, and a broken intramedullary stainless steel nail. Characterization of the bent nail indicates that those metals are vulnerable to corrosion with the evidence of increased surface roughness and embrittlement. Depredated surface of the Ti plate resulted debris particles in the surrounding tissue of 15.2 ± 6.5 μm in size. Nanoparticles were observed in transmission electron microscope. The electron diffraction pattern of the debris indicates a combination of nanocrystalline and amorphous phases. The failure mode of the broken nail made of stainless steel was found to be fatigue initiated from the surface. This study clearly shows the biological-attack induced surface degradation resulting in debris and fatigue. Future design and selection of implant materials should consider such factors for improvement.

Three-Dimensional Morphological and Chemical Evolution of Nanoporous Stainless Steel by Liquid Metal Dealloying [3D Morphological and Chemical Evolution of Nanoporous Stainless Steel by Liquid Metal Dealloying

DOE PAGES

Zhao, Chonghang; Wada, Takeshi; De Andrade, Vincent; ...

2017-09-04

Nanoporous materials, especially those fabricated by liquid metal dealloying processes, possess great potential in a wide range of applications due to their high surface area, bicontinuous structure with both open pores for transport and solid phase for conductivity or support, and low material cost. Here, we used X-ray nanotomography and X-ray fluorescence microscopy to reveal the three-dimensional (3D) morphology and elemental distribution within materials. Focusing on nanoporous stainless steel, we evaluated the 3D morphology of the dealloying front and established a quantitative processing-structure-property relationship at a later stage of dealloying. The morphological differences of samples created by liquid metal dealloyingmore » and aqueous dealloying methods were also discussed. Here, we concluded that it is particularly important to consider the dealloying, coarsening, and densification mechanisms in influencing the performance-determining, critical 3D parameters, such as tortuosity, pore size, porosity, curvature, and interfacial shape.« less

Three-Dimensional Morphological and Chemical Evolution of Nanoporous Stainless Steel by Liquid Metal Dealloying [3D Morphological and Chemical Evolution of Nanoporous Stainless Steel by Liquid Metal Dealloying

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhao, Chonghang; Wada, Takeshi; De Andrade, Vincent

Nanoporous materials, especially those fabricated by liquid metal dealloying processes, possess great potential in a wide range of applications due to their high surface area, bicontinuous structure with both open pores for transport and solid phase for conductivity or support, and low material cost. Here, we used X-ray nanotomography and X-ray fluorescence microscopy to reveal the three-dimensional (3D) morphology and elemental distribution within materials. Focusing on nanoporous stainless steel, we evaluated the 3D morphology of the dealloying front and established a quantitative processing-structure-property relationship at a later stage of dealloying. The morphological differences of samples created by liquid metal dealloyingmore » and aqueous dealloying methods were also discussed. Here, we concluded that it is particularly important to consider the dealloying, coarsening, and densification mechanisms in influencing the performance-determining, critical 3D parameters, such as tortuosity, pore size, porosity, curvature, and interfacial shape.« less

Joining characteristics of titanium-based orthodontic wires connected by laser and electrical welding methods.

PubMed

Matsunaga, Junko; Watanabe, Ikuya; Nakao, Noriko; Watanabe, Etsuko; Elshahawy, Waleed; Yoshida, Noriaki

2015-01-01

This study investigated the possibility of electrical and laser welding to connect titanium-based alloy (beta-titanium and nickel-titanium) wires and stainless-steel or cobalt-chromium alloy wires for fabrication of combination arch-wires. Four kinds of straight orthodontic rectangular wires (0.017 × 0.025 inch) were used: stainless-steel (S-S), cobalt-chromium (Co-Cr), beta-titanium alloy (β-Ti), and nickel-titanium (Ni-Ti). Homogeneous and heterogeneous end-to-end joints (15 mm long each) were made by electrical welding and laser welding. Non-welded wires (30 mm long) were also used as a control. Maximum loads at fracture (N) and elongation (%) were measured by conducting tensile test. The data (n = 10) were statistically analyzed using analysis of variance/Tukey test (P < 0.05).The S-S/S-S and Co-Cr/Co-Cr specimens showed significantly higher values of the maximum load (ML) at fracture and elongation (EL) than those of the Ni-Ti/Ni-Ti and β-Ti/β-Ti specimens for electrical welding and those of the S-S/S-S and Co-Cr/Co-Cr specimens welded by laser. On the other hand, the laser-welded Ni-Ti/Ni-Ti and β-Ti/β-Ti specimens exhibited higher values of the ML and EL compared to those of the corresponding specimens welded by electrical method. In the heterogeneously welded combinations, the electrically welded Ni-Ti/S-S, β-Ti/S-S and β-Ti/Co-Cr specimens showed significantly (P < 0.05) higher ML and EL than those of the corresponding specimens welded by laser. Electrical welding exhibited the higher values of maximum load at fracture and elongation for heterogeneously welded combinations than laser-welding.

Finite element analysis of slot wall deformation in stainless steel and titanium orthodontic brackets during simulated palatal root torque.

PubMed

Magesh, Varadaraju; Harikrishnan, Pandurangan; Kingsly Jeba Singh, Devadhas

2018-04-01

Torque applied on anterior teeth is vital for root positioning and stability. The aim of this study was to evaluate the detailed slot wall deformation in stainless steel (SS) and titanium (Ti) edgewise brackets during palatal root torque using finite element analysis. A finite element model was developed from a maxillary central incisor SS bracket (0.022 in). The generated torque values from an SS rectangular archwire (0.019 × 0.025 in) while twisting from 5° to 40° were obtained experimentally by a spine tester, and the calculated torque force was applied in the bracket slot. The deformations of the slot walls in both SS and Ti brackets were measured at various locations. There were gradual increases in the deformations of both bracket slot walls from the bottom to top locations. In the SS bracket slot for the 40° twist, the deformations were 9.28, 36.8, and 44.8 μm in the bottom, middle, and top slot wall locations, respectively. Similarly, in the Ti bracket slot for the 40° twist, the deformations were 39.2, 62.4, and 76.2 μm in the bottom, middle, and top slot wall locations, respectively. The elastic limits were reached at 28° for SS and at 37° for Ti. Both SS and Ti bracket slots underwent deformation during torque application. There are variations in the deformations at different locations in the slot walls and between the materials. Copyright © 2017 American Association of Orthodontists. Published by Elsevier Inc. All rights reserved.

Synthesis of transparent BaTiO3 nanoparticle/polymer composite film using DC field

NASA Astrophysics Data System (ADS)

Kondo, Yusuke; Okumura, Yasuko; Oi, Chifumi; Sakamoto, Wataru; Yogo, Toshinobu

2008-10-01

Transparent BaTiO3 nanoparticle/polymer composite films were synthesized from titanium-organic film and barium ion in aqueous solution under direct current (DC) field. Titanium-organic precursor was synthesized from titanium isopropoxide, acetylacetone and methacrylate derivative. The UV treatment was effective to increase the anti-solubility of the titanium-organic film during DC processing. BaTiO3 nanoparticles were crystallized in the precursor films on stainless substrates without high temperature process, as low as 40°C. The crystallite size of BaTiO3 increased with increasing reaction temperature from 40 to 50 °C at 3.0 V/cm. BaTiO3 nanoparticles also grew in size with increasing reaction time from 15 min to 45 min at 3.0 V/cm and 50 °C. Transparent BaTiO3 nanoparticle/polymer films were synthesized on stainless substrates at 3.0 V/cm and 50°C for 45 min.

M23C6 carbides and Cr2N nitrides in aged duplex stainless steel: A SEM, TEM and FIB tomography investigation.

PubMed

Maetz, J-Y; Douillard, T; Cazottes, S; Verdu, C; Kléber, X

2016-05-01

The precipitation evolution during ageing of a 2101 lean duplex stainless steel was investigated, revealing that the precipitate type and morphology depends on the nature of the grain boundary. Triangular M23C6 carbides precipitate only at γ/δ interfaces and rod-like Cr2N nitrides precipitate at both γ/δ and δ/δ interfaces. After 15min of ageing, the M23C6 size no longer evolves, whereas that of the Cr2N continues to evolve. For Cr2N, the morphology is maintained at γ/δ interfaces, whereas percolation occurs to form a continuous layer at δ/δ interfaces. By combining 2D and 3D characterisation at the nanoscale using transmission electron microscopy (TEM) and focused ion beam (FIB) tomography, a complete description of the precipitation evolution was obtained, including the composition, crystallographic structure, orientation relationship with the matrix phases, location, morphology, size and volume fraction. Copyright © 2016 Elsevier Ltd. All rights reserved.

Corrosion behavior of ferritic stainless steel with 15wt% chromium for the automobile exhaust system

NASA Astrophysics Data System (ADS)

Li, Hua-bing; Jiang, Zhou-hua; Feng, Hao; Zhu, Hong-chun; Sun, Bin-han; Li, Zhen

2013-09-01

The effect of chloride ion concentration, pH value, and grain size on the pitting corrosion resistance of a new ferritic stainless steel with 15wt% Cr was investigated using the anodic polarization method. The semiconducting properties of passive films with different chloride ion concentrations were performed using capacitance measurement and Mott-Schottky analysis methods. The aging precipitation and intergranular corrosion behavior were evaluated at 400-900°C. It is found that the pitting potential decreases when the grain size increases. With the increase in chloride ion concentration, the doping density and the flat-bland potential increase but the thickness of the space charge layer decreases. The pitting corrosion resistance increases rapidly with the decrease in pH value. Precipitants is identified as Nb(C,N) and NbC, rather than Cr-carbide. The intergranular corrosion is attributed to the synergistic effects of Nb(C,N) and NbC precipitates and Cr segregation adjacent to the precipitates.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tanaka, T.; Kameyama, M.; Urabe, Y.

At present, cast duplex stainless steel has been used for the primary coolant piping of PWRs in Japan and joints of dissimilar material have been applied for welding to reactor vessels and steam generators. For the primary coolant piping of the next APWR plants, application of low alloy steel that results in designing main loops with the same material is being studied. It means that there is no need to weld low alloy steel with stainless steel and that makes it possible to reduce the welding length. Attenuation of Ultra Sonic Wave Intensity is lower for low alloy steel thanmore » for stainless steel and they have advantageous inspection characteristics. In addition to that, the thermal expansion rate is smaller for low alloy steel than for stainless steel. In consideration of the above features of low alloy steel, the overall reliability of primary coolant piping is expected to be improved. Therefore, for the evaluation of crack stability of low alloy steel piping to be applied for primary loops, elastic-plastic future mechanics analysis was performed by means of a three-dimensioned FEM. The evaluation results for the low alloy steel pipings show that cracks will not grow into unstable fractures under maximum design load conditions, even when such a circumferential crack is assumed to be 6 times the size of the wall thickness.« less

Study on Pot Forming of Induction Heater Type Rice Cookers by Forging Cast Process

NASA Astrophysics Data System (ADS)

Ohnishi, Masayuki; Yamaguchi, Mitsugi; Ohashi, Osamu

This paper describes a study result on pot fabrication by the forging cast process of stainless steel with aluminum. Rice cooked with the new bowl-shaped pot for the induction heater type rice cookers is better tasting than rice cooked with the conventional cylindrical one, due to the achievement of better heat conduction and convection. The conventional pot is made of the clad sheet, consisting of stainless steel and aluminum. However, it is rather difficult to form a bowl shape from the clad sheet, primarily due to the problem of a material spring back. The fabrication of a new type of a pot was made possible by means of the adoption of a forging cast process instead of the clad sheet. In this process, iron powder is inserted between stainless steel and aluminum in order to alleviate the large difference on the coefficient of expansion between each material. It was made clear that the application of two kinds of iron particle, namely 10 μm size powder on the stainless steel side and 44 μm on the aluminum side, enables the joints to become strong enough. The joint strength of the new pot by this fabrication process was confirmed by the tests of the shear strength and the fatigue tests together with the stress analysis.

Localized corrosion behaviour in simulated human body fluids of commercial Ni-Ti orthodontic wires.

PubMed

Rondelli, G; Vicentini, B

1999-04-01

The corrosion performances in simulated human body fluids of commercial equiatomic Ni-Ti orthodontic wires having various shape and size and produced by different manufacturers were evaluated; for comparison purposes wires made of stainless steel and of cobalt-based alloy were also examined. Potentiodynamic tests in artificial saliva at 40 degrees C indicated a sufficient pitting resistance for the Ni-Ti wires, similar to that of cobalt-based alloy wire; the stainless steel wire, instead, exhibited low pitting potential. Potentiodynamic tests at 40 degrees C in isotonic saline solution (0.9% NaCl) showed, for Ni-Ti and stainless steel wires, pitting potential values in the range approximately 200-400 mV and approximately 350 mV versus SCE, respectively: consequently, according to literature data (Hoar TP, Mears DC. Proc Roy Soc A 1996;294:486-510), these materials should be considered potentially susceptible to pitting; only the cobalt-based alloy should be immune from pitting. The localized corrosion potentials determined in the same environment by the ASTM F746 test (approximately 0-200 mV and 130 mV versus SCE for Ni-Ti and stainless steel, respectively) pointed out that for these materials an even higher risk of localized corrosion. Slight differences in localized corrosion behaviour among the various Ni-Ti wires were detected.

Electromagnetic scattering and radiation from microstrip patch antennas and spirals residing in a cavity

NASA Technical Reports Server (NTRS)

Volakis, J. L.; Gong, J.; Alexanian, A.; Woo, A.

1992-01-01

A new hybrid method is presented for the analysis of the scattering and radiation by conformal antennas and arrays comprised of circular or rectangular elements. In addition, calculations for cavity-backed spiral antennas are given. The method employs a finite element formulation within the cavity and the boundary integral (exact boundary condition) for terminating the mesh. By virtue of the finite element discretization, the method has no restrictions on the geometry and composition of the cavity or its termination. Furthermore, because of the convolutional nature of the boundary integral and the inherent sparseness of the finite element matrix, the storage requirement is kept very low at O(n). These unique features of the method have already been exploited in other scattering applications and have permitted the analysis of large-size structures with remarkable efficiency. In this report, we describe the method's formulation and implementation for circular and rectangular patch antennas in different superstrate and substrate configurations which may also include the presence of lumped loads and resistive sheets/cards. Also, various modelling approaches are investigated and implemented for characterizing a variety of feed structures to permit the computation of the input impedance and radiation pattern. Many computational examples for rectangular and circular patch configurations are presented which demonstrate the method's versatility, modeling capability and accuracy.

Simplified Method for the Characterization of Rectangular Straw Bales (RSB) Thermal Conductivity

NASA Astrophysics Data System (ADS)

Conti, Leonardo; Goli, Giacomo; Monti, Massimo; Pellegrini, Paolo; Rossi, Giuseppe; Barbari, Matteo

2017-10-01

This research aims to design and implement tools and methods focused at the assessment of the thermal properties of full size Rectangular Straw Bales (RSB) of various nature and origin, because their thermal behaviour is one of the key topics in market development of sustainable building materials. As a first approach a method based on a Hot-Box in agreement with the ASTM C1363 - 11 standard was adopted. This method was found to be difficult for the accurate measurement of energy flows. Instead, a method based on a constant energy input was developed. With this approach the thermal conductivity of a Rectangular Straw-Bale (RSB λ) can be determined by knowing the thermal conductivity of the materials used to build the chamber and the internal and external temperature of the samples and of the chamber. A measurement a metering chamber was built and placed inside a climate chamber, maintained at constant temperature. A known quantity of energy was introduced inside the metering chamber. A series of thermopiles detects the temperature of the internal and external surfaces of the metering chamber and of the specimens allowing to calculate the thermal conductivity of RSB in its natural shape. Different cereal samples were tested. The values were found consistent with those published in scientific literature.

On the Lateral Static Stability of Low-Aspect-Ratio Rectangular Wings

NASA Astrophysics Data System (ADS)

Linehan, Thomas; Mohseni, Kamran

2017-11-01

Low-aspect-ratio rectangular wings experience a reduction in lateral static stability at angles of attack distinct from that of lift stall. Stereoscopic digital particle image velocimetry is used to elucidate the flow physics behind this trend. Rectangular wings of AR = 0.75, 1, 1.5, 3 were tested at side-slip angles β = -10° and 0° with angle of attack varied in the range α =10° -40° . In side-slip, the leading-edge separation region emerges on the leeward wing where leading-edge flow reattachment is highly intermittent due to vortex shedding. The tip vortex downwash of the AR < 1.5 wings is sufficient to restrict the shedding of leading-edge vorticity, enabling sustained lift from the leading-edge separation region to high angles of attack. The windward tip vortex grows in size with increasing angle of attack, occupying an increasingly larger percentage of the windward wing. At high angles of attack pre-lift stall, the windward tip vortex lifts off the wing, resulting in separated flow underneath it. The downwash of the AR = 3 wing is insufficient to reattach the leading-edge flow at high incidence. The flow stalls on the leeward wing with stalled flow expanding upstream toward the windward wing with increasing angle of attack.

Numerical investigation on forced convection in rectangular cross section micro-channels with nanofluids

NASA Astrophysics Data System (ADS)

Buonomo, B.; Cirillo, L.; Manca, O.; Nardini, S.; Tamburrino, S.

2017-01-01

In this paper a numerical investigation on laminar forced convection flow of a water-Al2O3 nanofluid in a rectangular microchannel is accomplished. A constant and uniform heat flux on the external surfaces has been applied and a single-phase model approach has been employed. The analysis has been performed in steady state regime for particle size in nanofluids equal to 38 nm. The CFD commercial code Fluent has been employed in order to solve the 3-D numerical model. The geometrical configuration under consideration consists in a duct with a rectangular shaped crossing area. A steady laminar flow and different nanoparticle volume fractions have been considered. The base fluid is water and nanoparticles are made up of alumina (Al2O3). The length the edge and height of the duct are 0.030 m, 1.7 x10-7 and 1.1 x10-7 m, respectively. Results are presented in terms of temperature and velocity distributions, surface shear stress and heat transfer convective coefficient, Nusselt number and required pumping power profiles. Comparison with results related to the fluid dynamic and thermal behaviors are carried out in order to evaluate the enhancement due to the presence of nanoparticles in terms of volumetric concentration.

Effect of baffle size and orientation on lateral sloshing of partially filled containers: a numerical study

NASA Astrophysics Data System (ADS)

Ali, Sajid; Kamran, Muhammad Ali; Khan, Sikandar

2017-11-01

The fluid sloshing in partially filled road tankers has significantly increased the number of road accidents for the last few decades. Significant research is needed to investigate and to come up with optimum baffles designs that can help to increase the rollover stability of the partially filled tankers. In this investigation, a detailed analysis of the anti-slosh effectiveness of different baffle configurations is presented. This investigation extends the already available studies in the literature by introducing new modified rectangular tank's shapes that correspond to maximum rollover stability as compared to the already available standard tank designs. The various baffles configurations that are analysed in this study are horizontal, vertical, vertical-horizontal and diagonal. In the current study, numerical investigations are performed for rectangular, elliptical and circular tank shapes. Lateral sloshing, caused by constant radius turn manoeuvre, was simulated numerically using the volume-of-fluid method, and effect of the different baffle configurations was analysed. The effect of tank fill levels on sloshing measured in terms of horizontal force and pressure moments is also reported for with and without baffles configurations. Vertical baffles were the most effective at reducing sloshing in modified rectangular tanks, whereas a combination of horizontal and vertical baffles gave better results for the circular and elliptical tanks geometries.

An analytical method to calculate equivalent fields to irregular symmetric and asymmetric photon fields.

PubMed

Tahmasebi Birgani, Mohamad J; Chegeni, Nahid; Zabihzadeh, Mansoor; Hamzian, Nima

2014-01-01

Equivalent field is frequently used for central axis depth-dose calculations of rectangular- and irregular-shaped photon beams. As most of the proposed models to calculate the equivalent square field are dosimetry based, a simple physical-based method to calculate the equivalent square field size was used as the basis of this study. The table of the sides of the equivalent square or rectangular fields was constructed and then compared with the well-known tables by BJR and Venselaar, et al. with the average relative error percentage of 2.5 ± 2.5% and 1.5 ± 1.5%, respectively. To evaluate the accuracy of this method, the percentage depth doses (PDDs) were measured for some special irregular symmetric and asymmetric treatment fields and their equivalent squares for Siemens Primus Plus linear accelerator for both energies, 6 and 18MV. The mean relative differences of PDDs measurement for these fields and their equivalent square was approximately 1% or less. As a result, this method can be employed to calculate equivalent field not only for rectangular fields but also for any irregular symmetric or asymmetric field. © 2013 American Association of Medical Dosimetrists Published by American Association of Medical Dosimetrists All rights reserved.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ranjan, Devesh

Diffusion bonded heat exchangers are the leading candidates for the sCO 2 Brayton cycles in next generation nuclear power plants. Commercially available diffusion bonded heat exchangers utilize set of continuous semi-circular zigzag micro channels to increase the heat transfer area and enhance heat transfer through increased turbulence production. Such heat exchangers can lead to excessive pressure drop as well as flow maldistribution in the case of poorly designed flow distribution headers. The goal of the current project is to fabricate and test potential discontinuous fin patterns for diffusion bonded heat exchangers; which can achieve desired thermal performance at lower pressuremore » drops. Prototypic discontinuous offset rectangular and Airfoil fin surface geometries were chemically etched on to 316 stainless steel plate and sealed against an un-etched flat pate using O-ring seal emulating diffusion bonded heat exchangers. Thermal-hydraulic performance of these prototypic discontinuous fin geometries was experimentally evaluated and compared to the existing data for the continuous zigzag channels. The data generated from this project will serve as the database for future testing and validation of numerical models.« less

Dynamic recrystallization in friction surfaced austenitic stainless steel coatings

DOE Office of Scientific and Technical Information (OSTI.GOV)

Puli, Ramesh, E-mail: rameshpuli2000@gmail.com; Janaki Ram, G.D.

2012-12-15

Friction surfacing involves complex thermo-mechanical phenomena. In this study, the nature of dynamic recrystallization in friction surfaced austenitic stainless steel AISI 316L coatings was investigated using electron backscattered diffraction and transmission electron microscopy. The results show that the alloy 316L undergoes discontinuous dynamic recrystallization under conditions of moderate Zener-Hollomon parameter during friction surfacing. - Highlights: Black-Right-Pointing-Pointer Dynamic recrystallization in alloy 316L friction surfaced coatings is examined. Black-Right-Pointing-Pointer Friction surfacing leads to discontinuous dynamic recrystallization in alloy 316L. Black-Right-Pointing-Pointer Strain rates in friction surfacing exceed 400 s{sup -1}. Black-Right-Pointing-Pointer Estimated grain size matches well with experimental observations in 316L coatings.

Rectangularization of the survival curve in The Netherlands, 1950-1992.

PubMed

Nusselder, W J; Mackenbach, J P

1996-12-01

In this article we determine whether rectangularization of the survival curve occurred in the Netherlands in the period 1950-1992. Rectangularization is defined as a trend toward a more rectangular shape of the survival curve due to increased survival and concentration of deaths around the mean age at death. We distinguish between absolute and relative rectangularization, depending on whether an increase in life expectancy is accompanied by concentration of deaths into a smaller age interval or into a smaller proportion of total life expectancy. We used measures of variability based on Keyfitz' H and the standard deviation, both life table-based. Our results show that absolute and relative rectangularization of the entire survival curve occurred in both sexes and over the complete period (except for the years 1955-1959 and 1965-1969 in men). At older ages, results differ between sexes, periods, and an absolute versus a relative definition of rectangularization. Above age 60 1/2, relative rectangularization occurred in women over the complete period and in men since 1975-1979 only, whereas absolute rectangularization occurred in both sexes since the period of 1980-1984. The implications of the recent rectangularization at older ages for achieving compression of morbidity are discussed.

Performance of terahertz metamaterials as high-sensitivity sensor

NASA Astrophysics Data System (ADS)

He, Yanan; Zhang, Bo; Shen, Jingling

2017-09-01

A high-sensitivity sensor based on the resonant transmission characteristics of terahertz (THz) metamaterials was investigated, with the proposal and fabrication of rectangular bar arrays of THz metamaterials exhibiting a period of 180 μm on a 25 μm thick flexible polyimide. Varying the size of the metamaterial structure revealed that the length of the rectangular unit modulated the resonant frequency, which was verified by both experiment and simulation. The sensing characteristics upon varying the surrounding media in the sample were tested by simulation and experiment. Changing the surrounding medium from that of air to that of alcohol or oil produced resonant frequency redshifts of 80 GHz or 150 GHz, respectively, which indicates that the sensor possessed a high sensitivity of 667 GHz per unit of refractive index. Finally, the influence of the sample substrate thickness on the sensor sensitivity was investigated by simulation. It may be a reference for future sensor design.

The investigation of ferromagnetic resonance linewidth in Ni{sub 80}Fe{sub 20} films with submicron rectangular elements

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, D.; School of Physical Science and Information Engineering, Liaocheng University, Liaocheng, 252059; Yue, J. J.

Patterned magnetic films with nano-scaled dots exhibit some special magnetic properties. In this paper, we investigate the in-plane shape anisotropy and the magnetization dynamic damping in permalloy (Ni{sub 80}Fe{sub 20}) arrays of submicron rectangular elements using ferromagnetic resonance (FMR). The FMR linewidth exhibits a dependence on the element size, and mainly comes from the contribution of the intrinsic damping. Also the contribution of two-magnon scattering plays an important role and is reduced with increasing aspect ratio. The damping coefficient decreases from 0.0129 to 0.0118 with the element length increasing from 300 nm to 1200 nm, and the theoretical calculation suggestsmore » that the change of damping results from the longitudinal and transverse interlayer spin current due to the spatially inhomogeneous magnetization dynamics.« less

Design of Quad-Band Terahertz Metamaterial Absorber Using a Perforated Rectangular Resonator for Sensing Applications.

PubMed

Xie, Qin; Dong, Guangxi; Wang, Ben-Xin; Huang, Wei-Qing

2018-05-08

Quad-band terahertz absorber with single-sized metamaterial design formed by a perforated rectangular resonator on a gold substrate with a dielectric gap in between is investigated. The designed metamaterial structure enables four absorption peaks, of which the first three peaks have large absorption coefficient while the last peak possesses a high Q (quality factor) value of 98.33. The underlying physical mechanisms of these peaks are explored; it is found that their near-field distributions are different. Moreover, the figure of merit (FOM) of the last absorption peak can reach 101.67, which is much higher than that of the first three absorption modes and even absorption bands of other works operated in the terahertz frequency. The designed device with multiple-band absorption and high FOM could provide numerous potential applications in terahertz technology-related fields.

Volumetric flame synthesis of well-defined molybdenum oxide nanocrystals.

PubMed

Merchan-Merchan, Wilson; Saveliev, Alexei V; Desai, Milind

2009-11-25

Well-defined faceted inorganic Mo oxide nanocrystals are synthesized in the gas phase using a solid-fed-precursor flame synthesis method. The solid crystals have rectangular cross-section with characteristic size of 10-20 nm and with lengths ranging from 50 nm to a few hundred nanometres. A 1 mm diameter high purity Mo probe introduced in the oxygen-rich part of the flame serves as the material source. A combination of the strong temperature gradient and varying chemical species concentrations within the flame volume provides the ideal conditions for the rapid and direct formation of these unique nanocrystals. Oxidation and evaporation of MoO3 in the oxygen-rich zone are followed by reduction to MoO2 in the lower temperature, more fuel-rich zone. The MoO3 vapours formed are pushed in the direction of the gas flow and transformed into mature well-defined convex polyhedron nanocrystals bounded with six faces resembling rectangular parallelepipeds.

Experimental and modeling study of Newtonian and non-Newtonian fluid flow in pore network micromodels.

PubMed

Perrin, Christian L; Tardy, Philippe M J; Sorbie, Ken S; Crawshaw, John C

2006-03-15

The in situ rheology of polymeric solutions has been studied experimentally in etched silicon micromodels which are idealizations of porous media. The rectangular channels in these etched networks have dimensions typical of pore sizes in sandstone rocks. Pressure drop/flow rate relations have been measured for water and non-Newtonian hydrolyzed-polyacrylamide (HPAM) solutions in both individual straight rectangular capillaries and in networks of such capillaries. Results from these experiments have been analyzed using pore-scale network modeling incorporating the non-Newtonian fluid mechanics of a Carreau fluid. Quantitative agreement is seen between the experiments and the network calculations in the Newtonian and shear-thinning flow regions demonstrating that the 'shift factor,'alpha, can be calculated a priori. Shear-thickening behavior was observed at higher flow rates in the micromodel experiments as a result of elastic effects becoming important and this remains to be incorporated in the network model.

Design of Quad-Band Terahertz Metamaterial Absorber Using a Perforated Rectangular Resonator for Sensing Applications

NASA Astrophysics Data System (ADS)

Xie, Qin; Dong, Guangxi; Wang, Ben-Xin; Huang, Wei-Qing

2018-05-01

Quad-band terahertz absorber with single-sized metamaterial design formed by a perforated rectangular resonator on a gold substrate with a dielectric gap in between is investigated. The designed metamaterial structure enables four absorption peaks, of which the first three peaks have large absorption coefficient while the last peak possesses a high Q (quality factor) value of 98.33. The underlying physical mechanisms of these peaks are explored; it is found that their near-field distributions are different. Moreover, the figure of merit (FOM) of the last absorption peak can reach 101.67, which is much higher than that of the first three absorption modes and even absorption bands of other works operated in the terahertz frequency. The designed device with multiple-band absorption and high FOM could provide numerous potential applications in terahertz technology-related fields.

An exploratory drilling exhaustion sequence plot program

USGS Publications Warehouse

Schuenemeyer, J.H.; Drew, L.J.

1977-01-01

The exhaustion sequence plot program computes the conditional area of influence for wells in a specified rectangular region with respect to a fixed-size deposit. The deposit is represented by an ellipse whose size is chosen by the user. The area of influence may be displayed on computer printer plots consisting of a maximum of 10,000 grid points. At each point, a symbol is presented that indicates the probability of that point being exhausted by nearby wells with respect to a fixed-size ellipse. This output gives a pictorial view of the manner in which oil fields are exhausted. In addition, the exhaustion data may be used to estimate the number of deposits remaining in a basin. ?? 1977.

Coherent and partially coherent dark hollow beams with rectangular symmetry and paraxial propagation properties

NASA Astrophysics Data System (ADS)

Cai, Yangjian; Zhang, Lei

2006-07-01

A theoretical model is proposed to describe coherent dark hollow beams (DHBs) with rectangular symmetry. The electric field of a coherent rectangular DHB is expressed as a superposition of a series of the electric field of a finite series of fundamental Gaussian beams. Analytical propagation formulas for a coherent rectangular DHB passing through paraxial optical systems are derived in a tensor form. Furthermore, for the more general case, we propose a theoretical model to describe a partially coherent rectangular DHB. Analytical propagation formulas for a partially coherent rectangular DHB passing through paraxial optical systems are derived. The beam propagation factor (M2 factor) for both coherent and partially coherent rectangular DHBs are studied. Numerical examples are given by using the derived formulas. Our models and method provide an effective way to describe and treat the propagation of coherent and partially coherent rectangular DHBs.

Compact waveguide circular polarizer

DOEpatents

Tantawi, Sami G.

2016-08-16

A multi-port waveguide is provided having a rectangular waveguide that includes a Y-shape structure with first top arm having a first rectangular waveguide port, a second top arm with second rectangular waveguide port, and a base arm with a third rectangular waveguide port for supporting a TE.sub.10 mode and a TE.sub.20 mode, where the end of the third rectangular waveguide port includes rounded edges that are parallel to a z-axis of the waveguide, a circular waveguide having a circular waveguide port for supporting a left hand and a right hand circular polarization TE.sub.11 mode and is coupled to a base arm broad wall, and a matching feature disposed on the base arm broad wall opposite of the circular waveguide for terminating the third rectangular waveguide port, where the first rectangular waveguide port, the second rectangular waveguide port and the circular waveguide port are capable of supporting 4-modes of operation.

Bioaccessibility, bioavailability and toxicity of commercially relevant iron- and chromium-based particles: in vitro studies with an inhalation perspective.

PubMed

Hedberg, Yolanda; Gustafsson, Johanna; Karlsson, Hanna L; Möller, Lennart; Odnevall Wallinder, Inger

2010-09-03

Production of ferrochromium alloys (FeCr), master alloys for stainless steel manufacture, involves casting and crushing processes where particles inevitably become airborne and potentially inhaled. The aim of this study was to assess potential health hazards induced by inhalation of different well-characterized iron- and chromium-based particles, i.e. ferrochromium (FeCr), ferrosiliconchromium (FeSiCr), stainless steel (316L), iron (Fe), chromium (Cr), and chromium(III)oxide (Cr2O3), in different size fractions using in vitro methods. This was done by assessing the extent and speciation of released metals in synthetic biological medium and by analyzing particle reactivity and toxicity towards cultured human lung cells (A549). The amount of released metals normalized to the particle surface area increased with decreasing particle size for all alloy particles, whereas the opposite situation was valid for particles of the pure metals. These effects were evident in artificial lysosomal fluid (ALF) of pH 4.5 containing complexing agents, but not in neutral or weakly alkaline biological media. Chromium, iron and nickel were released to very low extent from all alloy particles, and from particles of Cr due to the presence of a Cr(III)-rich protective surface oxide. Released elements were neither proportional to the bulk nor to the surface composition after the investigated 168 hours of exposure. Due to a surface oxide with less protective properties, significantly more iron was released from pure iron particles compared with the alloys. Cr was predominantly released as Cr(III) from all particles investigated and was strongly complexed by organic species of ALF. Cr2O3 particles showed hemolytic activity, but none of the alloy particles did. Fine-sized particles of stainless steel caused however DNA damage, measured with the comet assay after 4 h exposure. None of the particles revealed any significant cytotoxicity in terms of cell death after 24 h exposure. It is evident that particle and alloy characteristics such as particle size and surface composition are important aspects to consider when assessing particle toxicity and metal release from alloy particles compared to pure metal particles. Generated results clearly elucidate that neither the low released concentrations of metals primarily as a result of protective and poorly soluble surface oxides, nor non-bioavailable chromium complexes, nor the particles themselves of occupational relevance induced significant acute toxic response, with exception of DNA damage from stainless steel.

Bioaccessibility, bioavailability and toxicity of commercially relevant iron- and chromium-based particles: in vitro studies with an inhalation perspective

PubMed Central

2010-01-01

Background Production of ferrochromium alloys (FeCr), master alloys for stainless steel manufacture, involves casting and crushing processes where particles inevitably become airborne and potentially inhaled. The aim of this study was to assess potential health hazards induced by inhalation of different well-characterized iron- and chromium-based particles, i.e. ferrochromium (FeCr), ferrosiliconchromium (FeSiCr), stainless steel (316L), iron (Fe), chromium (Cr), and chromium(III)oxide (Cr2O3), in different size fractions using in vitro methods. This was done by assessing the extent and speciation of released metals in synthetic biological medium and by analyzing particle reactivity and toxicity towards cultured human lung cells (A549). Results The amount of released metals normalized to the particle surface area increased with decreasing particle size for all alloy particles, whereas the opposite situation was valid for particles of the pure metals. These effects were evident in artificial lysosomal fluid (ALF) of pH 4.5 containing complexing agents, but not in neutral or weakly alkaline biological media. Chromium, iron and nickel were released to very low extent from all alloy particles, and from particles of Cr due to the presence of a Cr(III)-rich protective surface oxide. Released elements were neither proportional to the bulk nor to the surface composition after the investigated 168 hours of exposure. Due to a surface oxide with less protective properties, significantly more iron was released from pure iron particles compared with the alloys. Cr was predominantly released as Cr(III) from all particles investigated and was strongly complexed by organic species of ALF. Cr2O3 particles showed hemolytic activity, but none of the alloy particles did. Fine-sized particles of stainless steel caused however DNA damage, measured with the comet assay after 4 h exposure. None of the particles revealed any significant cytotoxicity in terms of cell death after 24 h exposure. Conclusion It is evident that particle and alloy characteristics such as particle size and surface composition are important aspects to consider when assessing particle toxicity and metal release from alloy particles compared to pure metal particles. Generated results clearly elucidate that neither the low released concentrations of metals primarily as a result of protective and poorly soluble surface oxides, nor non-bioavailable chromium complexes, nor the particles themselves of occupational relevance induced significant acute toxic response, with exception of DNA damage from stainless steel. PMID:20815895

Heating times for round and rectangular cross sections of wood in steam

Treesearch

William T. Simpson

2001-01-01

Heat sterilization of wood in various forms is currently receiving attention as a means of killing insects or pathogens to prevent their transfer from one region of the world to another in trade. One concern is the amount of time required to heat wood of various cross-sectional sizes and configurations to a temperature that will kill the insects or pathogens....

Laser surface alloying of FeCoCrAlNi high-entropy alloy on 304 stainless steel to enhance corrosion and cavitation erosion resistance

NASA Astrophysics Data System (ADS)

Zhang, S.; Wu, C. L.; Zhang, C. H.; Guan, M.; Tan, J. Z.

2016-10-01

FeCoCrAlNi high-entropy alloy coating was synthesized with premixed high-purity Co, Cr, Al and Ni powders on 304 stainless steel by laser surface alloying, aiming at improving corrosion and cavitation erosion resistance. Phase constituents, microstructure and microhardness were investigated using XRD, SEM, and microhardness tester, respectively. The cavitation erosion and electrochemical corrosion behavior of FeCoCrAlNi coating in 3.5% NaCl solution were also evaluated using an ultrasonic vibrator and potentiodynamic polarization measurement. Experimental results showed that with appropriate laser processing parameters, FeCoCrAlNi coating with good metallurgical bonding to the substrate could be achieved. FeCoCrAlNi coating was composed of a single BCC solid solution. The formation of simple solid solutions in HEAs was the combined effect of mixing entropy (ΔSmix), mixing enthalpy (ΔHmix), atom-size difference (δ) and valence electron concentration (VEC), and the effect of ΔSmix was much larger than that of the other factors. The microhardness of the FeCoCrAlNi coating was ~3 times that of the 304 stainless steel. Both the corrosion and cavitation erosion resistance of the coating were improved. The cavitation erosion resistance for FeCoCrAlNi HEA coating was ~7.6 times that of 304 stainless steel. The corrosion resistance was also improved as reflected by a reduction in the current density of one order of magnitude as compared with 304 stainless steel.

Electromagnetic characterization of photo-definable ferrite loaded polymers and their applications in micro-rectangular coaxial phase shifters

NASA Astrophysics Data System (ADS)

Sholiyi, Olusegun Samuel

As the demand for smaller size, lighter weight, lower loss and cost of communications transmit and receive (T/R) modules increases, there is an urgent need to focus investigation to the major subsystem or components that can improve these parameters. Phase shifters contribute greatly to the cost of T/R modules, and thus this research investigation examines a new way to reduce the weight and cost by miniaturizing the phaser design. Characterization of hexaferrite powders compatible with the sequential multilayer micro-fabrication technology and numerical simulations of a novel rectangular micro-coaxial phase shifter are investigated. This effort aims to integrate ferrite material into a rectangular micro-coaxial waveguide at Ka-band using electromagnetic finite element numerical tools. The proposed technique exploits rectangular coaxial waveguide with a symmetrically placed inner signal conductor inside an outer conductor connected to the ground. Strontium ferrite-SU8 composite is used as an anisotropic material of choice in the modelled design. Numerical modeling is employed using High Frequency Structure Simulator, HFSS, a 3-D full wave electromagnetic solver for analyzing the performance of the device. Two model structures were designed for reciprocal and non-reciprocal applications. The first model (Model A) produced a tunable phase shift of almost 60 degrees /cm across 0 to 400 kA/m applied field and at 1800 Gauss. In model B, a non-reciprocal phase shift performance of 20 degrees /cm from a reference phase of 24 degrees at 0 A/m was realized at the same saturation magnetization. A return loss better than 20 dB and an insertion loss less than 1.5 dB were obtained for both models.

A porous stainless steel membrane system for extraterrestrial crop production

NASA Technical Reports Server (NTRS)

Koontz, H. V.; Prince, R. P.; Berry, W. L.; Knott, W. M. (Principal Investigator)

1990-01-01

A system was developed in which nutrient flow to plant roots is controlled by a thin (0.98 or 1.18 mm) porous (0.2 or 0.5 microns) stainless steel sheet membrane. The flow of nutrient solution through the membrane is controlled by adjusting the relative negative pressure on the nutrient solution side of the membrane. Thus, the nutrient solution is contained by the membrane and cannot escape from the compartment even under microgravity conditions if the appropriate pressure gradient across the membrane is maintained. Plant roots grow directly on the top surface of the membrane and pull the nutrient solution through this membrane interface. The volume of nutrient solution required by this system for plant growth is relatively small, since the plenum, which contains the nutrient solution in contact with the membrane, needs only to be of sufficient size to provide for uniform flow to all parts of the membrane. Solution not passing through the membrane to the root zone is recirculated through a reservoir where pH and nutrient levels are controlled. The size of the solution reservoir depends on the sophistication of the replenishment system. The roots on the surface of the membrane are covered with a polyethylene film (white on top, black on bottom) to maintain a high relative humidity and also limit light to prevent algal growth. Seeds are sown directly on the stainless steel membrane under the holes in the polyethylene film that allow a pathway for the shoots.

The Effects of In-Office Reconditioning on the Slot Dimensions and Static Frictional Resistance of Stainless Steel Brackets

PubMed Central

Nellore, Chaitanya; Karnati, Praveen Kumar Reddy; Thalapaneni, Ashok Kumar; Myla, Vijay Bhaskar; Ramyasree, Konda; Prasad, Mandava

2016-01-01

Introduction Orthodontists are commonly faced with the decision of what to do with loose brackets, and with inaccurately located brackets that need repositioning during treatment. One solution is to recycle the brackets. The potential effects of reconditioning a bracket are dependent upon many factors which may result in physical changes like alteration in slot tolerance, which may influence sliding mechanics by affecting frictional resistance. Aim To study and compare the dimensional changes in the bracket slot width and depth in reconditioned brackets from unused brackets under scanning electronic microscope and to study and compare any consequent effects on the static frictional resistance of stainless steel brackets after reconditioning and in unused brackets. Materials and Methods Dentarum manufactured 90 stainless steel central incisors edgewise brackets of size 0.22 X 0.030″ inch and 0° tip and 0°angulation were taken. 60 samples for measuring frictional resistance and 30 samples for measuring slot dimensions. Ortho organizers manufactured stainless steel arch wires 0.019 X 0.025″ straight lengths 60 in number were considered for measuring static frictional resistance. Results The mean slot width and depth of new brackets were 0.0251″ and 0.0471″, which exceeded the manufacturers reported nominal size of 0.022″ X 0.030″, by 0.003″ and 0.017″. The reconditioned brackets demonstrated a further increase in mean slot width and depth to 0.028″ and 0.0518″ that is by 0.0035″ and 0.0047″ which is statistically significant (p=0.001, 0.002). The mean static frictional forces of the reconditioned brackets was nearly similar to that of new brackets that is 0.3167N for reconditioned brackets and 0.2613 N for new brackets. Conclusion Although the reconditioning process results in physical changes to bracket structure this does not appear to result in significant effect on ex-vivo static frictional resistance. PMID:26894182

The Effects of In-Office Reconditioning on the Slot Dimensions and Static Frictional Resistance of Stainless Steel Brackets.

PubMed

Iluru, Rohini; Nellore, Chaitanya; Karnati, Praveen Kumar Reddy; Thalapaneni, Ashok Kumar; Myla, Vijay Bhaskar; Ramyasree, Konda; Prasad, Mandava

2016-01-01

Orthodontists are commonly faced with the decision of what to do with loose brackets, and with inaccurately located brackets that need repositioning during treatment. One solution is to recycle the brackets. The potential effects of reconditioning a bracket are dependent upon many factors which may result in physical changes like alteration in slot tolerance, which may influence sliding mechanics by affecting frictional resistance. To study and compare the dimensional changes in the bracket slot width and depth in reconditioned brackets from unused brackets under scanning electronic microscope and to study and compare any consequent effects on the static frictional resistance of stainless steel brackets after reconditioning and in unused brackets. Dentarum manufactured 90 stainless steel central incisors edgewise brackets of size 0.22 X 0.030″ inch and 0° tip and 0°angulation were taken. 60 samples for measuring frictional resistance and 30 samples for measuring slot dimensions. Ortho organizers manufactured stainless steel arch wires 0.019 X 0.025″ straight lengths 60 in number were considered for measuring static frictional resistance. The mean slot width and depth of new brackets were 0.0251″ and 0.0471″, which exceeded the manufacturers reported nominal size of 0.022″ X 0.030″, by 0.003″ and 0.017″. The reconditioned brackets demonstrated a further increase in mean slot width and depth to 0.028″ and 0.0518″ that is by 0.0035″ and 0.0047″ which is statistically significant (p=0.001, 0.002). The mean static frictional forces of the reconditioned brackets was nearly similar to that of new brackets that is 0.3167N for reconditioned brackets and 0.2613 N for new brackets. Although the reconditioning process results in physical changes to bracket structure this does not appear to result in significant effect on ex-vivo static frictional resistance.

Effect of Stress Relief Annealing on Microstructure & Mechanical Properties of Welded Joints Between Low Alloy Carbon Steel and Stainless Steel

NASA Astrophysics Data System (ADS)

Nivas, R.; Das, G.; Das, S. K.; Mahato, B.; Kumar, S.; Sivaprasad, K.; Singh, P. K.; Ghosh, M.

2017-01-01

Two types of welded joints were prepared using low alloy carbon steel and austenitic stainless steel as base materials. In one variety, buttering material and weld metal were Inconel 82. In another type, buttering material and weld metal were Inconel 182. In case of Inconel 82, method of welding was GTAW. For Inconel 182, welding was done by SMAW technique. For one set of each joints after buttering, stress relief annealing was done at 923 K (650 °C) for 90 minutes before further joining with weld metal. Microstructural investigation and sub-size in situ tensile testing in scanning electron microscope were carried out for buttered-welded and buttered-stress relieved-welded specimens. Adjacent to fusion boundary, heat-affected zone of low alloy steel consisted of ferrite-pearlite phase combination. Immediately after fusion boundary in low alloy steel side, there was increase in matrix grain size. Same trend was observed in the region of austenitic stainless steel that was close to fusion boundary between weld metal-stainless steel. Close to interface between low alloy steel-buttering material, the region contained martensite, Type-I boundary and Type-II boundary. Peak hardness was obtained close to fusion boundary between low alloy steel and buttering material. In this respect, a minimum hardness was observed within buttering material. The peak hardness was shifted toward buttering material after stress relief annealing. During tensile testing no deformation occurred within low alloy steel and failure was completely through buttering material. Crack initiated near fusion boundary between low alloy steel-buttering material for welded specimens and the same shifted away from fusion boundary for stress relieved annealed specimens. This observation was at par with the characteristics of microhardness profile. In as welded condition, joints fabricated with Inconel 82 exhibited superior bond strength than the weld produced with Inconel 182. Stress relief annealing reduced the strength of transition joints and the reduction was maximum for specimen welded with Inconel 82.

Nonlocal Poisson-Fermi double-layer models: Effects of nonuniform ion sizes on double-layer structure

NASA Astrophysics Data System (ADS)

Xie, Dexuan; Jiang, Yi

2018-05-01

This paper reports a nonuniform ionic size nonlocal Poisson-Fermi double-layer model (nuNPF) and a uniform ionic size nonlocal Poisson-Fermi double-layer model (uNPF) for an electrolyte mixture of multiple ionic species, variable voltages on electrodes, and variable induced charges on boundary segments. The finite element solvers of nuNPF and uNPF are developed and applied to typical double-layer tests defined on a rectangular box, a hollow sphere, and a hollow rectangle with a charged post. Numerical results show that nuNPF can significantly improve the quality of the ionic concentrations and electric fields generated from uNPF, implying that the effect of nonuniform ion sizes is a key consideration in modeling the double-layer structure.

Development of concept for concurrent biocide generation and water system purification. [with application to Skylab water tanks

NASA Technical Reports Server (NTRS)

1974-01-01

An attempt was made to construct an electrochemical system, using iodine, for water purification in Skylab. Data cover measurements of iodine production rates, effect of electrode size and geometry on iodine production rates, and feasibility of using stainless steels as reference electrodes.

Differences in shoaling behavior in two species of freshwater fish (Danio rerio and Hyphessobrycon herbertaxelrodi).

PubMed

Gimeno, Elisabet; Quera, Vicenç; Beltran, Francesc S; Dolado, Ruth

2016-11-01

Fish can gain significant adaptive advantages when living in a group and they exhibit a wide variety of types of collective motion. The scientific literature recognizes 2 main patterns: shoals (aggregations of individuals that remain close to each other), and schools (aggregations of aligned, or polarized, individuals). We analyzed the collective motion of 2 social fish species, zebrafish (Danio rerio) and black neon tetra (Hyphessobrycon herbertaxelrodi), and compared their patterns of movement and the effect of group size and environmental constraints such as water column height and tank geometry on the collective motion of both species. We recorded the movement of groups of fish (n = 10 and n = 20) using 2 tank geometries: a rectangular shape and a rectangular shape with rounded corners; and we also manipulated the water column height (15 and 25 cm). We extracted the individual fish trajectories and calculated indices of cohesion, coordination, group density and group shape. The results showed that the 2 species had different types of collective motion: the zebrafish's global motion matched that of a shoal, while the black neon tetra's motion matched that of a school. Indirect evidence indicated that the 2 species tended to occupy the vertical space differently while swimming in a group. Finally, we found that tank geometry did not affect group polarization, whereas group size had an effect on black neon tetra density, which was higher in small group sizes than in large ones. (PsycINFO Database Record (c) 2016 APA, all rights reserved).

Gas tungsten arc welding and friction stir welding of ultrafine grained AISI 304L stainless steel: Microstructural and mechanical behavior characterization

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sabooni, S., E-mail: s.sabooni@ma.iut.ac.ir; Karimzadeh, F.; Enayati, M.H.

In the present study, an ultrafine grained (UFG) AISI 304L stainless steel with the average grain size of 650 nm was successfully welded by both gas tungsten arc welding (GTAW) and friction stir welding (FSW). GTAW was applied without any filler metal. FSW was also performed at a constant rotational speed of 630 rpm and different welding speeds from 20 to 80 mm/min. Microstructural characterization was carried out by High Resolution Scanning Electron Microscopy (HRSEM) with Electron Backscattered Diffraction (EBSD) and Transmission Electron Microscopy (TEM). Nanoindentation, microhardness measurements and tensile tests were also performed to study the mechanical properties ofmore » the base metal and weldments. The results showed that the solidification mode in the GTAW welded sample is FA (ferrite–austenite) type with the microstructure consisting of an austenite matrix embedded with lath type and skeletal type ferrite. The nugget zone microstructure in the FSW welded samples consisted of equiaxed dynamically recrystallized austenite grains with some amount of elongated delta ferrite. Sigma phase precipitates were formed in the region ahead the rotating tool during the heating cycle of FSW, which were finally fragmented into nanometric particles and distributed in the weld nugget. Also there is a high possibility that the existing delta ferrite in the microstructure rapidly transforms into sigma phase particles during the short thermal cycle of FSW. These suggest that high strain and deformation during FSW can promote sigma phase formation. The final austenite grain size in the nugget zone was found to decrease with increasing Zener–Hollomon parameter, which was obtained quantitatively by measuring the peak temperature, calculating the strain rate during FSW and exact examination of hot deformation activation energy by considering the actual grain size before the occurrence of dynamic recrystallization. Mechanical properties observations showed that the welding efficiency of the FSW welded sample is around 70%, which is more than 20% higher than the GTAW welded sample. - Highlights: • Microstructure and mechanical properties of UFG 304L stainless steel were studied during GTAW and FSW. • Sigma phase formation mechanism was studied during FSW of 304L stainless steel. • THERMOCALC analysis was performed to obtain possible formation temperatures for sigma phase. • Nano-mechanical twins were found in the TMAZ region.« less

Wind tunnel research concerning lateral control devices, particularly at high angles of attack VII : Handley Page tip and full-span slots with ailerons and spoilers

NASA Technical Reports Server (NTRS)

Weick, Fred E; Wenzinger, Carl J

1933-01-01

Tests were made with ordinary ailerons and different sizes of spoilers on rectangular Clark Y wing models with Handley Page tip and full span slots. The tests showed the effect of the control devices on the general performance of the wings as well as on the lateral control and lateral stability characteristics.

77 FR 29905 - Sea Turtle Conservation; Shrimp and Summer Flounder Trawling Requirements

Federal Register 2010, 2011, 2012, 2013, 2014

2012-05-21

... a bottom-opening, straight-bar grid with 2-inch bar spacing installed at an angle of 55 degrees. As...: Using \\1/4\\ inch (0.63 cm) thick and 1\\1/2\\ inch (3.8 cm) deep flat bar, and rectangular and oval pipe... currently-approved TED grids; increasing maximum mesh size on escape flaps from 1\\5/8\\ to 2 inches (4.1 to 5...

A process model for the heat-affected zone microstructure evolution in duplex stainless steel weldments: Part I. the model

NASA Astrophysics Data System (ADS)

Hemmer, H.; Grong, Ø.

1999-11-01

The present investigation is concerned with modeling of the microstructure evolution in duplex stainless steels under thermal conditions applicable to welding. The important reactions that have been modeled are the dissolution of austenite during heating, subsequent grain growth in the delta ferrite regime, and finally, the decomposition of the delta ferrite to austenite during cooling. As a starting point, a differential formulation of the underlying diffusion problem is presented, based on the internal-state variable approach. These solutions are later manipulated and expressed in terms of the Scheil integral in the cases where the evolution equation is separable or can be made separable by a simple change of variables. The models have then been applied to describe the heat-affected zone microstructure evolution during both thick-plate and thin-plate welding of three commercial duplex stainless steel grades: 2205, 2304, and 2507. The results may conveniently be presented in the form of novel process diagrams, which display contours of constant delta ferrite grain size along with information about dissolution and reprecipitation of austenite for different combinations of weld input energy and peak temperature. These diagrams are well suited for quantitative readings and illustrate, in a condensed manner, the competition between the different variables that lead to structural changes during welding of duplex stainless steels.

Irradiation response of delta ferrite in as-cast and thermally aged cast stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Zhangbo; Lo, Wei-Yang; Chen, Yiren

To enable the life extension of Light Water Reactors (LWRs) beyond 60 years, it is critical to gain adequate knowledge for making conclusive predictions to assure the integrity of duplex stainless steel reactor components, e.g. primary pressure boundary and reactor vessel internal. Microstructural changes in the ferrite of thermally aged, neutron irradiated only, and neutron irradiated after being thermally aged cast austenitic stainless steels (CASS) were investigated using atom probe tomography. The thermal aging was performed at 400 °C for 10,000 h and the irradiation was conducted in the Halden reactor at ~315 °C to 0.08 dpa (5.6 × 10more » 19 n/cm 2 E > 1 MeV). Low dose neutron irradiation at a dose rate of 5 × 10 -9 dpa/s was found to induce spinod,al decomposition in the ferrite of as-cast microstructure, and further to enhance the spinodal decomposition in the thermally aged cast alloys. Regarding the G-phase precipitates, the neutron irradiation dramatically increases the precipitate size, and alters the composition of the precipitates with increased, Mn, Ni, Si and Mo and reduced Fe and Cr contents. Lastly, The results have shown that low dose neutron irradiation can further accelerate the degradation of ferrite in a duplex stainless steel at the LWR relevant condition.« less

Irradiation response of delta ferrite in as-cast and thermally aged cast stainless steel

DOE PAGES

Li, Zhangbo; Lo, Wei-Yang; Chen, Yiren; ...

2015-08-08

To enable the life extension of Light Water Reactors (LWRs) beyond 60 years, it is critical to gain adequate knowledge for making conclusive predictions to assure the integrity of duplex stainless steel reactor components, e.g. primary pressure boundary and reactor vessel internal. Microstructural changes in the ferrite of thermally aged, neutron irradiated only, and neutron irradiated after being thermally aged cast austenitic stainless steels (CASS) were investigated using atom probe tomography. The thermal aging was performed at 400 °C for 10,000 h and the irradiation was conducted in the Halden reactor at ~315 °C to 0.08 dpa (5.6 × 10more » 19 n/cm 2 E > 1 MeV). Low dose neutron irradiation at a dose rate of 5 × 10 -9 dpa/s was found to induce spinod,al decomposition in the ferrite of as-cast microstructure, and further to enhance the spinodal decomposition in the thermally aged cast alloys. Regarding the G-phase precipitates, the neutron irradiation dramatically increases the precipitate size, and alters the composition of the precipitates with increased, Mn, Ni, Si and Mo and reduced Fe and Cr contents. Lastly, The results have shown that low dose neutron irradiation can further accelerate the degradation of ferrite in a duplex stainless steel at the LWR relevant condition.« less

A Solar Volumetric Receiver: Influence of Absorbing Cells Configuration on Device Thermal Performance

NASA Astrophysics Data System (ADS)

Yilbas, B. S.; Shuja, S. Z.

2017-01-01

Thermal performance of a solar volumetric receiver incorporating the different cell geometric configurations is investigated. Triangular, hexagonal, and rectangular absorbing cells are incorporated in the analysis. The fluid volume fraction, which is the ratio of the volume of the working fluid over the total volume of solar volumetric receiver, is introduced to assess the effect of cell size on the heat transfer rates in the receiver. In this case, reducing the fluid volume fraction corresponds to increasing cell size in the receiver. SiC is considered as the cell material, and air is used as the working fluid in the receiver. The Lambert's Beer law is incorporated to account for the solar absorption in the receiver. A finite element method is used to solve the governing equation of flow and heat transfer. It is found that the fluid volume fraction has significant effect on the flow field in the solar volumetric receiver, which also modifies thermal field in the working fluid. The triangular absorbing cell gives rise to improved effectiveness of the receiver and then follows the hexagonal and rectangular cells. The second law efficiency of the receiver remains high when hexagonal cells are used. This occurs for the fluid volume fraction ratio of 0.5.

Micron-scale pattern formation in prestressed polygonal films

NASA Astrophysics Data System (ADS)

Annabattula, R. K.; Onck, P. R.

2011-02-01

In this paper we explore the spontaneous formation of micropatterns in thin prestressed polygonal films using finite element simulations. We study films with different size, thickness, and shape, including square, rectangular, pentagonal, and hexagonal films. Patterns form when the films release the internal eigenstrain by buckling-up, after which the films bond-back to the substrate. After an initial symmetric evolution of the buckling profile, the symmetry of the deflection pattern breaks when the wavelength of wriggles near the film edges decreases. During bond back the deflection morphology converges to a fourfold, fivefold, and sixfold ridging pattern for the square, pentagonal and hexagonal films, respectively, showing a close resemblance with experimental film systems of similar size and shape. Rectangular films of large length to width ratio go through a transition in buckling shapes from the initial Euler mode, through the varicose mode into the antisymmetric telephone-cord mode. For all the film shapes, the ratio of the film height to the effective film width scales with the square root of eigenstrain and is independent of thickness. The bond-back mechanism determines the final wrinkle morphology and is governed by the eigenstrain value at the end of the buckling-up stage and the dimensionless parameter (Γ /EWeq)(Weq/t)3, relating the interface energy to the strain energy in the film.

Experimental investigation of solidification in metal foam enhanced phase change material

NASA Astrophysics Data System (ADS)

Beyne, W.; Bağci, O.; Huisseune, H.; Canière, H.; Danneels, J.; Daenens, D.; De Paepe, M.

2017-10-01

A major challenge for the use of phase change materials (PCMs) in thermal energy storage (TES) is overcoming the low thermal conductivity of PCM’s. The low conductivity gives rise to limited power during charging and discharging TES. Impregnating metal foam with PCM, however, has been found to enhance the heat transfer. On the other hand, the effect of foam parameters such as porosity, pore size and material type has remained unclear. In this paper, the effect of these foam parameters on the solidification time is investigated. Different samples of PCM-impregnated metal foam were experimentally tested and compared to one without metal foam. The samples varied with respect to choice of material, porosity and pore size. They were placed in a rectangular cavity and cooled from one side using a coolant flowing through a cold plate. The other sides of the rectangular cavity were Polymethyl Methacrylate (PM) walls exposed to ambient. The temperature on the exterior walls of the cavity was monitored as well as the coolant flow rate and its temperature. The metal foam inserts reduced the solidification times by at least 25 %. However, the difference between the best performing and worst performing metal foam is about 28 %. This shows a large potential for future research.

Rise characteristics of gas bubbles in a 2D rectangular column: VOF simulations vs experiments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Krishna, R.; Baten, J.M. van

About five centuries ago, Leonardo da Vinci described the sinuous motion of gas bubbles rising in water. The authors have attempted to simulate the rise trajectories of bubbles of 4, 5, 7, 8, 9, 12, and 20 mm in diameter rising in a 2D rectangular column filled with water. The simulations were carried out using the volume-of-fluid (VOF) technique developed by Hirt and Nichols (J. Computational Physics, 39, 201--225 (1981)). To solve the Navier-Stokes equations of motion the authors used a commercial solver, CFX 4.1c of AEA Technology, UK. They developed their own bubble-tracking algorithm to capture sinuous bubble motions.more » The 4 and 5 mm bubbles show large lateral motions observed by Da Vinci. The 7, 8 and 9 mm bubble behave like jellyfish. The 12 mm bubble flaps its wings like a bird. The extent of lateral motion of the bubbles decreases with increasing bubble size. Bubbles larger than 20 mm in size assume a spherical cap form and simulations of the rise characteristics match experiments exactly. VOF simulations are powerful tools for a priori determination of the morphology and rise characteristics of bubbles rising in a liquid. Bubble-bubble interactions are also properly modeled by the VOF technique.« less

Experimental investigation on the phenomena around the onset nucleate boiling during the impacting of a droplet on the hot surface

NASA Astrophysics Data System (ADS)

Mitrakusuma, Windy H.; Deendarlianto, Kamal, Samsul; Indarto, Nuriyadi, M.

2016-06-01

Onset of nucleate boiling of a droplet when impacted onto hot surface was investigated. Three kinds of surfaces, normal stainless steel (NSS), stainless steel with TiO2 coating (UVN), and stainless steel with TiO2 coating and radiated by ultraviolet ray were employed to examine the effect of wettability. The droplet size was 2.4 mm diameter, and dropped under different We number. The image is generated by high speed camera with the frame speed of 1000 fps. The boiling conditions are identified as natural convection, nucleate boiling, critical heat flux, transition, and film boiling. In the present report, the discussion will be focused on the beginning of nucleate boiling on the droplet. Nucleate boiling occurs when bubbles are generated. These bubbles are probably caused by nucleation on the impurities within the liquid rather than at nucleation sites on the heated surface because the bubbles appear to be in the bulk of the liquid instead of at the liquid-solid interface. In addition, the smaller the contact angle, the fastest the boiling.

Carbon molecular sieve membranes on porous composite tubular supports for high performance gas separations

DOE PAGES

Lee, Pyung -Soo; Bhave, Ramesh R.; Nam, Seung -Eun; ...

2016-01-11

Thin carbon molecular sieve membranes (<500 nm) were fabricated inside of long geometry (9 inch) of stainless steel tubes with all welded construction. Alumina intermediate layer on porous stainless steel tube support was used to reduce effective support pore size and to provide a more uniform surface roughness. Novolac phenolic resin solution was then coated on the inside of porous stainless steel tube by slip casting while their viscosities were controlled from 5 centipoises to 30 centipoises. Carbonization was carried out at 700 °C in which thermal stress was minimized and high quality carbon films were prepared. The highest separationmore » performance characteristics were obtained using 20 cP phenolic resin solutions. The fabricated CMSM showed good separation factor for He/N 2 462, CO 2/N 2 97, and O 2/N 2 15.4. As the viscosity of polymer precursor solution was reduced from 20 cP to 15 cP, gas permeance values almost doubled with somewhat lower separation factor He/N 2 156, CO 2/N 2 88, and O 2/N 2 7.7.« less

Factors Affecting Impact Toughness in Stabilized Intermediate Purity 21Cr Ferritic Stainless Steels and Their Simulated Heat-Affected Zones

NASA Astrophysics Data System (ADS)

Anttila, Severi; Alatarvas, Tuomas; Porter, David A.

2017-12-01

The correlation between simulated weld heat-affected zone microstructures and toughness parameters has been investigated in four intermediate purity 21Cr ferritic stainless steels stabilized with titanium and niobium either separately or in combination. Extensive Charpy V impact toughness testing was carried out followed by metallography including particle analysis using electron microscopy. The results confirmed that the grain size and the number density of particle clusters rich in titanium nitride and carbide with an equivalent circular diameter of 2 µm or more are statistically the most critical factors influencing the ductile-to-brittle transition temperature. Other inclusions and particle clusters, as well as grain boundary precipitates, are shown to be relatively harmless. Stabilization with niobium avoids large titanium-rich inclusions and also suppresses excessive grain growth in the heat-affected zone when reasonable heat inputs are used. Thus, in order to maximize the limited heat-affected zone impact toughness of 21Cr ferritic stainless steels containing 380 to 450 mass ppm of interstitials, the stabilization should be either titanium free or the levels of titanium and nitrogen should be moderated.

Comparative study of various pixel photodiodes for digital radiography: Junction structure, corner shape and noble window opening

NASA Astrophysics Data System (ADS)

Kang, Dong-Uk; Cho, Minsik; Lee, Dae Hee; Yoo, Hyunjun; Kim, Myung Soo; Bae, Jun Hyung; Kim, Hyoungtaek; Kim, Jongyul; Kim, Hyunduk; Cho, Gyuseong

2012-05-01

Recently, large-size 3-transistors (3-Tr) active pixel complementary metal-oxide silicon (CMOS) image sensors have been being used for medium-size digital X-ray radiography, such as dental computed tomography (CT), mammography and nondestructive testing (NDT) for consumer products. We designed and fabricated 50 µm × 50 µm 3-Tr test pixels having a pixel photodiode with various structures and shapes by using the TSMC 0.25-m standard CMOS process to compare their optical characteristics. The pixel photodiode output was continuously sampled while a test pixel was continuously illuminated by using 550-nm light at a constant intensity. The measurement was repeated 300 times for each test pixel to obtain reliable results on the mean and the variance of the pixel output at each sampling time. The sampling rate was 50 kHz, and the reset period was 200 msec. To estimate the conversion gain, we used the mean-variance method. From the measured results, the n-well/p-substrate photodiode, among 3 photodiode structures available in a standard CMOS process, showed the best performance at a low illumination equivalent to the typical X-ray signal range. The quantum efficiencies of the n+/p-well, n-well/p-substrate, and n+/p-substrate photodiodes were 18.5%, 62.1%, and 51.5%, respectively. From a comparison of pixels with rounded and rectangular corners, we found that a rounded corner structure could reduce the dark current in large-size pixels. A pixel with four rounded corners showed a reduced dark current of about 200fA compared to a pixel with four rectangular corners in our pixel sample size. Photodiodes with round p-implant openings showed about 5% higher dark current, but about 34% higher sensitivities, than the conventional photodiodes.

Multilayered nano-architecture of variable sized graphene nanosheets for enhanced supercapacitor electrode performance.

PubMed

Biswas, Sanjib; Drzal, Lawrence T

2010-08-01

The diverse physical and chemical aspects of graphene nanosheets such as particle size surface area and edge chemistry were combined to fabricate a new supercapacitor electrode architecture consisting of a highly aligned network of large-sized nanosheets as a series of current collectors within a multilayer configuration of bulk electrode. Capillary driven self-assembly of monolayers of graphene nanosheets was employed to create a flexible, multilayer, free-standing film of highly hydrophobic nanosheets over large macroscopic areas. This nanoarchitecture exhibits a high-frequency capacitative response and a nearly rectangular cyclic voltammogram at 1000 mV/s scanning rate and possesses a rapid current response, small equivalent series resistance (ESR), and fast ionic diffusion for high-power electrical double-layer capacitor (EDLC) application.

Evaluation of MR issues for the latest standard brands of orthopedic metal implants: plates and screws.

PubMed

Zou, Yue-Fen; Chu, Bin; Wang, Chuan-Bing; Hu, Zhi-Yi

2015-03-01

The study was performed to evaluate magnetic resonance (MR) issues for the latest standard brands of plates and screws used in orthopedic surgery at a 1.5-T MR system, including the safety and metallic artifacts. The plates and screws (made of titanium alloy and stainless steel materials, according to the latest standard brands) were assessed for displacement in degrees, MRI-related heating and artifacts at a 1.5-T MR system. The displacement in degrees of the plates and screws was evaluated on an angel-measurement instrument at the entrance of the MR scanner. The MRI-related heating was assessed on a swine leg fixed with a plate by using a "worst-case" pulse sequence. A rectangular water phantom was designed to evaluate metallic artifacts of a screw on different sequences (T1/T2-weighted FSE, STIR, T2-FSE fat saturation, GRE, DWI) and then artifacts were evaluated on T2-weighted FSE sequence by modifying the scanning parameters including field of view (FOV), echo train length (ETL) and bandwidth to identify the influence of parameters on metallic artifacts. 15 volunteers with internal vertebral fixation (titanium alloy materials) were scanned with MR using axial and sagittal T2-FSE, sagittal T2-FSE fat suppression and STIR with conventional and optimized parameters, respectively. Then all images were graded by two experienced radiologists having the experience of more than 7 years under double-blind studies that is neither of them knew which was conventional parameter group and optimized parameter group. The average deflection angle of titanium alloy and stainless steel implants were 4.3° and 7.7°, respectively, (less than 45°) which indicated that the magnetically induced force was less than the weight of the object. The deflection angle of the titanium alloy implants was less than the stainless steel one (t=9.69, P<0.001). The average temperature changes of titanium alloy before and after the scan was 0.48°C and stainless steel implants was 0.74°C, respectively, with the background temperature changes of 0.24°C. The water phantom test indicated that the DWI sequence produced largest artifacts, while FSE pulse sequence produced smallest artifacts. And T2-weighted FSE fat saturation sequence produced larger artifacts than STIR sequence. The influence of the scanning parameters on metallic artifacts was verified that metallic artifacts increased with longer echo train length and bigger FOV, while decreased with larger bandwidth. The interreader agreement was good or excellent for each set of images graded with Cohen's Kappa statistic. Image grading of axial and sagittal T2-FSE with optimized parameters were significantly superior to that with conventional parameters (grade, 3.3±0.5 vs 2.7±0.6, P=0.003; 3.2±0.4 vs 1.9±0.7, P=0.001) and image of STIR sequence received a better grade than T2-FSE FS sequence (grade, 3.4±0.5 vs 1.7±0.6, P<0.001). The latest standard plates and screws used in orthopedic surgery do not pose an additional hazard or risk to patients undergoing MR imaging at 1.5-T or less. Though artifacts caused by them cannot be ignored because of their relatively large size, it is possible to be minimized by choosing appropriate pulse sequences and optimizing scanning parameters, such as FSE and STIR sequence with large bandwidth, small FOV and appropriate echo train length. Copyright © 2014 Elsevier Ireland Ltd. All rights reserved.

The structural and bio-corrosion barrier performance of Mg-substituted fluorapatite coating on 316L stainless steel human body implant

NASA Astrophysics Data System (ADS)

Sharifnabi, A.; Fathi, M. H.; Eftekhari Yekta, B.; Hossainalipour, M.

2014-01-01

In this study, Mg-substituted fluorapatite coatings were deposited on medical grade AISI 316L stainless steel via sol-gel dip coating method. Phase composition, crystallite size and degree of crystallinity of the obtained coatings were evaluated by X-ray diffraction (XRD) analysis. Fourier transform infrared (FTIR) spectroscopy was also used to evaluate functional groups of the obtained coatings. The surface morphology and cross-section of the final coatings were studied using scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) spectroscopy was used to determine elemental chemical composition of the obtained coatings. In order to determine and compare the corrosion behavior of uncoated and Mg-substituted fluorapatite coated 316L stainless steel, electrochemical potentiodynamic polarization tests were performed in physiological solutions at 37 ± 1 °C. Moreover, the released metallic ions from uncoated and coated substrates were measured by inductively coupled plasma-optical emission spectrometry (ICP-OES) within 2 months of immersing in Ringer's solution at 36.5 ± 1 °C as an indication of biocompatibility. The results showed that fluoride and magnesium were successfully incorporated into apatite lattice structure and the prepared coatings were nanostructured with crystallinity of about 70%. Obtained coatings were totally crack-free and uniform and led to decrease in corrosion current densities of 316L stainless steel in physiological solutions. In addition, coated sample released much less ions such as Fe, Cr and Ni in physiological media. Therefore, it was concluded that Mg-substituted fluorapatite coatings could improve the corrosion resistance and biocompatibility of 316L stainless steel human body implants.

Advanced designs for non-imaging submillimeter-wave Winston cone concentrators

NASA Astrophysics Data System (ADS)

Nelson, A. O.; Grossman, E. N.

2014-05-01

We describe the design and simulation of several non-imaging concentrators designed to couple submillimeter wavelength radiation from free space into highly overmoded, rectangular, WR-10 waveguide. Previous designs are altered to improve the uniformity of efficiency rather than the efficiency itself. The concentrators are intended for use as adapters between instruments using overmoded WR-10 waveguide as input or output and sources propagating through free space. Previous simulation and measurement have shown that the angular response is primarily determined by the Winston cone and is well predicted by geometric optics theory while the efficiencies are primarily determined by the transition section. Additionally, previous work has shown insensitivity to polarization, orientation and beam size. Several separate concentrator designs are studied, all of which use a Winston cone (also known as a compound parabolic concentrator) with an input diameter ranging from 4 mm to 16 mm, and "throat" diameters of less than 0.5 mm to 4 mm as the initial interface. The use of various length adiabatic circular-to-rectangular transition sections is investigated, along with the effect of an additional, 25 mm waveguide section designed to model the internal waveguide of the power meter. Adapters without a transition section and a rectangular Winston cone throat aperture and double cone configurations are also studied. Adapters are analyzed in simulation for consistent efficiency across the opening aperture.

Tunable morphology synthesis of LiFePO4 nanoparticles as cathode materials for lithium ion batteries.

PubMed

Ma, Zhipeng; Shao, Guangjie; Fan, Yuqian; Wang, Guiling; Song, Jianjun; Liu, Tingting

2014-06-25

Olivine LiFePO4 with nanoplate, rectangular prism nanorod and hexagonal prism nanorod morphologies with a short b-axis were successfully synthesized by a solvothermal in glycerol and water system. The influences of solvent composition on the morphological transformation and electrochemical performances of olivine LiFePO4 are systematically investigated by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and galvanostatic charge-discharge tests. It is found that with increasing water content in solvent, the LiFePO4 nanoplates gradually transform into hexagonal prism nanorods that are similar to the thermodynamic equilibrium shape of the LiFePO4 crystal. This indicates that water plays an important role in the morphology transformation of the olivine LiFePO4. The electrochemical performances vary significantly with the particle morphology. The LiFePO4 rectangular prism nanorods (formed in a glycerol-to-water ratio of 1:1) exhibit superior electrochemical properties compared with the other morphological particles because of their moderate size and shorter Li(+) ion diffusion length along the [010] direction. The initial discharge capacity of the LiFePO4@C with a rectangular prism nanorod morphology reaches to 163.8 mAh g(-1) at 0.2 C and over 75 mAh g(-1) at the high discharging rate of 20 C, maintaining good stability at each discharging rate.

77 FR 1915 - Light-Walled Rectangular Pipe and Tube From Mexico; Final Results of Antidumping Duty...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-01-12

... DEPARTMENT OF COMMERCE International Trade Administration [A-201-836] Light-Walled Rectangular... preliminary results of the administrative review of the antidumping duty order on light-walled rectangular... period of review (POR) from August 1, 2009, through July 31, 2010. \\1\\ See Light-Walled Rectangular Pipe...

75 FR 55559 - Light-Walled Rectangular Pipe and Tube From Mexico: Preliminary Results of Antidumping Duty...

Federal Register 2010, 2011, 2012, 2013, 2014

2010-09-13

... DEPARTMENT OF COMMERCE International Trade Administration [A-201-836] Light-Walled Rectangular... administrative review of the antidumping duty order on light-walled rectangular pipe and tube (LWRPT) from Mexico... Light-Walled Rectangular Pipe and Tube from Mexico, the People's Republic of China, and the Republic of...

Eigenvalues of Rectangular Waveguide Using FEM With Hybrid Elements

NASA Technical Reports Server (NTRS)

Deshpande, Manohar D.; Hall, John M.

2002-01-01

A finite element analysis using hybrid triangular-rectangular elements is developed to estimate eigenvalues of a rectangular waveguide. Use of rectangular vector-edge finite elements in the vicinity of the PEC boundary and triangular elements in the interior region more accurately models the physical nature of the electromagnetic field, and consequently quicken the convergence.

POLLUTION PREVENTION ASSESSMENT FOR A MANUFACTURER OF STAINLESS STEEL PIPES AND FITTINGS (EPA/600/S-95/017)

EPA Science Inventory

The U.S. Environmental Protection Agency (EPA) has funded a pilot project to assist small and medium-size manufacturers who want to minimize their generation of waste but who lack the expertise to do so. Waste Minimization Assessment Centers (WMACs) were established at selected u...

Photochemical potential of forest fire smoke

Treesearch

W. Henry Benner; Paul Urone; Charles K. McMahon; Paul Ryan

1977-01-01

A stainless steel laboratory chamber to hold the entire combustion products from a small scale pine needle fire was useful for measuring the photochemical activity of pine needle fire smoke. Particle size distributions indicated that the nucleation of small numbers of submicron particles was sufficient to increase the amount of light a plume would scatter. Artificial...

Estimation of regional pulmonary deposition and exposure for fumes from SMAW and GMAW mild and stainless steel consumables.

PubMed

Hewett, P

1995-02-01

The particle size distributions and bulk fume densities for mild steel and stainless steel welding fumes generated using two welding processes (shielded metal arc welding [SMAW] and gas metal arc welding [GMAW]) were used in mathematical models to estimate regional pulmonary deposition (the fraction of each fume expected to deposit in each region of the pulmonary system) and regional pulmonary exposure (the fraction of each fume expected to penetrate to each pulmonary region and would be collected by a particle size-selective sampling device). Total lung deposition for GMAW fumes was estimated at 60% greater than that of SMAW fumes. Considering both the potential for deposition and the fume specific surface areas, it is likely that for equal exposure concentrations GMAW fumes deliver nearly three times the particle surface area to the lungs as SMAW fumes. This leads to the hypothesis that exposure to GMAW fumes constitutes a greater pulmonary hazard than equal exposure to SMAW fumes. The implications of this hypothesis regarding the design of future health studies of welders is discussed.

Fast wettability transition from hydrophilic to superhydrophobic laser-textured stainless steel surfaces under low-temperature annealing

NASA Astrophysics Data System (ADS)

Ngo, Chi-Vinh; Chun, Doo-Man

2017-07-01

Recently, the fabrication of superhydrophobic metallic surfaces by means of pulsed laser texturing has been developed. After laser texturing, samples are typically chemically coated or aged in ambient air for a relatively long time of several weeks to achieve superhydrophobicity. To accelerate the wettability transition from hydrophilicity to superhydrophobicity without the use of additional chemical treatment, a simple annealing post process has been developed. In the present work, grid patterns were first fabricated on stainless steel by a nanosecond pulsed laser, then an additional low-temperature annealing post process at 100 °C was applied. The effect of 100-500 μm step size of the textured grid upon the wettability transition time was also investigated. The proposed post process reduced the transition time from a couple of months to within several hours. All samples showed superhydrophobicity with contact angles greater than 160° and sliding angles smaller than 10° except samples with 500 μm step size, and could be applied in several potential applications such as self-cleaning and control of water adhesion.

A simple shape-free model for pore-size estimation with positron annihilation lifetime spectroscopy

NASA Astrophysics Data System (ADS)

Wada, Ken; Hyodo, Toshio

2013-06-01

Positron annihilation lifetime spectroscopy is one of the methods for estimating pore size in insulating materials. We present a shape-free model to be used conveniently for such analysis. A basic model in classical picture is modified by introducing a parameter corresponding to an effective size of the positronium (Ps). This parameter is adjusted so that its Ps-lifetime to pore-size relation merges smoothly with that of the well-established Tao-Eldrup model (with modification involving the intrinsic Ps annihilation rate) applicable to very small pores. The combined model, i.e., modified Tao-Eldrup model for smaller pores and the modified classical model for larger pores, agrees surprisingly well with the quantum-mechanics based extended Tao-Eldrup model, which deals with Ps trapped in and thermally equilibrium with a rectangular pore.

Effect of Nb and Cu on the high temperature creep properties of a high Mn–N austenitic stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lee, Kyu-Ho, E-mail: kyuhos@korea.ac.kr; Department of Materials Science and Engineering, Korea University, Seoul 136-713; Suh, Jin-Yoo, E-mail: jinyoo@kist.re.kr

2013-09-15

The effect of Nb and Cu addition on the creep properties of a high Mn–N austenitic stainless steel was investigated at 600 and 650 °C. In the original high Mn–N steel, which was initially precipitate-free, the precipitation of M{sub 23}C{sub 6} (M = Cr, Fe) and Cr{sub 2}N took place mostly on grain boudaries during creep deformation. On the other hand, the minor addition of Nb resulted in high number density of Z-phases (CrNbN) and MX (M = Nb; X = C, N) carbonitrides inside grains by combining with a high content of N, while suppressing the formation of Cr{submore » 2}N. The addition of Cu gave rise to the independent precipitation of nanometer-sized metallic Cu particles. The combination of the different precipitate-forming mechanisms associated with Z-phase, MX and Cu-rich precipitates turned out to improve the creep-resistance significantly. The thermodynamics and kinetics of the precipitation were discussed using thermo-kinetic simulations. - Highlights: • The creep rupture life was improved by Nb and Cu addition. • The creep resistance of the steel A2 in this study was comparable to that of TP347HFG. • The size of Z-phase and MX carbonitride did not change significantly after creep test. • The nanometer sized Cu-rich precipitate was observed after creep. • The predicted size of precipitates by MatCalc agreed well with measured size.« less

RF window assembly comprising a ceramic disk disposed within a cylindrical waveguide which is connected to rectangular waveguides through elliptical joints

DOEpatents

Tantawi, Sami G.; Dolgashev, Valery A.; Yeremian, Anahid D.

2016-03-15

A high-power microwave RF window is provided that includes a cylindrical waveguide, where the cylindrical waveguide includes a ceramic disk concentrically housed in a central region of the cylindrical waveguide, a first rectangular waveguide, where the first rectangular waveguide is connected by a first elliptical joint to a proximal end of the cylindrical waveguide, and a second rectangular waveguide, where the second rectangular waveguide is connected by a second elliptical joint to a distal end of the cylindrical waveguide.

A model of posttraumatic epilepsy after penetrating brain injuries: effect of lesion size and metal fragments.

PubMed

Kendirli, M Tansel; Rose, Dominique T; Bertram, Edward H

2014-12-01

Penetrating brain injury (PBI) has the highest risk for inducing posttraumatic epilepsy, and those PBIs with retained foreign materials such as bullet fragments carry the greatest risk. This study examines the potential contribution of copper, a major component of bullets, to the development of epilepsy following PBI. Anesthetized adult male rats received a penetrating injury from the dorsal cortex to the ventral hippocampus from a high speed small bit drill. In one group of animals, copper wire was inserted into the lesion. Control animals had only the lesion or the lesion plus stainless steel wire (biologically inert foreign body). From 6 to up to 11 months following the injury the rats were monitored intermittently for the development of epilepsy with video-electroencephalography (EEG). A separate set of animals was examined for possible acute seizures in the week following the injury. Twenty-two of the 23 animals with copper wire developed chronic epilepsy, compared to three of the 20 control rats (lesion and lesion with stainless steel). Copper was associated with more extensive injury. The control rats with epilepsy had larger lesions. In the acute injury group, there was no difference in the incidence of seizures (83% lesion plus stainless steel, 70% lesion plus copper). Copper increases the risk for epilepsy and may increase damage over time, but there were no differences between the groups in the incidence of acute postinjury seizures. Lesion size may contribute to epilepsy development in lesion-only animals. Copper may be an independent risk factor for the development of epilepsy and possible secondary injury, but lesion size also contributes to the development of epilepsy. The consequences of prolonged exposure of the brain to copper observed in these animals may have clinical implications that require further evaluation. Wiley Periodicals, Inc. © 2014 International League Against Epilepsy.

Densification behavior and mechanical properties of nanocrystalline TiC reinforced 316L stainless steel composite parts fabricated by selective laser melting

NASA Astrophysics Data System (ADS)

Zhao, Shuming; Shen, Xianfeng; Yang, Jialin; Teng, Wenhua; Wang, Yingying

2018-07-01

Metal matrix composite parts produced using selective laser melting have superior mechanical properties to those produced using traditional powder metallurgy. In this study, nanocrystalline TiC reinforced 316L stainless steel composite parts were fabricated using selective laser melting, and the effects of the TiC mass fraction, particle size, and processing parameters on the relative density, microhardness, and mechanical properties of the TiC/316L composites were investigated. The results show that the relative density of the fabricated parts is related to the laser power and exposure time, and increases when these parameters are increased. The greater the mass fraction of nano-TiC added, the more severe the degree of spheroidization and the lower the density of the resulting material. The microhardness of the 316L stainless steel parts is enhanced by the nano-TiC particles, and increases with increasing nano-TiC mass fraction. The tensile strength is improved with longer exposure time and with the addition of 2 wt% nano-TiC particles. Compared with pure 316L, the microhardness of the TiC/316L composite parts fabricated with 2 wt% 40 nm TiC enhanced from HV0.3 = 219.1 to 277.6, and the ultimate tensile strength significantly increased from 627.5 to 748.6 MPa. The strengthening mechanism of TiC particles is the refinement of the grain size of the 316L matrix, and the greater amount of TiC particles added, the better the grain refinement of 316L.

Agricultural and Ranching area, Rio Sao Francisco, Brazil

NASA Technical Reports Server (NTRS)

1990-01-01

This agricultural and Ranching area, Rio Sao Francisco, Brazil (13.0S, 43.5W) has been under study for several years. See scene STS-31-92-045 for comparison. This area has many small single family subsistence farms, large square and rectangular commercial farms and pastures for livestock grazing. Over the several years of observation, the number and size of farms has increased and center-pivot, swing-arm irrigation systems have been installed.

Agricultural fields, Khartoum, Sudan, Africa

NASA Technical Reports Server (NTRS)

1992-01-01

This herringbone pattern of irrigated agricultural fields near Khartoum, Sudan (14.5N, 33.5E) is very distinctive in both size and shape. The region contains thousands of these rectangular fields bounded by canals which carry water from both the White and Blue Nile Rivers. A crop rotation system is used so that some fields are in cotton, millit, sorghum or fallow to conserve moisture and control weeds and insects. See also STS049-96-003.

X-ray Diffraction Investigation of Annealing Behavior of Peened Surface Deformation Layer on Precipitation Hardening Stainless Steel

NASA Astrophysics Data System (ADS)

Huang, Junjie; Wang, Zhou; Gan, Jin; Yang, Ying; Huang, Feng; Wu, Gang; Meng, Qingshuai

2018-05-01

In order to investigate the recrystallization behavior of peened surface deformation layer of precipitation hardening stainless steel, a classic x-ray diffraction line profile analysis, Voigt method, was carried out on peened 17-4PH with different isothermal annealing temperatures. The activation energy of domain boundary migration ( Q a) and the activation energy of microstrain relaxation ( Q b) were calculated by regression analysis in different annealing temperature conditions. The results show that the value of Q a decreases with annealing temperature increasing, which is due to the influence of precipitation (ɛ-Cu) size on the movements of grain and subgrain boundaries. The maximum growth rate of ɛ-Cu particles occurs during 400 to 500 °C interval. Compared with growth behavior of domain size, microstrain relaxation behavior is less sensitive to precipitation particle size. The effects of annealing temperature and time on dislocation density are both significant when annealing temperature is lower than 500 °C. However, the effect of annealing temperature on dislocation density becomes insignificant when annealing temperature is higher than 500 °C. 300 °C annealing temperature only leads to the microstrain relaxation but nearly cannot lead to the domain size growth even if prolonging annealing time. Microstructure enhancement effect still exists in plastic deformation layer when 300 °C annealing temperature lasts for 60 min but nearly disappears when 600 °C annealing temperature lasts for 20 min.

X-ray Diffraction Investigation of Annealing Behavior of Peened Surface Deformation Layer on Precipitation Hardening Stainless Steel

NASA Astrophysics Data System (ADS)

Huang, Junjie; Wang, Zhou; Gan, Jin; Yang, Ying; Huang, Feng; Wu, Gang; Meng, Qingshuai

2018-04-01

In order to investigate the recrystallization behavior of peened surface deformation layer of precipitation hardening stainless steel, a classic x-ray diffraction line profile analysis, Voigt method, was carried out on peened 17-4PH with different isothermal annealing temperatures. The activation energy of domain boundary migration (Q a) and the activation energy of microstrain relaxation (Q b) were calculated by regression analysis in different annealing temperature conditions. The results show that the value of Q a decreases with annealing temperature increasing, which is due to the influence of precipitation (ɛ-Cu) size on the movements of grain and subgrain boundaries. The maximum growth rate of ɛ-Cu particles occurs during 400 to 500 °C interval. Compared with growth behavior of domain size, microstrain relaxation behavior is less sensitive to precipitation particle size. The effects of annealing temperature and time on dislocation density are both significant when annealing temperature is lower than 500 °C. However, the effect of annealing temperature on dislocation density becomes insignificant when annealing temperature is higher than 500 °C. 300 °C annealing temperature only leads to the microstrain relaxation but nearly cannot lead to the domain size growth even if prolonging annealing time. Microstructure enhancement effect still exists in plastic deformation layer when 300 °C annealing temperature lasts for 60 min but nearly disappears when 600 °C annealing temperature lasts for 20 min.

Inertial focusing of spherical particles in rectangular microchannels over a wide range of Reynolds numbers.

PubMed

Liu, Chao; Hu, Guoqing; Jiang, Xingyu; Sun, Jiashu

2015-02-21

Inertial microfluidics has emerged as an important tool for manipulating particles and cells. For a better design of inertial microfluidic devices, we conduct 3D direct numerical simulations (DNS) and experiments to determine the complicated dependence of focusing behaviour on the particle size, channel aspect ratio, and channel Reynolds number. We find that the well-known focusing of the particles at the two centers of the long channel walls occurs at a relatively low Reynolds number, whereas additional stable equilibrium positions emerge close to the short walls with increasing Reynolds number. Based on the numerically calculated trajectories of particles, we propose a two-stage particle migration which is consistent with experimental observations. We further present a general criterion to secure good focusing of particles for high flow rates. This work thus provides physical insight into the multiplex focusing of particles in rectangular microchannels with different geometries and Reynolds numbers, and paves the way for efficiently designing inertial microfluidic devices.

Asymptotic modal analysis of a rectangular acoustic cavity excited by wall vibration

NASA Technical Reports Server (NTRS)

Peretti, Linda F.; Dowell, Earl H.

1992-01-01

Asymptotic modal analysis, a method that has recently been developed for structural dynamical systems, has been applied to a rectangular acoustic cavity. The cavity had a flexible vibrating portion on one wall, and the other five walls were rigid. Banded white noise was transmitted through the flexible portion (plate) only. Both the location along the wall and the size of the plate were varied. The mean square pressure levels of the cavity interior were computed as a ratio of the result obtained from classical modal analysis to that obtained from asymptotic modal analysis for the various plate configurations. In general, this ratio converged to 1.0 as the number of responding modes increased. Intensification effects were found due to both the excitation location and the response location. The asymptotic modal analysis method was both efficient and accurate in solving the given problem. The method has advantages over the traditional methods that are used for solving dynamics problems with a large number of responding modes.

Bandwidth enhancement of monopole antenna with DGS for SHF and reconfigurable structure for WiMAX, WLAN and C-band applications

NASA Astrophysics Data System (ADS)

Beigi, P.; Mohammadi, P.

2017-11-01

In this study a reconfigurable antenna for WiMAX, WLAN, C-bands and SHF applications has been presented. The main body of antenna includes rectangular and L-shaped slotted ground plane and a rectangular patch with slotted feed line, for impedance bandwidth enhancement. In the proposed antenna, a PIN diode is used to adjust the frequency band to SHF, WiMAX, WLAN and C-bands applications. When PIN diode is forward-biased, the antenna covers the 3.5-31 GHz frequency range (i.e. a 160% bandwidth) and when the PIN diode is in its off-state, it operates between 3.4-5.8 GHz. The designed antenna, with a very small size of 12 × 18 × 1.6 mm3, has been fabricated and tested. The radiation pattern is approximately omnidirectional. Simulations and experimental results are in a good agreement with each other and suggest good performance for the presented antenna.

Modal density of rectangular structures in a wide frequency range

NASA Astrophysics Data System (ADS)

Parrinello, A.; Ghiringhelli, G. L.

2018-04-01

A novel approach to investigate the modal density of a rectangular structure in a wide frequency range is presented. First, the modal density is derived, in the whole frequency range of interest, on the basis of sound transmission through the infinite counterpart of the structure; then, it is corrected by means of the low-frequency modal behavior of the structure, taking into account actual size and boundary conditions. A statistical analysis reveals the connection between the modal density of the structure and the transmission of sound through its thickness. A transfer matrix approach is used to compute the required acoustic parameters, making it possible to deal with structures having arbitrary stratifications of different layers. A finite element method is applied on coarse grids to derive the first few eigenfrequencies required to correct the modal density. Both the transfer matrix approach and the coarse grids involved in the finite element analysis grant high efficiency. Comparison with alternative formulations demonstrates the effectiveness of the proposed methodology.

Note: Development of target changeable palm-top pyroelectric x-ray tube

DOE Office of Scientific and Technical Information (OSTI.GOV)

Imashuku, Susumu; Kawai, Jun

2012-01-15

A target changeable palm-top size x-ray tube was realized using pyroelectric crystal and detachable vacuum flanges. The target metals can be exchanged easily by attaching them on the brass stage with carbon tape. When silver and titanium palates (area: 10 mm{sup 2}) were used as targets, silver L{alpha} and titanium K lines were clearly observed by bombarding electrons on the targets for 90 s. The intensities were the same or higher than those of previously reported pyroelectric x-ray tubes. Chromium, iron, nickel, copper, and zinc K lines in the x-ray tube (stainless steel and brass) disappeared by replacing the brassmore » stage and the stainless steel vacuum flange with a carbon stage and a glass tube, respectively.« less

Thermo-mechanical process for treatment of welds

DOE Office of Scientific and Technical Information (OSTI.GOV)

Malik, R K

1980-03-01

Benefits from thermo-mechanical processing (TMP) of austenitic stainless steel weldments, analogous to hot isostatic pressing (HIP) of castings, most likely result from compressive plastic deformation, enhanced diffusion, and/or increased dislocation density. TMP improves ultrasonic inspectability of austenitic stainless steel welds owing to: conversion of cast dendrites into equiaxed austenitic grains, reduction in size and number of stringers and inclusions, and reduction of delta ferrite content. TMP induces structural homogenization and healing of void-type defects and thus contributes to an increase in elongation, impact strength, and fracture toughness as well as a significant reduction in data scatter for these properties. Anmore » optimum temperature for TMP or HIP of welds is one which causes negligible grain growth and an acceptable reduction in yield strength, and permits healing of porosity.« less

Laser etching of austenitic stainless steels for micro-structural evaluation

NASA Astrophysics Data System (ADS)

Baghra, Chetan; Kumar, Aniruddha; Sathe, D. B.; Bhatt, R. B.; Behere, P. G.; Afzal, Mohd

2015-06-01

Etching is a key step in metallography to reveal microstructure of polished specimen under an optical microscope. A conventional technique for producing micro-structural contrast is chemical etching. As an alternate, laser etching is investigated since it does not involve use of corrosive reagents and it can be carried out without any physical contact with sample. Laser induced etching technique will be beneficial especially in nuclear industry where materials, being radioactive in nature, are handled inside a glove box. In this paper, experimental results of pulsed Nd-YAG laser based etching of few austenitic stainless steels such as SS 304, SS 316 LN and SS alloy D9 which are chosen as structural material for fabrication of various components of upcoming Prototype Fast Breeder Reactor (PFBR) at Kalpakkam India were reported. Laser etching was done by irradiating samples using nanosecond pulsed Nd-YAG laser beam which was transported into glass paneled glove box using optics. Experiments were carried out to understand effect of laser beam parameters such as wavelength, fluence, pulse repetition rate and number of exposures required for etching of austenitic stainless steel samples. Laser etching of PFBR fuel tube and plug welded joint was also carried to evaluate base metal grain size, depth of fusion at welded joint and heat affected zone in the base metal. Experimental results demonstrated that pulsed Nd-YAG laser etching is a fast and effortless technique which can be effectively employed for non-contact remote etching of austenitic stainless steels for micro-structural evaluation.

High-Power Rf Load

DOEpatents

Tantawi, Sami G.; Vlieks, Arnold E.

1998-09-01

A compact high-power RF load comprises a series of very low Q resonators, or chokes [16], in a circular waveguide [10]. The sequence of chokes absorb the RF power gradually in a short distance while keeping the bandwidth relatively wide. A polarizer [12] at the input end of the load is provided to convert incoming TE.sub.10 mode signals to circularly polarized TE.sub.11 mode signals. Because the load operates in the circularly polarized mode, the energy is uniformly and efficiently absorbed and the load is more compact than a rectangular load. Using these techniques, a load having a bandwidth of 500 MHz can be produced with an average power dissipation level of 1.5 kW at X-band, and a peak power dissipation of 100 MW. The load can be made from common lossy materials, such as stainless steel, and is less than 15 cm in length. These techniques can also produce loads for use as an alternative to ordinary waveguide loads in small and medium RF accelerators, in radar systems, and in other microwave applications. The design is easily scalable to other RF frequencies and adaptable to the use of other lossy materials.

Evaluation in vitro of the tensile strength of crimpable hooks used for stabilization in orthognathic surgery.

PubMed

Andrade Gomes, Nascimento Leonard Euller; Melo, Pithon Matheus; Lacerda, Santos Rogério; D'Albuquerque, Medeiros Paulo Jose

2012-03-01

The aim of this study was to evaluate the tensile strength of crimpable hooks used for arch stabilization in orthognatic surgery. Ninety stainless steel wire (0.019" × 0.026") segments, each measuring 6 cm long, were used and attached to crimpable hooks of different commercial brands. Six groups were formed (n = 10) denominated as follows: control, in which the wire segments were perpendicularly welded by spot welding machine; and the hooks groups M (Morelli), MS (Morelli with weld), TP (TP Ortho), TPS (TP with weld), TPTg (TP-tungsten), TPTgS (TP-tungsten with weld), AO (American Orthodontics), and AOS (American Orthodontics with weld). The test specimen topography was evaluated by scanning electron microscopy before and after the tensile strength tests. After obtaining the results, the analysis of variance and Kruskal-Wallis multiple-comparison tests were applied. Compared with the control group, the AOS ball hooks and those from TPS required a greater amount of force to be displaced along the rectangular arch. The hooks in group M were significantly easier to displace, followed by those from AO. The best ball hooks for clinical application are those from AOS and TPS. Copyright © 2012 Elsevier Inc. All rights reserved.

Optimization of robotic welding procedures for maintenance repair of hydraulic turbines

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lamarche, L.; Galopin, M.; Simoneau, R.

1996-12-31

A six axes super-compact robot is used for field repair of cavitation damages found on the discharge ring of hydraulic turbines. Optimization of overlay welding procedures to minimize surface distortion and reduce tearing forces on anchors in concrete, were studied through experimentation and FEM modelling. Planned experimentation has been used to develop optimum pulsed GMAW schedules of stainless steel overlays in 2G position. Best welding sequence was resolved through over lay welding of free plates. Each overlay consisted in one or two layers which were welded in the longitudinal and/or transverse direction of the rectangular plate. A bidirectional welding mode,more » a longitudinal layer followed by a transverse layer position and no cooling between the two layers, were found to be most effective in reducing distortion. The optimized 2G welding procedure was applied to a simulated field repair. Plate was anchored on a massive iron bracket with a set of instrumented bolts, to understand how normal tearing forces in anchors evolve. Preliminary results on FEM modelling of lateral force on anchors indicate good correlation with experiments, for an elementary design.« less

Benchmarking criticality analysis of TRIGA fuel storage racks.

PubMed

Robinson, Matthew Loren; DeBey, Timothy M; Higginbotham, Jack F

2017-01-01

A criticality analysis was benchmarked to sub-criticality measurements of the hexagonal fuel storage racks at the United States Geological Survey TRIGA MARK I reactor in Denver. These racks, which hold up to 19 fuel elements each, are arranged at 0.61m (2 feet) spacings around the outer edge of the reactor. A 3-dimensional model was created of the racks using MCNP5, and the model was verified experimentally by comparison to measured subcritical multiplication data collected in an approach to critical loading of two of the racks. The validated model was then used to show that in the extreme condition where the entire circumference of the pool was lined with racks loaded with used fuel the storage array is subcritical with a k value of about 0.71; well below the regulatory limit of 0.8. A model was also constructed of the rectangular 2×10 fuel storage array used in many other TRIGA reactors to validate the technique against the original TRIGA licensing sub-critical analysis performed in 1966. The fuel used in this study was standard 20% enriched (LEU) aluminum or stainless steel clad TRIGA fuel. Copyright © 2016. Published by Elsevier Ltd.

On size and geometry effects on the brittle fracture of ferritic and tempered martensitic steels

NASA Astrophysics Data System (ADS)

Odette, G. R.; Chao, B. L.; Lucas, G. E.

1992-09-01

A finite element computation of nonsingular crack tip fields was combined with a weakest link statistics model of cleavage fracture. Model predictions for three point bend specimens with various widths and crack depth to width ratios are qualitatively consistent with a number of trends observed in a 12 Cr martensitic stainless steel. The toughness “benefits” of small sizes and shallow cracks are primarily reflected in strain limits rather than net section stress capacities, which is significant to fusion structures subject to large secondary stresses.

Data development for ASTM E24.06.02 round robin program on instability prediction

NASA Technical Reports Server (NTRS)

Mccabe, D. E.

1979-01-01

Basis data for use in an ASTM E24.06.02 task group round robin activity was developed. Compact specimens were made of 2024-T351, 7075-T651 aluminum alloys, and 304 stainless steel. All were 12.7 mm thick and planar dimension variables incorporated were for 1T, 2T and 4T sizes. Representative raw data for each material and specimen size are contained herein. R-curves plotted in terms of delta a physical and delta a effective are plotted for each material.

Enhanced Circular Dichroism of Gold Bilayered Slit Arrays Embedded with Rectangular Holes.

PubMed

Zhang, Hao; Wang, Yongkai; Luo, Lina; Wang, Haiqing; Zhang, Zhongyue

2017-01-01

Gold bilayered slit arrays with rectangular holes embedded into the metal surface are designed to enhance the circular dichroism (CD) effect of gold bilayered slit arrays. The rectangular holes in these arrays block electric currents and generate localized surface plasmons around these holes, thereby strengthening the CD effect. The CD enhancement factor depends strongly on the rotational angle and the structural parameters of the rectangular holes; this factor can be enhanced further by drilling two additional rectangular holes into the metal surfaces of the arrays. These results help facilitate the design of chiral structures to produce a strong CD effect and large electric fields.

Propagation of THz pulses in rectangular subwavelength dielectric waveguides

NASA Astrophysics Data System (ADS)

Lu, Yao; Wu, Qiang; Zhang, Qi; Wang, Ride; Zhao, Wenjuan; Zhang, Deng; Pan, Chongpei; Qi, Jiwei; Xu, Jingjun

2018-06-01

Rectangular subwavelength waveguides are necessary for the development of micro/nanophotonic devices and on-chip platforms. Using a time-resolved imaging system, we studied the transient properties and the propagation modes of THz pulses in rectangular subwavelength dielectric waveguides. The dynamic process of THz pulses was systematically recorded to a movie. In addition, an anomalous group velocity dispersion was demonstrated in rectangular subwavelength waveguides. By using the effective index method, we theoretically calculated the modes in rectangular subwavelength waveguides, which agree well with the experiments and simulations. This work provides the opportunity to improve the analysis and design of the integrated platforms and photonic devices.

Effects of spoiler surfaces on the aeroelastic behavior of a low-aspect-ratio rectangular wing

NASA Technical Reports Server (NTRS)

Cole, Stanley R.

1990-01-01

An experimental research study to determine the effectiveness of spoiler surfaces in suppressing flutter onset for a low-aspect-ratio, rectangular wing was conducted in the Langley Transonic Dynamics Tunnel (TDT). The wing model used in this flutter test consisted of a rigid wing mounted to the wind-tunnel wall by a flexible, rectangular beam. The flexible beam was connected to the wing root and cantilever mounted to the wind-tunnel wall. The wing had a 1.5 aspect ratio based on wing semispan and a NACA 64A010 airfoil shape. The spoiler surfaces consisted of thin, rectangular aluminum plates that were vertically mounted to the wing surface. The spoiler surface geometry and location on the wing surface were varied to determine the effects of these parameters on the classical flutter of the wing model. Subsonically, the experiment showed that spoiler surfaces increased the flutter dynamic pressure with each successive increase in spoiler height or width. This subsonic increase in flutter dynamic pressure was approximately 15 percent for the maximum height spoiler configuration and for the maximum width spoiler configuration. At transonic Mach numbers, the flutter dynamic pressure conditions were increased even more substantially than at subsonic Mach numbers for some of the smaller spoiler surfaces. But greater than a certain spoiler size (in terms of either height or width) the spoilers forced a torsional instability in the transonic regime that was highly Mach number dependent. This detrimental torsional instability was found at dynamic pressures well below the expected flutter conditions. Variations in the spanwise location of the spoiler surfaces on the wing showed little effect on flutter. Flutter analysis was conducted for the basic configuration (clean wing with all spoiler surface mass properties included). The analysis correlated well with the clean wing experimental flutter results.

Experimental investigation on the phenomena around the onset nucleate boiling during the impacting of a droplet on the hot surface

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mitrakusuma, Windy H., E-mail: windyhm@polban.ac.id; Refrigeration and Airconditioning Department, Politeknik Negeri Bandung, Jl. Gegerkalong Hilir, Ds. Ciwaruga Kotak Pos 1234 Bandung; Deendarlianto,

2016-06-03

Onset of nucleate boiling of a droplet when impacted onto hot surface was investigated. Three kinds of surfaces, normal stainless steel (NSS), stainless steel with TiO{sub 2} coating (UVN), and stainless steel with TiO{sub 2} coating and radiated by ultraviolet ray were employed to examine the effect of wettability. The droplet size was 2.4 mm diameter, and dropped under different We number. The image is generated by high speed camera with the frame speed of 1000 fps. The boiling conditions are identified as natural convection, nucleate boiling, critical heat flux, transition, and film boiling. In the present report, the discussionmore » will be focused on the beginning of nucleate boiling on the droplet. Nucleate boiling occurs when bubbles are generated. These bubbles are probably caused by nucleation on the impurities within the liquid rather than at nucleation sites on the heated surface because the bubbles appear to be in the bulk of the liquid instead of at the liquid-solid interface. In addition, the smaller the contact angle, the fastest the boiling.« less

Strain Evolution in Cold-Warm Forged Steel Components Studied by Means of EBSD Technique

PubMed Central

Bonollo, Franco; Bassan, Fabio; Berto, Filippo

2017-01-01

Electron BackScatter Diffraction (EBSD) in conjunction with Field-Emission Environmental Scanning Electron Microscopy (FEG-ESEM) has been used to evaluate the microstructural and local plastic strain evolution in different alloys (AISI 1005, AISI 304L and Duplex 2205) deformed by a single-stage cold and warm forging process. The present work is aimed to describe the different behavior of the austenite and ferrite during plastic deformation as a function of different forging temperatures. Several topological EBSD maps have been measured on the deformed and undeformed states. Then, image quality factor, distributions of the grain size and misorientation have been analyzed in detail. In the austenitic stainless steel, the γ-phase has been found to harden more easily, then α-phase and γ-phase in AISI 1005 and in duplex stainless steel, sequentially. Compared to the high fraction of continuous dynamic recrystallized austenitic zones observed in stainless steels samples forged at low temperatures, the austenitic microstructure of samples forged at higher temperatures, 600–700 °C, has been found to be mainly characterized by large and elongated grains with some colonies of fine nearly-equiaxed grains attributed to discontinuous dynamic recrystallization. PMID:29258249

On the measurement of austenite in supermartensitic stainless steel by X-ray diffraction

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tolchard, Julian Richard, E-mail: tolchard@material.ntnu.no; Sømme, Astri; Solberg, Jan Ketil

2015-01-15

Sections of a 13Cr supermartensitic stainless steel were investigated to determine the optimum sample preparation for measurement of the austenite content by X-ray diffraction. The surface of several samples was mechanically ground or polished using media of grit sizes in the range 1–120 μm. The strained surface layer was afterwards removed stepwise by electropolishing, and the austenite content measured at each step. It was found that any level of mechanical grinding or polishing results in a reduction of the measured austenite fraction relative to the true bulk value, and that coarser grinding media impart greater damage and greater reduction inmore » the measured austenite content. The results thus highlight the importance of the electropolishing step in preparation of such samples, but suggest that the American Society for Testing and Materials standard E975-03 substantially overestimates the amount of material which needs to be removed to recover the true “bulk” content. - Highlights: • Quantitative Rietveld analysis of austenite/martensite ratio in supermartensitic stainless steels • Critical evaluation of sample preparation for residual austenite measurements by X-ray diffraction • Highlighting of the importance of electropolishing as a final preparation step.« less

Grain refinement of a nickel and manganese free austenitic stainless steel produced by pressurized solution nitriding

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mohammadzadeh, Roghayeh, E-mail: r_mohammadzadeh@sut.ac.ir; Akbari, Alireza, E-mail: akbari@sut.ac.ir

2014-07-01

Prolonged exposure at high temperatures during solution nitriding induces grain coarsening which deteriorates the mechanical properties of high nitrogen austenitic stainless steels. In this study, grain refinement of nickel and manganese free Fe–22.75Cr–2.42Mo–1.17N high nitrogen austenitic stainless steel plates was investigated via a two-stage heat treatment procedure. Initially, the coarse-grained austenitic stainless steel samples were subjected to an isothermal heating at 700 °C to be decomposed into the ferrite + Cr{sub 2}N eutectoid structure and then re-austenitized at 1200 °C followed by water quenching. Microstructure and hardness of samples were characterized using X-ray diffraction, optical and scanning electron microscopy, andmore » micro-hardness testing. The results showed that the as-solution-nitrided steel decomposes non-uniformly to the colonies of ferrite and Cr{sub 2}N nitrides with strip like morphology after isothermal heat treatment at 700 °C. Additionally, the complete dissolution of the Cr{sub 2}N precipitates located in the sample edges during re-austenitizing requires longer times than 1 h. In order to avoid this problem an intermediate nitrogen homogenizing heat treatment cycle at 1200 °C for 10 h was applied before grain refinement process. As a result, the initial austenite was uniformly decomposed during the first stage, and a fine grained austenitic structure with average grain size of about 20 μm was successfully obtained by re-austenitizing for 10 min. - Highlights: • Successful grain refinement of Fe–22.75Cr–2.42Mo–1.17N steel by heat treatment • Using the γ → α + Cr{sub 2}N reaction for grain refinement of a Ni and Mn free HNASS • Obtaining a single phase austenitic structure with average grain size of ∼ 20 μm • Incomplete dissolution of Cr{sub 2}N during re-austenitizing at 1200 °C for long times • Reducing re-austenitizing time by homogenizing treatment before grain refinement.« less

Characterization of particle exposure in ferrochromium and stainless steel production.

PubMed

Järvelä, Merja; Huvinen, Markku; Viitanen, Anna-Kaisa; Kanerva, Tomi; Vanhala, Esa; Uitti, Jukka; Koivisto, Antti J; Junttila, Sakari; Luukkonen, Ritva; Tuomi, Timo

2016-07-01

This study describes workers' exposure to fine and ultrafine particles in the production chain of ferrochromium and stainless steel during sintering, ferrochromium smelting, stainless steel melting, and hot and cold rolling operations. Workers' personal exposure to inhalable dust was assessed using IOM sampler with a cellulose acetate filter (AAWP, diameter 25 mm; Millipore, Bedford, MA). Filter sampling methods were used to measure particle mass concentrations in fixed locations. Particle number concentrations and size distributions were examined using an SMPS+C sequential mobile particle sizer and counter (series 5.400, Grimm Aerosol Technik, Ainring, Germany), and a hand-held condensation particle counter (CPC, model 3007, TSI Incorporated, MN). The structure and elemental composition of particles were analyzed using TEM-EDXA (TEM: JEM-1220, JEOL, Tokyo, Japan; EDXA: Noran System Six, Thermo Fisher Scientific Inc., Madison,WI). Workers' personal exposure to inhalable dust averaged 1.87, 1.40, 2.34, 0.30, and 0.17 mg m(-3) in sintering plant, ferrochromium smelter, stainless steel melting shop, hot rolling mill, and the cold rolling mill, respectively. Particle number concentrations measured using SMPS+C varied from 58 × 10(3) to 662 × 10(3) cm(-3) in the production areas, whereas concentrations measured using SMPS+C and CPC3007 in control rooms ranged from 24 × 10(3) to 243 × 10(3) cm(-3) and 5.1 × 10(3) to 97 × 10(3) cm(-3), respectively. The elemental composition and the structure of particles in different production phases varied. In the cold-rolling mill non-process particles were abundant. In other sites, chromium and iron originating from ore and recycled steel scrap were the most common elements in the particles studied. Particle mass concentrations were at the same level as that reported earlier. However, particle number measurements showed a high amount of ultrafine particles, especially in sintering, alloy smelting and melting, and tapping operations. Particle number concentration and size distribution measurements provide important information regarding exposure to ultrafine particles, which cannot be seen in particle mass measurements.

Mass Estimation and Its Applications

DTIC Science & Technology

2012-02-23

parameters); e.g., the rect- angular kernel function has fixed width or fixed per unit size. But the rectangular function used in mass has no parameter...MassTER is implemented in JAVA , and we use DBSCAN in WEKA [13] and a version of DENCLUE implemented in R (www.r-project.org) in our empirical evaluation...Proceedings of SIGKDD, 2010, 989-998. [13] I.H. Witten and E. Frank, Data Mining: Practical Machine Learning Tools and Techniques with Java Implementations

Studying gas-sheared liquid film in horizontal rectangular duct with laser-induced fluorescence technique

NASA Astrophysics Data System (ADS)

Cherdantsev, Andrey; Hann, David; Azzopardi, Barry

2013-11-01

High-speed LIF-technique is applied to study gas-sheared liquid film in horizontal rectangular duct with 161 mm width. Instantaneous distributions of film thickness resolved in both longitudinal and transverse coordinates were obtained with a frequency of 10 kHz and spatial resolution from 0.125 mm to 0.04 mm. Processes of generation of fast and slow ripples by disturbance waves are the same as described in literature for downwards annular pipe flow. Disturbance waves are often localized by transverse coordinate and may have curved or slanted fronts. Fast ripples, covering disturbance waves, are typically horseshoe-shaped and placed in staggered order. Their characteristic transverse size is of order 1 cm and it decreases with gas velocity. Entrainment of liquid from film surface can also be visualized. Mechanisms of ripple disruption, known as ``bag break-up'' and ``ligament break-up,'' were observed. Both mechanisms may occur on the same disturbance waves. Various scenarios of droplet deposition on the liquid film are observed, including the impact, slow sinking and bouncing, characterized by different outcome of secondary droplets or entrapped bubbles. Number and size of bubbles increase greatly inside the disturbance waves. Both quantities increase with gas and liquid flow rates. EPSRC Programme Grant MEMPHIS (EP/K003976/1), and Roll-Royce UTC (Nottingham, for access to flow facility).

Spin wave eigenmodes in single and coupled sub-150 nm rectangular permalloy dots

DOE Office of Scientific and Technical Information (OSTI.GOV)

Carlotti, G., E-mail: giovanni.carlotti@fisica.unipg.it; Madami, M.; Tacchi, S.

2015-05-07

We present the results of a Brillouin light scattering investigation of thermally excited spin wave eigenmodes in square arrays of either isolated rectangular dots of permalloy or twins of dipolarly coupled elements, placed side-by-side or head-to-tail. The nanodots, fabricated by e-beam lithography and lift-off, are 20 nm thick and have the major size D in the range between 90 nm and 150 nm. The experimental spectra show the presence of two main peaks, corresponding to modes localized either at the edges or in the center of the dots. Their frequency dependence on the dot size and on the interaction with adjacent elements hasmore » been measured and successfully interpreted on the basis of dynamical micromagnetic simulations. The latter enabled us also to describe the spatial profile of the eigenmodes, putting in evidence the effects induced by the dipolar interaction between coupled dots. In particular, in twinned dots the demagnetizing field is appreciably modified in proximity of the “internal edges” if compared to the “external” ones, leading to a splitting of the edge mode. These results can be relevant for the exploitation of sub-150 nm magnetic dots in new applications, such as magnonic metamaterials, bit-patterned storage media, and nano-magnetic logic devices.« less

Indium oxide thin film as potential photoanodes for corrosion protection of stainless steel under visible light

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Yan; Yu, Jianqiang, E-mail: jianqyu@qdu.edu.cn; Sun, Kai

Graphical abstract: If the conduction band potential of In{sub 2}O{sub 3} is more negative than the corrosion potential of stainless steel, photo-induced electrons will be transferred from In{sub 2}O{sub 3} to the steel, thus shifting the potential of the steel into a corrosion immunity region and preventing the steel from the corrosion. - Highlights: • Indium oxide performed novel application under visible light. • Indium oxide by sol–gel method behaved better photoelectrochemical properties. • Electrons were transferred to stainless steel from indium oxide once light on. - Abstract: This paper reports the photoelectrochemical cathodic protection of 304 stainless steel bymore » In{sub 2}O{sub 3} thin-film under visible-light. The films were fabricated with In{sub 2}O{sub 3} powders, synthesized by both sol–gel (In{sub 2}O{sub 3}-sg) and solid-state (In{sub 2}O{sub 3}-ss) processes. The photo-induced open circuit potential and the photo-to-current efficiency measurements suggested that In{sub 2}O{sub 3} could be a promising candidate material for photoelectrochemical cathodic protection of metallic alloys under visible light. Moreover, the polarization curve experimental results indicated that In{sub 2}O{sub 3}-sg thin-film can mitigate the corrosion potential of 304 stainless steel to much more negative values with a higher photocurrent density than the In{sub 2}O{sub 3}-ss film under visible-light illumination. All the results demonstrated that the In{sub 2}O{sub 3}-sg thin-film provides a better photoelectrochemical cathodic protection for 304 stainless steel than In{sub 2}O{sub 3}-ss thin-film under visible-light illumination. The higher photoelectrochemical efficiency is possibly due to the uniform thin films produced with the smaller particle size of In{sub 2}O{sub 3}-sg, which facilitates the transfer of the photo-induced electrons from bulk to the surface and suppresses the charge recombination of the electrons and holes.« less

On the modified grain-size-distribution method to evaluate the dynamic recrystallisation fraction in AISI 304 stainless steel

NASA Astrophysics Data System (ADS)

Hong, D. H.; Park, J. K.

2018-04-01

The purpose of the present work was to verify the grain size distribution (GSD) method, which was recently proposed by one of the present authors as a method for evaluating the fraction of dynamic recrystallisation (DRX) in a microalloyed medium carbon steel. To verify the GSD-method, we have selected a 304 stainless steel as a model system and have measured the evolution of the overall grain size distribution (including both the recrystallised and unrecrystallised grains) during hot compression at 1,000 °C in a Gleeble machine; the DRX fraction estimated using the GSD method is compared with the experimentally measured value via EBSD. The results show that the previous GSD method tends to overestimate the DRX fraction due to the utilisation of a plain lognormal distribution function (LDF). To overcome this shortcoming, we propose a modified GSD-method wherein an area-weighted LDF, in place of a plain LDF, is employed to model the evolution of GSD during hot deformation. Direct measurement of the DRX fraction using EBSD confirms that the modified GSD-method provides a reliable method for evaluating the DRX fraction from the experimentally measured GSDs. Reasonable agreement between the DRX fraction and softening fraction suggests that the Kocks-Mecking method utilising the Voce equation can be satisfactorily used to model the work hardening and dynamic recovery behaviour of steels during hot deformation.

Bend losses in rectangular culverts.

DOT National Transportation Integrated Search

2008-09-01

This study investigated bend losses for open channel flow in rectangular channels or culverts. Laboratory experiments were performed for sub-critical flow in rectangular channels with abrupt bends. Bend angles of approximately 30, 45, 60, 75 and 90 d...

Finite element fatigue analysis of rectangular clutch spring of automatic slack adjuster

NASA Astrophysics Data System (ADS)

Xu, Chen-jie; Luo, Zai; Hu, Xiao-feng; Jiang, Wen-song

2015-02-01

The failure of rectangular clutch spring of automatic slack adjuster directly affects the work of automatic slack adjuster. We establish the structural mechanics model of automatic slack adjuster rectangular clutch spring based on its working principle and mechanical structure. In addition, we upload such structural mechanics model to ANSYS Workbench FEA system to predict the fatigue life of rectangular clutch spring. FEA results show that the fatigue life of rectangular clutch spring is 2.0403×105 cycle under the effect of braking loads. In the meantime, fatigue tests of 20 automatic slack adjusters are carried out on the fatigue test bench to verify the conclusion of the structural mechanics model. The experimental results show that the mean fatigue life of rectangular clutch spring is 1.9101×105, which meets the results based on the finite element analysis using ANSYS Workbench FEA system.

Analysis of junior high school students' difficulty in resolving rectangular conceptual problems

NASA Astrophysics Data System (ADS)

Utami, Aliksia Kristiana Dwi; Mardiyana, Pramudya, Ikrar

2017-08-01

Geometry is one part of the mathematics that must be learned in school and it has important effects on the development of creative thinking skills of learners, but in fact, there are some difficulties experienced by the students. This research focuses on analysis difficulty in resolving rectangular conceptual problems among junior high school students in every creative thinking skills level. This research used a descriptive method aimed to identify the difficulties and cause of the difficulties experienced by five students. The difficulties are associated with rectangular shapes and related problems. Data collection was done based on students' work through test, interview, and observations. The result revealed that student' difficulties in understanding the rectangular concept can be found at every creative thinking skills level. The difficulties are identifying the objects rectangular in the daily life except for a rectangle and square, analyzing the properties of rectangular shapes, and seeing the interrelationships between figures.

Effect of Nb Addition to Ti-Bearing Super Martensitic Stainless Steel on Control of Austenite Grain Size and Strengthening

NASA Astrophysics Data System (ADS)

Ma, Xiaoping; Langelier, Brian; Gault, Baptiste; Subramanian, Sundaresa

2017-05-01

The role of Nb in normalized and tempered Ti-bearing 13Cr5Ni2Mo super martensitic stainless steel is investigated through in-depth characterization of the bimodal chemistry and size of Nb-rich precipitates/atomic clusters and Nb in solid solution. Transmission electron microscopy and atom probe tomography are used to analyze the samples and clarify precipitates/atom cluster interactions with dislocations and austenite grain boundaries. The effect of 0.1 wt pct Nb addition on the promotion of (Ti, Nb)N-Nb(C,N) composite precipitates, as well as the retention of Nb in solution after cooling to room temperature, are analyzed quantitatively. (Ti, Nb)N-Nb(C,N) composite precipitates with average diameters of approximately 24 ± 8 nm resulting from epitaxial growth of Nb(C,N) on pre-existing (Ti,Nb)N particles, with inter-particle spacing on the order of 205 ± 68 nm, are found to be associated with mean austenite grain size of 28 ± 10 µm in the sample normalized at 1323 K (1050 °C). The calculated Zener limiting austenite grain size of 38 ± 13 µm is in agreement with the experimentally observed austenite grain size distribution. 0.08 wt pct Nb is retained in the as-normalized condition, which is able to promote Nb(C, N) atomic clusters at dislocations during tempering at 873 K (600 °C) for 2 hours, and increases the yield strength by 160 MPa, which is predicted to be close to maximum increase in strengthening effect. Retention of solute Nb before tempering also leads to it preferentially combing with C and N to form Nb(C, N) atom clusters, which suppresses the occurrence of Cr- and Mo-rich carbides during tempering.

Processing and evaluation of long fiber thermoplastic composite plates for internal fixation

NASA Astrophysics Data System (ADS)

Warren, Paul B.

The metallic plates used in internal fracture fixation may have up to ten times the elastic modulus of normal bone tissue, causing stress shielding-induced osteopenia in healed bone that can lead to re-fracture after plate removal and prolonged and painful recovery. Thermoplastic polymer matrix composites reinforced with long carbon fiber are promising alternative materials for internal fixation plates because they may be produced with relative ease and be tailored to have specific mechanical properties, alleviating the stress shielding problem. Long carbon fiber-reinforced polyetheretherketone (LCF PEEK) plates were produced using the extrusion / compression molding process. Static flexural testing determined that LCF PEEK plates with rectangular cross-section had an average flexural modulus of 12 GPa, or 23% of the flexural modulus of a stainless steel plate. The LCF PEEK plates also experienced negligible (14.7%, 14.5%, and 16.7%) reductions in modulus after fatigue testing at applied moments of 2.5, 3.0, and 3.5 N•m, respectively, over 106 load cycles. Aging the plates in 0.9% NaCl solution for four and eight weeks caused 0.34% and 0.28% increases in plate mass, respectively. No significant decrease of flexural properties due to aging was detected. Differential scanning calorimetry (DSC) revealed the PEEK matrix of the plates to be 24.5% crystalline, which is lower than typical PEEK crystallinity values of 30-35%. Scanning electron microscopy (SEM) revealed three times as many fiber pullout areas in LCF PEEK fracture surfaces as in fracture surfaces of long carbon fiber-reinforced polyphenylenesulfide (LCF PPS), another plate material tested. DSC and SEM data suggest that improvements in processing conditions and fiber/matrix bonding, along with higher carbon fiber fractions, would enhance LCF PEEK plate performance. LCF PEEK remains a promising alternative to stainless steel for internal fixation plates.

Wind-tunnel research comparing lateral control devices, particularly at high angles of attack XII : upper-surface ailerons on wings with split flaps

NASA Technical Reports Server (NTRS)

Weick, Fred E; Wenzinger, Carl J

1935-01-01

This report covers the twelfth of a series of tests conducted to compare different lateral control devices with particular reference to their effectiveness at high angles of attack. The present wind tunnel tests were made with two sizes of upper-surface ailerons on rectangular Clark Y wing models equipped with full span split flaps. The tests showed the effect of the upper-surface ailerons and of the split flaps on the general performance characteristics of the wings, and on the lateral controllability and stability characteristics. The results are compared with those for plain wings with ordinary ailerons of similar sizes.

Sexual dimorphism in the human face assessed by euclidean distance matrix analysis.

PubMed Central

Ferrario, V F; Sforza, C; Pizzini, G; Vogel, G; Miani, A

1993-01-01

The form of any object can be viewed as a combination of size and shape. A recently proposed method (euclidean distance matrix analysis) can differentiate between size and shape differences. It has been applied to analyse the sexual dimorphism in facial form in a sample of 108 healthy young adults (57 men, 51 women). The face was wider and longer in men than in women. A global shape difference was demonstrated, the male face being more rectangular and the female face more square. Gender variations involved especially the lower third of the face and, in particular, the position of the pogonion relative to the other structures. PMID:8300436

77 FR 28568 - Grant of Authority for Subzone Status; North American Stainless, (Stainless Steel), Ghent, KY

Federal Register 2010, 2011, 2012, 2013, 2014

2012-05-15

... Status; North American Stainless, (Stainless Steel), Ghent, KY Pursuant to its authority under the... application to the Board for authority to establish a special-purpose subzone at the stainless steel mill of... stainless steel at the facility of North American Stainless, located in Ghent, Kentucky (Subzone 29L), as...

DOE Office of Scientific and Technical Information (OSTI.GOV)

Washenfelder, D. J.; Girardot, C. L.; Wilson, E. R.

The twenty-eight double-shell underground radioactive waste storage tanks at the U. S. Department of Energy’s Hanford Site near Richland, WA are interconnected by the Waste Transfer System network of buried steel encased pipelines and pipe jumpers in below-grade pits. The pipeline material is stainless steel or carbon steel in 51 mm to 152 mm (2 in. to 6 in.) sizes. The pipelines carry slurries ranging up to 20 volume percent solids and supernatants with less than one volume percent solids at velocities necessary to prevent settling. The pipelines, installed between 1976 and 2011, were originally intended to last until themore » 2028 completion of the double-shell tank storage mission. The mission has been subsequently extended. In 2010 the Tank Operating Contractor began a systematic evaluation of the Waste Transfer System pipeline conditions applying guidelines from API 579-1/ASME FFS-1 (2007), Fitness-For-Service. Between 2010 and 2014 Fitness-for-Service examinations of the Waste Transfer System pipeline materials, sizes, and components were completed. In parallel, waste throughput histories were prepared allowing side-by-side pipeline wall thinning rate comparisons between carbon and stainless steel, slurries and supernatants and throughput volumes. The work showed that for transfer volumes up to 6.1E+05 m 3 (161 million gallons), the highest throughput of any pipeline segment examined, there has been no detectable wall thinning in either stainless or carbon steel pipeline material regardless of waste fluid characteristics or throughput. The paper describes the field and laboratory evaluation methods used for the Fitness-for-Service examinations, the results of the examinations, and the data reduction methodologies used to support Hanford Waste Transfer System pipeline wall thinning conclusions.« less

Comparison of spring characteristics of titanium-molybdenum alloy and stainless steel

PubMed Central

Salehi, Anahita; Asatourian, Armen

2017-01-01

Background Titanium-molybdenum alloy (TMA) and stainless steel (SS) wires are commonly used in orthodontics as arch-wires for tooth movement. However, plastic deformation phenomenon in these arch-wires seems to be a major concern among orthodontists. This study aimed to compare the mechanical properties of TMA and SS wires with different dimensions. Material and Methods Seventy-two wire samples (36 TMA and 36 SS) of three different sizes (19×25, 17×25 and 16×22) were analyzed in vitro, with 12 samples in each group. Various mechanical properties of the wires, including spring-back, bending moment and stiffness were determined using a universal testing machine. Student’s t-test showed statistically significant differences in the mean values of all the groups. In addition, metallographic comparison of SS and TMA wires was conducted under an optical microscope. Results The degree of stiffness of 16×22-sized SS and TMA springs was found to be 12±2 and 5±0.4, respectively, while the bending moment was estimated to be 1927±352 (gm-mm) and 932±16 (gm-mm), respectively; the spring-back index was determined to be 0.61±0.2 and 0.4±.09, respectively (p<0.001). There were no statistically significant differences in spring-back index in larger dimensions of the wires. Conclusions Systematic analysis indicated that springs made of TMA were superior compared to those made of SS. Although both from economic and functionality viewpoints the use of TMA is suggested, further clinical investigations are recommended. Key words:Bending moment, optical microscope, spring-back, stainless steel, stiffness, titanium‒molybdenum alloy. PMID:28149469

Nutrient Recovery from the Dry Grind Process Using Sequential Micro and Ultrafiltration of Thin Stillage

USDA-ARS?s Scientific Manuscript database

The effectiveness of microfiltration (MF) and ultrafiltration (UF) for nutrient recovery from a thin stillage stream was determined. When a stainless steel MF membrane (0.1 um pore size) was used, the content of solids increased from 7.0% to 22.8% with a mean permeate flux rate of 45 L/m**2/h (LMH)...

Vapor-liquid phase separator permeability results

NASA Technical Reports Server (NTRS)

Yuan, S. W. K.; Frederking, T. H. K.

1981-01-01

Continued studies are described in the area of vapor-liquid phase separator work with emphasis on permeabilities of porous sintered plugs (stainless steel, nominal pore size 2 micrometer). The temperature dependence of the permeability has been evaluated in classical fluid using He-4 gas at atmospheric pressure and in He-2 on the basis of a modified, thermosmotic permeability of the normal fluid.

Automatic welding of stainless steel tubing

NASA Technical Reports Server (NTRS)

Clautice, W. E.

1978-01-01

The use of automatic welding for making girth welds in stainless steel tubing was investigated as well as the reduction in fabrication costs resulting from the elimination of radiographic inspection. Test methodology, materials, and techniques are discussed, and data sheets for individual tests are included. Process variables studied include welding amperes, revolutions per minute, and shielding gas flow. Strip chart recordings, as a definitive method of insuring weld quality, are studied. Test results, determined by both radiographic and visual inspection, are presented and indicate that once optimum welding procedures for specific sizes of tubing are established, and the welding machine operations are certified, then the automatic tube welding process produces good quality welds repeatedly, with a high degree of reliability. Revised specifications for welding tubing using the automatic process and weld visual inspection requirements at the Kennedy Space Center are enumerated.

The Effect of Multiple Shot Peening on the Corrosion Behavior of Duplex Stainless Steel

NASA Astrophysics Data System (ADS)

Feng, Qiang; She, Jia; Wu, Xueyan; Wang, Chengxi; Jiang, Chuanhai

2018-03-01

Various types of shot peening treatments were applied to duplex stainless steel. The effects of shot peening intensity and working procedures on the microstructure were investigated. The domain size and microstrain evolution in the surface layer were characterized utilizing the Rietveld method. As the shot peening intensity increased, the surface roughness increased in the surface layer; however, it decreased after multiple (dual and triple) shot peening. The mole fraction of strain-induced martensite as a function of the intensity of shot peening was evaluated by XRD measurements. Both potentiodynamic polarization curves and salt spray tests of shot-peened samples in NaCl solution were investigated. The results indicate that traditional shot peening has negative effects on corrosion resistance with increasing shot peening intensity; however, the corrosion rate can be reduced by means of multiple shot peening.

A Shear Strain Route Dependency of Martensite Formation in 316L Stainless Steel.

PubMed

Kang, Suk Hoon; Kim, Tae Kyu; Jang, Jinsung; Oh, Kyu Hwan

2015-06-01

In this study, the effect of simple shearing on microstructure evolution and mechanical properties of 316L austenitic stainless steel were investigated. Two different shear strain routes were obtained by twisting cylindrical specimens in the forward and backward directions. The strain-induced martensite phase was effectively obtained by alteration of the routes. Formation of the martensite phase clearly resulted in significant hardening of the steel. Grain-size reduction and strain-induced martensitic transformation within the deformed structures of the strained specimens were characterized by scanning electron microscopy - electron back-scattered diffraction, X-ray diffraction, and the TEM-ASTAR (transmission electron microscopy - analytical scanning transmission atomic resolution, automatic crystal orientation/phase mapping for TEM) system. Significant numbers of twin networks were formed by alteration of the shear strain routes, and the martensite phases were nucleated at the twin interfaces.

Influence of brazing conditions on the strength of brazed joints of alumina dispersion-strengthened copper to 316 stainless steel

NASA Astrophysics Data System (ADS)

Nishi, H.; Kikuchi, K.

1998-10-01

Brazing of alumina dispersion-strengthened copper (DS Cu) to 316 stainless steel were conducted in order to investigate the influence of filler metals and brazing conditions on the joint strength. The brazing were performed with a silver-base (BAg-8) and three kinds of gold-base (BAu-2,4,11) filler metals with varying brazing joint clearance and brazing time. The filler metal had a greater effect on the joint strength than the brazing joint clearance and brazing time. The joint with BAu-2 was superior to the joint with other filler metals. The tensile strength of the joint with BAu-2 was as large as that of DS Cu, however, the Charpy and low cycle fatigue strength were lower than those of DS Cu. The DS Cu melted near the brazed zone, consequently recrystallization and agglomeration of alumina occurred in the diffusion layer for all filler metals. The grain size after the recrystallization was small in order of BAu-2, BAu-4 and BAu-11, that was in accordance with the order of the brazing temperature. The excellent fracture strength for the joint with BAu-2 was attributed to the smallest grain size.

Flexible Metal-Fabric Radiators

NASA Technical Reports Server (NTRS)

Cross, Cynthia; Nguyen, Hai D.; Ruemmele, Warren; Andish, Kambiz K.; McCalley, Sean

2005-01-01

Flexible metal-fabric radiators have been considered as alternative means of dissipating excess heat from spacecraft and space suits. The radiators also may be useful in such special terrestrial applications as rejecting heat from space-suit-like protective suits worn in hot work environments. In addition to flexibility and consequent ease of deployment and installation on objects of varying sizes and shapes, the main advantages of these radiators over conventional rigid radiators are that they weigh less and occupy less volume for a given amount of cooling capacity. A radiator of this type includes conventional stainless-steel tubes carrying a coolant fluid. The main radiating component consists of a fabric of interwoven aluminum-foil strips bonded to the tubes by use of a proprietary process. The strip/tube bonds are strong and highly thermally conductive. Coolant is fed to and from the tubes via flexible stainless-steel manifolds designed to accommodate flexing of, and minimize bending forces on, the fabric. The manifolds are sized to minimize pressure drops and distribute the flow of coolant evenly to all the tubes. The tubes and manifolds are configured in two independent flow loops for operational flexibility and protective redundancy.

Influence of Heat Treatment on the Microstructure and Corrosion Resistance of 13 Wt Pct Cr-Type Martensitic Stainless Steel

NASA Astrophysics Data System (ADS)

Lu, Si-Yuan; Yao, Ke-Fu; Chen, Yun-Bo; Wang, Miao-Hui; Ge, Xue-Yuan

2015-12-01

The effect of heat treatment on the microstructure and the electrochemical properties of a typical corrosion-resistant plastic mold steel in Cl--containing solution were studied in this research. Through X-ray diffraction patterns, SEM and TEM analysis, it was found that the sequence of the precipitates in the steels tempered at 573 K, 773 K, and 923 K (300 °C, 500 °C, and 650 °C) was θ-M3C carbides, nano-sized Cr-rich M23C6 carbides, and micro/submicron-sized Cr-rich M23C6 carbides, respectively. The results of the electrochemical experiments showed that the pitting potential of the as-quenched martensitic stainless steels increased with the austenitizing temperature. However, the corrosion resistance of the steels would decreased after tempering, especially when tempered at 773 K (500 °C), no passivation regime could be found in the polarization curve of the MSSs and no effective passive film could be formed on the steels in Cl--containing environments. The present results suggested that the temperature around 773 K (500 °C) should be avoided for tempering process of MSS used as plastic molds.

Bubble propagation on a rail: a concept for sorting bubbles by size

NASA Astrophysics Data System (ADS)

Franco-Gómez, Andrés; Thompson, Alice B.; Hazel, Andrew L.; Juel, Anne

We demonstrate experimentally that the introduction of a rail, a small height constriction, within the cross-section of a rectangular channel could be used as a robust passive sorting device in two-phase fluid flows. Single air bubbles carried within silicone oil are generally transported on one side of the rail. However, for flow rates marginally larger than a critical value, a narrow band of bubble sizes can propagate (stably) over the rail, while bubbles of other sizes segregate to the side of the rail. The width of this band of bubble sizes increases with flow rate and the size of the most stable bubble can be tuned by varying the rail width. We present a complementary theoretical analysis based on a depth-averaged theory, which is in qualitative agreement with the experiments. The theoretical study reveals that the mechanism relies on a non-trivial interaction between capillary and viscous forces that is fully dynamic, rather than being a simple modification of capillary static solutions.

The effect of retentive groove, sandblasting and cement type on the retentive strength of stainless steel crowns in primary second molars--an in vitro comparative study.

PubMed

Veerabadhran, M M; Reddy, V; Nayak, U A; Rao, A P; Sundaram, M A

2012-01-01

This in vitro study was conducted to find out the effect of retentive groove, sand blasting and cement type on the retentive strength of stainless steel crowns in primary second molars. Thirty-two extracted intact human maxillary and mandibular primary second molars were embedded in aluminum blocks utilizing autopolymerising acrylic resin. After tooth preparation, the 3M stainless steel crown was adjusted to the prepared tooth. Then weldable buccal tubes were welded on the buccal and lingual surfaces of each crown as an attachment for the testing machine. A full factorial design matrix for four factors (retentive groove placement on the tooth, cement type, sandblasting and primary second molar) at two levels each was developed and the study was conducted as dictated by the matrix. The lower and upper limits for each factor were without and with retentive groove placement on the tooth, GIC and RMGIC, without and with sandblasting of crown, maxillary and mandibular second primary molar. For those teeth for which the design matrix dictated groove placement, the retentive groove was placed on the middle third of the buccal surface of the tooth horizontally and for those crowns for which sandblasting of the crowns are to be done, sandblasting was done with aluminium oxide with a particle size of 250 mm. The crowns were luted with either GIC or RMGIC, as dictated by the design matrix. Then the retentive strength of each sample was evaluated by means of an universal testing machine. The obtained data was analyzed using ANOVA for statistical analysis of the data and 't'- tests for pairwise comparison. The mean retentive strength in kg/cm 2 stainless steel crowns luted with RMGIC was 19.361 and the mean retentive strength of stainless steel crowns luted with GIC was 15.964 kg/cm 2 with a mean difference of 3.397 kg/cm 2 and was statistically significant. The mean retentive strength in kg/cm 2 of stainless steel crowns, which was not sandblasted, was 18.880 and which was sandblasted was 16.445 kg/cm 2 with a mean difference of 2.436 kg/cm 2 . These results were again statistically significant. It was found that the crowns luted with resin-modified glass ionomer cements (RMGIC's) offered better retentive strength of crowns than glass ionomer cements (GIC) and stainless steel crowns which were cemented without sandblasting showed higher mean retentive strength than with sandblasting of crowns. The presence of groove did not influence the retentive strength of stainless steel crowns.

Method and structure for cache aware transposition via rectangular subsections

DOEpatents

Gustavson, Fred Gehrung; Gunnels, John A

2014-02-04

A method and structure for transposing a rectangular matrix A in a computer includes subdividing the rectangular matrix A into one or more square submatrices and executing an in-place transposition for each of the square submatrices A.sub.ij.

Lid design for low level waste container

DOEpatents

Holbrook, R.H.; Keener, W.E.

1995-02-28

A container for low level waste includes a shell and a lid. The lid has a frame to which a planar member is welded. The lid frame includes a rectangular outer portion made of square metal tubing, a longitudinal beam extending between axial ends of the rectangular outer portion, and a transverse beam extending between opposite lateral sides of the rectangular outer portion. Two pairs of diagonal braces extend between the longitudinal beam and the four corners of the rectangular outer portion of the frame. 6 figs.

Lid design for low level waste container

DOEpatents

Holbrook, Richard H.; Keener, Wendell E.

1995-01-01

A container for low level waste includes a shell and a lid. The lid has a frame to which a planar member is welded. The lid frame includes a rectangular outer portion made of square metal tubing, a longitudinal beam extending between axial ends of the rectangular outer portion, and a transverse beam extending between opposite lateral sides of the rectangular outer portion. Two pairs of diagonal braces extend between the longitudinal beam and the four corners of the rectangular outer portion of the frame.

Stainless steel wear debris of a scoliotic growth guidance system has little local and systemic effect in an animal model.

PubMed

Singh, Vaneet; Rawlinson, Jeremy; Hallab, Nadim

2018-01-11

Options to treat early-onset scoliosis include guided-growth systems with sliding action between rods and pedicle screws. The wear was previously measured in an in vitro test, and in this in vivo rabbit model, we evaluated the local and systemic biological response to the stainless steel debris. Compared to the previous study, a relatively higher volume of representative wear particles with a median particle size of 0.84 μm were generated. Bolus dosages were injected into the epidural space at L4-L5 for a minimum of 36 rabbits across three treatment groups (negative control, 1.5 mg, and 4.0 mg) and two timepoints (12 and 24 weeks). Gross pathology evaluated distant organs and the injection site with a dorsal laminectomy to examine the epidural space and dosing site. Peri-implanted particle tissues were stained for immunohistochemical and quantitatively analyzed for IL-6 and TNF-α cytokines. Based on ISO 10993-6:2007 scoring, particles in the high-dose group were primarily non-irritant (12 weeks) with one slightly irritant. At 24 weeks, inflammatory cell infiltration was non-existent to minimal with all groups considered non-irritant at the injection site. Material characterization confirmed that particles detected in distant organs were stainless steel or contaminants. At 12 weeks, stainless steel groups demonstrated statistically increased amounts of cytokine levels compared to control but there was a statistical decrease for both at 24 weeks. These findings indicate that stainless steel wear debris, comparable to the expected usage from a simulated growth guidance system, had no discernible untoward biological effects locally and systemically in an animal model. © 2018 Orthopaedic Research Society. Published by Wiley Periodicals, Inc. J Orthop Res. © 2018 Orthopaedic Research Society. Published by Wiley Periodicals, Inc.

Evaluation of the Efficacy of Caries Removal Using Polymer Bur, Stainless Steel Bur, Carisolv, Papacarie - An Invitro Comparative Study.

PubMed

Divya, Gaddam; Prasad, Madhu Ghanashyam; Vasa, Aron Arun Kumar; Vasanthi, Done; Ramanarayana, Boyapati; Mynampati, Praffulla

2015-07-01

Dental caries continues to affect a significant portion of the world population and treatment of the decay is associated with pain by many patients. Intervention and application of rotary instruments for treatment of carious lesions has often resulted in considerable removal of tooth structure. Chemo-mechanical method, a minimal invasive technique for caries removal was developed to overcome these shortcomings. This innovative method seems to be efficient in removing infected dentine without altering the healthy dental tissue or harming the adjacent oral mucosa. To evaluate the efficacy and efficiency of Caries removal Using Polymer Bur, Stainless Steel Bur, Carisolv and Papacarie. A total of 120 sectioned specimens were obtained from 60 extracted teeth. Each tooth was sectioned mesiodistally in the center of the carious lesion so that two halves (buccal and lingual or palatal) having equal sized carious lesions are compared. The sectioned specimens were subdivided into four groups (Polymer Bur, Stainless Steel Bur, Carisolv, Papacarie) allotting 30 specimens to each for caries excavation. One-way ANOVA, Chi-square test analysis was done for comparison between groups which showed significant results with Stainless Steel Bur excavation taking less mean time when compared to other agents and Polymer Bur showed more amount of bacterial remnants after excavation whereas Carisolv and Papacarie were efficient with less dentinal tubule destruction and bacterial remnants after excavation. Further inter comparison between groups was done using Paired t-test and Fischer's Exact-test. The Mean time taken by Stainless Steel Bur excavation was found to be less and caused more amount of dentinal tubule destruction when compared to Polymer Bur, Carisolv and Papacarie. Chemo-mechanical methods found to be more efficient with lesser amount of bacterial remnants and dentinal tubule destruction after caries excavation when compared to conventional methods.

Evaluation of the Efficacy of Caries Removal Using Polymer Bur, Stainless Steel Bur, Carisolv, Papacarie – An Invitro Comparative Study

PubMed Central

Prasad, Madhu Ghanashyam; Vasa, Aron Arun Kumar; Vasanthi, Done; Ramanarayana, Boyapati; Mynampati, Praffulla

2015-01-01

Context Dental caries continues to affect a significant portion of the world population and treatment of the decay is associated with pain by many patients. Intervention and application of rotary instruments for treatment of carious lesions has often resulted in considerable removal of tooth structure. Chemo-mechanical method, a minimal invasive technique for caries removal was developed to overcome these shortcomings. This innovative method seems to be efficient in removing infected dentine without altering the healthy dental tissue or harming the adjacent oral mucosa. Aim To evaluate the efficacy and efficiency of Caries removal Using Polymer Bur, Stainless Steel Bur, Carisolv and Papacarie. Materials and Methods A total of 120 sectioned specimens were obtained from 60 extracted teeth. Each tooth was sectioned mesiodistally in the center of the carious lesion so that two halves (buccal and lingual or palatal) having equal sized carious lesions are compared. The sectioned specimens were subdivided into four groups (Polymer Bur, Stainless Steel Bur, Carisolv, Papacarie) allotting 30 specimens to each for caries excavation. Results One-way ANOVA, Chi-square test analysis was done for comparison between groups which showed significant results with Stainless Steel Bur excavation taking less mean time when compared to other agents and Polymer Bur showed more amount of bacterial remnants after excavation whereas Carisolv and Papacarie were efficient with less dentinal tubule destruction and bacterial remnants after excavation. Further inter comparison between groups was done using Paired t-test and Fischer’s Exact-test. Conclusion The Mean time taken by Stainless Steel Bur excavation was found to be less and caused more amount of dentinal tubule destruction when compared to Polymer Bur, Carisolv and Papacarie. Chemo-mechanical methods found to be more efficient with lesser amount of bacterial remnants and dentinal tubule destruction after caries excavation when compared to conventional methods. PMID:26393204

Effect of boundary conditions on thermal plume growth

NASA Astrophysics Data System (ADS)

Kondrashov, A.; Sboev, I.; Rybkin, K.

2016-07-01

We have investigated the influence of boundary conditions on the growth rate of convective plumes. Temperature and rate fields were studied in a rectangular convective cell heated by a spot heater. The results of the full-scale test were compared with the numerical data calculated using the ANSYS CFX software package. The relationship between the heat plume growth rate and heat boundary conditions, the width and height of the cell, size of heater for different kinds of liquid was established.

Cooperative and noncooperative magnetization reversal in alnicos

DOE PAGES

Skomski, Ralph; Ke, Liqin; Kramer, Matthew J.; ...

2017-02-08

Here, we investigate how magnetostatic interactions affect the coercivity of alnico-type magnets. Starting from exact micromagnetic relations, we also analyze two limits, namely cooperative reversal processes operative on short lengths scales and noncooperative reversal processes on long length scales. Furthermore, in alnicos, intrawire interactions are predominantly cooperative, whereas interwire effects are typically noncooperative. However, the transition between the regimes depends on feature size and hysteresis-loop shape, and interwire cooperative effects are largest for nearly rectangular loops. Our analysis revises the common shape-anisotropy interpretation of alnicos.

Agricultural and Ranching area, Rio Sao Francisco, Brazil

NASA Image and Video Library

1990-12-10

STS035-73-082 (2-10 Dec 1990) --- This agricultural and ranching area, Rio Sao Francisco, Brazil (13.0S, 43.5W) has been under study for several years. See scene STS-31-92-045 for comparison. This area has many small single family subsistence farms, large square and rectangular commercial farms and pastures for livestock grazing. Over the several years of observation, the number and size of farms has increased and center-pivot, swing-arm irrigation systems have been installed.

Flow dynamics in bioreactors containing tissue engineering scaffolds.

PubMed

Lawrence, Benjamin J; Devarapalli, Mamatha; Madihally, Sundararajan V

2009-02-15

Bioreactors are widely used in tissue engineering as a way to distribute nutrients within porous materials and provide physical stimulus required by many tissues. However, the fluid dynamics within the large porous structure are not well understood. In this study, we explored the effect of reactor geometry by using rectangular and circular reactors with three different inlet and outlet patterns. Geometries were simulated with and without the porous structure using the computational fluid dynamics software Comsol Multiphysics 3.4 and/or ANSYS CFX 11 respectively. Residence time distribution analysis using a step change of a tracer within the reactor revealed non-ideal fluid distribution characteristics within the reactors. The Brinkman equation was used to model the permeability characteristics with in the chitosan porous structure. Pore size was varied from 10 to 200 microm and the number of pores per unit area was varied from 15 to 1,500 pores/mm(2). Effect of cellular growth and tissue remodeling on flow distribution was also assessed by changing the pore size (85-10 microm) while keeping the number of pores per unit area constant. These results showed significant increase in pressure with reduction in pore size, which could limit the fluid flow and nutrient transport. However, measured pressure drop was marginally higher than the simulation results. Maximum shear stress was similar in both reactors and ranged approximately 0.2-0.3 dynes/cm(2). The simulations were validated experimentally using both a rectangular and circular bioreactor, constructed in-house. Porous structures for the experiments were formed using 0.5% chitosan solution freeze-dried at -80 degrees C, and the pressure drop across the reactor was monitored.

Dissolution enhancement of gliclazide using pH change approach in presence of twelve stabilizers with various physico-chemical properties.

PubMed

Talari, Roya; Varshosaz, Jaleh; Mostafavi, Seyed Abolfazl; Nokhodchi, Ali

2009-01-01

The micronization using milling process to enhance dissolution rate is extremely inefficient due to a high energy input, and disruptions in the crystal lattice which can cause physical or chemical instability. Therefore, the aim of the present study is to use in situ micronization process through pH change method to produce micron-size gliclazide particles for fast dissolution hence better bioavailability. Gliclazide was recrystallized in presence of 12 different stabilizers and the effects of each stabilizer on micromeritic behaviors, morphology of microcrystals, dissolution rate and solid state of recrystallized drug particles were investigated. The results showed that recrystallized samples showed faster dissolution rate than untreated gliclazide particles and the fastest dissolution rate was observed for the samples recrystallized in presence of PEG 1500. Some of the recrystallized drug samples in presence of stabilizers dissolved 100% within the first 5 min showing at least 10 times greater dissolution rate than the dissolution rate of untreated gliclazide powders. Micromeritic studies showed that in situ micronization technique via pH change method is able to produce smaller particle size with a high surface area. The results also showed that the type of stabilizer had significant impact on morphology of recrystallized drug particles. The untreated gliclazide is rod or rectangular shape, whereas the crystals produced in presence of stabilizers, depending on the type of stabilizer, were very fine particles with irregular, cubic, rectangular, granular and spherical/modular shape. The results showed that crystallization of gliclazide in presence of stabilizers reduced the crystallinity of the samples as confirmed by XRPD and DSC results. In situ micronization of gliclazide through pH change method can successfully be used to produce micron-sized drug particles to enhance dissolution rate.

Investigation of Dispersed and Dispersed Annular (rivulet or Thin Film) Flow Phase Separation in Tees.

NASA Astrophysics Data System (ADS)

McCreery, Glenn Ernest

An experimental and analytical investigation of dispersed and dispersed-annular (rivulet or thin film) flow phase separation in tees has been successfully completed. The research was directed at, but is not specific to, determining flow conditions, following a loss of coolant accident, in the large rectangular passageways leading to vacuum buildings in the containment envelope of some CANDU nuclear reactors. The primary objectives of the research were to: (1) obtain experimental data to help formulate and test mechanistic analytical models of phase separation, and (2) develop the analytical models in computer programs which predict phase separation from upstream flow and pressure conditions and downstream and side branch pressure boundary conditions. To meet these objectives an air-water experimental apparatus was constructed, and consists of large air blowers attached to a long rectangular duct leading to a tee in the horizontal plane. A variety of phenomena was investigated including, for comparison with computer predictions, air streamlines and eddy boundary geometry, drop size spectra, macroscopic mass balances, liquid rivulet pathlines, and trajectories of drops of known size and velocity. Four separate computer programs were developed to analyze phase separation. Three of the programs are used sequentially to calculate dispersed mist phase separation in a tee. The fourth is used to calculate rivulet or thin film pathlines. Macroscopic mass balances are calculated from a summation of mass balances for drops with representative sizes (and masses) spaced across the drop size spectrum. The programs are tested against experimental data, and accurately predict gas flow fields, drop trajectories, rivulet pathlines and macroscopic mass balances. In addition to development of the computer programs, analysis was performed to specify the scaling of dispersed mist and rivulet or thin film flow, to investigate pressure losses in tees, and the inter-relationship of loss coefficients, contraction coefficients, and eddy geometry. The important transient effects of liquid storage in eddies were also analyzed.

Articles comprising ferritic stainless steels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rakowski, James M.

An article of manufacture comprises a ferritic stainless steel that includes a near-surface region depleted of silicon relative to a remainder of the ferritic stainless steel. The article has a reduced tendency to form an electrically resistive silica layer including silicon derived from the steel when the article is subjected to high temperature oxidizing conditions. The ferritic stainless steel is selected from the group comprising AISI Type 430 stainless steel, AISI Type 439 stainless steel, AISI Type 441 stainless steel, AISI Type 444 stainless steel, and E-BRITE.RTM. alloy, also known as UNS 44627 stainless steel. In certain embodiments, the articlemore » of manufacture is a fuel cell interconnect for a solid oxide fuel cell.« less

Experimental Avalanches in a Rotating Drum

NASA Astrophysics Data System (ADS)

Hubard, Aline; O'Hern, Corey; Shattuck, Mark

We address the question of universality in granular avalanches and the system size effects on it. We set up an experiment made from a quasi-two-dimensional rotating drum half-filled with a monolayer of stainless-steel spheres. We measure the size of the avalanches created by the increased gravitational stress on the pile as we quasi-statically rotate the drum. We find two kinds of avalanches determined by the drum size. The size and duration distributions of the avalanches that do not span the whole system follow a power law and the avalanche shapes are self-similar and nearly parabolic. The distributions of the avalanches that span the whole system are limited by the maximal amount of potential energy stored in the system at the moment of the avalanche. NSF CMMI-1462439, CMMI-1463455.

76 FR 64105 - Light-Walled Rectangular Pipe From Taiwan; Scheduling of an Expedited Five-Year Review Concerning...

Federal Register 2010, 2011, 2012, 2013, 2014

2011-10-17

... INTERNATIONAL TRADE COMMISSION [Investigation No. 731-TA-410 (Third Review)] Light-Walled... Order on Light-Walled Rectangular Pipe From Taiwan AGENCY: United States International Trade Commission... determine whether revocation of the antidumping duty order on light-walled rectangular pipe from Taiwan...

77 FR 3497 - Light-Walled Rectangular Pipe and Tube From Taiwan

Federal Register 2010, 2011, 2012, 2013, 2014

2012-01-24

... INTERNATIONAL TRADE COMMISSION [Investigation No. 731-TA-410 (Third Review)] Light-Walled... order on light-walled rectangular pipe and tube from Taiwan would be likely to lead to continuation or... views of the Commission are contained in USITC Publication 4301 (January 2012), Light-Walled Rectangular...

Effective way of reducing coupling loss between rectangular microwaveguide and fiber.

PubMed

Zhou, Hang; Chen, Zilun; Xi, Xiaoming; Hou, Jing; Chen, Jinbao

2012-01-20

We introduce an anamorphic photonic crystal fiber (PCF) produced by postprocessing techniques to improve the coupling loss between a conventional single-mode fiber and rectangular microwaveguide. One end of the round core is connected with the conventional fiber, and the other end of the rectangular core is connected with the rectangular microwaveguide, then the PCF is tapered pro rata. In this way, the loss of mode mismatch between the output of the conventional fiber and the input of the waveguide would be reduced, which results in enhanced coupling efficiency. The conclusion was confirmed by numerical simulation: the new method is better than straight coupling between the optical fiber and the rectangular microwaveguide, and more than 2.8 dB improvement of coupling efficiency is achieved. © 2012 Optical Society of America

Electromagnetic Scattering from Arbitrarily Shaped Aperture Backed by Rectangular Cavity Recessed in Infinite Ground Plane

NASA Technical Reports Server (NTRS)

Cockrell, C. R.; Beck, Fred B.

1997-01-01

The electromagnetic scattering from an arbitrarily shaped aperture backed by a rectangular cavity recessed in an infinite ground plane is analyzed by the integral equation approach. In this approach, the problem is split into two parts: exterior and interior. The electromagnetic fields in the exterior part are obtained from an equivalent magnetic surface current density assumed to be flowing over the aperture and backed by an infinite ground plane. The electromagnetic fields in the interior part are obtained in terms of rectangular cavity modal expansion functions. The modal amplitudes of cavity modes are determined by enforcing the continuity of the electric field across the aperture. The integral equation with the aperture magnetic current density as an unknown is obtained by enforcing the continuity of magnetic fields across the aperture. The integral equation is then solved for the magnetic current density by the method of moments. The electromagnetic scattering properties of an aperture backed by a rectangular cavity are determined from the magnetic current density. Numerical results on the backscatter radar cross-section (RCS) patterns of rectangular apertures backed by rectangular cavities are compared with earlier published results. Also numerical results on the backscatter RCS patterns of a circular aperture backed by a rectangular cavity are presented.

Microemulsion characterization by the use of a noninvasive backscatter fiber optic probe

NASA Technical Reports Server (NTRS)

Ansari, Rafat R.; Dhadwal, Harbans S.; Cheung, H. M.; Meyer, William V.

1993-01-01

This paper demonstrates the utility of a noninvasive backscatter fiber optic probe for dynamic light-scattering characterization of a microemulsion comprising sodium dodecyl sulfate/1-butanol/ brine/heptane. The fiber probe, comprising two optical fibers precisely positioned in a stainless steel body, is a miniaturized and efficient self-beating dynamic light-scattering system. Accuracy of particle size estimation is better than +/- 2 percent.

Hexagonal Pixels and Indexing Scheme for Binary Images

NASA Technical Reports Server (NTRS)

Johnson, Gordon G.

2004-01-01

A scheme for resampling binaryimage data from a rectangular grid to a regular hexagonal grid and an associated tree-structured pixel-indexing scheme keyed to the level of resolution have been devised. This scheme could be utilized in conjunction with appropriate image-data-processing algorithms to enable automated retrieval and/or recognition of images. For some purposes, this scheme is superior to a prior scheme that relies on rectangular pixels: one example of such a purpose is recognition of fingerprints, which can be approximated more closely by use of line segments along hexagonal axes than by line segments along rectangular axes. This scheme could also be combined with algorithms for query-image-based retrieval of images via the Internet. A binary image on a rectangular grid is generated by raster scanning or by sampling on a stationary grid of rectangular pixels. In either case, each pixel (each cell in the rectangular grid) is denoted as either bright or dark, depending on whether the light level in the pixel is above or below a prescribed threshold. The binary data on such an image are stored in a matrix form that lends itself readily to searches of line segments aligned with either or both of the perpendicular coordinate axes. The first step in resampling onto a regular hexagonal grid is to make the resolution of the hexagonal grid fine enough to capture all the binaryimage detail from the rectangular grid. In practice, this amounts to choosing a hexagonal-cell width equal to or less than a third of the rectangular- cell width. Once the data have been resampled onto the hexagonal grid, the image can readily be checked for line segments aligned with the hexagonal coordinate axes, which typically lie at angles of 30deg, 90deg, and 150deg with respect to say, the horizontal rectangular coordinate axis. Optionally, one can then rotate the rectangular image by 90deg, then again sample onto the hexagonal grid and check for line segments at angles of 0deg, 60deg, and 120deg to the original horizontal coordinate axis. The net result is that one has checked for line segments at angular intervals of 30deg. For even finer angular resolution, one could, for example, then rotate the rectangular-grid image +/-45deg before sampling to perform checking for line segments at angular intervals of 15deg.

Influence of beam efficiency through the patient-specific collimator on secondary neutron dose equivalent in double scattering and uniform scanning modes of proton therapy.

PubMed

Hecksel, D; Anferov, V; Fitzek, M; Shahnazi, K

2010-06-01

Conventional proton therapy facilities use double scattering nozzles, which are optimized for delivery of a few fixed field sizes. Similarly, uniform scanning nozzles are commissioned for a limited number of field sizes. However, cases invariably occur where the treatment field is significantly different from these fixed field sizes. The purpose of this work was to determine the impact of the radiation field conformity to the patient-specific collimator on the secondary neutron dose equivalent. Using a WENDI-II neutron detector, the authors experimentally investigated how the neutron dose equivalent at a particular point of interest varied with different collimator sizes, while the beam spreading was kept constant. The measurements were performed for different modes of dose delivery in proton therapy, all of which are available at the Midwest Proton Radiotherapy Institute (MPRI): Double scattering, uniform scanning delivering rectangular fields, and uniform scanning delivering circular fields. The authors also studied how the neutron dose equivalent changes when one changes the amplitudes of the scanned field for a fixed collimator size. The secondary neutron dose equivalent was found to decrease linearly with the collimator area for all methods of dose delivery. The relative values of the neutron dose equivalent for a collimator with a 5 cm diameter opening using 88 MeV protons were 1.0 for the double scattering field, 0.76 for rectangular uniform field, and 0.6 for the circular uniform field. Furthermore, when a single circle wobbling was optimized for delivery of a uniform field 5 cm in diameter, the secondary neutron dose equivalent was reduced by a factor of 6 compared to the double scattering nozzle. Additionally, when the collimator size was kept constant, the neutron dose equivalent at the given point of interest increased linearly with the area of the scanned proton beam. The results of these experiments suggest that the patient-specific collimator is a significant contributor to the secondary neutron dose equivalent to a distant organ at risk. Improving conformity of the radiation field to the patient-specific collimator can significantly reduce secondary neutron dose equivalent to the patient. Therefore, it is important to increase the number of available generic field sizes in double scattering systems as well as in uniform scanning nozzles.

Using weighted power mean for equivalent square estimation.

PubMed

Zhou, Sumin; Wu, Qiuwen; Li, Xiaobo; Ma, Rongtao; Zheng, Dandan; Wang, Shuo; Zhang, Mutian; Li, Sicong; Lei, Yu; Fan, Qiyong; Hyun, Megan; Diener, Tyler; Enke, Charles

2017-11-01

Equivalent Square (ES) enables the calculation of many radiation quantities for rectangular treatment fields, based only on measurements from square fields. While it is widely applied in radiotherapy, its accuracy, especially for extremely elongated fields, still leaves room for improvement. In this study, we introduce a novel explicit ES formula based on Weighted Power Mean (WPM) function and compare its performance with the Sterling formula and Vadash/Bjärngard's formula. The proposed WPM formula is ESWPMa,b=waα+1-wbα1/α for a rectangular photon field with sides a and b. The formula performance was evaluated by three methods: standard deviation of model fitting residual error, maximum relative model prediction error, and model's Akaike Information Criterion (AIC). Testing datasets included the ES table from British Journal of Radiology (BJR), photon output factors (S cp ) from the Varian TrueBeam Representative Beam Data (Med Phys. 2012;39:6981-7018), and published S cp data for Varian TrueBeam Edge (J Appl Clin Med Phys. 2015;16:125-148). For the BJR dataset, the best-fit parameter value α = -1.25 achieved a 20% reduction in standard deviation in ES estimation residual error compared with the two established formulae. For the two Varian datasets, employing WPM reduced the maximum relative error from 3.5% (Sterling) or 2% (Vadash/Bjärngard) to 0.7% for open field sizes ranging from 3 cm to 40 cm, and the reduction was even more prominent for 1 cm field sizes on Edge (J Appl Clin Med Phys. 2015;16:125-148). The AIC value of the WPM formula was consistently lower than its counterparts from the traditional formulae on photon output factors, most prominent on very elongated small fields. The WPM formula outperformed the traditional formulae on three testing datasets. With increasing utilization of very elongated, small rectangular fields in modern radiotherapy, improved photon output factor estimation is expected by adopting the WPM formula in treatment planning and secondary MU check. © 2017 The Authors. Journal of Applied Clinical Medical Physics published by Wiley Periodicals, Inc. on behalf of American Association of Physicists in Medicine.

Characterization of Particulate Fume and Oxides Emission from Stainless Steel Plasma Cutting.

PubMed

Wang, Jun; Hoang, Tien; Floyd, Evan L; Regens, James L

2017-04-01

Plasma cutting is a metal fabrication process that employs an electrically conductive plasma arc to cut metals. The metal fume emitted from stainless steel plasma cutting may consist of hexavalent chromium (Cr6+), which is a carcinogen, and other toxicants. Overexposure to plasma cutting fume may cause pulmonary toxicity and other health effects. This study was to evaluate the effects of operation parameters (arc current and arc time) on the fume formation rates, Cr6+ and other oxides concentrations, particle size distributions (PSD), and particle morphology. A fume chamber and high-volume pump were used to collect fume produced from cutting ER308L stainless steel plates with arc currents varying between 20 and 50 A. The amount of fume collected on glass fiber filters was gravimetrically determined and normalized to arc time. Cr6+ and other oxides in the fume were analyzed using ion chromatography. PSD of the fume was examined using a scanning mobility particle sizer and an aerodynamic particle sizer for fine and coarse fractions, respectively. The particle morphology was imaged through a transmission electron microscope (TEM). Total fume generation rate increased with arc current and ranged from 16.5 mg min-1 at 20 A to 119.0 mg min-1 at 50 A. Cr6+ emissions (219.8-480.0 µg min-1) from the plasma cutting were higher than welding fume in a previous study. Nitrogen oxides level can be an indicator of oxidation level and Cr6+ formation (R = 0.93). Both PSD measurement and TEM images confirmed a multimodal size distribution. A high concentration of a fine fraction of particles with geometric mean sizes from 96 to 235 nm was observed. Higher arc current yielded more particles, while lower arc current was not able to penetrate the metal plates. Hence, the worker should optimize the arc current to balance cut performance and fume emission. The findings indicated that arc current was the dominant factor in fume emission from plasma cutting. Appropriate ventilation and respiratory protection should be used to reduce workers' exposure. © The Author 2017. Published by Oxford University Press on behalf of the British Occupational Hygiene Society.

The influence of nanostructured features on bacterial adhesion and bone cell functions on severely shot peened 316L stainless steel.

PubMed

Bagherifard, Sara; Hickey, Daniel J; de Luca, Alba C; Malheiro, Vera N; Markaki, Athina E; Guagliano, Mario; Webster, Thomas J

2015-12-01

Substrate grain structure and topography play major roles in mediating cell and bacteria activities. Severe plastic deformation techniques, known as efficient metal-forming and grain refining processes, provide the treated material with novel mechanical properties and can be adopted to modify nanoscale surface characteristics, possibly affecting interactions with the biological environment. This in vitro study evaluates the capability of severe shot peening, based on severe plastic deformation, to modulate the interactions of nanocrystallized metallic biomaterials with cells and bacteria. The treated 316L stainless steel surfaces were first investigated in terms of surface topography, grain size, hardness, wettability and residual stresses. The effects of the induced surface modifications were then separately studied in terms of cell morphology, adhesion and proliferation of primary human osteoblasts (bone forming cells) as well as the adhesion of multiple bacteria strains, specifically Staphylococcus aureus, Staphylococcus epidermidis, Pseudomonas aeruginosa, and ampicillin-resistant Escherichia coli. The results indicated a significant enhancement in surface work hardening and compressive residual stresses, maintenance of osteoblast adhesion and proliferation as well as a remarkable decrease in the adhesion and growth of gram-positive bacteria (S. aureus and S. epidermidis) compared to non-treated and conventionally shot peened samples. Impressively, the decrease in bacteria adhesion and growth was achieved without the use of antibiotics, for which bacteria can develop a resistance towards anyway. By slightly grinding the surface of severe shot peened samples to remove differences in nanoscale surface roughness, the effects of varying substrate grain size were separated from those of varying surface roughness. The expression of vinculin focal adhesions from osteoblasts was found to be singularly and inversely related to grain size, whereas the attachment of gram-positive bacteria (S. aureus and S. epidermidis) decreased with increasing nanoscale surface roughness, and was not affected by grain refinement. Ultimately, this study demonstrated the advantages of the proposed shot peening treatment to produce multifunctional 316L stainless steel materials for improved implant functions without necessitating the use of drugs. Copyright © 2015 Elsevier Ltd. All rights reserved.

Prediction of the Wall Factor of Arbitrary Particle Settling through Various Fluid Media in a Cylindrical Tube Using Artificial Intelligence

PubMed Central

Li, Mingzhong; Xue, Jianquan; Li, Yanchao; Tang, Shukai

2014-01-01

Considering the influence of particle shape and the rheological properties of fluid, two artificial intelligence methods (Artificial Neural Network and Support Vector Machine) were used to predict the wall factor which is widely introduced to deduce the net hydrodynamic drag force of confining boundaries on settling particles. 513 data points were culled from the experimental data of previous studies, which were divided into training set and test set. Particles with various shapes were divided into three kinds: sphere, cylinder, and rectangular prism; feature parameters of each kind of particle were extracted; prediction models of sphere and cylinder using artificial neural network were established. Due to the little number of rectangular prism sample, support vector machine was used to predict the wall factor, which is more suitable for addressing the problem of small samples. The characteristic dimension was presented to describe the shape and size of the diverse particles and a comprehensive prediction model of particles with arbitrary shapes was established to cover all types of conditions. Comparisons were conducted between the predicted values and the experimental results. PMID:24772024

Velocity-based analysis of sediment incipient deposition in rigid boundary open channels.

PubMed

Aksoy, Hafzullah; Safari, Mir Jafar Sadegh; Unal, Necati Erdem; Mohammadi, Mirali

2017-11-01

Drainage systems must be designed in a way to minimize undesired problems such as decrease in hydraulic capacity of the channel, blockage and transport of pollutants due to deposition of sediment. Channel design considering self-cleansing criteria are used to solve the sedimentation problem. Incipient deposition is one of the non-deposition self-cleansing design criteria that can be used as a conservative method for channel design. Experimental studies have been carried out in five different cross-section channels, namely trapezoidal, rectangular, circular, U-shape and V-bottom. Experiments were performed in a tilting flume using four different sizes of sands as sediment in nine different channel bed slopes. Two well-known methods, namely the Novak & Nalluri and Yang methods are considered for the analysis of sediment motion. Equations developed using experimental data are found to be in agreement with the literature. It is concluded that the design velocity depends on the shape of the channel cross-section. Rectangular and V-bottom channels need lower and higher incipient deposition velocities, respectively, in comparison with other channels.

Prediction of the wall factor of arbitrary particle settling through various fluid media in a cylindrical tube using artificial intelligence.

PubMed

Li, Mingzhong; Zhang, Guodong; Xue, Jianquan; Li, Yanchao; Tang, Shukai

2014-01-01

Considering the influence of particle shape and the rheological properties of fluid, two artificial intelligence methods (Artificial Neural Network and Support Vector Machine) were used to predict the wall factor which is widely introduced to deduce the net hydrodynamic drag force of confining boundaries on settling particles. 513 data points were culled from the experimental data of previous studies, which were divided into training set and test set. Particles with various shapes were divided into three kinds: sphere, cylinder, and rectangular prism; feature parameters of each kind of particle were extracted; prediction models of sphere and cylinder using artificial neural network were established. Due to the little number of rectangular prism sample, support vector machine was used to predict the wall factor, which is more suitable for addressing the problem of small samples. The characteristic dimension was presented to describe the shape and size of the diverse particles and a comprehensive prediction model of particles with arbitrary shapes was established to cover all types of conditions. Comparisons were conducted between the predicted values and the experimental results.

Improved GO/PO method and its application to wideband SAR image of conducting objects over rough surface

NASA Astrophysics Data System (ADS)

Jiang, Wang-Qiang; Zhang, Min; Nie, Ding; Jiao, Yong-Chang

2018-04-01

To simulate the multiple scattering effect of target in synthetic aperture radar (SAR) image, the hybrid method GO/PO method, which combines the geometrical optics (GO) and physical optics (PO), is employed to simulate the scattering field of target. For ray tracing is time-consuming, the Open Graphics Library (OpenGL) is usually employed to accelerate the process of ray tracing. Furthermore, the GO/PO method is improved for the simulation in low pixel situation. For the improved GO/PO method, the pixels are arranged corresponding to the rectangular wave beams one by one, and the GO/PO result is the sum of the contribution values of all the rectangular wave beams. To get high-resolution SAR image, the wideband echo signal is simulated which includes information of many electromagnetic (EM) waves with different frequencies. Finally, the improved GO/PO method is used to simulate the SAR image of targets above rough surface. And the effects of reflected rays and the size of pixel matrix on the SAR image are also discussed.

Transurethral illumination probe design for deep photoacoustic imaging of prostate

NASA Astrophysics Data System (ADS)

Ai, Min; Salcudean, Tim; Rohling, Robert; Abolmaesumi, Purang; Tang, Shuo

2018-02-01

Photoacoustic (PA) imaging with internal light illumination through optical fiber could enable imaging of internal organs at deep penetration. We have developed a transurethral probe with a multimode fiber inserted in a rigid cystoscope sheath for illuminating the prostate. At the distal end, the fiber tip is processed to diffuse light circumferentially over 2 cm length. A parabolic cylinder mirror then reflects the light to form a rectangular-shaped parallel beam which has at least 1 cm2 at the probe surface. The relatively large rectangular beam size can reduce the laser fluence rate on the urethral wall and thus reduce the potential of tissue damage. A 3 cm optical penetration in chicken tissue is achieved at a fluence rate around 7 mJ/cm2 . For further validation, a prostate phantom was built with similar optical properties of the human prostate. A 1.5 cm penetration depth is achieved in the prostate mimicking phantom at 10 mJ/cm2 fluence rate. PA imaging of prostate can potentially be carried out in the future by combining a transrectal ultrasound transducer and the transurethral illumination.

An experimental study of the vortex wake at Mach number of 3

NASA Astrophysics Data System (ADS)

Shmakov, A. S.; Shevchenko, A. M.

2017-10-01

The results of experimental study of the flow in the wing wake at Mach number of 3 are presented. These experiments extends the data obtained in the same experimental setup at Mach numbers of 2.5 and 4 [1]. Experiments were carried out in supersonic wind tunnel T-325 of ITAM SB RAS. Rectangular half-wing with sharp edges with a chord length of 30 mm and semispan of 95 mm was used to generate vortex wake. Experimental data were obtained in two cross sections located 1.5 and 6 chord length downstream of the trailing edge at wing angle of attack of 10 degrees. Constant temperature hot-wire anemometer was used to measure disturbances in supersonic flow. Hot-wire aemometer was made of a tungsten wire with a diameter of 10 µm and length of 1.5 mm. Shlieren flow visualization were performed. As a result, the position and size of the vortex core in the wake of a rectangular wing were determined. For the first time mass flow distribution and its pulsations in the supersonic longitudinal vortex was measured at Mach number of 3.

Metal Standards for Waveguide Characterization of Materials

NASA Technical Reports Server (NTRS)

Lambert, Kevin M.; Kory, Carol L.

2009-01-01

Rectangular-waveguide inserts that are made of non-ferromagnetic metals and are sized and shaped to function as notch filters have been conceived as reference standards for use in the rectangular- waveguide method of characterizing materials with respect to such constitutive electromagnetic properties as permittivity and permeability. Such standards are needed for determining the accuracy of measurements used in the method, as described below. In this method, a specimen of a material to be characterized is cut to a prescribed size and shape and inserted in a rectangular- waveguide test fixture, wherein the specimen is irradiated with a known source signal and detectors are used to measure the signals reflected by, and transmitted through, the specimen. Scattering parameters [also known as "S" parameters (S11, S12, S21, and S22)] are computed from ratios between the transmitted and reflected signals and the source signal. Then the permeability and permittivity of the specimen material are derived from the scattering parameters. Theoretically, the technique for calculating the permeability and permittivity from the scattering parameters is exact, but the accuracy of the results depends on the accuracy of the measurements from which the scattering parameters are obtained. To determine whether the measurements are accurate, it is necessary to perform comparable measurements on reference standards, which are essentially specimens that have known scattering parameters. To be most useful, reference standards should provide the full range of scattering-parameter values that can be obtained from material specimens. Specifically, measurements of the backscattering parameter (S11) from no reflection to total reflection and of the forward-transmission parameter (S21) from no transmission to total transmission are needed. A reference standard that functions as a notch (band-stop) filter can satisfy this need because as the signal frequency is varied across the frequency range for which the filter is designed, the scattering parameters vary over the ranges of values between the extremes of total reflection and total transmission. A notch-filter reference standard in the form of a rectangular-waveguide insert that has a size and shape similar to that of a material specimen is advantageous because the measurement configuration used for the reference standard can be the same as that for a material specimen. Typically a specimen is a block of material that fills a waveguide cross-section but occupies only a small fraction of the length of the waveguide. A reference standard of the present type (see figure) is a metal block that fills part of a waveguide cross section and contains a slot, the long dimension of which can be chosen to tailor the notch frequency to a desired value. The scattering parameters and notch frequency can be estimated with high accuracy by use of commercially available electromagnetic-field-simulating software. The block can be fabricated to the requisite precision by wire electrical-discharge machining. In use, the accuracy of measurements is determined by comparison of (1) the scattering parameters calculated from the measurements with (2) the scattering parameters calculated by the aforementioned software.

Remote detection of stress corrosion cracking: Surface composition and crack detection

NASA Astrophysics Data System (ADS)

Lissenden, Cliff J.; Jovanovic, Igor; Motta, Arthur T.; Xiao, Xuan; Le Berre, Samuel; Fobar, David; Cho, Hwanjeong; Choi, Sungho

2018-04-01

Chloride induced stress corrosion cracking (SCC) of austenitic stainless steel is a potential issue in long term dry storage of spent nuclear fuel canisters. In order for SCC to occur there must be a corrosive environment, a susceptible material, and a driving force. Because it is likely that the material in the heat affected zone (HAZ) of welded stainless steel structures has been sensitized as a result of chromium depletion at the grain boundaries and a thermal residual stress driving force is likely present if solution annealing is not performed, two issues are critical. Is the environment corrosive, i.e., are chlorides present in solution on the surface? And then, are there cracks that could propagate? Remote detection of chlorides on the surface can be accomplished by laser induced breakdown spectroscopy (LIBS), while cracks can be detected by shear horizontal guided waves generated by electromagnetic acoustic transducers (EMATs). Both are noncontact methods that are amenable to robotic delivery systems and harsh environments. The sensitivity to chlorine on stainless steel of a LIBS system that employs optical fiber for pulse delivery is demonstrated. Likewise, the ability of the EMAT system to detect cracks of a prescribed size and orientation is shown. These results show the potential for remote detection of Cl and cracks in dry storage spent fuel canisters.

Interfacial Phenomena in Fe/Stainless Steel-TiC Systems and the Effect of Mo

NASA Astrophysics Data System (ADS)

Kiviö, Miia; Holappa, Lauri; Yoshikawa, Takeshi; Tanaka, Toshihiro

2014-12-01

Titanium carbide is used as reinforcement particles in composites due to its hardness, wear resistance and stability. This work is a part of the study in which titanium carbides are formed in stainless steel castings in the mold to improve the wear resistance of a certain surface of the casting. Such local reinforcement is a very potential method but it is a quite demanding task requiring profound knowledge of interfacial phenomena in the system, wettability, stability, dissolution and precipitation of new phases in production of these materials. Good wetting between different constituents in the material is a key factor to attain maximal positive effects. Mo is used with TiC or Ti(C,N) reinforcement in composites to improve wettability. In this work the effect of Mo on the phenomena in Fe/stainless steel-TiC systems was examined by wetting experiments between the substrate and the alloy. Wetting was not significantly improved by adding Mo to the systems. Core-rim type carbides as well as more homogenous carbide particles were observed. Overall the carbide particles are very complex regarding to their chemistry, size and shape which aspects have to be taken into account in the development of these materials and manufacturing processes.

Influence of Austenitizing Heat Treatment on the Properties of the Tempered Type 410-1Mo Stainless Steel

NASA Astrophysics Data System (ADS)

Mabruri, E.; Syahlan, Z. A.; Sahlan; Prifiharni, S.; Anwar, M. S.; Chandra, S. A.; Romijarso, T. B.; Adjiantoro, B.

2017-05-01

The modified 410-1Mo stainless steel has been developed with higher tensile strength and elongation compared to the standard 410 stainless steel. This paper reports the influence of austenitizing temperature on the microstructure, hardness, impact resistance and corrosion resistance of the modified 410-1Mo steel. The steel samples were prepared by a process sequence of induction melting, hot forging, annealing, hardening, and tempering. The microstructure of the tempered steels revealed additional phase of delta ferrite at pre-austenitizing temperatures of 950 to 1050 °C and disappeared at a temperature of 1100 °C. The steels which underwent pre-austenitizing at 1100 °C showed the largest sized lath martensite and the largest amount of retained austenite. The tempered steels maintained hardness at austenitizing temperatures of 950 °C to 1000 °C and showed an increasing hardness at austenitizing temperatures from 1000 to 1100 °C. At a range of austenitizing temperatures, it was investigated that the steels exhibited higher impact resistance at 1050 °C. The tempered steels that were pre-austenitized at 950 °C and 1100 °C showed the lowest pitting potential due to the existence of carbides and coarse-high carbon martensite, respectively.

Characterization of Heat Treated Titanium-Based Implants by Nondestructive Eddy Current and Ultrasonic Tests

NASA Astrophysics Data System (ADS)

Mutlu, Ilven; Ekinci, Sinasi; Oktay, Enver

2014-06-01

This study presents nondestructive characterization of microstructure and mechanical properties of heat treated Ti, Ti-Cu, and Ti-6Al-4V titanium-based alloys and 17-4 PH stainless steel alloy for biomedical implant applications. Ti, Ti-Cu, and 17-4 PH stainless steel based implants were produced by powder metallurgy. Ti-6Al-4V alloy was investigated as bulk wrought specimens. Effects of sintering temperature, aging, and grain size on mechanical properties were investigated by nondestructive and destructive tests comparatively. Ultrasonic velocity in specimens was measured by using pulse-echo and transmission methods. Electrical conductivity of specimens was determined by eddy current tests. Determination of Young's modulus and strength is important in biomedical implants. Young's modulus of specimens was calculated by using ultrasonic velocities. Calculated Young's modulus values were compared and correlated with experimental values.

Effects of Static Recrystallization and Precipitation on Mechanical Properties of 00Cr12 Ferritic Stainless Steel

NASA Astrophysics Data System (ADS)

Shao, Yi; Liu, Chenxi; Yue, Tengxiao; Liu, Yongchang; Yan, Zesheng; Li, Huijun

2018-05-01

The 00Cr12 ferritic stainless steel samples were isothermally held at different temperatures in the range of 700 °C to 1000 °C to investigate the effect of static recrystallization and precipitation on mechanical properties, such as microhardness, tensile strength, and yield strength. The results show that the formation of the fine recrystallized grain, as well as precipitation, coarsening, and dissolution of the second-phase particles, influences the mechanical properties remarkably. The fine recrystallized grain can provide a positive grain boundary-strengthening effect in the sample under a relatively high holding temperature. Coarsening and dissolution of M23C6 result in partial depletion of precipitate hardening. In contrast, the size and number density of MX particles are almost constant, regardless of the holding temperature; therefore, it can provide a better precipitation-hardening effect.

[Experimental study on carbon fiber reinforced plastic plate--analysis of stabilizing force required for plate].

PubMed

Iizuka, H

1990-11-01

Plates currently in use for the management of bone fracture made of metal present with various problems. We manufactured carbon fiber reinforced plastic (CFRP) plates from Pyrofil T/530 puriplegs overlaid at cross angles of +/- 10 degrees, +/- 20 degrees, and +/- 30 degrees for trial and carried out an experimental study on rabbit tibiofibular bones using 316L stainless steel plates of comparable shape and size as controls. The results indicate the influence of CFRP plate upon cortical bone was milder than that of stainless steel plate, with an adequate stabilizing force for the repair of fractured rabbit tibiofibular bones. CFRP has the advantages over metals of being virtually free from corrosion and fatigue, reasonably radiolucent and able to meet a wide range of mechanical requirements. This would make CFRP plate quite promising as a new devices of treating fracture of bones.

Parametric study for use of stainless steel as a material for thermal shield in PIP2IT transferline at Fermilab

NASA Astrophysics Data System (ADS)

Rane, Tejas; Chakravarty, Anindya; Klebaner, Arkadiy

2017-12-01

Transferline thermal shields are cooled by dedicated cooling lines welded/brazed to the shield at a single point along the circumference. Copper/Aluminium is widely used to fabricate thermal shields because of their higher thermal diffusivity. This causes uniformity of temperature along the surface of the shield thus reducing thermal stresses within allowable values. However, factors such as raw material price, the cost of fabrication depending on standard sizes of pipes/tubes, often drives up the final price of thermal shields. To reduce the cost by making use of easily available stock of standard pipe/tube, it is decided to use stainless steel as a material for thermal shields in the PIP2IT transferline. The present paper discusses the design approach, various factors affecting the conservative selection of thermal shield design.

Influence of airflow rate and substrate nature on heterogeneous struvite precipitation.

PubMed

Saidou, H; Ben Moussa, S; Ben Amor, M

2009-01-01

In wastewater treatment plants a hard scale consisting of struvite crystals can be formed, in pipes and recirculation pumps, during anaerobic digestion of wastewater. This study was conducted to evaluate the effect of airflow rate and substrate nature on nucleation type, induction period and supersaturation coefficient during struvite precipitation. A crystallization reactor similar to that designed for calcium carbonate precipitation was used. The pH of synthetic wastewater solution was increased by air bubbling. Experimental results indicated that the airflow increased heterogeneous precipitation of struvite. The susceptibility to scale formation was more important on polyamide and polyvinyl chloride than on stainless steel. In all cases, X-ray diffraction and infrared spectroscopy showed that the precipitated solid phase was solely struvite. No difference in crystal morphology was observed. However, at similar experimental conditions, the particle size of struvite was higher for stainless-steel material than that for plastic materials.

Modification of surface properties of solids by femtosecond LIPSS writing: comparative studies on silicon and stainless steel

NASA Astrophysics Data System (ADS)

Varlamova, Olga; Hoefner, Kevin; Ratzke, Markus; Reif, Juergen; Sarker, Debasish

2017-12-01

We investigate the implication of modified surface morphology on wettability of stainless steel (AISI 304) and silicon (100) targets covered by laser-induced periodic surface structures (LIPSS) on extended areas (10 × 10 mm2). Using multiple pulses from a Ti: Sapphire laser (790 nm/100 fs/1 kHz) at a fluence in the range of 0.35-2.1 J/cm2 on a spot of 1.13 × 10- 4 cm2, we scanned the target under the spot to cover a large area. A systematical variation of the irradiation dose by changing the scanning speed and thus dwelling time per spot results in the formation of surface patterns ranging from very regular linear structures with a lateral period of about 500-600 nm to complex patterns of 3D microstructures with several-µm feature size, hierarchically covered by nano-ripples.

Application of nonlinear ultrasonics to inspection of stainless steel for dry storage

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ulrich, Timothy James II; Anderson, Brain E.; Remillieux, Marcel C.

This report summarized technical work conducted by LANL staff an international collaborators in support of the UFD Storage Experimentation effort. The focus of the current technical work is on the detection and imaging of a failure mechanism known as stress corrosion cracking (SCC) in stainless steel using the nonlinear ultrasonic technique known as TREND. One of the difficulties faced in previous work is in finding samples that contain realistically sized SCC. This year such samples were obtained from EPRI. Reported here are measurements made on these samples. One of the key findings is the ability to detect subsurface changes tomore » the direction in which a crack is penetrating into the sample. This result follows from last year's report that demonstrated the ability of TREND techniques to image features below the sample surface. A new collaboration was established with AGH University of Science and Technology, Krakow, Poland.« less

Automatic Welding of Stainless Steel Tubing

NASA Technical Reports Server (NTRS)

Clautice, W. E.

1978-01-01

To determine if the use of automatic welding would allow reduction of the radiographic inspection requirement, and thereby reduce fabrication costs, a series of welding tests were performed. In these tests an automatic welder was used on stainless steel tubing of 1/2, 3/4, and 1/2 inch diameter size. The optimum parameters were investigated to determine how much variation from optimum in machine settings could be tolerate and still result in a good quality weld. The process variables studied were the welding amperes, the revolutions per minute as a function of the circumferential weld travel speed, and the shielding gas flow. The investigation showed that the close control of process variables in conjunction with a thorough visual inspection of welds can be relied upon as an acceptable quality assurance procedure, thus permitting the radiographic inspection to be reduced by a large percentage when using the automatic process.

Two-Phase Flow in Microchannels with Non-Circular Cross Section

NASA Astrophysics Data System (ADS)

Eckett, Chris A.; Strumpf, Hal J.

2002-11-01

Two-phase flow in microchannels is of practical importance in several microgravity space technology applications. These include evaporative and condensing heat exchangers for thermal management systems and vapor cycle systems, phase separators, and bioreactors. The flow passages in these devices typically have a rectangular cross-section or some other non-circular cross-section; may include complex flow paths with branches, merges and bends; and may involve channel walls of different wettability. However, previous experimental and analytical investigations of two-phase flow in reduced gravity have focussed on straight, circular tubes. This study is an effort to determine two-phase flow behavior, both with and without heat transfer, in microchannel configurations other than straight, circular tubes. The goals are to investigate the geometrical effects on flow pattern, pressure drop and liquid holdup, as well as to determine the relative importance of capillary, surface tension, inertial, and gravitational forces in such geometries. An evaporative heat exchanger for microgravity thermal management systems has been selected as the target technology in this investigation. Although such a heat exchanger has never been developed at Honeywell, a preliminary sizing has been performed based on knowledge of such devices in normal gravity environments. Fin shapes considered include plain rectangular, offset rectangular, and wavy fin configurations. Each of these fin passages represents a microchannel of non-circular cross section. The pans at the inlet and outlet of the heat exchanger are flow branches and merges, with up to 90-deg bends. R-134a has been used as the refrigerant fluid, although ammonia may well be used in the eventual application.

Nonionic Fluorinated Surfactant Removal from Mesoporous Film Using sc-CO2.

PubMed

Chavez Panduro, Elvia A; Assaker, Karine; Beuvier, Thomas; Blin, Jean-Luc; Stébé, Marie-José; Konovalov, Oleg; Gibaud, Alain

2017-01-25

Surfactant templated silica thin films were self-assembled on solid substrates by dip-coating using a partially fluorinated surfactant R 8 F (EO) 9 as the liquid crystal template. The aim was 2-fold: first we checked which composition in the phase diagram was corresponding to a 2D rectangular highly ordered crystalline phase and second we exposed the films to sc-CO 2 to foster the removal of the surfactant. The films were characterized by in situ X-ray reflectivity (XRR) and grazing incidence small angle X-ray scattering (GISAXS) under CO 2 pressure from 0 to 100 bar at 34 °C. GISAXS patterns reveal the formation of a 2-D rectangular structure at a molar ratio R 8 F (EO) 9 /Si equal to 0.1. R 8 F (EO) 9 micelles have a cylindrical shape, which have a core/shell structure ordered in a hexagonal system. The core contains the R 8 F part and the shell is a mixture of (EO) 9 embedded in the silica matrix. We further evidence that the extraction of the template using supercritical carbon dioxide can be successfully achieved. This can be attributed to both the low solubility parameter of the surfactants and the fluorine and ethylene oxide CO 2 -philic groups. The initial 2D rectangular structure was well preserved after depressurization of the cell and removal of the surfactant. We attribute the very high stability of the rinsed film to the large value of the wall thickness relatively to the small pore size.

High-performance mushroom plasmonic metamaterial absorbers for infrared polarimetric imaging

NASA Astrophysics Data System (ADS)

Ogawa, Shinpei; Fujisawa, Daisuke; Hata, Hisatoshi; Uetsuki, Mitsuharu; Kuboyama, Takafumi; Kimata, Masafumi

2017-02-01

Infrared (IR) polarimetric imaging is a promising approach to enhance object recognition with conventional IR imaging for applications such as artificial object recognition from the natural environment and facial recognition. However, typical infrared polarimetric imaging requires the attachment of polarizers to an IR camera or sensor, which leads to high cost and lower performance caused by their own IR radiation. We have developed asymmetric mushroom plasmonic metamaterial absorbers (A-MPMAs) to address this challenge. The A-MPMAs have an all-Al construction that consists of micropatches and a reflector layer connected with hollow rectangular posts. The asymmetric-shaped micropatches lead to strong polarization-selective IR absorption due to localized surface plasmon resonance at the micropatches. The operating wavelength region can be controlled mainly by the micropatch and the hollow rectangular post size. AMPMAs are complicated three-dimensional structures, the fabrication of which is challenging. Hollow rectangular post structures are introduced to enable simple fabrication using conventional surface micromachining techniques, such as sacrificial layer etching, with no degradation of the optical properties. The A-MPMAs have a smaller thermal mass than metal-insulator-metal based metamaterials and no influence of the strong non-linear dispersion relation of the insulator materials constant, which produces a gap in the wavelength region and additional absorption insensitive to polarization. A-MPMAs are therefore promising candidates for uncooled IR polarimetric image sensors in terms of both their optical properties and ease of fabrication. The results presented here are expected to contribute to the development of highperformance polarimetric uncooled IR image sensors that do not require polarizers.

Strain-Annealing Based Grain Boundary Engineering to Evaluate its Sole Implication on Intergranular Corrosion in Extra-Low Carbon Type 304L Austenitic Stainless Steel

NASA Astrophysics Data System (ADS)

Pradhan, S. K.; Bhuyan, P.; Kaithwas, C.; Mandal, Sumantra

2018-05-01

Strain-annealing based thermo-mechanical processing has been performed to promote grain boundary engineering (GBE) in an extra-low carbon type austenitic stainless steel without altering the grain size and residual strain to evaluate its sole influence on intergranular corrosion. Single-step processing comprising low pre-strain ( 5 and 10 pct) followed by annealing at 1273 K for 1 hour have resulted in a large fraction of Σ3 n boundaries and significant disruption in random high-angle grain boundaries (RHAGBs) connectivity. This is due to the occurrence of prolific multiple twinning in these specimens as confirmed by their large twin-related domain and twin-related grain size ratio. Among the iterative processing, the schedule comprising two cycles of 10 and 5 pct deformation followed by annealing at 1173 K for 1 hour has yielded the optimum GBE microstructure with the grain size and residual strain akin to the as-received condition. The specimens subjected to the higher number of iterations failed to realize GBE microstructures due to the occurrence of partial recrystallization. Owing to the optimum grain boundary character distribution, the GBE specimen has exhibited remarkable resistance against sensitization and intergranular corrosion as compared to the as-received condition. Furthermore, the lower depth of percolation in the GBE specimen is due to the significant disruption of RHAGBs connectivity as confirmed from its large twin-related domain and lower fractal dimension.

Strain-Annealing Based Grain Boundary Engineering to Evaluate its Sole Implication on Intergranular Corrosion in Extra-Low Carbon Type 304L Austenitic Stainless Steel

NASA Astrophysics Data System (ADS)

Pradhan, S. K.; Bhuyan, P.; Kaithwas, C.; Mandal, Sumantra

2018-07-01

Strain-annealing based thermo-mechanical processing has been performed to promote grain boundary engineering (GBE) in an extra-low carbon type austenitic stainless steel without altering the grain size and residual strain to evaluate its sole influence on intergranular corrosion. Single-step processing comprising low pre-strain ( 5 and 10 pct) followed by annealing at 1273 K for 1 hour have resulted in a large fraction of Σ3 n boundaries and significant disruption in random high-angle grain boundaries (RHAGBs) connectivity. This is due to the occurrence of prolific multiple twinning in these specimens as confirmed by their large twin-related domain and twin-related grain size ratio. Among the iterative processing, the schedule comprising two cycles of 10 and 5 pct deformation followed by annealing at 1173 K for 1 hour has yielded the optimum GBE microstructure with the grain size and residual strain akin to the as-received condition. The specimens subjected to the higher number of iterations failed to realize GBE microstructures due to the occurrence of partial recrystallization. Owing to the optimum grain boundary character distribution, the GBE specimen has exhibited remarkable resistance against sensitization and intergranular corrosion as compared to the as-received condition. Furthermore, the lower depth of percolation in the GBE specimen is due to the significant disruption of RHAGBs connectivity as confirmed from its large twin-related domain and lower fractal dimension.

Chemomechanical preparation by hand instrumentation and by Mtwo engine-driven rotary files, an ex vivo study.

PubMed

Krajczár, Károly; Tigyi, Zoltán; Papp, Viktória; Marada, Gyula; Sára, Jeges; Tóth, Vilmos

2012-07-01

To compare the disinfecting efficacy of the sodium hypochlorite irrigation by root canal preparation with stainless steel hand files, taper 0.02 and nickel-titanium Mtwo files with taper 0.04-0.06. 40 extracted human teeth were sterilized, and then inoculated with Enterococcus faecalis (ATCC 29212). After 6 day incubation time the root canals were prepared by hand with K-files (n=20) and by engine-driven Mtwo files (VDW, Munich, Germany) (n=20). Irrigation was carried out with 2.5% NaOCl in both cases. Samples were taken and determined in colony forming units (CFU) from the root canals before and after the preparation with instruments #25 and #35. Significant reduction in bacterial count was determined after filing at both groups. The number of bacteria kept on decreasing with the extension of apical preparation diameter. There was no significant difference between the preparation sizes in the bacterial counts after hand or engine-driven instrumentation at the same apical size. Statistical analysis was carried out with Mann-Whitney test, paired t-test and independent sample t-test. Significant reduction in CFU was achieved after the root canal preparation completed with 2.5% NaOCl irrigation, both with stainless steel hand or nickel-titanium rotary files. The root canal remained slightly infected after chemo mechanical preparation in both groups. Key words:Chemomechanical preparation, root canal disinfection, nickel-titanium, conicity, greater taper, apical size.

Chemomechanical preparation by hand instrumentation and by Mtwo engine-driven rotary files, an ex vivo study

PubMed Central

Krajczár, Károly; Tigyi, Zoltán; Papp, Viktória; Sára, Jeges; Tóth, Vilmos

2012-01-01

Objective: To compare the disinfecting efficacy of the sodium hypochlorite irrigation by root canal preparation with stainless steel hand files, taper 0.02 and nickel-titanium Mtwo files with taper 0.04-0.06. Study Design: 40 extracted human teeth were sterilized, and then inoculated with Enterococcus faecalis (ATCC 29212). After 6 day incubation time the root canals were prepared by hand with K-files (n=20) and by engine-driven Mtwo files (VDW, Munich, Germany) (n=20). Irrigation was carried out with 2.5% NaOCl in both cases. Samples were taken and determined in colony forming units (CFU) from the root canals before and after the preparation with instruments #25 and #35. Results: Significant reduction in bacterial count was determined after filing at both groups. The number of bacteria kept on decreasing with the extension of apical preparation diameter. There was no significant difference between the preparation sizes in the bacterial counts after hand or engine-driven instrumentation at the same apical size. Statistical analysis was carried out with Mann-Whitney test, paired t-test and independent sample t-test. Conclusions: Significant reduction in CFU was achieved after the root canal preparation completed with 2.5% NaOCl irrigation, both with stainless steel hand or nickel-titanium rotary files. The root canal remained slightly infected after chemo mechanical preparation in both groups. Key words:Chemomechanical preparation, root canal disinfection, nickel-titanium, conicity, greater taper, apical size. PMID:24558545

A new beam theory using first-order warping functions

NASA Technical Reports Server (NTRS)

Ie, C. A.; Kosmatka, J. B.

1990-01-01

Due to a certain type of loading and geometrical boundary conditions, each beam will respond differently depending on its geometrical form of the cross section and its material definition. As an example, consider an isotropic rectangular beam under pure bending. Plane sections perpendicular to the longitudinal axis of the beam will remain plane and perpendicular to the deformed axis after deformation. However, due to the Poisson effect, particles in the planes will move relative to each other resulting in a form of anticlastic deformation. In other words, even in pure bending of an isotropic beam, each cross section will deform in the plane. If the material of the beam above is replaced by a generally anisotropic material, then the cross sections will not only deform in the plane, but also out of plane. Hence, in general, both in-plane deformation and out-of-plane warping will exist and depend on the geometrical form and material definition of the cross sections and also on the loadings. For the purpose of explanation, an analogy is made. The geometrical forms of the bodies of each individual are unique. Hence, different sizes of clothes are needed. Finding the sizes of clothes for individuals is like determining the warping functions in beams. A new beam theory using first-order warping functions is introduced. Numerical examples will be presented for an isotropic beam with rectangular cross section. The theory can be extended for composite beams.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Lifeng, E-mail: walfe@nuaa.edu.cn; Hu, Haiyan

The thermal vibration of a rectangular single-layered graphene sheet is investigated by using a rectangular nonlocal elastic plate model with quantum effects taken into account when the law of energy equipartition is unreliable. The relation between the temperature and the Root of Mean Squared (RMS) amplitude of vibration at any point of the rectangular single-layered graphene sheet in simply supported case is derived first from the rectangular nonlocal elastic plate model with the strain gradient of the second order taken into consideration so as to characterize the effect of microstructure of the graphene sheet. Then, the RMS amplitude of thermalmore » vibration of a rectangular single-layered graphene sheet simply supported on an elastic foundation is derived. The study shows that the RMS amplitude of the rectangular single-layered graphene sheet predicted from the quantum theory is lower than that predicted from the law of energy equipartition. The maximal relative difference of RMS amplitude of thermal vibration appears at the sheet corners. The microstructure of the graphene sheet has a little effect on the thermal vibrations of lower modes, but exhibits an obvious effect on the thermal vibrations of higher modes. The quantum effect is more important for the thermal vibration of higher modes in the case of smaller sides and lower temperature. The relative difference of maximal RMS amplitude of thermal vibration of a rectangular single-layered graphene sheet decreases monotonically with an increase of temperature. The absolute difference of maximal RMS amplitude of thermal vibration of a rectangular single-layered graphene sheet increases slowly with the rising of Winkler foundation modulus.« less

Hollow nanotubular toroidal polymer microrings.

PubMed

Lee, Jiyeong; Baek, Kangkyun; Kim, Myungjin; Yun, Gyeongwon; Ko, Young Ho; Lee, Nam-Suk; Hwang, Ilha; Kim, Jeehong; Natarajan, Ramalingam; Park, Chan Gyung; Sung, Wokyung; Kim, Kimoon

2014-02-01

Despite the remarkable progress made in the self-assembly of nano- and microscale architectures with well-defined sizes and shapes, a self-organization-based synthesis of hollow toroids has, so far, proved to be elusive. Here, we report the synthesis of polymer microrings made from rectangular, flat and rigid-core monomers with anisotropically predisposed alkene groups, which are crosslinked with each other by dithiol linkers using thiol-ene photopolymerization. The resulting hollow toroidal structures are shape-persistent and mechanically robust in solution. In addition, their size can be tuned by controlling the initial monomer concentrations, an observation that is supported by a theoretical analysis. These hollow microrings can encapsulate guest molecules in the intratoroidal nanospace, and their peripheries can act as templates for circular arrays of metal nanoparticles.

Gravitational effects on weld pool shape and microstructural evolution during gas tungsten arc and laser beam welding on 304 stainless steel, nickel, and aluminum-4 wt.% copper alloy

NASA Astrophysics Data System (ADS)

Kang, Namhyun

The objective of the present work was to investigate effects of gravitational (acceleration) level and orientation on Ni 200 alloy (99.5% Ni purity), 304 stainless steel, and Al-4 wt.% Cu alloy during gas tungsten arc welding (GTAW) and laser beam welding (LBW). Main characterization was focused on the weld pool shape, microstructure, and solute distribution as a function of gravitational level and orientation. The welds were divided into two classes, i.e., 'stable' and 'unstable' welds, in view of the variation of weld pool shape as a function of gravitational level and orientation. In general, higher arc current and translational GTAW produced more significant effects of gravitational orientation on the weld pool shape than the case of lower arc current and spot welding. Cross-sectional area (CSA) was a secondary factor in determining the stability of weld pool shape. For the 'stable' weld of 304 stainless steel GTAW, the II-U weld showed less convexity in the pool bottom and more depression of the free surface, therefore producing deeper penetration (10--20%) than the case of II-D weld. The II-D weld of 304 stainless steel showed 31% deeper penetration, 28% narrower width, and more hemispherical shape of the weld pool than the case of II-U weld. For GTAW on 304 stainless steel, gravitational level variation from low gravity (LG ≈ 1.2 go) to high gravity (HG ≈ 1.8 go) caused 10% increase in width and 10% decrease in depth while maintaining the overall weld pool volume. Furthermore, LBW on 304 stainless steels showed mostly constant shape of weld pool as a function of gravitational orientation. GTAW on Ni showed similar trends of weld pool shape compared with GTAW on 304 stainless steel, i.e., the weld pool became unstable by showing more penetration in the II-D weld for slower arc translational velocity (V a) and larger weld pool size. However, the Ni weld pool shape had greater stability of the weld pool shape with respect to the gravitational orientation than the case of 304 stainless steel, i.e., higher current boundary and no humping. Regardless of the gravitational level, the ferrite content and the distribution of the solutes (Cr and Ni) remained constant for GTAW on 304 stainless steel. However, for GTAW on Al-4 wt.% Cu alloys, the gravitational orientation changed the weld pool shape associated with convection flows. In summary, gravity influenced the weld pool shape that was associated with convection flows and weld surface deformation for specific welding conditions. The variation of convection flows and weld pool shape played a role in modifying VS and GL. Solidification orientation and morphology were affected because VS and GL were changed as a function of gravity. Studies of gravity on the welding process are expected to play a significant role in the space-station construction and circumferential pipe welding on the earth. (Abstract shortened by UMI.)

78 FR 54864 - Light-Walled Rectangular Pipe and Tube From Mexico: Preliminary Results and Partial Rescission of...

Federal Register 2010, 2011, 2012, 2013, 2014

2013-09-06

... DEPARTMENT OF COMMERCE International Trade Administration [A-201-836] Light-Walled Rectangular... the antidumping duty order on light-walled rectangular pipe and tube (LWR pipe and tube) from Mexico... The merchandise subject to the order is certain welded carbon- quality light-walled steel pipe and...

Experimental Modal Analysis of Rectangular and Circular Beams

ERIC Educational Resources Information Center

Emory, Benjamin H.; Zhu, Wei Dong

2006-01-01

Analytical and experimental methods are used to determine the natural frequencies and mode shapes of Aluminum 6061-T651 beams with rectangular and circular cross-sections. A unique test stand is developed to provide the rectangular beam with different boundary conditions including clamped-free, clamped-clamped, clamped-pinned, and pinned-pinned.…

77 FR 4278 - Light-Walled Rectangular Pipe and Tube From Turkey: Extension of Time Limits for Preliminary...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-01-27

... DEPARTMENT OF COMMERCE International Trade Administration [A-489-815] Light-Walled Rectangular Pipe and Tube From Turkey: Extension of Time Limits for Preliminary Results of Antidumping Duty..., light- walled rectangular pipe and tube from Turkey for the May 1, 2010, through April 30, 2011, period...

76 FR 57953 - Light-Walled Rectangular Pipe and Tube From Turkey; Notice of Final Results of Antidumping Duty...

Federal Register 2010, 2011, 2012, 2013, 2014

2011-09-19

... Pipe and Tube From Turkey; Notice of Final Results of Antidumping Duty Administrative Review AGENCY... pipe and tube from Turkey. See Light-Walled Rectangular Pipe and Tube From Turkey; Notice of... order covering light- walled rectangular pipe and tube from Turkey. See Preliminary Results. The...

78 FR 74161 - Light-Walled Rectangular Pipe and Tube From China, Korea, Mexico, and Turkey; Scheduling of Full...

Federal Register 2010, 2011, 2012, 2013, 2014

2013-12-10

...-Walled Rectangular Pipe and Tube From China, Korea, Mexico, and Turkey; Scheduling of Full Five-Year... Turkey AGENCY: United States International Trade Commission. ACTION: Notice. SUMMARY: The Commission... on light- walled rectangular pipe and tube from China, Korea, Mexico, and Turkey would be likely to...

Factorization of differential expansion for non-rectangular representations

NASA Astrophysics Data System (ADS)

Morozov, A.

2018-04-01

Factorization of the differential expansion (DE) coefficients for colored HOMFLY-PT polynomials of antiparallel double braids, originally discovered for rectangular representations R, in the case of rectangular representations R, is extended to the first non-rectangular representations R = [2, 1] and R = [3, 1]. This increases chances that such factorization will take place for generic R, thus fixing the shape of the DE. We illustrate the power of the method by conjecturing the DE-induced expression for double-braid polynomials for all R = [r, 1]. In variance with the rectangular case, the knowledge for double braids is not fully sufficient to deduce the exclusive Racah matrix S¯ — the entries in the sectors with nontrivial multiplicities sum up and remain unseparated. Still, a considerable piece of the matrix is extracted directly and its other elements can be found by solving the unitarity constraints.

Triple-band metamaterial absorption utilizing single rectangular hole

NASA Astrophysics Data System (ADS)

Kim, Seung Jik; Yoo, Young Joon; Kim, Young Ju; Lee, YoungPak

2017-01-01

In the general metamaterial absorber, the single absorption band is made by the single meta-pattern. Here, we introduce the triple-band metamaterial absorber only utilizing single rectangular hole. We also demonstrate the absorption mechanism of the triple absorption. The first absorption peak was caused by the fundamental magnetic resonance in the metallic part between rectangular holes. The second absorption was generated by induced tornado magnetic field. The process of realizing the second band is also presented. The third absorption was induced by the third-harmonic magnetic resonance in the metallic region between rectangular holes. In addition, the visible-range triple-band absorber was also realized by using similar but smaller single rectangular-hole structure. These results render the simple metamaterials for high frequency in large scale, which can be useful in the fabrication of metamaterials operating in the optical range.

Fracture control method for composite tanks with load sharing liners

NASA Technical Reports Server (NTRS)

Bixler, W. D.

1975-01-01

The experimental program was based on the premise that the plastic sizing cycle, which each pressure vessel is subjected to prior to operation, acts as an effective proof test of the liner, screening out all flaws or cracks larger than a critical size. In doing so, flaw growth potential is available for cyclic operation at pressures less than the sizing pressure. Static fracture and cyclic life tests, involving laboratory type specimens and filament overwrapped tanks, were conducted on three liner materials: (1) 2219-T62 aluminum, (2) Inconel X750 STA, and (3) cryoformed 301 stainless steel. Variables included material condition, thickness, flaw size, flaw shape, temperature, sizing stress level, operating stress level and minimum-to-maximum operating stress ratio. From the empirical data base obtained, a procedure was established by which the service life of composite tanks with load sharing liners could be guaranteed with a high degree of confidence.

The Moment of Inertia of a Rectangular Rod

NASA Astrophysics Data System (ADS)

Takeuchi, Takao

2007-11-01

Recently an inexpensive setup to obtain the moment of inertia of a rotating system was proposed by Peter E. Banks. An equally simple and inexpensive experiment to obtain the moment of inertia of a uniform rod is proposed in this paper. A rectangular rod with a hole somewhere in the rod was used for this purpose. The moment of inertia of a rectangular rod around the hole location was attempted. The experimental setup is shown in Fig. 1. Various supporting rods, clamps, and rubber stoppers to hold the rectangular rod in place at point p are not shown.

All-fiber optical filter with an ultranarrow and rectangular spectral response.

PubMed

Zou, Xihua; Li, Ming; Pan, Wei; Yan, Lianshan; Azaña, José; Yao, Jianping

2013-08-15

Optical filters with an ultranarrow and rectangular spectral response are highly desired for high-resolution optical/electrical signal processing. An all-fiber optical filter based on a fiber Bragg grating with a large number of phase shifts is designed and fabricated. The measured spectral response shows a 3 dB bandwidth of 650 MHz and a rectangular shape factor of 0.513 at the 25 dB bandwidth. This is the narrowest rectangular bandpass response ever reported for an all-fiber filter, to the best of our knowledge. The filter has also the intrinsic advantages of an all-fiber implementation.

Rectangular-cladding silicon slot waveguide with improved nonlinear performance

NASA Astrophysics Data System (ADS)

Huang, Zengzhi; Huang, Qingzhong; Wang, Yi; Xia, Jinsong

2018-04-01

Silicon slot waveguides have great potential in hybrid silicon integration to realize nonlinear optical applications. We propose a rectangular-cladding hybrid silicon slot waveguide. Simulation result shows that, with a rectangular-cladding, the slot waveguide can be formed by narrower silicon strips, so the two-photon absorption (TPA) loss in silicon is decreased. When the cladding material is a nonlinear polymer, the calculated TPA figure of merit (FOMTPA) is 4.4, close to the value of bulk nonlinear polymer of 5.0. This value confirms the good nonlinear performance of rectangular-cladding silicon slot waveguides.

Physicochemical Characterization of Aerosol Generated in the Gas Tungsten Arc Welding of Stainless Steel.

PubMed

Miettinen, Mirella; Torvela, Tiina; Leskinen, Jari T T

2016-10-01

Exposure to stainless steel (SS) welding aerosol that contain toxic heavy metals, chromium (Cr), manganese (Mn), and nickel (Ni), has been associated with numerous adverse health effects. The gas tungsten arc welding (GTAW) is commonly applied to SS and produces high number concentration of substantially smaller particles compared with the other welding techniques, although the mass emission rate is low. Here, a field study in a workshop with the GTAW as principal welding technique was conducted to determine the physicochemical properties of the airborne particles and to improve the understanding of the hazard the SS welding aerosols pose to welders. Particle number concentration and number size distribution were measured near the breathing zone (50cm from the arc) and in the middle of the workshop with condensation particle counters and electrical mobility particle sizers, respectively. Particle morphology and chemical composition were studied using scanning and transmission electron microscopy and energy-dispersive X-ray spectroscopy. In the middle of the workshop, the number size distribution was unimodal with the geometric mean diameter (GMD) of 46nm. Near the breathing zone the number size distribution was multimodal, and the GMDs of the modes were in the range of 10-30nm. Two different agglomerate types existed near the breathing zone. The first type consisted of iron oxide primary particles with size up to 40nm and variable amounts of Cr, Mn, and Ni replacing iron in the structure. The second type consisted of very small primary particles and contained increased proportion of Ni compared to the proportion of (Cr + Mn) than the first agglomerate type. The alterations in the distribution of Ni between different welding aerosol particles have not been reported previously. © The Author 2016. Published by Oxford University Press on behalf of the British Occupational Hygiene Society.

Stainless steel anodes for alkaline water electrolysis and methods of making

DOEpatents

Soloveichik, Grigorii Lev

2014-01-21

The corrosion resistance of stainless steel anodes for use in alkaline water electrolysis was increased by immersion of the stainless steel anode into a caustic solution prior to electrolysis. Also disclosed herein are electrolyzers employing the so-treated stainless steel anodes. The pre-treatment process provides a stainless steel anode that has a higher corrosion resistance than an untreated stainless steel anode of the same composition.

Impact of orthodontic appliances on the quality of craniofacial anatomical magnetic resonance imaging and real-time speech imaging.

PubMed

Wylezinska, Marzena; Pinkstone, Marie; Hay, Norman; Scott, Andrew D; Birch, Malcolm J; Miquel, Marc E

2015-12-01

The aim of this work was to investigate the effects of commonly used orthodontic appliances on the magnetic resonance (MR) image quality of the craniofacial region, with special interest in the soft palate and velopharyngeal wall using real-time speech imaging sequences and anatomical imaging of the temporomandibular joints (TMJ) and pituitaries. Common orthodontic appliances were studied on 1.5 T scanner using standard spin and gradient echo sequences (based on the American Society for Testing and Materials standard test method) and sequences previously applied for high-resolution anatomical and dynamic real-time imaging during speech. Images were evaluated for the presence and size of artefacts. Metallic orthodontic appliances had different effects on image quality. The most extensive individual effects were associated with the presence of stainless steel archwire, particularly if combined with stainless steel brackets and stainless steel molar bands. With those appliances, diagnostic quality of magnetic resonance imaging speech and palate images will be most likely severely degraded, or speech imaging and imaging of pituitaries and TMJ will be not possible. All non-metallic, non-metallic with Ni/Cr reinforcement or Ni/Ti alloys appliances were of little concern. The results in the study are only valid at 1.5 T and for the sequences and devices used and cannot necessarily be extrapolated to all sequences and devices. Furthermore, both geometry and size of some appliances are subject dependent, and consequently, the effects on the image quality can vary between subjects. Therefore, the results presented in this article should be treated as a guide when assessing the risks of image quality degradation rather than an absolute evaluation of possible artefacts. Appliances manufactured from stainless steel cause extensive artefacts, which may render image non-diagnostic. The presence and type of orthodontic appliances should be always included in the patient's screening, so the risks of artefacts can be assessed prior to imaging. Although the risks to patients with fixed orthodontic appliances at 1.5 T MR scanners are low, their secure attachment should be confirmed prior to the examination. © The Author 2015. Published by Oxford University Press on behalf of the European Orthodontic Society. All rights reserved. For permissions, please email: journals.permissions@oup.com.

In vitro biomechanical comparison of multistrand cables with conventional cervical stabilization.

PubMed

Weis, J C; Cunningham, B W; Kanayama, M; Parker, L; McAfee, P C

1996-09-15

The biomechanical stability of six different methods of cervical spine stabilization, three using multistrand cables, were evaluated in a bovine model. To quantify and compare the in vitro biomechanical properties of multistrand cables used for posterior cervical wiring to standard cervical fixation techniques. Fixation of the posterior cervical spine with monofilament stainless steel wire is a proven technique for stabilization of the cervical spine. Recently, multistrand braided cables have been used as a substitute for monofilament stainless steel wires. These cables, made of stainless steel, titanium, or polyethylene, are reported to be stronger, more flexible, and fatigue resistant than are monofilament wire based on mechanical testing. However, no in vitro biomechanical studies have been performed testing a standard posterior cervical wiring technique using multistrand cables. Thirty-six fresh frozen cervical calf spines consistent in size and age were mounted and fixed rigidly to isolate the C4-C5 motion segment. Six different reconstruction techniques were evaluated for Rogers' posterior cervical wiring technique using: 1) 20-gauge stainless steel monofilament wire, 2) stainless steel cable, 3) titanium cable, 4) polyethylene cables, 5) anterior locking plate construct with interbody graft, and 6) posterior plate construct. Six cervical spines were included in each group (n = 6), with each specimen statically evaluated under three stability conditions: 1) intact, 2) reconstructed, and 3) postfatigue. The instability model created before the reconstruction consisted of a distractive flexion Stage 3 injury at C4-C5. Nondestructive static biomechanical testing, performed on an material testing machine (MTS 858 Bionix test system, Minneapolis, MN), included axial compression, axial rotation, flexion-extension, and lateral bending. After reconstruction and static analysis, the specimens were fatigued for 1500 cycles and then statically retested. Data analysis included normalization of the reconstructed and postfatigue data to the intact condition. The calculated static parameters included operative functional unit stiffness and range of motion. Posterior cervical reconstruction with stainless steel monofilament wire proved inadequate under fatigue testing. Two of the six specimens failed with fatigue, and this construct permitted the greatest degree of flexion-extension motion after fatigue in comparison with all other constructs (P < 0.05). There were no significant differences in flexural stiffness or range of motion between stainless steel, titanium, or polyethylene cable constructs before or after fatigue testing. The posterior cervical plate constructs were the stiffest constructs under flexion, extension, and lateral bending modes, before and after fatigue testing (P < 0.05). Multistrand cables were superior to monofilament wire with fatigue testing using an in vitro calf cervical spine model. There were no failures or detectable differences in elongation after fatigue testing between the stainless steel, titanium, and polyethylene cables, as shown by the flexion-extension range of motion. The posterior cervical plate construct offered the greatest stability compared with all other constructs.

78 FR 1199 - Light-Walled Rectangular Pipe and Tube From Mexico: Final Results of Antidumping Duty...

Federal Register 2010, 2011, 2012, 2013, 2014

2013-01-08

... DEPARTMENT OF COMMERCE International Trade Administration [A-201-836] Light-Walled Rectangular... order on light-walled rectangular pipe and tube (LWR pipe and tube) from Mexico. This review covers two... but received no such comments. We also did not receive a request for a hearing. \\1\\ See Light-Walled...

77 FR 21527 - Certain Cut-to-Length Carbon-Quality Steel Plate Products From the Republic of Korea: Final...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-04-10

... in coils) and without patterns in relief), of iron or non-alloy quality steel; and (2) flat-rolled... rectangular or non-rectangular cross section where such non-rectangular cross-section is achieved subsequent... characteristics that are painted, varnished, or coated with plastic or other non-metallic substances are included...

Sampling Scattered Data Onto Rectangular Grids for Volume Visualization

DTIC Science & Technology

1989-12-01

30 4.4 Building A Rectangular Grid ..... ................ 30 4.5 Sampling Methds ...... ...................... 34 4.6...dimensional data have been developed recently. In computational fluid flow analysis, methods for constructing three dimen- sional numerical grids are...structure of rectangular grids. Because finite element analysis is useful in fields other than fluid flow analysis and the numerical grid has promising

78 FR 42546 - Light-Walled Rectangular Pipe and Tube From China, Korea, Mexico, and Turkey: Notice of...

Federal Register 2010, 2011, 2012, 2013, 2014

2013-07-16

...-Walled Rectangular Pipe and Tube From China, Korea, Mexico, and Turkey: Notice of Commission... light-walled rectangular pipe and tube from China, Korea, Mexico, and Turkey would be likely to lead to... institution from the Government of Turkey, the Commission found that the respondent interested party group...

75 FR 33779 - Light-Walled Rectangular Pipe and Tube from Turkey; Notice of Preliminary Results of Antidumping...

Federal Register 2010, 2011, 2012, 2013, 2014

2010-06-15

... Pipe and Tube from Turkey; Notice of Preliminary Results of Antidumping Duty Administrative Review... review of the antidumping duty order on light-walled rectangular pipe and tube from Turkey. Atlas Tube... the antidumping duty order on light-walled rectangular ripe and tube from Turkey on May 30, 2008. See...

77 FR 55455 - Light-Walled Rectangular Pipe and Tube From Turkey: Notice of Final Results of Antidumping Duty...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-09-10

... Pipe and Tube From Turkey: Notice of Final Results of Antidumping Duty Administrative Review AGENCY... administrative review of the antidumping duty order on light-walled rectangular pipe and tube from Turkey.\\1\\ The... entitled ``Final Results of Review'' below. \\1\\ See Light-Walled Rectangular Pipe and Tube from Turkey...

Cracking behavior and microstructure of austenitic stainless steels and alloy 690 irradiated in BOR-60 reactor, phase I.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Y.; Chopra, O. K.; Soppet, W. K.

2010-02-16

Cracking behavior of stainless steels specimens irradiated in the BOR-60 at about 320 C is studied. The primary objective of this research is to improve the mechanistic understanding of irradiation-assisted stress corrosion cracking (IASCC) of core internal components under conditions relevant to pressurized water reactors. The current report covers several baseline tests in air, a comparison study in high-dissolved-oxygen environment, and TEM characterization of irradiation defect structure. Slow strain rate tensile (SSRT) tests were conducted in air and in high-dissolved-oxygen (DO) water with selected 5- and 10-dpa specimens. The results in high-DO water were compared with those from earlier testsmore » with identical materials irradiated in the Halden reactor to a similar dose. The SSRT tests produced similar results among different materials irradiated in the Halden and BOR-60 reactors. However, the post-irradiation strength for the BOR-60 specimens was consistently lower than that of the corresponding Halden specimens. The elongation of the BOR-60 specimens was also greater than that of their Halden specimens. Intergranular cracking in high-DO water was consistent for most of the tested materials in the Halden and BOR-60 irradiations. Nonetheless, the BOR-60 irradiation was somewhat less effective in stimulating IG fracture among the tested materials. Microstructural characterization was also carried out using transmission electron microscopy on selected BOR-60 specimens irradiated to {approx}25 dpa. No voids were observed in irradiated austenitic stainless steels and cast stainless steels, while a few voids were found in base and grain-boundary-engineered Alloy 690. All the irradiated microstructures were dominated by a high density of Frank loops, which varied in mean size and density for different alloys.« less

Electrochemical Studies of Benzophenone and Fluorenone Imines, Amines and Diphenyldiazomethane.

DTIC Science & Technology

1982-01-01

exhaustive, controlled-potential electrolyses has also been described. 2 Cells. electrodes. and electrolysis procedures. All electrochemical experiments...scale electrolyses was monitored periodically by cyclic voltammetry. At the conclusion of the experiment, the electrolysis mixture was protonated in a...stainless steel * column packed with LiChrosorb RP8 or LiChrosorb RP18, 10-pm mean particle size. The eluting solvent was a mixture of methanol and water

Nickel-free austenitic stainless steels for medical applications.

PubMed

Yang, Ke; Ren, Yibin

2010-02-01

The adverse effects of nickel ions being released into the human body have prompted the development of high-nitrogen nickel-free austenitic stainless steels for medical applications. Nitrogen not only replaces nickel for austenitic structure stability but also much improves steel properties. Here we review the harmful effects associated with nickel in medical stainless steels, the advantages of nitrogen in stainless steels, and emphatically, the development of high-nitrogen nickel-free stainless steels for medical applications. By combining the benefits of stable austenitic structure, high strength and good plasticity, better corrosion and wear resistances, and superior biocompatibility compared to the currently used 316L stainless steel, the newly developed high-nitrogen nickel-free stainless steel is a reliable substitute for the conventional medical stainless steels.

Nickel-free austenitic stainless steels for medical applications

PubMed Central

Yang, Ke; Ren, Yibin

2010-01-01

The adverse effects of nickel ions being released into the human body have prompted the development of high-nitrogen nickel-free austenitic stainless steels for medical applications. Nitrogen not only replaces nickel for austenitic structure stability but also much improves steel properties. Here we review the harmful effects associated with nickel in medical stainless steels, the advantages of nitrogen in stainless steels, and emphatically, the development of high-nitrogen nickel-free stainless steels for medical applications. By combining the benefits of stable austenitic structure, high strength and good plasticity, better corrosion and wear resistances, and superior biocompatibility compared to the currently used 316L stainless steel, the newly developed high-nitrogen nickel-free stainless steel is a reliable substitute for the conventional medical stainless steels. PMID:27877320

Effect of Plate Hardening Behavior on the Deformation of Stainless Steel Metal Bellows

NASA Astrophysics Data System (ADS)

Hao, Zengliang; Luo, Shuyi; Zhao, He; Zhang, Chunxiang; Luo, Junting

2017-11-01

Tensile tests of original plate samples from three types of stainless steel metal bellows were performed at room temperature. The constitutive equations for the three hardening curves were obtained and fitted. The analysis results of the microstructure and fracture morphology of the tensile specimens show that the grain size of the plate with a high logarithmic-exponential hardening rate is uneven and the dimple of the shear fracture is elongated into an ellipse. By contrast, the grain size of the plate with a relatively low linear hardening rate is even and the dimple of the fracture is uniformly equiaxial. Finite element simulations of the hydraulic bulging and repeated limit bending deformation of the metal bellows of the three types of materials were also conducted. The repeated limit bending deformation process was tested experimentally. Although the effect of the hardening exponent on the residual stress of the metal bellows after hydraulic bulging is minimal, this exponent considerably influences the repeated limit bending deformation of the metal bellows after subsequent use. The trough hardening phenomenon is serious in the repeated limit bending process. Moreover, when the hardening exponent of the original plate is high, the resistance to bending fracture at the trough area is poor.

Influence of connection tubing in modern size exclusion chromatography and its impact on the characterization of mAbs.

PubMed

Fekete, Szabolcs; Guillarme, Davy

2018-02-05

The goal of the study was to evaluate the impact of connection tubing in modern size exclusion chromatography (SEC), since it may strongly impact the apparent column efficiency, as the compounds are not retained in SEC. For this purpose, a reference SEC column of 150×4.6mm, 1.8μm was considered, and various proteins were tested as model compounds. Different tube geometries (lengths and internal diameters) and materials (stainless steel and PEEK) were evaluated in a systematic way. Large proteins always showed larger tube dispersion vs. small molecules, especially when the residence time in the tube was long (at low flow rate). This confirms the need to drastically reduce the tube volume (using the shortest and narrowest connector tubing) to attain the full benefits of UHPSEC columns. In addition, PEEK tubing were found to be more appropriate than stainless steel tubing, since adsorption of proteins was less pronounced, and higher plate count can be obtained. Finally, after a careful system optimization, up to 40% increase of apparent column efficiency can be achieved compared to a regular UHPLC system, when using a 150×4.6mm UHPSEC columns packed with sub-3μm particles. Copyright © 2017 Elsevier B.V. All rights reserved.

Fabrication and Wettability Study of WO3 Coated Photocatalytic Membrane for Oil-Water Separation: A Comparative Study with ZnO Coated Membrane.

PubMed

Gondal, Mohammed A; Sadullah, Muhammad S; Qahtan, Talal F; Dastageer, Mohamed A; Baig, Umair; McKinley, Gareth H

2017-05-10

Superhydrophilic and underwater superoleophobic surfaces were fabricated by facile spray coating of nanostructured WO 3 on stainless steel meshes and compared its performance in oil-water separation with ZnO coated meshes. The gravity driven oil-water separation system was designed using these surfaces as the separation media and it was noticed that WO 3 coated stainless steel mesh showed high separation efficiency (99%), with pore size as high as 150 µm, whereas ZnO coated surfaces failed in the process of oil-water separation when the pore exceeded 50 µm size. Since, nanostructured WO 3 is a well known catalyst, the simultaneous photocatalytic degradation of organic pollutants present in the separated water from the oil water separation process were tested using WO 3 coated surfaces under UV radiation and the efficiency of this degradation was found to be quite significant. These results assure that with little improvisation on the oil water separation system, these surfaces can be made multifunctional to work simultaneously for oil-water separation and demineralization of organic pollutants from the separated water. Fabrication of the separating surface, their morphological characteristics, wettability, oil water separation efficiency and photo-catalytic degradation efficiency are enunciated.

Comprehensive Understanding of Ductility Loss Mechanisms in Various Steels with External and Internal Hydrogen

NASA Astrophysics Data System (ADS)

Takakuwa, Osamu; Yamabe, Junichiro; Matsunaga, Hisao; Furuya, Yoshiyuki; Matsuoka, Saburo

2017-11-01

Hydrogen-induced ductility loss and related fracture morphologies are comprehensively discussed in consideration of the hydrogen distribution in a specimen with external and internal hydrogen by using 300-series austenitic stainless steels (Types 304, 316, 316L), high-strength austenitic stainless steels (HP160, XM-19), precipitation-hardened iron-based super alloy (A286), low-alloy Cr-Mo steel (JIS-SCM435), and low-carbon steel (JIS-SM490B). External hydrogen is realized by a non-charged specimen tested in high-pressure gaseous hydrogen, and internal hydrogen is realized by a hydrogen-charged specimen tested in air or inert gas. Fracture morphologies obtained by slow-strain-rate tensile tests (SSRT) of the materials with external or internal hydrogen could be comprehensively categorized into five types: hydrogen-induced successive crack growth, ordinary void formation, small-sized void formation related to the void sheet, large-sized void formation, and facet formation. The mechanisms of hydrogen embrittlement are broadly classified into hydrogen-enhanced decohesion (HEDE) and hydrogen-enhanced localized plasticity (HELP). In the HEDE model, hydrogen weakens interatomic bonds, whereas in the HELP model, hydrogen enhances localized slip deformations. Although various fracture morphologies are produced by external or internal hydrogen, these morphologies can be explained by the HELP model rather than by the HEDE model.

Modeling and experimental study of oil/water contact angle on biomimetic micro-parallel-patterned self-cleaning surfaces of selected alloys used in water industry

NASA Astrophysics Data System (ADS)

Nickelsen, Simin; Moghadam, Afsaneh Dorri; Ferguson, J. B.; Rohatgi, Pradeep

2015-10-01

In the present study, the wetting behavior of surfaces of various common metallic materials used in the water industry including C84400 brass, commercially pure aluminum (99.0% pure), Nickle-Molybdenum alloy (Hastelloy C22), and 316 Stainless Steel prepared by mechanical abrasion and contact angles of several materials after mechanical abrasion were measured. A model to estimate roughness factor, Rf, and fraction of solid/oil interface, ƒso, for surfaces prepared by mechanical abrasion is proposed based on the assumption that abrasive particles acting on a metallic surface would result in scratches parallel to each other and each scratch would have a semi-round cross-section. The model geometrically describes the relation between sandpaper particle size and water/oil contact angle predicted by both the Wenzel and Cassie-Baxter contact type, which can then be used for comparison with experimental data to find which regime is active. Results show that brass and Hastelloy followed Cassie-Baxter behavior, aluminum followed Wenzel behavior and stainless steel exhibited a transition from Wenzel to Cassie-Baxter. Microstructural studies have also been done to rule out effects beyond the Wenzel and Cassie-Baxter theories such as size of structural details.

Failure analysis of eleven Gates Glidden drills that fractured intraorally during post space preparation. A retrieval analysis study.

PubMed

Al Jabbari, Youssef S; Fournelle, Raymond; Al Taweel, Sara M; Zinelis, Spiros

2017-07-19

The purpose of this study was to determine the failure mechanism of clinically failed Gates Glidden (GG) drills. Eleven retrieved GG drills (sizes #1 to #3) which fractured during root canal preparation were collected and the fracture location was recorded based on macroscopic observation. All fracture surfaces were investigated by a SEM. Then the fractured parts were embedded in acrylic resin and after metallographic preparation, the microstructure and elemental composition was evaluated by SEM and EDS. The Vickers hardness (HV) of all specimens was also determined. Macroscopic examination and SEM analysis showed that the drills failed near the hand piece end by torsional fatigue with fatigue cracks initiating at several locations around the circumference and propagating toward the center. Final fracture followed by a tensile overloading at the central region of cross section. Microstructural analysis, hardness measurements and EDS show that the drills are made of a martensitic stainless steel like AISI 440C. Based on the findings of this study, clinicians should expect fatigue fracture of GG drills that have small size during root canal preparation. Selection of a more fatigue resistant stainless steel alloy and enhancing the instrument design might reduce the incidence of quasi-cleavage fracture on GG drills.

The radiation dose from a proposed measurement of arsenic and selenium in human skin

NASA Astrophysics Data System (ADS)

Gherase, Mihai R.; Mader, Joanna E.; Fleming, David E. B.

2010-09-01

Dose measurements following 10 min irradiations with a portable x-ray fluorescence spectrometer composed of a miniature x-ray tube and a silicon PiN diode detector were performed using thermoluminescent dosimeters consisting of LiF:Mg,Ti chips of 3 mm diameter and 0.4 mm thickness. The table-top setup of the spectrometer was used for all measurements. The setup included a stainless steel lid which served as a radiation shield. Two rectangular polyethylene skin/soft tissue phantoms with two cylindrical plaster of Paris bone phantoms were used to study the effect of x-ray beam attenuation and backscatter on the measured dose. Eight different irradiation experiments were performed. The average dose rate values measured with TLD chips within a 1 × 1 cm2 area were between 4.8 and 12.8 mGy min-1. The equivalent dose for a 1 × 1 cm2 skin area was estimated to be 13.2 mSv. The maximum measured dose rate values with a single TLD chip were between 7.5 and 25.1 mGy min-1. The effective dose corresponding to a proposed arsenic/selenium skin measurement was estimated to be 0.13 µSv for a 2 min irradiation.

Photoelastic analysis of stress generated by wires when conventional and self-ligating brackets are used: A pilot study

PubMed Central

Sobral, Guilherme Caiado; Vedovello, Mário; Degan, Viviane Veroni; Santamaria, Milton

2014-01-01

OBJECTIVE: By means of a photoelastic model, this study analyzed the stress caused on conventional and self-ligating brackets with expanded arch wires. METHOD: Standard brackets were adhered to artificial teeth and a photoelastic model was prepared using the Interlandi 19/12 diagram as base. Successive activations were made with 0.014-in and 0.018-in rounded cross section Nickel-Titanium wires (NiTi) and 0.019 x 0.025-in rectangular stainless steel wires all of which made on 22/14 Interlandi diagram. The model was observed on a plane polariscope - in a dark field microscope configuration - and photographed at each exchange of wire. Then, they were replaced by self-ligating brackets and the process was repeated. Analysis was qualitative and observed stress location and pattern on both models analyzed. CONCLUSIONS: Results identified greater stress on the region of the apex of premolars in both analyzed models. Upon comparing the stress between models, a greater amount of stress was found in the model with conventional brackets in all of its wires. Therefore, the present pilot study revealed that alignment of wires in self-ligating brackets produced lower stress in periodontal tissues in expansive mechanics. PMID:25715719

Unsteady Diffusion Flames: Ignition, Travel, and Burnout (SUBCORE Project: Simplified Unsteady Burning of Contained Reactants)

NASA Technical Reports Server (NTRS)

Fendell, Francis; Rungaldier, Harald

1999-01-01

An experimental apparatus for the examination of a planar, virtually strain-rate-free diffusion flame in microgravity has been designed and fabricated. Such a diffusion flame is characterized by relatively large spatial scale and high symmetry (to facilitate probing), and by relatively long fluid-residence time (to facilitate investigation of rates associated with sooting phenomena). Within the squat rectangular apparatus, with impervious, noncatalytic isothermal walls of stainless steel, a thin metallic splitter plate subdivides the contents into half-volumes. One half-volume initially contains fuel vapor diluted with an inert gas, and the other, oxidizer diluted with another inert gas-so that the two domains have equal pressure, density, and temperature. As the separator is removed, by translation in its own plane, through a tightly fitting slit in one side wall, a line ignitor in the opposite side wall initiates a triple-flame propagation across the narrow layer of combustible mixture formed near midheight in the chamber. The planar diffusion flame so emplaced is quickly disrupted in earth gravity. In microgravity, the planar flame persists, and travels ultimately into the half-volume containing the stoichiometrically deficient reactant; the flame eventually becomes extinguished owing to reactant depletion and heat loss to the walls.

A Novel Method of Coating Orthodontic Archwires with Nanoparticles

PubMed Central

Syed, Shibli S; Kulkarni, Dinraj; Todkar, Rohit; Bagul, Ravikiran S; Parekh, Kreena; Bhujbal, Nikita

2015-01-01

Background: The major hazard to the orthodontic tooth movement is the friction developing at the bracket wire interface. In the past, there have been various attempts to reduce this friction. We believe that coating the commercially available orthodontic wires with nanoparticles can result in a successful reduction of this friction. The objective of this study is to develop a novel method of coating orthodontic archwires with nanoparticles. Materials and Methods: Stainless steel (Ormco, CA, USA), titanium molybdenum alloy (Ormco, CA, USA) and nickel-titanium (G and H Wire Company, USA) orthodontic wires with a rectangular cross-section dimension of 0.019”× 0.025”, were selected. The wires were later coated with a uniform and smooth nanoparticle film using 100 ml nanocremics. The coating procedure described in this article is a sol-gel thin film dip coating method. Results: The coating procedure was verified by comparing the surface topography of nanocoated archwires with the commercially available archwires in an environmental scanning electron microscope (ESEM). The ESEM images prove that the surface topography of the coated wires was found to be smoother with less surface deteriorations as compared to the commercially available wires. Conclusion: Commercially available orthodontic wires can be successfully coated using a novel method of sol-gel thin film dip coating method. PMID:26028899

Study of LED layout in indoor visible light communication and performance analysis

NASA Astrophysics Data System (ADS)

Wang, Jiaan; Che, Ying; Wang, Xinlan; Guo, Linyang; Li, Jing

2017-10-01

Light emitting diodes(LED) could provide both illumination and data communication in indoor visible light communication(VLC) that owns the modulation bandwith from several from several MHz to seneral hundreds of MHz. The layout of LED plays an important role in maintaining a steady optical power distribution over the receiving plane. The existing rectangular LED layout does not provide a full coverage on the receiving plane leaving receiving optical power outage area, which in turn affects the best performance of the VLC system. This paper design a circular layout scheme of LED in 5mX5mX3m room based on the criterion of the illumination minimum mean square deviation. The influence of the distribution of the intensity of illumination with the radius of 1m and 1.5m,for including the wall reflection and not including the wall reflection, and make a comparison with rectangular LED layout of illumination distribution, when the number of LEDs with rectangular layout as same as circular layout. Including the number of LEDs are 4 and 16.For a specific simulation parameters as following:height of receiving plane is 0.85m,a single LEDs is composed of 60X60 LED chips, the parameters of a single chip is that transmitting power is 20mW,center luminous intensity is 0.73cd.semiangle at half power is 70deg.The parameters of concentrator is that photodiode area is 1cm2,photodiode responsivity is 0.4,field of view at the receiver is 85deg.Other parameters are that reflective index of concentrator is 1.5,reflectivity of wall is 0.8.Circular layout and rectangular layout are analyzed through simulation of the received optical power distribution, signal noise ratio distribution in non line of sight(including the wall reflection) and line of sight(not including the wall reflection),when the number of the LED is different. It is clear from the results that the received optical power distribution of non line of sight is better than line of sight, when the number of the LED are same, but the signal noise ratio distribution is decreased result of the reflection of the wall. It is found that the received optical power of circular layout is better than the received optical power distribution of rectangulr layout, and circular layout is a good solution that add the received optical power at the 4 corners of room, improve the system ability of communication, when making a contrast of rectangular lyout with circular layout,at the same time,the fluctuate of circular layout's signal to noise ratio of is smller than rectangular layuot.The radius of circular layout or the location of rectangular layout is keeping, the received optical power of receiving plane is increased, by adding the number of LED,in the meantime, the interference between LED light source also increase. But the increase of the circular layout radius when the number of LED remain the same is helpful to reduce the inter symbol interference that work out between LED each other, enhance the system signal noise ratio. In this paper, the results of the reaearch provides a new idea for indoor visible light communication with non-standard room (Size of room is not 5mX5mX3m), at the same time, provides guiding significance for future setting up the indoor visible light communication links.

Round versus rectangular: Does the plot shape matter?

NASA Astrophysics Data System (ADS)

Iserloh, Thomas; Bäthke, Lars; Ries, Johannes B.

2016-04-01

Field rainfall simulators are designed to study soil erosion processes and provide urgently needed data for various geomorphological, hydrological and pedological issues. Due to the different conditions and technologies applied, there are several methodological aspects under review of the scientific community, particularly concerning design, procedures and conditions of measurement for infiltration, runoff and soil erosion. Extensive discussions at the Rainfall Simulator Workshop 2011 in Trier and the Splinter Meeting at EGU 2013 "Rainfall simulation: Big steps forward!" lead to the opinion that the rectangular shape is the more suitable plot shape compared to the round plot. A horizontally edging Gerlach trough is installed for sample collection without forming unnatural necks as is found at round or triangle plots. Since most research groups did and currently do work with round plots at the point scale (<1m²), a precise analysis of the differences between the output of round and square plots are necessary. Our hypotheses are: - Round plot shapes disturb surface runoff, unnatural fluvial dynamics for the given plot size such as pool development especially directly at the plot's outlet occur. - A square plot shape prevent these problems. A first comparison between round and rectangular plots (Iserloh et al., 2015) indicates that the rectangular plot could indeed be the more suitable, but the rather ambiguous results make a more elaborate test setup necessary. The laboratory test setup includes the two plot shapes (round, square), a standardised silty substrate and three inclinations (2°, 6°, 12°). The analysis of the laboratory test provide results on the best performance concerning undisturbed surface runoff and soil/water sampling at the plot's outlet. The analysis of the plot shape concerning its influence on runoff and erosion shows that clear methodological standards are necessary in order to make rainfall simulation experiments comparable. Reference: Iserloh, T., Pegoraro, D., Schlösser, A., Thesing, H., Seeger, M., Ries, J.B. (2015): Rainfall simulation experiments: Influence of water temperature, water quality and plot design on soil erosion and runoff. Geophysical Research Abstracts, Vol. 17, EGU2015-5817.

TU-F-CAMPUS-J-04: Impact of Voxel Anisotropy On Statistic Texture Features of Oncologic PET: A Simulation Study

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yang, F; Byrd, D; Bowen, S

2015-06-15

Purpose: Texture metrics extracted from oncologic PET have been investigated with respect to their usefulness as definitive indicants for prognosis in a variety of cancer. Metric calculation is often based on cubic voxels. Most commonly used PET scanners, however, produce rectangular voxels, which may change texture metrics. The objective of this study was to examine the variability of PET texture feature metrics resulting from voxel anisotropy. Methods: Sinograms of NEMA NU-2 phantom for 18F-FDG were simulated using the ASIM simulation tool. The obtained projection data was reconstructed (3D-OSEM) on grids of cubic and rectangular voxels, producing PET images of resolutionmore » of 2.73x2.73x3.27mm3 and 3.27x3.27x3.27mm3, respectively. An interpolated dataset obtained from resampling the rectangular voxel data for isotropic voxel dimension (3.27mm) was also considered. For each image dataset, 28 texture parameters based on grey-level co-occurrence matrices (GLCOM), intensity histograms (GLIH), neighborhood difference matrices (GLNDM), and zone size matrices (GLZSM) were evaluated within lesions of diameter of 33, 28, 22, and 17mm. Results: In reference to the isotopic image data, texture features appearing on the rectangular voxel data varied with a range of -34-10% for GLCOM based, -31-39% for GLIH based, -80 -161% for GLNDM based, and −6–45% for GLZSM based while varied with a range of -35-23% for GLCOM based, -27-35% for GLIH based, -65-86% for GLNDM based, and -22 -18% for GLZSM based for the interpolated image data. For the anisotropic data, GLNDM-cplx exhibited the largest extent of variation (161%) while GLZSM-zp showed the least (<1%). As to the interpolated data, GLNDM-busy varied the most (86%) while GLIH-engy varied the least (<1%). Conclusion: Variability of texture appearance on oncologic PET with respect to voxel representation is substantial and feature-dependent. It necessitates consideration of standardized voxel representation for inter-institution studies attempting to validate prognostic values of PET texture features in cancer treatment.« less

Size, shape and flow characterization of ground wood chip and ground wood pellet particles

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rezaei, Hamid; Lim, C. Jim; Lau, Anthony

Size, shape and density of biomass particles influence their transportation, fluidization, rates of drying and thermal decomposition. Pelleting wood particles increases the particle density and reduces the variability of physical properties among biomass particles. In this study, pine chips prepared for pulping and commercially produced pine pellets were ground in a hammer mill using grinder screens of 3.2, 6.3, 12.7 and 25.4mmperforations. Pellets consumed about 7 times lower specific grinding energy than chips to produce the same size of particles. Grinding pellets produced the smaller particles with narrower size distribution than grinding chips. Derived shape factors in digital image analysismore » showed that chip particles were rectangular and had the aspect ratios about one third of pellet particles. Pellet particles were more circular shape. The mechanical sieving underestimated the actual particle size and did not represent the size of particles correctly. Instead, digital imaging is preferred. Angle of repose and compressibility tests represented the flow properties of ground particles. Pellet particles made a less compacted bulk, had lower cohesion and did flow easier in a pile of particles. In conclusion, particle shape affected the flow properties more than particle size« less

Size, shape and flow characterization of ground wood chip and ground wood pellet particles

DOE PAGES

Rezaei, Hamid; Lim, C. Jim; Lau, Anthony; ...

2016-07-11

Size, shape and density of biomass particles influence their transportation, fluidization, rates of drying and thermal decomposition. Pelleting wood particles increases the particle density and reduces the variability of physical properties among biomass particles. In this study, pine chips prepared for pulping and commercially produced pine pellets were ground in a hammer mill using grinder screens of 3.2, 6.3, 12.7 and 25.4mmperforations. Pellets consumed about 7 times lower specific grinding energy than chips to produce the same size of particles. Grinding pellets produced the smaller particles with narrower size distribution than grinding chips. Derived shape factors in digital image analysismore » showed that chip particles were rectangular and had the aspect ratios about one third of pellet particles. Pellet particles were more circular shape. The mechanical sieving underestimated the actual particle size and did not represent the size of particles correctly. Instead, digital imaging is preferred. Angle of repose and compressibility tests represented the flow properties of ground particles. Pellet particles made a less compacted bulk, had lower cohesion and did flow easier in a pile of particles. In conclusion, particle shape affected the flow properties more than particle size« less

Nanopatterning of magnetic domains: Fe coverage of self-assembled alumina nanostructure

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wu, Qibin; Wang, Bo -Yao; Lin, Wen -Chin

2015-08-19

Nanosized ultrathin magnetic films were prepared by controlling the deposition of Fe onto an oxidized NiAl(001) surface with an alumina nanostructure on it. Because the ultrathin ferromagnetic Fe films on the bare NiAl(001) surface are separated by paramagnetic Fe nanoparticles on the alumina stripes, as determined by scanning electron microscopy with spin analysis, they form rectangular domains with sizes ranging from tens of nanometer to larger than a micrometer. Furthermore, magnetic domain patterning can thus be achieved by controlling the Fe coverage and nanostructured template.

Design optimization of large-size format edge-lit light guide units

NASA Astrophysics Data System (ADS)

Hastanin, J.; Lenaerts, C.; Fleury-Frenette, K.

2016-04-01

In this paper, we present an original method of dot pattern generation dedicated to large-size format light guide plate (LGP) design optimization, such as photo-bioreactors, the number of dots greatly exceeds the maximum allowable number of optical objects supported by most common ray-tracing software. In the proposed method, in order to simplify the computational problem, the original optical system is replaced by an equivalent one. Accordingly, an original dot pattern is splitted into multiple small sections, inside which the dot size variation is less than the ink dots printing typical resolution. Then, these sections are replaced by equivalent cells with continuous diffusing film. After that, we adjust the TIS (Total Integrated Scatter) two-dimensional distribution over the grid of equivalent cells, using an iterative optimization procedure. Finally, the obtained optimal TIS distribution is converted into the dot size distribution by applying an appropriate conversion rule. An original semi-empirical equation dedicated to rectangular large-size LGPs is proposed for the initial guess of TIS distribution. It allows significantly reduce the total time needed to dot pattern optimization.

Method of manufacturing a large-area segmented photovoltaic module

DOEpatents

Lenox, Carl

2013-11-05

One embodiment of the invention relates to a segmented photovoltaic (PV) module which is manufactured from laminate segments. The segmented PV module includes rectangular-shaped laminate segments formed from rectangular-shaped PV laminates and further includes non-rectangular-shaped laminate segments formed from rectangular-shaped and approximately-triangular-shaped PV laminates. The laminate segments are mechanically joined and electrically interconnected to form the segmented module. Another embodiment relates to a method of manufacturing a large-area segmented photovoltaic module from laminate segments of various shapes. Other embodiments relate to processes for providing a photovoltaic array for installation at a site. Other embodiments and features are also disclosed.

Electromagnetic Field Penetration Studies

NASA Technical Reports Server (NTRS)

Deshpande, M.D.

2000-01-01

A numerical method is presented to determine electromagnetic shielding effectiveness of rectangular enclosure with apertures on its wall used for input and output connections, control panels, visual-access windows, ventilation panels, etc. Expressing EM fields in terms of cavity Green's function inside the enclosure and the free space Green's function outside the enclosure, integral equations with aperture tangential electric fields as unknown variables are obtained by enforcing the continuity of tangential electric and magnetic fields across the apertures. Using the Method of Moments, the integral equations are solved for unknown aperture fields. From these aperture fields, the EM field inside a rectangular enclosure due to external electromagnetic sources are determined. Numerical results on electric field shielding of a rectangular cavity with a thin rectangular slot obtained using the present method are compared with the results obtained using simple transmission line technique for code validation. The present technique is applied to determine field penetration inside a Boeing-757 by approximating its passenger cabin as a rectangular cavity filled with a homogeneous medium and its passenger windows by rectangular apertures. Preliminary results for, two windows, one on each side of fuselage were considered. Numerical results for Boeing-757 at frequencies 26 MHz, 171-175 MHz, and 428-432 MHz are presented.

Development of a biaxial compression device for biological samples: preliminary experimental results for a closed cell foam.

PubMed

Little, J P; Tevelen, G; Adam, C J; Evans, J H; Pearcy, M J

2009-07-01

Biological tissues are subjected to complex loading states in vivo and in order to define constitutive equations that effectively simulate their mechanical behaviour under these loads, it is necessary to obtain data on the tissue's response to multiaxial loading. Single axis and shear testing of biological tissues is often carried out, but biaxial testing is less common. We sought to design and commission a biaxial compression testing device, capable of obtaining repeatable data for biological samples. The apparatus comprised a sealed stainless steel pressure vessel specifically designed such that a state of hydrostatic compression could be created on the test specimen while simultaneously unloading the sample along one axis with an equilibrating tensile pressure. Thus a state of equibiaxial compression was created perpendicular to the long axis of a rectangular sample. For the purpose of calibration and commissioning of the vessel, rectangular samples of closed cell ethylene vinyl acetate (EVA) foam were tested. Each sample was subjected to repeated loading, and nine separate biaxial experiments were carried out to a maximum pressure of 204 kPa (30 psi), with a relaxation time of two hours between them. Calibration testing demonstrated the force applied to the samples had a maximum error of 0.026 N (0.423% of maximum applied force). Under repeated loading, the foam sample demonstrated lower stiffness during the first load cycle. Following this cycle, an increased stiffness, repeatable response was observed with successive loading. While the experimental protocol was developed for EVA foam, preliminary results on this material suggest that this device may be capable of providing test data for biological tissue samples. The load response of the foam was characteristic of closed cell foams, with consolidation during the early loading cycles, then a repeatable load-displacement response upon repeated loading. The repeatability of the test results demonstrated the ability of the test device to provide reproducible test data and the low experimental error in the force demonstrated the reliability of the test data.

Evaluation of the Friction of Self-Ligating and Conventional Bracket Systems

PubMed Central

Tecco, Simona; Di Iorio, Donato; Nucera, Riccardo; Di Bisceglie, Beatrice; Cordasco, Giancarlo; Festa, Felice

2011-01-01

Objectives: This in vitro study evaluated the friction (F) generated by aligned stainless steel (SS) conventional brackets, self-ligating Damon MX© brackets (SDS Ormco, Glendora, California, USA), Time3© brackets (American Orthodontics, Sheboygan, Wisconsin, USA), Vision LP© brackets (American Orthodontics), and low-friction Slide© ligatures (Leone, Firenze, Italy) coupled with various SS, nickel-titanium (NiTi), and beta-titanium (TMA) archwires. Methods: All brackets had a 0.022-inch slot, and the orthodontic archwires were 0.014-inch, 0.016-inch, 0.014×0.025-inch, 0.018×0.025-inch, and 0.019×0.025-inch NiTi; 0.017×0.025-inch TMA; and 0.019×0.025-inch SS. Each bracket-archwire combination was tested 10 times. In the test, 10 brackets of the same group were mounted in alignment on a metal bar. The archwires moved through all the 10 brackets at a crosshead speed of 0.5 mm/min (each run lasted approximately 5 min). The differences among 5 groups of brackets were analyzed through the Kruskal-Wallis test, and a Mann-Whitney test was calculated as post hoc analysis. The P value was set at 0.05. Results: Coupled with 0.014-inch NiTi and 0.016-inch NiTi, Victory Series© brackets generated the greatest F, while Damon MX© and Vision LP© brackets generated the lowest (P<.05); no significant differences were observed between Time3© brackets and Slide© ligatures. Coupled with all the rectangular archwires, Victory Series© brackets, Slide© ligatures, and Vision LP© self-ligating brackets generated significantly lower F than did Time3© and Damon MX© self-ligating brackets (P<.05). Conclusions: These findings suggest that self-ligating brackets are a family of brackets that, in vitro, can generate different levels of F when coupled with thin or thick, rectangular, or round archwires. Clinical conclusions based on our results are not possible due to the limitations of the experimental conditions. PMID:21769273

Micro sized implantable ball lens-based fiber optic probe design

NASA Astrophysics Data System (ADS)

Cha, Jaepyeong; Kang, Jin U.

2014-02-01

A micro sized implantable ball lens-based fiber optic probe design is described for continuous monitoring of brain activity in freely behaving mice. A prototype uses a 500-micron ball lens and a highly flexible 350-micron-diameter fiber bundle, which are enclosed by a 21G stainless steel sheath. Several types and thickness of brain tissue, consisting of fluorescent probes such as GFP, GCaMP3 calcium indicator, are used to evaluate the performance of the imaging probe. Measured working distance is approximately 400-μm, but is long enough to detect neural activities from cortical and cerebellar tissues of mice brain.

Detection and Sizing of Defects in Structural Components of a Nuclear Power Plant by ECT

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen Zhenmao; Miya, Kenzo

2005-04-09

In this paper, progress of ECT technique for inspection of stress corrosion cracks in a structural component of a nuclear power plant is reported. Access and scanning vehicle (robot), advanced probes for SG tube inspection, development and evaluation of new probes for welding joint, and ECT based crack sizing technique are described respectively. Based on these new techniques, it is clarified that ECT can play as a supplement of UT for the welding zone inspection. It is also proved in this work that new ECT sensors are efficient even for a stainless plate as thick as 15mm.

Corrosion behavior of 2205 duplex stainless steel.

PubMed

Platt, J A; Guzman, A; Zuccari, A; Thornburg, D W; Rhodes, B F; Oshida, Y; Moore, B K

1997-07-01

The corrosion of 2205 duplex stainless steel was compared with that of AISI type 316L stainless steel. The 2205 stainless steel is a potential orthodontic bracket material with low nickel content (4 to 6 wt%), whereas the 316L stainless steel (nickel content: 10 to 14 wt%) is a currently used bracket material. Both stainless steels were subjected to electrochemical and immersion (crevice) corrosion tests in 37 degrees C, 0.9 wt% sodium chloride solution. Electrochemical testing indicates that 2205 has a longer passivation range than 316L. The corrosion rate of 2205 was 0.416 MPY (milli-inch per year), whereas 316L exhibited 0.647 MPY. When 2205 was coupled to 316L with equal surface area ratio, the corrosion rate of 2205 reduced to 0.260 MPY, indicating that 316L stainless steel behaved like a sacrificial anode. When 316L is coupled with NiTi, TMA, or stainless steel arch wire and was subjected to the immersion corrosion test, it was found that 316L suffered from crevice corrosion. On the other hand, 2205 stainless steel did not show any localized crevice corrosion, although the surface of 2205 was covered with corrosion products, formed when coupled to NiTi and stainless steel wires. This study indicates that considering corrosion resistance, 2205 duplex stainless steel is an improved alternative to 316L for orthodontic bracket fabrication when used in conjunction with titanium, its alloys, or stainless steel arch wires.

Numerical solutions of 3-dimensional Navier-Stokes equations for closed bluff-bodies

NASA Technical Reports Server (NTRS)

Abolhassani, J. S.; Tiwari, S. N.

1985-01-01

The Navier-Stokes equations are solved numerically. These equations are unsteady, compressible, viscous, and three-dimensional without neglecting any terms. The time dependency of the governing equations allows the solution to progress naturally for an arbitrary initial guess to an asymptotic steady state, if one exists. The equations are transformed from physical coordinates to the computational coordinates, allowing the solution of the governing equations in a rectangular parallelepiped domain. The equations are solved by the MacCormack time-split technique which is vectorized and programmed to run on the CDc VPS 32 computer. The codes are written in 32-bit (half word) FORTRAN, which provides an approximate factor of two decreasing in computational time and doubles the memory size compared to the 54-bit word size.

A reduced-order integral formulation to account for the finite size effect of isotropic square panels using the transfer matrix method.

PubMed

Bonfiglio, Paolo; Pompoli, Francesco; Lionti, Riccardo

2016-04-01

The transfer matrix method is a well-established prediction tool for the simulation of sound transmission loss and the sound absorption coefficient of flat multilayer systems. Much research has been dedicated to enhancing the accuracy of the method by introducing a finite size effect of the structure to be simulated. The aim of this paper is to present a reduced-order integral formulation to predict radiation efficiency and radiation impedance for a panel with equal lateral dimensions. The results are presented and discussed for different materials in terms of radiation efficiency, sound transmission loss, and the sound absorption coefficient. Finally, the application of the proposed methodology for rectangular multilayer systems is also investigated and validated against experimental data.

75 FR 81966 - Top of the Stove Stainless Steel Cooking Ware From the Republic of Korea: Final Results of Sunset...

Federal Register 2010, 2011, 2012, 2013, 2014

2010-12-29

... Stainless Steel Cooking Ware From the Republic of Korea: Final Results of Sunset Reviews and Revocation of... reviews of the antidumping and countervailing duty orders on top of the stove stainless steel cooking ware... the stove stainless steel cooking ware from Korea includes all non-electric cooking ware of stainless...

78 FR 14270 - Stainless Steel Sheet and Strip in Coils From Mexico: Notice of Settlement of NAFTA Proceedings

Federal Register 2010, 2011, 2012, 2013, 2014

2013-03-05

... DEPARTMENT OF COMMERCE International Trade Administration [A-201-822] Stainless Steel Sheet and... stainless steel sheet and strip in coils from Mexico (SSSS from Mexico). See Stainless Steel Sheet and Strip..., 2010, as a result of a sunset review. See Stainless Steel Sheet and Strip in Coils from Germany, Italy...

Development of a flocculation sub-model for a 3-D CFD model based on rectangular settling tanks.

PubMed

Gong, M; Xanthos, S; Ramalingam, K; Fillos, J; Beckmann, K; Deur, A; McCorquodale, J A

2011-01-01

To assess performance and evaluate alternatives to improve the efficiency of rectangular Gould II type final settling tanks (FSTs), New York City Department of Environmental Protection and City College of NY developed a 3D computer model depicting the actual structural configuration of the tanks and the current and proposed hydraulic and solids loading rates. Fluent 6.3.26™ was the base platform for the computational fluid dynamics (CFD) model, for which sub-models of the SS settling characteristics, turbulence, flocculation and rheology were incorporated. This was supplemented by field and bench scale experiments to quantify the coefficients integral to the sub-models. The 3D model developed can be used to consider different baffle arrangements, sludge withdrawal mechanisms and loading alternatives to the FSTs. Flocculation in the front half of the rectangular tank especially in the region before and after the inlet baffle is one of the vital parameters that influences the capture efficiency of SS. Flocculation could be further improved by capturing medium and small size particles by creating an additional zone with an in-tank baffle. This was one of the methods that was adopted in optimizing the performance of the tank where the CCNY 3D CFD model was used to locate the in-tank baffle position. This paper describes the development of the flocculation sub-model and the relationship of the flocculation coefficients in the known Parker equation to the initial mixed liquor suspended solids (MLSS) concentration X0. A new modified equation is proposed removing the dependency of the breakup coefficient to the initial value of X0 based on preliminary data using normal and low concentration mixed liquor suspended solids values in flocculation experiments performed.

Uniform field loop-gap resonator and rectangular TEU02 for aqueous sample EPR at 94 GHz

NASA Astrophysics Data System (ADS)

Sidabras, Jason W.; Sarna, Tadeusz; Mett, Richard R.; Hyde, James S.

2017-09-01

In this work we present the design and implementation of two uniform-field resonators: a seven-loop-six-gap loop-gap resonator (LGR) and a rectangular TEU02 cavity resonator. Each resonator has uniform-field-producing end-sections. These resonators have been designed for electron paramagnetic resonance (EPR) of aqueous samples at 94 GHz. The LGR geometry employs low-loss Rexolite end-sections to improve the field homogeneity over a 3 mm sample region-of-interest from near-cosine distribution to 90% uniform. The LGR was designed to accommodate large degassable Polytetrafluorethylen (PTFE) tubes (0.81 mm O.D.; 0.25 mm I.D.) for aqueous samples. Additionally, field modulation slots are designed for uniform 100 kHz field modulation incident at the sample. Experiments using a point sample of lithium phthalocyanine (LiPC) were performed to measure both the uniformity of the microwave magnetic field and 100 kHz field modulation, and confirm simulations. The rectangular TEU02 cavity resonator employs over-sized end-sections with sample shielding to provide an 87% uniform field for a 0.1 × 2 × 6 mm3 sample geometry. An evanescent slotted window was designed for light access to irradiate 90% of the sample volume. A novel dual-slot iris was used to minimize microwave magnetic field perturbations and maintain cross-sectional uniformity. Practical EPR experiments using the application of light irradiated rose bengal (4,5,6,7-tetrachloro-2‧,4‧,5‧,7‧-tetraiodofluorescein) were performed in the TEU02 cavity. The implementation of these geometries providing a practical designs for uniform field resonators that continue resonator advancements towards quantitative EPR spectroscopy.

Solid Freeform Fabrication Symposium Proceedings Held in Austin, Texas on August 9-11, 1993

DTIC Science & Technology

1993-09-01

between the accuracy and the size of the geometric description. Highly non-linear surfaces, such as those that comprise turbine blades , manifolds...flange. The fan blades were modeled using different surfacing techniques. Seven blades are then combined with the rotor to make the completed fan. Figure...successfully cast in aluminum, titanium , beryllium-copper, and stainless steel, with RMS surface finish as low as 1 micrometer, without any subsequent

The particle size distribution, density, and specific surface area of welding fumes from SMAW and GMAW mild and stainless steel consumables.

PubMed

Hewett, P

1995-02-01

Particle size distributions were measured for fumes from mild steel (MS) and stainless steel (SS); shielded metal arc welding (SMAW) and gas metal arc welding (GMAW) consumables. Up to six samples of each type of fume were collected in a test chamber using a micro-orifice uniform deposit (cascade) impactor. Bulk samples were collected for bulk fume density and specific surface area analysis. Additional impactor samples were collected using polycarbonate substrates and analyzed for elemental content. The parameters of the underlying mass distributions were estimated using a nonlinear least squares analysis method that fits a smooth curve to the mass fraction distribution histograms of all samples for each type of fume. The mass distributions for all four consumables were unimodal and well described by a lognormal distribution; with the exception of the GMAW-MS and GMAW-SS comparison, they were statistically different. The estimated mass distribution geometric means for the SMAW-MS and SMAW-SS consumables were 0.59 and 0.46 micron aerodynamic equivalent diameter (AED), respectively, and 0.25 micron AED for both the GMAW-MS and GMAW-SS consumables. The bulk fume densities and specific surface areas were similar for the SMAW-MS and SMAW-SS consumables and for the GMAW-MS and GMAW-SS consumables, but differed between SMAW and GMAW. The distribution of metals was similar to the mass distributions. Particle size distributions and physical properties of the fumes were considerably different when categorized by welding method. Within each welding method there was little difference between MS and SS fumes.

Dynamic behavior of semivolatile organic compounds in indoor air. 2. Nicotine and phenanthrene with carpet and wallboard.

PubMed

Van Loy, M D; Riley, W J; Daisey, J M; Nazaroff, W W

2001-02-01

The surface interactions of nicotine and phenanthrene with carpet, painted wallboard, and stainless steel were investigated in a room-sized environmental test chamber. Adsorption kinetics were tested by flash evaporating a known mass of each compound into a sealed 20 m3 chamber containing one or more of the tested sorbents. In each experiment, one or more emissions were performed after the gas-phase concentration had reached an apparent plateau. At the end of each experiment, the chamber was ventilated and resealed to monitor reemission of the compound from the sorbents. Kinetic sorption parameters were determined by fitting a mass-balance model to the experimental results. The sorption capacity of stainless steel was of similar magnitude for nicotine and phenanthrene. Sorption of nicotine on carpet and wallboard was much stronger, with equilibrium partitioning values 2-3 orders of magnitude higher. The sorption capacities of phenanthrene on carpet and wallboard were smaller, approximately 10-20% of the stainless steel values. The rates of uptake are of similar magnitude for all sorbate--sorbent pairs and are consistent with the limit imposed by gas-phase boundary-layer mass transport. The rates of desorption are much faster for phenanthrene than for nicotine. Model simulations predict average nicotine levels in a typical smoking residence that are consistent with published data.

Solute diffusion through fibrotic tissue formed around protective cage system for implantable devices.

PubMed

Prihandana, Gunawan Setia; Ito, Hikaru; Tanimura, Kohei; Yagi, Hiroshi; Hori, Yuki; Soykan, Orhan; Sudo, Ryo; Miki, Norihisa

2015-08-01

This article presents the concept of an implantable cage system that can house and protect implanted biomedical sensing and therapeutic devices in the body. Cylinder-shaped cages made of porous polyvinyl alcohol (PVA) sheets with an 80-µm pore size and/or stainless steel meshes with 0.54-mm openings were implanted subcutaneously in the dorsal region of rats for 5 weeks. Analysis of the explanted cages showed the formation of fibrosis tissue around the cages. PVA cages had fibrotic tissue growing mostly along the outer surface of cages, while stainless steel cages had fibrotic tissue growing into the inside surface of the cage structure, due to the larger porosity of the stainless steel meshes. As the detection of target molecules with short time lags for biosensors and mass transport with low diffusion resistance into and out of certain therapeutic devices are critical for the success of such devices, we examined whether the fibrous tissue formed around the cages were permeable to molecules of our interest. For that purpose, bath diffusion and microfluidic chamber diffusion experiments using solutions containing the target molecules were performed. Diffusion of sodium, potassium and urea through the fibrosis tissue was confirmed, thus suggesting the potential of these cylindrical cages surrounded by fibrosis tissue to successfully encase implantable sensors and therapeutic apparatus. © 2014 Wiley Periodicals, Inc.

The effect of gap fluctuations on interacting and non-interacting polarization for nano-superconducting grains in electron- and hole-doped cuprates

NASA Astrophysics Data System (ADS)

Afzali, R.; Alizadeh, A.

2017-12-01

The behavior of non-interacting and interacting polarization under influence of fluctuations of the superconducting gap with D-wave symmetry and under consideration of the gap dependence on nano- grain size is obtained in terms of the frequency, temperature and the size at zero and finite temperatures for rectangular cuprate nano-superconducting grains. By using Eliashberg equations and applying the relations of the fermionic dispersion for the hole-doped and electron-doped cuprates, we numerically compute the real part of size-dependent polarization for both types of cuprates. We show that the peak of real part of polarization moves to higher frequency by including the additional fluctuating part of gap (or the nano-size effect). Also, we obtain the temperatures for different frequencies, in which the effect of gap fluctuations fades. In the case of size-dependent gap, there is a critical frequency; for frequencies lower (higher) than the critical frequency, the nano-effect weakens (improves) the superconducting state. Moreover, it is concluded that the real part of polarization for hole- doped cuprates in terms of the grain size has more significant amount in comparison with electron-doped ones.

Development of nano-structured duplex and ferritic stainless steels by pulverisette planetary milling followed by pressureless sintering

DOE Office of Scientific and Technical Information (OSTI.GOV)

R, Shashanka, E-mail: shashankaic@gmail.com; Chaira, D., E-mail: chaira.debasis@gmail.com

Nano-structured duplex and ferritic stainless steel powders are prepared by planetary milling of elemental Fe, Cr and Ni powder for 40 h and then consolidated by conventional pressureless sintering. The progress of milling and the continuous refinement of stainless steel powders have been confirmed by means of X-ray diffraction and scanning electron microscopy. Activation energy for the formation of duplex and ferritic stainless steels is calculated by Kissinger method using differential scanning calorimetry and is found to be 159.24 and 90.17 KJ/mol respectively. Both duplex and ferritic stainless steel powders are consolidated at 1000, 1200 and 1400 °C in argonmore » atmosphere to study microstructure, density and hardness. Maximum sintered density of 90% and Vickers microhardness of 550 HV are achieved for duplex stainless steel sintered at 1400 °C for 1 h. Similarly, 92% sintered density and 263 HV microhardness are achieved for ferritic stainless steel sintered at 1400 °C. - Highlights: • Synthesized duplex and ferritic stainless steels by pulverisette planetary milling • Calculated activation energy for the formation of duplex and ferritic stainless steels • Studied the effect of sintering temperature on density, hardness and microstructure • Duplex stainless steel exhibits 90% sintered density and microhardness of 550 HV. • Ferritic stainless steel shows 92% sintered density and 263 HV microhardness.« less

Recovery and radiation corrections and time constants of several sizes of shielded and unshielded thermocouple probes for measuring gas temperature

NASA Technical Reports Server (NTRS)

Glawe, G. E.; Holanda, R.; Krause, L. N.

1978-01-01

Performance characteristics were experimentally determined for several sizes of a shielded and unshielded thermocouple probe design. The probes are of swaged construction and were made of type K wire with a stainless steel sheath and shield and MgO insulation. The wire sizes ranged from 0.03- to 1.02-mm diameter for the unshielded design and from 0.16- to 0.81-mm diameter for the shielded design. The probes were tested through a Mach number range of 0.2 to 0.9, through a temperature range of room ambient to 1420 K, and through a total-pressure range of 0.03 to 0.2.2 MPa (0.3 to 22 atm). Tables and graphs are presented to aid in selecting a particular type and size. Recovery corrections, radiation corrections, and time constants were determined.

Rectangular optical filter based on high-order silicon microring resonators

NASA Astrophysics Data System (ADS)

Bao, Jia-qi; Yu, Kan; Wang, Li-jun; Yin, Juan-juan

2017-07-01

The rectangular optical filter is one of the most important optical switching components in the dense wavelength division multiplexing (DWDM) fiber-optic communication system and the intelligent optical network. The integrated highorder silicon microring resonator (MRR) is one of the best candidates to achieve rectangular filtering spectrum response. In general, the spectrum response rectangular degree of the single MRR is very low, so it cannot be used in the DWDM system. Using the high-order MRRs, the bandwidth of flat-top pass band, the out-of-band rejection degree and the roll-off coefficient of the edge will be improved obviously. In this paper, a rectangular optical filter based on highorder MRRs with uniform couplers is presented and demonstrated. Using 15 coupled race-track MRRs with 10 μm in radius, the 3 dB flat-top pass band of 2 nm, the out-of-band rejection ratio of 30 dB and the rising and falling edges of 48 dB/nm can be realized successfully.

Optimal neighborhood indexing for protein similarity search.

PubMed

Peterlongo, Pierre; Noé, Laurent; Lavenier, Dominique; Nguyen, Van Hoa; Kucherov, Gregory; Giraud, Mathieu

2008-12-16

Similarity inference, one of the main bioinformatics tasks, has to face an exponential growth of the biological data. A classical approach used to cope with this data flow involves heuristics with large seed indexes. In order to speed up this technique, the index can be enhanced by storing additional information to limit the number of random memory accesses. However, this improvement leads to a larger index that may become a bottleneck. In the case of protein similarity search, we propose to decrease the index size by reducing the amino acid alphabet. The paper presents two main contributions. First, we show that an optimal neighborhood indexing combining an alphabet reduction and a longer neighborhood leads to a reduction of 35% of memory involved into the process, without sacrificing the quality of results nor the computational time. Second, our approach led us to develop a new kind of substitution score matrices and their associated e-value parameters. In contrast to usual matrices, these matrices are rectangular since they compare amino acid groups from different alphabets. We describe the method used for computing those matrices and we provide some typical examples that can be used in such comparisons. Supplementary data can be found on the website http://bioinfo.lifl.fr/reblosum. We propose a practical index size reduction of the neighborhood data, that does not negatively affect the performance of large-scale search in protein sequences. Such an index can be used in any study involving large protein data. Moreover, rectangular substitution score matrices and their associated statistical parameters can have applications in any study involving an alphabet reduction.

Optimal neighborhood indexing for protein similarity search

PubMed Central

Peterlongo, Pierre; Noé, Laurent; Lavenier, Dominique; Nguyen, Van Hoa; Kucherov, Gregory; Giraud, Mathieu

2008-01-01

Background Similarity inference, one of the main bioinformatics tasks, has to face an exponential growth of the biological data. A classical approach used to cope with this data flow involves heuristics with large seed indexes. In order to speed up this technique, the index can be enhanced by storing additional information to limit the number of random memory accesses. However, this improvement leads to a larger index that may become a bottleneck. In the case of protein similarity search, we propose to decrease the index size by reducing the amino acid alphabet. Results The paper presents two main contributions. First, we show that an optimal neighborhood indexing combining an alphabet reduction and a longer neighborhood leads to a reduction of 35% of memory involved into the process, without sacrificing the quality of results nor the computational time. Second, our approach led us to develop a new kind of substitution score matrices and their associated e-value parameters. In contrast to usual matrices, these matrices are rectangular since they compare amino acid groups from different alphabets. We describe the method used for computing those matrices and we provide some typical examples that can be used in such comparisons. Supplementary data can be found on the website . Conclusion We propose a practical index size reduction of the neighborhood data, that does not negatively affect the performance of large-scale search in protein sequences. Such an index can be used in any study involving large protein data. Moreover, rectangular substitution score matrices and their associated statistical parameters can have applications in any study involving an alphabet reduction. PMID:19087280

Characterization of friction stir welded joint of low nickel austenitic stainless steel and modified ferritic stainless steel

NASA Astrophysics Data System (ADS)

Mondal, Mounarik; Das, Hrishikesh; Ahn, Eun Yeong; Hong, Sung Tae; Kim, Moon-Jo; Han, Heung Nam; Pal, Tapan Kumar

2017-09-01

Friction stir welding (FSW) of dissimilar stainless steels, low nickel austenitic stainless steel and 409M ferritic stainless steel, is experimentally investigated. Process responses during FSW and the microstructures of the resultant dissimilar joints are evaluated. Material flow in the stir zone is investigated in detail by elemental mapping. Elemental mapping of the dissimilar joints clearly indicates that the material flow pattern during FSW depends on the process parameter combination. Dynamic recrystallization and recovery are also observed in the dissimilar joints. Among the two different stainless steels selected in the present study, the ferritic stainless steels shows more severe dynamic recrystallization, resulting in a very fine microstructure, probably due to the higher stacking fault energy.

Tensiometer methods

DOEpatents

Grover, Blair K.; Hubbell, Joel M.; Sisson, James B.; Casper, William L.

2005-12-20

A method for collecting data regarding a matric potential of a media includes providing a tensiometer having a stainless steel tensiometer casing, the stainless steel tensiometer casing comprising a tip portion which includes a wetted porous stainless steel membrane through which a matric potential of a media is sensed; driving the tensiometer into the media using an insertion tube comprising a plurality of probe casing which are selectively coupled to form the insertion tube as the tensiometer is progressively driven deeper into the media, wherein the wetted porous stainless steel membrane is in contact with the media; and sensing the matric potential the media exerts on the wetted porous stainless steel membrane by a pressure sensor in fluid hydraulic connection with the porous stainless steel membrane. A tensiometer includes a stainless steel casing.

A modal approach to piano soundboard vibroacoustic behavior.

PubMed

Trévisan, Benjamin; Ege, Kerem; Laulagnet, Bernard

2017-02-01

This paper presents an analytical method for modeling the vibro-acoustic behavior of ribbed non-rectangular orthotropic clamped plates. To do this, the non-rectangular plate is embedded in an extended rectangular simply supported plate on which a spring distribution is added, blocking the extended part of the surface, and allowing the description of any inner surface shapes. The acoustical radiation of the embedded plate is ensured using the radiation impedances of the extended rectangular simply supported plate. This method is applied to an upright piano soundboard: a non-rectangular orthotropic plate ribbed in both directions by several straight stiffeners. A modal decomposition is adopted on the basis of the rectangular extended simply supported plate modes, making it possible to calculate the modes of a piano soundboard in the frequency range [0;3000] Hz, showing the different associated mode families. Likewise, the acoustical radiation is calculated using the radiation impedances of a simply supported baffled plate, demonstrating the influence of the string coupling point positions on the acoustic radiated power. The paper ends with the introduction of indicators taking into account spatial and spectral variations of the excitation depending on the notes, which add to the accuracy of the study from the musical standpoint. A parametrical study, which includes several variations of soundboard design, highlights the complexity of rendering high-pitched notes homogeneous.

Turbulence Measurements of Rectangular Nozzles with Bevel

NASA Technical Reports Server (NTRS)

Bridges, James; Wernet, Mark P.

2015-01-01

This paper covers particle image velocimetry measurements of a family of rectangular nozzles with aspect ratios 2, 4, and 8, in the high subsonic flow regime. Far-field acoustic results, presented previously, showed that increasing aspect ratios increased the high frequency noise, especially directed in the polar plane containing the minor axis of the nozzle. The measurements presented here have important implications in the modeling of turbulent sources for acoustic analogy theories. While the nonaxisymmetric mean flow from the rectangular nozzles can be studied reliably using computational solutions, the nonaxisymmetry of the turbulent fluctuations, particularly at the level of velocity components, cannot; only measurements such as these can determine the impact of nozzle geometry on acoustic source anisotropy. Additional nozzles were constructed that extended the wide lip on one side of these nozzles to form beveled nozzles. The paper first documents the velocity fields, mean and variance, from the round, rectangular, and beveled rectangular nozzles at high subsonic speeds. A second section introduces measures of the isotropy of the turbulence, such as component ratios and lengthscales, first by showing them for a round jet and then for the rectangular nozzles. From these measures the source models of acoustic analogy codes can be judged or modified to account for these anisotropies.

Analysis of the rectangular resonator with butterfly MMI coupler using SOI

NASA Astrophysics Data System (ADS)

Kim, Sun-Ho; Park, Jun-Hee; Kim, Eudum; Jeon, Su-Jin; Kim, Ji-Hoon; Choi, Young-Wan

2018-02-01

We propose a rectangular resonator sensor structure with butterfly MMI coupler using SOI. It consists of the rectangular resonator, total internal reflection (TIR) mirror, and the butterfly MMI coupler. The rectangular resonator is expected to be used as bio and chemical sensors because of the advantages of using MMI coupler and the absence of bending loss unlike ring resonators. The butterfly MMI coupler can miniaturize the device compared to conventional MMI by using a linear butterfly shape instead of a square in the MMI part. The width, height, and slab height of the rib type waveguide are designed to be 1.5 μm, 1.5 μm, and 0.9 μm, respectively. This structure is designed as a single mode. When designing a TIR mirror, we considered the Goos-Hänchen shift and critical angle. We designed 3:1 MMI coupler because rectangular resonator has no bending loss. The width of MMI is designed to be 4.5 μm and we optimize the length of the butterfly MMI coupler using finite-difference time-domain (FDTD) method for higher Q-factor. It has the equal performance with conventional MMI even though the length is reduced by 1/3. As a result of the simulation, Qfactor of rectangular resonator can be obtained as 7381.

Sound attenuation of fiberglass lined ventilation ducts

NASA Astrophysics Data System (ADS)

Albright, Jacob

Sound attenuation is a crucial part of designing any HVAC system. Most ventilation systems are designed to be in areas occupied by one or more persons. If these systems do not adequately attenuate the sound of the supply fan, compressor, or any other source of sound, the affected area could be subject to an array of problems ranging from an annoying hum to a deafening howl. The goals of this project are to quantify the sound attenuation properties of fiberglass duct liner and to perform a regression analysis to develop equations to predict insertion loss values for both rectangular and round duct liners. The first goal was accomplished via insertion loss testing. The tests performed conformed to the ASTM E477 standard. Using the insertion loss test data, regression equations were developed to predict insertion loss values for rectangular ducts ranging in size from 12-in x 18-in to 48-in x 48-in in lengths ranging from 3ft to 30ft. Regression equations were also developed to predict insertion loss values for round ducts ranging in diameters from 12-in to 48-in in lengths ranging from 3ft to 30ft.

Characterization of the Shielded Neutron Source at Triangle Universities Nuclear Laboratory

NASA Astrophysics Data System (ADS)

Hobson, Chad; Finch, Sean; Howell, Calvin; Malone, Ron; Tornow, Wernew

2016-09-01

In 2015, Triangle Universities Nuclear Laboratory rebuilt its shielded neutron source (SNS) with the goal of improving neutron beam collimation and reducing neutron and gamma-ray backgrounds. Neutrons are produced via the 2H(d,n)3He reaction and then collimated by heavy shielding to form a beam. The SNS has the ability to produce both a rectangular and circular neutron beam through use of two collimators with different beam apertures. Our work characterized both the neutron beam profiles as well as the neutron and gamma-ray backgrounds at various locations around the SNS. This characterization was performed to provide researchers who use the SNS with beam parameters necessary to plan and conduct an experiment. Vertical and horizontal beam profiles were measured at two different distances from the neutron production cell by scanning a small plastic scintillator across the face of the beam at various energies for each collimator. Background neutron and gamma-ray intensities were measured using time-of-flight techniques at 10 MeV and 16 MeV with the rectangular collimator. We present results on the position and size of neutron beam as well as on the structure and magnitude of the backgrounds.

Vibrational modes and frequencies of borophene in comparison with graphene nanosheets

NASA Astrophysics Data System (ADS)

Sadeghzadeh, S.; Khatibi, M. M.

2018-05-01

In this paper, for the first time, by applying molecular dynamics simulation in conjugation with frequency domain decomposition, it was demonstrated that borophene resonators are at least 100% more efficient than graphene ones. It was also shown that this significant superiority does not arise solely from the difference between the molecular weights of borophene and graphene, but rather from the amazing intrinsic mechanical properties of borophene. Interest in detecting lower masses and lower pressures has led to a scientific race to find resonators with higher resonant frequencies. As a powerful rival of graphene, and used to fabricate sensors with lower-than-zeptogram resolutions, borophene promises enhanced future capabilities. Studies of the effects of geometrical parameters have verified that resonance is fully dependent on resonator size and chirality. The fundamental natural frequency of a rectangular borophene sheet is much higher when its zigzag edge is longer than the armchair edge, but not the other way around. Generally, it can be concluded that a rectangular borophene resonator with a longer zigzag edge achieves a higher resonance than a graphene resonator of equivalent weight. As a final fascinating conclusion: Borophene seems to be superior to graphene in resonance applications.

Effect of Secondary Cooling Conditions on Solidification Structure and Central Macrosegregation in Continuously Cast High-Carbon Rectangular Billet

NASA Astrophysics Data System (ADS)

Zeng, Jie; Chen, Weiqing

2015-10-01

Solidification structures of high carbon rectangular billet with a size of 180 mm × 240 mm in different secondary cooling conditions were simulated using cellular automaton-finite element (CAFE) coupling model. The adequacy of the model was compared with the simulated and the actual macrostructures of 82B steel. Effects of the secondary cooling water intensity on solidification structures including the equiaxed grain ratio and the equiaxed grain compactness were discussed. It was shown that the equiaxed grain ratio and the equiaxed grain compactness changed in the opposite direction at different secondary cooling water intensities. Increasing the secondary cooling water intensity from 0.9 or 1.1 to 1.3 L/kg could improve the equiaxed grain compactness and decrease the equiaxed grain ratio. Besides, the industrial test was conducted to investigate the effect of different secondary cooling water intensities on the center carbon macrosegregation of 82B steel. The optimum secondary cooling water intensity was 0.9 L/kg, while the center carbon segregation degree was 1.10. The relationship between solidification structure and center carbon segregation was discussed based on the simulation results and the industrial test.

Numerical simulation of magnetic nano drug targeting in patient-specific lower respiratory tract

NASA Astrophysics Data System (ADS)

Russo, Flavia; Boghi, Andrea; Gori, Fabio

2018-04-01

Magnetic nano drug targeting, with an external magnetic field, can potentially improve the drug absorption in specific locations of the body. However, the effectiveness of the procedure can be reduced due to the limitations of the magnetic field intensity. This work investigates this technique with the Computational Fluid Dynamics (CFD) approach. A single rectangular coil generates the external magnetic field. A patient-specific geometry of the Trachea, with its primary and secondary bronchi, is reconstructed from Digital Imaging and Communications in Medicine (DICOM) formatted images, throughout the Vascular Modelling Tool Kit (VMTK) software. A solver, coupling the Lagrangian dynamics of the magnetic nanoparticles with the Eulerian dynamics of the air, is used to perform the simulations. The resistive pressure, the pulsatile inlet velocity and the rectangular coil magnetic field are the boundary conditions. The dynamics of the injected particles is investigated without and with the magnetic probe. The flow field promotes particles adhesion to the tracheal wall. The particles volumetric flow rate in both cases has been calculated. The magnetic probe is shown to increase the particles flow in the target region, but at a limited extent. This behavior has been attributed to the small particle size and the probe configuration.

Traction-free vibrations of finite trigonal elastic cylinders.

PubMed

Heyliger, Paul R; Johnson, Ward L

2003-04-01

The unrestrained, traction-free vibrations of finite elastic cylinders with trigonal material symmetry are studied using two approaches, based on the Ritz method, which formulate the weak form of the equations of motion in cylindrical and rectangular coordinates. Elements of group theory are used to divide approximation functions into orthogonal subsets, thus reducing the size of the computational problem and classifying the general symmetries of the vibrational modes. Results for the special case of an isotropic cylinder are presented and compared with values published by other researchers. For the isotropic case, the relative accuracy of the formulations in cylindrical and rectangular coordinates can be evaluated, because exact analytical solutions are known for the torsional modes. The calculation in cylindrical coordinates is found to be more accurate for a given number of terms in the series approximation functions. For a representative trigonal material, langatate, calculations of the resonant frequencies and the sensitivity of the frequencies on each of the elastic constants are presented. The dependence on geometry (ratio of length to diameter) is briefly explored. The special case of a transversely isotropic cylinder (with the elastic stiffness C14 equal to zero) is also considered.

ENDOR with band-selective shaped inversion pulses

NASA Astrophysics Data System (ADS)

Tait, Claudia E.; Stoll, Stefan

2017-04-01

Electron Nuclear DOuble Resonance (ENDOR) is based on the measurement of nuclear transition frequencies through detection of changes in the polarization of electron transitions. In Davies ENDOR, the initial polarization is generated by a selective microwave inversion pulse. The rectangular inversion pulses typically used are characterized by a relatively low selectivity, with full inversion achieved only for a limited number of spin packets with small resonance offsets. With the introduction of pulse shaping to EPR, the rectangular inversion pulses can be replaced with shaped pulses with increased selectivity. Band-selective inversion pulses are characterized by almost rectangular inversion profiles, leading to full inversion for spin packets with resonance offsets within the pulse excitation bandwidth and leaving spin packets outside the excitation bandwidth largely unaffected. Here, we explore the consequences of using different band-selective amplitude-modulated pulses designed for NMR as the inversion pulse in ENDOR. We find an increased sensitivity for small hyperfine couplings compared to rectangular pulses of the same bandwidth. In echo-detected Davies-type ENDOR, finite Fourier series inversion pulses combine the advantages of increased absolute ENDOR sensitivity of short rectangular inversion pulses and increased sensitivity for small hyperfine couplings of long rectangular inversion pulses. The use of pulses with an almost rectangular frequency-domain profile also allows for increased control of the hyperfine contrast selectivity. At X-band, acquisition of echo transients as a function of radiofrequency and appropriate selection of integration windows during data processing allows efficient separation of contributions from weakly and strongly coupled nuclei in overlapping ENDOR spectra within a single experiment.

Global field synchronization in gamma range of the sleep EEG tracks sleep depth: Artifact introduced by a rectangular analysis window.

PubMed

Rusterholz, Thomas; Achermann, Peter; Dürr, Roland; Koenig, Thomas; Tarokh, Leila

2017-06-01

Investigating functional connectivity between brain networks has become an area of interest in neuroscience. Several methods for investigating connectivity have recently been developed, however, these techniques need to be applied with care. We demonstrate that global field synchronization (GFS), a global measure of phase alignment in the EEG as a function of frequency, must be applied considering signal processing principles in order to yield valid results. Multichannel EEG (27 derivations) was analyzed for GFS based on the complex spectrum derived by the fast Fourier transform (FFT). We examined the effect of window functions on GFS, in particular of non-rectangular windows. Applying a rectangular window when calculating the FFT revealed high GFS values for high frequencies (>15Hz) that were highly correlated (r=0.9) with spectral power in the lower frequency range (0.75-4.5Hz) and tracked the depth of sleep. This turned out to be spurious synchronization. With a non-rectangular window (Tukey or Hanning window) these high frequency synchronization vanished. Both, GFS and power density spectra significantly differed for rectangular and non-rectangular windows. Previous papers using GFS typically did not specify the applied window and may have used a rectangular window function. However, the demonstrated impact of the window function raises the question of the validity of some previous findings at higher frequencies. We demonstrated that it is crucial to apply an appropriate window function for determining synchronization measures based on a spectral approach to avoid spurious synchronization in the beta/gamma range. Copyright © 2017 Elsevier B.V. All rights reserved.

Operation in the turbulent jet field of a linear array of multiple rectangular jets using a two-dimensional jet (Variation of mean velocity field)

NASA Astrophysics Data System (ADS)

Fujita, Shigetaka; Harima, Takashi

2016-03-01

The mean flowfield of a linear array of multiple rectangular jets run through transversely with a two-dimensional jet, has been investigated, experimentally. The object of this experiment is to operate both the velocity scale and the length scale of the multiple rectangular jets using a two-dimensional jet. The reason of the adoption of this nozzle exit shape was caused by the reports of authors in which the cruciform nozzle promoted the inward secondary flows strongly on both the two jet axes. Aspect ratio of the rectangular nozzle used in this experiment was 12.5. Reynolds number based on the nozzle width d and the exit mean velocity Ue (≅ 39 m / s) was kept constant 25000. Longitudinal mean velocity was measured using an X-array Hot-Wire Probe (lh = 3.1 μm in diameter, dh = 0.6 mm effective length : dh / lh = 194) operated by the linearized constant temperature anemometers (DANTEC), and the spanwise and the lateral mean velocities were measured using a yaw meter. The signals from the anemometers were passed through the low-pass filters and sampled using A.D. converter. The processing of the signals was made by a personal computer. Acquisition time of the signals was usually 60 seconds. From this experiment, it was revealed that the magnitude of the inward secondary flows on both the y and z axes in the upstream region of the present jet was promoted by a two-dimensional jet which run through transversely perpendicular to the multiple rectangular jets, therefore the potential core length on the x axis of the present jet extended 2.3 times longer than that of the multiple rectangular jets, and the half-velocity width on the rectangular jet axis of the present jet was suppressed 41% shorter compared with that of the multiple rectangular jets.

77 FR 60673 - Drawn Stainless Steel Sinks From the People's Republic of China: Antidumping Duty Investigation

Federal Register 2010, 2011, 2012, 2013, 2014

2012-10-04

... countertop). Stainless steel sinks with multiple drawn bowls that are joined through a welding operation to... the stainless steel, and then welding and finishing the vertical corners to form the bowls. Stainless...

Mechanical properties and microstructure of copper alloys and copper alloy-stainless steel laminates for fusion reactor high heat flux applications

NASA Astrophysics Data System (ADS)

Leedy, Kevin Daniel

A select group of copper alloys and bonded copper alloy-stainless steel panels are under consideration for heat sink applications in first wall and divertor structures of a planned thermonuclear fusion reactor. Because these materials must retain high strengths and withstand high heat fluxes, their material properties and microstructures must be well understood. Candidate copper alloys include precipitate strengthened CuNiBe and CuCrZr and dispersion strengthened Cu-Alsb2Osb3 (CuAl25). In this study, uniaxial mechanical fatigue tests were conducted on bulk copper alloy materials at temperatures up to 500sp°C in air and vacuum environments. Based on standardized mechanical properties measurement techniques, a series of tests were also implemented to characterize copper alloy-316L stainless steel joints produced by hot isostatic pressing or by explosive bonding. The correlation between mechanical properties and the microstructure of fatigued copper alloys and the interface of copper alloy-stainless steel laminates was examined. Commercial grades of these alloys were used to maintain a degree of standardization in the materials testing. The commercial alloys used were OMG Americas Glidcop CuAl25 and CuAl15; Brush Wellman Hycon 3HP and Trefimetaux CuNiBe; and Kabelmetal Elbrodur and Trefimetaux CuCrZr. CuAl25 and CuNiBe alloys possessed the best combination of fatigue resistance and microstructural stability. The CuAl25 alloy showed only minimal microstructural changes following fatigue while the CuNiBe alloy consistently exhibited the highest fatigue strength. Transmission electron microscopy observations revealed that small matrix grain sizes and high densities of submicron strengthening phases promoted homogeneous slip deformation in the copper alloys. Thus, highly organized fatigue dislocation structure formation, as commonly found in oxygen-free high conductivity Cu, was inhibited. A solid plate of CuAl25 alloy hot isostatically pressed to a 316L stainless steel plate showed the best overall mechanical properties of the studied bi-metallic bonded panels. Bond properties were nominally inferior to constituent bulk material properties and fracture toughness values, in particular, were quite low for all bonded laminates. Delamination near the copper alloy-stainless steel interface was the dominate failure mode in the bi-metallic panels. The joining processes caused microstructural alterations in the bond interfacial regions including: microporosity, new precipitate formation, existing precipitate morphology changes and interdiffusion of constituent elements.

Stainless steel reinforcement as a replacement for epoxy coated steel in bridge decks : final report.

DOT National Transportation Integrated Search

2013-08-01

The corrosion resistance of 2304 stainless steel reinforcement and stainless steel clad reinforcement was compared to conventional and epoxy-coated reinforcement (ECR). 2304 stainless steel was tested in both the as-received condition (dark mottled f...

Tensiometer methods and apparatus

DOEpatents

Grover, Blair K.; Hubbell, Joel M.; Sisson, James B.; Casper, William L.

2004-08-10

A method for collecting data regarding a matric potential of a media includes providing a tensiometer having a stainless steel tensiometer casing, the stainless steel tensiometer casing comprising a tip portion which includes a wetted porous stainless steel membrane through which a matric potential of a media is sensed; driving the tensiometer into the media using an insertion tube comprising a plurality of probe casing which are selectively coupled to form the insertion tube as the tensiometer is progressively driven deeper into the media, wherein the wetted porous stainless steel membrane is in contact with the media; and sensing the matric potential the media exerts on the wetted porous stainless steel membrane by a pressure sensor in fluid hydraulic connection with the porous stainless steel membrane. A tensiometer includes a stainless steel casing.

Enhanced Mechanical Properties of 316L Stainless Steel Prepared by Aluminothermic Reaction Subjected to Multiple Warm Rolling

NASA Astrophysics Data System (ADS)

Li, Z. N.; Wei, F. A.; La, P. Q.; Ma, F. L.

2018-05-01

Large dimensional bulk 316L stainless steels were prepared by aluminothermic reaction method and rolled at 973 K (700 °C) with different deformation, the microstructures evolution and mechanical properties were characterized in detail. The results showed that the microstructure of casting steel consists of nanocrystalline/submicrocrystalline/microcrystalline austenite and submicrocrystalline ferrite. After rolling to thickness reduction of 30, 50 and 70%, the submicrocrystalline austenite grains were crushed and dispersed more uniformly in the matrix of the steel, the grain size of submicrocrystalline austenite decreased from 246 to 136 nm. The mechanical properties of the rolled steels were significantly enhanced, with the thickness reduction increased from 30 to 70%, the tensile strength increased from 632 to 824 MPa, the yield strength increased from 425 to 615 MPa, and the elongation increased from 11 to 24%. After rolling to thickness reduction of 70%, the optimized combination of high strength and high ductility was obtained.

The effects of cold work on the microstructure and mechanical properties of intermetallic strengthened alumina-forming austenitic stainless steels

DOE PAGES

Hu, Bin; Baker, Ian; Miller, Michael K.; ...

2015-06-12

In order to achieve energy conversion efficiencies of >50 pct for steam turbines/boilers in power generation systems, materials are required that are both strong and corrosion-resistant at >973 K (700 °C), and economically viable. Austenitic steels strengthened with Laves phase, NiAl and Ni 3Al precipitates, and alloyed with aluminum to improve oxidation resistance, are potential candidate materials for these applications. The microstructure and microchemistry of recently developed alumina-forming austenitic stainless steels have been characterized by scanning electron microscopy, transmission electron microscopy, and synchrotron X-ray diffraction. Different thermo-mechanical treatments were performed on these steels to improve their mechanical performance. These reducedmore » the grain size significantly to the nanoscale (~100 nm) and the room temperature yield strength to above 1000 MPa. Lastly, a solutionizing anneal at 1473 K (1200 °C) was found to be effective for uniformly redistributing the Laves phase precipitates that form upon casting.« less

In situ TEM study of G-phase precipitates under heavy ion irradiation in CF8 cast austenitic stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Wei-Ying; Li, Meimei; Zhang, Xuan

2015-09-01

Thermally-aged cast austenitic stainless steels (CASS) CF8 was irradiated with 1 MeV Kr ions at 300, 350 and 400°C to 1.88x10^15 ions/cm2 (~3 dpa) at the IVEM-Tandem Facility at the Argonne National Laboratory. Before irradiation, the distribution of G-phase precipitates in the ferrite showed strong spatial variations, and both their size and density were affected by the ferrite-austenite phase boundary and presence of M23C6 carbides. Under 300°C irradiation, in-situ TEM observation showed G-phase precipitates were relatively unchanged in the vicinity of the phase boundary M23C6 carbides, while the density of G-phase precipitates increased with increasing dose within the ferrite matrix.more » Coarsening of G-phase precipitates was observed in the vicinity of phase boundary M23C6 carbides at 350°C and 400°C.« less

Effect of cold deformation on the electrochemical behaviour of 304L stainless steel in contaminated sulfuric acid environment

NASA Astrophysics Data System (ADS)

Luo, Hong; Su, Huaizhi; Ying, Guobing; Dong, Chaofang; Li, Xiaogang

2017-12-01

The effect of cold deformation on the microstructure and electrochemical corrosion behaviour of 304L stainless steel in contaminated sulfuric acid solutions (simulated proton exchange membrane fuel cells environments) were evaluated using electron backscatter diffraction analyses, electrochemical measurements, and surface analyses. The internal microstructure,including the grain sizes, angles of the grain boundaries, low coincidence site lattice boundaries, and phase transformations, was changed due to the cold deformation. No noticeable modifications of the pitting corrosion potential were observed during the various deformations, except for a slight enhancement in the passive current density with an increase in the deformation. The CrO3 and metal Ni species in the passive film were investigated after deformation. After heavy deformation (greater than 60%), nickel oxides were detected. Moreover, the Cr/Fe and O2-/OH- ratios in the passive film were higher before deformation, and they decreased with an increase in the deformation level.

The mechanical and morphological properties of bone beneath internal fixation plates of differing rigidity.

PubMed

Claes, L

1989-01-01

The internal fixation of diaphyseal fractures by bone plates is a well recognized treatment. The normal physiological stress of bone is reduced by plates that cause a negative balance of bone-remodeling processes. Many investigators have shown that the degree of stress protection is dependent on the rigidity of the plates. It was the aim of this study to quantify mechanical and morphological changes at different locations in a plated diaphyseal bone as a function of differing plate rigidity. Two types of plates with the same size but different materials were used. The stainless steel plates had a modulus of elasticity and bending stiffness 3.2 times higher than the carbon fiber reinforced carbon plates. Both types of plates were applied to the intact right and left femora of six foxhounds for 6 months. The stiffer stainless steel plates led to a significantly higher bone loss and correspondingly greater loss of mechanical properties. These effects were greatest directly beneath the plate and less with increasing distance from the plate.

Effect of sintering atmosphere on properties of porous stainless steel for biomedical applications.

PubMed

Dudek, Agata; Włodarczyk, Renata

2013-01-01

This study discusses manufacturing of metallic biomaterials by means of powder metallurgy with consideration for their unquestionable advantages, i.e. opportunities of obtaining materials with controllable porosity. The paper focuses on properties of 316 L stainless steel obtained using the method of powder metallurgy with respect to compacting pressure and sintering atmosphere. All the specimens were compacted at 700, 400 and 225 MPa, and sintered at 1250 °C. In order to analyze the sintering atmosphere, three different media were used: dissociated ammonia, hydrogen and vacuum. The study covered sintering density, porosity, microstructure analysis and corrosion resistance. The proposed method of powder metallurgy allowed for obtaining materials with predictable size and distribution of pores, depending on the parameters of sinter preparation (compaction force, sinter atmosphere). High corrosion resistance of the materials (sintering in the atmosphere of hydrogen and in vacuum) and high porosity in the sinters studied offer opportunities for using them for medical purposes. Copyright © 2012 Elsevier B.V. All rights reserved.

In Situ Neutron Diffraction Study of the Influence of Microstructure on the Mechanical Response of Additively Manufactured 304L Stainless Steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brown, D. W.; Adams, D. P.; Balogh, L.

In situ neutron diffraction measurements were completed for this study during tensile and compressive deformation of stainless steel 304L additively manufactured (AM) using a high power directed energy deposition process. Traditionally produced wrought 304L material was also studied for comparison. The AM material exhibited roughly 200 MPa higher flow stress relative to the wrought material. Crystallite size, crystallographic texture, dislocation density, and lattice strains were all characterized to understand the differences in the macroscopic mechanical behavior. The AM material’s initial dislocation density was about 10 times that of the wrought material, and the flow strength of both materials obeyed themore » Taylor equation, indicating that the AM material’s increased yield strength was primarily due to greater dislocation density. Finally, a ~50 MPa flow strength tension/compression asymmetry was observed in the AM material, and several potential causes were examined.« less

Comparative shock response of additively manufactured versus conventionally wrought 304L stainless steel

NASA Astrophysics Data System (ADS)

Wise, J. L.; Adams, D. P.; Nishida, E. E.; Song, B.; Maguire, M. C.; Carroll, J.; Reedlunn, B.; Bishop, J. E.; Palmer, T. A.

2017-01-01

Gas-gun experiments have probed the compression and release behavior of impact-loaded 304L stainless steel specimens that were machined from additively manufactured (AM) blocks as well as baseline ingot-derived bar stock. The AM technology permits direct fabrication of net- or near-net-shape metal parts. For the present investigation, velocity interferometer (VISAR) diagnostics provided time-resolved measurements of sample response for one-dimensional (i.e., uniaxial strain) shock compression to peak stresses ranging from 0.2 to 7.0 GPa. The acquired wave-profile data have been analyzed to determine the comparative Hugoniot Elastic Limit (HEL), Hugoniot equation of state, spall strength, and high-pressure yield strength of the AM and conventional materials. The possible contributions of various factors, such as composition, porosity, microstructure (e.g., grain size and morphology), residual stress, and/or sample axis orientation relative to the additive manufacturing deposition trajectory, are considered to explain differences between the AM and baseline 304L dynamic material results.

Quasi-Isentropic Compression of Wrought and Additively Manufactures 304L Stainless Steel

NASA Astrophysics Data System (ADS)

Specht, Paul; Brown, Justin; Wise, Jack; Furnish, Michael; Adams, David

2017-06-01

The thermodynamic and constitutive responses of both additively manufactured (AM) and traditional wrought processed 304L stainless steel (SS) were investigated through quasi-isentropic compression to peak stresses near 1Mbar using Sandia National Laboratories' Z machine. The AM 304L SS samples were made with a laser engineered net shaping (LENS™) technique. Compared to traditional wrought processed 304L SS, the AM samples were highly textured with larger grain sizes (i.e.near 1mm) and residual stresses (> 100 MPa). Interferometric measurements of interface velocities enabled inference of the quasi-isentropes for each fabrication type of 304L SS. Release from peak stress provided flow strength measurements of the wrought and AM 304L SS. Sandia National Laboratories is a multi-mission laboratory managed and operated by Sandia Corporation, a wholly owned subsidiary of Lockheed Martin Corporation, for the U.S. Department of Energy's National Nuclear Security Administration under contract DE-AC04-94AL85000. Approved For Unclassified Unlimited Release SAND2017-2040A.

In Situ Neutron Diffraction Study of the Influence of Microstructure on the Mechanical Response of Additively Manufactured 304L Stainless Steel

DOE PAGES

Brown, D. W.; Adams, D. P.; Balogh, L.; ...

2017-10-10

In situ neutron diffraction measurements were completed for this study during tensile and compressive deformation of stainless steel 304L additively manufactured (AM) using a high power directed energy deposition process. Traditionally produced wrought 304L material was also studied for comparison. The AM material exhibited roughly 200 MPa higher flow stress relative to the wrought material. Crystallite size, crystallographic texture, dislocation density, and lattice strains were all characterized to understand the differences in the macroscopic mechanical behavior. The AM material’s initial dislocation density was about 10 times that of the wrought material, and the flow strength of both materials obeyed themore » Taylor equation, indicating that the AM material’s increased yield strength was primarily due to greater dislocation density. Finally, a ~50 MPa flow strength tension/compression asymmetry was observed in the AM material, and several potential causes were examined.« less

Influence of substrate microcrystallinity on the orientation of laser-induced periodic surface structures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nürnberger, P.; Reinhardt, H.; Kim, H-C.

2015-10-07

The research in this paper deals with the angular dependence of the formation of laser-induced periodic surface structures (LIPSS) by linearly polarized nanosecond laser pulses on polycrystalline austenitic stainless steel. Incident angles ranging from 45° to 70° lead to the generation of superimposed merely perpendicular oriented LIPSS on steel as well as on monocrystalline (100) silicon which was used as a reference material. Additional extraordinary orientations of superimposing LIPSS along with significantly different periodicities are found on polycrystalline steel but not on (100) silicon. Electron backscatter diffraction measurements indicate that the expansion of these LIPSS is limited to the grainmore » size and affected by the crystal orientation of the individual grains. Atomic force microscopy imaging shows that LIPSS fringe heights are in good agreement with the theoretically predicted penetration depths of surface plasmon polaritons into stainless steel. These results indicate that optical anisotropies must be taken into account to fully describe the theory of light-matter interaction leading to LIPSS formation.« less

748 K (475 °C) Embrittlement of Duplex Stainless Steel: Effect on Microstructure and Fracture Behavior

NASA Astrophysics Data System (ADS)

Örnek, Cem; Burke, M. G.; Hashimoto, T.; Engelberg, D. L.

2017-04-01

22Cr-5Ni duplex stainless steel (DSS) was aged at 748 K (475 °C) and the microstructure development correlated to changes in mechanical properties and fracture behavior. Tensile testing of aged microstructures confirmed the occurrence of 748 K (475 °C) embrittlement, which was accompanied by an increase of strength and hardness and loss of toughness. Aging caused spinodal decomposition of the ferrite phase, consisting of Cr-enriched α″ and Fe-rich α' and the formation of a large number of R-phase precipitates, with sizes between 50 and 400 nm. Fracture surface analyses revealed a gradual change of the fracture mode from ductile to brittle delamination fracture, associated with slip incompatibility between ferrite and austenite. Ferrite became highly brittle after 255 hours of aging, mainly due to the presence of precipitates, while austenite was ductile and accommodated most plastic strain. The fracture mechanism as a function of 748 K (475 °C) embrittlement is discussed in light of microstructure development.

In situ TEM study of G-phase precipitates under heavy ion irradiation in CF8 cast austenitic stainless steel

NASA Astrophysics Data System (ADS)

Chen, Wei-Ying; Li, Meimei; Zhang, Xuan; Kirk, Marquis A.; Baldo, Peter M.; Lian, Tiangan

2015-09-01

Thermally-aged cast austenitic stainless steels (CASS) CF8 was irradiated with 1 MeV Kr ions at 300, 350 and 400 °C to 1.88 × 1019 ions/m2 (∼3 dpa) at the IVEM-Tandem Facility at the Argonne National Laboratory. Before irradiation, the distribution of G-phase precipitates in the ferrite showed spatial variations, and both their size and density were affected by the ferrite-austenite phase boundary and presence of M23C6 carbides. Under 300 °C irradiation, in situ TEM observation showed G-phase precipitates were relatively unchanged in the vicinity of the phase boundary M23C6 carbides, while the density of G-phase precipitates increased with increasing dose within the ferrite matrix. Coarsening of G-phase precipitates was observed in the vicinity of phase boundary M23C6 carbides at 350 °C and 400 °C.

Influence of Solution Treatment Duration on Microstructural Features of an Industrial Forged UNS S32750/1.4410/F53 Super Duplex Stainless Steel (SDSS) Alloy

NASA Astrophysics Data System (ADS)

Cojocaru, Vasile Dănuţ; Răducanu, Doina; Angelescu, Mariana Lucia; Vintilă, Adrian Nicolae; Şerban, Nicolae; Dan, Ioan; Cojocaru, Elisabeta Mirela; Cinca, Ion

2017-08-01

The microstructural changes induced by solution treatment of an industrial forged F53 Super Duplex Stainless Steel alloy were studied, in order to emphasize how component phases are influenced by heat treatment temperature and duration. The solution treatment was done at a temperature of 1100°C, with variable holding times: 0.6 ks (10 min), 3.6 ks (60 min) and 10.8 ks (180 min). Scanning electron microscopy-electron backscattered diffraction was used as main characterization technique, to obtain and analyse data referring to microstructural features, such as: nature and morphology of constituent phases, average grain-size and grain misorientation. It was shown that in all studied cases the microstructure consisted of a mixture of about 45% δ-Fe (ferrite) and 55% γ-Fe (austenite). Besides δ-Fe and γ-Fe phases, other phases were also identified, such as τ-phase (chromium-iron carbide), σ-phase (chromium-iron) and δ-(Cr-Fe) (ferrite).

High Mn austenitic stainless steel

DOEpatents

Yamamoto, Yukinori [Oak Ridge, TN; Santella, Michael L [Knoxville, TN; Brady, Michael P [Oak Ridge, TN; Maziasz, Philip J [Oak Ridge, TN; Liu, Chain-tsuan [Knoxville, TN

2010-07-13

An austenitic stainless steel alloy includes, in weight percent: >4 to 15 Mn; 8 to 15 Ni; 14 to 16 Cr; 2.4 to 3 Al; 0.4 to 1 total of at least one of Nb and Ta; 0.05 to 0.2 C; 0.01 to 0.02 B; no more than 0.3 of combined Ti+V; up to 3 Mo; up to 3 Co; up to 1W; up to 3 Cu; up to 1 Si; up to 0.05 P; up to 1 total of at least one of Y, La, Ce, Hf, and Zr; less than 0.05 N; and base Fe, wherein the weight percent Fe is greater than the weight percent Ni, and wherein the alloy forms an external continuous scale including alumina, nanometer scale sized particles distributed throughout the microstructure, the particles including at least one of NbC and TaC, and a stable essentially single phase FCC austenitic matrix microstructure that is essentially delta-ferrite-free and essentially BCC-phase-free.

Effects of Cryogenic Treatment on the Strength Properties of Heat Resistant Stainless Steel (07X16H6)

NASA Astrophysics Data System (ADS)

Nadig, D. S.; Bhat, M. R.; Pavan, V. K.; Mahishi, Chandan

2017-09-01

Cryogenic treatment on metals is a well known technology where the materials are exposed to cryogenic temperature for prolonged time duration. The process involves three stages viz. slow cooling, holding at cryogenic temperature and warming to room temperature. During this process, hard and micro sized carbide particles are released within the steel material. In addition, soft and unconverted austenite of steel changes to strong martensite structure. These combined effects increase the strength and hardness of the cryotreated steel. In this experimental study, the effects of cryogenic treatment, austenitising and tempering on the mechanical properties of stainless steel (07X16H6) have been carried. After determining the strength properties of the original material, the specimens were cryotreated at 98K for 24 hours in a specially developed cryotreatment system. The effects of austenitising prior to cryogenic treatment and tempering post cryotreatment on the mechanical properties of steel samples have been experimentally determined and analysed.

Chairside CAD/CAM materials. Part 2: Flexural strength testing.

PubMed

Wendler, Michael; Belli, Renan; Petschelt, Anselm; Mevec, Daniel; Harrer, Walter; Lube, Tanja; Danzer, Robert; Lohbauer, Ulrich

2017-01-01

Strength is one of the preferred parameters used in dentistry for determining clinical indication of dental restoratives. However, small dimensions of CAD/CAM blocks limit reliable measurements with standardized uniaxial bending tests. The objective of this study was to introduce the ball-on-three-ball (B3B) biaxial strength test for dental for small CAD/CAM block in the context of the size effect on strength predicted by the Weibull theory. Eight representative chairside CAD/CAM materials ranging from polycrystalline zirconia (e.max ZirCAD, Ivoclar-Vivadent), reinforced glasses (Vitablocs Mark II, VITA; Empress CAD, Ivoclar-Vivadent) and glass-ceramics (e.max CAD, Ivoclar-Vivadent; Suprinity, VITA; Celtra Duo, Dentsply) to hybrid materials (Enamic, VITA; Lava Ultimate, 3M ESPE) have been selected. Specimens were prepared with highly polished surfaces in rectangular plate (12×12×1.2mm 3 ) or round disc (Ø=12mm, thickness=1.2mm) geometries. Specimens were tested using the B3B assembly and the biaxial strength was determined using calculations derived from finite element analyses of the respective stress fields. Size effects on strength were determined based on results from 4-point-bending specimens. A good agreement was found between the biaxial strength results for the different geometries (plates vs. discs) using the B3B test. Strength values ranged from 110.9MPa (Vitablocs Mark II) to 1303.21MPa (e.max ZirCAD). The strength dependency on specimen size was demonstrated through the calculated effective volume/surface. The B3B test has shown to be a reliable and simple method for determining the biaxial strength restorative materials supplied as small CAD/CAM blocks. A flexible solution was made available for the B3B test in the rectangular plate geometry. Copyright © 2016 The Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Fluid-acoustic interactions in a low area ratio supersonic jet ejector

NASA Technical Reports Server (NTRS)

Krothapalli, Anjaneyulu; Ross, Christopher; Yamomoto, K.; Joshi, M. C.

1994-01-01

An experimental investigation carried out to determine aerodynamic and acoustic characteristics of a low area ratio rectangular jet ejector is reported. A supersonic primary jet issuing from a rectangular convergent-divergent nozzle of aspect ratio 4, into a rectangular duct of area ratio 3, was used. Improved performance was found when the ejector screech tone is most intense and appears to match the most unstable Strouhal number of the free rectangular jet. When the primary jet was operating at over and ideally expanded conditions, significant noise reduction was obtained with the ejector as compared to a corresponding free jet. Application of particle image velocimetry to high speed ejector flows was demonstrated through the measurement of instantaneous two dimensional velocity fields.

Influence of High Pulsed and Continuous Magnetic Fields on the Corrosion and Microstructure of Metallic Conductors

DTIC Science & Technology

2014-03-31

stainless steel , 416 stainless steel , 1018 steel , and 8620 steel as these offer structural integrity as well as both magnetic and...corrosion rate of untreated materials such as 304 stainless steel , 416 stainless steel , 1018 steel , 8620 steel . It is believed that the magnetic field...at characterizing the impact of a magnetic field on the corrosion behavior of the selected alloys, namely, 304 austenitic stainless steel

Boride Formation Induced by pcBN Tool Wear in Friction-Stir-Welded Stainless Steels

NASA Astrophysics Data System (ADS)

Park, Seung Hwan C.; Sato, Yutaka S.; Kokawa, Hiroyuki; Okamoto, Kazutaka; Hirano, Satoshi; Inagaki, Masahisa

2009-03-01

The wear of polycrystalline cubic boron nitride (pcBN) tool and its effect on second phase formation were investigated in stainless steel friction-stir (FS) welds. The nitrogen content and the flow stress were analyzed in these welds to examine pcBN tool wear. The nitrogen content in stir zone (SZ) was found to be higher in the austenitic stainless steel FS welds than in the ferritic and duplex stainless steel welds. The flow stress of austenitic stainless steels was almost 1.5 times larger than that of ferritic and duplex stainless steels. These results suggest that the higher flow stress causes the severe tool wear in austenitic stainless steels, which results in greater nitrogen pickup in austenitic stainless steel FS welds. From the microstructural observation, a possibility was suggested that Cr-rich borides with a crystallographic structure of Cr2B and Cr5B3 formed through the reaction between the increased boron and nitrogen and the matrix during FS welding (FSW).

Fatigue Crack Growth Behavior of Gas Metal Arc Welded AISI 409 Grade Ferritic Stainless Steel Joints

NASA Astrophysics Data System (ADS)

Lakshminarayanan, A. K.; Shanmugam, K.; Balasubramanian, V.

2009-10-01

The effect of filler metals such as austenitic stainless steel, ferritic stainless steel, and duplex stainless steel on fatigue crack growth behavior of the gas metal arc welded ferritic stainless steel joints was investigated. Rolled plates of 4 mm thickness were used as the base material for preparing single ‘V’ butt welded joints. Center cracked tensile specimens were prepared to evaluate fatigue crack growth behavior. Servo hydraulic controlled fatigue testing machine with a capacity of 100 kN was used to evaluate the fatigue crack growth behavior of the welded joints. From this investigation, it was found that the joints fabricated by duplex stainless steel filler metal showed superior fatigue crack growth resistance compared to the joints fabricated by austenitic and ferritic stainless steel filler metals. Higher yield strength and relatively higher toughness may be the reasons for superior fatigue performance of the joints fabricated by duplex stainless steel filler metal.

laboratory studies on the uptake of organic compounds by ice crystals

NASA Astrophysics Data System (ADS)

Fries, E.; Jaeschke, W.

2003-04-01

Anthropogenic aerosols produced from biomass burning are known to increase the number of cloud condensation nuclei in the atmosphere at most latitudes. This reduces cloud droplet size, which prevents raindrop formation at shallower levels in the atmosphere. Vertical convection processes force particles and water vapor to rise up to the upper troposphere. At lower temperatures, ice crystals are formed via heterogeneous freezing of supercooled droplets containing particles known as ice nuclei (IN) and/or via condensation of supercooled water onto IN directly from the vapor, followed by freezing. Ice crystals grow by vapor deposition, by collision of supercooled drops with ice particles and by collision of ice crystals. The grown ice crystals melt on their way down and turn into rain. Most of the precipitation falling to the surface at midlatitudes originates as ice. The adsorption of organic gases emitted from fossil fuel combustion like BTEX may alter particle growth and sublimation rates in the atmosphere. This may also change precipitation rates, which impact the climate world-wide. Considering importance of ice in atmospheric science, laboratory studies are carried out to quantify organic vapor adsorption onto ice. At temperatures between 0 and -40^oC, organic gases at ppb gas levels are allowed to adsorb to the surface of ice crystals with surface properties similar to atmospheric ice. For the experiments, a vertical ice chamber (stainless-steel) with 10 different screen inserts (stainless-steel) was constructed. The chamber is 39 cm in length and 10,5 cm in diameter. The size of the stainless-steel mesh of the screens was chosen by the size of the ice crystals and is 0.14 cm. The ice chamber is located inside a 2x2 m walk-in cold chamber. Prior to the addition of the organic gases, the precleaned carrier gas of synthetic air is humidified to ice saturation in the walk-in cold chamber by passing the carrier stream through a 10 m long and 5 cm in diameter aluminum pipe. Resulting super cooled droplets are removed by stainless-steel-wool. The carrier gas is mixed outside the ice chamber in various proportions with a defined gas mixture of 60 different organic compounds. This mixture is allowed to flow through the ice chamber at defined pressures and temperatures. The concentrations of the compounds in the gas phase are determined at the inlet and the outlet of the ice chamber by a mobile GC (AirmoVoc1020). Additionally, the amount of adsorbed compounds is determined by a very sensitive method based on solid-phase-micro-extraction (SPME) followed by GC/FID. The resulting sorption coefficients for different gas concentrations are plotted vs the reciprocal of the absolute temperature for all substances. First results dealing with the adsorption properties of the investigated organic compounds.

Hot Corrosion Behavior of Stainless Steel with Al-Si/Al-Si-Cr Coating

NASA Astrophysics Data System (ADS)

Fu, Guangyan; Wu, Yongzhao; Liu, Qun; Li, Rongguang; Su, Yong

2017-03-01

The 1Cr18Ni9Ti stainless steel with Al-Si/Al-Si-Cr coatings is prepared by slurry process and vacuum diffusion, and the hot corrosion behavior of the stainless steel with/without the coatings is studied under the condition of Na2SO4 film at 950 °C in air. Results show that the corrosion kinetics of stainless steel, the stainless steel with Al-Si coating and the stainless steel with Al-Si-Cr coating follow parabolic laws in several segments. After 24 h corrosion, the sequence of the mass gain for the three alloys is the stainless steel with Al-Si-Cr coating < the stainless steel with Al-Si coating < the stainless steel without any coating. The corrosion products of the three alloys are layered. Thereinto, the corrosion products of stainless steel without coating are divided into two layers, where the outside layer contains a composite of Fe2O3 and FeO, and the inner layer is Cr2O3. The corrosion products of the stainless steel with Al-Si coating are also divided into two layers, of which the outside layer mainly consists of Cr2O3, and the inner layer is mainly SiO2. The corrosion film of the stainless steel with Al-Si-Cr coating is thin and dense, which combines well with substrate. Thereinto, the outside layer is mainly Cr2O3, and the inside layer is Al2O3. In the matrix of all of the three alloys, there exist small amount of sulfides. Continuous and protective films of Cr2O3, SiO2 and Al2O3 form on the surface of the stainless steel with Al-Si and Al-Si-Cr coatings, which prevent further oxidation or sulfide corrosion of matrix metals, and this is the main reason for the much smaller mass gain of the two alloys than that of the stainless steel without any coatings in the 24 h hot corrosion process.

Preformed posterior stainless steel crowns: an update.

PubMed

Croll, T P

1999-02-01

For almost 50 years, dentists have used stainless steel crowns for primary and permanent posterior teeth. No other type of restoration offers the convenience, low cost, durability, and reliability of such crowns when interim full-coronal coverage is required. Preformed stainless steel crowns have improved over the years. Better luting cements have been developed and different methods of crown manipulation have evolved. This article reviews stainless steel crown procedures for primary and permanent posterior teeth. Step-by-step placement of a primary molar stainless steel crown is documented and permanent molar stainless steel crown restoration is described. A method for repairing a worn-through crown also is reviewed.

Manufacturing Methods for the Production of Field Effect Electron Emitters from Oxide-Metal Composites.

DTIC Science & Technology

1977-12-01

Internal Zone Melting, Oxide-Metal Eutectic Structures ABSTRACT (Continue X reverae elde II neceaetrry end Identity by block nwbor* -^>This report...To- Uranium (0/U) Ratio B. Storage of "As-Received" Powders C. Moisture Content D. Oxidation Properties E. Sintering Properties F. Particle Size... Nickel - Vanadium 3.3 Nickel -Al203 3.4 Nickel -Tungsten 3.5 Copper-410 Stainless Steel C. Etching 1. Chemical Etching 2. Thermal Annealing 3. Ion

Growth of CH3NH3PbI3 Perovskite on Stainless Steel Substrate Layered by ZnO Nanoparticles Using One-Step Spin Coating Route

NASA Astrophysics Data System (ADS)

Fuad, A.; Fibriyanti, A. A.; Mufti, N.; Taufiq, A.; Maryam, S.; Hidayat, N.

2018-04-01

In this work, we report the preparation of CH3NH3PbI3 perovskite using one-step spin coating route for solar cell application. CH3NH3I• PbI2•DMF•DMSO complexes were coated on stainless steel as a subtrate layered by ZnO nanoparticles as an electron transport layer. To obtain samples with a special performance, we annealed the samples at a temperature of 100, 120, and 140°C for 10 minutes. The samples were then characterized by means of XRD, SEM/EDX, and Spectroscopic Ellipsometry. The analysis of XRD data presented that the CH3NH3PbI3 perovskites were successfully prepared and crystallized in tetragonal structure confirming from crystalline planes (110) and (220). Meanwhile, the particle size of the samples prepared at a temperature of 100, 120, and 140°C presented 42.96, 54.73, and 55.19 nm, respectively with coincide with the SEM images. The results indicated that the increase in temperature during synthesis influenced the particle growth. Furthermore, the characterization using Spectroscopic Ellipsometry exhibited that the CH3NH3PbI3 successfully layered on the substrate sizing nano metric scale that open high opportunity to be applied to solar cells with high performance.