Sample records for small core diameter

  1. High Sensitivity Refractometer Based on Reflective Smf-Small Diameter No Core Fiber Structure.

    PubMed

    Zhou, Guorui; Wu, Qiang; Kumar, Rahul; Ng, Wai Pang; Liu, Hao; Niu, Longfei; Lalam, Nageswara; Yuan, Xiaodong; Semenova, Yuliya; Farrell, Gerald; Yuan, Jinhui; Yu, Chongxiu; Zeng, Jie; Tian, Gui Yun; Fu, Yong Qing

    2017-06-16

    A high sensitivity refractive index sensor based on a single mode-small diameter no core fiber structure is proposed. In this structure, a small diameter no core fiber (SDNCF) used as a sensor probe, was fusion spliced to the end face of a traditional single mode fiber (SMF) and the end face of the SDNCF was coated with a thin film of gold to provide reflective light. The influence of SDNCF diameter and length on the refractive index sensitivity of the sensor has been investigated by both simulations and experiments, where results show that the diameter of SDNCF has significant influence. However, SDNCF length has limited influence on the sensitivity. Experimental results show that a sensitivity of 327 nm/RIU (refractive index unit) has been achieved for refractive indices ranging from 1.33 to 1.38, which agrees well with the simulated results with a sensitivity of 349.5 nm/RIU at refractive indices ranging from 1.33 to 1.38.

  2. Management of the high-order mode content in large (40 microm) core photonic bandgap Bragg fiber laser.

    PubMed

    Gaponov, D A; Février, S; Devautour, M; Roy, P; Likhachev, M E; Aleshkina, S S; Salganskii, M Y; Yashkov, M V; Guryanov, A N

    2010-07-01

    Very large-mode-area Yb(3+)-doped single-mode photonic bandgap (PBG) Bragg fiber oscillators are considered. The transverse hole-burning effect is numerically modeled, which helps properly design the PBG cladding and the Yb(3+)-doped region for the high-order mode content to be carefully controlled. A ratio of the Yb(3+)-doped region diameter to the overall core diameter of 40% allows for single-mode emission, even for small spool diameters of 15 cm. Such a fiber was manufactured and subsequently used as the core element of a cw oscillator. Very good beam quality parameter M(2)=1.12 and slope efficiency of 80% were measured. Insensitivity to bending, exemplified by the absence of temporal drift of the beam, was demonstrated for curvature diameter as small as 15 cm.

  3. Evaluation of Contemporary Holmium Laser Fibers for Performance Characteristics.

    PubMed

    Lusch, Achim; Heidari, Emon; Okhunov, Zhamshid; Osann, Kathryn; Landman, Jaime

    2016-05-01

    Several holmium:YAG laser fibers for urologic applications are currently commercially available. We compared contemporary holmium laser fibers with different core sizes for performance characteristics, including energy transmission, fiber failure, fiber flexibility, and core diameter. Single-use fibers from Cook, Boston Scientific, and Storz were tested in small (200 and 272/273 μm), medium (365 μm), and large (550 and 940/1000 μm) core sizes. Fibers were tested in straight and deflected configurations. All fibers were evaluated for flexibility, true fiber diameter, energy transmission, and fiber failure. For energy transmission, fibers were tested at a pulse energy of 1 J and a frequency of 10 Hz for 30 seconds. All tests were performed on a 30 W holmium laser. For the small core fibers, Storz, Cook OptiLite, and Smart Sync had the smallest core diameter (p < 0.005). In the large core group, Cook OptiLite and Boston Scientific AccuMax showed the smallest diameter. Among the small core fibers, Storz and Cook Smart Sync showed a significant higher deflection, whereas in the 550 μm group, Boston Scientific AccuMax and Cook Smart Sync were the most flexible fibers. In the large and medium core groups, Boston Scientific AccuMax showed superior energy transmission (p = 0.007 and p = 0.001, respectively), whereas in the small core group, there was no significant difference between the fibers, except for 272/3 μm (Storz was inferior compared with the competitors [p < 0.0005]). For fiber failure, Storz, Cook OptiLite, and BS AccuTrac completed all testing without failing (200 μm, bending radius <0.5 cm). In the 365 μm group, Cook OptiLite showed superior results, whereas in the large core group, Boston Scientific AccuMax was superior. Performance characteristics differ significantly between different laser fiber diameters and manufacturers, and fiber choice should depend on specific surgical requirements. There is a trend for less fiber fracture at long pulse, high energy, and low frequency, but this finding will require further investigation.

  4. Multiple Small Diameter Drillings Increase Femoral Neck Stability Compared with Single Large Diameter Femoral Head Core Decompression Technique for Avascular Necrosis of the Femoral Head.

    PubMed

    Brown, Philip J; Mannava, Sandeep; Seyler, Thorsten M; Plate, Johannes F; Van Sikes, Charles; Stitzel, Joel D; Lang, Jason E

    2016-10-26

    Femoral head core decompression is an efficacious joint-preserving procedure for treatment of early stage avascular necrosis. However, postoperative fractures have been described which may be related to the decompression technique used. Femoral head decompressions were performed on 12 matched human cadaveric femora comparing large 8mm single bore versus multiple 3mm small drilling techniques. Ultimate failure strength of the femora was tested using a servo-hydraulic material testing system. Ultimate load to failure was compared between the different decompression techniques using two paired ANCOVA linear regression models. Prior to biomechanical testing and after the intervention, volumetric bone mineral density was determined using quantitative computed tomography to account for variation between cadaveric samples and to assess the amount of bone disruption by the core decompression. Core decompression, using the small diameter bore and multiple drilling technique, withstood significantly greater load prior to failure compared with the single large bore technique after adjustment for bone mineral density (p< 0.05). The 8mm single bore technique removed a significantly larger volume of bone compared to the 3mm multiple drilling technique (p< 0.001). However, total fracture energy was similar between the two core decompression techniques. When considering core decompression for the treatment of early stage avascular necrosis, the multiple small bore technique removed less bone volume, thereby potentially leading to higher load to failure.

  5. 33 CFR 148.405 - What are the procedures for notifying the Commandant (CG-5) of proposed site evaluation and pre...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... proposed location and purpose of the activities, including: (1) Gravity and magneto-metric measurements; (2...) Sediment sampling of a limited nature using either core or grab samplers, and the specified diameter and...) Hydrographic and oceanographic measurements, including the setting of instruments; and (7) Small diameter core...

  6. 33 CFR 148.405 - What are the procedures for notifying the Commandant (CG-5) of proposed site evaluation and pre...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... proposed location and purpose of the activities, including: (1) Gravity and magneto-metric measurements; (2...) Sediment sampling of a limited nature using either core or grab samplers, and the specified diameter and...) Hydrographic and oceanographic measurements, including the setting of instruments; and (7) Small diameter core...

  7. Management of non-traumatic avascular necrosis of the femoral head-a comparative analysis of the outcome of multiple small diameter drilling and core decompression with fibular grafting.

    PubMed

    Mohanty, S P; Singh, K A; Kundangar, R; Shankar, V

    2017-04-01

    The purpose of this study was to compare the clinical and radiological outcomes of multiple small diameter drilling and core decompression with fibular strut grafting in the management of non-traumatic avascular necrosis (AVN) of the femoral head. Outcomes of patients with AVN treated by multiple small diameter drilling (group 1) were compared retrospectively with patients treated by core decompression and fibular grafting (group 2). Harris hip score (HHS) was used to assess the clinical status pre- and postoperatively. Modified Ficat and Arlet classification was used to assess the radiological stage pre- and postoperatively. Forty-six patients (68 hips) were included in this study. Group 1 consisted of 33 hips, and group 2 consisted of 35 hips. In stages I and IIB, there was no statistically significant difference in the final HHS between the two groups. However, in stages IIA and III, hips in group 2 had a better final HHS (P < 0.05). In terms of radiographic progression, there was no statistical difference between hips in stages I, IIA and stage IIB. However, in stage III, hips belonging to group 2 had better results (P < 0.05). Kaplan-Meier survivorship analysis showed better outcome in group 2 in stage III (P < 0.05). Hips with AVN in the precollapse stage can be salvaged by core decompression with or without fibular grafting. Multiple small diameter drilling is relatively simple and carries less morbidity and hence preferred in stages I and II. However, in stage III disease, core decompression with fibular strut grafting gives better results.

  8. Dowel-nut connection in Douglas-fir peeler cores

    Treesearch

    Ronald W. Wolfe; John R. King; Agron Gjinolli

    As part of an effort to encourage more efficient use of small-diameter timber, the Forest Products Laboratory cooperated with Geiger Engineers in a study of the structural properties of Douglas-fir peeler cores and the efficacy of a bdowel-nutc connection detail for application in the design of a space frame roof system. A 44.5-mm- (1.75-in.-) diameter dowel-nut...

  9. High power 938 nanometer fiber laser and amplifier

    DOEpatents

    Dawson, Jay W [Livermore, CA; Liao, Zhi Ming [Pleasanton, CA; Beach, Raymond J [Livermore, CA; Drobshoff, Alexander D [Livermore, CA; Payne, Stephen A [Castro Valley, CA; Pennington, Deanna M [Livermore, CA; Hackenberg, Wolfgang [Munich, DE; Calia, Domenico Bonaccini [Garching, DE; Taylor, Luke [Montauban de Bretagne, FR

    2006-05-02

    An optical fiber amplifier includes a length of silica optical fiber having a core doped with neodymium, a first cladding and a second cladding each with succeeding lower refractive indices, where the first cladding diameter is less than 10 times the diameter of the core. The doping concentration of the neodymium is chosen so that the small signal absorption for 816 nm light traveling within the core is less than 15 dB/m above the other fiber losses. The amplifier is optically pumped with one laser into the fiber core and with another laser into the first cladding.

  10. Stress-induced phase sensitivity of small diameter polarization maintaining solid-core photonic crystal fibre

    NASA Astrophysics Data System (ADS)

    Zhang, Zhihao; Zhang, Chunxi; Xu, Xiaobin

    2017-09-01

    Small diameter (cladding and coating diameter of 100 and 135 μm) polarization maintaining photonic crystal fibres (SDPM-PCFs) possess many unique properties and are extremely suitable for applications in fibre optic gyroscopes. In this study, we have investigated and measured the stress characteristics of an SDPM-PCF using the finite-element method and a Mach-Zehnder interferometer, respectively. Our results reveal a radial and axial sensitivity of 0.315 ppm/N/m and 25.2 ppm per 1 × 105 N/m2, respectively, for the SDPM-PCF. These values are 40% smaller than the corresponding parameters of conventional small diameter (cladding and coating diameter of 80 and 135 μm) panda fibres.

  11. Extremely small-core photonic crystal fiber fusion splicing with a single-mode fiber

    NASA Astrophysics Data System (ADS)

    Tiburcio, Bruno D.; Fernandes, Gil M.; Pinto, Armando N.

    2013-11-01

    We present a low-loss fusion splicing of a non-linear photonic-crystal fiber (NL-PCF) with a single-mode fiber (SMF), helped by an intermediate fiber, using a electric-arc splicer. We also analysed the splice loss between SMF and intermediate fiber, as a function of the electrical discharge duration, to achieve a low-loss transition between SMF and intermediate fiber, through a thermally expanded core splice (TEC). The NL-PCF has a external cladding diameter of 105 μm, a core diameter of 1.7 μm and mode-field diameter (MFD) of 1.5 μm. We also performed mechanical strength tests to verify the robustness of the splice joints obtained.

  12. Space-frame connection for small-diameter round timber

    Treesearch

    Ronald W. Wolfe; Agron E. Gjinolli; John R. King

    2000-01-01

    To promote more efficient use of small-diameter timber, research efforts are being focused on the development and evaluation of connection methods that can be easily applied to non-standard round wood profiles. This report summarizes an evaluation of a bdowel-nut connectionc as an option for the use of Douglas-fir peeler cores in three-dimensional truss or bspace-...

  13. Preliminary Engineering Study of Long-Lead Time Equipment Required for Large Lightweight Mirror Manufacture

    DTIC Science & Technology

    1981-06-01

    numnber) Annealing Fusion Sealed Mirrors ULED Mirrors Boule Large Lightweight Mirror Core Low Expansion Glass Coremaker Mirror Blanks Forming Furnace...Experiments 34 4 10.6 Grinder Procurement 35 J 1 I GLOSSARY Alpha - Coef. of thermal expansion. Boule - The disc of glass formed in the furnace. Cell...turning over of large plates, cores or mirrors. Flowout - Method used to produce large diameter plates from small diameter boules. Glass - Used in the

  14. Small core fiber coupled 60-W laser diode

    NASA Astrophysics Data System (ADS)

    Fernie, Douglas P.; Mannonen, Ilkka; Raven, Anthony L.

    1995-05-01

    Semiconductor laser diodes are compact, efficient and reliable sources of laser light and 25 W fiber coupled systems developed by Diomed have been in clinical use for over three years. For certain applications, particularly in the treatment of benign prostatic hyperplasia and flexible endoscopy, higher powers are desirable. In these applications the use of flexible optical fibers of no more than 600 micrometers core diameter is essential for compatibility with most commercial delivery fibers and instrumentation. A high power 60 W diode laser system for driving these small core fibers has been developed. The design requirements for medical applications are analyzed and system performance and results of use in gastroenterology and urology with small core fibers will be presented.

  15. Thulium fiber laser ablation of kidney stones using a 50-μm-core silica optical fiber

    NASA Astrophysics Data System (ADS)

    Blackmon, Richard L.; Hutchens, Thomas C.; Hardy, Luke A.; Wilson, Christopher R.; Irby, Pierce B.; Fried, Nathaniel M.

    2015-01-01

    Our laboratory is currently studying the experimental thulium fiber laser (TFL) as a potential alternative laser lithotripter to the gold standard, clinical Holmium:YAG laser. We have previously demonstrated the efficient coupling of TFL energy into fibers as small as 100-μm-core-diameter without damage to the proximal end. Although smaller fibers have a greater tendency to degrade at the distal tip during lithotripsy, fiber diameters (≤200 μm) have been shown to increase the saline irrigation rates through the working channel of a flexible ureteroscope, to maximize the ureteroscope deflection, and to reduce the stone retropulsion during laser lithotripsy. In this study, a 50-μm-core-diameter, 85-μm-outer-diameter, low-OH silica fiber is characterized for TFL ablation of human calcium oxalate monohydrate urinary stones, ex vivo. The 50-μm-core fiber consumes approximately 30 times less cross-sectional area inside the single working channel of a ureteroscope than the standard 270-μm-core fiber currently used in the clinic. The ureteroscope working channel flow rate, including the 50-μm fiber, decreased by only 10% with no impairment of ureteroscope deflection. The fiber delivered up to 15.4±5.9 W under extreme bending (5-mm-radius) conditions. The stone ablation rate measured 70±22 μg/s for 35-mJ-pulse-energy, 500-μs-pulse-duration, and 50-Hz-pulse-rate. Stone retropulsion and fiber burnback averaged 201±336 and 3000±2600 μm, respectively, after 2 min. With further development, thulium fiber laser lithotripsy using ultra-small, 50-μm-core fibers may introduce new integration and miniaturization possibilities and potentially provide an alternative to conventional Holmium:YAG laser lithotripsy using larger fibers.

  16. A Composite Depth Scale for Sediments from Crevice Lake, Montana

    USGS Publications Warehouse

    Rosenbaum, J.G.; Skipp, G.; Honke, J.; Chapman, C.

    2010-01-01

    As part of a study to derive records of past environmental change from lake sediments in the western United States, a set of cores was collected from Crevice Lake, Montana, in late February and early March 2001. Crevice Lake (latitude 45.000N, longitude 110.578W, elevation 1,713 meters) lies adjacent to the Yellowstone River at the north edge of Yellowstone National Park. The lake is more than 31 meters deep and has a surface area of 7.76 hectares. The combination of small surface area and significant depth promote anoxic bottom-water conditions that preserve annual laminations (varves) in the sediment. Three types of cores were collected through the ice. The uppermost sediments were obtained in freeze cores that preserved the sediment water interface. Two sites were cored with a 5-centimeter diameter corer. Five cores were taken with a 2-meter-long percussion piston corer. The percussion core uses a plastic core liner with an inside diameter of 9 centimeters. Coring was done at two sites. Because of the relatively large diameter of the percussion cores, samples from these cores were used for a variety of analyses including pollen, charcoal, diatoms, stable isotopes, organic and inorganic carbon, elemental analyses, and magnetic properties.

  17. Do modern techniques improve core decompression outcomes for hip osteonecrosis?

    PubMed

    Marker, David R; Seyler, Thorsten M; Ulrich, Slif D; Srivastava, Siddharth; Mont, Michael A

    2008-05-01

    Core decompression procedures have been used in osteonecrosis of the femoral head to attempt to delay the joint destruction that may necessitate hip arthroplasty. The efficacy of core decompressions has been variable with many variations of technique described. To determine whether the efficacy of this procedure has improved during the last 15 years using modern techniques, we compared recently reported radiographic and clinical success rates to results of surgeries performed before 1992. Additionally, we evaluated the outcomes of our cohort of 52 patients (79 hips) who were treated with multiple small-diameter drillings. There was a decrease in the proportion of patients undergoing additional surgeries and an increase in radiographic success when comparing pre-1992 results to patients treated in the last 15 years. However, there were fewer Stage III hips in the more recent reports, suggesting that patient selection was an important reason for this improvement. The results of the small-diameter drilling cohort were similar to other recent reports. Patients who had small lesions and were Ficat Stage I had the best results with 79% showing no radiographic progression. Our study confirms core decompression is a safe and effective procedure for treating early stage femoral head osteonecrosis.

  18. Influence of fibre design and curvature on crosstalk in multi-core fibre

    NASA Astrophysics Data System (ADS)

    Egorova, O. N.; Astapovich, M. S.; Melnikov, L. A.; Salganskii, M. Yu; Mishkin, V. P.; Nishchev, K. N.; Semjonov, S. L.; Dianov, E. M.

    2016-03-01

    We have studied the influence of cross-sectional structure and bends on optical cross-talk in a multicore fibre. A reduced refractive index layer produced between the cores of such fibre with a small centre-to-centre spacing between neighbouring cores (27 μm) reduces optical cross-talk by 20 dB. The cross-talk level achieved, 30 dB per kilometre of the length of the multicore fibre, is acceptable for a number of applications where relatively small lengths of fibre are needed. Moreover, a significant decrease in optical cross-talk has been ensured by reducing the winding diameter of multicore fibres with identical cores.

  19. Highly non-linear solid core photonic crystal fiber with one nano hole

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Gangwar, Rahul Kumar, E-mail: rahul0889@gmail.com; Bhardwaj, Vanita, E-mail: bhardwajphy12@gmail.com; Singh, Vinod Kumar, E-mail: singh.vk.ap@ismdhanbad.co.in

    2015-08-28

    The numerical study of newly designed solid core photonic crystal fiber (SCPCF) having three hexagonal air hole rings in cladding region and one small nano hole at the center are presented. By using full vectorial finite element method (FV-FEM), we analyses the optical properties like effective area, nonlinearity and confinement loss of the proposed PCF. Results show that the change in core diameter controls the effective area, nonlinearity and confinement loss. A low effective area (3.34 µm{sup 2}), high nonlinearity (36.34 W{sup −1}km{sup −1}) and low confinement loss (0.00106 dB/km) are achieved at the communication wavelength 1.55 µm for themore » SCPCF having core air hole diameter 0.10 µm, cladding air holes diameter 1.00 µm and pitch 2.50 µm. This type of PCF is very useful in non-linear applications such as supercontinuum generation, four wave mixing, second harmonic generation etc.« less

  20. Tailoring sphere density for high pressure physical property measurements on liquids

    NASA Astrophysics Data System (ADS)

    Secco, R. A.; Tucker, R. F.; Balog, S. P.; Rutter, M. D.

    2001-04-01

    We present a new method of tailoring the density of a sphere for use as a probe in high pressure-temperature physical property experiments on liquids. The method consists of a composite sphere made of an inner, high density, metallic, spherical core and an exterior, low density, refractory, spherical shell or mantle. Micromechanical techniques are used to fabricate the composite sphere. We describe a relatively simple mechanical device that can grind hemispherical recesses as small as 200 μm in diameter in sapphire and as small as 500 μm in diameter in ruby hemispheres. Examples of composite spheres made with a Pt or WC core and Al2O3 shell used in metallic liquids pressurized to 16 GPa and 1900 K are shown.

  1. Influence of fibre design and curvature on crosstalk in multi-core fibre

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Egorova, O N; Astapovich, M S; Semjonov, S L

    2016-03-31

    We have studied the influence of cross-sectional structure and bends on optical cross-talk in a multicore fibre. A reduced refractive index layer produced between the cores of such fibre with a small centre-to-centre spacing between neighbouring cores (27 μm) reduces optical cross-talk by 20 dB. The cross-talk level achieved, 30 dB per kilometre of the length of the multicore fibre, is acceptable for a number of applications where relatively small lengths of fibre are needed. Moreover, a significant decrease in optical cross-talk has been ensured by reducing the winding diameter of multicore fibres with identical cores. (fiber optics)

  2. Diameter Growth in Even- and Uneven-Aged Northern Hardwoods in New Hampshire Under Partial Cutting

    Treesearch

    William B. Leak

    2004-01-01

    One important concern in the conversion of even-aged stands to an uneven aged condition through individual-tree or small-group cutting is the growth response throughout the diameter-class distribution, especially of the understoty trees Increment-core sampling of an older, uneven-aged northern hardwood stand in New Hampshire under management for about 50 years...

  3. Tapered polysilicon core fibers for nonlinear photonics.

    PubMed

    Suhailin, Fariza H; Shen, Li; Healy, Noel; Xiao, Limin; Jones, Maxwell; Hawkins, Thomas; Ballato, John; Gibson, Ursula J; Peacock, Anna C

    2016-04-01

    We propose and demonstrate a novel approach to obtaining small-core polysilicon waveguides from the silicon fiber platform. The fibers were fabricated via a conventional drawing tower method and, subsequently, tapered down to achieve silicon core diameters of ∼1  μm, the smallest optical cores for this class of fiber to date. Characterization of the material properties have shown that the taper process helps to improve the local crystallinity of the silicon core, resulting in a significant reduction in the material loss. By exploiting the combination of small cores and low losses, these tapered fibers have enabled the first observation of nonlinear transmission within a polycrystalline silicon waveguide of any type. As the fiber drawing method is highly scalable, it opens a route for the development of low-cost and flexible nonlinear silicon photonic systems.

  4. Optofluidic tuning of multimode interference fiber filters

    NASA Astrophysics Data System (ADS)

    Antonio-Lopez, J. E.; May-Arrioja, D. A.; LiKamWa, P.

    2009-05-01

    We report on the optofluidic tuning of MMI-based bandpass filters. It is well known that MMI devices exhibit their highest sensitivity when their diameter (D) is modified, since they have a D2 wavelength dependence. In order to increase the MMF diameter we use a special fiber, called No-Core fiber, which is basically a MMF with a diameter of 125 μm with air as the cover. Therefore, when this No-Core fiber is immersed in liquids with different refractive indexes, as a result of the Goes-Hänchen shift the effective width (fundamental mode width) of the No-Core fiber is increased, and thus the peak wavelength is tuned. A tunability of almost 40 nm in going from air (n=1.333) to ethylene glycol (n=1.434) was easily obtained, with a minimum change in peak transmission, contrast, and bandwidth. Moreover, since replacing the entire liquid can be difficult, the device was placed vertically and the liquid was covering the No-Core fiber in small steps. This provided similar amount of tuning as before, but a more controllable tuning mechanism.

  5. Impact of the Curve Diameter and Laser Settings on Laser Fiber Fracture.

    PubMed

    Haddad, Mattieu; Emiliani, Esteban; Rouchausse, Yann; Coste, Frederic; Doizi, Steeve; Berthe, Laurent; Butticé, Salvatore; Somani, Bhaskar; Traxer, Olivier

    2017-09-01

    To analyze the risk factors for laser fiber fractures when deflected to form a curve, including laser settings, size of the laser fiber, and the fiber bending diameter. Single-use 272 and 365 μm fibers (Rocamed ® , Monaco) were employed along with a holmium laser (Rocamed). Five different fiber curve diameters were tested: 9, 12, 15, 18, and 20 mm. Fragmentation and dusting settings were used at a theoretical power of 7.5 W. The laser was activated for 5 minutes and the principal judgment criterion was fiber fracture. Every test for each parameter, bending diameter, and fiber size combinations was repeated 10 times. With dusting settings, fibers broke more frequently at a curved diameter of 9 mm for both 272 and 365 μm fibers (p = 0.037 and 0.006, respectively). Using fragmentation settings, fibers broke more frequently at 12 mm for 272 μm and 15 mm for 365 μm (p = 0.007 and 0.033, respectively). Short pulse and high energy were significant risk factors for fiber fracture using the 365 μm fibers (p = 0.02), but not for the 272 μm fibers (p = 0.35). Frequency was not a risk factor for fiber rupture. Fiber diameters also seemed to be involved in the failure with a higher number of broken fibers for the 365 μm fibers, but this was not statistically significant when compared with the 272 μm fibers (p > 0.05). Small-core fibers are more resistant than large-core fibers as lower bending diameters (<9 mm) are required to break smaller fibers. In acute angles, the use of small-core fibers, at a low energy and long-pulse (dusting) setting, will reduce the risk of fiber rupture.

  6. Preliminary evaluation of steel-roller round baler for woody biomass baling

    Treesearch

    B. J. Stokes; D. L. Sirois; S. L. Woodfin

    1987-01-01

    A round hay baler with little modification was used to bale small-diameter, crushed trees. The trees had been crushed using a series of compression rollers. Bale cores had to be developed by hand before the baler became self-feeding. Windrowed material was packed off the ground by the baler system after a core had been developed.

  7. Wood density and anatomical properties in suppressed-growth trees : comparison of two methods

    Treesearch

    David W. Vahey; J. Y. Zhu; C. Tim Scott

    2007-01-01

    Interest in the commercial value of small-diameter timber has led to testing core samples with SilviScan to characterize density and transverse fiber dimensions. Data showed that latewood density and tracheid diameter in suppressed-growth material can vary spatially on a scale comparable to the 50-_m resolution of the instrument used in our testing. An optical imaging...

  8. The Auto-Gopher Deep Drill

    NASA Technical Reports Server (NTRS)

    Badescu, Mircea

    2014-01-01

    Subsurface penetration by coring, drilling or abrading is of great importance for a large number of space and earth applications. An Ultrasonic/Sonic Drill/Corer (USDC) has been in development at JPL's Nondestructive Evaluation and Advanced Actuators (NDEAA) lab as an adaptable tool for many of these applications. The USDC uses a novel drive mechanism to transform the high frequency ultrasonic or sonic vibrations of the tip of a horn into a lower frequency sonic hammering of a drill bit through an intermediate free-flying mass. The USDC device idea has been implemented at various scales from handheld drills to large diameter coring devices. A series of computer programs that model the function and performance of the USDC device were developed and were later integrated into an automated modeling package. The USDC has also evolved from a purely hammering drill to a rotary hammer drill as the design requirements increased form small diameter shallow drilling to large diameter deep coring. A synthesis of the Auto-Gopher development is presented in this paper.

  9. Characterization of core–shell MOF particles by depth profiling experiments using on-line single particle mass spectrometry

    DOE PAGES

    Cahill, J. F.; Fei, H.; Cohen, S. M.; ...

    2015-01-05

    Materials with core-shell structures have distinct properties that lend themselves to a variety of potential applications. Characterization of small particle core-shell materials presents a unique analytical challenge. Herein, single particles of solid-state materials with core-shell structures were measured using on-line aerosol time-of-flight mass spectrometry (ATOFMS). Laser 'depth profiling' experiments verified the core-shell nature of two known core-shell particle configurations (< 2 mu m diameter) that possessed inverted, complimentary core-shell compositions (ZrO2@SiO2 versus SiO2@ZrO2). The average peak area ratios of Si and Zr ions were calculated to definitively show their core-shell composition. These ratio curves acted as a calibrant for anmore » uncharacterized sample - a metal-organic framework (MOF) material surround by silica (UiO-66(Zr)@SiO2; UiO = University of Oslo). ATOFMS depth profiling was used to show that these particles did indeed exhibit a core-shell architecture. The results presented here show that ATOFMS can provide unique insights into core-shell solid-state materials with particle diameters between 0.2-3 mu m.« less

  10. Magnetization pinning in modulated nanowires: from topological protection to the "corkscrew" mechanism.

    PubMed

    Fernandez-Roldan, Jose Angel; Perez Del Real, Rafael; Bran, Cristina; Vazquez, Manuel; Chubykalo-Fesenko, Oksana

    2018-03-29

    Diameter-modulated nanowires offer an important paradigm to design the magnetization response of 3D magnetic nanostructures by engineering the domain wall pinning. With the aim to understand its nature and to control the process, we analyze the magnetization response in FeCo periodically modulated polycrystalline nanowires varying the minor segment diameter. Our modelling indicates a very complex behavior with a strong dependence on the disorder distribution and an important role of topologically non-trivial magnetization structures. We demonstrate that modulated nanowires with a small diameter difference are characterized by an increased coercive field in comparison to the straight ones, which is explained by a formation of topologically protected walls formed by two 3D skyrmions with opposite chiralities. For a large diameter difference we report the occurrence of a novel pinning type called here the "corkscrew": the magnetization of the large diameter segment forms a skyrmion tube with a core position in a helical modulation along the nanowire. This structure is pinned at the constriction and in order to penetrate the narrow segments the vortex/skyrmion core size should be reduced.

  11. PVDF core-free actuator for Braille displays: design, fabrication process, and testing

    NASA Astrophysics Data System (ADS)

    Levard, Thomas; Diglio, Paul J.; Lu, Sheng-Guo; Gorny, Lee J.; Rahn, Christopher D.; Zhang, Q. M.

    2011-04-01

    Refreshable Braille displays require many, small diameter actuators to move the pins. The electrostrictive P(VDF-TrFECFE) terpolymer can provide the high strain and actuation force under modest electric fields that are required of this application. In this paper, we develop core-free tubular actuators and integrate them into a 3 × 2 Braille cell. The films are solution cast, stretched to 6 μm thick, electroded, laminated into a bilayer, rolled into a 2 mm diameter tube, bonded, and provided with top and bottom contacts. Experimental testing of 17 actuators demonstrates significant strains (up to 4%). A novel Braille cell is designed and fabricated using six of these actuators.

  12. All fiber passively Q-switched laser

    DOEpatents

    Soh, Daniel B. S.; Bisson, Scott E

    2015-05-12

    Embodiments relate to an all fiber passively Q-switched laser. The laser includes a large core doped gain fiber having a first end. The large core doped gain fiber has a first core diameter. The laser includes a doped single mode fiber (saturable absorber) having a second core diameter that is smaller than the first core diameter. The laser includes a mode transformer positioned between a second end of the large core doped gain fiber and a first end of the single mode fiber. The mode transformer has a core diameter that transitions from the first core diameter to the second core diameter and filters out light modes not supported by the doped single mode fiber. The laser includes a laser cavity formed between a first reflector positioned adjacent the large core doped gain fiber and a second reflector positioned adjacent the doped single mode fiber.

  13. Energy Deposition and Condition of the Metal Core in Exploding Wire Experiments

    NASA Astrophysics Data System (ADS)

    Sarkisov, G. S.; Rosenthal, S. E.; Struve, K. W.; McDaniel, D. H.; Waisman, E. M.; Sasorov, P. V.

    2002-11-01

    Measurements of the Joule energy deposition into exploding wire and its relation with condition of the expanding wire core are presented. Wires of nine different metals with diameters of 10-30 microns, have been exploded by fast 150A/ns and slow 20A/ns pulses, in vacuum and in air. It has been shown by interferometry and light emission that expanding wire core has different conditions. The substances with small atomization enthalpy (Ag, Al, Cu, Au) demonstrate full vaporization of the wire core. The refractory metals (Ti, Pt, Mo, W) demonstrates that core consists from vapor and small and hot microparticles. In this case we observe "firework effect" when large radiation from the wire exceed the energy deposition time in a three order of magnitude. For non-refractory metals radiation dropping fast in 100 ns time scale due to effective adiabatic cooling. It is possible if main part of the metal core was vaporized. The interferometrical investigation of the refraction coefficient of expanding metal core is proof this conclusion. It has been shown that energy deposition before surface breakdown dependent strongly from current rate, surface coatings, environment, wire diameter and radial electric field. The regime of wire explosion in vacuum without shunting plasma shell has been realized for fast exploding mode. In this case we observe anomaly high energy deposition in to the wire core exceeding regular value in almost 20 times. The experimental results for Al wire have been compared with ALEGRA 2D MHD simulations. *Sandia is a multi-program laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the United States Department of Energy under Contract DE-AC04-94AL8500.

  14. Influence of item distribution pattern and abundance on efficiency of benthic core sampling

    USGS Publications Warehouse

    Behney, Adam C.; O'Shaughnessy, Ryan; Eichholz, Michael W.; Stafford, Joshua D.

    2014-01-01

    ore sampling is a commonly used method to estimate benthic item density, but little information exists about factors influencing the accuracy and time-efficiency of this method. We simulated core sampling in a Geographic Information System framework by generating points (benthic items) and polygons (core samplers) to assess how sample size (number of core samples), core sampler size (cm2), distribution of benthic items, and item density affected the bias and precision of estimates of density, the detection probability of items, and the time-costs. When items were distributed randomly versus clumped, bias decreased and precision increased with increasing sample size and increased slightly with increasing core sampler size. Bias and precision were only affected by benthic item density at very low values (500–1,000 items/m2). Detection probability (the probability of capturing ≥ 1 item in a core sample if it is available for sampling) was substantially greater when items were distributed randomly as opposed to clumped. Taking more small diameter core samples was always more time-efficient than taking fewer large diameter samples. We are unable to present a single, optimal sample size, but provide information for researchers and managers to derive optimal sample sizes dependent on their research goals and environmental conditions.

  15. More than threefold expansion of highly nonlinear photonic crystal fiber cores for low-loss fusion splicing.

    PubMed

    Chen, Z; Xiong, C; Xiao, L M; Wadsworth, W J; Birks, T A

    2009-07-15

    We have formed low-loss fusion splices from highly nonlinear (HNL) photonic crystal fibers (PCFs) with small cores and high air-filling fractions to fibers with much larger mode field diameters (MFDs). The PCF core was locally enlarged by the controlled collapse of holes around the core while keeping other holes open. The fiber was then cleaved at the enlarged core and spliced to the large MFD fiber with a conventional electric arc fusion splicer. Splice losses as low as 0.36 dB were achieved between a PCF and a standard single-mode fiber (SMF) with MFDs of 1.8 microm and 5.9 microm, respectively.

  16. Managing Geothermal Exploratory Drilling Risks Drilling Geothermal Exploration and Delineation Wells with Small-Footprint Highly Portable Diamond Core Drills

    NASA Astrophysics Data System (ADS)

    Tuttle, J.; Listi, R.; Combs, J.; Welch, V.; Reilly, S.

    2012-12-01

    Small hydraulic core rigs are highly portable (truck or scow-mounted), and have recently been used for geothermal exploration in areas such as Nevada, California, the Caribbean Islands, Central and South America and elsewhere. Drilling with slim diameter core rod below 7,000' is common, with continuous core recovery providing native-state geological information to aid in identifying the resource characteristics and boundaries; this is a highly cost-effective process. Benefits associated with this innovative exploration and delineation technology includes the following: Low initial Capital Equipment Cost and consumables costs Small Footprint, reducing location and road construction, and cleanup costs Supporting drill rod (10'/3meter) and tools are relatively low weight and easily shipped Speed of Mobilization and rig up Reduced requirements for support equipment (cranes, backhoes, personnel, etc) Small mud systems and cementing requirements Continuous, simplified coring capability Depth ratings comparable to that of large rotary rigs (up to ~10,000'+) Remote/small-location accessible (flown into remote areas or shipped in overseas containers) Can be scow or truck-mounted This technical presentation's primary goal is to share the technology of utilizing small, highly portable hydraulic coring rigs to provide exploratory drilling (and in some cases, production drilling) for geothermal projects. Significant cost and operational benefits are possible for the Geothermal Operator, especially for those who are pursuing projects in remote locations or countries, or in areas that are either inaccessible or in which a small footprint is required. John D. Tuttle Sinclair Well Products jtuttle@sinclairwp.com

  17. Effect of Mechanical Stresses in Rapidly Heated Fe73Cu1Nb3Si16B7 Ribbon Arising During the Ring Core Formation on Their Magnetic Properties

    NASA Astrophysics Data System (ADS)

    Nosenko, Anton; Mika, Taras; Semyrga, Olexandr; Nosenko, Viktor

    2017-04-01

    The influence of winding-induced mechanical stresses on the magnetic anisotropy and core loss in toroidal cores made of Fe73Cu1Nb3Si16B7 ribbon is studied. The ribbon for the cores was rapidly pre-heated under tensile stress up to 120 MPa. It was found that magnetic characteristics of the material (magnetic anisotropy energy and the core loss) can be controlled by varying the tensile stress during the preliminary rapid heating of the ribbon. It was shown that with reducing core diameter, the magnetic anisotropy energy and core loss significantly increase. However, relatively high winding-induced core loss in small cores can be significantly reduced by increasing tensile stresses applied to the ribbon during pre-heating.

  18. Effect of Mechanical Stresses in Rapidly Heated Fe73Cu1Nb3Si16B7 Ribbon Arising During the Ring Core Formation on Their Magnetic Properties.

    PubMed

    Nosenko, Anton; Mika, Taras; Semyrga, Olexandr; Nosenko, Viktor

    2017-12-01

    The influence of winding-induced mechanical stresses on the magnetic anisotropy and core loss in toroidal cores made of Fe 73 Cu 1 Nb 3 Si 16 B 7 ribbon is studied. The ribbon for the cores was rapidly pre-heated under tensile stress up to 120 MPa. It was found that magnetic characteristics of the material (magnetic anisotropy energy and the core loss) can be controlled by varying the tensile stress during the preliminary rapid heating of the ribbon. It was shown that with reducing core diameter, the magnetic anisotropy energy and core loss significantly increase. However, relatively high winding-induced core loss in small cores can be significantly reduced by increasing tensile stresses applied to the ribbon during pre-heating.

  19. Novel Crystal Structure C60 Nanowire

    NASA Astrophysics Data System (ADS)

    Mickelson, William; Aloni, Shaul; Han, Weiqiang; Cumings, John; Zettl, Alex

    2003-03-01

    We have created insulated C60 nanowire by packing C60 molecules into the interior of insulating boron nitride (BN) nanotubes. For small-diameter BN tubes, the wire consists of a linear chain of C60's. With increasing BN tube inner diameter, novel C60 stacking configurations are obtained (including helical, hollow core, and incommensurate) which are unknown for bulk or thin film forms of C60. C60 in BN nanotubes presents a model system for studying the properties of new dimensionally-constrained "silo" crystal structures.

  20. Reduction of diffusion barriers in isolated rat islets improves survival, but not insulin secretion or transplantation outcome

    PubMed Central

    Janette Williams, S; Huang, Han-Hung; Kover, Karen; Moore, Wayne; Berkland, Cory; Singh, Milind; Smirnova, Irina V; MacGregor, Ronal

    2010-01-01

    For people with type 1 diabetes and severe hypoglycemic unawareness, islet transplants offer hope for improving the quality of life. However, islet cell death occurs quickly during or after transplantation, requiring large quantities of islets per transplant. The purpose of this study was to determine whether poor function demonstrated in large islets was a result of diffusion barriers and if removing those barriers could improve function and transplantation outcomes. Islets were isolated from male DA rats and measured for cell viability, islet survival, glucose diffusion and insulin secretion. Modeling of diffusion barriers was completed using dynamic partial differential equations for a sphere. Core cell death occurred in 100% of the large islets (diameter >150 µm), resulting in poor survival within 7 days after isolation. In contrast, small islets (diameter <100 µm) exhibited good survival rates in culture (91%). Glucose diffusion into islets was tracked with 2-NBDG; 4.2 µm/min in small islets and 2.8 µm/min in large islets. 2-NBDG never permeated to the core cells of islets larger than 150 µm diameter. Reducing the diffusion barrier in large islets improved their immediate and long-term viability in culture. However, reduction of the diffusion barrier in large islets failed to improve their inferior in vitro insulin secretion compared to small islets, and did not return glucose control to diabetic animals following transplantation. Thus, diffusion barriers lead to low viability and poor survival for large islets, but are not solely responsible for the inferior insulin secretion or poor transplantation outcomes of large versus small islets. PMID:20885858

  1. ANALYSIS OF LEAD IN CANDLE PARTICULATE EMISSIONS BY XRF USING UNIQUANT 4

    EPA Science Inventory

    As part of an extensive program to study the small combustion sources of indoor fine particulate matter (PM), candles with lead-core wicks were burned in a 46-L glass flow- through chamber. The particulate emissions with aerodynamic diameters <10 micrometers (PM10) were captured ...

  2. Core-free rolled actuators for Braille displays using P(VDF-TrFE-CFE)

    NASA Astrophysics Data System (ADS)

    Levard, Thomas; Diglio, Paul J.; Lu, Sheng-Guo; Rahn, Christopher D.; Zhang, Q. M.

    2012-01-01

    Refreshable Braille displays require many small diameter actuators to move the pins. The electrostrictive P(VDF-TrFE-CFE) terpolymer can provide the high strain and actuation force under modest electric fields that are required for this application. In this paper, we develop core-free tubular actuators and integrate them into a 3 × 2 Braille cell. The terpolymer films are solution cast, stretched to 6 μm thick, electroded, laminated into a bilayer, rolled into a 2 mm diameter tube, bonded, and provided with top and bottom contacts. Experimental testing of 17 actuators demonstrates significant strains (up to 4%) and blocking forces (1 N) at moderate electric fields (100 MV m-1). A novel Braille cell is designed and fabricated using six of these actuators.

  3. Internal structure of normal maize starch granules revealed by chemical surface gelatinization.

    PubMed

    Pan, D D; Jane, J I

    2000-01-01

    Normal maize starch was fractionated into two sizes: large granules with diameters more than 5 microns and small granules with diameters less than 5 microns. The large granules were surface gelatinized by treating them with an aqueous LiCl solution (13 M) at 22-23 degrees C. Surface-gelatinized remaining granules were obtained by mechanical blending, and gelatinized surface starch was obtained by grinding with a mortar and a pestle. Starches of different granular sizes and radial locations, obtained after different degrees of surface gelatinization, were subjected to scanning electron microscopy, iodine potentiometric titration, gel-permeation chromatography, and amylopectin branch chain length analysis. Results showed that the remaining granules had a rough surface with a lamella structure. Amylose was more concentrated at the periphery than at the core of the granule. Amylopectin had longer long B-chains at the core than at the periphery of the granule. Greater proportions of the long B-chains were present at the core than at the periphery of the granule.

  4. Verification of the FBR fuel bundle-duct interaction analysis code BAMBOO by the out-of-pile bundle compression test with large diameter pins

    NASA Astrophysics Data System (ADS)

    Uwaba, Tomoyuki; Ito, Masahiro; Nemoto, Junichi; Ichikawa, Shoichi; Katsuyama, Kozo

    2014-09-01

    The BAMBOO computer code was verified by results for the out-of-pile bundle compression test with large diameter pin bundle deformation under the bundle-duct interaction (BDI) condition. The pin diameters of the examined test bundles were 8.5 mm and 10.4 mm, which are targeted as preliminary fuel pin diameters for the upgraded core of the prototype fast breeder reactor (FBR) and for demonstration and commercial FBRs studied in the FaCT project. In the bundle compression test, bundle cross-sectional views were obtained from X-ray computer tomography (CT) images and local parameters of bundle deformation such as pin-to-duct and pin-to-pin clearances were measured by CT image analyses. In the verification, calculation results of bundle deformation obtained by the BAMBOO code analyses were compared with the experimental results from the CT image analyses. The comparison showed that the BAMBOO code reasonably predicts deformation of large diameter pin bundles under the BDI condition by assuming that pin bowing and cladding oval distortion are the major deformation mechanisms, the same as in the case of small diameter pin bundles. In addition, the BAMBOO analysis results confirmed that cladding oval distortion effectively suppresses BDI in large diameter pin bundles as well as in small diameter pin bundles.

  5. Water dynamics in large and small reverse micelles: From two ensembles to collective behavior

    PubMed Central

    Moilanen, David E.; Fenn, Emily E.; Wong, Daryl; Fayer, Michael D.

    2009-01-01

    The dynamics of water in Aerosol-OT reverse micelles are investigated with ultrafast infrared spectroscopy of the hydroxyl stretch. In large reverse micelles, the dynamics of water are separable into two ensembles: slow interfacial water and bulklike core water. As the reverse micelle size decreases, the slowing effect of the interface and the collective nature of water reorientation begin to slow the dynamics of the core water molecules. In the smallest reverse micelles, these effects dominate and all water molecules have the same long time reorientational dynamics. To understand and characterize the transition in the water dynamics from two ensembles to collective reorientation, polarization and frequency selective infrared pump-probe experiments are conducted on the complete range of reverse micelle sizes from a diameter of 1.6–20 nm. The crossover between two ensemble and collective reorientation occurs near a reverse micelle diameter of 4 nm. Below this size, the small number of confined water molecules and structural changes in the reverse micelle interface leads to homogeneous long time reorientation. PMID:19586114

  6. High sensitivity refractive index sensor based on a tapered small core single-mode fiber structure.

    PubMed

    Liu, Dejun; Mallik, Arun Kumar; Yuan, Jinhui; Yu, Chongxiu; Farrell, Gerald; Semenova, Yuliya; Wu, Qiang

    2015-09-01

    A high sensitivity refractive index (RI) sensor based on a tapered small core single-mode fiber (SCSMF) structure sandwiched between two traditional single-mode fibers (SMF28) is reported. The microheater brushing technique was employed to fabricate the tapered fiber structures with different waist diameters of 12.5, 15.0, and 18.8 μm. Experiments demonstrate that the fiber sensor with a waist diameter of 12.5 μm offers the best sensitivity of 19212.5  nm/RIU (RI unit) in the RI range of 1.4304 to 1.4320. All sensors fabricated in this Letter show good linearity in terms of the spectral wavelength shift versus changes in RI. Furthermore, the sensor with the best sensitivity to RI was also used to measure relative humidity (RH) without any coating materials applied to the fiber surface. Experimental results show that the spectral wavelength shift changes exponentially as the RH varies from 60% to 95%. A maximum sensitivity of 18.3 nm per relative humidity unit (RHU) was achieved in the RH range of 90.4% to 94.5% RH.

  7. DOE Office of Scientific and Technical Information (OSTI.GOV)

    Pavlou, A. T.; Betzler, B. R.; Burke, T. P.

    Uncertainties in the composition and fabrication of fuel compacts for the Fort St. Vrain (FSV) high temperature gas reactor have been studied by performing eigenvalue sensitivity studies that represent the key uncertainties for the FSV neutronic analysis. The uncertainties for the TRISO fuel kernels were addressed by developing a suite of models for an 'average' FSV fuel compact that models the fuel as (1) a mixture of two different TRISO fuel particles representing fissile and fertile kernels, (2) a mixture of four different TRISO fuel particles representing small and large fissile kernels and small and large fertile kernels and (3)more » a stochastic mixture of the four types of fuel particles where every kernel has its diameter sampled from a continuous probability density function. All of the discrete diameter and continuous diameter fuel models were constrained to have the same fuel loadings and packing fractions. For the non-stochastic discrete diameter cases, the MCNP compact model arranged the TRISO fuel particles on a hexagonal honeycomb lattice. This lattice-based fuel compact was compared to a stochastic compact where the locations (and kernel diameters for the continuous diameter cases) of the fuel particles were randomly sampled. Partial core configurations were modeled by stacking compacts into fuel columns containing graphite. The differences in eigenvalues between the lattice-based and stochastic models were small but the runtime of the lattice-based fuel model was roughly 20 times shorter than with the stochastic-based fuel model. (authors)« less

  8. Proof of Principle: Immobilisation of Robust CuII3 TbIII -Macrocycles on Small, Suitably Pre-functionalised Gold Nanoparticles.

    PubMed

    Feltham, Humphrey L C; Dumas, Christophe; Mannini, Matteo; Otero, Edwige; Sainctavit, Philippe; Sessoli, Roberta; Meledandri, Carla J; Brooker, Sally

    2017-02-21

    In a proof-of-principle study, a soluble macrocyclic single-molecule magnet (SMM) containing a Cu II 3 Tb III magnetic core was covalently grafted onto small gold nanoparticles pre-functionalised with carboxylate-terminated tethers. A modified microemulsion method allowed production of the small and monodisperse nanoparticles (approximately 3.5 nm in diameter) for the chemisorption of a large amount of intact macrocyclic complexes in the hybrid system. © 2017 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

  9. Self-assembly of core-shell structure PtO2@Pt nanodots and their formation evolution

    NASA Astrophysics Data System (ADS)

    Yang, Weijia; Liu, Junjie; Liu, Mingquan; Zhao, Zhicheng; Song, Yapeng; Tang, Xiufeng; Luo, Jianyi; Zeng, Qingguang; He, Xin

    2018-05-01

    Core-shell structure PtO2@Pt nanodots have been self-assembly by vacuum sputtering and high temperature annealing. First, Pt thin films with a small amount of PtO2 are grown on the sapphire substrates by vacuum sputtering. And then high temperature annealing on the thin films is carried out at 800 °C for 2 min to form Pt nanodots. During the cooling process, the atmosphere is deployed to supplant the nitrogen. Finally, even distributed core-shell structure PtO2@Pt nanodots with a diameter from 100 to 300 nm are achieved. Furthermore, the formation evolution of core-shell structure PtO2@Pt nanodots is also proposed. This work open up a new approach for fabricating core-shell structure nanodots.

  10. Superconducting magnets for traveling-wave maser application. Technical documentary report, Oct 1960--Mar 1962

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Okwit, S.; Siegel, K.; Smith, J.G.

    1962-09-01

    Results of an investigation to determine the feasibility of incorporating superconducting magnet techniques in the design of traveling-wave maser systems are reported. Several different types of magnet configurations were investigated: isomagnets, Helmholtz coils, modified Helmholtz coils, air-core solenoids, and magnetic end-loaded air-core solenoids. The magnetic end-loaded air-core solenoid was found to be the best configuration for the S-band maser under consideration. This technique yielded relatively large regions of field homogeneity with relatively small aspect ratios (length of solenoid/diameter of solenoid). Several small-scale models of full-length superconducting magnets and foreshortened end-loaded superconducting magnets were constructed using un-annealed niobium wire. Measurements havemore » shown that these magnets were adequate for traveling-wave maser applications that require magnetic fields up to 2,200 G and marginal for magnetic fields up to 2,500 G.« less

  11. The truth about laser fiber diameters.

    PubMed

    Kronenberg, Peter; Traxer, Olivier

    2014-12-01

    To measure the various diameters of laser fibers from various manufacturers and compare them with the advertised diameter. Fourteen different unused laser fibers from 6 leading manufacturers with advertised diameters of 200, 270, 272, 273, 365, and 400 μm were measured by light microscopy. The outer diameter (including the fiber coating, cladding, and core), cladding diameter (including the cladding and the fiber core), and core diameter were measured. Industry representatives of the manufacturers were interviewed about the diameter of their fibers. For all fibers, the outer and cladding diameters differed significantly from the advertised diameter (P <.00001). The outer diameter, which is of most practical relevance for urologists, exhibited a median increase of 87.3% (range, 50.7%-116.7%). The outer, cladding, and core diameters of fibers with equivalent advertised diameters differed by up to 180, 100, and 78 μm, respectively. Some 200-μm fibers had larger outer diameters than the 270- to 273-μm fibers. All packaging material and all laser fibers lacked clear and precise fiber diameter information labels. Of 12 representatives interviewed, 8, 3, and 1 considered the advertised diameter to be the outer, the cladding, and the core diameter, respectively. Representatives within the same company frequently gave different answers. This study suggests that, at present, there is a lack of uniformity between laser fiber manufacturers, and most of the information conveyed to urologists regarding laser fiber diameter may be incorrect. Because fibers larger than the advertised laser fibers are known to influence key interventional parameters, this misinformation can have surgical repercussions. Copyright © 2014 Elsevier Inc. All rights reserved.

  12. Ultra-fast magnetic vortex core reversal by a local field pulse

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Rückriem, R.; Albrecht, M., E-mail: manfred.albrecht@physik.uni-augsburg.de; Schrefl, T.

    2014-02-03

    Magnetic vortex core reversal of a 20-nm-thick permalloy disk with a diameter of 100 nm was studied by micromagnetic simulations. By applying a global out-of-plane magnetic field pulse, it turned out that the final core polarity is very sensitive to pulse width and amplitude, which makes it hard to control. The reason for this phenomenon is the excitation of radial spin waves, which dominate the reversal process. The excitation of spin waves can be strongly suppressed by applying a local field pulse within a small area at the core center. With this approach, ultra-short reversal times of about 15 ps weremore » achieved, which are ten times faster compared to a global pulse.« less

  13. Internal magnetic structure of magnetite nanoparticles at low temperature

    NASA Astrophysics Data System (ADS)

    Krycka, K. L.; Borchers, J. A.; Booth, R. A.; Hogg, C. R.; Ijiri, Y.; Chen, W. C.; Watson, S. M.; Laver, M.; Gentile, T. R.; Harris, S.; Dedon, L. R.; Rhyne, J. J.; Majetich, S. A.

    2010-05-01

    Small-angle neutron scattering with polarization analysis reveals that Fe3O4 nanoparticles with 90 Å diameters have ferrimagnetic moments significantly reduced from that of bulk Fe3O4 at 10 K, nominal saturation. Combined with previous results for an equivalent applied field at 200 K, a core-disordered shell picture of a spatially reduced ferrimagnetic core emerges, even well below the bulk blocking temperature. Zero-field cooling suggests that this magnetic morphology may be intrinsic to the nanoparticle, rather than field induced, at 10 K.

  14. Nuclear reactor fuel element with vanadium getter on cladding

    DOEpatents

    Johnson, Carl E.; Carroll, Kenneth G.

    1977-01-01

    A nuclear reactor fuel element is described which has an outer cladding, a central core of fissionable or mixed fissionable and fertile fuel material and a layer of vanadium as an oxygen getter on the inner surface of the cladding. The vanadium reacts with oxygen released by the fissionable material during irradiation of the core to prevent the oxygen from reacting with and corroding the cladding. Also described is a method for coating the inner surface of small diameter tubes of cladding with a layer of vanadium.

  15. Characterization of Juvenile wood in Lodgepole Pine in the Intermountain West

    Treesearch

    Thomas M. Gorman; David E. Kretschmann

    2012-01-01

    Juvenile wood (core wood) is typically characterized as being less dimensionally stable and having lower mechanical properties than mature wood. Determination of the age of transition from juvenile wood to mature wood can provide basic information needed to assess dimensional stability and better utilize small-diameter trees growing in the intermountain west as solid-...

  16. Single-mode annular chirally-coupled core fibers for fiber lasers

    NASA Astrophysics Data System (ADS)

    Zhang, Haitao; Hao, He; He, Linlu; Gong, Mali

    2018-03-01

    Chirally-coupled core (CCC) fiber can transmit single fundamental mode and effectively suppresses higher-order mode (HOM) propagation, thus improve the beam quality. However, the manufacture of CCC fiber is complicated due to its small side core. To decrease the manufacture difficulty in China, a novel fiber structure is presented, defined as annular chirally-coupled core (ACCC) fiber, replacing the small side core by a larger side annulus. In this paper, we designed the fiber parameters of this new structure, and demonstrated that the new structure has a similar property of single mode with traditional CCC fiber. Helical coordinate system was introduced into the finite element method (FEM) to analyze the mode field in the fiber, and the beam propagation method (BPM) was employed to analyze the influence of the fiber parameters on the mode loss. Based on the result above, the fiber structure was optimized for efficient single-mode transmission, in which the core diameter is 35 μm with beam quality M2 value of 1.04 and an optical to optical conversion efficiency of 84%. In this fiber, fundamental mode propagates in an acceptable loss, while the HOMs decay rapidly.

  17. Dual-Channel, Molecular-Sieving Core/Shell ZIF@MOF Architectures as Engineered Fillers in Hybrid Membranes for Highly Selective CO2 Separation.

    PubMed

    Song, Zhuonan; Qiu, Fen; Zaia, Edmond W; Wang, Zhongying; Kunz, Martin; Guo, Jinghua; Brady, Michael; Mi, Baoxia; Urban, Jeffrey J

    2017-11-08

    A novel core/shell porous crystalline structure was prepared using a large pore metal organic framework (MOF, UiO-66-NH 2 , pore size, ∼ 0.6 nm) as core surrounded by a small pore zeolitic imidazolate framework (ZIF, ZIF-8, pore size, ∼ 0.4 nm) through a layer-by-layer deposition method and subsequently used as an engineered filler to construct hybrid polysulfone (PSF) membranes for CO 2 capture. Compared to traditional fillers utilizing only one type of porous material with rigid channels (either large or small), our custom designed core/shell fillers possess clear advantages via pore engineering: the large internal channels of the UiO-66-NH 2 MOFs create molecular highways to accelerate molecular transport through the membrane, while the thin shells with small pores (ZIF-8) or even smaller pores generated at the interface by the imperfect registry between the overlapping pores of ZIF and MOF enhance molecular sieving thus serving to distinguish slightly larger N 2 molecules (kinetic diameter, 0.364 nm) from smaller CO 2 molecules (kinetic diameter, 0.33 nm). The resultant core/shell ZIF@MOF and as-prepared hybrid PSF membranes were characterized by transmission electron microscopy, X-ray diffraction, wide-angle X-ray scattering, scanning electron microscopy, Fourier transform infrared, thermogravimetric analysis, differential scanning calorimetry, and contact angle tests. The dependence of the separation performance of the membranes on the MOF/ZIF ratio was also studied by varying the number of layers of ZIF coatings. The integrated PSF-ZIF@MOF hybrid membrane (40 wt % loading) with optimized ZIF coating cycles showed improved hydrophobicity and excellent CO 2 separation performance by simultaneously increasing CO 2 permeability (CO 2 permeability of 45.2 barrer, 710% higher than PSF membrane) and CO 2 /N 2 selectivity (CO 2 /N 2 selectivity of 39, 50% higher than PSF membrane), which is superior to most reported hybrid PSF membranes. The strategy of using dual-channel molecular sieving core/shell porous crystals in hybrid membranes thus provides a promising means for CO 2 capture from flue gas.

  18. Core decompression of the femoral head for osteonecrosis using percutaneous multiple small-diameter drilling.

    PubMed

    Mont, Michael A; Ragland, Phillip S; Etienne, Gracia

    2004-12-01

    Osteonecrosis is a disease with a wide ranging etiology and poorly understood pathogenesis seen commonly in young patients. Core decompression has historically been used in patients with small-sized or medium-sized precollapse lesions in an attempt to forestall disease progression. Typically, an 8-10 mm wide cannula trephine is used to do this procedure. The authors report on a new technique using multiple small drillings with a 3-mm Steinman pin to effectuate the core decompression. In this report, there were 32 of 45 hips (71%; 35 patients) with a successful clinical result at a mean followup of 2 years (range, 20-39 months). Twenty four of 30 Stage I hips (80%; 23 patients) had successful outcomes compared with 8 of 15 Stage II hips (57%; 12 patients) with no surgical complications occurring with this technique. This procedure is technically straightforward and led to minimal morbidity with no surgical complications. It may be effective in delaying the need for total hip arthroplasty in young patients with early (precollapse) stages of femoral head osteonecrosis.

  19. A comparative study on liquid core formulation on the diameter on the alginate capsules

    NASA Astrophysics Data System (ADS)

    Ong, Hui-Yen; Lee, Boon-Beng; Radzi, AkmalHadi Ma'; Zakaria, Zarina; Chan, Eng-Seng

    2015-08-01

    Liquid core capsule has vast application in biotechnology related industries such as pharmaceutical, medical, agriculture and food. Formulation of different types of capsule was important to determine the performance of the capsule. Generally, the liquid core capsule with different formulations generated different size of capsule.Therefore, the aim of this project is to investigate the effect of different liquid core solution formulations on the diameter of capsule. The capsule produced by extruding liquid core solutions into sodium alginate solution. Three types of liquid core solutions (chitosan, xanthan gum, polyethylene glycol (PEG)) were investigated. The results showed that there is significant change in capsule diameter despite in different types of liquid core solution were used and a series of capsule range in diameter of 3.1 mm to 4.5 mm were produced. Alginate capsule with chitosan formulation appeared to be the largest capsule among all.

  20. Porosity and pore size distribution in a sedimentary rock: Implications for the distribution of chlorinated solvents

    NASA Astrophysics Data System (ADS)

    Shapiro, Allen M.; Evans, Christopher E.; Hayes, Erin C.

    2017-08-01

    Characterizing properties of the rock matrix that control retention and release of chlorinated solvents is essential in evaluating the extent of contamination and the application of remediation technologies in fractured rock. Core samples from seven closely spaced boreholes in a mudstone subject to trichloroethene (TCE) contamination were analyzed using Mercury Intrusion Porosimetry to investigate porosity and pore size distribution as a function of mudstone characteristics, and depth and lateral extent in the aquifer; organic carbon content was also evaluated to identify the potential for adsorption. Porosity and retardation factor varied over two orders of magnitude, with the largest porosities and largest retardation factors associated with carbon-rich mudstone layers. Larger porosities were also measured in the shallow rock that has been subject to enhanced groundwater flow. Porosity also varied over more than an order of magnitude in spatially continuous mudstone layers. The analyses of the rock cores indicated that the largest pore diameters may be accessible to entry of the nonaqueous form of TCE. Although the porosity associated with the largest pore diameters is small ( 0.1%), that volume of TCE can significantly affect the total TCE that is retained in the rock matrix. The dimensions of the largest pore diameters may also be accessible to microbes responsible for reductive dechlorination; however, the small percentage of the pore space that can accommodate microbes may limit the extent of reductive dechlorination in the rock matrix.

  1. Porosity and pore size distribution in a sedimentary rock: Implications for the distribution of chlorinated solvents

    USGS Publications Warehouse

    Shapiro, Allen M.; Evans, Chrsitopher E.; Hayes, Erin C.

    2017-01-01

    Characterizing properties of the rock matrix that control retention and release of chlorinated solvents is essential in evaluating the extent of contamination and the application of remediation technologies in fractured rock. Core samples from seven closely spaced boreholes in a mudstone subject to trichloroethene (TCE) contamination were analyzed using Mercury Intrusion Porosimetry to investigate porosity and pore size distribution as a function of mudstone characteristics, and depth and lateral extent in the aquifer; organic carbon content was also evaluated to identify the potential for adsorption. Porosity and retardation factor varied over two orders of magnitude, with the largest porosities and largest retardation factors associated with carbon-rich mudstone layers. Larger porosities were also measured in the shallow rock that has been subject to enhanced groundwater flow. Porosity also varied over more than an order of magnitude in spatially continuous mudstone layers. The analyses of the rock cores indicated that the largest pore diameters may be accessible to entry of the nonaqueous form of TCE. Although the porosity associated with the largest pore diameters is small (~ 0.1%), that volume of TCE can significantly affect the total TCE that is retained in the rock matrix. The dimensions of the largest pore diameters may also be accessible to microbes responsible for reductive dechlorination; however, the small percentage of the pore space that can accommodate microbes may limit the extent of reductive dechlorination in the rock matrix.

  2. Preparation, characterization, and optical properties of gold, silver, and gold-silver alloy nanoshells having silica cores.

    PubMed

    Kim, Jun-Hyun; Bryan, William W; Lee, T Randall

    2008-10-07

    This report describes the structural and optical properties of a series of spherical shell/core nanoparticles in which the shell is comprised of a thin layer of gold, silver, or gold-silver alloy, and the core is comprised of a monodispersed silica nanoparticle. The silica core particles were prepared using the Stöber method, functionalized with terminal amine groups, and then seeded with small gold nanoparticles (approximately 2 nm in diameter). The gold-seeded silica particles were coated with a layer of gold, silver, or gold-silver alloy via solution-phase reduction of an appropriate metal ion or mixture of metal ions. The size, morphology, and elemental composition of the composite nanoparticles were characterized by field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, thermal gravimetric analysis (TGA), dynamic light scattering (DLS), and transmission electron microscopy (TEM). The optical properties of the nanoparticles were analyzed by UV-vis spectroscopy, which showed strong absorptions ranging from 400 nm into the near-IR region, where the position of the plasmon band reflected not only the thickness of the metal shell, but also the nature of the metal comprising the shell. Importantly, the results demonstrate a new strategy for tuning the position of the plasmon resonance without having to vary the core diameter or the shell thickness.

  3. Packing C60 in Boron Nitride Nanotubes

    NASA Astrophysics Data System (ADS)

    Mickelson, W.; Aloni, S.; Han, Wei-Qiang; Cumings, John; Zettl, A.

    2003-04-01

    We have created insulated C60 nanowire by packing C60 molecules into the interior of insulating boron nitride nanotubes (BNNTs). For small-diameter BNNTs, the wire consists of a linear chain of C60 molecules. With increasing BNNT inner diameter, unusual C60 stacking configurations are obtained (including helical, hollow core, and incommensurate) that are unknown for bulk or thin-film forms of C60. C60 in BNNTs thus presents a model system for studying the properties of dimensionally constrained ``silo'' crystal structures. For the linear-chain case, we have fused the C60 molecules to form a single-walled carbon nanotube inside the insulating BNNT.

  4. Core break-off mechanism

    NASA Technical Reports Server (NTRS)

    Myrick, Thomas M. (Inventor)

    2003-01-01

    A mechanism for breaking off and retaining a core sample of a drill drilled into a ground substrate has an outer drill tube and an inner core break-off tube sleeved inside the drill tube. The break-off tube breaks off and retains the core sample by a varying geometric relationship of inner and outer diameters with the drill tube. The inside diameter (ID) of the drill tube is offset by a given amount with respect to its outer diameter (OD). Similarly, the outside diameter (OD) of the break-off tube is offset by the same amount with respect to its inner diameter (ID). When the break-off tube and drill tube are in one rotational alignment, the two offsets cancel each other such that the drill can operate the two tubes together in alignment with the drill axis. When the tubes are rotated 180 degrees to another positional alignment, the two offsets add together causing the core sample in the break-off tube to be displaced from the drill axis and applying shear forces to break off the core sample.

  5. Effect of Osteonecrosis Intervention Rod Versus Core Decompression Using Multiple Small Drill Holes on Early Stages of Necrosis of the Femoral Head: A Prospective Study on a Series of 60 Patients with a Minimum 1-Year-Follow-Up.

    PubMed

    Miao, Haixiong; Ye, Dongping; Liang, Weiguo; Yao, Yicun

    2015-01-01

    The conventional CD used 10 mm drill holes associated with a lack of structural support. Thus, alternative methods such as a tantalum implant, small drill holes, and biological treatment were developed to prevent deterioration of the joint. The treatment of CD by multiple 3.2 mm drill holes could reduce the femoral neck fracture and partial weight bearing was allowed. This study was aimed to evaluate the effect of osteonecrosis intervention rod versus core decompression using multiple small drill holes on early stages of necrosis of the femoral head. From January 2011 to January 2012, 60 patients undergoing surgery for osteonecrosis with core decompression were randomly assigned into 2 groups based on the type of core decompression used: (1) a total of 30 osteonecrosis patients (with 16 hips on Steinburg stageⅠ,20 hips on Steinburg stageⅡ) were treated with a porous tantalum rod insertion. The diameter of the drill hole for the intervention rod was 10mm.(2) a total of 30 osteonecrosis patients (with 14 hips on Steinburg stageⅠ,20 hips on Steinburg stageⅡ) were treated with core decompression using five drill holes on the lateral femur, the diameter of the hole was 3.2 mm. The average age of the patient was 32.6 years (20-45 years) and the average time of follow-up was 25.6 months (12- 28 months) in the rod implanted group. The average age of the patient was 35.2 years (22- 43 years) and the average time of follow-up was 26.3 months (12-28 months) in the small drill holes group. The average of surgical time was 40 min, and the mean volume of blood loss was 30 ml in both surgical groups. The average of Harris score was improved from 56.2 ± 7.1 preoperative to 80.2 ± 11.4 at the last follow-up in the rod implanted group (p < 0.05). The mean Harris score was improved from 53.8 ± 6.6 preoperative to 79.7 ± 13.2 at the last follow-up in the small drill holes group (p<0. 05). No significant difference was observed in Harris score between the two groups. At the last follow-up, 28 of 36 hips were at the same radiographic stages as pre-operation, and 8 deteriorated in the rod implanted group. 26 of 34 hips were at the same radiographic stage as pre-operation, and 8 deteriorated in the small drill holes group. No significant difference was observed in radiographic stage between the two groups. There was no favourable result on the outcome of a tantalum intervention implant compared to multiple small drill holes. CD via multiple small drill holes would allow similar postoperative load-bearing and seems to result in similar or even better clinical outcome without the prolonged implantation of an expensive tantalum implant. A tantalum rod intervention and core decompression using multiple small drill holes were effective on the stage I hips rather than stage II hips.

  6. Modeling individual tree growth by fusing diameter tape and increment core data

    Treesearch

    Erin M. Schliep; Tracy Qi Dong; Alan E. Gelfand; Fan. Li

    2014-01-01

    Tree growth estimation is a challenging task as difficulties associated with data collection and inference often result in inaccurate estimates. Two main methods for tree growth estimation are diameter tape measurements and increment cores. The former involves repeatedly measuring tree diameters with a cloth or metal tape whose scale has been adjusted to give diameter...

  7. Phytoscreening with SPME: Variability Analysis.

    PubMed

    Limmer, Matt A; Burken, Joel G

    2015-01-01

    Phytoscreening has been demonstrated at a variety of sites over the past 15 years as a low-impact, sustainable tool in delineation of shallow groundwater contaminated with chlorinated solvents. Collection of tree cores is rapid and straightforward, but low concentrations in tree tissues requires sensitive analytics. Solid-phase microextraction (SPME) is amenable to the complex matrix while allowing for solvent-less extraction. Accurate quantification requires the absence of competitive sorption, examined here both in laboratory experiments and through comprehensive examination of field data. Analysis of approximately 2,000 trees at numerous field sites also allowed testing of the tree genus and diameter effects on measured tree contaminant concentrations. Collectively, while these variables were found to significantly affect site-adjusted perchloroethylene (PCE) concentrations, the explanatory power of these effects was small (adjusted R(2) = 0.031). 90th quantile chemical concentrations in trees were significantly reduced by increasing Henry's constant and increasing hydrophobicity. Analysis of replicate tree core data showed no correlation between replicate relative standard deviation (RSD) and wood type or tree diameter, with an overall median RSD of 30%. Collectively, these findings indicate SPME is an appropriate technique for sampling and analyzing chlorinated solvents in wood and that phytoscreening is robust against changes in tree type and diameter.

  8. Specific Internalisation of Gold Nanoparticles into Engineered Porous Protein Cages via Affinity Binding

    PubMed Central

    Peng, Tao; Free, Paul; Fernig, David G.; Lim, Sierin; Tomczak, Nikodem

    2016-01-01

    Porous protein cages are supramolecular protein self-assemblies presenting pores that allow the access of surrounding molecules and ions into their core in order to store and transport them in biological environments. Protein cages’ pores are attractive channels for the internalisation of inorganic nanoparticles and an alternative for the preparation of hybrid bioinspired nanoparticles. However, strategies based on nanoparticle transport through the pores are largely unexplored, due to the difficulty of tailoring nanoparticles that have diameters commensurate with the pores size and simultaneously displaying specific affinity to the cages’ core and low non-specific binding to the cages’ outer surface. We evaluated the specific internalisation of single small gold nanoparticles, 3.9 nm in diameter, into porous protein cages via affinity binding. The E2 protein cage derived from the Geobacillus stearothermophilus presents 12 pores, 6 nm in diameter, and an empty core of 13 nm in diameter. We engineered the E2 protein by site-directed mutagenesis with oligohistidine sequences exposing them into the cage’s core. Dynamic light scattering and electron microscopy analysis show that the structures of E2 protein cages mutated with bis- or penta-histidine sequences are well conserved. The surface of the gold nanoparticles was passivated with a self-assembled monolayer made of a mixture of short peptidols and thiolated alkane ethylene glycol ligands. Such monolayers are found to provide thin coatings preventing non-specific binding to proteins. Further functionalisation of the peptide coated gold nanoparticles with Ni2+ nitrilotriacetic moieties enabled the specific binding to oligohistidine tagged cages. The internalisation via affinity binding was evaluated by electron microscopy analysis. From the various mutations tested, only the penta-histidine mutated E2 protein cage showed repeatable and stable internalisation. The present work overcomes the limitations of currently available approaches and provides a new route to design tailored and well-controlled hybrid nanoparticles. PMID:27622533

  9. Underwater noise from geotechnical drilling and standard penetration testing.

    PubMed

    Erbe, Christine; McPherson, Craig

    2017-09-01

    Geotechnical site investigations prior to marine construction typically involve shallow, small-core drilling and standard penetration testing (SPT), during which a small tube is hammered into the ground at the bottom of the borehole. Drilling (120 kW, 83 mm diameter drillbit, 1500 rpm, 16-17 m drill depth in sand and mudstone) and SPT (50 mm diameter test tube, 15 mm wall thickness, 100 kg hammer, 1 m drop height) by a jack-up rig in 7-13 m of water were recorded with a drifting hydrophone at 10-50 m range. Source levels were 142-145 dB re 1 μPa rms @ 1 m (30-2000 Hz) for drilling and 151-160 dB re 1 μPa 2 s @ 1 m (20-24 000 Hz) for SPT.

  10. Respiration and body movement analysis during sleep in bed using hetero-core fiber optic pressure sensors without constraint to human activity.

    PubMed

    Nishyama, Michiko; Miyamoto, Mitsuo; Watanabe, Kazuhiro

    2011-01-01

    We describe respiration monitoring in sleep using hetero-core fiber optic pressure sensors. The proposed hetero-core fiber optic sensor is highly sensitive to macrobending as a result of the core diameter difference due to stable single-mode transmission. Pressure sensors based on hetero-core fiber optics were fabricated to have a high sensitivity to small pressure changes resulting from minute body motions, such as respiration, during sleep and large pressure changes, such as those caused by a rollover. The sensors are installed in a conventional bed. The pressure characteristic performance of all the fabricated hetero-core fiber optic pressure sensors is found to show a monotonic response with weight changes. A respiration monitoring test in seven subjects efficiently demonstrates the effective use of eight hetero-core pressure sensors installed in a bed. Additionally, even in the case of different body postures, such as lying on one's side, a slight body movement due to respiration is detected by the hetero-core pressure sensors.

  11. Respiration and body movement analysis during sleep in bed using hetero-core fiber optic pressure sensors without constraint to human activity

    NASA Astrophysics Data System (ADS)

    Nishyama, Michiko; Miyamoto, Mitsuo; Watanabe, Kazuhiro

    2011-01-01

    We describe respiration monitoring in sleep using hetero-core fiber optic pressure sensors. The proposed hetero-core fiber optic sensor is highly sensitive to macrobending as a result of the core diameter difference due to stable single-mode transmission. Pressure sensors based on hetero-core fiber optics were fabricated to have a high sensitivity to small pressure changes resulting from minute body motions, such as respiration, during sleep and large pressure changes, such as those caused by a rollover. The sensors are installed in a conventional bed. The pressure characteristic performance of all the fabricated hetero-core fiber optic pressure sensors is found to show a monotonic response with weight changes. A respiration monitoring test in seven subjects efficiently demonstrates the effective use of eight hetero-core pressure sensors installed in a bed. Additionally, even in the case of different body postures, such as lying on one's side, a slight body movement due to respiration is detected by the hetero-core pressure sensors.

  12. Transvaginal photoacoustic imaging probe and system based on a multiport fiber-optic beamsplitter and a real time imager for ovarian cancer detection

    NASA Astrophysics Data System (ADS)

    Kumavor, Patrick D.; Alqasemi, Umar; Tavakoli, Behnoosh; Li, Hai; Yang, Yi; Zhu, Quing

    2013-03-01

    This paper presents a real-time transvaginal photoacoustic imaging probe for imaging human ovaries in vivo. The probe consists of a high-throughput (up to 80%) fiber-optic 1 x 19 beamsplitters, a commercial array ultrasound transducer, and a fiber protective sheath. The beamsplitter has a 940-micron core diameter input fiber and 240-micron core diameter output fibers numbering 36. The 36 small-core output fibers surround the ultrasound transducer and delivers light to the tissue during imaging. A protective sheath, modeled in the form of the transducer using a 3-D printer, encloses the transducer with array of fibers. A real-time image acquisition system collects and processes the photoacoustic RF signals from the transducer, and displays the images formed on a monitor in real time. Additionally, the system is capable of coregistered pulse-echo ultrasound imaging. In this way, we obtain both morphological and functional information from the ovarian tissue. Photoacousitc images of malignant human ovaries taken ex vivo with the probe revealed blood vascular and networks that was distinguishable from normal ovaries, making the probe potential useful for characterizing ovarian tissue.

  13. Pressure-assisted melt-filling and optical characterization of Au nano-wires in microstructured fibers.

    PubMed

    Lee, H W; Schmidt, M A; Russell, R F; Joly, N Y; Tyagi, H K; Uebel, P; Russell, P St J

    2011-06-20

    We report a novel splicing-based pressure-assisted melt-filling technique for creating metallic nanowires in hollow channels in microstructured silica fibers. Wires with diameters as small as 120 nm (typical aspect ration 50:1) could be realized at a filling pressure of 300 bar. As an example we investigate a conventional single-mode step-index fiber with a parallel gold nanowire (wire diameter 510 nm) running next to the core. Optical transmission spectra show dips at wavelengths where guided surface plasmon modes on the nanowire phase match to the glass core mode. By monitoring the side-scattered light at narrow breaks in the nanowire, the loss could be estimated. Values as low as 0.7 dB/mm were measured at resonance, corresponding to those of an ultra-long-range eigenmode of the glass-core/nanowire system. By thermal treatment the hollow channel could be collapsed controllably, permitting creation of a conical gold nanowire, the optical properties of which could be monitored by side-scattering. The reproducibility of the technique and the high optical quality of the wires suggest applications in fields such as nonlinear plasmonics, near-field scanning optical microscope tips, cylindrical polarizers, optical sensing and telecommunications.

  14. Nano-Scale Sample Acquisition Systems for Small Class Exploration Spacecraft

    NASA Astrophysics Data System (ADS)

    Paulsen, G.

    2015-12-01

    The paradigm for space exploration is changing. Large and expensive missions are very rare and the space community is turning to smaller, lighter, and less expensive missions that could still perform great exploration. These missions are also within reach of commercial companies such as the Google Lunar X Prize teams that develop small scale lunar missions. Recent commercial endeavors such as "Planet Labs inc." and Sky Box Imaging, inc. show that there are new benefits and business models associated with miniaturization of space hardware. The Nano-Scale Sample Acquisition System includes NanoDrill for capture of small rock cores and PlanetVac for capture of surface regolith. These two systems are part of the ongoing effort to develop "Micro Sampling" systems for deployment by the small spacecraft with limited payload capacities. The ideal applications include prospecting missions to the Moon and Asteroids. The MicroDrill is a rotary-percussive coring drill that captures cores 7 mm in diameter and up to 2 cm long. The drill weighs less than 1 kg and can capture a core from a 40 MPa strength rock within a few minutes, with less than 10 Watt power and less than 10 Newton of preload. The PlanetVac is a pneumatic based regolith acquisition system that can capture surface sample in touch-and-go maneuver. These sampling systems were integrated within the footpads of commercial quadcopter for testing. As such, they could also be used by geologists on Earth to explore difficult to get to locations.

  15. Tellurite microstructure fibers with small hexagonal core for supercontinuum generation.

    PubMed

    Liao, Meisong; Chaudhari, Chitrarekha; Qin, Guanshi; Yan, Xin; Suzuki, Takenobu; Ohishi, Yasutake

    2009-07-06

    Tellurite glass microstructure fibers with a 1 microm hexagonal core were fabricated successfully by accurately controlling the temperature field in the fiber-drawing process. The diameter ratio of holey region to core (DRHC) for the fiber can be adjusted freely in the range of 1-20 by pumping a positive pressure into the holes when drawing fiber, which provides much freedom in engineering the chromatic dispersion. With the increase of DRHC from 3.5 to 20, the zero dispersion wavelengths were shifted several hundred nanometers, the cutoff wavelength due to confinement loss was increased from 1600 nm to 3800 nm, and the nonlinear coefficient gamma was increased from 3.9 to 5.7 W(-1)/m. Efficient visible emissions due to third harmonic generation were found for fibers with a DRHC of 10 and 20 under the 1557 nm pump of a femtosecond fiber laser. One octave flattened supercontinuum spectrum was generated from fibers with a DRHC of 3.5, 10 and 20 by the 1064 nm pump of a picosecond fiber laser. To the best of our knowledge, we have for the first time fabricated a hexagonal core fiber by soft glass with such a small core size, and have demonstrated a large influence of the holey region on the dispersion, nonlinear coefficient and supercontinuum generation for such fiber.

  16. Ru-core/Cu-shell bimetallic nanoparticles with controlled size formed in one-pot synthesis.

    PubMed

    Helgadottir, I; Freychet, G; Arquillière, P; Maret, M; Gergaud, P; Haumesser, P H; Santini, C C

    2014-12-21

    Suspensions of bimetallic nanoparticles (NPs) of Ru and Cu have been synthesized by simultaneous decomposition of two organometallic compounds in an ionic liquid. These suspensions have been characterized by Anomalous Small-Angle X-ray Scattering (ASAXS) at energies slightly below the Ru K-edge. It is found that the NPs adopt a Ru-core, a Cu-shell structure, with a constant Ru core diameter of 1.9 nm for all Ru : Cu compositions, while the Cu shell thickness increases with Cu content up to 0.9 nm. The formation of RuCuNPs thus proceeds through rapid decomposition of the Ru precursor into RuNPs of constant size followed by the reaction of the Cu precursor and agglomeration as a Cu shell. Thus, the different decomposition kinetics of precursors make possible the elaboration of core-shell NPs composed of two metals without chemical affinity.

  17. How temperature determines formation of maghemite nanoparticles

    NASA Astrophysics Data System (ADS)

    Girod, Matthias; Vogel, Stefanie; Szczerba, Wojciech; Thünemann, Andreas F.

    2015-04-01

    We report on the formation of polymer-stabilized superparamagnetic single-core and multi-core maghemite nanoparticles. The particle formation was carried out by coprecipitation of Fe(II) and Fe(III) sulfate in a continuous aqueous process using a micromixer system. Aggregates containing 50 primary particles with sizes of 2 nm were formed at a reaction temperature of 30 °C. These particles aggregated further with time and were not stable. In contrast, stable single-core particles with a diameter of 7 nm were formed at 80 °C as revealed by small-angle X-ray scattering (SAXS) coupled in-line with the micromixer for particle characterization. X-ray diffraction and TEM confirmed the SAXS results. X-ray absorption near-edge structure spectroscopy (XANES) identified the iron oxide phase as maghemite.

  18. Molecular pathways in the transformation of model discoidal lipoprotein complexes induced by lecithin:cholesterol acyltransferase.

    PubMed

    Nichols, A V; Blanche, P J; Gong, E L; Shore, V G; Forte, T M

    1985-05-17

    Incubation (24 h, 37 degrees C) of discoidal complexes of phosphatidylcholine and apolipoprotein A-I (molar ratio 95 +/- 10 egg yolk phosphatidylcholine-apolipoprotein A-I; 10.5 X 4.0 nm, long X short dimension; designated, class 3 complexes) with the ultracentrifugal d greater than 1.21 g/ml fraction transformed the discoidal complexes to a small product with apparent mean hydrated and nonhydrated diameter of 7.8 and 6.6 nm, respectively. Formation of the small product was associated with marked reduction in phosphatidylcholine-apolipoprotein AI molar ratio of the complexes (on average from 95:1 to 45:1). Phospholipase A2 activity of lecithin:cholesterol acyltransferase participated in the depletion process, as evidenced by production of unesterified fatty acids. In the presence of the d greater than 1.21 g/ml fraction or partially purified lecithin:cholesterol acyltransferase and a source of unesterified cholesterol, the small product could be transformed to a core-containing (cholesteryl ester) round product with a hydrated and nonhydrated diameter of 8.6 and 7.5 nm, respectively. By means of cross-linking with dimethylsuberimidate, the protein moiety of the small product was shown to contain primarily two apolipoprotein A-I molecules per particle, while the large product contained three apolipoprotein A-I molecules per particle. The increase in number of apolipoprotein A-I molecules per particle during transformation of the small to the large product appeared to result from fusion of the small particles during core build-up and release of excess apolipoprotein A-I from the fusion product. The results obtained with the model complexes were consistent for the most part with recent observations (Chen, C., Applegate, K., King, W.C., Glomset, J.A., Norum, K.R. and Gjone, E. (1984) J. Lipid Res. 25, 269-282) on the transformation, by lecithin:cholesterol acyltransferase, of the small spherical high-density lipoproteins of patients with familial lecithin:cholesterol acyltransferase deficiency.

  19. Hollow carbon nanospheres using an asymmetric triblock copolymer structure directing agent.

    PubMed

    Li, Yunqi; Tan, Haibo; Salunkhe, Rahul R; Tang, Jing; Shrestha, Lok Kumar; Bastakoti, Bishnu Prasad; Rong, Hongpan; Takei, Toshiaki; Henzie, Joel; Yamauchi, Yusuke; Ariga, Katsuhiko

    2016-12-20

    We introduce a simple method to prepare hollow carbon nanospheres (HCNs) by using triblock copolymer poly(styrene-b-2-vinylpyridine-b-ethylene oxide) (PS-b-P2VP-b-PEO) micelles as a new class of soft-templates. Simply by changing the solvent we can prepare ultra-small sized micelles of the triblock copolymer PS-b-P2VP-b-PEO soft template to obtain HCNs with ultra-small diameters (43 nm) and hollow cores (19 nm). Furthermore, we use these HCNs to make electric double-layer capacitors (EDLCs) that exhibit superior performance.

  20. Micropore and nanopore fabrication in hollow antiresonant reflecting optical waveguides

    PubMed Central

    Holmes, Matthew R.; Shang, Tao; Hawkins, Aaron R.; Rudenko, Mikhail; Measor, Philip; Schmidt, Holger

    2011-01-01

    We demonstrate the fabrication of micropore and nanopore features in hollow antiresonant reflecting optical waveguides to create an electrical and optical analysis platform that can size select and detect a single nanoparticle. Micropores (4 μm diameter) are reactive-ion etched through the top SiO2 and SiN layers of the waveguides, leaving a thin SiN membrane above the hollow core. Nanopores are formed in the SiN membranes using a focused ion-beam etch process that provides control over the pore size. Openings as small as 20 nm in diameter are created. Optical loss measurements indicate that micropores did not significantly alter the loss along the waveguide. PMID:21922035

  1. Micropore and nanopore fabrication in hollow antiresonant reflecting optical waveguides.

    PubMed

    Holmes, Matthew R; Shang, Tao; Hawkins, Aaron R; Rudenko, Mikhail; Measor, Philip; Schmidt, Holger

    2010-01-01

    We demonstrate the fabrication of micropore and nanopore features in hollow antiresonant reflecting optical waveguides to create an electrical and optical analysis platform that can size select and detect a single nanoparticle. Micropores (4 μm diameter) are reactive-ion etched through the top SiO(2) and SiN layers of the waveguides, leaving a thin SiN membrane above the hollow core. Nanopores are formed in the SiN membranes using a focused ion-beam etch process that provides control over the pore size. Openings as small as 20 nm in diameter are created. Optical loss measurements indicate that micropores did not significantly alter the loss along the waveguide.

  2. Investigation of the interfacial properties of polyurethane/carbon nanotube hybrid composites: A molecular dynamics study

    NASA Astrophysics Data System (ADS)

    Goclon, Jakub; Panczyk, Tomasz; Winkler, Krzysztof

    2018-03-01

    Considering the varied applications of hybrid polymer/carbon nanotube composites and the constant progress in the synthesis methods of such materials, we report a theoretical study of interfacial layer formation between pristine single-wall carbon nanotubes (SWCNTs) and polyurethane (PU) using molecular dynamic simulations. We vary the SWCNT diameter and the number of PU chains to examine various PU-SWCNT interaction patterns. Our simulations indicate the important role of intra-chain forces in PU. No regular polymeric structures could be identified on the carbon nanotube surface during the simulations. We find that increasing the SWCNT diameter results in stronger polymer binding. However, higher surface loadings of PU lead to stronger interpenetration by the polymeric segments; this effect is more apparent for SWCNTs with small diameters. Our core finding is that the attached PU binds most strongly to the carbon nanotubes with the largest diameters. Polymer dynamics reveal the loose distribution of PU chains in these systems.

  3. ZnO core spike particles and nano-networks and their wide range of applications

    NASA Astrophysics Data System (ADS)

    Wille, S.; Mishra, Y. K.; Gedamu, D.; Kaps, S.; Jin, X.; Koschine, T.; Bathnagar, A.; Adelung, R.

    2011-05-01

    In our approach we are producing a polymer composite material with ZnO core spike particles as concave fillers. The core spike particles are synthesized by a high throughput method. Using PDMS (Polydimethylsiloxane) as a matrix material the core spike particles achieve not only a high mechanical reinforcement but also influence other material properties in a very interesting way, making such a composite very interesting for a wide range of applications. In a very similar synthesis route a nanoscopic ZnO-network is produced. As a ceramic this network can withstand high temperatures like 1300 K. In addition this material is quite elastic. To find a material with these two properties is a really difficult task, as polymers tend to decompose already at lower temperatures and metals melt. Especially under ambient conditions, often oxygen creates a problem for metals at these temperatures. If this material is at the same time a semiconductor, it has a high potential as a multifunctional material. Ceramic or classical semiconductors like III-V or IIVI type are high temperature stable, but typically brittle. This is different on the nanoscale. Even semiconductor wires like silicon with a very small diameter do not easily built up enough stress that leads to a failure while being bent, because in a first order approximation the maximum stress of a fiber scales with its diameter.

  4. Core-shell biopolymer nanoparticle delivery systems: synthesis and characterization of curcumin fortified zein-pectin nanoparticles.

    PubMed

    Hu, Kun; Huang, Xiaoxia; Gao, Yongqing; Huang, Xulin; Xiao, Hang; McClements, David Julian

    2015-09-01

    Biopolymer core-shell nanoparticles were fabricated using a hydrophobic protein (zein) as the core and a hydrophilic polysaccharide (pectin) as the shell. Particles were prepared by coating cationic zein nanoparticles with anionic pectin molecules using electrostatic deposition (pH 4). The core-shell nanoparticles were fortified with curcumin (a hydrophobic bioactive molecule) at a high loading efficiency (>86%). The resulting nanoparticles were spherical, relatively small (diameter ≈ 250 nm), and had a narrow size distribution (polydispersity index ≈ 0.24). The encapsulated curcumin was in an amorphous (rather than crystalline form) as detected by differential scanning calorimetry (DSC). Fourier transform infrared (FTIR) and Raman spectra indicated that the encapsulated curcumin interacted with zein mainly through hydrophobic interactions. The nanoparticles were converted into a powdered form that had good water-dispersibility. These core-shell biopolymer nanoparticles could be useful for incorporating curcumin into functional foods and beverages, as well as dietary supplements and pharmaceutical products. Copyright © 2015 Elsevier Ltd. All rights reserved.

  5. The Tom Core Complex

    PubMed Central

    Ahting, Uwe; Thun, Clemens; Hegerl, Reiner; Typke, Dieter; Nargang, Frank E.; Neupert, Walter; Nussberger, Stephan

    1999-01-01

    Translocation of nuclear-encoded preproteins across the outer membrane of mitochondria is mediated by the multicomponent transmembrane TOM complex. We have isolated the TOM core complex of Neurospora crassa by removing the receptors Tom70 and Tom20 from the isolated TOM holo complex by treatment with the detergent dodecyl maltoside. It consists of Tom40, Tom22, and the small Tom components, Tom6 and Tom7. This core complex was also purified directly from mitochondria after solubilization with dodecyl maltoside. The TOM core complex has the characteristics of the general insertion pore; it contains high-conductance channels and binds preprotein in a targeting sequence-dependent manner. It forms a double ring structure that, in contrast to the holo complex, lacks the third density seen in the latter particles. Three-dimensional reconstruction by electron tomography exhibits two open pores traversing the complex with a diameter of ∼2.1 nm and a height of ∼7 nm. Tom40 is the key structural element of the TOM core complex. PMID:10579717

  6. Characterization of Three-Stream Jet Flow Fields

    NASA Technical Reports Server (NTRS)

    Henderson, Brenda S.; Wernet, Mark P.

    2016-01-01

    Flow-field measurements were conducted on single-, dual- and three-stream jets using two-component and stereo Particle Image Velocimetry (PIV). The flow-field measurements complimented previous acoustic measurements. The exhaust system consisted of externally-plugged, externally-mixed, convergent nozzles. The study used bypass-to-core area ratios equal to 1.0 and 2.5 and tertiary-to-core area ratios equal to 0.6 and 1.0. Axisymmetric and offset tertiary nozzles were investigated for heated and unheated high-subsonic conditions. Centerline velocity decay rates for the single-, dual- and three-stream axisymmetric jets compared well when axial distance was normalized by an equivalent diameter based on the nozzle system total exit area. The tertiary stream had a greater impact on the mean axial velocity for the small bypass-to-core area ratio nozzles than for large bypass-to-core area ratio nozzles. Normalized turbulence intensities were similar for the single-, dual-, and three-stream unheated jets due to the small difference (10 percent) in the core and bypass velocities for the dual-stream jets and the low tertiary velocity (50 percent of the core stream) for the three-stream jets. For heated jet conditions where the bypass velocity was 65 percent of the core velocity, additional regions of high turbulence intensity occurred near the plug tip which were not present for the unheated jets. Offsetting the tertiary stream moved the peak turbulence intensity levels upstream relative to those for all axisymmetric jets investigated.

  7. Characterization of Three-Stream Jet Flow Fields

    NASA Technical Reports Server (NTRS)

    Henderson, Brenda S.; Wernet, Mark P.

    2016-01-01

    Flow-field measurements were conducted on single-, dual- and three-stream jets using two-component and stereo Particle Image Velocimetry (PIV). The flow-field measurements complimented previous acoustic measurements. The exhaust system consisted of externally-plugged, externally-mixed, convergent nozzles. The study used bypass-to-core area ratios equal to 1.0 and 2.5 and tertiary-to-core area ratios equal to 0.6 and 1.0. Axisymmetric and offset tertiary nozzles were investigated for heated and unheated high-subsonic conditions. Centerline velocity decay rates for the single-, dual- and three-stream axisymmetric jets compared well when axial distance was normalized by an equivalent diameter based on the nozzle system total exit area. The tertiary stream had a greater impact on the mean axial velocity for the small bypass-to-core area ratio nozzles than for large bypass-to-core area ratio nozzles. Normalized turbulence intensities were similar for the single-, dual-, and three-stream unheated jets due to the small difference (10%) in the core and bypass velocities for the dual-stream jets and the low tertiary velocity (50% of the core stream) for the three-stream jets. For heated jet conditions where the bypass velocity was 65% of the core velocity, additional regions of high turbulence intensity occurred near the plug tip which were not present for the unheated jets. Offsetting the tertiary stream moved the peak turbulence intensity levels upstream relative to those for all axisymmetric jets investigated.

  8. 75 FR 37876 - Buy America Waiver Notification

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-06-30

    ... hollow core threaded share anchor rods in construction of Federal-aid project X-STP-1525 (004) in Oregon... is appropriate for the use of non- domestic 1'' diameter hollow core threaded share anchor rods for... to issue a waiver for the 1'' diameter hollow core threaded share anchor rods ( http://www.fhwa.dot...

  9. Numerical and analytical simulation of the production process of ZrO2 hollow particles

    NASA Astrophysics Data System (ADS)

    Safaei, Hadi; Emami, Mohsen Davazdah

    2017-12-01

    In this paper, the production process of hollow particles from the agglomerated particles is addressed analytically and numerically. The important parameters affecting this process, in particular, the initial porosity level of particles and the plasma gun types are investigated. The analytical model adopts a combination of quasi-steady thermal equilibrium and mechanical balance. In the analytical model, the possibility of a solid core existing in agglomerated particles is examined. In this model, a range of particle diameters (50μm ≤ D_{p0} ≤ 160 μ m) and various initial porosities ( 0.2 ≤ p ≤ 0.7) are considered. The numerical model employs the VOF technique for two-phase compressible flows. The production process of hollow particles from the agglomerated particles is simulated, considering an initial diameter of D_{p0} = 60 μm and initial porosity of p = 0.3, p = 0.5, and p = 0.7. Simulation results of the analytical model indicate that the solid core diameter is independent of the initial porosity, whereas the thickness of the particle shell strongly depends on the initial porosity. In both models, a hollow particle may hardly develop at small initial porosity values ( p < 0.3), while the particle disintegrates at high initial porosity values ( p > 0.6.

  10. Impact of thorium based molten salt reactor on the closure of the nuclear fuel cycle

    NASA Astrophysics Data System (ADS)

    Jaradat, Safwan Qasim Mohammad

    Molten salt reactor (MSR) is one of six reactors selected by the Generation IV International Forum (GIF). The liquid fluoride thorium reactor (LFTR) is a MSR concept based on thorium fuel cycle. LFTR uses liquid fluoride salts as a nuclear fuel. It uses 232Th and 233U as the fertile and fissile materials, respectively. Fluoride salt of these nuclides is dissolved in a mixed carrier salt of lithium and beryllium (FLiBe). The objective of this research was to complete feasibility studies of a small commercial thermal LFTR. The focus was on neutronic calculations in order to prescribe core design parameter such as core size, fuel block pitch (p), fuel channel radius, fuel path, reflector thickness, fuel salt composition, and power. In order to achieve this objective, the applicability of Monte Carlo N-Particle Transport Code (MCNP) to MSR modeling was verified. Then, a prescription for conceptual small thermal reactor LFTR and relevant calculations were performed using MCNP to determine the main neutronic parameters of the core reactor. The MCNP code was used to study the reactor physics characteristics for the FUJI-U3 reactor. The results were then compared with the results obtained from the original FUJI-U3 using the reactor physics code SRAC95 and the burnup analysis code ORIPHY2. The results were comparable with each other. Based on the results, MCNP was found to be a reliable code to model a small thermal LFTR and study all the related reactor physics characteristics. The results of this study were promising and successful in demonstrating a prefatory small commercial LFTR design. The outcome of using a small core reactor with a diameter/height of 280/260 cm that would operate for more than five years at a power level of 150 MWth was studied. The fuel system 7LiF - BeF2 - ThF4 - UF4 with a (233U/ 232Th) = 2.01 % was the candidate fuel for this reactor core.

  11. Airfoil gust response and the sound produced by airifoil-vortex interaction

    NASA Technical Reports Server (NTRS)

    Amiet, R. K.

    1986-01-01

    This paper contributes to the understanding of the noise generation process of an airfoil encountering an unsteady upwash. By using a fast Fourier transform together with accurate airfoil response functions, the lift-time waveform for an airfoil encountering a delta function gust (the indicial function) is calculated for a flat plate airfoil in a compressible flow. This shows the interesting property that the lift is constant until the generated acoustic wave reaches the trailing edge. Expressions are given for the magnitude of this constant and for the pressure distribution on the airfoil during this time interval. The case of an airfoil cutting through a line vortex is also analyzed. The pressure-time waveform in the far field is closely related to the left-time waveform for the above problem of an airfoil entering a delta function gust. The effects of varying the relevant parameters in the problem are studied, including the observed position, the core diameter of the vortex, the vortex orientation and the airfoil span. The far field sound varies significantly with observer position, illustrating the importance of non-compactness effects. Increasing the viscous core diameter tends to smooth the pressure-time waveform. For small viscous core radius and infinite span, changing the vortex orientation changes only the amplitude of the pressure-time waveform, and not the shape.

  12. Trapping and Propelling Microparticles at Long Range by Using an Entirely Stripped and Slightly Tapered No-Core Optical Fiber

    PubMed Central

    Sheu, Fang-Wen; Huang, Yen-Si

    2013-01-01

    A stripped no-core optical fiber with a 125 μm diameter was transformed into a symmetric and unbroken optical fiber that tapers slightly to a 45-μm-diameter waist. The laser light can be easily launched into the no-core optical fiber. The enhanced evanescent wave of the slightly tapered no-core optical fiber can attract nearby 5-μm-diameter polystyrene microparticles onto the surface of the tapered multimode optical fiber within fast flowing fluid and propel the trapped particles in the direction of the light propagation to longer delivery range than is possible using a slightly tapered telecom single-mode optical fiber. PMID:23449118

  13. Trapping and propelling microparticles at long range by using an entirely stripped and slightly tapered no-core optical fiber.

    PubMed

    Sheu, Fang-Wen; Huang, Yen-Si

    2013-02-28

    A stripped no-core optical fiber with a 125 µm diameter was transformed into a symmetric and unbroken optical fiber that tapers slightly to a 45-µm-diameter waist. The laser light can be easily launched into the no-core optical fiber. The enhanced evanescent wave of the slightly tapered no-core optical fiber can attract nearby 5-µm-diameter polystyrene microparticles onto the surface of the tapered multimode optical fiber within fast flowing fluid and propel the trapped particles in the direction of the light propagation to longer delivery range than is possible using a slightly tapered telecom single-mode optical fiber.

  14. Fiber up-tapering and down-tapering for low-loss coupling between anti-resonant hollow-core fiber and solid-core fiber

    NASA Astrophysics Data System (ADS)

    Zhang, Naiqian; Wang, Zefeng; Xi, Xiaoming

    2017-10-01

    In this paper, we demonstrate a novel method for the low-loss coupling between solid-core multi-mode fibers (MMFs) and anti-resonant hollow-core fibers (AR-HCFs). The core/cladding diameter of the MMF is 50/125μm and the mode field diameter of the AR-HCFs are 33.3μm and 71.2μm of the ice-cream type AR-HCFs and the non-node type ARHCFs, respectively. In order to match the mode field diameters of these two specific AR-HCFs, the mode field diameter of the MMFs is increased or decreased by up-tapering or down-tapering the MMFs. Then, according to the principle of coupled fiber mode matching, the optimal diameter of tapered fiber for low-loss coupling is calculated. Based on beam propagation method, the calculated coupling losses without tapering process are 0.31dB and 0.89dB, respectively for a MMF-HCF-MMF structure of the ice-cream type AR-HCFs and the non-node type AR-HCFs. These values can be reduced to 0.096dB and 0.047dB when the outer diameters of the MMF are down-tapered to 116μm and up-tapered to 269μm, respectively. What's more, these results can also be verified by existing experiments.

  15. Core-Exsolved SiO2 Dispersal in the Earth's Mantle

    NASA Astrophysics Data System (ADS)

    Helffrich, George; Ballmer, Maxim D.; Hirose, Kei

    2018-01-01

    SiO2 may have been expelled from the core directly following core formation in the early stages of Earth's accretion and onward through the present day. On account of SiO2's low density with respect to both the core and the lowermost mantle, we examine the process of SiO2 accumulation at the core-mantle boundary (CMB) and its incorporation into the mantle by buoyant rise. Today, if SiO2 is 100-10,000 times more viscous than lower mantle material, the dimensions of SiO2 diapirs formed by the viscous Rayleigh-Taylor instability at the CMB would cause them to be swept into the mantle as inclusions of 100 m-10 km diameter. Under early Earth conditions of rapid heat loss after core formation, SiO2 diapirs of ˜1 km diameter could have risen independently of mantle flow to their level of neutral buoyancy in the mantle, trapping them there due to a combination of intrinsically high viscosity and neutral buoyancy. We examine the SiO2 yield by assuming Si + O saturation at the conditions found at the base of a magma ocean and find that for a range of conditions, dispersed bodies could reach as high as 8.5 vol % in parts of the lower mantle. At such low concentration, their effect on aggregate seismic wave speeds is within observational seismology uncertainty. However, their presence can account for small-scale scattering in the lower mantle due to the bodies' large-velocity contrast. We conclude that the shallow lower mantle (700-1,500 km depth) could harbor SiO2 released in early Earth times.

  16. A tunable single-polarization photonic crystal fiber filter based on surface plasmon resonance

    NASA Astrophysics Data System (ADS)

    Zhang, Shuhuan; Li, Jianshe; Li, Shuguang; Liu, Qiang; Liu, Yingchao; Zhang, Zhen; Wang, Yujun

    2018-06-01

    A tunable single polarizing filter is proposed by selectively coating gold film on the air holes of photonic crystal fiber (PCF). The polarization properties of the PCF filter are evaluated by the finite-element method. Simulation results show that the loss of y-polarized core mode at 1250 and 1550 nm is 136.23 and 839.73 dB/cm, respectively. Furthermore, we innovatively combine stable modulation with flexible modulation. To be specific, the resonance wavelengths are slowly controlled in a small wavelength range by altering the diameter of the air-hole-coated gold film, while the resonance wavelengths are flexibly controlled in a wide wavelength range by altering the thickness of the gold film or the diameter of the small air holes. When the length of the PCF is 500 µm, the bandwidth of extinction ratio greater than - 20 dB is only 60 nm at the communication window of 1550 nm. It is beneficial to fabricate a narrow-band polarization filter.

  17. PMMA/PS coaxial electrospinning: a statistical analysis on processing parameters

    NASA Astrophysics Data System (ADS)

    Rahmani, Shahrzad; Arefazar, Ahmad; Latifi, Masoud

    2017-08-01

    Coaxial electrospinning, as a versatile method for producing core-shell fibers, is known to be very sensitive to two classes of influential factors including material and processing parameters. Although coaxial electrospinning has been the focus of many studies, the effects of processing parameters on the outcomes of this method have not yet been well investigated. A good knowledge of the impacts of processing parameters and their interactions on coaxial electrospinning can make it possible to better control and optimize this process. Hence, in this study, the statistical technique of response surface method (RSM) using the design of experiments on four processing factors of voltage, distance, core and shell flow rates was applied. Transmission electron microscopy (TEM), scanning electron microscopy (SEM), oil immersion and Fluorescent microscopy were used to characterize fiber morphology. The core and shell diameters of fibers were measured and the effects of all factors and their interactions were discussed. Two polynomial models with acceptable R-squares were proposed to describe the core and shell diameters as functions of the processing parameters. Voltage and distance were recognized as the most significant and influential factors on shell diameter, while core diameter was mainly under the influence of core and shell flow rates besides the voltage.

  18. Axial contraction in etched optical fiber due to internal stress reduction.

    PubMed

    Lim, Kok-Sing; Yang, Hang-Zhou; Chong, Wu-Yi; Cheong, Yew-Ken; Lim, Chin-Hong; Ali, Norfizah M; Ahmad, Harith

    2013-02-11

    When an optical fiber is dipped in an etching solution, the internal stress profile in the fiber varies with the fiber diameter. We observed a physical contraction as much as 0.2% in the fiber axial dimension when the fiber was reduced from its original diameter to ~6 µm through analysis using high resolution microscope images of the grating period of an etched FBG at different fiber diameters. This axial contraction is related to the varying axial stress profile in the fiber when the fiber diameter is reduced. On top of that, the refractive index of fiber core increases with reducing fiber diameter due to stress-optic effect. The calculated index increment is as much as 1.8 × 10(-3) at the center of fiber core after the diameter is reduced down to ~6 µm. In comparison with the conventional model that assumes constant grating period and neglects the variation in stress-induced index change in fiber core, our proposed model indicates a discrepancy as much as 3nm in Bragg wavelength at a fiber diameter of ~6 µm.

  19. Experimental investigation on the high-order modes in supercontinuum generation from step-index As-S fibers

    NASA Astrophysics Data System (ADS)

    Chen, Peng; Xue, Zugang; Tian, Youmei; Zhao, Zheming; Wang, Xunsi; Liu, Zijun; Zhang, Peiqing; Dai, Shixun; Nie, Qiuhua; Wang, Rongping

    2018-06-01

    Two kinds of step-index As-S fibers have been fabricated by an isolated extrusion method with a numerical aperture (NA) of 0.52, but with different core size of 10 or 50 µm. With a femtosecond laser pumping, their supercontinnum (SC) generation spectra were recorded in order to testify the effect of high-order modes on SC generation. The spectra spanning from 1.0 to 6.7 µm and from 1.5 to 8.6 µm can be obtained in a 16-cm-long fiber with 10 µm-core diameter pumping by central wavelength of 2.9 and 4.0 µm, respectively. The results show that high-order modes would deplete the spectra spanning in red-shifting part. The SC generation in small-core fiber is much more efficient than that in large-core fiber. This is the first comparative investigation on the SC generation from the quasi single- and multi-mode ChG fibers under the same conditions.

  20. Rydberg atoms in hollow-core photonic crystal fibres.

    PubMed

    Epple, G; Kleinbach, K S; Euser, T G; Joly, N Y; Pfau, T; Russell, P St J; Löw, R

    2014-06-19

    The exceptionally large polarizability of highly excited Rydberg atoms-six orders of magnitude higher than ground-state atoms--makes them of great interest in fields such as quantum optics, quantum computing, quantum simulation and metrology. However, if they are to be used routinely in applications, a major requirement is their integration into technically feasible, miniaturized devices. Here we show that a Rydberg medium based on room temperature caesium vapour can be confined in broadband-guiding kagome-style hollow-core photonic crystal fibres. Three-photon spectroscopy performed on a caesium-filled fibre detects Rydberg states up to a principal quantum number of n=40. Besides small energy-level shifts we observe narrow lines confirming the coherence of the Rydberg excitation. Using different Rydberg states and core diameters we study the influence of confinement within the fibre core after different exposure times. Understanding these effects is essential for the successful future development of novel applications based on integrated room temperature Rydberg systems.

  1. Small Angle Neutron-Scattering Studies of the Core Structure of Intact Neurosecretory Vesicles.

    NASA Astrophysics Data System (ADS)

    Krueger, Susan Takacs

    Small angle neutron scattering (SANS) was used to study the state of the dense cores within intact neurosecretory vesicles. These vesicles transport the neurophysin proteins, along with their associated hormones, oxytocin or vasopressin, from the posterior pituitary gland to the bloodstream, where the entire vesicle contents are released. Knowledge of the vesicle core structure is important in developing an understanding of this release mechanism. Since the core constituents exist in a dense state at concentrations which cannot be reproduced (in solution) in the laboratory, a new method was developed to determine the core structure from SANS experiments performed on intact neurosecretory vesicles. These studies were complemented by biochemical assays performed to determine the role, if any, played by phospholipids in the interactions between the core constituents. H_2O/D_2 O ratio in the solvent can be adjusted, using the method of contrast variation, such that the scattering due to the vesicle membranes is minimized, thus emphasizing the scattering originating from the cores. The applicability of this method for examining the interior of biological vesicles was tested by performing an initial study on human red blood cells, which are similar in structure to other biological vesicles. Changes in intermolecular hemoglobin interactions, occurring when the ionic strength of the solvent was varied or when the cells were deoxygenated, were examined. The results agreed with those expected for dense protein solutions, indicating that the method developed was suitable for the study of hemoglobin within the cells. Similar SANS studies were then performed on intact neurosecretory vesicles. The experimental results were inconsistent with model calculations which assumed that the cores consisted of small, densely-packed particles or large, globular aggregates. Although a unique model could not be determined, the data suggest that the core constituents form long aggregates of varying cross-sectional diameters. The biochemical experiments not only confirmed the ability of the core constituents to form large aggregates but also established that phospholipids do not play a role in this aggregate formation.

  2. Monitoring of vegetation response to elk population and habitat management in Rocky Mountain National Park, 2008–14

    USGS Publications Warehouse

    Zeigenfuss, Linda C.; Johnson, Therese L.

    2015-12-17

    Increases in the number of small-diameter, tree-sized (stems greater than 2.5 meter height) aspen stems were observed but only inside fences that excluded ungulates. In unfenced areas, stand structure was stagnant, with many medium- and large-diameter (older) stems and no replacement of small-diameter stems. By 2013, aspen saplings (stems less than or equal to 2.5 meter height) were recruiting on 29 percent of sampled sites, an increase from 13 percent of sites at baseline, but this was mainly due to growth inside fences. Upland herbaceous offtake dropped below baseline levels (61 percent) on both core and noncore winter range in 2010–14. Less than 10 percent of the upland areas had intense herbivory (greater than 85 percent offtake), and less than 30 percent of the landscape had offtake greater than 70 percent after 2009. Offtake levels in 2013 and 2014 indicated an increase in grazing pressure on upland sites compared to 2010–12 levels, but this change may have been in response to loss of large patches of both herbaceous and woody forage in Moraine Park following the 2012 Fern Lake Fire. Winter willow offtake remained steady from 2009 to 2014, and although there were no substantial increases in offtake, there were also no consistent declines. Winter-range willow offtake was below the baseline level of 35 percent only in 2013 and 2014. Willow heights have stayed at or above baseline levels of 0.9 meter. Average heights of willow increased compared to baseline measures within fenced habitat on the core winter range and on noncore (all unfenced) winter range. Willow cover increased at least 75 percent compared to baseline within core winter-range fenced areas and roughly 25 percent in noncore winter range. Overall, during the first 5 years of implementation, the EVMP at Rocky Mountain National Park seems to be making steady progress toward the vegetation objectives set out by the EVMP. Habitat fencing has been the most effective means of improving aspen and willow habitat conditions.

  3. Development of a fuel-rod simulator and small-diameter thermocouples for high-temperature, high-heat-flux tests in the Gas-Cooled Fast Reactor Core Flow Test Loop

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    McCulloch, R.W.; MacPherson, R.E.

    1983-03-01

    The Core Flow Test Loop was constructed to perform many of the safety, core design, and mechanical interaction tests in support of the Gas-Cooled Fast Reactor (GCFR) using electrically heated fuel rod simulators (FRSs). Operation includes many off-normal or postulated accident sequences including transient, high-power, and high-temperature operation. The FRS was developed to survive: (1) hundreds of hours of operation at 200 W/cm/sup 2/, 1000/sup 0/C cladding temperature, and (2) 40 h at 40 W/cm/sup 2/, 1200/sup 0/C cladding temperature. Six 0.5-mm type K sheathed thermocouples were placed inside the FRS cladding to measure steady-state and transient temperatures through cladmore » melting at 1370/sup 0/C.« less

  4. Study of High-Efficiency Motors Using Soft Magnetic Cores

    NASA Astrophysics Data System (ADS)

    Tokoi, Hirooki; Kawamata, Shoichi; Enomoto, Yuji

    We have been developed a small and highly efficient axial gap motor whose stator core is made of a soft magnetic core. First, the loss sensitivities to various motor design parameters were evaluated using magnetic field analysis. It was found that the pole number and core dimensions had low sensitivity (≤ 2.2dB) in terms of the total loss, which is the sum of the copper loss and the iron losses in the stator core and the rotor yoke respectively. From this, we concluded that to improve the motor efficiency, it is essential to reduce the iron loss in the rotor yoke and minimize other losses. With this in mind, a prototype axial gap motor is manufactured and tested. The motor has four poles and six slots. The motor is 123mm in diameter and the axial length is 47mm. The rotor has parallel magnetized magnets and a rotor yoke with magnetic steel sheets. The maximum measured motor efficiency is 93%. This value roughly agrees with the maximum calculated efficiency of 95%.

  5. Composite casting/bonding construction of an air-cooled, high temperature radial turbine wheel

    NASA Technical Reports Server (NTRS)

    Hammer, A. N.; Aigret, G.; Rodgers, C.; Metcalfe, A. G.

    1983-01-01

    A composite casting/bonding technique has been developed for the fabrication of a unique air-cooled, high temperature radial inflow turbine wheel design applicable to auxilliary power units with small rotor diameters and blade entry heights. The 'split blade' manufacturing procedure employed is an alternative to complex internal ceramic coring. Attention is given to both aerothermodynamic and structural design, of which the latter made advantageous use of the exploration of alternative cooling passage configurations through CAD/CAM system software modification.

  6. Particle levitation and guidance in hollow-core photonic crystal fiber.

    PubMed

    Benabid, Fetah; Knight, J; Russell, P

    2002-10-21

    We report the guidance of dry micron-sized dielectric particles in hollow core photonic crystal fiber. The particles were levitated in air and then coupled to the air-core of the fiber using an Argon ion laser beam operating at a wavelength of 514 nm. The diameter of the hollow core of the fiber is 20 m . A laser power of 80 mW was sufficient to levitate a 5 m diameter polystyrene sphere and guide it through a ~150 mm long hollow-core crystal photonic fiber. The speed of the guided particle was measured to be around 1 cm/s.

  7. 13.1 Foot Diameter Fluted-Core Sandwich Composite Test Article

    NASA Image and Video Library

    2013-09-26

    White light shape and measurement of a 13.1 Foot diameter fluted-core sandwich composite test article designed by LaRC and fabricated by Boeing Under Space Act Agreement SAA1-737, Annex 14. to be tested in LaRC's combined Loads Testing System (COLTS).

  8. 13.1 Foot Diameter Fluted-Core Sandwich Composite Test Article

    NASA Image and Video Library

    2013-09-25

    White light shape and measurement of a 13.1 Foot diameter fluted-core sandwich composite test article designed by LaRC and fabricated by Boeing Under Space Act Agreement SAA1-737, Annex 14. to be tested in LaRC's combined Loads Testing System (COLTS).

  9. Magnetization reversal in circular vortex dots of small radius.

    PubMed

    Goiriena-Goikoetxea, M; Guslienko, K Y; Rouco, M; Orue, I; Berganza, E; Jaafar, M; Asenjo, A; Fernández-Gubieda, M L; Fernández Barquín, L; García-Arribas, A

    2017-08-10

    We present a detailed study of the magnetic behavior of Permalloy (Ni 80 Fe 20 alloy) circular nanodots with small radii (30 nm and 70 nm) and different thicknesses (30 nm or 50 nm). Despite the small size of the dots, the measured hysteresis loops manifestly display the features of classical vortex behavior with zero remanence and lobes at high magnetic fields. This is remarkable because the size of the magnetic vortex core is comparable to the dot diameter, as revealed by magnetic force microscopy and micromagnetic simulations. The dot ground states are close to the border of the vortex stability and, depending on the dot size, the magnetization distribution combines attributes of the typical vortex, single domain states or even presents features resembling magnetic skyrmions. An analytical model of the dot magnetization reversal, accounting for the large vortex core size, is developed to explain the observed behavior, providing a rather good agreement with the experimental results. The study extends the understanding of magnetic nanodots beyond the classical vortex concept (where the vortex core spins have a negligible influence on the magnetic behavior) and can therefore be useful for improving emerging spintronic applications, such as spin-torque nano-oscillators. It also delimits the feasibility of producing a well-defined vortex configuration in sub-100 nm dots, enabling the intracellular magneto-mechanical actuation for biomedical applications.

  10. Core-exsolved SiO2 Dispersal in the Earth's Mantle

    NASA Astrophysics Data System (ADS)

    Helffrich, G. R.; Ballmer, M.; Hirose, K.

    2017-12-01

    SiO2 may have been expelled from the core following its formation in the early stages of Earth's accretion and onwards through the present day. On account of SiO2's low density with respect to both the core and the lowermost mantle, we examine the process of SiO2 accumulation at the core-mantle boundary (CMB) and its incorporation into the mantle by buoyant rise. Today, the if SiO2 is 100-10000 times more viscous than lower mantle material, the dimensions of SiO2 diapirs formed by the viscous Rayleigh-Taylor instability at the CMB would cause them to be swept into the mantle as inclusions of 100 m - 10 km diameter. Under early Earth conditions of rapid heat loss after core formation, SiO2 diapirs of 5-80 km diameter could have risen independently of mantle flow to their level of neutral buoyancy in the mantle, trapping them there due to a combination of high viscosity and neutral buoyancy. We examine the SiO2 yield by assuming Si+O saturation at the conditions found at the base of a magma ocean and find that for a range of conditions, dispersed bodies could reach as high as 2 volume percent in shallow parts of the lower mantle, with their abundance decreasing with depth. At such low concentrations, their effect on aggregate seismic wavespeeds would be within the uncertainty of the radial Earth model PREM. However, their presence would be revealed by small-scale scattering in the lower mantle due to the bodies' large velocity contrast. We conclude that the shallow lower mantle (700-1500 km depth) could harbor SiO2 released in early Earth times.

  11. Exchange coupling and microwave absorption in core/shell-structured hard/soft ferrite-based CoFe2O4/NiFe2O4 nanocapsules

    NASA Astrophysics Data System (ADS)

    Feng, Chao; Liu, Xianguo; Or, Siu Wing; Ho, S. L.

    2017-05-01

    Core/shell-structured, hard/soft spinel-ferrite-based CoFe2O4/NiFe2O4 (CFO/NFO) nanocapsules with an average diameter of 17 nm are synthesized by a facile two-step hydrothermal process using CFO cores of ˜15 nm diameter as the hard magnetic phase and NFO shells of ˜1 nm thickness as the soft magnetic phase. The single-phase-like hysteresis loop with a high remnant-to-saturation magnetization ratio of 0.7, together with a small grain size of ˜16 nm, confirms the existence of exchange-coupling interaction between the CFO cores and the NFO shells. The effect of hard/soft exchange coupling on the microwave absorption properties is studied. Comparing to CFO and NFO nanoparticles, the finite-size NFO shells and the core/shell structure enable a significant reduction in electric resistivity and an enhancement in dipole and interfacial polarizations in the CFO/NFO nanocapsules, resulting in an obvious increase in dielectric permittivity and loss in the whole S-Ku bands of microwaves of 2-18 GHz, respectively. The exchange-coupling interaction empowers a more favorable response of magnetic moment to microwaves, leading to enhanced exchange resonances in magnetic permeability and loss above 10 GHz. As a result, strong absorption, as characterized by a large reflection loss (RL) of -20.1 dB at 9.7 GHz for an absorber thickness of 4.5 mm as well as a broad effective absorption bandwidth (for RL<-10 dB) of 8.4 GHz (7.8-16.2 GHz) at an absorber thickness range of 3.0-4.5 mm, is obtained.

  12. The effects of substrate size, surface area, and density on coat thickness of multi-particulate dosage forms.

    PubMed

    Heinicke, Grant; Matthews, Frank; Schwartz, Joseph B

    2005-01-01

    Drugs layering experiments were performed in a fluid bed fitted with a rotor granulator insert using diltiazem as a model drug. The drug was applied in various quantities to sugar spheres of different mesh sizes to give a series of drug-layered sugar spheres (cores) of different potency, size, and weight per particle. The drug presence lowered the bulk density of the cores in proportion to the quantity of added drug. Polymer coating of each core lot was performed in a fluid bed fitted with a Wurster insert. A series of polymer-coated cores (pellets) was removed from each coating experiment. The mean diameter of each core and each pellet sample was determined by image analysis. The rate of change of diameter on polymer addition was determined for each starting size of core and compared to calculated values. The core diameter was displaced from the line of best fit through the pellet diameter data. Cores of different potency with the same size distribution were made by layering increasing quantities of drug onto sugar spheres of decreasing mesh size. Equal quantities of polymer were applied to the same-sized core lots and coat thickness was measured. Weight/weight calculations predict equal coat thickness under these conditions, but measurable differences were found. Simple corrections to core charge weight in the Wurster insert were successfully used to manufacture pellets having the same coat thickness. The sensitivity of the image analysis technique in measuring particle size distributions (PSDs) was demonstrated by measuring a displacement in PSD after addition of 0.5% w/w talc to a pellet sample.

  13. Study of the effect of varying core diameter, shell thickness and strain velocity on the tensile properties of single crystals of Cu-Ag core-shell nanowire using molecular dynamics simulations

    NASA Astrophysics Data System (ADS)

    Sarkar, Jit; Das, D. K.

    2018-01-01

    Core-shell type nanostructures show exceptional properties due to their unique structure having a central solid core of one type and an outer thin shell of another type which draw immense attention among researchers. In this study, molecular dynamics simulations are carried out on single crystals of copper-silver core-shell nanowires having wire diameter ranging from 9 to 30 nm with varying core diameter, shell thickness, and strain velocity. The tensile properties like yield strength, ultimate tensile strength, and Young's modulus are studied and correlated by varying one parameter at a time and keeping the other two parameters constant. The results obtained for a fixed wire size and different strain velocities were extrapolated to calculate the tensile properties like yield strength and Young's modulus at standard strain rate of 1 mm/min. The results show ultra-high tensile properties of copper-silver core-shell nanowires, several times than that of bulk copper and silver. These copper-silver core-shell nanowires can be used as a reinforcing agent in bulk metal matrix for developing ultra-high strength nanocomposites.

  14. Monitoring of NMR porosity changes in the full-size core salvage through the drying process

    NASA Astrophysics Data System (ADS)

    Fattakhov, Artur; Kosarev, Victor; Doroginitskii, Mikhail; Skirda, Vladimir

    2015-04-01

    Currently the principle of nuclear magnetic resonance (NMR) is one of the most popular technologies in the field of borehole geophysics and core analysis. Results of NMR studies allow to calculate the values of the porosity and permeability of sedimentary rocks with sufficient reliability. All standard tools for the study of core salvage on the basis of NMR have significant limitations: there is considered only long relaxation times corresponding to the mobile formation fluid. Current trends in energy obligate to move away from conventional oil to various alternative sources of energy. One of these sources are deposits of bitumen and high-viscosity oil. In Kazan (Volga Region) Federal University (Russia) there was developed a mobile unit for the study of the full-length core salvage by the NMR method ("NMR-Core") together with specialists of "TNG-Group" (a company providing maintenance services to oil companies). This unit is designed for the study of core material directly on the well, after removing it from the core receiver. The maximum diameter of the core sample may be up to 116 mm, its length (or length of the set of samples) may be up to 1000 mm. Positional precision of the core sample relative to the measurement system is 1 mm, and the spatial resolution along the axis of the core is 10 mm. Acquisition time of the 1 m core salvage varies depending on the mode of research and is at least 20 minutes. Furthermore, there is implemented a special investigation mode of the core samples with super small relaxation times (for example, heavy oil) is in the tool. The aim of this work is tracking of the NMR porosity changes in the full-size core salvage in time. There was used a water-saturated core salvage from the shallow educational well as a sample. The diameter of the studied core samples is 93 mm. There was selected several sections length of 1m from the 200-meter coring interval. The studied core samples are being measured several times. The time interval between the measurements is from 1 hour to 48 hours. Making the measurements it possible to draw conclusions about that the processes of NMR porosity changes in time as a result of evaporation of the part of fluid from the surface layer of the core salvage and suggest a core analysis technique directly on the well. This work is supported by the grant of Ministry of Education and Science of the Russian Federation (project No. 02.G25.31.0029).

  15. Studies on low-loss coupling of non-node anti-resonant hollow-core fiber and tapered fiber

    NASA Astrophysics Data System (ADS)

    Zhang, Naiqian; Wang, Zefeng; Liu, Wenbo; Xi, Xiaoming

    2017-10-01

    Up to now, near almost optical fiber gas lasers employ/adopt the scheme of free-space coupling, which increases the difficulty to adjust the optical path, and has poor stability. All-fiber structure fiber-gas lasers are important development directions in the future. We established the numerical model of SMF-28 type tapered single-mode fiber and non-node hollow-core fiber. When the SMF-28 type single-mode fiber has a waist diameter of 40μm when the light source is LP01 fundamental mode with 1550nm wavelength, the mode field diameter is the largest. Meanwhile, we simulated that the equivalent mode field diameter of non-node anti-resonant hollow-core fiber is about 75μm at the same 1550nm wavelength light source. Then, we use different waist diameters of SMF-28 type tapered fibers injected to the non-node anti-resonant hollow-core fiber in simulation and experiments. In the scheme of the single-ended low-loss coupling, the simulation results indicate that the best waist diameter of tapered fiber is 40μm, and the calculated maximum coupling efficiency is 83.55%. Meanwhile, the experimental result of maximum coupling efficiency is 80.74% when the best waist diameter of tapered fiber is also 40μm. As for the double-ended low-loss coupling, the calculated maximum coupling efficiency is near 83.38%.

  16. Spatial patterns of giant sequoia (Sequoiadendron giganteum) in two sequoia groves in Sequoia National Park, California

    USGS Publications Warehouse

    Stohlgren, Thomas J.

    1993-01-01

    Although Muir Grove and Castle Creek Grove are similar in area, elevation, and number of giant sequoias, various spatial pattern analysis techniques showed that they had dissimilar spatial patterns for similar-sized trees. Two-dimensional and transect two-term local quadrat variance techniques detected general trends in the spatial patterns of different-sized trees, detected multiple-scale patterns within individual size classes, and provided information on the scale and intensity of patches of individual size classes of trees in Muir and Castle Creek groves. In Muir Grove, midsized sequoias (1.5 to 2.4 m DBH classes) had major pattern scales 350–450 m in diameter, whereas the same-sized trees in Castle Creek Grove had pattern scales >1000 m in diameter. Many size classes of trees had minor patches superimposed on larger scale patterns in both groves. There may be different recruitment patterns in core (i.e., central) areas compared with peripheral areas of sequoia groves; core areas of both groves had more small live sequoias and dead sequoias than peripheral areas of the groves. Higher densities of sequoias and, perhaps, more rapid turnover of individuals in core areas may indicate (i) differences in disturbance histories and favorability of microsites in the core and peripheral areas of groves; (ii) different responses to disturbance due to shifts in the species composition of the stand and thus, the relative influences of intra- to inter-specific competition; or (iii) slower growth or lower survivorship rates in marginal habitat (i.e., peripheral areas).

  17. Improved Thermoplastic/Iron-Particle Transformer Cores

    NASA Technical Reports Server (NTRS)

    Wincheski, Russell A.; Bryant, Robert G.; Namkung, Min

    2004-01-01

    A method of fabricating improved transformer cores from composites of thermoplastic matrices and iron-particles has been invented. Relative to commercially available laminated-iron-alloy transformer cores, the cores fabricated by this method weigh less and are less expensive. Relative to prior polymer-matrix/ iron-particle composite-material transformer cores, the cores fabricated by this method can be made mechanically stronger and more magnetically permeable. In addition, whereas some prior cores have exhibited significant eddy-current losses, the cores fabricated by this method exhibit very small eddy-current losses. The cores made by this method can be expected to be attractive for use in diverse applications, including high-signal-to-noise transformers, stepping motors, and high-frequency ignition coils. The present method is a product of an experimental study of the relationships among fabrication conditions, final densities of iron particles, and mechanical and electromagnetic properties of fabricated cores. Among the fabrication conditions investigated were molding pressures (83, 104, and 131 MPa), and molding temperatures (250, 300, and 350 C). Each block of core material was made by uniaxial-compression molding, at the applicable pressure/temperature combination, of a mixture of 2 weight percent of LaRC (or equivalent high-temperature soluble thermoplastic adhesive) with 98 weight percent of approximately spherical iron particles having diameters in the micron range. Each molded block was cut into square cross-section rods that were used as core specimens in mechanical and electromagnetic tests. Some of the core specimens were annealed at 900 C and cooled slowly before testing. For comparison, a low-carbon-steel core was also tested. The results of the tests showed that density, hardness, and rupture strength generally increased with molding pressure and temperature, though the correlation was rather weak. The weakness of the correlation was attributed to the pores in the specimens. The maximum relative permeabilities of cores made without annealing ranged from 30 to 110, while those of cores made with annealing ranged from 900 to 1,400. However, the greater permeabilities of the annealed specimens were not associated with noticeably greater densities. The major practical result of the investigation was the discovery of an optimum distribution of iron-particle sizes: It was found that eddy-current losses in the molded cores were minimized by using 100 mesh (corresponding to particles with diameters less than or equal to 100 m) iron particles. The effect of optimization of particle sizes on eddy-current losses is depicted in the figure.

  18. Effect of waist diameter and twist on tapered asymmetrical dual-core fiber MZI filter.

    PubMed

    Liu, Yan; Li, Yang; Yan, Xiaojun; Li, Weidong

    2015-10-01

    A compact in-fiber Mach-Zehnder interferometer (MZI) filter fabricated from custom-designed asymmetrical dual-core fiber is numerically analyzed in detail and experimentally verified. The asymmetrical dual-core fiber has core diameters and a core pitch of 6.9, 6, and 19.9 μm, respectively. The fiber tapering technique is introduced to fuse the originally uncoupled cores into strong coupling tapered regions. The length and diameter of the waist region have a close impact on the splitting ratio, which further affects the spectral properties of the MZI filter. The field evolution with varied waist parameters is characterized by the finite element method and beam propagation method. Repeatable comb filters with ∼15  dB extinction ratio are successfully achieved under the guidance of simulated optimum conditions. The twist-induced circular birefringence gives rise to a retardance that causes the spectral shifts of the MZI filter. The theoretical and experimental results confirm that the relative wavelength shift is proportional to the retardance, which follows a sinc function in the limit of a large twist rate.

  19. Optimal design for crosstalk analysis in 12-core 5-LP mode homogeneous multicore fiber for different lattice structure

    NASA Astrophysics Data System (ADS)

    Kumar, Dablu; Ranjan, Rakesh

    2018-03-01

    12-Core 5-LP mode homogeneous multicore fibers have been proposed for analysis of inter-core crosstalk and dispersion, with four different lattice structures (circular, 2-ring, square lattice, and triangular lattice) having cladding diameter of 200 μm and a fixed cladding thickness of 35 μm. The core-to-core crosstalk impact has been studied numerically with respect to bending radius, core pitch, transmission distance, wavelength, and core diameter for all 5-LP modes. In anticipation of further reduction in crosstalk levels, the trench-assisted cores have been incorporated for all respective designs. Ultra-low crosstalk (-138 dB/100 km) has been achieved through the triangular lattice arrangement, with trench depth Δ2 = -1.40% for fundamental (LP01) mode. It has been noted that the impact of mode polarization on crosstalk behavior is minor, with difference in crosstalk levels between two polarized spatial modes as ≤0.2 dB. Moreover, the optimized cladding diameter has been obtained for all 5-LP modes for a target value of crosstalk of -50 dB/100 km, with all the core arrangements. The dispersion characteristic has also been analyzed with respect to wavelength, which is nearly 2.5 ps/nm km at operating wavelength 1550 nm. The relative core multiplicity factor (RCMF) for the proposed design is obtained as 64.

  20. Magnetic core shell nanoparticles trapping in a microdevice generating high magnetic gradient.

    PubMed

    Teste, Bruno; Malloggi, Florent; Gassner, Anne-Laure; Georgelin, Thomas; Siaugue, Jean-Michel; Varenne, Anne; Girault, Hubert; Descroix, Stéphanie

    2011-03-07

    Magnetic core shell nanoparticles (MCSNPs) 30 nm diameter with a magnetic weight of 10% are usually much too small to be trapped in microfluidic systems using classical external magnets. Here, a simple microchip for efficient MCSNPs trapping and release is presented. It comprises a bed of micrometric iron beads (6-8 μm diameter) packed in a microchannel against a physical restriction and presenting a low dead volume of 0.8 nL. These beads of high magnetic permeability are used to focus magnetic field lines from an external permanent magnet and generate local high magnetic gradients. The nanoparticles magnetic trap has been characterised both by numerical simulations and fluorescent MCSNPs imaging. Numerical simulations have been performed to map both the magnetic flux density and the magnetic force, and showed that MCSNPs are preferentially trapped at the iron bead magnetic poles where the magnetic force is increased by 3 orders of magnitude. The trapping efficiency was experimentally determined using fluorescent MCSNPs for different flow rates, different iron beads and permanent magnet positions. At a flow rate of 100 μL h(-1), the nanoparticles trapping/release can be achieved within 20 s with a preconcentration factor of 4000.

  1. Transmission characteristics of femtosecond optical pulses in hollow-core fibers

    NASA Astrophysics Data System (ADS)

    Mohebbi, Mohammad

    2005-09-01

    Hollow-core fibers with fused silica and metal claddings are studied for transmission of femtosecond optical pulses at a wavelength of 800 nm. The measured transmission loss of a silver-coated hollow fiber with a core diameter of 250 μm is 0.44 dB/m. A bending loss of 1.1 dB/m was measured for this waveguide with a radius of curvature of 1 m. It is shown that the fundamental hybrid mode HE 11 has negligible pulse spreading. In the presence of higher order modes modal dispersion becomes dominant and depends strongly on the core diameter.

  2. Core sample extractor

    NASA Technical Reports Server (NTRS)

    Akins, James; Cobb, Billy; Hart, Steve; Leaptrotte, Jeff; Milhollin, James; Pernik, Mark

    1989-01-01

    The problem of retrieving and storing core samples from a hole drilled on the lunar surface is addressed. The total depth of the hole in question is 50 meters with a maximum diameter of 100 millimeters. The core sample itself has a diameter of 60 millimeters and will be two meters in length. It is therefore necessary to retrieve and store 25 core samples per hole. The design utilizes a control system that will stop the mechanism at a certain depth, a cam-linkage system that will fracture the core, and a storage system that will save and catalogue the cores to be extracted. The Rod Changer and Storage Design Group will provide the necessary tooling to get into the hole as well as to the core. The mechanical design for the cam-linkage system as well as the conceptual design of the storage device are described.

  3. 76 FR 36092 - Small Diameter Graphite Electrodes From the People's Republic of China: Extension of Time Limit...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-06-21

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-570-929] Small Diameter Graphite... antidumping duty order on small diameter graphite electrodes from the People's Republic of China (``PRC'') for... preliminary results of this review were published on March 7, 2011. See Small Diameter Graphite Electrodes...

  4. 77 FR 6060 - Small Diameter Graphite Electrodes from the People's Republic of China: Extension of Time Limit...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2012-02-07

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-570-929] Small Diameter Graphite... Department) initiated an administrative review of the antidumping duty order on small diameter graphite... preliminary results of this review by 95 days until February 3, 2012. See Small Diameter Graphite Electrodes...

  5. Fiber optic muzzle brake tip for reducing fiber burnback and stone retropulsion during thulium fiber laser lithotripsy

    NASA Astrophysics Data System (ADS)

    Hutchens, Thomas C.; Gonzalez, David A.; Irby, Pierce B.; Fried, Nathaniel M.

    2017-01-01

    The experimental thulium fiber laser (TFL) is being explored as an alternative to the current clinical gold standard Holmium:YAG laser for lithotripsy. The near single-mode TFL beam allows coupling of higher power into smaller optical fibers than the multimode Holmium laser beam profile, without proximal fiber tip degradation. A smaller fiber is desirable because it provides more space in the ureteroscope working channel for increased saline irrigation rates and allows maximum ureteroscope deflection. However, distal fiber tip burnback increases as fiber diameter decreases. Previous studies utilizing hollow steel sheaths around recessed distal fiber tips reduced fiber burnback but increased stone retropulsion. A "fiber muzzle brake" was tested for reducing both fiber burnback and stone retropulsion by manipulating vapor bubble expansion. TFL lithotripsy studies were performed at 1908 nm, 35 mJ, 500 μs, and 300 Hz using a 100-μm-core fiber. The optimal stainless steel muzzle brake tip tested consisted of a 1-cm-long, 560-μm-outer-diameter, 360-μm-inner-diameter tube with a 275-μm-diameter through hole located 250 μm from the distal end. The fiber tip was recessed a distance of 500 μm. Stone phantom retropulsion, fiber tip burnback, and calcium oxalate stone ablation studies were performed ex vivo. Small stones with a mass of 40±4 mg and 4-mm-diameter were ablated over a 1.5-mm sieve in 25±4 s (n=10) without visible distal fiber tip burnback. Reduction in stone phantom retropulsion distance by 50% and 85% was observed when using muzzle brake tips versus 100-μm-core bare fibers and hollow steel tip fibers, respectively. The muzzle brake fiber tip simultaneously provided efficient stone ablation, reduced stone retropulsion, and minimal fiber degradation during TFL lithotripsy.

  6. Suspended core subwavelength fibers: towards practical designs for low-loss terahertz guidance.

    PubMed

    Rozé, Mathieu; Ung, Bora; Mazhorova, Anna; Walther, Markus; Skorobogatiy, Maksim

    2011-05-09

    In this work we report two designs of subwavelength fibers packaged for practical terahertz wave guiding. We describe fabrication, modeling and characterization of microstructured polymer fibers featuring a subwavelength-size core suspended in the middle of a large porous outer cladding. This design allows convenient handling of the subwavelength fibers without distorting their modal profile. Additionally, the air-tight porous cladding serves as a natural enclosure for the fiber core, thus avoiding the need for a bulky external enclosure for humidity-purged atmosphere. Fibers of 5 mm and 3 mm in outer diameters with a 150 µm suspended solid core and a 900 µm suspended porous core respectively, were obtained by utilizing a combination of drilling and stacking techniques. Characterization of the fiber optical properties and the subwavelength imaging of the guided modes were performed using a terahertz near-field microscopy setup. Near-field imaging of the modal profiles at the fiber output confirmed the effectively single-mode behavior of such waveguides. The suspended core fibers exhibit transmission from 0.10 THz to 0.27 THz (larger core), and from 0.25 THz to 0.51 THz (smaller core). Due to the large fraction of power that is guided in the holey cladding, fiber propagation losses as low as 0.02 cm(-1) are demonstrated specifically for the small core fiber. Low-loss guidance combined with the core isolated from environmental perturbations make these all-dielectric fibers suitable for practical terahertz imaging and sensing applications. © 2011 Optical Society of America

  7. Coring device with a improved core sleeve and anti-gripping collar with a collective core catcher

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Story, A.L.; Filshtinsky, M.

    1986-01-28

    This patent describes an improved coring apparatus used in combination with a coring bit and drill string. This device consists of: an outer driving structure adapted to be connected at one end to the coring bit for cutting a core in a borehole, and at the other end to the lower end of the drill string in telescoping and co-rotatable manner therewith; an inner barrel disposed within the outer driving structure and including a lower end portion adjacent to the bit; first means supporting the inner barrel in spaced relationship to the outer driving structure while permitting rotation of themore » driving structure with respect to the inner barrel; a woven metal mesh sleeve mounted in surrounding relation on at least a portion of the exterior surface of the inner barrel; second means, connected to a free end of the sleeve opposite the leading portion of the sleeve, for maintaining the portion of the sleeve which surrounds the inner barrel in compression and to maintain an inside diameter greater than the outside diameter of the inner barrel of the portion of the sleeve surrounding the inner barrel while the portion of the sleeve positioned inside the inner barrel being in tension to grip and compress a core received within the sleeve and having an outside diameter less than the inside diameter of the inner barrel when in tension, wherein the second means is also for engaging the core when the means is drawn into the inner barrel, and third means positioned within the inner barrel and connected to the leading portion of the sleeve to draw the sleeve within the inner barrel and to apply tension to the portion of the sleeve within the barrel to encase and grip the core as it is cut.« less

  8. Design and synthesis of magnetic nanoparticles with gold shells for single particle optical tracking

    NASA Astrophysics Data System (ADS)

    Lim, Jitkang

    The design, synthesis, and characterization of iron oxide core, gold shell nanoparticles are studied in this thesis. Firstly, nanoparticles with 18 +/- 1.7 nm diameter iron oxide cores with ˜5 nm thick gold shells were synthesized via a new seed-mediated electroless deposition method. The nanoparticles were superparamagnetic at room temperature and could be reversibly collected by a permanent magnet. These nanoparticles displayed a sharp localized surface plasmon resonance peak at 605 nm, as predicted by scattering theory, and their large scattering cross-section allowed them to be individually resolved in darkfield optical microscopy while undergoing Brownian motion in aqueous suspension. Later, commercially available 38 +/- 3.8 nm diameter spherical iron oxide nanoparticles (from Ocean Nanotech, Inc) were employed to make core-shell particles. These particles were decorated with cationic poly(diallyldimethylammonium chloride) (PDDA) which further promotes the attachment of small gold clusters. After gold seeding, the average hydrodynamic diameter of the core-shell particles is 172 +/- 65.9 nm. The magnetophoretic motion of these particles was guided by a piece of magnetized mu-metal. Individual particle trajectories were observed by darkfield optical microscopy. The typical magnetophoretic velocity achieved was within the range of 1--10 mum/sec. Random walk analysis performed on these particles while undergoing Brownian motion confirmed that individual particles were indeed being imaged. The particle size variation within the observed sample obtained through random walk analysis was within the size distribution obtained by dynamic light scattering. When the current to the solenoid used to magnetize the mu-metal was turned off, all the collected core-shell particles were readily redispersed by diffusion back into the surrounding environment. A Peclet number analysis was performed to probe the convective motion of nanospheres and nanorods under the influence of magnetophoresis and diffusion. Under most circumstances, magnetophoretic behavior dominates diffusion for nanorods, as the magnetic field lines tend to align the magnetic moment along the rod axis. The synthesis and dispersion of fluorophore-tagged nanorods are described. Fluorescence microscopy was employed to image the nanorod motion in a magnetic field gradient. The preliminary experimental data are consistent with the Peclet number analysis. Lastly, the colloidal stability of iron oxide core, gold shell nanoparticles in high ionic strength media was investigated. Such particles are sufficiently charged to be stable against flocculation without modification in low ionic strength media, but they require surface modification to be stably dispersed in elevated ionic strength media that are appropriate for biotechnological applications. Dynamic light scattering and ultraviolet-visible spectrophotometry were used to monitor the colloidal stability of core-shell particles in pH 7.4, 150 mM ionic strength phosphate buffered saline (PBS). While uncoated particles flocculated immediately upon being introduced into PBS, core-shell particles with adsorbed layers of bovine serum albumin or the amphiphilic triblock copolymers Pluronic F127 and Pluronic F68 resist flocculation after more than five days in PBS. Adsorbed dextran allowed flocculation that was limited to the formation of small clusters, while poly(ethylene glycol) homopolymers ranging in molecular weight from 6,000 to 100,000 were ineffective steric stabilizers. The effectiveness of adsorbed Pluronic copolymers as steric stabilizers was interpreted in terms of the measured adsorbed layer thickness and extended DLVO theory predictions of the interparticle interactions.

  9. Vertical velocity in oceanic convection off tropical Australia

    NASA Technical Reports Server (NTRS)

    Lucas, Christopher; Zipser, Edward J.; Lemone, Margaret A.

    1994-01-01

    Time series of 1-Hz vertical velocity data collected during aircraft penetrations of oceanic cumulonimbus clouds over the western Pacific warm pool as part of the Equatorial Mesoscale Experiment (EMEX) are analyzed for updraft and downdraft events called cores. An updraft core is defined as occurring whenever the vertical velocity exceeds 1 m/sec for at least 500 m. A downdraft core is defined analogously. Over 19,000 km of straight and level flight legs are used in the analysis. Five hundred eleven updraft cores and 253 downdraft cores are included in the dataset. Core properties are summarized as distributions of average and maximum vertical velocity, diameter, and mass flux in four altitude intervals between 0.2 and 5.8 km. Distributions are approximately lognormal at all levels. Examination of the variation of the statistics with height suggests a maximum in vertical velocity between 2 and 3 km; slightly lower or equal vertical velocity is indicated at 5 km. Near the freezing level, virtual temperature deviations are found to be slightly positive for both updraft and downdraft cores. The excess in updraft cores is much smaller than that predicted by parcel theory. Comparisons with other studies that use the same analysis technique reveal that EMEX cores have approximately the same strength as cores of other oceanic areas, despite warmer sea surface temperatures. Diameter and mass flux are greater than those in the Global Atmospheric Research Program (GATE) but smaller than those in hurricane rainbands. Oceanic cores are much weaker and appear to be slightly smaller than those observed over land during the Thunderstorm Project. The markedly weaker oceanic vertical velocities below 5.8 km (compared to the continental cores) cannot be attributed to smaller total convective available potential energy or to very high water loading. Rather, it is suggested that water loading, although less than adiabatic, is more effective in reducing buoyancy of oceanic cores because of the smaller potential buoyancy below 5.8 km. Entrainment appears to be more effective in reducing buoyancy to well below adiabatic values in oceanic cores, a result consistent with the smaller oceanic core diameters in the lower cloud layer. It is speculated further that core diameters are related to boundary layer depth, which is clearly smaller over the oceans.

  10. Calculation of hydraulic friction losses in dc motors filled with liquid dielectric

    NASA Astrophysics Data System (ADS)

    Morozkin, V. P.

    1984-06-01

    Hydraulic friction during rotation of the armature in a dc motor filled with liquid dielectric is a major source of power loss, up to 40% of all power losses in such a motor. These losses are usually reduced by impregnating the end turns of armature coils with a compound and smoothing their outside surfaces. Hydraulic losses are best determined experimentally on a model armature and then calculated according to the theory of similarity for any other motor. This was with the armatures of DPK-8-3000, DPK-08-1000 small motors and P-42, Mu-52 large motors as test models. For subsequent calculations the armature is treated as a structure consisting of three cylinders: (1) slotted wound active core rotating inside a stationary cylinder with a radial gap between them; (2) end turns of coils rotating in free space; and (3) slotted commutator rotating in free space. The back plate of the armature constitutes a rotating disk. Considering that the hydraulic drag coefficient is a function of the Reynolds number only, it is calculated for each component of the armature on the basis of semiempirical relations with length and radius, gap width between stator (field) bore and active rotor core, angular velocity or rpm, and density of the dielectric as parameters. The resultant hydraulic drag coefficient is found by weighted combining of the four partial ones, with use of diameter ratios and a length-to-diameter ratio for the active core.

  11. Effect of core diameter and surface treatment on the retention of resin composite cores to prefabricated endodontic posts.

    PubMed

    Artopoulou, Ioli-Ioanna; O'Keefe, Kathy L; Powers, John M

    2006-01-01

    With advances in adhesive dentistry and current emphasis on esthetic restorations, dowel systems have been developed to take advantage of these new techniques. Of interest when using these systems is the interaction between core materials and post materials. This investigation compared the tensile retentive force of two resin composite core materials to two metallic and one non-metallic prefabricated endodontic posts. Two dimensions of core build-up and two post-surface treatments were tested. One hundred twenty posts (stainless steel, titanium alloy, and glass fiber-impregnated resin) were secured in a jig with 4 mm of the post extending into a cylindrical matrix. The matrix formed cylinders with diameters of 3 and 5 mm into which resin composite was inserted. The posts were treated or not treated with a bonding agent. After storage for 24 hours at 100% humidity, five specimens per condition were tested in an Instron testing machine at a crosshead speed of 0.5 mm/min. Failure loads were recorded in kilograms and failure modes were observed under light microscopy (40 x). Four-way analysis of variance and multiple comparison testing were used to compare means at the 0.05 level of significance. The means and standard deviations of tensile loads were calculated. All variables were significant in either main effects or interactions ( p<0.05). Fisher's PLSD intervals for post, core, treatment, and diameter were 2.0, 1.6, 1.6, and 1.6 kg, respectively. In most cases, the retentive force recorded for metallic posts was higher than that of glass fiber posts. Titanium posts had higher retentive forces than did the stainless steel posts. For metallic posts, 5-mm cores provided higher forces than 3-mm cores. In the glass fiber group, core diameter was not significant. For core materials, Build-It gave higher results with stainless steel posts, and FluoroCore gave higher results with the titanium ones. The surface treatment results were mixed. In the metallic post groups the adhesive failure data ranged between 80% and 100%, whereas in the glass fiber post groups, adhesive failures ranged between 60% and 70%. Within the limitations of this study, the metallic post groups always provided higher tensile retentive forces, with the titanium post groups showing higher retentive forces than the stainless steel ones. In the glass fiber post groups, different core diameters did not affect retention values.

  12. SU-F-207-05: Excess Heat Corrections in a Prototype Calorimeter for Direct Realization of CT Absorbed Dose to Phantom

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Chen-Mayer, H; Tosh, R

    2015-06-15

    Purpose: To reconcile air kerma and calorimetry measurements in a prototype calorimeter for obtaining absorbed dose in diagnostic CT beams. While corrections for thermal artifacts are routine and generally small in calorimetry of radiotherapy beams, large differences in relative stopping powers of calorimeter materials at the lower energies typical of CT beams greatly magnify their effects. Work-to-date on the problem attempts to reconcile laboratory measurements with modeling output from Monte Carlo and finite-element analysis of heat transfer. Methods: Small thermistor beads were embedded in a polystyrene (PS) core element of 1 cm diameter, which was inserted into a cylindrical HDPEmore » phantom of 30 cm diameter and subjected to radiation in a diagnostic CT x-ray imaging system. Resistance changes in the thermistors due to radiation heating were monitored via lock-in amplifier. Multiple 3-second exposures were recorded at 8 different dose-rates from the CT system, and least-squares fits to experimental data were compared to an expected thermal response obtained by finite-element analysis incorporating source terms based on semi-empirical modeling and Monte Carlo simulation. Results: Experimental waveforms exhibited large thermal artifacts with fast time constants, associated with excess heat in wires and glass, and smaller steps attributable to radiation heating of the core material. Preliminary finite-element analysis follows the transient component of the signal qualitatively, but predicts a slower decay of temperature spikes. This was supplemented by non-linear least-squares fits incorporating semi-empirical formulae for heat transfer, which were used to obtain dose-to-PS in reasonable agreement with the output of Monte Carlo calculations that converts air kerma to absorbed dose. Conclusion: Discrepancies between the finite-element analysis and our experimental data testify to the very significant heat transfer correction required for absorbed dose calorimetry of diagnostic CT beams. The results obtained here are being used to refine both simulations and design of calorimeter core components.« less

  13. St. Petersburg Coastal and Marine Science Center's Core Archive Portal

    USGS Publications Warehouse

    Reich, Chris; Streubert, Matt; Dwyer, Brendan; Godbout, Meg; Muslic, Adis; Umberger, Dan

    2012-01-01

    This Web site contains information on rock cores archived at the U.S. Geological Survey (USGS) St. Petersburg Coastal and Marine Science Center (SPCMSC). Archived cores consist of 3- to 4-inch-diameter coral cores, 1- to 2-inch-diameter rock cores, and a few unlabeled loose coral and rock samples. This document - and specifically the archive Web site portal - is intended to be a 'living' document that will be updated continually as additional cores are collected and archived. This document may also contain future references and links to a catalog of sediment cores. Sediment cores will include vibracores, pushcores, and other loose sediment samples collected for research purposes. This document will: (1) serve as a database for locating core material currently archived at the USGS SPCMSC facility; (2) provide a protocol for entry of new core material into the archive system; and, (3) set the procedures necessary for checking out core material for scientific purposes. Core material may be loaned to other governmental agencies, academia, or non-governmental organizations at the discretion of the USGS SPCMSC curator.

  14. A six-color four-laser mobile platform for multi-spectral fluorescence imaging endoscopy

    NASA Astrophysics Data System (ADS)

    Black, John F.; Tate, Tyler; Keenan, Molly; Swan, Elizabeth; Utzinger, Urs; Barton, Jennifer

    2015-03-01

    The properties of multi-spectral fluorescence imaging using deep-UV-illumination have recently been explored using a fiber-coupled thermal source at 280 nm. The resulting images show a remarkable level of contrast thought to result from the signal being overwhelmingly generated in the uppermost few cell layers of tissue, making this approach valuable for the study of diseases that originate in the endothelial tissues of the body. With a view to extending the technique with new wavelengths, and improving beam quality for efficient small core fiber coupling we have developed a mobile self-contained tunable solid-state laser source of deep UV light. An alexandrite laser, lasing at around 750 nm is frequency doubled to produce 375 nm and then tripled to produce 250 nm light. An optical deck added to the system allows other laser sources to be incorporated into the UV beam-line and a lens system has been designed to couple these sources into a single delivery fiber with core diameters down to 50 microns. Our system incorporates five wavelengths [250 nm, 375 nm, 442 nm (HeCd), 543 nm (HeNe) and 638 nm (diode laser)] as the illumination source for a small diameter falloposcope designed for the study of the distal Fallopian tube origins of high grade serous ovarian cancer. The tunability of alexandrite offers the potential to generate other wavelengths in the 720-800, 360-400 and 240-265 nm ranges, plus other non-linear optical conversion techniques taking advantage of the high peak powers of the laser.

  15. A New Method of Stress Measurement Based upon Elastic Deformation of Core Sample with Stress Relief by Drilling

    NASA Astrophysics Data System (ADS)

    Ito, T.; Funato, A.; Tamagawa, T.; Tezuka, K.; Yabe, Y.; Abe, S.; Ishida, A.; Ogasawara, H.

    2017-12-01

    When rock is cored at depth by drilling, anisotropic expansion occurs with the relief of anisotropic rock stresses, resulting in a sinusoidal variation of core diameter with a period of 180 deg. in the core roll angle. The circumferential variation of core diameter is given theoretically as a function of rock stresses. These new findings can lead various ideas to estimate the rock stress from circumferential variation of core diameter measured after the core retrieving. In the simplest case when a single core sample is only available, the difference between the maximum and minimum components of rock stress in a plane perpendicular to the drilled hole can be estimated from the maximum and minimum core diameters (see the detail in, Funato and Ito, IJRMMS, 2017). The advantages of this method include, (i) much easier measurement operation than those in other in-situ or in-lab estimation methods, and (ii) applicability in high stress environment where stress measurements need pressure for packers or pumping system for the hydro-fracturing methods higher than their tolerance levels. We have successfully tested the method at deep seismogenic zones in South African gold mines, and we are going to apply it to boreholes collared at 3 km depth and intersecting a M5.5 rupture plane several hundred meters below the mine workings in the ICDP project of "Drilling into Seismogenic zones of M2.0 - M5.5 earthquakes in deep South African gold mines" (DSeis) (e.g., http://www.icdp-online.org/projects/world/africa/orkney-s-africa/details/). If several core samples with different orientation are available, all of three principal components of 3D rock stress can be estimated. To realize this, we should have several boreholes drilled in different directions in a rock mass where the stress field is considered to be uniform. It is commonly carried out to dill boreholes in different directions from a mine gallery. Even in a deep borehole drilled vertically from the ground surface, the downhole tool of rotary sidewall coring allows us to take core samples with different orientations at depths of interest from the sidewall of the vertically-drilled borehole. The theoretical relationship between the core expansion and rock stress has been verified through the examination of core samples prepared in laboratory experiments and retrieved field cores.

  16. Reaction growth of MF2/a-C (M = Ca, Mg) core/shell nanowires at the interface of vapor and solid reactants.

    PubMed

    Huang, Chih-Hao; Chang, Yu-Hsu; Lee, Chi-Young; Chiu, Hsin-Tien

    2006-01-03

    C(6)F(6) vapor is employed to react with CaC(2) and Mg(3)N(2) to grow CaF(2)/a-C and Mg(2)F(2)/a-C core/shell nanowires (tens of micrometers in length, tens to hundreds of nanometers in wire diameter, and tens of nanometers in core diameter), respectively, in high yields. The growth mechanism is proposed to proceed via a reaction at the interface of the vapor and solid reactants.

  17. DOE Office of Scientific and Technical Information (OSTI.GOV)

    Martin, William R.; Lee, John C.; baxter, Alan

    Information and measured data from the intial Fort St. Vrain (FSV) high temperature gas reactor core is used to develop a benchmark configuration to validate computational methods for analysis of a full-core, commercial HTR configuration. Large uncertainties in the geometry and composition data for the FSV fuel and core are identified, including: (1) the relative numbers of fuel particles for the four particle types, (2) the distribution of fuel kernel diameters for the four particle types, (3) the Th:U ratio in the initial FSV core, (4) and the buffer thickness for the fissile and fertile particles. Sensitivity studies were performedmore » to assess each of these uncertainties. A number of methods were developed to assist in these studies, including: (1) the automation of MCNP5 input files for FSV using Python scripts, (2) a simple method to verify isotopic loadings in MCNP5 input files, (3) an automated procedure to conduct a coupled MCNP5-RELAP5 analysis for a full-core FSV configuration with thermal-hydraulic feedback, and (4) a methodology for sampling kernel diameters from arbitrary power law and Gaussian PDFs that preserved fuel loading and packing factor constraints. A reference FSV fuel configuration was developed based on having a single diameter kernel for each of the four particle types, preserving known uranium and thorium loadings and packing factor (58%). Three fuel models were developed, based on representing the fuel as a mixture of kernels with two diameters, four diameters, or a continuous range of diameters. The fuel particles were put into a fuel compact using either a lattice-bsed approach or a stochastic packing methodology from RPI, and simulated with MCNP5. The results of the sensitivity studies indicated that the uncertainties in the relative numbers and sizes of fissile and fertile kernels were not important nor were the distributions of kernel diameters within their diameter ranges. The uncertainty in the Th:U ratio in the intial FSV core was found to be important with a crude study. The uncertainty in the TRISO buffer thickness was estimated to be unimportant but the study was not conclusive. FSV fuel compacts and a regular FSV fuel element were analyzed with MCNP5 and compared with predictions using a modified version of HELIOS that is capable of analyzing TRISO fuel configurations. The HELIOS analyses were performed by SSP. The eigenvalue discrepancies between HELIOS and MCNP5 are currently on the order of 1% but these are still being evaluated. Full-core FSV configurations were developed for two initial critical configurations - a cold, clean critical loading and a critical configuration at 70% power. MCNP5 predictions are compared to experimental data and the results are mixed. Analyses were also done for the pulsed neutron experiments that were conducted by GA for the initial FSV core. MCNP5 was used to model these experiments and reasonable agreement with measured results has been observed.« less

  18. Erosion Characteristics and Horizontal Variability for Small Erosion Depths in the Sacramento - San Joaquin River Delta, California, USA

    NASA Astrophysics Data System (ADS)

    Schoellhamer, D. H.; Manning, A. J.; Work, P. A.

    2015-12-01

    Cohesive sediment in the Sacramento-San Joaquin River Delta affects pelagic fish habitat, contaminant transport, and marsh accretion. Observations of suspended-sediment concentration in the delta indicate that about 0.05 to 0.20 kg/m2 are eroded from the bed during a tidal cycle. If erosion is horizontally uniform, the erosion depth is about 30 to 150 microns, the typical range in diameter of suspended flocs. Application of an erosion microcosm produces similarly small erosion depths. In addition, core erodibility in the microcosm calculated with a horizontally homogeneous model increases with depth, contrary to expectations for a consolidating bed, possibly because the eroding surface area increases as applied shear stress increases. Thus, field observations and microcosm experiments, combined with visual observation of horizontally varying biota and texture at the surface of sediment cores, indicate that a conceptual model of erosion that includes horizontally varying properties may be more appropriate than assuming horizontally homogeneous erosive properties. To test this hypothesis, we collected five cores and measured the horizontal variability of shear strength within each core in the top 5.08 cm with a shear vane. Small tubes built by a freshwater worm and macroalgae were observed on the surface of all cores. The shear vane was inserted into the sediment until the top of the vane was at the top of the sediment, torque was applied to the vane until the sediment failed and the vane rotated, and the corresponding dial reading in Nm was recorded. The dial reading was assumed to be proportional to the surface strength. The horizontal standard deviation of the critical shear stress was about 30% of the mean. Results of the shear vane test provide empirical evidence that surface strength of the bed varies horizontally. A numerical simulation of erosion with an areally heterogeneous bed reproduced erosion characteristics observed in the microcosm.

  19. Small Launch Vehicle Design Approaches: Clustered Cores Compared with Multi-Stage Inline Concepts

    NASA Technical Reports Server (NTRS)

    Waters, Eric D.; Beers, Benjamin; Esther, Elizabeth; Philips, Alan; Threet, Grady E., Jr.

    2013-01-01

    In an effort to better define small launch vehicle design options two approaches were investigated from the small launch vehicle trade space. The primary focus was to evaluate a clustered common core design against a purpose built inline vehicle. Both designs focused on liquid oxygen (LOX) and rocket propellant grade kerosene (RP-1) stages with the terminal stage later evaluated as a LOX/methane (CH4) stage. A series of performance optimization runs were done in order to minimize gross liftoff weight (GLOW) including alternative thrust levels, delivery altitude for payload, vehicle length to diameter ratio, alternative engine feed systems, re-evaluation of mass growth allowances, passive versus active guidance systems, and rail and tower launch methods. Additionally manufacturability, cost, and operations also play a large role in the benefits and detriments for each design. Presented here is the Advanced Concepts Office's Earth to Orbit Launch Team methodology and high level discussion of the performance trades and trends of both small launch vehicle solutions along with design philosophies that shaped both concepts. Without putting forth a decree stating one approach is better than the other; this discussion is meant to educate the community at large and let the reader determine which architecture is truly the most economical; since each path has such a unique set of limitations and potential payoffs.

  20. Strike action electromagnetic machine for immersion of rod elements into ground

    NASA Astrophysics Data System (ADS)

    Usanov, K. M.; Volgin, A. V.; Chetverikov, E. A.; Kargin, V. A.; Moiseev, A. P.; Ivanova, Z. I.

    2017-10-01

    During construction, survey work, and drilling shallow wells by striking, operations associated with dipping and removing the rod elements are the most common. At the same time relatively long, with small diameter, elements, in which the ratio of length to diameter l/d is 100 or more, constitute a significant proportion. At present, the application of power pulse linear electromagnetic motors to drive drum machines is recognized to be highly effective. However, the mechanical method of transmission of shocks does not allow dipping long longitudinally unstable core elements. In this case, mechanical energy must be transferred from the motor to the rod through its side surface. The design of the strike action electromagnetic machine with a through axial channel for non-mechanical end striking of the pile of long, longitudinally unstable metal rods is proposed. Electromagnetic striking machine for non-mechanical end striking rod elements provides operations characterized by ecological compatibility, safety and high quality.

  1. Modal noise investigation in multimode polymer waveguides

    NASA Astrophysics Data System (ADS)

    Beals, Joseph, IV; Bamiedakis, Nikos; Penty, Richard V.; White, Ian H.; DeGroot, Jon V., Jr.; Clapp, Terry V.

    2007-11-01

    In this work the recent interest in waveguides for use in short optical links has motivated a study of the modal noise dependence on launch conditions in short-reach step-index multimode polymer waveguides. Short optical links, especially those with several connection interfaces and utilising a restricted launch are likely to be subject to a modal noise power penalty. We therefore experimentally study the modal noise impact of restricted launches for a short-reach optical link employing a 50 x 50 μm polymer multimode waveguide. Lens launches resulting in small diameter input spots are investigated as are restricted launches from an 8 μm core optical fibre. For a launch spot of 10 μm diameter no impairment is observed for up to 9 dBo of mode selective loss, and for a fibre launch with a dynamic input movement of 6 μm no impairment is seen for up to 8 dBo of mode selective loss.

  2. High pressure fiber optic sensor system

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Guida, Renato; Xia, Hua; Lee, Boon K

    2013-11-26

    The present application provides a fiber optic sensor system. The fiber optic sensor system may include a small diameter bellows, a large diameter bellows, and a fiber optic pressure sensor attached to the small diameter bellows. Contraction of the large diameter bellows under an applied pressure may cause the small diameter bellows to expand such that the fiber optic pressure sensor may measure the applied pressure.

  3. Axial residual stresses in boron fibers

    NASA Technical Reports Server (NTRS)

    Behrendt, D. R.

    1978-01-01

    The axial residual stress distribution as a function of radius was determined from the fiber surface to the core including the average residual stress in the core. Such measurements on boron on tungsten (B/W) fibers show that the residual stresses for 102, 142, 203, and 366 micron diameter fibers were similar, being compressive at the surface and changing monotonically to a region of tensile within the boron. At approximately 25 percent of the original radius, the stress reaches a maximum tensile stress of about 860 mn/sq.m and then decreases to a compressive stress near the tungsten boride core. Data were presented for 203 micron diameter B/W fibers that show annealing above 900 C reduces the residual stresses. A comparison between 102 micron diameter B/W and boron on carbon (b/C) shows that the residual stresses were similar in the outer regions of the fibers, but that large differences near and in the core were observed. The effects of these residual stresses on the fracture of boron fibers were discussed.

  4. Structure modeling and manufacturing PCFs for the range of 2-25 μm

    NASA Astrophysics Data System (ADS)

    Lvov, Alexandr; Salimgareev, Dmitrii; Korsakov, Michail; Korsakov, Alexandr; Zhukova, Liya

    2017-11-01

    Photostable and flexible materials transparent at the wide spectral range are necessary for the development of optical fiber units. Solid solutions of silver and monadic thallium halides are the most suitable crystal media for this purpose. The goal of our research was the search of optimum structure for the fibers with a single mode operation and a rather large core diameter. We modelled fiber structures (solid-core, hollow-core, active-core PCF) with various ratio of inserts diameters and increments between the inserts, basing on two crystal systems: AgCl-AgBr and AgBr-TlI. Then we chose the single mode fiber structure and manufactured it by means of extrusion.

  5. Evaluation of a small-diameter sampling method in magnetic susceptibility, AMS and X-ray CT studies and its applications to mafic microgranular enclaves (MMEs) in granite

    NASA Astrophysics Data System (ADS)

    Zhu, Kong-Yang; Li, Ming-Yue; Shentu, Lu-Feng; Shen, Zhong-Yue; Yu, Yi-Hao

    2017-07-01

    This paper reviews the technical details of the small diameter sampling method in a study of anisotropy of magnetic susceptibility (AMS) and X-ray CT (computed tomography) and their applications to studies of MMEs (Mafic Microgranular Enclaves) in granite. The AMS results based on 9 mm diameter cylinder specimens collected from the Cretaceous Tongkengxi mafic dykes in South China were consistent with results using 25 mm diameter specimens. The first case study demonstrated the variation of AMS in the interior of a large MME from South China, which contained a center of strong short-range magnetic lineation. This type of magnetic fabric could be detected only by using sample cores with a small diameter. In the foliation direction, the host granite interacted with the MME more heavily and produced a region with a high magnetite content. The second case study was the investigation of the MMEs in the Early Cretaceous Muchen complex in eastern South China. The MME swarms exhibited relatively uniform magnetic fabrics at the outcrop scale, but the fabrics varied significantly at the intrusion scale. AMS of the MME swarms is coaxial with that of the host granite only at some localities. The disagreement of AMS between MME and host granite either imply different magma flow directions, or different magma flow velocities, or disturbance of the granite fabric by the MME. The MMEs in a mylonitic granite from eastern North China were also studied. The MME specimens show highly variable magnetic susceptibility and lineations. They can be only studied appropriately by a small drill. In the three cases, the three magnetic susceptibility axes of the MMEs are consistent with the volume-weighted maximum eigenvector of long/intermediate/short axes of magnetite. The orientations of the magnetite long axes in the three cases form several modes and the concentration of the modes results in a strong lineation. One implication of this study is that MMEs, with the same magmatic fabrics as their host granite, most likely represent mafic magmas flowing with granitic magmas. Another implication is that the interaction between MMEs and host granite, which is strengthened by magmatic flows or ductile deformations, may promote crystallization of magnetite and formation of magnetite-rich granitoids. The presented 9 mm sampling methods provides easy ways to study the petrofabrics and other properties of small-sized features such as MMEs and their detailed internal textures.

  6. Nanocomposites Derived From a Low-Color Aromatic Polyimide (CP2) and Amine-Functionalized Vapor-Grown Carbon Nanofibers: In Situ Polymerization and Characterization (Preprint)

    DTIC Science & Technology

    2007-01-01

    small metal catalyst (e.g., ferrocene, Fe (CO)5, etc.). They have an outer diameter of 60-200 nm, a hollow core of 30-90 nm, and length on the order...diffractions (WAXS) of compression-molded samples were recorded with a Rigaku RU-200 diffractometer using Ni-filtered Cu KR radiation (40 kV, 100 mA, λ...attributable to the sp3 C-H and sp2 C-H defects as methane is used as the major component in the feedstock for its production . Based on hydrogen

  7. Core-Shell Magnetic Morphology of Structurally Uniform Magnetite Nanoparticles

    NASA Astrophysics Data System (ADS)

    Krycka, K. L.; Booth, R. A.; Hogg, C. R.; Ijiri, Y.; Borchers, J. A.; Chen, W. C.; Watson, S. M.; Laver, M.; Gentile, T. R.; Dedon, L. R.; Harris, S.; Rhyne, J. J.; Majetich, S. A.

    2010-05-01

    A new development in small-angle neutron scattering with polarization analysis allows us to directly extract the average spatial distributions of magnetic moments and their correlations with three-dimensional directional sensitivity in any magnetic field. Applied to a collection of spherical magnetite nanoparticles 9.0 nm in diameter, this enhanced method reveals uniformly canted, magnetically active shells in a nominally saturating field of 1.2 T. The shell thickness depends on temperature, and it disappears altogether when the external field is removed, confirming that these canted nanoparticle shells are magnetic, rather than structural, in origin.

  8. Receptosecretory nature of type III cells in the taste bud.

    PubMed

    Yoshie, Sumio

    2009-01-01

    Type III cells in taste buds form chemical synapses with intragemmal afferent nerve fibers and are characterized by the presence of membrane-bound vesicles in the cytoplasm. Although the vesicles differ in shape and size among species, they are primarily categorized into small clear (40 nm in diameter) and large dense-cored (90-200 nm) types. As such vesicles tend to be closely juxtaposed to the synaptic membrane of the cells, it is reasonable to consider that the vesicles include transmitter(s) towards the gustatory nerve. In the guinea-pig taste bud, stimulation with various taste substances (sucrose, sodium chloride, quinine hydrochloride, or monosodium L-glutamate) causes ultrastructural alterations of the type III cells. At the synapse, the presynaptic plasma membrane often displays invaginations of 90 nm in a mean diameter towards the cytoplasm, which indicates the dense-cored vesicles opening into the synaptic cleft by means of exocytosis. The vesicles are also exocytosed at the non-synaptic region into the intercellular space. These findings strongly suggest that the transmitters presumably contained in the vesicles are released to conduct the excitement of the type III cells to the nerves and also to exert their paracrine effects upon the surroundings, such as the Ebner's salivary gland, acting as local hormones.

  9. Minimizing or eliminating refueling of nuclear reactor

    DOEpatents

    Doncals, Richard A.; Paik, Nam-Chin; Andre, Sandra V.; Porter, Charles A.; Rathbun, Roy W.; Schwallie, Ambrose L.; Petras, Diane S.

    1989-01-01

    Demand for refueling of a liquid metal fast nuclear reactor having a life of 30 years is eliminated or reduced to intervals of at least 10 years by operating the reactor at a low linear-power density, typically 2.5 kw/ft of fuel rod, rather than 7.5 or 15 kw/ft, which is the prior art practice. So that power of the same magnitude as for prior art reactors is produced, the volume of the core is increased. In addition, the height of the core and it diameter are dimensioned so that the ratio of the height to the diameter approximates 1 to the extent practicable considering the requirement of control and that the pressure drop in the coolant shall not be excessive. The surface area of a cylinder of given volume is a minimum if the ratio of the height to the diameter is 1. By minimizing the surface area, the leakage of neutrons is reduced. By reducing the linear-power density, increasing core volume, reducing fissile enrichment and optimizing core geometry, internal-core breeding of fissionable fuel is substantially enhanced. As a result, core operational life, limited by control worth requirements and fuel burnup capability, is extended up to 30 years of continuous power operation.

  10. The Driving Magnetic Field and Reconnection in CME/Flare Eruptions and Coronal Jets

    NASA Technical Reports Server (NTRS)

    Moore, Ronald L.

    2010-01-01

    Signatures of reconnection in major CME (coronal mass ejection)/flare eruptions and in coronal X-ray jets are illustrated and interpreted. The signatures are magnetic field lines and their feet that brighten in flare emission. CME/flare eruptions are magnetic explosions in which: 1. The field that erupts is initially a closed arcade. 2. At eruption onset, most of the free magnetic energy to be released is not stored in field bracketing a current sheet, but in sheared field in the core of the arcade. 3. The sheared core field erupts by a process that from its start or soon after involves fast "tether-cutting" reconnection at an initially small current sheet low in the sheared core field. If the arcade has oppositely-directed field over it, the eruption process from its start or soon after also involves fast "breakout" reconnection at an initially small current sheet between the arcade and the overarching field. These aspects are shown by the small area of the bright field lines and foot-point flare ribbons in the onset of the eruption. 4. At either small current sheet, the fast reconnection progressively unleashes the erupting core field to erupt with progressively greater force. In turn, the erupting core field drives the current sheet to become progressively larger and to undergo progressively greater fast reconnection in the explosive phase of the eruption, and the flare arcade and ribbons grow to become comparable to the pre-eruption arcade in lateral extent. In coronal X-ray jets: 1. The magnetic energy released in the jet is built up by the emergence of a magnetic arcade into surrounding unipolar "open" field. 2. A simple jet is produced when a burst of reconnection occurs at the current sheet between the arcade and the open field. This produces a bright reconnection jet and a bright reconnection arcade that are both much smaller in diameter that the driving arcade. 3. A more complex jet is produced when the arcade has a sheared core field and undergoes an ejective eruption in the manner of a miniature CME/flare eruption. The jet is then a combination of a miniature CME and the products of more widely distributed reconnection of the erupting arcade with the open field than in simple jets.

  11. Tailoring the morphology and luminescence of GaN/InGaN core-shell nanowires using bottom-up selective-area epitaxy

    NASA Astrophysics Data System (ADS)

    Nami, Mohsen; Eller, Rhett F.; Okur, Serdal; Rishinaramangalam, Ashwin K.; Liu, Sheng; Brener, Igal; Feezell, Daniel F.

    2017-01-01

    Controlled bottom-up selective-area epitaxy (SAE) is used to tailor the morphology and photoluminescence properties of GaN/InGaN core-shell nanowire arrays. The nanowires are grown on c-plane sapphire substrates using pulsed-mode metal organic chemical vapor deposition. By varying the dielectric mask configuration and growth conditions, we achieve GaN nanowire cores with diameters ranging from 80 to 700 nm that exhibit various degrees of polar, semipolar, and nonpolar faceting. A single InGaN quantum well (QW) and GaN barrier shell is also grown on the GaN nanowire cores and micro-photoluminescence is obtained and analyzed for a variety of nanowire dimensions, array pitch spacings, and aperture diameters. By increasing the nanowire pitch spacing on the same growth wafer, the emission wavelength redshifts from 440 to 520 nm, while increasing the aperture diameter results in a ˜35 nm blueshift. The thickness of one QW/barrier period as a function of pitch and aperture diameter is inferred using scanning electron microscopy, with larger pitches showing significantly thicker QWs. Significant increases in indium composition were predicted for larger pitches and smaller aperture diameters. The results are interpreted in terms of local growth conditions and adatom capture radius around the nanowires. This work provides significant insight into the effects of mask configuration and growth conditions on the nanowire properties and is applicable to the engineering of monolithic multi-color nanowire LEDs on a single chip.

  12. Influence of region of interest size and ultrasound lesion size on the performance of 2D shear wave elastography (SWE) in solid breast masses.

    PubMed

    Skerl, K; Vinnicombe, S; Giannotti, E; Thomson, K; Evans, A

    2015-12-01

    To evaluate the influence of the region of interest (ROI) size and lesion diameter on the diagnostic performance of 2D shear wave elastography (SWE) of solid breast lesions. A study group of 206 consecutive patients (age range 21-92 years) with 210 solid breast lesions (70 benign, 140 malignant) who underwent core biopsy or surgical excision was evaluated. Lesions were divided into small (diameter <15 mm, n=112) and large lesions (diameter ≥15 mm, n=98). An ROI with a diameter of 1, 2, and 3 mm was positioned over the stiffest part of the lesion. The maximum elasticity (Emax), mean elasticity (Emean) and standard deviation (SD) for each ROI size were compared to the pathological outcome. Statistical analysis was undertaken using the chi-square test and receiver operating characteristic (ROC) analysis. The ROI size used has a significant impact on the performance of Emean and SD but not on Emax. Youden's indices show a correlation with the ROI size and lesion size: generally, the benign/malignant threshold is lower with increasing ROI size but higher with increasing lesion size. No single SWE parameter has superior performance. Lesion size and ROI size influence diagnostic performance. Copyright © 2015. Published by Elsevier Ltd.

  13. Lactoferrin conjugated iron oxide nanoparticles for targeting brain glioma cells in magnetic particle imaging

    NASA Astrophysics Data System (ADS)

    Tomitaka, Asahi; Arami, Hamed; Gandhi, Sonu; Krishnan, Kannan M.

    2015-10-01

    Magnetic Particle Imaging (MPI) is a new real-time imaging modality, which promises high tracer mass sensitivity and spatial resolution directly generated from iron oxide nanoparticles. In this study, monodisperse iron oxide nanoparticles with median core diameters ranging from 14 to 26 nm were synthesized and their surface was conjugated with lactoferrin to convert them into brain glioma targeting agents. The conjugation was confirmed with the increase of the hydrodynamic diameters, change of zeta potential, and Bradford assay. Magnetic particle spectrometry (MPS), performed to evaluate the MPI performance of these nanoparticles, showed no change in signal after lactoferrin conjugation to nanoparticles for all core diameters, suggesting that the MPI signal is dominated by Néel relaxation and thus independent of hydrodynamic size difference or presence of coating molecules before and after conjugations. For this range of core sizes (14-26 nm), both MPS signal intensity and spatial resolution improved with increasing core diameter of nanoparticles. The lactoferrin conjugated iron oxide nanoparticles (Lf-IONPs) showed specific cellular internalization into C6 cells with a 5-fold increase in MPS signal compared to IONPs without lactoferrin, both after 24 h incubation. These results suggest that Lf-IONPs can be used as tracers for targeted brain glioma imaging using MPI.

  14. Power Peaking Effect of OTTO Fuel Scheme Pebble Bed Reactor

    NASA Astrophysics Data System (ADS)

    Setiadipura, T.; Suwoto; Zuhair; Bakhri, S.; Sunaryo, G. R.

    2018-02-01

    Pebble Bed Reactor (PBR) type of Hight Temperature Gas-cooled Reactor (HTGR) is a very interesting nuclear reactor design to fulfill the growing electricity and heat demand with a superior passive safety features. Effort to introduce the PBR design to the market can be strengthen by simplifying its system with the Once-through-then-out (OTTO) cycle PBR in which the pebble fuel only pass the core once. Important challenge in the OTTO fuel scheme is the power peaking effect which limit the maximum nominal power or burnup of the design. Parametric survey is perform in this study to investigate the contribution of different design parameters to power peaking effect of OTTO cycle PBR. PEBBED code is utilized in this study to perform the equilibrium PBR core analysis for different design parameter and fuel scheme. The parameters include its core diameter, height-per-diameter (H/D), power density, and core nominal power. Results of this study show that diameter and H/D effectsare stronger compare to the power density and nominal core power. Results of this study might become an importance guidance for design optimization of OTTO fuel scheme PBR.

  15. From Mixed-Metal MOFs to Carbon-Coated Core-Shell Metal Alloy@Metal Oxide Solid Solutions: Transformation of Co/Ni-MOF-74 to CoxNi1-x@CoyNi1-yO@C for the Oxygen Evolution Reaction.

    PubMed

    Sun, Dengrong; Ye, Lin; Sun, Fangxiang; García, Hermenegildo; Li, Zhaohui

    2017-05-01

    Calcination of the mixed-metal species Co/Ni-MOF-74 leads to the formation of carbon-coated Co x Ni 1-x @Co y Ni 1-y O with a metal core diameter of ∼3.2 nm and a metal oxide shell thickness of ∼2.4 nm embedded uniformly in the ligand-derived carbon matrix. The close proximity of Co and Ni in the mixed-metal Co/Ni-MOF-74 promotes the metal alloying and the formation of a solid solution of metal oxide during the calcination process. The presence of the tightly coated carbon shell prohibits particle agglomeration and stabilizes the Co x Ni 1-x @Co y Ni 1-y O nanoparticles in small size. The Co x Ni 1-x @Co y Ni 1-y O@C derived from Co/Ni-MOF-74 nanocomposites show superior performance for the oxygen evolution reaction (OER). The use of mixed-metal MOFs as precursors represents a powerful strategy for the fabrication of metal alloy@metal oxide solid solution nanoparticles in small size. This method also holds great promise in the development of multifunctional carbon-coated complex core-shell metal/metal oxides owing to the diversified MOF structures and their flexible chemistry.

  16. Programmed Nanoparticle-Loaded Nanoparticles for Deep-Penetrating 3D Cancer Therapy.

    PubMed

    Kim, Jinhwan; Jo, Changshin; Lim, Won-Gwang; Jung, Sungjin; Lee, Yeong Mi; Lim, Jun; Lee, Haeshin; Lee, Jinwoo; Kim, Won Jong

    2018-05-18

    Tumors are 3D, composed of cellular agglomerations and blood vessels. Therapies involving nanoparticles utilize specific accumulations due to the leaky vascular structures. However, systemically injected nanoparticles are mostly uptaken by cells located on the surfaces of cancer tissues, lacking deep penetration into the core cancer regions. Herein, an unprecedented strategy, described as injecting "nanoparticle-loaded nanoparticles" to address the long-lasting problem is reported for effective surface-to-core drug delivery in entire 3D tumors. The "nanoparticle-loaded nanoparticle" is a silica nanoparticle (≈150 nm) with well-developed, interconnected channels (diameter of ≈30 nm), in which small gold nanoparticles (AuNPs) (≈15 nm) with programmable DNA are located. The nanoparticle (AuNPs)-loaded nanoparticles (silica): (1) can accumulate in tumors through leaky vascular structures by protecting the inner therapeutic AuNPs during blood circulation, and then (2) allow diffusion of the AuNPs for penetration into the entire surface-to-core tumor tissues, and finally (3) release a drug triggered by cancer-characteristic pH gradients. The hierarchical "nanoparticle-loaded nanoparticle" can be a rational design for cancer therapies because the outer large nanoparticles are effective in blood circulation and in protection of the therapeutic nanoparticles inside, allowing the loaded small nanoparticles to penetrate deeply into 3D tumors with anticancer drugs. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  17. Core-shell-corona micelles by PS-b-P2VP-b-PEO copolymers: focus on the water-induced micellization process.

    PubMed

    Willet, Nicolas; Gohy, Jean-François; Auvray, Loïc; Varshney, Sunil; Jérôme, Robert; Leyh, Bernard

    2008-04-01

    It is now well established that amphiphilic PS-b-P2VP-b-PEO linear triblock copolymers can form multilayered assemblies, thus core-shell-corona (CSC) micelles, in water. Micellization is triggered by addition of a small amount of water into a dilute solution of the PS-b-P2VP-b-PEO copolymer in a non-selective organic solvent. However, the phenomena that take place at the very beginning of this process are poorly documented. How these copolymer chains are perturbed by addition of water was investigated in this work by light and neutron scattering techniques and transmission electron microscopy. It was accordingly possible to determine the critical water concentration (CWC), the compactness of the nano-objects in solution, their number of aggregation, and their hydrodynamic diameter at each step of the micellization process.

  18. Low-Loss Coupling of Quantum Cascade Lasers into Hollow-Core Waveguides with Single-Mode Output in the 3.7-7.6 μm Spectral Range.

    PubMed

    Patimisco, Pietro; Sampaolo, Angelo; Mihai, Laura; Giglio, Marilena; Kriesel, Jason; Sporea, Dan; Scamarcio, Gaetano; Tittel, Frank K; Spagnolo, Vincenzo

    2016-04-13

    We demonstrated low-loss and single-mode laser beam delivery through hollow-core waveguides (HCWs) operating in the 3.7-7.6 μm spectral range. The employed HCWs have a circular cross section with a bore diameter of 200 μm and metallic/dielectric internal coatings deposited inside a glass capillary tube. The internal coatings have been produced to enhance the spectral response of the HCWs in the range 3.5-12 µm. We demonstrated Gaussian-like outputs throughout the 4.5-7.6 µm spectral range. A quasi single-mode output beam with only small beam distortions was achieved when the wavelength was reduced to 3.7 μm. With a 15-cm-long HCW and optimized coupling conditions, we measured coupling efficiencies of >88% and transmission losses of <1 dB in the investigated infrared spectral range.

  19. Improvement of optical damage in specialty fiber at 266 nm wavelength

    NASA Astrophysics Data System (ADS)

    Tobisch, T.; Ohlmeyer, H.; Zimmermann, H.; Prein, S.; Kirchhof, J.; Unger, S.; Belz, M.; Klein, K.-F.

    2014-02-01

    Improved multimode UV-fibers with core diameters ranging from 70 to 600 μm diameter have been manufactured based on novel preform modifications and fiber processing techniques. Only E'-centers at 214 nm and NBOHC at 260 nm are generated in these fibers. A new generation of inexpensive laser-systems have entered the market and generated a multitude of new and attractive applications in the bio-life science, chemical and material processing field. However, for example pulsed 355 nm Nd:YAG lasers generate significant UV-damages in commercially available fibers. For lower wavelengths, no results on suitable multi-mode or low-mode fibers with high UV resistance at 266 nm wavelength (pulsed 4th harmonic Nd:YAG laser) have been published. In this report, double-clad fibers with 70 μm or 100 μm core diameter and a large claddingto- core ratio will be recommended. Laser-induced UV-damages will be compared between these new fiber type and traditional UV fibers with similar core sizes. Finally, experimental results will be cross compared against broadband cw deuterium lamp damage standards.

  20. Achieving the broader frequency electromagnetic absorber by development of magnetic core-shell composite with tunable shell/core sizes

    NASA Astrophysics Data System (ADS)

    Cheng, Ye; Guo, Yuhang; Zhang, Zhenya; Dong, Songtao; Liu, Suwei; Wang, Hongying

    2018-03-01

    Magnetic absorber has been regarded as the advanced electromagnetic energy transfer material to solve the increasingly high frequency electromagnetic interference issue. Even so, the pure magnetic material, in particular magnetic metal nanoparticle, suffering from the poor chemical stability and strong eddy current effect, thus limits it further application. To overcome this shortage, surrounded the magnetic metal nanoparticle (MPs) with insulated oxide shell has been considered to be an efficient route to suppress such an eddy current effect. Meanwhile, the combined insulated shell with good impedance matching feature, shows a positive role on the electromagnetic energy transfer intensity. In this regard, the binary Fe@α-Fe2O3 composite with the average size of ∼ 20 nm was prepared by a facile self-oxidation reaction. Interestingly, both the core diameter and shell thickness is controllable by controlling the oxide degree. The electromagnetic energy transfer performance revealed the maximum absorption frequency bandwidth of the optimal Fe@α-Fe2O3 composite is up to 5.3 G(8.2-13.5 GHz)under a small coating thickness of 1.5 mm.

  1. Paleoenvironmental reconstruction of lagoonal strata from Sri Lanka using multiple physical properties proxies to assure stratigraphic continuity

    NASA Astrophysics Data System (ADS)

    Ranasinghage, P. N.; Ortiz, J. D.; Moore, A.; Siriwardana, C.

    2009-12-01

    Core collapsing is a common problem in studies of lagoonal sediment cores. Coring liquefied sediments below the water table can lead to collapse of material from upper core drives in to the hole. This can be prevented by casing the hole. But casing is not always possible due to practical issues such as coring device type, resources, or time constraints. In such cases identifying the collapsed material in each drive is necessary to ensure accurate results. Direct visual identification of collapsed portion is not always possible and may not be precise. This study successfully recognized collapsed material using a suite of physical properties measurements including: visible (VIS) reflectance spectroscopy, magnetic susceptibility and grain size spectra. This enables us to use the verified stratigraphically continuous records for paleo-environmental studies. Sediment cores were collected from three coastal lagoons and a swale along south eastern and eastern Sri Lanka. Cores were collected using a customized AMS soil coring device with a 1-m long sample barrel. The metal barrel of this instrument collects a 2.5 cm diameter sample in 1-m long plastic tubes. Coring was conducted to refusal, with a maximum depth of 5 m. Casing was not applied to the holes due to small core diameter and time constrains. Drill holes were placed at locations situated both below and above the water level of the lagoons. A total of 100 m of sediment core were obtained from these locations. After opening the cores, suspected collapsed material was initially identified by visual observation using a high power binocular microscope. Particle size, magnetic susceptibility, X-ray fluorescence (XRF) and Diffuse Spectral Reflectance (DSR) was then measured on all cores at 1-2 cm resolution to precisely define the repeated sediment intervals. Down core variation plots of magnetic susceptibility, CIE L* (lightness), a*(red/green difference), b* (blue and yellow difference) clearly record abrupt changes at core drive boundaries at the presence of collapsed material. The correlation of grain-size spectra from the bottom and top of consecutive drives was used to precisely determine the thickness of the collapsed material between drives. Our analysis of 48 m of core material thus far indicates that ~4.4m or ~9% of the record represents collapsed material which can be excluded from further study. The remaining continuous record was analyzed for paleoenvironmental studies. Down core variation of grain size, geochemical ratios, principle components of DSR and geochemical data, and magnetic susceptibility from all locations indicate a gradual filling of these deep lagoons and a transition from reducing to oxic conditions. According to an age model constructed for a nearby lagoon the onset of regression began ~6,000 years BP. Several instantaneous sedimentation events were recorded in all lagoons. Further studies will be carried out to determine whether these represent tsunami, storm surge, or flood deposits.

  2. Selective control of small versus large diameter axons using infrared laser light (Conference Presentation)

    NASA Astrophysics Data System (ADS)

    Lothet, Emilie H.; Shaw, Kendrick M.; Horn, Charles C.; Lu, Hui; Wang, Yves T.; Jansen, E. Duco; Chiel, Hillel J.; Jenkins, Michael W.

    2016-03-01

    Sensory information is conveyed to the central nervous system via small diameter unmyelinated fibers. In general, smaller diameter axons have slower conduction velocities. Selective control of such fibers could create new clinical treatments for chronic pain, nausea in response to chemo-therapeutic agents, or hypertension. Electrical stimulation can control axonal activity, but induced axonal current is proportional to cross-sectional area, so that large diameter fibers are affected first. Physiologically, however, synaptic inputs generally affect small diameter fibers before large diameter fibers (the size principle). A more physiological modality that first affected small diameter fibers could have fewer side effects (e.g., not recruiting motor axons). A novel mathematical analysis of the cable equation demonstrates that the minimum length along the axon for inducing block scales with the square root of axon diameter. This implies that the minimum length along an axon for inhibition will scale as the square root of axon diameter, so that lower radiant exposures of infrared light will selectively affect small diameter, slower conducting fibers before those of large diameter. This prediction was tested in identified neurons from the marine mollusk Aplysia californica. Radiant exposure to block a neuron with a slower conduction velocity (B43) was consistently lower than that needed to block a faster conduction velocity neuron (B3). Furthermore, in the vagus nerve of the musk shrew, lower radiant exposure blocked slow conducting fibers before blocking faster conducting fibers. Infrared light can selectively control smaller diameter fibers, suggesting many novel clinical treatments.

  3. Design of measuring system for wire diameter based on sub-pixel edge detection algorithm

    NASA Astrophysics Data System (ADS)

    Chen, Yudong; Zhou, Wang

    2016-09-01

    Light projection method is often used in measuring system for wire diameter, which is relatively simpler structure and lower cost, and the measuring accuracy is limited by the pixel size of CCD. Using a CCD with small pixel size can improve the measuring accuracy, but will increase the cost and difficulty of making. In this paper, through the comparative analysis of a variety of sub-pixel edge detection algorithms, polynomial fitting method is applied for data processing in measuring system for wire diameter, to improve the measuring accuracy and enhance the ability of anti-noise. In the design of system structure, light projection method with orthogonal structure is used for the detection optical part, which can effectively reduce the error caused by line jitter in the measuring process. For the electrical part, ARM Cortex-M4 microprocessor is used as the core of the circuit module, which can not only drive double channel linear CCD but also complete the sampling, processing and storage of the CCD video signal. In addition, ARM microprocessor can complete the high speed operation of the whole measuring system for wire diameter in the case of no additional chip. The experimental results show that sub-pixel edge detection algorithm based on polynomial fitting can make up for the lack of single pixel size and improve the precision of measuring system for wire diameter significantly, without increasing hardware complexity of the entire system.

  4. Fiber optic muzzle brake tip for reducing fiber burnback and stone retropulsion during thulium fiber laser lithotripsy.

    PubMed

    Hutchens, Thomas C; Gonzalez, David A; Irby, Pierce B; Fried, Nathaniel M

    2017-01-01

    The experimental thulium fiber laser (TFL) is being explored as an alternative to the current clinical gold standard Holmium:YAG laser for lithotripsy. The near single-mode TFL beam allows coupling of higher power into smaller optical fibers than the multimode Holmium laser beam profile, without proximal fiber tip degradation. A smaller fiber is desirable because it provides more space in the ureteroscope working channel for increased saline irrigation rates and allows maximum ureteroscope deflection. However, distal fiber tip burnback increases as fiber diameter decreases. Previous studies utilizing hollow steel sheaths around recessed distal fiber tips reduced fiber burnback but increased stone retropulsion. A “fiber muzzle brake” was tested for reducing both fiber burnback and stone retropulsion by manipulating vapor bubble expansion. TFL lithotripsy studies were performed at 1908 nm, 35 mJ, 500 ?? ? s , and 300 Hz using a 100 - ? m -core fiber. The optimal stainless steel muzzle brake tip tested consisted of a 1-cm-long, 560 - ? m -outer-diameter, 360 - ? m -inner-diameter tube with a 275 - ? m -diameter through hole located 250 ?? ? m from the distal end. The fiber tip was recessed a distance of 500 ?? ? m . Stone phantom retropulsion, fiber tip burnback, and calcium oxalate stone ablation studies were performed ex vivo. Small stones with a mass of 40 ± 4 ?? mg and 4-mm-diameter were ablated over a 1.5-mm sieve in 25 ± 4 ?? s

  5. Thermo-optical characterization of cadmium selenide/zinc sulfide (CdSe/ZnS) quantum dots embedded in biocompatible materials.

    PubMed

    Pilla, Viviane; Alves, Leandro P; Iwazaki, Adalberto N; Andrade, Acácio A; Antunes, Andrea; Munin, Egberto

    2013-09-01

    Cadmium selenide/zinc sulfide (CdSe/ZnS) core-shell quantum dots (QDs) embedded in biocompatible materials were thermally and optically characterized with a thermal lens (TL) technique. Transient TL measurements were performed with a mode-mismatched, dual-beam (excitation and probe) configuration. A thermo-optical study of the CdSe/ZnS QDs was performed for different core diameters (3.5, 4.0, 5.2, and 6.6 nm) in aqueous solution and synthetic saliva, and three different core diameters (2.4, 2.9, and 4.1 nm) embedded in restorative dental resin (0.025% by mass). The thermal diffusivity results are characteristic of the biocompatible matrices. The radiative quantum efficiencies for aqueous solution and biofluid materials are dependent on the core size of the CdSe/ZnS core-shell QDs. The results obtained from the fluorescence spectral measurements for the biocompatible materials support the TL results.

  6. Apparatus for measuring surface particulate contamination

    DOEpatents

    Woodmansee, Donald E.

    2002-01-01

    An apparatus for measuring surface particulate contamination includes a tool for collecting a contamination sample from a target surface, a mask having an opening of known area formed therein for defining the target surface, and a flexible connector connecting the tool to the mask. The tool includes a body portion having a large diameter section defining a surface and a small diameter section extending from the large diameter section. A particulate collector is removably mounted on the surface of the large diameter section for collecting the contaminants. The tool further includes a spindle extending from the small diameter section and a spool slidingly mounted on the spindle. A spring is disposed between the small diameter section and the spool for biasing the spool away from the small diameter section. An indicator is provided on the spindle so as to be revealed when the spool is pressed downward to compress the spring.

  7. Room temperature synthesis and optical properties of small diameter (5 nm) ZnO nanorod arrays.

    PubMed

    Cho, Seungho; Jang, Ji-Wook; Lee, Jae Sung; Lee, Kun-Hong

    2010-10-01

    We report a simple wet-chemical synthesis of ∼5 nm diameter ZnO nanorod arrays at room temperature (20 °C) and normal atmospheric pressure (1 atm) and their optical properties. They were single crystalline in nature, and grew in the [001] direction. These small diameter ZnO nanorod arrays can also be synthesized at 0 °C. Control experiments were also conducted. On the basis of the results, we propose a mechanism for the spontaneous growth of the small diameter ZnO structures. The optical properties of the 5 nm diameter ZnO nanorod arrays synthesized using this method were probed by UV-Visible diffuse reflectance spectroscopy. A clear blue-shift, relative to the absorption band from 50 nm diameter ZnO nanorod arrays, was attributed to the quantum confinement effects caused by the small nanocrystal size in the 5 nm diameter ZnO nanorods.

  8. Size resolved Internally Mixed Black Carbon and the Absorption Enhancement in the Indo-Gangetic Plain due to internally mixed BC

    NASA Astrophysics Data System (ADS)

    Tripathi, S. N.; Thamban, N.

    2017-12-01

    Indo-Gangetic Plain (IGP) is one of the most populated and polluted regions in northern India. Even though IGP is a well-known "absorbing aerosol hotspot", information of BC mixing state in IGP is mostly unknown. Our calculation on size resolved mixing state in IGP shown that the mixing state of BC changes with the core diameter of BC. The majority of BC particle were thickly coated ( 80%) at lower diameter (75-125 nm) and the externally mixed BC fraction was gradually increased at higher core diameter of BC (125-250 nm). The mean fraction of "thickly coated BC" particles (fTCBC) was found to be 61.6% for a BC core diameter of 70 to 450 nm, indicating that a large fraction of BC particles was internally mixed in IGP. The fTCBC increased after sunrise with a peak at about noontime, indicating that the formation of secondary organic aerosol under active photochemistry can enhance organic coating on a core of black carbon. A positive correlation between the fTCBC and the mass absorption cross-section at 781nm (MAC781) was also observed (r=0.58). Our results identify that the observed fTCBC in IGP could amplify the MAC781 approximately by a factor of 1.8, which may catalyze the positive radiative forcing.

  9. Measurement Sensitivity Of Liquid Droplet Parameters Using Optical Fibers

    NASA Astrophysics Data System (ADS)

    Das, Alok K.; Mandal, Anup K.

    1990-02-01

    A new clad probing technique is used to measure the size, number, refractive index and viscosity of liquid droplets sprayed from a pressure nozzle on an uncoated core-clad fiber. The probe monitors the clad mode power loss within the leaky ray zone represented as a three region fiber. Liquid droplets measured are Glycerine, commercial grade Turpentine, Linseed oil and some oil mixtures. The measurement sensitivity depends on probing conditions and clad diameter which is observed experimentally and verified analytically. A maximum sensitivity is obtained for the tapered probe-fiber diameter made equal to the clad thickness. A slowly tapered probe-fiber and a small end angle as well as separation of the sensor-fiber and the probe-fiber further improve the sensitivity. Under the best probing condition for 90-percent Glycerine droplets of - 50 micron diameter and a 50/125 micron sensor fiber with clad refractive index of 1.465 and 0.2 NA, the measured sensitivity per drop is 0.015 and 0.006 dB, respectively, for (10-20) and (100-200) droplets. Sensitivities for different systems are shown. The sensitivity is optimized by choosing proper fiber for known liquids.

  10. Ultrathin forward-imaging short multimode fiber probe for full-field optical coherence microscopy

    NASA Astrophysics Data System (ADS)

    Sato, Manabu; Saito, Daisuke; Shouji, Kou; Kurotani, Reiko; Abe, Hiroyuki; Nishidate, Izumi

    2016-12-01

    To extend the applications of optical coherence tomography (OCT) to the fields of physiology and clinical medicine, less invasive, robust, and reliable optical probes are required. Thus, we demonstrate an ultrathin forward-imaging short multimode fiber (SMMF) optical coherence microscopy (OCM) probe with a 50 μm core diameter, 125 μm total diameter, and 5.12 mm length. Imaging conditions and magnification were analyzed, and they correspond closely to the measured results. The dispersion of the SMMF was investigated, and the modal dispersion coefficient was found to be 2.3% of the material dispersion coefficient. The axial resolution was minimized at 2.15 μm using a 0.885-mm-thick dispersion compensator. The lateral resolution was evaluated to be 4.38 μm using a test pattern. The contrast of the OCM images was 5.7 times higher than that of the signal images owing to the coherence gate. The depth of focus and diameter of the field of view were measured to be 60 μm and 40-50 μm, respectively. OCM images of the dried fins of small fish (Medaka) were measured and internal structures could be recognized.

  11. Micro/Nanofibre Optical Sensors: Challenges and Prospects

    PubMed Central

    Tong, Limin

    2018-01-01

    Micro/nanofibres (MNFs) are optical fibres with diameters close to or below the vacuum wavelength of visible or near-infrared light. Due to its wavelength- or sub-wavelength scale diameter and relatively large index contrast between the core and cladding, an MNF can offer engineerable waveguiding properties including optical confinement, fractional evanescent fields and surface intensity, which is very attractive to optical sensing on the micro and nanometer scale. In particular, the waveguided low-loss tightly confined large fractional evanescent fields, enabled by atomic level surface roughness and extraordinary geometric and material uniformity in a glass MNF, is one of its most prominent merits in realizing optical sensing with high sensitivity and great versatility. Meanwhile, the mesoporous matrix and small diameter of a polymer MNF, make it an excellent host fibre for functional materials for fast-response optical sensing. In this tutorial, we first introduce the basics of MNF optics and MNF optical sensors, and review the progress and current status of this field. Then, we discuss challenges and prospects of MNF sensors to some extent, with several clues for future studies. Finally, we conclude with a brief outlook for MNF optical sensors.

  12. Design of dual-diameter nanoholes for efficient solar-light harvesting

    PubMed Central

    2014-01-01

    A dual-diameter nanohole (DNH) photovoltaic system is proposed, where a top (bottom) layer with large (small) nanoholes is used to improve the absorption for the short-wavelength (long-wavelength) solar incidence, leading to a broadband light absorption enhancement. Through three-dimensional finite-element simulation, the core device parameters, including the lattice constant, nanohole diameters, and nanohole depths, are engineered in order to realize the best light-matter coupling between nanostructured silicon and solar spectrum. The designed bare DNH system exhibits an outstanding absorption capability with a photocurrent density (under perfect internal quantum process) predicted to be 27.93 mA/cm2, which is 17.39%, 26.17%, and over 100% higher than the best single-nanohole (SNH) system, SNH system with an identical Si volume, and equivalent planar configuration, respectively. Considering the fabrication feasibility, a modified DNH system with an anti-reflection coating and back silver reflector is examined by simulating both optical absorption and carrier transport in a coupled way in frequency and three-dimensional spatial domains, achieving a light-conversion efficiency of 13.72%. PACS 85.60.-q; Optoelectronic device; 84.60.Jt; Photovoltaic conversion PMID:25258605

  13. Compact Fast Ignition experiments using Joule-class tailored drive pulses under counterbeam configuration

    NASA Astrophysics Data System (ADS)

    Mori, Yoshitaka; Hanayama, Ryohei; Ishii, Katsuhiro; Kitagawa, Yoneyoshi; Sekine, Takashi; Takeuchi, Yasuki; Kurita, Takashi; Katoh, Yoshinori; Satoh, Nakahiro; Kurita, Norio; Kawashima, Toshiyuki; Komeda, Osamu; Hioki, Tatsumi; Motohiro, Tomoyoshi; Sunahara, Atsushi; Sentoku, Yasuhiko; Miura, Eisuke; Iwamoto, Akifumi; Sakagami, Hitoshi

    2017-10-01

    Fast ignition (FI) is a form of inertial confinement fusion in which the ignition step and the compression step are separate processes resulting in a reduction of the symmetry requirement for hot spot generation. One of the problems of FI so far are the accessibility of an ignition laser pulse into the assembled core in which the driver energy is converted into relativistic electrons produced in the laser-plasma interaction. We have experimentally demonstrated that a tailored-pulse-assembled core with a diameter of 70 μ m, originally a deuterated polystyrene spherical shell of 500 μ m diameter, is flashed by directly counter irradiating 0.8 J/110 fs laser pulses [Y. MORI et al., PRL 2016]. This result indicates that once the assembled core is squeezed into the target center, the heating lasers can access the core's; edges and deposit their energy into the core. In this talk, we will discuss the heating effects in relation to formation of the assembled core.

  14. 78 FR 56864 - Small Diameter Graphite Electrodes From the People's Republic of China: Affirmative Final...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-09-16

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-570-929] Small Diameter Graphite... (Department) determines that imports from the People's Republic of China (PRC) of graphite electrodes... Act of 1930, as amended (the Act).\\1\\ \\1\\ See Antidumping Duty Order: Small Diameter Graphite...

  15. Microencapsulation Of Living Cells

    NASA Technical Reports Server (NTRS)

    Chang, Manchium; Kendall, James M.; Wang, Taylor G.

    1989-01-01

    In experimental technique, living cells and other biological materials encapsulated within submillimeter-diameter liquid-filled spheres. Sphere material biocompatible, tough, and compliant. Semipermeable, permitting relatively small molecules to move into and out of sphere core but preventing passage of large molecules. New technique promises to make such spherical capsules at high rates and in uniform, controllable sizes. Capsules injected into patient through ordinary hypodermic needle. Promising application for technique in treatment of diabetes. Also used to encapsulate pituitary cells and thyroid hormone adrenocortical cells for treatment of other hormonal disorders, to encapsulate other secreting cells for transplantation, and to package variety of pharmaceutical products and agricultural chemicals for controlled release.

  16. 20 W continuous-wave cladding-pumped Nd-doped fiber laser at 910 nm.

    PubMed

    Laroche, M; Cadier, B; Gilles, H; Girard, S; Lablonde, L; Robin, T

    2013-08-15

    We demonstrate a double-clad fiber laser operating at 910 nm with a record power of 20 W. Laser emission on the three-level scheme is enabled by the combination of a small inner cladding-to-core diameter ratio and a high brightness pump source at 808 nm. A laser conversion efficiency as high as 44% was achieved in CW operating regime by using resonant fiber Bragg reflectors at 910 nm that prevent the lasing at the 1060 nm competing wavelength. Furthermore, in a master oscillator power-amplifier scheme, an amplified power of 14.8 W was achieved at 914 nm in the same fiber.

  17. Estimating air-drying times of small-diameter ponderosa pine and Douglas-fir logs

    Treesearch

    William T. Simpson; Xiping Wang

    2004-01-01

    One potential use for small-diameter ponderosa pine and Douglas-fir timber is in log form. Many potential uses of logs require some degree of drying. Even though these small diameters may be considered small in the forestry context, their size when compared to typical lumber thickness dimensions is large. These logs, however, may require uneconomically long kiln-drying...

  18. Extrusion of small-diameter, thin-wall tungsten tubing

    NASA Technical Reports Server (NTRS)

    Blankenship, C. P.; Gyorgak, C. A.

    1967-01-01

    Small-diameter, thin-wall seamless tubing of tungsten has been fabricated in lengths of up to 10 feet by hot extrusion over a floating mandrel. Extrusion of 0.50-inch-diameter tubing over 0.4-inch-diameter mandrels was accomplished at temperatures ranging from 3000 degrees to 4000 degrees F.

  19. Multi-scale imaging and elastic simulation of carbonates

    NASA Astrophysics Data System (ADS)

    Faisal, Titly Farhana; Awedalkarim, Ahmed; Jouini, Mohamed Soufiane; Jouiad, Mustapha; Chevalier, Sylvie; Sassi, Mohamed

    2016-05-01

    Digital Rock Physics (DRP) is an emerging technology that can be used to generate high quality, fast and cost effective special core analysis (SCAL) properties compared to conventional experimental techniques and modeling techniques. The primary workflow of DRP conssits of three elements: 1) image the rock sample using high resolution 3D scanning techniques (e.g. micro CT, FIB/SEM), 2) process and digitize the images by segmenting the pore and matrix phases 3) simulate the desired physical properties of the rocks such as elastic moduli and velocities of wave propagation. A Finite Element Method based algorithm, that discretizes the basic Hooke's Law equation of linear elasticity and solves it numerically using a fast conjugate gradient solver, developed by Garboczi and Day [1] is used for mechanical and elastic property simulations. This elastic algorithm works directly on the digital images by treating each pixel as an element. The images are assumed to have periodic constant-strain boundary condition. The bulk and shear moduli of the different phases are required inputs. For standard 1.5" diameter cores however the Micro-CT scanning reoslution (around 40 μm) does not reveal smaller micro- and nano- pores beyond the resolution. This results in an unresolved "microporous" phase, the moduli of which is uncertain. Knackstedt et al. [2] assigned effective elastic moduli to the microporous phase based on self-consistent theory (which gives good estimation of velocities for well cemented granular media). Jouini et al. [3] segmented the core plug CT scan image into three phases and assumed that micro porous phase is represented by a sub-extracted micro plug (which too was scanned using Micro-CT). Currently the elastic numerical simulations based on CT-images alone largely overpredict the bulk, shear and Young's modulus when compared to laboratory acoustic tests of the same rocks. For greater accuracy of numerical simulation prediction, better estimates of moduli inputs for this current unresolved phase is important. In this work we take a multi-scale imaging approach by first extracting a smaller 0.5" core and scanning at approx 13 µm, then further extracting a 5mm diameter core scanned at 5 μm. From this last scale, region of interests (containing unresolved areas) are identified for scanning at higher resolutions using Focalised Ion Beam (FIB/SEM) scanning technique reaching 50 nm resolution. Numerical simulation is run on such a small unresolved section to obtain a better estimate of the effective moduli which is then used as input for simulations performed using CT-images. Results are compared with expeirmental acoustic test moduli obtained also at two scales: 1.5" and 0.5" diameter cores.

  20. 77 FR 59374 - Certain Small Diameter Carbon and Alloy Seamless Standard, Line and Pressure Pipe (Under 41/2

    Federal Register 2010, 2011, 2012, 2013, 2014

    2012-09-27

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-588-851] Certain Small Diameter Carbon and Alloy Seamless Standard, Line and Pressure Pipe (Under 4\\1/2\\ Inches) From Japan: Rescission... antidumping order on certain small diameter carbon and alloy seamless standard, line and pressure pipe (under...

  1. Method for applying pyrolytic carbon coatings to small particles

    DOEpatents

    Beatty, Ronald L.; Kiplinger, Dale V.; Chilcoat, Bill R.

    1977-01-01

    A method for coating small diameter, low density particles with pyrolytic carbon is provided by fluidizing a bed of particles wherein at least 50 per cent of the particles have a density and diameter of at least two times the remainder of the particles and thereafter recovering the small diameter and coated particles.

  2. Forest Products Laboratory research program on small-diameter material.

    Treesearch

    2000-01-01

    Forests in the United States contain a significant amount of small-diameter and underutilized material. These overstocked stands not only increase the risk of insect, disease, fire, and drought damage, but also are costly to remove. Finding economical and marketable uses for small-diameter and underutilized material would alleviate these problems while improving...

  3. 75 FR 64250 - Small Diameter Graphite Electrodes From the People's Republic of China: Extension of Time Limit...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-10-19

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-570-929] Small Diameter Graphite Electrodes From the People's Republic of China: Extension of Time Limit for the Preliminary Results of the... review of the antidumping duty order on small diameter graphite electrodes from the People's Republic of...

  4. Preparation of paclitaxel/chitosan co-assembled core-shell nanofibers for drug-eluting stent

    NASA Astrophysics Data System (ADS)

    Tang, Jing; Liu, Yongjia; Zhu, Bangshang; Su, Yue; Zhu, Xinyuan

    2017-01-01

    The paclitaxel/chitosan (PTX/CS) core-shell nanofibers (NFs) are easily prepared by co-assembly of PTX and CS and used in drug-eluting stent. The mixture solution of PTX (dissolved in ethanol) and CS (dissolved in 1% acetic acid water solution) under sonication will make the formation of NFs, in which small molecule PTX co-assembles with biomacromolecular CS through non-covalent interactions. The obtained NFs are tens to hundreds nanometers in diameter and millimeter level in length. Furthermore, the structure of PTX/CS NFs was characterized by confocal laser scanning microscopy (CLSM), zeta potential, X-ray photoelectron spectroscopy (XPS) and nanoscale infra-red (nanoIR), which provided evidences demonstrated that PTX/CS NFs are core-shell structures. The 'shell' of CS wrapped outside of the NFs, while PTX is located in the core. Thus it resulted in high drug loading content (>40 wt.%). The well-controlled drug release, low cytotoxicity and good haemocompatibility were also found in drug carrier system of PTX/CS NFs. In addition, the hydrophilic and flexible properties of NFs make them easily coating and filming on stent to prepare drug-eluting stent (DES). Therefore, this study provides a convenient method to prepare high PTX loaded NFs, which is a promising nano-drug carrier used for DES and other biomedical applications. The possible molecular mechanism of PTX and CS co-assembly and core-shell nanofiber formation is also explored.

  5. High performance carbon nanotube-Si core-shell wires with a rationally structured core for lithium ion battery anodes.

    PubMed

    Fan, Yu; Zhang, Qing; Lu, Congxiang; Xiao, Qizhen; Wang, Xinghui; Tay, Beng Kang

    2013-02-21

    Core-shell Si nanowires are very promising anode materials. Here, we synthesize vertically aligned carbon nanotubes (CNTs) with relatively large diameters and large inter-wire spacing as core wires and demonstrate a CNT-Si core-shell wire composite as a lithium ion battery (LIB) anode. Owing to the rationally engineered core structure, the composite shows good capacity retention and rate performance. The excellent performance is superior to most core-shell nanowires previously reported.

  6. Lumber volume and value recovery from small-diameter black cherry, sugar maple, and red oak logs

    Treesearch

    Jan Wiedenbeck; Matthew Scholl; Paul Blankenhorn; Chuck Ray

    2017-01-01

    While only a very small percentage of hardwood logs sawn by conventional sawmills in the U.S. have small-end diameters less than 10 in, portable and scragg mills often saw smaller logs. With the closure of regionally important oriented strand board and pulpwood operations, small-diameter logs are considered to have no value in some markets. This study was...

  7. Fabrication and electrical characterization of sub-micron diameter through-silicon via for heterogeneous three-dimensional integrated circuits

    NASA Astrophysics Data System (ADS)

    Abbaspour, R.; Brown, D. K.; Bakir, M. S.

    2017-02-01

    This paper presents the fabrication and electrical characterization of high aspect-ratio (AR) sub-micron diameter through silicon vias (TSVs) for densely interconnected three-dimensional (3D) stacked integrated circuits (ICs). The fabricated TSV technology features an AR of 16:1 with 680 nm diameter copper (Cu) core and 920 nm overall diameter. To address the challenges in scaling TSVs, scallop-free low roughness nano-Bosch silicon etching and direct Cu electroplating on a titanium-nitride (TiN) diffusion barrier layer have been developed as key enabling modules. The electrical resistance of the sub-micron TSVs is measured to be on average 1.2 Ω, and the Cu resistivity is extracted to be approximately 2.95 µΩ cm. Furthermore, the maximum achievable current-carrying capacity (CCC) of the scaled TSVs is characterized to be approximately 360 µA for the 680 nm Cu core.

  8. An innovative piston corer for large‐volume sediment samples

    PubMed Central

    Haselmair, Alexandra; Stachowitsch, Michael; Zuschin, Martin

    2016-01-01

    Abstract Coring is one of several standard procedures to extract sediments and their faunas from open marine, estuarine, and limnic environments. Achieving sufficiently deep penetration, obtaining large sediment volumes in single deployments, and avoiding sediment loss upon retrieval remain problematic. We developed a piston corer with a diameter of 16 cm that enables penetration down to 1.5 m in a broad range of soft bottom types, yields sufficient material for multiple analyses, and prevents sediment loss due to a specially designed hydraulic core catcher. A novel extrusion system enables very precise slicing and preserves the original sediment stratification by keeping the liners upright. The corer has moderate purchase costs and a robust and simple design that allows for a deployment from relatively small vessels as available at most marine science institutions. It can easily be operated by two to three researchers rather than by specially trained technicians. In the northern Adriatic Sea, the corer successfully extracted more than 50 cores from a range of fine mud to coarse sand, at water depths from three to 45 m. The initial evaluation of the cores demonstrated their usefulness for fauna sequences along with heavy metal, nutrient and pollutant analyses. Their length is particularly suited for historical ecological work requiring sedimentary and faunal sequences to reconstruct benthic communities over the last millennia. PMID:28111529

  9. Structure of Immune Stimulating Complex Matrices and Immune Stimulating Complexes in Suspension Determined by Small-Angle X-Ray Scattering

    PubMed Central

    Pedersen, Jan Skov; Oliveira, Cristiano L.P.; Hübschmann, Henriette Baun; Arleth, Lise; Manniche, Søren; Kirkby, Nicolai; Nielsen, Hanne Mørck

    2012-01-01

    Immune stimulating complex (ISCOM) particles consisting of a mixture of Quil-A, cholesterol, and phospholipids were structurally characterized by small-angle x-ray scattering (SAXS). The ISCOM particles are perforated vesicles of very well-defined structures. We developed and implemented a novel (to our knowledge) modeling method based on Monte Carlo simulation integrations to describe the SAXS data. This approach is similar to the traditional modeling of SAXS data, in which a structure is assumed, the scattering intensity is calculated, and structural parameters are optimized by weighted least-squares methods when the model scattering intensity is fitted to the experimental data. SAXS data from plain ISCOM matrix particles in aqueous suspension, as well as those from complete ISCOMs (i.e., with an antigen (tetanus toxoid) incorporated) can be modeled as a polydisperse distribution of perforated bilayer vesicles with icosahedral, football, or tennis ball structures. The dominating structure is the tennis ball structure, with an outer diameter of 40 nm and with 20 holes 5–6 nm in diameter. The lipid bilayer membrane is 4.6 nm thick, with a low-electron-density, 2.0-nm-thick hydrocarbon core. Surprisingly, in the ISCOMs, the tetanus toxoid is located just below the membrane inside the particles. PMID:22677391

  10. Soil respiration and root biomass responses to burning in calabrian pine (Pinus brutia) stands in Edirne, Turkey.

    PubMed

    Tufekcioglu, Aydin; Kucuk, Mehmet; Bilmis, Tuncay; Altun, Lokman; Yilmaz, Murat

    2010-01-01

    In this study soil properties and root biomass responses to prescribed fire were investigated in 25-30 year-old calabrian pine (Pinus brutia Ten.) stands in Edirne, Turkey. The stands were established by planting and were subjected to prescribed burning in July 2005. Soil respiration rates were determined every two months using the soda-lime method over a two-year period. Fine (> or = 2 mm diameter) and small root (> 2-5 mm diameter) biomass were sampled approximately bimonthly using the sequential coring method. Soil respiration rates in burned sites were significantly higher than in control sites during the summer season but there was no significant difference in the other seasons. Soil respiration rates were correlated significantly with soil moisture and soil temperature. Fine and small root biomass were significantly lower in burned sites than in control sites. Mean fine root biomass values were 3204 kg ha(-1) for burned and 3772 kg ha(-1) for control sites. Annual soil CO2 releases totaled 515 g Cm(-2) for burned and 418 g C m(-2) for control sites. Our results indicate that, depending on site conditions, fire could be used successfully as a tool in the management of calabrian pine stands in the study area.

  11. Tunable engineered skin mechanics via coaxial electrospun fiber core diameter.

    PubMed

    Blackstone, Britani Nicole; Drexler, Jason William; Powell, Heather Megan

    2014-10-01

    Autologous engineered skin (ES) offers promise as a treatment for massive full thickness burns. Unfortunately, ES is orders of magnitude weaker than normal human skin causing it to be difficult to apply surgically and subject to damage by mechanical shear in the early phases of engraftment. In addition, no manufacturing strategy has been developed to tune ES biomechanics to approximate the native biomechanics at different anatomic locations. To enhance and tune ES biomechanics, a coaxial (CoA) electrospun scaffold platform was developed from polycaprolactone (PCL, core) and gelatin (shell). The ability of the coaxial fiber core diameter to control both scaffold and tissue mechanics was investigated along with the ability of the gelatin shell to facilitate cell adhesion and skin development compared to pure gelatin, pure PCL, and a gelatin-PCL blended fiber scaffold. CoA ES exhibited increased cellular adhesion and metabolism versus PCL alone or gelatin-PCL blend and promoted the development of well stratified skin with a dense dermal layer and a differentiated epidermal layer. Biomechanics of the scaffold and ES scaled linearly with core diameter suggesting that this scaffold platform could be utilized to tailor ES mechanics for their intended grafting site and reduce graft damage in vitro and in vivo.

  12. Principles of quasi-equivalence and Euclidean geometry govern the assembly of cubic and dodecahedral cores of pyruvate dehydrogenase complexes.

    PubMed

    Izard, T; Aevarsson, A; Allen, M D; Westphal, A H; Perham, R N; de Kok, A; Hol, W G

    1999-02-16

    The pyruvate dehydrogenase multienzyme complex (Mr of 5-10 million) is assembled around a structural core formed of multiple copies of dihydrolipoyl acetyltransferase (E2p), which exhibits the shape of either a cube or a dodecahedron, depending on the source. The crystal structures of the 60-meric dihydrolipoyl acyltransferase cores of Bacillus stearothermophilus and Enterococcus faecalis pyruvate dehydrogenase complexes were determined and revealed a remarkably hollow dodecahedron with an outer diameter of approximately 237 A, 12 large openings of approximately 52 A diameter across the fivefold axes, and an inner cavity with a diameter of approximately 118 A. Comparison of cubic and dodecahedral E2p assemblies shows that combining the principles of quasi-equivalence formulated by Caspar and Klug [Caspar, D. L. & Klug, A. (1962) Cold Spring Harbor Symp. Quant. Biol. 27, 1-4] with strict Euclidean geometric considerations results in predictions of the major features of the E2p dodecahedron matching the observed features almost exactly.

  13. Production and cost of harvesting, processing, and transporting small-diameter (< 5 inches) trees for energy

    Treesearch

    Fei Pan; Han-Sup Han; Leonard R. Johnson; William J. Elliot

    2008-01-01

    Dense, small-diameter stands generally require thinning from below to improve fire-tolerance. The resulting forest biomass can be used for energy production. The cost of harvesting, processing, and transporting small-diameter trees often exceeds revenues due to high costs associated with harvesting and transportation and low market values for forest biomass....

  14. Options for small-diameter hardwood utilization: past and present

    Treesearch

    Matthew S. Bumgardner; Bruce G. Hansen; Albert T. Schuler; Philip A. Araman

    2000-01-01

    Effective and maximum value use of small-diameter hardwood timber has long been of interest to forest managers and researchers. In addition to being a significant component of the standing forest base, small-diameter hardwoods often are available after thinning or other tending operations. Although the use of this material is important to achieving healthy and...

  15. Evaluation of roll-off trailers in small-diameter applications

    Treesearch

    Bob Rummer; John Klepac

    2003-01-01

    Concern about wildfire in overstocked forests of the western U.S. has led to increased emphasis on extraction of small-diameter material. Removing this material improves forest health, reduces fuel loading, and may generate value that can be used to offset the costs of operation. However, the cost of small-diameter operations (both in-woods and secondary processing)...

  16. Small-diameter success stories II

    Treesearch

    Jean Livingston

    2006-01-01

    Many of our national forests are in critical need of restoration. These forests are dense, with an abundance of small-diameter, tightly spaced trees and underbrush that can contribute to the rapid growth of fire. If economic and value-added uses for this small-diameter and unmerchantable material can be found, forest restoration costs could be offset and catastrophic...

  17. Options for Small-Diameter Hardwood Utilization: Past and Present

    Treesearch

    Matthew S. Bumgardner; Bruce G. Hansen; Albert T. Schuler; Philip A. Araman; Philip A. Araman

    2001-01-01

    Effective and maximum value use of small-diameter hardwood timber has long been of interest to forest managers and researchers. In addition to being a significant component of the standing forest base, small-diameter hardwoods often are available after thinning or other tending operations. Although the use of this material is important to achieving healthy and...

  18. PS-b-PMMA/PLA blends for nanoporous templates with hierarchical and tunable pore size

    NASA Astrophysics Data System (ADS)

    Nguyen, Thi-Hoa; Vayer, Marylène; Sinturel, Christophe

    2018-01-01

    Blends of poly(styrene)-block-poly(methyl methacrylate) (PS-b-PMMA) and poly(lactide) (PLA) were deposited in the form of thin films on the surface of modified silicon wafers and exposed to tetrahydrofuran (THF) vapor annealing. It was shown that in specific experimental conditions, a core-shell morphology consisting in cylinders with a PMMA shell and a PLA core, within a continuous matrix of PS, was formed. In this case, PLA naturally segregated in the core of the PMMA cylinders, minimizing the PS/PLA interaction, which constitutes the most incompatible pair (the interaction strength between the various components was confirmed in thin films of the corresponding polymer blends). Compared to other block copolymer/homopolymer blends described in the literature, this system exhibits unexpected high increase of the characteristic lengths of the system (center-to-center distance and diameter). This was attributed to a partial solubilization of the PLA in the PMMA corona (the two polymers are highly compatible), inducing an enhanced level of PS and PLA stretching caused by the strong repulsion between these two polymers. The selective extraction of the PLA yielded to porous domains with small dimensions (6 ± 2.5 nm), reaching the performances that are currently attained in highly incompatible block polymers with low molecular weight. Further PMMA removal revealed a second porosity level, with higher pores diameter and center-to-center distance compared to the neat PS-b-PMMA system. This work highlights how PS-b-PMMA, that currently represents one of the industrial standards nanoporous template precursors, can be modified in an easy and costless approach using PLA homopolymer addition.

  19. Sans study of reverse micelles formed upon extraction of inorganic acids by TBP in n-octane.

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Chiarizia, R.; Briand, A.; Jensen, M. P.

    2008-01-01

    Small-angle neutron scattering (SANS) data for n-octane solutions of TBP loaded with progressively larger amounts of HNO{sub 3}, HClO{sub 4}, H{sub 2}SO{sub 4}, and H{sub 3}PO{sub 4} up to and beyond the LOC (limiting organic concentration of acid) condition, were interpreted using the Baxter model for hard spheres with surface adhesion. The coherent picture of the behavior of the TBP solutions derived from the SANS investigation discussed in this paper confirmed our recently developed model for third phase formation. This model analyses the features of the scattering data in the low Q region as arising from van der Waals interactionsmore » between the polar cores of reverse micelles. Our SANS data indicated that the TBP micelles swell when acid and water are extracted into their polar core. The swollen micelles have critical diameters ranging from 15 to 22 {angstrom}, and polar core diameters between 10 and 15 {angstrom}, depending on the specific system. At the respective LOC conditions, the TBP weight-average aggregation numbers are -4 for HClO{sub 4}, -6 for H2SO{sub 4}, -7 for HCl, and -10 for H{sub 3}PO{sub 4}. The comparison between the behavior of HNO{sub 3}, a non-third phase forming acid, and the other acids provided an explanation of the effect of the water molecules present in the polar core of the micelles on third phase formation. The thickness of the lipophilic shell of the micelles indicated that the butyl groups of TBP lie at an angle of -25 degrees relative to a plane tangent to the micellar core. The critical energy of intermicellar attraction, U(r), was about -2 k{sub B}T for all the acids investigated. This value is the same as that reported in our previous publications on the extraction of metal nitrates by TBP, confirming that the same mechanism and energetics are operative in the formation of a third phase, independent of whether the chemical species extracted are metal nitrate salts or inorganic acids.« less

  20. Shiitake mushroom production on small diameter oak logs in Ohio

    Treesearch

    S.M. Bratkovich

    1991-01-01

    Yields of different strains of shiitake mushrooms (Lentinus edodes) were evaluated when produced on small diameter oak logs in Ohio. Logs averaging between 3-4 inches in diameter were inoculated with four spawn strains in 1985.

  1. Effects of pore topology and iron oxide core on doxorubicin loading and release from mesoporous silica nanoparticles

    NASA Astrophysics Data System (ADS)

    Ronhovde, Cicily J.; Baer, John; Larsen, Sarah C.

    2017-06-01

    Mesoporous silica nanoparticles (MSNs) have a network of pores that give rise to extremely high specific surface areas, making them attractive materials for applications such as adsorption and drug delivery. The pore topology can be readily tuned to achieve a variety of structures such as the hexagonally ordered Mobil Crystalline Material 41 (MCM-41) and the disordered "wormhole" (WO) mesoporous silica (MS) structure. In this work, the effects of pore topology and iron oxide core on doxorubicin loading and release were investigated using MSNs with pore diameters of approximately 3 nm and sub-100 nm particle diameters. The nanoparticles were loaded with doxorubicin, and the drug release into phosphate-buffered saline (PBS, 10 mM, pH 7.4) at 37 °C was monitored by fluorescence spectroscopy. The release profiles were fit using the Peppas model. The results indicated diffusion-controlled release for all samples. Statistically significant differences were observed in the kinetic host-guest parameters for each sample due to the different pore topologies and the inclusion of an iron oxide core. Applying a static magnetic field to the iron oxide core WO-MS shell materials did not have a significant impact on the doxorubicin release. This is the first time that the effects of pore topology and iron oxide core have been isolated from pore diameter and particle size for these materials.

  2. Economic feasibility of products from inland West small-diameter timber

    Treesearch

    Spelter Henry; Rong Wang; Peter Ince

    1996-01-01

    A large part of the forests located in the Rocky Mountain region of the U.S. West (inland West) is characterized by densely packed, small-diameter stands. The purpose of this study was to examine the economic feasibility of using small-diameter material from this resource to manufacture various wood products: oriented strandboard (OSB), stud lumber, random-length...

  3. 78 FR 62597 - 36(b)(1) Arms Sales Notification

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-10-22

    ... Block II missiles, 1000 GBU-39/B Small Diameter Bomb (SDB) with BRU-61 carriage systems, 40 CATM-84H... missiles, 1000 GBU-39/B Small Diameter Bombs (SDB), 40 CATM-84H Captive Air Training Missiles (CATM), 20... Small Diameter Bomb (SDB) I weapon is a 250-lb class, all-up round (AUR) that provides greater than 50nm...

  4. 78 FR 62594 - 36(b)(1) Arms Sales Notification

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-10-22

    ... Consideration for Purchase: 5000 GBU-39/B Small Diameter Bombs (SDB) with BRU-61 carriage systems, 8 SDB Guided... Emirates has requested a possible sale of 5000 GBU-39/B Small Diameter Bombs (SDB) with BRU-61 carriage... environmental conditions. 5. The GBU-39/B Small Diameter Bomb (SDB) I weapon is a 250-lb class, all-up round...

  5. Suitability of live and fire-killed small-diameter ponderosa and lodgepole pine trees for manufacturing a new structural wood composite

    Treesearch

    J.M. Linton; H.M. Barnes; R.D. Seale; P.D. Jones; E. Lowell; S.S. Hummel

    2010-01-01

    Finding alternative uses for raw material from small-diameter trees is a critical problem throughout the United States. In western states, a lack of markets for small-diameter ponderosa pine (Pinus ponderosa) and lodgepole pine (Pinus contorta ) can contribute to problems associated with overstocking. To test the feasibility of...

  6. Test and Analysis of a Buckling-Critical Large-Scale Sandwich Composite Cylinder

    NASA Technical Reports Server (NTRS)

    Schultz, Marc R.; Sleight, David W.; Gardner, Nathaniel W.; Rudd, Michelle T.; Hilburger, Mark W.; Palm, Tod E.; Oldfield, Nathan J.

    2018-01-01

    Structural stability is an important design consideration for launch-vehicle shell structures and it is well known that the buckling response of such shell structures can be very sensitive to small geometric imperfections. As part of an effort to develop new buckling design guidelines for sandwich composite cylindrical shells, an 8-ft-diameter honeycomb-core sandwich composite cylinder was tested under pure axial compression to failure. The results from this test are compared with finite-element-analysis predictions and overall agreement was very good. In particular, the predicted buckling load was within 1% of the test and the character of the response matched well. However, it was found that the agreement could be improved by including composite material nonlinearity in the analysis, and that the predicted buckling initiation site was sensitive to the addition of small bending loads to the primary axial load in analyses.

  7. Diameter-dependent wetting of tungsten disulfide nanotubes

    PubMed Central

    Goldbart, Ohad; Cohen, Sidney R.; Kaplan-Ashiri, Ifat; Glazyrina, Polina; Wagner, H. Daniel; Enyashin, Andrey; Tenne, Reshef

    2016-01-01

    The simple process of a liquid wetting a solid surface is controlled by a plethora of factors—surface texture, liquid droplet size and shape, energetics of both liquid and solid surfaces, as well as their interface. Studying these events at the nanoscale provides insights into the molecular basis of wetting. Nanotube wetting studies are particularly challenging due to their unique shape and small size. Nonetheless, the success of nanotubes, particularly inorganic ones, as fillers in composite materials makes it essential to understand how common liquids wet them. Here, we present a comprehensive wetting study of individual tungsten disulfide nanotubes by water. We reveal the nature of interaction at the inert outer wall and show that remarkably high wetting forces are attained on small, open-ended nanotubes due to capillary aspiration into the hollow core. This study provides a theoretical and experimental paradigm for this intricate problem. PMID:27856759

  8. Magnetic particles as powerful purification tool for high sensitive mass spectrometric screening procedures.

    PubMed

    Peter, Jochen F; Otto, Angela M

    2010-02-01

    The effective isolation and purification of proteins from biological fluids is the most crucial step for a successful protein analysis when only minute amounts are available. While conventional purification methods such as dialysis, ultrafiltration or protein precipitation often lead to a marked loss of protein, SPE with small-sized particles is a powerful alternative. The implementation of particles with superparamagnetic cores facilitates the handling of those particles and allows the application of particles in the nanometer to low micrometer range. Due to the small diameters, magnetic particles are advantageous for increasing sensitivity when using subsequent MS analysis or gel electrophoresis. In the last years, different types of magnetic particles were developed for specific protein purification purposes followed by analysis or screening procedures using MS or SDS gel electrophoresis. In this review, the use of magnetic particles for different applications, such as, the extraction and analysis of DNA/RNA, peptides and proteins, is described.

  9. Effects of perturbation relative phase on transverse mode instability gain

    NASA Astrophysics Data System (ADS)

    Zervas, Michalis N.

    2018-02-01

    We have shown that the relative phase between the fundamental fiber mode and the transverse perturbation affects significantly the local transverse modal instability (TMI) gain. The gain variation is more pronounced as the core diameter increases. This finding can be used in conjunction with other proposed approaches to develop efficient strategies for mitigating TMI in high power fiber amplifiers and lasers. It also provides some physical insight on the physical origin of the observed large differences in the TMI threshold dependence on core diameter for narrow and broad linewidth operation.

  10. Synthesis of SiO2-coated ZnMnFe2O4 nanospheres with improved magnetic properties.

    PubMed

    Wang, Jun; Zhang, Kai; Zhu, Yuejin

    2005-05-01

    A core-shell structured composite, SiO2 coated ZnMnFe2O4 spinel ferrite nanoparticles (average diameter of approximately 80 nm), was prepared by hydrolysis of tetraethyl orthosilicate (TEOS) in the presence of ZnMnFe2O4 nanoparticles (average diameter of approximately 10 nm) synthesized by a hydrothermal method. The obtained samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), and field emission scanning electron microscopy (FESEM). The magnetic measurements were carried out on a vibrating sample magnetometer (VSM), and the measurement results indicate that the core-shell samples possess better magnetic properties at room temperature, compared with paramagnetic colloids with a magnetic core by a coprecipitation method. These core-shell nanospherical particles with self-assembly under additional magnetic fields could have potential application in biomedical systems.

  11. Synthesis of Various Metal/TiO2 Core/shell Nanorod Arrays

    NASA Astrophysics Data System (ADS)

    Zhu, Wei; Wang, Guan-zhong; Hong, Xun; Shen, Xiao-shuang

    2011-02-01

    We present a general approach to fabricate metal/TiO2 core/shell nanorod structures by two-step electrodeposition. Firstly, TiO2 nanotubes with uniform wall thickness are prepared in anodic aluminum oxide (AAO) membranes by electrodeposition. The wall thickness of the nanotubes could be easily controlled by modulating the deposition time, and their outer diameter and length are only limited by the channel diameter and the thickness of the AAO membranes, respectively. The nanotubes' tops prepared by this method are open, while the bottoms are connected directly with the Au film at the back of the AAO membranes. Secondly, Pd, Cu, and Fe elements are filled into the TiO2 nanotubes to form core/shell structures. The core/shell nanorods prepared by this two-step process are high density and free-standing, and their length is dependent on the deposition time.

  12. Porous metal oxide particles and their methods of synthesis

    DOEpatents

    Chen, Fanglin; Liu, Qiang

    2013-03-12

    Methods are generally disclosed for synthesis of porous particles from a solution formed from a leaving agent, a surfactant, and a soluble metal salt in a solvent. The surfactant congregates to form a nanoparticle core such that the metal salt forms about the nanoparticle core to form a plurality of nanoparticles. The solution is heated such that the leaving agent forms gas bubbles in the solution, and the plurality of nanoparticles congregate about the gas bubbles to form a porous particle. The porous particles are also generally disclosed and can include a particle shell formed about a core to define an average diameter from about 0.5 .mu.m to about 50 .mu.m. The particle shell can be formed from a plurality of nanoparticles having an average diameter of from about 1 nm to about 50 nm and defined by a metal salt formed about a surfactant core.

  13. Application of small-diameter FBG sensors for detection of damages in composites

    NASA Astrophysics Data System (ADS)

    Okabe, Yoji; Mizutani, Tadahito; Yashiro, Shigeki; Takeda, Nobuo

    2001-08-01

    Small-diameter fiber Bragg grating (FBG) sensors have been developed by Hitachi Cable Ltd. and the authors. Since the outside diameter of polyimide coating is 52 micrometers , embedding of the sensors into carbon fiber reinforced plastic (CFRP) composites prepregs of 125 micrometers in thickness does not deteriorate the mechanical properties of the composite laminates. In this research, the small-diameter FBG sensor was applied for the detection of transverse cracks in CFRP composites. The FBG sensor was embedded in 0 degree(s) ply of a CFRP cross-ply laminate.

  14. Polypeptide nanogels with hydrophobic moieties in the cross-linked ionic cores: Synthesis, characterization and implications for anticancer drug delivery

    PubMed Central

    Kim, Jong Oh; Oberoi, Hardeep S.; Desale, Swapnil; Kabanov, Alexander V.; Bronich, Tatiana K.

    2014-01-01

    Polymer nanogels have gained considerable attention as a potential platform for drug delivery applications. Here we describe the design and synthesis of novel polypeptide-based nanogels with hydrophobic moieties in the cross-linked ionic cores. Diblock copolymer, poly(ethylene glycol)-b-poly(L-glutamic acid), hydrophobically modified with L-phenylalanine methyl ester moieties was used for controlled template synthesis of nanogels with small size (ca. 70 nm in diameter) and narrow particle size distribution. Steady-state and time-resolved fluorescence studies using coumarin C153 indicated the existence of hydrophobic domains in the ionic cores of the nanogels. Stable doxorubicin-loaded nanogels were prepared at high drug capacity (30 w/w%). We show that nanogels are enzymatically-degradable leading to accelerated drug release under simulated lysosomal acidic pH. Furthermore, we demonstrate that the nanogel-based formulation of doxorubicin is well tolerated and exhibit an improved antitumor activity compared to a free doxorubicin in an ovarian tumor xenograft mouse model. Our results signify the point to a potential of these biodegradable nanogels as attractive carriers for delivery of chemotherapeutics. PMID:23998716

  15. Static and dynamic parasitic magnetizations and their control in superconducting accelerator dipoles

    NASA Astrophysics Data System (ADS)

    Collings, E. W.; Sumption, M. D.

    2001-05-01

    Long dipole magnets guide the particle beams in synchrotron-type high energy accelerators. In principal Cu-wound DC-excited dipoles could be designed to deliver a very uniform transverse bore field, i.e. with small or negligible harmonic (multipolar) distortion. But if the Cu is replaced by (a) superconducting strand that is (b) wound into a Rutherford cable carrying a time-varying transport current, extra magnetizations present within the windings cause distortions of the otherwise uniform field. The static (persistent-current) strand magnetization can be reduced by reducing the filament diameter, and the residue compensated or corrected by strategically placed active or passive components. The cable’s interstrand coupling currents can be controlled by increasing the interstrand contact resistance by: adjusting the level of native oxidation of the strand, coating it, or by inserting a ribbon-like core into the cable itself. Methods of locally compensating the magnetization of NbTi and Nb 3Sn strand and cable are discussed, progress in coupling-current suppression through the use of coatings and cores is reviewed, and a method of simultaneously reducing both the static and dynamic magnetizations of a NbTi cable by means of a thin Ni core is suggested.

  16. Rocket Motor Joint Construction Including Thermal Barrier

    NASA Technical Reports Server (NTRS)

    Steinetz, Bruce M. (Inventor); Dunlap, Patrick H., Jr. (Inventor)

    2002-01-01

    A thermal barrier for extremely high temperature applications consists of a carbon fiber core and one or more layers of braided carbon fibers surrounding the core. The thermal barrier is preferably a large diameter ring, having a relatively small cross-section. The thermal barrier is particularly suited for use as part of a joint structure in solid rocket motor casings to protect low temperature elements such as the primary and secondary elastomeric O-ring seals therein from high temperature gases of the rocket motor. The thermal barrier exhibits adequate porosity to allow pressure to reach the radially outward disposed O-ring seals allowing them to seat and perform the primary sealing function. The thermal barrier is disposed in a cavity or groove in the casing joint, between the hot propulsion gases interior of the rocket motor and primary and secondary O-ring seals. The characteristics of the thermal barrier may be enhanced in different applications by the inclusion of certain compounds in the casing joint, by the inclusion of RTV sealant or similar materials at the site of the thermal barrier, and/or by the incorporation of a metal core or plurality of metal braids within the carbon braid in the thermal barrier structure.

  17. Low-Loss Coupling of Quantum Cascade Lasers into Hollow-Core Waveguides with Single-Mode Output in the 3.7–7.6 μm Spectral Range

    PubMed Central

    Patimisco, Pietro; Sampaolo, Angelo; Mihai, Laura; Giglio, Marilena; Kriesel, Jason; Sporea, Dan; Scamarcio, Gaetano; Tittel, Frank K.; Spagnolo, Vincenzo

    2016-01-01

    We demonstrated low-loss and single-mode laser beam delivery through hollow-core waveguides (HCWs) operating in the 3.7–7.6 μm spectral range. The employed HCWs have a circular cross section with a bore diameter of 200 μm and metallic/dielectric internal coatings deposited inside a glass capillary tube. The internal coatings have been produced to enhance the spectral response of the HCWs in the range 3.5–12 µm. We demonstrated Gaussian-like outputs throughout the 4.5–7.6 µm spectral range. A quasi single-mode output beam with only small beam distortions was achieved when the wavelength was reduced to 3.7 μm. With a 15-cm-long HCW and optimized coupling conditions, we measured coupling efficiencies of >88% and transmission losses of <1 dB in the investigated infrared spectral range. PMID:27089343

  18. Non-condensable gas effects in ROSA/AP600 small-break LOCA experiments

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Nakamura, Hideo; Kukita, Yutaka; Shaw, R.A.

    1996-06-01

    Integral experiments simulating the postulated accidents in the Westinghouse AP600 reactor have been conducted using the ROSA-V Large Scale Test Facility (LSTF). These experiments allowed the N{sub 2} gas for the pressurization of accumulator tanks to enter the primary system after the depletion of the tank water inventory. The gas migrated into the Passive Residual Heat Removal (PRHR) system heat exchanger tubes and into the Core Makeup Tanks (CMTs), and influenced the performance of these components which are unique to the AP600 reactor. Specifically, the PRHR was disabled soon after the N{sub 2} gas discharge in most of the experiments,more » although the core decay power was removed well by the steam discharge through the Automatic Depressurization System (ADS) after the PRHR was disabled. The N{sub 2} gas ingress into the CMTs occurred in the experiments with relatively large breaks ({ge} 2 inch in equivalent diameter), and contributed to a smooth draindown of the CMT inventory into the primary system.« less

  19. Lubrication mechanisms of hollow-core inorganic fullerene-like nanoparticles: coupling experimental and computational works

    NASA Astrophysics Data System (ADS)

    Lahouij, I.; Bucholz, E. W.; Vacher, B.; Sinnott, S. B.; Martin, J. M.; Dassenoy, F.

    2012-09-01

    Inorganic fullerene-like (IF) nanoparticles made of metal dichalcogenides have previously been recognized to be good friction modifiers and anti-wear additives under boundary lubrication conditions. The tribological performance of these particles appears to be a result of their size, structure and morphology, along with the test conditions. However, the very small scale of the IF nanoparticles makes distinguishing the properties which affect the lubrication mechanism exceedingly difficult. In this work, a high resolution transmission electron microscope equipped with a nanoindentation holder is used to manipulate individual hollow IF-WS2 nanoparticles and to investigate their responses to compression. Additional atomistic molecular dynamics (MD) simulations of similarly structured, individual hollow IF-MoS2 nanoparticles are performed for compression studies between molybdenum surfaces on their major and minor axis diameters. MD simulations of these structures allows for characterization of the influence of structural orientation on the mechanical behavior and nano-sheet exfoliation of hollow-core IF nanoparticles. The experimental and theoretical results for these similar nanoparticles are qualitatively compared.

  20. Lubrication mechanisms of hollow-core inorganic fullerene-like nanoparticles: coupling experimental and computational works.

    PubMed

    Lahouij, I; Bucholz, E W; Vacher, B; Sinnott, S B; Martin, J M; Dassenoy, F

    2012-09-21

    Inorganic fullerene-like (IF) nanoparticles made of metal dichalcogenides have previously been recognized to be good friction modifiers and anti-wear additives under boundary lubrication conditions. The tribological performance of these particles appears to be a result of their size, structure and morphology, along with the test conditions. However, the very small scale of the IF nanoparticles makes distinguishing the properties which affect the lubrication mechanism exceedingly difficult. In this work, a high resolution transmission electron microscope equipped with a nanoindentation holder is used to manipulate individual hollow IF-WS(2) nanoparticles and to investigate their responses to compression. Additional atomistic molecular dynamics (MD) simulations of similarly structured, individual hollow IF-MoS(2) nanoparticles are performed for compression studies between molybdenum surfaces on their major and minor axis diameters. MD simulations of these structures allows for characterization of the influence of structural orientation on the mechanical behavior and nano-sheet exfoliation of hollow-core IF nanoparticles. The experimental and theoretical results for these similar nanoparticles are qualitatively compared.

  1. Design and Synthesis of Antiblinking and Antibleaching Quantum Dots in Multiple Colors via Wave Function Confinement.

    PubMed

    Cao, Hujia; Ma, Junliang; Huang, Lin; Qin, Haiyan; Meng, Renyang; Li, Yang; Peng, Xiaogang

    2016-12-07

    Single-molecular spectroscopy reveals that photoluminescence (PL) of a single quantum dot blinks, randomly switching between bright and dim/dark states under constant photoexcitation, and quantum dots photobleach readily. These facts cast great doubts on potential applications of these promising emitters. After ∼20 years of efforts, synthesis of nonblinking quantum dots is still challenging, with nonblinking quantum dots only available in red-emitting window. Here we report synthesis of nonblinking quantum dots covering most part of the visible window using a new synthetic strategy, i.e., confining the excited-state wave functions of the core/shell quantum dots within the core quantum dot and its inner shells (≤ ∼5 monolayers). For the red-emitting ones, the new synthetic strategy yields nonblinking quantum dots with small sizes (∼8 nm in diameter) and improved nonblinking properties. These new nonblinking quantum dots are found to be antibleaching. Results further imply that the PL blinking and photobleaching of quantum dots are likely related to each other.

  2. Analyzing the feasibility of utilizing small diameter hardwood timber for solid wood products and residues

    Treesearch

    Brian Perkins; Bob Smith; Philip Araman

    2008-01-01

    The eastern hardwood forest contains small diameter timber that is often of lower quality and lower value than larger sawtimber. This small diameter hardwood timber has traditionally been utilized for pulpwood, but it can also be used for lumber and residue production. In order to increase the utilization of this resource by sawmills, a number of analyses need to be...

  3. Measurement of oxygen tension within mesenchymal stem cell spheroids.

    PubMed

    Murphy, Kaitlin C; Hung, Ben P; Browne-Bourne, Stephen; Zhou, Dejie; Yeung, Jessica; Genetos, Damian C; Leach, J Kent

    2017-02-01

    Spheroids formed of mesenchymal stem cells (MSCs) exhibit increased cell survival and trophic factor secretion compared with dissociated MSCs, making them therapeutically advantageous for cell therapy. Presently, there is no consensus for the mechanism of action. Many hypothesize that spheroid formation potentiates cell function by generating a hypoxic core within spheroids of sufficiently large diameters. The purpose of this study was to experimentally determine whether a hypoxic core is generated in MSC spheroids by measuring oxygen tension in aggregates of increasing diameter and correlating oxygen tension values with cell function. MSC spheroids were formed with 15 000, 30 000 or 60 000 cells per spheroid, resulting in radii of 176 ± 8 µm, 251 ± 12 µm and 353 ± 18 µm, respectively. Oxygen tension values coupled with mathematical modelling revealed a gradient that varied less than 10% from the outer diameter within the largest spheroids. Despite the modest radial variance in oxygen tension, cellular metabolism from spheroids significantly decreased as the number of cells and resultant spheroid size increased. This may be due to adaptive reductions in matrix deposition and packing density with increases in spheroid diameter, enabling spheroids to avoid the formation of a hypoxic core. Overall, these data provide evidence that the enhanced function of MSC spheroids is not oxygen mediated. © 2017 The Author(s).

  4. A fast ultrasonic simulation tool based on massively parallel implementations

    NASA Astrophysics Data System (ADS)

    Lambert, Jason; Rougeron, Gilles; Lacassagne, Lionel; Chatillon, Sylvain

    2014-02-01

    This paper presents a CIVA optimized ultrasonic inspection simulation tool, which takes benefit of the power of massively parallel architectures: graphical processing units (GPU) and multi-core general purpose processors (GPP). This tool is based on the classical approach used in CIVA: the interaction model is based on Kirchoff, and the ultrasonic field around the defect is computed by the pencil method. The model has been adapted and parallelized for both architectures. At this stage, the configurations addressed by the tool are : multi and mono-element probes, planar specimens made of simple isotropic materials, planar rectangular defects or side drilled holes of small diameter. Validations on the model accuracy and performances measurements are presented.

  5. Biomechanics and load resistance of small-diameter and mini dental implants: a review of literature.

    PubMed

    Hasan, Istabrak; Bourauel, Christoph; Mundt, Torsten; Stark, Helmut; Heinemann, Friedhelm

    2014-02-01

    In recent years, the application of small-diameter and mini dental implants to support removable and fixed prosthesis has dramatically increased. However, the success of these implants under functional biting forces and the reaction of the bone around them need to be analyzed. This review was aimed to present studies that deal with the fatigue life of small-diameter and mini dental implants under normal biting force, and their survival rate. The numerical and experimental studies concluded that an increase in the risk of bone damage or implant failure may be assumed in critical clinical situations and implants with <3 mm diameter have a risk of fracture in clinical practice. The survival rate of the small-diameter and mini dental implants over 5 years was 98.3-99.4%.

  6. Engineering Photon-Photon Interactions within Rubidium-Filled Waveguides

    NASA Astrophysics Data System (ADS)

    Perrella, C.; Light, P. S.; Vahid, S. Afshar; Benabid, F.; Luiten, A. N.

    2018-04-01

    Strong photon-photon interactions are a required ingredient for deterministic two-photon optical quantum logic gates. Multiphoton transitions in dense atomic vapors have been shown to be a promising avenue for producing such interactions. The strength of a multiphoton interaction can be enhanced by conducting the interaction in highly confined geometries such as small-cross-section optical waveguides. We demonstrate, both experimentally and theoretically, that the strength of such interactions scale only with the optical mode diameter, d , not d2 as might be initially expected. This weakening of the interaction arises from atomic motion inside the waveguides. We create an interaction between two optical signals, at 780 and 776 nm, using the 5 S1 /2→5 D5 /2 two-photon transition in rubidium vapor within a range of hollow-core fibers with different core sizes. The interaction strength is characterized by observing the absorption and phase shift induced on the 780-nm beam, which is in close agreement with theoretical modeling that accounts for the atomic motion inside the fibers. These observations demonstrate that transit-time effects upon multiphoton transitions are of key importance when engineering photon-photon interactions within small-cross-section waveguides that might otherwise be thought to lead to enhanced optical nonlinearity through increased intensities.

  7. Evaluating growth assumptions using diameter or radial increments in natural even-aged longleaf pine

    Treesearch

    John C. Gilbert; Ralph S. Meldahl; Jyoti N. Rayamajhi; John S. Kush

    2010-01-01

    When using increment cores to predict future growth, one often assumes future growth is identical to past growth for individual trees. Once this assumption is accepted, a decision has to be made between which growth estimate should be used, constant diameter growth or constant basal area growth. Often, the assumption of constant diameter growth is used due to the ease...

  8. Large core fiber optic cleaver

    DOEpatents

    Halpin, John M.

    1996-01-01

    The present invention relates to a device and method for cleaving optical fibers which yields cleaved optical fiber ends possessing high damage threshold surfaces. The device can be used to cleave optical fibers with core diameters greater than 400 .mu.m.

  9. Misfit-guided self-organization of anticorrelated Ge quantum dot arrays on Si nanowires.

    PubMed

    Kwon, Soonshin; Chen, Zack C Y; Kim, Ji-Hun; Xiang, Jie

    2012-09-12

    Misfit-strain guided growth of periodic quantum dot (QD) arrays in planar thin film epitaxy has been a popular nanostructure fabrication method. Engineering misfit-guided QD growth on a nanoscale substrate such as the small curvature surface of a nanowire represents a new approach to self-organized nanostructure preparation. Perhaps more profoundly, the periodic stress underlying each QD and the resulting modulation of electro-optical properties inside the nanowire backbone promise to provide a new platform for novel mechano-electronic, thermoelectronic, and optoelectronic devices. Herein, we report a first experimental demonstration of self-organized and self-limited growth of coherent, periodic Ge QDs on a one-dimensional Si nanowire substrate. Systematic characterizations reveal several distinctively different modes of Ge QD ordering on the Si nanowire substrate depending on the core diameter. In particular, Ge QD arrays on Si nanowires of around 20 nm diameter predominantly exhibit an anticorrelated pattern whose wavelength agrees with theoretical predictions. The correlated pattern can be attributed to propagation and correlation of misfit strain across the diameter of the thin nanowire substrate. The QD array growth is self-limited as the wavelength of the QDs remains unchanged even after prolonged Ge deposition. Furthermore, we demonstrate a direct kinetic transformation from a uniform Ge shell layer to discrete QD arrays by a postgrowth annealing process.

  10. Westinghouse Small Modular Reactor nuclear steam supply system design

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Memmott, M. J.; Harkness, A. W.; Van Wyk, J.

    2012-07-01

    The Westinghouse Small Modular Reactor (SMR) is an 800 MWt (>225 MWe) integral pressurized water reactor (iPWR), in which all of the components typically associated with the nuclear steam supply system (NSSS) of a nuclear power plant are incorporated within a single reactor pressure vessel. This paper is the first in a series of four papers which describe the design and functionality of the Westinghouse SMR. Also described in this series are the key drivers influencing the design of the Westinghouse SMR and the unique passive safety features of the Westinghouse SMR. Several critical motivators contributed to the development andmore » integration of the Westinghouse SMR design. These design driving motivators dictated the final configuration of the Westinghouse SMR to varying degrees, depending on the specific features under consideration. These design drivers include safety, economics, AP1000{sup R} reactor expertise and experience, research and development requirements, functionality of systems and components, size of the systems and vessels, simplicity of design, and licensing requirements. The Westinghouse SMR NSSS consists of an integral reactor vessel within a compact containment vessel. The core is located in the bottom of the reactor vessel and is composed of 89 modified Westinghouse 17x17 Robust Fuel Assemblies (RFA). These modified fuel assemblies have an active core length of only 2.4 m (8 ft) long, and the entirety of the core is encompassed by a radial reflector. The Westinghouse SMR core operates on a 24 month fuel cycle. The reactor vessel is approximately 24.4 m (80 ft) long and 3.7 m (12 ft) in diameter in order to facilitate standard rail shipping to the site. The reactor vessel houses hot and cold leg channels to facilitate coolant flow, control rod drive mechanisms (CRDM), instrumentation and cabling, an intermediate flange to separate flow and instrumentation and facilitate simpler refueling, a pressurizer, a straight tube, recirculating steam generator, and eight reactor coolant pumps (RCP). The containment vessel is 27.1 m (89 ft) long and 9.8 m (32 ft) in diameter, and is designed to withstand pressures up to 1.7 MPa (250 psi). It is completely submerged in a pool of water serving as a heat sink and radiation shield. Housed within the containment are four combined core makeup tanks (CMT)/passive residual heat removal (PRHR) heat exchangers, two in-containment pools (ICP), two ICP tanks and four valves which function as the automatic depressurization system (ADS). The PRHR heat exchangers are thermally connected to two different ultimate heat sink (UHS) tanks which provide transient cooling capabilities. (authors)« less

  11. Tunable Engineered Skin Mechanics via Coaxial Electrospun Fiber Core Diameter

    PubMed Central

    Blackstone, Britani Nicole; Drexler, Jason William

    2014-01-01

    Autologous engineered skin (ES) offers promise as a treatment for massive full thickness burns. Unfortunately, ES is orders of magnitude weaker than normal human skin causing it to be difficult to apply surgically and subject to damage by mechanical shear in the early phases of engraftment. In addition, no manufacturing strategy has been developed to tune ES biomechanics to approximate the native biomechanics at different anatomic locations. To enhance and tune ES biomechanics, a coaxial (CoA) electrospun scaffold platform was developed from polycaprolactone (PCL, core) and gelatin (shell). The ability of the coaxial fiber core diameter to control both scaffold and tissue mechanics was investigated along with the ability of the gelatin shell to facilitate cell adhesion and skin development compared to pure gelatin, pure PCL, and a gelatin-PCL blended fiber scaffold. CoA ES exhibited increased cellular adhesion and metabolism versus PCL alone or gelatin-PCL blend and promoted the development of well stratified skin with a dense dermal layer and a differentiated epidermal layer. Biomechanics of the scaffold and ES scaled linearly with core diameter suggesting that this scaffold platform could be utilized to tailor ES mechanics for their intended grafting site and reduce graft damage in vitro and in vivo. PMID:24712409

  12. Core-shell monodisperse spherical mSiO2/Gd2O3:Eu3+@mSiO2 particles as potential multifunctional theranostic agents

    NASA Astrophysics Data System (ADS)

    Eurov, Daniil A.; Kurdyukov, Dmitry A.; Kirilenko, Demid A.; Kukushkina, Julia A.; Nashchekin, Alexei V.; Smirnov, Alexander N.; Golubev, Valery G.

    2015-02-01

    Core-shell nanoparticles with diameters in the range 100-500 nm have been synthesized as monodisperse spherical mesoporous (pore diameter 3 nm) silica particles with size deviation of less than 4 %, filled with gadolinium and europium oxides and coated with a mesoporous silica shell. It is shown that the melt technique developed for filling with gadolinium and europium oxides provides a nearly maximum filling of mesopores in a single-run impregnation, with gadolinium and europium uniformly distributed within the particles and forming no bulk oxides on their surface. The coating with a shell does not impair the monodispersity and causes no coagulation. The coating technique enables controlled variation of the shell thickness within the range 5-100 % relative to the core diameter. The thus produced nanoparticles are easily dispersed in water, have large specific surface area (300 m2 g-1) and pore volume (0.3 cm3 g-1), and are bright solid phosphor with superior stability in aqueous media. The core-shell structured particles can be potentially used for cancer treatment as a therapeutic agent (gadolinium neutron-capture therapy and drug delivery system) and, simultaneously, as a multimodal diagnostic tool (fluorescence and magnetic resonance imaging), thereby serving as a multifunctional theranostic agent.

  13. Diameter Control and Photoluminescence of ZnO Nanorods from Trialkylamines

    DOE PAGES

    Andelman, Tamar; Gong, Yinyan; Neumark, Gertrude; ...

    2007-01-01

    A novel solution method to control the diameter of ZnO nanorods is reported. Small diameter (2-3 nm) nanorods were synthesized from trihexylamine, and large diameter (50–80 nm) nanorods were synthesized by increasing the alkyl chain length to tridodecylamine. The defect (green) emission of the photoluminescence (PL) spectra of the nanorods varies with diameter, and can thus be controlled by the diameter control. The small ZnO nanorods have strong green emission, while the large diameter nanorods exhibit a remarkably suppressed green band. We show that this observation supports surface oxygen vacancies as the defect that gives rise to the green emission.

  14. Small tractors for harvesting fuelwood in low-volume small-diameter hardwood stands

    Treesearch

    Neil K. Huyler; Chris B. LeDoux

    1989-01-01

    Much of the nonindustrial, private forest land in the Northeast is characterized by small diameter trees with low volume. Conventional harvesting systems used in logging these stands generally results in submarginal economic returns. Often, small-scale harvesting systems have economic advantages in these areas. Time and motion studies were conducted for several small...

  15. Large core fiber optic cleaver

    DOEpatents

    Halpin, J.M.

    1996-03-26

    The present invention relates to a device and method for cleaving optical fibers which yields cleaved optical fiber ends possessing high damage threshold surfaces. The device can be used to cleave optical fibers with core diameters greater than 400 {micro}m. 30 figs.

  16. Measurements of characteristic parameters of extremely small cogged wheels with low module by means of low-coherence interferometry

    NASA Astrophysics Data System (ADS)

    Pakula, Anna; Tomczewski, Slawomir; Skalski, Andrzej; Biało, Dionizy; Salbut, Leszek

    2010-05-01

    This paper presents novel application of Low Coherence Interferometry (LCI) in measurements of characteristic parameters as circular pitch, foot diameter, heads diameter, in extremely small cogged wheels (cogged wheel diameter lower than θ=3 mm and module m = 0.15) produced from metal and ceramics. The most interesting issue concerning small diameter cogged wheels occurs during their production. The characteristic parameters of the wheel depend strongly on the manufacturing process and while inspecting small diameter wheels the shrinkage during the cast varies with the slight change of fabrication process. In the paper the LCI interferometric Twyman - Green setup with pigtailed high power light emitting diode, for cogged wheels measurement, is described. Due to its relatively big field of view the whole wheel can be examined in one measurement, without the necessity of numerical stitching. For purposes of small cogged wheel's characteristic parameters measurement the special binarization algorithm was developed and successfully applied. At the end the results of measurement of heads and foot diameters of two cogged wheels obtained by proposed LCI setup are presented and compared with the results obtained by the commercial optical profiler. The results of examination of injection moulds used for fabrication of measured cogged wheels are also presented. Additionally, the value of cogged wheels shrinkage is calculated as a conclusion for obtained results. Proposed method is suitable for complex measurements of small diameter cogged wheels with low module especially when there are no measurements standards for such objects.

  17. Isotachophoresis system having larger-diameter channels flowing into channels with reduced diameter and with selectable counter-flow

    DOEpatents

    Mariella, Jr., Raymond P.

    2018-03-06

    An isotachophoresis system for separating a sample containing particles into discrete packets including a flow channel, the flow channel having a large diameter section and a small diameter section; a negative electrode operably connected to the flow channel; a positive electrode operably connected to the flow channel; a leading carrier fluid in the flow channel; a trailing carrier fluid in the flow channel; and a control for separating the particles in the sample into discrete packets using the leading carrier fluid, the trailing carrier fluid, the large diameter section, and the small diameter section.

  18. LiNbO3 Cylinder Fiber

    NASA Technical Reports Server (NTRS)

    2004-01-01

    We have successfully fabricate optical fiber with a thin layer of LiNbO3 at the boundary of the glass core and dear glass cladding. The construction of this fiber is based on our successful Semiconductor Cylinder Fibers (SCF). A schematic representation of a LiNbO3 Cylinder Fiber is shown. These fibers can be used as light modulators, sonar detectors and in other applications. The core diameter of the fiber is sufficiently small compared to the light wavelength and the indices of refraction of the core and cladding glasses are sufficiently close in value so that there is sufficient light at the core cladding boundary to interact with the LiNbO3 layer. This fiber functions best when just a single light mode propagates through the fiber. The idea for a LiNbO3 Cylinder Fiber came from Dr. Tracee Jamison of NASA. The optical properties of LiNbO3 can be changed with strain or the application of an electric field. Thus these fibers can be used as acoustic sensors as for example in a sonar. They can also be used as electric field operated light modulators. However, for this application the fibers would be made with a cross section in the form of a 'D'. The core with its surrounding LiNbO, layer would be close to the flat portion of the 'D' shaped fiber. Two metal contacts would be deposited on the flat portion of the fiber on either side of the core. A voltage applied across these contacts will result in an electric field in the core region that can be used for modulating the optical properties of the LiNbO, layer. To our knowledge this is the first ever LiNbO, Cylinder Fiber made.

  19. LiNbO3 Cylinder Fiber

    NASA Technical Reports Server (NTRS)

    Kornreich, Philip

    2004-01-01

    We have successfully fabricate optical fiber with a thin layer of LiNbO3 at the boundary of the glass core and clear glass cladding. The construction of this fiber is based on our successful Semiconductor Cylinder Fibers (SCF). A schematic representation of a LiN bo, Cylinder Fiber. These fibers can be used as light modulators, sonar detectors and in other applications. The core diameter of the fiber is sufficiently small compared to the light wavelength and the indices of refraction of the core and cladding glasses are sufficiently close in value so that there is sufficient light at the core cladding boundary to interact with the LiNbO3 layer. This fiber functions best when just a single light mode propagates through the fiber. The idea for a LiNbO3 Cylinder Fiber came from Dr. Tracee Jamison of NASA. The optical properties of LiNbO3 can be changed with strain or the application of an electric field. Thus these fibers can be used as acoustic sensors as for example in a sonar. They can also be used as electric field operated light modulators. However, for this application the fibers would be made with a cross section in the form of a "D". The core with its surrounding LiNbO, layer would be close to the flat portion of the "D" shaped fiber. Two metal contacts would be deposited on the flat portion of the fiber on either side of the core. A voltage applied across these contacts will result in an electric field in the core region that can be used for modulating the optical properties of the LiNbO3 layer. To our knowledge this is the first ever LiNbO3 Cylinder Fiber made.

  20. Improved method for measuring water imbibition rates on low-permeability porous media

    USGS Publications Warehouse

    Humphrey, M.D.; Istok, J.D.; Flint, L.E.; Flint, A.L.

    1996-01-01

    Existing methods for measuring water imbibition rates are inadequate when imbibition rates are small (e.g., clay soils and many igneous rocks). We developed an improved laboratory method for performing imbibition measurements on soil or rock cores with a wide range of hydraulic properties. Core specimens are suspended from an electronic strain gauge (load cell) in a closed chamber while maintaining the lower end of the core in contact with a free water surface in a constant water level reservoir. The upper end of the core is open to the atmosphere. During imbibition, mass increase of the core is recorded continuously by a datalogger that converts the load cell voltage signal into mass units using a calibration curve. Computer automation allows imbibition rate measurement on as many as eight cores simultaneously and independently. Performance of each component of the imbibition apparatus was evaluated using a set of rock cores (2.5 cm in diameter and 2-5 cm in length) from a single lithostratigraphic unit composed of non-to-moderately welded ash-flow tuff (a glass-rich pyroclastic rock partially fused by heat and pressure) with porosities ranging from 0.094 to 0.533 m3 m-3. Reproducibility of sample handling and testing procedures was demonstrated using replicate measurements. Precision and accuracy of load cell measurements were assessed using mass balance calculations and indicated agreement within a few tenths of a percent of total mass. Computed values of sorptivity, S, ranged from 8.83 x 10-6 to 4.55 x 10-4 m s-0.5. The developed method should prove useful for measuring imbibition rates on a wide range of porous materials.

  1. Understanding the core-halo relation of quantum wave dark matter from 3D simulations.

    PubMed

    Schive, Hsi-Yu; Liao, Ming-Hsuan; Woo, Tak-Pong; Wong, Shing-Kwong; Chiueh, Tzihong; Broadhurst, Tom; Hwang, W-Y Pauchy

    2014-12-31

    We examine the nonlinear structure of gravitationally collapsed objects that form in our simulations of wavelike cold dark matter, described by the Schrödinger-Poisson (SP) equation with a particle mass ∼10(-22)  eV. A distinct gravitationally self-bound solitonic core is found at the center of every halo, with a profile quite different from cores modeled in the warm or self-interacting dark matter scenarios. Furthermore, we show that each solitonic core is surrounded by an extended halo composed of large fluctuating dark matter granules which modulate the halo density on a scale comparable to the diameter of the solitonic core. The scaling symmetry of the SP equation and the uncertainty principle tightly relate the core mass to the halo specific energy, which, in the context of cosmological structure formation, leads to a simple scaling between core mass (Mc) and halo mass (Mh), Mc∝a(-1/2)Mh(1/3), where a is the cosmic scale factor. We verify this scaling relation by (i) examining the internal structure of a statistical sample of virialized halos that form in our 3D cosmological simulations and by (ii) merging multiple solitons to create individual virialized objects. Sufficient simulation resolution is achieved by adaptive mesh refinement and graphic processing units acceleration. From this scaling relation, present dwarf satellite galaxies are predicted to have kiloparsec-sized cores and a minimum mass of ∼10(8)M⊙, capable of solving the small-scale controversies in the cold dark matter model. Moreover, galaxies of 2×10(12)M⊙ at z=8 should have massive solitonic cores of ∼2×10(9)M⊙ within ∼60  pc. Such cores can provide a favorable local environment for funneling the gas that leads to the prompt formation of early stellar spheroids and quasars.

  2. Rigid and Flexible Pavement Aircraft Tie-Downs

    DTIC Science & Technology

    2010-05-01

    Concrete Pier, Prior to PCC Placement Neenah anchors are equipped with two ½-in-diameter cored holes to allow insertion of a section of rebar through...facilitate this process, a Hilti drill was utilized to perform the concrete drilling process. The drill bit diameter exceeded the rebar diameter by...aggregate particles not become lodged against the rebar sections inside the dowel sleeves, impeding the flow of concrete and possibly creating air voids

  3. Influence of diameter on particle transport in a fractured shale saprolite

    USGS Publications Warehouse

    Cumbie, D.H.; McKay, L.D.

    1999-01-01

    Experiments in an undisturbed, saturated column of weathered and fractured shale saprolite using fluorescent carboxylate-coated latex microspheres as tracers indicate that particle diameter plays a major role in controlling transport. In this study the optimum microsphere diameter for transport was approximately 0.5 ??m. Microspheres larger than the optimum size were present in the effluent at lower relative concentrations, apparently because of greater retention due to gravitational settling and/or physical straining. The smaller than optimum microspheres also experienced greater retention, apparently related to their higher rates of diffusion. Faster diffusion can lead to more frequent collisions with, and attachment to, fracture walls and may also lead to movement of particles into zones of relatively immobile pore water in the fractures or in the fine pore structure of the clay-rich matrix between fractures. Dismantling of the soil column and mapping of the distribution of retained microspheres indicated that there was substantial size-segregation of the microspheres between different fractures or in 'channels' within a fracture. Examination of small core samples showed that the smallest microspheres (0.05-0.1 ??m) were present in the fine pores of the matrix at distances of up to 3-4 mm from the nearest fracture, which supports the hypothesis that small particles can be retained by diffusion into the matrix. Calculations of settling velocity and diffusion rate using simple 1D approaches suggest that these processes could both cause significant retention of the larger and smaller particles, respectively, even for the fast advective transport rates (up to 32 m/day) observed during the experiments. Copyright (C) 1999 Elsevier Science B.V.

  4. Small bowel dilation in children with short bowel syndrome is associated with mucosal damage, bowel-derived bloodstream infections, and hepatic injury.

    PubMed

    Hukkinen, Maria; Mutanen, Annika; Pakarinen, Mikko P

    2017-09-01

    Liver disease occurs frequently in short bowel syndrome. Whether small bowel dilation in short bowel syndrome could influence the risk of liver injury through increased bacterial translocation remains unknown. Our aim was to analyze associations between small bowel dilation, mucosal damage, bloodstream infections, and liver injury in short bowel syndrome patients. Among short bowel syndrome children (n = 50), maximal small bowel diameter was measured in contrast series and expressed as the ratio to the height of the fifth lumbar vertebra (small bowel diameter ratio), and correlated retrospectively to fecal calprotectin and plasma citrulline-respective markers of mucosal inflammation and mass-bloodstream infections, liver biochemistry, and liver histology. Patients with pathologic small bowel diameter ratio >2.17 had increased fecal calprotectin and decreased citrulline (P < .04 each). Of 33 bloodstream infections observed during treatment with parenteral nutrition, 16 were caused by intestinal bacteria, cultured 15 times more frequently when small bowel diameter ratio was >2.17 (P < .001). Intestinal bloodstream infections were predicted by small bowel diameter ratio (odds ratio 1.88, P = .017), and their frequency decreased after operative tapering procedures (P = .041). Plasma bilirubin concentration, gamma-glutamyl transferase activity, and histologic grade of cholestasis correlated with small bowel diameter ratio (0.356-0.534, P < .014 each), and were greater in the presence of intestinal bloodstream infections (P < .001 for all). Bloodstream infections associated with portal inflammation, cholestasis, and fibrosis grades (P < .031 for each). In linear regression, histologic cholestasis was predicted by intestinal bloodstream infections, small bowel diameter ratio, and parenteral nutrition (β = 0.36-1.29; P < .014 each), while portal inflammation by intestinal bloodstream infections only (β = 0.62; P = .033). In children with short bowel syndrome, small bowel dilation correlates with mucosal damage, bloodstream infections of intestinal origin, and cholestatic liver injury. In addition to parenteral nutrition, small bowel dilation and intestinal bloodstream infections contribute to development of short bowel syndrome-associated liver disease. Copyright © 2017 Elsevier Inc. All rights reserved.

  5. Establishing a Mouse Model of a Pure Small Fiber Neuropathy with the Ultrapotent Agonist of Transient Receptor Potential Vanilloid Type 1.

    PubMed

    Lee, Yi-Chen; Lu, Shui-Chin; Hsieh, Yu-Lin

    2018-02-13

    Patients with diabetes mellitus (DM) or those experiencing the neurotoxic effects of chemotherapeutic agents may develop sensation disorders due to degeneration and injury of small-diameter sensory neurons, referred to as small fiber neuropathy. Present animal models of small fiber neuropathy affect both large- and small-diameter sensory fibers and thus create a neuropathology too complex to properly assess the effects of injured small-diameter sensory fibers. Therefore, it is necessary to develop an experimental model of pure small fiber neuropathy to adequately examine these issues. This protocol describes an experimental model of small fiber neuropathy specifically affecting small-diameter sensory nerves with resiniferatoxin (RTX), an ultrapotent agonist of transient receptor potential vanilloid type 1 (TRPV1), through a single dose of intraperitoneal injection, referred to as RTX neuropathy. This RTX neuropathy showed pathological manifestations and behavioral abnormalities that mimic the clinical characteristics of patients with small fiber neuropathy, including intraepidermal nerve fiber (IENF) degeneration, specifically injury in small-diameter neurons, and induction of thermal hypoalgesia and mechanical allodynia. This protocol tested three doses of RTX (200, 50, and 10 µg/kg, respectively) and concluded that a critical dose of RTX (50 µg/kg) is required for the development of typical small fiber neuropathy manifestations, and prepared a modified immunostaining procedure to investigate IENF degeneration and neuronal soma injury. The modified procedure is fast, systematic, and economic. Behavioral evaluation of neuropathic pain is critical to reveal the function of small-diameter sensory nerves. The evaluation of mechanical thresholds in experimental rodents is particularly challenging and this protocol describes a customized metal mesh that is suitable for this type of assessment in rodents. In summary, RTX neuropathy is a new and easily established experimental model to evaluate the molecular significance and intervention underlying neuropathic pain for the development of therapeutic agents.

  6. Moisture contamination and welding parameter effects on flux cored arc welding diffusible hydrogen

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Kiefer, J.J.

    1994-12-31

    Gas metal arc (GMAW) and flux cored arc (FCAW) welding are gas shielded semiautomatic processes widely used for achieving high productivity in steel fabrication. Contamination of the shielding has can occur due to poorly maintained gas distribution systems. Moisture entering as a gas contaminant is a source of hydrogen that can cause delayed cold cracking in welds. Limiting heat-affected zone hardness is one method of controlling cracking. Even this is based on some assumptions about the hydrogen levels in the weld. A study was conducted to investigate the effect of shielding gas moisture contamination and welding parameters on the diffusiblemore » hydrogen content of gas shielded flux cored arc welding. The total wire hydrogen of various electrodes was also tested and compared to the diffusible weld hydrogen. An empirical equation has been developed that estimates the diffusible hydrogen in weld metal for gas shielded flux cored arc welding. The equation is suitable for small diameter electrodes and welding parameter ranges commonly used for out-of-position welding. by combining this with the results from the total wire hydrogen tests, it is possible to estimate diffusible hydrogen directly from measured welding parameters, shielding gas dew point, and total hydrogen of the consumable. These equations are also useful for evaluating the effect of welding procedure variations from known baseline conditions.« less

  7. Additively manufactured MEMS multiplexed coaxial electrospray sources for high-throughput, uniform generation of core-shell microparticles.

    PubMed

    Olvera-Trejo, D; Velásquez-García, L F

    2016-10-18

    This study reports the first MEMS multiplexed coaxial electrospray sources in the literature. Coaxial electrospraying is a microencapsulation technology based on electrohydrodynamic jetting of two immiscible liquids, which allows precise control with low size variation of the geometry of the core-shell particles it generates, which is of great importance in numerous biomedical and engineering applications, e.g., drug delivery and self-healing composites. By implementing monolithic planar arrays of miniaturized coaxial electrospray emitters that work uniformly in parallel, the throughput of the compound microdroplet source is greatly increased, making the microencapsulation technology compatible with low-cost commercial applications. Miniaturized core-shell particle generators with up to 25 coaxial electrospray emitters (25 emitters cm -2 ) were fabricated via stereolithography, which is an additive manufacturing process that can create complex microfluidic devices at a small fraction of the cost per device and fabrication time associated with silicon-based counterparts. The characterization of devices with the same emitter structure but different array sizes demonstrates uniform array operation. Moreover, the data demonstrate that the per-emitter current is approximately proportional to the square root of the flow rate of the driving liquid, and it is independent of the flow rate of the driven liquid, as predicted by the theory. The core/shell diameters and the size distribution of the generated compound microparticles can be modulated by controlling the flow rates fed to the emitters.

  8. Studies of a plasma with a hot dense core in LAPD

    NASA Astrophysics Data System (ADS)

    van Compernolle, Bart; Gekelman, Walter; Pribyl, Patrick; Cooper, Chris

    2009-11-01

    Recently, considerable effort in the LArge Plasma Device at UCLA (LAPD) has gone into the study of large cathodes which would enable higher discharge currents and higher densities. The new cathode is made out of Lanthanum HexaBoride (LaB6). LaB6 has a low work function and has higher emissivity than Barium oxide coated cathodes. The operating temperature of LaB6 cathodes lies above 1600 degrees Celsius. Tests of this cathode in the Enormous Toroidal Plasma Device (ETPD) showed that densities in excess of 2 10^13 cm-3 and electron temperatures of 12 eV are feasible. Small LaB6 cathodes (3mm - 2cm) have been used before in LAPD in several experiments on heat transport and on magnetized flux ropes. The cathode presented in this paper has a 8 cm diameter, and can be positioned at different radial locations. The cathode will be pulsed into the standard background plasma (ne= 2 10^12 cm-3, .25 <=Te<=6 eV, dia = 60 cm, L = 18 m) creating a plasma with a hot dense core. We present the characterization of the core plasma at different conditions. Studies of the heat transport and density spreading at the interface between the core plasma and background plasma will be done by use of a variety of probes (Langmuir, magnetic, Mach, emissive) as well as fast photography.

  9. Gallium ion-assisted room temperature synthesis of small-diameter ZnO nanorods.

    PubMed

    Cho, Seungho; Kim, Semi; Lee, Kun-Hong

    2011-09-15

    We report a method for synthesizing small-diameter ZnO nanorods at room temperature (20 °C), under normal atmospheric pressure (1 atm), and using a relatively short reaction time (1 h) by adding gallium salts to the reaction solution. The ZnO nanorods were, on average, 92 nm in length and 9 nm in diameter and were single crystalline in nature. Quantitative analyses revealed that gallium atoms were not incorporated into the synthesized nanocrystals. On the basis of the experimental results, we propose a mechanism for the formation of small-diameter ZnO nanorods in the presence of gallium ions. The optical properties were probed by UV-Vis diffuse reflectance spectroscopy. The absorption band of the small-diameter ZnO nanorods was blue-shifted relative to the absorption band of the ~230 nm diameter ZnO nanorods (control samples). Control experiments demonstrated that the absence of metal ion-containing precipitants (except ZnO) at room temperature is essential, and that the ZnO nanorod diameter distributions were narrow for the stirred reaction solution and broad when prepared without stirring. Copyright © 2011 Elsevier Inc. All rights reserved.

  10. Hepatitis Virus Capsid Polymorphs Respond Differently to Changes in Encapsulated Cargo Size

    PubMed Central

    He, Li; Porterfield, J. Zachary; van der Schoot, Paul; Zlotnick, Adam; Dragnea, Bogdan

    2017-01-01

    A templated assembly approach for Hepatitis B virus-like particles was employed to determine how the T = 3 and T = 4 polymorphs of the Hepatitis B virus (HBV) icosahedral cores respond to a systematic, gradual change in the encapsulated cargo size. It was found that assembly into complete virus-like particles occurs cooperatively around a variety of core diameters, albeit the degree of cooperativity varies. Among these virus-like particles, it was found that those of an outer diameter similar to T = 4 are able to accommodate the widest range of cargo sizes. PMID:24010404

  11. When is one core per tree sufficient to characterize stand attributes? Results of a Pinus ponderosa case study

    Treesearch

    C.W. Woodall

    2008-01-01

    Increment cores are invaluable for assessing tree attributes such as inside bark diameter, radial growth, and sapwood area. However, because trees accrue growth and sapwood unevenly around their pith, tree attributes derived from one increment core may not provide sufficient precision for forest management/research activities. To assess the variability in a tree's...

  12. Apparatus and Method for Increasing the Diameter of Metal Alloy Wires Within a Molten Metal Pool

    DOEpatents

    Hartman, Alan D.; Argetsinger, Edward R.; Hansen, Jeffrey S.; Paige, Jack I.; King, Paul E.; Turner, Paul C.

    2002-01-29

    In a dip forming process the core material to be coated is introduced directly into a source block of coating material eliminating the need for a bushing entrance component. The process containment vessel or crucible is heated so that only a portion of the coating material becomes molten, leaving a solid portion of material as the entrance port of, and seal around, the core material. The crucible can contain molten and solid metals and is especially useful when coating core material with reactive metals. The source block of coating material has been machined to include a close tolerance hole of a size and shape to closely fit the core material. The core material moves first through the solid portion of the source block of coating material where the close tolerance hole has been machined, then through a solid/molten interface, and finally through the molten phase where the diameter of the core material is increased. The crucible may or may not require water-cooling depending upon the type of material used in crucible construction. The system may operate under vacuum, partial vacuum, atmospheric pressure, or positive pressure depending upon the type of source material being used.

  13. Apparatus and method for increasing the diameter of metal alloy wires within a molten metal pool

    DOEpatents

    Hartman, Alan D.; Argetsinger, Edward R.; Hansen, Jeffrey S.; Paige, Jack I.; King, Paul E.; Turner, Paul C.

    2002-01-29

    In a dip forming process the core material to be coated is introduced directly into a source block of coating material eliminating the need for a bushing entrance component. The process containment vessel or crucible is heated so that only a portion of the coating material becomes molten, leaving a solid portion of material as the entrance port of, and seal around, the core material. The crucible can contain molten and solid metals and is especially useful when coating core material with reactive metals. The source block of coating material has been machined to include a close tolerance hole of a size and shape to closely fit the core material. The core material moves first through the solid portion of the source block of coating material where the close tolerance hole has been machined, then through a solid/molten interface, and finally through the molten phase where the diameter of the core material is increased. The crucible may or may not require water-cooling depending upon the type of material used in crucible construction. The system may operate under vacuum, partial vacuum, atmospheric pressure, or positive pressure depending upon the type of source material being used.

  14. Surface Plasmon Scattering in Exposed Core Optical Fiber for Enhanced Resolution Refractive Index Sensing.

    PubMed

    Klantsataya, Elizaveta; François, Alexandre; Ebendorff-Heidepriem, Heike; Hoffmann, Peter; Monro, Tanya M

    2015-09-29

    Refractometric sensors based on optical excitation of surface plasmons on the side of an optical fiber is an established sensing architecture that has enabled laboratory demonstrations of cost effective portable devices for biological and chemical applications. Here we report a Surface Plasmon Resonance (SPR) configuration realized in an Exposed Core Microstructured Optical Fiber (ECF) capable of optimizing both sensitivity and resolution. To the best of our knowledge, this is the first demonstration of fabrication of a rough metal coating suitable for spectral interrogation of scattered plasmonic wave using chemical electroless plating technique on a 10 μm diameter exposed core of the ECF. Performance of the sensor in terms of its refractive index sensitivity and full width at half maximum (FWHM) of SPR response is compared to that achieved with an unstructured bare core fiber with 140 μm core diameter. The experimental improvement in FWHM, and therefore the detection limit, is found to be a factor of two (75 nm for ECF in comparison to 150 nm for the large core fiber). Refractive index sensitivity of 1800 nm/RIU was achieved for both fibers in the sensing range of aqueous environment (1.33-1.37) suitable for biosensing applications.

  15. PHYSICAL PROPERTIES OF LARGE AND SMALL GRANULES IN SOLAR QUIET REGIONS

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Yu Daren; Xie Zongxia; Hu Qinghua

    The normal mode observations of seven quiet regions obtained by the Hinode spacecraft are analyzed to study the physical properties of granules. An artificial intelligence technique is introduced to automatically find the spatial distribution of granules in feature spaces. In this work, we investigate the dependence of granular continuum intensity, mean Doppler velocity, and magnetic fields on granular diameter. We recognized 71,538 granules by an automatic segmentation technique and then extracted five properties: diameter, continuum intensity, Doppler velocity, and longitudinal and transverse magnetic flux density to describe the granules. To automatically explore the intrinsic structures of the granules in themore » five-dimensional parameter space, the X-means clustering algorithm and one-rule classifier are introduced to define the rules for classifying the granules. It is found that diameter is a dominating parameter in classifying the granules and two families of granules are derived: small granules with diameters smaller than 1.''44, and large granules with diameters larger than 1.''44. Based on statistical analysis of the detected granules, the following results are derived: (1) the averages of diameter, continuum intensity, and Doppler velocity in the upward direction of large granules are larger than those of small granules; (2) the averages of absolute longitudinal, transverse, and unsigned flux density of large granules are smaller than those of small granules; (3) for small granules, the average of continuum intensity increases with their diameters, while the averages of Doppler velocity, transverse, absolute longitudinal, and unsigned magnetic flux density decrease with their diameters. However, the mean properties of large granules are stable; (4) the intensity distributions of all granules and small granules do not satisfy Gaussian distribution, while that of large granules almost agrees with normal distribution with a peak at 1.04 I{sub 0}.« less

  16. Venus small volcano classification and description

    NASA Technical Reports Server (NTRS)

    Aubele, J. C.

    1993-01-01

    The high resolution and global coverage of the Magellan radar image data set allows detailed study of the smallest volcanoes on the planet. A modified classification scheme for volcanoes less than 20 km in diameter is shown and described. It is based on observations of all members of the 556 significant clusters or fields of small volcanoes located and described by this author during data collection for the Magellan Volcanic and Magmatic Feature Catalog. This global study of approximately 10 exp 4 volcanoes provides new information for refining small volcano classification based on individual characteristics. Total number of these volcanoes was estimated to be 10 exp 5 to 10 exp 6 planetwide based on pre-Magellan analysis of Venera 15/16, and during preparation of the global catalog, small volcanoes were identified individually or in clusters in every C1-MIDR mosaic of the Magellan data set. Basal diameter (based on 1000 measured edifices) generally ranges from 2 to 12 km with a mode of 34 km, and follows an exponential distribution similar to the size frequency distribution of seamounts as measured from GLORIA sonar images. This is a typical distribution for most size-limited natural phenomena unlike impact craters which follow a power law distribution and continue to infinitely increase in number with decreasing size. Using an exponential distribution calculated from measured small volcanoes selected globally at random, we can calculate total number possible given a minimum size. The paucity of edifice diameters less than 2 km may be due to inability to identify very small volcanic edifices in this data set; however, summit pits are recognizable at smaller diameters, and 2 km may represent a significant minimum diameter related to style of volcanic eruption. Guest, et al, discussed four general types of small volcanic edifices on Venus: (1) small lava shields; (2) small volcanic cones; (3) small volcanic domes; and (4) scalloped margin domes ('ticks'). Steep-sided domes or 'pancake domes', larger than 20 km in diameter, were included with the small volcanic domes. For the purposes of this study, only volcanic edifices less than 20 km in diameter are discussed. This forms a convenient cutoff since most of the steep-sided domes ('pancake domes') and scalloped margin domes ('ticks') are 20 to 100 km in diameter, are much less numerous globally than are the smaller diameter volcanic edifices (2 to 3 orders of magnitude lower in total global number), and do not commonly occur in large clusters or fields of large numbers of edifices.

  17. Reproducibility of ECG-gated ultrasound diameter assessment of small abdominal aortic aneurysms.

    PubMed

    Bredahl, K; Eldrup, N; Meyer, C; Eiberg, J E; Sillesen, H

    2013-03-01

    No standardised ultrasound procedure to obtain reliable growth estimates for abdominal aortic aneurysms (AAA) is currently available. We investigated the feasibility and reproducibility of a novel approach controlling for a combination of vessel wall delineation and cardiac cycle variation. Prospective comparative study. Consecutive patients (N = 27) with an AAA, attending their 6-month control as part of a medical treatment trial, were scanned twice by two ultrasound operators. Then, all ultrasound recordings were transferred to a core facility and analysed by a third person. The AAA diameter was determined in four different ways: from the leading edge of adventitia on the anterior wall to either the leading edge of the adventitia (method A) or leading edge of the intima (method B) on the posterior wall, with both measurements performed in systole and diastole. Inter-operator reproducibility was ± 3 mm for all methods applied. There was no difference in outcome between methods A and B; likewise, end-diastolic measurement did not improve reproducibility in preference to peak-systolic measurement. The use of a standardised ultrasound protocol including ECG-gating and subsequent off-line reading with minute calliper placement reduces variability. This may be of use in developing protocols to better detect even small AAA growth rates during clinical trials. Copyright © 2012 European Society for Vascular Surgery. Published by Elsevier Ltd. All rights reserved.

  18. Microencapsulation of gallium-indium (Ga-In) liquid metal for self-healing applications.

    PubMed

    Blaiszik, B J; Jones, A R; Sottos, N R; White, S R

    2014-01-01

    Microcapsules containing a liquid metal alloy core of gallium-indium (Ga-In) are prepared via in situ urea-formaldehyde (UF) microencapsulation. The capsule size, shape, thermal properties, and shell wall thickness are investigated. We prepare ellipsoidal capsules with major and minor diameter aspect ratios ranging from 1.64 to 1.08 and with major diameters ranging from 245 µm to 3 µm. We observe that as the capsule major diameter decreases, the aspect ratio approaches 1. The thermal properties of the prepared microcapsules are investigated by thermogravimetric (TGA) and differential scanning calorimetry (DSC). Microcapsules are shown to survive incorporation into an epoxy matrix and to trigger via mechanical damage to the cured matrix. Microcapsules containing liquid metal cores may have diverse applications ranging from self-healing to contrast enhancement or the demonstration of mechano-adaptive circuitry.

  19. Hyaluronic acid enhancement of expanded polytetrafluoroethylene for small diameter vascular grafts

    NASA Astrophysics Data System (ADS)

    Lewis, Nicole R.

    Cardiovascular disease is the leading cause of mortality and morbidity in the United States and other developed countries. In the United States alone, 8 million people are diagnosed with peripheral arterial disease per year and over 250,000 patients have coronary bypass surgery each year. Autologous blood vessels are the standard graft used in small diameter (<6mm) arterial bypass procedures. Synthetic small diameter grafts have had limited success. While polyethylene (Dacron) and expanded polytetrafluoroethylene (ePTFE) are the most commonly used small diameter synthetic vascular graft materials, there are significant limitations that make these materials unfavorable for use in the low blood flow conditions of the small diameter arteries. Specifically, Dacron and ePTFE grafts display failure due to early thrombosis or late intimal hyperplasia. With the shortage of tissue donors and the limited supply of autologous blood vessels available, there is a need for a small diameter synthetic vascular graft alternative. The aim of this research is to create and characterize ePTFE grafts prepared with hyaluronic acid (HA), evaluate thrombogenic potential of ePTFE-HA grafts, and evaluate graft mechanical properties and coating durability. The results in this work indicate the successful production of ePTFE-HA materials using a solvent infiltration technique. Surface interactions with blood show increased platelet adhesion on HA-modified surfaces, though evidence may suggest less platelet activation and erythrocyte lysis. Significant changes in mechanical properties of HA-modified ePTFE materials were observed. Further investigation into solvent selection, uniformity of HA, endothelialization, and dynamic flow testing would be beneficial in the evaluation of these materials for use in small diameter vascular graft bypass procedures.

  20. 76 FR 67411 - Small Diameter Graphite Electrodes From the People's Republic of China: Extension of Time Limit...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-11-01

    ... DEPARTMENT OF COMMERCE International Trade Administration [A-570-929] Small Diameter Graphite... diameter graphite electrodes from the People's Republic of China (PRC) for the period February 1, 2010... Graphite, Co. The preliminary results of the review are currently due no later than October 31, 2011...

  1. Catheter placement for lysis of spontaneous intracerebral hematomas: does a catheter position in the core of the hematoma allow more effective and faster hematoma lysis?

    PubMed

    Malinova, Vesna; Schlegel, Anna; Rohde, Veit; Mielke, Dorothee

    2017-07-01

    For the fibrinolytic therapy of intracerebral hematomas (ICH) using recombinant tissue plasminogen activator (rtPA), a catheter position in the core of the hematoma along the largest clot diameter was assumed to be optimal for an effective clot lysis. However, it never had been proven that core position indeed enhances clot lysis if compared with less optimal catheter positions. In this study, the impact of the catheter position on the effectiveness and on the time course of clot lysis was evaluated. We analyzed the catheter position using a relative error calculating the distance perpendicular to the catheter's center in relation to hematoma's diameter and evaluated the relative hematoma volume reduction (RVR). The correlation of the RVR with the catheter position was evaluated. Additionally, we tried to identify patterns of clot lysis with different catheter positions. The patient's outcome at discharge was evaluated using the Glasgow outcome score. A total of 105 patients were included in the study. The mean hematoma volume was 56 ml. The overall RVR was 62.7 %. In 69 patients, a catheter position in the core of the clot was achieved. We found no significant correlation between catheter position and hematoma RVR (linear regression, p = 0.14). Core catheter position leads to more symmetrical hematoma RVR. Faster clot lysis happens in the vicinity of the catheter openings. We found no significant difference in the patient's outcome dependent on the catheter position (linear regression, p = 0.90). The catheter position in the core of the hematoma along its largest diameter does not significantly influence the effectiveness of clot lysis after rtPA application.

  2. Cervical stability training with and without core stability training for patients with cervical disc herniation: A randomized, single-blind study.

    PubMed

    Buyukturan, B; Guclu-Gunduz, A; Buyukturan, O; Dadali, Y; Bilgin, S; Kurt, E E

    2017-11-01

    This study aims at evaluating and comparing the effects of cervical stability training to combined cervical and core stability training in patients with neck pain and cervical disc herniation. Fifty patients with neck pain and cervical disc herniation were included in the study, randomly divided into two groups as cervical stability and cervical-core stability. Training was applied three times a week in three phases, and lasted for a total duration of 8 weeks. Pain, activation and static endurance of deep cervical flexor muscles, static endurance of neck muscles, cross-sectional diameter of M. Longus Colli, static endurance of trunk muscles, disability and kinesiophobia were assessed. Pain, activation and static endurance of deep cervical flexors, static endurance of neck muscles, cross-sectional diameter of M. Longus Colli, static endurance of trunk muscles, disability and kinesiophobia improved in both groups following the training sessions (p < 0.05). Comparison of the effectiveness of these two training methods revealed that the cervical stability group produced a greater increase in the right transverse diameter of M. Longus Colli (p < 0.05). However, static endurance of trunk muscles and kinesiophobia displayed better improvement in the cervical-core stability group (p < 0.05). Cervical stability training provided benefit to patients with cervical disc herniation. The addition of core stability training did not provide any additional significant benefit. Further research is required to investigate the efficacy of combining other techniques with cervical stability training in patients with cervical disc herniation. Both cervical stability training and its combination with core stability training were significantly and similarly effective on neck pain and neck muscle endurance in patients with cervical disc herniation. © 2017 European Pain Federation - EFIC®.

  3. Increasing number of small hole diameter microfracture compared with traditional microfracture in same size cartilage defects and effect of HA based aselluler scaffold. An animal study

    PubMed Central

    Uzer, Gökçer; Elmadağ, Nuh Mehmet; Yıldız, Fatih; Güzel, Yunus; Tok, Olgu Enis

    2017-01-01

    Purpose: The purpose of this study is small hole microfracure method comparing with traditional microfracture method and investigation of effect of HA based acellular matrix scaffold on microfracture area. Materials-Methods: 21 Twenty-one New Zealand white rabbits were used for the in vitro portion of this study, bilateral knee joint from the same rabbit were same technic. An articular cartilage defect was established in the femoral trochlear groove about 5 mm. Control group was established alone microfracture (MF). 6 groups were formed in this study and each group has 3 rabbits and their six knees. In 3 groups were applied different number of small diameter hole microfracture (4,5,6 small holes microfracture respectively)and the other 3 groups were applied different number of small diameter hole microfracture (4,5,6 small holes micro fracture respectively added HA based acellular matrix scaffold in the same size ostechondral lesion. The regenerated tissues were harvested for gross morphology, histology at 12 weeks postoperatively. Results: Cartilage were regenerated, maintaining a constant thickness of cartilage. MF group has worse Wakitani scores than 6 small diameter holes mıcrofracture groups(group 6 and group 7) in either parameter of the score. (p=0,043, p=0,016) Matrix addition did not contribute to healing. (p=1,000) Conclusions: Increasing number of the small diameter holes microfracture (minimum %15 of defect size) improves cartilage repair compared with traditional MF in the same size ostechondral lesion. Also small diameter holes microfracture combined with HA-based AM implantation didn’t result in improved quality of the regenerated cartilage tissue.

  4. Nuclear reactor

    DOEpatents

    Wade, Elman E.

    1979-01-01

    A nuclear reactor including two rotatable plugs and a positive top core holddown structure. The top core holddown structure is divided into two parts: a small core cover, and a large core cover. The small core cover, and the upper internals associated therewith, are attached to the small rotating plug, and the large core cover, with its associated upper internals, is attached to the large rotating plug. By so splitting the core holddown structures, under-the-plug refueling is accomplished without the necessity of enlarging the reactor pressure vessel to provide a storage space for the core holddown structure during refueling. Additionally, the small and large rotating plugs, and their associated core covers, are arranged such that the separation of the two core covers to permit rotation is accomplished without the installation of complex lifting mechanisms.

  5. Formation of Mesosiderites: Fragmentation and Reaccretion of a Large Differentiated Asteroid

    NASA Technical Reports Server (NTRS)

    Scott, Edward R. D.; Haack, Henning; Love, Stanley G.

    2001-01-01

    We propose that these stony-iron meteorites formed when a 50-150 km diameter projectile disrupted a 200-400 km diameter asteroid with a molten core. Several mineralogical features of mesosiderites need reinterpreting if our model is correct. Additional information is contained in the original extended abstract.

  6. Aerodynamic effect of a honeycomb rotor tip shroud on a 50.8-centimeter-tip-diameter core turbine

    NASA Technical Reports Server (NTRS)

    Moffitt, T. P.; Whitney, W. J.

    1983-01-01

    A 50.8-cm-tip-diameter turbine equipped with a rotor tip shroud of hexagonal cell (or honeycomb) cross section has been tested in warm air (416 K) for a range of shroud coolant to primary flow rates. Test results were also obtained for the same turbine operated with a solid shroud for comparison. The results showed that the combined effect of the honeycomb shroud and the coolant flow was to cause a reduction of 2.8 points in efficiency at design speed, pressure ratio, and coolant flow rate. With the coolant system inactivated, the honeycomb shroud caused a decrease in efficiency of 2.3 points. These results and those obtained from a small reference turbine indicate that the dominant factor governing honeycomb tip shroud loss is the ratio of honeycomb depth to blade span. The loss results of the two shrouds could be correlated on this basis. The same honeycomb and coolant effects are expected to occur for the hot (2200 K) version of this turbine.

  7. A small-diameter NMR logging tool for groundwater investigations

    USGS Publications Warehouse

    Walsh, David; Turner, Peter; Grunewald, Elliot; Zhang, Hong; Butler, James J.; Reboulet, Ed; Knobbe, Steve; Christy, Tom; Lane, John W.; Johnson, Carole D.; Munday, Tim; Fitzpatrick, Andrew

    2013-01-01

    A small-diameter nuclear magnetic resonance (NMR) logging tool has been developed and field tested at various sites in the United States and Australia. A novel design approach has produced relatively inexpensive, small-diameter probes that can be run in open or PVC-cased boreholes as small as 2 inches in diameter. The complete system, including surface electronics and various downhole probes, has been successfully tested in small-diameter monitoring wells in a range of hydrogeological settings. A variant of the probe that can be deployed by a direct-push machine has also been developed and tested in the field. The new NMR logging tool provides reliable, direct, and high-resolution information that is of importance for groundwater studies. Specifically, the technology provides direct measurement of total water content (total porosity in the saturated zone or moisture content in the unsaturated zone), and estimates of relative pore-size distribution (bound vs. mobile water content) and hydraulic conductivity. The NMR measurements show good agreement with ancillary data from lithologic logs, geophysical logs, and hydrogeologic measurements, and provide valuable information for groundwater investigations.

  8. Determination of relative phase permeabilities in stochastic model of pore channel distribution by diameter

    NASA Astrophysics Data System (ADS)

    Zemenkova, M. Y.; Shabarov, A.; Shatalov, A.; Puldas, L.

    2018-05-01

    The problem of the pore space description and the calculation of relative phase permeabilities (RPP) for two-phase filtration is considered. A technique for constructing a pore-network structure for constant and variable channel diameters is proposed. A description of the design model of RPP based on the capillary pressure curves is presented taking into account the variability of diameters along the length of pore channels. By the example of the calculation analysis for the core samples of the Urnenskoye and Verkhnechonskoye deposits, the possibilities of calculating RPP are shown when using the stochastic distribution of pores by diameters and medium-flow diameters.

  9. Effect of Two-Step Metal Organic Chemical Vapor Deposition Growth on Quality, Diameter and Density of InAs Nanowires on Si (111) Substrate

    NASA Astrophysics Data System (ADS)

    Yu, Hung Wei; Anandan, Deepak; Hsu, Ching Yi; Hung, Yu Chih; Su, Chun Jung; Wu, Chien Ting; Kakkerla, Ramesh Kumar; Ha, Minh Thien Huu; Huynh, Sa Hoang; Tu, Yung Yi; Chang, Edward Yi

    2018-02-01

    High-density (˜ 80/um2) vertical InAs nanowires (NWs) with small diameters (˜ 28 nm) were grown on bare Si (111) substrates by means of two-step metal organic chemical vapor deposition. There are two critical factors in the growth process: (1) a critical nucleation temperature for a specific In molar fraction (approximately 1.69 × 10-5 atm) is the key factor to reduce the size of the nuclei and hence the diameter of the InAs NWs, and (2) a critical V/III ratio during the 2nd step growth will greatly increase the density of the InAs NWs (from 45 μm-2 to 80 μm-2) and at the same time keep the diameter small. The high-resolution transmission electron microscopy and selected area diffraction patterns of InAs NWs grown on Si exhibit a Wurtzite structure and no stacking faults. The observed longitudinal optic peaks in the Raman spectra were explained in terms of the small surface charge region width due to the small NW diameter and the increase of the free electron concentration, which was consistent with the TCAD program simulation of small diameter (< 40 nm) InAs NWs.

  10. Material with core-shell structure

    DOEpatents

    Luhrs, Claudia [Rio Rancho, NM; Richard, Monique N [Ann Arbor, MI; Dehne, Aaron [Maumee, OH; Phillips, Jonathan [Rio Rancho, NM; Stamm, Kimber L [Ann Arbor, MI; Fanson, Paul T [Brighton, MI

    2011-11-15

    Disclosed is a material having a composite particle, the composite particle including an outer shell and a core. The core is made from a lithium alloying material and the outer shell has an inner volume that is greater in size than the core of the lithium alloying material. In some instances, the outer mean diameter of the outer shell is less than 500 nanometers and the core occupies between 5 and 99% of the inner volume. In addition, the outer shell can have an average wall thickness of less than 100 nanometers.

  11. Environmental performance of an elliptical core polarization maintaining optical fiber for fiber optic gyro applications

    NASA Astrophysics Data System (ADS)

    Martinelli, Vincent P.; Squires, Emily M.; Watkins, James J.

    1994-03-01

    Corning has introduced a new polarization-maintaining optical fiber to satisfy customer requirements for a range of commercial and military FOG applications. This fiber has an elliptical core, matched-clad design, and is intended for operation in the 780 to 850 nm wavelength region. The fiber has a beat length less than 1.5 mm, attenuation rate less than 10 dB/km, and a typical coiled h-parameter less than 1.5 X 10-4 m-1 in the designated operating wavelength range. It has a cladding diameter of 80 micrometers and a coating diameter of 185 micrometers . The coating is an acrylate system, similar to that used in telecommunications optical fibers. We report on the performance of this elliptical core fiber for a variety of environmental exposures representative of an automotive application.

  12. Integrated-optics heralded controlled-NOT gate for polarization-encoded qubits

    NASA Astrophysics Data System (ADS)

    Zeuner, Jonas; Sharma, Aditya N.; Tillmann, Max; Heilmann, René; Gräfe, Markus; Moqanaki, Amir; Szameit, Alexander; Walther, Philip

    2018-03-01

    Recent progress in integrated-optics technology has made photonics a promising platform for quantum networks and quantum computation protocols. Integrated optical circuits are characterized by small device footprints and unrivalled intrinsic interferometric stability. Here, we take advantage of femtosecond-laser-written waveguides' ability to process polarization-encoded qubits and present an implementation of a heralded controlled-NOT gate on chip. We evaluate the gate performance in the computational basis and a superposition basis, showing that the gate can create polarization entanglement between two photons. Transmission through the integrated device is optimized using thermally expanded core fibers and adiabatically reduced mode-field diameters at the waveguide facets. This demonstration underlines the feasibility of integrated quantum gates for all-optical quantum networks and quantum repeaters.

  13. Determination of bioactive compounds in the juice of pummelo (Citrus grandis Osbeck).

    PubMed

    Russo, Marina; Bonaccorsi, Ivana; Torre, Germana; Cotroneo, Antonella; Dugo, Paola; Mondello, Luigi

    2013-02-01

    The juice of pummelo (Citrus grandis Osbeck) was analyzed to determine its composition of flavonoids, polymethoxyflavones, coumarins and psoralens. The analyses were carried out by HPLC using columns packed with small diameter Fused-Core C18 particles to achieve high resolution in short analysis time. In addition, the profile of the native carotenoids present in the juice was determined using a C30 column. Identification of flavonoids was achieved by MS with ESI in negative mode; the MS acquisition of oxygenated heterocyclic compounds was performed in positive APCI; carotenoids were detected with a PDA detector. Nineteen native carotenoids were determined in pummelo juice for the first time. The composition of this juice is also discussed in comparison with other Citrus juices, especially grapefruit.

  14. Gas-driven pump for ground-water samples

    USGS Publications Warehouse

    Signor, Donald C.

    1978-01-01

    Observation wells installed for artificial-recharge research and other wells used in different ground-water programs are frequently cased with small-diameter steel pipe. To obtain samples from these small-diameter wells in order to monitor water quality, and to calibrate solute-transport models, a small-diameter pump with unique operating characteristics is required that causes a minimum alternation of samples during field sampling. A small-diameter gas-driven pump was designed and built to obtain water samples from wells of two-inch diameter or larger. The pump is a double-piston type with the following characteristics: (1) The water sample is isolated from the operating gas, (2) no source of electricity is ncessary, (3) operation is continuous, (4) use of compressed gas is efficient, and (5) operation is reliable over extended periods of time. Principles of operation, actual operation techniques, gas-use analyses and operating experience are described. Complete working drawings and a component list are included. Recent modifications and pump construction for high-pressure applications also are described. (Woodard-USGS)

  15. SMALL DIAMETER CEMENT LINING FROM STAIRWAY. United States Pipe ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    SMALL DIAMETER CEMENT LINING FROM STAIRWAY. - United States Pipe & Foundry Company Plant, Coating, Painting, Lining & Packaging Building, 2023 St. Louis Avenue at I-20/59, Bessemer, Jefferson County, AL

  16. Fusion splicing small-core photonic crystal fibers and single-mode fibers by repeated arc discharges.

    PubMed

    Xiao, Limin; Jin, Wei; Demokan, M S

    2007-01-15

    We demonstrate a novel method for low-loss splicing small-core photonic crystal fibers (PCFs) and single-mode fibers (SMFs) by repeated arc discharges using a conventional fusion splicer. An optimum mode field match at the interface of PCF-SMF and an adiabatic mode field variation in the longitudinal direction of the small-core PCF can be achieved by repeated arc discharges applied over the splicing joint to gradually collapse the air holes of the small-core PCF. This method is simple and offers a practical solution for light coupling between small-core PCFs and SMFs.

  17. Fusion splicing small-core photonic crystal fibers and single-mode fibers by repeated arc discharges

    NASA Astrophysics Data System (ADS)

    Xiao, Limin; Jin, Wei; Demokan, M. S.

    2007-01-01

    We demonstrate a novel method for low-loss splicing small-core photonic crystal fibers (PCFs) and single-mode fibers (SMFs) by repeated arc discharges using a conventional fusion splicer. An optimum mode field match at the interface of PCF-SMF and an adiabatic mode field variation in the longitudinal direction of the small-core PCF can be achieved by repeated arc discharges applied over the splicing joint to gradually collapse the air holes of the small-core PCF. This method is simple and offers a practical solution for light coupling between small-core PCFs and SMFs.

  18. Soil compaction after yarding of small-diameter Douglas-fir with a small tractor in southwest Oregon.

    Treesearch

    Michael P. Amaranthus; David E. Steinfeld

    1997-01-01

    This study evaluated the effect on soil bulk density of yarding small-diameter Douglas-fir (Pseudosuga menziesii var. glauca (Beissn.) Franco) with a small tractor. Levels of compaction were measured before yarding and after one trip, three trips, and six trips by the tractor. Bulk densities in the surface (10 cm) and...

  19. High energy, single-polarized, single-transverse-mode, nanosecond pulses generated by a multi-stage Yb-doped photonic crystal fiber amplifier

    NASA Astrophysics Data System (ADS)

    Shen, Xinglai; Zhang, Haitao; Hao, He; Li, Dan; Li, Qinghua; Yan, Ping; Gong, Mali

    2015-06-01

    We report the construction of a cascaded fiber amplifier where a 40-μm-core-diameter photonic crystal fiber is utilized in the main amplifier stage. Single-transverse-mode, linearly-polarized, 7.5 ns pulses with 1.5 mJ energy, 123 kW peak power and 10 nm spectral bandwidth centered at 1062 nm are generated. To our knowledge, the pulse energy we obtain is the highest from 40-μm-core-diameter photonic crystal fibers, and also the highest for long pulses (>1 ns) with linear polarization and single transverse mode.

  20. A wireline piston core barrel for sampling cohesionless sand and gravel below the water table

    USGS Publications Warehouse

    Zapico, Michael M.; Vales, Samuel; Cherry, John A.

    1987-01-01

    A coring device has been developed to obtain long and minimally disturbed samples of saturated cohesionless sand and gravel. The coring device, which includes a wireline and piston, was developed specifically for use during hollow-stem auger drilling but it also offers possibilities for cable tool and rotary drilling. The core barrel consists of an inner liner made of inexpensive aluminum or plastic tubing, a piston for core recovery, and an exterior steel housing that protects the liner when the core barrel is driven into the aquifer. The core barrel, which is approximately 1.6m (5.6 feet) long, is advanced ahead of the lead auger by hammering at the surface on drill rods that are attached to the core barrel. After the sampler has been driven 1.5m (5 feet), the drill rods are detached and a wireline is used to hoist the core barrel, with the sample contained in the aluminum or plastic liner, to the surface. A vacuum developed by the piston during the coring operation provides good recovery of both the sediment and aquifer fluids contained in the sediment. In the field the sample tubes can be easily split along their length for on-site inspection or they can be capped with the pore water fluids inside and transported to the laboratory. The cores are 5cm (2 inches) in diameter by 1.5m (5 feet) long. Core acquisition to depths of 35m (115 feet), with a recovery greater than 90 percent, has become routine in University of Waterloo aquifer studies. A large diameter (12.7cm [5 inch]) version has also been used successfully. Nearly continuous sample sequences from sand and gravel aquifers have been obtained for studies of sedimentology, hydraulic conductivity, hydrogeochemistry and microbiology.

  1. One-dimensional carrier confinement in “Giant” CdS/CdSe excitonic nanoshells

    DOE PAGES

    Razgoniaeva, Natalia; Moroz, Pavel; Yang, Mingrui; ...

    2017-05-23

    Here, the emerging generation of quantum dot optoelectronic devices offers an appealing prospect of a size-tunable band gap. The confinement-enabled control over electronic properties, however, requires nanoparticles to be sufficiently small, which leads to a large area of interparticle boundaries in a film. Such interfaces lead to a high density of surface traps which ultimately increase the electrical resistance of a solid. To address this issue, we have developed an inverse energy-gradient core/shell architecture supporting the quantum confinement in nanoparticles larger than the exciton Bohr radius. The assembly of such nanostructures exhibits a relatively low surface-to-volume ratio, which was manifestedmore » in this work through the enhanced conductance of solution-processed films. The reported core/shell geometry was realized by growing a narrow gap semiconductor layer (CdSe) on the surface of a wide-gap core material (CdS) promoting the localization of excitons in the shell domain, as was confirmed by ultrafast transient absorption and emission lifetime measurements. The band gap emission of fabricated nanoshells, ranging from 15 to 30 nm in diameter, has revealed a characteristic size-dependent behavior tunable via the shell thickness with associated quantum yields in the 4.4–16.0% range.« less

  2. A new method to quantitatively compare focal ratio degradation due to different end termination techniques

    NASA Astrophysics Data System (ADS)

    Poppett, Claire; Allington-Smith, Jeremy

    2010-07-01

    We investigate the FRD performance of a 150 μm core fibre for its suitability to the SIDE project.1 This work builds on our previous work2 (Paper 1) where we examined the dependence of FRD on length in fibres with a core size of 100 μm and proposed a new multi-component model to explain the results. In order to predict the FRD characteristics of a fibre, the most commonly used model is an adaptation of the Gloge8model by Carrasco and Parry3 which quantifies the the number of scattering defects within an optical bre using a single parameter, d0. The model predicts many trends which are seen experimentally, for example, a decrease in FRD as core diameter increases, and also as wavelength increases. However the model also predicts a strong dependence on FRD with length that is not seen experimentally. By adapting the single fibre model to include a second fibre, we can quantify the amount of FRD due to stress caused by the method of termination. By fitting the model to experimental data we find that polishing the fibre causes a small increase in stress to be induced in the end of the fibre compared to a simple cleave technique.

  3. In situ growth of hollow gold-silver nanoshells within porous silica offers tunable plasmonic extinctions and enhanced colloidal stability.

    PubMed

    Li, Chien-Hung; Jamison, Andrew C; Rittikulsittichai, Supparesk; Lee, Tai-Chou; Lee, T Randall

    2014-11-26

    Porous silica-coated hollow gold-silver nanoshells were successfully synthesized utilizing a procedure where the porous silica shell was produced prior to the transformation of the metallic core, providing enhanced control over the structure/composition of the bimetallic hollow core. By varying the reaction time and the precise amount of gold salt solution added to a porous silica-coated silver-core template solution, composite nanoparticles were tailored to reveal a readily tunable surface plasmon resonance that could be centered across the visible and near-IR spectral regions (∼445-800 nm). Characterization by X-ray photoelectron spectroscopy, energy-dispersive X-ray spectroscopy, scanning electron microscopy, and transmission electron microscopy revealed that the synthetic methodology afforded particles having uniform composition, size, and shape. The optical properties were evaluated by absorption/extinction spectroscopy. The stability of colloidal solutions of our composite nanoparticles as a function of pH was also investigated, revealing that the nanoshells remain intact over a wide range of conditions (i.e., pH 2-10). The facile tunability, enhanced stability, and relatively small diameter of these composite particles (∼110 nm) makes them promising candidates for use in tumor ablation or as photothermal drug-delivery agents.

  4. Experiments on the formation and properties of thin vortex rings in water.

    NASA Astrophysics Data System (ADS)

    Donnelly, Russell; Stange, Alex; Julian, Brian

    2001-11-01

    We have been experimenting for some time with a vortex gun 2.54 cm in diameter with a piston powered by a small servo motor . Strokes can be generated up to about 3 cm. The object has been to determine the properties of the rings formed by this gun as if they were thin rings in an inviscid fluid. That is, we are trying to characterize the rings by their radius, core parameter, velocity, and circulation. We are also studying the slowing of these rings as they propagate across the tank. Visualization is by means of an electrochemical (Baker) technique. In general the rings propagate with nearly constant radius and speed. The core size remains apparently unchanged, as would be expected with our visualization technique. We are able to propagate rings with velocities up to about 35 cm/s. Their radius at the exit of the gun grows with the stroke length. The core parameter and circulation appear fairly consistent with the slug model. We are attempting to devise a method of measuring the impulse of the vortex ring in flight, and will report on progress. The ultimate goal of the experiment is to study collisions of rings, and the role of reconnections for thin vortices.

  5. Electrospun Polyurethane-Core and Gelatin-Shell Coaxial Fibre Coatings for Miniature Implantable Biosensors

    PubMed Central

    Wang, Ning; Burugapalli, Krishna; Wijesuriya, Shavini; Far, Mahshid Yazdi; Song, Wenhui; Moussy, Francis; Zheng, Yudong; Ma, Yanxuan; Wu, Zhentao; Li, Kang

    2014-01-01

    The aim of this study was to introduce bioactivity to the electrospun coating for implantable glucose biosensors. Coaxial fibre membranes having polyurethane as the core and gelatin as the shell were produced using a range of polyurethane concentrations (2, 4, 6 & 8% wt/v) while keeping gelatin concentration (10% wt/v) constant in 2,2,2-trifluoroethanol. The gelatin shell was stabilized using glutaraldehyde vapour. The formation of core-shell structure was confirmed using TEM, SEM and FTIR. The coaxial fibre membranes showed uniaxial tensile properties intermediate to that of the pure polyurethane and the gelatin fibre membranes. The gelatin shell increased hydrophilicity and glucose transport flux across the coaxial fibre membranes. The coaxial fibre membranes having small fibre diameter (541 nm) and a thick gelatin shell (52%) did not affect the sensor sensitivity, but decreased sensor’s linearity in the long run. In contrast, thicker coaxial fibre membranes (1133 nm) having a thin gelatin shell (34%) maintained both sensitivity and linearity till 84 days of the study period. To conclude, polyurethane-gelatin co-axial fibre membranes, due to their faster permeability to glucose, tailorable mechanical properties and bioactivity are potential candidates for coatings to favourably modify the host responses to extend the reliable in vivo lifetime of implantable glucose biosensors. PMID:24346001

  6. One-dimensional carrier confinement in “Giant” CdS/CdSe excitonic nanoshells

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Razgoniaeva, Natalia; Moroz, Pavel; Yang, Mingrui

    Here, the emerging generation of quantum dot optoelectronic devices offers an appealing prospect of a size-tunable band gap. The confinement-enabled control over electronic properties, however, requires nanoparticles to be sufficiently small, which leads to a large area of interparticle boundaries in a film. Such interfaces lead to a high density of surface traps which ultimately increase the electrical resistance of a solid. To address this issue, we have developed an inverse energy-gradient core/shell architecture supporting the quantum confinement in nanoparticles larger than the exciton Bohr radius. The assembly of such nanostructures exhibits a relatively low surface-to-volume ratio, which was manifestedmore » in this work through the enhanced conductance of solution-processed films. The reported core/shell geometry was realized by growing a narrow gap semiconductor layer (CdSe) on the surface of a wide-gap core material (CdS) promoting the localization of excitons in the shell domain, as was confirmed by ultrafast transient absorption and emission lifetime measurements. The band gap emission of fabricated nanoshells, ranging from 15 to 30 nm in diameter, has revealed a characteristic size-dependent behavior tunable via the shell thickness with associated quantum yields in the 4.4–16.0% range.« less

  7. SMALL DIAMETER PRECEMENT LINING FROM CATWALK ABOVE. United States ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    SMALL DIAMETER PRE-CEMENT LINING FROM CATWALK ABOVE. - United States Pipe & Foundry Company Plant, Coating, Painting, Lining & Packaging Building, 2023 St. Louis Avenue at I-20/59, Bessemer, Jefferson County, AL

  8. 20 years of KVH fiber optic gyro technology: the evolution from large, low performance FOGs to compact, precise FOGs and FOG-based inertial systems

    NASA Astrophysics Data System (ADS)

    Napoli, Jay

    2016-05-01

    Precision fiber optic gyroscopes (FOGs) are critical components for an array of platforms and applications ranging from stabilization and pointing orientation of payloads and platforms to navigation and control for unmanned and autonomous systems. In addition, FOG-based inertial systems provide extremely accurate data for geo-referencing systems. Significant improvements in the performance of FOGs and FOG-based inertial systems at KVH are due, in large part, to advancements in the design and manufacture of optical fiber, as well as in manufacturing operations and signal processing. Open loop FOGs, such as those developed and manufactured by KVH Industries, offer tactical-grade performance in a robust, small package. The success of KVH FOGs and FOG-based inertial systems is due to innovations in key fields, including the development of proprietary D-shaped fiber with an elliptical core, and KVH's unique ThinFiber. KVH continually improves its FOG manufacturing processes and signal processing, which result in improved accuracies across its entire FOG product line. KVH acquired its FOG capabilities, including its patented E•Core fiber, when the company purchased Andrew Corporation's Fiber Optic Group in 1997. E•Core fiber is unique in that the light-guiding core - critical to the FOG's performance - is elliptically shaped. The elliptical core produces a fiber that has low loss and high polarization-maintaining ability. In 2010, KVH developed its ThinFiber, a 170-micron diameter fiber that retains the full performance characteristics of E•Core fiber. ThinFiber has enabled the development of very compact, high-performance open-loop FOGs, which are also used in a line of FOG-based inertial measurement units and inertial navigation systems.

  9. Photonic crystal fiber heat sensors

    NASA Astrophysics Data System (ADS)

    Twigg, S.; Coompson, J.; Colalillo, A.; Wynne, R.

    2011-04-01

    A sensing configuration based on commercially available triple-core photonic crystal fiber (PCF) for the image-based collection of thermal information is presented. Detection of thermal phenomena on the micro and nano scale is important for monitoring thermodynamic processes including cooling mechanisms for industry and basic research in both civil and mechanical systems. The thermal characteristics of the PCF combined with coupled-mode theory principles are used to construct a three core PCF with a 1-D core arrangement to simultaneously measure heat flux and temperature. The PCF sensor demonstrated high detection sensitivity (<1°C) and fast response times (<30μs), which is a significant improvement to current commercial standards. PCFs are specialty optical fibers that contain carefully spaced micronsized cavities that provide extraordinary waveguide characteristics not demonstrated by standard optical fiber. The three core PCF has a core diameter of 3.9μm, outer diameter of 132.5μm and varied inter core spacing. A single mode fiber is fusion spliced with the multi-core PCF such that the optical field is confined and launched into the PCF core. The output end of the fiber is inspected and imaged with a CCD camera. A 25mm section of the PCF is surrounded by a guarded hotplate configuration to control the thermal conditions for sensor characterization. Evanescent wave coupling occurs whereby power is transferred from the central core to a neighboring core. Minimum detection sensitivities of 0.2 °C were recorded. Theoretical sensitivities on the order of 10-2 °C are possible. Experimental results were in agreement with coupled-mode theoretical results.

  10. A 5-mm piezo-scanning fiber device for high speed ultrafast laser microsurgery

    PubMed Central

    Ferhanoglu, Onur; Yildirim, Murat; Subramanian, Kaushik; Ben-Yakar, Adela

    2014-01-01

    Towards developing precise microsurgery tools for the clinic, we previously developed image-guided miniaturized devices using low repetition rate amplified ultrafast lasers for surgery. To improve the speed of tissue removal while reducing device diameter, here we present a new 5-mm diameter device that delivers high-repetition rate laser pulses for high speed ultrafast laser microsurgery. The device consists of an air-core photonic bandgap fiber (PBF) for the delivery of high energy pulses, a piezoelectric tube actuator for fiber scanning, and two aspheric lenses for focusing the light. Its inline optical architecture provides easy alignment and substantial size reduction to 5 mm diameter as compared to our previous MEMS-scanning devices while realizing improved intensity squared (two-photon) lateral and axial resolutions of 1.16 μm and 11.46 μm, respectively. Our study also sheds light on the maximum pulse energies that can be delivered through the air-core PBF and identifies cladding damage at the input facet of the fiber as the limiting factor. We have achieved a maximum energy delivery larger than 700 nJ at 92% coupling efficiency. An in depth analysis reveals how this value is greatly affected by possible slight misalignments of the beam during coupling and the measured small beam pointing fluctuations. In the absence of these imperfections, self-phase modulation becomes the limiting factor for the maximum energy delivery, setting the theoretical upper bound to near 2 μJ for a 1-m long, 7-μm, air-core PBF. Finally, the use of a 300 kHz repetition rate fiber laser enabled rapid ablation of 150 µm x 150 µm area within only 50 ms. Such ablation speeds can now allow the surgeons to translate the surgery device as fast as ~4 mm/s to continuously remove a thin layer of a 150 µm wide tissue. Thanks to a high optical transmission efficiency of the in-line optical architecture of the device and improved resolution, we could successfully perform ablation of scarred cheek pouch tissue, drilling through a thin slice. With further development, this device can serve as a precise and high speed ultrafast laser scalpel in the clinic. PMID:25071946

  11. AUTOSAW simulations of lumber recovery for small-diameter Douglas-fir and ponderosa pine from southwestern Oregon.

    Treesearch

    R. James Barbour; Dean L. Parry; John Punches; John Forsman; Robert Ross

    2003-01-01

    Small-diameter (5- to 10-inch diameter at breast height) Douglas-fi r (Pseudotsuga menziesii (Mirb.) Franco) and ponderosa pine (Pinus ponderosa Dougl. ex Laws) trees were assessed for product potential by diagramming the location, size, and type of knots visible on the wood surface (inside bark) and using the AUTOSAW sawing simulator to evaluate...

  12. Ecological Importance of Small-Diameter Trees to the Structure, Diversity and Biomass of a Tropical Evergreen Forest at Rabi, Gabon.

    PubMed

    Memiaghe, Hervé R; Lutz, James A; Korte, Lisa; Alonso, Alfonso; Kenfack, David

    2016-01-01

    Tropical forests have long been recognized for their biodiversity and ecosystem services. Despite their importance, tropical forests, and particularly those of central Africa, remain understudied. Until recently, most forest inventories in Central Africa have focused on trees ≥10 cm in diameter, even though several studies have shown that small-diameter tree population may be important to demographic rates and nutrient cycling. To determine the ecological importance of small-diameter trees in central African forests, we used data from a 25-ha permanent plot that we established in the rainforest of Gabon to study the diversity and dynamics of these forests. Within the plot, we censused 175,830 trees ≥1 cm dbh from 54 families, 192 genera, and 345 species. Average tree density was 7,026 trees/ha, basal area 31.64 m2/ha, and above-ground biomass 369.40 Mg/ha. Fabaceae, Ebenaceae and Euphorbiaceae were the most important families by basal area, density and above-ground biomass. Small-diameter trees (1 cm ≥ dbh <10 cm) comprised 93.7% of the total tree population, 16.5% of basal area, and 4.8% of the above-ground biomass. They also had diversity 18% higher at family level, 34% higher at genus level, and 42% higher at species level than trees ≥10 cm dbh. Although the relative contribution of small-diameter trees to biomass was comparable to other forests globally, their contribution to forest density, and diversity was disproportionately higher. The high levels of diversity within small-diameter classes may give these forests high levels of structural resilience to anthropogenic/natural disturbance and a changing climate.

  13. Ecological Importance of Small-Diameter Trees to the Structure, Diversity and Biomass of a Tropical Evergreen Forest at Rabi, Gabon

    PubMed Central

    Memiaghe, Hervé R.; Lutz, James A.; Korte, Lisa; Alonso, Alfonso; Kenfack, David

    2016-01-01

    Tropical forests have long been recognized for their biodiversity and ecosystem services. Despite their importance, tropical forests, and particularly those of central Africa, remain understudied. Until recently, most forest inventories in Central Africa have focused on trees ≥10 cm in diameter, even though several studies have shown that small-diameter tree population may be important to demographic rates and nutrient cycling. To determine the ecological importance of small-diameter trees in central African forests, we used data from a 25-ha permanent plot that we established in the rainforest of Gabon to study the diversity and dynamics of these forests. Within the plot, we censused 175,830 trees ≥1 cm dbh from 54 families, 192 genera, and 345 species. Average tree density was 7,026 trees/ha, basal area 31.64 m2/ha, and above-ground biomass 369.40 Mg/ha. Fabaceae, Ebenaceae and Euphorbiaceae were the most important families by basal area, density and above-ground biomass. Small-diameter trees (1 cm ≥ dbh <10 cm) comprised 93.7% of the total tree population, 16.5% of basal area, and 4.8% of the above-ground biomass. They also had diversity 18% higher at family level, 34% higher at genus level, and 42% higher at species level than trees ≥10 cm dbh. Although the relative contribution of small-diameter trees to biomass was comparable to other forests globally, their contribution to forest density, and diversity was disproportionately higher. The high levels of diversity within small-diameter classes may give these forests high levels of structural resilience to anthropogenic/natural disturbance and a changing climate. PMID:27186658

  14. Brushed block copolymer micelles with pH-sensitive pendant groups for controlled drug delivery.

    PubMed

    Lee, Hyun Jin; Bae, Younsoo

    2013-08-01

    To investigate the effects of small aliphatic pendent groups conjugated through an acid-sensitive linker to the core of brushed block copolymer micelles on particle properties. The brushed block copolymers were synthesized by conjugating five types of 2-alkanone (2-butanone, 2-hexanone, 2-octanone, 2-decanone, and 2-dodecanone) through an acid-labile hydrazone linker to poly(ethylene glycol)-poly(aspartate hydrazide) block copolymers. Only block copolymers with 2-hexanone and 2-octanone (PEG-HEX and PEG-OCT) formed micelles with a clinically relevant size (< 50 nm in diameter), low critical micelle concentration (CMC, < 20 μM), and drug entrapment yields (approximately 5 wt.%). Both micelles degraded in aqueous solutions in a pH-dependent manner, while the degradation was accelerated in an acidic condition (pH 5.0) in comparison to pH 7.4. Despite these similar properties, PEG-OCT micelles controlled the entrapment and pH-dependent release of a hydrophobic drug most efficiently, without altering particle size, shape, and stability. The molecular weight of PEG (12 kDa vs 5 kDa) induced no change in pH-controlled drug release rates of PEG-OCT micelles. Acid-labile small aliphatic pendant groups are useful to control the entrapment and release of a hydrophobic drug physically entrapped in the core of brushed block copolymer micelles.

  15. Turbulent convection in microchannels

    NASA Astrophysics Data System (ADS)

    Adams, Thomas Mcdaniel

    1998-10-01

    Single-phase forced convection in microchannels is an effective cooling mechanism capable of accommodating the high heat fluxes encountered in fission reactor cores, accelerator targets, microelectronic heat sinks and micro-heat exchangers. Traditional Nusselt type correlations, however, have generally been obtained using data from channels with hydraulic diameters >2 cm. Application of such relationships to microchannels is therefore questionable. A diameter limit below which traditional correlations are invalid had not been established. The objective of this investigation was to systematically address the effect of small hydraulic diameter on turbulent single-phase forced convection of water. A number of microchannels having hydraulic diameters ranging from 0.76 to 1.13 mm were constructed and tested over a wide range of flow rates and heat fluxes. Experimentally obtained Nusselt numbers were significantly higher than the values predicted by the Gnielinski correlation for large channels, the effect of decreasing diameter being to further increase heat transfer enhancement. A working correlation predicting the heat transfer enhancement for turbulent convection in microchannels was developed. The correlation predicts the lower diameter limit below which traditional correlations are no longer valid to be approximately 1.2 mm. Of further interest was the effect of the desorption of noncondensable gases dissolved in the water on turbulent convection. In large channels noncondensables undergo little desorption and their effect is negligible. The large pressure drops coupled with large temperature increases for high heat fluxes in microchannels, however, leads to a two-phase, two-component flow thereby enhancing heat transfer coefficients above their liquid- only values. A detailed mathematical model was developed to predict the resulting void fractions and liquid- coolant accelerations due to the desorption of noncondensables in microchannels. Experiments were also performed to compare heat transfer coefficients for fully-degassed water to water saturated with air at test section inlet conditions. The data showed significant heat transfer enhancement for the air-saturated case over the fully-degassed case. The degree of enhancement was greatly under-predicted by current two-phase, two- component heat transfer correlations.

  16. Improving socket design to prevent difficult removal of locking screws.

    PubMed

    Lin, Chen-Huei; Chao, Ching-Kong; Tang, Yi-Hsuan; Lin, Jinn

    2018-03-01

    Reports of driver slippage leading to difficult locking screw removals have increased since the adoption of titanium for screw fabrication; the use of titanium is known to cause cross-threading and cold welding. Such problems occur most frequently in screws with hex sockets, and may cause serious surgical complications. This study aimed to improve screw socket design to prevent slippage and difficult screw removal. Three types of small sockets (hex, Torx, and cruciate) and six types of large sockets (hex, Torx, Octatorx, Torx+ I, Torx+ II, and Torx+ III) with screw head diameters of 5.5 mm were manufactured from titanium, and corresponding screwdrivers were manufactured from stainless steel. The screw heads and drivers were mounted on a material testing machine, and torsional tests were conducted to simulate screw usage in clinical settings at two insertion depths: 1 and 2 mm. Ten specimens were tested from each design, and the maximum torque and failure patterns were recorded and compared. For small sockets in 2 mm conditions, the hex with the largest driver core had the highest torque, followed by Torx and cruciate. In these tests, the drivers were twisted off in all specimens. However, under the 1 mm condition, the hex slipped and the torque decreased markedly. Overall, torque was higher for large sockets than for small sockets. The Octatorx, with a large core and simultaneous deformation of the driver and socket lobes, had the highest torque at almost twice that of the small hex. The hex had the lowest torque, a result of slippage in both the 1 and 2 mm conditions. Torx plus designs, with more designed degrees of freedom, were able to maintain a higher driving angle and larger core for higher torque. The hex design showed slipping tendencies with a marked decrease in torque, especially under conditions with inadequate driver engagement. Large sockets allowed for substantial increases in torque. The Torx, Octatorx, and Torx plus designs displayed better performance than the hexes. Improvements to the socket design could effectively prevent slippage and solve difficult screw removal problems. Copyright © 2018. Published by Elsevier Ltd.

  17. Synthesis and atomic scale characterization of Er2O3 nanoparticles: enhancement of magnetic properties and changes in the local structure

    NASA Astrophysics Data System (ADS)

    Corrêa, Eduardo L.; Bosch-Santos, Brianna; Freitas, Rafael S.; Potiens, Maria da Penha A.; Saiki, Mitiko; Carbonari, Artur W.

    2018-05-01

    In the investigation reported in this paper a modified thermal decomposition method was developed to produce very small Er2O3 nanoparticles (NPs). Particles structure, shape and size were characterized by x-ray diffraction and transmission electron microscopy which showed that the synthesis by thermal decomposition under O2 atmosphere produced very small and monodisperse NPs, allowing the investigation of finite-size and surface effects. Results of magnetization measurements showed that the smallest particles present the highest values of susceptibility that decrease as particle size increases. Specific heat measurements indicate that the sample with the smallest NPs (diameter ∼5 nm) has a Néel temperature of 0.54 K. The local structure of particles was investigated by measurements of hyperfine interactions with perturbed angular correlation spectroscopy using 111Cd as probe nuclei replacing the cationic sites. Results showed that the relative population of sites 8b increases in both the core and surface layer of particles.

  18. Synthesis and atomic scale characterization of Er2O3 nanoparticles: enhancement of magnetic properties and changes in the local structure.

    PubMed

    Corrêa, Eduardo L; Bosch-Santos, Brianna; Freitas, Rafael S; da Penha A Potiens, Maria; Saiki, Mitiko; Carbonari, Artur W

    2018-05-18

    In the investigation reported in this paper a modified thermal decomposition method was developed to produce very small Er 2 O 3 nanoparticles (NPs). Particles structure, shape and size were characterized by x-ray diffraction and transmission electron microscopy which showed that the synthesis by thermal decomposition under O 2 atmosphere produced very small and monodisperse NPs, allowing the investigation of finite-size and surface effects. Results of magnetization measurements showed that the smallest particles present the highest values of susceptibility that decrease as particle size increases. Specific heat measurements indicate that the sample with the smallest NPs (diameter ∼5 nm) has a Néel temperature of 0.54 K. The local structure of particles was investigated by measurements of hyperfine interactions with perturbed angular correlation spectroscopy using 111 Cd as probe nuclei replacing the cationic sites. Results showed that the relative population of sites 8b increases in both the core and surface layer of particles.

  19. Testing Small CPAS Parachutes Using HIVAS

    NASA Technical Reports Server (NTRS)

    Ray, Eric S.; Hennings, Elsa; Bernatovich, Michael A.

    2013-01-01

    The High Velocity Airflow System (HIVAS) facility at the Naval Air Warfare Center (NAWC) at China Lake was successfully used as an alternative to flight test to determine parachute drag performance of two small Capsule Parachute Assembly System (CPAS) canopies. A similar parachute with known performance was also tested as a control. Realtime computations of drag coefficient were unrealistically low. This is because HIVAS produces a non-uniform flow which rapidly decays from a high central core flow. Additional calibration runs were performed to characterize this flow assuming radial symmetry from the centerline. The flow field was used to post-process effective flow velocities at each throttle setting and parachute diameter using the definition of the momentum flux factor. Because one parachute had significant oscillations, additional calculations were required to estimate the projected flow at off-axis angles. The resulting drag data from HIVAS compared favorably to previously estimated parachute performance based on scaled data from analogous CPAS parachutes. The data will improve drag area distributions in the next version of the CPAS Model Memo.

  20. Misfit-guided self-organization of anti-correlated Ge quantum dot arrays on Si nanowires

    PubMed Central

    Kwon, Soonshin; Chen, Zack C.Y.; Kim, Ji-Hun; Xiang, Jie

    2012-01-01

    Misfit-strain guided growth of periodic quantum dot (QD) arrays in planar thin film epitaxy has been a popular nanostructure fabrication method. Engineering misfit-guided QD growth on a nanoscale substrate such as the small curvature surface of a nanowire represents a new approach to self-organized nanostructure preparation. Perhaps more profoundly, the periodic stress underlying each QD and the resulting modulation of electro-optical properties inside the nanowire backbone promise to provide a new platform for novel mechano-electronic, thermoelectronic, and optoelectronic devices. Herein, we report a first experimental demonstration of self-organized and self-limited growth of coherent, periodic Ge QDs on a one dimensional Si nanowire substrate. Systematic characterizations reveal several distinctively different modes of Ge QD ordering on the Si nanowire substrate depending on the core diameter. In particular, Ge QD arrays on Si nanowires of around 20 nm diameter predominantly exhibit an anti-correlated pattern whose wavelength agrees with theoretical predictions. The correlated pattern can be attributed to propagation and correlation of misfit strain across the diameter of the thin nanowire substrate. The QD array growth is self-limited as the wavelength of the QDs remains unchanged even after prolonged Ge deposition. Furthermore, we demonstrate a direct kinetic transformation from a uniform Ge shell layer to discrete QD arrays by a post-growth annealing process. PMID:22889063

  1. Intense mesoscale variability in the Sardinia Sea

    NASA Astrophysics Data System (ADS)

    Russo, Aniello; Borrione, Ines; Falchetti, Silvia; Knoll, Michaela; Fiekas, Heinz-Volker; Heywood, Karen; Oddo, Paolo; Onken, Reiner

    2015-04-01

    From the 6 to 25 June 2014, the REP14-MED sea trial was conducted by CMRE, supported by 20 partners from six different nations. The at-sea activities were carried out onboard the research vessels Alliance (NATO) and Planet (German Ministry of Defense), comprising a marine area of about 110 x 110 km2 to the west of the Sardinian coast. More than 300 CTD casts typically spaced at 10 km were collected; both ships continuously recorded vertical profiles of currents by means of their ADCPs, and a ScanFish® and a CTD chain were towed for almost three days by Alliance and Planet, respectively, following parallel routes. Twelve gliders from different manufacturers (Slocum, SeaGliderTM and SeaExplorer) were continuously sampling the study area following zonal tracks spaced at 10 km. In addition, six moorings, 17 surface drifters and one ARVOR float were deployed. From a first analysis of the observations, several mesoscale features were identified in the survey area, in particular: (i) a warm-core anticyclonic eddy in the southern part of the domain, about 50 km in diameter and with the strongest signal at about 50-m depth (ii) another warm-core anticyclonic eddy of comparable dimensions in the central part of the domain, but extending to greater depth than the former one, and (iii) a small (less than 15 km in diameter) cold-core cyclonic eddy of Winter Intermediate Water in the depth range between 170 m and 370 m. All three eddies showed intensified currents, up to 50 cm s-1. The huge high-resolution observational data set and the variety of observation techniques enabled the mesoscale features and their variability to be tracked for almost three weeks. In order to obtain a deeper understanding of the mesoscale dynamic behaviour and their interactions, assimilation studies with an ocean circulation model are underway.

  2. Recent advancements in transparent ceramics and crystal fibers for high power lasers

    NASA Astrophysics Data System (ADS)

    Kim, W.; Baker, C.; Villalobos, G.; Florea, C.; Gibson, D.; Shaw, L. B.; Bowman, S.; Bayya, S.; Sadowski, B.; Hunt, M.; Askins, C.; Peele, J.; Aggarwal, I. D.; Sanghera, J. S.

    2013-05-01

    In this paper, we present our recent progress in the development of rare-earth (Yb3+ or Ho3+) doped Lu2O3 and Y2O3 sesquioxides for high power solid state lasers. We have fabricated high quality transparent ceramics using nano-powders synthesized by a co-precipitation method. This was accomplished by developments in high purity powder synthesis and low temperature scalable sintering technology developed at NRL. The optical, spectral and morphological properties as well as the lasing performance from our highly transparent ceramics are presented. In the second part of the paper, we discuss our recent research effort in developing cladded-single crystal fibers for high power single frequency fiber lasers has the potential to significantly exceed the capabilities of existing silica fiber based lasers. Single crystal fiber cores with diameters as small as 35μm have been drawn using high purity rare earth doped ceramic or single crystal feed rods by the Laser Heated Pedestal Growth (LHPG) process. Our recent results on the development of suitable claddings on the crystal fiber core are discussed.

  3. Decoding structural complexity in conical carbon nanofibers.

    PubMed

    Zhu, Yi-An; Wang, Zi-Jun; Cheng, Hong-Ye; Yang, Qin-Min; Sui, Zhi-Jun; Zhou, Xing-Gui; Chen, De

    2017-06-07

    Conical carbon nanofibers (CNFs) exist primarily as graphitic ribbons that fold into a cylindrical structure with the formation of a hollow core. Structural analysis aided by molecular modeling proves useful for obtaining a full picture of how the size of the central channel varies from fiber to fiber. From a geometrical perspective, conical CNFs possibly have cone tips that are nearly closed. On the other hand, their fiber wall thickness can be reduced to a minimum possible value that is determined solely by the apex angle, regardless of the outer diameter. A formula has been developed to express the number of carbon atoms present in conical CNFs in terms of measurable structural parameters. It appears that the energetically preferred fiber wall thickness increases not only with the apex angle, but also with the number of atoms in the constituent graphitic cones. The origin of the empirical observation that conical CNFs with small apex angles tend to have a large hollow core lies in the fact that in graphene sheets that are more highly curved the curvature-induced strain energy rises more rapidly as the fiber wall thickens.

  4. Laboratory Mid-frequency (Kilohertz) Range Seismic Property Measurements and X-ray CT Imaging of Fractured Sandstone Cores During Supercritical CO2 Injection

    NASA Astrophysics Data System (ADS)

    Nakagawa, S.; Kneafsey, T. J.; Chang, C.; Harper, E.

    2014-12-01

    During geological sequestration of CO2, fractures are expected to play a critical role in controlling the migration of the injected fluid in reservoir rock. To detect the invasion of supercritical (sc-) CO2 and to determine its saturation, velocity and attenuation of seismic waves can be monitored. When both fractures and matrix porosity connected to the fractures are present, wave-induced dynamic poroelastic interactions between these two different types of rock porosity—high-permeability, high-compliance fractures and low-permeability, low-compliance matrix porosity—result in complex velocity and attenuation changes of compressional waves as scCO2 invades the rock. We conducted core-scale laboratory scCO2 injection experiments on small (diameter 1.5 inches, length 3.5-4 inches), medium-porosity/permeability (porosity 15%, matrix permeability 35 md) sandstone cores. During the injection, the compressional and shear (torsion) wave velocities and attenuations of the entire core were determined using our Split Hopkinson Resonant Bar (short-core resonant bar) technique in the frequency range of 1-2 kHz, and the distribution and saturation of the scCO2 determined via X-ray CT imaging using a medical CT scanner. A series of tests were conducted on (1) intact rock cores, (2) a core containing a mated, core-parallel fracture, (3) a core containing a sheared core-parallel fracture, and (4) a core containing a sheared, core-normal fracture. For intact cores and a core containing a mated sheared fracture, injections of scCO2 into an initially water-saturated sample resulted in large and continuous decreases in the compressional velocity as well as temporary increases in the attenuation. For a sheared core-parallel fracture, large attenuation was also observed, but almost no changes in the velocity occurred. In contrast, a sample containing a core-normal fracture exhibited complex behavior of compressional wave attenuation: the attenuation peaked as the leading edge of the scCO2 approached the fracture; followed by an immediate drop as scCO2 invaded the fracture; and by another, gradual increase as the scCO2 infiltrated into the other side of the fracture. The compressional wave velocity declined monotonically, but the rate of velocity decrease changed with the changes in attenuation.

  5. In situ-measurement of ice deformation from repeated borehole logging of the EPICA Dronning Maud Land (EDML) ice core, East Antarctica.

    NASA Astrophysics Data System (ADS)

    Jansen, Daniela; Weikusat, Ilka; Kleiner, Thomas; Wilhelms, Frank; Dahl-Jensen, Dorthe; Frenzel, Andreas; Binder, Tobias; Eichler, Jan; Faria, Sergio H.; Sheldon, Simon; Panton, Christian; Kipfstuhl, Sepp; Miller, Heinrich

    2017-04-01

    The European Project for Ice Coring in Antarctica (EPICA) ice core was drilled between 2001 and 2006 at the Kohnen Station, Antarctica. During the drilling process the borehole was logged repeatedly. Repeated logging of the borehole shape is a means of directly measuring the deformation of the ice sheet not only on the surface but also with depth, and to derive shear strain rates for the lower part, which control the volume of ice transported from the inner continent towards the ocean. The logging system continuously recorded the tilt of the borehole with respect to the vertical (inclination) as well as the heading of the borehole with respect to magnetic north (azimuth) by means of a compass. This dataset provides the basis for a 3-D reconstruction of the borehole shape, which is changing over time according to the predominant deformation modes with depth. The information gained from this analysis can then be evaluated in combination with lattice preferred orientation, grain size and grain shape derived by microstructural analysis of samples from the deep ice core. Additionally, the diameter of the borehole, which was originally circular with a diameter of 10 cm, was measured. As the ice flow velocity at the position of the EDML core is relatively slow (about 0.75 m/a), the changes of borehole shape between the logs during the drilling period were very small and thus difficult to interpret. Thus, the site has been revisited in the Antarctic summer season 2016 and logged again using the same measurement system. The change of the borehole inclination during the time period of 10 years clearly reveals the transition from a pure shear dominated deformation in the upper part of the ice sheet to shear deformation at the base. We will present a detailed analysis of the borehole parameters and the deduced shear strain rates in the lower part of the ice sheet. The results are discussed with respect to ice microstructural data derived from the EDML ice core. Microstructural data directly reflect the deformation conditions, as the ice polycrystal performs the deformation which leads e.g. to characteristic lattice orientation distributions and grain size and shape appearance. Though overprinted by recrystallization (due to the hot environment for the ice) and the slow deformation, analysis of statistically significant grain numbers reveals indications typical for the changing deformation regimes with depth. Additionally we compare our results with strain rates derived from a simulation with a model for large scale ice deformation, the Parallel Ice Sheet Model (PISM).

  6. Accretion rate of extraterrestrial matter: Iridium deposited over the last 70 million years

    NASA Technical Reports Server (NTRS)

    Kyte, Frank T.

    1988-01-01

    In order to quantify the accretion rate of extraterrestrial matter during the Cenozoic, Ir concentrations were measured in a continuous series of 450 samples across most of the length of piston core LL44-GPC3. LL44-GPC3 is a 25-meter-long, large-diameter piston core of abyssal clay from the central North Pacific. This core contains a nearly continuous record of sedimentation over the last 70 Ma, as this site migrated from a region near the Equator in the late Cretaceous to its present position north of Hawaii. The first-cut survey across the core is nearing completion, and all of the conclusions of the earlier study, in which was reported the concentrations of Ir, Co, and Sb across 9 meters of this core, remain unchanged. The only strongly enhanced Ir concentrations occur at the Cretaceous-Tertiary (K-T) boundary and outside the K-T boundary Ir correlates well with Co, a terrestrial element which is largely present in hydrogenous ferromanganese oxide precipitates from seawater. Concentrations of both elements appear to be inversely correlated with the sedimentation rate. Although the K-T Ir anomaly is unique in magnitude in this core, there are several small bumps in the Ir profile which may reflect smaller accretionary events. The most promising Ir enhancement was observed in a 30 cm section approximately 1 m below the K-T boundary. Preliminary data suggest deposition of an excess across this interval at a time estimate to be approximate 1 Ma before the K-T impact event, but there is insufficient evidence at present to prove that this reflects enhanced accretion of extraterrestrial matter. A detailed model is being prepared of the chemical record of sedimentation in this core using a combined database of 39 elements in approximately 450 samples across the Cenozoic. Preliminary working model indicates that the only sedimentary sources which contribute significantly to the Ir budget in this core are the hydrogenous precipitates and extraterrestrial particulates.

  7. Distant Secondary Craters and Age Constraints on Young Martian Terrains

    NASA Technical Reports Server (NTRS)

    McEwen, A.; Preblich, B.; Turtle, E.; Studer, D.; Artemieva, N.; Golombek, M.; Hurst, M.; Kirk, R.; Burr, D.

    2005-01-01

    Are small (less than approx. 1 km diameter) craters on Mars and the Moon dominated by primary impacts, by secondary impacts of much larger primary craters, or are both primaries and secondaries significant? This question is critical to age constraints for young terrains and for older terrains covering small areas, where only small craters are superimposed on the unit. If the martian rayed crater Zunil is representative of large impact events on Mars, then the density of secondaries should exceed the density of primaries at diameters a factor of 1000 smaller than that of the largest contributing primary crater. On the basis of morphology and depth/diameter measurements, most small craters on Mars could be secondaries. Two additional observations (discussed below) suggest that the production functions of Hartmann and Neukum predict too many primary craters smaller than a few hundred meters in diameter. Fewer small, high-velocity impacts may explain why there appears to be little impact regolith over Amazonian terrains. Martian terrains dated by small craters could be older than reported in recent publications.

  8. Thulium fiber laser lithotripsy using a muzzle brake fiber tip

    NASA Astrophysics Data System (ADS)

    Hutchens, Thomas C.; Gonzalez, David A.; Irby, Pierce B.; Fried, Nathaniel M.

    2017-02-01

    The Thulium fiber laser (TFL) is being explored as an alternative to Holmium:YAG laser for lithotripsy. TFL beam profile allows coupling of higher power into smaller fibers than multimode Holmium laser beam, without proximal fiber tip degradation. A smaller fiber provides more space in ureteroscope working channel for increased saline irrigation and allows maximum ureteroscope flexion. However, distal fiber tip burnback increases as fiber diameter decreases. Previous studies utilizing hollow steel sheaths around recessed distal fiber tips reduced fiber burnback, but increased retropulsion. In this study, a "fiber muzzle brake" was tested for reducing fiber burnback and stone retropulsion. TFL lithotripsy studies were performed at 1908 nm, 35 mJ, 500 μs, and 300 Hz using a 100-μm-core fiber. The optimal stainless steel muzzle brake tip tested consisted of a 1-cm-long, 560-μm-OD, 360-μm-ID tube with 275-μm thru hole located 250-μm from the distal end. The fiber tip was recessed a distance of 500 μm. Stone phantom retropulsion, fiber tip burnback, and calcium oxalate stone ablation studies were performed, ex vivo. Small stones with a mass of 40 +/- 4 mg and 4-mm-diameter were ablated over a 1.5-mm sieve in 25 +/- 4 s (n=10), without distal fiber tip burnback. Reduction in stone phantom retropulsion distance by 50% and 85% was observed when using muzzle brake tips versus 100-μm-core bare fibers and hollow steel tip fibers. The muzzle brake fiber tip provided efficient stone ablation, reduced stone retropulsion, and minimal fiber degradation during TFL lithotripsy.

  9. Magnetic properties of ferritin and akaganeite nanoparticles in aqueous suspension

    NASA Astrophysics Data System (ADS)

    Koralewski, Marceli; Pochylski, Mikołaj; Gierszewski, Jacek

    2013-09-01

    We have studied the magnetically induced optical birefringence Δ n of horse spleen ferritin (HSF) and aqueous suspensions of several different-sized iron oxyhydroxide nanoparticles coated with different polysaccharides mimicking ferritin. The structure and dimensions of the akaganeite mineral core were characterized by XRD and TEM, respectively. The stability of the suspensions in the measurement temperature range from 278 to 358 K was confirmed by UV-Vis absorption spectroscopy. The values of optical polarizability anisotropy Δ α, magnetic susceptibility anisotropy Δ χ, and permanent magnetic dipole moment μ m of the akaganeite nanoparticles have been estimated on the basis of the temperature dependence of the Cotton-Mouton (C-M) constant. The magnetic birefringence of Fe-sucrose has been described tentatively by different types of Langevin function allowing another estimation of Δ χ and μ m. The obtained permanent magnetic dipole moment μ m of the studied akaganeite nanoparticles proves small and comparable to that of HSF. The value of μ m is found to increase with decreasing nanoparticle diameter. Observed in a range spanning more than five orders of magnitude, the linear relation between the C-M constant and the iron concentration provides a basis for possible analytical application of the C-M effect in biomedicine. The established relation between the C-M constant and the nanoparticle diameter confirms that the dominant contribution to the measured magnetic birefringence comes from the magnetic susceptibility anisotropy Δ χ. A comparison of the C-M constants of the studied akaganeite nanoparticles with the data obtained for HSF provides evidence that the ferritin core behaves as a non-Euclidian solid.

  10. Entropic depletion in colloidal suspensions and polymer liquids: Role of nanoparticle surface topography

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Banerjee, Debapriya; Yang, Jian; Schweizer, Kenneth S.

    2015-01-01

    Here, we employ a hybrid Monte Carlo plus integral equation theory approach to study how dense fluids of small nanoparticles or polymer chains mediate entropic depletion interactions between topographically rough particles where all interaction potentials are hard core repulsion. The corrugated particle surfaces are composed of densely packed beads which present variable degrees of controlled topographic roughness and free volume associated with their geometric crevices. This pure entropy problem is characterized by competing ideal translational and (favorable and unfavorable) excess entropic contributions. Surface roughness generically reduces particle depletion aggregation relative to the smooth hard sphere case. However, the competition betweenmore » ideal and excess packing entropy effects in the bulk, near the particle surface and in the crevices, results in a non-monotonic variation of the particle-monomer packing correlation function as a function of the two dimensionless length scale ratios that quantify the effective surface roughness. As a result, the inter-particle potential of mean force (PMF), second virial coefficient, and spinodal miscibility volume fraction vary non-monotonically with the surface bead to monomer diameter and particle core to surface bead diameter ratios. A miscibility window is predicted corresponding to an optimum degree of surface roughness that completely destroys depletion attraction resulting in a repulsive PMF. Variation of the (dense) matrix packing fraction can enhance or suppress particle miscibility depending upon the amount of surface roughness. Connecting the monomers into polymer chains destabilizes the system via enhanced contact depletion attraction, but the non-monotonic variations with surface roughness metrics persist.« less

  11. Large core plastic planar optical splitter fabricated by 3D printing technology

    NASA Astrophysics Data System (ADS)

    Prajzler, Václav; Kulha, Pavel; Knietel, Marian; Enser, Herbert

    2017-10-01

    We report on the design, fabrication and optical properties of large core multimode optical polymer splitter fabricated using fill up core polymer in substrate that was made by 3D printing technology. The splitter was designed by the beam propagation method intended for assembling large core waveguide fibers with 735 μm diameter. Waveguide core layers were made of optically clear liquid adhesive, and Veroclear polymer was used as substrate and cover layers. Measurement of optical losses proved that the insertion optical loss was lower than 6.8 dB in the visible spectrum.

  12. Synthesis characterisation series of newly fabricated type II CdSe CdSe/CdTe nanocrystals and their optical properties

    NASA Astrophysics Data System (ADS)

    Ahmed, A. S.; Christopher, W.

    2018-03-01

    Nanocrystalline semiconductors exhibit different properties due to two basic factors. They possess high surface to volume ratio and the actual size of particle can determine the electronic and physical properties of the material. The small size results in an observable quantum confinement effect, defined by the increasing bandgap accompanied by the quantization of the energy levels to discrete values. In present work we have synthesized the series of cadmium selenide/cadmium telluride (CdSe/CdTe) core/shell and CdSe/CdTe/CdS core/shell/shell to investigate the biexciton energy through transient absorption measurements. These structures are type II nanocrystals are with a hole in the shell and the electron confined to the core. We specifically investigate the effect of nanoparticle shape on the electronic structure and ultrafast electronic dynamics in the band-edge exciton states of CdSe quantum dots, nanorods, and nanoplatelets. Particle size was chosen to enable straightforward comparisons of the effects of particle shape on the spectra and dynamics without retuning the laser source. In our results the Uv-vis showed only a mild redshift in the first excitonic an elongated tail with increasing shell thickness. High resolution Transmission Electron Microscopy (HRTEM) shows the slight agglomeration of the nanocrystals but still the size distribution was calculate able. Spherical small crystals ranging from 5.9 nm to 10 nm are observed. CdTe/CdSe structures were quasi spherical with a rough diameter 6 nm with some little agglomerated structure. . The spherical nanocrystals could be peanut shaped oriented along the c axis or the spherical only, which could explain the two peak emission. p-XRD results indicate the predominant wurtzite structure throughout.

  13. Small-Angle Neutron Scattering Studies of Magnetic Correlation Lengths in Nanoparticle Assemblies

    NASA Astrophysics Data System (ADS)

    Majetich, Sara

    2009-03-01

    Small-angle neutron scattering (SANS) measurements of ordered arrays of surfactant-coated magnetic nanoparticle reveal characteristic length scales associated with interparticle and intraparticle magnetic ordering. The high degree of uniformity in the monodisperse nanoparticle size and spacing leads to a pronounced diffraction peak and allows for a straightforward determination of these length scales [1]. There are notable differences in these length scales depending on the particle moment, which depends on the material (Fe, Co, Fe3O4) and diameter, and also on whether the metal particle core is surrounded by an oxide shell. For 8.5 nm particles containing an Fe core and thick Fe3O4 shell, evidence of a spin flop phase is seen in the magnetite shell when a field is applied , but not when the shell thickness is ˜0.5 nm [2]. 8.0 nm particles with an e-Co core and 0.75 nm CoO shell show no exchange bias effects while similar particles with a 2 nm thick shell so significant training effects below 90 K. Polarized SANS studied of 7 nm Fe3O4 nanoparticle assemblies show the ability to resolve the magnetization components in 3D. [4pt] [1] M. Sachan, C. Bonnoit, S. A. Majetich, Y. Ijiri, P. O. Mensah-Bonsu, J. A. Borchers, and J. J. Rhyne, Appl. Phys. Lett. 92, 152503 (2008). [0pt] [2] Yumi Ijiri, Christopher V. Kelly, Julie A. Borchers, James J. Rhyne, Dorothy F. Farrell, Sara A. Majetich, Appl. Phys. Lett. 86, 243102-243104 (2005). [0pt] [3] K. L. Krycka, R. Booth, J. A. Borchers, W. C. Chen, C. Conlon, T. Gentile, C. Hogg, Y. Ijiri, M. Laver, B. B. Maranville, S. A. Majetich, J. Rhyne, and S. M. Watson, Physica B (submitted).

  14. Affordable Development and Demonstration of a Small NTR Engine and Stage: How Small is Big Enough?

    NASA Technical Reports Server (NTRS)

    Borowski, Stanley K.; Sefcik, Robert J.; Fittje, James E.; McCurdy, David R.; Qualls, Arthur L.; Schnitzler, Bruce G.; Werner, James E.; Weitzberg (Abraham); Joyner, Claude R.

    2015-01-01

    The Nuclear Thermal Rocket (NTR) derives its energy from fission of uranium-235 atoms contained within fuel elements that comprise the engine's reactor core. It generates high thrust and has a specific impulse potential of approximately 900 seconds - a 100% increase over today's best chemical rockets. The Nuclear Thermal Propulsion (NTP) project, funded by NASA's AES program, includes five key task activities: (1) Recapture, demonstration, and validation of heritage graphite composite (GC) fuel (selected as the "Lead Fuel" option); (2) Engine Conceptual Design; (3) Operating Requirements Definition; (4) Identification of Affordable Options for Ground Testing; and (5) Formulation of an Affordable Development Strategy. During FY'14, a preliminary DDT&E plan and schedule for NTP development was outlined by GRC, DOE and industry that involved significant system-level demonstration projects that included GTD tests at the NNSS, followed by a FTD mission. To reduce cost for the GTD tests and FTD mission, small NTR engines, in either the 7.5 or 16.5 klbf thrust class, were considered. Both engine options used GC fuel and a "common" fuel element (FE) design. The small approximately 7.5 klbf "criticality-limited" engine produces approximately 157 megawatts of thermal power (MWt) and its core is configured with parallel rows of hexagonal-shaped FEs and tie tubes (TTs) with a FE to TT ratio of approximately 1:1. The larger approximately 16.5 klbf Small Nuclear Rocket Engine (SNRE), developed by LANL at the end of the Rover program, produces approximately 367 MWt and has a FE to TT ratio of approximately 2:1. Although both engines use a common 35 inch (approximately 89 cm) long FE, the SNRE's larger diameter core contains approximately 300 more FEs needed to produce an additional 210 MWt of power. To reduce the cost of the FTD mission, a simple "1-burn" lunar flyby mission was considered to reduce the LH2 propellant loading, the stage size and complexity. Use of existing and flight proven liquid rocket and stage hardware (e.g., from the RL10B-2 engine and Delta Cryogenic Second Stage) was also maximized to further aid affordability. This paper examines the pros and cons of using these two small engine options, including their potential to support future human exploration missions to the Moon, near Earth asteroids, and Mars, and recommends a preferred size. It also provides a preliminary assessment of the key activities, development options, and schedule required to affordably build, ground test and fly a small NTR engine and stage within a 10-year timeframe.

  15. Hydrologic response of desert wetlands to Holocene climate change: preliminary results from the Soda Springs area, Mojave National Preserve, California

    USGS Publications Warehouse

    Pigati, Jeffrey S.; Reheis, Marith C.; McGeehin, John P.; Honke, Jeffrey S.; Bright, J.

    2016-01-01

    Desert wetlands are common features in arid environments and include a variety of hydrologic facies, including seeps, springs, marshes, wet meadows, ponds, and spring pools. Wet ground conditions and dense stands of vegetation in these settings combine to trap eolian, alluvial, and fluvial sediments that accumulate over time. The resulting deposits are collectively called ground-water discharge (GWD) deposits, and contain information on how small desert watersheds responded to climate change in the past. Most GWD studies in the southwestern U.S. have focused on the late Pleistocene because the Holocene was too dry to support the extensive wetland systems that were so pervasive just a few millennia earlier. Here we describe the results of a pilot project that involves coring extant wetlands and analyzing the sedimentology and microfauna of the recovered sediment to infer Holocene hydrologic conditions. In 2011, a series of cores were taken near wetlands situated along the western margin of the Soda Lake basin in the Mojave National Preserve of southern California. The core sediments appear to show that the wetlands responded to the relatively minor climate fluctuations that characterized the Holocene. However, our analysis was limited by relatively low sediment recovery (which only averaged 70-80%) and a general paucity of datable materials in the cores. Additional studies aimed at improving recovery and developing new techniques for concentrating plant microfossils (plant remains that are <150 m in diameter) for radiocarbon dating are ongoing.

  16. Iron oxide nanoparticles stabilized with dendritic polyglycerols as selective MRI contrast agents

    NASA Astrophysics Data System (ADS)

    Nordmeyer, Daniel; Stumpf, Patrick; Gröger, Dominic; Hofmann, Andreas; Enders, Sven; Riese, Sebastian B.; Dernedde, Jens; Taupitz, Matthias; Rauch, Ursula; Haag, Rainer; Rühl, Eckart; Graf, Christina

    2014-07-01

    Monodisperse small iron oxide nanoparticles functionalized with dendritic polyglycerol (dPG) or dendritic polyglycerol sulfate (dPGS) are prepared. They are highly stable in aqueous solutions as well as physiological media. In particular, oleic acid capped iron oxide particles (core diameter = 11 +/- 1 nm) were modified by a ligand exchange process in a one pot synthesis with dPG and dPGS bearing phosphonate as anchor groups. Dynamic light scattering measurements performed in water and different biological media demonstrate that the hydrodynamic diameter of the particles is only slightly increased by the ligand exchange process resulting in a final diameter of less than 30 nm and that the particles are stable in these media. It is also revealed by magnetic resonance studies that their magnetic relaxivity is reduced by the surface modification but it is still sufficient for high contrast magnetic resonance imaging (MRI). Additionally, incubation of dPGS functionalized iron oxide nanoparticles with human umbilical vein endothelial cells showed a 50% survival at 85 nM (concentration of nanoparticles). Surface plasmon resonance (SPR) studies demonstrate that the dPGS functionalized iron oxide nanoparticles inhibit L-selectin ligand binding whereas the particles containing only dPG do not show this effect. Experiments in a flow chamber with human myelogenous leukemia cells confirmed L-selectin inhibition of the dPGS functionalized iron oxide nanoparticles and with that the L-selectin mediated leukocyte adhesion. These results indicate that dPGS functionalized iron oxide nanoparticles are a promising contrast agent for inflamed tissue probed by MRI.Monodisperse small iron oxide nanoparticles functionalized with dendritic polyglycerol (dPG) or dendritic polyglycerol sulfate (dPGS) are prepared. They are highly stable in aqueous solutions as well as physiological media. In particular, oleic acid capped iron oxide particles (core diameter = 11 +/- 1 nm) were modified by a ligand exchange process in a one pot synthesis with dPG and dPGS bearing phosphonate as anchor groups. Dynamic light scattering measurements performed in water and different biological media demonstrate that the hydrodynamic diameter of the particles is only slightly increased by the ligand exchange process resulting in a final diameter of less than 30 nm and that the particles are stable in these media. It is also revealed by magnetic resonance studies that their magnetic relaxivity is reduced by the surface modification but it is still sufficient for high contrast magnetic resonance imaging (MRI). Additionally, incubation of dPGS functionalized iron oxide nanoparticles with human umbilical vein endothelial cells showed a 50% survival at 85 nM (concentration of nanoparticles). Surface plasmon resonance (SPR) studies demonstrate that the dPGS functionalized iron oxide nanoparticles inhibit L-selectin ligand binding whereas the particles containing only dPG do not show this effect. Experiments in a flow chamber with human myelogenous leukemia cells confirmed L-selectin inhibition of the dPGS functionalized iron oxide nanoparticles and with that the L-selectin mediated leukocyte adhesion. These results indicate that dPGS functionalized iron oxide nanoparticles are a promising contrast agent for inflamed tissue probed by MRI. Electronic supplementary information (ESI) available: A detailed description of the synthesis of the ligands as well as the preparation and functionalization of the iron oxide nanoparticles including their physico-chemical characterization are presented. Further, details of the cell experiments and the SPR experiments are given. Two representative movies are provided showing leukocyte rolling on the ligand coated surface of the flow chamber. See DOI: 10.1039/c3nr04793h

  17. Effects of lipid emulsion particle size on satiety and energy intake: a randomised cross-over trial.

    PubMed

    Poppitt, Sally D; Budgett, Stephanie C; MacGibbon, Alastair K; Quek, Siew-Young; Kindleysides, Sophie; Wiessing, Katy R

    2018-03-01

    Emulsified lipids, with central lipid core surrounded by polar lipid 'protective coat', have been proposed to stimulate the ileal brake, alter appetite, food intake and aid weight control. In addition to lipid composition, emulsion particle size may contribute to efficacy with small droplets providing a larger surface area for gastrointestinal (GI) lipase action and larger droplets prolonging and delaying digestion in the GI tract. Tube feeding studies delivering emulsions directly into the small intestine show clear effects of smaller particle size on appetite and food intake, but evidence from oral feeding studies is sparse. The objective of this study was to determine the effects of lipid emulsion particle size on appetite response and food intake. In a three-arm randomised cross-over, high-phospholipid (PL) dairy lipid emulsions or matched control were consumed at breakfast within a yoghurt smoothie: (i) large-particle size emulsion, LPE (diameter 0.759 µm, 10 g lipid emulsion, 190 g yoghurt), (ii) small-particle size emulsion, SPE (diameter 0.290 µm, 10 g lipid emulsion, 190 g yoghurt), (iii) control non-emulsion, NE (10 g non-emulsion lipid, 190 g yoghurt). Twenty male participants completed the study, where postprandial appetite response was rated using visual analogue scales (VAS) and ad libitum energy intake at a lunch meal measured 3 h later. There was a trend for LPE to suppress hunger (P = 0.08) and enhance fullness (P = 0.24) relative to both SPE and NE but not statistically significant, and no significant effect of either emulsion on food intake at the lunch meal (P > 0.05). Altering particle size of a high-PL emulsion did not enhance satiety or alter eating behaviour in a group of lean men.

  18. Pilot study of radiofrequency ablation therapy without surgical excision for T1 breast cancer: evaluation with MRI and vacuum-assisted core needle biopsy and safety management.

    PubMed

    Yamamoto, Naohito; Fujimoto, Hiroshi; Nakamura, Rikiya; Arai, Manabu; Yoshii, Atsushi; Kaji, Sachiko; Itami, Makiko

    2011-01-01

    There is increasing demand for minimally invasive treatments for small breast cancer mainly because of the desire for better cosmetic results. Although radiofrequency ablation (RFA) is an attractive approach as a local control method for small breast cancer, the problems of histological effectiveness and safety management remain. A total of 29 patients including one patient with bilateral breast cancer were enrolled in this study. The mean tumor size of 30 breasts was 12.8 mm (range 5-19 mm). Under general anesthesia, RFA was performed with a Cool-tip RF system (Valleylab, Boulder, CO, USA) after sentinel lymph node biopsy. Postoperative evaluation with magnetic resonance imaging (MRI) and vacuum-assisted core needle biopsy was done 3-4 weeks after RFA before radiotherapy. Ablated tumors were evaluated with hematoxylin-eosin (H&E) and nicotinamide adenine dinucleotide (NADH)-diaphorase staining. If needed, adjuvant chemo and/or endocrine therapy was performed. All patients except one completed one session of RFA. The mean temperature near the center of the tumors was 89.6°C (range 78-100°C). Postoperative MRI showed the ablated zone clearly in all patients. MRI revealed no hypervascularity of the tumors in the ablated zone. Evaluation with H&E staining of the tumors showed remarkable degenerative changes in only three patients. NADH-diaphorase staining showed no viable tumor tissue in 24 patients out of 26 examined. Three patients received small diameter grade 3 skin burns, two on the outside of the thigh from the grounding pad and one on the breast skin. One patient had a breast lesion like a chronic granulomatous mastitis resulting from overreaction of the ablated zone. RFA therapy appeared relevant and applicable for patients with small breast cancer. Because small skin burns were observed as adverse events, close attention should be paid in the course of the RFA procedure.

  19. Formation of hexagonal boron nitride nanoscrolls induced by inclusion and exclusion of self-assembling molecules in solution process

    NASA Astrophysics Data System (ADS)

    Hwang, Da Young; Suh, Dong Hack

    2014-05-01

    Unlike nanoscrolls of 2D graphene, those of 2D h-BN have not been demonstrated, except for only a few experimental reports. Nanoscrolls of h-BN with high yields and reproducibility are first synthesized by a simple solution process. Inner-tube diameters of BNSs including LCAs, N-(2-aminoethyl)-3α-hydroxy-5β-cholan-24-amide, a bile acid derivative and self-assembling material, can be controlled by adjusting the diameter of the LCA fiber which is grown by self-assembly. TEM and SEM images show that BNSs have a tube-like morphology and the inner-tube diameter of BNSs can be controlled in the range from 20 to 60 nm for a smaller diameter, up to 300 nm for a larger diameter by LCA fiber growth inside the BNSs. Finally, open cylindrical BNSs with hollow cores were obtained by dissolving LCAs inside BNSs.Unlike nanoscrolls of 2D graphene, those of 2D h-BN have not been demonstrated, except for only a few experimental reports. Nanoscrolls of h-BN with high yields and reproducibility are first synthesized by a simple solution process. Inner-tube diameters of BNSs including LCAs, N-(2-aminoethyl)-3α-hydroxy-5β-cholan-24-amide, a bile acid derivative and self-assembling material, can be controlled by adjusting the diameter of the LCA fiber which is grown by self-assembly. TEM and SEM images show that BNSs have a tube-like morphology and the inner-tube diameter of BNSs can be controlled in the range from 20 to 60 nm for a smaller diameter, up to 300 nm for a larger diameter by LCA fiber growth inside the BNSs. Finally, open cylindrical BNSs with hollow cores were obtained by dissolving LCAs inside BNSs. Electronic supplementary information (ESI) available. See DOI: 10.1039/c4nr00897a

  20. Stimulated Raman scattering in AsSe2-As2S5 microstructured optical fiber

    NASA Astrophysics Data System (ADS)

    Gao, Weiqing; Ni, Chenquan; Xu, Qiang; Li, Xue; Chen, Xiangcai; Chen, Li; Wen, Zhenqiang; Cheng, Tonglei; Xue, Xiaojie; Suzuki, Takenobu; Ohishi, Yasutake

    2017-02-01

    We demonstrate the effects of stimulated Raman scattering (SRS) in the all-solid-core chalcogenide microstructured optical fibers (MOFs) with AsSe2 core and As2S5 cladding, which are fabricated by the rod-in-tube drawing technique. The core diameters of the MOFs are 6.3 (Fiber I), 3.0 (Fiber II), 2.6 (Fiber III) and 2.2 (Fiber IV) μm, respectively. The chromatic dispersion of the fundamental mode in Fibers I-IV is simulated by the full-vectorial mode solver technique. The first-order Stokes wave is investigated in the fibers with different core diameters pumped by the picosecond pulses at 1958 nm. In Fiber I, no obvious Raman peak is observed with the pump power increasing, because the effective nonlinearity is not high. In Fiber II, a Raman Stokes peak at 2065 nm begins to emerge at the pump power of 110 mW. The conversion efficiency is as weak as -36.6 dB at 150 mW pumping. In Fiber III, the first-order Raman peak at 2060 nm begins to emerge at 40 mW pumping. The conversion efficiency is -15.0 dB, which is 21.6 dB higher than that in Fiber II. In Fiber IV, the Stokes peak at 2070 nm begins to appear at 56 mW pumping. The maximum conversion efficiency of the first-order Stokes wave is obtained in the MOF with the core diameter of 2.6 μm. The evolution of the first-order Stokes wave with pump power and fiber length is investigated. This is the first demonstration of Raman effects in the AsSe2-As2S5 MOF, to the best of our knowledge.

  1. Characterization of wood strands from young, small-diameter Douglas-fir and western hemlock trees

    Treesearch

    Vikram Yadama; Eini C. Lowell; Christopher E. Langum

    2012-01-01

    Tensile properties of strands processed from small-diameter Douglas-fir and western hemlock trees grown on the Washington coast were analyzed and effects of location within the tree on properties was examined. Reduction factors for strand properties relative to small, clear solid wood specimen properties were determined by correlating strand properties to previously...

  2. Fabrication of size-controlled nanoring arrays by selective incorporation of ionic liquids in diblock copolymer micellar cores

    NASA Astrophysics Data System (ADS)

    Kim, Sung-Soo; Kang, Donghwi; Sohn, Byeong-Hyeok

    2017-06-01

    We report the synthesis of arrayed nanorings with tunable physical dimensions from thin films of polystyrene-block-poly(4-vinylpyridine) (PS-P4VP) micelles. For accurate control of the inner and outer diameters of the nanorings, we added imidazolium-based ionic liquids (ILs) into the micellar solution, which were eventually incorporated into the micellar cores. We observed the structural changes of the micellar cores coated on a substrate due to the presence of ILs. The spin-coated micellar cores were treated with an acidic precursor solution and generated toroid nanostructures, of which size depended on the amount of IL loaded into the micelles. We then treated the transformed micellar films with oxygen plasma to produce arrays of various metal and oxide nanorings on a substrate. The spacings and diameters of nanorings were governed by the molecular weight of the PS-P4VP and the amount of IL used. We also demonstrated that arrayed Pt nanorings enabled the fabrication of reduced graphene oxide anti-nanoring arrays via a catalytic tailoring process.

  3. Hollow-core screw dislocations in 6H-SiC single crystals: A test of Frank`s theory

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Si, W.; Dudley, M.; Glass, R.

    1997-03-01

    Hollow-core screw dislocations, also known as `micropipes`, along the [0001] axis in 6H-SiC single crystals, have been studied by synchrotron white beam x-ray topography (SWBXT), scanning electron microscopy (SEM), and Nomarski optical microscopy (NOM). Using SWBXT, the magnitude of the burgers vector of screw dislocations has been determined by measuring the following four parameters: (1) the diameter of dislocation images in back-reflection topographs; (2) the width of bimodal dislocation images in transmission topographs; (3) the magnitude of the tilt of lattice planes on both sides of dislocation core in projection topographs; and (4) the magnitude of the tilt of latticemore » planes in section topographs. The four methods show good agreement. The burgers vector magnitude of screw dislocations, b, and the diameter of associated micropipes, D, were fitted to Frank`s prediction for hollow-core screw dislocations: D = {mu}b{sup 2}/4{pi}{sup 2}{gamma}, where {mu} is shear modulus, and {gamma} is specific surface energy. 15 refs., 17 figs.« less

  4. A sensitivity-enhanced refractive index sensor using a single-mode thin-core fiber incorporating an abrupt taper.

    PubMed

    Shi, Jie; Xiao, Shilin; Yi, Lilin; Bi, Meihua

    2012-01-01

    A sensitivity-enhanced fiber-optic refractive index (RI) sensor based on a tapered single-mode thin-core diameter fiber is proposed and experimentally demonstrated. The sensor head is formed by splicing a section of tapered thin-core diameter fiber (TCF) between two sections of single-mode fibers (SMFs). The cladding modes are excited at the first SMF-TCF interface, and then interfere with the core mode at the second interface, thus forming an inter-modal interferometer (IMI). An abrupt taper (tens of micrometers long) made by the electric-arc-heating method is utilized, and plays an important role in improving sensing sensitivity. The whole manufacture process only involves fiber splicing and tapering, and all the fabrication process can be achieved by a commercial fiber fusion splicer. Using glycerol and water mixture solution as an example, the experimental results show that the refractive index sensitivity is measured to be 0.591 nm for 1% change of surrounding RI. The proposed sensor structure features simple structure, low cost, easy fabrication, and high sensitivity.

  5. Thulium fiber laser lithotripsy using small spherical distal fiber tips

    NASA Astrophysics Data System (ADS)

    Wilson, Christopher R.; Hardy, Luke A.; Kennedy, Joshua D.; Irby, Pierce B.; Fried, Nathaniel M.

    2016-02-01

    This study tests a 100-μm-core fiber with 300-μm-diameter ball tip during Thulium fiber laser (TFL) lithotripsy. The TFL was operated at 1908 nm wavelength with 35-mJ pulse energy, 500-μs pulse duration, and 300-Hz pulse rate. Calcium oxalate/phosphate stone samples were weighed, laser procedure times measured, and ablation rates calculated for ball tip fibers, with comparison to bare tip fibers. Photographs of ball tips were taken before and after each procedure to observe ball tip degradation and determine number of procedures completed before need to replace fiber. Saline irrigation rates and ureteroscope deflection were measured with and without TFL fiber present. There was no statistical difference (P > 0.05) between stone ablation rates for single-use ball tip fiber (1.3 +/- 0.4 mg/s) (n=10), multiple-use ball tip fiber (1.3 +/- 0.5 mg/s) (n=44), and conventional single-use bare tip fibers (1.3 +/- 0.2 mg/s) (n=10). Ball tip durability varied widely, but fibers averaged > 4 stone procedures before decline in stone ablation rates due to mechanical damage at front surface of ball tip. The small fiber diameter did not impact ureteroscope deflection or saline flow rates. The miniature ball tip fiber may provide a cost-effective design for safe fiber insertion through the ureteroscope working channel and the ureter without risk of scope damage or tissue perforation, and without compromising stone ablation efficiency during TFL ablation of kidney stones.

  6. Holmium: YAG laser-induced liquid jet knife: possible novel method for dissection.

    PubMed

    Nakagawa, Atsuhiro; Hirano, Takayuki; Komatsu, Makoto; Sato, Mariko; Uenohara, Hiroshi; Ohyama, Hideki; Kusaka, Yasuko; Shirane, Reizo; Takayama, Kazuyoshi; Yoshimoto, Takashi

    2002-01-01

    Making surgical incisions in vessel-rich organs without causing bleeding is difficult. Thus, it is necessary to develop new devices for this purpose, especially for surgery involving small vessels as in neurosurgery, where damage against even small cerebral vessels result in severe neurological deficits. A laser-induced liquid jet was generated by irradiating pulsed Holmium Yttrium-Aluminum-Garnet (Ho: YAG) laser (beams of 350 microseconds pulse width) within a copper tube (internal diameter, 1 mm) with pure water (150 ml /hour). Ho: YAG laser beams were irradiated through an optical fiber (core diameter, 0.4 mm). The influence of the input of laser energy, structure of the nozzle, and the stand-off distance between the optical fiber tip and nozzle exit on the jet velocity was measured by a high-speed video camera to evaluate controllability of jet. The effect on artificial organs made of 10 and 30%(w/v) gelatin, each of which represent features of soft tissue and blood vessels. Jet velocity increased in proportion to gain in laser energy input, and maximum penetration depth into 10%(w/v) gelatin was 35 mm by single exposure at 350 mJ/pulse without impairing a vessel model. Shapes of nozzle also modified jet velocity with optimal nozzle/tube area ratio of 0.25. The laser-induced liquid jet has excellent potential as a new tool for removing soft tissue without damaging vital structures. Copyright 2002 Wiley-Liss, Inc.

  7. Impact of agglomeration on the relaxometric properties of paramagnetic ultra-small gadolinium oxide nanoparticles

    NASA Astrophysics Data System (ADS)

    Faucher, Luc; Gossuin, Yves; Hocq, Aline; Fortin, Marc-André

    2011-07-01

    Ultra-small gadolinium oxide nanoparticles (US-Gd2O3) are used to provide 'positive' contrast effects in magnetic resonance imaging (MRI), and are being considered for molecular and cellular imaging applications. However, these nanoparticles can aggregate over time in aqueous medium, as well as when internalized into cells. This study is aimed at measuring in vitro, in aqueous medium, the impact of aggregation on the relaxometric properties of paramagnetic US-Gd2O3 particles. First, the nanoparticle core size as well as aggregation behaviour was assessed by HRTEM. DLS (hydrodynamic diameter) was used to measure the hydrodynamic diameter of nanoparticles and nanoaggregates. The relaxometric properties were measured by NMRD profiling, as well as with 1H NMR relaxometers. Then, the positive contrast enhancement effect was assessed by using magnetic resonance scanners (at 1.5 and 7 T). At every magnetic field, the longitudinal relaxivity (r1) decreased upon agglomeration, while remaining high enough to provide positive contrast. On the other hand, the transverse relaxivity (r2) slightly decreased at 0.47 and 1.41 T, but it was enhanced at higher fields (7 and 11.7 T) upon agglomeration. All NMRD profiles revealed a characteristic relaxivity peak in the range 60-100 MHz, suggesting the possibility to use US-Gd2O3 as an efficient 'positive-T1' contrast agent at clinical magnetic fields (1-3 T), in spite of aggregation.

  8. Modelling the impact of altered axonal morphometry on the response of regenerative nervous tissue to electrical stimulation through macro-sieve electrodes.

    PubMed

    Zellmer, Erik R; MacEwan, Matthew R; Moran, Daniel W

    2018-04-01

    Regenerated peripheral nervous tissue possesses different morphometric properties compared to undisrupted nerve. It is poorly understood how these morphometric differences alter the response of the regenerated nerve to electrical stimulation. In this work, we use computational modeling to explore the electrophysiological response of regenerated and undisrupted nerve axons to electrical stimulation delivered by macro-sieve electrodes (MSEs). A 3D finite element model of a peripheral nerve segment populated with mammalian myelinated axons and implanted with a macro-sieve electrode has been developed. Fiber diameters and morphometric characteristics representative of undisrupted or regenerated peripheral nervous tissue were assigned to core conductor models to simulate the two tissue types. Simulations were carried out to quantify differences in thresholds and chronaxie between undisrupted and regenerated fiber populations. The model was also used to determine the influence of axonal caliber on recruitment thresholds for the two tissue types. Model accuracy was assessed through comparisons with in vivo recruitment data from chronically implanted MSEs. Recruitment thresholds of individual regenerated fibers with diameters  >2 µm were found to be lower compared to same caliber undisrupted fibers at electrode to fiber distances of less than about 90-140 µm but roughly equal or higher for larger distances. Caliber redistributions observed in regenerated nerve resulted in an overall increase in average recruitment thresholds and chronaxie during whole nerve stimulation. Modeling results also suggest that large diameter undisrupted fibers located close to a longitudinally restricted current source such as the MSE have higher average recruitment thresholds compared to small diameter fibers. In contrast, large diameter regenerated nerve fibers located in close proximity of MSE sites have, on average, lower recruitment thresholds compared to small fibers. Utilizing regenerated fiber morphometry and caliber distributions resulted in accurate predictions of in vivo recruitment data. Our work uses computational modeling to show how morphometric differences between regenerated and undisrupted tissue results in recruitment threshold discrepancies, quantifies these differences, and illustrates how large undisrupted nerve fibers close to longitudinally restricted current sources have higher recruitment thresholds compared to adjacently positioned smaller fibers while the opposite is true for large regenerated fibers.

  9. Modelling the impact of altered axonal morphometry on the response of regenerative nervous tissue to electrical stimulation through macro-sieve electrodes

    NASA Astrophysics Data System (ADS)

    Zellmer, Erik R.; MacEwan, Matthew R.; Moran, Daniel W.

    2018-04-01

    Objective. Regenerated peripheral nervous tissue possesses different morphometric properties compared to undisrupted nerve. It is poorly understood how these morphometric differences alter the response of the regenerated nerve to electrical stimulation. In this work, we use computational modeling to explore the electrophysiological response of regenerated and undisrupted nerve axons to electrical stimulation delivered by macro-sieve electrodes (MSEs). Approach. A 3D finite element model of a peripheral nerve segment populated with mammalian myelinated axons and implanted with a macro-sieve electrode has been developed. Fiber diameters and morphometric characteristics representative of undisrupted or regenerated peripheral nervous tissue were assigned to core conductor models to simulate the two tissue types. Simulations were carried out to quantify differences in thresholds and chronaxie between undisrupted and regenerated fiber populations. The model was also used to determine the influence of axonal caliber on recruitment thresholds for the two tissue types. Model accuracy was assessed through comparisons with in vivo recruitment data from chronically implanted MSEs. Main results. Recruitment thresholds of individual regenerated fibers with diameters  >2 µm were found to be lower compared to same caliber undisrupted fibers at electrode to fiber distances of less than about 90-140 µm but roughly equal or higher for larger distances. Caliber redistributions observed in regenerated nerve resulted in an overall increase in average recruitment thresholds and chronaxie during whole nerve stimulation. Modeling results also suggest that large diameter undisrupted fibers located close to a longitudinally restricted current source such as the MSE have higher average recruitment thresholds compared to small diameter fibers. In contrast, large diameter regenerated nerve fibers located in close proximity of MSE sites have, on average, lower recruitment thresholds compared to small fibers. Utilizing regenerated fiber morphometry and caliber distributions resulted in accurate predictions of in vivo recruitment data. Significance. Our work uses computational modeling to show how morphometric differences between regenerated and undisrupted tissue results in recruitment threshold discrepancies, quantifies these differences, and illustrates how large undisrupted nerve fibers close to longitudinally restricted current sources have higher recruitment thresholds compared to adjacently positioned smaller fibers while the opposite is true for large regenerated fibers.

  10. Rheology of dilute cohesive granular gases

    NASA Astrophysics Data System (ADS)

    Takada, Satoshi; Hayakawa, Hisao

    2018-04-01

    Rheology of a dilute cohesive granular gas is theoretically and numerically studied. The flow curve between the shear viscosity and the shear rate is derived from the inelastic Boltzmann equation for particles having square-well potentials in a simple shear flow. It is found that (i) the stable uniformly sheared state only exists above a critical shear rate and (ii) the viscosity in the uniformly sheared flow is almost identical to that for uniformly sheared flow of hard core granular particles. Below the critical shear rate, clusters grow with time, in which the viscosity can be approximated by that for the hard-core fluids if we replace the diameter of the particle by the mean diameter of clusters.

  11. Porosity characterization for heterogeneous shales using integrated multiscale microscopy

    NASA Astrophysics Data System (ADS)

    Rassouli, F.; Andrew, M.; Zoback, M. D.

    2016-12-01

    Pore size distribution analysis plays a critical role in gas storage capacity and fluid transport characterization of shales. Study of the diverse distribution of pore size and structure in such low permeably rocks is withheld by the lack of tools to visualize the microstructural properties of shale rocks. In this paper we try to use multiple techniques to investigate the full pore size range in different sample scales. Modern imaging techniques are combined with routine analytical investigations (x-ray diffraction, thin section analysis and mercury porosimetry) to describe pore size distribution of shale samples from Haynesville formation in East Texas to generate a more holistic understanding of the porosity structure in shales, ranging from standard core plug down to nm scales. Standard 1" diameter core plug samples were first imaged using a Versa 3D x-ray microscope at lower resolutions. Then we pick several regions of interest (ROIs) with various micro-features (such as micro-cracks and high organic matters) in the rock samples to run higher resolution CT scans using a non-destructive interior tomography scans. After this step, we cut the samples and drill 5 mm diameter cores out of the selected ROIs. Then we rescan the samples to measure porosity distribution of the 5 mm cores. We repeat this step for samples with diameter of 1 mm being cut out of the 5 mm cores using a laser cutting machine. After comparing the pore structure and distribution of the samples measured form micro-CT analysis, we move to nano-scale imaging to capture the ultra-fine pores within the shale samples. At this stage, the diameter of the 1 mm samples will be milled down to 70 microns using the laser beam. We scan these samples in a nano-CT Ultra x-ray microscope and calculate the porosity of the samples by image segmentation methods. Finally, we use images collected from focused ion beam scanning electron microscopy (FIB-SEM) to be able to compare the results of porosity measurements from all different imaging techniques. These multi-scale characterization techniques are then compared with traditional analytical techniques such as Mercury Porosimetry.

  12. Sound controlled rotation of a cluster of small particles on an ultrasonically vibrating metal strip

    NASA Astrophysics Data System (ADS)

    Zhang, Xueyi; Zheng, Yun; Hu, Junhui

    2008-01-01

    We show that a vibrating metal strip, mechanically driven by an ultrasonic transducer, can rotate a cluster of small particles around a fixed point, and the diameter of the cluster of small particles can reach a stable value (steady diameter) for a given driving condition. The rotation is very stable when the vibration of the metal strip is appropriate. The revolution speed, its direction, and steady diameter of the particle cluster can be controlled by the operating frequency of the ultrasonic transducer. For shrimp eggs, a revolution speed up to 360rpm can be obtained.

  13. Additional nuclear criticality safety calculations for small-diameter containers

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Hone, M.J.

    This report documents additional criticality safety analysis calculations for small diameter containers, which were originally documented in Reference 1. The results in Reference 1 indicated that some of the small diameter containers did not meet the criteria established for criticality safety at the Portsmouth facility (K{sub eff} +2{sigma}<.95) when modeled under various contingency assumptions of reflection and moderation. The calculations performed in this report reexamine those cases which did not meet the criticality safety criteria. In some cases, unnecessary conservatism is removed, and in other cases mass or assay limits are established for use with the respective containers.

  14. Silica-Assisted Nucleation of Polymer Foam Cells with Nanoscopic Dimensions: Impact of Particle Size, Line Tension, and Surface Functionality.

    PubMed

    Liu, Shanqiu; Eijkelenkamp, Rik; Duvigneau, Joost; Vancso, G Julius

    2017-11-01

    Core-shell nanoparticles consisting of silica as core and surface-grafted poly(dimethylsiloxane) (PDMS) as shell with different diameters were prepared and used as heterogeneous nucleation agents to obtain CO 2 -blown poly(methyl methacrylate) (PMMA) nanocomposite foams. PDMS was selected as the shell material as it possesses a low surface energy and high CO 2 -philicity. The successful synthesis of core-shell nanoparticles was confirmed by Fourier transform infrared spectroscopy, thermogravimetric analysis, and transmission electron microscopy. The cell size and cell density of the PMMA micro- and nanocellular materials were determined by scanning electron microscopy. The cell nucleation efficiency using core-shell nanoparticles was significantly enhanced when compared to that of unmodified silica. The highest nucleation efficiency observed had a value of ∼0.5 for nanoparticles with a core diameter of 80 nm. The particle size dependence of cell nucleation efficiency is discussed taking into account line tension effects. Complete engulfment by the polymer matrix of particles with a core diameter below 40 nm at the cell wall interface was observed corresponding to line tension values of approximately 0.42 nN. This line tension significantly increases the energy barrier of heterogeneous nucleation and thus reduces the nucleation efficiency. The increase of the CO 2 saturation pressure to 300 bar prior to batch foaming resulted in an increased line tension length. We observed a decrease of the heterogeneous nucleation efficiency for foaming after saturation with CO 2 at 300 bar, which we attribute to homogenous nucleation becoming more favorable at the expense of heterogeneous nucleation in this case. Overall, it is shown that the contribution of line tension to the free energy barrier of heterogeneous foam cell nucleation must be considered to understand foaming of viscoelastic materials. This finding emphasizes the need for new strategies including the use of designer nucleating particles to enhance the foam cell nucleation efficiency.

  15. Preparation of Fragrant Microencapsules and Coating on Textiles

    NASA Astrophysics Data System (ADS)

    Shah Jafari, M. H.; Parvinzadeh, M.; Najafi, F.

    2007-08-01

    A microcapsule is a small sphere with a uniform wall around it. Microcapsules range in diameter from 1 to 1000 μm. The move by the more developed countries into textiles with new properties and added value, into medical and technical textiles, has encouraged the industry to use microencapsulation process as a means of imparting finishes and properties on textiles which were not possible or cost-effective using other technology. Numerous attempts have been made at adding fragrances directly to fiber and fabrics but all fail to survive after one or two wash cycle. Only through microencapsulation, fragrances are able to remain on a garment during a significant part of its lifetime. This research has tried to prepare microcapsules with poly methyl methacrylate (PMMA) as wall and Rose fragrance as core.

  16. Beam collimation and focusing and error analysis of LD and fiber coupling system based on ZEMAX

    NASA Astrophysics Data System (ADS)

    Qiao, Lvlin; Zhou, Dejian; Xiao, Lei

    2017-10-01

    Laser diodde has many advantages, such as high efficiency, small volume, low cost and easy integration, so it is widely used. Because of its poor beam quality, the application of semiconductor laser has also been seriously hampered. In view of the poor beam quality, the ZEMAX optical design software is used to simulate the far field characteristics of the semiconductor laser beam, and the coupling module of the semiconductor laser and the optical fiber is designed and optimized. And the beam is coupled into the fiber core diameter d=200µm, the numerical aperture NA=0.22 optical fiber, the output power can reach 95%. Finally, the influence of the three docking errors on the coupling efficiency during the installation process is analyzed.

  17. Design of graded refractive index profile for silica multimode optical fibers with improved effective modal bandwidth for short-distance laser-based multi-Gigabit data transmission over "O"-band

    NASA Astrophysics Data System (ADS)

    Bourdine, Anton V.; Zhukov, Alexander E.

    2017-04-01

    High bit rate laser-based data transmission over silica optical fibers with enlarged core diameter in comparison with standard singlemode fibers is found variety infocommunication applications. Since IEEE 802.3z standard was ratified on 1998 this technique started to be widely used for short-range in-premises distributed multi-Gigabit networks based on new generation laser optimized multimode fibers 50/125 of Cat. OM2…OM4. Nowadays it becomes to be in demand for on-board cable systems and industrial network applications requiring 1Gps and more bit rates over fibers with extremely enlarged core diameter up to 100 μm. This work presents an alternative method for design the special refractive index profiles of silica few-mode fibers with extremely enlarged core diameter, that provides modal bandwidth enhancing under a few-mode regime of laser-based data optical transmission. Here some results are presented concerning with refractive index profile synthesis for few-mode fibers with reduced differential mode delay for "O"-band central region, as well as computed differential mode delay spectral curves corresponding to profiles for fibers 50/125 and 100/125 for in-premises and on-board/industrial cable systems.

  18. Evaluation of moisture reduction in small diameter trees after crushing

    Treesearch

    Donald L. Sirois; Cynthia L. Rawlins; Bryce J. Stokes

    1991-01-01

    Past studies have suggested that processing small diameter whole trees like those foumd on rights-of-way (ROWs) would help reduce transportion costs and increase energy value by lowering stem moisture content. Small stems were crushed by a roller crusher/splitter test bench machine and allowed dry under field conditions in Alabama. Tests were conducted in winter and...

  19. Users guide for STHARVEST: software to estimate the cost of harvesting small timber.

    Treesearch

    Roger D. Fight; Xiaoshan Zhang; Bruce R. Hartsough

    2003-01-01

    The STHARVEST computer application is Windows-based, public-domain software used to estimate costs for harvesting small-diameter stands or the small-diameter component of a mixed-sized stand. The equipment production rates were developed from existing studies. Equipment operating cost rates were based on November 1998 prices for new equipment and wage rates for the...

  20. Advanced UVOIR Mirror Technology Development (AMTD) for Very Large Space Telescopes

    NASA Technical Reports Server (NTRS)

    Postman, Marc; Soummer, Remi; Sivramakrishnan, Annand; Macintosh, Bruce; Guyon, Olivier; Krist, John; Stahl, H. Philip; Smith, W. Scott; Mosier, Gary; Kirk, Charles; hide

    2013-01-01

    AMTD partner Exelis developed & demonstrated a technique to manufacture a 400 mm thick substrate via stacking and fusing core structural elements to front and back faceplates; making a 40 cm cut-out of a 4 meter diameter 60 kilograms per square meter mirror. This new process offers a lower cost approach for manufacturing large-diameter high-stiffness mirrors.

  1. Spectral efficiency in crosstalk-impaired multi-core fiber links

    NASA Astrophysics Data System (ADS)

    Luís, Ruben S.; Puttnam, Benjamin J.; Rademacher, Georg; Klaus, Werner; Agrell, Erik; Awaji, Yoshinari; Wada, Naoya

    2018-02-01

    We review the latest advances on ultra-high throughput transmission using crosstalk-limited single-mode multicore fibers and compare these with the theoretical spectral efficiency of such systems. We relate the crosstalkimposed spectral efficiency limits with fiber parameters, such as core diameter, core pitch, and trench design. Furthermore, we investigate the potential of techniques such as direction interleaving and high-order MIMO to improve the throughput or reach of these systems when using various modulation formats.

  2. Effective separation technique for small diameter whiskers.

    NASA Technical Reports Server (NTRS)

    Westfall, L. J.

    1972-01-01

    Description of a technique for separating small-diameter whiskers from the as-grown matt by gently agitating the whisker matts in a solution of deionized or distilled water for six to eight hours. High-strength Al2O3 whiskers were effectively separated by this technique, comprising an average 48% of the original weight of the whisker matt. According to estimation, more than 90% of separated whiskers had diameters between 0.7 and 2.0 microns.

  3. Wood and bark specific gravity of small-diameter, pine-site hardwood in the south

    Treesearch

    F.G. Manwiller

    1979-01-01

    Ten small-diameter trees from each of the 22 species (220 trees) were sampled from throughout the southern United States. Mean SG was determined for stem wood and bark and the whole stem, for branch wood and bark and whole branches (to a minimum diameter of 0.05 in.), and for tree wood and bark and the whole tree. Significant differences were determined a) among the...

  4. Small-Diameter Awls Improve Articular Cartilage Repair After Microfracture Treatment in a Translational Animal Model.

    PubMed

    Orth, Patrick; Duffner, Julia; Zurakowski, David; Cucchiarini, Magali; Madry, Henning

    2016-01-01

    Microfracture is the most commonly applied arthroscopic marrow stimulation procedure. Articular cartilage repair is improved when the subchondral bone is perforated by small-diameter microfracture awls compared with larger awls. Controlled laboratory study. Standardized rectangular (4 × 8 mm) full-thickness chondral defects (N = 24) were created in the medial femoral condyle of 16 adult sheep and debrided down to the subchondral bone plate. Three treatment groups (n = 8 defects each) were tested: 6 microfracture perforations using small-diameter awls (1.0 mm; group 1), large-diameter awls (1.2 mm; group 2), or without perforations (debridement control; group 3). Osteochondral repair was assessed at 6 months in vivo using established macroscopic, histological, immunohistochemical, biochemical, and micro-computed tomography analyses. Compared with control defects, histological cartilage repair was always improved after both microfracture techniques (P < .023). Application of 1.0-mm microfracture awls led to a significantly improved histological overall repair tissue quality (7.02 ± 0.70 vs 9.03 ± 0.69; P = .008) and surface grading (1.05 ± 0.28 vs 2.10 ± 0.19; P = .001) compared with larger awls. The small-diameter awl decreased relative bone volume of the subarticular spongiosa (bone volume/tissue volume ratio: 23.81% ± 3.37% vs 30.58% ± 2.46%; P = .011). Subchondral bone cysts and intralesional osteophytes were frequently observed after either microfracture treatment. Macroscopic grading, DNA, proteoglycan, and type I and type II collagen contents as well as degenerative changes within the adjacent cartilage remained unaffected by the awl diameter. Small-diameter microfracture awls improve articular cartilage repair in the translational sheep model more effectively than do larger awls. These data support the use of small microfracture instruments for the surgical treatment of cartilage defects and warrant prolonged clinical investigations. © 2015 The Author(s).

  5. A SPACESHIP WITH NUCLEAR PROPULSION

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Polorny, J.

    1962-01-01

    ABS>A proposed space vehicle with nuclear propulsion for a round-trip Martian mission is described. It would be powered by a 270-Mw graphite- moderated, U-fueled nuclear reactor with a core 1 m high by 1 m in diameter, and use gas as propellant. The gas would be heated to the maximum temperature in the reactor and additionally accelerated by an electromagnetic field. To this end, small quantities of K would be injected into the gas stream to increase its electric conductivity. The required electrical energy would be produced by liquid-Na-cooled thermionic converters. The vehicle would weigh 115000 kg, including 43000 kgmore » of H propellant with tankage, and 7000 kg of sustenance material for one year. Chemical rockets would launch the vehicle with a crew of three men into an earth orbit where nuclear propulsion would take over. Upon reactor start-up, three heat exchangers (minimum dimensions 30 x 18 m) would be fanned out. A shielded well with a diameter of 2.5 m would protect the crew from radiation during reactor operation, passage through the earth radiation belts, and at periods of solar flares. (OTS)« less

  6. Polarization-induced local pore-wall functionalization for biosensing: from micropore to nanopore.

    PubMed

    Liu, Jie; Pham, Pascale; Haguet, Vincent; Sauter-Starace, Fabien; Leroy, Loïc; Roget, André; Descamps, Emeline; Bouchet, Aurélie; Buhot, Arnaud; Mailley, Pascal; Livache, Thierry

    2012-04-03

    The use of biological-probe-modified solid-state pores in biosensing is currently hindered by difficulties in pore-wall functionalization. The surface to be functionalized is small and difficult to target and is usually chemically similar to the bulk membrane. Herein, we demonstrate the contactless electrofunctionalization (CLEF) approach and its mechanism. This technique enables the one-step local functionalization of the single pore wall fabricated in a silica-covered silicon membrane. CLEF is induced by polarization of the pore membrane in an electric field and requires a sandwich-like composition and a conducting or semiconducting core for the pore membrane. The defects in the silica layer of the micropore wall enable the creation of an electric pathway through the silica layer, which allows electrochemical reactions to take place locally on the pore wall. The pore diameter is not a limiting factor for local wall modification using CLEF. Nanopores with a diameter of 200 nm fabricated in a silicon membrane and covered with native silica layer have been successfully functionalized with this method, and localized pore-wall modification was obtained. Furthermore, through proof-of-concept experiments using ODN-modified nanopores, we show that functionalized nanopores are suitable for translocation-based biosensing.

  7. Miniature ureteroscope tip designs for use in thulium fiber laser lithotripsy

    NASA Astrophysics Data System (ADS)

    Kennedy, Joshua D.; Wilson, Christopher R.; Irby, Pierce B.; Fried, Nathaniel M.

    2017-02-01

    A miniature ureteroscope has the potential to eliminate need for full anesthesia and dilation, increase comfort and safety of laser lithotripsy via ureteroscopy, and reduce hospital costs via an office based procedure. A prototype, 4.5 Fr (1.5-mm-OD), five channel ureteroscope tip was developed, housing a 200-μm-ID central channel for insertion of small, 100-μm-core fibers and four surrounding channels, each with 510-μm-ID for instrumentation, irrigation, imaging, and illumination, respectively. Common urological instruments (including fibers, guidewires, and stone baskets) were inserted through tip's working channels to demonstrate feasibility. Low irrigation rates were measured, revealing a need for manual pump-assisted irrigation. Imaging was conducted using 3k, 6k, and 10k pixel miniature flexible endoscopes with 0.4, 0.6, and 0.9 mm outer diameters, respectively. The 3k pixel endoscope with integrated illumination was inserted through the prototype unimpeded, and successfully demonstrated ability to differentiate between hard tissues (e.g. kidney stones) and soft tissues (e.g. ureter wall), for visibility and safety during potential clinical application. Based on both image quality and instrument diameter, the 6k pixel endoscope provided an optimal solution for miniature ureteroscopy.

  8. Realization of a fiber optic sensor detecting the presence of a liquid

    NASA Astrophysics Data System (ADS)

    Guzowski, B.; Łakomski, M.; Nowogrodzki, K.

    2016-11-01

    Over the past thirty years, optical fibers have revolutionized the telecommunication market. Fiber optics play also important roles in other numerous applications. One of these applications is fiber sensing - very fast developing area. In this paper, realization of different configurations of a fiber optic sensor detecting the presence of liquid is presented. In the presented sensor, two multimode fibers (MMF) are placed opposite each other, where the first one transmits the light radiation, while the second one is a receiver. Due to the small size of the core (50 μm diameter), they had to be precisely positioned. Therefore the optical fibers were placed in the etched channels in the silicon substrate. In order to make sensors more sensitive, ball-lensed optical fibers were used. Four different diameters of lenses were examined. Sensitivity to the presence of liquids was compared in all realized sensors. Moreover, the influence of distance between the transmitting and receiving optical fiber on the received optical power is also described in this paper. All developed sensors were tested at 1300 nm wavelength. In the last part of this paper the detailed discussion is given.

  9. Femoral head necrosis: A finite element analysis of common and novel surgical techniques.

    PubMed

    Cilla, Myriam; Checa, Sara; Preininger, Bernd; Winkler, Tobias; Perka, Carsten; Duda, Georg N; Pumberger, Matthias

    2017-10-01

    Femoral head necrosis is a common cause of secondary osteoarthritis. At the early stages, treatment strategies are normally based on core decompression techniques, where the number, location and diameter of the drilling holes varies depending on the selected approach. The purpose of this study was to investigate the risk of femoral head, neck and subtrochanteric fracture following six different core decompression techniques. Five common and a newly proposed techniques were analyzed in respect to their biomechanical consequences using finite element analysis. The geometry of a femur was reconstructed from computed-tomography images. Thereafter, the drilling configurations were simulated. The strains in the intact and drilled femurs were determined under physiological, patient-specific, muscle and joint contact forces. The following results were observed: i) - an increase in collapse and fracture risk of the femur head by disease progression ii) - for a single hole approach at the subtrochanteric region, the fracture risk increases with the diameter iii) - the highest fracture risks occur for an 8mm single hole drilling at the subtrochanteric region and approaches with multiple drilling at various entry points iv) - the proposed novel approach resulted in the most physiological strains (closer to the experienced by the healthy bone). Our results suggest that all common core decompression methods have a significant impact on the biomechanical competence of the proximal femur and impact its mechanical potential. Fracture risk increases with drilling diameter and multiple drilling with smaller diameter. We recommend the anterior approach due to its reduced soft tissue trauma and its biomechanical performance. Copyright © 2017 Elsevier Ltd. All rights reserved.

  10. Magneto-plasmonic Au-Coated Co nanoparticles synthesized via hot-injection method

    NASA Astrophysics Data System (ADS)

    Souza, João B., Jr.; Varanda, Laudemir C.

    2018-02-01

    A synthetic procedure is described for the obtaining of superparamagnetic Co nanoparticles (NPs) via hot-injection method in the presence of sodium borohydride. The Co NPs obtained have an average diameter of 5.3 nm and saturation magnetization of 115 emu g-1. A modified Langevin equation is fitted to the magnetization curves using a log-normal distribution for the particle diameter and an effective field to account for dipolar interactions. The calculated magnetic diameter of the Co NPs is 0.6 nm smaller than TEM-derived values, implying a magnetic dead layer of 0.3 nm. The magnetic core is coated with Au to prevent oxidation, resulting in water-stable magneto-plasmonic Co/Au core/shell NPs with saturation of 71.6 emu g-1. The coating adds a localized surface plasmon resonance property with absorbance in the so-called ‘therapeutic window’ (690-900 nm), suitable for biomedical applications. It is suggested that these multifunctional NPs are distinguished as a potential platform for applied and fundamental research.

  11. Gravity-Independent Mobility and Drilling on Natural Rock using Microspines

    NASA Technical Reports Server (NTRS)

    Parness, Aaron; Frost, Matthew; Thatte, Nitish; King, Jonathan P.

    2012-01-01

    To grip rocks on the surfaces of asteroids and comets, and to grip the cliff faces and lava tubes of Mars, a 250 mm diameter omni-directional anchor is presented that utilizes a hierarchical array of claws with suspension flexures, called microspines, to create fast, strong attachment. Prototypes have been demonstrated on vesicular basalt and a'a lava rock supporting forces in all directions away from the rock. Each anchor can support >160 N tangent, >150 N at 45?, and >180 N normal to the surface of the rock. A two-actuator selectively- compliant ankle interfaces these anchors to the Lemur IIB robot for climbing trials. A rotary percussive drill was also integrated into the anchor, demonstrating self-contained rock coring regardless of gravitational orientation. As a harder- than-zero-g proof of concept, 20mm diameter boreholes were drilled 83 mm deep in vesicular basalt samples, retaining a 12 mm diameter rock core in 3-6 pieces while in an inverted configuration, literally drilling into the ceiling.

  12. Cutting Diameter Influences Early Survival and Growth of Several Populus Clones

    Treesearch

    Donald Dickmann; Howard Phipps; Daniel Netzer

    1980-01-01

    The effects of cutting diameter on early survival and growth of several Populus clones were studied in field tests in Wisconsin and Michigan. Generally, large diameter cuttings survived and grew better than small diameter cuttings. Response differences among clones were evident.

  13. The use of hollow-core photonic crystal fibres as biological sensors

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Malinin, A V; Skibina, Yu S; Tuchin, Valerii V

    2011-04-30

    The results of development and study of a new type of a hollow-core photonic crystal fibre with radially increasing diameter of capillaries in the structured cladding are presented. The waveguide possesses a specific transmission spectrum and can be used as an efficient analyser of biological media. (optical technologies in biophysics and medicine)

  14. An approach to model reactor core nodalization for deterministic safety analysis

    NASA Astrophysics Data System (ADS)

    Salim, Mohd Faiz; Samsudin, Mohd Rafie; Mamat @ Ibrahim, Mohd Rizal; Roslan, Ridha; Sadri, Abd Aziz; Farid, Mohd Fairus Abd

    2016-01-01

    Adopting good nodalization strategy is essential to produce an accurate and high quality input model for Deterministic Safety Analysis (DSA) using System Thermal-Hydraulic (SYS-TH) computer code. The purpose of such analysis is to demonstrate the compliance against regulatory requirements and to verify the behavior of the reactor during normal and accident conditions as it was originally designed. Numerous studies in the past have been devoted to the development of the nodalization strategy for small research reactor (e.g. 250kW) up to the bigger research reactor (e.g. 30MW). As such, this paper aims to discuss the state-of-arts thermal hydraulics channel to be employed in the nodalization for RTP-TRIGA Research Reactor specifically for the reactor core. At present, the required thermal-hydraulic parameters for reactor core, such as core geometrical data (length, coolant flow area, hydraulic diameters, and axial power profile) and material properties (including the UZrH1.6, stainless steel clad, graphite reflector) have been collected, analyzed and consolidated in the Reference Database of RTP using standardized methodology, mainly derived from the available technical documentations. Based on the available information in the database, assumptions made on the nodalization approach and calculations performed will be discussed and presented. The development and identification of the thermal hydraulics channel for the reactor core will be implemented during the SYS-TH calculation using RELAP5-3D® computer code. This activity presented in this paper is part of the development of overall nodalization description for RTP-TRIGA Research Reactor under the IAEA Norwegian Extra-Budgetary Programme (NOKEBP) mentoring project on Expertise Development through the Analysis of Reactor Thermal-Hydraulics for Malaysia, denoted as EARTH-M.

  15. Sample Acquisition and Caching architecture for the Mars Sample Return mission

    NASA Astrophysics Data System (ADS)

    Zacny, K.; Chu, P.; Cohen, J.; Paulsen, G.; Craft, J.; Szwarc, T.

    This paper presents a Mars Sample Return (MSR) Sample Acquisition and Caching (SAC) study developed for the three rover platforms: MER, MER+, and MSL. The study took into account 26 SAC requirements provided by the NASA Mars Exploration Program Office. For this SAC architecture, the reduction of mission risk was chosen by us as having greater priority than mass or volume. For this reason, we selected a “ One Bit per Core” approach. The enabling technology for this architecture is Honeybee Robotics' “ eccentric tubes” core breakoff approach. The breakoff approach allows the drill bits to be relatively small in diameter and in turn lightweight. Hence, the bits could be returned to Earth with the cores inside them with only a modest increase to the total returned mass, but a significant decrease in complexity. Having dedicated bits allows a reduction in the number of core transfer steps and actuators. It also alleviates the bit life problem, eliminates cross contamination, and aids in hermetic sealing. An added advantage is faster drilling time, lower power, lower energy, and lower Weight on Bit (which reduces Arm preload requirements). Drill bits are based on the BigTooth bit concept, which allows re-use of the same bit multiple times, if necessary. The proposed SAC consists of a 1) Rotary-Percussive Core Drill, 2) Bit Storage Carousel, 3) Cache, 4) Robotic Arm, and 5) Rock Abrasion and Brushing Bit (RABBit), which is deployed using the Drill. The system also includes PreView bits (for viewing of cores prior to caching) and Powder bits for acquisition of regolith or cuttings. The SAC total system mass is less than 22 kg for MER and MER+ size rovers and less than 32 kg for the MSL-size rover.

  16. An approach to model reactor core nodalization for deterministic safety analysis

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Salim, Mohd Faiz, E-mail: mohdfaizs@tnb.com.my; Samsudin, Mohd Rafie, E-mail: rafies@tnb.com.my; Mamat Ibrahim, Mohd Rizal, E-mail: m-rizal@nuclearmalaysia.gov.my

    Adopting good nodalization strategy is essential to produce an accurate and high quality input model for Deterministic Safety Analysis (DSA) using System Thermal-Hydraulic (SYS-TH) computer code. The purpose of such analysis is to demonstrate the compliance against regulatory requirements and to verify the behavior of the reactor during normal and accident conditions as it was originally designed. Numerous studies in the past have been devoted to the development of the nodalization strategy for small research reactor (e.g. 250kW) up to the bigger research reactor (e.g. 30MW). As such, this paper aims to discuss the state-of-arts thermal hydraulics channel to bemore » employed in the nodalization for RTP-TRIGA Research Reactor specifically for the reactor core. At present, the required thermal-hydraulic parameters for reactor core, such as core geometrical data (length, coolant flow area, hydraulic diameters, and axial power profile) and material properties (including the UZrH{sub 1.6}, stainless steel clad, graphite reflector) have been collected, analyzed and consolidated in the Reference Database of RTP using standardized methodology, mainly derived from the available technical documentations. Based on the available information in the database, assumptions made on the nodalization approach and calculations performed will be discussed and presented. The development and identification of the thermal hydraulics channel for the reactor core will be implemented during the SYS-TH calculation using RELAP5-3D{sup ®} computer code. This activity presented in this paper is part of the development of overall nodalization description for RTP-TRIGA Research Reactor under the IAEA Norwegian Extra-Budgetary Programme (NOKEBP) mentoring project on Expertise Development through the Analysis of Reactor Thermal-Hydraulics for Malaysia, denoted as EARTH-M.« less

  17. Fermi energy dependence of the optical emission in core/shell InAs nanowire homostructures

    NASA Astrophysics Data System (ADS)

    Möller, M.; Oliveira, D. S.; Sahoo, P. K.; Cotta, M. A.; Iikawa, F.; Motisuke, P.; Molina-Sánchez, A.; de Lima, M. M., Jr.; García-Cristóbal, A.; Cantarero, A.

    2017-07-01

    InAs nanowires grown by vapor-liquid-solid (VLS) method are investigated by photoluminescence. We observe that the Fermi energy of all samples is reduced by ˜20 meV when the size of the Au nanoparticle used for catalysis is increased from 5 to 20 nm. Additional capping with a thin InP shell enhances the optical emission and does not affect the Fermi energy. The unexpected behavior of the Fermi energy is attributed to the differences in the residual donor (likely carbon) incorporation in the axial (low) and lateral (high incorporation) growth in the VLS and vapor-solid (VS) methods, respectively. The different impurity incorporation rate in these two regions leads to a core/shell InAs homostructure. In this case, the minority carriers (holes) diffuse to the core due to the built-in electric field created by the radial impurity distribution. As a result, the optical emission is dominated by the core region rather than by the more heavily doped InAs shell. Thus, the photoluminescence spectra and the Fermi energy become sensitive to the core diameter. These results are corroborated by a theoretical model using a self-consistent method to calculate the radial carrier distribution and Fermi energy for distinct diameters of Au nanoparticles.

  18. Production of small diameter high-temperature-strength refractory metal wires

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Signorelli, R. A.; King, G. W.

    1973-01-01

    Special thermomechanical techniques (schedules) have been developed to produce small diameter wire from three refractory metal alloys: colombian base alloy, tantalum base alloy, and tungsten base alloy. High strengths of these wires indicate their potential for contributing increased strength to metallic composites.

  19. Toward Small-Diameter Carbon Nanotubes Synthesized from Captured Carbon Dioxide: Critical Role of Catalyst Coarsening.

    PubMed

    Douglas, Anna; Carter, Rachel; Li, Mengya; Pint, Cary L

    2018-06-06

    Small-diameter carbon nanotubes (CNTs) often require increased sophistication and control in synthesis processes, but exhibit improved physical properties and greater economic value over their larger-diameter counterparts. Here, we study mechanisms controlling the electrochemical synthesis of CNTs from the capture and conversion of ambient CO 2 in molten salts and leverage this understanding to achieve the smallest-diameter CNTs ever reported in the literature from sustainable electrochemical synthesis routes, including some few-walled CNTs. Here, Fe catalyst layers are deposited at different thicknesses onto stainless steel to produce cathodes, and atomic layer deposition of Al 2 O 3 is performed on Ni to produce a corrosion-resistant anode. Our findings indicate a correlation between the CNT diameter and Fe metal layer thickness following electrochemical catalyst reduction at the cathode-molten salt interface. Further, catalyst coarsening during long duration synthesis experiments leads to a 2× increase in average diameters from 3 to 60 min durations, with CNTs produced after 3 min exhibiting a tight diameter distribution centered near ∼10 nm. Energy consumption analysis for the conversion of CO 2 into CNTs demonstrates energy input costs much lower than the value of CNTs-a concept that strictly requires and motivates small-diameter CNTs-and is more favorable compared to other costly CO 2 conversion techniques that produce lower-value materials and products.

  20. Flowfield predictions for multiple body launch vehicles

    NASA Technical Reports Server (NTRS)

    Deese, Jerry E.; Pavish, D. L.; Johnson, Jerry G.; Agarwal, Ramesh K.; Soni, Bharat K.

    1992-01-01

    A method is developed for simulating inviscid and viscous flow around multicomponent launch vehicles. Grids are generated by the GENIE general-purpose grid-generation code, and the flow solver is a finite-volume Runge-Kutta time-stepping method. Turbulence effects are simulated using Baldwin and Lomax (1978) turbulence model. Calculations are presented for three multibody launch vehicle configurations: one with two small-diameter solid motors, one with nine small-diameter solid motors, and one with three large-diameter solid motors.

  1. Precision wire feeder for small diameter wire

    DOEpatents

    Brandon, Eldon D.; Hooper, Frederick M.; Reichenbach, Marvin L.

    1992-01-01

    A device for feeding small diameter wire having a diameter less than 0.04 mm (16 mil) to a welding station includes a driving wheel for controllably applying a non-deforming driving force to the wire to move the free end of the wire towards the welding station; and a tension device such as a torque motor for constantly applying a reverse force to the wire in opposition to the driving force to keep the wire taut.

  2. Precision wire feeder for small diameter wire

    DOEpatents

    Brandon, E.D.; Hooper, F.M.; Reichenbach, M.L.

    1992-08-11

    A device for feeding small diameter wire having a diameter less than 0.04 mm (16 mil) to a welding station includes a driving wheel for controllably applying a non-deforming driving force to the wire to move the free end of the wire towards the welding station; and a tension device such as a torque motor for constantly applying a reverse force to the wire in opposition to the driving force to keep the wire taut. 1 figure.

  3. Long-term results of small-diameter proximal splenorenal venous shunt: A retrospective study

    PubMed Central

    Chen, Hao; Yang, Wei-Ping; Yan, Ji-Qi; Li, Qin-Yu; Ma, Di; Li, Hong-Wei

    2011-01-01

    AIM: To investigate recurrent variceal hemorrhage and long-term survival rates of patients treated with partial proximal splenorenal venous shunt. METHODS: Patients with variceal hemorrhage who were treated with small-diameter proximal splenorenal venous shunt in Ruijin Hospital between 1996 and 2009 were included in this study. Shunt diameter was determined before operation using Duplex Doppler ultrasonography. Peri-operative and long-term results in term of rehemorrhage, encephalopathy and mortality were followed up. RESULTS: Ninety-eight patients with Child A and B variceal hemorrhage received small-diameter proximal splenorenal venous shunt with a diameter of 7-10 mm. After operation, the patients’ mean free portal pressure (P < 0.01) and the flow rate of main portal vein (P < 0.01) decreased significantly compared with that before operation. The rates of rebleeding and mortality were 6.12% (6 cases) and 2.04% (2 cases), respectively. Ninety-one patients were followed up for 7 mo-14 years (median, 48.57 mo). Long-term rates of rehemorrhage and encephalopathy were 4.40% (4 cases) and 3.30% (3 cases), respectively. Thirteen patients (14.29%) died mainly due to progressive hepatic dysfunction. Five- and ten-year survival rates were 82.12% and 71.24%, respectively. CONCLUSION: Small-diameter proximal splenorenal venous shunt affords protection against variceal rehemorrhage with a low occurrence of encephalopathy in patients with normal liver function. PMID:21876638

  4. Fabrication of bundle-structured tube-leaky optical fibers for infrared thermal imaging

    NASA Astrophysics Data System (ADS)

    Kobayashi, T.; Katagiri, T.; Matsuura, Y.

    2017-02-01

    Bundled glass tubular fibers were fabricated by glass drawing technique for endoscopic infrared-thermal imaging. The bundle fibers were made of borosilicate glass and have a structure like a photonic crystal fiber having multiple hollow cores. Fabricated fibers have a length of 90 cm and each pixel sizes are less than 80 μm. By setting the thickness of glass wall to a quarter-wavelength optical thickness, light is confined in the air core as a leaky mode with a low loss owing to the interference effect of the thin glass wall and this type of hollow-core fibers is known as tube leaky fibers. The transmission losses of bundled fibers were firstly measured and it was found that bundled tube-leaky fibers have reasonably low transmission losses in spite of the small pixel size. Then thermal images were delivered by the bundled fibers combining with an InSb infrared camera. Considering applications with rigid endoscopes, an imaging system composed of a 30-cm long fiber bundle and a half-ball lens with a diameter of 2 mm was fabricated. By using this imaging system, a metal wire with a thickness of 200 μm was successfully observed and another test showed that the minimum detected temperature was 32.0 °C and the temperature resolution of the system was around 0.7 °C.

  5. Polypyrrole coated phase-change contrast agents for sono-photoacoustic imaging (Conference Presentation)

    NASA Astrophysics Data System (ADS)

    Li, David S.; Yoon, Soon Joon; Matula, Thomas J.; O'Donnell, Matthew; Pozzo, Lilo D.

    2017-03-01

    A new light and sound sensitive nanoemulsion contrast agent is presented. The agents feature a low boiling point liquid perfluorocarbon core and a broad light spectrum absorbing polypyrrole (PPy) polymer shell. The PPy coated nanoemulsions can reversibly convert from liquid to gas phase upon cavitation of the liquid perfluorocarbon core. Cavitation can be initiated using a sufficiently high intensity acoustic pulse or from heat generation due to light absorption from a laser pulse. The emulsions can be made between 150 and 350 nm in diameter and PPy has a broad optical absorption covering both the visible spectrum and extending into the near-infrared spectrum (peak absorption 1053 nm). The size, structure, and optical absorption properties of the PPy coated nanoemulsions were characterized and compared to PPy nanoparticles (no liquid core) using dynamic light scattering, ultraviolet-visible spectrophotometry, transmission electron microscopy, and small angle X-ray scattering. The cavitation threshold and signal intensity were measured as a function of both acoustic pressure and laser fluence. Overlapping simultaneous transmission of an acoustic and laser pulse can significantly reduce the activation energy of the contrast agents to levels lower than optical or acoustic activation alone. We also demonstrate that simultaneous light and sound cavitation of the agents can be used in a new sono-photoacoustic imaging method, which enables greater sensitivity than traditional photoacoustic imaging.

  6. The design and fabrication of supramolecular semiconductor nanowires formed by benzothienobenzothiophene (BTBT)-conjugated peptides.

    PubMed

    Khalily, Mohammad Aref; Usta, Hakan; Ozdemir, Mehmet; Bakan, Gokhan; Dikecoglu, F Begum; Edwards-Gayle, Charlotte; Hutchinson, Jessica A; Hamley, Ian W; Dana, Aykutlu; Guler, Mustafa O

    2018-05-31

    π-Conjugated small molecules based on a [1]benzothieno[3,2-b]benzothiophene (BTBT) unit are of great research interest in the development of solution-processable semiconducting materials owing to their excellent charge-transport characteristics. However, the BTBT π-core has yet to be demonstrated in the form of electro-active one-dimensional (1D) nanowires that are self-assembled in aqueous media for potential use in bioelectronics and tissue engineering. Here we report the design, synthesis, and self-assembly of benzothienobenzothiophene (BTBT)-peptide conjugates, the BTBT-peptide (BTBT-C3-COHN-Ahx-VVAGKK-Am) and the C8-BTBT-peptide (C8-BTBT-C3-COHN-Ahx-VVAGKK-Am), as β-sheet forming amphiphilic molecules, which self-assemble into highly uniform nanofibers in water with diameters of 11-13(±1) nm and micron-size lengths. Spectroscopic characterization studies demonstrate the J-type π-π interactions among the BTBT molecules within the hydrophobic core of the self-assembled nanofibers yielding an electrical conductivity as high as 6.0 × 10-6 S cm-1. The BTBT π-core is demonstrated, for the first time, in the formation of self-assembled peptide 1D nanostructures in aqueous media for potential use in tissue engineering, bioelectronics and (opto)electronics. The conductivity achieved here is one of the highest reported to date in a non-doped state.

  7. Majorana states in prismatic core-shell nanowires

    NASA Astrophysics Data System (ADS)

    Manolescu, Andrei; Sitek, Anna; Osca, Javier; Serra, Llorenç; Gudmundsson, Vidar; Stanescu, Tudor Dan

    2017-09-01

    We consider core-shell nanowires with conductive shell and insulating core and with polygonal cross section. We investigate the implications of this geometry on Majorana states expected in the presence of proximity-induced superconductivity and an external magnetic field. A typical prismatic nanowire has a hexagonal profile, but square and triangular shapes can also be obtained. The low-energy states are localized at the corners of the cross section, i.e., along the prism edges, and are separated by a gap from higher energy states localized on the sides. The corner localization depends on the details of the shell geometry, i.e., thickness, diameter, and sharpness of the corners. We study systematically the low-energy spectrum of prismatic shells using numerical methods and derive the topological phase diagram as a function of magnetic field and chemical potential for triangular, square, and hexagonal geometries. A strong corner localization enhances the stability of Majorana modes to various perturbations, including the orbital effect of the magnetic field, whereas a weaker localization favorizes orbital effects and reduces the critical magnetic field. The prismatic geometry allows the Majorana zero-energy modes to be accompanied by low-energy states, which we call pseudo Majorana, and which converge to real Majoranas in the limit of small shell thickness. We include the Rashba spin-orbit coupling in a phenomenological manner, assuming a radial electric field across the shell.

  8. Adsorption of Small Cationic Nanoparticles onto Large Anionic Particles from Aqueous Solution: A Model System for Understanding Pigment Dispersion and the Problem of Effective Particle Density.

    PubMed

    North, S M; Jones, E R; Smith, G N; Mykhaylyk, O O; Annable, T; Armes, S P

    2017-02-07

    The present study focuses on the use of copolymer nanoparticles as a dispersant for a model pigment (silica). Reversible addition-fragmentation chain transfer (RAFT) alcoholic dispersion polymerization was used to synthesize sterically stabilized diblock copolymer nanoparticles. The steric stabilizer block was poly(2-(dimethylamino)ethyl methacrylate) (PDMA) and the core-forming block was poly(benzyl methacrylate) (PBzMA). The mean degrees of polymerization for the PDMA and PBzMA blocks were 71 and 100, respectively. Transmission electron microscopy (TEM) studies confirmed a near-monodisperse spherical morphology, while dynamic light scattering (DLS) studies indicated an intensity-average diameter of 30 nm. Small-angle X-ray scattering (SAXS) reported a volume-average diameter of 29 ± 0.5 nm and a mean aggregation number of 154. Aqueous electrophoresis measurements confirmed that these PDMA 71 -PBzMA 100 nanoparticles acquired cationic character when transferred from ethanol to water as a result of protonation of the weakly basic PDMA chains. Electrostatic adsorption of these nanoparticles from aqueous solution onto 470 nm silica particles led to either flocculation at submonolayer coverage or steric stabilization at or above monolayer coverage, as judged by DLS. This technique indicated that saturation coverage was achieved on addition of approximately 465 copolymer nanoparticles per silica particle, which corresponds to a fractional surface coverage of around 0.42. These adsorption data were corroborated using thermogravimetry, UV spectroscopy and X-ray photoelectron spectroscopy. TEM studies indicated that the cationic nanoparticles remained intact on the silica surface after electrostatic adsorption, while aqueous electrophoresis confirmed that surface charge reversal occurred below pH 7. The relatively thick layer of adsorbed nanoparticles led to a significant reduction in the effective particle density of the silica particles from 1.99 g cm -3 to approximately 1.74 g cm -3 , as judged by disk centrifuge photosedimentometry (DCP). Combining the DCP and SAXS data suggests that essentially no deformation of the PBzMA cores occurs during nanoparticle adsorption onto the silica particles.

  9. Self-expanding Portico Valve Versus Balloon-expandable SAPIEN XT Valve in Patients With Small Aortic Annuli: Comparison of Hemodynamic Performance.

    PubMed

    Del Trigo, María; Dahou, Abdellaziz; Webb, John G; Dvir, Danny; Puri, Rishi; Abdul-Jawad Altisent, Omar; Campelo-Parada, Francisco; Thompson, Chris; Leipsic, Jonathon; Stub, Dion; DeLarochellière, Robert; Paradis, Jean-Michel; Dumont, Eric; Doyle, Daniel; Mohammadi, Siamak; Pasian, Sergio; Côté, Melanie; Pibarot, Philippe; Rodés-Cabau, Josep

    2016-05-01

    The self-expanding Portico valve is a new transcatheter aortic valve system yielding promising preliminary results, yet there are no comparative data against earlier generation transcatheter aortic valve systems. The aim of this study was to compare the hemodynamic performance of the Portico and balloon-expandable SAPIEN XT valves in a case-matched study with echocardiographic core laboratory analysis. Twenty-two patients underwent transcatheter aortic valve implantation with the Portico 23-mm valve and were matched for aortic annulus area and mean diameter measured by multidetector computed tomography, left ventricular ejection fraction, body surface area, and body mass index with 40 patients treated with the 23-mm SAPIEN XT. Mean aortic annulus diameters were 19.6±1.3mm by transthoracic echocardiography and 21.4±1.2mm by computed tomography, with no significant between-group differences. Doppler echocardiographic images were collected at baseline and at 1-month of follow-up and were analyzed in a central echocardiography core laboratory. There were no significant between-group differences in residual mean transaortic gradients (SAPIEN XT: 10.4±3.7mmHg; Portico: 9.8±1.1mmHg; P=.49) and effective orifice areas (SAPIEN XT: 1.36±0.27cm(2); Portico, 1.37±.29cm(2); P=.54). Rates of severe prosthesis-patient mismatch (effective orifice area<0.65cm(2)/m(2)) were similar (SAPIEN XT: 13.5%; Portico: 10.0%; P=.56). No between-group differences were found in the occurrence of moderate-severe paravalvular leaks (5.0% vs 4.8% of SAPIEN XT and Portico respectively; P=.90). Transcatheter aortic valve implantation with the self-expanding Portico system yielded similar short-term hemodynamic performance compared with the balloon-expandable SAPIEN XT system for treating patients with severe aortic stenosis and small annuli. Further prospective studies with longer-term follow-up and in patients with larger aortic annuli are required. Copyright © 2015 Sociedad Española de Cardiología. Published by Elsevier España, S.L.U. All rights reserved.

  10. Design of a Phase /Doppler Light-Scattering System for Measurement of Small-Diameter Glass Fibers During Fiberglass Manufacturing

    NASA Astrophysics Data System (ADS)

    Schaub, Scott A.; Naqwi, Amir A.; Harding, Foster L.

    1998-01-01

    We present fundamental studies examining the design of a phase /Doppler laser light-scattering system applicable to on-line measurements of small-diameter ( <15 m) fibers during fiberglass manufacturing. We first discuss off-line diameter measurement techniques currently used in the fiberglass industry and outline the limitations and problems associated with these methods. For the phase /Doppler design study we have developed a theoretical computer model for the response of the measurement system to cylindrical fibers, which is based on electromagnetic scattering theory. The model, valid for arbitrary fiber diameters and hardware configurations, generates simulated detector output as a function of time for a finite absorbing, cylindrical fiber oriented perpendicular to the two incident laser beams. Results of experimental measurements are presented, confirming predictions of the theoretical model. Parametric studies have also been conducted using the computer model to identify experimental arrangements that provide linear phase -diameter relationships for small-diameter fibers, within the measurement constraints imposed by the fiberglass production environment. The effect of variations in optical properties of the glass as well as fiber orientation effects are discussed. Through this research we have identified phase /Doppler arrangements that we expect to have future applications in the fiberglass industry for on-line diameter monitoring and process control.

  11. Design of a phase/doppler light-scattering system for measurement of small-diameter glass fibers during fiberglass manufacturing.

    PubMed

    Schaub, S A; Naqwi, A A; Harding, F L

    1998-01-20

    We present fundamental studies examining the design of a phase/Doppler laser light-scattering system applicable to on-line measurements of small-diameter (<15 mum) fibers during fiberglass manufacturing. We first discuss off-line diameter measurement techniques currently used in the fiberglass industry and outline the limitations and problems associated with these methods. For the phase/Doppler design study we have developed a theoretical computer model for the response of the measurement system to cylindrical fibers, which is based on electromagnetic scattering theory. The model, valid for arbitrary fiber diameters and hardware configurations, generates simulated detector output as a function of time for a finite absorbing, cylindrical fiber oriented perpendicular to the two incident laser beams. Results of experimental measurements are presented, confirming predictions of the theoretical model. Parametric studies have also been conducted using the computer model to identify experimental arrangements that provide linear phase-diameter relationships for small-diameter fibers, within the measurement constraints imposed by the fiberglass production environment. The effect of variations in optical properties of the glass as well as fiber orientation effects are discussed. Through this research we have identified phase/Doppler arrangements that we expect to have future applications in the fiberglass industry for on-line diameter monitoring and process control.

  12. Measured Performance of a Varied Airflow Small-Diameter Duct System

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Poerschke, Andrew

    2017-03-01

    This study tests the performance of a variable airflow small-diameter duct heating, ventilation, and air conditioning (HVAC) system in a new construction unoccupied low-load test house in Pittsburgh, Pennsylvania. The duct system was installed entirely in conditioned space and was operated from the winter through summer seasons. Measurements were collected on the in-room temperatures and energy consumed by the air handler and heat pump unit. Operation modes with three different volumes of airflow were compared to determine the ideal airflow scenario that maximizes room-to-room thermal uniformity while minimizing fan energy consumption. Black felt infrared imagery was used as a measuremore » of diffuser throw and in-room air mixing. Measured results indicate the small-diameter, high velocity airflow system can provide comfort under some conditions. Solar heat gains resulted in southern rooms drifting beyond acceptable temperature limits. Insufficient airflow to some bedrooms also resulted in periods of potential discomfort. Homebuilders or HVAC contractors can use these results to assess whether this space conditioning strategy is an attractive alternative to a traditional duct system. The team performed a cost analysis of two duct system configurations: (1) a conventional diameter and velocity duct system, and (2) the small-diameter duct system. This work applies to both new and retrofit homes that have achieved a low heating and cooling density either by energy conservation or by operation in a mild climate with few heating or cooling degree days. Guidance is provided on cost trade-offs between the conventional duct system and the small-diameter duct system.« less

  13. Measured Performance of a Varied Airflow Small-Diameter Duct System

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Poerschke, Andrew

    This study tests the performance of a variable airflow small-diameter duct heating, ventilation, and air conditioning (HVAC) system in a new construction unoccupied low-load test house in Pittsburgh, Pennsylvania. The duct system was installed entirely in conditioned space and was operated from the winter through summer seasons. Measurements were collected on the in-room temperatures and energy consumed by the air handler and heat pump unit. Operation modes with three different volumes of airflow were compared to determine the ideal airflow scenario that maximizes room-to-room thermal uniformity while minimizing fan energy consumption. Black felt infrared imagery was used as a measuremore » of diffuser throw and in-room air mixing. Measured results indicate the small-diameter, high velocity airflow system can provide comfort under some conditions. Solar heat gains resulted in southern rooms drifting beyond acceptable temperature limits. Insufficient airflow to some bedrooms also resulted in periods of potential discomfort. Homebuilders or HVAC contractors can use these results to assess whether this space conditioning strategy is an attractive alternative to a traditional duct system. The team performed a cost analysis of two duct system configurations: (1) a conventional diameter and velocity duct system, and (2) the small-diameter duct system. This work applies to both new and retrofit homes that have achieved a low heating and cooling density either by energy conservation or by operation in a mild climate with few heating or cooling degree days. Guidance is provided on cost trade-offs between the conventional duct system and the small-diameter duct system.« less

  14. Building America Case Study: High-Velocity Small-Diameter Duct System, Pittsburgh, Pennsylvania

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    A. Poerschke

    This study tests the performance of a variable airflow small-diameter duct heating, ventilation, and air conditioning (HVAC) system in a new construction unoccupied low-load test house in Pittsburgh, Pennsylvania. The duct system was installed entirely in conditioned space and was operated from the winter through summer seasons. Measurements were collected on the in-room temperatures and energy consumed by the air handler and heat pump unit. Operation modes with three different volumes of airflow were compared to determine the ideal airflow scenario that maximizes room-to-room thermal uniformity while minimizing fan energy consumption. Black felt infrared imagery was used as a measuremore » of diffuser throw and in-room air mixing. Measured results indicate the small-diameter, high velocity airflow system can provide comfort under some conditions. Solar heat gains resulted in southern rooms drifting beyond acceptable temperature limits. Insufficient airflow to some bedrooms also resulted in periods of potential discomfort. Homebuilders or HVAC contractors can use these results to assess whether this space conditioning strategy is an attractive alternative to a traditional duct system. The team performed a cost analysis of two duct system configurations: (1) a conventional diameter and velocity duct system, and (2) the small-diameter duct system. This work applies to both new and retrofit homes that have achieved a low heating and cooling density either by energy conservation or by operation in a mild climate with few heating or cooling degree days. Guidance is provided on cost trade-offs between the conventional duct system and the small-diameter duct system.« less

  15. Fabrication of micro-alginate gel tubes utilizing micro-gelatin fibers

    NASA Astrophysics Data System (ADS)

    Sakaguchi, Katsuhisa; Arai, Takafumi; Shimizu, Tatsuya; Umezu, Shinjiro

    2017-05-01

    Tissues engineered utilizing biofabrication techniques have recently been the focus of much attention, because these bioengineered tissues have great potential to improve the quality of life of patients with various hard-to-treat diseases. Most tissues contain micro-tubular structures including blood vessels, lymphatic vessels, and bile canaliculus. Therefore, we bioengineered a micro diameter tube using alginate gel to coat the core gelatin gel. Micro-gelatin fibers were fabricated by the coacervation method and then coated with a very thin alginate gel layer by dipping. A micro diameter alginate tube was produced by dissolving the core gelatin gel. Consequently, these procedures led to the formation of micro-alginate gel tubes of various shapes and sizes. This biofabrication technique should contribute to tissue engineering research fields.

  16. Crash testing of Louisiana's 3 1/2" diameter multi-directional, single steel post, small sign support : final report.

    DOT National Transportation Integrated Search

    1993-03-01

    The Louisiana Department of Transportation and Development (LDOTD) contracted with the Texas Transportation Institute (TTI) to evaluate the impact characteristics of Louisiana's multi-directional, 8.9 cm (3-1/2 in) diameter steel post, small sigh sup...

  17. Radiation collimator and systems incorporating same

    DOEpatents

    Norman, Daren R [Idaho Falls, ID; Yoon, Woo Y [Idaho Falls, ID; Jones, James L [Idaho Falls, ID; Haskell, Kevin J [Idaho Falls, ID; Bennett, Brion D [Idaho Falls, ID; Tschaggeny, Charles W [Woods Cross, UT; Jones, Warren F [Idaho Falls, ID

    2011-09-13

    A collimator including a housing having disposed therein a shield element surrounding a converter core in which a photon beam is generated from electrons emanating from a linear accelerator. A beam channeler longitudinally adjacent the shield element has a beam aperture therethrough coaxially aligned with, and of the same diameter as, an exit bore of the converter core. A larger entry bore in the converter core is coaxial with, and longitudinally separated from, the exit bore thereof. Systems incorporating the collimator are also disclosed.

  18. Brittle Materials Design, High Temperature Gas Turbine

    DTIC Science & Technology

    1981-03-01

    slides and core pins which formed the outer diameter and the hollow struts. Inner inserts were used to form the inside surface of the nose cone...ceramic component development. Figure 1 illustrates this by showing, in turn, ready removal in the test cell of a ceramic regenerator core , combusior...objective. This Executive Summary briefly reviews the highlights of the program. VII ■■■ *»W*w»«»^il»^.3«£*a;-^ -,Al^».t, „ . Regenerator Core Removal

  19. Photonic bandgap single-mode optical fibre with ytterbium-doped silica glass core

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Egorova, O N; Semenov, S L; Vel'miskin, V V

    2011-01-24

    A photonic bandgap fibre with an ytterbium-doped silica glass core is fabricated and investigated. The possibility of implementing single-mode operation of such fibres in a wide spectral range at a large (above 20 {mu}m) mode field diameter makes them promising for fibre lasers and amplifiers. To ensure a high quality of the beam emerging from the fibre, particular attention is paid to increasing the optical homogeneity of the ytterbium-doped core glass. (optical fibres)

  20. Stratigraphy of the Apollo 15 drill core

    NASA Technical Reports Server (NTRS)

    Heiken, G.; Duke, M.; Fryxell, R.; Nagle, J. S.; Scott, R.; Sellers, G. A.

    1972-01-01

    The crew of Apollo 15 collected at 242-centimeter-long core of the regolith of the moon developed on the surface of Palus Putredinis 3 deg 39 min 20 sec E, 26 deg 26 min 00 sec N. The 2.04-centimeter-diameter core, which has a mass of 1333.2 grams, consists of 42 major textural units, with thicknesses ranging from a few milliliters to 13 centimeters thick. The regolith is not homogeneous and is composed of many layers that are mostly ejecta from impact events.

  1. Quantized orbits in weakly coupled Belousov-Zhabotinsky reactors

    NASA Astrophysics Data System (ADS)

    Weiss, S.; Deegan, R. D.

    2015-06-01

    Using numerical and experimental tools, we study the motion of two coupled spiral cores in a light-sensitive variant of the Belousov-Zhabotinsky reaction. Each core resides on a separate two-dimensional domain, and is coupled to the other by light. When both spirals have the same sense of rotation, the cores are attracted to a circular trajectory with a diameter quantized in integer units of the spiral wavelength λ. When the spirals have opposite senses of rotation, the cores are attracted towards different but parallel straight trajectories, separated by an integer multiple of λ/2. We present a model that explains this behavior as the result of a spiral wavefront-core interaction that produces a deterministic displacement of the core and a retardation of its phase.

  2. Micropillar Compression Technique Applied to Micron-Scale Mudstone Elasto-Plastic Deformation

    NASA Astrophysics Data System (ADS)

    Dewers, T. A.; Boyce, B.; Buchheit, T.; Heath, J. E.; Chidsey, T.; Michael, J.

    2010-12-01

    Mudstone mechanical testing is often limited by poor core recovery and sample size, preservation and preparation issues, which can lead to sampling bias, damage, and time-dependent effects. A micropillar compression technique, originally developed by Uchic et al. 2004, here is applied to elasto-plastic deformation of small volumes of mudstone, in the range of cubic microns. This study examines behavior of the Gothic shale, the basal unit of the Ismay zone of the Pennsylvanian Paradox Formation and potential shale gas play in southeastern Utah, USA. Precision manufacture of micropillars 5 microns in diameter and 10 microns in length are prepared using an ion-milling method. Characterization of samples is carried out using: dual focused ion - scanning electron beam imaging of nano-scaled pores and distribution of matrix clay and quartz, as well as pore-filling organics; laser scanning confocal (LSCM) 3D imaging of natural fractures; and gas permeability, among other techniques. Compression testing of micropillars under load control is performed using two different nanoindenter techniques. Deformation of 0.5 cm in diameter by 1 cm in length cores is carried out and visualized by a microscope loading stage and laser scanning confocal microscopy. Axisymmetric multistage compression testing and multi-stress path testing is carried out using 2.54 cm plugs. Discussion of results addresses size of representative elementary volumes applicable to continuum-scale mudstone deformation, anisotropy, and size-scale plasticity effects. Other issues include fabrication-induced damage, alignment, and influence of substrate. This work is funded by the US Department of Energy, Office of Basic Energy Sciences. Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed Martin Company, for the United States Department of Energy’s National Nuclear Security Administration under contract DE-AC04-94AL85000.

  3. Accuracy study of computer-assisted drilling: the effect of bone density, drill bit characteristics, and use of a mechanical guide.

    PubMed

    Hüfner, T; Geerling, J; Oldag, G; Richter, M; Kfuri, M; Pohlemann, T; Krettek, C

    2005-01-01

    This study was designed to determine the clinical relevant accuracy of CT-based navigation for drilling. Experimental model. Laboratory. Twelve drills of varying lengths and diameters were tested with 2 different set-ups. Group 1 used free-hand navigated drilling technique with foam blocks equipped with titanium target points. Group 2 (control) used a newly developed 3-dimensional measurement device equipped with titanium target points with a fixed entry for the navigated drill to minimize bending forces. One examiner performed 690 navigated drillings using solely the monitor screen for control in both groups. The difference between the planned and the actual starting and target point (up to 150 mm distance) was measured (mm). Levene test and a nonpaired t test. Significance level was set as P < 0.05. The core accuracy of the navigation system measured with the 3-dimensional device was 0.5 mm. The mean distance from planned to actual entry points in group 1 was 1.3 (range, 0.6-3.4 mm). The mean distance between planned and actual target point was 3.4 (range, 1.7-5.8 mm). Free-hand navigated drilling showed an increased difference with increased length of the drill bits as well as with increased drilling channel for drill bits 2.5 and 3.2 mm and not for 3.5 and 4.5 mm (P < 0.05). The core accuracy of the navigation system is high. Compared with the navigated free-hand technique, the results suggest that drill bit deflection interferes directly with the precision. The precision is decreased when using small diameter and longer drill bits.

  4. Historical ecology of the northern Adriatic Sea: Field methods and coring device

    NASA Astrophysics Data System (ADS)

    Haselmair, Alexandra; Gallmetzer, Ivo; Tomasovych, Adam; Stachowitsch, Michael; Zuschin, Martin

    2014-05-01

    For an ongoing study on the historical ecology of the northern Adriatic Sea, the objective was to retrieve a high number of sediment cores at seven sampling stations spread across the entire basin. One set of cores is intended for sediment analyses including radiometric Pb-sediment-dating, grain size, TOC, TAC and heavy metal analyses. The other set of cores delivered enough shelly remains of endo- or epibenthic hard part producers (e.g. molluscs, crustaceans, echinoderms) to enable the reconstruction of death assemblages in core layers from top to bottom. The down-core changes of such assemblages record ecological shifts in a marine environment that has endured strong human impacts over several centuries. A 1.5 m-long core could, according to the available sedimentation data for the area, cover up to 2000 or even more years of ecological history. The coring method had to meet the following requirements: a) deliver 1.5-m-long cores from different sediment settings (mud to sand, reflecting a wide range of benthic habitats in the northern Adriatic); b) enable quick and easy deployment to ensure that multiple cores can be taken at the individual sampling stations within a short time; c) be relatively affordable and allow handling by the researchers themselves, potentially using a small vessel in order to further contain the operating costs. Two types of UWITEC™ piston corers were used to meet these requirements. A model with 90 mm of diameter (samples for sediment analysis) and another one with 160 mm, specifically designed to obtain the large amount of material needed for shell analysis, successfully delivered a total of 54 cores. The device consists of a stabilizing tripod and the interchangeable coring cylinders. It is equipped with a so-called hammer action that makes it possible, at least for the smaller cylinder, to penetrate even harder sediments. A closing mechanism of the corer retains the sediment in the cylinder upon extraction; it works either automatically through hydraulic pressure once the final core-length is reached, or can be triggered manually anytime from the surface using a connected hose and water pump. The whole coring device weighs less than 300 kg and can readily be transported in a van. It can easily be assembled, disassembled and operated by two to three persons after a brief training. With a newly designed, very simple and effective slicing device, the cores can be sliced in an upright position directly on board after extraction. This type of corer can be highly recommended for any smaller coring operations on lakes, streams, or at sea.

  5. Assessing the accuracy of using oscillating gradient spin echo sequences with AxCaliber to infer micron-sized axon diameters.

    PubMed

    Mercredi, Morgan; Vincent, Trevor J; Bidinosti, Christopher P; Martin, Melanie

    2017-02-01

    Current magnetic resonance imaging (MRI) axon diameter measurements rely on the pulsed gradient spin-echo sequence, which is unable to provide diffusion times short enough to measure small axon diameters. This study combines the AxCaliber axon diameter fitting method with data generated from Monte Carlo simulations of oscillating gradient spin-echo sequences (OGSE) to infer micron-sized axon diameters, in order to determine the feasibility of using MRI to infer smaller axon diameters in brain tissue. Monte Carlo computer simulation data were synthesized from tissue geometries of cylinders of different diameters using a range of gradient frequencies in the cosine OGSE sequence . Data were fitted to the AxCaliber method modified to allow the new pulse sequence. Intra- and extra-axonal water were studied separately and together. The simulations revealed the extra-axonal model to be problematic. Rather than change the model, we found that restricting the range of gradient frequencies such that the measured apparent diffusion coefficient was constant over that range resulted in more accurate fitted diameters. Thus a careful selection of frequency ranges is needed for the AxCaliber method to correctly model extra-axonal water, or adaptations to the method are needed. This restriction helped reduce the necessary gradient strengths for measurements that could be performed with parameters feasible for a Bruker BG6 gradient set. For these experiments, the simulations inferred diameters as small as 0.5 μm on square-packed and randomly packed cylinders. The accuracy of the inferred diameters was found to be dependent on the signal-to-noise ratio (SNR), with smaller diameters more affected by noise, although all diameter distributions were distinguishable from one another for all SNRs tested. The results of this study indicate the feasibility of using MRI with OGSE on preclinical scanners to infer small axon diameters.

  6. Small-diameter utilization issues and opportunities

    Treesearch

    John Rusty Dramm

    1999-01-01

    This presentation provides a thought-provoking look at options for utilizing small- diameter wood to help reduce the widespread risk of catastrophic wildfire throughout the West while providing economic recovery of timber-depressed communities and sustaining viable forest products industry. Potentially viable utilization and marketing options are explored and current...

  7. Diffusion Raman stimulée à trois ondes dans une fibre optique.

    PubMed

    Saissy, A; Botineau, J; Azema, A; Gires, F

    1980-05-15

    Three-wave stimulated Raman scattering in optical fibers has been studied theoretically in connection with the characteristics of the fiber (core diameter, core-cladding refractive-index difference) and excitation conditions. We observe experimentally this type of scattering in a silica fiber, from which we can estimate the nonlinearity of silica and the index difference of the fiber.

  8. Generation of a mesoporous silica MSU shell onto solid core silica nanoparticles using a simple two-step sol-gel process.

    PubMed

    Allouche, Joachim; Dupin, Jean-Charles; Gonbeau, Danielle

    2011-07-14

    Silica core-shell nanoparticles with a MSU shell have been synthesized using several non-ionic poly(ethylene oxide) based surfactants via a two step sol-gel method. The materials exhibit a typical worm-hole pore structure and tunable pore diameters between 2.4 nm and 5.8 nm.

  9. Raccoon spatial requirements and multi-scale habitat selection within an intensively managed central Appalachian forest

    USGS Publications Warehouse

    Owen, Sheldon F.; Berl, Jacob L.; Edwards, John W.; Ford, W. Mark; Wood, Petra Bohall

    2015-01-01

    We studied a raccoon (Procyon lotor) population within a managed central Appalachian hardwood forest in West Virginia to investigate the effects of intensive forest management on raccoon spatial requirements and habitat selection. Raccoon home-range (95% utilization distribution) and core-area (50% utilization distribution) size differed between sexes with males maintaining larger (2×) home ranges and core areas than females. Home-range and core-area size did not differ between seasons for either sex. We used compositional analysis to quantify raccoon selection of six different habitat types at multiple spatial scales. Raccoons selected riparian corridors (riparian management zones [RMZ]) and intact forests (> 70 y old) at the core-area spatial scale. RMZs likely were used by raccoons because they provided abundant denning resources (i.e., large-diameter trees) as well as access to water. Habitat composition associated with raccoon foraging locations indicated selection for intact forests, riparian areas, and regenerating harvest (stands <10 y old). Although raccoons were able to utilize multiple habitat types for foraging resources, a selection of intact forest and RMZs at multiple spatial scales indicates the need of mature forest (with large-diameter trees) for this species in managed forests in the central Appalachians.

  10. Lunar deep drill apparatus

    NASA Technical Reports Server (NTRS)

    Harvey, Jill (Editor)

    1989-01-01

    A self contained, mobile drilling and coring system was designed to operate on the Lunar surface and be controlled remotely from earth. The system uses SKITTER (Spatial Kinematic Inertial Translatory Tripod Extremity Robot) as its foundation and produces Lunar core samples two meters long and fifty millimeters in diameter. The drill bit used for this is composed of 30 per carat diamonds in a sintered tungsten carbide matrix. To drill up to 50 m depths, the bit assembly will be attached to a drill string made from 2 m rods which will be carried in racks on SKITTER. Rotary power for drilling will be supplied by a Curvo-Synchronous motor. SKITTER is to support this system through a hexagonal shaped structure which will contain the drill motor and the power supply. A micro-coring drill will be used to remove a preliminary sample 5 mm in diameter and 20 mm long from the side of the core. This whole system is to be controlled from earth. This is carried out by a continuously monitoring PLC onboard the drill rig. A touch screen control console allows the operator on earth to monitor the progress of the operation and intervene if necessary.

  11. Multicore photonic crystal fiber force meters

    NASA Astrophysics Data System (ADS)

    Reimlinger, M.; Colalillo, A.; Coompson, J.; Wynne, R.

    2011-04-01

    A silica based three core photonic crystal fiber (PCF) force meter with fast response times (<30μs) for low wind speed detection is presented. Results are provided for PCF structures containing cores with varied lattice spacing. Force meters with high spatial resolution (sample regions <10cm) specially outfitted for extreme environmental conditions are of interest to both industry and basic research institutions. The featured PCF force meter exhibited sensitivities that agreed with theoretical predictions that are useful for the detection of minimum displacements for wind speeds <30m/s. The results of this investigation are relevant to civil engineering applications including urban sensing technologies that involve air quality monitoring. The deflection of the PCF detection interface was measured as a function of the fiber deflection or the applied force (e.g. wind speed). The three core PCF has a core diameter of 3.9μm, outer diameter of 132.5μm and 7.56μm core-core spacing. A 4cm length of the PCF is attached to the surface of a thin metal beam. One end of the PCF section is fusion spliced to a single mode fiber (SMF) at the fiber input. The remaining fiber end is coupled to a CCD camera with a lens at the PCF output. The applied force deflects the supported PCF such that the intensity distribution of the optical field for the multiple cores changes as a function of displacement. Experimental results from static deflection measurements are in agreement with coupled-mode theory and simple beam deflection theory models.

  12. The Effect of Luting Cement and Titanium Base on the Final Color of Zirconium Oxide Core Material.

    PubMed

    Capa, Nuray; Tuncel, Ilkin; Tak, Onjen; Usumez, Aslihan

    2017-02-01

    To evaluate the effects of different types of luting cements and different colors of zirconium cores on the final color of the restoration that simulates implant-supported fixed partial dentures (FPDs) by using a titanium base on the bottom. One hundred and twenty zirconium oxide core plates (Zr-Zahn; 10 mm in width, 5 mm in length, 0.5 mm in height) were prepared in different shades (n = 20; noncolored, A2, A3, B1, C2, D2). The specimens were subdivided into two subgroups for the two types of luting cements (n = 10). The initial color measurements were made on zirconium oxide core plates using a spectrometer. To create the cement thicknesses, stretch strips with holes in the middle (5 mm in diameter, 70 μm in height) were used. The second measurement was done on the zirconium oxide core plates after the application of the resin cement (U-200, A2 Shade) or polycarboxylate cement (Lumicon). The final measurement was done after placing the titanium discs (5 mm in diameter, 3 mm in height) in the bottom. The data were analyzed with two-way ANOVA and Tukey's honestly significant differences (HSD) tests (α = 0.05). The ∆E* ab value was higher in the resin cement-applied group than in the polycarboxylate cement-applied group (p < 0.001). The highest ∆E* ab value was recorded for the zirconium oxide core-resin cement-titanium base, and the lowest was recorded for the polycarboxylate cement-zirconium oxide core (p < 0.001). The luting cement, the presence of titanium, and the color of zirconium are all important factors that determine the final shade of zirconia cores in implant-supported FPDs. © 2015 by the American College of Prosthodontists.

  13. Effect of hole geometry and Electric-Discharge Machining (EDM) on airflow rates through small diameter holes in turbine blade material

    NASA Technical Reports Server (NTRS)

    Hippensteele, S. A.; Cochran, R. P.

    1980-01-01

    The effects of two design parameters, electrode diameter and hole angle, and two machine parameters, electrode current and current-on time, on air flow rates through small-diameter (0.257 to 0.462 mm) electric-discharge-machined holes were measured. The holes were machined individually in rows of 14 each through 1.6 mm thick IN-100 strips. The data showed linear increase in air flow rate with increases in electrode cross sectional area and current-on time and little change with changes in hole angle and electrode current. The average flow-rate deviation (from the mean flow rate for a given row) decreased linearly with electrode diameter and increased with hole angle. Burn time and finished hole diameter were also measured.

  14. Coordinate measuring machine test standard apparatus and method

    DOEpatents

    Bieg, L.F.

    1994-08-30

    A coordinate measuring machine test standard apparatus and method are disclosed which includes a rotary spindle having an upper phase plate and an axis of rotation, a kinematic ball mount attached to the phase plate concentric with the axis of rotation of the phase plate, a groove mounted at the circumference of the phase plate, and an arm assembly which rests in the groove. The arm assembly has a small sphere at one end and a large sphere at the other end. The small sphere may be a coordinate measuring machine probe tip and may have variable diameters. The large sphere is secured in the kinematic ball mount and the arm is held in the groove. The kinematic ball mount includes at least three mounting spheres and the groove is an angular locating groove including at least two locking spheres. The arm may have a hollow inner core and an outer layer. The rotary spindle may be a ratio reducer. The device is used to evaluate the measuring performance of a coordinate measuring machine for periodic recertification, including 2 and 3 dimensional accuracy, squareness, straightness, and angular accuracy. 5 figs.

  15. Coordinate measuring machine test standard apparatus and method

    DOEpatents

    Bieg, Lothar F.

    1994-08-30

    A coordinate measuring machine test standard apparatus and method which iudes a rotary spindle having an upper phase plate and an axis of rotation, a kinematic ball mount attached to the phase plate concentric with the axis of rotation of the phase plate, a groove mounted at the circumference of the phase plate, and an arm assembly which rests in the groove. The arm assembly has a small sphere at one end and a large sphere at the other end. The small sphere may be a coordinate measuring machine probe tip and may have variable diameters. The large sphere is secured in the kinematic ball mount and the arm is held in the groove. The kinematic ball mount includes at least three mounting spheres and the groove is an angular locating groove including at least two locking spheres. The arm may have a hollow inner core and an outer layer. The rotary spindle may be a ratio reducer. The device is used to evaluate the measuring performance of a coordinate measuring machine for periodic recertification, including 2 and 3 dimensional accuracy, squareness, straightness, and angular accuracy.

  16. Microfluidic based high throughput synthesis of lipid-polymer hybrid nanoparticles with tunable diameters

    PubMed Central

    Feng, Qiang; Zhang, Lu; Liu, Chao; Li, Xuanyu; Hu, Guoqing; Sun, Jiashu; Jiang, Xingyu

    2015-01-01

    Core-shell hybrid nanoparticles (NPs) for drug delivery have attracted numerous attentions due to their enhanced therapeutic efficacy and good biocompatibility. In this work, we fabricate a two-stage microfluidic chip to implement a high-throughput, one-step, and size-tunable synthesis of mono-disperse lipid-poly (lactic-co-glycolic acid) NPs. The size of hybrid NPs is tunable by varying the flow rates inside the two-stage microfluidic chip. To elucidate the mechanism of size-controllable generation of hybrid NPs, we observe the flow field in the microchannel with confocal microscope and perform the simulation by a numerical model. Both the experimental and numerical results indicate an enhanced mixing effect at high flow rate, thus resulting in the assembly of small and mono-disperse hybrid NPs. In vitro experiments show that the large hybrid NPs are more likely to be aggregated in serum and exhibit a lower cellular uptake efficacy than the small ones. This microfluidic chip shows great promise as a robust platform for optimization of nano drug delivery system. PMID:26180574

  17. Multi-wavelength photoacoustic system based on high-power diode laser bars

    NASA Astrophysics Data System (ADS)

    Leggio, Luca; Wiśniowski, Bartosz; Gawali, Sandeep Babu; Rodríguez, Sergio; Sánchez, Miguel; Gallego, Daniel; Carpintero, Guillermo; Lamela, Horacio

    2017-03-01

    Multi-wavelength laser sources are necessary for a functional photoacoustic (PA) spectroscopy. The use of high-power diode lasers (HPDLs) has aroused great interest for their relatively low costs and small sizes if compared to solid state lasers. However, HPDLs are only available at few wavelengths and can deliver low optical energy (normally in the order of μJ), while diode laser bars (DLBs) offer more wavelengths in the market and can deliver more optical energy. We show the simulations of optical systems for beam coupling of single high-power DLBs operating at different wavelengths (i.e. 808 nm, 880 nm, 910 nm, 940 nm, and 980 nm) into 400-μm optical fibers. Then, in a separate design, the beams of the DLBs are combined in a compact system making use of dichroic mirrors and focusing lenses for beam coupling into a 400-μm optical fiber. The use of optical fibers with small core diameter (< 1 mm) is particularly suggestive for future photoacoustic endoscopy (PAE) applications that require interior examination of the body.

  18. Assessment of In-Stent Restenosis Using 64-MDCT: Analysis of the CORE-64 Multicenter International Trial

    PubMed Central

    Wykrzykowska, Joanna J.; Arbab-Zadeh, Armin; Godoy, Gustavo; Miller, Julie M.; Lin, Shezhang; Vavere, Andrea; Paul, Narinder; Niinuma, Hiroyuki; Hoe, John; Brinker, Jeffrey; Khosa, Faisal; Sarwar, Sheryar; Lima, Joao; Clouse, Melvin E.

    2012-01-01

    OBJECTIVE Evaluations of stents by MDCT from studies performed at single centers have yielded variable results with a high proportion of unassessable stents. The purpose of this study was to evaluate the accuracy of 64-MDCT angiography (MDCTA) in identifying in-stent restenosis in a multicenter trial. MATERIALS AND METHODS The Coronary Evaluation Using Multidetector Spiral Computed Tomography Angiography Using 64 Detectors (CORE-64) Multicenter Trial and Registry evaluated the accuracy of 64-MDCTA in assessing 405 patients referred for coronary angiography. A total of 75 stents in 52 patients were assessed: 48 of 75 stents (64%) in 36 of 52 patients (69%) could be evaluated. The prevalence of in-stent restenosis by quantitative coronary angiography (QCA) in this subgroup was 23% (17/75). Eighty percent of the stents were ≤ 3.0 mm in diameter. RESULTS The overall sensitivity, specificity, positive predictive value, and negative predictive value to detect 50% in-stent stenosis visually using MDCT compared with QCA was 33.3%, 91.7%, 57.1%, and 80.5%, respectively, with an overall accuracy of 77.1% for the 48 assessable stents. The ability to evaluate stents on MDCTA varied by stent type: Thick-strut stents such as Bx Velocity were assessable in 50% of the cases; Cypher, 62.5% of the cases; and thinner-strut stents such as Taxus, 75% of the cases. We performed quantitative assessment of in-stent contrast attenuation in Hounsfield units and correlated that value with the quantitative percentage of stenosis by QCA. The correlation coefficient between the average attenuation decrease and ≥ 50% stenosis by QCA was 0.25 (p = 0.073). Quantitative assessment failed to improve the accuracy of MDCT over qualitative assessment. CONCLUSION The results of our study showed that 64-MDCT has poor ability to detect in-stent restenosis in small-diameter stents. Evaluability and negative predictive value were better in large-diameter stents. Thus, 64-MDCT may be appropriate for stent assessment in only selected patients. PMID:20028909

  19. Miniature ball-tip optical fibers for use in thulium fiber laser ablation of kidney stones

    NASA Astrophysics Data System (ADS)

    Wilson, Christopher R.; Hardy, Luke A.; Kennedy, Joshua D.; Irby, Pierce B.; Fried, Nathaniel M.

    2016-01-01

    Optical fibers, consisting of 240-μm-core trunk fibers with rounded, 450-μm-diameter ball tips, are currently used during Holmium:YAG laser lithotripsy to reduce mechanical damage to the inner lining of the ureteroscope working channel during fiber insertion and prolong ureteroscope lifetime. Similarly, this study tests a smaller, 100-μm-core fiber with 300-μm-diameter ball tip during thulium fiber laser (TFL) lithotripsy. TFL was operated at a wavelength of 1908 nm, with 35-mJ pulse energy, 500-μs pulse duration, and 300-Hz pulse rate. Calcium oxalate/phosphate stone samples were weighed, laser procedure times were measured, and ablation rates were calculated for ball tip fibers, with comparison to bare tip fibers. Photographs of ball tips were taken before and after each procedure to track ball tip degradation and determine number of procedures completed before need for replacement. A high speed camera also recorded the cavitation bubble dynamics during TFL lithotripsy. Additionally, saline irrigation rates and ureteroscope deflection were measured with and without the presence of TFL fiber. There was no statistical difference (P>0.05) between stone ablation rates for single-use ball tip fiber (1.3±0.4 mg/s) (n=10), multiple-use ball tip fiber (1.3±0.5 mg/s) (n=44), and conventional single-use bare tip fibers (1.3±0.2 mg/s) (n=10). Ball tip durability varied widely, but fibers averaged greater than four stone procedures before failure, defined by rapid decline in stone ablation rates. Mechanical damage at the front surface of the ball tip was the limiting factor in fiber lifetime. The small fiber diameter did not significantly impact ureteroscope deflection or saline flow rates. The miniature ball tip fiber may provide a cost-effective design for safe fiber insertion through the ureteroscope working channel and into the ureter without risk of instrument damage or tissue perforation, and without compromising stone ablation efficiency during TFL lithotripsy.

  20. Size-dependent characterization of embedded Ge nanocrystals: Structural and thermal properties

    NASA Astrophysics Data System (ADS)

    Araujo, L. L.; Giulian, R.; Sprouster, D. J.; Schnohr, C. S.; Llewellyn, D. J.; Kluth, P.; Cookson, D. J.; Foran, G. J.; Ridgway, M. C.

    2008-09-01

    A combination of conventional and synchrotron-based techniques has been used to characterize the size-dependent structural and thermal properties of Ge nanocrystals (NCs) embedded in a silica (a-SiO2) matrix. Ge NC size distributions with four different diameters ranging from 4.0 to 9.0 nm were produced by ion implantation and thermal annealing as characterized with small-angle x-ray scattering and transmission electron microscopy. The NCs were well represented by the superposition of bulklike crystalline and amorphous environments, suggesting the formation of an amorphous layer separating the crystalline NC core and the a-SiO2 matrix. The amorphous fraction was quantified with x-ray-absorption near-edge spectroscopy and increased as the NC diameter decreased, consistent with the increase in surface-to-volume ratio. The structural parameters of the first three nearest-neighbor shells were determined with extended x-ray-absorption fine-structure (EXAFS) spectroscopy and evolved linearly with inverse NC diameter. Specifically, increases in total disorder, interatomic distance, and the asymmetry in the distribution of distances were observed as the NC size decreased, demonstrating that finite-size effects govern the structural properties of embedded Ge NCs. Temperature-dependent EXAFS measurements in the range of 15-300 K were employed to probe the mean vibrational frequency and the variation of the interatomic distance distribution (mean value, variance, and asymmetry) with temperature for all NC distributions. A clear trend of increased stiffness (higher vibrational frequency) and decreased thermal expansion with decreasing NC size was evident, confirming the close relationship between the variation of structural and thermal/vibrational properties with size for embedded Ge NCs. The increase in surface-to-volume ratio and the presence of an amorphous Ge layer separating the matrix and crystalline NC core are identified as the main factors responsible for the observed behavior, with the surrounding a-SiO2 matrix also contributing to a lesser extent. Such results are compared to previous reports and discussed in terms of the influence of the surface-to-volume ratio in objects of nanometer dimensions.

  1. Sample-morphology effects on x-ray photoelectron peak intensities. III. Simulated spectra of model core–shell nanoparticles

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Powell, Cedric J., E-mail: cedric.powell@nist.gov; Chudzicki, Maksymilian; Werner, Wolfgang S. M.

    2015-09-15

    The National Institute of Standards and Technology database for the simulation of electron spectra for surface analysis has been used to simulate Cu 2p photoelectron spectra for four types of spherical copper–gold nanoparticles (NPs). These simulations were made to extend the work of Tougaard [J. Vac. Sci. Technol. A 14, 1415 (1996)] and of Powell et al. [J. Vac. Sci. Technol. A 31, 021402 (2013)] who performed similar simulations for four types of planar copper–gold films. The Cu 2p spectra for the NPs were compared and contrasted with analogous results for the planar films and the effects of elastic scatteringmore » were investigated. The new simulations were made for a monolayer of three types of Cu/Au core–shell NPs on a Si substrate: (1) an Au shell of variable thickness on a Cu core with diameters of 0.5, 1.0, 2.0, 5.0, and 10.0 nm; (2) a Cu shell of variable thickness on an Au core with diameters of 0.5, 1.0, 2.0, 5.0, and 10.0 nm; and (3) an Au shell of variable thickness on a 1 nm Cu shell on an Au core with diameters of 0.5, 1.0, 2.0, 5.0, and 10.0 nm. For these three morphologies, the outer-shell thickness was varied until the Cu 2p{sub 3/2} peak intensity was the same (within 2%) as that found in our previous work with planar Cu/Au morphologies. The authors also performed similar simulations for a monolayer of spherical NPs consisting of a CuAu{sub x} alloy (also on a Si substrate) with diameters of 0.5, 1.0, 2.0, 5.0, and 10.0 nm. In the latter simulations, the relative Au concentration (x) was varied to give the same Cu 2p{sub 3/2} peak intensity (within 2%) as that found previously. For each morphology, the authors performed simulations with elastic scattering switched on and off. The authors found that elastic-scattering effects were generally strong for the Cu-core/Au-shell and weak for the Au-core/Cu-shell NPs; intermediate elastic-scattering effects were found for the Au-core/Cu-shell/Au-shell NPs. The shell thicknesses required to give the selected Cu 2p{sub 3/2} peak intensity for the three types of core–shell NPs were less than the corresponding film thicknesses of planar samples since Cu 2p photoelectrons can be detected from the sides and, for the smaller NPs, bottoms of the NPs. Elastic-scattering effects were also observed on the Au atomic fractions found for the CuAu{sub x} NP alloys with different diameters.« less

  2. ALMA Detects CO(3-2) within a Super Star Cluster in NGC 5253

    NASA Astrophysics Data System (ADS)

    Turner, Jean L.; Consiglio, S. Michelle; Beck, Sara C.; Goss, W. M.; Ho, Paul. T. P.; Meier, David S.; Silich, Sergiy; Zhao, Jun-Hui

    2017-09-01

    We present observations of CO(3-2) and 13CO(3-2) emission near the supernebula in the dwarf galaxy NGC 5253, which contains one of the best examples of a potential globular cluster in formation. The 0.″3 resolution images reveal an unusual molecular cloud, “Cloud D1,” that is coincident with the radio-infrared supernebula. The ˜6 pc diameter cloud has a linewidth, Δ v = 21.7 {km} {{{s}}}-1, that reflects only the gravitational potential of the star cluster residing within it. The corresponding virial mass is 2.5 × 105 {M}⊙ . The cluster appears to have a top-heavy initial mass function, with M * ≳ 1-2 {M}⊙ . Cloud D1 is optically thin in CO(3-2), probably because the gas is hot. Molecular gas mass is very uncertain but constitutes <35% of the dynamical mass within the cloud boundaries. In spite of the presence of an estimated ˜1500-2000 O stars within the small cloud, the CO appears relatively undisturbed. We propose that Cloud D1 consists of molecular clumps or cores, possibly star-forming, orbiting with more evolved stars in the core of the giant cluster.

  3. Freckle Defect Formation near the Casting Interfaces of Directionally Solidified Superalloys

    PubMed Central

    Hong, Jianping; Ma, Dexin; Wang, Jun; Wang, Fu; Sun, Baode; Dong, Anping; Li, Fei; Bührig-Polaczek, Andreas

    2016-01-01

    Freckle defects usually appear on the surface of castings and industrial ingots during the directional solidification process and most of them are located near the interface between the shell mold and superalloys. Ceramic cores create more interfaces in the directionally solidified (DS) and single crystal (SX) hollow turbine blades. In order to investigate the location of freckle occurrence in superalloys, superalloy CM247 LC was directionally solidified in an industrial-sized Bridgman furnace. Instead of ceramic cores, Alumina tubes were used inside of the casting specimens. It was found that freckles occur not only on the casting external surfaces, but also appear near the internal interfaces between the ceramic core and superalloys. Meanwhile, the size, initial position, and area of freckle were investigated in various diameters of the specimens. The initial position of the freckle chain reduces when the diameter of the rods increase. Freckle area follows a linear relationship in various diameters and the average freckle fraction is 1.1% of cross sectional area of casting specimens. The flow of liquid metal near the interfaces was stronger than that in the interdendritic region in the mushy zone, and explained why freckle tends to occur on the outer or inner surfaces of castings. This new phenomenon suggests that freckles are more likely to occur on the outer or inner surfaces of the hollow turbine blades. PMID:28774050

  4. Freckle Defect Formation near the Casting Interfaces of Directionally Solidified Superalloys.

    PubMed

    Hong, Jianping; Ma, Dexin; Wang, Jun; Wang, Fu; Sun, Baode; Dong, Anping; Li, Fei; Bührig-Polaczek, Andreas

    2016-11-16

    Freckle defects usually appear on the surface of castings and industrial ingots during the directional solidification process and most of them are located near the interface between the shell mold and superalloys. Ceramic cores create more interfaces in the directionally solidified (DS) and single crystal (SX) hollow turbine blades. In order to investigate the location of freckle occurrence in superalloys, superalloy CM247 LC was directionally solidified in an industrial-sized Bridgman furnace. Instead of ceramic cores, Alumina tubes were used inside of the casting specimens. It was found that freckles occur not only on the casting external surfaces, but also appear near the internal interfaces between the ceramic core and superalloys. Meanwhile, the size, initial position, and area of freckle were investigated in various diameters of the specimens. The initial position of the freckle chain reduces when the diameter of the rods increase. Freckle area follows a linear relationship in various diameters and the average freckle fraction is 1.1% of cross sectional area of casting specimens. The flow of liquid metal near the interfaces was stronger than that in the interdendritic region in the mushy zone, and explained why freckle tends to occur on the outer or inner surfaces of castings. This new phenomenon suggests that freckles are more likely to occur on the outer or inner surfaces of the hollow turbine blades.

  5. Does pan diameter influence carbon monoxide levels during heating of water to boiling point with a camping stove?

    PubMed

    Leigh-Smith, Simon; Stevenson, Richard; Watt, Martin; Watt, Ian; McFadyen, Angus; Grant, Stan

    2004-01-01

    To determine whether pan diameter influences carbon monoxide (CO) concentration during heating of water to boiling point with a camping stove. The hypothesis was that increasing pan diameter increases CO concentration because of greater flame dispersal and a larger flame. This was a randomized, prospective study. A Coleman Dual Fuel 533 stove was used to heat pans of water to boiling point, with CO concentration monitored every 30 seconds for 5 minutes. The stove was inside a partially ventilated 200-L cardboard box model that was inside an environmental chamber at -6 degrees C. Water temperature, water volume, and flame characteristics were all standardized. Ten trials were performed for each of 2 pan diameters (base diameters of 165 mm [small] and 220 mm [large]). There was a significant difference (P = .002) between the pans for CO levels at each measurement interval from 60 seconds onward. These differences were markedly larger after 90 seconds, with a mean difference of 185 ppm (95% CI 115, 276 ppm) for all the results from 120 seconds onwards. This study has shown that there is significantly higher CO production with a large-diameter pan compared with a small-diameter pan. These findings were evident by using a camping stove to heat water to boiling point when a maximum blue flame was present throughout. Thus, in enclosed environments it is recommended that small-diameter pans be used in an attempt to prevent high CO levels.

  6. Tunable ultrasmall visible-to-extended near-infrared emitting silver sulfide quantum dots for integrin-targeted cancer imaging.

    PubMed

    Tang, Rui; Xue, Jianpeng; Xu, Baogang; Shen, Duanwen; Sudlow, Gail P; Achilefu, Samuel

    2015-01-27

    The large size of many near-infrared (NIR) fluorescent nanoparticles prevents rapid extravasation from blood vessels and subsequent diffusion to tumors. This confines in vivo uptake to the peritumoral space and results in high liver retention. In this study, we developed a viscosity modulated approach to synthesize ultrasmall silver sulfide quantum dots (QDs) with distinct tunable light emission from 500 to 1200 nm and a QD core diameter between 1.5 and 9 nm. Conjugation of a tumor-avid cyclic pentapeptide (Arg-Gly-Asp-DPhe-Lys) resulted in monodisperse, water-soluble QDs (hydrodynamic diameter < 10 nm) without loss of the peptide's high binding affinity to tumor-associated integrins (KI = 1.8 nM/peptide). Fluorescence and electron microscopy showed that selective integrin-mediated internalization was observed only in cancer cells treated with the peptide-labeled QDs, demonstrating that the unlabeled hydrophilic nanoparticles exhibit characteristics of negatively charged fluorescent dye molecules, which typically do not internalize in cells. The biodistribution profiles of intravenously administered QDs in different mouse models of cancer reveal an exceptionally high tumor-to-liver uptake ratio, suggesting that the small sized QDs evaded conventional opsonization and subsequent high uptake in the liver and spleen. The seamless tunability of the QDs over a wide spectral range with only a small increase in size, as well as the ease of labeling the bright and noncytotoxic QDs with biomolecules, provides a platform for multiplexing information, tracking the trafficking of single molecules in cells, and selectively targeting disease biomarkers in living organisms without premature QD opsonization in circulating blood.

  7. Emission enhancement, light extraction and carrier dynamics in InGaAs/GaAs nanowire arrays

    NASA Astrophysics Data System (ADS)

    Kivisaari, Pyry; Chen, Yang; Anttu, Nicklas

    2018-03-01

    Nanowires (NWs) have the potential for a wide range of new optoelectronic applications. For example, light-emitting diodes that span over the whole visible spectrum are currently being developed from NWs to overcome the well known green gap problem. However, due to their small size, NW devices exhibit special properties that complicate their analysis, characterization, and further development. In this paper, we develop a full optoelectronic simulation tool for NW array light emitters accounting for carrier transport and wave-optical emission enhancement (EE), and we use the model to simulate InGaAs/GaAs NW array light emitters with different geometries and temperatures. Our results show that NW arrays emit light preferentially to certain angles depending on the NW diameter and temperature, encouraging temperature- and angle-resolved measurements of NW array light emission. On the other hand, based on our results both the EE and light extraction efficiency can easily change by at least a factor of two between room temperature and 77 K, complicating the characterization of NW light emitters if conventional methods are used. Finally, simulations accounting for surface recombination emphasize its major effect on the device performance. For example, a surface recombination velocity of 104 cm s-1 reported earlier for bare InGaAs surfaces results in internal quantum efficiencies less than 30% for small-diameter NWs even at the temperature of 30 K. This highlights that core-shell structures or high-quality passivation techniques are eventually needed to achieve efficient NW-based light emitters.

  8. Solid State Digital Propulsion "Cluster Thrusters" For Small Satellites Using High Performance Electrically Controlled Extinguishable Solid Propellants (ECESP)

    NASA Technical Reports Server (NTRS)

    Sawka, Wayne N.; Katzakian, Arthur; Grix, Charles

    2005-01-01

    Electrically controlled extinguishable solid propellants (ESCSP) are capable of multiple ignitions, extinguishments and throttle control by the application of electrical power. Both core and end burning no moving parts ECESP grains/motors to three inches in diameter have now been tested. Ongoing research has led to a newer family of even higher performance ECESP providing up to 10% higher performance, manufacturing ease, and significantly higher electrical conduction. The high conductivity was not found to be desirable for larger motors; however it is ideal for downward scaling to micro and pico- propulsion applications with a web thickness of less than 0.125 inch/ diameter. As a solid solution propellant, this ECESP is molecularly uniform, having no granular structure. Because of this homogeneity and workable viscosity it can be directly cast into thin layers or vacuum cast into complex geometries. Both coaxial and grain stacks have been demonstrated. Combining individual propellant coaxial grains and/or grain stacks together form three-dimensional arrays yield modular cluster thrusters. Adoption of fabless manufacturing methods and standards from the electronics industry will provide custom, highly reproducible micro-propulsion arrays and clusters at low costs. These stack and cluster thruster designs provide a small footprint saving spacecraft surface area for solar panels and/or experiments. The simplicity of these thrusters will enable their broad use on micro-pico satellites for primary propulsion, ACS and formation flying applications. Larger spacecraft may find uses for ECESP thrusters on extended booms, on-orbit refueling, pneumatic actuators, and gas generators.

  9. Localized compliance of small airways in excised rat lungs using microfocal X-ray computed tomography.

    PubMed

    Sera, Toshihiro; Fujioka, Hideki; Yokota, Hideo; Makinouchi, Akitake; Himeno, Ryutaro; Schroter, Robert C; Tanishita, Kazuo

    2004-05-01

    Airway compliance is a key factor in understanding lung mechanics and is used as a clinical diagnostic index. Understanding such mechanics in small airways physiologically and clinically is critical. We have determined the "morphometric change" and "localized compliance" of small airways under "near"-physiological conditions; namely, the airways were embedded in parenchyma without dehydration and fixation. Previously, we developed a two-step method to visualize small airways in detail by staining the lung tissue with a radiopaque solution and then visualizing the tissue with a cone-beam microfocal X-ray computed tomography system (Sera et al. J Biomech 36: 1587-1594, 2003). In this study, we used this technique to analyze changes in diameter and length of the same small airways ( approximately 150 microm ID) and then evaluated the localized compliance as a function of airway generation (Z). For smaller (<300-microm-diameter) airways, diameter was 36% larger at end-tidal inspiration and 89% larger at total lung capacity; length was 18% larger at end-tidal inspiration and 43% larger at total lung capacity than at functional residual capacity. Diameter, especially at smaller airways, did not behave linearly with V(1/3) (where V is volume). With increasing lung pressure, diameter changed dramatically at a particular pressure and length changed approximately linearly during inflation and deflation. Percentage of airway volume for smaller airways did not behave linearly with that of lung volume. Smaller airways were generally more compliant than larger airways with increasing Z and exhibited hysteresis in their diameter behavior. Airways at higher Z deformed at a lower pressure than those at lower Z. These results indicated that smaller airways did not behave homogeneously.

  10. [Development of a simultaneous strain and temperature sensor with small-diameter FBG].

    PubMed

    Liu, Rong-mei; Liang, Da-kai

    2011-03-01

    Manufacture of the small diameter FBG was designed. Cross sensitivity of temperature and strain at sensing point was solved. Based on coupled-mode theory, optical properties of the designed FBG were studied. The reflection and transmission spectra of the designed FBG in small diameter were studied A single mode optical fiber, whose cladding diameter is 80 microm, was manufactured to a fiber Bragg grating (phi80FBG). According to spectrum simulation, the grating length and period were chosen as the wavelength was 1528 nm. The connector of the small diameter FBG with demodulation was designed too. In applications, the FBG measures the total deformation including strain due to forces applied to the structures as well as thermal expansion. In order to overcome this inconvenience and to measure both parameters at the same time and location, a novel scheme for simultaneous strain and temperature sensor was presented. Since the uniform strength beam has same deformation at all points, a pair of phi80 FBG was attached on a uniform strength cantilever. One of the FBG was on the upper surface, with the other one on the below. Therefore, the strains at the monitoring points were equal in magnitude but of opposite sign. The strain and temperature in sensing point could be discriminated by matrix equation. The determination of the K is not null and thus matrix inversion is well conditioned, even the values for the K elements are close. Consequently, the cross sensitivity of the FBG with temperature and strain can be experimentally solved. Experiments were carried out to study the strain discriminability of small-diameter FBG sensors. The temperature and strain were calculated and the errors were, respectively, 5% and 6%.

  11. Influence of the core material and the glass infiltration mode on the color of glass-infiltrated ceramic veneers over discolored backgrounds. A spectrophotometric evaluation.

    PubMed

    Koutayas, Spiridon-Oumvertos; Charisis, Dimitrios

    2008-01-01

    The purpose of this study was to evaluate the influence of the core material (Spinell or Alumina) and the glass infiltration mode (under or without vacuum) on the color of 2M2 Vita In-Ceram Spinell and Alumina ceramic veneers (Vident) for the restoration of 5M1 discolored backgrounds. A total of 40 In-Ceram Spinell (SP, n = 20) and Alumina (AL, n = 20) disks (diameter 10.0 mm, thickness 0.4 mm, Vident) were glass-infiltrated under (V, n = 20) or without vacuum (A, n = 20) using a translucent glass (S1, Vident) and then veneered (2M2 Vitadur Alpha, total thickness 0.7 mm). The veneer specimens were bonded onto the 5M1 color backgrounds (Vitadur Alpha, diameter 10.0 mm, thickness 2.0 mm) using a dual curing adhesive cement (Panavia F 2.0 Light, Kuraray), to create the study groups (SPV, SPA, ALV, ALA, each n = 10). Ten 2M2 feldspathic veneer disks (Vitadur Alpha, diameter 10.0 mm, thickness 0.7 mm) bonded onto 2M2 color backgrounds (Vitadur Alpha, diameter 10.0 mm, thickness 2.0 mm) were used as control (CTR group). L*a*b* color coordinates were measured 5 times for each study group and control specimen using a Vita Easyshade spectrophotometer (Vident). Mean color differences (DeltaE) were calculated using the equation DeltaE = (DeltaL*2 + Deltaa*2 + Deltab*2)1/2. Mean color differences and standard deviations between each study group and the control group were: 7.31 +/- 0.99 for SPV; 7.23 +/- 0.61 for SPA; 5.81 +/- 1.41 for ALV; and 6.25 +/- 0.89 for ALA. Two-way ANOVA followed by t test showed that only the core material had a statistically significant effect on the final color performance (alpha = .05, P = .000). The core material (Spinell or Alumina) significantly influenced the core-related opacity, while the glass infiltration mode (under or without vacuum) had a minor effect on the final color establishment of both glass-infiltrated veneers over discolored backgrounds. Regarding the reported clinical visible thresholds, In-Ceram Alumina ceramic veneers showed the greatest improvement in the color performance of discolored teeth compared with all other groups.

  12. Modeling and testing of ethernet transformers

    NASA Astrophysics Data System (ADS)

    Bowen, David

    2011-12-01

    Twisted-pair Ethernet is now the standard home and office last-mile network technology. For decades, the IEEE standard that defines Ethernet has required electrical isolation between the twisted pair cable and the Ethernet device. So, for decades, every Ethernet interface has used magnetic core Ethernet transformers to isolate Ethernet devices and keep users safe in the event of a potentially dangerous fault on the network media. The current state-of-the-art Ethernet transformers are miniature (<5mm diameter) ferrite-core toroids wrapped with approximately 10 to 30 turns of wire. As small as current Ethernet transformers are, they still limit further Ethernet device miniaturization and require a separate bulky package or jack housing. New coupler designs must be explored which are capable of exceptional miniaturization or on-chip fabrication. This dissertation thoroughly explores the performance of the current commercial Ethernet transformers to both increase understanding of the device's behavior and outline performance parameters for replacement devices. Lumped element and distributed circuit models are derived; testing schemes are developed and used to extract model parameters from commercial Ethernet devices. Transfer relation measurements of the commercial Ethernet transformers are compared against the model's behavior and it is found that the tuned, distributed models produce the best transfer relation match to the measured data. Process descriptions and testing results on fabricated thin-film dielectric-core toroid transformers are presented. The best results were found for a 32-turn transformer loaded with 100Ω, the impedance of twisted pair cable. This transformer gave a flat response from about 10MHz to 40MHz with a height of approximately 0.45. For the fabricated transformer structures, theoretical methods to determine resistance, capacitance and inductance are presented. A special analytical and numerical analysis of the fabricated transformer inductance is presented. Planar cuts of magnetic slope fields around the dielectric-core toroid are shown that describe the effect of core height and winding density on flux uniformity without a magnetic core.

  13. A simple and inexpensive technique for assessing microbial contamination during drilling operations

    NASA Astrophysics Data System (ADS)

    Friese, André; Vuillemin, Aurèle; Kallmeyer, Jens; Wagner, Dirk

    2016-04-01

    Exploration of the Deep Biosphere relies on drilling, which inevitably causes infiltration of drilling fluids, containing allochthonous microbes from the surface, into the core. Therefore it is absolutely necessary to trace contamination of the sediment core in order to identify uncontaminated samples for microbiological investigations. Several techniques have been used in the past, including fluorescent dyes, perfluorocarbon tracers and fluorescent microspheres. Fluorescent dyes are inexpensive and easy to analyze on-site but are sensitive to light, pH and water chemistry. Furthermore, significant sorption to clays can decrease the fluorescence signal. Perfluorocarbon tracers are chemically inert hydrophobic compounds that can be detected with high sensitivity via gas chromatography, which might be a problem for on-site analysis. Samples have to be taken immediately after core retrieval as otherwise the volatile tracer will have diffused out of the core. Microsphere tracers are small (0.2 - 0.5 μm diameter) fluorescent plastic particles that are mixed into the drilling fluid. For analysis, these particles can be extracted from the sediment sample, transferred onto a filter and quantified via fluorescence microscopy. However, they are very expensive and therefore unsuitable for deep drilling operations that need large amounts of drilling fluids. Here, we present an inexpensive contamination control approach using fluorescent pigments initially used for coloring plastics. The price of this tracer is nearly three orders of magnitude lower than conventional microsphere tracers. Its suitability for large drilling campaigns was tested at the ICDP Deep Drilling at Lake Towuti, Sulawesi, Indonesia. The tracer was diluted 1:1000 in lake water, which was used as the drilling fluid. Additionally, a plastic bag filled with 20 mL of undiluted tracer was attached to the core catcher to increase the amount of particles in the liner fluid right at the core. After core retrieval, the core was cut and the liner fluid collected. From each whole round core (WRC) that was taken for microbiological and biogeochemical analyses, small samples of 1 cc were retrieved with sterile cutoff syringes from the rim, the center and an intermediate position. After dilution and homogenization in 9 mL MilliQ water, 10 μL of the sediment slurry was transferred onto a filter membrane and particles counted via fluorescence microscopy. Additionally, particles in the liner fluid were also quantified. This allows the quantification of the amount of drilling fluid that has entered the sediment sample during drilling. The minimum detectable volume of drilling fluid was in the order of single nanoliters per cc of sediment, which is in the range of established techniques. The presented method requires only a minimum of equipment and allows rapid determination of contamination in the sediment core and an easy to handle on-site analysis at low costs. The sensitivity is in the same range as perfluorocarbon and microsphere tracer applications. Thus, it offers an inexpensive but powerful technique for contamination assessment for future drilling campaigns.

  14. Small-diameter log evaluation for value-added structural applications

    Treesearch

    Ronald Wolfe; Cassandra Moseley

    2000-01-01

    Three species of small-diameter logs from the Klamath/Siskiyou Mountains and the Cascade Range in southwest Oregon were tested for their potential for value-added structural applications. The logs were tested in bending and compression parallel to the grain. Strength and stiffness values were correlated to possible nondestructive evaluation grading parameters and...

  15. Small-diameter trees used for chemithermomechanical pulps.

    Treesearch

    Gary C. Myers; R. James Barbour; Said M. Abubakr

    1999-01-01

    During the course of restoring and maintaining forest ecosystem health and function in the western interior of the United States, many small-diameter stems are removed from densely stocked stands. In general, these materials are considered nonusable or underutilized. Information on the properties of these resources is needed to help managers understand when timber...

  16. 78 FR 41369 - Certain Small Diameter Carbon and Alloy Seamless Standard, Line and Pressure Pipe From Romania...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-07-10

    ... Carbon and Alloy Seamless Standard, Line and Pressure Pipe From Romania: Preliminary Results of..., line and pressure pipe (small diameter seamless pipe) from Romania. The period of review (POR) is... and Alloy Seamless Standard, Line and Pressure Pipe from Romania,'' dated concurrently with this...

  17. Unmanned Aircraft Systems for Logistics Applications

    DTIC Science & Technology

    2011-01-01

    Jane’s Air-Launched Weapons, “ GBU - 39 /B Small Diameter Bomb (SDB) and SDB II (United States),” June 5, 2009. As of September 11, 2009: http...www.janes.com/articles/Janes-Air-Launched-Weapons/ GBU - 39 -B-Small- Diameter-Bomb-SDB-and-SDB-II-United-States.html [subscription required] Jane’s Electro

  18. Biomass utilization for bioenergy in the Western United States

    Treesearch

    D.L. Nicholls; R. Monserud; D. Dykstra

    2008-01-01

    Wildfires, hazardous fuel buildups, small-diameter timber, wildland-urban interface zones, biomass. These are some of the terms becoming familiar to communities throughout the Western United States after the record-breaking fire seasons of the past decade. Although small-diameter stems are generally expensive to remove and often have limited utilization options, the...

  19. Thermocouple design for measuring temperatures of small insects

    Treesearch

    A.A. Hanson; R.C. Venette

    2013-01-01

    Contact thermocouples often are used to measure surface body temperature changes of insects during cold exposure. However, small temperature changes of minute insects can be difficult to detect, particularly during the measurement of supercooling points. We developed two thermocouple designs, which use 0.51 mm diameter or 0.127 mm diameter copper-constantan wires, to...

  20. Small-diameter success stories

    Treesearch

    Jean Livingston

    2004-01-01

    Public and private forests are in critical need of restoration by thinning small-diameter timber. If economical and value-added uses for this thinned material can be found, forest restoration costs could be offset and catastrophic wildfires would be minimized. At the same time, forestry- dependent rural communities?faced with diminishing timber supplies, loss of jobs,...

  1. Measurements of droplet size in shear-driven atomization using ultra-small angle x-ray scattering

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Kastengren, A.; Ilavsky, J.; Viera, Juan Pablo

    Measurements of droplet size in optically-thick, non-evaporating, shear-driven sprays have been made using ultra-small angle x-ray scattering (USAXS). The sprays are produced by orifice-type nozzles coupled to diesel injectors, with measurements conducted from 1 – 24 mm from the orifice, spanning from the optically-dense near-nozzle region to more dilute regions where optical diagnostics are feasible. The influence of nozzle diameter, liquid injection pressure, and ambient density were examined. The USAXS measurements reveal few if any nanoscale droplets, in conflict with a popular computational model of diesel spray breakup. The average droplet diameter rapidly decreases with downstream distance from the nozzlemore » until a plateau value is reached, after which only small changes are seen in droplet diameter. This plateau droplet size is consistent with the droplets being small enough to be stable with respect to further breakup. As a result, liquid injection pressure and nozzle diameter have the biggest impact on droplet size, while ambient density has a smaller effect.« less

  2. Measurements of droplet size in shear-driven atomization using ultra-small angle x-ray scattering

    DOE PAGES

    Kastengren, A.; Ilavsky, J.; Viera, Juan Pablo; ...

    2017-03-16

    Measurements of droplet size in optically-thick, non-evaporating, shear-driven sprays have been made using ultra-small angle x-ray scattering (USAXS). The sprays are produced by orifice-type nozzles coupled to diesel injectors, with measurements conducted from 1 – 24 mm from the orifice, spanning from the optically-dense near-nozzle region to more dilute regions where optical diagnostics are feasible. The influence of nozzle diameter, liquid injection pressure, and ambient density were examined. The USAXS measurements reveal few if any nanoscale droplets, in conflict with a popular computational model of diesel spray breakup. The average droplet diameter rapidly decreases with downstream distance from the nozzlemore » until a plateau value is reached, after which only small changes are seen in droplet diameter. This plateau droplet size is consistent with the droplets being small enough to be stable with respect to further breakup. As a result, liquid injection pressure and nozzle diameter have the biggest impact on droplet size, while ambient density has a smaller effect.« less

  3. Heterogeneous Delivery of Silicate and Metal to the Earth via Large Planetesimals

    NASA Astrophysics Data System (ADS)

    Marchi, S.; Canup, R. M.; Walker, R. J.

    2017-12-01

    Earth's mantle abundances of at least some highly siderophile elements, (HSE; Re, Os, Ir, Ru, Pt, Rh, Pd, and Au), are much higher than would result from metal-silicate equilibration during terrestrial core formation, and can be better explained as a result of late accretion of a minimum of 0.5% Earth's masses after core formation was complete. Traditional models assume that HSEs delivered by late projectiles completely mixed and chemically equilibrated with the Earth's mantle. This appears likely for undifferentiated, well-mixed projectiles, or for relatively small, differentiated projectiles. However several arguments suggest that late projectiles may have been large (> 1500 km in diameter) and differentiated, and in this case, portions of the projectile's core may merge with the Earth's core, rather than being mixed into the Earth's mantle. We investigate projectile mixing with a suite of SPH simulations of differentiated planetesimal colliding with the Earth. A range of outcomes emerge from our simulations suggesting that for large impactors (>1500 km), the delivery of HSE to the Earth's mantle may be disproportionate with the overall delivery of mass. For impacts with impact angles < 45° , between ˜ 20% to 80% of the impactor's core may merge directly with the Earth's core; while for impact angle > 60°, most of the impactor core escapes for moderate impact speeds. An implication is that the late accreted mass inferred from terrestrial HSE abundances may be a substantial underestimate, by a factor 2-5. In addition, partial mixing of projectiles result in an enrichment in mantle vs core material delivered to the bulk silicate Earth, implying substantial compositional variations in the accreted mass. Such variations could produce initially localized domains in Earth's mantle with distinct, mass independent isotopic signatures, given the isotopic variability resulting from nucleosynthetic heterogeneities among genetically diverse meteorites. In general we find that larger, low angle collisions would be more likely to produce initial mantle domains of anomalous composition material. We discuss the implications of these findings in the light of isotopic anomalies (e.g. W) in ancient terrestrial rocks.

  4. The use of mini-samples in palaeomagnetism

    NASA Astrophysics Data System (ADS)

    Böhnel, Harald; Michalk, Daniel; Nowaczyk, Norbert; Naranjo, Gildardo Gonzalez

    2009-10-01

    Rock cores of ~25 mm diameter are widely used in palaeomagnetism. Occasionally smaller diameters have been used as well which represents distinct advantages in terms of throughput, weight of equipment and core collections. How their orientation precision compares to 25 mm cores, however, has not been evaluated in detail before. Here we compare the site mean directions and their statistical parameters for 12 lava flows sampled with 25 mm cores (standard samples, typically 8 cores per site) and with 12 mm drill cores (mini-samples, typically 14 cores per site). The site-mean directions for both sample sizes appear to be indistinguishable in most cases. For the mini-samples, site dispersion parameters k on average are slightly lower than for the standard samples reflecting their larger orienting and measurement errors. Applying the Wilcoxon signed-rank test the probability that k or α95 have the same distribution for both sizes is acceptable only at the 17.4 or 66.3 per cent level, respectively. The larger mini-core numbers per site appears to outweigh the lower k values yielding also slightly smaller confidence limits α95. Further, both k and α95 are less variable for mini-samples than for standard size samples. This is interpreted also to result from the larger number of mini-samples per site, which better averages out the detrimental effect of undetected abnormal remanence directions. Sampling of volcanic rocks with mini-samples therefore does not present a disadvantage in terms of the overall obtainable uncertainty of site mean directions. Apart from this, mini-samples do present clear advantages during the field work, as about twice the number of drill cores can be recovered compared to 25 mm cores, and the sampled rock unit is then more widely covered, which reduces the contribution of natural random errors produced, for example, by fractures, cooling joints, and palaeofield inhomogeneities. Mini-samples may be processed faster in the laboratory, which is of particular advantage when carrying out palaeointensity experiments.

  5. Short-Range Correlated Magnetic Core-Shell CrO₂/Cr₂O₃ Nanorods: Experimental Observations and Theoretical Considerations.

    PubMed

    Gandhi, Ashish C; Li, Tai-Yue; Chan, Ting Shan; Wu, Sheng Yun

    2018-05-09

    With the evolution of synthesis and the critical characterization of core-shell nanostructures, short-range magnetic correlation is of prime interest in employing their properties to develop novel devices and widespread applications. In this regard, a novel approach of the magnetic core-shell saturated magnetization (CSSM) cylinder model solely based on the contribution of saturated magnetization in one-dimensional CrO₂/Cr₂O₃ core-shell nanorods (NRs) has been developed and applied for the determination of core-diameter and shell-thickness. The nanosized effect leads to a short-range magnetic correlation of ferromagnetic core-CrO₂ extracted from CSSM, which can be explained using finite size scaling method. The outcome of this study is important in terms of utilizing magnetic properties for the critical characterization of core-shell nanomagnetic materials.

  6. Tunable plasmon resonances in anisotropic metal nanostructures

    NASA Astrophysics Data System (ADS)

    Penninkhof, J. J.

    2006-09-01

    Coherent oscillations of free electrons in a metal, localized in a small volume or at an interface between a metal and a dielectric medium, have attracted a lot of attention in the past decades. These so-called surface plasmons have special optical properties that can be used in many applications ranging from optoelectronics to sensing of small quantities of molecules. One of the key issues is that electromagnetic energy can be confined to a relatively small volume close to the metal surface. This field enhancement and the resonance frequency strongly depend on the shape and size of the metal structures. In this thesis, several fabrication methods to create these metal structures on the nanometer to micrometer scale are presented. The optical properties are studied with a special emphasis on the effect of shape anisotropy. Self-assembled 2D colloidal crystals are used as mask to fabricate arrays of metal triangles on a substrate. One of the limitations of this nanosphere lithography technique is that the size of the holes in the colloidal mask (through which the metal is evaporated) is determined by the size of the colloids in the mask. The masks, however, can be modified by use of MeV ion beams and/or wet-chemical growth of a thin layer of silica, resulting in a reduced hole size. Arbitrary symmetry and spacing can be obtained by use of optical tweezers and angle-resolved metal deposition. In contrast to pure metals, amorphous materials like silica are known to show anisotropic plastic deformation at constant volume when subject to MeV ion irradiation. Gold cores embedded in a silica matrix, however, show an elongation along the direction of the ion beam, whereas silver cores rather disintegrate. Silver nanocrystals in an ion-exchanged soda-lime glass redistribute themselves in arrays along the ion beam direction. The optical extinction becomes polarization-dependent, with red- and blue-shifts of the plasmon resonances for polarizations longitudinal and transverse to the arrays, respectively. The band splitting is attributed to near-field electromagnetic plasmon coupling within the arrays. Finite difference time domain simulations indicate that the combination of particle center-to-center spacing and diameter, rather than inter-particle spacing alone, is the key parameter determining the coupling strength. The resonant electric field is concentrated in the very small gaps between the particles in the array. With the MeV ion beam technique, it is possible to fabricate large substrates with relatively monodisperse oblate ellipsoidal silica-core/metal-shell colloids, with the short axis aligned in the direction of the ion beam. The optical extinction of these particles, is a complex function of the core radius and the shell thickness, due to a competition between phase retardation effects and the coupling between the surface plasmons at the inner and outer surfaces of the shell. After deformation, the extinction is angle- and polarization-dependent. Calculations indicate that large Au-shell particles can sustain cavity modes, for which the electric field is enhanced in almost the full volume of the dielectric core. The resonance frequency is sensitive to the size, shape and dielectric constant of the core, and the polarization direction.

  7. Compact Hybrid Laser Rod and Laser System

    NASA Technical Reports Server (NTRS)

    Pierrottet, Diego F. (Inventor); Busch, George E. (Inventor); Amzajerdian, Farzin (Inventor)

    2017-01-01

    A hybrid fiber rod includes a fiber core and inner and outer cladding layers. The core is doped with an active element. The inner cladding layer surrounds the core, and has a refractive index substantially equal to that of the core. The outer cladding layer surrounds the inner cladding layer, and has a refractive index less than that of the core and inner cladding layer. The core length is about 30 to 2000 times the core diameter. A hybrid fiber rod laser system includes an oscillator laser, modulating device, the rod, and pump laser diode(s) energizing the rod from opposite ends. The rod acts as a waveguide for pump radiation but allows for free-space propagation of laser radiation. The rod may be used in a laser resonator. The core length is less than about twice the Rayleigh range. Degradation from single-mode to multi-mode beam propagation is thus avoided.

  8. Supercontinuum generation from 437 to 2850 nm in a tapered fluorotellurite microstructured fiber

    NASA Astrophysics Data System (ADS)

    Wang, F.; Jia, Z. X.; Yao, C. F.; Wang, S. B.; Hu, M. L.; Wu, C. F.; Ohishi, Y.; Qin, W. P.; Qin, G. S.

    2016-12-01

    We demonstrated supercontinuum (SC) generation in a tapered fluorotellurite microstructured fiber (MF) with a sub-micrometer core diameter. Fluorotellurite MFs based on TeO2-BaF2-Y2O3 glasses were fabricated by using a rod-in-tube method and a tapered fluorotellurite MF with a minimum core diameter of ~0.65 µm was prepared by employing a tapering system. A 1560 nm femtosecond fiber laser was used as the pumping source. With increasing the peak power of the launched pump laser to ~11 kW, SC light expanding from 437 to 2850 nm was generated in the tapered fluorotellurite MF. In addition, relatively strong blue-shifted dispersive wave at ~489 nm was also observed from the tapered fluorotellurite MF.

  9. Research turbine for high-temperature core engine application. 2: Effect of rotor tip clearance on overall performance

    NASA Technical Reports Server (NTRS)

    Szanca, E. M.; Behning, F. P.; Schum, H. J.

    1974-01-01

    A 25.4-cm (10-in) tip diameter turbine was tested to determine the effect of rotor radial tip clearance on turbine overall performance. The test turbine was a half-scale model of a 50.8-cm-(20-in.-) diameter research turbine designed for high-temperature core engine application. The test turbine was fabricated with solid vanes and blades with no provision for cooling air and tested at much reduced inlet conditions. The tests were run at design speed over a range of pressure ratios for three different rotor clearances ranging from 2.3 to 6.7 percent of the annular blade passage height. The results obtained are compared to the results obtained with three other turbines of varying amounts of reaction.

  10. Nanoformulation for anticancer drug delivery: Enhanced pharmacokinetics and circulation

    NASA Astrophysics Data System (ADS)

    Parekh, Gaurav

    In this study, we have explored the application of the Layer-by-Layer (LbL) assembly technique for improving injectable drug delivery systems of low soluble anticancer drugs (e.g. Camptothecin (CPT), Paclitaxel (PTX) or Doxorubicin (DOX)). For this study, a polyelectrolyte shell encapsulates different types of drug nanocores (e.g. soft core, nanomicelle or solid lipid nanocores).The low soluble drugs tend to crystallize and precipitate in an aqueous medium. This is the reason they cannot be injected and may have low concentrations and low circulation time in the blood. Even though these drugs when present in the cancer microenvironment have high anti-tumor inhibition, the delivery to the tumor site after intravenous administration is a challenge. We have used FDA-approved biopolymers for the process and elaborated formation of 60-90 nm diameter initial cores, which was stabilized by multilayer LbL shells for controlled release and longer circulation. A washless LbL assembly process was applied as an essential advancement in nano-assembly technology using low density nanocore (lipids) and preventing aggregation. This advancement reduced the number of process steps, enhanced drug loading capacity, and prevented the loss of expensive polyelectrolytes. Finally, we elaborated a general nano-encapsulation process, which allowed these three important anticancer drug core-shell nanocapsules with diameters of ca. 100-130 nm (this small size is a record for LbL encapsulation technique) to be stable in the serum and the blood for at least one week, efficient for cancer cell culture studies, injectable to mice with circulation for 4 hrs, and effective in suppressing tumors. This work is divided into three studies. The first study (CHAPTER 4) explores the application of LbL assembly for encapsulating a soft core of albumin protein and CPT anticancer drug. In order to preserve the activity of drug in the core, a unique technique of pH reversal is employed where the first few layers of the LbL shell are assembled at acidic pH 3, and the final layers (2-3) are assembled at a slightly basic pH of 7.4. These LbL-encapsulated nanocores are not stable and immediately aggregate in water or the serum. A final layer of 5 kDa PEG was assembled to improve circulation time. It showed higher colloidal stability in PBS, high drug loading concentration of 0.5 mg/mL, and an improved drug chemical stability in Fetal Bovine Serum with high lactone fraction of 99%. It also showed 3 times improved cytotoxicity against glioblastoma cancer cells. For the first time we applied a new method of the LbL capsule assembly at different pH values, the first 4 bilayers at pH 3, and the following 3 bilayers at pH 7.4. In the second study (CHAPTER 5), the developed LbL assembly for low solubility drug encapsulation was extended for the delivery of PTX loaded in nanomicelle cores. PTX, as a nanomicelle core, is encapsulated with fewer layers of LbL assembly, followed by an extra layer of PEG (PEGylation). A significant improvement was seen in reducing the process steps through reduction in the number of LbL layers, while smaller nano-colloids, ~100 nm, were produced with improved drug loading capacity, higher cytotoxicity, and high mice survival rate. In the third study (CHAPTER 6), we have applied the concepts learned and the techniques developed from the previous two studies to modify the surface of the nanostructured solid lipid carriers (NLC) with LbL architecture, plus extra PEGylation. The NLC are co-loaded with DOX and docosahexaenoic acid (DHA). This study is an attempt to further increase drug circulation time in the blood. We improved the colloidal stability with a narrow distribution size, 128 nm, polydispersity of 0.098, a higher longevity in the blood, a 1.5 times lower accumulation in the liver, a 2.25 times higher accumulation in tumors, and a significant ~3.5 times greater tumor growth inhibition in 4T1 murine tumor model in mice. In conclusion, we developed a general model of an LbL nanoassembly core-shell drug delivery system of three anticancer drugs. The capsules had diameters of ca. 100170 nm, were stable in the serum and the blood for three weeks, were injectable to small animals with a circulation time of 1-4 hrs., and effectively suppressed cancerous tumors in mice.

  11. Novel splice techniques and micro-hole collapse effect in photonic crystal fibers

    NASA Astrophysics Data System (ADS)

    Xiao, Limin

    Photonic crystal fibers (PCFs) represent one of the most active research areas today in the field of fiber optics. Because of the freedom they offer in their design and novel wave-guiding properties, PCFs have resulted in a number of applications that are difficult to achieve with conventional fibers. In practical applications, low-loss connection PCFs with conventional fibers is a key issue for integrating PCF devices into existing fiber optic systems. However, connecting PCFs to conventional fibers without incurring too much loss is a very challenging problem. Two novel techniques were proposed to solve this problem in the thesis. One is fusion splicing technique; the other is micro-tip technique. First, fusion splicing technique for PCFs is investigated. For fusion splicing SMFs and PCFs having similar mode field diameters, a low-loss joint with good mechanical strength can be formed by choosing a suitably weak fusion current, short fusion time, offset and overlap to minimize the collapse of air holes and well melt two fibers together. For small-core PCFs, an optimum mode field match and an adiabatic mode field variation can be achieved by repeated arc discharges. Low-loss fusion splicing of five different PCFs with SMFs are achieved, including large mode PCF, hollow-core PCF, nonlinear PCFs with low and high air-filling fraction and polarization maintaining PCF. The other novel technique is using micro-tips. The method is based on growing photopolymer micro-tips directly on the end face of SMFs. The shape and the size of the tips can be controlled, by adjusting the laser power, the exposure time and the oxygen diffusion concentration for polymerization, to match its mode field to the small-core PCFs. Micro-hole collapse effect can be used to fabricate selective injection PCFs. The suitable arc discharge energy can cause the cladding holes to collapse while leaving the central hollow core to remain open. Thus a simple method for selective filling the central hole of PCFs is developed. Hybrid PCF guides light by a novel guiding mechanism, which is a combination of index-guiding and bandgap-guiding. The properties of the hybrid PCF are systematically investigated.

  12. A comparison of the effects of 2 cattle-cooling systems on dairy cows in a desert environment.

    PubMed

    Ortiz, X A; Smith, J F; Bradford, B J; Harner, J P; Oddy, A

    2010-10-01

    An experiment was conducted to investigate the effects of operation time and size of Korral Kool (KK; Korral Kool Inc., Mesa, AZ) systems on core body temperature (CBT) of dairy cows. Two KK systems were compared: a system with 1.29-m-diameter, 3-hp fans spaced 6 m apart (referred to as small) and a system with 1.52-m-diameter, 5-hp fans spaced 8 m apart (referred to as big). Forty-eight multiparous Holstein cows were assigned randomly to 8 pens (4 big, 4 small), and pens were assigned randomly to a sequence of treatments (KK operated for 21 or 24 h/d) in a switchback design. A complementary calorimetric analysis was developed to investigate the cooling area under the KK units of the big and small systems. Twenty-five sensors distributed equally under the KK units measured ambient temperature at 5-min intervals for 2 h. Average ambient temperature was 35.0±0.6°C and relative humidity was 45±8%. There were significant treatment effects on mean CBT: cows on the small 24-h treatment had a lower mean CBT than cows on the small 21-h treatment (39.22 vs. 39.36±0.14°C), and cows on the big 24-h treatment had a lower mean CBT than cows on the big 21-h treatment (38.95 vs. 39.09±0.13°C). A significant treatment by time interaction was observed. The greatest difference between systems occurred at 0100 h; treatment means at this time were 39.05, 39.01, 39.72, and 39.89±0.16°C for the big 24-h, big 21-h, small 24-h, and small 21-h treatments, respectively. At certain times of day, the big system reduced CBT more than the small system. These results show that CBT of multiparous cows decreased when KK system operational time was increased from 21 to 24 h regardless of the size of the KK cooling system used. The calorimetric analysis showed that even though the big system resulted in lower mean ambient temperatures than the small system, the distance between units in the big system should be decreased to reduce the variation in temperature under the big units. Copyright © 2010 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

  13. Rapid-quench axially staged combustor

    DOEpatents

    Feitelberg, Alan S.; Schmidt, Mark Christopher; Goebel, Steven George

    1999-01-01

    A combustor cooperating with a compressor in driving a gas turbine includes a cylindrical outer combustor casing. A combustion liner, having an upstream rich section, a quench section and a downstream lean section, is disposed within the outer combustor casing defining a combustion chamber having at least a core quench region and an outer quench region. A first plurality of quench holes are disposed within the liner at the quench section having a first diameter to provide cooling jet penetration to the core region of the quench section of the combustion chamber. A second plurality of quench holes are disposed within the liner at the quench section having a second diameter to provide cooling jet penetration to the outer region of the quench section of the combustion chamber. In an alternative embodiment, the combustion chamber quench section further includes at least one middle region and at least a third plurality of quench holes disposed within the liner at the quench section having a third diameter to provide cooling jet penetration to at least one middle region of the quench section of the combustion chamber.

  14. Measuring helium bubble diameter distributions in tungsten with grazing incidence small angle x-ray scattering (GISAXS)

    NASA Astrophysics Data System (ADS)

    Thompson, M.; Kluth, P.; Doerner, R. P.; Kirby, N.; Riley, D.; Corr, C. S.

    2016-02-01

    Grazing incidence small angle x-ray scattering was performed on tungsten samples exposed to helium plasma in the MAGPIE and Pisces-A linear plasma devices to measure the size distributions of resulting helium nano-bubbles. Nano-bubbles were fitted assuming spheroidal particles and an exponential diameter distribution. These particles had mean diameters between 0.36 and 0.62 nm. Pisces-A exposed samples showed more complex patterns, which may suggest the formation of faceted nano-bubbles or nano-scale surface structures.

  15. Shrinking plastic tubing and nonstandard diameters

    NASA Technical Reports Server (NTRS)

    Ruiz, W. V.; Thatcher, C. S.

    1980-01-01

    Process allows larger-than-normal postshrink diameters without splitting. Tetrafluoroethylene tubing on mandrel is supported within hot steel pipe by several small diameter coil sections. Rising temperature of mandrel is measured via thermocouple so assembly can be removed without overshrinking (and splitting) of tubing.

  16. Integrated NMR Core and Log Investigations With Respect to ODP LEG 204

    NASA Astrophysics Data System (ADS)

    Arnold, J.; Pechnig, R.; Clauser, C.; Anferova, S.; Blümich, B.

    2005-12-01

    NMR techniques are widely used in the oil industry and are one of the most suitable methods to evaluate in-situ formation porosity and permeability. Recently, efforts are directed towards adapting NMR methods also to the Ocean Drilling Program (ODP) and the upcoming Integrated Ocean Drilling Program (IODP). We apply a newly developed light-weight, mobile NMR core scanner as a non-destructive instrument to determine routinely rock porosity and to estimate the pore size distribution. The NMR core scanner is used for transverse relaxation measurements on water-saturated core sections using a CPMG sequence with a short echo time. A regularized Laplace-transform analysis yields the distribution of transverse relaxation times T2. In homogeneous magnetic fields, T2 is proportional to the pore diameter of rocks. Hence, the T2 signal maps the pore-size distribution of the studied rock samples. For fully saturated samples the integral of the distribution curve and the CPMG echo amplitude extrapolated to zero echo time are proportional to porosity. Preliminary results show that the NMR core scanner is a suitable tool to determine rock porosity and to estimate pore size distribution of limestones and sandstones. Presently our investigations focus on Leg 204, where NMR Logging-While-Drilling (LWD) was performed for the first time in ODP. Leg 204 was drilled into Hydrate Ridge on the Cascadia accretionary margin, offshore Oregon. All drilling and logging operations were highly successful, providing excellent core, wireline, and LWD data from adjacent boreholes. Cores recovered during Leg 204 consist mainly of clay and claystone. As the NMR core scanner operates at frequencies higher than that of the well-logging sensor it has a shorter dead time. This advantage makes the NMR core scanner sensitive to signals with T2 values down to 0.1 ms as compared to 3 ms in NMR logging. Hence, we can study even rocks with small pores, such as the mudcores recovered during Leg 204. We present a comparison of data from core scanning and NMR logging. Future integration of conventional wireline data and electrical borehole wall images (RAB/FMS) will provide a detailed characterization of the sediments in terms of lithology, petrophysics and, fluid flow properties.

  17. 77 FR 67336 - Certain Small Diameter Carbon and Alloy Seamless Standard, Line and Pressure Pipe From Romania...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2012-11-09

    ... products subject to the order are small diameter seamless carbon and alloy (other than stainless) steel... Carbon and Alloy Seamless Standard, Line and Pressure Pipe From Romania: Final Results of Antidumping... alloy seamless standard, line and pressure pipe from Romania. The period of review is August 1, 2010...

  18. Investigating the use of small-diameter softwood as guardrail posts (dynamic test results)

    Treesearch

    Jason A. Hascall; John D. Reid; Ronald K. Faller; Dean L. Sicking; David E. Kretschmann

    2007-01-01

    A modified version of the Midwest Guardrail System (MGS), utilizing small-diameter round wood posts, was developed, tested, and evaluated. Three systems were developed using different species of timber, Douglas Fir, Ponderosa Pine, and Southern Yellow Pine. A combination of Barrier VII computer simulation modeling and several series of cantilever bogie tests, conducted...

  19. Small-diameter roundwood, strong-post W-beam guardrail systems

    Treesearch

    David Kretschmann; Ronald Faller; John Reid; Jason Hascall; Dean Sicking; John Rohde

    2006-01-01

    Round guardrail posts may provide an important value-added option for small-diameter thinnings. Such posts require minimum processing and are believed to have higher strength for the equivalent rectangular volume. The resulting value-added product may bring a higher return compared to lumber. The obstacles to immediate utilization of ponderosa pine and Douglas-fir...

  20. Small-diameter trees used for chemithermomechanical pulps.

    Treesearch

    Gary C. Myers; R. James Barbour; Said M. AbuBakr

    2003-01-01

    To restore and maintain forest ecosystem health and function in the western interior of the United States, many small-diameter stems need to be removed from densely stocked stands. In general, these materials are underutilized. Information on the properties of these resources is needed to help forest managers understand when timber sales are a viable option to...

  1. Optimizing lodgepole pine submerchantable log thermomechanical pulp

    Treesearch

    Gary C. Myers

    2004-01-01

    To restore and maintain ecosystem health and function in the western interior of the United States, many small-diameter stems need to be removed from densely stocked stands. These stems are considered nonusable or underutilized (good, economical uses need to be developed). As of now, the most logical use for the small-diameter resource is pulp. In this study,...

  2. Strength of small-diameter round and tapered bending members

    Treesearch

    Ron Wolfe; Joe Murphy

    2005-01-01

    An early focus on structural use of processed rather than round timber resulted in an underestimation of the structural advantages of retaining the natural form of small-diameter round timber. In the round and tapered form, timbers are not susceptible to the strength-reducing effects of diving grain and exposed juvenile wood. Fiber continuity around knots on the...

  3. Potential for small-diameter sawtimber utilization by the current sawmill industry in western North America.

    Treesearch

    Francis G. Wagner; Charles E. Keegan; Roger D. Fight; Susan Willits

    1998-01-01

    New silvicultural prescriptions for ecosystem management on both public and private timberlands in western North America will likely result in an influx of relatively small-diameter sawtimber for processing. Since sawmills currently process a majority of sawtimber harvested in western North America (more than 80% in some regions), this study concentrated on...

  4. Assessment of subsurface chlorinated solvent contamination using tree cores at the front street site and a former dry cleaning facility at the Riverfront Superfund site, New Haven, Missouri, 1999-2003

    USGS Publications Warehouse

    Schumacher, John G.; Struckhoff, Garrett C.; Burken, Joel G.

    2004-01-01

    Tree-core sampling has been a reliable and inexpensive tool to quickly assess the presence of shallow (less than about 30 feet deep) tetrachloroethene (PCE) and trichloroethene (TCE) contamination in soils and ground water at the Riverfront Superfund Site. This report presents the results of tree-core sampling that was successfully used to determine the presence and extent of chlorinated solvent contamination at two sites, the Front Street site (operable unit OU1) and the former dry cleaning facility, that are part of the overall Riverfront Superfund Site. Traditional soil and ground-water sampling at these two sites later confirmed the results from the tree-core sampling. Results obtained from the tree-core sampling were used to design and focus subsequent soil and ground-water investigations, resulting in substantial savings in time and site assessment costs. The Front Street site is a small (less than 1-acre) site located on the Missouri River alluvium in downtown New Haven, Missouri, about 500 feet from the south bank of the Missouri River. Tree-core sampling detected the presence of subsurface PCE contamination at the Front Street site and beneath residential property downgradient from the site. Core samples from trees at the site contained PCE concentrations as large as 3,850 mg-h/kg (micrograms in headspace per kilogram of wet core) and TCE concentrations as large as 249 mg-h/kg. Soils at the Front Street site contained PCE concentrations as large as 6,200,000 mg/kg (micrograms per kilogram) and ground-water samples contained PCE concentrations as large as 11,000 mg/L (micrograms per liter). The former dry cleaning facility is located at the base of the upland that forms the south bank of the Missouri River alluvial valley. Tree-core sampling did not indicate the presence of PCE or TCE contamination at the former dry cleaning facility, a finding that was later confirmed by the analyses of soil samples collected from the site. The lateral extent of PCE contamination in trees was in close agreement with the extent of subsurface PCE contamination determined using traditional soil and ground-water sampling methods. Trees growing in soils containing PCE concentrations of 60 to 5,700 mg/kg or larger or overlying ground water containing PCE concentrations from 5 to 11,000 mg/L generally contained detectable concentrations of PCE. The depth to contaminated ground water was about 20 to 25 feet below the land surface. Significant quantitative relations [probability (p) values of less than 0.05 and correlation coefficient (r2) values of 0.88 to 0.90] were found between PCE concentrations in trees and subsurface soils between 4 and 16 feet deep. The relation between PCE concentrations in trees and underlying ground water was less apparent (r2 value of 0.17) and the poor relation is thought to be the result of equilibrium with PCE concentrations in soil and vapor in the unsaturated zone. Based on PCE concentrations detected in trees at the Front Street site and trees growing along contaminated tributaries in other operable units, and from field hydroponic experiments using hybrid poplar cuttings, analysis of tree-core samples appears to be able to detect subsurface PCE contamination in soils at levels of several hundred micrograms per liter or less and PCE concentrations in the range of 8 to 30 mg/L in ground water in direct contact with the roots. Loss of PCE from tree trunks by diffusion resulted in an exponential decrease in PCE concentrations with increasing height above the land surface in most trees. The rate of loss also appeared to be a function of the size and growth characteristics of the tree as some trees exhibited a linear loss with increasing height. Diffusional loss of PCE in small (0.5-inch diameter) trees was observed to occur at a rate more than 10 times larger than in trees 6.5 inches in diameter. Concentrations of PCE also exhibited directional variability around the tree trunks and concentration differe

  5. The effects of hindlimb unweighting on the capacitance of rat small mesenteric veins

    NASA Technical Reports Server (NTRS)

    Dunbar, S. L.; Berkowitz, D. E.; Brooks-Asplund, E. M.; Shoukas, A. A.

    2000-01-01

    Microgravity is associated with an impaired cardiac output response to orthostatic stress. Mesenteric veins are critical in modulating cardiac filling through venoconstriction. The purpose of this study was to determine the effects of simulated microgravity on the capacitance of rat mesenteric small veins. We constructed pressure-diameter relationships from vessels of 21-day hindlimb-unweighted (HLU) rats and control rats by changing the internal pressure and measuring the external diameter. Pressure-diameter relationships were obtained both before and after stimulation with norepinephrine (NE). The pressure-diameter curves of HLU vessels were shifted to larger diameters than control vessels. NE (10(-4) M) constricted veins from control animals such that the pressure-diameter relationship was significantly shifted downward (i.e., to smaller diameters at equal pressure). NE had no effect on vessels from HLU animals. These results indicate that, after HLU, unstressed vascular volume may be increased and can no longer decrease in response to sympathetic stimulation. This may partially underlie the mechanism leading to the exaggerated fall in cardiac output and stroke volume seen in astronauts during an orthostatic stress after exposure to microgravity.

  6. Ecological Importance of Large-Diameter Trees in a Temperate Mixed-Conifer Forest

    PubMed Central

    Lutz, James A.; Larson, Andrew J.; Swanson, Mark E.; Freund, James A.

    2012-01-01

    Large-diameter trees dominate the structure, dynamics and function of many temperate and tropical forests. Although both scaling theory and competition theory make predictions about the relative composition and spatial patterns of large-diameter trees compared to smaller diameter trees, these predictions are rarely tested. We established a 25.6 ha permanent plot within which we tagged and mapped all trees ≥1 cm dbh, all snags ≥10 cm dbh, and all shrub patches ≥2 m2. We sampled downed woody debris, litter, and duff with line intercept transects. Aboveground live biomass of the 23 woody species was 507.9 Mg/ha, of which 503.8 Mg/ha was trees (SD = 114.3 Mg/ha) and 4.1 Mg/ha was shrubs. Aboveground live and dead biomass was 652.0 Mg/ha. Large-diameter trees comprised 1.4% of individuals but 49.4% of biomass, with biomass dominated by Abies concolor and Pinus lambertiana (93.0% of tree biomass). The large-diameter component dominated the biomass of snags (59.5%) and contributed significantly to that of woody debris (36.6%). Traditional scaling theory was not a good model for either the relationship between tree radii and tree abundance or tree biomass. Spatial patterning of large-diameter trees of the three most abundant species differed from that of small-diameter conspecifics. For A. concolor and P. lambertiana, as well as all trees pooled, large-diameter and small-diameter trees were spatially segregated through inter-tree distances <10 m. Competition alone was insufficient to explain the spatial patterns of large-diameter trees and spatial relationships between large-diameter and small-diameter trees. Long-term observations may reveal regulation of forest biomass and spatial structure by fire, wind, pathogens, and insects in Sierra Nevada mixed-conifer forests. Sustaining ecosystem functions such as carbon storage or provision of specialist species habitat will likely require different management strategies when the functions are performed primarily by a few large trees as opposed to many smaller trees. PMID:22567132

  7. Rare-earth-doped optical-fiber core deposition using full vapor-phase SPCVD process

    NASA Astrophysics Data System (ADS)

    Barnini, A.; Robin, T.; Cadier, B.; Aka, G.; Caurant, D.; Gotter, T.; Guyon, C.; Pinsard, E.; Guitton, P.; Laurent, A.; Montron, R.

    2017-02-01

    One key parameter in the race toward ever-higher power fiber lasers remains the rare earth doped optical core quality. Modern Large Mode Area (LMA) fibers require a fine radial control of the core refractive index (RI) close to the silica level. These low RI are achieved with multi-component materials that cannot be readily obtained using conventional solution doping based Modified Chemical Vapor Deposition (MCVD) technology. This paper presents a study of such optical material obtained through a full-vapor phase Surface Plasma Chemical Vapor Deposition (SPCVD). The SPCVD process generates straight glassy films on the inner surface of a thermally regulated synthetic silica tube under vacuum. The first part of the presented results points out the feasibility of ytterbium-doped aluminosilicate fibers by this process. In the second part we describe the challenge controlling the refractive index throughout the core diameter when using volatile fluorine to create efficient LMA fiber profiles. It has been demonstrated that it is possible to counter-act the loss of fluorine at the center of the core by adjusting the core composition locally. Our materials yielded, when used in optical fibers with numerical apertures ranging from 0.07 to 0.09, power conversion efficiency up to 76% and low background losses below 20 dB/km at 1100nm. Photodarkening has been measured to be similar to equivalent MCVD based fibers. The use of cerium as a co-dopant allowed for a complete mitigation of this laser lifetime detrimental effect. The SPCVD process enables high capacity preforms and is particularly versatile when it comes to radial tailoring of both rare earth doping level and RI. Large core diameter preforms - up to 4mm - were successfully produced.

  8. Feasibility of utilizing small diameter southern pine for biomass in the Virginia Coastal Plain

    Treesearch

    Nathan C. Hanzelka; M. Chad Bolding; Scott M. Barrett; Jay Sullivan

    2016-01-01

    New or retrofitted wood-fired energy plants have increased demand for woody biomass in the stateof Virginia. Loblolly pine (Pinus taeda) commonly serves as a feedstock for these energy plants. Pulpwood conventionally requires a minimum diameter of 4 inches diameter at breast height (DBH) for merchantability, whereas a minimum merchantable diameter...

  9. An automated full waveform logging system for high-resolution P-wave profiles in marine sediments

    NASA Astrophysics Data System (ADS)

    Breitzke, Monika; Spieβ, Volkhard

    1993-11-01

    An automated, PC-based logging system has been developed to investigate marine sediment cores by full waveform transmission seismograms. High-resolution P-wave velocity and amplitude attenuation profiles are simultaneously derived from the transmission data to characterize the acoustic properties of the sediment column. A pair of ultrasonic, piezoelectric wheel probes is used to generate and record the transmission signals travelling radially through the sediment core. Both unsplit and split cores are allowed. Mounted in a carriage driven by a stepping motor via a shaft the probes automatically move along the core liner, stopping at equidistant spacings to provide a quasi-continuous inspection of the core by the transmission data. The axial travel distance and the core diameter are determined by digital measuring tools. First arrivals are picked automatically from the transmission seismograms using either a threshold in the seismogram's envelope or a cross-correlation algorithm taking the ‘zero-offset’ signal of both wheel probes into account. Combined with the core diameter these first arrivals lead to a P-wave velocity profile with a relative precision of 1 to 2 m s-1. Simultaneously, the maximum peak-to-peak amplitudes of the transmission seismograms are evaluated to get a first idea on the amplitude attenuation along the sediment core. Two examples of gravity cores taken during a recent cruise of R.V. METEOR in the Western Equatorial Atlantic are presented. They yield that the P-wave profiles can be used for locating strong and fine-scale lithological changes, e.g. turbidite layers and slight variations in the sand, silt or clay content. In addition, the transmission seismograms and their amplitude spectra obviously seem to reveal a correlation between the relative amount of low-frequency spectral components and the sediment grain size, and thus provide a tool for the determination of additional, related physical or sedimentological parameters in future investigations.

  10. Soil architecture relationships with dynamic soil physical processes: a conceptual study using natural, artificial, and 3D-printed soil cores

    NASA Astrophysics Data System (ADS)

    Lamandé, Mathieu; Schjønning, Per; Dal Ferro, Nicola; Morari, Francesco

    2017-04-01

    Pore system architecture is a key feature for understanding physical, biological and chemical processes in soils. Development of visualisation technics, especially x-ray CT, during recent years has been useful in describing the complex relationships between soil architecture and soil functions. We believe that combining visualization with physical models is a step further towards a better understanding of these relationships. We conducted a concept study using natural, artificial and 3D-printed soil cores. Eight natural soil cores (100 cm3) were sampled in a cultivated stagnic Luvisol at two depths (topsoil and subsoil), representing contrasting soil pore systems. Cylinders (100 cm3) were produced from plastic or from autoclaved aerated concrete. Holes of diameters 1.5 and 3 mm were drilled in the cylinder direction for the plastic cylinder and for one of the AAC cylinders. All natural and artificial cores were scanned in a micro x-ray CT scanner at a resolution of 35 µm. The reconstructed image of each soil core was printed with 3D multijet printing technology at a resolution of 29 µm. In some reconstructed digital volumes of the natural soil cores, pores of different sizes (equivalent diameter of 35, 70, 100, and 200 µm) were removed before additional 3D printing. Effective air-filled porosity, Darcian air permeability, and oxygen diffusion were measured on all natural, artificial and printed cores. The comparison of the natural and the artificial cores emphasized the difference in pore architecture between topsoil (sponge like) and subsoil (dominated by large vertical macropores). This study showed the high potential of using printed soil cores for understanding soil pore functions. The results confirm the suitability of the Ball model partitioning the pore system into arterial, marginal and remote pores to describe effects of soil structure on gas transport.

  11. Single-Step Assembly of Multi-Modal Imaging Nanocarriers: MRI and Long-Wavelength Fluorescence Imaging

    PubMed Central

    Pinkerton, Nathalie M.; Gindy, Marian E.; Calero-DdelC, Victoria L.; Wolfson, Theodore; Pagels, Robert F.; Adler, Derek; Gao, Dayuan; Li, Shike; Wang, Ruobing; Zevon, Margot; Yao, Nan; Pacheco, Carlos; Therien, Michael J.; Rinaldi, Carlos; Sinko, Patrick J.

    2015-01-01

    MRI and NIR-active, multi-modal Composite NanoCarriers (CNCs) are prepared using a simple, one-step process, Flash NanoPrecipitation (FNP). The FNP process allows for the independent control of the hydrodynamic diameter, co-core excipient and NIR dye loading, and iron oxide-based nanocrystal (IONC) content of the CNCs. In the controlled precipitation process, 10 nm IONCs are encapsulated into poly(ethylene glycol) stabilized CNCs to make biocompatible T2 contrast agents. By adjusting the formulation, CNC size is tuned between 80 and 360 nm. Holding the CNC size constant at an intensity weighted average diameter of 99 ± 3 nm (PDI width 28 nm), the particle relaxivity varies linearly with encapsulated IONC content ranging from 66 to 533 mM-1s-1 for CNCs formulated with 4 to 16 wt% IONC. To demonstrate the use of CNCs as in vivo MRI contrast agents, CNCs are surface functionalized with liver targeting hydroxyl groups. The CNCs enable the detection of 0.8 mm3 non-small cell lung cancer metastases in mice livers via MRI. Incorporating the hydrophobic, NIR dye PZn3 into CNCs enables complementary visualization with long-wavelength fluorescence at 800 nm. In vivo imaging demonstrates the ability of CNCs to act both as MRI and fluorescent imaging agents. PMID:25925128

  12. Temperature structure in the Perseus cluster core observed with Hitomi

    NASA Astrophysics Data System (ADS)

    Hitomi Collaboration; Aharonian, Felix; Akamatsu, Hiroki; Akimoto, Fumie; Allen, Steven W.; Angelini, Lorella; Audard, Marc; Awaki, Hisamitsu; Axelsson, Magnus; Bamba, Aya; Bautz, Marshall W.; Blandford, Roger; Brenneman, Laura W.; Brown, Gregory V.; Bulbul, Esra; Cackett, Edward M.; Chernyakova, Maria; Chiao, Meng P.; Coppi, Paolo S.; Costantini, Elisa; de Plaa, Jelle; de Vries, Cor P.; den Herder, Jan-Willem; Done, Chris; Dotani, Tadayasu; Ebisawa, Ken; Eckart, Megan E.; Enoto, Teruaki; Ezoe, Yuichiro; Fabian, Andrew C.; Ferrigno, Carlo; Foster, Adam R.; Fujimoto, Ryuichi; Fukazawa, Yasushi; Furukawa, Maki; Furuzawa, Akihiro; Galeazzi, Massimiliano; Gallo, Luigi C.; Gandhi, Poshak; Giustini, Margherita; Goldwurm, Andrea; Gu, Liyi; Guainazzi, Matteo; Haba, Yoshito; Hagino, Kouichi; Hamaguchi, Kenji; Harrus, Ilana M.; Hatsukade, Isamu; Hayashi, Katsuhiro; Hayashi, Takayuki; Hayashida, Kiyoshi; Hiraga, Junko S.; Hornschemeier, Ann; Hoshino, Akio; Hughes, John P.; Ichinohe, Yuto; Iizuka, Ryo; Inoue, Hajime; Inoue, Yoshiyuki; Ishida, Manabu; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iwai, Masachika; Kaastra, Jelle; Kallman, Tim; Kamae, Tsuneyoshi; Kataoka, Jun; Kato, Yuichi; Katsuda, Satoru; Kawai, Nobuyuki; Kelley, Richard L.; Kilbourne, Caroline A.; Kitaguchi, Takao; Kitamoto, Shunji; Kitayama, Tetsu; Kohmura, Takayoshi; Kokubun, Motohide; Koyama, Katsuji; Koyama, Shu; Kretschmar, Peter; Krimm, Hans A.; Kubota, Aya; Kunieda, Hideyo; Laurent, Philippe; Lee, Shiu-Hang; Leutenegger, Maurice A.; Limousin, Olivier; Loewenstein, Michael; Long, Knox S.; Lumb, David; Madejski, Greg; Maeda, Yoshitomo; Maier, Daniel; Makishima, Kazuo; Markevitch, Maxim; Matsumoto, Hironori; Matsushita, Kyoko; McCammon, Dan; McNamara, Brian R.; Mehdipour, Missagh; Miller, Eric D.; Miller, Jon M.; Mineshige, Shin; Mitsuda, Kazuhisa; Mitsuishi, Ikuyuki; Miyazawa, Takuya; Mizuno, Tsunefumi; Mori, Hideyuki; Mori, Koji; Mukai, Koji; Murakami, Hiroshi; Mushotzky, Richard F.; Nakagawa, Takao; Nakajima, Hiroshi; Nakamori, Takeshi; Nakashima, Shinya; Nakazawa, Kazuhiro; Nobukawa, Kumiko K.; Nobukawa, Masayoshi; Noda, Hirofumi; Odaka, Hirokazu; Ohashi, Takaya; Ohno, Masanori; Okajima, Takashi; Ota, Naomi; Ozaki, Masanobu; Paerels, Frits; Paltani, Stéphane; Petre, Robert; Pinto, Ciro; Porter, Frederick S.; Pottschmidt, Katja; Reynolds, Christopher S.; Safi-Harb, Samar; Saito, Shinya; Sakai, Kazuhiro; Sasaki, Toru; Sato, Goro; Sato, Kosuke; Sato, Rie; Sawada, Makoto; Schartel, Norbert; Serlemtsos, Peter J.; Seta, Hiromi; Shidatsu, Megumi; Simionescu, Aurora; Smith, Randall K.; Soong, Yang; Stawarz, Łukasz; Sugawara, Yasuharu; Sugita, Satoshi; Szymkowiak, Andrew; Tajima, Hiroyasu; Takahashi, Hiromitsu; Takahashi, Tadayuki; Takeda, Shiníchiro; Takei, Yoh; Tamagawa, Toru; Tamura, Takayuki; Tanaka, Takaaki; Tanaka, Yasuo; Tanaka, Yasuyuki T.; Tashiro, Makoto S.; Tawara, Yuzuru; Terada, Yukikatsu; Terashima, Yuichi; Tombesi, Francesco; Tomida, Hiroshi; Tsuboi, Yohko; Tsujimoto, Masahiro; Tsunemi, Hiroshi; Tsuru, Takeshi Go; Uchida, Hiroyuki; Uchiyama, Hideki; Uchiyama, Yasunobu; Ueda, Shutaro; Ueda, Yoshihiro; Uno, Shiníchiro; Urry, C. Megan; Ursino, Eugenio; Watanabe, Shin; Werner, Norbert; Wilkins, Dan R.; Williams, Brian J.; Yamada, Shinya; Yamaguchi, Hiroya; Yamaoka, Kazutaka; Yamasaki, Noriko Y.; Yamauchi, Makoto; Yamauchi, Shigeo; Yaqoob, Tahir; Yatsu, Yoichi; Yonetoku, Daisuke; Zhuravleva, Irina; Zoghbi, Abderahmen

    2018-03-01

    The present paper explains the temperature structure of X-ray emitting plasma in the core of the Perseus cluster based on 1.8-20.0 keV data obtained with the Soft X-ray Spectrometer (SXS) on board the Hitomi Observatory. A series of four observations was carried out, with a total effective exposure time of 338 ks that covered a central region of ˜7΄ in diameter. SXS was operated with an energy resolution of ˜5 eV (full width at half maximum) at 5.9 keV. Not only fine structures of K-shell lines in He-like ions, but also transitions from higher principal quantum numbers were clearly resolved from Si through Fe. That enabled us to perform temperature diagnostics using the line ratios of Si, S, Ar, Ca, and Fe, and to provide the first direct measurement of the excitation temperature and ionization temperature in the Perseus cluster. The observed spectrum is roughly reproduced by a single-temperature thermal plasma model in collisional ionization equilibrium, but detailed line-ratio diagnostics reveal slight deviations from this approximation. In particular, the data exhibit an apparent trend of increasing ionization temperature with the atomic mass, as well as small differences between the ionization and excitation temperatures for Fe, the only element for which both temperatures could be measured. The best-fit two-temperature models suggest a combination of 3 and 5 keV gas, which is consistent with the idea that the observed small deviations from a single-temperature approximation are due to the effects of projecting the known radial temperature gradient in the cluster core along the line of sight. A comparison with the Chandra/ACIS and the XMM-Newton/RGS results, on the other hand, suggests that additional lower-temperature components are present in the intracluster medium (ICM), but not detectable with Hitomi/SXS giving its 1.8-20 keV energy band.

  13. Directional Solidification and Convection in Small Diameter Crucibles

    NASA Technical Reports Server (NTRS)

    Chen, J.; Sung, P. K.; Tewari, S. N.; Poirier, D. R.; DeGroh, H. C., III

    2003-01-01

    Pb-2.2 wt% Sb alloy was directionally solidified in 1, 2, 3 and 7 mm diameter crucibles. Pb-Sb alloy presents a solutally unstable case. Under plane-front conditions, the resulting macrosegregation along the solidified length indicates that convection persists even in the 1 mm diameter crucible. Al-2 wt% Cu alloy was directionally solidified because this alloy was expected to be stable with respect to convection. Nevertheless, the resulting macrosegregation pattern and the microstructure in solidified examples indicated the presence of convection. Simulations performed for both alloys show that convection persists for crucibles as small as 0.6 mm of diameter. For the solutally stable alloy, Al-2 wt% Cu, the simulations indicate that the convection arises from a lateral temperature gradient.

  14. Development of welded metal bellows having minimum effective diameter change

    NASA Technical Reports Server (NTRS)

    Henschel, J. K.; Stevens, J. B.; Harvey, A. C.; Howland, J. S.; Rhee, S. S.

    1972-01-01

    A program of analysis, design, and fabrication was conducted to develop welded metal bellows having a minimum change in effective diameter for cryogenic turbomachinery face seal applications. Linear analysis of the principle types of bellows provided identification of concepts capable of meeting basic operation requirements. For the 6-inch (.152 m) mean diameter, 1.5-inch free length bellows studied, nonlinear analysis showed that opposed and nested toroidal bellows plates stiffened by means of alternating stiffener rings were capable of maintaining constant effective diameter within 0.3% and 0.1% respectively under the operating conditions of interest. Changes in effective diameter were due principally to bellows axial deflection with pressure differential having a lesser influence. Fabrication problems associated with joining the thin bellows plates to the relatively heavy stiffener rings were encountered and precluded assembly and testing of a bellows core. Fabrication problems are summarized and recommended fabrication methods for future effort are presented.

  15. Formation of hexagonal boron nitride nanoscrolls induced by inclusion and exclusion of self-assembling molecules in solution process.

    PubMed

    Hwang, Da Young; Suh, Dong Hack

    2014-06-07

    Unlike nanoscrolls of 2D graphene, those of 2D h-BN have not been demonstrated, except for only a few experimental reports. Nanoscrolls of h-BN with high yields and reproducibility are first synthesized by a simple solution process. Inner-tube diameters of BNSs including LCAs, N-(2-aminoethyl)-3α-hydroxy-5β-cholan-24-amide, a bile acid derivative and self-assembling material, can be controlled by adjusting the diameter of the LCA fiber which is grown by self-assembly. TEM and SEM images show that BNSs have a tube-like morphology and the inner-tube diameter of BNSs can be controlled in the range from 20 to 60 nm for a smaller diameter, up to 300 nm for a larger diameter by LCA fiber growth inside the BNSs. Finally, open cylindrical BNSs with hollow cores were obtained by dissolving LCAs inside BNSs.

  16. In situ X-ray micro-CT characterization of chemo-mechanical relaxations during Sn lithiation

    NASA Astrophysics Data System (ADS)

    Gonzalez, Joseph F.; Antartis, Dimitrios A.; Chasiotis, Ioannis; Dillon, Shen J.; Lambros, John

    2018-03-01

    Sn has been proposed for use as a high capacity anode material. Because of its ductile metallic nature, Sn may exhibit unique stress evolution during lithiation. Here, 2D radiography and 3D tomography are employed to visualize the evolution of geometry, internal structure, alloying, and damage during lithiation, delithiation, and rest of Sn wires with micron scale diameters. Lithiation proceeds isotropically, resulting in geometric and dimensional changes after 25% of total lithiation when the tensile stresses are sufficiently high to exceed the flow stress of the unlithiated Sn core and cause elongation and diameter increase. Damage occurs at later stages in the form of cracks terminating at the wire surface and voids forming in the unlithiated core. Notably, significant fragmentation occurs during delithiation which, due to void formation that accommodates the resulting stresses, does not measurably alter the wire cross-section and length. The distinguishing feature of the chemo-mechanics of Sn compared to Si or Ge is the pronounced creep rate at applied strain rates as high as 10-6 s-1, which promotes large strains in the core, eventually leading to void nucleation in the unlithiated core during lithiation, and more importantly, continues driving the deformation of the anode while at rest.

  17. Manson impact structure, Iowa: First geochemical results for drill core M-1

    NASA Technical Reports Server (NTRS)

    Koeberl, Christian; Anderson, Raymond R.; Hartung, Jack B.; Reimold, Wolf Uwe

    1993-01-01

    The Manson Impact Structure is a large complex impact crater centered ca. S km north of the town of Manson, Iowa. It is the largest intact impact structure recognized in the United States (35 km in diameter). Its Ar-40/Ar-39 age is indistinguishable from that of the Cretaceous-Tertiary (K-T) boundary. The Manson structure may be one element of the events at the K-T boundary. The crater is completely covered by Quaternary glacial sedimentary deposits that are normally underlain by Cretaceous clastic sediments and flat-lying carbonate sediments of Phanerozoic age, as well as Proterozoic red clastic, metamorphic, volcanic, and plutonic rock sequences. The study of a reflection seismic profile, provided by Amoco, was critical in interpreting the structure. In the 35 km diameter zone that marks the extension of the crater the normal rock sequence is disturbed due to the impact, and at the center of the structure granitic basement rocks are present that have been uplifted from about 4 km depth. Our studies consist of detailed petrological and geochemical characterization of all cores, with emphasis on a detailed description of all rock types found in the core samples and their relationship to target rocks. Geochemical data on samples from the Manson M-1 core are presented.

  18. Manson impact structure, Iowa: First geochemical results for drill core M-1

    NASA Astrophysics Data System (ADS)

    Koeberl, Christian; Anderson, Raymond R.; Hartung, Jack B.; Reimold, Wolf Uwe

    1993-03-01

    The Manson Impact Structure is a large complex impact crater centered ca. S km north of the town of Manson, Iowa. It is the largest intact impact structure recognized in the United States (35 km in diameter). Its Ar-40/Ar-39 age is indistinguishable from that of the Cretaceous-Tertiary (K-T) boundary. The Manson structure may be one element of the events at the K-T boundary. The crater is completely covered by Quaternary glacial sedimentary deposits that are normally underlain by Cretaceous clastic sediments and flat-lying carbonate sediments of Phanerozoic age, as well as Proterozoic red clastic, metamorphic, volcanic, and plutonic rock sequences. The study of a reflection seismic profile, provided by Amoco, was critical in interpreting the structure. In the 35 km diameter zone that marks the extension of the crater the normal rock sequence is disturbed due to the impact, and at the center of the structure granitic basement rocks are present that have been uplifted from about 4 km depth. Our studies consist of detailed petrological and geochemical characterization of all cores, with emphasis on a detailed description of all rock types found in the core samples and their relationship to target rocks. Geochemical data on samples from the Manson M-1 core are presented.

  19. One step growth of GaN/SiO2 core/shell nanowire in vapor-liquid-solid route by chemical vapor deposition technique

    NASA Astrophysics Data System (ADS)

    Barick, B. K.; Yadav, Shivesh; Dhar, S.

    2017-11-01

    GaN/SiO2 core/shell nanowires are grown by cobalt phthalocyanine catalyst assisted vapor-liquid-solid route, in which Si wafer coated with a mixture of gallium and indium is used as the source for Ga and Si and ammonia is used as the precursor for nitrogen and hydrogen. Gallium in the presence of indium and hydrogen, which results from the dissociation of ammonia, forms Si-Ga-In alloy at the growth temperature ∼910 °C. This alloy acts as the source of Si, Ga and In. A detailed study using a variety of characterization tools reveals that these wires, which are several tens of micron long, has a diameter distribution of the core ranging from 20 to 50 nm, while the thickness of the amorphous SiO2 shell layer is about 10 nm. These wires grow along [ 1 0 1 bar 0 ] direction. It has also been observed that the average diameter of these wires decreases, while their density increases as the gallium proportion in the Ga-In mixture is increased.

  20. Effect of nonionic compound emulsifiers Tween80 and Span80 on the properties of microencapsulated phase change materials.

    PubMed

    Zhan, Shiping; Zhou, Zhiyi; Wang, Weijing; Zhao, Qicheng; Hou, Weimin

    2014-01-01

    In this article, the nonionic compound emulsifiers Tween80 and Span80 were used to prepare microcapsules containing phase change materials (microPCMs) with melamine-formaldehyde (MF) shells by in situ polymerization method. The effects of compound emulsifiers Tween80 and Span80 on the structure, morphologies and properties of microPCMs containing paraffin were studied. SEM morphological investigation suggests that a complex of Tween80 and Span80 as emulsifiers are optimal for the fabrication of microPCMs in this study compared to Tween60 or OP-10. The diameter distributions of microPCMs synthesized with different amounts of compound emulsifiers are uniform, whereas compound emulsifiers' amount affect the mean diameter of microPCMs decreasing from 5.34 to 3.05 µm. These microPCMs with the core/shell weight ratio 3/1 have smoother surface and a higher core content of 68.7% than other core/shell ratio. Anti-osmosis measurements indicate that microPCMs have good compactness and stable performance compared to those synthesized by one type of emulsifier.

  1. Control of the shell structural properties and cavity diameter of hollow magnesium fluoride particles.

    PubMed

    Nandiyanto, Asep Bayu Dani; Ogi, Takashi; Okuyama, Kikuo

    2014-03-26

    Control of the shell structural properties [i.e., thickness (8-25 nm) and morphology (dense and raspberry)] and cavity diameter (100-350 nm) of hollow particles was investigated experimentally, and the results were qualitatively explained based on the available theory. We found that the selective deposition size and formation of the shell component on the surface of a core template played important roles in controlling the structure of the resulting shell. To achieve the selective deposition size and formation of the shell component, various process parameters (i.e., reaction temperature and charge, size, and composition of the core template and shell components) were tested. Magnesium fluoride (MgF2) and polystyrene spheres were used as models for shell and core components, respectively. MgF2 was selected because, to the best of our knowledge, the current reported approaches to date were limited to synthesis of MgF2 in film and particle forms only. Therefore, understanding how to control the formation of MgF2 with various structures (both the thickness and morphology) is a prospective for advanced lens synthesis and applications.

  2. Angiographic core laboratory reproducibility analyses: implications for planning clinical trials using coronary angiography and left ventriculography end-points.

    PubMed

    Steigen, Terje K; Claudio, Cheryl; Abbott, David; Schulzer, Michael; Burton, Jeff; Tymchak, Wayne; Buller, Christopher E; John Mancini, G B

    2008-06-01

    To assess reproducibility of core laboratory performance and impact on sample size calculations. Little information exists about overall reproducibility of core laboratories in contradistinction to performance of individual technicians. Also, qualitative parameters are being adjudicated increasingly as either primary or secondary end-points. The comparative impact of using diverse indexes on sample sizes has not been previously reported. We compared initial and repeat assessments of five quantitative parameters [e.g., minimum lumen diameter (MLD), ejection fraction (EF), etc.] and six qualitative parameters [e.g., TIMI myocardial perfusion grade (TMPG) or thrombus grade (TTG), etc.], as performed by differing technicians and separated by a year or more. Sample sizes were calculated from these results. TMPG and TTG were also adjudicated by a second core laboratory. MLD and EF were the most reproducible, yielding the smallest sample size calculations, whereas percent diameter stenosis and centerline wall motion require substantially larger trials. Of the qualitative parameters, all except TIMI flow grade gave reproducibility characteristics yielding sample sizes of many 100's of patients. Reproducibility of TMPG and TTG was only moderately good both within and between core laboratories, underscoring an intrinsic difficulty in assessing these. Core laboratories can be shown to provide reproducibility performance that is comparable to performance commonly ascribed to individual technicians. The differences in reproducibility yield huge differences in sample size when comparing quantitative and qualitative parameters. TMPG and TTG are intrinsically difficult to assess and conclusions based on these parameters should arise only from very large trials.

  3. High-gradient compact linear accelerator

    DOEpatents

    Carder, B.M.

    1998-05-26

    A high-gradient linear accelerator comprises a solid-state stack in a vacuum of five sets of disc-shaped Blumlein modules each having a center hole through which particles are sequentially accelerated. Each Blumlein module is a sandwich of two outer conductive plates that bracket an inner conductive plate positioned between two dielectric plates with different thicknesses and dielectric constants. A third dielectric core in the shape of a hollow cylinder forms a casing down the series of center holes, and it has a dielectric constant different that the two dielectric plates that sandwich the inner conductive plate. In operation, all the inner conductive plates are charged to the same DC potential relative to the outer conductive plates. Next, all the inner conductive plates are simultaneously shorted to the outer conductive plates at the outer diameters. The signal short will propagate to the inner diameters at two different rates in each Blumlein module. A faster wave propagates quicker to the third dielectric core across the dielectric plates with the closer spacing and lower dielectric constant. When the faster wave reaches the inner extents of the outer and inner conductive plates, it reflects back outward and reverses the field in that segment of the dielectric core. All the field segments in the dielectric core are then in unipolar agreement until the slower wave finally propagates to the third dielectric core across the dielectric plates with the wider spacing and higher dielectric constant. During such unipolar agreement, particles in the core are accelerated with gradients that exceed twenty megavolts per meter. 10 figs.

  4. High-gradient compact linear accelerator

    DOEpatents

    Carder, Bruce M.

    1998-01-01

    A high-gradient linear accelerator comprises a solid-state stack in a vacuum of five sets of disc-shaped Blumlein modules each having a center hole through which particles are sequentially accelerated. Each Blumlein module is a sandwich of two outer conductive plates that bracket an inner conductive plate positioned between two dielectric plates with different thicknesses and dielectric constants. A third dielectric core in the shape of a hollow cylinder forms a casing down the series of center holes, and it has a dielectric constant different that the two dielectric plates that sandwich the inner conductive plate. In operation, all the inner conductive plates are charged to the same DC potential relative to the outer conductive plates. Next, all the inner conductive plates are simultaneously shorted to the outer conductive plates at the outer diameters. The signal short will propagate to the inner diameters at two different rates in each Blumlein module. A faster wave propagates quicker to the third dielectric core across the dielectric plates with the closer spacing and lower dielectric constant. When the faster wave reaches the inner extents of the outer and inner conductive plates, it reflects back outward and reverses the field in that segment of the dielectric core. All the field segments in the dielectric core are then in unipolar agreement until the slower wave finally propagates to the third dielectric core across the dielectric plates with the wider spacing and higher dielectric constant. During such unipolar agreement, particles in the core are accelerated with gradients that exceed twenty megavolts per meter.

  5. Creep Behavior of Oxide/Oxide Composites with Monazite Fiber Coating at 1100 deg C in Air and in Steam Environments

    DTIC Science & Technology

    2008-09-01

    monolithic ceramics initiates at small defects formed during processing. Minimization of such defects may improve performance, but thermal shock and cyclic...fiber tows are used in CMCs, where the use of small -diameter fibers causes a reduction in scale of microstructural defects associated with the fibers [7... Small Diameter · Improves matrix strength and facilitates fab- rication of thin and complex-shaped CMCs. · Low Density · Improves CMC specific properties

  6. A study on fatigue strength reduction factor for small diameter socket welded pipe joints

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Higuchi, Makoto; Nakagawa, Akira; Hayashi, Makoto

    1996-12-01

    Factors that may exert influence on the fatigue strength of small diameter socket welded joints of nominal diameter in the 20--50 mm range have been investigated by the fully reversed four-point bending fatigue test with the material, diameter, pipe schedule, throat depth, bead shape, slip-on gap, and root defect as the testing parameters. The fatigue strength of socket joints depended acutely on the diameter. When the diameter is large, the fatigue strength tended to be low and the fracture is of the root-failure mode; when it is small, on the other hand, the fatigue strength is high and the fracturemore » is of the toe-failure mode. Stainless steel proved to be superior to carbon steel; it gave rise to 1.37 times the fatigue strength of the latter for socket joints of nominal diameter 50 mm; the fatigue strength reduction factor determined at 10{sup 7} cycles with respect to the fatigue strength of smooth base metal in the fully reversed fatigue was about 4 for stainless steel and about 5 for carbon steel. The fatigue strength was higher, the larger the Sche number (i.e., the thicker the pipe wall); it was improved markedly by placing one final refinement pass on the toe or by eliminating the slip-on gap. An empirical formula relating the size of the root defect to the fatigue strength reduction has been proposed.« less

  7. Combination of small size and carboxyl functionalisation causes cytotoxicity of short carbon nanotubes

    PubMed Central

    Fröhlich, Eleonore; Meindl, Claudia; Höfler, Anita; Leitinger, Gerd; Roblegg, Eva

    2012-01-01

    The use of carbon nanotubes (CNTs) could improve medical diagnosis and treatment provided they show no adverse effects in the organism. In this study, short CNTs with different diameters with and without carboxyl surface functionalisation were assessed. After physicochemical characterisation, cytotoxicity in phagocytic and non-phagocytic cells was determined. The role of oxidative stress was evaluated according to the intracellular glutathione levels and protection by N-acetyl cysteine (NAC). In addition to this, the mode of cell death was also investigated. CNTs <8 nm acted more cytotoxic than CNTs ≥20 nm and carboxylated CNTs more than pristine CNTs. Protection by NAC was maximal for large diameter pristine CNTs and minimal for small diameter carboxylated CNTs. Thin (<8 nm) CNTs acted mainly by disruption of membrane integrity and CNTs with larger diameter induced mainly apoptotic changes. It is concluded that cytotoxicity of small carboxylated CNTs occurs by necrosis and cannot be prevented by antioxidants. PMID:22963691

  8. Piston core record of Late Paleogene (31 Ma) to recent seafloor hydrothermal activity in the Southwest Pacific Basin

    NASA Astrophysics Data System (ADS)

    Stancin, Andrea M.; Gleason, James D.; Owen, Robert M.; Rea, David K.; Blum, Joel D.

    2008-03-01

    A large diameter piston core containing 8.35 m of metalliferous sediment has been recovered from a small abyssal valley in the remote Southwest Pacific Basin (31° 42.194'S, 143° 30° 331'W; 5082 m water depth), providing unique insight into hydrothermal activity and eolian sedimentation there since the early Oligocene. A combination of fish-teeth Sr-isotope stratigraphy and INAA geochemical data reveals an exponentially decreasing hydrothermal flux 31 Ma to the present. Although hydrothermal sedimentation related to seafloor spreading explains this trend, a complex history of late Eocene/early Oligocene ridge jumps, propagating rifts and plate tectonic reorganization of South Pacific seafloor could have also played a role. A possible hiatus in deposition, as recorded by changes in core composition just below 2 m depth, is beyond the resolution of the fish teeth Sr isotope dating method employed here; however, the timing of this interval may be coincident with extinction of the Pacific-Farallon Ridge at ˜20 Ma. A low flux eolian component accumulating at this site shows an increase relative to the hydrothermal component above 2 m depth, consistent with dust-generating continental sources far to the west (Australia/New Zealand). This is the first long-term paleoceanographic record obtained from within the South Pacific "bare zone" (Rea et al., 2006), an anomalous region where Pacific seafloor has largely escaped sediment accumulation since the Late Cretaceous.

  9. On the Scattering of Sound by a Rectilinear Vortex

    NASA Astrophysics Data System (ADS)

    HOWE, M. S.

    1999-11-01

    A re-examination is made of the two-dimensional interaction of a plane, time-harmonic sound wave with a rectilinear vortex of small core diameter at low Mach number. Sakov [1] and Ford and Smith [2] have independently resolved the “infinite forward scatter” paradox encountered in earlier applications of the Born approximation to this problem. The first order scattered field (Born approximation) has nulls in the forward and back scattering directions, but the interaction of the wave with non-acoustically compact components of the vortex velocity field causes wavefront distortion, and the phase of the incident wave to undergo a significant variation across a parabolic domain whose axis extends along the direction of forward scatter from the vortex core. The transmitted wave crests of the incident wave become concave and convex, respectively, on opposite sides of the axis of the parabola, and focusing and defocusing of wave energy produces corresponding increases and decreases in wave amplitude. Wave front curvature decreases with increasing distance from the vortex core, with the result that the wave amplitude and phase are asymptotically equal to the respective values they would have attained in the absence of the vortex. The transverse acoustic dipole generated by translational motion of the vortex at the incident wave acoustic particle velocity, and the interaction of the incident wave with acoustically compact components of the vortex velocity field, are responsible for a system of cylindrically spreading, scattered waves outside the parabolic domain.

  10. Fabrication of multifilamentary Nb/sub 3/(Al,Ge) wires through a modified jelly roll process

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Tachikawa, K.; Kamisada, Y.; Suzuki, E.

    Recently, development of Nb/sub 3/Al multifilamentary wires has gained much interests since high-field performance superior to that of Nb/sub 3/Sn can be expected in these wires. In this study, Nb/Al-Ge alloy composites were fabricated into multifilamentary wires through a modified jelly roll (MJR) process. A Nb mesh sheet produced at the Teledyne Wah Chang Co. was used as Nb component. An Al-Ge alloy prepared by a conventional casting process was forged and rolled into a sheet of 0.2 mm in thickness. The Nb/Al-Ge composite was prepared by wrapping the Nb mesh sheet together with the Al-Ge alloy sheet around amore » Nb core into a jelly roll form. The MJR composite was encased in a Cu-Ni alloy tube of which outer diameter was 43 mm. The resulting composite was hydrostatically pressed and extruded into a rod of 18 mm in diameter. A Nb barrier was then inserted between the MJR and the Cu-Ni jacket. The composite rod was swaged and drawn into a wire without any intermediate annealing. The wire was able to be drawn down to a very small diameter of 0.1 mm. The cross-sectional configuration of the MJR composite was not much disturbed by the fabrication. Superconducting transition temperature Tc of the wire, after different heat treatment including a rapid quenching from high temperatures by a continuous electron beam irradiation, was studied, and an onset Tc of 19.3K has been achieved.« less

  11. Co7Fe3 and Co7Fe3@SiO2 Nanospheres with Tunable Diameters for High-Performance Electromagnetic Wave Absorption.

    PubMed

    Chen, Na; Jiang, Jian-Tang; Xu, Cheng-Yan; Yuan, Yong; Gong, Yuan-Xun; Zhen, Liang

    2017-07-05

    Ferromagnetic metal/alloy nanoparticles have attracted extensive interest for electromagnetic wave-absorbing applications. However, ferromagnetic nanoparticles are prone to oxidization and producing eddy currents, leading to the deterioration of electromagnetic properties. In this work, a simple and scalable liquid-phase reduction method was employed to synthesize uniform Co 7 Fe 3 nanospheres with diameters ranging from 350 to 650 nm for high-performance microwave absorption application. Co 7 Fe 3 @SiO 2 core-shell nanospheres with SiO 2 shell thicknesses of 30 nm were then fabricated via a modified Stöber method. When tested as microwave absorbers, bare Co 7 Fe 3 nanospheres with a diameter of 350 nm have a maximum reflection loss (RL) of 78.4 dB and an effective absorption with RL > 10 dB from 10 to 16.7 GHz at a small thickness of 1.59 mm. Co 7 Fe 3 @SiO 2 nanospheres showed a significantly enhanced microwave absorption capability for an effective absorption bandwidth and a shift toward a lower frequency, which is ascribed to the protection of the SiO 2 shell from direct contact among Co 7 Fe 3 nanospheres, as well as improved crystallinity and decreased defects upon annealing. This work illustrates a simple and effective method to fabricate Co 7 Fe 3 and Co 7 Fe 3 @SiO 2 nanospheres as promising microwave absorbers, and the design concept can also be extended to other ferromagnetic alloy particles.

  12. Size-dependent melting modes and behaviors of Ag nanoparticles: a molecular dynamics study

    NASA Astrophysics Data System (ADS)

    Liang, Tianshou; Zhou, Dejian; Wu, Zhaohua; Shi, Pengpeng

    2017-12-01

    The size-dependent melting behaviors and mechanisms of Ag nanoparticles (NPs) with diameters of 3.5-16 nm were investigated by molecular dynamics (MD). Two distinct melting modes, non-premelting and premelting with transition ranges of about 7-8 nm, for Ag NPs were demonstrated via the evolution of distribution and transition of atomic physical states during annealing. The small Ag NPs (3.5-7 nm) melt abruptly without a stable liquid shell before the melting point, which is characterized as non-premelting. A solid-solid crystal transformation is conducted through the migration of adatoms on the surface of Ag NPs with diameters of 3.5-6 nm before the initial melting, which is mainly responsible for slightly increasing the melting point of Ag NPs. On the other hand, surface premelting of Ag NPs with diameters of 8-16 nm propagates from the outer shell to the inner core with initial anisotropy and late isotropy as the temperature increases, and the close-packed facets {111} melt by a side-consumed way which is responsible for facets {111} melting in advance relative to the crystallographic plane {111}. Once a stable liquid shell is formed, its size-independent minimum thickness is obtained, and a three-layer structure of atomic physical states is set up. Lastly, the theory of point defect-pair (vacancy-interstitial) severing as the mechanism of formation and movement of the solid-liquid interface was also confirmed. Our study provides a basic understanding and theoretical guidance for the research, production and application of Ag NPs.

  13. Inclined Jet in Crossflow Interacting with a Vortex Generator

    NASA Technical Reports Server (NTRS)

    Zaman, K. B. M. Q.; Rigby, D .L.; Heidmann, J. D.

    2011-01-01

    An experiment is conducted on the effectiveness of a vortex generator in preventing liftoff of a jet in crossflow, with possible relevance to film-cooling applications. The jet issues into the boundary layer at an angle of 20 degreees to the freestream. The effect of a triangular ramp-shaped vortex generator is studied while varying its geometry and location. Detailed flowfield properties are obtained for a case in which the height of the vortex generator and the diameter of the orifice are comparable with the approach boundary-layer thickness. The vortex generator produces a streamwise vortex pair with a vorticity magnitude 3 times larger (and of opposite sense) than that found in the jet in crossflow alone. Such a vortex generator appears to be most effective in keeping the jet attached to the wall. The effect of parametric variation is studied mostly from surveys 10 diameters downstream from the orifice. Results over a range of jet-to-freestream momentum flux ratio (1 < J < 11) show that the vortex generator has a significant effect even at the highest J covered in the experiment. When the vortex generator height is halved, there is a liftoff of the jet. On the other hand, when the height is doubled, the jet core is dissipated due to larger turbulence intensity. Varying the location of the vortex generator, over a distance of three diameters from the orifice, is found to have little impact. Rounding off the edges of the vortex generator with the increasing radius of curvature progressively diminishes its effect. However, allowing for a small radius of curvature may be quite tolerable in practice.

  14. High peak-power kilohertz laser system employing single-stage multi-pass amplification

    DOEpatents

    Shan, Bing; Wang, Chun; Chang, Zenghu

    2006-05-23

    The present invention describes a technique for achieving high peak power output in a laser employing single-stage, multi-pass amplification. High gain is achieved by employing a very small "seed" beam diameter in gain medium, and maintaining the small beam diameter for multiple high-gain pre-amplification passes through a pumped gain medium, then leading the beam out of the amplifier cavity, changing the beam diameter and sending it back to the amplifier cavity for additional, high-power amplification passes through the gain medium. In these power amplification passes, the beam diameter in gain medium is increased and carefully matched to the pump laser's beam diameter for high efficiency extraction of energy from the pumped gain medium. A method of "grooming" the beam by means of a far-field spatial filter in the process of changing the beam size within the single-stage amplifier is also described.

  15. Improved utilization of small-diameter ponderosa pine in glulam timber

    Treesearch

    Roland Hernandez; David W. Green; David E. Kretschmann; Steven P. Verrill

    2005-01-01

    This study involved the evaluation of ponderosa pine glulam made from lumber that was sawn from a small-diameter timber resource. Two different glulam beam depths were evaluated: 8 and 13 laminations. A comprehensive glulam test program was conducted to evaluate edgewise and flat-wise bending, shear, and tensile strength. Beam deflection was measured and a variety of...

  16. Investigating the use of small-diameter softwood as guardrail posts: static test results

    Treesearch

    David E. Kretschmann; Ron Faller; Jason Hascall; John Reid; Dean Sicking; John Rohde; Dick Shilts; Tim Nelson

    2007-01-01

    Round guardrail posts may provide an important value added option for small-diameter thinnings. Such posts require minimum processing and have been shown to have higher strength compared to the equivalent rectangular volume. The resulting value-added product may bring a higher return compared to lumber. The obstacles to immediate utilization of ponderosa pine and...

  17. Structural lumber from dense stands of small-diameter Douglas-fir trees.

    Treesearch

    David W. Green; Eini C. Lowell; Roland Hernandez

    2005-01-01

    Small-diameter trees growing in overstocked dense stands are often targeted for thinning to reduce fire hazard and improve forest health and ecosystem diversity. In the Pacific Northwest and Intermountain regions, Douglas-fir can be a predominant species in such stands. In this study, mechanical properties and grade yield of structural products were estimated for 2 by...

  18. It's not easy being green: the tricky world of small-diameter timber.

    Treesearch

    Sally Duncan

    1998-01-01

    Big shifts have been made over the last decade in how society thinks forest lands should be managed. Forest policy has subsequently changed. Land managers now grapple with how to make society's intentions work in the forests of today.This issue of PNW Science Findings presents the Colville study's examination of the vast forests of small-diameter...

  19. Research challenges for structural use of small-diameter round timbers

    Treesearch

    Ron Wolfe

    2000-01-01

    Forest managers have identified forest stands overstocked with small-diameter trees as a critical forest health issue. Overstocked stands are subject to attack by insects and disease and, as a result of the heavy fuel load, risk total destruction by fire. Prescribed burning is an economic tool for suppressing the growth of brush and tree seedlings, but its use is often...

  20. Prediction of wood Quality in Small-Diameter Douglas-Fir using site and Stand Characteristics

    Treesearch

    C.D. Morrow; T.M. Gorman; J.W. Evans; D.E. Kretschmann; C.A. Hatfield

    2013-01-01

    Standing stress wave measurements were taken on 274 small-diameter Douglas-fir trees in western Montana. Stand, site, and soil measurements collected in the field and remotely through geographical information system (GIS) data layers were used to model dynamic modulus of elasticity (DMOE) in those trees. The best fit linear model developed resulted in an adjusted

  1. Exploring the uses for small-diameter trees

    Treesearch

    Susan L. LeVan-Green; Jean. Livingston

    2001-01-01

    Small-diameter and underutilized (SDU) material refers to the timber that is left in the forest because it is not economical to remove, or local capacity to process it does not exist. SDU material also includes the dense, understory present through-out the forest as a result of 50 years of successful fire suppression. It has become apparent that there are many...

  2. Cost and productivity of new technology for harvesting and in-woods processing small-diameter trees.

    Treesearch

    Michael B Lambert; James O. Howard

    1990-01-01

    A study was conducted on the productivity and cost of an integrated harvesting and processing system operating in small-diameter timber (western hemlock-type) on the Olympic Peninsula of western Washington. The system uses a new steep-slope fellerbuncher, a clam-bunk grapple-skidder (forwarder), a prototype chain-flail debarker delimber, a chipper, a conveyor system,...

  3. Deriving biomass models for small-diameter loblolly pine on the Crossett Experimental Forest

    Treesearch

    K.M. McElligott; D.C. Bragg

    2013-01-01

    Foresters and landowners have a growing interest in carbon sequestration and cellulosic biofuels in southern pine forests, and hence need to be able to accurately predict them. To this end, we derived a set of aboveground biomass models using data from 62 small-diameter loblolly pines (Pinus taeda) sampled on the Crossett Experimental Forest in...

  4. User guide for HCR Estimator 2.0: software to calculate cost and revenue thresholds for harvesting small-diameter ponderosa pine.

    Treesearch

    Dennis R. Becker; Debra Larson; Eini C. Lowell; Robert B. Rummer

    2008-01-01

    The HCR (Harvest Cost-Revenue) Estimator is engineering and financial analysis software used to evaluate stand-level financial thresholds for harvesting small-diameter ponderosa pine (Pinus ponderosa Dougl. ex Laws.) in the Southwest United States. The Windows-based program helps contractors and planners to identify costs associated with tree...

  5. Porous structure and fluid partitioning in polyethylene cores from 3D X-ray microtomographic imaging.

    PubMed

    Prodanović, M; Lindquist, W B; Seright, R S

    2006-06-01

    Using oil-wet polyethylene core models, we present the development of robust throat finding techniques for the extraction, from X-ray microtomographic images, of a pore network description of porous media having porosity up to 50%. Measurements of volume, surface area, shape factor, and principal diameters are extracted for pores and area, shape factor and principal diameters for throats. We also present results on the partitioning of wetting and non-wetting phases in the pore space at fixed volume increments of the injected fluid during a complete cycle of drainage and imbibition. We compare these results with fixed fractional flow injection, where wetting and non-wetting phase are simultaneously injected at fixed volume ratio. Finally we demonstrate the ability to differentiate three fluid phases (oil, water, air) in the pore space.

  6. Mathematical modelling of powder material motion and transportation in high-temperature flow core during plasma coatings application

    NASA Astrophysics Data System (ADS)

    Bogdanovich, V. I.; Giorbelidze, M. G.

    2018-03-01

    A problem of mathematical modelling of powder material motion and transportation in gas thermal flow core has been addressed. Undertaken studies indicate significant impact on dynamics of motion of sprayed particles of phenomenological law for drag coefficient and accounting momentum loss of a plasma jet upon acceleration of these particles and their diameter. It is determined that at great dispersion of spraying particles, they reach detail surface at different velocity and significant particles separation takes place at spraying spot. According to the results of mathematical modelling, requirements for admissible dispersion of diameters of particles used for spraying have been formulated. Research has also allowed reducing separation of particles at the spraying spot due to the selection of the method of powder feed to the anode channel of the plasma torch.

  7. Demonstrations of Gravity-Independent Mobility and Drilling on Natural Rock using Microspines

    NASA Technical Reports Server (NTRS)

    Parness, Aaron; Frost, Matthew; King, Jonathan P.; Thatte, Nitish

    2012-01-01

    The video presents microspine-based anchors be ing developed for gripping rocks on the surfaces of comets and asteroids, or for use on cliff faces and lava tubes on Mars. Two types of anchor prototypes are shown on supporting forces in all directions away from the rock; >160 N tangent, >150 N at 45?, and >180 N normal to the surface of the rock. A compliant robotic ankle with two active degrees of freedom interfaces these anchors to the Lemur IIB robot for future climbing trials. Finally, a rotary percussive drill is shown coring into rock regardless of gravitational orientation. As a harder- than-zero-g proof of concept, inverted drilling was performed creating 20mm diameter boreholes 83 mm deep in vesicular basalt samples while retaining 12 mm diameter rock cores in 3-6 pieces.

  8. Formation of metal clusters in halloysite clay nanotubes

    NASA Astrophysics Data System (ADS)

    Vinokurov, Vladimir A.; Stavitskaya, Anna V.; Chudakov, Yaroslav A.; Ivanov, Evgenii V.; Shrestha, Lok Kumar; Ariga, Katsuhiko; Darrat, Yusuf A.; Lvov, Yuri M.

    2017-12-01

    We developed ceramic core-shell materials based on abundant halloysite clay nanotubes with enhanced heavy metal ions loading through Schiff base binding. These clay tubes are formed by rolling alumosilicate sheets and have diameter of c.50 nm, a lumen of 15 nm and length 1 μm. This allowed for synthesis of metal nanoparticles at the selected position: (1) on the outer surface seeding 3-5 nm metal particles on the tubes; (2) inside the tube's central lumen resulting in 10-12 nm diameter metal cores shelled with ceramic wall; and (3) smaller metal nanoparticles intercalated in the tube's wall allowing up to 9 wt% of Ru, and Ag loading. These composite materials have high surface area providing a good support for catalytic nanoparticles, and can also be used for sorption of metal ions from aqueous solutions.

  9. Formation of metal clusters in halloysite clay nanotubes.

    PubMed

    Vinokurov, Vladimir A; Stavitskaya, Anna V; Chudakov, Yaroslav A; Ivanov, Evgenii V; Shrestha, Lok Kumar; Ariga, Katsuhiko; Darrat, Yusuf A; Lvov, Yuri M

    2017-01-01

    We developed ceramic core-shell materials based on abundant halloysite clay nanotubes with enhanced heavy metal ions loading through Schiff base binding. These clay tubes are formed by rolling alumosilicate sheets and have diameter of c .50 nm, a lumen of 15 nm and length ~1 μm. This allowed for synthesis of metal nanoparticles at the selected position: (1) on the outer surface seeding 3-5 nm metal particles on the tubes; (2) inside the tube's central lumen resulting in 10-12 nm diameter metal cores shelled with ceramic wall; and (3) smaller metal nanoparticles intercalated in the tube's wall allowing up to 9 wt% of Ru, and Ag loading. These composite materials have high surface area providing a good support for catalytic nanoparticles, and can also be used for sorption of metal ions from aqueous solutions.

  10. Development of innovative oil-core self-organized nanovesicles prepared with chitosan and lecithin using a 2(3) full-factorial design.

    PubMed

    Haas, Sandra Elisa; de Andrade, Cristiane; Sansone, Pedro Ernesto da Silva; Guterres, Silvia; Dalla Costa, Teresa

    2014-11-01

    The aim of this study was to develop innovative nanosystems with isopropyl myristate as the oil core of self-assembly nanovesicles constituted of chitosan and lecithin using a 2(3) factorial design. The factors analyzed were chitosan (X1, levels 4 and 8  mg/ml), oil (X2, levels 10 and 20  mg/ml) and lecithin (X3, levels 4 and 8 mg/ml). The responses evaluated were diameter, zeta potential, pH, viscosity, and backscattering analysis. The bioavailability was evaluated after oral administration of clozapine free and nanoencapsulated in rats. The diameter ranged from 0.348 to 1.5 µm for F2 (X1, 4; X2, 10; X3, 8 mg/ml) and F7 (X1, 8; X2, 20; X3, 4  mg/ml), respectively. Laser diffractometry analysis revealed only one diameter population for all batches. Zeta potential was positive, being influenced by X1 and X2/X3 association. Viscosity values were dependent on the X1 and X2 concentrations used. A structure proposed for the nanosystem consists of chitosan forming the hydrophilic shell layer that protects the core comprised of lecithin and the hydrophobic groups of oil. The AUC0-∞ was almost 3 times higher with the clozapine nanoencapsuted in relation to free drug. It was developed a new nanosystem which is able of improving the absorption of drugs.

  11. Formation of high electrical-resistivity thin surface layer on carbonyl-iron powder (CIP) and thermal stability of nanocrystalline structure and vortex magnetic structure of CIP

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Sugimura, K.; Miyajima, Y.; Sonehara, M.

    2016-05-15

    This study focuses on the carbonyl-iron powder (CIP) used in the metal composite bulk magnetic core for high-efficient/light-weight SiC/GaN power device MHz switching dc-dc converter, where the fine CIP with a mean diameter of 1.1 μm is used to suppress the MHz band eddy current inside the CIP body. When applying the CIP to composite core together with the resin matrix, high electrical resistivity layer must be formed on the CIP-surface in order to suppress the overlapped eddy current between adjacent CIPs. In this study, tens nm thick silica (SiO{sub 2}) was successfully deposited on the CIP-surface by using hydrolysismore » of TEOS (Si(OC{sub 2}H{sub 5}){sub 4}). Also tens nm thick oxidized layer of the CIP-surface was successfully formed by using CIP annealing in dry air. The SiC/GaN power device can operate at ambient temperature over 200 degree-C, and the composite magnetic core is required to operate at such ambient temperature. The as-made CIP had small coercivity below 800 A/m (10 Oe) due to its nanocrystalline-structure and had a single vortex magnetic structure. From the experimental results, both nanocrystalline and single vortex magnetic structure were maintained after heat-exposure of 250 degree-C, and the powder coercivity after same heat-exposure was nearly same as that of the as-made CIP. Therefore, the CIP with thermally stable nanocrystalline-structure and vortex magnetic state was considered to be heat-resistant magnetic powder used in the iron-based composite core for SiC/GaN power electronics.« less

  12. Formation of high electrical-resistivity thin surface layer on carbonyl-iron powder (CIP) and thermal stability of nanocrystalline structure and vortex magnetic structure of CIP

    NASA Astrophysics Data System (ADS)

    Sugimura, K.; Miyajima, Y.; Sonehara, M.; Sato, T.; Hayashi, F.; Zettsu, N.; Teshima, K.; Mizusaki, H.

    2016-05-01

    This study focuses on the carbonyl-iron powder (CIP) used in the metal composite bulk magnetic core for high-efficient/light-weight SiC/GaN power device MHz switching dc-dc converter, where the fine CIP with a mean diameter of 1.1 μm is used to suppress the MHz band eddy current inside the CIP body. When applying the CIP to composite core together with the resin matrix, high electrical resistivity layer must be formed on the CIP-surface in order to suppress the overlapped eddy current between adjacent CIPs. In this study, tens nm thick silica (SiO2) was successfully deposited on the CIP-surface by using hydrolysis of TEOS (Si(OC2H5)4). Also tens nm thick oxidized layer of the CIP-surface was successfully formed by using CIP annealing in dry air. The SiC/GaN power device can operate at ambient temperature over 200 degree-C, and the composite magnetic core is required to operate at such ambient temperature. The as-made CIP had small coercivity below 800 A/m (10 Oe) due to its nanocrystalline-structure and had a single vortex magnetic structure. From the experimental results, both nanocrystalline and single vortex magnetic structure were maintained after heat-exposure of 250 degree-C, and the powder coercivity after same heat-exposure was nearly same as that of the as-made CIP. Therefore, the CIP with thermally stable nanocrystalline-structure and vortex magnetic state was considered to be heat-resistant magnetic powder used in the iron-based composite core for SiC/GaN power electronics.

  13. Strontium Isotope Dating of Metalliferous Sediment in the SW Pacific Basin

    NASA Astrophysics Data System (ADS)

    Stancin, A. M.; Gleason, J. D.; Owen, B. M.; Rea, D. K.; Moore, T. C.; Hendy, I. L.; Lyle, M. W.; Blum, J. D.

    2007-12-01

    A 2 million km2 region virtually devoid of sediment was identified in the remote SW Pacific Basin during the TUIM- 3 2005 drill site survey cruise. This region, termed the "South Pacific Bare Zone", comprises ocean floor dating back to the Late Cretaceous. Within the Bare Zone, a small (1km2) abyssal valley containing sediment to a depth of 24 m was sampled using a large diameter piston core (MV0502-15JC, 31 ° 42.194'S, 143 ° 30.331'W), leading to recovery of 8.35 m of metalliferous sediment at 5082 m water depth. Fish-teeth Sr-isotope stratigraphy reveals a continuous record of sedimentation from 31 Ma to present at this site. The fish teeth age-depth profile and INAA geochemistry reveal an exponentially decreasing hydrothermal flux, with sedimentation rates approaching 0.05 mm/kyr after 20 Ma. The source of hydrothermal activity at this site was likely the Pacific- Farallon Ridge, which went extinct at 20 Ma. A second piston core (MV0502-16JC; 28 ° 05.151'S, 140 ° 14.140'W) was collected near MacDonald Seamounts located on the southeastern end of the Cook-Austral island chain outside the Bare Zone and recovered 10.5 m of hydrothermal sediment and biogenic ooze. The lower 65 cm of the core consists of a coccolith ooze. From 10 mbsf depth to 1.5 mbsf depth, the core contians reddish black zeolitic clay, while the upper 1.5 mbsf contains biogenic ooze associated with abundant Late Pleistocene foraminifera remains. Concordant nannofossil and fish teeth ages at the base of the core (27-28 Ma), and Pleistocene ages near the top of the core reinforce the validity of the Sr fish teeth method for dating hydrothermal cores. These independent records suggest that regional hydrothermal activity during the Oligocene may have been related to a series of late Eocene/early Oligocene ridge jumps, propagating rifts and seafloor spreading centers that accompanied large-scale plate tectonic reorganization of South Pacific seafloor.

  14. Laboratory ultrasonic pulse velocity logging for determination of elastic properties from rock core

    NASA Astrophysics Data System (ADS)

    Blacklock, Natalie Erin

    During the development of deep underground excavations spalling and rockbursting have been recognized as significant mechanisms of violent brittle failure. In order to predict whether violent brittle failure will occur, it is important to identify the location of stiffness transitions that are associated with geologic structure. One approach to identify the effect of geologic structures is to apply borehole geophysical tools ahead of the tunnel advance. Stiffness transitions can be identified using mechanical property analysis surveys that combine acoustic velocity and density data to calculate acoustic estimates of elastic moduli. However, logistical concerns arise since the approach must be conducted at the advancing tunnel face. As a result, borehole mechanical property analyses are rarely used. Within this context, laboratory ultrasonic pulse velocity testing has been proposed as a potential alternative to borehole mechanical property analysis since moving the analysis to the laboratory would remove logistical constraints and improve safety for the evaluators. In addition to the traditional method of conducting velocity testing along the core axis, two new methodologies for point-focused testing were developed across the core diameter, and indirectly along intact lengths of drill core. The indirect test procedure was implemented in a continuous ultrasonic velocity test program along 573m of drill core to identify key geologic structures that generated transitions in ultrasonic elastic moduli. The test program was successful at identifying the location of geologic contacts, igneous intrusions, faults and shear structures. Ultrasonic values of Young's modulus and bulk modulus were determined at locations of significant velocity transitions to examine the potential for energy storage and energy release. Comparison of results from different ultrasonic velocity test configurations determined that the indirect test configuration provided underestimates for values of Young's modulus. This indicated that the test procedure will require modifications to improve coupling of the transducers to the core surface. In order to assess whether laboratory testing can be an alternative to borehole surveys, laboratory velocity testing must be directly assessed with results from acoustic borehole logging. There is also potential for the laboratory velocity program to be used to assess small scale stiffness changes, differences in mineral composition and the degree of fracturing of drill core.

  15. Nanoparticle functionalised small-core suspended-core fibre - a novel platform for efficient sensing.

    PubMed

    Doherty, Brenda; Csáki, Andrea; Thiele, Matthias; Zeisberger, Matthias; Schwuchow, Anka; Kobelke, Jens; Fritzsche, Wolfgang; Schmidt, Markus A

    2017-02-01

    Detecting small quantities of specific target molecules is of major importance within bioanalytics for efficient disease diagnostics. One promising sensing approach relies on combining plasmonically-active waveguides with microfluidics yielding an easy-to-use sensing platform. Here we introduce suspended-core fibres containing immobilised plasmonic nanoparticles surrounding the guiding core as a concept for an entirely integrated optofluidic platform for efficient refractive index sensing. Due to the extremely small optical core and the large adjacent microfluidic channels, over two orders of magnitude of nanoparticle coverage densities have been accessed with millimetre-long sample lengths showing refractive index sensitivities of 170 nm/RIU for aqueous analytes where the fibre interior is functionalised by gold nanospheres. Our concept represents a fully integrated optofluidic sensing system demanding small sample volumes and allowing for real-time analyte monitoring, both of which are highly relevant within invasive bioanalytics, particularly within molecular disease diagnostics and environmental science.

  16. Feasibility study of full-reactor gas core demonstration test

    NASA Technical Reports Server (NTRS)

    Kunze, J. F.; Lofthouse, J. H.; Shaffer, C. J.; Macbeth, P. J.

    1973-01-01

    Separate studies of nuclear criticality, flow patterns, and thermodynamics for the gas core reactor concept have all given positive indications of its feasibility. However, before serious design for a full scale gas core application can be made, feasibility must be shown for operation with full interaction of the nuclear, thermal, and hydraulic effects. A minimum sized, and hence minimum expense, test arrangement is considered for a full gas core configuration. It is shown that the hydrogen coolant scattering effects dominate the nuclear considerations at elevated temperatures. A cavity diameter of somewhat larger than 4 ft (122 cm) will be needed if temperatures high enough to vaporize uranium are to be achieved.

  17. Multiphoton endoscopy based on a mode-filtered single-mode fiber

    NASA Astrophysics Data System (ADS)

    Moon, Sucbei; Liu, Gangjun; Chen, Zhongping

    2011-03-01

    We present a new low-nonlinearity fiber of mode-filtered large-core fiber for flexible beam delivery of intense pulsed light aiming at multi-photon endoscopy application. A multimode fiber of a large core diameter (20 μm) equips a mode filtering means in the middle of the fiber link to suppress the high-order modes selectively. A large effective core area of ~200 μm2 has been achieved at 0.8-μm and 1.0-μm bands. This is 8 times larger than the core area of a conventional SMF used for those spectral bands. Various advantages of our large-mode area fiber will be demonstrated and discussed in this report.

  18. Hydrostatic Pressure Sensing with High Birefringence Photonic Crystal Fibers

    PubMed Central

    Fávero, Fernando C.; Quintero, Sully M. M.; Martelli, Cicero; Braga, Arthur M.B.; Silva, Vinícius V.; Carvalho, Isabel C. S.; Llerena, Roberth W. A.; Valente, Luiz C. G.

    2010-01-01

    The effect of hydrostatic pressure on the waveguiding properties of high birefringence photonic crystal fibers (HiBi PCF) is evaluated both numerically and experimentally. A fiber design presenting form birefringence induced by two enlarged holes in the innermost ring defining the fiber core is investigated. Numerical results show that modal sensitivity to the applied pressure depends on the diameters of the holes, and can be tailored by independently varying the sizes of the large or small holes. Numerical and experimental results are compared showing excellent agreement. A hydrostatic pressure sensor is proposed and demonstrated using an in-fiber modal interferometer where the two orthogonally polarized modes of a HiBi PCF generate fringes over the optical spectrum of a broad band source. From the analysis of experimental results, it is concluded that, in principle, an operating limit of 92 MPa in pressure could be achieved with 0.0003% of full scale resolution. PMID:22163435

  19. Scientific goals of Nano-JASMINE

    NASA Astrophysics Data System (ADS)

    Yamada, Yoshiyuki; Fujita, Sho; Gouda, Naoteru; Kobayashi, Yukiyasu; Hara, Takuji; Nishi, Ryoichi; Yoshioka, Satoshi; Hozumi, Shunsuke

    2013-02-01

    Nano-JASMINE is an ultrasmall Japanese satellite (with a weight of 35 kg), designed to carry out an astrometric mission. The target accuracy is 3 milliarcseconds (mas) for stars brighter than magnitude 7.5 at zw-band wavelengths of 0.6-1.0 μm. The observational strategy is the same as that of Gaia and Hipparcos. The time span of 20 years since the Hipparcos mission will enable us to update the proper motion data obtained at that time. With the help of these updated measurements, we expect that some stars will be resolved into multiple stars. In addition, taking advantage of the small primary mirror (with a diameter of 5 cm), we can measure bright stars which cannot be observed with Gaia because of saturation limits. The core data reduction for the Nano-JASMINE mission will use Gaia's Astrometric Global Iterative Solution (agis). A collaboration between the Gaia agis and Nano-JASMINE teams was initiated in 2007.

  20. Microfiber Optical Sensors: A Review

    PubMed Central

    Lou, Jingyi; Wang, Yipei; Tong, Limin

    2014-01-01

    With diameter close to or below the wavelength of guided light and high index contrast between the fiber core and the surrounding, an optical microfiber shows a variety of interesting waveguiding properties, including widely tailorable optical confinement, evanescent fields and waveguide dispersion. Among various microfiber applications, optical sensing has been attracting increasing research interest due to its possibilities of realizing miniaturized fiber optic sensors with small footprint, high sensitivity, fast response, high flexibility and low optical power consumption. Here we review recent progress in microfiber optical sensors regarding their fabrication, waveguide properties and sensing applications. Typical microfiber-based sensing structures, including biconical tapers, optical gratings, circular cavities, Mach-Zehnder interferometers and functionally coated/doped microfibers, are summarized. Categorized by sensing structures, microfiber optical sensors for refractive index, concentration, temperature, humidity, strain and current measurement in gas or liquid environments are reviewed. Finally, we conclude with an outlook for challenges and opportunities of microfiber optical sensors. PMID:24670720

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