Study on the Optimization and Process Modeling of the Rotary Ultrasonic Machining of Zerodur Glass-Ceramic

NASA Astrophysics Data System (ADS)

Pitts, James Daniel

Rotary ultrasonic machining (RUM), a hybrid process combining ultrasonic machining and diamond grinding, was created to increase material removal rates for the fabrication of hard and brittle workpieces. The objective of this research was to experimentally derive empirical equations for the prediction of multiple machined surface roughness parameters for helically pocketed rotary ultrasonic machined Zerodur glass-ceramic workpieces by means of a systematic statistical experimental approach. A Taguchi parametric screening design of experiments was employed to systematically determine the RUM process parameters with the largest effect on mean surface roughness. Next empirically determined equations for the seven common surface quality metrics were developed via Box-Behnken surface response experimental trials. Validation trials were conducted resulting in predicted and experimental surface roughness in varying levels of agreement. The reductions in cutting force and tool wear associated with RUM, reported by previous researchers, was experimentally verified to also extended to helical pocketing of Zerodur glass-ceramic.

Optical Interactions at Randomly Rough Surfaces

DTIC Science & Technology

2003-03-10

frequency range. The design of a random surface that acts as a Lambertian diffuser, especially in the infrared region of the optical spectrum, is...FTIR grazing angle microscopy. Recently, an experimental study was performed of the far-field scattering at small grazing angles, especially the enhanced...a specular component in the scattered light, in this frequency range. The design of a random surface that acts as a Lambertian diffuser, especially in

Broadband angle-independent antireflection coatings on nanostructured light trapping solar cells

NASA Astrophysics Data System (ADS)

Vázquez-Guardado, Abraham; Boroumand, Javaneh; Franklin, Daniel; Chanda, Debashis

2018-03-01

Backscattering from nanostructured surfaces greatly diminishes the efficacy of light trapping solar cells. While the analytical design of broadband, angle-independent antireflection coatings on nanostructured surfaces proved inefficient, numerical optimization proves a viable alternative. Here, we numerically design and experimentally verify the performance of single and bilayer antireflection coatings on a 2D hexagonal diffractive light trapping pattern on crystalline silicon substrates. Three well-known antireflection coatings, aluminum oxide, silicon nitride, and silicon oxide, which also double as high-quality surface passivation materials, are studied in the 400-1000 nm band. By varying thickness and conformity, the optimal parameters that minimize the broadband total reflectance (specular and scattering) from the nanostructured surface are obtained. The design results in a single-layer antireflection coating with normal-angle wavelength-integrated reflectance below 4% and a bilayer antireflection coating demonstrating reflection down to 1.5%. We show experimentally an angle-averaged reflectance of ˜5.2 % up to 60° incident angle from the optimized bilayer antireflection-coated nanostructured surface, paving the path toward practical implementation of the light trapping solar cells.

An experimental study of pressures on 60 deg Delta wings with leading edge vortex flaps

NASA Technical Reports Server (NTRS)

Marchman, J. F., III; Terry, J. E.; Donatelli, D. A.

1983-01-01

An experimental study was conducted in the Virginia Tech Stability Wind Tunnel to determine surface pressures over a 60 deg sweep delta wing with three vortex flap designs. Extensive pressure data was collected to provide a base data set for comparison with computational design codes and to allow a better understanding of the flow over vortex flaps. The results indicated that vortex flaps can be designed which will contain the leading edge vortex with no spillage onto the wing upper surface. However, the tests also showed that flaps designed without accounting for flap thickness will not be optimum and the result can be oversized flaps, early flap vortex reattachment and a second separation and vortex at the wing/flap hinge line.

Mars integrated transportation system multistage Mars mission

NASA Technical Reports Server (NTRS)

1991-01-01

In accordance with the objective of the Mars Integrated Transport System (MITS) program, the Multistage Mars Mission (MSMM) design team developed a profile for a manned mission to Mars. The purpose of the multistage mission is to send a crew of five astronauts to the martian surface by the year 2019. The mission continues man's eternal quest for exploration of new frontiers. This mission has a scheduled duration of 426 days that includes experimentation en route as well as surface exploration and experimentation. The MSMM is also designed as a foundation for a continuing program leading to the colonization of the planet Mars.

The Complicate Observations and Multi-Parameter Land Information Constructions on Allied Telemetry Experiment (COMPLICATE)

PubMed Central

Tian, Xin; Li, Zengyuan; Chen, Erxue; Liu, Qinhuo; Yan, Guangjian; Wang, Jindi; Niu, Zheng; Zhao, Shaojie; Li, Xin; Pang, Yong; Su, Zhongbo; van der Tol, Christiaan; Liu, Qingwang; Wu, Chaoyang; Xiao, Qing; Yang, Le; Mu, Xihan; Bo, Yanchen; Qu, Yonghua; Zhou, Hongmin; Gao, Shuai; Chai, Linna; Huang, Huaguo; Fan, Wenjie; Li, Shihua; Bai, Junhua; Jiang, Lingmei; Zhou, Ji

2015-01-01

The Complicate Observations and Multi-Parameter Land Information Constructions on Allied Telemetry Experiment (COMPLICATE) comprises a network of remote sensing experiments designed to enhance the dynamic analysis and modeling of remotely sensed information for complex land surfaces. Two types of experimental campaigns were established under the framework of COMPLICATE. The first was designed for continuous and elaborate experiments. The experimental strategy helps enhance our understanding of the radiative and scattering mechanisms of soil and vegetation and modeling of remotely sensed information for complex land surfaces. To validate the methodologies and models for dynamic analyses of remote sensing for complex land surfaces, the second campaign consisted of simultaneous satellite-borne, airborne, and ground-based experiments. During field campaigns, several continuous and intensive observations were obtained. Measurements were undertaken to answer key scientific issues, as follows: 1) Determine the characteristics of spatial heterogeneity and the radiative and scattering mechanisms of remote sensing on complex land surfaces. 2) Determine the mechanisms of spatial and temporal scale extensions for remote sensing on complex land surfaces. 3) Determine synergist inversion mechanisms for soil and vegetation parameters using multi-mode remote sensing on complex land surfaces. Here, we introduce the background, the objectives, the experimental designs, the observations and measurements, and the overall advances of COMPLICATE. As a result of the implementation of COMLICATE and for the next several years, we expect to contribute to quantitative remote sensing science and Earth observation techniques. PMID:26332035

Investigation of a 0.6 hub-tip radius-ratio transonic turbine designed for secondary-flow study I : design and experimental performance of standard turbine

NASA Technical Reports Server (NTRS)

Rohlik, Harold E; Wintucky, William T; Scibbe, Herbert W

1957-01-01

Detailed design information including overall performance parameters, velocity diagrams, and blade surface velocities is presented. Experimental performance includes maps based on rating as well as total-pressure ratios showing the effect of exit whirl. Also included are results of surveys at the stator exit and downstream of the rotor at design speed and specific work. This information will be used as a standard for comparison with subsequent secondary-flow work.

Stress Regression Analysis of Asphalt Concrete Deck Pavement Based on Orthogonal Experimental Design and Interlayer Contact

NASA Astrophysics Data System (ADS)

Wang, Xuntao; Feng, Jianhu; Wang, Hu; Hong, Shidi; Zheng, Supei

2018-03-01

A three-dimensional finite element box girder bridge and its asphalt concrete deck pavement were established by ANSYS software, and the interlayer bonding condition of asphalt concrete deck pavement was assumed to be contact bonding condition. Orthogonal experimental design is used to arrange the testing plans of material parameters, and an evaluation of the effect of different material parameters in the mechanical response of asphalt concrete surface layer was conducted by multiple linear regression model and using the results from the finite element analysis. Results indicated that stress regression equations can well predict the stress of the asphalt concrete surface layer, and elastic modulus of waterproof layer has a significant influence on stress values of asphalt concrete surface layer.

Establishment of a new pull-out strength testing method to quantify early osseointegration-An experimental pilot study.

PubMed

Nonhoff, J; Moest, T; Schmitt, Christian Martin; Weisel, T; Bauer, S; Schlegel, K A

2015-12-01

The animal study aims to evaluate a new experimental model for measuring sole the influence of the surface characteristics independent from implant macro-design on the level of osseointegration by registering the pull-out strength needed for removal of experimental devices with different surfaces from artificial defects. Seventy-two test bodies (36 with the FRIADENT(®) plus surface, 36 with the P15/HAp biofunctionalized surface) were inserted in six adult domestic pigs with artificial calvarial defects. The experimental devices were designed to fit in the defects leaving a gap between the test body and the local bone. After 21 days of healing, the animals were sacrificed and the test bodies were pulled out with a standardised reproducible pull-out device measuring the pull-out strength. The pull-out strength for both groups was compared. Twenty-one days after insertion a mean force of 412 ± 142 N for the P15/HAp group and 183 ± 105 N for the FRIADENT(®) plus group was measured for the removal of the specimens from the calvarial bone. The difference between the groups was statistically significant (p < 0.0001). The experimental set-up seems to be a suitable method when measuring the impact of implant surfaces on the early stage of osseointegration. Copyright © 2015 European Association for Cranio-Maxillo-Facial Surgery. Published by Elsevier Ltd. All rights reserved.

Photocatalytic degradation using design of experiments: a review and example of the Congo red degradation.

PubMed

Sakkas, Vasilios A; Islam, Md Azharul; Stalikas, Constantine; Albanis, Triantafyllos A

2010-03-15

The use of chemometric methods such as response surface methodology (RSM) based on statistical design of experiments (DOEs) is becoming increasingly widespread in several sciences such as analytical chemistry, engineering and environmental chemistry. Applied catalysis, is certainly not the exception. It is clear that photocatalytic processes mated with chemometric experimental design play a crucial role in the ability of reaching the optimum of the catalytic reactions. The present article reviews the major applications of RSM in modern experimental design combined with photocatalytic degradation processes. Moreover, the theoretical principles and designs that enable to obtain a polynomial regression equation, which expresses the influence of process parameters on the response are thoroughly discussed. An original experimental work, the photocatalytic degradation of the dye Congo red (CR) using TiO(2) suspensions and H(2)O(2), in natural surface water (river water) is comprehensively described as a case study, in order to provide sufficient guidelines to deal with this subject, in a rational and integrated way. (c) 2009 Elsevier B.V. All rights reserved.

Study and design of cryogenic propellant acquisition systems. Volume 1: Design studies

NASA Technical Reports Server (NTRS)

Burge, G. W.; Blackmon, J. B.

1973-01-01

An in-depth study and selection of practical propellant surface tension acquisition system designs for two specific future cryogenic space vehicles, an advanced cryogenic space shuttle auxiliary propulsion system and an advanced space propulsion module is reported. A supporting laboratory scale experimental program was also conducted to provide design information critical to concept finalization and selection. Designs using localized pressure isolated surface tension screen devices were selected for each application and preliminary designs were generated. Based on these designs, large scale acquisition prototype hardware was designed and fabricated to be compatible with available NASA-MSFC feed system hardware.

Comparative efficacy of two battery-powered toothbrushes on dental plaque removal.

PubMed

Ruhlman, C Douglas; Bartizek, Robert D; Biesbrock, Aaron R

2002-01-01

A number of clinical studies have consistently demonstrated that power toothbrushes deliver superior plaque removal compared to manual toothbrushes. Recently, a new power toothbrush (Crest SpinBrush) has been marketed with a design that fundamentally differs from other marketed power toothbrushes. Other power toothbrushes feature a small, round head designed to oscillate for enhanced cleaning between the teeth and below the gumline. The new power toothbrush incorporates a similar round oscillating head in conjunction with fixed bristles, which allows the user to brush with optimal manual brushing technique. The objective of this randomized, examiner-blind, parallel design study was to compare the plaque removal efficacy of a positive control power toothbrush (Colgate Actibrush) to an experimental toothbrush (Crest SpinBrush) following a single use among 59 subjects. Baseline plaque scores were 1.64 and 1.40 for the experimental toothbrush and control toothbrush treatment groups, respectively. With regard to all surfaces examined, the experimental toothbrush delivered an adjusted (via analysis of covariance) mean difference between baseline and post-brushing plaque scores of 0.47, while the control toothbrush delivered an adjusted mean difference of 0.33. On average, the difference between toothbrushes was statistically significant (p = 0.013). Because the covariate slope for the experimental group was statistically significantly greater (p = 0.001) than the slope for the control group, a separate slope model was used. Further analysis demonstrated that the experimental group had statistically significantly greater plaque removal than the control group for baseline plaque scores above 1.43. With respect to buccal surfaces, using a separate slope analysis of covariance, the experimental toothbrush delivered an adjusted mean difference between baseline and post-brushing plaque scores of 0.61, while the control toothbrush delivered an adjusted mean difference of 0.39. This difference between toothbrushes was also statistically significant (p = 0.002). On average, the results on lingual surfaces demonstrated similar directional scores favoring the experimental toothbrush; however these results did not achieve statistical significance. In conclusion, the experimental Crest SpinBrush, with its novel fixed and oscillating bristle design, was found to be more effective than the positive control Colgate Actibrush, which is designed with a small round oscillating cluster of bristles.

Experimental design methodologies in the optimization of chiral CE or CEC separations: an overview.

PubMed

Dejaegher, Bieke; Mangelings, Debby; Vander Heyden, Yvan

2013-01-01

In this chapter, an overview of experimental designs to develop chiral capillary electrophoresis (CE) and capillary electrochromatographic (CEC) methods is presented. Method development is generally divided into technique selection, method optimization, and method validation. In the method optimization part, often two phases can be distinguished, i.e., a screening and an optimization phase. In method validation, the method is evaluated on its fit for purpose. A validation item, also applying experimental designs, is robustness testing. In the screening phase and in robustness testing, screening designs are applied. During the optimization phase, response surface designs are used. The different design types and their application steps are discussed in this chapter and illustrated by examples of chiral CE and CEC methods.

Experimental investigation on hard turning of AISI 4340 steel using cemented coated carbide insert

NASA Astrophysics Data System (ADS)

Pradeep Kumar, J.; Kishore, K. P.; Ranjith Kumar, M.; Saran Karthick, K. R.; Vishnu Gowtham, S.

2018-02-01

Hard turning is a developing technology that offers many potential advantages compared to grinding, which remains the standard finishing process for critical hardened surfaces. In this work, an attempt has been made to experimentally investigate hard turning of AISI 4340 steel under wet and dry condition using cemented coated carbide insert. Hardness of the workpiece material is tested using Brinell and Rockwell hardness testers. CNC LATHE and cemented coated carbide inserts of designation CNMG 120408 are used for conducting experimental trials. Significant cutting parameters like cutting speed, feed rate and depth of cut are considered as controllable input parameters and surface roughness (Ra), tool wear are considered as output response parameters. Design of experiments is carried out with the help of Taguchi’s L9 orthogonal array. Results of response parameters like surface roughness and tool wear under wet and dry condition are analysed. It is found that surface roughness and tool wear are higher under dry machining condition when compared to wet machining condition. Feed rate significantly influences the surface roughness followed by cutting speed. Depth of cut significantly influences the tool wear followed by cutting speed.

Achieving optimal SERS through enhanced experimental design.

PubMed

Fisk, Heidi; Westley, Chloe; Turner, Nicholas J; Goodacre, Royston

2016-01-01

One of the current limitations surrounding surface-enhanced Raman scattering (SERS) is the perceived lack of reproducibility. SERS is indeed challenging, and for analyte detection, it is vital that the analyte interacts with the metal surface. However, as this is analyte dependent, there is not a single set of SERS conditions that are universal. This means that experimental optimisation for optimum SERS response is vital. Most researchers optimise one factor at a time, where a single parameter is altered first before going onto optimise the next. This is a very inefficient way of searching the experimental landscape. In this review, we explore the use of more powerful multivariate approaches to SERS experimental optimisation based on design of experiments and evolutionary computational methods. We particularly focus on colloidal-based SERS rather than thin film preparations as a result of their popularity. © 2015 The Authors. Journal of Raman Spectroscopy published by John Wiley & Sons, Ltd.

A Surrogate Approach to the Experimental Optimization of Multielement Airfoils

NASA Technical Reports Server (NTRS)

Otto, John C.; Landman, Drew; Patera, Anthony T.

1996-01-01

The incorporation of experimental test data into the optimization process is accomplished through the use of Bayesian-validated surrogates. In the surrogate approach, a surrogate for the experiment (e.g., a response surface) serves in the optimization process. The validation step of the framework provides a qualitative assessment of the surrogate quality, and bounds the surrogate-for-experiment error on designs "near" surrogate-predicted optimal designs. The utility of the framework is demonstrated through its application to the experimental selection of the trailing edge ap position to achieve a design lift coefficient for a three-element airfoil.

[Optimization of vacuum belt drying process of Gardeniae Fructus in Reduning injection by Box-Behnken design-response surface methodology].

PubMed

Huang, Dao-sheng; Shi, Wei; Han, Lei; Sun, Ke; Chen, Guang-bo; Wu Jian-xiong; Xu, Gui-hong; Bi, Yu-an; Wang, Zhen-zhong; Xiao, Wei

2015-06-01

To optimize the belt drying process conditions optimization of Gardeniae Fructus extract from Reduning injection by Box-Behnken design-response surface methodology, on the basis of single factor experiment, a three-factor and three-level Box-Behnken experimental design was employed to optimize the drying technology of Gardeniae Fructus extract from Reduning injection. With drying temperature, drying time, feeding speed as independent variables and the content of geniposide as dependent variable, the experimental data were fitted to a second order polynomial equation, establishing the mathematical relationship between the content of geniposide and respective variables. With the experimental data analyzed by Design-Expert 8. 0. 6, the optimal drying parameter was as follows: the drying temperature was 98.5 degrees C , the drying time was 89 min, the feeding speed was 99.8 r x min(-1). Three verification experiments were taked under this technology and the measured average content of geniposide was 564. 108 mg x g(-1), which was close to the model prediction: 563. 307 mg x g(-1). According to the verification test, the Gardeniae Fructus belt drying process is steady and feasible. So single factor experiments combined with response surface method (RSM) could be used to optimize the drying technology of Reduning injection Gardenia extract.

Exploratory studies of the cruise performance of upper surface blown configurations. Experimental program: Test facilities, model design instrumentation, and lowspeed, high-lift tests

NASA Technical Reports Server (NTRS)

Braden, J. A.; Hancock, J. P.; Burdges, K. P.; Hackett, J. E.

1980-01-01

The model hardware, test facilities and instrumentation utilized in an experimental study of upper surface blown configurations at cruise is described. The high speed (subsonic) experimental work, studying the aerodynamic effects of wing nacelle geometric variations, was conducted around semispan model configurations composed of diversified, interchangeable components. Power simulation was provided by high pressure air ducted through closed forebody nacelles. Nozzle geometry was varied across size, exit aspect ratio, exit position and boattail angle. Three dimensional force and two dimensional pressure measurements were obtained at cruise Mach numbers from 0.5 to 0.8 and at nozzle pressure ratios up to about 3.0. The experimental investigation was supported by an analytical synthesis of the system using a vortex lattice representation with first order power effects. Results are also presented from a compatibility study in which a short haul transport is designed on the basis of the aerodynamic findings in the experimental study as well as acoustical data obtained in a concurrent program. High lift test data are used to substantiate the projected performance of the selected transport design.

Design method of LED rear fog lamp based on freeform micro-surface reflectors

NASA Astrophysics Data System (ADS)

Yu, Jindong; Wu, Heng

2017-11-01

We propose a practical method for the design of a light-emitting diode (LED) rear fog lamp based on freeform micro-surface reflectors. The lamp consists of nine LEDs and each of them has a freeform micro-surface reflector correspondingly. The micro-surface reflector design includes three steps. An initial freeform reflector is first built based on the light energy maps. The micro-surface reflector is then constructed on the bias of the initial one. Finally, a two-step method is designed to optimize the micro-surface reflector. With the proposed method, a module is designed and LCW DURIS E5 LED source whose emitting surface is 5.7 mm × 3.0 mm is adopted for simulation. A prototype is also assembled and fabricated to verify the real performance. Both the simulation and experimental results demonstrate that the luminous intensity distribution can well fulfill the requirements of ECE No.38 regulation. Furthermore, more than 79% energy can be saved when compared with the rear fog lamps using conventional sources.

Dispersionless Manipulation of Reflected Acoustic Wavefront by Subwavelength Corrugated Surface

PubMed Central

Zhu, Yi-Fan; Zou, Xin-Ye; Li, Rui-Qi; Jiang, Xue; Tu, Juan; Liang, Bin; Cheng, Jian-Chun

2015-01-01

Free controls of optic/acoustic waves for bending, focusing or steering the energy of wavefronts are highly desirable in many practical scenarios. However, the dispersive nature of the existing metamaterials/metasurfaces for wavefront manipulation necessarily results in limited bandwidth. Here, we propose the concept of dispersionless wavefront manipulation and report a theoretical, numerical and experimental work on the design of a reflective surface capable of controlling the acoustic wavefront arbitrarily without bandwidth limitation. Analytical analysis predicts the possibility to completely eliminate the frequency dependence with a specific gradient surface which can be implemented by designing a subwavelength corrugated surface. Experimental and numerical results, well consistent with the theoretical predictions, have validated the proposed scheme by demonstrating a distinct phenomenon of extraordinary acoustic reflection within an ultra-broad band. For acquiring a deeper insight into the underlying physics, a simple physical model is developed which helps to interpret this extraordinary phenomenon and predict the upper cutoff frequency precisely. Generations of planar focusing and non-diffractive beam have also been exemplified. With the dispersionless wave-steering capability and deep discrete resolution, our designed structure may open new avenue to fully steer classical waves and offer design possibilities for broadband optical/acoustical devices. PMID:26077772

On the use of response surface methodology to predict and interpret the preferred c-axis orientation of sputtered AlN thin films

NASA Astrophysics Data System (ADS)

Adamczyk, J.; Horny, N.; Tricoteaux, A.; Jouan, P.-Y.; Zadam, M.

2008-01-01

This paper deals with experimental design applied to response surface methodology (RSM) in order to determine the influence of the discharge conditions on preferred c-axis orientation of sputtered AlN thin films. The thin films have been deposited by DC reactive magnetron sputtering on Si (1 0 0) substrates. The preferred orientation was evaluated using a conventional Bragg-Brentano X-ray diffractometer ( θ-2 θ) with the CuKα radiation. We have first determined the experimental domain for 3 parameters: sputtering pressure (2-6 mTorr), discharge current (312-438 mA) and nitrogen percentage (17-33%). For the setup of the experimental design we have used a three factors Doehlert matrix which allows the use of the statistical response surface methodology (RSM) in a spherical domain. A four dimensional surface response, which represents the (0 0 0 2) peak height as a function of sputtering pressure, discharge current and nitrogen percentage, was obtained. It has been found that the main interaction affecting the preferential c-axis orientation was the pressure-nitrogen percentage interaction. It has been proved that a Box-Cox transformation is a very useful method to interpret and discuss the experimental results and leads to predictions in good agreement with experiments.

Probing the effects of surface hydrophobicity and tether orientation on antibody-antigen binding

NASA Astrophysics Data System (ADS)

Bush, Derek B.; Knotts, Thomas A.

2017-04-01

Antibody microarrays have the potential to revolutionize molecular detection for many applications, but their current use is limited by poor reliability, and efforts to change this have not yielded fruitful results. One difficulty which limits the rational engineering of next-generation devices is that little is known, at the molecular level, about the antibody-antigen binding process near solid surfaces. Atomic-level structural information is scant because typical experimental techniques (X-ray crystallography and NMR) cannot be used to image proteins bound to surfaces. To overcome this limitation, this study uses molecular simulation and an advanced, experimentally validated, coarse-grain, protein-surface model to compare fab-lysozyme binding in bulk solution and when the fab is tethered to hydrophobic and hydrophilic surfaces. The results show that the tether site in the fab, as well as the surface hydrophobicity, significantly impacts the binding process and suggests that the optimal design involves tethering fabs upright on a hydrophilic surface. The results offer an unprecedented, molecular-level picture of the binding process and give hope that the rational design of protein-microarrays is possible.

Response surface modeling of acid activation of raw diatomite using in sunflower oil bleaching by: Box-Behnken experimental design.

PubMed

Larouci, M; Safa, M; Meddah, B; Aoues, A; Sonnet, P

2015-03-01

The optimum conditions for acid activation of diatomite for maximizing bleaching efficiency of the diatomite in sun flower oil treatment were studied. Box-Behnken experimental design combining with response surface modeling (RSM) and quadratic programming (QP) was employed to obtain the optimum conditions of three independent variables (acid concentration, activation time and solid to liquid) for acid activation of diatomite. The significance of independent variables and their interactions were tested by means of the analysis of variance (ANOVA) with 95 % confidence limits (α = 0.05). The optimum values of the selected variables were obtained by solving the quadratic regression model, as well as by analyzing the response surface contour plots. The experimental conditions at this global point were determined to be acid concentration = 8.963 N, activation time = 11.9878 h, and solid to liquid ratio = 221.2113 g/l, the corresponding bleaching efficiency was found to be about 99 %.

Cost, performance, and esthetic impacts of an experimental forest road in Montana

Treesearch

Rulon B. Gardner

1978-01-01

An experimental logging road designed to minimize environmental and esthetic impact was constructed in northwest Montana. The road was single-lane (14-foot finished surface, 3-foot ditch), constructed along the contour. Esthetically, the single-lane experimental road was judged far superior to existing roads on the forest.

Experimental verification of ‘waveguide’ plasmonics

NASA Astrophysics Data System (ADS)

Prudêncio, Filipa R.; Costa, Jorge R.; Fernandes, Carlos A.; Engheta, Nader; Silveirinha, Mário G.

2017-12-01

Surface plasmons polaritons are collective excitations of an electron gas that occur at an interface between negative-ɛ and positive-ɛ media. Here, we report the experimental observation of such surface waves using simple waveguide metamaterials filled only with available positive-ɛ media at microwave frequencies. In contrast to optical designs, in our setup the propagation length of the surface plasmons can be rather long as low loss conventional dielectrics are chosen to avoid typical losses from negative-ɛ media. Plasmonic phenomena have potential applications in enhancing light-matter interactions, implementing nanoscale photonic circuits and integrated photonics.

Project GEOS-C. [designed to measure the topography of ocean surface and the sea state

NASA Technical Reports Server (NTRS)

1975-01-01

An oceanographic-geodetic satellite, designated Geodynamics Experimental Ocean Satellite-C (GEOS-C), an earth-orbiting spacecraft designed to measure precisely the topography of the ocean surface and the sea state (wave height, wave period, wave propagation direction) is described. Launch operations, spacecraft description, and mission objectives are included along with a brief flight history of the NASA satellite geodesy program. Principal investigations to be performed by the GEOS-C mission are discussed.

Effects of pavement surface texture on noise and frictional characteristics.

DOT National Transportation Integrated Search

1987-02-01

An experimental modification of the transverse groove : surface texture of a section of an urban interstate highway was : performed by the Iowa Department of Transportation. Transverse : groove texturing is a design feature required by the Federal : ...

Heat transfer and flow characteristics on a gas turbine shroud.

PubMed

Obata, M; Kumada, M; Ijichi, N

2001-05-01

The work described in this paper is an experimental investigation of the heat transfer from the main flow to a turbine shroud surface, which may be applicable to ceramic gas turbines. Three kinds of turbine shrouds are considered with a flat surface, a taper surface and a spiral groove surface opposite to the blades in an axial flow turbine of actual turbo-charger. Heat transfer measurements were performed for the experimental conditions of a uniform heat flux or a uniform wall temperature. The effects of the inlet flow angle, rotational speed, and tip clearance on the heat transfer coefficient were clarified under on- and off-design flow conditions. The mean heat transfer coefficient was correlated to the blade Reynolds number and tip clearance, and compared with an experimental correlation and measurements of a flat surface. A comparison was also made for the measurement of static pressure distributions.

Design of a hybrid emissivity domestic electric oven

NASA Astrophysics Data System (ADS)

Isik, Ozgur; Onbasioglu, Seyhan Uygur

2017-10-01

In this study, the radiative properties of the surfaces of an electric oven were investigated. Using experimental data related to an oven-like enclosure, a novel combination of surface properties was developed. Three different surface emissivity combinations were analysed experimentally: low-emissivity, high emissivity (black-coated), and hybrid emissivity. The term "hybrid emissivity design" here corresponds to an enclosure with some high emissive and some low-emissive surfaces. The experiments were carried out according to the EN 50304 standard. When a brick (load) was placed in the enclosure, the view factors between its surfaces were calculated with the Monte Carlo method. These and the measured surface temperatures were then used to calculate the radiative heat fluxes on the surfaces of the load. The three different models were compared with respect to energy consumption and baking time. The hybrid model performed best, with the highest radiative heat transfer between the surfaces of the enclosure and the load and minimum heat loss from the cavity. Thus, it was the most efficient model with the lowest energy consumption and the shortest baking time. The recent European Union regulation regarding the energy labelling of domestic ovens was used.

Optimizing Force Deployment and Force Structure for the Rapid Deployment Force

DTIC Science & Technology

1984-03-01

Analysis . . . . .. .. ... ... 97 Experimental Design . . . . . .. .. .. ... 99 IX. Use of a Flexible Response Surface ........ 10.2 Selection of a...setS . ere designe . arun, programming methodology , where the require: s.stem re..r is input and the model optimizes the num=er. :::pe, cargo. an...to obtain new computer outputs" (Ref 38:23). The methodology can be used with any decision model, linear or nonlinear. Experimental Desion Since the

Theoretical and experimental researches of the liquid evaporation during thermal vacuum influences

NASA Astrophysics Data System (ADS)

Trushlyakov, V.; Panichkin, A.; Prusova, O.; Zharikov, K.; Dron, M.

2018-01-01

The mathematical model of the evaporation process of model liquid with the free surface boundary conditions of the "mirror" type under thermal vacuum influence and the numerical estimates of the evaporation process parameters are developed. An experimental stand, comprising a vacuum chamber, an experimental model tank with a heating element is designed; the experimental data are obtained. A comparative analysis of numerical and experimental results showed their close match.

Computational design of protein interactions: designing proteins that neutralize influenza by inhibiting its hemagglutinin surface protein

NASA Astrophysics Data System (ADS)

Fleishman, Sarel

2012-02-01

Molecular recognition underlies all life processes. Design of interactions not seen in nature is a test of our understanding of molecular recognition and could unlock the vast potential of subtle control over molecular interaction networks, allowing the design of novel diagnostics and therapeutics for basic and applied research. We developed the first general method for designing protein interactions. The method starts by computing a region of high affinity interactions between dismembered amino acid residues and the target surface and then identifying proteins that can harbor these residues. Designs are tested experimentally for binding the target surface and successful ones are affinity matured using yeast cell surface display. Applied to the conserved stem region of influenza hemagglutinin we designed two unrelated proteins that, following affinity maturation, bound hemagglutinin at subnanomolar dissociation constants. Co-crystal structures of hemagglutinin bound to the two designed binders were within 1Angstrom RMSd of their models, validating the accuracy of the design strategy. One of the designed proteins inhibits the conformational changes that underlie hemagglutinin's cell-invasion functions and blocks virus infectivity in cell culture, suggesting that such proteins may in future serve as diagnostics and antivirals against a wide range of pathogenic influenza strains. We have used this method to obtain experimentally validated binders of several other target proteins, demonstrating the generality of the approach. We discuss the combination of modeling and high-throughput characterization of design variants which has been key to the success of this approach, as well as how we have used the data obtained in this project to enhance our understanding of molecular recognition. References: Science 332:816 JMB, in press Protein Sci 20:753

Study of surface integrity AISI 4140 as result of hard, dry and high speed machining using CBN

NASA Astrophysics Data System (ADS)

Ginting, B.; Sembiring, R. W.; Manurung, N.

2017-09-01

The concept of hard, dry and high speed machining can be combined, to produce high productivity, with lower production costs in manufacturing industry. Hard lathe process can be a solution to reduce production time. In lathe hard alloy steels reported problems relating to the integrity of such surface roughness, residual stress, the white layer and the surface integrity. AISI 4140 material is used for high reliable hydraulic system components. This material includes in cold work tool steel. Consideration election is because this material is able to be hardened up to 55 HRC. In this research, the experimental design using CCD model fit with three factors, each factor is composed of two levels, and six central point, experiments were conducted with 1 replications. The experimental design research using CCD model fit.

CO adsorption on the “29” Cu xO/Cu(111) surface: An integrated DFT, STM, and TPD study

DOE PAGES

Hensley, Alyssa J. R.; Therrien, Andrew J.; Zhang, Renqin; ...

2016-10-04

The elucidation of an accurate atomistic model of surface structures is crucial for the design and understanding of effective catalysts, a process requiring a close collaboration between experimental observations and theoretical models. Any developed surface theoretical model must agree with experimental results for the surface when both clean and adsorbate covered. Here, we present a detailed study of the adsorption of CO on the “29” Cu xO/ Cu(111) surface, which is important in the understanding of ubiquitous Cubased catalysis. This study uses scanning tunneling microscopy, temperatureprogrammed desorption, and density functional theory to analyze CO adsorption on the “29” Cu xO/Cu(111)more » surface. From the experimental scanning tunneling microscopy images, CO was found to form six different ordered structures on the “29” Cu xO/Cu(111) surface depending on the surface CO coverage. By modeling the adsorption of CO on our atomistic model of the “29” Cu xO/Cu(111) surface at different coverages, we were able to match the experimentally observed CO ordered structures to specific combinations of sites on the “29” Cu xO/Cu(111) surface. Lastly, the high degree of agreement seen here between experiment and theory for the adsorption of CO on the “29” Cu xO/Cu(111) surface at various CO coverages provides further support that our atomistic model of the “29” Cu xO/Cu(111) surface is experimentally accurate.« less

Review of Surface Properties of Thermal Protection Materials for the Design of IXV Thermal Protection System

NASA Astrophysics Data System (ADS)

Thoemel, J.; Cosson, E.; Chazot, O.

2009-01-01

In the framework of the creation of an aerothermodynamic database for the design the Intermediate Experimental Vehicle, surface properties of heat shield materials that represent the boundary conditions are reviewed. Catalytic and radiative characteristics available in the literature are critically analyzed and summarized. It turns out that large uncertainties on the parameters exist. Finally, simple and conservative values are proposed.

Investigation of optical/infrared sensor techniques for application satellites

NASA Technical Reports Server (NTRS)

Kaufman, I.

1972-01-01

A method of scanning an optical sensor array by acoustic surface waves is discussed. Data cover detailed computer based analysis of the operation of a multielement acoustic surface-wave-scanned optical sensor, the development of design and operation techniques that were used to show the feasibility of an integrated array to design several such arrays, and experimental verification of a number of the calculations with discrete sensor devices.

Experimental validation of a new heterogeneous mechanical test design

NASA Astrophysics Data System (ADS)

Aquino, J.; Campos, A. Andrade; Souto, N.; Thuillier, S.

2018-05-01

Standard material parameters identification strategies generally use an extensive number of classical tests for collecting the required experimental data. However, a great effort has been made recently by the scientific and industrial communities to support this experimental database on heterogeneous tests. These tests can provide richer information on the material behavior allowing the identification of a more complete set of material parameters. This is a result of the recent development of full-field measurements techniques, like digital image correlation (DIC), that can capture the heterogeneous deformation fields on the specimen surface during the test. Recently, new specimen geometries were designed to enhance the richness of the strain field and capture supplementary strain states. The butterfly specimen is an example of these new geometries, designed through a numerical optimization procedure where an indicator capable of evaluating the heterogeneity and the richness of strain information. However, no experimental validation was yet performed. The aim of this work is to experimentally validate the heterogeneous butterfly mechanical test in the parameter identification framework. For this aim, DIC technique and a Finite Element Model Up-date inverse strategy are used together for the parameter identification of a DC04 steel, as well as the calculation of the indicator. The experimental tests are carried out in a universal testing machine with the ARAMIS measuring system to provide the strain states on the specimen surface. The identification strategy is accomplished with the data obtained from the experimental tests and the results are compared to a reference numerical solution.

Design of experimental system for supercritical CO2 fracturing under confining pressure conditions

NASA Astrophysics Data System (ADS)

Wang, H.; Lu, Q.; Li, X.; Yang, B.; Zheng, Y.; Shi, L.; Shi, X.

2018-03-01

Supercritical CO2 has the characteristics of low viscosity, high diffusion and zero surface tension, and it is considered as a new fluid for non-polluting and non-aqueous fracturing which can be used for shale gas development. Fracturing refers to a method of utilizing the high-pressure fluid to generate fractures in the rock formation so as to improve the oil and gas flow conditions and increase the oil and gas production. In this article, a new type of experimental system for supercritical CO2 fracturing under confining pressure conditions is designed, which is based on characteristics of supercritical CO2, shale reservoir and down-hole environment. The experimental system consists of three sub-systems, including supercritical CO2 generation system, supercritical CO2 fracturing system and data analysis system. It can be used to simulate supercritical CO2 fracturing under geo-stress conditions, thus to study the rock initiation pressure, the formation of the rock fractures, fractured surface morphology and so on. The experimental system has successfully carried out a series of supercritical CO2 fracturing experiments. The experimental results confirm the feasibility of the experimental system and the high efficiency of supercritical CO2 in fracturing tight rocks.

Folded Fabry-Perot quasi-optical ring resonator diplexer Theory and experiment

NASA Technical Reports Server (NTRS)

Pickett, H. M.; Chiou, A. E. T.

1983-01-01

Performance of folded Fabry-Perot quasi-optical ring resonator diplexers with different geometries of reflecting surfaces is investigated both theoretically and experimentally. Design of optimum surface geometry for minimum diffraction, together with the figure of merit indicating improvement in performance, are given.

Metamaterial bricks and quantization of meta-surfaces

PubMed Central

Memoli, Gianluca; Caleap, Mihai; Asakawa, Michihiro; Sahoo, Deepak R.; Drinkwater, Bruce W.; Subramanian, Sriram

2017-01-01

Controlling acoustic fields is crucial in diverse applications such as loudspeaker design, ultrasound imaging and therapy or acoustic particle manipulation. The current approaches use fixed lenses or expensive phased arrays. Here, using a process of analogue-to-digital conversion and wavelet decomposition, we develop the notion of quantal meta-surfaces. The quanta here are small, pre-manufactured three-dimensional units—which we call metamaterial bricks—each encoding a specific phase delay. These bricks can be assembled into meta-surfaces to generate any diffraction-limited acoustic field. We apply this methodology to show experimental examples of acoustic focusing, steering and, after stacking single meta-surfaces into layers, the more complex field of an acoustic tractor beam. We demonstrate experimentally single-sided air-borne acoustic levitation using meta-layers at various bit-rates: from a 4-bit uniform to 3-bit non-uniform quantization in phase. This powerful methodology dramatically simplifies the design of acoustic devices and provides a key-step towards realizing spatial sound modulators. PMID:28240283

Metamaterial bricks and quantization of meta-surfaces

NASA Astrophysics Data System (ADS)

Memoli, Gianluca; Caleap, Mihai; Asakawa, Michihiro; Sahoo, Deepak R.; Drinkwater, Bruce W.; Subramanian, Sriram

2017-02-01

Controlling acoustic fields is crucial in diverse applications such as loudspeaker design, ultrasound imaging and therapy or acoustic particle manipulation. The current approaches use fixed lenses or expensive phased arrays. Here, using a process of analogue-to-digital conversion and wavelet decomposition, we develop the notion of quantal meta-surfaces. The quanta here are small, pre-manufactured three-dimensional units--which we call metamaterial bricks--each encoding a specific phase delay. These bricks can be assembled into meta-surfaces to generate any diffraction-limited acoustic field. We apply this methodology to show experimental examples of acoustic focusing, steering and, after stacking single meta-surfaces into layers, the more complex field of an acoustic tractor beam. We demonstrate experimentally single-sided air-borne acoustic levitation using meta-layers at various bit-rates: from a 4-bit uniform to 3-bit non-uniform quantization in phase. This powerful methodology dramatically simplifies the design of acoustic devices and provides a key-step towards realizing spatial sound modulators.

Metamaterial bricks and quantization of meta-surfaces.

PubMed

Memoli, Gianluca; Caleap, Mihai; Asakawa, Michihiro; Sahoo, Deepak R; Drinkwater, Bruce W; Subramanian, Sriram

2017-02-27

Controlling acoustic fields is crucial in diverse applications such as loudspeaker design, ultrasound imaging and therapy or acoustic particle manipulation. The current approaches use fixed lenses or expensive phased arrays. Here, using a process of analogue-to-digital conversion and wavelet decomposition, we develop the notion of quantal meta-surfaces. The quanta here are small, pre-manufactured three-dimensional units-which we call metamaterial bricks-each encoding a specific phase delay. These bricks can be assembled into meta-surfaces to generate any diffraction-limited acoustic field. We apply this methodology to show experimental examples of acoustic focusing, steering and, after stacking single meta-surfaces into layers, the more complex field of an acoustic tractor beam. We demonstrate experimentally single-sided air-borne acoustic levitation using meta-layers at various bit-rates: from a 4-bit uniform to 3-bit non-uniform quantization in phase. This powerful methodology dramatically simplifies the design of acoustic devices and provides a key-step towards realizing spatial sound modulators.

Use of statistical design of experiments for surface modification of Kapton films by CF4sbnd O2 microwave plasma treatment

NASA Astrophysics Data System (ADS)

Grandoni, Andrea; Mannini, Giacomo; Glisenti, Antonella; Manariti, Antonella; Galli, Giancarlo

2017-10-01

A statistical design of experiments (DoE) was used to evaluate the effects of CF4sbnd O2 plasma on Kapton films in which the duration of treatment, volume ratio of plasma gases, and microwave power were selected as effective experimental factors for systematic investigation of surface modification. Static water contact angle (θW), polar component of surface free energy (γSp) and surface O/C atomic ratio were analyzed as response variables. A significant enhancement in wettability and polarity of the treated films compared to untreated Kapton films was observed; depending on the experimental conditions, θW very significantly decreased, showing full wettability, and γSp rose dramatically, up to ten times. Within the DoE the conditions of plasma treatment were identified that resulted in selected optimal values of θW, γSp and O/C responses. Surface chemical changes were detected by XPS and ATR-IR investigations that evidenced both the introduction of fluorinated groups and the opening of the imide ring in the plasma-treated films.

Response surface methodology as an approach to determine optimal activities of lipase entrapped in sol-gel matrix using different vegetable oils.

PubMed

Pinheiro, Rubiane C; Soares, Cleide M F; de Castro, Heizir F; Moraes, Flavio F; Zanin, Gisella M

2008-03-01

The conditions for maximization of the enzymatic activity of lipase entrapped in sol-gel matrix were determined for different vegetable oils using an experimental design. The effects of pH, temperature, and biocatalyst loading on lipase activity were verified using a central composite experimental design leading to a set of 13 assays and the surface response analysis. For canola oil and entrapped lipase, statistical analyses showed significant effects for pH and temperature and also the interactions between pH and temperature and temperature and biocatalyst loading. For the olive oil and entrapped lipase, it was verified that the pH was the only variable statistically significant. This study demonstrated that response surface analysis is a methodology appropriate for the maximization of the percentage of hydrolysis, as a function of pH, temperature, and lipase loading.

Experimental aeroelastic control using adaptive wing model concepts

NASA Astrophysics Data System (ADS)

Costa, Antonio P.; Moniz, Paulo A.; Suleman, Afzal

2001-06-01

The focus of this study is to evaluate the aeroelastic performance and control of adaptive wings. Ailerons and flaps have been designed and implemented into 3D wings for comparison with adaptive structures and active aerodynamic surface control methods. The adaptive structures concept, the experimental setup and the control design are presented. The wind-tunnel tests of the wing models are presented for the open- and closed-loop systems. The wind tunnel testing has allowed for quantifying the effectiveness of the piezoelectric vibration control of the wings, and also provided performance data for comparison with conventional aerodynamic control surfaces. The results indicate that a wing utilizing skins as active structural elements with embedded piezoelectric actuators can be effectively used to improve the aeroelastic response of aeronautical components. It was also observed that the control authority of adaptive wings is much greater than wings using conventional aerodynamic control surfaces.

Assessment of Response Surface Models using Independent Confirmation Point Analysis

NASA Technical Reports Server (NTRS)

DeLoach, Richard

2010-01-01

This paper highlights various advantages that confirmation-point residuals have over conventional model design-point residuals in assessing the adequacy of a response surface model fitted by regression techniques to a sample of experimental data. Particular advantages are highlighted for the case of design matrices that may be ill-conditioned for a given sample of data. The impact of both aleatory and epistemological uncertainty in response model adequacy assessments is considered.

Status of the New Surface Muon Beamline at J-PARC MUSE

NASA Astrophysics Data System (ADS)

Strasser, P.; Koda, A.; Kojima, K. M.; Ito, T. U.; Fujimori, H.; Irie, Y.; Aoki, M.; Nakatsugawa, Y.; Higemoto, W.; Hiraishi, M.; Li, H.; Okabe, H.; Takeshita, S.; Shimomura, K.; Kawamura, N.; Kadono, R.; Miyake, Y.

A new surface muon beamline (S-line) dedicated to condensed matter physics experiments is being constructed at the Muon Science Facility (MUSE) located in the Materials and Life Science Facility (MLF) building at J-PARC. This beamline designed to provide high-intensity surface muons with a momentum of 28 MeV/c will comprise four beam legs and four experimental areas that will share the double-pulsed muon beam. The key feature is a new kicker system comprising two electric kickers to deliver the muon beam to the four experimental areas ensuring an optimum and seamless sharing of the double-pulsed muon beam. At present, only one experimental area (S1) has been completed and is now open to the user program since February 2017. An overview of the different aspects of this new surface muon beamline and the present status of the beam commissioning are presented.

First-Principles Studies of Structure-Property Relationships: Enabling Design of Functional Materials

NASA Astrophysics Data System (ADS)

Zhou, Qunfei

First-principles calculations based on quantum mechanics have been proved to be powerful for accurately regenerating experimental results, uncovering underlying myths of experimental phenomena, and accelerating the design of innovative materials. This work has been motivated by the demand to design next-generation thermionic emitting cathodes and techniques to allow for synthesis of photo-responsive polymers on complex surfaces with controlled thickness and patterns. For Os-coated tungsten thermionic dispenser cathodes, we used first-principles methods to explore the bulk and surface properties of W-Os alloys in order to explain the previously observed experimental phenomena that thermionic emission varies significantly with W-Os alloy composition. Meanwhile, we have developed a new quantum mechanical approach to quantitatively predict the thermionic emission current density from materials perspective without any semi-empirical approximations or complicated analytical models, which leads to better understanding of thermionic emission mechanism. The methods from this work could be used to accelerate the design of next-generation thermionic cathodes. For photoresponsive materials, we designed a novel type of azobenzene-containing monomer for light-mediated ring-opening metathesis polymerization (ROMP) toward the fabrication of patterned, photo-responsive polymers by controlling ring strain energy (RSE) of the monomer that drives ROMP. This allows for unprecedented remote, noninvasive, instantaneous spatial and temporal control of photo-responsive polymer deposition on complex surfaces.This work on the above two different materials systems showed the power of quantum mechanical calculations on predicting, understanding and discovering the structures and properties of both known and unknown materials in a fast, efficient and reliable way.

Mariner 9 mapping science sequence design.

NASA Technical Reports Server (NTRS)

Goldman, A. M., Jr.

1973-01-01

The primary mission of Mariner 9 was to map the Martian surface. This paper discusses in detail the design of the mapping science sequences which were executed by the spacecraft in sixty days and during which over eighty percent of the surface was photographed. The sequence design was influenced by many factors: experimenter scientific objectives, instrument capabilities, spacecraft capabilities, orbit characteristics, and data return rates, which are illustrated graphically. Typical orbits are depicted for each of the three different mapping phases lasting twenty days. Examples of typical orbital sequence plans prepared daily during mission operations are given.

Analytical and scale model research aimed at improved hangglider design

NASA Technical Reports Server (NTRS)

Kroo, I.; Chang, L. S.

1979-01-01

Research consisted of a theoretical analysis which attempts to predict aerodynamic characteristics using lifting surface theory and finite-element structural analysis as well as an experimental investigation using 1/5 scale elastically similar models in the NASA Ames 2m x 3m (7' x 10') wind tunnel. Experimental data were compared with theoretical results in the development of a computer program which may be used in the design and evaluation of ultralight gliders.

Design of an experimental apparatus for measurement of the surface tension of metastable fluids

NASA Astrophysics Data System (ADS)

Vinš, V.; Hrubý, J.; Hykl, J.; Blaha, J.; Šmíd, B.

2013-04-01

A unique experimental apparatus for measurement of the surface tension of aqueous mixtures has been designed, manufactured, and tested in our laboratory. The novelty of the setup is that it allows measurement of surface tension by two different methods: a modified capillary elevation method in a long vertical capillary tube and a method inspired by the approach of Hacker (National Advisory Committee for Aeronautics, Technical Note 2510, 1-20, 1951), i.e. in a short horizontal capillary tube. Functionality of all main components of the apparatus, e.g., glass chamber with the capillary tube, temperature control unit consisting of two thermostatic baths with special valves for rapid temperature jumps, helium distribution setup allowing pressure variation above the liquid meniscus inside the capillary tube, has been successfully tested. Preliminary results for the surface tension of the stable and metastable supercooled water measured by the capillary elevation method at atmospheric pressure are provided. The surface tension of water measured at temperatures between +26 °C and -11 °C is in good agreement with the extrapolated IAPWS correlation (IAPWS Release on Surface Tension of Ordinary Water Substance, September 1994); however it disagrees with data by Hacker.

An Experimental Study of the Ground Transportation System (GTS) Model in the NASA Ames 7- by 10-Ft Wind Tunnel

NASA Technical Reports Server (NTRS)

Storms, Bruce L.; Ross, James C.; Heineck, James T.; Walker, Stephen M.; Driver, David M.; Zilliac, Gregory G.; Bencze, Daniel P. (Technical Monitor)

2001-01-01

The 1/8-scale Ground Transportation System (GTS) model was studied experimentally in the NASA Ames 7- by 10-Ft Wind Tunnel. Designed for validation of computational fluid dynamics (CFD), the GTS model has a simplified geometry with a cab-over-engine design and no tractor-trailer gap. As a further simplification, all measurements of the GTS model were made without wheels. Aerodynamic boattail plates were also tested on the rear of the trailer to provide a simple geometry modification for computation. The experimental measurements include body-axis drag, surface pressures, surface hot-film anemometry, oil-film interferometry, and 3-D particle image velocimetry (PIV). The wind-averaged drag coefficient with and without boattail plates was 0.225 and 0.277, respectively. PIV measurements behind the model reveal a significant reduction in the wake size due to the flow turning provided by the boattail plates. Hot-film measurements on the side of the cab indicate laminar separation with turbulent reattachment within 0.08 trailer width for zero and +/- 10 degrees yaw. Oil film interferometry provided quantitative measurements of skin friction and qualitative oil flow images. A complete set of the experimental data and the surface definition of the model are included on a CD-ROM for further analysis and comparison.

A bee-hive frequency selective surface for Wi-Max and GPS applications

NASA Astrophysics Data System (ADS)

Ray, A.; Kahar, M.; Sarkar, P. P.

2013-10-01

The paper presents investigations on a bee-hive cell, concentric aperture frequency selective surface (FSS) tuned to pass 1.5 GHz for global positioning system application and 3.5 GHz for worldwide interoperability for microwave access applications. The designed dual-band FSS screen is easy to fabricate with low cost materials, exhibiting low weight, with two broad transmission bands, where the maximum recorded -10 dB transmission percentage bandwidth is 68.67 %. Due to symmetrical nature of design, FSS is insensitive to variation of RF incidence angle for 60° rotations. A computationally efficient method for analysing this FSS is presented. Experimental investigation is performed using standard microwave test bench. It is observed that the computed and experimental results are in close agreement.

Determination of B-complex vitamins in pharmaceutical formulations by surface-enhanced Raman spectroscopy

NASA Astrophysics Data System (ADS)

Junior, Benedito Roberto Alvarenga; Soares, Frederico Luis Felipe; Ardila, Jorge Armando; Durango, Luis Guillermo Cuadrado; Forim, Moacir Rossi; Carneiro, Renato Lajarim

2018-01-01

The aim of this work was to quantify B-complex vitamins in pharmaceutical samples by surface enhanced Raman spectroscopy technique using gold colloid substrate. Synthesis of gold nanoparticles was performed according to an adapted Turkevich method. Initial essays were able to suggest the orientation of molecules on gold nanoparticles surface. Central Composite design was performed to obtain the highest SERS signal for nicotinamide and riboflavin. The evaluated parameters in the experimental design were volume of AuNPs, concentration of vitamins and sodium chloride concentration. The best condition for nicotinamide was NaCl 2.3 × 10- 3 mol L- 1 and 700 μL of AuNPs colloid and this same condition showed to be adequate to quantify thiamine. The experimental design for riboflavin shows the best condition at NaCl 1.15 × 10- 2 mol L- 1 and 2.8 mL of AuNPs colloid. It was possible to quantify thiamine and nicotinamide in presence of others vitamins and excipients in two solid multivitamin formulations using the standard addition procedure. The standard addition curve presented a R2 higher than 0.96 for both nicotinamide and thiamine, at orders of magnitude 10- 7 and 10- 8 mol L- 1, respectively. The nicotinamide content in a cosmetic gel sample was also quantified by direct analysis presenting R2 0.98. The t-student test presented no significant difference regarding HPLC method. Despite the experimental design performed for riboflavin, it was not possible its quantification in the commercial samples.

Absolute surface reconstruction by slope metrology and photogrammetry

NASA Astrophysics Data System (ADS)

Dong, Yue

Developing the manufacture of aspheric and freeform optical elements requires an advanced metrology method which is capable of inspecting these elements with arbitrary freeform surfaces. In this dissertation, a new surface measurement scheme is investigated for such a purpose, which is to measure the absolute surface shape of an object under test through its surface slope information obtained by photogrammetric measurement. A laser beam propagating toward the object reflects on its surface while the vectors of the incident and reflected beams are evaluated from the four spots they leave on the two parallel transparent windows in front of the object. The spots' spatial coordinates are determined by photogrammetry. With the knowledge of the incident and reflected beam vectors, the local slope information of the object surface is obtained through vector calculus and finally yields the absolute object surface profile by a reconstruction algorithm. An experimental setup is designed and the proposed measuring principle is experimentally demonstrated by measuring the absolute surface shape of a spherical mirror. The measurement uncertainty is analyzed, and efforts for improvement are made accordingly. In particular, structured windows are designed and fabricated to generate uniform scattering spots left by the transmitted laser beams. Calibration of the fringe reflection instrument, another typical surface slope measurement method, is also reported in the dissertation. Finally, a method for uncertainty analysis of a photogrammetry measurement system by optical simulation is investigated.

Experimental study of the response functions of direct-reading instruments measuring surface-area concentration of airborne nanostructured particles

NASA Astrophysics Data System (ADS)

Bau, Sébastien; Witschger, Olivier; Gensdarmes, François; Thomas, Dominique

2009-05-01

An increasing number of experimental and theoretical studies focus on airborne nanoparticles (NP) in relation with many aspects of risk assessment to move forward our understanding of the hazards, the actual exposures in the workplace, and the limits of engineering controls and personal protective equipment with regard to NP. As a consequence, generating airborne NP with controlled properties constitutes an important challenge. In parallel, toxicological studies have been carried out, and most of them support the concept that surface-area could be a relevant metric for characterizing exposure to airborne NP [1]. To provide NP surface-area concentration measurements, some direct-reading instruments have been designed, based on attachment rate of unipolar ions to NP by diffusion. However, very few information is available concerning the performances of these instruments and the parameters that could affect their responses. In this context, our work aims at characterizing the actual available instruments providing airborne NP surface-area concentration. The instruments (a- LQ1-DC, Matter Engineering; b-AeroTrak™ 9000, TSI; c- NSAM, TSI model 3550;) are thought to be relevant for further workplace exposure characterization and monitoring. To achieve our work, an experimental facility (named CAIMAN) was specially designed, built and characterized.

Effect of Groove Surface Texture on Tribological Characteristics and Energy Consumption under High Temperature Friction.

PubMed

Wu, Wei; Chen, Guiming; Fan, Boxuan; Liu, Jianyou

2016-01-01

Energy consumption and tribological properties could be improved by proper design of surface texture in friction. However, some literature focused on investigating their performance under high temperature. In the study, different groove surface textures were fabricated on steels by a laser machine, and their tribological behaviors were experimentally studied with the employment of the friction and wear tester under distinct high temperature and other working conditions. The friction coefficient was recorded, and wear performance were characterized by double light interference microscope, scanning electron microscope (SEM) and x-ray energy dispersive spectrometry (EDS). Then, the performances of energy consumptions were carefully estimated. Results showed that friction coefficient, wear, and energy consumption could almost all be reduced by most textures under high temperature conditions, but to a different extent which depends on the experimental conditions and texture parameters. The main improvement mechanisms were analyzed, such as the hardness change, wear debris storage, thermal stress release and friction induced temperature reduction by the textures. Finally, a scattergram of the relatively reduced ratio of the energy consumption was drawn for different surface textures under four distinctive experimental conditions to illustrate the comprehensive energy consumption improving ability of textures, which was of benefit for the application of texture design.

Effect of Groove Surface Texture on Tribological Characteristics and Energy Consumption under High Temperature Friction

PubMed Central

Wu, Wei; Chen, Guiming; Fan, Boxuan; Liu, Jianyou

2016-01-01

Energy consumption and tribological properties could be improved by proper design of surface texture in friction. However, some literature focused on investigating their performance under high temperature. In the study, different groove surface textures were fabricated on steels by a laser machine, and their tribological behaviors were experimentally studied with the employment of the friction and wear tester under distinct high temperature and other working conditions. The friction coefficient was recorded, and wear performance were characterized by double light interference microscope, scanning electron microscope (SEM) and x-ray energy dispersive spectrometry (EDS). Then, the performances of energy consumptions were carefully estimated. Results showed that friction coefficient, wear, and energy consumption could almost all be reduced by most textures under high temperature conditions, but to a different extent which depends on the experimental conditions and texture parameters. The main improvement mechanisms were analyzed, such as the hardness change, wear debris storage, thermal stress release and friction induced temperature reduction by the textures. Finally, a scattergram of the relatively reduced ratio of the energy consumption was drawn for different surface textures under four distinctive experimental conditions to illustrate the comprehensive energy consumption improving ability of textures, which was of benefit for the application of texture design. PMID:27035658

Loading an Equidistant Ion Chain in a Ring Shaped Surface Trap and Anomalous Heating Studies with a High Optical Access Trap

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tabakov, Boyan

2015-07-01

Microfabricated segmented surface ion traps are one viable avenue to scalable quantum information processing. At Sandia National Laboratories we design, fabricate, and characterize such traps. Our unique fabrication capabilities allow us to design traps that facilitate tasks beyond quantum information processing. The design and performance of a trap with a target capability of storing hundreds of equally spaced ions on a ring is described. Such a device could aid experimental studies of phenomena as diverse as Hawking radiation, quantum phase transitions, and the Aharonov - Bohm effect. The fabricated device is demonstrated to hold a ~ 400 ion circular crystal,more » with 9 μm average spacing between ions. The task is accomplished by first characterizing undesired electric fields in the trapping volume and then designing and applying an electric field that substantially reduces the undesired fields. In addition, experimental efforts are described to reduce the motional heating rates in a surface trap by low energy in situ argon plasma treatment that reduces the amount of surface contaminants. The experiment explores the premise that carbonaceous compounds present on the surface contribute to the anomalous heating of secular motion modes in surface traps. This is a research area of fundamental interest to the ion trapping community, as heating adversely affects coherence and thus gate fidelity. The device used provides high optical laser access, substantially reducing scatter from the surface, and thus charging that may lead to excess micromotion. Heating rates for different axial mode frequencies are compared before and after plasma treatment. The presence of a carbon source near the plasma prevents making a conclusion on the observed absence of change in heating rates.« less

Metal-wool heat shields for space shuttle. [design, fabrication, and attachment to structure

NASA Technical Reports Server (NTRS)

Miller, R. C.; Clure, J. L.

1974-01-01

The packaging of metal wool for reusable thermal heat shields applied to aerodynamic and other surfaces for the space shuttle was analyzed and designed, and samples were fabricated and experimentally studied. Parametric trends were prepared for selected configurations. An all-metal thermally efficient, reliable, reusable and producible heat shield system was designed and structurally tested for use on spacecraft aerodynamic surfaces where temperatures do not exceed 810 K. Stainless steel sheet, primarily for structure and secondarily in the transverse plane for thermal expansion, was shown to accommodate thermal expansion in all directions when restrained at the edges and heated to 1360 K. Aerodynamic loads of 0.35 x 1000,000 newtons/sq meter, and higher, may be easily accepted by structures of this design. Seven all-metal thermal protection specimens, 12.7 cm square and 2.5 cm thick were fabricated and are being experimentally evaluated at simulated shuttle entry conditions in an arc jet facility.

A conceptual design study of point focusing thin-film solar concentrators

NASA Technical Reports Server (NTRS)

1981-01-01

Candidates for reflector panel design concepts, including materials and configurations, were identified. The large list of candidates was screened and reduced to the five most promising ones. Cost and technical factors were used in making the final choices for the panel conceptual design, which was a stiffened steel skin substrate with a bonded, acrylic overcoated, aluminized polyester film reflective surface. Computer simulations were run for the concentrator optics using the selected panel design, and experimentally determined specularity and reflectivity values. Intercept factor curves and energy to the aperture curves were produced. These curves indicate that surface errors of 2 mrad (milliradians) or less would be required to capture the desired energy for a Brayton cycle 816 C case. Two test panels were fabricated to demonstrate manufacturability and optically tested for surface error. Surface errors in the range of 1.75 mrad and 2.2 mrad were measured.

Electrografted diazonium salt layers for antifouling on the surface of surface plasmon resonance biosensors.

PubMed

Zou, Qiongjing; Kegel, Laurel L; Booksh, Karl S

2015-02-17

Electrografted diazonium salt layers on the surface of surface plasmon resonance (SPR) sensors present potential for a significant improvement in antifouling coatings. A pulsed potential deposition profile was used in order to circumvent mass-transport limitations for layer deposition rate. The influence of number of pulses with respect to antifouling efficacy was evaluated by nonspecific adsorption surface coverage of crude bovine serum proteins. Instead of using empirical and rough estimated values, the penetration depth and sensitivity of the SPR instrument were experimentally determined for the calculation of nonspecific adsorption surface coverage. This provides a method to better examine antifouling surface coatings and compare crossing different coatings and experimental systems. Direct comparison of antifouling performance of different diazonium salts was facilitated by a tripad SPR sensor design. The electrografted 4-phenylalanine diazonium chloride (4-APhe) layers with zwitterionic characteristic demonstrate ultralow fouling.

Design and Performance Calculations of a Propeller for Very High Altitude Flight. Degree awarded by Case Western Univ.

NASA Technical Reports Server (NTRS)

Koch, L. Danielle

1998-01-01

Reported here is a design study of a propeller for a vehicle capable of subsonic flight in Earth's stratosphere. All propellers presented were required to absorb 63.4 kW (85 hp) at 25.9 km (85,000 ft) while aircraft cruise velocity was maintained at Mach 0.40. To produce the final design, classic momentum and blade-element theories were combined with two and three-dimensional results from the Advanced Ducted Propfan Analysis Code (ADPAC), a numerical Navier-Stokes analysis code. The Eppler 387 airfoil was used for each of the constant section propeller designs compared. Experimental data from the Langley Low-Turbulence Pressure Tunnel was used in the strip theory design and analysis programs written. The experimental data was also used to validate ADPAC at a Reynolds numbers of 60,000 and a Mach number of 0.20. Experimental and calculated surface pressure coefficients are compared for a range of angles of attack. Since low Reynolds number transonic experimental data was unavailable, ADPAC was used to generate two-dimensional section performance predictions for Reynolds numbers of 60,000 and 100,000 and Mach numbers ranging from 0.45 to 0.75. Surface pressure coefficients are presented for selected angles of attack. in addition to the variation of lift and drag coefficients at each flow condition. A three-dimensional model of the final design was made which ADPAC used to calculated propeller performance. ADPAC performance predictions were compared with strip-theory calculations at design point. Propeller efficiency predicted by ADPAC was within 1.5% of that calculated by strip theory methods, although ADPAC predictions of thrust, power, and torque coefficients were approximately 5% lower than the strip theory results. Simplifying assumptions made in the strip theory account for the differences seen.

From the generalized reflection law to the realization of perfect anomalous reflectors

PubMed Central

Díaz-Rubio, Ana; Asadchy, Viktar S.; Elsakka, Amr; Tretyakov, Sergei A.

2017-01-01

The use of the generalized Snell’s law opens wide possibilities for the manipulation of transmitted and reflected wavefronts. However, known structures designed to shape reflection wavefronts suffer from significant parasitic reflections in undesired directions. We explore the limitations of the existing solutions for the design of passive planar reflectors and demonstrate that strongly nonlocal response is required for perfect performance. A new paradigm for the design of perfect reflectors based on energy surface channeling is introduced. We realize and experimentally verify a perfect design of an anomalously reflective surface using an array of rectangular metal patches backed by a metallic plate. This conceptually new mechanism for wavefront manipulation allows the design of thin perfect reflectors, offering a versatile design method applicable to other scenarios, such as focusing reflectors, surface wave manipulations, or metasurface holograms, extendable to other frequencies. PMID:28819642

Experimental Evaluation of the Thermal Performance of a Water Shield for a Surface Power Reactor

NASA Technical Reports Server (NTRS)

Pearson, J. Boise; Stewart, Eric T.; Reid, Robert S.

2007-01-01

A water based shielding system is being investigated for use on initial lunar surface power systems. The use of water may lower overall cost (as compared to development cost for other materials) and simplify operations in the setup and handling. The thermal hydraulic performance of the shield is of significant interest. The mechanism for transferring heat through the shield is natural convection. Natural convection in a representative lunar surface reactor shield design is evaluated at various power levels in the Water Shield Testbed (WST) at the NASA Marshall Space Flight Center. The experimental data from the WST is used to anchor a CFD model. Performance of a water shield on the lunar surface is then predicted by CFD models anchored to test data. The accompanying viewgraph presentation includes the following topics: 1) Testbed Configuration; 2) Core Heater Placement and Instrumentation; 3) Thermocouple Placement; 4) Core Thermocouple Placement; 5) Outer Tank Thermocouple Placement; 6) Integrated Testbed; 7) Methodology; 8) Experimental Results: Core Temperatures; 9) Experimental Results; Outer Tank Temperatures; 10) CFD Modeling; 11) CFD Model: Anchored to Experimental Results (1-g); 12) CFD MOdel: Prediction for 1/6-g; and 13) CFD Model: Comparison of 1-g to 1/6-g.

Experimental Evaluation of a Water Shield for a Surface Power Reactor

NASA Technical Reports Server (NTRS)

Pearson, J. B.; Reid, R.; Sadasivan, P.; Stewart, E.

2007-01-01

A water based shielding system is being investigated for use on initial lunar surface power systems. The use of water may lower overall cost (as compared to development cost for other materials) and simplify operations in the setup and handling. The thermal hydraulic performance of the shield is of significant interest. The mechanism for transferring heat through the shield is natural convection. A representative lunar surface reactor design is evaluated at various power levels in the Water Shield Testbed (WST) at the NASA Marshall Space Flight Center. The evaluation compares the experimental data from the WST to CFD models. Performance of a water shield on the lunar surface is predicted by CFD models anchored to test data, and by matching relevant dimensionless parameters.

A unified approach for determining the ultimate strength of RC members subjected to combined axial force, bending, shear and torsion

PubMed Central

Huang, Zhen

2017-01-01

This paper uses experimental investigation and theoretical derivation to study the unified failure mechanism and ultimate capacity model of reinforced concrete (RC) members under combined axial, bending, shear and torsion loading. Fifteen RC members are tested under different combinations of compressive axial force, bending, shear and torsion using experimental equipment designed by the authors. The failure mechanism and ultimate strength data for the four groups of tested RC members under different combined loading conditions are investigated and discussed in detail. The experimental research seeks to determine how the ultimate strength of RC members changes with changing combined loads. According to the experimental research, a unified theoretical model is established by determining the shape of the warped failure surface, assuming an appropriate stress distribution on the failure surface, and considering the equilibrium conditions. This unified failure model can be reasonably and systematically changed into well-known failure theories of concrete members under single or combined loading. The unified calculation model could be easily used in design applications with some assumptions and simplifications. Finally, the accuracy of this theoretical unified model is verified by comparisons with experimental results. PMID:28414777

Classes of Split-Plot Response Surface Designs for Equivalent Estimation

NASA Technical Reports Server (NTRS)

Parker, Peter A.; Kowalski, Scott M.; Vining, G. Geoffrey

2006-01-01

When planning an experimental investigation, we are frequently faced with factors that are difficult or time consuming to manipulate, thereby making complete randomization impractical. A split-plot structure differentiates between the experimental units associated with these hard-to-change factors and others that are relatively easy-to-change and provides an efficient strategy that integrates the restrictions imposed by the experimental apparatus. Several industrial and scientific examples are presented to illustrate design considerations encountered in the restricted randomization context. In this paper, we propose classes of split-plot response designs that provide an intuitive and natural extension from the completely randomized context. For these designs, the ordinary least squares estimates of the model are equivalent to the generalized least squares estimates. This property provides best linear unbiased estimators and simplifies model estimation. The design conditions that allow for equivalent estimation are presented enabling design construction strategies to transform completely randomized Box-Behnken, equiradial, and small composite designs into a split-plot structure.

Comparative Evaluation of Quantitative Test Methods for Gases on a Hard Surface

DTIC Science & Technology

2017-02-01

COMPARATIVE EVALUATION OF QUANTITATIVE TEST METHODS FOR GASES ON A HARD SURFACE ECBC-TR-1426 Vipin Rastogi...1 COMPARATIVE EVALUATION OF QUANTITATIVE TEST METHODS FOR GASES ON A HARD SURFACE 1. INTRODUCTION Members of the U.S. Environmental...Generator 4 2.4 Experimental Design Each quantitative method was performed three times on three consecutive days. For the CD runs, three

Weathering of iron sulfides under Mars surface ambient conditions

NASA Technical Reports Server (NTRS)

Blackburn, T. R.

1981-01-01

The study of iron sulfide surface alternation reactions under Mars' surface ambient conditions begun during 1980 was extended through improved irradiation design and experimental protocols. A wider range of humidities and more intense irradiation were incorporated in the study. X-ray photoelectron spectra of irradiated chips suggest formation of FeSO4, FeCO3, and an iron oxide on the iron sulfide substrates studied.

Surface Wave Cloak from Graded Refractive Index Nanocomposites

PubMed Central

La Spada, L.; McManus, T. M.; Dyke, A.; Haq, S.; Zhang, L.; Cheng, Q.; Hao, Y.

2016-01-01

Recently, a great deal of interest has been re-emerged on the possibility to manipulate surface waves, in particular, towards the THz and optical regime. Both concepts of Transformation Optics (TO) and metamaterials have been regarded as one of key enablers for such applications in applied electromagnetics. In this paper, we experimentally demonstrate for the first time a dielectric surface wave cloak from engineered gradient index materials to illustrate the possibility of using nanocomposites to control surface wave propagation through advanced additive manufacturing. The device is designed analytically and validated through numerical simulations and measurements, showing good agreement and performance as an effective surface wave cloak. The underlying design approach has much wider applications, which span from microwave to optics for the control of surface plasmon polaritons (SPPs) and radiation of nanoantennas. PMID:27416815

Computational simulation of biomolecules transport with multi-physics near microchannel surface for development of biomolecules-detection devices.

PubMed

Suzuki, Yuma; Shimizu, Tetsuhide; Yang, Ming

2017-01-01

The quantitative evaluation of the biomolecules transport with multi-physics in nano/micro scale is demanded in order to optimize the design of microfluidics device for the biomolecules detection with high detection sensitivity and rapid diagnosis. This paper aimed to investigate the effectivity of the computational simulation using the numerical model of the biomolecules transport with multi-physics near a microchannel surface on the development of biomolecules-detection devices. The biomolecules transport with fluid drag force, electric double layer (EDL) force, and van der Waals force was modeled by Newtonian Equation of motion. The model validity was verified in the influence of ion strength and flow velocity on biomolecules distribution near the surface compared with experimental results of previous studies. The influence of acting forces on its distribution near the surface was investigated by the simulation. The trend of its distribution to ion strength and flow velocity was agreement with the experimental result by the combination of all acting forces. Furthermore, EDL force dominantly influenced its distribution near its surface compared with fluid drag force except for the case of high velocity and low ion strength. The knowledges from the simulation might be useful for the design of biomolecules-detection devices and the simulation can be expected to be applied on its development as the design tool for high detection sensitivity and rapid diagnosis in the future.

Modeling and experimental study on near-field acoustic levitation by flexural mode.

PubMed

Liu, Pinkuan; Li, Jin; Ding, Han; Cao, Wenwu

2009-12-01

Near-field acoustic levitation (NFAL) has been used in noncontact handling and transportation of small objects to avoid contamination. We have performed a theoretical analysis based on nonuniform vibrating surface to quantify the levitation force produced by the air film and also conducted experimental tests to verify our model. Modal analysis was performed using ANSYS on the flexural plate radiator to obtain its natural frequency of desired mode, which is used to design the measurement system. Then, the levitation force was calculated as a function of levitation distance based on squeeze gas film theory using measured amplitude and phase distributions on the vibrator surface. Compared with previous fluid-structural analyses using a uniform piston motion, our model based on the nonuniform radiating surface of the vibrator is more realistic and fits better with experimentally measured levitation force.

Surface Traps in Colloidal Quantum Dots: A Combined Experimental and Theoretical Perspective.

PubMed

Giansante, Carlo; Infante, Ivan

2017-10-19

Surface traps are ubiquitous to nanoscopic semiconductor materials. Understanding their atomistic origin and manipulating them chemically have capital importance to design defect-free colloidal quantum dots and make a leap forward in the development of efficient optoelectronic devices. Recent advances in computing power established computational chemistry as a powerful tool to describe accurately complex chemical species and nowadays it became conceivable to model colloidal quantum dots with realistic sizes and shapes. In this Perspective, we combine the knowledge gathered in recent experimental findings with the computation of quantum dot electronic structures. We analyze three different systems: namely, CdSe, PbS, and CsPbI 3 as benchmark semiconductor nanocrystals showing how different types of trap states can form at their surface. In addition, we suggest experimental healing of such traps according to their chemical origin and nanocrystal composition.

Noise characteristics of upper surface blown configurations: Analytical Studies

NASA Technical Reports Server (NTRS)

Reddy, N. N.; Tibbetts, J. G.; Pennock, A. P.; Tam, C. K. W.

1978-01-01

Noise and flow results of upper surface blown configurations were analyzed. The dominant noise source mechanisms were identified from experimental data. From far-field noise data for various geometric and operational parameters, an empirical noise prediction program was developed and evaluated by comparing predicted results with experimental data from other tests. USB aircraft compatibility studies were conducted using the described noise prediction and a cruise performance data base. A final design aircraft was selected and theory was developed for the noise from the trailing edge wake assuming it as a highly sheared layer.

Plaque removal efficacy of a battery-operated toothbrush compared to a manual toothbrush.

PubMed

Ruhlman, C D; Bartizek, R D; Biesbrock, A R

2001-08-01

Recently, a new power toothbrush has been marketed with a design that fundamentally differs from other marketed power toothbrushes, in that it incorporates a round oscillating head, in conjunction with fixed bristles. The objective of this study was to compare the plaque removal efficacy of a control manual toothbrush (Colgate Navigator) to this experimental power toothbrush (Crest SpinBrush) following a single use. This study was a randomized, controlled, examiner-blind, 4-period crossover design which examined plaque removal with the two toothbrushes following a single use in 40 completed subjects. Plaque was scored before and after brushing using the Turesky Modification of the Quigley-Hein Index. Baseline plaque scores were 1.77 for both the experimental toothbrush and control toothbrush treatment groups. With respect to all surfaces examined, the experimental toothbrush delivered an adjusted (via analysis of covariance) mean difference between baseline and post-brushing plaque scores of 0.48 while the control toothbrush delivered an adjusted mean difference of 0.35. The experimental toothbrush removed, on average, 37.6% more plaque than the control toothbrush. These results were statistically significant (P< 0.001). With respect to buccal surfaces, the experimental toothbrush delivered an adjusted mean difference between baseline and post-brushing plaque scores of 0.54 while the control toothbrush delivered an adjusted mean difference of 0.42. This represents 27.8% more plaque removal with the experimental toothbrush compared to the control toothbrush. These results were also statistically significant (P= 0.001). Results on lingual surfaces also demonstrated statistically significantly (P< 0.001) greater plaque removal for the experimental toothbrush with an average of 53.4% more plaque removal.

Effects of Terminological Concreteness on Middle-School Students' Learning of Experimental Design

ERIC Educational Resources Information Center

Siler, Stephanie Ann; Klahr, David

2016-01-01

One obstacle to understanding abstract concepts such as the "control of variables" strategy (CVS) is the tendency for learners to focus on surface rather than deep features in instructional materials. However, in tasks such as learning CVS, these same surface features may also support understanding, provided learners realize the…

Improvement of MRR and surface roughness during electrical discharge machining (EDM) using aluminum oxide powder mixed dielectric fluid

NASA Astrophysics Data System (ADS)

Khan, A. A.; Mohiuddin, A. K. M.; Latif, M. A. A.

2018-01-01

This paper discusses the effect of aluminium oxide (Al203) addition to dielectric fluid during electrical discharge machining (EDM). Aluminium oxide was added to the dielectric used in the EDM process to improve its performance when machining the stainless steel AISI 304, while copper was used as the electrode. Effect of the concentration of Al203 (0.3 mg/L) in dielectric fluid was compared with EDM without any addition of Al203. Surface quality of stainless steel and the material removal rate were investigated. Design of the experiment (DOE) was used for the experimental plan. Statistical analysis was done using ANOVA and then appropriate model was designated. The experimental results show that with dispersing of aluminium oxide in dielectric fluid surface roughness was improved while the material removal rate (MRR) was increased to some extent. These indicate the improvement of EDM performance using aluminium oxide in dielectric fluid. It was also found that with increase in pulse on time both MRR and surface roughness increase sharply.

Calibration Designs for Non-Monolithic Wind Tunnel Force Balances

NASA Technical Reports Server (NTRS)

Johnson, Thomas H.; Parker, Peter A.; Landman, Drew

2010-01-01

This research paper investigates current experimental designs and regression models for calibrating internal wind tunnel force balances of non-monolithic design. Such calibration methods are necessary for this class of balance because it has an electrical response that is dependent upon the sign of the applied forces and moments. This dependency gives rise to discontinuities in the response surfaces that are not easily modeled using traditional response surface methodologies. An analysis of current recommended calibration models is shown to lead to correlated response model terms. Alternative modeling methods are explored which feature orthogonal or near-orthogonal terms.

Experiment Design for Complex VTOL Aircraft with Distributed Propulsion and Tilt Wing

NASA Technical Reports Server (NTRS)

Murphy, Patrick C.; Landman, Drew

2015-01-01

Selected experimental results from a wind tunnel study of a subscale VTOL concept with distributed propulsion and tilt lifting surfaces are presented. The vehicle complexity and automated test facility were ideal for use with a randomized designed experiment. Design of Experiments and Response Surface Methods were invoked to produce run efficient, statistically rigorous regression models with minimized prediction error. Static tests were conducted at the NASA Langley 12-Foot Low-Speed Tunnel to model all six aerodynamic coefficients over a large flight envelope. This work supports investigations at NASA Langley in developing advanced configurations, simulations, and advanced control systems.

Designing perfect linear polarization converters using perfect electric and magnetic conducting surfaces

PubMed Central

Zhou, Gaochao; Tao, Xudong; Shen, Ze; Zhu, Guanghao; Jin, Biaobing; Kang, Lin; Xu, Weiwei; Chen, Jian; Wu, Peiheng

2016-01-01

We propose a kind of general framework for the design of a perfect linear polarization converter that works in the transmission mode. Using an intuitive picture that is based on the method of bi-directional polarization mode decomposition, it is shown that when the device under consideration simultaneously possesses two complementary symmetry planes, with one being equivalent to a perfect electric conducting surface and the other being equivalent to a perfect magnetic conducting surface, linear polarization conversion can occur with an efficiency of 100% in the absence of absorptive losses. The proposed framework is validated by two design examples that operate near 10 GHz, where the numerical, experimental and analytic results are in good agreements. PMID:27958313

An experimental study on low-velocity low-gravity collisions into granular surfaces

NASA Astrophysics Data System (ADS)

Sunday, C.; Murdoch, N.; Mimoun, D.

2014-07-01

The Japanese Space Agency (JAXA) is scheduled to launch the asteroid sample-return mission, Hayabusa-2, to target body 1999 JU_3 in December 2014 [1]. The spacecraft will arrive at the C-type near-Earth asteroid in mid-2018 and deploy several science payloads to its surface. Among these payloads is a 10-kg lander, the Mobile Asteroid Surface Scout (MASCOT), provided by the German Space Agency (DLR) with cooperation from the Centre National d'Etudes Spatiales (CNES). MASCOT will reach the asteroid's surface with an anticipated impact speed of 10--20 cm/s. In addition to housing four instruments for in-situ science investigation, MASCOT contains a mobility mechanism that will correct its orientation and enable it to ''hop'' to various measurement sites [2]. Based on thermal infrared observations [3,4,5] and previous space missions [6,7], it is strongly believed that 1999 JU_3 is covered by loose regolith. The asteroid's granular surface, in combination with the low surface gravity, makes it difficult to predict the lander's collision behavior from existing theoretical models. However, to ensure that MASCOT can successfully fulfill its mission, it is vital to understand the rebound dynamics of the lander in the asteroid surface environment. The objective of this work, derived from the needs of current and future asteroid missions, is to present an experiment designed to study low-velocity, low-gravity collisions into granular surfaces. The experiment measures the amount of energy lost during impact via a projectile's coefficient of restitution and also the acceleration profile of the projectile during collision. The key challenge to designing an asteroid collision experiment is finding a way to simulate reduced gravity conditions on the Earth so that the prevailing forces in micro-gravity collisions can be reflected in the experimental results. The proposed way to achieve this goal is to let a free-falling projectile impact a surface with a constant downward acceleration, or an acceleration less than that of gravity, so that the effective surface acceleration felt by the grains at impact is very small. In reducing the effective surface acceleration of the granular material, the medium's inter-grain cohesion forces will become more important compared to its weight force [8], and the properties of the granular material will become more representative of those on an asteroid's surface. The concept of effective acceleration drives the design of this experiment and results in the following key features: First, the granular surface is given a constant downward acceleration using an Atwood machine, or a system of pulleys and counterweights. Next, the projectile and surface are simultaneously released from rest using a magnetic solenoid and hook assembly. The starting height of the surface container and the initial separation distance between the projectile and surface are variable and chosen to accommodate collision velocities of 10--20 cm/s and effective accelerations of 0.3--1.0 m/s^2. Finally, wireless accelerometers, placed on the surface container and in the projectile, provide acceleration data, while high-speed cameras capable of recording 100,000 frames per second capture the collision and act as secondary data sources. The experiment is built into an existing 6-m drop-tower frame and requires the custom design of all components, including the projectile, surface sample container, release mechanism, and deceleration system. This work will present the detailed design of the asteroid-collision experiment as well as a discussion on the planned experimental trials. The experimental results, once obtained, will be used to create a scaling law that will help predict a projectile's rebound and acceleration behavior during a low-velocity collision into a granular surface in micro-gravity conditions.

Theoretical Design and Experimental Realization of Quasi Single Electron Enhancement in Plasmonic Catalysis.

PubMed

Wang, Jiale; Alves, Tiago V; Trindade, Fabiane J; de Aquino, Caroline B; Pieretti, Joana C; Domingues, Sergio H; Ando, Romulo A; Ornellas, Fernando R; Camargo, Pedro H C

2015-11-23

By a combination of theoretical and experimental design, we probed the effect of a quasi-single electron on the surface plasmon resonance (SPR)-mediated catalytic activities of Ag nanoparticles. Specifically, we started by theoretically investigating how the E-field distribution around the surface of a Ag nanosphere was influenced by static electric field induced by one, two, or three extra fixed electrons embedded in graphene oxide (GO) next to the Ag nanosphere. We found that the presence of the extra electron(s) changed the E-field distributions and led to higher electric field intensities. Then, we experimentally observed that a quasi-single electron trapped at the interface between GO and Ag NPs in Ag NPs supported on graphene oxide (GO-Ag NPs) led to higher catalytic activities as compared to Ag and GO-Ag NPs without electrons trapped at the interface, representing the first observation of catalytic enhancement promoted by a quasi-single electron. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Optimization of photocatalytic degradation of methyl blue using silver ion doped titanium dioxide by combination of experimental design and response surface approach.

PubMed

Sahoo, C; Gupta, A K

2012-05-15

Photocatalytic degradation of methyl blue (MYB) was studied using Ag(+) doped TiO(2) under UV irradiation in a batch reactor. Catalytic dose, initial concentration of dye and pH of the reaction mixture were found to influence the degradation process most. The degradation was found to be effective in the range catalytic dose (0.5-1.5g/L), initial dye concentration (25-100ppm) and pH of reaction mixture (5-9). Using the three factors three levels Box-Behnken design of experiment technique 15 sets of experiments were designed considering the effective ranges of the influential parameters. The results of the experiments were fitted to two quadratic polynomial models developed using response surface methodology (RSM), representing functional relationship between the decolorization and mineralization of MYB and the experimental parameters. Design Expert software version 8.0.6.1 was used to optimize the effects of the experimental parameters on the responses. The optimum values of the parameters were dose of Ag(+) doped TiO(2) 0.99g/L, initial concentration of MYB 57.68ppm and pH of reaction mixture 7.76. Under the optimal condition the predicted decolorization and mineralization rate of MYB were 95.97% and 80.33%, respectively. Regression analysis with R(2) values >0.99 showed goodness of fit of the experimental results with predicted values. Copyright © 2012 Elsevier B.V. All rights reserved.

Determination of B-complex vitamins in pharmaceutical formulations by surface-enhanced Raman spectroscopy.

PubMed

Junior, Benedito Roberto Alvarenga; Soares, Frederico Luis Felipe; Ardila, Jorge Armando; Durango, Luis Guillermo Cuadrado; Forim, Moacir Rossi; Carneiro, Renato Lajarim

2018-01-05

The aim of this work was to quantify B-complex vitamins in pharmaceutical samples by surface enhanced Raman spectroscopy technique using gold colloid substrate. Synthesis of gold nanoparticles was performed according to an adapted Turkevich method. Initial essays were able to suggest the orientation of molecules on gold nanoparticles surface. Central Composite design was performed to obtain the highest SERS signal for nicotinamide and riboflavin. The evaluated parameters in the experimental design were volume of AuNPs, concentration of vitamins and sodium chloride concentration. The best condition for nicotinamide was NaCl 2.3×10 -3 molL -1 and 700μL of AuNPs colloid and this same condition showed to be adequate to quantify thiamine. The experimental design for riboflavin shows the best condition at NaCl 1.15×10 -2 molL -1 and 2.8mL of AuNPs colloid. It was possible to quantify thiamine and nicotinamide in presence of others vitamins and excipients in two solid multivitamin formulations using the standard addition procedure. The standard addition curve presented a R 2 higher than 0.96 for both nicotinamide and thiamine, at orders of magnitude 10 -7 and 10 -8 molL -1 , respectively. The nicotinamide content in a cosmetic gel sample was also quantified by direct analysis presenting R 2 0.98. The t-student test presented no significant difference regarding HPLC method. Despite the experimental design performed for riboflavin, it was not possible its quantification in the commercial samples. Copyright © 2017 Elsevier B.V. All rights reserved.

Active Surfaces and Interfaces of Soft Materials

NASA Astrophysics Data System (ADS)

Wang, Qiming

A variety of intriguing surface patterns have been observed on developing natural systems, ranging from corrugated surface of white blood cells at nanometer scales to wrinkled dog skins at millimeter scales. To mimetically harness functionalities of natural morphologies, artificial transformative skin systems by using soft active materials have been rationally designed to generate versatile patterns for a variety of engineering applications. The study of the mechanics and design of these dynamic surface patterns on soft active materials are both physically interesting and technologically important. This dissertation starts with studying abundant surface patterns in Nature by constructing a unified phase diagram of surface instabilities on soft materials with minimum numbers of physical parameters. Guided by this integrated phase diagram, an electroactive system is designed to investigate a variety of electrically-induced surface instabilities of elastomers, including electro-creasing, electro-cratering, electro-wrinkling and electro-cavitation. Combing experimental, theoretical and computational methods, the initiation, evolution and transition of these instabilities are analyzed. To apply these dynamic surface instabilities to serving engineering and biology, new techniques of Dynamic Electrostatic Lithography and electroactive anti-biofouling are demonstrated.

A Quasi-Experimental Design Determining the Effectiveness of Dynamic Seating on Classroom Off-Task Behaviors

ERIC Educational Resources Information Center

Eggleston, Jessica

2017-01-01

Elementary students spend an average of five and a quarter hours per day seated on a hard surface which provides little sensory input and possibly contributes to discomfort. Sensory integration was found to improve executive functioning skills in elementary students by helping their comfort level at being seated. This quasi-experimental study…

Theoretical and experimental investigation of design for multioptical-axis freeform progressive addition lenses

NASA Astrophysics Data System (ADS)

Xiang, HuaZhong; Chen, JiaBi; Zhu, TianFen; Wei, YeFei; Fu, DongXiang

2015-11-01

A freeform progressive addition lens (PAL) provides a good solution to correct presbyopia and prevent juvenile myopia by distributing pupils' optical powers of distance zone, near zone, and intermediate zone and is more widely adopted in the present optometric study. However, there is still a lack of a single-optical-axis system for the design of a PAL. This paper focuses on the research for an approach for designing a freeform PAL. A multioptical-axis system based on real viewing conditions using the eyes is employed for the representation of the freeform surface. We filled small pupils in the intermediate zone as a progressive corridor and the distance- and near-vision portions were defined as the standard spherical surfaces delimited by quadratic curves. Three freeform PALs with a spherical surface as the front side and a freeform surface as the backside were designed. We demonstrate the fabrication and measurement technologies for the PAL surface using computer numerical control machine tools from Schneider Smart and a Visionix VM-2000 Lens Power Mapper. Surface power and astigmatic values were obtained. Preliminary results showed that the approach for the design and fabrication is helpful to advance the design procedure optimization and mass production of PALs in optometry.

The importance of surface recombination and energy-bandgap narrowing in p-n-junction silicon solar cells

NASA Technical Reports Server (NTRS)

Fossum, J. G.; Lindholm, F. A.; Shibib, M. A.

1979-01-01

Experimental data demonstrating the sensitivity of open-circuit voltage to front-surface conditions are presented for a variety of p-n-junction silicon solar cells. Analytical models accounting for the data are defined and supported by additional experiments. The models and the data imply that a) surface recombination significantly limits the open-circuit voltage (and the short-circuit current) of typical silicon cells, and b) energy-bandgap narrowing is important in the manifestation of these limitations. The models suggest modifications in both the structural design and the fabrication processing of the cells that would result in substantial improvements in cell performance. The benefits of one such modification - the addition of a thin thermal silicon-dioxide layer on the front surface - are indicated experimentally.

Application of response surface methodology for optimization of polygalacturonase production by Aspergillus niger.

PubMed

Yadav, Kaushlesh K; Garg, Neelima; Kumar, Devendra; Kumar, Sanjay; Singh, Achal; Muthukumar, M

2015-01-01

Polygalacturonase (PG) degrades pectin into D-galacturonic acid monomers and is used widely in food industry especially for juice clarification. In the present study,. fermentation conditions for polygalacturonase production by Asgergillus niger NAIMCCF-02958, using mango peel as substrate, were optimized using the 2(3) factorial design with central composite rotatable experimental design (CCRD) of response surface methodology (RSM). The maximum PG activity 723.66 U g(-1) was achieved under pH 4.0, temperature 30 degrees C and 2% inoculum by response surface curve. The experimental value of PG activity wkas higher 607.65 U g(-1) than the predicted value 511.75 U g(-1). Under the proposed optimized conditions, the determination coefficient (R2) was equal to 0.66 indicating that the model could explain 66% of the total variation as well as establish the relationship between the variables and the responses. ANOVA analysis and the three dimensional plots also confirmed interactions among the parameters.

An Experimental Framework for Generating Evolvable Chemical Systems in the Laboratory

NASA Astrophysics Data System (ADS)

Baum, David A.; Vetsigian, Kalin

2017-12-01

Most experimental work on the origin of life has focused on either characterizing the chemical synthesis of particular biochemicals and their precursors or on designing simple chemical systems that manifest life-like properties such as self-propagation or adaptive evolution. Here we propose a new class of experiments, analogous to artificial ecosystem selection, where we select for spontaneously forming self-propagating chemical assemblages in the lab and then seek evidence of a response to that selection as a key indicator that life-like chemical systems have arisen. Since surfaces and surface metabolism likely played an important role in the origin of life, a key experimental challenge is to find conditions that foster nucleation and spread of chemical consortia on surfaces. We propose high-throughput screening of a diverse set of conditions in order to identify combinations of "food," energy sources, and mineral surfaces that foster the emergence of surface-associated chemical consortia that are capable of adaptive evolution. Identification of such systems would greatly advance our understanding of the emergence of self-propagating entities and the onset of adaptive evolution during the origin of life.

Pressure variation of developed lapping tool on surface roughness

NASA Astrophysics Data System (ADS)

Hussain, A. K.; Lee, K. Q.; Aung, L. M.; Abu, A.; Tan, L. K.; Kang, H. S.

2018-01-01

Improving the surface roughness is always one of the major concerns in the development of lapping process as high precision machining caters a great demand in manufacturing process. This paper aims to investigate the performance of a newly designed lapping tool in term of surface roughness. Polypropylene is used as the lapping tool head. The lapping tool is tested for different pressure to identify the optimum working pressure for lapping process. The theoretical surface roughness is also calculated using Vickers Hardness. The present study shows that polypropylene is able to produce good quality and smooth surface roughness. The optimum lapping pressure in the present study is found to be 45 MPa. By comparing the theoretical and experimental values, the present study shows that the newly designed lapping tool is capable to produce finer surface roughness.

PHYSICAL MODELING OF CONTRACTED FLOW.

USGS Publications Warehouse

Lee, Jonathan K.

1987-01-01

Experiments on steady flow over uniform grass roughness through centered single-opening contractions were conducted in the Flood Plain Simulation Facility at the U. S. Geological Survey's Gulf Coast Hydroscience Center near Bay St. Louis, Miss. The experimental series was designed to provide data for calibrating and verifying two-dimensional, vertically averaged surface-water flow models used to simulate flow through openings in highway embankments across inundated flood plains. Water-surface elevations, point velocities, and vertical velocity profiles were obtained at selected locations for design discharges ranging from 50 to 210 cfs. Examples of observed water-surface elevations and velocity magnitudes at basin cross-sections are presented.

Interface design for CMOS-integrated Electrochemical Impedance Spectroscopy (EIS) biosensors.

PubMed

Manickam, Arun; Johnson, Christopher Andrew; Kavusi, Sam; Hassibi, Arjang

2012-10-29

Electrochemical Impedance Spectroscopy (EIS) is a powerful electrochemical technique to detect biomolecules. EIS has the potential of carrying out label-free and real-time detection, and in addition, can be easily implemented using electronic integrated circuits (ICs) that are built through standard semiconductor fabrication processes. This paper focuses on the various design and optimization aspects of EIS ICs, particularly the bio-to-semiconductor interface design. We discuss, in detail, considerations such as the choice of the electrode surface in view of IC manufacturing, surface linkers, and development of optimal bio-molecular detection protocols. We also report experimental results, using both macro- and micro-electrodes to demonstrate the design trade-offs and ultimately validate our optimization procedures.

Evaluation of thermal loading on a methane injector at high pressure and temperature

NASA Technical Reports Server (NTRS)

Harvin, Stephen F.

1990-01-01

Experimental and numerical analyses are conducted to determine the surface temperature on a methane fuel injector used to produce a high enthalpy test stream for a combustion-fed subscale wind tunnel facility. It was found that the ratio of the methane fuel injection velocity to the air stream velocity is a significant factor in the production of high injector surface temperatures which lead to rapid deterioration of the fuel injector structure. The numerical code utilized for the computational analysis was found to be representative of the experimentally measured data since the experimental trends were reproduced by the numerical simulation. The quantitative accuracy of the numerical predictions could not be assessed from the data gathered because of the difficulty of making a noninterfering injector surface temperature measurement. The numerical code can be used for parametric evaluation of combustor parameters and thus will serve as an important tool in the design of such fuel injector systems.

Surface Traps in Colloidal Quantum Dots: A Combined Experimental and Theoretical Perspective

PubMed Central

2017-01-01

Surface traps are ubiquitous to nanoscopic semiconductor materials. Understanding their atomistic origin and manipulating them chemically have capital importance to design defect-free colloidal quantum dots and make a leap forward in the development of efficient optoelectronic devices. Recent advances in computing power established computational chemistry as a powerful tool to describe accurately complex chemical species and nowadays it became conceivable to model colloidal quantum dots with realistic sizes and shapes. In this Perspective, we combine the knowledge gathered in recent experimental findings with the computation of quantum dot electronic structures. We analyze three different systems: namely, CdSe, PbS, and CsPbI3 as benchmark semiconductor nanocrystals showing how different types of trap states can form at their surface. In addition, we suggest experimental healing of such traps according to their chemical origin and nanocrystal composition. PMID:28972763

Single actuator wave-like robot (SAW): design, modeling, and experiments.

PubMed

Zarrouk, David; Mann, Moshe; Degani, Nir; Yehuda, Tal; Jarbi, Nissan; Hess, Amotz

2016-07-01

In this paper, we present a single actuator wave-like robot, a novel bioinspired robot which can move forward or backward by producing a continuously advancing wave. The robot has a unique minimalistic mechanical design and produces an advancing sine wave, with a large amplitude, using only a single motor but with no internal straight spine. Over horizontal surfaces, the robot does not slide relative to the surface and its direction of locomotion is determined by the direction of rotation of the motor. We developed a kinematic model of the robot that accounts for the two-dimensional mechanics of motion and yields the speed of the links relative to the motor. Based on the optimization of the kinematic model, and accounting for the mechanical constraints, we have designed and built multiple versions of the robot with different sizes and experimentally tested them (see movie). The experimental results were within a few percentages of the expectations. The larger version attained a top speed of 57 cm s(-1) over a horizontal surface and is capable of climbing vertically when placed between two walls. By optimizing the parameters, we succeeded in making the robot travel by 13% faster than its own wave speed.

Developing an Empirical Model for Jet-Surface Interaction Noise

NASA Technical Reports Server (NTRS)

Brown, Clifford A.

2014-01-01

The process of developing an empirical model for jet-surface interaction noise is described and the resulting model evaluated. Jet-surface interaction noise is generated when the high-speed engine exhaust from modern tightly integrated or conventional high-bypass ratio engine aircraft strikes or flows over the airframe surfaces. An empirical model based on an existing experimental database is developed for use in preliminary design system level studies where computation speed and range of configurations is valued over absolute accuracy to select the most promising (or eliminate the worst) possible designs. The model developed assumes that the jet-surface interaction noise spectra can be separated from the jet mixing noise and described as a parabolic function with three coefficients: peak amplitude, spectral width, and peak frequency. These coefficients are fit to functions of surface length and distance from the jet lipline to form a characteristic spectra which is then adjusted for changes in jet velocity and/or observer angle using scaling laws from published theoretical and experimental work. The resulting model is then evaluated for its ability to reproduce the characteristic spectra and then for reproducing spectra measured at other jet velocities and observer angles; successes and limitations are discussed considering the complexity of the jet-surface interaction noise versus the desire for a model that is simple to implement and quick to execute.

Developing an Empirical Model for Jet-Surface Interaction Noise

NASA Technical Reports Server (NTRS)

Brown, Clif

2014-01-01

The process of developing an empirical model for jet-surface interaction noise is described and the resulting model evaluated. Jet-surface interaction noise is generated when the high-speed engine exhaust from modern tightly integrated or conventional high-bypass ratio engine aircraft strikes or flows over the airframe surfaces. An empirical model based on an existing experimental database is developed for use in preliminary design system level studies where computation speed and range of configurations is valued over absolute accuracy to select the most promising (or eliminate the worst) possible designs. The model developed assumes that the jet-surface interaction noise spectra can be separated from the jet mixing noise and described as a parabolic function with three coefficients: peak amplitude, spectral width, and peak frequency. These coefficients are t to functions of surface length and distance from the jet lipline to form a characteristic spectra which is then adjusted for changes in jet velocity and/or observer angle using scaling laws from published theoretical and experimental work. The resulting model is then evaluated for its ability to reproduce the characteristic spectra and then for reproducing spectra measured at other jet velocities and observer angles; successes and limitations are discussed considering the complexity of the jet-surface interaction noise versus the desire for a model that is simple to implement and quick to execute.

Heat Transfer and Fluid Dynamics Measurements in the Expansion Space of a Stirling Cycle Engine

NASA Technical Reports Server (NTRS)

Jiang, Nan; Simon, Terrence W.

2006-01-01

The heater (or acceptor) of a Stirling engine, where most of the thermal energy is accepted into the engine by heat transfer, is the hottest part of the engine. Almost as hot is the adjacent expansion space of the engine. In the expansion space, the flow is oscillatory, impinging on a two-dimensional concavely-curved surface. Knowing the heat transfer on the inside surface of the engine head is critical to the engine design for efficiency and reliability. However, the flow in this region is not well understood and support is required to develop the CFD codes needed to design modern Stirling engines of high efficiency and power output. The present project is to experimentally investigate the flow and heat transfer in the heater head region. Flow fields and heat transfer coefficients are measured to characterize the oscillatory flow as well as to supply experimental validation for the CFD Stirling engine design codes. Presented also is a discussion of how these results might be used for heater head and acceptor region design calculations.

Micro-channel filling flow considering surface tension effect

NASA Astrophysics Data System (ADS)

Kim, Dong Sung; Lee, Kwang-Cheol; Kwon, Tai Hun; Lee, Seung S.

2002-05-01

Understanding filling flow into micro-channels is important in designing micro-injection molding, micro-fluidic devices and an MIMIC (micromolding in capillaries) process. In this paper, we investigated, both experimentally and numerically, 'transient filling' flow into micro-channels, which differs from steady-state completely 'filled' flow in micro-channels. An experimental flow visualization system was devised to facilitate observation of flow characteristics in filling into micro-channels. Three sets of micro-channels of various widths of different thicknesses (20, 30, and 40 μm) were fabricated using SU-8 on the silicon substrate to find a geometric effect with regard to pressure gradient, viscous force and, in particular, surface tension. A numerical analysis system has also been developed taking into account the surface tension effect with a contact angle concept. Experimental observations indicate that surface tension significantly affects the filling flow to such an extent that even a flow blockage phenomenon was observed at channels of small width and thickness. A numerical analysis system also confirms that the flow blockage phenomenon could take place due to the flow hindrance effect of surface tension, which is consistent with experimental observation. For proper numerical simulations, two correction factors have also been proposed to correct the conventional hydraulic radius for the filling flow in rectangular cross-sectioned channels.

Marine pastures: a by-product of large (100 megawatt or larger) floating ocean thermal power plants. Progress report, February 1, 1975--January 31, 1976

DOE Office of Scientific and Technical Information (OSTI.GOV)

Roels, O.A.; Laurence, S.; Petersen, J.

1976-01-01

Our on-shore experimental area for primary- and secondary-producers was complete 1 November 1975. The system is built around six 2000-liter concrete tanks (''reactors''), to which deep water (from 870 m) is supplied while surface water is pumped from a shallow-water line extending 100 ft north of the beach facility in S. Croix. An experimental rack has been built which is capable of holding 90 separate test populations. Flow into reactors and experimental rack is regulated by constant-head devices. The system design provides flexibility for controlled manipulation and investigation of a wide variety of parameters at various trophic levels. Based onmore » preliminary results of experimentation with continuous culturing of phytoplankton in mixtures of deep and surface water, we can say that a 70:30 (deep/surface) mixture is optimal for producing algal blooms which will sustain rapid growth of Tapes semidecussata in on-shore controlled growth conditions. An open-ocean structure has been designed for growing bivalves, and is anchored off-shore near the intake of the deep-water pipeline. The structure is being tested for stability, durability, and ease of handling. A second design (for non-attaching shellfish) is being built. A modified computer program has been developed to search NODC data tapes containing measurements to within 10 percent of the ocean bottom on a seasonal basis. We have computed parameters, listed and stored seasonal data, and will refine an existing program to plot T' on a Mercator projection map of the region from 17/sup 0/ to 19/sup 0/N; 64/sup 0/ to 66/sup 0/W.« less

Development of a special-purpose test surface guided by uncertainty analysis - Introduction of a new uncertainty analysis step

NASA Technical Reports Server (NTRS)

Wang, T.; Simon, T. W.

1988-01-01

Development of a recent experimental program to investigate the effects of streamwise curvature on boundary layer transition required making a bendable, heated and instrumented test wall, a rather nonconventional surface. The present paper describes this surface, the design choices made in its development and how uncertainty analysis was used, beginning early in the test program, to make such design choices. Published uncertainty analysis techniques were found to be of great value; but, it became clear that another step, one herein called the pre-test analysis, would aid the program development. Finally, it is shown how the uncertainty analysis was used to determine whether the test surface was qualified for service.

Aerodynamic heating and surface temperatures on vehicles for computer-aided design studies

NASA Technical Reports Server (NTRS)

Dejarnette, F. R.; Kania, L. A.; Chitty, A.

1983-01-01

A computer subprogram has been developed to calculate aerodynamic and radiative heating rates and to determine surface temperatures by integrating the heating rates along the trajectory of a vehicle. Convective heating rates are calculated by applying the axisymmetric analogue to inviscid surface streamlines and using relatively simple techniques to calculate laminar, transitional, or turbulent heating rates. Options are provided for the selection of gas model, transition criterion, turbulent heating method, Reynolds Analogy factor, and entropy-layer swallowing effects. Heating rates are compared to experimental data, and the time history of surface temperatures are given for a high-speed trajectory. The computer subprogram is developed for preliminary design and mission analysis where parametric studies are needed at all speeds.

Evaluation and improvement of micro-surfacing mix design method and modelling of asphalt emulsion mastic in terms of filler-emulsion interaction

NASA Astrophysics Data System (ADS)

Robati, Masoud

This Doctorate program focuses on the evaluation and improving the rutting resistance of micro-surfacing mixtures. There are many research problems related to the rutting resistance of micro-surfacing mixtures that still require further research to be solved. The main objective of this Ph.D. program is to experimentally and analytically study and improve rutting resistance of micro-surfacing mixtures. During this Ph.D. program major aspects related to the rutting resistance of micro-surfacing mixtures are investigated and presented as follow: 1) evaluation of a modification of current micro-surfacing mix design procedures: On the basis of this effort, a new mix design procedure is proposed for type III micro-surfacing mixtures as rut-fill materials on the road surface. Unlike the current mix design guidelines and specification, the new mix design is capable of selecting the optimum mix proportions for micro-surfacing mixtures; 2) evaluation of test methods and selection of aggregate grading for type III application of micro-surfacing: Within the term of this study, a new specification for selection of aggregate grading for type III application of micro-surfacing is proposed; 3) evaluation of repeatability and reproducibility of micro-surfacing mixture design tests: In this study, limits for repeatability and reproducibility of micro-surfacing mix design tests are presented; 4) a new conceptual model for filler stiffening effect on asphalt mastic of micro-surfacing: A new model is proposed, which is able to establish limits for minimum and maximum filler concentrations in the micro-surfacing mixture base on only the filler important physical and chemical properties; 5) incorporation of reclaimed asphalt pavement and post-fabrication asphalt shingles in micro-surfacing mixture: The effectiveness of newly developed mix design procedure for micro-surfacing mixtures is further validated using recycled materials. The results present the limits for the use of RAP and RAS amount in micro-surfacing mixtures; 6) new colored micro-surfacing formulations with improved durability and performance: The significant improvement of around 45% in rutting resistance of colored and conventional micro-surfacing mixtures is achieved through employing low penetration grade bitumen polymer modified asphalt emulsion stabilized using nanoparticles.

Experimental Research and Mathematical Modeling of Parameters Effecting on Cutting Force and SurfaceRoughness in CNC Turning Process

NASA Astrophysics Data System (ADS)

Zeqiri, F.; Alkan, M.; Kaya, B.; Toros, S.

2018-01-01

In this paper, the effects of cutting parameters on cutting forces and surface roughness based on Taguchi experimental design method are determined. Taguchi L9 orthogonal array is used to investigate the effects of machining parameters. Optimal cutting conditions are determined using the signal/noise (S/N) ratio which is calculated by average surface roughness and cutting force. Using results of analysis, effects of parameters on both average surface roughness and cutting forces are calculated on Minitab 17 using ANOVA method. The material that was investigated is Inconel 625 steel for two cases with heat treatment and without heat treatment. The predicted and calculated values with measurement are very close to each other. Confirmation test of results showed that the Taguchi method was very successful in the optimization of machining parameters for maximum surface roughness and cutting forces in the CNC turning process.

Design and Control of Functional Microbubbles for Medical Applications of Ultrasound

NASA Astrophysics Data System (ADS)

Takagi, Shu; Osaki, Taichi; Ariyoshi, Takuya; Azuma, Takashi; Ichiyanagi, Mitsuhisa; Kinefuchi, Ikuya

2015-11-01

Microbubbles are used as a contrast agent for ultrasound diagnosis. It is also expected to be use for the treatment. One of the possible applications is microbubble DDS. For that purpose, microbubbles need to be well-controlled for the generating process and manipulation. In this talk, for the design and control of the functional microbubbles, an experimental study on generation and surface modification of microbubbles are explained. Using a T-junction type microchannel, small bubbles about 5 μm size are successfully generated. For the surface modification, Biotin-coated microbubbles are tried to adhere the Avidin-coated wall. Furthermore, the manipulation of the microbubbles using ultrasound is also discussed. Plane-wave and focused ultrasound is used to manipulate a microbubble and bubble clusters. The experimental results are shown in the presentation. Supported by JSPS KAKENHI Grant Number 15K13865.

Experimental Design for a Macrofoam Swab Study Relating the Recovery Efficiency and False Negative Rate to Low Concentrations of Two Bacillus anthracis Surrogates on Four Surface Materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Piepel, Gregory F.; Hutchison, Janine R.

2014-04-16

This report describes the experimental design for a laboratory study to quantify the recovery efficiencies and false negative rates of a validated, macrofoam swab sampling method for low concentrations of Bacillus anthracis Sterne (BAS) and Bacillus atrophaeus (BG) spores on four surface materials (stainless steel, glass, vinyl tile, plastic light cover panel). Two analytical methods (plating/counting and polymerase chain reaction) will be used. Only one previous study has investigated false negative as a function of affecting test factors. The surrogates BAS and BG have not been tested together in the same study previously. Hence, this study will provide for completingmore » gaps in the available information on the performance of macrofoam swab sampling at low concentrations.« less

Experimental Design for a Macrofoam-Swab Study Relating the Recovery Efficiency and False Negative Rate to Low Concentrations of Two Bacillus anthracis Surrogates on Four Surface Materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Piepel, Gregory F.; Hutchison, Janine R.

This report describes the experimental design for a laboratory study to quantify the recovery efficiencies and false negative rates of a validated, macrofoam-swab sampling method for low concentrations of Bacillus anthracis Sterne (BAS) and Bacillus atrophaeus (BG) spores on four surface materials (stainless steel, glass, vinyl tile, plastic light cover panel). Two analytical methods (culture and polymerase chain reaction) will be used. Only one previous study has investigated how the false negative rate depends on test factors. The surrogates BAS and BG have not been tested together in the same study previously. Hence, this study will provide for completing gapsmore » in the available information on the performance of macrofoam-swab sampling at low concentrations.« less

Additive manufacturing and mechanical characterization of graded porosity scaffolds designed based on triply periodic minimal surface architectures.

PubMed

Afshar, M; Anaraki, A Pourkamali; Montazerian, H; Kadkhodapour, J

2016-09-01

Since the advent of additive manufacturing techniques, triply periodic minimal surfaces have emerged as a novel tool for designing porous scaffolds. Whereas scaffolds are expected to provide multifunctional performance, spatially changing pore patterns have been a promising approach to integrate mechanical characteristics of different architectures into a unique scaffold. Smooth morphological variations are also frequently seen in nature particularly in bone and cartilage structures and can be inspiring for designing of artificial tissues. In this study, we carried out experimental and numerical procedures to uncover the mechanical properties and deformation mechanisms of linearly graded porosity scaffolds for two different mathematically defined pore structures. Among TPMS-based scaffolds, P and D surfaces were subjected to gradient modeling to explore the mechanical responses for stretching and bending dominated deformations, respectively. Moreover, the results were compared to their corresponding uniform porosity structures. Mechanical properties were found to be by far greater for the stretching dominated structure (P-Surface). For bending dominated architecture (D-Surface), although there was no global fracture for uniform structures, graded structure showed a brittle fracture at 0.08 strain. A layer by layer deformation mechanism for stretching dominated structure was observed. For bending dominated scaffolds, deformation was accompanied by development of 45° shearing bands. Finite element simulations were also performed and the results showed a good agreement with the experimental observations. Copyright © 2016 Elsevier Ltd. All rights reserved.

[Optimization of ultrasonic-assisted extraction of total flavonoids from leaves of the Artocarpus heterophyllus by response surface methodology].

PubMed

Wang, Hong-wu; Liu, Yan-qing; Wang, Yuan-hong

2011-07-01

To investigate the ultrasonic-assisted extract on of total flavonoids from leaves of the Artocarpus heterophyllus. Investigated the effects of ethanol concentration, extraction time, and liquid-solid ratio on flavonoids yield. A 17-run response surface design involving three factors at three levels was generated by the Design-Expert software and experimental data obtained were subjected to quadratic regression analysis to create a mathematical model describing flavonoids extraction. The optimum ultrasonic assisted extraction conditions were: ethanol volume fraction 69.4% and liquid-solid ratio of 22.6:1 for 32 min. Under these optimized conditions, the yield of flavonoids was 7.55 mg/g. The Box-Behnken design and response surface analysis can well optimize the ultrasonic-assisted extraction of total flavonoids from Artocarpus heterophyllus.

An experimental study of a three-dimensional shock wave/turbulent boundary-layer interaction at a hypersonic Mach number

NASA Technical Reports Server (NTRS)

Kussoy, M. I.; Horstman, K. C.; Kim, K.-S.

1991-01-01

Experimental data for a series of three-dimensional shock-wave/turbulent-boundary-layer interaction flows at Mach 8.2 are presented. The test bodies, composed of sharp fins fastened to a flat-plate test surface, were designed to generate flows with varying degrees of pressure gradient, boundary-layer separation, and turning angle. The data include surface-pressure, heat-transfer, and skin-friction distributions, as well as limited mean flowfield surveys both in the undisturbed and interaction regimes. The data were obtained for the purpose of validating computational models of these hypersonic interactions.

Compact Heat Exchanger Design and Testing for Advanced Reactors and Advanced Power Cycles

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sun, Xiaodong; Zhang, Xiaoqin; Christensen, Richard

The goal of the proposed research is to demonstrate the thermal hydraulic performance of innovative surface geometries in compact heat exchangers used as intermediate heat exchangers (IHXs) and recuperators for the supercritical carbon dioxide (s-CO 2) Brayton cycle. Printed-circuit heat exchangers (PCHEs) are the primary compact heat exchangers of interest. The overall objectives are: To develop optimized PCHE designs for different working fluid combinations including helium to s-CO 2, liquid salt to s-CO 2, sodium to s-CO 2, and liquid salt to helium; To experimentally and numerically investigate thermal performance, thermal stress and failure mechanism of PCHEs under various transients;more » and To study diffusion bonding techniques for elevated-temperature alloys and examine post-test material integrity of the PCHEs. The project objectives were accomplished by defining and executing five different tasks corresponding to these specific objectives. The first task involved a thorough literature review and a selection of IHX candidates with different surface geometries as well as a summary of prototypic operational conditions. The second task involved optimization of PCHE design with numerical analyses of thermal-hydraulic performances and mechanical integrity. The subsequent task dealt with the development of testing facilities and engineering design of PCHE to be tested in s-CO 2 fluid conditions. The next task involved experimental investigation and validation of the thermal-hydraulic performances and thermal stress distribution of prototype PCHEs manufactured with particular surface geometries. The last task involved an investigation of diffusion bonding process and posttest destructive testing to validate mechanical design methods adopted in the design process. The experimental work utilized the two test facilities at The Ohio State University (OSU) including one existing High-Temperature Helium Test Facility (HTHF) and the newly developed s-CO 2 test loop (STL) facility and s-CO 2 test facility at University of Wisconsin – Madison (UW).« less

Backscattered EM-wave manipulation using low cost 1-bit reflective surface at W-band

NASA Astrophysics Data System (ADS)

Taher Al-Nuaimi, Mustafa K.; Hong, Wei; He, Yejun

2018-04-01

The design of low cost 1-bit reflective (non-absorptive) surfaces for manipulation of backscattered EM-waves and radar cross section (RCS) reduction at W-band is presented in this article. The presented surface is designed based on the reflection phase cancellation principle. The unit cell used to compose the proposed surface has an obelus (division symbol of short wire and two disks above and below) like shape printed on a grounded dielectric material. Using this unit cell, surfaces that can efficiently manipulate the backscattered RCS pattern by using the proposed obelus-shaped unit cell (as ‘0’ element) and its mirrored unit cell (as ‘1’ element) in one surface with a 180°  ±  35° reflection phase difference between their reflection phases are designed. The proposed surfaces can generate various kinds of backscattered RCS patterns, such as single, three, or four lobes or even a low-level (reduced RCS) diffused reflection pattern when those two unit cells are distributed randomly across the surface aperture. For experimental characterization purposes, a 50  ×  50 mm2 surface is fabricated and measured.

Does the S.D.E.P. increase performance?

NASA Astrophysics Data System (ADS)

Syltebo, Andy

2003-05-01

Through the guidance of the program, "Physical Systems," at The Evergreen State College in Olympia Washington, Andy Syltebo will be investigating how the Surface Drive Enhancement Project will affect the performance of a planing hull powered by surface drive propulsion. A radio controlled model boat of the forementioned design is the prototype vehicle used for experimentation and analysis. The idea of this project revolves around harnessing the energy in the water of a rooster tail ejected from the wake of a surface drive propeller of a boat with a planing hull design. The Surface Drive Enhancement Project (S.D.E.P. for short) is an angled set of adjustable platforms placed in the path of the rooster tail. Theoretically, it experiences the normal force of the water on its surface which, through conservation of momentum, distributes a force on the boat, with which the S.D.E.P. is attached, in both the upwards and forwards directions. This design will be tested and documented to see if it increases forward velocity without sacrificing handling characteristics.

An automated high throughput tribometer for adhesion, wear, and friction measurements

NASA Astrophysics Data System (ADS)

Kalihari, Vivek; Timpe, Shannon J.; McCarty, Lyle; Ninke, Matthew; Whitehead, Jim

2013-03-01

Understanding the origin and correlation of different surface properties under a multitude of operating conditions is critical in tribology. Diverse tribological properties and a lack of a single instrument to measure all make it difficult to compare and correlate properties, particularly in light of the wide range of interfaces commonly investigated. In the current work, a novel automated tribometer has been designed and validated, providing a unique experimental platform capable of high throughput adhesion, wear, kinetic friction, and static friction measurements. The innovative design aspects are discussed that allow for a variety of probes, sample surfaces, and testing conditions. Critical components of the instrument and their design criteria are described along with examples of data collection schemes. A case study is presented with multiple surface measurements performed on a set of characteristic substrates. Adhesion, wear, kinetic friction, and static friction are analyzed and compared across surfaces, highlighting the comprehensive nature of the surface data that can be generated using the automated high throughput tribometer.

[Optimization of one-step pelletization technology of Biqiu granules by Plackett-Burman design and Box-Behnken response surface methodology].

PubMed

Zhang, Yan-jun; Liu, Li-li; Hu, Jun-hua; Wu, Yun; Chao, En-xiang; Xiao, Wei

2015-11-01

First with the qualified rate of granules as the evaluation index, significant influencing factors were firstly screened by Plackett-Burman design. Then, with the qualified rate and moisture content as the evaluation indexes, significant factors that affect one-step pelletization technology were further optimized by Box-Behnken design; experimental data were imitated by multiple regression and second-order polynomial equation; and response surface method was used for predictive analysis of optimal technology. The best conditions were as follows: inlet air temperature of 85 degrees C, sample introduction speed of 33 r x min(-1), density of concrete 1. 10. One-step pelletization technology of Biqiu granules by Plackett-Burman design and Box-Behnken response surface methodology was stable and feasible with good predictability, which provided reliable basis for the industrialized production of Biqiu granules.

Heat Transfer and Flow on the First Stage Blade Tip of a Power Generation Gas Turbine. Part 1; Experimental Results

NASA Technical Reports Server (NTRS)

Bunker, Ronald S.; Bailey, Jeremy C.; Ameri, Ali A.

1999-01-01

A combined computational and experimental study has been performed to investigate the detailed distribution of convective heat transfer coefficients on the first stage blade tip surface for a geometry typical of large power generation turbines(>100MW). This paper is concerned with the design and execution of the experimental portion of the study. A stationary blade cascade experiment has been run consisting of three airfoils, the center airfoil having a variable tip gap clearance. The airfoil models the aerodynamic tip section of a high pressure turbine blade with inlet Mach number of 0.30, exit Mach number of 0.75, pressure ratio of 1.45, exit Reynolds number based on axial chord of 2.57 x 10(exp 6), and total turning of about 110 degrees. A hue detection based liquid crystal method is used to obtain the detailed heat transfer coefficient distribution on the blade tip surface for flat, smooth tip surfaces with both sharp and rounded edges. The cascade inlet turbulence intensity level took on values of either 5% or 9%. The cascade also models the casing recess in the shroud surface ahead of the blade. Experimental results are shown for the pressure distribution measurements on the airfoil near the tip gap, on the blade tip surface, and on the opposite shroud surface. Tip surface heat transfer coefficient distributions are shown for sharp-edge and rounded-edge tip geometries at each of the inlet turbulence intensity levels.

[An experimental research on the fabrication of the fused porcelain to CAD/CAM molar crown].

PubMed

Dai, Ning; Zhou, Yongyao; Liao, Wenhe; Yu, Qing; An, Tao; Jiao, Yiqun

2007-02-01

This paper introduced the fabrication process of the fused porcelain to molar crown with CAD/CAM technology. Firstly, preparation teeth data was retrieved by the 3D-optical measuring system. Then, we have reconstructed the inner surface designed the outer surface shape with the computer aided design software. Finally, the mini high-speed NC milling machine was used to produce the fused porcelain to CAD/CAM molar crown. The result has proved that the fabrication process is reliable and efficient. The dental restoration quality is steady and precise.

Simulation in production of open rotor propellers: from optimal surface geometry to automated control of mechanical treatment

NASA Astrophysics Data System (ADS)

Grinyok, A.; Boychuk, I.; Perelygin, D.; Dantsevich, I.

2018-03-01

A complex method of the simulation and production design of open rotor propellers was studied. An end-to-end diagram was proposed for the evaluating, designing and experimental testing the optimal geometry of the propeller surface, for the machine control path generation as well as for simulating the cutting zone force condition and its relationship with the treatment accuracy which was defined by the propeller elastic deformation. The simulation data provided the realization of the combined automated path control of the cutting tool.

Design of a CO2 laser power control system for a Spacelab microgravity experiment

NASA Technical Reports Server (NTRS)

Wenzler, Carl J.; Eichenberg, Dennis J.

1990-01-01

The surface tension driven convection experiment (STDCE) is a Space Transportation System flight experiment manifested to fly aboard the USML-1 Spacelab mission. A CO2 laser is used to heat a spot on the surface of silicone oil contained inside a test chamber. Several CO2 laser control systems were evaluated and the selected system will be interfaced with the balance of the experimental hardware to constitute a working engineering model. Descriptions and a discussion of these various design approaches are presented.

Parametric design and analysis on the landing gear of a planet lander using the response surface method

NASA Astrophysics Data System (ADS)

Zheng, Guang; Nie, Hong; Luo, Min; Chen, Jinbao; Man, Jianfeng; Chen, Chuanzhi; Lee, Heow Pueh

2018-07-01

The purpose of this paper is to obtain the design parameter-landing response relation for designing the configuration of the landing gear in a planet lander quickly. To achieve this, parametric studies on the landing gear are carried out using the response surface method (RSM), based on a single landing gear landing model validated by experimental results. According to the design of experiment (DOE) results of the landing model, the RS (response surface)-functions of the three crucial landing responses are obtained, and the sensitivity analysis (SA) of the corresponding parameters is performed. Also, two multi-objective optimizations designs on the landing gear are carried out. The analysis results show that the RS (response surface)-model performs well for the landing response design process, with a minimum fitting accuracy of 98.99%. The most sensitive parameters for the three landing response are the design size of the buffers, struts friction and the diameter of the bending beam. Moreover, the good agreement between the simulated model and RS-model results are obtained in two optimized designs, which show that the RS-model coupled with the FE (finite element)-method is an efficient method to obtain the design configuration of the landing gear.

Jet-Surface Interaction Test: Flow Measurements Results

NASA Technical Reports Server (NTRS)

Brown, Cliff; Wernet, Mark

2014-01-01

Modern aircraft design often puts the engine exhaust in close proximity to the airframe surfaces. Aircraft noise prediction tools must continue to develop in order to meet the challenges these aircraft present. The Jet-Surface Interaction Tests have been conducted to provide a comprehensive quality set of experimental data suitable for development and validation of these exhaust noise prediction methods. Flow measurements have been acquired using streamwise and cross-stream particle image velocimetry (PIV) and fluctuating surface pressure data acquired using flush mounted pressure transducers near the surface trailing edge. These data combined with previously reported far-field and phased array noise measurements represent the first step toward the experimental data base. These flow data are particularly applicable to development of noise prediction methods which rely on computational fluid dynamics to uncover the flow physics. A representative sample of the large flow data set acquired is presented here to show how a surface near a jet affects the turbulent kinetic energy in the plume, the spatial relationship between the jet plume and surface needed to generate surface trailing-edge noise, and differences between heated and unheated jet flows with respect to surfaces.

Compact antenna for efficient and unidirectional launching and decoupling of surface plasmons.

PubMed

Baron, Alexandre; Devaux, Eloïse; Rodier, Jean-Claude; Hugonin, Jean-Paul; Rousseau, Emmanuel; Genet, Cyriaque; Ebbesen, Thomas W; Lalanne, Philippe

2011-10-12

Controlling the launching efficiencies and the directionality of surface plasmon polaritons (SPPs) and their decoupling to freely propagating light is a major goal for the development of plasmonic devices and systems. Here, we report on the design and experimental observation of a highly efficient unidirectional surface plasmon launcher composed of eleven subwavelength grooves, each with a distinct depth and width. Our observations show that, under normal illumination by a focused Gaussian beam, unidirectional SPP launching with an efficiency of at least 52% is achieved experimentally with a compact device of total length smaller than 8 μm. Reciprocally, we report that the same device can efficiently convert SPPs into a highly directive light beam emanating perpendicularly to the sample.

Optimization of process parameters in CNC turning of aluminium alloy using hybrid RSM cum TLBO approach

NASA Astrophysics Data System (ADS)

Rudrapati, R.; Sahoo, P.; Bandyopadhyay, A.

2016-09-01

The main aim of the present work is to analyse the significance of turning parameters on surface roughness in computer numerically controlled (CNC) turning operation while machining of aluminium alloy material. Spindle speed, feed rate and depth of cut have been considered as machining parameters. Experimental runs have been conducted as per Box-Behnken design method. After experimentation, surface roughness is measured by using stylus profile meter. Factor effects have been studied through analysis of variance. Mathematical modelling has been done by response surface methodology, to made relationships between the input parameters and output response. Finally, process optimization has been made by teaching learning based optimization (TLBO) algorithm. Predicted turning condition has been validated through confirmatory experiment.

Rocket Engine Turbine Blade Surface Pressure Distributions Experiment and Computations

NASA Technical Reports Server (NTRS)

Hudson, Susan T.; Zoladz, Thomas F.; Dorney, Daniel J.; Turner, James (Technical Monitor)

2002-01-01

Understanding the unsteady aspects of turbine rotor flow fields is critical to successful future turbine designs. A technology program was conducted at NASA's Marshall Space Flight Center to increase the understanding of unsteady environments for rocket engine turbines. The experimental program involved instrumenting turbine rotor blades with miniature surface mounted high frequency response pressure transducers. The turbine model was then tested to measure the unsteady pressures on the rotor blades. The data obtained from the experimental program is unique in two respects. First, much more unsteady data was obtained (several minutes per set point) than has been possible in the past. Also, an extensive steady performance database existed for the turbine model. This allowed an evaluation of the effect of the on-blade instrumentation on the turbine's performance. A three-dimensional unsteady Navier-Stokes analysis was also used to blindly predict the unsteady flow field in the turbine at the design operating conditions and at +15 degrees relative incidence to the first-stage rotor. The predicted time-averaged and unsteady pressure distributions show good agreement with the experimental data. This unique data set, the lessons learned for acquiring this type of data, and the improvements made to the data analysis and prediction tools are contributing significantly to current Space Launch Initiative turbine airflow test and blade surface pressure prediction efforts.

A new experimental design method to optimize formulations focusing on a lubricant for hydrophilic matrix tablets.

PubMed

Choi, Du Hyung; Shin, Sangmun; Khoa Viet Truong, Nguyen; Jeong, Seong Hoon

2012-09-01

A robust experimental design method was developed with the well-established response surface methodology and time series modeling to facilitate the formulation development process with magnesium stearate incorporated into hydrophilic matrix tablets. Two directional analyses and a time-oriented model were utilized to optimize the experimental responses. Evaluations of tablet gelation and drug release were conducted with two factors x₁ and x₂: one was a formulation factor (the amount of magnesium stearate) and the other was a processing factor (mixing time), respectively. Moreover, different batch sizes (100 and 500 tablet batches) were also evaluated to investigate an effect of batch size. The selected input control factors were arranged in a mixture simplex lattice design with 13 experimental runs. The obtained optimal settings of magnesium stearate for gelation were 0.46 g, 2.76 min (mixing time) for a 100 tablet batch and 1.54 g, 6.51 min for a 500 tablet batch. The optimal settings for drug release were 0.33 g, 7.99 min for a 100 tablet batch and 1.54 g, 6.51 min for a 500 tablet batch. The exact ratio and mixing time of magnesium stearate could be formulated according to the resulting hydrophilic matrix tablet properties. The newly designed experimental method provided very useful information for characterizing significant factors and hence to obtain optimum formulations allowing for a systematic and reliable experimental design method.

Experimental design data for the biosynthesis of citric acid using Central Composite Design method.

PubMed

Kola, Anand Kishore; Mekala, Mallaiah; Goli, Venkat Reddy

2017-06-01

In the present investigation, we report that statistical design and optimization of significant variables for the microbial production of citric acid from sucrose in presence of filamentous fungi A. niger NCIM 705. Various combinations of experiments were designed with Central Composite Design (CCD) of Response Surface Methodology (RSM) for the production of citric acid as a function of six variables. The variables are; initial sucrose concentration, initial pH of medium, fermentation temperature, incubation time, stirrer rotational speed, and oxygen flow rate. From experimental data, a statistical model for this process has been developed. The optimum conditions reported in the present article are initial concentration of sucrose of 163.6 g/L, initial pH of medium 5.26, stirrer rotational speed of 247.78 rpm, incubation time of 8.18 days, fermentation temperature of 30.06 °C and flow rate of oxygen of 1.35 lpm. Under optimum conditions the predicted maximum citric acid is 86.42 g/L. The experimental validation carried out under the optimal values and reported citric acid to be 82.0 g/L. The model is able to represent the experimental data and the agreement between the model and experimental data is good.

The Sea of Simulation: Improving Naval Shiphandling Training and Readiness through Game-Based Learning

DTIC Science & Technology

2012-03-01

Officer SWOI Surface Warfare Officer Introduction SWOS Surface Warfare Officers School xvii TFT Thin Film Transistor ULTRA Unit Level Training...designed the experiment , including participants, procedures, facilities selection, and materials. Chapter IV: Results and Discussion. This chapter...contains the results of experimentation and an interpretation of those results . Chapter V: Conclusions. This chapter provides an overall assessment

EXPERIMENTAL EVALUATION OF THE THERMAL PERFORMANCE OF A WATER SHIELD FOR A SURFACE POWER REACTOR

DOE Office of Scientific and Technical Information (OSTI.GOV)

REID, ROBERT S.; PEARSON, J. BOSIE; STEWART, ERIC T.

2007-01-16

Water based reactor shielding is being investigated for use on initial lunar surface power systems. A water shield may lower overall cost (as compared to development cost for other materials) and simplify operations in the setup and handling. The thermal hydraulic performance of the shield is of significant interest. The mechanism for transferring heat through the shield is natural convection. Natural convection in a 100 kWt lunar surface reactor shield design is evaluated with 2 kW power input to the water in the Water Shield Testbed (WST) at the NASA Marshall Space Flight Center. The experimental data from the WSTmore » is used to validate a CFD model. Performance of the water shield on the lunar surface is then predicted with a CFD model anchored to test data. The experiment had a maximum water temperature of 75 C. The CFD model with 1/6-g predicts a maximum water temperature of 88 C with the same heat load and external boundary conditions. This difference in maximum temperature does not greatly affect the structural design of the shield, and demonstrates that it may be possible to use water for a lunar reactor shield.« less

Tile-based rigidization surface parametric design study

NASA Astrophysics Data System (ADS)

Giner Munoz, Laura; Luntz, Jonathan; Brei, Diann; Kim, Wonhee

2018-03-01

Inflatable technologies have proven useful in consumer goods as well as in more recent applications including civil structures, aerospace, medical, and robotics. However, inflatable technologies are typically lacking in their ability to provide rigid structural support. Particle jamming improves upon this by providing structures which are normally flexible and moldable but become rigid when air is removed. Because these are based on an airtight bladder filled with loose particles, they always occupy the full volume of its rigid state, even when not rigidized. More recent developments in layer jamming have created thin, compact rigidizing surfaces replacing the loose volume of particles with thinly layered surface materials. Work in this area has been applied to several specific applications with positive results but have not generally provided the broader understanding of the rigidization performance as a function of design parameters required for directly adapting layer rigidization technology to other applications. This paper presents a parametric design study of a new layer jamming vacuum rigidization architecture: tile-based vacuum rigidization. This form of rigidization is based on layers of tiles contained within a thin vacuum bladder which can be bent, rolled, or otherwise compactly stowed, but when deployed flat, can be vacuumed and form a large, flat, rigid plate capable of supporting large forces both localized and distributed over the surface. The general architecture and operation detailing rigidization and compliance mechanisms is introduced. To quantitatively characterize the rigidization behavior, prototypes rigidization surfaces are fabricated and an experimental technique is developed based on a 3-point bending test. Performance evaluation metrics are developed to describe the stiffness, load-bearing capacity, and internal slippage of tested prototypes. A set of experimental parametric studies are performed to better understand the impact of variations in geometric design parameters, operating parameters, and architectural variations on the performance evaluation metrics. The results of this study bring insight into the rigidization behavior of this architecture, and provide design guidelines and expose tradeoffs to form the basis for the design of tile-based rigidization surfaces for a wide range of applications.

Experimental Investigations on the Surface-Driven Capillary Flow of Aqueous Microparticle Suspensions in the Microfluidic Laboratory-On Systems

NASA Astrophysics Data System (ADS)

Mukhopadhyay, Subhadeep

In this work, total 1592 individual leakage-free polymethylmethacrylate (PMMA) microfluidic devices as laboratory-on-a-chip systems are fabricated by maskless lithography, hot embossing lithography, and direct bonding technique. Total 1094 individual Audio Video Interleave Files as experimental outputs related to the surface-driven capillary flow have been recorded and analyzed. The influence of effective viscosity, effect of surface wettability, effect of channel aspect ratio, and effect of centrifugal force on the surface-driven microfluidic flow of aqueous microparticle suspensions have been successfully and individually investigated in these laboratory-on-a-chip systems. Also, 5 micron polystyrene particles have been separated from the aqueous microparticle suspensions in the microfluidic lab-on-a-chip systems of modified design with 98% separation efficiency, and 10 micron polystyrene particles have been separated with 100% separation efficiency. About the novelty of this work, the experimental investigations have been performed on the surface-driven microfluidic flow of aqueous microparticle suspensions with the investigations on the separation time in particle-size based separation mechanism to control these suspensions in the microfluidic lab-on-a-chip systems. This research work contains a total of 10,112 individual experimental outputs obtained using total 30 individual instruments by author’s own hands-on completely during more than three years continuously. Author has performed the experimental investigations on both the fluid statics and fluid dynamics to develop an automated fluid machine.

Water adsorption on surface-modified cellulose nanocrystals

NASA Astrophysics Data System (ADS)

Wei, Zonghui; Sinko, Robert; Keten, Sinan; Luijten, Erik

Cellulose nanocrystals (CNCs) have attracted much attention as a filler phase for polymer nanocomposites due to their impressive mechanical properties, low cost, and environmental sustainability. Despite their promise for this application, there are still numerous obstacles that prevent optimal performance of CNC-polymer nanocomposites, such as poor filler dispersion and high levels of water absorption. One way to mitigate these negative effects is to modify CNC surfaces. Computational approaches can be utilized to obtain direct insight into the properties of modified CNC surfaces and probe the interactions of CNCs with other materials to facilitate the experimental design of nanocomposites. We use atomistic grand-canonical Monte Carlo simulations to study how surface modification of ion-exchanged sulfated cellulose nanocrystals (Na-CNCs) impacts water adsorption. We find that methyl(triphenyl)phosphonium-exchanged CNCs adsorb less water than Na-CNCs at the same relative humidity, supporting recent experimental dynamic vapor sorption measurements. By characterizing the distribution and configuration of water molecules near the modified CNC surfaces we determine how surface modifications disrupt CNC-water interactions.

Experimental Investigation of Turbine Vane Heat Transfer for Alternative Fuels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nix, Andrew Carl

The focus of this program was to experimentally investigate advanced gas turbine cooling schemes and the effects of and factors that contribute to surface deposition from particulate matter found in coal syngas exhaust flows on turbine airfoil heat transfer and film cooling, as well as to characterize surface roughness and determine the effects of surface deposition on turbine components. The program was a comprehensive, multi-disciplinary collaborative effort between aero-thermal and materials faculty researchers and the Department of Energy, National Energy Technology Laboratory (NETL). The primary technical objectives of the program were to evaluate the effects of combustion of syngas fuelsmore » on heat transfer to turbine vanes and blades in land-based power generation gas turbine engines. The primary questions to be answered by this investigation were; What are the factors that contribute to particulate deposition on film cooled gas turbine components? An experimental program was performed in a high-temperature and pressure combustion rig at the DOE NETL; What is the effect of coal syngas combustion and surface deposition on turbine airfoil film cooling? Deposition of particulate matter from the combustion gases can block film cooling holes, decreasing the flow of the film coolant and the film cooling effectiveness; How does surface deposition from coal syngas combustion affect turbine surface roughness? Increased surface roughness can increase aerodynamic losses and result in decreased turbine hot section efficiency, increasing engine fuel consumption to maintain desired power output. Convective heat transfer is also greatly affected by the surface roughness of the airfoil surface; Is there any significant effect of surface deposition or erosion on integrity of turbine airfoil thermal barrier coatings (TBC) and do surface deposits react with the TBC in any way to decrease its thermal insulating capability? Spallation and erosion of TBC is a persistent problem in modern turbine engines; and What advancements in film cooling hole geometry and design can increase effectiveness of film cooling in turbines burning high-hydrogen coal syngas due to the higher heat loads and mass flow rates of the core flow? Experimental and numerical investigations of advanced cooling geometries that can improve resistance to surface deposition were performed. The answers to these questions were investigated through experimental measurements of turbine blade surface temperature and coolant coverage (via infrared camera images and thermocouples) and time-varying surface roughness in the NETL high-pressure combustion rig with accelerated, simulated surface deposition and advanced cooling hole concepts, coupled with detailed materials analysis and characterization using conventional methods of Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), X-Ray Diffraction (XRD), 3-D Surface Topography (using a 3-D stylus profilometer). Detailed surface temperatures and cooling effectiveness could not be measured due to issues with the NETL infrared camera system. In collaboration with faculty startup funding from the principal investigator, experimental and numerical investigations were performed of an advanced film cooling hole geometry, the anti-vortex hole (AVH), focusing on improving cooling effectiveness and decreasing the counter-rotating vortex of conventional cooling holes which can entrain mainstream particulate matter to the surface. The potential benefit of this program is in gaining a fundamental understanding of how the use of alternative fuels will effect the operation of modern gas turbine engines, providing valuable data for more effective cooling designs for future turbine systems utilizing alternative fuels.« less

Surface Roughness and Morphology Customization of Additive Manufactured Open Porous Ti6Al4V Structures

PubMed Central

Pyka, Grzegorz; Kerckhofs, Greet; Papantoniou, Ioannis; Speirs, Mathew; Schrooten, Jan; Wevers, Martine

2013-01-01

Additive manufacturing (AM) is a production method that enables the building of porous structures with a controlled geometry. However, there is a limited control over the final surface of the product. Hence, complementary surface engineering strategies are needed. In this work, design of experiments (DoE) was used to customize post AM surface treatment for 3D selective laser melted Ti6Al4V open porous structures for bone tissue engineering. A two-level three-factor full factorial design was employed to assess the individual and interactive effects of the surface treatment duration and the concentration of the chemical etching solution on the final surface roughness and beam thickness of the treated porous structures. It was observed that the concentration of the surface treatment solution was the most important factor influencing roughness reduction. The designed beam thickness decreased the effectiveness of the surface treatment. In this case study, the optimized processing conditions for AM production and the post-AM surface treatment were defined based on the DoE output and were validated experimentally. This allowed the production of customized 3D porous structures with controlled surface roughness and overall morphological properties, which can assist in more controlled evaluation of the effect of surface roughness on various functional properties. PMID:28788357

Surface Roughness and Morphology Customization of Additive Manufactured Open Porous Ti6Al4V Structures.

PubMed

Pyka, Grzegorz; Kerckhofs, Greet; Papantoniou, Ioannis; Speirs, Mathew; Schrooten, Jan; Wevers, Martine

2013-10-22

Additive manufacturing (AM) is a production method that enables the building of porous structures with a controlled geometry. However, there is a limited control over the final surface of the product. Hence, complementary surface engineering strategies are needed. In this work, design of experiments (DoE) was used to customize post AM surface treatment for 3D selective laser melted Ti6Al4V open porous structures for bone tissue engineering. A two-level three-factor full factorial design was employed to assess the individual and interactive effects of the surface treatment duration and the concentration of the chemical etching solution on the final surface roughness and beam thickness of the treated porous structures. It was observed that the concentration of the surface treatment solution was the most important factor influencing roughness reduction. The designed beam thickness decreased the effectiveness of the surface treatment. In this case study, the optimized processing conditions for AM production and the post-AM surface treatment were defined based on the DoE output and were validated experimentally. This allowed the production of customized 3D porous structures with controlled surface roughness and overall morphological properties, which can assist in more controlled evaluation of the effect of surface roughness on various functional properties.

A FRAMEWORK TO DESIGN AND OPTIMIZE CHEMICAL FLOODING PROCESSES

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mojdeh Delshad; Gary A. Pope; Kamy Sepehrnoori

2005-07-01

The goal of this proposed research is to provide an efficient and user friendly simulation framework for screening and optimizing chemical/microbial enhanced oil recovery processes. The framework will include (1) a user friendly interface to identify the variables that have the most impact on oil recovery using the concept of experimental design and response surface maps, (2) UTCHEM reservoir simulator to perform the numerical simulations, and (3) an economic model that automatically imports the simulation production data to evaluate the profitability of a particular design. Such a reservoir simulation framework is not currently available to the oil industry. The objectivesmore » of Task 1 are to develop three primary modules representing reservoir, chemical, and well data. The modules will be interfaced with an already available experimental design model. The objective of the Task 2 is to incorporate UTCHEM reservoir simulator and the modules with the strategic variables and developing the response surface maps to identify the significant variables from each module. The objective of the Task 3 is to develop the economic model designed specifically for the chemical processes targeted in this proposal and interface the economic model with UTCHEM production output. Task 4 is on the validation of the framework and performing simulations of oil reservoirs to screen, design and optimize the chemical processes.« less

A Framework to Design and Optimize Chemical Flooding Processes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mojdeh Delshad; Gary A. Pope; Kamy Sepehrnoori

2006-08-31

The goal of this proposed research is to provide an efficient and user friendly simulation framework for screening and optimizing chemical/microbial enhanced oil recovery processes. The framework will include (1) a user friendly interface to identify the variables that have the most impact on oil recovery using the concept of experimental design and response surface maps, (2) UTCHEM reservoir simulator to perform the numerical simulations, and (3) an economic model that automatically imports the simulation production data to evaluate the profitability of a particular design. Such a reservoir simulation framework is not currently available to the oil industry. The objectivesmore » of Task 1 are to develop three primary modules representing reservoir, chemical, and well data. The modules will be interfaced with an already available experimental design model. The objective of the Task 2 is to incorporate UTCHEM reservoir simulator and the modules with the strategic variables and developing the response surface maps to identify the significant variables from each module. The objective of the Task 3 is to develop the economic model designed specifically for the chemical processes targeted in this proposal and interface the economic model with UTCHEM production output. Task 4 is on the validation of the framework and performing simulations of oil reservoirs to screen, design and optimize the chemical processes.« less

A FRAMEWORK TO DESIGN AND OPTIMIZE CHEMICAL FLOODING PROCESSES

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mojdeh Delshad; Gary A. Pope; Kamy Sepehrnoori

2004-11-01

The goal of this proposed research is to provide an efficient and user friendly simulation framework for screening and optimizing chemical/microbial enhanced oil recovery processes. The framework will include (1) a user friendly interface to identify the variables that have the most impact on oil recovery using the concept of experimental design and response surface maps, (2) UTCHEM reservoir simulator to perform the numerical simulations, and (3) an economic model that automatically imports the simulation production data to evaluate the profitability of a particular design. Such a reservoir simulation framework is not currently available to the oil industry. The objectivesmore » of Task 1 are to develop three primary modules representing reservoir, chemical, and well data. The modules will be interfaced with an already available experimental design model. The objective of the Task 2 is to incorporate UTCHEM reservoir simulator and the modules with the strategic variables and developing the response surface maps to identify the significant variables from each module. The objective of the Task 3 is to develop the economic model designed specifically for the chemical processes targeted in this proposal and interface the economic model with UTCHEM production output. Task 4 is on the validation of the framework and performing simulations of oil reservoirs to screen, design and optimize the chemical processes.« less

Modifying glass fiber surface with grafting acrylamide by UV-grafting copolymerization for preparation of glass fiber reinforced PVDF composite membrane.

PubMed

Luo, Nan; Zhong, Hui; Yang, Min; Yuan, Xing; Fan, Yaobo

2016-01-01

Experimental design and response surface methodology (RSM) were used to optimize the modification of conditions for glass surface grafting with acrylamide (AM) monomer for preparation of a glass fiber reinforced poly(vinylidene fluoride) (PVDF) composite membrane (GFRP-CM). The factors considered for experimental design were the UV (ultraviolet)-irradiation time, the concentrations of the initiator and solvent, and the kinds and concentrations of the silane coupling agent. The optimum operating conditions determined were UV-irradiation time of 25 min, an initiator concentration of 0-0.25 wt.%, solvent of N-Dimethylacetamide (DMAC), and silane coupling agent KH570 with a concentration of 7 wt.%. The obtained optimal parameters were located in the valid region and the experimental confirmation tests conducted showed good accordance between predicted and experimental values. Under these optimal conditions, the water absorption of the grafted modified glass fiber was improved from 13.6% to 23%; the tensile strength was enhanced and the peeling strength of the glass fiber reinforced PVDF composite membrane was improved by 23.7% and 32.6% with an AM concentration at 1 wt.% and 2 wt.%. The surface composition and microstructure of AM grafted glass fiber were studied via several techniques including Field Emission Scanning Electron Microscopy (FESEM), Fourier transform infrared spectroscopy-attenuated total reflectance (FTIR-ATR) and energy dispersive X-ray spectroscopy (EDX). The analysis of the EDX and FTIR-ATR results confirmed that the AM was grafted to the glass fiber successfully by detecting and proving the existence of nitrogen atoms in the GFRP-CM. Copyright © 2015. Published by Elsevier B.V.

Wetting, superhydrophobicity, and icephobicity in biomimetic composite materials

NASA Astrophysics Data System (ADS)

Hejazi, Vahid

Recent developments in nano- and bio-technology require new materials. Among these new classes of materials which have emerged in the recent years are biomimetic materials, which mimic structure and properties of materials found in living nature. There are a large number of biological objects including bacteria, animals and plants with properties of interest for engineers. Among these properties is the ability of the lotus leaf and other natural materials to repel water, which has inspired researchers to prepare similar surfaces. The Lotus effect involving roughness-induced superhydrophobicity is a way to design nonwetting, self-cleaning, omniphobic, icephobic, and antifouling surfaces. The range of actual and potential applications of superhydrophobic surfaces is diverse including optical, building and architecture, textiles, solar panels, lab-on-a-chip, microfluidic devices, and applications requiring antifouling from biological and organic contaminants. In this thesis, in chapter one, we introduce the general concepts and definitions regarding the wetting properties of the surfaces. In chapter two, we develop novel models and conduct experiments on wetting of composite materials. To design sustainable superhydrophobic metal matrix composite (MMC) surfaces, we suggest using hydrophobic reinforcement in the bulk of the material, rather than only at its surface. We experimentally study the wetting properties of graphite-reinforced Al- and Cu-based composites and conclude that the Cu-based MMCs have the potential to be used in the future for the applications where the wear-resistant superhydrophobicity is required. In chapter three, we introduce hydrophobic coating at the surface of concrete materials making them waterproof to prevent material failure, because concretes and ceramics cannot stop water from seeping through them and forming cracks. We create water-repellant concretes with CA close to 160o using superhydrophobic coating. In chapter four, experimental data are collected in terms of oleophobicity especially when underwater applications are of interest. We develop models for four-phase rough interface of underwater oleophobicity and develop a novel approach to predict the CA of organic liquid on the rough surfaces immersed in water. We investigate wetting transition on a patterned surface in underwater systems, using a phase field model. We demonstrated that roughening on an immersed solid surface can drive the transition from Wenzel to Cassie-Baxter state. This discovery improves our understanding of underwater systems and their surface interactions during the wetting phenomenon and can be applied for the development of underwater oil-repellent materials which are of interest for various applications in the water industry, and marine devices. In chapter five, we experimentally and theoretically investigate the icephobicity of composite materials. A novel comprehensive definition of icephobicity, broad enough to cover a variety of situations including low adhesion strength, delayed ice crystallization, and bouncing is determined. Wetting behavior and ice adhesion properties of various samples are theoretically and experimentally compared. We conclude superhydrophobic surfaces are not necessarily icephobic. The models are tested against the experimental data to verify the good agreement between them. The models can be used for the design of novel superhydrophobic, oleophobic, omniphobic and icephobic composite materials. Finally we conclude that creating surface micro/nanostructures using mechanical abrasion or chemical etching as well as applying low energy materials are the most simple, inexpensive, and durable techniques to create superhydrophobic, oleophobic, and icephobic materials.

Nanoscale effects in the characterization of viscoelastic materials with atomic force microscopy: coupling of a quasi-three-dimensional standard linear solid model with in-plane surface interactions.

PubMed

Solares, Santiago D

2016-01-01

Significant progress has been accomplished in the development of experimental contact-mode and dynamic-mode atomic force microscopy (AFM) methods designed to measure surface material properties. However, current methods are based on one-dimensional (1D) descriptions of the tip-sample interaction forces, thus neglecting the intricacies involved in the material behavior of complex samples (such as soft viscoelastic materials) as well as the differences in material response between the surface and the bulk. In order to begin to address this gap, a computational study is presented where the sample is simulated using an enhanced version of a recently introduced model that treats the surface as a collection of standard-linear-solid viscoelastic elements. The enhanced model introduces in-plane surface elastic forces that can be approximately related to a two-dimensional (2D) Young's modulus. Relevant cases are discussed for single- and multifrequency intermittent-contact AFM imaging, with focus on the calculated surface indentation profiles and tip-sample interaction force curves, as well as their implications with regards to experimental interpretation. A variety of phenomena are examined in detail, which highlight the need for further development of more physically accurate sample models that are specifically designed for AFM simulation. A multifrequency AFM simulation tool based on the above sample model is provided as supporting information.

Experimental Investigation of a High Pressure Ratio Aspirated Fan Stage

NASA Technical Reports Server (NTRS)

Merchant, Ali; Kerrebrock, Jack L.; Adamczyk, John J.; Braunscheidel, Edward

2004-01-01

The experimental investigation of an aspirated fan stage designed to achieve a pressure ratio of 3.4:1 at 1500 ft/sec is presented in this paper. The low-energy viscous flow is aspirated from diffusion-limiting locations on the blades and flowpath surfaces of the stage, enabling a very high pressure ratio to be achieved in a single stage. The fan stage performance was mapped at various operating speeds from choke to stall in a compressor facility at fully simulated engine conditions. The experimentally determined stage performance, in terms of pressure ratio and corresponding inlet mass flow rate, was found to be in good agreement with the three-dimensional viscous computational prediction, and in turn close to the design intent. Stage pressure ratios exceeding 3:1 were achieved at design speed, with an aspiration flow fraction of 3.5 percent of the stage inlet mass flow. The experimental performance of the stage at various operating conditions, including detailed flowfield measurements, are presented and discussed in the context of the computational analyses. The sensitivity of the stage performance and operability to reduced aspiration flow rates at design and off design conditions are also discussed.

Phase-compensated metasurface for a conformal microwave antenna

NASA Astrophysics Data System (ADS)

Germain, Dylan; Seetharamdoo, Divitha; Nawaz Burokur, Shah; de Lustrac, André

2013-09-01

The in-phase radiation from a conformal metamaterial surface is numerically and experimentally reported. The LC-resonant metasurface is composed of a simultaneously capacitive and an inductive grid constituted by copper strips printed on both sides of a dielectric board. The metasurface is designed to fit a curved surface by modifying its local phase. The latter phase-compensated metasurface is used as a reflector in a conformal Fabry-Pérot resonant cavity designed to operate at microwave frequencies. Far-field measurements performed on a fabricated prototype allow showing the good performances of such a phase-compensated metasurface in restoring in-phase emissions from the conformal surface and producing a directive emission in the desired direction.

The use of interpractive graphic displays for interpretation of surface design parameters

NASA Technical Reports Server (NTRS)

Talcott, N. A., Jr.

1981-01-01

An interactive computer graphics technique known as the Graphic Display Data method has been developed to provide a convenient means for rapidly interpreting large amounts of surface design data. The display technique should prove valuable in such disciplines as aerodynamic analysis, structural analysis, and experimental data analysis. To demonstrate the system's features, an example is presented of the Graphic Data Display method used as an interpretive tool for radiation equilibrium temperature distributions over the surface of an aerodynamic vehicle. Color graphic displays were also examined as a logical extension of the technique to improve its clarity and to allow the presentation of greater detail in a single display.

Application of Plackett-Burman experimental design in the development of muffin using adlay flour

NASA Astrophysics Data System (ADS)

Valmorida, J. S.; Castillo-Israel, K. A. T.

2018-01-01

The application of Plackett-Burman experimental design was made to identify significant formulation and process variables in the development of muffin using adlay flour. Out of the seven screened variables, levels of sugar, levels of butter and baking temperature had the most significant influence on the product model in terms of physicochemical and sensory acceptability. Results of the experiment further demonstrate the effectiveness of Plackett-Burman design in choosing the best adlay variety for muffin production. Hence, the statistical method used in the study permits an efficient selection of important variables needed in the development of muffin from adlay which can be optimized using response surface methodology.

Anisotropic transmissive coding metamaterials based on dispersion modulation of spoof surface plasmon polaritons

NASA Astrophysics Data System (ADS)

Pang, Yongqiang; Li, Yongfeng; Zhang, Jieqiu; Chen, Hongya; Xu, Zhuo; Qu, Shaobo

2018-06-01

Anisotropic transmissive coding metamaterials (CMMs) have been designed and demonstrated in this work. High-efficiency transmission with the amplitudes close to unity is achieved by ultrathin metallic tapered blade structures, on which incident waves can be highly coupled into spoof surface plasmon polaritons (SSPPs). The transmission phase can be therefore manipulated with much freedom by designing the dispersion of the SSPPs. These tapered blade structures are designed as the anisotropic unit cells of the CMMs. Two 1-bit anisotropic CMMs with different coding sequences were first designed and simulated, and then a 2-bit anisotropic CMM was designed and measured experimentally. The measured results agree well with the simulations. It is expected that this work provides an alternative method for designing the transmissive CMMs, and may find potential applications in the beam forming technique.

Mechanism and experimental research on ultra-precision grinding of ferrite

NASA Astrophysics Data System (ADS)

Ban, Xinxing; Zhao, Huiying; Dong, Longchao; Zhu, Xueliang; Zhang, Chupeng; Gu, Yawen

2017-02-01

Ultra-precision grinding of ferrite is conducted to investigate the removal mechanism. Effect of the accuracy of machine tool key components on grinding surface quality is analyzed. The surface generation model of ferrite ultra-precision grinding machining is established. In order to reveal the surface formation mechanism of ferrite in the process of ultraprecision grinding, furthermore, the scientific and accurate of the calculation model are taken into account to verify the grinding surface roughness, which is proposed. Orthogonal experiment is designed using the high precision aerostatic turntable and aerostatic spindle for ferrite which is a typical hard brittle materials. Based on the experimental results, the influence factors and laws of ultra-precision grinding surface of ferrite are discussed through the analysis of the surface roughness. The results show that the quality of ferrite grinding surface is the optimal parameters, when the wheel speed of 20000r/mm, feed rate of 10mm/min, grinding depth of 0.005mm, and turntable rotary speed of 5r/min, the surface roughness Ra can up to 75nm.

Snag longevity and surface fuel accumulation following post-fire logging in a ponderosa pine dominated forest

Treesearch

Martin W. Ritchie; Eric E. Knapp; Carl N. Skinner

2013-01-01

In a study of post-fire logging effects over an 8 year period at Blacks Mountain Experimental Forest, salvage logging was conducted at varying levels of intensity after a 2002 wildfire event. In a designed experiment, harvest prescriptions with snag retention levels ranging from 0% to 100% in 15 experimental units were installed. Observations of standing snags and...

Physics of heat pipe rewetting

NASA Technical Reports Server (NTRS)

Chan, S. H.

1994-01-01

This is the final report which summarizes the research accomplishments under the project entitled 'Physics of Heat Pipe Rewetting' under NASA Grant No. NAG 9-525, Basic, during the period of April 1, 1991 to January 31, 1994. The objective of the research project was to investigate both analytically and experimentally the rewetting characteristics of the heated, grooved plate. The grooved plate is to simulate the inner surface of the vapor channel in monogroove heat pipes for space station design. In such designs, the inner surface of the vapor channel is threaded with monogrooves. When the heat pipe is thermally overloaded, dryout of the monogroove surface occurs. Such a dryout surface should be promptly rewetted to prevent the failure of the heat pipe operation in the thermal radiator of the space station.

Control of crankshaft finish by scattering technique

NASA Astrophysics Data System (ADS)

Fontani, Daniela; Francini, Franco; Longobardi, Giuseppe; Sansoni, Paola

2001-06-01

The paper describes a new sensor dedicated to measure and check the surface quality of mechanical products. The results were obtained comparing the light scattered from two different ranges of angles by means of 16 photodiodes. The device is designed for obtaining valid data from curved surfaces as that of a crankshaft. Experimental measurements show that the ratio between scattered and reflected light intensity increases with the surface roughness. This device was developed for the off-tolerance detection of mechanical pieces in industrial production. Results of surface quality on crankshaft supplied by Renault were carried out.

Circulation of spoof surface plasmon polaritons: Implementation and verification

NASA Astrophysics Data System (ADS)

Pan, Junwei; Wang, Jiafu; Qiu, Tianshuo; Pang, Yongqiang; Li, Yongfeng; Zhang, Jieqiu; Qu, Shaobo

2018-05-01

In this letter, we are dedicated to implementation and experimental verification of broadband circulator for spoof surface plasmon polaritons (SSPPs). For the ease of fabrication, a circulator operating in X band was firstly designed. The comb-like transmission lines (CL-TLs), a typical SSPP structure, are adopted as the three branches of the Y-junction. To enable broadband coupling of SSPP, a transition section is added on each end of the CL-TLs. Through such a design, the circulator can operate under the sub-wavelength SSPP mode in a broad band. The simulation results show that the insertion loss is less than 0.5dB while the isolation and return loss are higher than 20dB in 9.4-12.0GHz. A prototype was fabricated and measured. The experimental results are consistent with the simulation results and verify the broadband circulation performance in X band.

Subcritical water liquefaction of oil palm fruit press fiber in the presence of sodium hydroxide: an optimisation study using response surface methodology.

PubMed

Mazaheri, Hossein; Lee, Keat Teong; Bhatia, Subhash; Mohamed, Abdul Rahman

2010-12-01

Thermal decomposition of oil palm fruit press fiber (FPF) into a liquid product (LP) was achieved using subcritical water treatment in the presence of sodium hydroxide in a high pressure batch reactor. This study uses experimental design and process optimisation tools to maximise the LP yield using response surface methodology (RSM) with central composite rotatable design (CCRD). The independent variables were temperature, residence time, particle size, specimen loading, and additive loading. The mathematical model that was developed fit the experimental results well for all of the response variables that were studied. The optimal conditions were found to be a temperature of 551 K, a residence time of 40 min, a particle size of 710-1000 microm, a specimen loading of 5 g, and a additive loading of 9 wt.% to achieve a LP yield of 76.16%. 2010 Elsevier Ltd. All rights reserved.

A Computational and Experimental Investigation of a Three-Dimensional Hypersonic Scramjet Inlet Flow Field. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Holland, Scott Douglas

1991-01-01

A combined computational and experimental parametric study of the internal aerodynamics of a generic three dimensional sidewall compression scramjet inlet configuration was performed. The study was designed to demonstrate the utility of computational fluid dynamics as a design tool in hypersonic inlet flow fields, to provide a detailed account of the nature and structure of the internal flow interactions, and to provide a comprehensive surface property and flow field database to determine the effects of contraction ratio, cowl position, and Reynolds number on the performance of a hypersonic scramjet inlet configuration.

Optimization of Culture Conditions for Production of the Anti-Leukemic Glutaminase Free L-Asparaginase by Newly Isolated Streptomyces olivaceus NEAE-119 Using Response Surface Methodology.

PubMed

El-Naggar, Noura El-Ahmady; Moawad, Hassan; El-Shweihy, Nancy M; El-Ewasy, Sara M

2015-01-01

Among the antitumor drugs, bacterial enzyme L-asparaginase has been employed as the most effective chemotherapeutic agent in pediatric oncotherapy especially for acute lymphoblastic leukemia. Glutaminase free L-asparaginase producing actinomycetes were isolated from soil samples collected from Egypt. Among them, a potential culture, strain NEAE-119, was selected and identified on the basis of morphological, cultural, physiological, and biochemical properties together with 16S rRNA sequence as Streptomyces olivaceus NEAE-119 and sequencing product (1509 bp) was deposited in the GenBank database under accession number KJ200342. The optimization of different process parameters for L-asparaginase production by Streptomyces olivaceus NEAE-119 using Plackett-Burman experimental design and response surface methodology was carried out. Fifteen variables (temperature, pH, incubation time, inoculum size, inoculum age, agitation speed, dextrose, starch, L-asparagine, KNO3, yeast extract, K2HPO4, MgSO4·7H2O, NaCl, and FeSO4·7H2O) were screened using Plackett-Burman experimental design. The most positive significant independent variables affecting enzyme production (temperature, inoculum age, and agitation speed) were further optimized by the face-centered central composite design-response surface methodology.

Optimization of Culture Conditions for Production of the Anti-Leukemic Glutaminase Free L-Asparaginase by Newly Isolated Streptomyces olivaceus NEAE-119 Using Response Surface Methodology

PubMed Central

El-Naggar, Noura El-Ahmady; Moawad, Hassan; El-Shweihy, Nancy M.; El-Ewasy, Sara M.

2015-01-01

Among the antitumor drugs, bacterial enzyme L-asparaginase has been employed as the most effective chemotherapeutic agent in pediatric oncotherapy especially for acute lymphoblastic leukemia. Glutaminase free L-asparaginase producing actinomycetes were isolated from soil samples collected from Egypt. Among them, a potential culture, strain NEAE-119, was selected and identified on the basis of morphological, cultural, physiological, and biochemical properties together with 16S rRNA sequence as Streptomyces olivaceus NEAE-119 and sequencing product (1509 bp) was deposited in the GenBank database under accession number KJ200342. The optimization of different process parameters for L-asparaginase production by Streptomyces olivaceus NEAE-119 using Plackett-Burman experimental design and response surface methodology was carried out. Fifteen variables (temperature, pH, incubation time, inoculum size, inoculum age, agitation speed, dextrose, starch, L-asparagine, KNO3, yeast extract, K2HPO4, MgSO4·7H2O, NaCl, and FeSO4·7H2O) were screened using Plackett-Burman experimental design. The most positive significant independent variables affecting enzyme production (temperature, inoculum age, and agitation speed) were further optimized by the face-centered central composite design-response surface methodology. PMID:26180806

Design and construction of an experimental pervious paved parking area to harvest reusable rainwater.

PubMed

Gomez-Ullate, E; Novo, A V; Bayon, J R; Hernandez, Jorge R; Castro-Fresno, Daniel

2011-01-01

Pervious pavements are sustainable urban drainage systems already known as rainwater infiltration techniques which reduce runoff formation and diffuse pollution in cities. The present research is focused on the design and construction of an experimental parking area, composed of 45 pervious pavement parking bays. Every pervious pavement was experimentally designed to store rainwater and measure the levels of the stored water and its quality over time. Six different pervious surfaces are combined with four different geotextiles in order to test which materials respond better to the good quality of rainwater storage over time and under the specific weather conditions of the north of Spain. The aim of this research was to obtain a good performance of pervious pavements that offered simultaneously a positive urban service and helped to harvest rainwater with a good quality to be used for non potable demands.

Response Surface Modeling of Combined-Cycle Propulsion Components using Computational Fluid Dynamics

NASA Technical Reports Server (NTRS)

Steffen, C. J., Jr.

2002-01-01

Three examples of response surface modeling with CFD are presented for combined cycle propulsion components. The examples include a mixed-compression-inlet during hypersonic flight, a hydrogen-fueled scramjet combustor during hypersonic flight, and a ducted-rocket nozzle during all-rocket flight. Three different experimental strategies were examined, including full factorial, fractionated central-composite, and D-optimal with embedded Plackett-Burman designs. The response variables have been confined to integral data extracted from multidimensional CFD results. Careful attention to uncertainty assessment and modeling bias has been addressed. The importance of automating experimental setup and effectively communicating statistical results are emphasized.

Potential flow analysis of glaze ice accretions on an airfoil

NASA Technical Reports Server (NTRS)

Zaguli, R. J.

1984-01-01

The results of an analytical/experimental study of the flow fields about an airfoil with leading edge glaze ice accretion shapes are presented. Tests were conducted in the Icing Research Tunnel to measure surface pressure distributions and boundary layer separation reattachment characteristics on a general aviation wing section to which was affixed wooden ice shapes which approximated typical glaze ice accretions. Comparisons were made with predicted pressure distributions using current airfoil analysis codes as well as the Bristow mixed analysis/design airfoil panel code. The Bristow code was also used to predict the separation reattachment dividing streamline by inputting the appropriate experimental surface pressure distribution.

LSAH: a fast and efficient local surface feature for point cloud registration

NASA Astrophysics Data System (ADS)

Lu, Rongrong; Zhu, Feng; Wu, Qingxiao; Kong, Yanzi

2018-04-01

Point cloud registration is a fundamental task in high level three dimensional applications. Noise, uneven point density and varying point cloud resolutions are the three main challenges for point cloud registration. In this paper, we design a robust and compact local surface descriptor called Local Surface Angles Histogram (LSAH) and propose an effectively coarse to fine algorithm for point cloud registration. The LSAH descriptor is formed by concatenating five normalized sub-histograms into one histogram. The five sub-histograms are created by accumulating a different type of angle from a local surface patch respectively. The experimental results show that our LSAH is more robust to uneven point density and point cloud resolutions than four state-of-the-art local descriptors in terms of feature matching. Moreover, we tested our LSAH based coarse to fine algorithm for point cloud registration. The experimental results demonstrate that our algorithm is robust and efficient as well.

Secondary-electron-emission losses in multistage depressed collectors and traveling-wave-tube efficiency improvements with carbon collector electrode surfaces

NASA Technical Reports Server (NTRS)

Ramins, P.; Ebihara, B. T.

1986-01-01

Secondary-electron-emission losses in multistage depressed collectors (MDC's) and their effects on overall traveling-wave-tube (TWT) efficiency were investigated. Two representative TWT's and several computer-modeled MDC's were used. The experimental techniques provide the measurement of both the TWT overall and the collector efficiencies. The TWT-MDC performance was optimized and measured over a wide range of operating conditions, with geometrically identical collectors, which utilized different electrode surface materials. Comparisons of the performance of copper electrodes to that of various forms of carbon, including pyrolytic and iisotropic graphites, were stressed. The results indicate that: (1) a significant improvement in the TWT overall efficiency was obtained in all cases by the use of carbon, rather than copper electrodes, and (2) that the extent of this efficiency enhancement depended on the characteristics of the TWT, the TWT operating point, the MDC design, and collector voltages. Ion textured graphite was found to be particularly effective in minimizing the secondary-electron-emission losses. Experimental and analytical results, however, indicate that it is at least as important to provide a maximum amount of electrostatic suppression of secondary electrons by proper MDC design. Such suppression, which is obtained by ensuring that a substantial suppressing electric field exists over the regions of the electrodes where most of the current is incident, was found to be very effective. Experimental results indicate that, with proper MDC design and the use of electrode surfaces with low secondary-electron yield, degradation of the collector efficiency can be limited to a few percent.

Nonlinear aerodynamic wing design

NASA Technical Reports Server (NTRS)

Bonner, Ellwood

1985-01-01

The applicability of new nonlinear theoretical techniques is demonstrated for supersonic wing design. The new technology was utilized to define outboard panels for an existing advanced tactical fighter model. Mach 1.6 maneuver point design and multi-operating point compromise surfaces were developed and tested. High aerodynamic efficiency was achieved at the design conditions. A corollary result was that only modest supersonic penalties were incurred to meet multiple aerodynamic requirements. The nonlinear potential analysis of a practical configuration arrangement correlated well with experimental data.

On the theory of compliant wall drag reduction in turbulent boundary layers

NASA Technical Reports Server (NTRS)

Ash, R. L.

1974-01-01

A theoretical model has been developed which can explain how the motion of a compliant wall reduces turbulent skin friction drag. Available experimental evidence at low speeds has been used to infer that a compliant surface selectively removes energy from the upper frequency range of the energy containing eddies and through resulting surface motions can produce locally negative Reynolds stresses at the wall. The theory establishes a preliminary amplitude and frequency criterion as the basis for designing effective drag reducing compliant surfaces.

Scanning and Measuring Device for Diagnostic of Barrel Bore

NASA Astrophysics Data System (ADS)

Marvan, Ales; Hajek, Josef; Vana, Jan; Dvorak, Radim; Drahansky, Martin; Jankovych, Robert; Skvarek, Jozef

The article discusses the design, mechanical design, electronics and software for robot diagnosis of barrels with caliber of 120 mm to 155 mm. This diagnostic device is intended primarily for experimental research and verification of appropriate methods and technologies for the diagnosis of the main bore guns. Article also discusses the design of sensors and software, the issue of data processing and image reconstruction obtained by scanning of the surface of the bore.

A Review on the Wettability of Dental Implant Surfaces II: Biological and Clinical Aspects

PubMed Central

Gittens, Rolando A.; Scheideler, Lutz; Rupp, Frank; Hyzy, Sharon L.; Geis-Gerstorfer, Jürgen; Schwartz, Zvi; Boyan, Barbara D.

2014-01-01

Dental and orthopaedic implants have been under continuous advancement to improve their interactions with bone and ensure a successful outcome for patients. Surface characteristics such as surface topography and surface chemistry can serve as design tools to enhance the biological response around the implant, with in vitro, in vivo and clinical studies confirming their effects. However, the comprehensive design of implants to promote early and long-term osseointegration requires a better understanding of the role of surface wettability and the mechanisms by which it affects the surrounding biological environment. This review provides a general overview of the available information about the contact angle values of experimental and of marketed implant surfaces, some of the techniques used to modify surface wettability of implants, and results from in vitro and clinical studies. We aim to expand the current understanding on the role of wettability of metallic implants at their interface with blood and the biological milieu, as well as with bacteria, and hard and soft tissues. PMID:24709541

A passive means for cancellation of structurally radiated tones.

PubMed

Zapfe, Jeffrey A; Ungar, Eric E

2003-01-01

The concept of cancellation of constant-frequency sound radiated from a vibrating surface by means of an attached mechanical oscillator is discussed. It is observed that the mass of a mechanical oscillator whose spring is attached to the vibrating surface will vibrate at comparatively large amplitudes and out of phase with that surface, provided that the surface vibrates at a frequency that is slightly higher than the oscillator's natural frequency. From this observation it is concluded that an oscillator's mass with a relatively small surface area can produce a volume velocity that is equal and opposite to that of the vibrating surface, resulting in cancellation of the sound radiated from the surface. Practical considerations in the design of such an oscillator are discussed, and the canceling performance from oscillators consisting of edge-supported circular disks is analyzed. An experimental canceling oscillator consisting of an edge-supported disk is described, and measurements made with this disk attached to a piston are shown to be in good agreement with analytical predictions. A tonal noise reduction exceeding 20 dB was demonstrated experimentally.

Modeling of a Micro-Electronic Mechanical Systems (MEMS) Deformable Mirror for Simulation and Characterization

DTIC Science & Technology

2016-09-01

1  II.  MODEL DESIGN ...Figure 10.  Experimental Optical Layout for the Boston DM Characterization ..........13  Figure 11.  Side View Showing the Curved Surface on a DM...of different methods for deposition, patterning, and etching until the desired design of the device is achieved. While a large number of devices

Design Expert Supported Mathematical Optimization and Predictability Study of Buccoadhesive Pharmaceutical Wafers of Loratadine

PubMed Central

Dey, Surajit; Parcha, Versha; Bhattacharya, Shiv Sankar; Ghosh, Amitava

2013-01-01

Objective. The objective of this work encompasses the application of the response surface approach in the development of buccoadhesive pharmaceutical wafers of Loratadine (LOR). Methods. Experiments were performed according to a 32 factorial design to evaluate the effects of buccoadhesive polymer, sodium alginate (A), and lactose monohydrate as ingredient, of hydrophilic matrix former (B) on the bioadhesive force, disintegration time, percent (%) swelling index, and time taken for 70% drug release (t 70%). The effect of the two independent variables on the response variables was studied by response surface plots and contour plots generated by the Design-Expert software. The desirability function was used to optimize the response variables. Results. The compatibility between LOR and the wafer excipients was confirmed by differential scanning calorimetry, FTIR spectroscopy, and X-ray diffraction (XRD) analysis. Bioadhesion force, measured with TAXT2i texture analyzer, showed that the wafers had a good bioadhesive property which could be advantageous for retaining the drug into the buccal cavity. Conclusion. The observed responses taken were in agreement with the experimental values, and Loratadine wafers were produced with less experimental trials, and a patient compliant product was achieved with the concept of formulation by design. PMID:23781498

Heterogeneous catalysis: Enigmas, illusions, challenges, realities, and emergent strategies of design

NASA Astrophysics Data System (ADS)

Thomas, John Meurig

2008-05-01

Predominantly this article deals with the question of how to design new solid catalysts for a variety of industrial and laboratory-orientated purposes. A generally applicable strategy, illustrated by numerous examples, is made possible based on the use of nanoporous materials on to the (high-area) inner surfaces of which well-defined (experimentally and computationally) active centers are placed in a spatially separated fashion. Such single-site catalysts, which have much in common with metal-centered homogenous catalysts and enzymes, enable a wide range of new catalysts to be designed for a variety of selective oxidations, hydrogenations, hydrations and hydrodewaxing, and other reactions that the "greening" of industrial processes demand. Examples are given of new shape-selective, regio-selective, and enantioselective catalysts, many of which operate under mild, environmentally benign conditions. Also considered are some of the reasons why detailed studies of adsorption and stoichiometric reactions at single-crystal surfaces have, disappointingly, not hitherto paved the way to the design and production of many new heterogenous catalysts. Recent work of a theoretical and high-throughout nature, allied to some experimental studies of well-chosen model systems, holds promise for the identification of new catalysts for simple, but industrially important reactions.

Design of a surface-scanning coil detector for direct bacteria detection on food surfaces using a magnetoelastic biosensor

NASA Astrophysics Data System (ADS)

Chai, Yating; Wikle, Howard C.; Wang, Zhenyu; Horikawa, Shin; Best, Steve; Cheng, Zhongyang; Dyer, Dave F.; Chin, Bryan A.

2013-09-01

The real-time, in-situ bacteria detection on food surfaces was achieved by using a magnetoelastic biosensor combined with a surface-scanning coil detector. This paper focuses on the coil design for signal optimization. The coil was used to excite the sensor's vibration and detect its resonant frequency signal. The vibrating sensor creates a magnetic flux change around the coil, which then produces a mutual inductance. In order to enhance the signal amplitude, a theory of the sensor's mutual inductance with the measurement coil is proposed. Both theoretical calculations and experimental data showed that the working length of the coil has a significant effect on the signal amplitude. For a 1 mm-long sensor, a coil with a working length of 1.3 mm showed the best signal amplitude. The real-time detection of Salmonella bacteria on a fresh food surface was demonstrated using this new technology.

EXPERIMENTAL INVESTIGATION OF THE ORTHO/PARA RATIO OF NEWLY FORMED MOLECULAR HYDROGEN ON AMORPHOUS SOLID WATER

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gavilan, L.; Lemaire, J. L.; Dulieu, F.

2012-11-20

Several astronomical observations have shown that the ortho/para ratio (OPR) of H{sub 2} can differ from the expected statistical value of 3 or the local thermodynamic equilibrium (LTE) value at the gas or dust temperature. It is thus important to know the OPR of H{sub 2} newly formed on dust grain surfaces, in order to clarify the dependence of the observed OPR in space on the formation process. Using an experimental setup designed to mimic interstellar medium environments, we measured the OPR of H{sub 2} and D{sub 2} formed on the surface of porous amorphous water ice held at 10more » K. We report for the first time the OPR value for newly formed D{sub 2}, consistent with the expected LTE value at the high-temperature limit found by previous theoretical and experimental works on the determination of the OPR upon H{sub 2} formation on surfaces at low temperature.« less

Photonic crystals possessing multiple Weyl points and the experimental observation of robust surface states

PubMed Central

Chen, Wen-Jie; Xiao, Meng; Chan, C. T.

2016-01-01

Weyl points, as monopoles of Berry curvature in momentum space, have captured much attention recently in various branches of physics. Realizing topological materials that exhibit such nodal points is challenging and indeed, Weyl points have been found experimentally in transition metal arsenide and phosphide and gyroid photonic crystal whose structure is complex. If realizing even the simplest type of single Weyl nodes with a topological charge of 1 is difficult, then making a real crystal carrying higher topological charges may seem more challenging. Here we design, and fabricate using planar fabrication technology, a photonic crystal possessing single Weyl points (including type-II nodes) and multiple Weyl points with topological charges of 2 and 3. We characterize this photonic crystal and find nontrivial 2D bulk band gaps for a fixed kz and the associated surface modes. The robustness of these surface states against kz-preserving scattering is experimentally observed for the first time. PMID:27703140

NaOH-based high temperature heat-of-fusion thermal energy storage device

NASA Technical Reports Server (NTRS)

Cohen, B. M.; Rice, R. E.

1978-01-01

A material called Thermkeep, developed as a low-cost method for the storage of thermal energy for solar electric power generating systems is discussed. The storage device consists of an insulated cylinder containing Thermkeep in which coiled tubular heat exchangers are immersed. A one-tenth scale model of the design contains 25 heat-exchanger tubes and 1500 kg of Thermkeep. Its instrumentation includes thermocouples to measure internal Thermkeep temperatures, vessel surface, heated shroud surface, and pressure gauges to indicate heat-exchanger pressure drops. The test-circuit design is presented and experimental results are discussed.

Time-oriented experimental design method to optimize hydrophilic matrix formulations with gelation kinetics and drug release profiles.

PubMed

Shin, Sangmun; Choi, Du Hyung; Truong, Nguyen Khoa Viet; Kim, Nam Ah; Chu, Kyung Rok; Jeong, Seong Hoon

2011-04-04

A new experimental design methodology was developed by integrating the response surface methodology and the time series modeling. The major purposes were to identify significant factors in determining swelling and release rate from matrix tablets and their relative factor levels for optimizing the experimental responses. Properties of tablet swelling and drug release were assessed with ten factors and two default factors, a hydrophilic model drug (terazosin) and magnesium stearate, and compared with target values. The selected input control factors were arranged in a mixture simplex lattice design with 21 experimental runs. The obtained optimal settings for gelation were PEO, LH-11, Syloid, and Pharmacoat with weight ratios of 215.33 (88.50%), 5.68 (2.33%), 19.27 (7.92%), and 3.04 (1.25%), respectively. The optimal settings for drug release were PEO and citric acid with weight ratios of 191.99 (78.91%) and 51.32 (21.09%), respectively. Based on the results of matrix swelling and drug release, the optimal solutions, target values, and validation experiment results over time were similar and showed consistent patterns with very small biases. The experimental design methodology could be a very promising experimental design method to obtain maximum information with limited time and resources. It could also be very useful in formulation studies by providing a systematic and reliable screening method to characterize significant factors in the sustained release matrix tablet. Copyright © 2011 Elsevier B.V. All rights reserved.

Application of a statistical design to the optimization of parameters and culture medium for alpha-amylase production by Aspergillus oryzae CBS 819.72 grown on gruel (wheat grinding by-product).

PubMed

Kammoun, Radhouane; Naili, Belgacem; Bejar, Samir

2008-09-01

The production optimization of alpha-amylase (E.C.3.2.1.1) from Aspergillus oryzae CBS 819.72 fungus, using a by-product of wheat grinding (gruel) as sole carbon source, was performed with statistical methodology based on three experimental designs. The optimisation of temperature, agitation and inoculum size was attempted using a Box-Behnken design under the response surface methodology. The screening of nineteen nutrients for their influence on alpha-amylase production was achieved using a Plackett-Burman design. KH(2)PO(4), urea, glycerol, (NH(4))(2)SO(4), CoCl(2), casein hydrolysate, soybean meal hydrolysate, MgSO(4) were selected based on their positive influence on enzyme formation. The optimized nutrients concentration was obtained using a Taguchi experimental design and the analysis of the data predicts a theoretical increase in the alpha-amylase expression of 73.2% (from 40.1 to 151.1 U/ml). These conditions were validated experimentally and revealed an enhanced alpha-amylase yield of 72.7%.

Experimental design based response surface methodology optimization of ultrasonic assisted adsorption of safaranin O by tin sulfide nanoparticle loaded on activated carbon

NASA Astrophysics Data System (ADS)

Roosta, M.; Ghaedi, M.; Daneshfar, A.; Sahraei, R.

2014-03-01

In this research, the adsorption rate of safranine O (SO) onto tin sulfide nanoparticle loaded on activated carbon (SnS-NPAC) was accelerated by the ultrasound. SnS-NP-AC was characterized by different techniques such as SEM, XRD and UV-Vis measurements. The present results confirm that the ultrasound assisted adsorption method has remarkable ability to improve the adsorption efficiency. The influence of parameters such as the sonication time, adsorbent dosage, pH and initial SO concentration was examined and evaluated by central composite design (CCD) combined with response surface methodology (RSM) and desirability function (DF). Conducting adsorption experiments at optimal conditions set as 4 min of sonication time, 0.024 g of adsorbent, pH 7 and 18 mg L-1 SO make admit to achieve high removal percentage (98%) and high adsorption capacity (50.25 mg g-1). A good agreement between experimental and predicted data in this study was observed. The experimental equilibrium data fitting to Langmuir, Freundlich, Tempkin and Dubinin-Radushkevich models show that the Langmuir model is a good and suitable model for evaluation and the actual behavior of adsorption. Kinetic evaluation of experimental data showed that the adsorption processes followed well pseudo-second-order and intraparticle diffusion models.

Optimization and modeling of laccase production by Trametes versicolor in a bioreactor using statistical experimental design.

PubMed

Tavares, A P M; Coelho, M A Z; Agapito, M S M; Coutinho, J A P; Xavier, A M R B

2006-09-01

Experimental design and response surface methodologies were applied to optimize laccase production by Trametes versicolor in a bioreactor. The effects of three factors, initial glucose concentration (0 and 9 g/L), agitation (100 and 180 rpm), and pH (3.0 and 5.0), were evaluated to identify the significant effects and its interactions in the laccase production. The pH of the medium was found to be the most important factor, followed by initial glucose concentration and the interaction of both factors. Agitation did not seem to play an important role in laccase production, nor did the interaction agitation x medium pH and agitation x initial glucose concentration. Response surface analysis showed that an initial glucose concentration of 11 g/L and pH controlled at 5.2 were the optimal conditions for laccase production by T. versicolor. Under these conditions, the predicted value for laccase activity was >10,000 U/L, which is in good agreement with the laccase activity obtained experimentally (11,403 U/L). In addition, a mathematical model for the bioprocess was developed. It is shown that it provides a good description of the experimental profile observed, and that it is capable of predicting biomass growth based on secondary process variables.

Experimental Optimization of a Free-to-Rotate Wing for Small UAS

NASA Technical Reports Server (NTRS)

Logan, Michael J.; DeLoach, Richard; Copeland, Tiwana; Vo, Steven

2014-01-01

This paper discusses an experimental investigation conducted to optimize a free-to-rotate wing for use on a small unmanned aircraft system (UAS). Although free-to-rotate wings have been used for decades on various small UAS and small manned aircraft, little is known about how to optimize these unusual wings for a specific application. The paper discusses some of the design rationale of the basic wing. In addition, three main parameters were selected for "optimization", wing camber, wing pivot location, and wing center of gravity (c.g.) location. A small apparatus was constructed to enable some simple experimental analysis of these parameters. A design-of-experiment series of tests were first conducted to discern which of the main optimization parameters were most likely to have the greatest impact on the outputs of interest, namely, some measure of "stability", some measure of the lift being generated at the neutral position, and how quickly the wing "recovers" from an upset. A second set of tests were conducted to develop a response-surface numerical representation of these outputs as functions of the three primary inputs. The response surface numerical representations are then used to develop an "optimum" within the trade space investigated. The results of the optimization are then tested experimentally to validate the predictions.

A Compact, Broadband Antenna for Planetary Surface-to-Surface Wireless Communications

NASA Technical Reports Server (NTRS)

Barr, Philip; Zaman, Afroz; Miranda, Felix

2006-01-01

The Compact Microstrip Monopole Antenna (CMMA) is a novel antenna design that combines a microstrip patch antenna with a three-dimensional structure to attain a highly directive, broadband, compact antenna. A Tri-Lobed Patch (TLP) was designed to minimize the patch's area while reducing the antenna's operating frequency. A Grounding Wall (GW) connects the patch to the ground plane and a Vertical Enclosure Wall (VEW) extends up away from portions of the patch's perimeter. This VEW supplies the antenna with a higher directivity in the radial direction as well as reduces the operating frequency. The CMMA was designed to operate at 2.23 GHz, but experimental results have shown this antenna resonates at 2.05 GHz which is on the order of approximately Lambda(sub o)/11.6 with respect to the antenna's largest dimension, with a directivity and bandwidth of 6.0 dBi, and 130 MHz (6.3 percent), respectively. This miniature, radially emitting antenna makes the CMMA attractive for planetary-based surface-to-surface communications.

Experimental and numerical analysis on noise reduction in a multi-blade centrifugal fan

NASA Astrophysics Data System (ADS)

Chen, X. J.; Y Cao, T.; Su, J.; Qin, G. L.

2013-12-01

In this work, analysis on noise source and reduction in a multi-blade centrifugal fan used for air-conditioners was carried out by experimental and numerical methods. Firstly, an experimental system using microphone mounted on volute surface for measuring surface pressure fluctuations of volute was designed and introduced, then surface pressure fluctuations of the whole volute for a multi-blade centrifugal fan were measured by this system, and the inlet noise for this fan was also obtained. And then, based on the experimental results, the aerodynamic noise source of the studied fan was analysed. The surface pressure fluctuations of the volute showed that there were largest surface pressure fluctuations near the volute tongue, and peaks appeared at the Blade Passing Frequency (BPF). The spectra of fan inlet noise showed that the peaks also appeared at BPF, and noise levels in a wide range of frequency were also larger. Secondly, the internal flow of the fan was simulated by commercial software under the same conditions with the experiment, and then the fluid flow and acoustic power field were obtained and discussed. The contours of acoustic power level showed that the larger noise was generated at the impeller area close to the outlet of scroll and at the volute tongue, which is same as that from experiment. Based on all of the results, we can find that the vortex noise is an important part of fan noise for the studied fan, and the rotation noise also cannot be neglected. Finally, several reduction methods that are thought to be effective based on experimental and numerical results were suggested.

Structured surface reflector design for oblique incidence beam splitter at 610 GHz.

PubMed

Defrance, F; Casaletti, M; Sarrazin, J; Wiedner, M C; Gibson, H; Gay, G; Lefèvre, R; Delorme, Y

2016-09-05

An iterative alternate projection-based algorithm is developed to design structured surface reflectors to operate as beam splitters at GHz and THz frequencies. To validate the method, a surface profile is determined to achieve a reflector at 610 GHz that generates four equal-intensity beams towards desired directions of ±12.6° with respect to the specular reflection axis. A prototype is fabricated and the beam splitter behavior is experimentally demonstrated. Measurements confirm a good agreement (within 1%) with computer simulations using Feko, validating the method. The beam splitter at 610 GHz has a measured efficiency of 78% under oblique incidence illumination that ensures a similar intensity between the four reflected beams (variation of about 1%).

Security hologram foil labels with a design facilitating authenticity testing: effects of mechanical bending of substrates with the glued on holograms

NASA Astrophysics Data System (ADS)

Aubrecht, Ivo

2015-05-01

Optimal design of security holograms or diffractive optically variable image devices (DOVIDs) that would be complex enough to deter counterfeiters from attempts of mimicking but contains features readily recognizable by laymen has been addressed by many experts. This paper tries to discuss effects of mechanical bending of a flexible substrate to visual appearance of a glued-on foil DOVID. Initially plane, the DOVID is deformed to a convex- or concave-shaped curved surface. Theoretical analyses and experimental results assume the surface to be a cylindrical segment and concern rainbow-type surface-relief holograms that are recorded piecewise in a photoresist material, coated on planar and non-planar substrates.

A new surface-potential-based compact model for the MoS2 field effect transistors in active matrix display applications

NASA Astrophysics Data System (ADS)

Cao, Jingchen; Peng, Songang; Liu, Wei; Wu, Quantan; Li, Ling; Geng, Di; Yang, Guanhua; Ji, Zhouyu; Lu, Nianduan; Liu, Ming

2018-02-01

We present a continuous surface-potential-based compact model for molybdenum disulfide (MoS2) field effect transistors based on the multiple trapping release theory and the variable-range hopping theory. We also built contact resistance and velocity saturation models based on the analytical surface potential. This model is verified with experimental data and is able to accurately predict the temperature dependent behavior of the MoS2 field effect transistor. Our compact model is coded in Verilog-A, which can be implemented in a computer-aided design environment. Finally, we carried out an active matrix display simulation, which suggested that the proposed model can be successfully applied to circuit design.

Tree-shaped fractal meta-surface with left-handed characteristics for absorption application

NASA Astrophysics Data System (ADS)

Faruque, M. R. I.; Hasan, M. M.; Islam, M. T.

2018-02-01

A tri-band fractal meta-surface absorber composed of metallic branches of a tree connected with a straight metal strip has been presented in this paper for high absorption application. The proposed tree-shaped structure shows resonance in C-, X-, and Ku-bands and left-handed characteristics in 14.15 GHz. The dimension of the tree-shaped meta-surface single unit cell structure is 9 × 9 mm2 and the effective medium ratio is 5.50. In addition, the designed absorber structure shows absorption above 84%, whereas the absorber structure printed on epoxy resin fiber substrate material. The FIT-based CST-MWS has been utilized for the design, simulation, and analysis purposes. Fabrication is also done for the experimental validation.

[Experimental study on a novel esophageal prosthesis made of composite biomaterials].

PubMed

Qin, Xiong; Xu, Zhi-fei; Shi, Hong-can; Zhao, Xue-wei; Sun, Kang; Gao, Xiang-yang

2003-07-01

To design and develop a novel esophageal prosthesis by selecting appropriate biomaterials, developing special manufacturing techniques, and investigating the feasibility of replacement of cervical esophagus in mongrel dogs. In accordance with the requirements of ideal esophageal substitutes, we designed a new type of esophageal prostheses. The inner stent were made with polyurethane of medical grade, and the outer surface of the prosthesis was coated with collagen-chitosan sponge. The silicone tube was used as a control. Thirteen adult mongrel dogs that were divided into two groups were used to establish the experimental models. In the experimental group (n = 8), the esophageal prostheses were completely incorporated with the native esophagus and adherent to the surrounding host connective tissues. Epithelial linings of varying degrees were formed on the luminal surface, and complete epithelization was seen in 1 month postoperatively. The granulation at the sites of the anastomosis in this group was less significant than that of the control group. One dog has been surviving for 12 months up to now without any complications. In the control group (n = 5), esophageal epithelial was not observed on the luminal surface, constriction of the regenerated esophagus progressed and all the dogs died within 2 months after operation. These observations suggest that this esophageal prosthesis made of composite biomaterials has high biocompatibility and potential for long-segment esophageal reconstruction, which is promising for the clinical repair of esophageal defects.

Modeling and optimization of trihalomethanes formation potential of surface water (a drinking water source) using Box-Behnken design.

PubMed

Singh, Kunwar P; Rai, Premanjali; Pandey, Priyanka; Sinha, Sarita

2012-01-01

The present research aims to investigate the individual and interactive effects of chlorine dose/dissolved organic carbon ratio, pH, temperature, bromide concentration, and reaction time on trihalomethanes (THMs) formation in surface water (a drinking water source) during disinfection by chlorination in a prototype laboratory-scale simulation and to develop a model for the prediction and optimization of THMs levels in chlorinated water for their effective control. A five-factor Box-Behnken experimental design combined with response surface and optimization modeling was used for predicting the THMs levels in chlorinated water. The adequacy of the selected model and statistical significance of the regression coefficients, independent variables, and their interactions were tested by the analysis of variance and t test statistics. The THMs levels predicted by the model were very close to the experimental values (R(2) = 0.95). Optimization modeling predicted maximum (192 μg/l) TMHs formation (highest risk) level in water during chlorination was very close to the experimental value (186.8 ± 1.72 μg/l) determined in laboratory experiments. The pH of water followed by reaction time and temperature were the most significant factors that affect the THMs formation during chlorination. The developed model can be used to determine the optimum characteristics of raw water and chlorination conditions for maintaining the THMs levels within the safe limit.

Achieving optimal SERS through enhanced experimental design

PubMed Central

Fisk, Heidi; Westley, Chloe; Turner, Nicholas J.

2016-01-01

One of the current limitations surrounding surface‐enhanced Raman scattering (SERS) is the perceived lack of reproducibility. SERS is indeed challenging, and for analyte detection, it is vital that the analyte interacts with the metal surface. However, as this is analyte dependent, there is not a single set of SERS conditions that are universal. This means that experimental optimisation for optimum SERS response is vital. Most researchers optimise one factor at a time, where a single parameter is altered first before going onto optimise the next. This is a very inefficient way of searching the experimental landscape. In this review, we explore the use of more powerful multivariate approaches to SERS experimental optimisation based on design of experiments and evolutionary computational methods. We particularly focus on colloidal‐based SERS rather than thin film preparations as a result of their popularity. © 2015 The Authors. Journal of Raman Spectroscopy published by John Wiley & Sons, Ltd. PMID:27587905

Flow in a centrifugal fan impeller at off-design conditions

NASA Astrophysics Data System (ADS)

Wright, T.; Tzou, K. T. S.; Madhavan, S.

1984-06-01

A fully three-dimensional finite element analysis of inviscid, incompressible blade channel flow is the basis of the present study of both predicted and measured surface velocity and pressure distributions in the internal flow channels of a centrifugal fan impeller, for volume flow rates of 80-125 percent the design flow rate. The experimental results made extensive use of blade and sidewall surface pressure taps installed in a scale model of an airfoil-bladed centrifugal fan impeller. The results obtained illustrate the ability of both flow analyses to predict the dominant features of the impeller flow field, including peak blade surface velocities and adverse gradients at flows far from the design point. Insight is also gained into the limiting channel diffusion values for typical centrifugal cascade performance, together with the influence of viscous effects, as seen in deviations from ideal flow predictions.

A new optimal sliding mode controller design using scalar sign function.

PubMed

Singla, Mithun; Shieh, Leang-San; Song, Gangbing; Xie, Linbo; Zhang, Yongpeng

2014-03-01

This paper presents a new optimal sliding mode controller using the scalar sign function method. A smooth, continuous-time scalar sign function is used to replace the discontinuous switching function in the design of a sliding mode controller. The proposed sliding mode controller is designed using an optimal Linear Quadratic Regulator (LQR) approach. The sliding surface of the system is designed using stable eigenvectors and the scalar sign function. Controller simulations are compared with another existing optimal sliding mode controller. To test the effectiveness of the proposed controller, the controller is implemented on an aluminum beam with piezoceramic sensor and actuator for vibration control. This paper includes the control design and stability analysis of the new optimal sliding mode controller, followed by simulation and experimental results. The simulation and experimental results show that the proposed approach is very effective. © 2013 ISA. Published by Elsevier Ltd. All rights reserved.

Numerical and experimental hydrodynamic analysis of suction cup bio-logging tag designs for marine mammals

NASA Astrophysics Data System (ADS)

Murray, Mark; Shorter, Alex; Howle, Laurens; Johnson, Mark; Moore, Michael

2012-11-01

The improvement and miniaturization of sensing technologies has made bio-logging tags, utilized for the study of marine mammal behavior, more practical. These sophisticated sensing packages require a housing which protects the electronics from the environment and provides a means of attachment to the animal. The hydrodynamic forces on these housings can inadvertently remove the tag or adversely affect the behavior or energetics of the animal. A modification to the original design of a suction cup bio-logging tag housing was desired to minimize the adverse forces. In this work, hydrodynamic loading of two suction cup tag designs, original and modified designs, were analyzed using computational fluid dynamics (CFD) models and validated experimentally. Overall, the simulation and experimental results demonstrated that a tag housing that minimized geometric disruptions to the flow reduced drag forces, and that a tag housing with a small frontal cross-sectional area close to the attachment surface reduced lift forces. Preliminary results from experimental work with a common dolphin cadaver indicates that the suction cups used to attach the tags to the animal provide sufficient attachment force to resist failure at predicted drag and lift forces in 10 m/s flow.

Patchy particles made by colloidal fusion

NASA Astrophysics Data System (ADS)

Gong, Zhe; Hueckel, Theodore; Yi, Gi-Ra; Sacanna, Stefano

2017-10-01

Patches on the surfaces of colloidal particles provide directional information that enables the self-assembly of the particles into higher-order structures. Although computational tools can make quantitative predictions and can generate design rules that link the patch motif of a particle to its internal microstructure and to the emergent properties of the self-assembled materials, the experimental realization of model systems of particles with surface patches (or `patchy' particles) remains a challenge. Synthetic patchy colloidal particles are often poor geometric approximations of the digital building blocks used in simulations and can only rarely be manufactured in sufficiently high yields to be routinely used as experimental model systems. Here we introduce a method, which we refer to as colloidal fusion, for fabricating functional patchy particles in a tunable and scalable manner. Using coordination dynamics and wetting forces, we engineer hybrid liquid-solid clusters that evolve into particles with a range of patchy surface morphologies on addition of a plasticizer. We are able to predict and control the evolutionary pathway by considering surface-energy minimization, leading to two main branches of product: first, spherical particles with liquid surface patches, capable of forming curable bonds with neighbouring particles to assemble robust supracolloidal structures; and second, particles with a faceted liquid compartment, which can be cured and purified to yield colloidal polyhedra. These findings outline a scalable strategy for the synthesis of patchy particles, first by designing their surface patterns by computer simulation, and then by recreating them in the laboratory with high fidelity.

Aerial Refueling Simulator Validation Using Operational Experimentation and Response Surface Methods with Time Series Responses

DTIC Science & Technology

2013-03-21

10 2.3 Time Series Response Data ................................................................................. 12 2.4 Comparison of Response...to 12 evaluating the efficiency of the parameter estimates. In the past, the most popular form of response surface design used the D-optimality...as well. A model can refer to almost anything in math , statistics, or computer science. It can be any “physical, mathematical, or logical

A flowing liquid lithium limiter for the Experimental Advanced Superconducting Tokamak

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ren, J.; Zuo, G. Z.; Hu, J. S.

2015-02-15

A program involving the extensive and systematic use of lithium (Li) as a “first,” or plasma-facing, surface in Tokamak fusion research devices located at Institute of Plasma Physics, Chinese Academy of Sciences, was started in 2009. Many remarkable results have been obtained by the application of Li coatings in Experimental Advanced Superconducting Tokamak (EAST) and liquid Li limiters in the HT-7 Tokamak—both located at the institute. In furtherance of the lithium program, a flowing liquid lithium (FLiLi) limiter system has been designed and manufactured for EAST. The design of the FLiLi limiter is based on the concept of a thinmore » flowing film which was previously tested in HT-7. Exploiting the capabilities of the existing material and plasma evaluation system on EAST, the limiter will be pre-wetted with Li and mechanically translated to the edge of EAST during plasma discharges. The limiter will employ a novel electro-magnetic pump which is designed to drive liquid Li flow from a collector at the bottom of limiter into a distributor at its top, and thus supply a continuously flowing liquid Li film to the wetted plasma-facing surface. This paper focuses on the major design elements of the FLiLi limiter. In addition, a simulation of incoming heat flux has shown that the distribution of heat flux on the limiter surface is acceptable for a future test of power extraction on EAST.« less

Performance Prediction Relationships for AM2 Airfield Matting Developed from Full-Scale Accelerated Testing and Laboratory Experimentation

DTIC Science & Technology

2018-01-01

work, the prevailing methods used to predict the performance of AM2 were based on the CBR design procedure for flexible pavements using a small number...suitable for design and evaluation frameworks currently used for airfield pavements and matting systems. DISCLAIMER: The contents of this report...methods used to develop the equivalency curves equated the mat-surfaced area to an equivalent thickness of flexible pavement using the CBR design

Comparative hydraulics of two fishery research circular tanks and recommendations for control of experimental bias

USGS Publications Warehouse

Odeh, M.; Schrock, R.M.; Gannam, A.

2003-01-01

Hydraulic characteristics inside two research circular tanks (1.5-m and 1.2-m diameter) with the same volume of water were studied to understand how they might affect experimental bias by influencing the behavior and development of juvenile fish. Water velocities inside each tank were documented extensively and flow behavior studied. Surface inflow to the 1.5-m tank created a highly turbulent and aerated surface, and produced unevenly distributed velocities within the tank. A low-flow velocity, or "dead" zone, persisted just upstream of the surface inflow. A single submerged nozzle in the 1.2-m tank created uniform flow and did not cause undue turbulence or introduce air. Flow behavior in the 1.5-m tank is believed to have negatively affected the feeding behavior and physiological development of a group of juvenile fall chinook salmon, Oncorhynchus tshawytscha. A new inflow nozzle design provided comparable flow behavior regardless of tank size and water depth. Maintaining similar hydraulic conditions inside tanks used for various biological purposes, including fish research, would minimize experimental bias caused by differences in flow behavior. Other sources of experimental bias are discussed and recommendations given for reporting and control of experimental conditions in fishery research tank experiments.

Plasma treatment of polyethylene tubes in continuous regime using surface dielectric barrier discharge with water electrodes

NASA Astrophysics Data System (ADS)

Galmiz, Oleksandr; Zemánek, Miroslav; Pavliňák, David; Černák, Mirko

2018-05-01

Combining the surface dielectric barrier discharges generated in contact with water based electrolytes, as the discharge electrodes, we have designed a new type of surface electric discharge, generating thin layers of plasma which propagate along the treated polymer surfaces. The technique was aimed to achieve uniform atmospheric pressure plasma treatment of polymeric tubes and other hollow bodies. The results presented in this work show the possibility of such system to treat outer surface of polymer materials in a continuous mode. The technical details of experimental setup are discussed as well as results of treatment of polyethylene tubes are shown.

Experimental method for testing diffraction properties of reflection waveguide holograms.

PubMed

Xie, Yi; Kang, Ming-Wu; Wang, Bao-Ping

2014-07-01

Waveguide holograms' diffraction properties include peak wavelength and diffraction efficiency, which play an important role in determining their display performance. Based on the record and reconstruction theory of reflection waveguide holograms, a novel experimental method for testing diffraction properties is introduced and analyzed in this paper, which uses a plano-convex lens optically contacted to the surface of the substrate plate of the waveguide hologram, so that the diffracted light beam can be easily detected. Then an experiment is implemented. The designed reconstruction wavelength of the test sample is 530 nm, and its diffraction efficiency is 100%. The experimental results are a peak wavelength of 527.7 nm and a diffraction efficiency of 94.1%. It is shown that the tested value corresponds well with the designed value.

Wetting and Dewetting Transitions on Submerged Superhydrophobic Surfaces with Hierarchical Structures.

PubMed

Wu, Huaping; Yang, Zhe; Cao, Binbin; Zhang, Zheng; Zhu, Kai; Wu, Bingbing; Jiang, Shaofei; Chai, Guozhong

2017-01-10

The wetting transition on submersed superhydrophobic surfaces with hierarchical structures and the influence of trapped air on superhydrophobic stability are predicted based on the thermodynamics and mechanical analyses. The dewetting transition on the hierarchically structured surfaces is investigated, and two necessary thermodynamic conditions and a mechanical balance condition for dewetting transition are proposed. The corresponding thermodynamic phase diagram of reversible transition and the critical reversed pressure well explain the experimental results reported previously. Our theory provides a useful guideline for precise controlling of breaking down and recovering of superhydrophobicity by designing superhydrophobic surfaces with hierarchical structures under water.

Frequency splitter based on the directional emission from surface modes in dielectric photonic crystal structures.

PubMed

Tasolamprou, Anna C; Zhang, Lei; Kafesaki, Maria; Koschny, Thomas; Soukoulis, Costas M

2015-06-01

We demonstrate the numerical design and the experimental validation of frequency dependent directional emission from a dielectric photonic crystal structure. The wave propagates through a photonic crystal line-defect waveguide, while a surface layer at the termination of the photonic crystal enables the excitation of surface modes and a subsequent grating layer transforms the surface energy into outgoing propagating waves of the form of a directional beam. The angle of the beam is controlled by the frequency and the structure operates as a frequency splitter in the intermediate and far field region.

Frequency splitter based on the directional emission from surface modes in dielectric photonic crystal structures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tasolamprou, Anna C.; Zhang, Lei; Kafesaki, Maria

2015-05-19

We demonstrate the numerical design and the experimental validation of frequency dependent directional emission from a dielectric photonic crystal structure. The wave propagates through a photonic crystal line-defect waveguide, while a surface layer at the termination of the photonic crystal enables the excitation of surface modes and a subsequent grating layer transforms the surface energy into outgoing propagating waves of the form of a directional beam. Furthermore, the angle of the beam is controlled by the frequency and the structure operates as a frequency splitter in the intermediate and far field region.

A Laboratory Experimental Study: An FBG-PVC Tube Integrated Device for Monitoring the Slip Surface of Landslides.

PubMed

Wang, Kai; Zhang, Shaojie; Chen, Jiang; Teng, Pengxiao; Wei, Fangqiang; Chen, Qiao

2017-10-30

A new detection device was designed by integrating fiber Bragg grating (FBG) and polyvinyl chloride (PVC) tube in order to monitor the slip surface of a landslide. Using this new FBG-based device, a corresponding slope model with a pre-set slip surface was designed, and seven tests with different soil properties were carried out in laboratory conditions. The FBG sensing fibers were fixed on the PVC tube to measure strain distributions of PVC tube at different elevation. Test results indicated that the PVC tube could keep deformation compatible with soil mass. The new device was able to monitor slip surface location before sliding occurrence, and the location of monitored slip surface was about 1-2 cm above the pre-set slip surface, which basically agreed with presupposition results. The monitoring results are expected to be used to pre-estimate landslide volume and provide a beneficial option for evaluating the potential impact of landslides on shipping safety in the Three Gorges area.

A Laboratory Experimental Study: An FBG-PVC Tube Integrated Device for Monitoring the Slip Surface of Landslides

PubMed Central

Zhang, Shaojie; Chen, Jiang; Teng, Pengxiao; Wei, Fangqiang; Chen, Qiao

2017-01-01

A new detection device was designed by integrating fiber Bragg grating (FBG) and polyvinyl chloride (PVC) tube in order to monitor the slip surface of a landslide. Using this new FBG-based device, a corresponding slope model with a pre-set slip surface was designed, and seven tests with different soil properties were carried out in laboratory conditions. The FBG sensing fibers were fixed on the PVC tube to measure strain distributions of PVC tube at different elevation. Test results indicated that the PVC tube could keep deformation compatible with soil mass. The new device was able to monitor slip surface location before sliding occurrence, and the location of monitored slip surface was about 1–2 cm above the pre-set slip surface, which basically agreed with presupposition results. The monitoring results are expected to be used to pre-estimate landslide volume and provide a beneficial option for evaluating the potential impact of landslides on shipping safety in the Three Gorges area. PMID:29084157

Computational Design of a Krueger Flap Targeting Conventional Slat Aerodynamics

NASA Technical Reports Server (NTRS)

Akaydin, H. Dogus; Housman, Jeffrey A.; Kiris, Cetin C.; Bahr, Christopher J.; Hutcheson, Florence V.

2016-01-01

In this study, we demonstrate the design of a Krueger flap as a substitute for a conventional slat in a high-lift system. This notional design, with the objective of matching equivalent-mission performance on aircraft approach, was required for a comparative aeroacoustic study with computational and experimental components. We generated a family of high-lift systems with Krueger flaps based on a set of design parameters. Then, we evaluated the high-lift systems using steady 2D RANS simulations to find a good match for the conventional slat, based on total lift coefficients in free-air. Finally, we evaluated the mean aerodynamics of the high-lift systems with Krueger flap and conventional slat as they were installed in an open-jet wind tunnel flow. The surface pressures predicted with the simulations agreed well with experimental results.

Component Performance Investigation of J71 Experimental Turbine. Part 2; Internal-Flow Conditions with 97-Percent-Design Stator Areas

NASA Technical Reports Server (NTRS)

Rebeske, John J., Jr.; Petrash, Donald A.

1956-01-01

An experimental investigation of the internal-flow conditions of a J71 experimental turbine equipped with 97-percent-design stator areas was conducted at equivalent design speed and near equivalent design work. The results of the investigation indicate that the stage work distribution closely approximates design, the actual distribution being 44.1, 33.4, and 22.5 percent for the first, second, and third stages, respectively. The first-, second-, and third-stage efficiencies were 0.894, 0.858, and 0.792, respectively. The first and second stages exhibited loss regions near the hub and tip at the rotor blade outlets. The hub loss region is attributed to stator secondary flows, and a contributing factor to the tip loss region may be the high design diffusion on the rotor blade suction surface near the tip. The loss in the third stage is appreciably greater than that in the first or second stage. The fact that the third rotor is unshrouded and has a nominal tip clearance of 0.120 inch may contribute to the higher loss in the tip region of the third stage.

Experimental Investigation of the Flow Field in a Transonic, Axial Flow Compressor with Respect to the Development of Blockage and Loss

NASA Technical Reports Server (NTRS)

Suder, Kenneth L.

1996-01-01

A detailed experimental investigation to understand and quantify the development of loss and blockage in the flow field of a transonic, axial flow compressor rotor has been undertaken. Detailed laser anemometer measurements were acquired upstream, within, and downstream of a transonic, axial compressor rotor operating at design and off-design conditions. The rotor was operated at 100%, 85%, 80%, and 60% of design speed which provided inlet relative Mach numbers at the blade tip of 1.48, 1.26, 1.18, and 0.89 respectively. At design speed the blockage is evaluated ahead of the rotor passage shock, downstream of the rotor passage shock, and near the trailing edge of the blade row. The blockage is evaluated in the core flow area as well as in the casing endwall region. Similarly at pm speed conditions for the cases of (1) where the rotor passage shock is much weaker than that at design speed and (2) where there is no rotor passage shock, the blockage and loss are evaluated and compared to the results at design speed. Specifically, the impact of the rotor passage shock on the blockage and loss development, pertaining to both the shock/boundary layer interactions and the shock/tip clearance flow interactions, is discussed. In addition, the blockage evaluated from the experimental data is compared to (1) an existing correlation of blockage development which was based on computational results, and (2) computational results on a limited basis. The results indicate that for this rotor the blockage in the endwall region is 2-3 times that of the core flow region and the blockage in the core flow region more than doubles when the shock strength is sufficient to separate the suction surface boundary layer. The distribution of losses in the care flow region indicate that the total loss is primarily comprised of the shock loss when the shock strength is not sufficient to separate the suction surface boundary layer. However, when the shock strength is sufficient to separate the suction surface boundary layer, the profile loss is comparable to the shock loss and can exceed the shock loss.

A new laboratory-scale experimental facility for detailed aerothermal characterizations of volumetric absorbers

NASA Astrophysics Data System (ADS)

Gomez-Garcia, Fabrisio; Santiago, Sergio; Luque, Salvador; Romero, Manuel; Gonzalez-Aguilar, Jose

2016-05-01

This paper describes a new modular laboratory-scale experimental facility that was designed to conduct detailed aerothermal characterizations of volumetric absorbers for use in concentrating solar power plants. Absorbers are generally considered to be the element with the highest potential for efficiency gains in solar thermal energy systems. The configu-ration of volumetric absorbers enables concentrated solar radiation to penetrate deep into their solid structure, where it is progressively absorbed, prior to being transferred by convection to a working fluid flowing through the structure. Current design trends towards higher absorber outlet temperatures have led to the use of complex intricate geometries in novel ceramic and metallic elements to maximize the temperature deep inside the structure (thus reducing thermal emission losses at the front surface and increasing efficiency). Although numerical models simulate the conjugate heat transfer mechanisms along volumetric absorbers, they lack, in many cases, the accuracy that is required for precise aerothermal validations. The present work aims to aid this objective by the design, development, commissioning and operation of a new experimental facility which consists of a 7 kWe (1.2 kWth) high flux solar simulator, a radiation homogenizer, inlet and outlet collector modules and a working section that can accommodate volumetric absorbers up to 80 mm × 80 mm in cross-sectional area. Experimental measurements conducted in the facility include absorber solid temperature distributions along its depth, inlet and outlet air temperatures, air mass flow rate and pressure drop, incident radiative heat flux, and overall thermal efficiency. In addition, two windows allow for the direct visualization of the front and rear absorber surfaces, thus enabling full-coverage surface temperature measurements by thermal imaging cameras. This paper presents the results from the aerothermal characterization of a siliconized silicon carbide monolithic honeycomb, conducted at realistic conditions of incident radiative power per unit mass flow rate in order to validate its operation.

Optimization of the combined ultrasonic assisted/adsorption method for the removal of malachite green by gold nanoparticles loaded on activated carbon: Experimental design

NASA Astrophysics Data System (ADS)

Roosta, M.; Ghaedi, M.; Shokri, N.; Daneshfar, A.; Sahraei, R.; Asghari, A.

2014-01-01

The present study was aimed to experimental design optimization applied to removal of malachite green (MG) from aqueous solution by ultrasound-assisted removal onto the gold nanoparticles loaded on activated carbon (Au-NP-AC). This nanomaterial was characterized using different techniques such as FESEM, TEM, BET, and UV-vis measurements. The effects of variables such as pH, initial dye concentration, adsorbent dosage (g), temperature and sonication time on MG removal were studied using central composite design (CCD) and the optimum experimental conditions were found with desirability function (DF) combined response surface methodology (RSM). Fitting the experimental equilibrium data to various isotherm models such as Langmuir, Freundlich, Tempkin and Dubinin-Radushkevich models show the suitability and applicability of the Langmuir model. Kinetic models such as pseudo -first order, pseudo-second order, Elovich and intraparticle diffusion models applicability was tested for experimental data and the second-order equation and intraparticle diffusion models control the kinetic of the adsorption process. The small amount of proposed adsorbent (0.015 g) is applicable for successful removal of MG (RE > 99%) in short time (4.4 min) with high adsorption capacity (140-172 mg g-1).

Nodal aberration theory applied to freeform surfaces

NASA Astrophysics Data System (ADS)

Fuerschbach, Kyle; Rolland, Jannick P.; Thompson, Kevin P.

2014-12-01

When new three-dimensional packages are developed for imaging optical systems, the rotational symmetry of the optical system is often broken, changing its imaging behavior and making the optical performance worse. A method to restore the performance is to use freeform optical surfaces that compensate directly the aberrations introduced from tilting and decentering the optical surfaces. In order to effectively optimize the shape of a freeform surface to restore optical functionality, it is helpful to understand the aberration effect the surface may induce. Using nodal aberration theory the aberration fields induced by a freeform surface in an optical system are explored. These theoretical predications are experimentally validated with the design and implementation of an aberration generating telescope.

Jumping-Droplet-Enhanced Condensation on Scalable Superhydrophobic Nanostructured Surfaces

DOE Office of Scientific and Technical Information (OSTI.GOV)

Miljkovic, N; Enright, R; Nam, Y

When droplets coalesce on a superhydrophobic nanostructured surface, the resulting droplet can jump from the surface due to the release of excess surface energy. If designed properly, these superhydrophobic nanostructured surfaces can not only allow for easy droplet removal at micrometric length scales during condensation but also promise to enhance heat transfer performance. However, the rationale for the design of an ideal nanostructured surface as well as heat transfer experiments demonstrating the advantage of this jumping behavior are lacking. Here, we show that silanized copper oxide surfaces created via a simple fabrication method can achieve highly efficient jumping-droplet condensation heatmore » transfer. We experimentally demonstrated a 25% higher overall heat flux and 30% higher condensation heat transfer coefficient compared to state-of-the-art hydrophobic condensing surfaces at low supersaturations (<1.12). This work not only shows significant condensation heat transfer enhancement but also promises a low cost and scalable approach to increase efficiency for applications such as atmospheric water harvesting and dehumidification. Furthermore, the results offer insights and an avenue to achieve high flux superhydrophobic condensation.« less

Experimental demonstration of a metal-dielectric metamaterial refractive index sensor

NASA Astrophysics Data System (ADS)

Li, Shengyong; Ai, Xiaochuan; Wu, Ronghua; Chen, Jiajun

2018-03-01

A metamaterial equipment is designed and experimental verified in the near-infrared with two reflectivity dips. The metamaterial equipment shows independent of polarization. Simulated results indicate that the reflectivity dip is excited by the coupling of localized surface plasmon (LSP) modes. The metamaterial equipment can work as a refractive index detection sensor with high figure of merit (FOM) value. This proposed metamaterial sensor can be applied in detecting different biochemical liquid.

Observation of plasmonic dipolar anti-bonding mode in silver nanoring structures.

PubMed

Ye, Jian; Van Dorpe, Pol; Lagae, Liesbet; Maes, Guido; Borghs, Gustaaf

2009-11-18

We report on a clear experimental observation of the plasmonic dipolar anti-bonding resonance in silver nanorings. The data can be explained effectively by the plasmon hybridization model, which is confirmed by the numerical calculations of the electromagnetic field and surface charge distribution profiles. The experimental demonstration of the plasmon hybridization model indicates its usefulness as a valuable tool to understand, design and predict optical properties of metallic nanostructures.

Observation of plasmonic dipolar anti-bonding mode in silver nanoring structures

NASA Astrophysics Data System (ADS)

Ye, Jian; Van Dorpe, Pol; Lagae, Liesbet; Maes, Guido; Borghs, Gustaaf

2009-11-01

We report on a clear experimental observation of the plasmonic dipolar anti-bonding resonance in silver nanorings. The data can be explained effectively by the plasmon hybridization model, which is confirmed by the numerical calculations of the electromagnetic field and surface charge distribution profiles. The experimental demonstration of the plasmon hybridization model indicates its usefulness as a valuable tool to understand, design and predict optical properties of metallic nanostructures.

Noise characteristics of upper surface blown configurations: Summary

NASA Technical Reports Server (NTRS)

Reddy, N. N.; Gibson, J. S.

1978-01-01

A systematic experimental program was conducted to develop a data base for the noise and related flow characteristics of upper surface blown configurations. The effect of various geometric and flow parameters was investigated experimentally. The dominant noise was identified from the measured flow and noise characteristics to be generated downstream of the trailing edge. The possibilities of noise reduction techniques were explored. An upper surface blown (USB) noise prediction program was developed to calculate noise levels at any point and noise contours (footprints). Using this noise prediction program and a cruise performance data base, aircraft design studies were conducted to integrate low noise and good performance characteristics. A theory was developed for the noise from the highly sheared layer of a trailing edge wake. Theoretical results compare favorably with the measured noise of the USB model.

Unsteady loads due to propulsive lift configurations. Part D: The development of an experimental facility for the investigation of scaling effects on propulsive lift configurations

NASA Technical Reports Server (NTRS)

Haviland, J. K.; Herling, W. W.

1978-01-01

The design and construction of an experimental facility for the investigation of scaling effects in propulsive lift configurations are described. The facility was modeled after an existing full size NASA facility which consisted of a coaxial turbofan jet engine with a rectangular nozzle in a blown surface configuration. The flow field of the model facility was examined with and without a simulated wing surface in place at several locations downstream of the nozzle exit plane. Emphasis was placed on obtaining pressure measurements which were made with static probes and surface pressure ports connected via plastic tubing to condenser microphones for fluctuating measurements. Several pressure spectra were compared with those obtained from the NASA facility, and were used in a preliminary evaluation of scaling laws.

Role of urban surface roughness in road-deposited sediment build-up and wash-off

NASA Astrophysics Data System (ADS)

Zhao, Hongtao; Jiang, Qian; Xie, Wenxia; Li, Xuyong; Yin, Chengqing

2018-05-01

Urban road surface roughness is one of the most important factors in estimation of surface runoff loads caused by road-deposited sediment (RDS) wash-off and design of its control measures. However, because of a lack of experimental data to distinguish the role of surface roughness, the effects of surface roughness on RDS accumulation and release are not clear. In this study, paired asphalt and concrete road surfaces and rainfall simulation designs were used to distinguish the role of surface roughness in RDS build-up and wash-off. Our results showed that typical asphalt surfaces often have higher depression depths than typical concrete surfaces, indicating that asphalt surfaces are relatively rougher than concrete surface. Asphalt surfaces can retain a larger RDS amount, relative higher percentage of coarser particles, larger RDS wash-off loads, and lower wash-off percentage, than concrete surfaces. Surface roughness has different effects in RDS motilities with different particle sizes during rainfall runoff, and the settleable particles (44-149 μm) were notably influenced by it. Furthermore, the first flush phenomenon tended to be greater on relatively smooth surfaces than relatively rough surfaces. Overall, surface roughness plays an important role in influencing the complete process of RDS build-up and wash-off on different road characteristics.

The influence of surface-active agents in gas mixture on the intensity of jet condensation

NASA Astrophysics Data System (ADS)

Yezhov, YV; Okhotin, VS

2017-11-01

The report presents: the methodology of calculation of contact condensation of steam from the steam-gas mixture into the stream of water, taking into account: the mass flow of steam through the boundary phase, particularly the change in turbulent transport properties near the interface and their connection to the interface perturbations due to the surface tension of the mixture; the method of calculation of the surface tension at the interface water - a mixture of fluorocarbon vapor and water, based on the previously established analytical methods we calculate the surface tension for simple one - component liquid-vapor systems. The obtained analytical relation to calculate the surface tension of the mixture is a function of temperature and volume concentration of the fluorocarbon gas in the mixture and is true for all sizes of gas molecules. On the newly created experimental stand is made verification of experimental studies to determine the surface tension of pure substances: water, steam, C3F8 pair C3F8, produced the first experimental data on surface tension at the water - a mixture of water vapor and fluorocarbon C3F8. The obtained experimental data allow us to refine the values of the two constants used in the calculated model of the surface tension of the mixture. Experimental study of jet condensation was carried out with the flow in the zone of condensation of different gases. The condensation process was monitored by measurement of consumption of water flowing from the nozzle, and the formed condensate. When submitting C3F8, there was a noticeable, intensification condensation process compared with the condensation of pure water vapor. The calculation results are in satisfactory agreement with the experimental data on surface tension of the mixture and steam condensation from steam-gas mixture. Analysis of calculation results shows that the presence of surfactants in the condensation zone affects the partial vapor pressure on the interfacial surface, and the thermal conductivity of the liquid jet. The first circumstance leads to deterioration of the condensation process, the second to the intensification of this process. There is obviously an optimum value of concentration of the additive surfactants to the vapour when the condensation process is maximum. According to the developed design methodology contact condensation can evaluate these optimum conditions, their practical effect in the field study.

Defining Dose across Different Experimental Designs: Fiber Equivalent Diameter and Surface Area

EPA Science Inventory

Inhaled fibers (elongated bio-durable particles) of all lengths have been shown to induce pathological responses, but different sizes are respirable in different species. To be able to accurately assess the health effects observed in toxicological or epidemiological studies,...

Ignition of combustible fluids by heated surfaces

NASA Astrophysics Data System (ADS)

Bennett, Joseph Michael

The ignition of flammable fluids leaking onto hot machinery components is a common cause of fires and property loss to society. For example, the U.S. Air Force has over 100 engine fires per year. There is a comparable number in the civilian air fleet. Many of these fires are due to ruptured fuel, oil or hydraulic lines impinging on hot engine components. Also, over 500,000 vehicle fires occur each year on U.S. roads. Many of these are due to leaking fluids onto hot exhaust manifolds or other exhaust components. The design of fire protection systems for aircraft and road vehicles must take into account the problems of hot surface ignition as well as re-ignition that can occur once the fire is initially extinguished. The lack of understanding of ignition and re-ignition results in heavy, high-capacity fire extinguishers to address the fire threat. It is desired to better understand the mechanisms that control this phenomenon, and exploit this understanding in producing machinery designs that can mitigate this threat. The purpose of this effort is to gain a fundamental understanding of ignition by heated surfaces. This is done by performing experimental measurements on the impingement of vertical streams of combustible fluids onto horizontal heated surfaces, and then determine the mechanisms that control the process, in terms of physical, controllable parameters (such as fuel type, flow rate and surface temperature). An initial exhaustive review of the literature revealed a small sample of pertinent findings of previous investigators, focused on droplet ignition. Boiling modes present during contact with the heated surface were also shown to control evaporation rates and ignition delays, in addition to surface temperatures and fluid properties. An experimental apparatus was designed and constructed to create the scenario of interest in a controllable fashion, with a 20 cm horizontal heated plate with variable heating supply. Fuels were applied as streams ranging from 0.67 ml/sec to 9.5 ml/sec. Heptane, hexadecane, dodecane and kerosene were the fuels investigated in the study, and experiments were performed over a range of surface temperatures. Of the 388 fuel impingement experiments performed, 226 resulted in ignition events. Of these, 124 were classified as "airborne" ignitions, where spontaneous ignition occurred up to 60 cm above the surface. A model was derived as a predictor of ignition delays observed in these experiments, based upon a fuel evaporation rate-dominated process. This model, which utilized information derived from prior Nusselt number heat transfer correlations and simple plume models, exhibited a high degree of successful correlation with experimental data. This model was sufficiently robust to be applied to all the fuels studied, and all boiling modes (nucleate, transition and boiling) and flow rates. This facilitated a means of predicting ignition delay times based upon fundamental operating parameters of fuel type, flow rate and surface temperature, and assist in the design of fire-safe systems.

Mirrors design, analysis and manufacturing of the 550mm Korsch telescope experimental model

NASA Astrophysics Data System (ADS)

Huang, Po-Hsuan; Huang, Yi-Kai; Ling, Jer

2017-08-01

In 2015, NSPO (National Space Organization) began to develop the sub-meter resolution optical remote sensing instrument of the next generation optical remote sensing satellite which follow-on to FORMOSAT-5. Upgraded from the Ritchey-Chrétien Cassegrain telescope optical system of FORMOSAT-5, the experimental optical system of the advanced optical remote sensing instrument was enhanced to an off-axis Korsch telescope optical system which consists of five mirrors. It contains: (1) M1: 550mm diameter aperture primary mirror, (2) M2: secondary mirror, (3) M3: off-axis tertiary mirror, (4) FM1 and FM2: two folding flat mirrors, for purpose of limiting the overall volume, reducing the mass, and providing a long focal length and excellent optical performance. By the end of 2015, we implemented several important techniques including optical system design, opto-mechanical design, FEM and multi-physics analysis and optimization system in order to do a preliminary study and begin to develop and design these large-size lightweight aspheric mirrors and flat mirrors. The lightweight mirror design and opto-mechanical interface design were completed in August 2016. We then manufactured and polished these experimental model mirrors in Taiwan; all five mirrors ware completed as spherical surfaces by the end of 2016. Aspheric figuring, assembling tests and optical alignment verification of these mirrors will be done with a Korsch telescope experimental structure model in 2018.

An experimental and theoretical investigation into the ``worm-hole'' effect

NASA Astrophysics Data System (ADS)

Zhao, Liang; Su, Jiancang; Zhang, Xibo; Pan, Yafeng; Wang, Limin; Fang, Jinpeng; Sun, Xu; Li, Rui; Zeng, Bo; Cheng, Jie

2013-08-01

On a nanosecond time scale, solid insulators abnormally fail in bulk rather than on surface, which is termed as the "worm-hole" effect. By using a generator with adjustable output pulse width and dozens of organic glass (PMMA) and polystyrene (PS) samples, experiments to verify this effect are conducted. The results show that under short pulses of 10 ns, all the samples fail due to bulk breakdown, whereas when the pulse width is tuned to a long pulse of 7 μs, the samples fail as a result of surface flashover. The experimental results are interpreted by analyzing the conditions for the bulk breakdown and the surface flashover. It is found that under short pulses, the flashover threshold would be as high as the bulk breakdown strength (EBD) and the flashover time delay (td) would be longer than the pulse width (τ), both of which make the dielectrics' cumulative breakdown occur easily; whereas under long pulses, that Ef is much lower than EBD and td is smaller than τ is advantageous to the occurrence of the surface flashover. In addition, a general principle on solid insulation design under short pulse condition is proposed based on the experimental results and the theoretical analysis.

Treatment of dyeing wastewater by TiO2/H2O2/UV process: experimental design approach for evaluating total organic carbon (TOC) removal efficiency.

PubMed

Lee, Seung-Mok; Kim, Young-Gyu; Cho, Il-Hyoung

2005-01-01

Optimal operating conditions in order to treat dyeing wastewater were investigated by using the factorial design and responses surface methodology (RSM). The experiment was statistically designed and carried out according to a 22 full factorial design with four factorial points, three center points, and four axial points. Then, the linear and nonlinear regression was applied on the data by using SAS package software. The independent variables were TiO2 dosage, H2O2 concentration and total organic carbon (TOC) removal efficiency of dyeing wastewater was dependent variable. From the factorial design and responses surface methodology (RSM), maximum removal efficiency (85%) of dyeing wastewater was obtained at TiO2 dosage (1.82 gL(-1)), H2O2 concentration (980 mgL(-1)) for oxidation reaction (20 min).

Non-uniform Erosion and Surface Evolution of Plasma-Facing Materials for Electric Propulsion

NASA Astrophysics Data System (ADS)

Matthes, Christopher Stanley Rutter

A study regarding the surface evolution of plasma-facing materials is presented. Experimental efforts were performed in the UCLA Pi Facility, designed to explore the physics of plasma-surface interactions. The influence of micro-architectured surfaces on the effects of plasma sputtering is compared with the response of planar samples. Ballistic deposition of sputtered atoms as a result of geometric re-trapping is observed. This provides a self-healing mechanism of micro-architectured surfaces during plasma exposure. This result is quantified using a QCM to demonstrate the evolution of surface features and the corresponding influence on the instantaneous sputtering yield. The sputtering yield of textured molybdenum samples exposed to 300 eV Ar plasma is found to be roughly 1 of the 2 corresponding value of flat samples, and increases with ion fluence. Mo samples exhibited a sputtering yield initially as low as 0.22+/-8%, converging to 0.4+/-8% at high fluence. Although the yield is dependent on the initial surface structure, it is shown to be transient, reaching a steady-state value that is independent of initial surface conditions. A continuum model of surface evolution resulting from sputtering, deposition and surface diffusion is also derived to resemble the damped Kuramoto-Sivashinsky (KS) equation of non-linear dynamics. Linear stability analysis of the evolution equation provides an estimate of the selected wavelength, and its dependence on the ion energy and angle of incidence. The analytical results are confirmed by numerical simulations of the equation with a Fast Fourier Transform method. It is shown that for an initially flat surface, small perturbations lead to the evolution of a selected surface pattern that has nano- scale wavelength. When the surface is initially patterned by other means, the final resulting pattern is a competition between the "templated" pattern and the "self-organized" structure. Potential future routes of research are also discussed, corresponding to a design analysis of the current experimental study.

Doehlert experimental design applied to optimization of light emitting textile structures

NASA Astrophysics Data System (ADS)

Oguz, Yesim; Cochrane, Cedric; Koncar, Vladan; Mordon, Serge R.

2016-07-01

A light emitting fabric (LEF) has been developed for photodynamic therapy (PDT) for the treatment of dermatologic diseases such as Actinic Keratosis (AK). A successful PDT requires homogenous and reproducible light with controlled power and wavelength on the treated skin area. Due to the shape of the human body, traditional PDT with external light sources is unable to deliver homogenous light everywhere on the skin (head vertex, hand, etc.). For better light delivery homogeneity, plastic optical fibers (POFs) have been woven in textile in order to emit laterally the injected light. The previous studies confirmed that the light power could be locally controlled by modifying the radius of POF macro-bendings within the textile structure. The objective of this study is to optimize the distribution of macro-bendings over the LEF surface in order to increase the light intensity (mW/cm2), and to guarantee the best possible light deliver homogeneity over the LEF which are often contradictory. Fifteen experiments have been carried out with Doehlert experimental design involving Response Surface Methodology (RSM). The proposed models are fitted to the experimental data to enable the optimal set up of the warp yarns tensions.

Experimental design and response surface modelling for optimization of vat dye from water by nano zero valent iron (NZVI).

PubMed

Arabi, Simin; Sohrabi, Mahmoud Reza

2013-01-01

In this study, NZVI particles was prepared and studied for the removal of vat green 1 dye from aqueous solution. A four-factor central composite design (CCD) combined with response surface modeling (RSM) to evaluate the combined effects of variables as well as optimization was employed for maximizing the dye removal by prepared NZVI based on 30 different experimental data obtained in a batch study. Four independent variables, viz. NZVI dose (0.1-0.9 g/L), pH (1.5-9.5), contact time (20-100 s), and initial dye concentration (10-50 mg/L) were transform to coded values and quadratic model was built to predict the responses. The significant of independent variables and their interactions were tested by the analysis of variance (ANOVA). Adequacy of the model was tested by the correlation between experimental and predicted values of the response and enumeration of prediction errors. The ANOVA results indicated that the proposed model can be used to navigate the design space. Optimization of the variables for maximum adsorption of dye by NZVI particles was performed using quadratic model. The predicted maximum adsorption efficiency (96.97%) under the optimum conditions of the process variables (NZVI dose 0.5 g/L, pH 4, contact time 60 s, and initial dye concentration 30 mg/L) was very close to the experimental value (96.16%) determined in batch experiment. In the optimization, R2 and R2adj correlation coefficients for the model were evaluated as 0.95 and 0.90, respectively.

Highly Efficient Design-of-Experiments Methods for Combining CFD Analysis and Experimental Data

NASA Technical Reports Server (NTRS)

Anderson, Bernhard H.; Haller, Harold S.

2009-01-01

It is the purpose of this study to examine the impact of "highly efficient" Design-of-Experiments (DOE) methods for combining sets of CFD generated analysis data with smaller sets of Experimental test data in order to accurately predict performance results where experimental test data were not obtained. The study examines the impact of micro-ramp flow control on the shock wave boundary layer (SWBL) interaction where a complete paired set of data exist from both CFD analysis and Experimental measurements By combining the complete set of CFD analysis data composed of fifteen (15) cases with a smaller subset of experimental test data containing four/five (4/5) cases, compound data sets (CFD/EXP) were generated which allows the prediction of the complete set of Experimental results No statistical difference were found to exist between the combined (CFD/EXP) generated data sets and the complete Experimental data set composed of fifteen (15) cases. The same optimal micro-ramp configuration was obtained using the (CFD/EXP) generated data as obtained with the complete set of Experimental data, and the DOE response surfaces generated by the two data sets were also not statistically different.

Surface normal coupling to multiple-slot and cover-slotted silicon nanocrystalline waveguides and ring resonators

NASA Astrophysics Data System (ADS)

Covey, John; Chen, Ray T.

2014-03-01

Grating couplers are ideal for coupling into the tightly confined propagation modes of semiconductor waveguides. In addition, nonlinear optics has benefited from the sub-diffraction limit confinement of horizontal slot waveguides. By combining these two advancements, slot-based nonlinear optics with mode areas less than 0.02 μm2 can become as routine as twisting fiber connectors together. Surface normal fiber alignment to a chip is also highly desirable from time, cost, and manufacturing considerations. To meet these considerable design challenges, a custom genetic algorithm is created which, starting from purely random designs, creates a unique four stage grating coupler for two novel horizontal slot waveguide platforms. For horizontal multiple-slot waveguides filled with silicon nanocrystal, a theoretical fiber-towaveguide coupling efficiency of 68% is obtained. For thin silicon waveguides clad with optically active silicon nanocrystal, known as cover-slot waveguides, a theoretical fiber-to-waveguide coupling efficiency of 47% is obtained, and 1 dB and 3 dB theoretical bandwidths of 70 nm and 150 nm are obtained, respectively. Both waveguide platforms are fabricated from scratch, and their respective on-chip grating couplers are experimentally measured from a standard single mode fiber array that is mounted surface normally. The horizontal multiple-slot grating coupler achieved an experimental 60% coupling efficiency, and the horizontal cover-slot grating coupler achieved an experimental 38.7% coupling efficiency, with an extrapolated 1 dB bandwidth of 66 nm. This report demonstrates the promise of genetic algorithm-based design by reducing to practice the first large bandwidth vertical grating coupler to a novel silicon nanocrystal horizontal cover-slot waveguide.

Operator Localization of Virtual Objects

NASA Technical Reports Server (NTRS)

Ellis, Stephen R.; Menges, Brian M.; Null, Cynthia H. (Technical Monitor)

1998-01-01

Errors in the localization of nearby virtual objects presented via see-through, helmet mounted displays are examined as a function of viewing conditions and scene content. Monocular, biocular or stereoscopic presentation of the virtual objects, accommodation (required focus), subjects'age, and the position of physical surfaces are examined. Nearby physical surfaces are found to introduce localization errors that differ depending upon the other experimental factors. The apparent physical size and transparency of the virtual objects and physical surfaces respectively are also influenced by their relative position when superimposed. Design implications are discussed.

Electrostatic propulsion beam divergence effects on spacecraft surfaces, volume 2

NASA Technical Reports Server (NTRS)

Hall, D. F.

1973-01-01

The third phase of a program to develop understanding of and tolerance-level criteria for the deleterious effects of electrostatic rocket exhaust (Cs, Cs(+), Hg, Hg(+)) and materials of rocket construction impinging on typical classes of spacecraft (S/C) surfaces was completed. Models of ion engine effluents and models describing the degradation of S/C surfaces by these effluents are presented. Experimental data from previous phases are summarized and Phase 2 data and analysis are presented in detail. The spacecraft design implications of ion engine contaminants are discussed.

Guiding, bending, and splitting of coupled defect surface modes in a surface-wave photonic crystal

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gao, Zhen; Gao, Fei; Zhang, Baile, E-mail: blzhang@ntu.edu.sg

2016-01-25

We experimentally demonstrate a type of waveguiding mechanism for coupled surface-wave defect modes in a surface-wave photonic crystal. Unlike conventional spoof surface plasmon waveguides, waveguiding of coupled surface-wave defect modes is achieved through weak coupling between tightly localized defect cavities in an otherwise gapped surface-wave photonic crystal, as a classical wave analogue of tight-binding electronic wavefunctions in solid state lattices. Wave patterns associated with the high transmission of coupled defect surface modes are directly mapped with a near-field microwave scanning probe for various structures including a straight waveguide, a sharp corner, and a T-shaped splitter. These results may find usemore » in the design of integrated surface-wave devices with suppressed crosstalk.« less

A response surface methodology based damage identification technique

NASA Astrophysics Data System (ADS)

Fang, S. E.; Perera, R.

2009-06-01

Response surface methodology (RSM) is a combination of statistical and mathematical techniques to represent the relationship between the inputs and outputs of a physical system by explicit functions. This methodology has been widely employed in many applications such as design optimization, response prediction and model validation. But so far the literature related to its application in structural damage identification (SDI) is scarce. Therefore this study attempts to present a systematic SDI procedure comprising four sequential steps of feature selection, parameter screening, primary response surface (RS) modeling and updating, and reference-state RS modeling with SDI realization using the factorial design (FD) and the central composite design (CCD). The last two steps imply the implementation of inverse problems by model updating in which the RS models substitute the FE models. The proposed method was verified against a numerical beam, a tested reinforced concrete (RC) frame and an experimental full-scale bridge with the modal frequency being the output responses. It was found that the proposed RSM-based method performs well in predicting the damage of both numerical and experimental structures having single and multiple damage scenarios. The screening capacity of the FD can provide quantitative estimation of the significance levels of updating parameters. Meanwhile, the second-order polynomial model established by the CCD provides adequate accuracy in expressing the dynamic behavior of a physical system.

Experimental Analysis of Displacements and Shears at the Surface on Contact between Two Loaded Bodies,

DTIC Science & Technology

1980-07-01

thin bars are extended. The complete solution is presented in graphs for the use of designers . The theoretical development is correlated with experiments...The concept of "coefficient of efficiency" is introduced to evaluate the degree of optimization. An ideal design of the inside boundary of a tube...efficiency coefficient is increased from 0.59 to 0.95. Tests with a brittle material show an increase in strength of 20Z. An ideal design of the boundary of

Development and Design Application of Rigidized Surface Insulation Thermal Protection Systems, Volume 1. [for the space shuttle

NASA Technical Reports Server (NTRS)

1972-01-01

Materials and design technology of the all-silica LI-900 rigid surface insulation (RSI) thermal protection system (TPS) concept for the shuttle spacecraft is presented. All results of contract development efforts are documented. Engineering design and analysis of RSI strain arrestor plate material selections, sizing, and weight studies are reported. A shuttle prototype test panel was designed, analyzed, fabricated, and delivered. Thermophysical and mechanical properties of LI-900 were experimentally established and reported. Environmental tests, including simulations of shuttle loads represented by thermal response, turbulent duct, convective cycling, and chemical tolerance tests are described and results reported. Descriptions of material test samples and panels fabricated for testing are included. Descriptions of analytical sizing and design procedures are presented in a manner formulated to allow competent engineering organizations to perform rational design studies. Results of parametric studies involving material and system variables are reported. Material performance and design data are also delineated.

Optimal color design of psychological counseling room by design of experiments and response surface methodology.

PubMed

Liu, Wenjuan; Ji, Jianlin; Chen, Hua; Ye, Chenyu

2014-01-01

Color is one of the most powerful aspects of a psychological counseling environment. Little scientific research has been conducted on color design and much of the existing literature is based on observational studies. Using design of experiments and response surface methodology, this paper proposes an optimal color design approach for transforming patients' perception into color elements. Six indices, pleasant-unpleasant, interesting-uninteresting, exciting-boring, relaxing-distressing, safe-fearful, and active-inactive, were used to assess patients' impression. A total of 75 patients participated, including 42 for Experiment 1 and 33 for Experiment 2. 27 representative color samples were designed in Experiment 1, and the color sample (L = 75, a = 0, b = -60) was the most preferred one. In Experiment 2, this color sample was set as the 'central point', and three color attributes were optimized to maximize the patients' satisfaction. The experimental results show that the proposed method can get the optimal solution for color design of a counseling room.

Optimal Color Design of Psychological Counseling Room by Design of Experiments and Response Surface Methodology

PubMed Central

Chen, Hua; Ye, Chenyu

2014-01-01

Color is one of the most powerful aspects of a psychological counseling environment. Little scientific research has been conducted on color design and much of the existing literature is based on observational studies. Using design of experiments and response surface methodology, this paper proposes an optimal color design approach for transforming patients’ perception into color elements. Six indices, pleasant-unpleasant, interesting-uninteresting, exciting-boring, relaxing-distressing, safe-fearful, and active-inactive, were used to assess patients’ impression. A total of 75 patients participated, including 42 for Experiment 1 and 33 for Experiment 2. 27 representative color samples were designed in Experiment 1, and the color sample (L = 75, a = 0, b = -60) was the most preferred one. In Experiment 2, this color sample was set as the ‘central point’, and three color attributes were optimized to maximize the patients’ satisfaction. The experimental results show that the proposed method can get the optimal solution for color design of a counseling room. PMID:24594683

Analysis of experimental results of the inlet for the NASA hypersonic research engine aerothermodynamic integration model. [wind tunnel tests of ramjet engine hypersonic inlets

NASA Technical Reports Server (NTRS)

Andrews, E. H., Jr.; Mackley, E. A.

1976-01-01

An aerodynamic engine inlet analysis was performed on the experimental results obtained at nominal Mach numbers of 5, 6, and 7 from the NASA Hypersonic Research Engine (HRE) Aerothermodynamic Integration Model (AIM). Incorporation on the AIM of the mixed-compression inlet design represented the final phase of an inlet development program of the HRE Project. The purpose of this analysis was to compare the AIM inlet experimental results with theoretical results. Experimental performance was based on measured surface pressures used in a one-dimensional force-momentum theorem. Results of the analysis indicate that surface static-pressure measurements agree reasonably well with theoretical predictions except in the regions where the theory predicts large pressure discontinuities. Experimental and theoretical results both based on the one-dimensional force-momentum theorem yielded inlet performance parameters as functions of Mach number that exhibited reasonable agreement. Previous predictions of inlet unstart that resulted from pressure disturbances created by fuel injection and combustion appeared to be pessimistic.

Superomniphobic Surfaces for Military Applications: Nano- and Micro-Fabrication Methods. Chapter 1: Lithographic Fabrication of Surfaces with Different Microgeometries and Investigation of Their Wetting Behaviour

DTIC Science & Technology

2011-01-01

plus important, comparativement à une échelle plus large. Les résultats indiquent qu’un effet de cette nature est attribuable à des facteurs...par un angle de contact à l’avancement plus petit et un angle de contact au retrait plus important, comparativement à une échelle plus large. Les...Methods ............................................................................................................ 10 3.1 Experimental Design

Combined Homogeneous Surface Diffusion Model - Design of experiments approach to optimize dye adsorption considering both equilibrium and kinetic aspects.

PubMed

Muthukkumaran, A; Aravamudan, K

2017-12-15

Adsorption, a popular technique for removing azo dyes from aqueous streams, is influenced by several factors such as pH, initial dye concentration, temperature and adsorbent dosage. Any strategy that seeks to identify optimal conditions involving these factors, should take into account both kinetic and equilibrium aspects since they influence rate and extent of removal by adsorption. Hence rigorous kinetics and accurate equilibrium models are required. In this work, the experimental investigations pertaining to adsorption of acid orange 10 dye (AO10) on activated carbon were carried out using Central Composite Design (CCD) strategy. The significant factors that affected adsorption were identified to be solution temperature, solution pH, adsorbent dosage and initial solution concentration. Thermodynamic analysis showed the endothermic nature of the dye adsorption process. The kinetics of adsorption has been rigorously modeled using the Homogeneous Surface Diffusion Model (HSDM) after incorporating the non-linear Freundlich adsorption isotherm. Optimization was performed for kinetic parameters (color removal time and surface diffusion coefficient) as well as the equilibrium affected response viz. percentage removal. Finally, the optimum conditions predicted were experimentally validated. Copyright © 2017 Elsevier Ltd. All rights reserved.

A megawatt-level surface wave oscillator in Y-band with large oversized structure driven by annular relativistic electron beam.

PubMed

Wang, Jianguo; Wang, Guangqiang; Wang, Dongyang; Li, Shuang; Zeng, Peng

2018-05-03

High power vacuum electronic devices of millimeter wave to terahertz regime are attracting extensive interests due to their potential applications in science and technologies. In this paper, the design and experimental results of a powerful compact oversized surface wave oscillator (SWO) in Y-band are presented. The cylindrical slow wave structure (SWS) with rectangular corrugations and large diameter about 6.8 times the radiation wavelength is proposed to support the surface wave interacting with annular relativistic electron beam. By choosing appropriate beam parameters, the beam-wave interaction takes place near the π-point of TM 01 mode dispersion curve, giving high coupling impedance and temporal growth rate compared with higher TM 0n modes. The fundamental mode operation of the device is verified by the particle-in-cell (PIC) simulation results, which also indicate its capability of tens of megawatts power output in the Y-band. Finally, a compact experimental setup is completed to validate our design. Measurement results show that a terahertz pulse with frequency in the range of 0.319-0.349 THz, duration of about 2 ns and radiation power of about 2.1 MW has been generated.

Design, integration and preliminary results of the IXV Catalysis experiment

NASA Astrophysics Data System (ADS)

Viladegut, Alan; Panerai, F.; Chazot, O.; Pichon, T.; Bertrand, P.; Verdy, C.; Coddet, C.

2017-06-01

The CATalytic Experiment (CATE) is an in-flight demonstration of catalysis effects at the surface of thermal protection materials. A high-catalytic coating was applied over the baseline ceramic material on the windward side of the intermediate experimental vehicle (IXV). The temperature jump due to different catalytic activities was detected during re-entry through measurements made with near-surface thermocouples on the windward side of the vehicle. The experiment aimed at contributing to the development and validation of gas/surface interaction models for re-entry applications. The present paper summarizes the design of CATE and its integration on the windward side of the IXV. Results of a qualification campaign at the Plasmatron facility of the von Karman Institute for Fluid Dynamics are presented. They provided an experimental evidence of the temperature jump at the low-to-high catalytic interface of the heat shield under aerothermal conditions relevant to the actual IXV flight. These tests also gave confidence so that the high-catalytic patch would not endanger the integrity of the vehicle and the safety of the mission. A preliminary assessment of flight data from the thermocouple measurements shows consistency with results of the qualification tests.

Surface topography acquisition method for double-sided near-right-angle structured surfaces based on dual-probe wavelength scanning interferometry.

PubMed

Zhang, Tao; Gao, Feng; Jiang, Xiangqian

2017-10-02

This paper proposes an approach to measure double-sided near-right-angle structured surfaces based on dual-probe wavelength scanning interferometry (DPWSI). The principle and mathematical model is discussed and the measurement system is calibrated with a combination of standard step-height samples for both probes vertical calibrations and a specially designed calibration artefact for building up the space coordinate relationship of the dual-probe measurement system. The topography of the specially designed artefact is acquired by combining the measurement results with white light scanning interferometer (WLSI) and scanning electron microscope (SEM) for reference. The relative location of the two probes is then determined with 3D registration algorithm. Experimental validation of the approach is provided and the results show that the method is able to measure double-sided near-right-angle structured surfaces with nanometer vertical resolution and micrometer lateral resolution.

A validated computational model for the design of surface textures in full-film lubricated sliding

NASA Astrophysics Data System (ADS)

Schuh, Jonathon; Lee, Yong Hoon; Allison, James; Ewoldt, Randy

2016-11-01

Our recent experimental work showed that asymmetry is needed for surface textures to decrease friction in full-film lubricated sliding (thrust bearings) with Newtonian fluids; textures reduce the shear load and produce a separating normal force. The sign of the separating normal force is not predicted by previous 1-D theories. Here we model the flow with the Reynolds equation in cylindrical coordinates, numerically implemented with a pseudo-spectral method. The model predictions match experiments, rationalize the sign of the normal force, and allow for design of surface texture geometry. To minimize sliding friction with angled cylindrical textures, an optimal angle of asymmetry β exists. The optimal angle depends on the film thickness but not the sliding velocity within the applicable range of the model. The model has also been used to optimize generalized surface texture topography while satisfying manufacturability constraints.

Theoretical studies on the mechanical behavior of granular materials under very low intergranular stresses

NASA Technical Reports Server (NTRS)

French, Kenneth W., Jr.

1986-01-01

The salient aspects of the theoretical modeling of a conventional triaxial test (CTC) of a cohesionless granular medium with stress and strain rate loading are described. Included are a controllable gravitational body force and provision for low confining pressure and/or very low intergranular stress. The modeling includes rational, analytic, and numerical phases, all in various stages of development. The numerical evolutions of theoretical models will be used in final design stages and in the analysis of the experimental data. In this the experimental design stage, it is of special interest to include in the candidate considerations every anomaly found in preliminary terrestrial experimentation. Most of the anomalies will be eliminated by design or enhanced for measurement as the project progresses. The main aspect of design being not the physical apparatus but the type and trajectories of loading elected. The major considerations that have been treated are: appearance and growth of local surface aberrations, stress-power coefficients, strain types, optical strain, radial bead migration, and measures of rotation for the proper stress flux.

Decolorization and mineralization of Diarylide Yellow 12 (PY12) by photo-Fenton process: the Response Surface Methodology as the optimization tool.

PubMed

GilPavas, Edison; Dobrosz-Gómez, Izabela; Gómez-García, Miguel Ángel

2012-01-01

The Response Surface Methodology (RSM) was applied as a tool for the optimization of the operational conditions of the photo-degradation of highly concentrated PY12 wastewater, resulting from a textile industry located in the suburbs of Medellin (Colombia). The Box-Behnken experimental Design (BBD) was chosen for the purpose of response optimization. The photo-Fenton process was carried out in a laboratory-scale batch photo-reactor. A multifactorial experimental design was proposed, including the following variables: the initial dyestuff concentration, the H(2)O(2) and the Fe(+2) concentrations, as well as the UV wavelength radiation. The photo-Fenton process performed at the optimized conditions resulted in ca. 100% of dyestuff decolorization, 92% of COD and 82% of TOC degradation. A kinetic study was accomplished, including the identification of some intermediate compounds generated during the oxidation process. The water biodegradability reached a final DBO(5)/DQO = 0.86 value.

Optimization by response surface methodology of lutein recovery from paprika leaves using accelerated solvent extraction.

PubMed

Kang, Jae-Hyun; Kim, Suna; Moon, BoKyung

2016-08-15

In this study, we used response surface methodology (RSM) to optimize the extraction conditions for recovering lutein from paprika leaves using accelerated solvent extraction (ASE). The lutein content was quantitatively analyzed using a UPLC equipped with a BEH C18 column. A central composite design (CCD) was employed for experimental design to obtain the optimized combination of extraction temperature (°C), static time (min), and solvent (EtOH, %). The experimental data obtained from a twenty sample set were fitted to a second-order polynomial equation using multiple regression analysis. The adjusted coefficient of determination (R(2)) for the lutein extraction model was 0.9518, and the probability value (p=0.0000) demonstrated a high significance for the regression model. The optimum extraction conditions for lutein were temperature: 93.26°C, static time: 5 min, and solvent: 79.63% EtOH. Under these conditions, the predicted extraction yield of lutein was 232.60 μg/g. Copyright © 2016 Elsevier Ltd. All rights reserved.

Choice of crystal surface finishing for a dual-ended readout depth-of-interaction (DOI) detector.

PubMed

Fan, Peng; Ma, Tianyu; Wei, Qingyang; Yao, Rutao; Liu, Yaqiang; Wang, Shi

2016-02-07

The objective of this study was to choose the crystal surface finishing for a dual-ended readout (DER) DOI detector. Through Monte Carlo simulations and experimental studies, we evaluated 4 crystal surface finishing options as combinations of crystal surface polishing (diffuse or specular) and reflector (diffuse or specular) options on a DER detector. We also tested one linear and one logarithm DOI calculation algorithm. The figures of merit used were DOI resolution, DOI positioning error, and energy resolution. Both the simulation and experimental results show that (1) choosing a diffuse type in either surface polishing or reflector would improve DOI resolution but degrade energy resolution; (2) crystal surface finishing with a diffuse polishing combined with a specular reflector appears a favorable candidate with a good balance of DOI and energy resolution; and (3) the linear and logarithm DOI calculation algorithms show overall comparable DOI error, and the linear algorithm was better for photon interactions near the ends of the crystal while the logarithm algorithm was better near the center. These results provide useful guidance in DER DOI detector design in choosing the crystal surface finishing and DOI calculation methods.

Variable curvature mirror having variable thickness: design and fabrication

NASA Astrophysics Data System (ADS)

Zhao, Hui; Xie, Xiaopeng; Xu, Liang; Ding, Jiaoteng; Shen, Le; Gong, Jie

2017-10-01

Variable curvature mirror (VCM) can change its curvature radius dynamically and is usually used to correct the defocus and spherical aberration caused by thermal lens effect to improve the output beam quality of high power solid-state laser. Recently, the probable application of VCM in realizing non-moving element optical zoom imaging in visible band has been paid much attention. The basic requirement for VCM lies in that it should provide a large enough saggitus variation and still maintains a high enough surface figure at the same time. Therefore in this manuscript, by combing the pressurization based actuation with a variable thickness mirror design, the purpose of obtaining large saggitus variation and maintaining quite good surface figure accuracy at the same time could be achieved. A prototype zoom mirror with diameter of 120mm and central thickness of 8mm is designed, fabricated and tested. Experimental results demonstrate that the zoom mirror having an initial surface figure accuracy superior to 1/80λ could provide bigger than 36um saggitus variation and after finishing the curvature variation its surface figure accuracy could still be superior to 1/40λ with the spherical aberration removed, which proves that the effectiveness of the theoretical design.

Investigating Cell-Material Interactions of Magnetospirillum magneticum as an Approach for Probing Submerged Surface Structural Integrity

DTIC Science & Technology

2012-07-01

developed a microscope- based , offset Helmholtz coil system with a custom-designed microcontroller. We have developed a microfabrication approach for...implemented an experimental model system using ferromagnetic beads. We have applied direct and frequency based magnetic fields for controlling magnetotactic...fields. Expanded Accomplishments We have developed a microscope- based , offset Helmholtz coil system with a custom- designed microcontroller. To be

Computational design of cyclic peptides for the customized oriented immobilization of globular proteins.

PubMed

Soler, Miguel A; Rodriguez, Alex; Russo, Anna; Adedeji, Abimbola Feyisara; Dongmo Foumthuim, Cedrix J; Cantarutti, Cristina; Ambrosetti, Elena; Casalis, Loredana; Corazza, Alessandra; Scoles, Giacinto; Marasco, Daniela; Laio, Alessandro; Fortuna, Sara

2017-01-25

The oriented immobilization of proteins, key for the development of novel responsive biomaterials, relies on the availability of effective probes. These are generally provided by standard approaches based on in vivo maturation and in vitro selection of antibodies and/or aptamers. These techniques can suffer technical problems when a non-immunogenic epitope needs to be targeted. Here we propose a strategy to circumvent this issue by in silico design. In our method molecular binders, in the form of cyclic peptides, are computationally evolved by stochastically exploring their sequence and structure space to identify high-affinity peptides for a chosen epitope of a target globular protein: here a solvent-exposed site of β2-microglobulin (β2m). Designed sequences were screened by explicit solvent molecular dynamics simulations (MD) followed by experimental validation. Five candidates gave dose-response surface plasmon resonance signals with dissociation constants in the micromolar range. One of them was further analyzed by means of isothermal titration calorimetry, nuclear magnetic resonance, and 250 ns of MD. Atomic-force microscopy imaging showed that this peptide is able to immobilize β2m on a gold surface. In short, we have shown by a variety of experimental techniques that it is possible to capture a protein through an epitope of choice by computational design.

Development, optimization, and in vitro characterization of dasatinib-loaded PEG functionalized chitosan capped gold nanoparticles using Box-Behnken experimental design.

PubMed

Adena, Sandeep Kumar Reddy; Upadhyay, Mansi; Vardhan, Harsh; Mishra, Brahmeshwar

2018-03-01

The purpose of this research study was to develop, optimize, and characterize dasatinib loaded polyethylene glycol (PEG) stabilized chitosan capped gold nanoparticles (DSB-PEG-Ch-GNPs). Gold (III) chloride hydrate was reduced with chitosan and the resulting nanoparticles were coated with thiol-terminated PEG and loaded with dasatinib (DSB). Plackett-Burman design (PBD) followed by Box-Behnken experimental design (BBD) were employed to optimize the process parameters. Polynomial equations, contour, and 3D response surface plots were generated to relate the factors and responses. The optimized DSB-PEG-Ch-GNPs were characterized by FTIR, XRD, HR-SEM, EDX, TEM, SAED, AFM, DLS, and ZP. The results of the optimized DSB-PEG-Ch-GNPs showed particle size (PS) of 24.39 ± 1.82 nm, apparent drug content (ADC) of 72.06 ± 0.86%, and zeta potential (ZP) of -13.91 ± 1.21 mV. The responses observed and the predicted values of the optimized process were found to be close. The shape and surface morphology studies showed that the resulting DSB-PEG-Ch-GNPs were spherical and smooth. The stability and in vitro drug release studies confirmed that the optimized formulation was stable at different conditions of storage and exhibited a sustained drug release of the drug of up to 76% in 48 h and followed Korsmeyer-Peppas release kinetic model. A process for preparing gold nanoparticles using chitosan, anchoring PEG to the particle surface, and entrapping dasatinib in the chitosan-PEG surface corona was optimized.

Optimization of Extraction Conditions for Phenolic Acids from the Leaves of Melissa officinalis L. Using Response Surface Methodology

PubMed Central

Yoo, Guijae; Lee, Il Kyun; Park, Seonju; Kim, Nanyoung; Park, Jun Hyung; Kim, Seung Hyun

2018-01-01

Background: Melissa officinalis L. is a well-known medicinal plant from the family Lamiaceae, which is distributed throughout Eastern Mediterranean region and Western Asia. Objective: In this study, response surface methodology (RSM) was utilized to optimize the extraction conditions for bioactive compounds from the leaves of M. officinalis L. Materials and Methods: A Box–Behnken design (BBD) was utilized to evaluate the effects of three independent variables, namely extraction temperature (°C), methanol concentration (%), and solvent-to-material ratio (mL/g) on the responses of the contents of caffeic acid and rosmarinic acid. Results: Regression analysis showed a good fit of the experimental data. The optimal condition was obtained at extraction temperature 80.53°C, methanol concentration 29.89%, and solvent-to-material ratio 30 mL/g. Conclusion: These results indicate the suitability of the model employed and the successful application of RSM in optimizing the extraction conditions. This study may be useful for standardizing production quality, including improving the efficiency of large-scale extraction systems. SUMMARY The optimum conditions for the extraction of major phenolic acids from the leaves of Melissa officinalis L. were determined using response surface methodologyBox–Behnken design was utilized to evaluate the effects of three independent variablesQuadratic polynomial model provided a satisfactory description of the experimental dataThe optimized condition for simultaneous maximum contents of caffeic acid and rosmarinic acid was determined. Abbreviations used: RSM: Response surface methodology, BBD: Box–Behnken design, CA: Caffeic acid, RA: Rosmarinic acid, HPLC: High-performance liquid chromatography. PMID:29720824

Pixelated Checkerboard Metasurface for Ultra-Wideband Radar Cross Section Reduction.

PubMed

Haji-Ahmadi, Mohammad-Javad; Nayyeri, Vahid; Soleimani, Mohammad; Ramahi, Omar M

2017-09-12

In this paper we designed and fabricated a metasurface working as a radar cross section (RCS) reducer over an ultra wide band of frequency from 3.8 to 10.7 GHz. The designed metasurface is a chessboard-like surface made of alternating tiles, with each tile composed of identical unit cells. We develop a novel, simple, highly robust and fully automated approach for designing the unit cells. First, a topology optimization algorithm is used to engineer the shape of the two unit cells. The area of each unit cell is pixelated. A particle swarm optimization algorithm is applied wherein each pixel corresponds to a bit having a binary value of 1 or 0 indicating metallization or no metallization. With the objective of reducing the RCS over a specified frequency range, the optimization algorithm is then linked to a full wave three-dimensional electromagnetic simulator. To validate the design procedure, a surface was designed, fabricated and experimentally tested showing significantly enhanced performance than previous works. Additionally, angular analysis is also presented showing good stability and wide-angle behavior of the designed RCS reducer. The automated design procedure has a wide range of applications and can be easily extended to design surfaces for antennas, energy harvesters, noise mitigation in electronic circuit boards amongst others.

E-healthcare at an experimental welfare techno house in Japan.

PubMed

Tamura, Toshiyo; Kawarada, Atsushi; Nambu, Masayuki; Tsukada, Akira; Sasaki, Kazuo; Yamakoshi, Ken-Ichi

2007-01-01

An automated monitoring system for home health care has been designed for an experimental house in Japan called the Welfare Techno House (WTH). Automated electrocardiogram (ECG) measurements can be taken while in bed, in the bathtub, and on the toilet, without the subject's awareness, and without using body surface electrodes. In order to evaluate this automated health monitoring system, overnight measurements were performed to monitor health status during the daily lives of both young and elderly subjects.

Controlling surface-plasmon-polaritons launching with hot spot cylindrical waves in a metallic slit structure.

PubMed

Yao, Wenjie; Sun, Chengwei; Gong, Qihuang; Chen, Jianjun

2016-09-23

Plasmonic nanostructures, which are used to generate surface plasmon polaritons (SPPs), always involve sharp corners where the charges can accumulate. This can result in strong localized electromagnetic fields at the metallic corners, forming the hot spots. The influence of the hot spots on the propagating SPPs are investigated theoretically and experimentally in a metallic slit structure. It is found that the electromagnetic fields radiated from the hot spots, termed as the hot spot cylindrical wave (HSCW), can greatly manipulate the SPP launching in the slit structure. The physical mechanism behind the manipulation of the SPP launching with the HSCW is explicated by a semi-analytic model. By using the HSCW, unidirectional SPP launching is experimentally realized in an ultra-small metallic step-slit structure. The HSCW bridges the localized surface plasmons and the propagating surface plasmons in an integrated platform and thus may pave a new route to the design of plasmonic devices and circuits.

Experimental aerothermodynamic research of hypersonic aircraft

NASA Technical Reports Server (NTRS)

Cleary, Joseph W.

1987-01-01

The 2-D and 3-D advance computer codes being developed for use in the design of such hypersonic aircraft as the National Aero-Space Plane require comparison of the computational results with a broad spectrum of experimental data to fully assess the validity of the codes. This is particularly true for complex flow fields with control surfaces present and for flows with separation, such as leeside flow. Therefore, the objective is to provide a hypersonic experimental data base required for validation of advanced computational fluid dynamics (CFD) computer codes and for development of more thorough understanding of the flow physics necessary for these codes. This is being done by implementing a comprehensive test program for a generic all-body hypersonic aircraft model in the NASA/Ames 3.5 foot Hypersonic Wind Tunnel over a broad range of test conditions to obtain pertinent surface and flowfield data. Results from the flow visualization portion of the investigation are presented.

Experimental rig to estimate the coefficient of friction between tire and surface in airplane touchdown simulations.

PubMed

Li, Chengwei; Zhan, Liwei

2015-08-01

To estimate the coefficient of friction between tire and runway surface during airplane touchdowns, we designed an experimental rig to simulate such events and to record the impact and friction forces being executed. Because of noise in the measured signals, we developed a filtering method that is based on the ensemble empirical mode decomposition and the bandwidth of probability density function of each intrinsic mode function to extract friction and impact force signals. We can quantify the coefficient of friction by calculating the maximum values of the filtered force signals. Signal measurements are recorded for different drop heights and tire rotational speeds, and the corresponding coefficient of friction is calculated. The result shows that the values of the coefficient of friction change only slightly. The random noise and experimental artifact are the major reason of the change.

The Landscape Evolution Observatory: a large-scale controllable infrastructure to study coupled Earth-surface processes

USGS Publications Warehouse

Pangle, Luke A.; DeLong, Stephen B.; Abramson, Nate; Adams, John; Barron-Gafford, Greg A.; Breshears, David D.; Brooks, Paul D.; Chorover, Jon; Dietrich, William E.; Dontsova, Katerina; Durcik, Matej; Espeleta, Javier; Ferré, T.P.A.; Ferriere, Regis; Henderson, Whitney; Hunt, Edward A.; Huxman, Travis E.; Millar, David; Murphy, Brendan; Niu, Guo-Yue; Pavao-Zuckerman, Mitch; Pelletier, Jon D.; Rasmussen, Craig; Ruiz, Joaquin; Saleska, Scott; Schaap, Marcel; Sibayan, Michael; Troch, Peter A.; Tuller, Markus; van Haren, Joost; Zeng, Xubin

2015-01-01

Zero-order drainage basins, and their constituent hillslopes, are the fundamental geomorphic unit comprising much of Earth's uplands. The convergent topography of these landscapes generates spatially variable substrate and moisture content, facilitating biological diversity and influencing how the landscape filters precipitation and sequesters atmospheric carbon dioxide. In light of these significant ecosystem services, refining our understanding of how these functions are affected by landscape evolution, weather variability, and long-term climate change is imperative. In this paper we introduce the Landscape Evolution Observatory (LEO): a large-scale controllable infrastructure consisting of three replicated artificial landscapes (each 330 m2 surface area) within the climate-controlled Biosphere 2 facility in Arizona, USA. At LEO, experimental manipulation of rainfall, air temperature, relative humidity, and wind speed are possible at unprecedented scale. The Landscape Evolution Observatory was designed as a community resource to advance understanding of how topography, physical and chemical properties of soil, and biological communities coevolve, and how this coevolution affects water, carbon, and energy cycles at multiple spatial scales. With well-defined boundary conditions and an extensive network of sensors and samplers, LEO enables an iterative scientific approach that includes numerical model development and virtual experimentation, physical experimentation, data analysis, and model refinement. We plan to engage the broader scientific community through public dissemination of data from LEO, collaborative experimental design, and community-based model development.

Experimental design based response surface methodology optimization of ultrasonic assisted adsorption of safaranin O by tin sulfide nanoparticle loaded on activated carbon.

PubMed

Roosta, M; Ghaedi, M; Daneshfar, A; Sahraei, R

2014-03-25

In this research, the adsorption rate of safranine O (SO) onto tin sulfide nanoparticle loaded on activated carbon (SnS-NPAC) was accelerated by the ultrasound. SnS-NP-AC was characterized by different techniques such as SEM, XRD and UV-Vis measurements. The present results confirm that the ultrasound assisted adsorption method has remarkable ability to improve the adsorption efficiency. The influence of parameters such as the sonication time, adsorbent dosage, pH and initial SO concentration was examined and evaluated by central composite design (CCD) combined with response surface methodology (RSM) and desirability function (DF). Conducting adsorption experiments at optimal conditions set as 4 min of sonication time, 0.024 g of adsorbent, pH 7 and 18 mg L(-1) SO make admit to achieve high removal percentage (98%) and high adsorption capacity (50.25 mg g(-)(1)). A good agreement between experimental and predicted data in this study was observed. The experimental equilibrium data fitting to Langmuir, Freundlich, Tempkin and Dubinin-Radushkevich models show that the Langmuir model is a good and suitable model for evaluation and the actual behavior of adsorption. Kinetic evaluation of experimental data showed that the adsorption processes followed well pseudo-second-order and intraparticle diffusion models. Copyright © 2013. Published by Elsevier B.V.

Radiation Beamline Testbeds for the Simulation of Planetary and Spacecraft Environments for Human and Robotic Mission Risk Assessment

NASA Technical Reports Server (NTRS)

Wilkins, Richard

2010-01-01

The Center for Radiation Engineering and Science for Space Exploration (CRESSE) at Prairie View A&M University, Prairie View, Texas, USA, is establishing an integrated, multi-disciplinary research program on the scientific and engineering challenges faced by NASA and the international space community caused by space radiation. CRESSE focuses on space radiation research directly applicable to astronaut health and safety during future long term, deep space missions, including Martian, lunar, and other planetary body missions beyond low earth orbit. The research approach will consist of experimental and theoretical radiation modeling studies utilizing particle accelerator facilities including: 1. NASA Space Radiation Laboratory (NSRL) at Brookhaven National Laboratory; 2. Proton Synchrotron at Loma Linda University Medical Center; and 3. Los Alamos Neutron Science Center (LANSCE) at Los Alamos National Laboratory. Specifically, CRESSE investigators are designing, developing, and building experimental test beds that simulate the lunar and Martian radiation environments for experiments focused on risk assessment for astronauts and instrumentation. The testbeds have been designated the Bioastronautics Experimental Research Testbeds for Environmental Radiation Nostrum Investigations and Education (BERT and ERNIE). The designs of BERT and ERNIE will allow for a high degree of flexibility and adaptability to modify experimental configurations to simulate planetary surface environments, planetary habitats, and spacecraft interiors. In the nominal configuration, BERT and ERIE will consist of a set of experimental zones that will simulate the planetary atmosphere (Solid CO2 in the case of the Martian surface.), the planetary surface, and sub-surface regions. These experimental zones can be used for dosimetry, shielding, biological, and electronic effects radiation studies in support of space exploration missions. BERT and ERNIE are designed to be compatible with the experimental areas associated with the above facilities. CRESSE has broad expertise in space radiation in the areas of space radiation environment modeling, Monte-Carlo radiation transport modeling, space radiation instrumentation and dosimetry, radiation effects on electronics, and multi-functional composite shielding materials. The BERT and ERNIE testbeds will be utilized in individual and collaborative research incorporating this expertise. The research goal is to maximize the technical readiness level (TRL) of radiation instrumentation for human and robotic missions, optimizing the return value of CRESSE for NASA exploration and international co-operative missions. Outcomes and knowledge from research utilizing BERT and ERNIE will be applied to a variety of scientific and engineering disciplines vital for safe and reliable execution of future space exploration missions, which can be negatively impacted by the space radiation environment. The testbeds will be central to a variety of university educational activities and educational goals of NASA. Specifically, BERT and ERNIE will enhance educational opportunities in science, technology, engineering and mathematics (STEM) disciplines for engineering and science students at PVAMU, a historically black college/university. Preliminary data on prototype testbed configurations, including simulated lunar regolith (JSC-1A stimulant based on Apollo 11 samples), regolith/polyethylene composites, and dry ice, will be presented to demonstrate the usefulness of BERT and ERNIE in radiation beam line experiments.

Radiation beamline testbeds for the simulation of planetary and spacecraft environments for human and robotic mission risk assessment

NASA Astrophysics Data System (ADS)

Wilkins, Richard

The Center for Radiation Engineering and Science for Space Exploration (CRESSE) at Prairie View A&M University, Prairie View, Texas, USA, is establishing an integrated, multi-disciplinary research program on the scientific and engineering challenges faced by NASA and the inter-national space community caused by space radiation. CRESSE focuses on space radiation research directly applicable to astronaut health and safety during future long term, deep space missions, including Martian, lunar, and other planetary body missions beyond low earth orbit. The research approach will consist of experimental and theoretical radiation modeling studies utilizing particle accelerator facilities including: 1. NASA Space Radiation Laboratory (NSRL) at Brookhaven National Laboratory; 2. Proton Synchrotron at Loma Linda University Med-ical Center; and 3. Los Alamos Neutron Science Center (LANSCE) at Los Alamos National Laboratory. Specifically, CRESSE investigators are designing, developing, and building experimental test beds that simulate the lunar and Martian radiation environments for experiments focused on risk assessment for astronauts and instrumentation. The testbeds have been designated the Bioastronautics Experimental Research Testbeds for Environmental Radiation Nostrum Investigations and Education (BERT and ERNIE). The designs of BERT and ERNIE will allow for a high degree of flexibility and adaptability to modify experimental configurations to simulate planetary surface environments, planetary habitats, and spacecraft interiors. In the nominal configuration, BERT and ERIE will consist of a set of experimental zones that will simulate the planetary atmosphere (Solid CO2 in the case of the Martian surface.), the planetary surface, and sub-surface regions. These experimental zones can be used for dosimetry, shielding, biological, and electronic effects radiation studies in support of space exploration missions. BERT and ERNIE are designed to be compatible with the experimental areas associated with the above facilities. CRESSE has broad expertise in space radiation in the areas of space radiation environment modeling, Monte-Carlo radiation transport modeling, space radiation instrumentation and dosimetry, radiation effects on electronics, and multi-functional composite shielding materi-als. The BERT and ERNIE testbeds will be utilized in individual and collaborative research incorporating this expertise. The research goal is to maximize the technical readiness level (TRL) of radiation instrumentation for human and robotic missions, optimizing the return value of CRESSE for NASA exploration and international co-operative missions. Outcomes and knowledge from research utilizing BERT and ERNIE will be applied to a variety of scien-tific and engineering disciplines vital for safe and reliable execution of future space exploration missions, which can be negatively impacted by the space radiation environment. The testbeds will be central to a variety of university educational activities and educational goals of NASA. Specifically, BERT and ERNIE will enhance educational opportunities in science, technol-ogy, engineering and mathematics (STEM) disciplines for engineering and science students at PVAMU, a historically black college/university. Preliminary data on prototype testbed configurations, including simulated lunar regolith (JSC-1A stimulant based on Apollo 11 samples), regolith/polyethylene composites, and dry ice, will be presented to demonstrate the usefulness of BERT and ERNIE in radiation beam line experiments.

Supersonic, nonlinear, attached-flow wing design for high lift with experimental validation

NASA Technical Reports Server (NTRS)

Pittman, J. L.; Miller, D. S.; Mason, W. H.

1984-01-01

Results of the experimental validation are presented for the three dimensional cambered wing which was designed to achieve attached supercritical cross flow for lifting conditions typical of supersonic maneuver. The design point was a lift coefficient of 0.4 at Mach 1.62 and 12 deg angle of attack. Results from the nonlinear full potential method are presented to show the validity of the design process along with results from linear theory codes. Longitudinal force and moment data and static pressure data were obtained in the Langley Unitary Plan Wind Tunnel at Mach numbers of 1.58, 1.62, 1.66, 1.70, and 2.00 over an angle of attack range of 0 to 14 deg at a Reynolds number of 2.0 x 10 to the 6th power per foot. Oil flow photographs of the upper surface were obtained at M = 1.62 for alpha approx. = 8, 10, 12, and 14 deg.

Prediction of Cutting Force in Turning Process-an Experimental Approach

NASA Astrophysics Data System (ADS)

Thangarasu, S. K.; Shankar, S.; Thomas, A. Tony; Sridhar, G.

2018-02-01

This Paper deals with a prediction of Cutting forces in a turning process. The turning process with advanced cutting tool has a several advantages over grinding such as short cycle time, process flexibility, compatible surface roughness, high material removal rate and less environment problems without the use of cutting fluid. In this a full bridge dynamometer has been used to measure the cutting forces over mild steel work piece and cemented carbide insert tool for different combination of cutting speed, feed rate and depth of cut. The experiments are planned based on taguchi design and measured cutting forces were compared with the predicted forces in order to validate the feasibility of the proposed design. The percentage contribution of each process parameter had been analyzed using Analysis of Variance (ANOVA). Both the experimental results taken from the lathe tool dynamometer and the designed full bridge dynamometer were analyzed using Taguchi design of experiment and Analysis of Variance.

In Situ Guided Wave Structural Health Monitoring System

NASA Technical Reports Server (NTRS)

Zhao, George; Tittmann, Bernhard R.

2011-01-01

Aircraft engine rotating equipment operates at high temperatures and stresses. Noninvasive inspection of microcracks in those components poses a challenge for nondestructive evaluation. A low-cost, low-profile, high-temperature ultrasonic guided wave sensor was developed that detects cracks in situ. The transducer design provides nondestructive evaluation of structures and materials. A key feature of the sensor is that it withstands high temperatures and excites strong surface wave energy to inspect surface and subsurface cracks. The sol-gel bismuth titanate-based surface acoustic wave (SAW) sensor can generate efficient SAWs for crack inspection. The sensor is very thin (submillimeter) and can generate surface waves up to 540 C. Finite element analysis of the SAW transducer design was performed to predict the sensor behavior, and experimental studies confirmed the results. The sensor can be implemented on structures of various shapes. With a spray-coating process, the sensor can be applied to the surface of large curvatures. It has minimal effect on airflow or rotating equipment imbalance, and provides good sensitivity.

Estimation of design space for an extrusion-spheronization process using response surface methodology and artificial neural network modelling.

PubMed

Sovány, Tamás; Tislér, Zsófia; Kristó, Katalin; Kelemen, András; Regdon, Géza

2016-09-01

The application of the Quality by Design principles is one of the key issues of the recent pharmaceutical developments. In the past decade a lot of knowledge was collected about the practical realization of the concept, but there are still a lot of unanswered questions. The key requirement of the concept is the mathematical description of the effect of the critical factors and their interactions on the critical quality attributes (CQAs) of the product. The process design space (PDS) is usually determined by the use of design of experiment (DoE) based response surface methodologies (RSM), but inaccuracies in the applied polynomial models often resulted in the over/underestimation of the real trends and changes making the calculations uncertain, especially in the edge regions of the PDS. The completion of RSM with artificial neural network (ANN) based models is therefore a commonly used method to reduce the uncertainties. Nevertheless, since the different researches are focusing on the use of a given DoE, there is lack of comparative studies on different experimental layouts. Therefore, the aim of present study was to investigate the effect of the different DoE layouts (2 level full factorial, Central Composite, Box-Behnken, 3 level fractional and 3 level full factorial design) on the model predictability and to compare model sensitivities according to the organization of the experimental data set. It was revealed that the size of the design space could differ more than 40% calculated with different polynomial models, which was associated with a considerable shift in its position when higher level layouts were applied. The shift was more considerable when the calculation was based on RSM. The model predictability was also better with ANN based models. Nevertheless, both modelling methods exhibit considerable sensitivity to the organization of the experimental data set, and the use of design layouts is recommended, where the extreme values factors are more represented. Copyright © 2016 Elsevier B.V. All rights reserved.

X-33 Experimental Aeroheating at Mach 6 Using Phosphor Thermography

NASA Technical Reports Server (NTRS)

Horvath, Thomas J.; Berry, Scott A.; Hollis, Brian R.; Liechty, Derek S.; Hamilton, H. Harris, II; Merski, N. Ronald

1999-01-01

The goal of the NASA Reusable Launch Vehicle (RLV) technology program is to mature and demonstrate essential, cost effective technologies for next generation launch systems. The X-33 flight vehicle presently being developed by Lockheed Martin is an experimental Single Stage to Orbit (SSTO) demonstrator that seeks to validate critical technologies and insure applicability to a full scale RLV. As with the design of any hypersonic vehicle, the aeroheating environment is an important issue and one of the key technologies being demonstrated on X-33 is an advanced metallic Thermal Protection System (TPS). As part of the development of this TPS system, the X-33 aeroheating environment is being defined through conceptual analysis, ground based testing, and computational fluid dynamics. This report provides an overview of the hypersonic aeroheating wind tunnel program conducted at the NASA Langley Research Center in support of the ground based testing activities. Global surface heat transfer images, surface streamline patterns, and shock shapes were measured on 0.013 scale (10-in.) ceramic models of the proposed X-33 configuration in Mach 6 air. The test parametrics include angles of attack from -5 to 40 degs, unit Reynolds numbers from 1x106 to 8x106/ft, and body flap deflections of 0, 10, and 20 deg. Experimental and computational results indicate the presence of shock/shock interactions that produced localized heating on the deflected flaps and boundary layer transition on the canted fins. Comparisons of the experimental data to laminar and turbulent predictions were performed. Laminar windward heating data from the wind tunnel was extrapolated to flight surface temperatures and generally compared to within 50 deg F of flight prediction along the centerline. When coupled with the phosphor technique, this rapid extrapolation method would serve as an invaluable TPS design tool.

Experimental verification of the rainbow trapping effect in adiabatic plasmonic gratings

PubMed Central

Gan, Qiaoqiang; Gao, Yongkang; Wagner, Kyle; Vezenov, Dmitri; Ding, Yujie J.; Bartoli, Filbert J.

2011-01-01

We report the experimental observation of a trapped rainbow in adiabatically graded metallic gratings, designed to validate theoretical predictions for this unique plasmonic structure. One-dimensional graded nanogratings were fabricated and their surface dispersion properties tailored by varying the grating groove depth, whose dimensions were confirmed by atomic force microscopy. Tunable plasmonic bandgaps were observed experimentally, and direct optical measurements on graded grating structures show that light of different wavelengths in the 500–700-nm region is “trapped” at different positions along the grating, consistent with computer simulations, thus verifying the “rainbow” trapping effect. PMID:21402936

Experimental demonstration of a ferroelectric liquid crystal tunable filter for fast demodulation of FBG sensors

NASA Astrophysics Data System (ADS)

Mathews, Sunish; Semenova, Yuliya; Rajan, Ginu; Farrell, Gerald

2009-05-01

A discretely tunable Surface-Stabilized Ferroelectric Liquid Crystal based Lyot Filter, with tuning speeds in the order of microseconds, is demonstrated experimentally as a channel dropper for the demodulation of multiple Fibre Bragg Grating sensors. The 3-stage Lyot Filter designed and experimentally verified can be used together with the high-speed ratiometric wavelength measurement system employing a fibre bend loss edge filter. Such systems can be used for the demodulation of distributed Fibre Bragg Grating sensors employed in applications such as structural monitoring, industrial sensing and haptic telerobotic surgical systems.

Nanoscale effects in the characterization of viscoelastic materials with atomic force microscopy: Coupling of a quasi-three-dimensional standard linear solid model with in-plane surface interactions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Solares, Santiago D.

Significant progress has been accomplished in the development of experimental contact-mode and dynamic-mode atomic force microscopy (AFM) methods designed to measure surface material properties. However, current methods are based on one-dimensional (1D) descriptions of the tip-sample interaction forces, thus neglecting the intricacies involved in the material behavior of complex samples (such as soft viscoelastic materials) as well as the differences in material response between the surface and the bulk. In order to begin to address this gap, a computational study is presented where the sample is simulated using an enhanced version of a recently introduced model that treats the surfacemore » as a collection of standard-linear-solid viscoelastic elements. The enhanced model introduces in-plane surface elastic forces that can be approximately related to a two-dimensional (2D) Young's modulus. Relevant cases are discussed for single-and multifrequency intermittent-contact AFM imaging, with focus on the calculated surface indentation profiles and tip-sample interaction force curves, as well as their implications with regards to experimental interpretation. A variety of phenomena are examined in detail, which highlight the need for further development of more physically accurate sample models that are specifically designed for AFM simulation. As a result, a multifrequency AFM simulation tool based on the above sample model is provided as supporting information.« less

Nanoscale effects in the characterization of viscoelastic materials with atomic force microscopy: Coupling of a quasi-three-dimensional standard linear solid model with in-plane surface interactions

DOE PAGES

Solares, Santiago D.

2016-04-15

Significant progress has been accomplished in the development of experimental contact-mode and dynamic-mode atomic force microscopy (AFM) methods designed to measure surface material properties. However, current methods are based on one-dimensional (1D) descriptions of the tip-sample interaction forces, thus neglecting the intricacies involved in the material behavior of complex samples (such as soft viscoelastic materials) as well as the differences in material response between the surface and the bulk. In order to begin to address this gap, a computational study is presented where the sample is simulated using an enhanced version of a recently introduced model that treats the surfacemore » as a collection of standard-linear-solid viscoelastic elements. The enhanced model introduces in-plane surface elastic forces that can be approximately related to a two-dimensional (2D) Young's modulus. Relevant cases are discussed for single-and multifrequency intermittent-contact AFM imaging, with focus on the calculated surface indentation profiles and tip-sample interaction force curves, as well as their implications with regards to experimental interpretation. A variety of phenomena are examined in detail, which highlight the need for further development of more physically accurate sample models that are specifically designed for AFM simulation. As a result, a multifrequency AFM simulation tool based on the above sample model is provided as supporting information.« less

Modeling and simulation of protein-surface interactions: achievements and challenges.

PubMed

Ozboyaci, Musa; Kokh, Daria B; Corni, Stefano; Wade, Rebecca C

2016-01-01

Understanding protein-inorganic surface interactions is central to the rational design of new tools in biomaterial sciences, nanobiotechnology and nanomedicine. Although a significant amount of experimental research on protein adsorption onto solid substrates has been reported, many aspects of the recognition and interaction mechanisms of biomolecules and inorganic surfaces are still unclear. Theoretical modeling and simulations provide complementary approaches for experimental studies, and they have been applied for exploring protein-surface binding mechanisms, the determinants of binding specificity towards different surfaces, as well as the thermodynamics and kinetics of adsorption. Although the general computational approaches employed to study the dynamics of proteins and materials are similar, the models and force-fields (FFs) used for describing the physical properties and interactions of material surfaces and biological molecules differ. In particular, FF and water models designed for use in biomolecular simulations are often not directly transferable to surface simulations and vice versa. The adsorption events span a wide range of time- and length-scales that vary from nanoseconds to days, and from nanometers to micrometers, respectively, rendering the use of multi-scale approaches unavoidable. Further, changes in the atomic structure of material surfaces that can lead to surface reconstruction, and in the structure of proteins that can result in complete denaturation of the adsorbed molecules, can create many intermediate structural and energetic states that complicate sampling. In this review, we address the challenges posed to theoretical and computational methods in achieving accurate descriptions of the physical, chemical and mechanical properties of protein-surface systems. In this context, we discuss the applicability of different modeling and simulation techniques ranging from quantum mechanics through all-atom molecular mechanics to coarse-grained approaches. We examine uses of different sampling methods, as well as free energy calculations. Furthermore, we review computational studies of protein-surface interactions and discuss the successes and limitations of current approaches.

Bio-Inspired Control of Roughness and Trailing Edge Noise

NASA Astrophysics Data System (ADS)

Clark, Ian Andrew

Noise from fluid flow over rough surfaces is an important consideration in the design and performance of certain vehicles with high surface-area-to-perimeter ratios. A new method of noise control based on the anatomy of owls is developed and consists of fabric or fibrous canopies suspended above the surface. The method is tested experimentally and is found to reduce the total far-field noise emitted by the surface. The treatment also is found to reduce the magnitude of pressure fluctuations felt by the underlying surface by up to three orders of magnitude. Experimental investigations into the effects of geometric parameters of the canopies lead to an optimized design which maximizes noise reduction. The results obtained during the canopy experiment inspired a separate new device for the reduction of trailing edge noise. This type of noise is generated by flow past the wing of an aircraft or the blades of a wind turbine, and is a source of annoyance for those in surrounding communities. The newly developed treatment consists of small fins, or "finlets," placed near the trailing edge of an airfoil. The treatment is tested experimentally at near-full-scale conditions and is found to reduce the magnitude of far-field noise by up to 10 dB. Geometric parameters of the finlets are tested to determine the optimal size and spacing of the finlets to maximize noise reduction. Follow-up computational and experimental studies reveal the fluid mechanics behind the noise reduction by showing that the finlets produce a velocity deficit in the flow near the trailing edge and limit the magnitude and spanwise correlation lengthscale of turbulence near the trailing edge, factors which determine the magnitude of far-field noise. In a final experiment, the finlets are applied to a marine propeller and are found to reduce not only trailing edge noise, but also noise caused by the bluntness of the trailing edge. The results of this experiment show the potential usefulness of finlets to reduce noise from rotating systems, such as fans or propellers, as well as from structures which feature blunt trailing edges.

Buckling analysis of stiff thin films suspended on a substrate with tripod surface relief structure

NASA Astrophysics Data System (ADS)

Yu, Qingmin; Chen, Furong; Li, Ming; Cheng, Huanyu

2017-09-01

A wavy configuration is a simple yet powerful structural design strategy, which has been widely used in flexible and stretchable electronics. A buckled structure created from a prestretch-contact-release process represents an early effort. Substrates with engineered surface relief structures (e.g., rectangular islands or tripod structure) have enabled stretchability to the devices without sacrificing their electric performance (e.g., high areal coverage for LEDs/photovoltaics/batteries/supercapacitors). In particular, the substrate with a tripod surface relief structure allows wrinkled devices to be suspended on a soft tripod substrate. This minimizes the contact area between devices and the deformed substrate, which contributes to a significantly reduced interfacial stress/strain. To uncover the underlying mechanism of such a design, we exploit the energy method to analytically investigate the buckling and postbuckling behaviors of stiff films suspended on a stretchable polymeric substrate with a tripod surface relief structure. Validated by finite element analysis, the predications from such an analytical study elucidate the deformed profile and maximum strain in the buckled and postbuckled stiff thin device films, providing a useful toolkit for future experimental designs.

Influence of microclimate on the sustainability and reliability of weathering steel bridge

NASA Astrophysics Data System (ADS)

Kubzova, M.; Krivy, V.; Kreislova, K.

2018-04-01

Reliability and sustainability of bridge structures designed from weathering steel are influenced by the development of a sufficiently protective layer of corrosion products on its surface. The development of this protective layer is affected by several parameters such as air pollution around the bridge structure, the microclimate under the bridge, the location of surface within the bridge structure and the time of wetness. Design of structural details also significantly influences the development of the protective corrosion layer. The article deals with the results of the experimental tests carried out on the road bridge located in the city of Ostrava in the Czech Republic. The development of the protective corrosion layer on the surface of the bridge is significantly influenced by the intensive traffic under the bridge construction and the design solution of the bridge itself. Attention is focused mainly on the influence of chloride deposition on the protective function of the corrosion layer. Corrosion samples were placed on the bridge to evaluate the influence of the above-mentioned parameters. The deposition rate of chlorides spreading from the road to surfaces of the steel structure is also measured.

Superhydrophobic nanofluidic channels for enhanced electrokinetic conversion

NASA Astrophysics Data System (ADS)

Checco, Antonio; Al Hossain, Aktaruzzaman; Rahmani, Amir; Black, Charles; Doerk, Gregory; Colosqui, Carlos

2017-11-01

We present current efforts in the development of novel slit nanofluidic channels with superhydrophobic nanostructured surfaces designed to enhance hydrodynamic conductivity and improve selective transport and electrokinetic energy conversion efficiencies (mechanical-electrical energy conversion). The nanochannels are fabricated on silicon wafers using UV lithography, and their internal surface is patterned with conical nanostructures (feature size and spacing 30 nm) defined by block copolymer self-assembly and plasma etching. These nanostructures are rendered superhydrophobic by passivation with a hydrophobic silane monolayer. We experimentally characterize hydrodynamic conductivity, effective zeta potentials, and eletrokinetic flows for the patterned nanochannels, comparing against control channels with bare surfaces. Experimental observations are rationalized using both continuum-based modeling and molecular dynamics simulations. Scientific and technical knowledge produced by this work is particularly relevant for sustainable energy conversion and storage, separation processes and water treatment using nanoporous materials. The ONR Contract # N000141613178 and NSF-CBET award# 1605809.

Strain measurement of objects subjected to aerodynamic heating using digital image correlation: experimental design and preliminary results.

PubMed

Pan, Bing; Jiang, Tianyun; Wu, Dafang

2014-11-01

In thermomechanical testing of hypersonic materials and structures, direct observation and quantitative strain measurement of the front surface of a test specimen directly exposed to severe aerodynamic heating has been considered as a very challenging task. In this work, a novel quartz infrared heating device with an observation window is designed to reproduce the transient thermal environment experienced by hypersonic vehicles. The specially designed experimental system allows the capture of test article's surface images at various temperatures using an optical system outfitted with a bandpass filter. The captured images are post-processed by digital image correlation to extract full-field thermal deformation. To verify the viability and accuracy of the established system, thermal strains of a chromiumnickel austenite stainless steel sample heated from room temperature up to 600 °C were determined. The preliminary results indicate that the air disturbance between the camera and the specimen due to heat haze induces apparent distortions in the recorded images and large errors in the measured strains, but the average values of the measured strains are accurate enough. Limitations and further improvements of the proposed technique are discussed.

Generation of radio vortex beams with designable polarization using anisotropic frequency selective surface

NASA Astrophysics Data System (ADS)

Yang, Jin; Zhang, Cheng; Ma, Hui Feng; Zhao, Jie; Dai, Jun Yan; Yuan, Wei; Yang, Liu Xi; Cheng, Qiang; Cui, Tie Jun

2018-05-01

We propose a strategy to convert a linearly polarized wave from a single point source to an orbital angular momentum (OAM) wave by arbitrary polarization via an anisotropic frequency selective surface (FSS) in the microwave frequency. By tailoring the geometries of FSS elements, reflection-phases in x and y polarizations are engineered and encoded independently, which allows us to design the eventual polarization state of the generated OAM vortex beam by elaborately selecting individual coding sequences for each polarization. Two types of FSSs are designed and experimentally characterized to demonstrate the capability of OAM generation with circular and linear polarizations, respectively, showing excellent performance in a wide bandwidth from 14 to 16 GHz. This method provides opportunities for polarization multiplexing in microwave OAM communication systems.

Design and characterization of an integrated surface ion trap and micromirror optical cavity.

PubMed

Van Rynbach, Andre; Schwartz, George; Spivey, Robert F; Joseph, James; Vrijsen, Geert; Kim, Jungsang

2017-08-10

We have fabricated and characterized laser-ablated micromirrors on fused silica substrates for constructing stable Fabry-Perot optical cavities. We highlight several design features which allow these cavities to have lengths in the 250-300 μm range and be integrated directly with surface ion traps. We present a method to calculate the optical mode shape and losses of these micromirror cavities as functions of cavity length and mirror shape, and confirm that our simulation model is in good agreement with experimental measurements of the intracavity optical mode at a test wavelength of 780 nm. We have designed and tested a mechanical setup for dampening vibrations and stabilizing the cavity length, and explore applications for these cavities as efficient single-photon sources when combined with trapped Yb171 + ions.

Statistical optimization of process parameters for lipase-catalyzed synthesis of triethanolamine-based esterquats using response surface methodology in 2-liter bioreactor.

PubMed

Masoumi, Hamid Reza Fard; Basri, Mahiran; Kassim, Anuar; Abdullah, Dzulkefly Kuang; Abdollahi, Yadollah; Abd Gani, Siti Salwa; Rezaee, Malahat

2013-01-01

Lipase-catalyzed production of triethanolamine-based esterquat by esterification of oleic acid (OA) with triethanolamine (TEA) in n-hexane was performed in 2 L stirred-tank reactor. A set of experiments was designed by central composite design to process modeling and statistically evaluate the findings. Five independent process variables, including enzyme amount, reaction time, reaction temperature, substrates molar ratio of OA to TEA, and agitation speed, were studied under the given conditions designed by Design Expert software. Experimental data were examined for normality test before data processing stage and skewness and kurtosis indices were determined. The mathematical model developed was found to be adequate and statistically accurate to predict the optimum conversion of product. Response surface methodology with central composite design gave the best performance in this study, and the methodology as a whole has been proven to be adequate for the design and optimization of the enzymatic process.

Method of analysis for compressible flow through mixed-flow centrifugal impellers of arbitrary design

NASA Technical Reports Server (NTRS)

Hamrick, Joseph T; Ginsburg, Ambrose; Osborn, Walter M

1952-01-01

A method is presented for analysis of the compressible flow between the hub and the shroud of mixed-flow impellers of arbitrary design. Axial symmetry was assumed, but the forces in the meridional (hub to shroud) plane, which are derived from tangential pressure gradients, were taken into account. The method was applied to an experimental mixed-flow impeller. The analysis of the flow in the meridional plane of the impeller showed that the rotational forces, the blade curvature, and the hub-shroud profile can introduce severe velocity gradients along the hub and the shroud surfaces. Choked flow at the impeller inlet as determined by the analysis was verified by experimental results.

Hybrid surface design for robust superhydrophobicity.

PubMed

Dash, Susmita; Alt, Marie T; Garimella, Suresh V

2012-06-26

Surfaces may be rendered superhydrophobic by engineering the surface morphology to control the extent of the liquid-air interface and by the use of low-surface-energy coatings. The droplet state on a superhydrophobic surface under static and dynamic conditions may be explained in terms of the relative magnitudes of the wetting and antiwetting pressures acting at the liquid-air interface on the substrate. In this paper, we discuss the design and fabrication of hollow hybrid superhydrophobic surfaces which incorporate both communicating and noncommunicating air gaps. The surface design is analytically shown to exhibit higher capillary (or nonwetting) pressure compared to solid pillars with only communicating air gaps. Six hybrid surfaces are fabricated with different surface parameters selected such that the Cassie state of a droplet is energetically favorable. The robustness of the surfaces is tested under dynamic impingement conditions, and droplet dynamics are explained using pressure-based transitions between Cassie and Wenzel states. During droplet impingement, the effective water hammer pressure acting due to the sudden change in the velocity of the droplet is determined experimentally and is found to be at least 2 orders of magnitude less than values reported in the literature. The experiments show that the water hammer pressure depends on the surface morphology and capillary pressure of the surface. We propose that the observed reduction in shock pressure may be attributed to the presence of air gaps in the substrate. This feature allows liquid deformation and hence avoids the sudden stoppage of the droplet motion as opposed to droplet behavior on smooth surfaces.

Global Design Optimization for Aerodynamics and Rocket Propulsion Components

NASA Technical Reports Server (NTRS)

Shyy, Wei; Papila, Nilay; Vaidyanathan, Rajkumar; Tucker, Kevin; Turner, James E. (Technical Monitor)

2000-01-01

Modern computational and experimental tools for aerodynamics and propulsion applications have matured to a stage where they can provide substantial insight into engineering processes involving fluid flows, and can be fruitfully utilized to help improve the design of practical devices. In particular, rapid and continuous development in aerospace engineering demands that new design concepts be regularly proposed to meet goals for increased performance, robustness and safety while concurrently decreasing cost. To date, the majority of the effort in design optimization of fluid dynamics has relied on gradient-based search algorithms. Global optimization methods can utilize the information collected from various sources and by different tools. These methods offer multi-criterion optimization, handle the existence of multiple design points and trade-offs via insight into the entire design space, can easily perform tasks in parallel, and are often effective in filtering the noise intrinsic to numerical and experimental data. However, a successful application of the global optimization method needs to address issues related to data requirements with an increase in the number of design variables, and methods for predicting the model performance. In this article, we review recent progress made in establishing suitable global optimization techniques employing neural network and polynomial-based response surface methodologies. Issues addressed include techniques for construction of the response surface, design of experiment techniques for supplying information in an economical manner, optimization procedures and multi-level techniques, and assessment of relative performance between polynomials and neural networks. Examples drawn from wing aerodynamics, turbulent diffuser flows, gas-gas injectors, and supersonic turbines are employed to help demonstrate the issues involved in an engineering design context. Both the usefulness of the existing knowledge to aid current design practices and the need for future research are identified.

Gas/Surface Interaction Study Applied to Si-based Materials Used in Driven Micro- and Nano-scale Devices

DTIC Science & Technology

2010-01-01

science and engineering. For example, by measuring the frequency shift of sensor oscillations, one can measure gas adsorption on the sensor surface...free-molecular regime with varied gas pressure. The measurement path of the experimental setup is schematically shown in Fig. 3.1. The sensor is...excited by the electric field between the sensor and fixed electrode by means of a specially designed system of self-induced oscillations. The

Wind and Wind Stress Measurements in HiRes

DTIC Science & Technology

2008-09-30

to design the experimental system to be conducted on R /P FLIP. Data from a past experiment are also being analyzed with respect to processes...For the HiRes experiment on R /P FLIP, the air temperature profile will be measured along with wind stress, surface heat flux, sea surface...the best as it registered the lower ambient temperature. In preparation for the HiRes experiment onboard R /P FLIP a mast prototype was built in

Use of CFD Analyses to Predict Disk Friction Loss of Centrifugal Compressor Impellers

NASA Astrophysics Data System (ADS)

Cho, Leesang; Lee, Seawook; Cho, Jinsoo

To improve the total efficiency of centrifugal compressors, it is necessary to reduce disk friction loss, which is expressed as the power loss. In this study, to reduce the disk friction loss due to the effect of axial clearance and surface roughness is analyzed and methods to reduce disk friction loss are proposed. The rotating reference frame technique using a commercial CFD tool (FLUENT) is used for steady-state analysis of the centrifugal compressor. Numerical results of the CFD analysis are compared with theoretical results using established experimental empirical equations. The disk friction loss of the impeller is decreased in line with increments in axial clearance until the axial clearance between the impeller disk and the casing is smaller than the boundary layer thickness. In addition, the disk friction loss of the impeller is increased in line with the increments in surface roughness in a similar pattern as that of existing experimental empirical formulas. The disk friction loss of the impeller is more affected by the surface roughness than the change of the axial clearance. To minimize disk friction loss on the centrifugal compressor impeller, the axial clearance and the theoretical boundary layer thickness should be designed to be the same. The design of the impeller requires careful consideration in order to optimize axial clearance and minimize surface roughness.

Three-dimensional inviscid analysis of radial-turbine flow and a limited comparison with experimental data

NASA Technical Reports Server (NTRS)

Choo, Y. K.; Civinskas, K. C.

1985-01-01

The three-dimensional inviscid DENTON code is used to analyze flow through a radial-inflow turbine rotor. Experimental data from the rotor are compared with analytical results obtained by using the code. The experimental data available for comparison are the radial distributions of circumferentially averaged values of absolute flow angle and total pressure downstream of the rotor exit. The computed rotor-exit flow angles are generally underturned relative to the experimental values, which reflect the boundary-layer separation at the trailing edge and the development of wakes downstream of the rotor. The experimental rotor is designed for a higher-than-optimum work factor of 1.126 resulting in a nonoptimum positive incidence and causing a region of rapid flow adjustment and large velocity gradients. For this experimental rotor, the computed radial distribution of rotor-exit to turbine-inlet total pressure ratios are underpredicted due to the errors in the finite-difference approximations in the regions of rapid flow adjustment, and due to using the relatively coarser grids in the middle of the blade region where the flow passage is highly three-dimensional. Additional results obtained from the three-dimensional inviscid computation are also presented, but without comparison due to the lack of experimental data. These include quasi-secondary velocity vectors on cross-channel surfaces, velocity components on the meridional and blade-to-blade surfaces, and blade surface loading diagrams. Computed results show the evolution of a passage vortex and large streamline deviations from the computational streamwise grid lines. Experience gained from applying the code to a radial turbine geometry is also discussed.

Three-dimensional inviscid analysis of radial turbine flow and a limited comparison with experimental data

NASA Technical Reports Server (NTRS)

Choo, Y. K.; Civinskas, K. C.

1985-01-01

The three-dimensional inviscid DENTON code is used to analyze flow through a radial-inflow turbine rotor. Experimental data from the rotor are compared with analytical results obtained by using the code. The experimental data available for comparison are the radial distributions of circumferentially averaged values of absolute flow angle and total pressure downstream of the rotor exit. The computed rotor-exit flow angles are generally underturned relative to the experimental values, which reflect the boundary-layer separation at the trailing edge and the development of wakes downstream of the rotor. The experimental rotor is designed for a higher-than-optimum work factor of 1.126 resulting in a nonoptimum positive incidence and causing a region of rapid flow adjustment and large velocity gradients. For this experimental rotor, the computed radial distribution of rotor-exit to turbine-inlet total pressure ratios are underpredicted due to the errors in the finite-difference approximations in the regions of rapid flow adjustment, and due to using the relatively coarser grids in the middle of the blade region where the flow passage is highly three-dimensional. Additional results obtained from the three-dimensional inviscid computation are also presented, but without comparison due to the lack of experimental data. These include quasi-secondary velocity vectors on cross-channel surfaces, velocity components on the meridional and blade-to-blade surfaces, and blade surface loading diagrams. Computed results show the evolution of a passage vortex and large streamline deviations from the computational streamwise grid lines. Experience gained from applying the code to a radial turbine geometry is also discussed.

Experimental and analytical investigation of fan flow interaction with downstream struts

NASA Technical Reports Server (NTRS)

Olsen, T. L.; Ng, W. F.; Obrien, W. F., Jr.

1985-01-01

An investigation which was designed to provide insight into the fundamental aspects of fan rotor-downstream strut interaction was undertaken. High response, miniature pressure transducers were embedded in the rotor blades of an experimental fan rig. Five downstream struts were placed at several downstream locations in the discharge flow annulus of the single-stage machine. Significant interaction of the rotor blade surface pressures with the flow disturbance produced by the downstream struts was measured. Several numerical procedures for calculating the quasi-steady rotor response due to downstream flow obstructions were developed. A preliminary comparison of experimental and calculated fluctuating blade pressures on the rotor blades shows general agreement between the experimental and calculated values.

Spatial tuning of a RF frequency selective surface through origami

NASA Astrophysics Data System (ADS)

Fuchi, Kazuko; Buskohl, Philip R.; Bazzan, Giorgio; Durstock, Michael F.; Joo, James J.; Reich, Gregory W.; Vaia, Richard A.

2016-05-01

Origami devices have the ability to spatially reconfigure between 2D and 3D states through folding motions. The precise mapping of origami presents a novel method to spatially tune radio frequency (RF) devices, including adaptive antennas, sensors, reflectors, and frequency selective surfaces (FSSs). While conventional RF FSSs are designed based upon a planar distribution of conductive elements, this leaves the large design space of the out of plane dimension underutilized. We investigated this design regime through the computational study of four FSS origami tessellations with conductive dipoles. The dipole patterns showed increased resonance shift with decreased separation distances, with the separation in the direction orthogonal to the dipole orientations having a more significant effect. The coupling mechanisms between dipole neighbours were evaluated by comparing surface charge densities, which revealed the gain and loss of coupling as the dipoles moved in and out of alignment via folding. Collectively, these results provide a basis of origami FSS designs for experimental study and motivates the development of computational tools to systematically predict optimal fold patterns for targeted frequency response and directionality.

Traveling wave electrode design of electro-optically modulated coupled-cavity surface-emitting lasers.

PubMed

Zujewski, Mateusz; Thienpont, Hugo; Panajotov, Krassimir

2012-11-19

We present a novel design of an electro-optically modulated coupled-cavity vertical-cavity surface-emitting laser (CC-VCSEL) with traveling wave electrodes of the modulator cavity, which allows to overcome the RC time constant of a traditional lumped electrode structures. The CC-VCSEL optical design is based on longitudinal mode switching which has recently experimentally demonstrated a record modulation speed. We carry out segmented transmission line electrical design of the modulator cavity in order to compensate for the low impedance of the modulator section and to match the 50 Ω electrical network. We have optimized two types of highly efficient modulator structures reaching -3 dB electrical cut-off frequency of f(cut-off) = 330 GHz with maximum reflection of -22 dB in the range from f(LF) = 100 MHz to f(cut-off) and 77 - 89% modulation efficiency.

Optimization of the combined ultrasonic assisted/adsorption method for the removal of malachite green by gold nanoparticles loaded on activated carbon: experimental design.

PubMed

Roosta, M; Ghaedi, M; Shokri, N; Daneshfar, A; Sahraei, R; Asghari, A

2014-01-24

The present study was aimed to experimental design optimization applied to removal of malachite green (MG) from aqueous solution by ultrasound-assisted removal onto the gold nanoparticles loaded on activated carbon (Au-NP-AC). This nanomaterial was characterized using different techniques such as FESEM, TEM, BET, and UV-vis measurements. The effects of variables such as pH, initial dye concentration, adsorbent dosage (g), temperature and sonication time on MG removal were studied using central composite design (CCD) and the optimum experimental conditions were found with desirability function (DF) combined response surface methodology (RSM). Fitting the experimental equilibrium data to various isotherm models such as Langmuir, Freundlich, Tempkin and Dubinin-Radushkevich models show the suitability and applicability of the Langmuir model. Kinetic models such as pseudo -first order, pseudo-second order, Elovich and intraparticle diffusion models applicability was tested for experimental data and the second-order equation and intraparticle diffusion models control the kinetic of the adsorption process. The small amount of proposed adsorbent (0.015 g) is applicable for successful removal of MG (RE>99%) in short time (4.4 min) with high adsorption capacity (140-172 mg g(-1)). Copyright © 2013. Published by Elsevier B.V.

A dynamic monitoring approach for the surface morphology evolution measurement of plasma facing components by means of speckle interferometry

NASA Astrophysics Data System (ADS)

Wang, Hongbei; Cui, Xiaoqian; Feng, Chunlei; Li, Yuanbo; Zhao, Mengge; Luo, Guangnan; Ding, Hongbin

2017-11-01

Plasma Facing Components (PFCs) in a magnetically confined fusion plasma device will be exposed to high heat load and particle fluxes, and it would cause PFCs' surface morphology to change due to material erosion and redeposition from plasma wall interactions. The state of PFCs' surface condition will seriously affect the performance of long-pulse or steady state plasma discharge in a tokamak; it will even constitute an enormous threat to the operation and the safety of fusion plasma devices. The PFCs' surface morphology evolution measurement could provide important information about PFCs' real-time status or damage situation and it would help to a better understanding of the plasma wall interaction process and mechanism. Meanwhile through monitoring the distribution of dust deposition in a tokamak and providing an upper limit on the amount of loose dust, the PFCs' surface morphology measurement could indirectly contribute to keep fusion operational limits and fusion device safety. Aiming at in situ dynamic monitoring PFCs' surface morphology evolution, a laboratory experimental platform DUT-SIEP (Dalian University of Technology-speckle interferometry experimental platform) based on the speckle interferometry technique has been constructed at Dalian University of Technology (DUT) in China. With directional specific designing and focusing on the real detection condition of EAST (Experimental Advanced Superconducting Tokamak), the DUT-SIEP could realize a variable measurement range, widely increased from 0.1 μm to 300 μm, with high spatial resolution (<1 mm) and ultra-high time resolution (<2 s for EAST measuring conditions). Three main components of the DUT-SIEP are all integrated and synchronized by a time schedule control and data acquisition terminal and coupled with a three-dimensional phase unwrapping algorithm, the surface morphology information of target samples can be obtained and reconstructed in real-time. A local surface morphology of the real divertor tiles adopted from EAST has been measured, and the feasibility and reliability of this new experimental platform have been demonstrated.

Prediction of Experimental Surface Heat Flux of Thin Film Gauges using ANFIS

NASA Astrophysics Data System (ADS)

Sarma, Shrutidhara; Sahoo, Niranjan; Unal, Aynur

2018-05-01

Precise quantification of surface heat fluxes in highly transient environment is of paramount importance from the design point of view of several engineering equipment like thermal protection or cooling systems. Such environments are simulated in experimental facilities by exposing the surface with transient heat loads typically step/impulsive in nature. The surface heating rates are then determined from highly transient temperature history captured by efficient surface temperature sensors. The classical approach is to use thin film gauges (TFGs) in which temperature variations are acquired within milliseconds, thereby allowing calculation of surface heat flux, based on the theory of one-dimensional heat conduction on a semi-infinite body. With recent developments in the soft computing methods, the present study is an attempt for the application of intelligent system technique, called adaptive neuro fuzzy inference system (ANFIS) to recover surface heat fluxes from a given temperature history recorded by TFGs without having the need to solve lengthy analytical equations. Experiments have been carried out by applying known quantity of `impulse heat load' through laser beam on TFGs. The corresponding voltage signals have been acquired and surface heat fluxes are estimated through classical analytical approach. These signals are then used to `train' the ANFIS model, which later predicts output for `test' values. Results from both methods have been compared and these surface heat fluxes are used to predict the non-linear relationship between thermal and electrical properties of the gauges that are exceedingly pertinent to the design of efficient TFGs. Further, surface plots have been created to give an insight about dimensionality effect of the non-linear dependence of thermal/electrical parameters on each other. Later, it is observed that a properly optimized ANFIS model can predict the impulsive heat profiles with significant accuracy. This paper thus shows the appropriateness of soft computing technique as a practically constructive replacement for tedious analytical formulation and henceforth, effectively quantifies the modeling of TFGs.

The Influence of Roughness on Gear Surface Fatigue

NASA Technical Reports Server (NTRS)

Krantz, Timothy

2005-01-01

Gear working surfaces are subjected to repeated rolling and sliding contacts, and often designs require loads sufficient to cause eventual fatigue of the surface. This research provides experimental data and analytical tools to further the understanding of the causal relationship of gear surface roughness to surface fatigue. The research included evaluations and developments of statistical tools for gear fatigue data, experimental evaluation of the surface fatigue lives of superfinished gears with a near-mirror quality, and evaluations of the experiments by analytical methods and surface inspections. Alternative statistical methods were evaluated using Monte Carlo studies leading to a final recommendation to describe gear fatigue data using a Weibull distribution, maximum likelihood estimates of shape and scale parameters, and a presumed zero-valued location parameter. A new method was developed for comparing two datasets by extending the current methods of likelihood-ratio based statistics. The surface fatigue lives of superfinished gears were evaluated by carefully controlled experiments, and it is shown conclusively that superfinishing of gears can provide for significantly greater lives relative to ground gears. The measured life improvement was approximately a factor of five. To assist with application of this finding to products, the experimental condition was evaluated. The fatigue life results were expressed in terms of specific film thickness and shown to be consistent with bearing data. Elastohydrodynamic and stress analyses were completed to relate the stress condition to fatigue. Smooth-surface models do not adequately explain the improved fatigue lives. Based on analyses using a rough surface model, it is concluded that the improved fatigue lives of superfinished gears is due to a reduced rate of near-surface micropitting fatigue processes, not due to any reduced rate of spalling (sub-surface) fatigue processes. To complete the evaluations, surface inspection were completed. The surface topographies of the ground gears changed substantially due to running, but the topographies of the superfinished gears were essentially unchanged with running.

Investigation of phononic crystals for dispersive surface acoustic wave ozone sensors

NASA Astrophysics Data System (ADS)

Westafer, Ryan S.

The object of this research was to investigate dispersion in surface phononic crystals (PnCs) for application to a newly developed passive surface acoustic wave (SAW) ozone sensor. Frequency band gaps and slow sound already have been reported for PnC lattice structures. Such engineered structures are often advertised to reduce loss, increase sensitivity, and reduce device size. However, these advances have not yet been realized in the context of surface acoustic wave sensors. In early work, we computed SAW dispersion in patterned surface structures and we confirmed that our finite element computations of SAW dispersion in thin films and in one dimensional surface PnC structures agree with experimental results obtained by laser probe techniques. We analyzed the computations to guide device design in terms of sensitivity and joint spectral operating point. Next we conducted simulations and experiments to determine sensitivity and limit of detection for more conventional dispersive SAW devices and PnC sensors. Finally, we conducted extensive ozone detection trials on passive reflection mode SAW devices, using distinct components of the time dispersed response to compensate for the effect of temperature. The experimental work revealed that the devices may be used for dosimetry applications over periods of several days.

Control of the Pore Texture in Nanoporous Silicon via Chemical Dissolution.

PubMed

Secret, Emilie; Wu, Chia-Chen; Chaix, Arnaud; Galarneau, Anne; Gonzalez, Philippe; Cot, Didier; Sailor, Michael J; Jestin, Jacques; Zanotti, Jean-Marc; Cunin, Frédérique; Coasne, Benoit

2015-07-28

The surface and textural properties of porous silicon (pSi) control many of its physical properties essential to its performance in key applications such as optoelectronics, energy storage, luminescence, sensing, and drug delivery. Here, we combine experimental and theoretical tools to demonstrate that the surface roughness at the nanometer scale of pSi can be tuned in a controlled fashion using partial thermal oxidation followed by removal of the resulting silicon oxide layer with hydrofluoric acid (HF) solution. Such a process is shown to smooth the pSi surface by means of nitrogen adsorption, electron microscopy, and small-angle X-ray and neutron scattering. Statistical mechanics Monte Carlo simulations, which are consistent with the experimental data, support the interpretation that the pore surface is initially rough and that the oxidation/oxide removal procedure diminishes the surface roughness while increasing the pore diameter. As a specific example considered in this work, the initial roughness ξ ∼ 3.2 nm of pSi pores having a diameter of 7.6 nm can be decreased to 1.0 nm following the simple procedure above. This study allows envisioning the design of pSi samples with optimal surface properties toward a specific process.

Design of a High Viscosity Couette Flow Facility for Patterned Surface Drag Measurements

NASA Astrophysics Data System (ADS)

Johnson, Tyler; Lang, Amy

2009-11-01

Direct drag measurements can be difficult to obtain with low viscosity fluids such as air or water. In this facility, mineral oil is used as the working fluid to increase the shear stress across the surface of experimental models. A mounted conveyor creates a flow within a plexiglass tank. The experimental model of a flat or patterned surface is suspended above a moving belt. Within the gap between the model and moving belt a Couette flow with a linear velocity profile is created. PIV measurements are used to determine the exact velocities and the Reynolds numbers for each experiment. The model is suspended by bars that connect to the pillow block housing of each bearing. Drag is measured by a force gauge connected to linear roller bearings that slide along steel rods. The patterned surfaces, initially consisting of 2-D cavities, are embedded in a plexiglass plate so as to keep the total surface area constant for each experiment. First, the drag across a flat plate is measured and compared to theoretical values for laminar Couette flow. The drag for patterned surfaces is then measured and compared to a flat plate.

Design and optimization of surface profilometer based on coplanar guide rail

NASA Astrophysics Data System (ADS)

Chen, Shuai; Dai, Yifan; Hu, Hao; Tie, Guipeng

2017-10-01

In order to implement the sub-micron precision measurement, a surface profilometer which based on the coplanar guide rail is designed. This profilometer adopts the open type air floating load and is driven by the magnetic force. As to achieve sub-micron accuracy, the flatness of granite guide working face and aerodynamic block are both processed to the micron level based on the homogenization of air flotation film theory. Permanent magnet which could reduce the influence of the driving disturbance to the measurement accuracy is used as the driving part. In this paper, the bearing capacity and the air floating stiffness of air floating block are both simulated and analyzed as to optimize the design parameters firstly. The layout and magnetic force of the magnet are also simulated. According to the simulation results, type selection and the position arrangement of the magnets are then confirmed. The test results on the experimental platform show that the surface profilometer based on coplanar guide rail possess the basis for realizing the submicron precision measurement.

New valve and bonding designs for microfluidic biochips containing proteins.

PubMed

Lu, Chunmeng; Xie, Yubing; Yang, Yong; Cheng, Mark M-C; Koh, Chee-Guan; Bai, Yunling; Lee, L James; Juang, Yi-Je

2007-02-01

Two major concerns in the design and fabrication of microfluidic biochips are protein binding on the channel surface and protein denaturing during device assembly. In this paper, we describe new methods to solve these problems. A "fishbone" microvalve design based on the concept of superhydrophobicity was developed to replace the capillary valve in applications where the chip surface requires protein blocking to prevent nonspecific binding. Our experimental results show that the valve functions well in a CD-like ELISA device. The packaging of biochips containing pre-loaded proteins is also a challenging task since conventional sealing methods often require the use of high temperatures, electric voltages, or organic solvents that are detrimental to the protein activity. Using CO2 gas to enhance the diffusion of polymer molecules near the device surface can result in good bonding at low temperatures and low pressure. This bonding method has little influence on the activity of the pre-loaded proteins after bonding.

Characterization of a conical null-screen corneal topographer

NASA Astrophysics Data System (ADS)

Osorio-Infante, Arturo I.; Campos-García, Manuel; Cossio-Guerrero, Cesar

2017-06-01

In this work, we perform the characterization of a conical null-screen corneal topographer. For this, we design a custom null-screens for testing a reference spherical surfaces with a radius of curvature of 7.8 mm. We also test a 1/2-inch (12.7 mm) diameter stainless steel sphere and an aspherical surface with a radius of curvature of 7.77 mm. We designed some different target distributions with the same target size to evaluate the shape of the reference surfaces. The shape of each surface was recovered by fitting the experimental data to a custom shape using the least square methods with an iterative algorithm. The target distributions were modified to improve the accuracy of the measurements. We selected a distribution and evaluate the accuracy of the algorithms to measure spherical surfaces with a radius of curvature from 6 mm to 8.2 mm by simulating the reflected pattern. We also simulate the reflected patter by changing the position of the surface along the optical axis and then we measure the resulting radius of curvature.

A novel facility for reduced-gravity testing: A setup for studying low-velocity collisions into granular surfaces

NASA Astrophysics Data System (ADS)

Sunday, C.; Murdoch, N.; Cherrier, O.; Morales Serrano, S.; Valeria Nardi, C.; Janin, T.; Avila Martinez, I.; Gourinat, Y.; Mimoun, D.

2016-08-01

This work presents an experimental design for studying low-velocity collisions into granular surfaces in low-gravity. In the experiment apparatus, reduced-gravity is simulated by releasing a free-falling projectile into a surface container with a downward acceleration less than that of Earth's gravity. The acceleration of the surface is controlled through the use of an Atwood machine, or a system of pulleys and counterweights. The starting height of the surface container and the initial separation distance between the projectile and surface are variable and chosen to accommodate collision velocities up to 20 cm/s and effective accelerations of ˜0.1 to 1.0 m/s2. Accelerometers, placed on the surface container and inside the projectile, provide acceleration data, while high-speed cameras capture the collision and act as secondary data sources. The experiment is built into an existing 5.5 m drop tower frame and requires the custom design of all components, including the projectile, surface sample container, release mechanism, and deceleration system. Data from calibration tests verify the efficiency of the experiment's deceleration system and provide a quantitative understanding of the performance of the Atwood system.

A novel facility for reduced-gravity testing: A setup for studying low-velocity collisions into granular surfaces.

PubMed

Sunday, C; Murdoch, N; Cherrier, O; Morales Serrano, S; Valeria Nardi, C; Janin, T; Avila Martinez, I; Gourinat, Y; Mimoun, D

2016-08-01

This work presents an experimental design for studying low-velocity collisions into granular surfaces in low-gravity. In the experiment apparatus, reduced-gravity is simulated by releasing a free-falling projectile into a surface container with a downward acceleration less than that of Earth's gravity. The acceleration of the surface is controlled through the use of an Atwood machine, or a system of pulleys and counterweights. The starting height of the surface container and the initial separation distance between the projectile and surface are variable and chosen to accommodate collision velocities up to 20 cm/s and effective accelerations of ∼0.1 to 1.0 m/s(2). Accelerometers, placed on the surface container and inside the projectile, provide acceleration data, while high-speed cameras capture the collision and act as secondary data sources. The experiment is built into an existing 5.5 m drop tower frame and requires the custom design of all components, including the projectile, surface sample container, release mechanism, and deceleration system. Data from calibration tests verify the efficiency of the experiment's deceleration system and provide a quantitative understanding of the performance of the Atwood system.

Divergent Vegetation Growth Patterns Relative to Bioinfiltration Unit Size and Plant Placement

EPA Science Inventory

In 2009, the U.S. Environmental Protection Agency constructed six experimental bioinfiltration units at the Edison Environmental Center in Edison, New Jersey. They were designed as two sets of three bioinfiltration units with drainage area to surface area ratios of 5.5:1, 11:1, ...

Thermal and structural tests of a hydrogen cooled panel

NASA Technical Reports Server (NTRS)

Richard, C. E.; Duncan, J. D.; Gellersen, E. W.; Demogenes, C.

1972-01-01

An experimental evaluation of the thermal and structural performance of a hydrogen-cooled panel is presented. The panel, which was of brazed Inconel 625 and Inconel 718 construction, was designed for a heat flux of 100 BTU per second-foot squared and an external surface pressure of 100 psi.

Research on Cleaning Up in San Diego.

ERIC Educational Resources Information Center

Middleman, Stanley

1983-01-01

Discusses the evolution of a set of research programs (dealing with the removal of liquid contaminants from surfaces) used to introduce graduate students to methods of design, evaluation, and modification within the context of a larger research program. Stresses the simultaneity and interaction of theoretical and experimental studies. (JM)

Design of a Helium Vapor Shroud for Liquid Hydrogen Fueling of an Unmanned Aerial Vehicle (UAV)

NASA Astrophysics Data System (ADS)

Cavender, K.; Evans, C.; Haney, J.; Leachman, J.

2017-12-01

Filling a vehicular liquid hydrogen fuel tank presents the potential for flammable mixtures due to oxygen concentration from liquid air condensation. Current liquid hydrogen tank designs utilize insulating paradigms such as aerogel/fiberglass materials, vacuum jackets, or inert gas purge systems to keep the outer surface from reaching the condensation temperature of air. This work examines the heat transfer at the refuelling connection of the tank to identify potential areas of condensation, as well as the surface temperature gradient. A shrouded inert gas purge was designed to minimize vehicle weight and refuelling time. The design of a shrouded inert gas purge system is presented to displace air preventing air condensation. The design investigates 3D printed materials for an inert gas shroud, as well as low-temperature sealing designs. Shroud designs and temperature profiles were measured and tested by running liquid nitrogen through the filling manifold. Materials for the inert gas shroud are discussed and experimental results are compared to analytical model predictions. Suggestions for future design improvements are made.

Improvement of patient return electrodes in electrosurgery by experimental investigations and numerical field calculations.

PubMed

Golombeck, M A; Dössel, O; Raiser, J

2003-09-01

Numerical field calculations and experimental investigations were performed to examine the heating of the surface of human skin during the application of a new electrode design for the patient return electrode. The new electrode is characterised by an equipotential ring around the central electrode pads. A multi-layer thigh model was used, to which the patient return electrode and the active electrode were connected. The simulation geometry and the dielectric tissue parameters were set according to the frequency of the current. The temperature rise at the skin surface due to the flow of current was evaluated using a two-step numerical solving procedure. The results were compared with experimental thermographical measurements that yielded a mean value of maximum temperature increase of 3.4 degrees C and a maximum of 4.5 degrees C in one test case. The calculated heating patterns agreed closely with the experimental results. However, the calculated mean value in ten different numerical models of the maximum temperature increase of 12.5 K (using a thermodynamic solver) exceeded the experimental value owing to neglect of heat transport by blood flow and also because of the injection of a higher test current, as in the clinical tests. The implementation of a simple worst-case formula that could significantly simplify the numerical process led to a substantial overestimation of the mean value of the maximum skin temperature of 22.4 K and showed only restricted applicability. The application of numerical methods confirmed the experimental assertions and led to a general understanding of the observed heating effects and hotspots. Furthermore, it was possible to demonstrate the beneficial effects of the new electrode design with an equipotential ring. These include a balanced heating pattern and the absence of hotspots.

Comparative performance of conventional OPC concrete and HPC designed by densified mixture design algorithm

NASA Astrophysics Data System (ADS)

Huynh, Trong-Phuoc; Hwang, Chao-Lung; Yang, Shu-Ti

2017-12-01

This experimental study evaluated the performance of normal ordinary Portland cement (OPC) concrete and high-performance concrete (HPC) that were designed by the conventional method (ACI) and densified mixture design algorithm (DMDA) method, respectively. Engineering properties and durability performance of both the OPC and HPC samples were studied using the tests of workability, compressive strength, water absorption, ultrasonic pulse velocity, and electrical surface resistivity. Test results show that the HPC performed good fresh property and further showed better performance in terms of strength and durability as compared to the OPC.

Vacuum insulation of the high energy negative ion source for fusion application.

PubMed

Kojima, A; Hanada, M; Hilmi, A; Inoue, T; Watanabe, K; Taniguchi, M; Kashiwagi, M; Umeda, N; Tobari, H; Kobayashi, S; Yamano, Y; Grisham, L R

2012-02-01

Vacuum insulation on a large size negative ion accelerator with multiple extraction apertures and acceleration grids for fusion application was experimentally examined and designed. In the experiment, vacuum insulation characteristics were investigated in the JT-60 negative ion source with >1000 apertures on the grid with the surface area of ∼2 m(2). The sustainable voltages varied with a square root of the gap lengths between the grids, and decreased with number of the apertures and with the surface area of the grids. Based on the obtained results, the JT-60SA (super advanced) negative ion source is designed to produce 22 A, 500 keV D(-) ion beams for 100 s.

Adhesion design maps for bio-inspired attachment systems.

PubMed

Spolenak, Ralph; Gorb, Stanislav; Arzt, Eduard

2005-01-01

Fibrous surface structures can improve the adhesion of objects to other surfaces. Animals, such as flies and geckos, take advantage of this principle by developing "hairy" contact structures which ensure controlled and repeatable adhesion and detachment. Mathematical models for fiber adhesion predict pronounced dependencies of contact performance on the geometry and the elastic properties of the fibers. In this paper the limits of such contacts imposed by fiber strength, fiber condensation, compliance, and ideal contact strength are modeled for spherical contact tips. Based on this, we introduce the concept of "adhesion design maps" which visualize the predicted mechanical behavior. The maps are useful for understanding biological systems and for guiding experimentation to achieve optimum artificial contacts.

Circular polarization analyzer with polarization tunable focusing of surface plasmon polaritons

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Sen; Zhang, Yan, E-mail: yzhang@mail.cnu.edu.cn; Beijing Key Laboratory for Metamaterials and Devices, and Key Laboratory of Terahertz Optoelectronics, Ministry of Education, Department of Physics, Capital Normal University, Beijing 100048

2015-12-14

A practical circular polarization analyzer (CPA) that can selectively focus surface plasmon polaritons (SPPs) at two separate locations, according to the helicity of the circularly polarized light, is designed and experimentally verified in the terahertz frequency range. The CPA consists of fishbone-slit units and is designed using the simulated annealing algorithm. By differentially detecting the intensities of the two SPPs focuses, the helicity of the incident circularly polarized light can be obtained and the CPA is less vulnerable to the noise of incident light. The proposed device may also have wide potential applications in chiral SPPs photonics and the analysismore » of chiral molecules in biology.« less

Surface-electrode point Paul trap

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kim, Tony Hyun; Herskind, Peter F.; Chuang, Isaac L.

2010-10-15

We present a model as well as experimental results for a surface electrode radiofrequency Paul trap that has a circular electrode geometry well suited for trapping single ions and two-dimensional planar ion crystals. The trap design is compatible with microfabrication and offers a simple method by which the height of the trapped ions above the surface may be changed in situ. We demonstrate trapping of single {sup 88}Sr{sup +} ions over an ion height range of 200-1000 {mu}m for several hours under Doppler laser cooling and use these to characterize the trap, finding good agreement with our model.

Critical Role of Surface Energy in Guiding Crystallization of Solution-Coated Conjugated Polymer Thin Films

DOE PAGES

Zhang, Fengjiao; Mohammadi, Erfan; Luo, Xuyi; ...

2017-10-02

It is well-known that substrate surface properties have a profound impact on morphology of thin films solution coated atop and the resulting solid-state properties. However, design rules for guiding the substrate selection have not yet been established. Such design rules are particularly important for solution coated semiconducting polymers, as the substratedirected thin film morphology can impact charge transport properties by orders of magnitude. We hypothesize that substrate surface energies dictate the thin film morphology by modulating the free energy barrier to heterogeneous nucleation. To test this hypothesis, we systematically vary the substrate surface energy via surface functionalization techniques. We performmore » in-depth morphology and device characterizations to establish the relationship between substrate surface energy, thin film morphology and charge transport properties, employing a donor-accepter (D-A) conjugated polymer. Here, we find that decreasing the substrate surface energy progressively increases thin film crystallinity, degree of molecular ordering and extent of domain alignment. Notably, the enhanced morphology on the lowest surface energy substrate lead to a 10-fold increase in the charge carrier mobility. We further develop a free energy model relating the substrate surface energy to the penalty of heterogeneous nucleation from solution in the thin film geometry. The model correctly predicts the experimental trend, thereby validating our hypothesis. This work is a significant step towards establishing design rules and understanding the critical role of substrates in determining morphology of solution coated thin films.« less

Critical Role of Surface Energy in Guiding Crystallization of Solution-Coated Conjugated Polymer Thin Films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Fengjiao; Mohammadi, Erfan; Luo, Xuyi

It is well-known that substrate surface properties have a profound impact on morphology of thin films solution coated atop and the resulting solid-state properties. However, design rules for guiding the substrate selection have not yet been established. Such design rules are particularly important for solution coated semiconducting polymers, as the substratedirected thin film morphology can impact charge transport properties by orders of magnitude. We hypothesize that substrate surface energies dictate the thin film morphology by modulating the free energy barrier to heterogeneous nucleation. To test this hypothesis, we systematically vary the substrate surface energy via surface functionalization techniques. We performmore » in-depth morphology and device characterizations to establish the relationship between substrate surface energy, thin film morphology and charge transport properties, employing a donor-accepter (D-A) conjugated polymer. Here, we find that decreasing the substrate surface energy progressively increases thin film crystallinity, degree of molecular ordering and extent of domain alignment. Notably, the enhanced morphology on the lowest surface energy substrate lead to a 10-fold increase in the charge carrier mobility. We further develop a free energy model relating the substrate surface energy to the penalty of heterogeneous nucleation from solution in the thin film geometry. The model correctly predicts the experimental trend, thereby validating our hypothesis. This work is a significant step towards establishing design rules and understanding the critical role of substrates in determining morphology of solution coated thin films.« less

Numerical Prediction of the Onset of the Magnetorotational Instability in the Princeton MRI Apparatus

NASA Astrophysics Data System (ADS)

Gilson, Erik; Caspary, Kyle; Ebrahimi, Fatima; Goodman, Jeremy; Ji, Hantao; Nuñez, Tahiri; Wei, Xing

2016-10-01

The liquid metal magnetorotational instability experiment at PPPL is designed to search for the MRI in a controlled laboratory setup. MRI is thought to be the primary mechanism behind turbulence in accretion disks, leading to an enhanced effective viscosity that can explain observed fast accretion rates. The apparatus has several key differences from an accretion disk. The top and bottom surfaces of the vessel exert stresses on the surfaces of the working fluid. There are no surface stresses on an accretion disk, but rather a free-surface. To interpret experimental results, the Spectral Finite Element Maxwell and Navier Stokes (SFEMaNS) code (Guermond et al., 2009) has been used to simulate experiments in the MRI apparatus and study MRI onset in the presence of residual flows induced by the boundaries. These Ekman flows lead to the generation of radial magnetic fields that can obfuscate the MRI signal. Simulation results are presented that show the full spatial distribution of the velocity field and the magnetic field over a range of experimental operating parameters, including both above and below the expected MRI threshold. Both the residual flow and the radial magnetic field at the location of the diagnostics are computed for comparisons with experimental results. This research is supported by DOE, NSF, and NASA.

Modeling the Effect of Temperature and Potential on the In Vitro Corrosion Performance of Biomedical Hydroxyapatite Coatings

NASA Astrophysics Data System (ADS)

Coşkun, M. İbrahim; Karahan, İsmail H.; Yücel, Yasin; Golden, Teresa D.

2016-10-01

CoCrMo biomedical alloys were coated with a hydroxyapatite layer to improve biocompatibility and in vitro corrosion performance. A fast electrodeposition process was completed in 5 minutes for the hydroxyapatite coating. Effect of the solution temperature and applied potential on the in vitro corrosion performance of the hydroxyapatite coatings was modeled by response surface methodology (RSM) coupled with central composite design (CCD). A 5-level-2-factor experimental plan designed by CCD was used; the experimental plan contained 13 coating experiments with a temperature range from 283 K to 347 K (10 °C to 74 °C) and potential range from -1.2 to -1.9 V. Corrosion potential ( E corr) of the coatings in a simulated body fluid solution was chosen as response for the model. Predicted and experimental values fitted well with an R 2 value of 0.9481. Response surface plots of the impedance and polarization resistance ( R P) were investigated. Optimized parameters for electrodeposition of hydroxyapatite were determined by RSM as solution temperature of 305.48 K (32.33 °C) and potential of -1.55 V. Hydroxyapatite coatings fabricated at optimized parameters showed excellent crystal formation and high in vitro corrosion resistance.

Designing a multicolor long range nanoscopic ruler for the imaging of heterogeneous tumor cells

NASA Astrophysics Data System (ADS)

Chavva, Suhash Reddy; Viraka Nellore, Bhanu Priya; Pramanik, Avijit; Sinha, Sudarson Sekhar; Jones, Stacy; Ray, Paresh Chandra

2016-07-01

Tumor heterogeneity is one of the biggest challenges in cancer treatment and diagnosis. A multicolor optical ruler is essential to address the heterogeneous tumor cell complexity. Driven by this need, the current article reports the design of a multicolor long range nanoscopic ruler for screening tumor heterogeneity by accurately identifying epithelial cells and cancer stem cells (CSCs) simultaneously. A nanoscopic surface energy transfer (NSET) ruler has been developed using blue fluorescence polymer dots (PDs) and red fluorescence gold cluster dots (GCDs) as multicolor fluorescence donor and plasmonic gold nanoparticle (GNP) acts as an excellent acceptor. Reported experimental results demonstrated that the multicolor nanoscopic ruler's working window is above 35 nm distances, which is more than three times farther than that of Förster resonance energy transfer (FRET) distance limit. Theoretical modeling using Förster dipole-dipole coupling and dipole to nanoparticle surface energy transfer have been used to discuss the possible mechanism for multicolor nanoscopic ruler's long-range capability. Using RNA aptamers that are specific for the target cancer cells, experimental data demonstrate that the nanoscopic ruler can be used for screening epithelial and CSCs simultaneously from a whole blood sample with a detection capability of 10 cells per mL. Experimental data show that the nanoscopic ruler can distinguish targeted cells from non-targeted cells.

Sequential Design of Experiments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Anderson-Cook, Christine Michaela

2017-06-30

A sequential design of experiments strategy is being developed and implemented that allows for adaptive learning based on incoming results as the experiment is being run. The plan is to incorporate these strategies for the NCCC and TCM experimental campaigns to be run in the coming months. This strategy for experimentation has the advantages of allowing new data collected during the experiment to inform future experimental runs based on their projected utility for a particular goal. For example, the current effort for the MEA capture system at NCCC plans to focus on maximally improving the quality of prediction of COmore » 2 capture efficiency as measured by the width of the confidence interval for the underlying response surface that is modeled as a function of 1) Flue Gas Flowrate [1000-3000] kg/hr; 2) CO 2 weight fraction [0.125-0.175]; 3) Lean solvent loading [0.1-0.3], and; 4) Lean solvent flowrate [3000-12000] kg/hr.« less

Experimental spectroscopy for the high-school Physics curriculum

NASA Astrophysics Data System (ADS)

Kinra, Rajeev; Karpetis, Adonios

2008-11-01

The present work explores the feasibility of including spectroscopic experiments in high-school physics curricula. Two experimental optics ``modules'' were constructed for this purpose: (a) a simple CCD detector, in combination with appropriate filters, was used for the measurement of solar spectra and the determination of the sun's surface temperature; (b) the same detector was used, in combination with a transmissive diffraction grating and some miniature optics, to form a spectrophotometer that can be used for the determination of spectra with high resolution. Both modules were designed and constructed with portability and low cost in mind, and their objective is to introduce experimental spectroscopy to high school students in an intriguing, educational and phase-appropriate manner without sacrificing scientific rigor. A large variety of experiments may be designed around the basic devices that were built during this work, and a number of possible examples will be presented, from research on plant phototropism to human color cognition.

Optimisation of the synthesis of vancomycin-selective molecularly imprinted polymer nanoparticles using automatic photoreactor

PubMed Central

2014-01-01

A novel optimized protocol for solid-state synthesis of molecularly imprinted polymer nanoparticles (nanoMIPs) with specificity for antibiotic vancomycin is described. The experimental objective was optimization of the synthesis parameters (factors) affecting the yield of obtained nanoparticles which have been synthesized using the first prototype of an automated solid-phase synthesizer. Applications of experimental design (or design of experiments) in optimization of nanoMIP yield were carried out using MODDE 9.0 software. The factors chosen in the model were the amount of functional monomers in the polymerization mixture, irradiation time, temperature during polymerization, and elution temperature. In general, it could be concluded that the irradiation time is the most important and the temperature was the least important factor which influences the yield of nanoparticles. Overall, the response surface methodology proved to be an effective tool in reducing time required for optimization of complex experimental conditions. PMID:24685151

Optimisation of the synthesis of vancomycin-selective molecularly imprinted polymer nanoparticles using automatic photoreactor.

PubMed

Muzyka, Kateryna; Karim, Khalku; Guerreiro, Antonio; Poma, Alessandro; Piletsky, Sergey

2014-03-31

A novel optimized protocol for solid-state synthesis of molecularly imprinted polymer nanoparticles (nanoMIPs) with specificity for antibiotic vancomycin is described. The experimental objective was optimization of the synthesis parameters (factors) affecting the yield of obtained nanoparticles which have been synthesized using the first prototype of an automated solid-phase synthesizer. Applications of experimental design (or design of experiments) in optimization of nanoMIP yield were carried out using MODDE 9.0 software. The factors chosen in the model were the amount of functional monomers in the polymerization mixture, irradiation time, temperature during polymerization, and elution temperature. In general, it could be concluded that the irradiation time is the most important and the temperature was the least important factor which influences the yield of nanoparticles. Overall, the response surface methodology proved to be an effective tool in reducing time required for optimization of complex experimental conditions.

Optimisation of the synthesis of vancomycin-selective molecularly imprinted polymer nanoparticles using automatic photoreactor

NASA Astrophysics Data System (ADS)

Muzyka, Kateryna; Karim, Khalku; Guerreiro, Antonio; Poma, Alessandro; Piletsky, Sergey

2014-03-01

A novel optimized protocol for solid-state synthesis of molecularly imprinted polymer nanoparticles (nanoMIPs) with specificity for antibiotic vancomycin is described. The experimental objective was optimization of the synthesis parameters (factors) affecting the yield of obtained nanoparticles which have been synthesized using the first prototype of an automated solid-phase synthesizer. Applications of experimental design (or design of experiments) in optimization of nanoMIP yield were carried out using MODDE 9.0 software. The factors chosen in the model were the amount of functional monomers in the polymerization mixture, irradiation time, temperature during polymerization, and elution temperature. In general, it could be concluded that the irradiation time is the most important and the temperature was the least important factor which influences the yield of nanoparticles. Overall, the response surface methodology proved to be an effective tool in reducing time required for optimization of complex experimental conditions.

Enzymatic catalysis treatment method of meat industry wastewater using lacasse.

PubMed

Thirugnanasambandham, K; Sivakumar, V

2015-01-01

The process of meat industry produces in a large amount of wastewater that contains high levels of colour and chemical oxygen demand (COD). So they must be pretreated before their discharge into the ecological system. In this paper, enzymatic catalysis (EC) was adopted to treat the meat wastewater. Box-Behnken design (BBD), an experimental design for response surface methodology (RSM), was used to create a set of 29 experimental runs needed for optimizing of the operating conditions. Quadratic regression models with estimated coefficients were developed to describe the colour and COD removals. The experimental results show that EC could effectively reduce colour (95 %) and COD (86 %) at the optimum conditions of enzyme dose of 110 U/L, incubation time of 100 min, pH of 7 and temperature of 40 °C. RSM could be effectively adopted to optimize the operating multifactors in complex EC process.

An experimental study of the Rayleigh-Taylor instability critical wave length

NASA Astrophysics Data System (ADS)

Kong, Xujing; Wang, Youchun; Zhang, Shufei; Xu, Hongkun

1992-06-01

A physical model has been constructed to represent the condensate film pattern on a horizontal downward-facing surface with fins, which is based on visual observation in experiment. The results of analysis using this model confirms the validity of the critical wave length formula obtained from Rayleigh-Taylor stability analysis. This formula may be used as a criterion to design horizontal downward-facing surfaces with fins that can best destabilize the condensate film, thus enhancing condensation heat transfer.

Experimental Investigation of a Morphing Nacelle Ducted Fan

NASA Technical Reports Server (NTRS)

Kondor, Shayne A.; Moore, Mark

2005-01-01

The application of Circulation Control to the nacelle of a shrouded fan is proposed as a means to enhance off-design performance of the shrouded fan. Typically, a fixed geometry shroud is efficient at a single operating condition. Modifying circulation about the fixed geometry is proposed as a means to virtually morph the shroud without moving surfaces. This approach will enhance off-design-point performance with minimal complexity, weight, and cost. Termed the Morphing Nacelle, this concept provides an attractive propulsion option for Vertical Take-off and Landing (VTOL) aircraft, such conceptual Personal Air Vehicle (PAV) configurations proposed by NASA. An experimental proof of concept investigation of the Morphing Nacelle is detailed in this paper. A powered model shrouded fan model was constructed with Circulation Control (CC) devices integrated in the inlet and exit of the nacelle. Both CC devices consisted of an annular jet slot directing a jet sheet tangent to a curved surface, generally described as a Coanda surface. The model shroud was tailored for axial flight, with a diffusing inlet, but was operated off-design condition as a static lifting fan. Thrust stand experiments were conducted to determine if the CC devices could effectively improve off-design performance of the shrouded fan. Additional tests were conducted to explore the effectiveness of the CC devices a means to reduce peak static pressure on the ground below a lifting fan. Experimental results showed that off-design static thrust performance of the model was improved when the CC devices were employed under certain conditions. The exhaust CC device alone, while effective in diffusing the fan exhaust and improving weight flow into shroud inlet, tended to diminish performance of the fan with increased CC jet momentum. The inlet CC device was effective at reattaching a normally stalled inlet flow condition, proving an effective means of enhancing performance. A more dramatic improvement in static thrust was obtained when the inlet and exit CC devices were operated in unison, but only over a limited range of CC jet momentum. Operating the nacelle inlet and exit CC devices together proved very effective in reducing peak ground plane static pressure, while maintaining static thrust. The Morphing Nacelle concept proved effective at enhancing off-design performance of the model; however, additional investigation is necessary to generalize the results.

Effect of the surface roughness on interfacial breakdown between two dielectric surfaces

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fournier, D.

1996-12-31

Cable splices and accessories are the weak link in an underground power distribution system. Investigations of problems related to cable splices and accessories becomes quite intricate once the simpler causes of failures are dismissed to allow more complex phenomena to be examined. The interfacial breakdown between two internal dielectric surfaces represents one of the major causes of failure for power cable joints. In order to better understand this phenomenon, breakdown experiments were performed at interfaces found in cable splices. An experimental jig was designed to induce breakdown between dielectric surfaces longitudinally along their interface. Effects of surface roughness at EPDM/XLPEmore » and EPDM/EPDM interfaces as well as the presence of silicone grease are taken into account.« less

The role of chemistry and pH of solid surfaces for specific adsorption of biomolecules in solution--accurate computational models and experiment.

PubMed

Heinz, Hendrik

2014-06-18

Adsorption of biomolecules and polymers to inorganic nanostructures plays a major role in the design of novel materials and therapeutics. The behavior of flexible molecules on solid surfaces at a scale of 1-1000 nm remains difficult and expensive to monitor using current laboratory techniques, while playing a critical role in energy conversion and composite materials as well as in understanding the origin of diseases. Approaches to implement key surface features and pH in molecular models of solids are explained, and distinct mechanisms of peptide recognition on metal nanostructures, silica and apatite surfaces in solution are described as illustrative examples. The influence of surface energies, specific surface features and protonation states on the structure of aqueous interfaces and selective biomolecular adsorption is found to be critical, comparable to the well-known influence of the charge state and pH of proteins and surfactants on their conformations and assembly. The representation of such details in molecular models according to experimental data and available chemical knowledge enables accurate simulations of unknown complex interfaces in atomic resolution in quantitative agreement with independent experimental measurements. In this context, the benefits of a uniform force field for all material classes and of a mineral surface structure database are discussed.

Bioinspired surfaces for turbulent drag reduction

PubMed Central

Golovin, Kevin B.; Gose, James W.; Perlin, Marc; Ceccio, Steven L.; Tuteja, Anish

2016-01-01

In this review, we discuss how superhydrophobic surfaces (SHSs) can provide friction drag reduction in turbulent flow. Whereas biomimetic SHSs are known to reduce drag in laminar flow, turbulence adds many new challenges. We first provide an overview on designing SHSs, and how these surfaces can cause slip in the laminar regime. We then discuss recent studies evaluating drag on SHSs in turbulent flow, both computationally and experimentally. The effects of streamwise and spanwise slip for canonical, structured surfaces are well characterized by direct numerical simulations, and several experimental studies have validated these results. However, the complex and hierarchical textures of scalable SHSs that can be applied over large areas generate additional complications. Many studies on such surfaces have measured no drag reduction, or even a drag increase in turbulent flow. We discuss how surface wettability, roughness effects and some newly found scaling laws can help explain these varied results. Overall, we discuss how, to effectively reduce drag in turbulent flow, an SHS should have: preferentially streamwise-aligned features to enhance favourable slip, a capillary resistance of the order of megapascals, and a roughness no larger than 0.5, when non-dimensionalized by the viscous length scale. This article is part of the themed issue ‘Bioinspired hierarchically structured surfaces for green science’. PMID:27354731

Bioinspired surfaces for turbulent drag reduction.

PubMed

Golovin, Kevin B; Gose, James W; Perlin, Marc; Ceccio, Steven L; Tuteja, Anish

2016-08-06

In this review, we discuss how superhydrophobic surfaces (SHSs) can provide friction drag reduction in turbulent flow. Whereas biomimetic SHSs are known to reduce drag in laminar flow, turbulence adds many new challenges. We first provide an overview on designing SHSs, and how these surfaces can cause slip in the laminar regime. We then discuss recent studies evaluating drag on SHSs in turbulent flow, both computationally and experimentally. The effects of streamwise and spanwise slip for canonical, structured surfaces are well characterized by direct numerical simulations, and several experimental studies have validated these results. However, the complex and hierarchical textures of scalable SHSs that can be applied over large areas generate additional complications. Many studies on such surfaces have measured no drag reduction, or even a drag increase in turbulent flow. We discuss how surface wettability, roughness effects and some newly found scaling laws can help explain these varied results. Overall, we discuss how, to effectively reduce drag in turbulent flow, an SHS should have: preferentially streamwise-aligned features to enhance favourable slip, a capillary resistance of the order of megapascals, and a roughness no larger than 0.5, when non-dimensionalized by the viscous length scale.This article is part of the themed issue 'Bioinspired hierarchically structured surfaces for green science'. © 2016 The Author(s).

Optimization of Polyplex Formation between DNA Oligonucleotide and Poly(ʟ-Lysine): Experimental Study and Modeling Approach.

PubMed

Vasiliu, Tudor; Cojocaru, Corneliu; Rotaru, Alexandru; Pricope, Gabriela; Pinteala, Mariana; Clima, Lilia

2017-06-17

The polyplexes formed by nucleic acids and polycations have received a great attention owing to their potential application in gene therapy. In our study, we report experimental results and modeling outcomes regarding the optimization of polyplex formation between the double-stranded DNA (dsDNA) and poly(ʟ-Lysine) (PLL). The quantification of the binding efficiency during polyplex formation was performed by processing of the images captured from the gel electrophoresis assays. The design of experiments (DoE) and response surface methodology (RSM) were employed to investigate the coupling effect of key factors (pH and N/P ratio) affecting the binding efficiency. According to the experimental observations and response surface analysis, the N/P ratio showed a major influence on binding efficiency compared to pH. Model-based optimization calculations along with the experimental confirmation runs unveiled the maximal binding efficiency (99.4%) achieved at pH 5.4 and N/P ratio 125. To support the experimental data and reveal insights of molecular mechanism responsible for the polyplex formation between dsDNA and PLL, molecular dynamics simulations were performed at pH 5.4 and 7.4.

Optimization of Polyplex Formation between DNA Oligonucleotide and Poly(l-Lysine): Experimental Study and Modeling Approach

PubMed Central

Vasiliu, Tudor; Cojocaru, Corneliu; Rotaru, Alexandru; Pricope, Gabriela; Pinteala, Mariana; Clima, Lilia

2017-01-01

The polyplexes formed by nucleic acids and polycations have received a great attention owing to their potential application in gene therapy. In our study, we report experimental results and modeling outcomes regarding the optimization of polyplex formation between the double-stranded DNA (dsDNA) and poly(l-Lysine) (PLL). The quantification of the binding efficiency during polyplex formation was performed by processing of the images captured from the gel electrophoresis assays. The design of experiments (DoE) and response surface methodology (RSM) were employed to investigate the coupling effect of key factors (pH and N/P ratio) affecting the binding efficiency. According to the experimental observations and response surface analysis, the N/P ratio showed a major influence on binding efficiency compared to pH. Model-based optimization calculations along with the experimental confirmation runs unveiled the maximal binding efficiency (99.4%) achieved at pH 5.4 and N/P ratio 125. To support the experimental data and reveal insights of molecular mechanism responsible for the polyplex formation between dsDNA and PLL, molecular dynamics simulations were performed at pH 5.4 and 7.4. PMID:28629130

Experimental Design for a Sponge-Wipe Study to Relate the Recovery Efficiency and False Negative Rate to the Concentration of a Bacillus anthracis Surrogate for Six Surface Materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Piepel, Gregory F.; Amidan, Brett G.; Krauter, Paula

2011-05-01

Two concerns were raised by the Government Accountability Office following the 2001 building contaminations via letters containing Bacillus anthracis (BA). These included the: 1) lack of validated sampling methods, and 2) need to use statistical sampling to quantify the confidence of no contamination when all samples have negative results. Critical to addressing these concerns is quantifying the false negative rate (FNR). The FNR may depend on the 1) method of contaminant deposition, 2) surface concentration of the contaminant, 3) surface material being sampled, 4) sample collection method, 5) sample storage/transportation conditions, 6) sample processing method, and 7) sample analytical method.more » A review of the literature found 17 laboratory studies that focused on swab, wipe, or vacuum samples collected from a variety of surface materials contaminated by BA or a surrogate, and used culture methods to determine the surface contaminant concentration. These studies quantified performance of the sampling and analysis methods in terms of recovery efficiency (RE) and not FNR (which left a major gap in available information). Quantifying the FNR under a variety of conditions is a key aspect of validating sample and analysis methods, and also for calculating the confidence in characterization or clearance decisions based on a statistical sampling plan. A laboratory study was planned to partially fill the gap in FNR results. This report documents the experimental design developed by Pacific Northwest National Laboratory and Sandia National Laboratories (SNL) for a sponge-wipe method. The testing was performed by SNL and is now completed. The study investigated the effects on key response variables from six surface materials contaminated with eight surface concentrations of a BA surrogate (Bacillus atrophaeus). The key response variables include measures of the contamination on test coupons of surface materials tested, contamination recovered from coupons by sponge-wipe samples, RE, and FNR. The experimental design involves 16 test runs, performed in two blocks of eight runs. Three surface materials (stainless steel, vinyl tile, and ceramic tile) were tested in the first block, while three other surface materials (plastic, painted wood paneling, and faux leather) were tested in the second block. The eight surface concentrations of the surrogate were randomly assigned to test runs within each block. Some of the concentrations were very low and presented challenges for deposition, sampling, and analysis. However, such tests are needed to investigate RE and FNR over the full range of concentrations of interest. In each run, there were 10 test coupons of each of the three surface materials. A positive control sample was generated at the same time as each test sample. The positive control results will be used to 1) calculate RE values for the wipe sampling and analysis method, and 2) fit RE- and FNR-concentration equations, for each of the six surface materials. Data analyses will support 1) estimating the FNR for each combination of contaminant concentration and surface material, 2) estimating the surface concentrations and their uncertainties of the contaminant for each combination of concentration and surface material, 3) estimating RE (%) and their uncertainties for each combination of contaminant concentration and surface material, 4) fitting FNR-concentration and RE-concentration equations for each of the six surface materials, 5) assessing goodness-of-fit of the equations, and 6) quantifying the uncertainty in FNR and RE predictions made with the fitted equations.« less

Experimental Design for a Sponge-Wipe Study to Relate the Recovery Efficiency and False Negative Rate to the Concentration of a Bacillus anthracis Surrogate for Six Surface Materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Piepel, Gregory F.; Amidan, Brett G.; Krauter, Paula

2010-12-16

Two concerns were raised by the Government Accountability Office following the 2001 building contaminations via letters containing Bacillus anthracis (BA). These included the: 1) lack of validated sampling methods, and 2) need to use statistical sampling to quantify the confidence of no contamination when all samples have negative results. Critical to addressing these concerns is quantifying the probability of correct detection (PCD) (or equivalently the false negative rate FNR = 1 - PCD). The PCD/FNR may depend on the 1) method of contaminant deposition, 2) surface concentration of the contaminant, 3) surface material being sampled, 4) sample collection method, 5)more » sample storage/transportation conditions, 6) sample processing method, and 7) sample analytical method. A review of the literature found 17 laboratory studies that focused on swab, wipe, or vacuum samples collected from a variety of surface materials contaminated by BA or a surrogate, and used culture methods to determine the surface contaminant concentration. These studies quantified performance of the sampling and analysis methods in terms of recovery efficiency (RE) and not PCD/FNR (which left a major gap in available information). Quantifying the PCD/FNR under a variety of conditions is a key aspect of validating sample and analysis methods, and also for calculating the confidence in characterization or clearance decisions based on a statistical sampling plan. A laboratory study was planned to partially fill the gap in PCD/FNR results. This report documents the experimental design developed by Pacific Northwest National Laboratory and Sandia National Laboratories (SNL) for a sponge-wipe method. The study will investigate the effects on key response variables from six surface materials contaminated with eight surface concentrations of a BA surrogate (Bacillus atrophaeus). The key response variables include measures of the contamination on test coupons of surface materials tested, contamination recovered from coupons by sponge-wipe samples, RE, and PCD/FNR. The experimental design involves 16 test runs, to be performed in two blocks of eight runs. Three surface materials (stainless steel, vinyl tile, and ceramic tile) were tested in the first block, while three other surface materials (plastic, painted wood paneling, and faux leather) will be tested in the second block. The eight surface concentrations of the surrogate were randomly assigned to test runs within each block. Some of the concentrations will be very low and may present challenges for deposition, sampling, and analysis. However, such tests are needed to investigate RE and PCD/FNR over the full range of concentrations of interest. In each run, there will be 10 test coupons of each of the three surface materials. A positive control sample will be generated prior to each test sample. The positive control results will be used to 1) calculate RE values for the wipe sampling and analysis method, and 2) fit RE- and PCD-concentration equations, for each of the six surface materials. Data analyses will support 1) estimating the PCD for each combination of contaminant concentration and surface material, 2) estimating the surface concentrations and their uncertainties of the contaminant for each combination of concentration and surface material, 3) estimating RE (%) and their uncertainties for each combination of contaminant concentration and surface material, 4) fitting PCD-concentration and RE-concentration equations for each of the six surface materials, 5) assessing goodness-of-fit of the equations, and 6) quantifying the uncertainty in PCD and RE predictions made with the fitted equations.« less

Second-order sliding mode control with experimental application.

PubMed

Eker, Ilyas

2010-07-01

In this article, a second-order sliding mode control (2-SMC) is proposed for second-order uncertain plants using equivalent control approach to improve the performance of control systems. A Proportional + Integral + Derivative (PID) sliding surface is used for the sliding mode. The sliding mode control law is derived using direct Lyapunov stability approach and asymptotic stability is proved theoretically. The performance of the closed-loop system is analysed through an experimental application to an electromechanical plant to show the feasibility and effectiveness of the proposed second-order sliding mode control and factors involved in the design. The second-order plant parameters are experimentally determined using input-output measured data. The results of the experimental application are presented to make a quantitative comparison with the traditional (first-order) sliding mode control (SMC) and PID control. It is demonstrated that the proposed 2-SMC system improves the performance of the closed-loop system with better tracking specifications in the case of external disturbances, better behavior of the output and faster convergence of the sliding surface while maintaining the stability. 2010 ISA. Published by Elsevier Ltd. All rights reserved.

Extended mission/lunar rover, executive summary

NASA Technical Reports Server (NTRS)

1992-01-01

The design project selected to be undertaken by the 1991/92 Aerospace Design Group was that of conceptually designing an Extended Mission Rover for use on the Lunar Surface. This vehicle would serve the function as a mobile base of sorts, and be able to provide future astronauts with a mobile 'shirt-sleeve' self-sufficient living and working environment. Some of the proposed missions would be planetary surface exploration, construction and maintenance, hardware set-up and in-situ resource experimentation. The need for this type of vehicle has already been declared in the Stafford Group's report on the future of America's Space Program, entitled 'America at the Threshold: America's Space Exploration Initiative'. In the four architectures described within the report, the concept of a pressurized vehicle occurred multiple times. The approximate time frame that this vehicle would be put into use is 2010-2030.

Experimental studies on particle impaction and bounce: effects of substrate design and material

NASA Astrophysics Data System (ADS)

Chang, Mingchih; Kim, Seongheon; Sioutas, Constantinos

This paper presents an experimental investigation of the effects of impaction substrate designs and material in reducing particle bounce and reentrainment. Particle collection without coating by using combinations of different impaction substrate designs and surface materials was conducted using a personal particle sampler (PPS) developed by the University of Southern California. The PPS operates at flow rate of 4 l min -1 with a 50% cutpoint of approximately 0.9 μm in aerodynamic diameter. The laboratory results showed that the PPS collection efficiency for particles larger than 50% cutpoint is strikingly low (e.g., less than 50%) when an uncoated open cavity made of aluminum was used as an impaction substrate. The collection efficiency gradually increased when Teflon tape, Nuclepore, and glass fiber filters were used as impaction surfaces, respectively. Conical or partially enclosed cavity substrate designs increased collection efficiency of particles of 9 μm up to 80-90%. A conical cavity with glass fiber filter used as impaction surface was identified as the optimum configuration, resulting in a collection efficiency of 92% at Stokes numbers as high as 15.4 (corresponding to 9 μm in aerodynamic diameter). Particle losses were low (less than 10%) and relatively independent of particle size in any design with glass fiber filter. Losses seemed to increase slightly with particle size in all other configurations. Finally, outdoor PM 1 concentrations obtained with the PPS (in its optimum configuration) and a modified micro-orifice uniform deposit impactor (MOUDI) with coated impaction stages were in excellent agreement. The mean ratio of the PPS-to-MOUDI concentration was 1.13(±0.17) with a correlation coefficient R2=0.95. Results from this investigation can be readily applied to design particle bounce-free impaction substrates without the use of coating. This is a very important feature of impactors, especially when chemical analysis of the collected particulate matter is desirable.

Optimization of the photoelectrocatalytic oxidation of landfill leachate using copper and nitrate co-doped TiO2 (Ti) by response surface methodology

PubMed Central

Zhou, Shaoqi; Feng, Xinbin

2017-01-01

In this paper, a statistically-based experimental design with response surface methodology (RSM) was employed to examine the effects of functional conditions on the photoelectrocatalytic oxidation of landfill leachate using a Cu/N co-doped TiO2 (Ti) electrode. The experimental design method was applied to response surface modeling and the optimization of the operational parameters of the photoelectro-catalytic degradation of landfill leachate using TiO2 as a photo-anode. The variables considered were the initial chemical oxygen demand (COD) concentration, pH and the potential bias. Two dependent parameters were either directly measured or calculated as responses: chemical oxygen demand (COD) removal and total organic carbon (TOC) removal. The results of this investigation reveal that the optimum conditions are an initial pH of 10.0, 4377.98mgL-1 initial COD concentration and 25.0 V of potential bias. The model predictions and the test data were in satisfactory agreement. COD and TOC removals of 67% and 82.5%, respectively, were demonstrated. Under the optimal conditions, GC/MS showed 73 organic micro-pollutants in the raw landfill leachate which included hydrocarbons, aromatic compounds and esters. After the landfill leachate treatment processes, 38 organic micro-pollutants disappeared completely in the photoelectrocatalytic process. PMID:28671943

The "caviar" madreporic knee prosthesis.

PubMed

Kenesi, C

1979-01-01

The madreporic ("caviar") prosthesis is a hinged knee prosthesis that can be inserted without the use of cement. The surfaces of the intramedullary stems are constructed with contiguous spheres one mm in diameter. These spaces are filled by bone trabeculae and haversian bone, providing permanent biologic fixation. Experimental madreporic knee arthroplasties in dogs show that bone probes these surfaces and produces solid attachments. Histologically, the trabeculae remain separated from the metal by a fine layer of fibrous tissue. The method of insertion of the prosthesis is simple. Preparing the epiphyses before any bone resection avoids the possibility of rotational positioning errors. The form of the intramedullary stems offers good positioning in the frontal plane. The analysis of an initial series of 15 cases shows results that are far from outstanding. The 2 deaths, the 2 cases of sepsis, and the recuperation of only mediocre motion can be explained, at least in part, by the advanced age of the patients and the poor bone quality of the rheumatoid patients. Nevertheless, this type of prosthesis has 2 important advantages. It avoids the complications from the use of acrylic cement and allows for a revision operation for cases of failed surface replacement designs. Obviously further experimentation with noncemented designs will continue and definitive studies will be reported later.

Optimum Tolerance Design Using Component-Amount and Mixture-Amount Experiments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Piepel, Gregory F.; Ozler, Cenk; Sehirlioglu, Ali Kemal

2013-08-01

One type of tolerance design problem involves optimizing component and assembly tolerances to minimize the total cost (sum of manufacturing cost and quality loss). Previous literature recommended using traditional response surface (RS) designs and models to solve this type of tolerance design problem. In this article, component-amount (CA) and mixture-amount (MA) approaches are proposed as more appropriate for solving this type of tolerance design problem. The advantages of the CA and MA approaches over the RS approach are discussed. Reasons for choosing between the CA and MA approaches are also discussed. The CA and MA approaches (experimental design, response modeling,more » and optimization) are illustrated using real examples.« less

Surface-plasmon resonance-enhanced multiphoton emission of high-brightness electron beams from a nanostructured copper cathode.

PubMed

Li, R K; To, H; Andonian, G; Feng, J; Polyakov, A; Scoby, C M; Thompson, K; Wan, W; Padmore, H A; Musumeci, P

2013-02-15

We experimentally investigate surface-plasmon assisted photoemission to enhance the efficiency of metallic photocathodes for high-brightness electron sources. A nanohole array-based copper surface was designed to exhibit a plasmonic response at 800 nm, fabricated using the focused ion beam milling technique, optically characterized and tested as a photocathode in a high power radio frequency photoinjector. Because of the larger absorption and localization of the optical field intensity, the charge yield observed under ultrashort laser pulse illumination is increased by more than 100 times compared to a flat surface. We also present the first beam characterization results (intrinsic emittance and bunch length) from a nanostructured photocathode.

Hierarchical laser-induced periodic surface structures induced by femtosecond laser on the surface of a ZnO film

NASA Astrophysics Data System (ADS)

Wang, Shaojun; Jiang, Lan; Han, Weina; Hu, Jie; Li, Xiaowei; Wang, Qingsong; Lu, Yongfeng

2018-05-01

We realize hierarchical laser-induced periodic surface structures (LIPSSs) on the surface of a ZnO thin film in a single step by the irradiation of femtosecond laser pulses. The structures are characterized by the high-spatial-frequency LIPSSs (HSFLs) formed on the abnormal bumped low-spatial-frequency LIPSSs (LSFLs). Localized electric-field enhancement based on the initially formed LSFLs is proposed as a potential mechanism for the formation of HSFLs. The simulation results through the finite-difference time-domain method show good agreement with experiments. Furthermore, the crucial role of the LSFLs in the formation of HSFLs is validated by an elaborate experimental design with preprocessed HSFLs.

Design, fabrication and experimental validation of a novel dry-contact sensor for measuring electroencephalography signals without skin preparation.

PubMed

Liao, Lun-De; Wang, I-Jan; Chen, Sheng-Fu; Chang, Jyh-Yeong; Lin, Chin-Teng

2011-01-01

In the present study, novel dry-contact sensors for measuring electro-encephalography (EEG) signals without any skin preparation are designed, fabricated by an injection molding manufacturing process and experimentally validated. Conventional wet electrodes are commonly used to measure EEG signals; they provide excellent EEG signals subject to proper skin preparation and conductive gel application. However, a series of skin preparation procedures for applying the wet electrodes is always required and usually creates trouble for users. To overcome these drawbacks, novel dry-contact EEG sensors were proposed for potential operation in the presence or absence of hair and without any skin preparation or conductive gel usage. The dry EEG sensors were designed to contact the scalp surface with 17 spring contact probes. Each probe was designed to include a probe head, plunger, spring, and barrel. The 17 probes were inserted into a flexible substrate using a one-time forming process via an established injection molding procedure. With these 17 spring contact probes, the flexible substrate allows for high geometric conformity between the sensor and the irregular scalp surface to maintain low skin-sensor interface impedance. Additionally, the flexible substrate also initiates a sensor buffer effect, eliminating pain when force is applied. The proposed dry EEG sensor was reliable in measuring EEG signals without any skin preparation or conductive gel usage, as compared with the conventional wet electrodes.

Design, Fabrication and Experimental Validation of a Novel Dry-Contact Sensor for Measuring Electroencephalography Signals without Skin Preparation

PubMed Central

Liao, Lun-De; Wang, I-Jan; Chen, Sheng-Fu; Chang, Jyh-Yeong; Lin, Chin-Teng

2011-01-01

In the present study, novel dry-contact sensors for measuring electro-encephalography (EEG) signals without any skin preparation are designed, fabricated by an injection molding manufacturing process and experimentally validated. Conventional wet electrodes are commonly used to measure EEG signals; they provide excellent EEG signals subject to proper skin preparation and conductive gel application. However, a series of skin preparation procedures for applying the wet electrodes is always required and usually creates trouble for users. To overcome these drawbacks, novel dry-contact EEG sensors were proposed for potential operation in the presence or absence of hair and without any skin preparation or conductive gel usage. The dry EEG sensors were designed to contact the scalp surface with 17 spring contact probes. Each probe was designed to include a probe head, plunger, spring, and barrel. The 17 probes were inserted into a flexible substrate using a one-time forming process via an established injection molding procedure. With these 17 spring contact probes, the flexible substrate allows for high geometric conformity between the sensor and the irregular scalp surface to maintain low skin-sensor interface impedance. Additionally, the flexible substrate also initiates a sensor buffer effect, eliminating pain when force is applied. The proposed dry EEG sensor was reliable in measuring EEG signals without any skin preparation or conductive gel usage, as compared with the conventional wet electrodes. PMID:22163929

Experimental residual stress evaluation of hydraulic expansion transitions in Alloy 690 steam generator tubing

DOE Office of Scientific and Technical Information (OSTI.GOV)

McGregor, R.; Doherty, P.; Hornbach, D.

1995-12-31

Nuclear Steam Generator (SG) service reliability and longevity have been seriously affected worldwide by corrosion at the tube-to-tubesheet joint expansion. Current SG designs for new facilities and replacement projects enhance corrosion resistance through the use of advanced tubing materials and improved joint design and fabrication techniques. Here, transition zones of hydraulic expansions have undergone detailed experimental evaluation to define residual stress and cold-work distribution on and below the secondary-side surface. Using X-ray diffraction techniques, with supporting finite element analysis, variations are compared in tubing metallurgical condition, tube/pitch geometry, expansion pressure, and tube-to-hole clearance. Initial measurements to characterize the unexpanded tubemore » reveal compressive stresses associated with a thin work-hardened layer on the outer surface of the tube. The gradient of cold-work was measured as 3% to 0% within .001 inch of the surface. The levels and character of residual stresses following hydraulic expansion are primarily dependent on this work-hardened surface layer and initial stress state that is unique to each tube fabrication process. Tensile stresses following expansion are less than 25% of the local yield stress and are found on the transition in a narrow circumferential band at the immediate tube surface (< .0002 inch/0.005 mm depth). The measurements otherwise indicate a predominance of compressive stresses on and below the secondary-side surface of the transition zone. Excellent resistance to SWSCC initiation is offered by the low levels of tensile stress and cold-work. Propagation of any possible cracking would be deterred by the compressive stress field that surrounds this small volume of tensile material.« less

Experimental design to generate strong shear layers in a high-energy-density plasma

NASA Astrophysics Data System (ADS)

Harding, E. C.; Drake, R. P.; Aglitskiy, Y.; Gillespie, R. S.; Grosskopf, M. J.; Weaver, J. L.; Velikovich, A. L.; Visco, A.; Ditmar, J. R.

2010-06-01

The development of a new experimental system for generating a strong shear flow in a high-energy-density plasma is described in detail. The targets were designed with the goal of producing a diagnosable Kelvin-Helmholtz (KH) instability, which plays an important role in the transition turbulence but remains relatively unexplored in the high-energy-density regime. To generate the shear flow the Nike laser was used to drive a flow of Al plasma over a low-density foam surface with an initial perturbation. The interaction of the Al and foam was captured with a spherical crystal imager using 1.86 keV X-rays. The selection of the individual targets components is discussed and results are presented.

Surface pretreatment of plastics with an atmospheric pressure plasma jet - Influence of generator power and kinematics

NASA Astrophysics Data System (ADS)

Moritzer, E.; Leister, C.

2014-05-01

The industrial use of atmospheric pressure plasmas in the plastics processing industry has increased significantly in recent years. Users of this treatment process have the possibility to influence the target values (e.g. bond strength or surface energy) with the help of kinematic and electrical parameters. Until now, systematic procedures have been used with which the parameters can be adapted to the process or product requirements but only by very time-consuming methods. For this reason, the relationship between influencing values and target values will be examined based on the example of a pretreatment in the bonding process with the help of statistical experimental design. Because of the large number of parameters involved, the analysis is restricted to the kinematic and electrical parameters. In the experimental tests, the following factors are taken as parameters: gap between nozzle and substrate, treatment velocity (kinematic data), voltage and duty cycle (electrical data). The statistical evaluation shows significant relationships between the parameters and surface energy in the case of polypropylene. An increase in the voltage and duty cycle increases the polar proportion of the surface energy, while a larger gap and higher velocity leads to lower energy levels. The bond strength of the overlapping bond is also significantly influenced by the voltage, velocity and gap. The direction of their effects is identical with those of the surface energy. In addition to the kinematic influences of the motion of an atmospheric pressure plasma jet, it is therefore especially important that the parameters for the plasma production are taken into account when designing the pretreatment processes.

An experimental investigation devoted to determine heat transfer characteristics in a radiant ceiling heating system

NASA Astrophysics Data System (ADS)

Koca, Aliihsan; Acikgoz, Ozgen; Çebi, Alican; Çetin, Gürsel; Dalkilic, Ahmet Selim; Wongwises, Somchai

2018-02-01

Investigations on heated ceiling method can be considered as a new research area in comparison to the common wall heating-cooling and cooled ceiling methods. In this work, heat transfer characteristics of a heated radiant ceiling system was investigated experimentally. There were different configurations for a single room design in order to determine the convective and radiative heat transfer rates. Almost all details on the arrangement of the test chamber, hydraulic circuit and radiant panels, the measurement equipment and experimental method including uncertainty analysis were revealed in detail indicating specific international standards. Total heat transfer amount from the panels were calculated as the sum of radiation to the unheated surfaces, convection to the air, and conduction heat loss from the backside of the panels. Integral expression of the view factors was calculated by means of the numerical evaluations using Matlab code. By means of this experimental chamber, the radiative, convective and total heat-transfer coefficient values along with the heat flux values provided from the ceiling to the unheated surrounding surfaces have been calculated. Moreover, the details of 28 different experimental case study measurements from the experimental chamber including the convective, radiative and total heat flux, and heat output results are given in a Table for other researchers to validate their theoretical models and empirical correlations.

Experimental and Computational Investigation of a Translating-Throat Single-Expansion-Ramp Nozzle

NASA Technical Reports Server (NTRS)

Deere, Karen A.; Asbury, Scott C.

1999-01-01

An experimental and computational study was conducted on a high-speed, single-expansion-ramp nozzle (SERN) concept designed for efficient off-design performance. The translating-throat SERN concept adjusts the axial location of the throat to provide a variable expansion ratio and allow a more optimum jet exhaust expansion at various flight conditions in an effort to maximize nozzle performance. Three design points (throat locations) were investigated to simulate the operation of this concept at subsonic-transonic, low supersonic, and high supersonic flight conditions. The experimental study was conducted in the jet exit test facility at the Langley Research Center. Internal nozzle performance was obtained at nozzle pressure ratios (NPR's) up to 13 for six nozzles with design nozzle pressure ratios near 9, 42, and 102. Two expansion-ramp surfaces, one concave and one convex, were tested for each design point. Paint-oil flow and focusing schlieren flow visualization techniques were utilized to acquire additional flow data at selected NPR'S. The Navier-Stokes code, PAB3D, was used with a two-equation k-e turbulence model for the computational study. Nozzle performance characteristics were predicted at nozzle pressure ratios of 5, 9, and 13 for the concave ramp, low Mach number nozzle and at 10, 13, and 102 for the concave ramp, high Mach number nozzle.

``Smart'' Surfaces of Polymer Brushes

NASA Astrophysics Data System (ADS)

Wang, Qiang; Meng, Dong

2009-03-01

``Smart'' surfaces, also known as stimuli-responsive surfaces, can change their properties (e.g., wettability, adhesion, friction, elasticity, and biocompatibility) in response to external stimuli (e.g., temperature, pressure, light, solvent selectivity, ionic strength, type of salt, pH, applied electric field, etc.). In this work, we use numerical self-consistent field calculations to study in detail the structure and stimuli- responses of various polymer brushes, including (1) the thermo- response of PNIPAM brushes in water, (2) solvent-response of uncharged diblock copolymer brushes, and (3) the stimuli- response of charged two-component polymer brushes (including both the binary A/B brushes and diblock copolymer A-B brushes) to ionic strength, pH, and applied electric field. Among the many design parameters (e.g., chain lengths, grafting densities, A-B incompatibility, degree of ionization of charged polymers, etc.) we identify those that strongly affect the surface switchability. Such knowledge is useful to the experimental design of these smart polymer brushes for their applications.

Prediction Of Tensile And Shear Strength Of Friction Surfaced Tool Steel Deposit By Using Artificial Neural Networks

NASA Astrophysics Data System (ADS)

Manzoor Hussain, M.; Pitchi Raju, V.; Kandasamy, J.; Govardhan, D.

2018-04-01

Friction surface treatment is well-established solid technology and is used for deposition, abrasion and corrosion protection coatings on rigid materials. This novel process has wide range of industrial applications, particularly in the field of reclamation and repair of damaged and worn engineering components. In this paper, we present the prediction of tensile and shear strength of friction surface treated tool steel using ANN for simulated results of friction surface treatment. This experiment was carried out to obtain tool steel coatings of low carbon steel parts by changing contribution process parameters essentially friction pressure, rotational speed and welding speed. The simulation is performed by a 33-factor design that takes into account the maximum and least limits of the experimental work performed with the 23-factor design. Neural network structures, such as the Feed Forward Neural Network (FFNN), were used to predict tensile and shear strength of tool steel sediments caused by friction.

Pretreatment of rapeseed straw by sodium hydroxide.

PubMed

Kang, Kyeong Eop; Jeong, Gwi-Taek; Park, Don-Hee

2012-06-01

Pretreatment method for rapeseed straw by sodium hydroxide was investigated for production of bioethanol and biobutanol. Various pretreatment parameters, including temperature, time, and sodium hydroxide concentration were optimized using a statistical method which is a central composite design of response surface methodology. In the case of sodium hydroxide pretreatment, optimal pretreatment conditions were found to be 7.9% sodium hydroxide concentration, 5.5 h of reaction time, and 68.4 °C of reaction temperature. The maximum glucose yield which can be recovered by enzymatic hydrolysis at the optimum conditions was 95.7% and the experimental result was 94.0 ± 4.8%. This experimental result was in agreement with the model prediction. An increase of surface area and pore size in pretreated rapeseed straw by sodium hydroxide pretreatment was observed by scanning electron microscope.

Experimental investigation of the cornering of a C40 x 14-21 cantilever aircraft tire

NASA Technical Reports Server (NTRS)

Dreher, R. C.; Tanner, J. A.

1973-01-01

An experimental investigation was conducted at the Langley aircraft landing loads and traction facility to define the cornering characteristics of a size C40 x14-21 aircraft tire of cantilever design. These characteristics, which include the cornering-force and drag-force friction coefficients and self-alining torque, were obtained for the tire operating on dry, damp, and flooded runway surfaces over a range of yaw angles from 0 deg to 20 deg and at ground speeds of 5 to 100 knots, both with and without braking. The results of this investigation show that the cornering-force and drag-force friction coefficients and self-alining torque were influenced by the yaw angle, ground speed, brake torque, surface wetness, and the locked-wheel condition.

A technique for measurement of instantaneous heat transfer in steady-flow ambient-temperature facilities

NASA Technical Reports Server (NTRS)

O'Brien, James E.

1990-01-01

An experimental technique is described for obtaining time-resolved heat flux measurements with high-frequency response (up to 100 kHz) in a steady-flow ambient-temperature facility. The heat transfer test object is preheated and suddenly injected into an established steady flow. Thin-film gages deposited on the test surface detect the unsteady substrate surface temperature. Analog circuitry designed for use in short-duration facilities and based on one-dimensional semiinfinite heat conduction is used to perform the temperature/heat flux transformation. A detailed description of substrate properties, instrumentation, experimental procedure, and data reduction is given, along with representative results obtained in the stagnation region of a circular cylinder subjected to a wake-dominated unsteady flow. An in-depth discussion of related work is also provided.

A closer look at the physical and optical properties of gold nanostars: an experimental and computational study

DOE PAGES

Tsoulos, T. V.; Han, L.; Weir, J.; ...

2017-02-22

A combined experimental and computational study was carried out to design a semi-empirical method to determine the volume, surface area, and extinction coefficients of gold nanostars. The values obtained were confirmed by reconstructing the nanostar 3D topography through high-tilt TEM tomography and introducing the finite elements in COMSOL Multiphysics through which we have also calculated the morphology-dependent extinction coefficient. We have, for the first time, modeled the heat losses of a real, experimentally synthesized nanostar, and found the plasmon resonances to be in excellent agreement with those obtained experimentally. Furthermore, we believe that our approach could substantially improve the applicabilitymore » of this remarkable nanomaterial.« less

A closer look at the physical and optical properties of gold nanostars: an experimental and computational study

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tsoulos, T. V.; Han, L.; Weir, J.

A combined experimental and computational study was carried out to design a semi-empirical method to determine the volume, surface area, and extinction coefficients of gold nanostars. The values obtained were confirmed by reconstructing the nanostar 3D topography through high-tilt TEM tomography and introducing the finite elements in COMSOL Multiphysics through which we have also calculated the morphology-dependent extinction coefficient. We have, for the first time, modeled the heat losses of a real, experimentally synthesized nanostar, and found the plasmon resonances to be in excellent agreement with those obtained experimentally. Furthermore, we believe that our approach could substantially improve the applicabilitymore » of this remarkable nanomaterial.« less

Fabricating Superhydrophobic and Superoleophobic Surfaces with Multiscale Roughness Using Airbrush and Electrospray

NASA Astrophysics Data System (ADS)

AL-Milaji, Karam N.

Examples of superhydrophobic surfaces found in nature such as self-cleaning property of lotus leaf and walking on water ability of water strider have led to an extensive investigation in this area over the past few decades. When a water droplet rests on a textured surface, it may either form a liquid-solid-vapor composite interface by which the liquid droplet partially sits on air pockets or it may wet the surface in which the water replaces the trapped air depending on the surface roughness and the surface chemistry. Super water repellent surfaces have numerous applications in our daily life such as drag reduction, anti-icing, anti-fogging, energy conservation, noise reduction, and self-cleaning. In fact, the same concept could be applied in designing and producing surfaces that repel organic contaminations (e.g. low surface tension liquids). However, superoleophobic surfaces are more challenging to fabricate than superhydrophobic surfaces since the combination of multiscale roughness with re-entrant or overhang structure and surface chemistry must be provided. In this study, simple, cost-effective and potentially scalable techniques, i.e., airbrush and electrospray, were employed for the sake of making superhydrophobic and superoleophobic coatings with random and patterned multiscale surface roughness. Different types of silicon dioxide were utilized in this work to in order to study and to characterize the effect of surface morphology and surface roughness on surface wettability. The experimental findings indicated that super liquid repellent surfaces with high apparent contact angles and extremely low sliding angles were successfully fabricated by combining re-entrant structure, multiscale surface roughness, and low surface energy obtained from chemically treating the fabricated surfaces. In addition to that, the experimental observations regarding producing textured surfaces in mask-assisted electrospray were further validated by simulating the actual working conditions and geometries using COMSOL Multiphysics.

Emmons spot forcing for turbulent drag reduction

NASA Technical Reports Server (NTRS)

Goodman, W. L.

1985-01-01

An Emmons spot-generation wind tunnel system has been designed to trigger closely spaced Emmons spots in the spanwise and longitudinal directions of an aerodynamic surface. For certain combinations of generator frequencies and amplitude, hole size, and hole spacing, experimental results indicate smaller turbulence scales and a reduction in skin friction of about 15 percent.

Broiler litter x industrial by-products reduce nutrients and microbial losses in surface runoff when applied to forages

USDA-ARS?s Scientific Manuscript database

Rainfall simulations were used to determine the effect of broiler litter (BL) treated with N and P immobilizing agents on nutrient losses from a bermudagrass (Cynodon doctylon) hayfield on Marietta silt loam (Fine-loamy, siliceous, active, thermic Fluvaquentic Eutrudepts). The experimental design w...

Structural and functional connectivity as a driver of hillslope erosion following disturbance

Treesearch

C. Jason Williams; Frederick B. Pierson; Pete Robichaud; Osama Z. Al-Hamdan; Jan Boll; Eva K. Strand

2016-01-01

Hydrologic response to rainfall on fragmented or burnt hillslopes is strongly influenced by the ensuing connectivity of runoff and erosion processes. Yet cross-scale process connectivity is seldom evaluated in field studies owing to scale limitations in experimental design. This study quantified surface susceptibility and hydrologic response across point to...

Optimized extraction of polysaccharides from corn silk by pulsed electric field and response surface quadratic design.

PubMed

Zhao, Wenzhu; Yu, Zhipeng; Liu, Jingbo; Yu, Yiding; Yin, Yongguang; Lin, Songyi; Chen, Feng

2011-09-01

Corn silk is a traditional Chinese herbal medicine, which has been widely used for treatment of some diseases. In this study the effects of pulsed electric field on the extraction of polysaccharides from corn silk were investigated. Polysaccharides in corn silk were extracted by pulsed electric field and optimized by response surface methodology (RSM), based on a Box-Behnken design (BBD). Three independent variables, including electric field intensity (kV cm(-1) ), ratio of liquid to raw material and pulse duration (µs), were investigated. The experimental data were fitted to a second-order polynomial equation and also profiled into the corresponding 3-D contour plots. Optimal extraction conditions were as follows: electric field intensity 30 kV cm(-1) , ratio of liquid to raw material 50, and pulse duration 6 µs. Under these condition, the experimental yield of extracted polysaccharides was 7.31% ± 0.15%, matching well with the predicted value. The results showed that a pulsed electric field could be applied to extract value-added products from foods and/or agricultural matrix. Copyright © 2011 Society of Chemical Industry.

Enhanced α-amylase production by a marine protist, Ulkenia sp. using response surface methodology and genetic algorithm.

PubMed

Shirodkar, Priyanka V; Muraleedharan, Usha Devi

2017-11-26

Amylases are a group of enzymes with a wide variety of industrial applications. Enhancement of α-amylase production from the marine protists, thraustochytrids has been attempted for the first time by applying statistical-based experimental designs using response surface methodology (RSM) and genetic algorithm (GA) for optimization of the most influencing process variables. A full factorial central composite experimental design was used to study the cumulative interactive effect of nutritional components viz., glucose, corn starch, and yeast extract. RSM was performed on two objectives, that is, growth of Ulkenia sp. AH-2 (ATCC® PRA-296) and α-amylase activity. When GA was conducted for maximization of the enzyme activity, the optimal α-amylase activity was found to be 71.20 U/mL which was close to that obtained by RSM (71.93 U/mL), both of which were in agreement with the predicted value of 72.37 U/mL. Optimal growth at the optimized process variables was found to be 1.89A 660nm . The optimized medium increased α-amylase production by 1.2-fold.

Spectrophotometric determination of triclosan based on diazotization reaction: response surface optimization using Box-Behnken design.

PubMed

Kaur, Inderpreet; Gaba, Sonal; Kaur, Sukhraj; Kumar, Rajeev; Chawla, Jyoti

2018-05-01

A spectrophotometric method based on diazotization of aniline with triclosan has been developed for the determination of triclosan in water samples. The diazotization process involves two steps: (1) reaction of aniline with sodium nitrite in an acidic medium to form diazonium ion and (2) reaction of diazonium ion with triclosan to form a yellowish-orange azo compound in an alkaline medium. The resulting yellowish-orange product has a maximum absorption at 352 nm which allows the determination of triclosan in aqueous solution in the linear concentration range of 0.1-3.0 μM with R 2 = 0.998. The concentration of hydrochloric acid, sodium nitrite, and aniline was optimized for diazotization reaction to achieve good spectrophotometric determination of triclosan. The optimization of experimental conditions for spectrophotometric determination of triclosan in terms of concentration of sodium nitrite, hydrogen chloride and aniline was also carried out by using Box-Behnken design of response surface methodology and results obtained were in agreement with the experimentally optimized values. The proposed method was then successfully applied for analyses of triclosan content in water samples.

Experimental investigation on the miniature mixed refrigerant cooler driven by a mini-compressor

NASA Astrophysics Data System (ADS)

Chen, Gaofei; Gong, Maoqiong; Wu, Yinong

2018-05-01

Three miniature Joule-Thomson cryogenic coolers and a testing set up were built to investigate the cooling performance in this work. Shell-and-tube heat exchanger and plate fin heat exchangers with rectangular micro channels were designed to achieve high specific surface area. The main processing technology of micro mixed refrigerant cooler (MMRC) was described. The design and fabrication processing of the plate fin heat exchangers were also described. The new developed micro plate-fin type heat exchanger shows high compactness with the specific heat surface larger than 1.0x104 m2/m3. The results of experimental investigations on miniature mixed refrigerant J-T cryogenic coolers driven by a Mini-Compressor were discussed. The performance evaluation and comparison of the three coolers was made to find out the features for each type of cooler. Expressions of refrigeration coefficient and exergy efficiency were pointed out. No-load temperature of about 112 K, and the cooling power of 4.0W at 118K with the input power of 120W is achieved. The exergy efficiency of the SJTC is 5.14%.

Investigation of hydrodynamic characteristics of laminar flow condition around sphere using PIV system

NASA Astrophysics Data System (ADS)

Abed, A. H.; Shcheklein, S. E.

2018-05-01

This paper aims to determine the hydrodynamic characteristics of flow around the sphere in unsteady state condition. An experimental test-rig was designed and constructed for this purpose with the application of an adjusted laser optics system. It is based on the technology of pulsed particle visualization of micro tracers in the cross section per unit time interval. Visualization with Particle Image Velocimetry (PIV-system) is used to study the properties of the flow such as its structure. The PIV-system is the most accepted technique allowed one to measure the instantaneous velocity distribution in fluid applications. In this experimental study, o-ring is used to simulate turbulence on the sphere surface and creates very high-level fluctuations, which creates the flow undergoing a laminar-to-turbulent transition. This transition leads to a delay of the separation point of flow from the sphere surface causing a significant reduction in the drag coefficient, reaching 45%. New results obtained can be useful in the development of numerical validation as well as in design processes.

Comparison of Experimental Surface and Flow Field Measurements to Computational Results of the Juncture Flow Model

NASA Technical Reports Server (NTRS)

Roozeboom, Nettie H.; Lee, Henry C.; Simurda, Laura J.; Zilliac, Gregory G.; Pulliam, Thomas H.

2016-01-01

Wing-body juncture flow fields on commercial aircraft configurations are challenging to compute accurately. The NASA Advanced Air Vehicle Program's juncture flow committee is designing an experiment to provide data to improve Computational Fluid Dynamics (CFD) modeling in the juncture flow region. Preliminary design of the model was done using CFD, yet CFD tends to over-predict the separation in the juncture flow region. Risk reduction wind tunnel tests were requisitioned by the committee to obtain a better understanding of the flow characteristics of the designed models. NASA Ames Research Center's Fluid Mechanics Lab performed one of the risk reduction tests. The results of one case, accompanied by CFD simulations, are presented in this paper. Experimental results suggest the wall mounted wind tunnel model produces a thicker boundary layer on the fuselage than the CFD predictions, resulting in a larger wing horseshoe vortex suppressing the side of body separation in the juncture flow region. Compared to experimental results, CFD predicts a thinner boundary layer on the fuselage generates a weaker wing horseshoe vortex resulting in a larger side of body separation.

Aerodynamic Impact of an Aft-Facing Slat-Step on High Re Airfoils

NASA Astrophysics Data System (ADS)

Kibble, Geoffrey; Petrin, Chris; Jacob, Jamey; Elbing, Brian; Ireland, Peter; Black, Buddy

2016-11-01

Typically, the initial aerodynamic design and subsequent testing and simulation of an aircraft wing assumes an ideal wing surface without imperfections. In reality, however the surface of an in-service aircraft wing rarely matches the surface characteristics of the test wings used during the conceptual design phase and certification process. This disconnect is usually deemed negligible or overlooked entirely. Specifically, many aircraft incorporate a leading edge slat; however, the mating between the slat and the top surface of the wing is not perfectly flush and creates a small aft-facing step behind the slat. In some cases, the slat can create a step as large as one millimeter tall, which is entirely submerged within the boundary layer. This abrupt change in geometry creates a span-wise vortex behind the step and in transonic flow causes a shock to form near the leading edge. This study investigates both experimentally and computationally the implications of an aft-facing slat-step on an aircraft wing and is compared to the ideal wing surface for subsonic and transonic flow conditions. The results of this study are useful for design of flow control modifications for aircraft currently in service and important for improving the next generation of aircraft wings.

Optimization of submerged depth of surface aerators for a carrousel oxidation ditch based on large eddy simulation with Smagorinsky model.

PubMed

Wei, Wenli; Bai, Yu; Liu, Yuling

2016-01-01

This paper is concerned with the simulation and experimental study of hydraulic characteristics in a pilot Carrousel oxidation ditch for the optimization of submerged depth ratio of surface aerators. The simulation was based on the large eddy simulation with the Smagorinsky model, and the velocity was monitored in the ditches with an acoustic Doppler velocimeter method. Comparisons of the simulated velocities and experimental ones show a good agreement, which validates that the accuracy of this simulation is good. The best submerged depth ratio of 2/3 for surface aerators was obtained according to the analysis of the flow field structure, the ratio of gas and liquid in the bottom layer of a ditch, the average velocity of mixture and the flow region with a velocity easily causing sludge deposition under the four operation conditions with submerged depth ratios of 1/3, 1/2, 2/3 and 3/4 for surface aerators. The research result can provide a reference for the design of Carrousel oxidation ditches.

Experimental study on microsphere assisted nanoscope in non-contact mode

NASA Astrophysics Data System (ADS)

Ling, Jinzhong; Li, Dancui; Liu, Xin; Wang, Xiaorui

2018-07-01

Microsphere assisted nanoscope was proposed in existing literatures to capture super-resolution images of the nano-structures beneath the microsphere attached on sample surface. In this paper, a microsphere assisted nanoscope working in non-contact mode is designed and demonstrated, in which the microsphere is controlled with a gap separated to sample surface. With a gap, the microsphere is moved in parallel to sample surface non-invasively, so as to observe all the areas of interest. Furthermore, the influence of gap size on image resolution is studied experimentally. Only when the microsphere is close enough to the sample surface, super-resolution image could be obtained. Generally, the resolution decreases when the gap increases as the contribution of evanescent wave disappears. To keep an appropriate gap size, a quantitative method is implemented to estimate the gap variation by observing Newton's rings around the microsphere, serving as a real-time feedback for tuning the gap size. With a constant gap, large-area image with high resolution can be obtained during microsphere scanning. Our study of non-contact mode makes the microsphere assisted nanoscope more practicable and easier to implement.

Comparison of two surface temperature measurement using thermocouples and infrared camera

NASA Astrophysics Data System (ADS)

Michalski, Dariusz; Strąk, Kinga; Piasecka, Magdalena

This paper compares two methods applied to measure surface temperatures at an experimental setup designed to analyse flow boiling heat transfer. The temperature measurements were performed in two parallel rectangular minichannels, both 1.7 mm deep, 16 mm wide and 180 mm long. The heating element for the fluid flowing in each minichannel was a thin foil made of Haynes-230. The two measurement methods employed to determine the surface temperature of the foil were: the contact method, which involved mounting thermocouples at several points in one minichannel, and the contactless method to study the other minichannel, where the results were provided with an infrared camera. Calculations were necessary to compare the temperature results. Two sets of measurement data obtained for different values of the heat flux were analysed using the basic statistical methods, the method error and the method accuracy. The experimental error and the method accuracy were taken into account. The comparative analysis showed that although the values and distributions of the surface temperatures obtained with the two methods were similar but both methods had certain limitations.

Chip morphology as a performance predictor during high speed end milling of soda lime glass

NASA Astrophysics Data System (ADS)

Bagum, M. N.; Konneh, M.; Abdullah, K. A.; Ali, M. Y.

2018-01-01

Soda lime glass has application in DNA arrays and lab on chip manufacturing. Although investigation revealed that machining of such brittle material is possible using ductile mode under controlled cutting parameters and tool geometry, it remains a challenging task. Furthermore, ability of ductile machining is usually assed through machined surface texture examination. Soda lime glass is a strain rate and temperature sensitive material. Hence, influence on attainment of ductile surface due to adiabatic heat generated during high speed end milling using uncoated tungsten carbide tool is investigated in this research. Experimental runs were designed using central composite design (CCD), taking spindle speed, feed rate and depth of cut as input variable and tool-chip contact point temperature (Ttc) and the surface roughness (Rt) as responses. Along with machined surface texture, Rt and chip morphology was examined to assess machinability of soda lime glass. The relation between Ttc and chip morphology was examined. Investigation showed that around glass transition temperature (Tg) ductile chip produced and subsequently clean and ductile final machined surface produced.

A novel surface imprinted polymer/magnetic hydroxyapatite nanocomposite for selective dibenzothiophene scavenging

NASA Astrophysics Data System (ADS)

Ali, Hager R.; El-Maghrabi, Heba H.; Zahran, Fouad; Moustafa, Yasser Mohamed

2017-12-01

Highly selective adsorbent for dibenzothiophene (DBT) was successfully designed and prepared. Molecularly imprinted polymer (MIP) and magnetic hydroxyapatite (MHAP) were used as building blocks for the novel nanocomposite adsorbent. MIP/MHAP was synthesized by grafting polymerization and surface molecular imprinting using DBT as a template molecule. The microstructure and morphology of the designed nanoadsorbent were examined via FTIR, SEM and VSM. Specific surface area and pore size distribution were determined by Quantachrome Nova 3200S automated gas sorption apparatus. Additionally, static adsorption experiments, isotherms and selective recognition adsorption studies were carried out. Reversed-phase high performance liquid chromatography (RP-HPLC) was used to determine DBT. The experimental data exhibits excellent adsorption capacity for DBT reaches 247 mg/g within 60 min. Competitive adsorption results proved that MIP/MHAP have a greater affinity towards DBT molecules than benzothiophene analogues. Pseudo-second-order model and the Langmuir isotherm were used to describe the adsorption process.

Use of Mixture Designs to Investigate Contribution of Minor Sex Pheromone Components to Trap Catch of the Carpenterworm Moth, Chilecomadia valdiviana.

PubMed

Lapointe, Stephen L; Barros-Parada, Wilson; Fuentes-Contreras, Eduardo; Herrera, Heidy; Kinsho, Takeshi; Miyake, Yuki; Niedz, Randall P; Bergmann, Jan

2017-12-01

Field experiments were carried out to study responses of male moths of the carpenterworm, Chilecomadia valdiviana (Lepidoptera: Cossidae), a pest of tree and fruit crops in Chile, to five compounds previously identified from the pheromone glands of females. Previously, attraction of males to the major component, (7Z,10Z)-7,10-hexadecadienal, was clearly demonstrated while the role of the minor components was uncertain due to the use of an experimental design that left large portions of the design space unexplored. We used mixture designs to study the potential contributions to trap catch of the four minor pheromone components produced by C. valdiviana. After systematically exploring the design space described by the five pheromone components, we concluded that the major pheromone component alone is responsible for attraction of male moths in this species. The need for appropriate experimental designs to address the problem of assessing responses to mixtures of semiochemicals in chemical ecology is described. We present an analysis of mixture designs and response surface modeling and an explanation of why this approach is superior to commonly used, but statistically inappropriate, designs.

The Pliocene Model Intercomparison Project (PlioMIP) Phase 2: scientific objectives and experimental design

NASA Astrophysics Data System (ADS)

Haywood, Alan M.; Dowsett, Harry J.; Dolan, Aisling M.; Rowley, David; Abe-Ouchi, Ayako; Otto-Bliesner, Bette; Chandler, Mark A.; Hunter, Stephen J.; Lunt, Daniel J.; Pound, Matthew; Salzmann, Ulrich

2016-03-01

The Pliocene Model Intercomparison Project (PlioMIP) is a co-ordinated international climate modelling initiative to study and understand climate and environments of the Late Pliocene, as well as their potential relevance in the context of future climate change. PlioMIP examines the consistency of model predictions in simulating Pliocene climate and their ability to reproduce climate signals preserved by geological climate archives. Here we provide a description of the aim and objectives of the next phase of the model intercomparison project (PlioMIP Phase 2), and we present the experimental design and boundary conditions that will be utilized for climate model experiments in Phase 2. Following on from PlioMIP Phase 1, Phase 2 will continue to be a mechanism for sampling structural uncertainty within climate models. However, Phase 1 demonstrated the requirement to better understand boundary condition uncertainties as well as uncertainty in the methodologies used for data-model comparison. Therefore, our strategy for Phase 2 is to utilize state-of-the-art boundary conditions that have emerged over the last 5 years. These include a new palaeogeographic reconstruction, detailing ocean bathymetry and land-ice surface topography. The ice surface topography is built upon the lessons learned from offline ice sheet modelling studies. Land surface cover has been enhanced by recent additions of Pliocene soils and lakes. Atmospheric reconstructions of palaeo-CO2 are emerging on orbital timescales, and these are also incorporated into PlioMIP Phase 2. New records of surface and sea surface temperature change are being produced that will be more temporally consistent with the boundary conditions and forcings used within models. Finally we have designed a suite of prioritized experiments that tackle issues surrounding the basic understanding of the Pliocene and its relevance in the context of future climate change in a discrete way.

The Pliocene Model Intercomparison Project (PlioMIP) Phase 2: Scientific Objectives and Experimental Design

NASA Technical Reports Server (NTRS)

Haywood, Alan M.; Dowsett, Harry J.; Dolan, Aisling M.; Rowley, David; Abe-Ouchi, Ayako; Otto-Bliesner, Bette; Chandler, Mark A.; Hunter, Stephen J.; Lunt, Daniel J.; Pound, Matthew;

Phononic crystal diffraction gratings

NASA Astrophysics Data System (ADS)

Moiseyenko, Rayisa P.; Herbison, Sarah; Declercq, Nico F.; Laude, Vincent

2012-02-01

When a phononic crystal is interrogated by an external source of acoustic waves, there is necessarily a phenomenon of diffraction occurring on the external enclosing surfaces. Indeed, these external surfaces are periodic and the resulting acoustic diffraction grating has a periodicity that depends on the orientation of the phononic crystal. This work presents a combined experimental and theoretical study on the diffraction of bulk ultrasonic waves on the external surfaces of a 2D phononic crystal that consists of a triangular lattice of steel rods in a water matrix. The results of transmission experiments are compared with theoretical band structures obtained with the finite-element method. Angular spectrograms (showing frequency as a function of angle) determined from diffraction experiments are then compared with finite-element simulations of diffraction occurring on the surfaces of the crystal. The experimental results show that the diffraction that occurs on its external surfaces is highly frequency-dependent and has a definite relation with the Bloch modes of the phononic crystal. In particular, a strong influence of the presence of bandgaps and deaf bands on the diffraction efficiency is found. This observation opens perspectives for the design of efficient phononic crystal diffraction gratings.

Application of Statistical Design for the Production of Cellulase by Trichoderma reesei Using Mango Peel.

PubMed

Saravanan, P; Muthuvelayudham, R; Viruthagiri, T

2012-01-01

Optimization of the culture medium for cellulase production using Trichoderma reesei was carried out. The optimization of cellulase production using mango peel as substrate was performed with statistical methodology based on experimental designs. The screening of nine nutrients for their influence on cellulase production is achieved using Plackett-Burman design. Avicel, soybean cake flour, KH(2)PO(4), and CoCl(2)·6H(2)O were selected based on their positive influence on cellulase production. The composition of the selected components was optimized using Response Surface Methodology (RSM). The optimum conditions are as follows: Avicel: 25.30 g/L, Soybean cake flour: 23.53 g/L, KH(2)PO(4): 4.90 g/L, and CoCl(2)·6H(2)O: 0.95 g/L. These conditions are validated experimentally which revealed an enhanced Cellulase activity of 7.8 IU/mL.

Numerical analysis of the beam position monitor pickup for the Iranian light source facility

NASA Astrophysics Data System (ADS)

Shafiee, M.; Feghhi, S. A. H.; Rahighi, J.

2017-03-01

In this paper, we describe the design of a button type Beam Position Monitor (BPM) for the low emittance storage ring of the Iranian Light Source Facility (ILSF). First, we calculate sensitivities, induced power and intrinsic resolution based on solving Laplace equation numerically by finite element method (FEM), in order to find the potential at each point of BPM's electrode surface. After the optimization of the designed BPM, trapped high order modes (HOM), wakefield and thermal loss effects are calculated. Finally, after fabrication of BPM, it is experimentally tested by using a test-stand. The results depict that the designed BPM has a linear response in the area of 2×4 mm2 inside the beam pipe and the sensitivity of 0.080 and 0.087 mm-1 in horizontal and vertical directions. Experimental results also depict that they are in a good agreement with numerical analysis.

Optimum surface roughness prediction for titanium alloy by adopting response surface methodology

NASA Astrophysics Data System (ADS)

Yang, Aimin; Han, Yang; Pan, Yuhang; Xing, Hongwei; Li, Jinze

Titanium alloy has been widely applied in industrial engineering products due to its advantages of great corrosion resistance and high specific strength. This paper investigated the processing parameters for finish turning of titanium alloy TC11. Firstly, a three-factor central composite design of experiment, considering the cutting speed, feed rate and depth of cut, are conducted in titanium alloy TC11 and the corresponding surface roughness are obtained. Then a mathematic model is constructed by the response surface methodology to fit the relationship between the process parameters and the surface roughness. The prediction accuracy was verified by the one-way ANOVA. Finally, the contour line of the surface roughness under different combination of process parameters are obtained and used for the optimum surface roughness prediction. Verification experimental results demonstrated that material removal rate (MRR) at the obtained optimum can be significantly improved without sacrificing the surface roughness.

Composite Behavior of Insulated Concrete Sandwich Wall Panels Subjected to Wind Pressure and Suction.

PubMed

Choi, Insub; Kim, JunHee; Kim, Ho-Ryong

2015-03-19

A full-scale experimental test was conducted to analyze the composite behavior of insulated concrete sandwich wall panels (ICSWPs) subjected to wind pressure and suction. The experimental program was composed of three groups of ICSWP specimens, each with a different type of insulation and number of glass-fiber-reinforced polymer (GFRP) shear grids. The degree of composite action of each specimen was analyzed according to the load direction, type of the insulation, and number of GFRP shear grids by comparing the theoretical and experimental values. The failure modes of the ICSWPs were compared to investigate the effect of bonds according to the load direction and type of insulation. Bonds based on insulation absorptiveness were effective to result in the composite behavior of ICSWP under positive loading tests only, while bonds based on insulation surface roughness were effective under both positive and negative loading tests. Therefore, the composite behavior based on surface roughness can be applied to the calculation of the design strength of ICSWPs with continuous GFRP shear connectors.

Adsorption of Cationic Peptides to Solid Surfaces of Glass and Plastic

PubMed Central

Kristensen, Kasper; Henriksen, Jonas R.; Andresen, Thomas L.

2015-01-01

Cationic membrane-active peptides have been studied for years in the hope of developing them into novel types of therapeutics. In this article, we investigate an effect that might have significant experimental implications for investigators who wish to study these peptides, namely, that the peptides adsorb to solid surfaces of glass and plastic. Specifically, we use analytical HPLC to systematically quantify the adsorption of the three cationic membrane-active peptides mastoparan X, melittin, and magainin 2 to the walls of commonly used glass and plastic sample containers. Our results show that, at typical experimental peptide concentrations, 90% or more of the peptides might be lost from solution due to rapid adsorption to the walls of the sample containers. Thus, our results emphasize that investigators should always keep these adsorption effects in mind when designing and interpreting experiments on cationic membrane-active peptides. We conclude the article by discussing different strategies for reducing the experimental impact of these adsorption effects. PMID:25932639

Analysis and design of negative resistance oscillators using surface transverse wave-based single port resonators.

PubMed

Avramov, Ivan D

2003-03-01

This practically oriented paper presents the fundamentals for analysis, optimization, and design of negative resistance oscillators (NRO) stabilized with surface transverse wave (STW)-based single-port resonators (SPR). Data on a variety of high-Q, low-loss SPR devices in the 900- to 2000-MHz range, suitable for NRO applications, are presented, and a simple method for SPR parameter extraction through Pi-circuit measurements is outlined. Negative resistance analysis, based on S-parameter data of the active device, is performed on a tuned-base, grounded collector transistor NRO, known for its good stability and tuning at microwave frequencies. By adding a SPR in the emitter network, the static transducer capacitance is absorbed by the circuit and is used to generate negative resistance only over the narrow bandwidth of the acoustic device, eliminating the risk of spurious oscillations. The analysis allows exact prediction of the oscillation frequency, tuning range, loaded Q, and excess gain. Simulation and experimental data on a 915-MHz fixed-frequency NRO and a wide tuning range, voltage-controlled STW oscillator, built and tested experimentally, are presented. Practical design aspects including the choice of transistor, negative feedback circuits, load coupling, and operation at the highest phase slope for minimum phase noise are discussed.

Use of response surface methodology in a fed-batch process for optimization of tricarboxylic acid cycle intermediates to achieve high levels of canthaxanthin from Dietzia natronolimnaea HS-1.

PubMed

Nasri Nasrabadi, Mohammad Reza; Razavi, Seyed Hadi

2010-04-01

In this work, we applied statistical experimental design to a fed-batch process for optimization of tricarboxylic acid cycle (TCA) intermediates in order to achieve high-level production of canthaxanthin from Dietzia natronolimnaea HS-1 cultured in beet molasses. A fractional factorial design (screening test) was first conducted on five TCA cycle intermediates. Out of the five TCA cycle intermediates investigated via screening tests, alfaketoglutarate, oxaloacetate and succinate were selected based on their statistically significant (P<0.05) and positive effects on canthaxanthin production. These significant factors were optimized by means of response surface methodology (RSM) in order to achieve high-level production of canthaxanthin. The experimental results of the RSM were fitted with a second-order polynomial equation by means of a multiple regression technique to identify the relationship between canthaxanthin production and the three TCA cycle intermediates. By means of this statistical design under a fed-batch process, the optimum conditions required to achieve the highest level of canthaxanthin (13172 + or - 25 microg l(-1)) were determined as follows: alfaketoglutarate, 9.69 mM; oxaloacetate, 8.68 mM; succinate, 8.51 mM. Copyright 2009 The Society for Biotechnology, Japan. Published by Elsevier B.V. All rights reserved.

Conceptual Design and Architecture of Mars Exploration Rover (MER) for Seismic Experiments Over Martian Surfaces

NASA Astrophysics Data System (ADS)

Garg, Akshay; Singh, Amit

2012-07-01

Keywords: MER, Mars, Rover, Seismometer Mars has been a subject of human interest for exploration missions for quite some time now. Both rover as well as orbiter missions have been employed to suit mission objectives. Rovers have been preferentially deployed for close range reconnaissance and detailed experimentation with highest accuracy. However, it is essential to strike a balance between the chosen science objectives and the rover operations as a whole. The objective of this proposed mechanism is to design a vehicle (MER) to carry out seismic studies over Martian surface. The conceptual design consists of three units i.e. Mother Rover as a Surrogate (Carrier) and Baby Rovers (two) as seeders for several MEMS-based accelerometer / seismometer units (Nodes). Mother Rover can carry these Baby Rovers, having individual power supply with solar cells and with individual data transmission capabilities, to suitable sites such as Chasma associated with Valles Marineris, Craters or Sand Dunes. Mother rover deploys these rovers in two opposite direction and these rovers follow a triangulation pattern to study shock waves generated through firing tungsten carbide shells into the ground. Till the time of active experiments Mother Rover would act as a guiding unit to control spatial spread of detection instruments. After active shock experimentation, the babies can still act as passive seismometer units to study and record passive shocks from thermal quakes, impact cratering & landslides. Further other experiments / payloads (XPS / GAP / APXS) can also be carried by Mother Rover. Secondary power system consisting of batteries can also be utilized for carrying out further experiments over shallow valley surfaces. The whole arrangement is conceptually expected to increase the accuracy of measurements (through concurrent readings) and prolong life cycle of overall experimentation. The proposed rover can be customised according to the associated scientific objectives and further needs.

Vacuum insulation of the high energy negative ion source for fusion application

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kojima, A.; Hanada, M.; Inoue, T.

2012-02-15

Vacuum insulation on a large size negative ion accelerator with multiple extraction apertures and acceleration grids for fusion application was experimentally examined and designed. In the experiment, vacuum insulation characteristics were investigated in the JT-60 negative ion source with >1000 apertures on the grid with the surface area of {approx}2 m{sup 2}. The sustainable voltages varied with a square root of the gap lengths between the grids, and decreased with number of the apertures and with the surface area of the grids. Based on the obtained results, the JT-60SA (super advanced) negative ion source is designed to produce 22 A,more » 500 keV D{sup -} ion beams for 100 s.« less

Response surface methodology for the optimization of sludge solubilization by ultrasonic pre-treatment

NASA Astrophysics Data System (ADS)

Zheng, Mingyue; Zhang, Xiaohui; Lu, Peng; Cao, Qiguang; Yuan, Yuan; Yue, Mingxing; Fu, Yiwei; Wu, Libin

2018-02-01

The present study examines the optimization of the ultrasonic pre-treatment conditions with response surface experimental design in terms of sludge disintegration efficiency (solubilisation of organic components). Ultrasonic pre-treatment for the maximum solubilization with residual sludge enhanced the SCOD release. Optimization of the ultrasonic pre-treatment was conducted through a Box-Behnken design (three variables, a total of 17 experiments) to determine the effects of three independent variables (power, residence time and TS) on COD solubilization of sludge. The optimal COD was obtained at 17349.4mg/L, when the power was 534.67W, the time was 10.77, and TS was 2%, while the SE of this condition was 28792J/kg TS.

An analytical approach to test and design upper limb prosthesis.

PubMed

Veer, Karan

2015-01-01

In this work the signal acquiring technique, the analysis models and the design protocols of the prosthesis are discussed. The different methods to estimate the motion intended by the amputee from surface electromyogram (SEMG) signals based on time and frequency domain parameters are presented. The experiment proposed that the used techniques can help significantly in discriminating the amputee's motions among four independent activities using dual channel set-up. Further, based on experimental results, the design and working of an artificial arm have been covered under two constituents--the electronics design and the mechanical assembly. Finally, the developed hand prosthesis allows the amputated persons to perform daily routine activities easily.

Distinct ice patterns on solid surfaces with various wettabilities

PubMed Central

Liu, Jie; Zhu, Chongqin; Liu, Kai; Jiang, Ying; Song, Yanlin; Francisco, Joseph S.; Zeng, Xiao Cheng; Wang, Jianjun

2017-01-01

No relationship has been established between surface wettability and ice growth patterns, although ice often forms on top of solid surfaces. Here, we report experimental observations obtained using a process specially designed to avoid the influence of nucleation and describe the wettability-dependent ice morphology on solid surfaces under atmospheric conditions and the discovery of two growth modes of ice crystals: along-surface and off-surface growth modes. Using atomistic molecular dynamics simulation analysis, we show that these distinct ice growth phenomena are attributable to the presence (or absence) of bilayer ice on solid surfaces with different wettability; that is, the formation of bilayer ice on hydrophilic surface can dictate the along-surface growth mode due to the structural match between the bilayer hexagonal ice and the basal face of hexagonal ice (ice Ih), thereby promoting rapid growth of nonbasal faces along the hydrophilic surface. The dramatically different growth patterns of ice on solid surfaces are of crucial relevance to ice repellency surfaces. PMID:29073045

Distinct ice patterns on solid surfaces with various wettabilities.

PubMed

Liu, Jie; Zhu, Chongqin; Liu, Kai; Jiang, Ying; Song, Yanlin; Francisco, Joseph S; Zeng, Xiao Cheng; Wang, Jianjun

2017-10-24

No relationship has been established between surface wettability and ice growth patterns, although ice often forms on top of solid surfaces. Here, we report experimental observations obtained using a process specially designed to avoid the influence of nucleation and describe the wettability-dependent ice morphology on solid surfaces under atmospheric conditions and the discovery of two growth modes of ice crystals: along-surface and off-surface growth modes. Using atomistic molecular dynamics simulation analysis, we show that these distinct ice growth phenomena are attributable to the presence (or absence) of bilayer ice on solid surfaces with different wettability; that is, the formation of bilayer ice on hydrophilic surface can dictate the along-surface growth mode due to the structural match between the bilayer hexagonal ice and the basal face of hexagonal ice (ice I h ), thereby promoting rapid growth of nonbasal faces along the hydrophilic surface. The dramatically different growth patterns of ice on solid surfaces are of crucial relevance to ice repellency surfaces. Published under the PNAS license.

Creating unconventional geometric beams with large depth of field using double freeform-surface optics.

PubMed

Feng, Zexin; Froese, Brittany D; Huang, Chih-Yu; Ma, Donglin; Liang, Rongguang

2015-07-10

We consider here creation of an unconventional flattop beam with a large depth of field by employing double freeform optical surfaces. The output beam is designed with continuous variations from the flattop to almost zero near the edges to resist the influence of diffraction on its propagation. We solve this challenging problem by naturally incorporating an optimal transport map computation scheme for unconventional boundary conditions with a simultaneous point-by-point double surface construction procedure. We demonstrate experimentally the generation of a long-range propagated triangular beam through a plano-freeform lens pair fabricated by a diamond-tuning machine.

Investigation of high voltage spacecraft system interactions with plasma environments

NASA Technical Reports Server (NTRS)

Stevens, N. J.; Berkopec, F. D.; Purvis, C. K.; Grier, N.; Staskus, J. V.

1978-01-01

An experimental investigation was undertaken for insulator and conductor test surfaces biased up to + or - 1kV in a simulated low earth orbit charged particle environment. It was found that these interactions are controlled by the insulator surfaces surrounding the biased conductors. For positive applied voltages the electron current collection can be enhanced by the insulators. For negative applied voltages the insulator surface confines the voltage to the conductor region. Understanding these interactions and the technology to control their impact on system operation is essential to the design of solar cell arrays for ion drive propulsion applications that use direct drive power processing.

Sub-microradian Surface Slope Metrology with the ALS Developmental Long Trace Profiler

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yashchuk, Valeriy V; Barber, Samuel; Domning, Edward E.

2009-09-11

A new low budget slope measuring instrument, the Developmental Long Trace Profiler (DLTP), was recently brought to operation at the ALS Optical Metrology Laboratory. The design, instrumental control and data acquisition system, initial alignment and calibration procedures, as well as the developed experimental precautions and procedures are described in detail. The capability of the DLTP to achieve sub-microradian surface slope metrology is verified via cross-comparison measurements with other high performance slope measuring instruments when measuring the same high quality test optics. The directions of future work to develop a surface slope measuring profiler with nano-radian performance are also discussed.

Development of an Integrated Nozzle for a Symmetric, RBCC Launch Vehicle Configuration

NASA Technical Reports Server (NTRS)

Smith, Timothy D.; Canabal, Francisco, III; Rice, Tharen; Blaha, Bernard

2000-01-01

The development of rocket based combined cycle (RBCC) engines is highly dependent upon integrating several different modes of operation into a single system. One of the key components to develop acceptable performance levels through each mode of operation is the nozzle. It must be highly integrated to serve the expansion processes of both rocket and air-breathing modes without undue weight, drag, or complexity. The NASA GTX configuration requires a fixed geometry, altitude-compensating nozzle configuration. The initial configuration, used mainly to estimate weight and cooling requirements was a 1 So half-angle cone, which cuts a concave surface from a point within the flowpath to the vehicle trailing edge. Results of 3-D CFD calculations on this geometry are presented. To address the critical issues associated with integrated, fixed geometry, multimode nozzle development, the GTX team has initiated a series of tasks to evolve the nozzle design, and validate performance levels. An overview of these tasks is given. The first element is a design activity to develop tools for integration of efficient expansion surfaces With the existing flowpath and vehicle aft-body, and to develop a second-generation nozzle design. A preliminary result using a "streamline-tracing" technique is presented. As the nozzle design evolves, a combination of 3-D CFD analysis and experimental evaluation will be used to validate the design procedure and determine the installed performance for propulsion cycle modeling. The initial experimental effort will consist of cold-flow experiments designed to validate the general trends of the streamline-tracing methodology and anchor the CFD analysis. Experiments will also be conducted to simulate nozzle performance during each mode of operation. As the design matures, hot-fire tests will be conducted to refine performance estimates and anchor more sophisticated reacting-flow analysis.

Polarization-selective optical transmission through a plasmonic metasurface.

PubMed

Pelzman, Charles; Cho, Sang-Yeon

2015-06-22

We present the design, fabrication, and experimental characterization of a nanoslit-based metasurface that offers polarization-selective optical transmission for advanced imaging applications. The metasurface consists of an array of meta-atoms, constructed with two orthogonally coupled subwavelength apertures. Highly enhanced optical transmission was achieved by selective excitation of surface plasmon waves on the metasurface. By rotating the orientation of the linearly polarized incident beam, switching of enhanced optical transmission bands through the metasurface was experimentally demonstrated. This demonstration is a significant step towards developing advanced multispectral imaging devices.

Experimental validation of thermo-chemical algorithm for a simulation of pultrusion processes

NASA Astrophysics Data System (ADS)

Barkanov, E.; Akishin, P.; Miazza, N. L.; Galvez, S.; Pantelelis, N.

2018-04-01

To provide better understanding of the pultrusion processes without or with temperature control and to support the pultrusion tooling design, an algorithm based on the mixed time integration scheme and nodal control volumes method has been developed. At present study its experimental validation is carried out by the developed cure sensors measuring the electrical resistivity and temperature on the profile surface. By this verification process the set of initial data used for a simulation of the pultrusion process with rod profile has been successfully corrected and finally defined.

Polarization-selective optical transmission through a plasmonic metasurface

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pelzman, Charles; Cho, Sang-Yeon, E-mail: sangycho@nmsu.edu

2015-06-22

We present the design, fabrication, and experimental characterization of a nanoslit-based metasurface that offers polarization-selective optical transmission for advanced imaging applications. The metasurface consists of an array of meta-atoms, constructed with two orthogonally coupled subwavelength apertures. Highly enhanced optical transmission was achieved by selective excitation of surface plasmon waves on the metasurface. By rotating the orientation of the linearly polarized incident beam, switching of enhanced optical transmission bands through the metasurface was experimentally demonstrated. This demonstration is a significant step towards developing advanced multispectral imaging devices.

Nanoscale Fe/Ag particles activated persulfate: optimization using response surface methodology.

PubMed

Silveira, Jefferson E; Barreto-Rodrigues, Marcio; Cardoso, Tais O; Pliego, Gema; Munoz, Macarena; Zazo, Juan A; Casas, José A

2017-05-01

This work studied the bimetallic nanoparticles Fe-Ag (nZVI-Ag) activated persulfate (PS) in aqueous solution using response surface methodology. The Box-Behnken design (BBD) was employed to optimize three parameters (nZVI-Ag dose, reaction temperature, and PS concentration) using 4-chlorophenol (4-CP) as the target pollutant. The synthesis of nZVI-Ag particles was carried out through a reduction of FeCl 2 with NaBH 4 followed by reductive deposition of Ag. The catalyst was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Brunauer-Emmett-Teller (BET) surface area. The BBD was considered a satisfactory model to optimize the process. Confirmatory tests were carried out using predicted and experimental values under the optimal conditions (50 mg L -1 nZVI-Ag, 21 mM PS at 57 °C) and the complete removal of 4-CP achieved experimentally was successfully predicted by the model, whereas the mineralization degree predicted (90%) was slightly overestimated against the measured data (83%).

Ship wakes and spectrograms: mathematical modelling and experimental data for finite-depth flows

NASA Astrophysics Data System (ADS)

McCue, Scott; Pethiyagoda, Ravindra; Moroney, Timothy; Macfarlane, Gregor; Binns, Jonathan

2017-11-01

We are concerned with how properties of a ship wake can be extracted from surface height data collected at a single point as the ship travels past. The tool we use is a spectrogram, which is a heat map that visualises the time-dependent frequency spectrum of the surface height signal. In this talk, the focus will be on presenting the theoretical framework which involves an idealised mathematical model with a pressure distribution applied to the surface. A geometric argument based on linear water wave theory provides encouraging results for both subcritical and supercritical flow regimes. We then summarise some recent findings obtained by comparing our analysis to experimental data collected at the Australian Maritime College for various sailing speeds and hull shapes*. Our work has the potential to inform ship design, the detection of irregular vessels, and how coastal damage is attributed to specific vessels in shipping channels. We acknowledge support of the Australian Research Council via the Discovery Project DP140100933.

Designing transition metal surfaces for their adsorption properties and chemical reactivity

NASA Astrophysics Data System (ADS)

Montemore, Matthew M.

Many technological processes, such as catalysis, electrochemistry, corrosion, and some materials synthesis techniques, involve molecules bonding to and/or reacting on surfaces. For many of these applications, transition metals have proven to have excellent chemical reactivity, and this reactivity is strongly tied to the surface's adsorption properties. This thesis focuses on predicting adsorption properties for use in the design of transition metal surfaces for various applications. First, it is shown that adsorption through a particular atom (e.g, C or O) can be treated in a unified way. This allows predictions of all C-bound adsorbates from a single, simple adsorbate, such as CH3. In particular, consideration of the adsorption site can improve the applicability of previous approaches, and gas-phase bond energies correlate with adsorption energies for similarly bound adsorbates. Next, a general framework is presented for understanding and predicting adsorption through any atom. The energy of the adsorbate's highest occupied molecular orbital (HOMO) determines the strength of the repulsion between the adsorbate and the surface. Because adsorbates with similar HOMO energies behave similarly, their adsorption energies correlate. This can improve the efficiency of predictions, but more importantly it constrains catalyst design and suggests strategies for circumventing these constraints. Further, the behavior of adsorbates with dissimilar HOMO energies varies in a systematic way, allowing predictions of adsorption energy differences between any two adsorbates. These differences are also useful in surface design. In both of these cases, the dependence of adsorption energies on surface electronic properties is explored. This dependence is used to justify the unified treatments mentioned above, and is used to gain further insight into adsorption. The properties of the surface's d band and p band control variations in adsorption energy, as does the strength of the adsorbate-surface coupling. A single equation, with only a single adsorbate-dependent fitting parameter as well as a few universal fitting parameters, is developed that can predict the adsorption energy of any radical on any close-packed transition metal surface. The surface electronic properties that are input into this equation can be estimated based on the alloy structure of the surface, improving prospects for high-throughput screening and rational catalyst design. The methods discussed in this thesis are used to design a novel catalyst for ethylene epoxidation, which is experimentally synthesized and tested. Initial tests indicate that this catalyst may have improved selectivity over pure Ag.

Experimental design and statistical analysis for three-drug combination studies.

PubMed

Fang, Hong-Bin; Chen, Xuerong; Pei, Xin-Yan; Grant, Steven; Tan, Ming

2017-06-01

Drug combination is a critically important therapeutic approach for complex diseases such as cancer and HIV due to its potential for efficacy at lower, less toxic doses and the need to move new therapies rapidly into clinical trials. One of the key issues is to identify which combinations are additive, synergistic, or antagonistic. While the value of multidrug combinations has been well recognized in the cancer research community, to our best knowledge, all existing experimental studies rely on fixing the dose of one drug to reduce the dimensionality, e.g. looking at pairwise two-drug combinations, a suboptimal design. Hence, there is an urgent need to develop experimental design and analysis methods for studying multidrug combinations directly. Because the complexity of the problem increases exponentially with the number of constituent drugs, there has been little progress in the development of methods for the design and analysis of high-dimensional drug combinations. In fact, contrary to common mathematical reasoning, the case of three-drug combinations is fundamentally more difficult than two-drug combinations. Apparently, finding doses of the combination, number of combinations, and replicates needed to detect departures from additivity depends on dose-response shapes of individual constituent drugs. Thus, different classes of drugs of different dose-response shapes need to be treated as a separate case. Our application and case studies develop dose finding and sample size method for detecting departures from additivity with several common (linear and log-linear) classes of single dose-response curves. Furthermore, utilizing the geometric features of the interaction index, we propose a nonparametric model to estimate the interaction index surface by B-spine approximation and derive its asymptotic properties. Utilizing the method, we designed and analyzed a combination study of three anticancer drugs, PD184, HA14-1, and CEP3891 inhibiting myeloma H929 cell line. To our best knowledge, this is the first ever three drug combinations study performed based on the original 4D dose-response surface formed by dose ranges of three drugs.

Application of the experimental design of experiments (DoE) for the determination of organotin compounds in water samples using HS-SPME and GC-MS/MS.

PubMed

Coscollà, Clara; Navarro-Olivares, Santiago; Martí, Pedro; Yusà, Vicent

2014-02-01

When attempting to discover the important factors and then optimise a response by tuning these factors, experimental design (design of experiments, DoE) gives a powerful suite of statistical methodology. DoE identify significant factors and then optimise a response with respect to them in method development. In this work, a headspace-solid-phase micro-extraction (HS-SPME) combined with gas chromatography tandem mass spectrometry (GC-MS/MS) methodology for the simultaneous determination of six important organotin compounds namely monobutyltin (MBT), dibutyltin (DBT), tributyltin (TBT), monophenyltin (MPhT), diphenyltin (DPhT), triphenyltin (TPhT) has been optimized using a statistical design of experiments (DOE). The analytical method is based on the ethylation with NaBEt4 and simultaneous headspace-solid-phase micro-extraction of the derivative compounds followed by GC-MS/MS analysis. The main experimental parameters influencing the extraction efficiency selected for optimization were pre-incubation time, incubation temperature, agitator speed, extraction time, desorption temperature, buffer (pH, concentration and volume), headspace volume, sample salinity, preparation of standards, ultrasonic time and desorption time in the injector. The main factors (excitation voltage, excitation time, ion source temperature, isolation time and electron energy) affecting the GC-IT-MS/MS response were also optimized using the same statistical design of experiments. The proposed method presented good linearity (coefficient of determination R(2)>0.99) and repeatibilty (1-25%) for all the compounds under study. The accuracy of the method measured as the average percentage recovery of the compounds in spiked surface and marine waters was higher than 70% for all compounds studied. Finally, the optimized methodology was applied to real aqueous samples enabled the simultaneous determination of all compounds under study in surface and marine water samples obtained from Valencia region (Spain). © 2013 Elsevier B.V. All rights reserved.

Tuning and predicting the wetting of nanoengineered material surface

NASA Astrophysics Data System (ADS)

Ramiasa-MacGregor, M.; Mierczynska, A.; Sedev, R.; Vasilev, K.

2016-02-01

The wetting of a material can be tuned by changing the roughness on its surface. Recent advances in the field of nanotechnology open exciting opportunities to control macroscopic wetting behaviour. Yet, the benchmark theories used to describe the wettability of macroscopically rough surfaces fail to fully describe the wetting behaviour of systems with topographical features at the nanoscale. To shed light on the events occurring at the nanoscale we have utilised model gradient substrata where surface nanotopography was tailored in a controlled and robust manner. The intrinsic wettability of the coatings was varied from hydrophilic to hydrophobic. The measured water contact angle could not be described by the classical theories. We developed an empirical model that effectively captures the experimental data, and further enables us to predict the wetting of surfaces with nanoscale roughness by considering the physical and chemical properties of the material. The fundamental insights presented here are important for the rational design of advanced materials having tailored surface nanotopography with predictable wettability.The wetting of a material can be tuned by changing the roughness on its surface. Recent advances in the field of nanotechnology open exciting opportunities to control macroscopic wetting behaviour. Yet, the benchmark theories used to describe the wettability of macroscopically rough surfaces fail to fully describe the wetting behaviour of systems with topographical features at the nanoscale. To shed light on the events occurring at the nanoscale we have utilised model gradient substrata where surface nanotopography was tailored in a controlled and robust manner. The intrinsic wettability of the coatings was varied from hydrophilic to hydrophobic. The measured water contact angle could not be described by the classical theories. We developed an empirical model that effectively captures the experimental data, and further enables us to predict the wetting of surfaces with nanoscale roughness by considering the physical and chemical properties of the material. The fundamental insights presented here are important for the rational design of advanced materials having tailored surface nanotopography with predictable wettability. Electronic supplementary information (ESI) available: Detailed characterization of the nanorough substrates and model derivation. See DOI: 10.1039/c5nr08329j

Development of a ceramic surface replacement for the hip. An experimental Sialon model.

PubMed

Clarke, I C; Phillips, W; McKellop, H; Coster, I R; Hedley, A; Amstutz, H C

1979-01-01

The objective of this study was to investigate the design and fixation advantages of Sialon ceramic surface replacements implanted without acrylic bone cement. The biocompatibility and friction and wear properties of Sialon ceramic were compared with more conventional prosthetic materials such as stainless steel and alumina. A functional load-bearing canine hip surface replacement model was established to test Sialon femoral cups designed for fixation by bone ingrowth. The results of the polyethylene wear tests on highly polished ceramic and stainless steel counterfaces were essentially similar. These laboratory data indicated that the in-vivo polyethylene wear performance on metal or ceramic prosthetic surfaces could be expected to be indistinguishable, i.e. the ceramic/polyethylene combination would not offer any improved wear resistance in-vivo. It was found possible to get bone ingrowth into the macrokeying areas of the ceramic femoral cups but not into the microporous surfaces due to the presence of a fibrous membrane lining their internal surfaces. The biocompatability specimens also appeared to be invested with a fibrous membrane. Further studies are under way to determine the relationship between reaming procedures, micro motion at the interfaces and Sialon biocompatibility.

NASA supercritical laminar flow control airfoil experiment

NASA Technical Reports Server (NTRS)

Harvey, W. D.

1982-01-01

The design and goals of experimental investigations of supercritical LFC airfoils conducted in the NASA Langley 8-ft Transonic Pressure Tunnel beginning in March 1982 are reviewed. Topics addressed include laminarization aspects; flow-quality requirements; simulation of flight parameters; the setup of screens, honeycomb, and sonic throat; the design cycle; theoretical pressure distributions and shock-free limits; drag divergence and stability analysis; and the LFC suction system. Consideration is given to the LFC airfoil model, the air-flow control system, airfoil-surface instrumentation, liner design and hardware, and test options. Extensive diagrams, drawings, graphs, photographs, and tables of numerical data are provided.

Simultaneously 'pushing' and 'pulling' graphene oxide into low-polar solvents through a designed interface.

PubMed

Liu, Zhen; Liu, Jingquan; Wang, Yichao; Razal, Joselito M; Francis, Paul S; Biggs, Mark J; Barrow, Colin J; Yang, Wenrong

2018-08-03

Dispersing graphene oxide (GO) in low-polar solvents can realize a perfect self-assembly with functional molecules and application in removal of organic impurities that only dissolve in low-polar solvents. The surface chemistry of GO plays an important role in its dispersity in these solvents. The direct transfer of hydrophilic GO into low-polar solvents, however, has remained an experimental challenge. In this study, we design an interface to transfer GO by simultaneously 'pushing and pulling' the nanosheets into low-polar solvents. Our approach is outstanding due to the ability to obtain monolayers of chemically reduced GO (CRGO) with designed surface properties in the organic phase. Using the transferred GO or CRGO dispersions, we have fabricated GO/fullerene nanocomposites and assessed the ability of CRGOs for dye adsorption. We hope our work can provide a universal approach for the phase transfer of other nanomaterials.

Reconfigurable all-dielectric metamaterial frequency selective surface based on high-permittivity ceramics

NASA Astrophysics Data System (ADS)

Li, Liyang; Wang, Jun; Wang, Jiafu; Ma, Hua; Du, Hongliang; Zhang, Jieqiu; Qu, Shaobo; Xu, Zhuo

2016-04-01

Based on effective medium theory and dielectric resonator theory, we propose the design of reconfigurable all-dielectric metamaterial frequency selective surfaces (FSSs) using high-permittivity ceramics. The FSS is composed of ceramic resonators with different band stop responses under front and side incidences. By mechanically tuning the orientation of the ceramic resonators, reconfigurable electromagnetic (EM) responses between two adjacent stopbands can be achieved. The two broad stopbands originate from the first two resonant modes of the ceramic resonators. As an example, a reconfigurable FSS composed of cross-shaped ceramic resonators is demonstrated. Both numerical and experimental results show that the FSS can switch between two consecutive stopbands in 3.55-4.60 GHz and 4.54-4.94 GHz. The design method can be readily extended to the design of FSSs in other frequencies for high-power applications.

Designing cylindrical implosion experiments on NIF to study deceleration phase of Rayleigh-Taylor

NASA Astrophysics Data System (ADS)

Vazirani, N.; Kline, J. L.; Loomis, E.; Sauppe, J. P.; Palaniyappan, S.; Flippo, K.; Srinivasan, B.; Malka, E.; Bose, A.; Shvarts, D.

2017-10-01

The Rayleigh-Taylor (RT) hydrodynamic instability occurs when a lower density fluid pushes on a higher density fluid. This occurs in inertial confinement fusion (ICF) implosions at each of the capsule interfaces during the initial acceleration and the deceleration as it stagnates. The RT instabilities mix capsule material into the fusion fuel degrading the Deuterium-Tritium reactivity and ultimately play a key role in limiting target performance. While significant effort has focused on understanding RT at the outer capsule surface, little work has gone into understanding the inner surface RT instability growth during the deceleration phase. Direct measurements of the RT instability are difficult to make at high convergence in a spherical implosion. Here we present the design of a cylindrical implosion system for the National Ignition Facility for studying deceleration phase RT. We will discuss the experimental design, the estimated instability growth, and our outstanding concerns.

The design, analysis, and testing of a low-budget wind-tunnel flutter model with active aerodynamic controls

NASA Technical Reports Server (NTRS)

Bolding, R. M.; Stearman, R. O.

1976-01-01

A low budget flutter model incorporating active aerodynamic controls for flutter suppression studies was designed as both an educational and research tool to study the interfering lifting surface flutter phenomenon in the form of a swept wing-tail configuration. A flutter suppression mechanism was demonstrated on a simple semirigid three-degree-of-freedom flutter model of this configuration employing an active stabilator control, and was then verified analytically using a doublet lattice lifting surface code and the model's measured mass, mode shapes, and frequencies in a flutter analysis. Preliminary studies were significantly encouraging to extend the analysis to the larger degree of freedom AFFDL wing-tail flutter model where additional analytical flutter suppression studies indicated significant gains in flutter margins could be achieved. The analytical and experimental design of a flutter suppression system for the AFFDL model is presented along with the results of a preliminary passive flutter test.

Design of a 3-dimensional visual illusion speed reduction marking scheme.

PubMed

Liang, Guohua; Qian, Guomin; Wang, Ye; Yi, Zige; Ru, Xiaolei; Ye, Wei

2017-03-01

To determine which graphic and color combination for a 3-dimensional visual illusion speed reduction marking scheme presents the best visual stimulus, five parameters were designed. According to the Balanced Incomplete Blocks-Law of Comparative Judgment, three schemes, which produce strong stereoscopic impressions, were screened from the 25 initial design schemes of different combinations of graphics and colors. Three-dimensional experimental simulation scenes of the three screened schemes were created to evaluate four different effects according to a semantic analysis. The following conclusions were drawn: schemes with a red color are more effective than those without; the combination of red, yellow and blue produces the best visual stimulus; a larger area from the top surface and the front surface should be colored red; and a triangular prism should be painted as the graphic of the marking according to the stereoscopic impression and the coordination of graphics with the road.

Reconfigurable all-dielectric metamaterial frequency selective surface based on high-permittivity ceramics

PubMed Central

Li, Liyang; Wang, Jun; Wang, Jiafu; Ma, Hua; Du, Hongliang; Zhang, Jieqiu; Qu, Shaobo; Xu, Zhuo

2016-01-01

Based on effective medium theory and dielectric resonator theory, we propose the design of reconfigurable all-dielectric metamaterial frequency selective surfaces (FSSs) using high-permittivity ceramics. The FSS is composed of ceramic resonators with different band stop responses under front and side incidences. By mechanically tuning the orientation of the ceramic resonators, reconfigurable electromagnetic (EM) responses between two adjacent stopbands can be achieved. The two broad stopbands originate from the first two resonant modes of the ceramic resonators. As an example, a reconfigurable FSS composed of cross-shaped ceramic resonators is demonstrated. Both numerical and experimental results show that the FSS can switch between two consecutive stopbands in 3.55–4.60 GHz and 4.54–4.94 GHz. The design method can be readily extended to the design of FSSs in other frequencies for high-power applications. PMID:27052098

A calibration rig for multi-component internal strain gauge balance using the new design-of-experiment (DOE) approach

NASA Astrophysics Data System (ADS)

Nouri, N. M.; Mostafapour, K.; Kamran, M.

2018-02-01

In a closed water-tunnel circuit, the multi-component strain gauge force and moment sensor (also known as balance) are generally used to measure hydrodynamic forces and moments acting on scaled models. These balances are periodically calibrated by static loading. Their performance and accuracy depend significantly on the rig and the method of calibration. In this research, a new calibration rig was designed and constructed to calibrate multi-component internal strain gauge balances. The calibration rig has six degrees of freedom and six different component-loading structures that can be applied separately and synchronously. The system was designed based on the applicability of formal experimental design techniques, using gravity for balance loading and balance positioning and alignment relative to gravity. To evaluate the calibration rig, a six-component internal balance developed by Iran University of Science and Technology was calibrated using response surface methodology. According to the results, calibration rig met all design criteria. This rig provides the means by which various methods of formal experimental design techniques can be implemented. The simplicity of the rig saves time and money in the design of experiments and in balance calibration while simultaneously increasing the accuracy of these activities.

Biophysical model of bacterial cell interactions with nanopatterned cicada wing surfaces.

PubMed

Pogodin, Sergey; Hasan, Jafar; Baulin, Vladimir A; Webb, Hayden K; Truong, Vi Khanh; Phong Nguyen, The Hong; Boshkovikj, Veselin; Fluke, Christopher J; Watson, Gregory S; Watson, Jolanta A; Crawford, Russell J; Ivanova, Elena P

2013-02-19

The nanopattern on the surface of Clanger cicada (Psaltoda claripennis) wings represents the first example of a new class of biomaterials that can kill bacteria on contact based solely on their physical surface structure. The wings provide a model for the development of novel functional surfaces that possess an increased resistance to bacterial contamination and infection. We propose a biophysical model of the interactions between bacterial cells and cicada wing surface structures, and show that mechanical properties, in particular cell rigidity, are key factors in determining bacterial resistance/sensitivity to the bactericidal nature of the wing surface. We confirmed this experimentally by decreasing the rigidity of surface-resistant strains through microwave irradiation of the cells, which renders them susceptible to the wing effects. Our findings demonstrate the potential benefits of incorporating cicada wing nanopatterns into the design of antibacterial nanomaterials. Copyright © 2013 Biophysical Society. Published by Elsevier Inc. All rights reserved.

VACUUM SEALING MEANS FOR LOW VACUUM PRESSURES

DOEpatents

Milleron, N.

1962-06-12

S>A vacuum seal is designed in which the surface tension of a thin layer of liquid metal of low vapor pressure cooperates with adjacent surfaces to preclude passages of gases across pressure differentials as low as 10/sup -8/ mm Hg. Mating contiguous surfaces composed of copper, brass, stainless steel, nickel, molybdenum, tungsten, tantalum, glass, quartz, and/or synthetic mica are disposed to provide a maximum tolerance, D, expressed by 2 gamma /P/sub 1/, where gamma is the coefflcient of the surface tension of the metal sealant selected in dynes/cm/sub 2/. Means for heating the surfaces remotely is provided where temperatures drop below about 250 deg C. A sealant consisting of an alloy of gallium, indium, and tin, among other combinations tabulated, is disposed therebetween after treating the surfaces to improve wettability, as by ultrasonic vibrations, the surfaces and sealants being selected according to the anticipated experimental conditions of use. (AEC)

Influence of LaFeO 3 Surface Termination on Water Reactivity

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stoerzinger, Kelsey A.; Comes, Ryan; Spurgeon, Steven R.

2017-02-17

The polarity of oxide surfaces can dramatically impact their surface reactivity, in particular with polar molecules such as water. The surface species that result from this interaction change the oxide electronic structure and chemical reactivity in applications such as photoelectrochemistry, but are challenging to probe experimentally with atomic-scale understanding. Here we report a detailed study of the surface chemistry and electronic structure of the perovskite LaFeO3 in humid conditions using ambient pressure X-ray photoelectron spectroscopy. Comparing the two possible terminations of the polar (001)-oriented surface, we find that the LaO surface is more reactive toward water, forming hydroxyl species andmore » adsorbing molecular water at lower relative humidity than its FeO2-terminated counterpart. Our results demonstrate how the termination of a complex oxide can dramatically impact its reactivity, providing insight into the design of catalyst materials.« less

A structural model for surface-enhanced stabilization in some metallic glass formers

NASA Astrophysics Data System (ADS)

Levchenko, Elena V.; Evteev, Alexander V.; Yavari, Alain R.; Louzguine-Luzgin, Dmitri V.; Belova, Irina V.; Murch, Graeme E.

2013-01-01

A structural model for surface-enhanced stabilization in some metallic glass formers is proposed. In this model, the alloy surface structure is represented by five-layer Kagomé-net-based lateral ordering. Such surface structure has intrinsic abilities to stabilize icosahedral-like short-range order in the bulk, acting as 'a cloak of liquidity'. In particular, recent experimental observations of surface-induced lateral ordering and a very high glass forming ability of the liquid alloy Au49Ag5.5Pd2.3Cu26.9Si16.3 can be united using this structural model. This model may be useful for the interpretation of surface structure of other liquid alloys with a high glass forming ability. In addition, it suggests the possibility of guiding the design of the surface coating of solid containers for the stabilization of undercooled liquids.

Membrane fouling in a submerged membrane bioreactor: New method and its applications in interfacial interaction quantification.

PubMed

Hong, Huachang; Cai, Xiang; Shen, Liguo; Li, Renjie; Lin, Hongjun

2017-10-01

Quantification of interfacial interactions between two rough surfaces represents one of the most pressing requirements for membrane fouling prediction and control in membrane bioreactors (MBRs). This study firstly constructed regularly rough membrane and particle surfaces by using rigorous mathematical equations. Thereafter, a new method involving surface element integration (SEI) method, differential geometry and composite Simpson's rule was proposed to quantify the interfacial interactions between the two constructed rough surfaces. This new method were then applied to investigate interfacial interactions in a MBR with the data of surface properties of membrane and foulants experimentally measured. The feasibility of the new method was verified. It was found that asperity amplitude and period of the membrane surface exerted profound effects on the total interaction. The new method had broad potential application fields especially including guiding membrane surface design for membrane fouling mitigation. Copyright © 2017 Elsevier Ltd. All rights reserved.

An efficient reliability algorithm for locating design point using the combination of importance sampling concepts and response surface method

NASA Astrophysics Data System (ADS)

Shayanfar, Mohsen Ali; Barkhordari, Mohammad Ali; Roudak, Mohammad Amin

2017-06-01

Monte Carlo simulation (MCS) is a useful tool for computation of probability of failure in reliability analysis. However, the large number of required random samples makes it time-consuming. Response surface method (RSM) is another common method in reliability analysis. Although RSM is widely used for its simplicity, it cannot be trusted in highly nonlinear problems due to its linear nature. In this paper, a new efficient algorithm, employing the combination of importance sampling, as a class of MCS, and RSM is proposed. In the proposed algorithm, analysis starts with importance sampling concepts and using a represented two-step updating rule of design point. This part finishes after a small number of samples are generated. Then RSM starts to work using Bucher experimental design, with the last design point and a represented effective length as the center point and radius of Bucher's approach, respectively. Through illustrative numerical examples, simplicity and efficiency of the proposed algorithm and the effectiveness of the represented rules are shown.

Design Concept of Dialyzer Biomaterials: How to Find Biocompatible Polymers Based on the Biointerfacial Water Structure.

PubMed

Tanaka, Masaru

2017-01-01

Although various types of materials have been used widely in dialyzers, most biomaterials lack the desired functional properties to interface with blood and have not been engineered for optimum performance. Therefore, there is increasing demand to develop novel materials to address such problems in the dialysis arena. Numerous parameters of polymeric biomaterials can affect biocompatibility in a controlled manner. The mechanisms responsible for the biocompatibility of polymers at the molecular level have not been clearly demonstrated, although many theoretical and experimental efforts have been made to try and understand them. Moreover, water interactions have been recognized as fundamental for the blood response to contact with polymers. We have proposed the 'intermediate water' concept and hypothesized that intermediate water, which prevents the proteins and blood cells from directly contacting the polymer surface, or nonfreezing water on the polymer surface, plays an important role in the biocompatibility of polymers. This chapter provides an overview of the recent experimental progress of biocompatible polymers measured by thermal, spectroscopic, and surface force techniques. Additionally, it highlights recent developments in the use of biocompatible polymeric biomaterials for dialyzers and provides an overview of the progress made in the design of multifunctional biomedical polymers by controlling the biointerfacial water structure through precision polymer synthesis. Key Messages: Intermediate water was found only in hydrated biopolymers (proteins, polysaccharides, and nucleic acids, DNA and RNA) and hydrated biocompatible synthetic polymers. Intermediate water could be one of the main screening factors for the design of appropriate dialyzer materials. © 2017 S. Karger AG, Basel.

Optimal Experimental Design of Borehole Locations for Bayesian Inference of Past Ice Sheet Surface Temperatures

NASA Astrophysics Data System (ADS)

Davis, A. D.; Huan, X.; Heimbach, P.; Marzouk, Y.

2017-12-01

Borehole data are essential for calibrating ice sheet models. However, field expeditions for acquiring borehole data are often time-consuming, expensive, and dangerous. It is thus essential to plan the best sampling locations that maximize the value of data while minimizing costs and risks. We present an uncertainty quantification (UQ) workflow based on rigorous probability framework to achieve these objectives. First, we employ an optimal experimental design (OED) procedure to compute borehole locations that yield the highest expected information gain. We take into account practical considerations of location accessibility (e.g., proximity to research sites, terrain, and ice velocity may affect feasibility of drilling) and robustness (e.g., real-time constraints such as weather may force researchers to drill at sub-optimal locations near those originally planned), by incorporating a penalty reflecting accessibility as well as sensitivity to deviations from the optimal locations. Next, we extract vertical temperature profiles from these boreholes and formulate a Bayesian inverse problem to reconstruct past surface temperatures. Using a model of temperature advection/diffusion, the top boundary condition (corresponding to surface temperatures) is calibrated via efficient Markov chain Monte Carlo (MCMC). The overall procedure can then be iterated to choose new optimal borehole locations for the next expeditions.Through this work, we demonstrate powerful UQ methods for designing experiments, calibrating models, making predictions, and assessing sensitivity--all performed under an uncertain environment. We develop a theoretical framework as well as practical software within an intuitive workflow, and illustrate their usefulness for combining data and models for environmental and climate research.

Optimisation of warpage on plastic injection moulding part using response surface methodology (RSM)

NASA Astrophysics Data System (ADS)

Miza, A. T. N. A.; Shayfull, Z.; Nasir, S. M.; Fathullah, M.; Rashidi, M. M.

2017-09-01

The warpage is often encountered which occur during injection moulding process of thin shell part depending the process condition. The statistical design of experiment method which are Integrating Finite Element (FE) Analysis, moldflow analysis and response surface methodology (RSM) are the stage of few ways in minimize the warpage values of x,y and z on thin shell plastic parts that were investigated. A battery cover of a remote controller is one of the thin shell plastic part that produced by using injection moulding process. The optimum process condition parameter were determined as to achieve the minimum warpage from being occur. Packing pressure, Cooling time, Melt temperature and Mould temperature are 4 parameters that considered in this study. A two full factorial experimental design was conducted in Design Expert of RSM analysis as to combine all these parameters study. FE analysis result gain from analysis of variance (ANOVA) method was the one of the important process parameters influenced warpage. By using RSM, a predictive response surface model for warpage data will be shown.

Mass reduction patterning of silicon-on-oxide-based micromirrors

NASA Astrophysics Data System (ADS)

Hall, Harris J.; Green, Andrew; Dooley, Sarah; Schmidt, Jason D.; Starman, LaVern A.; Langley, Derrick; Coutu, Ronald A.

2016-10-01

It has long been recognized in the design of micromirror-based optical systems that balancing static flatness of the mirror surface through structural design with the system's mechanical dynamic response is challenging. Although a variety of mass reduction approaches have been presented in the literature to address this performance trade, there has been little quantifiable comparison reported. In this work, different mass reduction approaches, some unique to the work, are quantifiably compared with solid plate thinning in both curvature and mass using commercial finite element simulation of a specific square silicon-on-insulator-based micromirror geometry. Other important considerations for micromirror surfaces, including surface profile and smoothness, are also discussed. Fabrication of one of these geometries, a two-dimensional tessellated square pattern, was performed in the presence of a 400-μm-tall central post structure using a simple single mask process. Limited experimental curvature measurements of fabricated samples are shown to correspond well with properly characterized simulation results and indicate ˜67% improvement in radius of curvature in comparison to a solid plate design of equivalent mass.

Surface Finish Effects Using Coating Method on 3D Printing (FDM) Parts

NASA Astrophysics Data System (ADS)

Haidiezul, AHM; Aiman, AF; Bakar, B.

2018-03-01

One of three-dimensional (3-D) printing economical processes is by using Fused Deposition Modelling (FDM). The 3-D printed object was built using layer-by-layer approach which caused “stair stepping” effects. This situation leads to uneven surface finish which mostly affect the objects appearance for product designers in presenting their models or prototypes. The objective of this paper is to examine the surface finish effects from the application of XTC-3D coating developed by Smooth-On, USA on the 3D printed parts. From the experimental works, this study shows the application of XTC-3D coating to the 3-D printed parts has improve the surface finish by reducing the gap between the layer

Modeling equine race surface vertical mechanical behaviors in a musculoskeletal modeling environment.

PubMed

Symons, Jennifer E; Fyhrie, David P; Hawkins, David A; Upadhyaya, Shrinivasa K; Stover, Susan M

2015-02-26

Race surfaces have been associated with the incidence of racehorse musculoskeletal injury, the leading cause of racehorse attrition. Optimal race surface mechanical behaviors that minimize injury risk are unknown. Computational models are an economical method to determine optimal mechanical behaviors. Previously developed equine musculoskeletal models utilized ground reaction floor models designed to simulate a stiff, smooth floor appropriate for a human gait laboratory. Our objective was to develop a computational race surface model (two force-displacement functions, one linear and one nonlinear) that reproduced experimental race surface mechanical behaviors for incorporation in equine musculoskeletal models. Soil impact tests were simulated in a musculoskeletal modeling environment and compared to experimental force and displacement data collected during initial and repeat impacts at two racetracks with differing race surfaces - (i) dirt and (ii) synthetic. Best-fit model coefficients (7 total) were compared between surface types and initial and repeat impacts using a mixed model ANCOVA. Model simulation results closely matched empirical force, displacement and velocity data (Mean R(2)=0.930-0.997). Many model coefficients were statistically different between surface types and impacts. Principal component analysis of model coefficients showed systematic differences based on surface type and impact. In the future, the race surface model may be used in conjunction with previously developed the equine musculoskeletal models to understand the effects of race surface mechanical behaviors on limb dynamics, and determine race surface mechanical behaviors that reduce the incidence of racehorse musculoskeletal injury through modulation of limb dynamics. Copyright © 2015 Elsevier Ltd. All rights reserved.

Solution blow spinning: parameters optimization and effects on the properties of nanofibers from poly(lactic) acid/dimethyl carbonate solutions

USDA-ARS?s Scientific Manuscript database

Solution blow spinning (SBS) is a process to produce non-woven fiber sheets with high porosity and an extremely large amount of surface area. In this study, a Box-Behnken experimental design (BBD) was used to optimize the processing parameters for the production of nanofibers from polymer solutions ...

Modeling the survival of Salmonella on slice cooked ham as a function of apple skin polyphenols, acetic acid, oregano essential oil and carvacrol

USDA-ARS?s Scientific Manuscript database

Response surface methodology was applied to investigate the combined effect of apple skin polyphenols (ASP), acetic acid (AA), oregano essential oil (O) and carvacrol (C) on the inactivation of Salmonella on sliced cooked ham. A full factorial experimental design was employed with control variables ...

Grass seeding as a control for roadbank erosion.

Treesearch

A.G. Wollum

1962-01-01

Grass, seeded on a steep roadcut in western Oregon, reduced erosion but caused increased surface runoff during a 3-year period of observation. These results were obtained at H. J. Andrews Experimental Forest from a study designed to measure effectiveness of grass in controlling soil erosion from exposed roadbanks. Additional measurements for varying soil types will be...

A Computational-Experimental Development of Vortex Generator Use for a Transitioning S-Diffuser

NASA Technical Reports Server (NTRS)

Wendt, Bruce J.; Dudek, Julianne C.

1996-01-01

The development of an effective design strategy for surface-mounted vortex generator arrays in a subsonic diffuser is described in this report. This strategy uses the strengths of both computational and experimental analyses to determine beneficial vortex generator locations and sizes. A parabolized Navier-Stokes solver, RNS3D, was used to establish proper placement of the vortex generators for reduction in circumferential total pressure distortion. Experimental measurements were used to determine proper vortex generator sizing to minimize total pressure recovery losses associated with vortex generator device drag. The best result achieved a 59% reduction in the distortion index DC60, with a 0.3% reduction in total pressure recovery.

Reconfigurable Flight Control Using Nonlinear Dynamic Inversion with a Special Accelerometer Implementation

NASA Technical Reports Server (NTRS)

Bacon, Barton J.; Ostroff, Aaron J.

2000-01-01

This paper presents an approach to on-line control design for aircraft that have suffered either actuator failure, missing effector surfaces, surface damage, or any combination. The approach is based on a modified version of nonlinear dynamic inversion. The approach does not require a model of the baseline vehicle (effectors at zero deflection), but does require feedback of accelerations and effector positions. Implementation issues are addressed and the method is demonstrated on an advanced tailless aircraft. An experimental simulation analysis tool is used to directly evaluate the nonlinear system's stability robustness.

Preliminary results from DIMES: Dispersion in the ACC

NASA Astrophysics Data System (ADS)

Balwada, D.; Speer, K.; LaCasce, J. H.; Owens, B.

2012-04-01

The Diapycnal and Isopynal Mixing Experiment in the Southern Ocean (DIMES) is a CLIVAR process study designed to study mixing in the Antarctic Circumpolar Current. The experiment includes tracer release, float, and small-scale turbulence components. This presentation will report on some results of the float component, from floats deployed across the ACC in the Southeast Pacific Ocean. These are the first subsurface Lagrangian trajectories from the ACC. Floats were deployed to follow approximately a constant density surface for a period of 1-3 years. To help aid the experimental results virtual floats were advected using AVISO data and basic statistics were derived from both deployed and virtual float trajectories. Experimental design, initial results, comparison to virtual floats and single particle and relative dispersion calculations will be presented.

Experimental Results for a Flapped Natural-laminar-flow Airfoil with High Lift/drag Ratio

NASA Technical Reports Server (NTRS)

Mcghee, R. J.; Viken, J. K.; Pfenninger, W.; Beasley, W. D.; Harvey, W. D.

1984-01-01

Experimental results have been obtained for a flapped natural-laminar-flow airfoil, NLF(1)-0414F, in the Langley Low-Turbulence Pressure Tunnel. The tests were conducted over a Mach number range from 0.05 to 0.40 and a chord Reynolds number range from about 3.0 x 10(6) to 22.0 x 10(6). The airfoil was designed for 0.70 chord laminar flow on both surfaces at a lift coefficient of 0.40, a Reynolds number of 10.0 x 10(6), and a Mach number of 0.40. A 0.125 chord simple flap was incorporated in the design to increase the low-drag, lift-coefficient range. Results were also obtained for a 0.20 chord split-flap deflected 60 deg.

Experimental Analysis of Steady-State Maneuvering Effects on Transmission Vibration Patterns Recorded in an AH-1 Cobra Helicopter

NASA Technical Reports Server (NTRS)

Huff, Edward M.; Dzwonczyk, Mark; Norvig, Peter (Technical Monitor)

2000-01-01

Flight experiment was designed primarily to determine the extent to which steady-state maneuvers influence characteristic vibration patterns measured at the input pinion and output annulus gear locations of the main transmission. If results were to indicate that maneuvers systematically influence vibration patterns, more extensive studies would be planned to explore the response surface. It was also designed to collect baseline data for comparison with experimental data to be recorded at a later date from test stands at Glenn Research Center. Finally, because this was the first vibration flight study on the Cobra aircraft, considerable energy was invested in developing an in-flight recording apparatus, as well as exploring acceleration mounting methods, and generally learning about the overall vibratory characteristics of the aircraft itself.

Optimization of composite coagulant made from polyferric chloride and tapioca starch in landfill leachate treatment

NASA Astrophysics Data System (ADS)

Shaylinda, M. Z. N.; Hamidi, A. A.; Mohd, N. A.; Ariffin, A.; Irvan, D.; Hazreek, Z. A. M.; Nizam, Z. M.

2018-04-01

In this research, the performance of polyferric chloride and tapioca flour as composite coagulants for partially stabilized leachate was investigated. Response surface methodology (RSM) was used to optimize the coagulation and flocculation process of partially stabilized leachate. Central composite design a standard design tool in RSM was applied to evaluate the interactions and effects of dose and pH. Dose 0.2 g/L Fe and pH 4.71 were the optimum value suggested by RSM. Experimental test based on the optimum condition, resulted in 95.9%, 94.6% and 50.4% of SS, color and COD removals, respectively. The percentage difference recorded between experimental and model responses was <5%. Therefore, it can be concluded that RSM was an appropriate optimization tool for coagulation and flocculation process.

Plasmonic trapping potentials for cold atoms

NASA Astrophysics Data System (ADS)

Mildner, Matthias; Horrer, Andreas; Fleischer, Monika; Zimmermann, Claus; Slama, Sebastian

2018-07-01

This paper reports on conceptual and experimental work towards the realization of plasmonic surface traps for cold atoms. The trapping mechanism is based on the combination of a repulsive and an attractive potential generated by evanescent light waves that are plasmonically enhanced. The strength of enhancement can be locally manipulated via the thickness of a metal nanolayer deposited on top of a dielectric substrate. Thus, in principle the trapping geometry can be predefined by the metal layer design. We present simulations of a plasmonic lattice potential using a gold grating with sinusoidally modulated thickness. Experimentally, a first plasmonic test structure is presented and characterized. Furthermore, the surface potential landscape is detected by reflecting ultracold atom clouds from the test structure revealing the influence of both evanescent waves. A parameter range is identified where stable traps can be expected.

Development and demonstration of a flutter-suppression system using active controls. [wind tunnel tests

NASA Technical Reports Server (NTRS)

Sandford, M. C.; Abel, I.; Gray, D. L.

1975-01-01

The application of active control technology to suppress flutter was demonstrated successfully in the transonic dynamics tunnel with a delta-wing model. The model was a simplified version of a proposed supersonic transport wing design. An active flutter suppression method based on an aerodynamic energy criterion was verified by using three different control laws. The first two control laws utilized both leading-edge and trailing-edge active control surfaces, whereas the third control law required only a single trailing-edge active control surface. At a Mach number of 0.9 the experimental results demonstrated increases in the flutter dynamic pressure from 12.5 percent to 30 percent with active controls. Analytical methods were developed to predict both open-loop and closed-loop stability, and the results agreed reasonably well with the experimental results.

Preliminary Analysis of a Water Shield for a Surface Power Reactor

NASA Technical Reports Server (NTRS)

Pearson, J. Boise

2006-01-01

A water based shielding system is being investigated for use on initial lunar surface power systems. The use of water may lower overall cost (as compared to development cost for other materials) and simplify operations in the setup and handling. The thermal hydraulic performance of the shield is of significant interest. The mechanism for transferring heat through the shield is natural convection. A simple 1-D thermal model indicates the necessity of natural convection to maintain acceptable temperatures and pressures in the water shield. CFD analysis is done to quantify the natural convection in the shield, and predicts sufficient natural convection to transfer heat through the shield with small temperature gradients. A test program will he designed to experimentally verify the thermal hydraulic performance of the shield, and to anchor the CFD models to experimental results.

Hydrogenated amorphous silicon nitride photonic crystals for improved-performance surface electromagnetic wave biosensors.

PubMed

Sinibaldi, Alberto; Descrovi, Emiliano; Giorgis, Fabrizio; Dominici, Lorenzo; Ballarini, Mirko; Mandracci, Pietro; Danz, Norbert; Michelotti, Francesco

2012-10-01

We exploit the properties of surface electromagnetic waves propagating at the surface of finite one dimensional photonic crystals to improve the performance of optical biosensors with respect to the standard surface plasmon resonance approach. We demonstrate that the hydrogenated amorphous silicon nitride technology is a versatile platform for fabricating one dimensional photonic crystals with any desirable design and operating in a wide wavelength range, from the visible to the near infrared. We prepared sensors based on photonic crystals sustaining either guided modes or surface electromagnetic waves, also known as Bloch surface waves. We carried out for the first time a direct experimental comparison of their sensitivity and figure of merit with surface plasmon polaritons on metal layers, by making use of a commercial surface plasmon resonance instrument that was slightly adapted for the experiments. Our measurements demonstrate that the Bloch surface waves on silicon nitride photonic crystals outperform surface plasmon polaritons by a factor 1.3 in terms of figure of merit.

Feasibility study of patient-specific surgical templates for the fixation of pedicle screws.

PubMed

Salako, F; Aubin, C-E; Fortin, C; Labelle, H

2002-01-01

Surgery for scoliosis, as well as other posterior spinal surgeries, frequently uses pedicle screws to fix an instrumentation on the spine. Misplacement of a screw can lead to intra- and post-operative complications. The objective of this study is to design patient-specific surgical templates to guide the drilling operation. From the CT-scan of a vertebra, the optimal drilling direction and limit angles are computed from an inverse projection of the pedicle limits. The first template design uses a surface-to-surface registration method and was constructed in a CAD system by subtracting the vertebra from a rectangular prism and a cylinder with the optimal orientation. This template and the vertebra were built using rapid prototyping. The second design uses a point-to-surface registration method and has 6 adjustable screws to adjust the orientation and length of the drilling support device. A mechanism was designed to hold it in place on the spinal process. A virtual prototype was build with CATIA software. During the operation, the surgeon places either template on patient's vertebra until a perfect match is obtained before drilling. The second design seems better than the first one because it can be reused on different vertebra and is less sensible to registration errors. The next step is to build the second design and make experimental and simulations tests to evaluate the benefits of this template during a scoliosis operation.

Uranium mobility during interaction of rhyolitic glass with alkaline solutions: dissolution of glass

USGS Publications Warehouse

Zielinski, Robert A.

1977-01-01

This report concerns investigations designed to identify the important physical and chemical parameters influencing the rate of release of uranium from glass shards of rhyolitic air-fall ash. Oxidizing, silica undersaturated, alkaline solutions are eluted through a column of rhyolitic glass shards at a carefully controlled temperature, pressure, and flow rate. The solutions are monitored for the concentration of uranium and selected additional elements (Si, K, Li, F), and the glass is recovered and examined for physical and/or chemical evidence of attack. The flushing mode is designed to mimic leaching of glass shards by intermittent, near-surface waters with which the glass is not in equilibrium. Reported rates are applicable only to the experimental conditions (120?C, 7,000 psi), but it is assumed that the reaction mechanisms and the relative importance of rate-influencing parameters remain unchanged, at reduced temperature and pressure. Results of the above experiment indicate that silica and uranium are released from glass shards at comparable rates, while lithium and potassium are released faster and fluorine slower than either Si or U. Rates of release of silica and uranium correlate positively with the surface area of the shards. Rhyolitic shards release uranium at faster rates than rhyodacitic shards of comparable surface area. Changes in the shards resulting from experimental treatment and observed in the original glass separates from an Oligocene ash (compared to a Pleistocene ash) include; surface pitting, increased surface area, devitrification rinds (<1l micron wide) and reduced lithium contents. Future investigations will study the effect of temperature, pressure, solution composition, and flow rate on the relative mobility of U, Si, Li, F, and K.

Effects of different self-assembled monolayers on thin-film morphology: a combined DFT/MD simulation protocol.

PubMed

Alberga, Domenico; Mangiatordi, Giuseppe Felice; Motta, Alessandro; Nicolotti, Orazio; Lattanzi, Gianluca

2015-10-06

Organic thin film transistors (OTFTs) are multilayer field-effect transistors that employ an organic conjugated material as semiconductor. Several experimental groups have recently demonstrated that the insertion of an organic self-assembled monolayer (SAM) between the dielectric and the semiconductive layer is responsible for a sensible improvement of the OTFT performances in terms of an increased charge carrier mobility caused by a higher degree of order in the organic semiconductor layer. Here, we describe a combined periodic density functional theory (DFT) and classical molecular dynamics (MD) protocol applied to four different SAMs and a pentacene monolayer deposited onto their surfaces. In particular, we investigate the morphology and the surface of the four SAMs and the translational, orientational, and nematic order of the monolayer through the calculation of several distribution functions and order parameters pointing out the differences among the systems and relating them to known experimental results. Our calculations also suggest that small differences in the SAM molecular design will produce remarkable differences in the SAM surface and monolayer order. In particular, our simulations explain how a SAM with a bulky terminal group results in an irregular and rough surface that determines the deposition of a disordered semiconductive monolayer. On the contrary, SAMs with a small terminal group generate smooth surfaces with uninterrupted periodicity, thus favoring the formation of an ordered pentacene monolayer that increases the mobility of charge carriers and improves the overall performances of the OTFT devices. Our results clearly point out that the in silico procedure presented here might be of help in tuning the design of SAMs in order to improve the quality of OTFT devices.

Assessment of potential positive effects of nZVI surface modification and concentration levels on TCE dechlorination in the presence of competing strong oxidants, using an experimental design.

PubMed

Kaifas, Delphine; Malleret, Laure; Kumar, Naresh; Fétimi, Wafa; Claeys-Bruno, Magalie; Sergent, Michelle; Doumenq, Pierre

2014-05-15

Nanoscale zero-valent iron (nZVI) particles are efficient for the remediation of aquifers polluted by trichloroethylene (TCE). But for on-site applications, their reactivity can be affected by the presence of common inorganic co-pollutants, which are equally reduced by nZVI particles. The aim of this study was to assess the potential positive effects of nZVI surface modification and concentration level on TCE removal in the concomitant presence of two strong oxidants, i.e., Cr(VI) and NO3(-). A design of experiments, testing four factors (i.e. nZVI concentration, nZVI surface modification, Cr(VI) concentration and NO3(-) concentration), was used to select the best trials for the identification of the main effects of the factors and of the factors interactions. The effects of these factors were studied by measuring the following responses: TCE removal rates at different times, degradation kinetic rates, and the transformation products formed. As expected, TCE degradation was delayed or inhibited in most of the experiments, due to the presence of inorganics. The negative effects of co-pollutants can be palliated by combining surface modification with a slight increase in nZVI concentration. Encouragingly, complete TCE removal was achieved for some given experimental conditions. Noteworthily, nZVI surface modification was found to promote the efficient degradation of TCE. When degradation occurred, TCE was mainly transformed into innocuous non-chlorinated transformation products, while hazardous chlorinated transformation products accounted for a small percentage of the mass-balance. Copyright © 2014 Elsevier B.V. All rights reserved.

Robust parameter design for automatically controlled systems and nanostructure synthesis

NASA Astrophysics Data System (ADS)

Dasgupta, Tirthankar

2007-12-01

This research focuses on developing comprehensive frameworks for developing robust parameter design methodology for dynamic systems with automatic control and for synthesis of nanostructures. In many automatically controlled dynamic processes, the optimal feedback control law depends on the parameter design solution and vice versa and therefore an integrated approach is necessary. A parameter design methodology in the presence of feedback control is developed for processes of long duration under the assumption that experimental noise factors are uncorrelated over time. Systems that follow a pure-gain dynamic model are considered and the best proportional-integral and minimum mean squared error control strategies are developed by using robust parameter design. The proposed method is illustrated using a simulated example and a case study in a urea packing plant. This idea is also extended to cases with on-line noise factors. The possibility of integrating feedforward control with a minimum mean squared error feedback control scheme is explored. To meet the needs of large scale synthesis of nanostructures, it is critical to systematically find experimental conditions under which the desired nanostructures are synthesized reproducibly, at large quantity and with controlled morphology. The first part of the research in this area focuses on modeling and optimization of existing experimental data. Through a rigorous statistical analysis of experimental data, models linking the probabilities of obtaining specific morphologies to the process variables are developed. A new iterative algorithm for fitting a Multinomial GLM is proposed and used. The optimum process conditions, which maximize the above probabilities and make the synthesis process less sensitive to variations of process variables around set values, are derived from the fitted models using Monte-Carlo simulations. The second part of the research deals with development of an experimental design methodology, tailor-made to address the unique phenomena associated with nanostructure synthesis. A sequential space filling design called Sequential Minimum Energy Design (SMED) for exploring best process conditions for synthesis of nanowires. The SMED is a novel approach to generate sequential designs that are model independent, can quickly "carve out" regions with no observable nanostructure morphology, and allow for the exploration of complex response surfaces.

Fabrication of flower-like micro/nano dual scale structured copper oxide surfaces: Optimization of self-cleaning properties via Taguchi design

NASA Astrophysics Data System (ADS)

Moosavi, Saeideh Sadat; Norouzbeigi, Reza; Velayi, Elmira

2017-11-01

In the present work, copper oxide superhydrophobic surface is fabricated on a copper foil via the chemical bath deposition (CBD) method. The effects of some influential factors such as initial concentrations of Cu (II) ions and the surface energy modifier, solution pH, reaction and modification steps time on the wettability property of copper oxide surface were evaluated using Taguchi L16 experimental design. Results showed that the initial concentration of Cu (II) has the most significant impact on the water contact angle and wettability characteristics. The XRD, SEM, AFM and FTIR analyses were used to characterize the copper oxide surfaces. The Water contact angle (WCA) and contact angle hysteresis (CAH) were also measured. The SEM results indicated the formation of a flower-like micro/nano dual-scale structure of copper oxide on the substrate. This structure composed of numerous nano-petals with a thickness of about 50 nm. As a result, a copper oxide hierarchical surface with WCA of 168.4°± 3.5° and CAH of 2.73° exhibited the best superhydrophobicity under proposed optimum condition. This result has been obtained just by 10 min hydrolysis reaction. Besides, this surface showed a good stability under acidic and saline conditions.

Design of a workstation and its evaluation under the influence of noise and illumination for an assembly task.

PubMed

Muzammil, Mohammad; Ahmad, Saman; Khan, Abid Ali; Hasan, Faisal

2011-01-01

An experimental research was conducted to design a workstation for a lock manufacturing assembly. Two experiments were conducted in the present study. Nine male subjects in the age range of 18-35 years participated in the first experiment. For the second experiment, nine subjects in each of the three age groups (viz. 17-22, 23-28 and 29-35 years) volunteered for experimental investigations. The designed workstation was evaluated under varying levels of noise and illumination for workers of different age groups. Three different workstations were evaluated. The task was performed by a worker in two different sitting positions and three settings of arms position. It was found that workstation type, backrest support and arms positions were all having a statistically significant effect on task performance. Workstation with work surface to seat height ratio of 1.82 was found to be better when the task was performed using backrest and arms were supported on the work surface. This workstation was evaluated for three different age groups of workers under different levels of noise and illumination. The results of the study showed that age of the worker, illumination level and level of noise were all contributing significantly towards task performance. The design of a workstation for assembly task would help greatly in creating a better working environment and enhancing the productivity of workers exposed to environmental stressors like noise and illumination. © 2011 - IOS Press and the authors. All rights reserved

Supervised artificial neural network-based method for conversion of solar radiation data (case study: Algeria)

NASA Astrophysics Data System (ADS)

Laidi, Maamar; Hanini, Salah; Rezrazi, Ahmed; Yaiche, Mohamed Redha; El Hadj, Abdallah Abdallah; Chellali, Farouk

2017-04-01

In this study, a backpropagation artificial neural network (BP-ANN) model is used as an alternative approach to predict solar radiation on tilted surfaces (SRT) using a number of variables involved in physical process. These variables are namely the latitude of the site, mean temperature and relative humidity, Linke turbidity factor and Angstrom coefficient, extraterrestrial solar radiation, solar radiation data measured on horizontal surfaces (SRH), and solar zenith angle. Experimental solar radiation data from 13 stations spread all over Algeria around the year (2004) were used for training/validation and testing the artificial neural networks (ANNs), and one station was used to make the interpolation of the designed ANN. The ANN model was trained, validated, and tested using 60, 20, and 20 % of all data, respectively. The configuration 8-35-1 (8 inputs, 35 hidden, and 1 output neurons) presented an excellent agreement between the prediction and the experimental data during the test stage with determination coefficient of 0.99 and root meat squared error of 5.75 Wh/m2, considering a three-layer feedforward backpropagation neural network with Levenberg-Marquardt training algorithm, a hyperbolic tangent sigmoid and linear transfer function at the hidden and the output layer, respectively. This novel model could be used by researchers or scientists to design high-efficiency solar devices that are usually tilted at an optimum angle to increase the solar incident on the surface.

Analysis and design of a capsule landing system and surface vehicle control system for Mars exploration

NASA Technical Reports Server (NTRS)

Frederick, D. K.; Lashmet, P. K.; Sandor, G. N.; Shen, C. N.; Smith, E. V.; Yerazunis, S. W.

1973-01-01

Problems related to the design and control of a mobile planetary vehicle to implement a systematic plan for the exploration of Mars are reported. Problem areas include: vehicle configuration, control, dynamics, systems and propulsion; systems analysis, terrain modeling and path selection; and chemical analysis of specimens. These tasks are summarized: vehicle model design, mathematical model of vehicle dynamics, experimental vehicle dynamics, obstacle negotiation, electrochemical controls, remote control, collapsibility and deployment, construction of a wheel tester, wheel analysis, payload design, system design optimization, effect of design assumptions, accessory optimal design, on-board computer subsystem, laser range measurement, discrete obstacle detection, obstacle detection systems, terrain modeling, path selection system simulation and evaluation, gas chromatograph/mass spectrometer system concepts, and chromatograph model evaluation and improvement.

Biofluid lubrication for artificial joints

NASA Astrophysics Data System (ADS)

Pendleton, Alice Mae

This research investigated biofluid lubrication related to artificial joints using tribological and rheological approaches. Biofluids studied here represent two categories of fluids, base fluids and nanostructured biofluids. Base fluids were studied through comparison of synthetic fluids (simulated body fluid and hyaluronic acid) as well as natural biofluids (from dogs, horses, and humans) in terms of viscosity and fluid shear stress. The nano-structured biofluids were formed using molecules having well-defined shapes. Understanding nano-structured biofluids leads to new ways of design and synthesis of biofluids that are beneficial for artificial joint performance. Experimental approaches were utilized in the present research. This includes basic analysis of biofluids' property, such as viscosity, fluid shear stress, and shear rate using rheological experiments. Tribological investigation and surface characterization were conducted in order to understand effects of molecular and nanostructures on fluid lubrication. Workpiece surface structure and wear mechanisms were investigated using a scanning electron microscope and a transmission electron microscope. The surface topography was examined using a profilometer. The results demonstrated that with the adding of solid additives, such as crown ether or fullerene acted as rough as the other solids in the 3-body wear systems. In addition, the fullerene supplied low friction and low wear, which designates the lubrication purpose of this particular particle system. This dissertation is constructed of six chapters. The first chapter is an introduction to body fluids, as mentioned earlier. After Chapter II, it examines the motivation and approach of the present research, Chapter III discusses the experimental approaches, including materials, experimental setup, and conditions. In Chapter IV, lubrication properties of various fluids are discussed. The tribological properties and performance nanostructured biofluids are discussed in Chapter V, followed by summary and conclusions in Chapter VI.

Hypersonic engine component experiments in high heat flux, supersonic flow environment

NASA Technical Reports Server (NTRS)

Gladden, Herbert J.; Melis, Matthew E.

1993-01-01

A major concern in advancing the state-of-the-art technologies for hypersonic vehicles is the development of an aeropropulsion system capable of withstanding the sustained high thermal loads expected during hypersonic flight. Even though progress has been made in the computational understanding of fluid dynamics and the physics/chemistry of high speed flight, there is also a need for experimental facilities capable of providing a high heat flux environment for testing component concepts and verifying/calibrating these analyses. A hydrogen/oxygen rocket engine heat source was developed at the NASA Lewis Research Center as one element in a series of facilities at national laboratories designed to fulfill this need. This 'Hot Gas Facility' is capable of providing heat fluxes up to 450 w/sq cm on flat surfaces and up to 5,000 w/sq cm at the leading edge stagnation point of a strut in a supersonic flow stream. Gas temperatures up to 3050 K can also be attained. Two recent experimental programs conducted in this facility are discussed. The objective of the first experiment is to evaluate the erosion and oxidation characteristics of a coating on a cowl leading edge (or strut leading edge) in a supersonic, high heat flux environment. Macrophotographic data from a coated leading edge model show progressive degradation over several thermal cycles at aerothermal conditions representative of high Mach number flight. The objective of the second experiment is to assess the capability of cooling a porous surface exposed to a high temperature, high velocity flow environment and to provide a heat transfer data base for a design procedure. Experimental results from transpiration cooled surfaces in a supersonic flow environment are presented.

Functional surfaces for tribological applications: inspiration and design

NASA Astrophysics Data System (ADS)

Abdel-Aal, Hisham A.

2016-12-01

Surface texturing has been recognized as a method for enhancing the tribological properties of surfaces for many years. Adding a controlled texture to one of two faces in relative motion can have many positive effects, such as reduction of friction and wear and increase in load capacity. To date, the true potential of texturing has not been realized not because of the lack of enabling texturing technologies but because of the severe lack of detailed information about the mechanistic functional details of texturing in a tribological situation. Experimental as well as theoretical analysis of textured surfaces define important metrics for performance evaluation. These metrics represent the interaction between geometry of the texturing element and surface topology. To date, there is no agreement on the optimal values that should be implemented given a particular surface. More importantly, a well-defined methodology for the generation of deterministic textures of optimized designs virtually does not exist. Nature, on the other hand, offers many examples of efficient texturing strategies (geometries and topologies) specifically applied to mitigate frictional effects in a variety of situations. Studying these examples may advance the technology of surface engineering. This paper therefore, provides a comparative review of surface texturing that manifest viable synergy between tribology and biology. We attempt to provide successful emerging examples where borrowing from nature has inspired viable surface solutions that address difficult tribological problems both in dry and lubricated contact situations.

Investigation on the Flexural Creep Stiffness Behavior of PC-ABS Material Processed by Fused Deposition Modeling Using Response Surface Definitive Screening Design

NASA Astrophysics Data System (ADS)

Mohamed, Omar Ahmed; Masood, Syed Hasan; Bhowmik, Jahar Lal

2017-03-01

The resistance of polymeric materials to time-dependent plastic deformation is an important requirement of the fused deposition modeling (FDM) design process, its processed products, and their application for long-term loading, durability, and reliability. The creep performance of the material and part processed by FDM is the fundamental criterion for many applications with strict dimensional stability requirements, including medical implants, electrical and electronic products, and various automotive applications. Herein, the effect of FDM fabrication conditions on the flexural creep stiffness behavior of polycarbonate-acrylonitrile-butadiene-styrene processed parts was investigated. A relatively new class of experimental design called "definitive screening design" was adopted for this investigation. The effects of process variables on flexural creep stiffness behavior were monitored, and the best suited quadratic polynomial model with high coefficient of determination ( R 2) value was developed. This study highlights the value of response surface definitive screening design in optimizing properties for the products and materials, and it demonstrates its role and potential application in material processing and additive manufacturing.

Intelligent Computation for Optimal Fabrication Condition of a Protein Chip with Ni-Co Alloy-Coated Surface.

PubMed

Chang, Yaw-Jen; Chang, Cheng-Hao

2016-06-01

Based on the principle of immobilized metal affinity chromatography (IMAC), it has been found that a Ni-Co alloy-coated protein chip is able to immobilize functional proteins with a His-tag attached. In this study, an intelligent computational approach was developed to promote the performance and repeatability of a Ni-Co alloy-coated protein chip. This approach was launched out of L18 experiments. Based on the experimental data, the fabrication process model of a Ni-Co protein chip was established by using an artificial neural network, and then an optimal fabrication condition was obtained using the Taguchi genetic algorithm. The result was validated experimentally and compared with a nitrocellulose chip. Consequentially, experimental outcomes revealed that the Ni-Co alloy-coated chip, fabricated using the proposed approach, had the best performance and repeatability compared with the Ni-Co chips of an L18 orthogonal array design and the nitrocellulose chip. Moreover, the low fluorescent background of the chip surface gives a more precise fluorescent detection. Based on a small quantity of experiments, this proposed intelligent computation approach can significantly reduce the experimental cost and improve the product's quality. © 2015 Society for Laboratory Automation and Screening.

Supersonic Retropropulsion Experimental Results from the NASA Ames 9- x 7-Foot Supersonic Wind Tunnel

NASA Technical Reports Server (NTRS)

Berry, Scott A.; Rhode, Matthew N.; Edquist, Karl T.

2012-01-01

Supersonic retropropulsion was experimentally examined in the Ames Research Center 9x7-Foot Supersonic Wind Tunnel at Mach 1.8 and 2.4. The experimental model, previously designed for and tested in the Langley Research Center Unitary Plan Wind Tunnel at Mach 2.4, 3.5 and 4.6, was a 5-in diameter 70-deg sphere-cone forebody with a 9.55-in long cylindrical aftbody. The forebody was designed to accommodate up to four 4:1 area ratio nozzles, one on the model centerline and the other three on the half radius spaced 120-deg apart. Surface pressure and flow visualization were the primary measurements, including high-speed data to investigate the dynamics of the interactions between the bow and nozzle shocks. Three blowing configurations were tested with thrust coefficients up to 10 and angles of attack up to 20-deg. Preliminary results and observations from the test are provided

Application of Box-Behnken experimental design to optimize the extraction of insecticidal Cry1Ac from soil.

PubMed

Li, Yan-Liang; Fang, Zhi-Xiang; You, Jing

2013-02-20

A validated method for analyzing Cry proteins is a premise to study the fate and ecological effects of contaminants associated with genetically engineered Bacillus thuringiensis crops. The current study has optimized the extraction method to analyze Cry1Ac protein in soil using a response surface methodology with a three-level-three-factor Box-Behnken experimental design (BBD). The optimum extraction conditions were at 21 °C and 630 rpm for 2 h. Regression analysis showed a good fit of the experimental data to the second-order polynomial model with a coefficient of determination of 0.96. The method was sensitive and precise with a method detection limit of 0.8 ng/g dry weight and relative standard deviations at 7.3%. Finally, the established method was applied for analyzing Cry1Ac protein residues in field-collected soil samples. Trace amounts of Cry1Ac protein were detected in the soils where transgenic crops have been planted for 8 and 12 years.

Fundamental phenomena on fuel decomposition and boundary layer combustion processes with applications to hybrid rocket motors

NASA Technical Reports Server (NTRS)

Kuo, Kenneth K.; Lu, Y. C.; Chiaverini, Martin J.; Harting, George C.

1994-01-01

An experimental study on the fundamental processes involved in fuel decomposition and boundary layer combustion in hybrid rocket motors is being conducted at the High Pressure Combustion Laboratory of the Pennsylvania State University. This research should provide an engineering technology base for development of large scale hybrid rocket motors as well as a fundamental understanding of the complex processes involved in hybrid propulsion. A high pressure slab motor has been designed for conducting experimental investigations. Oxidizer (LOX or GOX) is injected through the head-end over a solid fuel (HTPB) surface. Experiments using fuels supplied by NASA designated industrial companies will also be conducted. The study focuses on the following areas: measurement and observation of solid fuel burning with LOX or GOX, correlation of solid fuel regression rate with operating conditions, measurement of flame temperature and radical species concentrations, determination of the solid fuel subsurface temperature profile, and utilization of experimental data for validation of a companion theoretical study also being conducted at PSU.

Experimental Verification of a Progressive Damage Model for IM7/5260 Laminates Subjected to Tension-Tension Fatigue

NASA Technical Reports Server (NTRS)

Coats, Timothy W.; Harris, Charles E.

1995-01-01

The durability and damage tolerance of laminated composites are critical design considerations for airframe composite structures. Therefore, the ability to model damage initiation and growth and predict the life of laminated composites is necessary to achieve structurally efficient and economical designs. The purpose of this research is to experimentally verify the application of a continuum damage model to predict progressive damage development in a toughened material system. Damage due to monotonic and tension-tension fatigue was documented for IM7/5260 graphite/bismaleimide laminates. Crack density and delamination surface area were used to calculate matrix cracking and delamination internal state variables to predict stiffness loss in unnotched laminates. A damage dependent finite element code predicted the stiffness loss for notched laminates with good agreement to experimental data. It was concluded that the continuum damage model can adequately predict matrix damage progression in notched and unnotched laminates as a function of loading history and laminate stacking sequence.

Mars ecopoiesis test bed: on earth and on the red planet

NASA Astrophysics Data System (ADS)

Todd, Paul; Kurk, Michael Andy; Boland, Eugene; Thomas, David; Scherzer, Christopher

2016-07-01

The concept of autotrophic organisms serving as planetary pioneers as a precursor to terraforming has been under consideration for several decades, and the term Ecopoiesis was introduced by the ecopoiets C. Sagan, M. Avener, R. Haynes and C. McKay to call attention to this possibility. There is a continuing need for experimental evidence to support this concept, one of them being the need to evaluate the survivability of terrestrial autotrophic microbes in a planetary environment. For this and other purposes a planetary simulation facility was constructed and operated at Techshot, Inc. in Indiana, USA. This facility has an accumulated record of more than one year's worth of experimentation under simulated Mars conditions. In a recent study this facility was operated for five weeks in a mode that simulated 35 sols on and just below the surface of Mars at low latitude. The diurnal lighting period was 12 hours:12 hours using xenon arc light filtered to simulate the solar intensity and spectrum on the Martian surface. A daily temperature profile followed that recorded at low latitudes with night-time minima at -80 C and noontime maxima at +26 C. Atmosphere was CO _{2} at <11 mbar. Moisture was monitored to confirm that no water could exist in the liquid phase. Test organisms included the cyanobacteria Anabena, sp., Chroococcidiopsis CCMEE171 and Plectonema boryanum and Eukaryota: Chlorella ellipsoidia maintained in the simulator under the above-described conditions. The exposed specimens were tested for intracellular esterase activity, chlorophyll content and reproductive survival. All tests yielded low-level positive survival results for these organisms. No definitive data relating to function and/or growth during exposure were sought. In parallel to these terrestrial studies a planned design study was undertaken for a proposed test bed to be operated on the surface of Mars. Design requirements include compact assembly for transport and installation on the planetary surface (multiple units per mission would be expected), protective internal package for the release of organisms, a means of atmosphere exchange, access to sunlight, a means of penetrating the planetary surface, and most importantly a means of acquiring regolith while meeting requirements of planetary protection. An enlarged-scale mock-up of this design was fabricated by additive manufacturing with moving parts that simulate the components of the design. This mock-up assembly marks a starting point for a planetary surface probe for safe implantation on the surface of the Red Planet some decades in the future. This research was supported by NASA NIAC Phase I Grant "Mars Ecopoiesis Testbed" NNX14AM97G.

Experimental designs for modeling retention patterns and separation efficiency in analysis of fatty acid methyl esters by gas chromatography-mass spectrometry.

PubMed

Skartland, Liv Kjersti; Mjøs, Svein A; Grung, Bjørn

2011-09-23

The retention behavior of components analyzed by chromatography varies with instrumental settings. Being able to predict how changes in these settings alter the elution pattern is useful, both with regards to component identification, as well as with regards to optimization of the chromatographic system. In this work, it is shown how experimental designs can be used for this purpose. Different experimental designs for response surface modeling of the separation of fatty acid methyl esters (FAME) as function of chromatographic conditions in GC have been evaluated. Full factorial, central composite, Doehlert and Box-Behnken designs were applied. A mixture of 38 FAMEs was separated on a polar cyanopropyl substituted polysilphenylene-siloxane phase capillary column. The temperature gradient, the start temperature of the gradient, and the carrier gas velocity were varied in the experiments. The modeled responses, as functions of chromatographic conditions, were retention time, retention indices, peak widths, separation efficiency and resolution between selected peak pairs. The designs that allowed inclusion of quadratic terms among the predictors performed significantly better than factorial design. Box-Behnken design provided the best results for prediction of retention, but the differences between the central composite, Doehlert and Box-Behnken designs were small. Retention indices could be modeled with much better accuracy than retention times. However, because the errors of predicted tR of closely eluting peaks were highly correlated, models of resolution (Rs) that were based on retention time had errors in the same range as corresponding models based on ECL. Copyright © 2011 Elsevier B.V. All rights reserved.

LOW-ENGINE-FRICTION TECHNOLOGY FOR ADVANCED NATURAL-GAS RECIPROCATING ENGINES

DOE Office of Scientific and Technical Information (OSTI.GOV)

Victor Wong; Tian Tian; Luke Moughon

2005-09-30

This program aims at improving the efficiency of advanced natural-gas reciprocating engines (ANGRE) by reducing piston and piston ring assembly friction without major adverse effects on engine performance, such as increased oil consumption and wear. An iterative process of simulation, experimentation and analysis is being followed towards achieving the goal of demonstrating a complete optimized low-friction engine system. To date, a detailed set of piston and piston-ring dynamic and friction models have been developed and applied that illustrate the fundamental relationships between design parameters and friction losses. Low friction ring designs have already been recommended in a previous phase, withmore » full-scale engine validation partially completed. Current accomplishments include the addition of several additional power cylinder design areas to the overall system analysis. These include analyses of lubricant and cylinder surface finish and a parametric study of piston design. The Waukesha engine was found to be already well optimized in the areas of lubricant, surface skewness and honing cross-hatch angle, where friction reductions of 12% for lubricant, and 5% for surface characteristics, are projected. For the piston, a friction reduction of up to 50% may be possible by controlling waviness alone, while additional friction reductions are expected when other parameters are optimized. A total power cylinder friction reduction of 30-50% is expected, translating to an engine efficiency increase of two percentage points from its current baseline towards the goal of 50% efficiency. Key elements of the continuing work include further analysis and optimization of the engine piston design, in-engine testing of recommended lubricant and surface designs, design iteration and optimization of previously recommended technologies, and full-engine testing of a complete, optimized, low-friction power cylinder system.« less

Optimization of Xylanase Production from Penicillium sp.WX-Z1 by a Two-Step Statistical Strategy: Plackett-Burman and Box-Behnken Experimental Design

PubMed Central

Cui, Fengjie; Zhao, Liming

2012-01-01

The objective of the study was to optimize the nutrition sources in a culture medium for the production of xylanase from Penicillium sp.WX-Z1 using Plackett-Burman design and Box-Behnken design. The Plackett-Burman multifactorial design was first employed to screen the important nutrient sources in the medium for xylanase production by Penicillium sp.WX-Z1 and subsequent use of the response surface methodology (RSM) was further optimized for xylanase production by Box-Behnken design. The important nutrient sources in the culture medium, identified by the initial screening method of Placket-Burman, were wheat bran, yeast extract, NaNO3, MgSO4, and CaCl2. The optimal amounts (in g/L) for maximum production of xylanase were: wheat bran, 32.8; yeast extract, 1.02; NaNO3, 12.71; MgSO4, 0.96; and CaCl2, 1.04. Using this statistical experimental design, the xylanase production under optimal condition reached 46.50 U/mL and an increase in xylanase activity of 1.34-fold was obtained compared with the original medium for fermentation carried out in a 30-L bioreactor. PMID:22949884

Optimization of Xylanase production from Penicillium sp.WX-Z1 by a two-step statistical strategy: Plackett-Burman and Box-Behnken experimental design.

PubMed

Cui, Fengjie; Zhao, Liming

2012-01-01

The objective of the study was to optimize the nutrition sources in a culture medium for the production of xylanase from Penicillium sp.WX-Z1 using Plackett-Burman design and Box-Behnken design. The Plackett-Burman multifactorial design was first employed to screen the important nutrient sources in the medium for xylanase production by Penicillium sp.WX-Z1 and subsequent use of the response surface methodology (RSM) was further optimized for xylanase production by Box-Behnken design. The important nutrient sources in the culture medium, identified by the initial screening method of Placket-Burman, were wheat bran, yeast extract, NaNO(3), MgSO(4), and CaCl(2). The optimal amounts (in g/L) for maximum production of xylanase were: wheat bran, 32.8; yeast extract, 1.02; NaNO(3), 12.71; MgSO(4), 0.96; and CaCl(2), 1.04. Using this statistical experimental design, the xylanase production under optimal condition reached 46.50 U/mL and an increase in xylanase activity of 1.34-fold was obtained compared with the original medium for fermentation carried out in a 30-L bioreactor.

Design of ice-free nanostructured surfaces based on repulsion of impacting water droplets.

PubMed

Mishchenko, Lidiya; Hatton, Benjamin; Bahadur, Vaibhav; Taylor, J Ashley; Krupenkin, Tom; Aizenberg, Joanna

2010-12-28

Materials that control ice accumulation are important to aircraft efficiency, highway and powerline maintenance, and building construction. Most current deicing systems include either physical or chemical removal of ice, both energy and resource-intensive. A more desirable approach would be to prevent ice formation rather than to fight its build-up. Much attention has been given recently to freezing of static water droplets resting on supercooled surfaces. Ice accretion, however, begins with the droplet/substrate collision followed by freezing. Here we focus on the behavior of dynamic droplets impacting supercooled nano- and microstructured surfaces. Detailed experimental analysis of the temperature-dependent droplet/surface interaction shows that highly ordered superhydrophobic materials can be designed to remain entirely ice-free down to ca. -25 to -30 °C, due to their ability to repel impacting water before ice nucleation occurs. Ice accumulated below these temperatures can be easily removed. Factors contributing to droplet retraction, pinning and freezing are addressed by combining classical nucleation theory with heat transfer and wetting dynamics, forming the foundation for the development of rationally designed ice-preventive materials. In particular, we emphasize the potential of hydrophobic polymeric coatings bearing closed-cell surface microstructures for their improved mechanical and pressure stability, amenability to facile replication and large-scale fabrication, and opportunities for greater tuning of their material and chemical properties.

Pressure Gradient Effects on Hypersonic Cavity Flow Heating

NASA Technical Reports Server (NTRS)

Everhart, Joel L.; Alter, Stephen J.; Merski, N. Ronald; Wood, William A.; Prabhu, Ramadas K.

2006-01-01

The effect of a pressure gradient on the local heating disturbance of rectangular cavities tested at hypersonic freestream conditions has been globally assessed using the two-color phosphor thermography method. These experiments were conducted in the Langley 31-Inch Mach 10 Tunnel and were initiated in support of the Space Shuttle Return-To-Flight Program. Two blunted-nose test surface geometries were developed, including an expansion plate test surface with nearly constant negative pressure gradient and a flat plate surface with nearly zero pressure gradient. The test surface designs and flow characterizations were performed using two-dimensional laminar computational methods, while the experimental boundary layer state conditions were inferred using the measured heating distributions. Three-dimensional computational predictions of the entire model geometry were used as a check on the design process. Both open-flow and closed-flow cavities were tested on each test surface. The cavity design parameters and the test condition matrix were established using the computational predictions. Preliminary conclusions based on an analysis of only the cavity centerline data indicate that the presence of the pressure gradient did not alter the open cavity heating for laminar-entry/laminar-exit flows, but did raise the average floor heating for closed cavities. The results of these risk-reduction studies will be used to formulate a heating assessment of potential damage scenarios occurring during future Space Shuttle flights.

Pressure Gradient Effects on Hypersonic Cavity Flow Heating

NASA Technical Reports Server (NTRS)

Everhart, Joel L.; Alter, Stephen J.; Merski, N. Ronald; Wood, William A.; Prabhu, Ramdas K.

2007-01-01

The effect of a pressure gradient on the local heating disturbance of rectangular cavities tested at hypersonic freestream conditions has been globally assessed using the two-color phosphor thermography method. These experiments were conducted in the Langley 31-Inch Mach 10 Tunnel and were initiated in support of the Space Shuttle Return-To-Flight Program. Two blunted-nose test surface geometries were developed, including an expansion plate test surface with nearly constant negative pressure gradient and a flat plate surface with nearly zero pressure gradient. The test surface designs and flow characterizations were performed using two-dimensional laminar computational methods, while the experimental boundary layer state conditions were inferred using the measured heating distributions. Three-dimensional computational predictions of the entire model geometry were used as a check on the design process. Both open-flow and closed-flow cavities were tested on each test surface. The cavity design parameters and the test condition matrix were established using the computational predictions. Preliminary conclusions based on an analysis of only the cavity centerline data indicate that the presence of the pressure gradient did not alter the open cavity heating for laminar-entry/laminar-exit flows, but did raise the average floor heating for closed cavities. The results of these risk-reduction studies will be used to formulate a heating assessment of potential damage scenarios occurring during future Space Shuttle flights.

Chitosan based grey wastewater treatment--a statistical design approach.

PubMed

Thirugnanasambandham, K; Sivakumar, V; Prakash Maran, J; Kandasamy, S

2014-01-01

In this present study, grey wastewater was treated under different operating conditions such as agitation time (1-3 min), pH (2.5-5.5), chitosan dose (0.3-0.6g/l) and settling time (10-20 min) using response surface methodology (RSM). Four factors with three levels Box-Behnken response surface design (BBD) were employed to optimize and investigate the effect of process variables on the responses such as turbidity, BOD and COD removal. The results were analyzed by Pareto analysis of variance (ANOVA) and second order polynomial models were developed in order to predict the responses. Under the optimum conditions, experimental values such as turbidity (96%), BOD (91%) and COD (73%) removals are closely agreed with predicted values. Copyright © 2013 Elsevier Ltd. All rights reserved.

Test load verification through strain data analysis

NASA Technical Reports Server (NTRS)

Verderaime, V.; Harrington, F.

1995-01-01

A traditional binding acceptance criterion on polycrystalline structures is the experimental verification of the ultimate factor of safety. At fracture, the induced strain is inelastic and about an order-of-magnitude greater than designed for maximum expected operational limit. At this extreme strained condition, the structure may rotate and displace at the applied verification load such as to unknowingly distort the load transfer into the static test article. Test may result in erroneously accepting a submarginal design or rejecting a reliable one. A technique was developed to identify, monitor, and assess the load transmission error through two back-to-back surface-measured strain data. The technique is programmed for expediency and convenience. Though the method was developed to support affordable aerostructures, the method is also applicable for most high-performance air and surface transportation structural systems.

Orientation-Dependent Exciton-Plasmon Coupling in Embedded Organic/Metal Nanowire Heterostructures.

PubMed

Li, Yong Jun; Hong, Yan; Peng, Qian; Yao, Jiannian; Zhao, Yong Sheng

2017-10-24

The excitation of surface plasmons by optical emitters based on exciton-plasmon coupling is important for plasmonic devices with active optical properties. It has been theoretically demonstrated that the orientation of exciton dipole can significantly influence the coupling strength, yet systematic study of the coupling process in nanostructures is still hindered by the lack of proper material systems. In this work, we have experimentally investigated the orientation-dependent exciton-plasmon coupling in a rationally designed organic/metal nanowire heterostructure system. The heterostructures were prepared by inserting silver nanowires into crystalline organic waveguides during the self-assembly of dye molecules. Structures with different exciton orientations exhibited varying coupling efficiencies. The near-field exciton-plasmon coupling facilitates the design of nanophotonic devices based on the directional surface plasmon polariton propagations.

Convective Heat Transfer with and without Film Cooling in High Temperature, Fuel Rich and Lean Environments

NASA Astrophysics Data System (ADS)

Greiner, Nathan J.

Modern turbine engines require high turbine inlet temperatures and pressures to maximize thermal efficiency. Increasing the turbine inlet temperature drives higher heat loads on the turbine surfaces. In addition, increasing pressure ratio increases the turbine coolant temperature such that the ability to remove heat decreases. As a result, highly effective external film cooling is required to reduce the heat transfer to turbine surfaces. Testing of film cooling on engine hardware at engine temperatures and pressures can be exceedingly difficult and expensive. Thus, modern studies of film cooling are often performed at near ambient conditions. However, these studies are missing an important aspect in their characterization of film cooling effectiveness. Namely, they do not model effect of thermal property variations that occur within the boundary and film cooling layers at engine conditions. Also, turbine surfaces can experience significant radiative heat transfer that is not trivial to estimate analytically. The present research first computationally examines the effect of large temperature variations on a turbulent boundary layer. Subsequently, a method to model the effect of large temperature variations within a turbulent boundary layer in an environment coupled with significant radiative heat transfer is proposed and experimentally validated. Next, a method to scale turbine cooling from ambient to engine conditions via non-dimensional matching is developed computationally and the experimentally validated at combustion temperatures. Increasing engine efficiency and thrust to weight ratio demands have driven increased combustor fuel-air ratios. Increased fuel-air ratios increase the possibility of unburned fuel species entering the turbine. Alternatively, advanced ultra-compact combustor designs have been proposed to decrease combustor length, increase thrust, or generate power for directed energy weapons. However, the ultra-compact combustor design requires a film cooled vane within the combustor. In both these environments, the unburned fuel in the core flow encounters the oxidizer rich film cooling stream, combusts, and can locally heat the turbine surface rather than the intended cooling of the surface. Accordingly, a method to quantify film cooling performance in a fuel rich environment is prescribed. Finally, a method to film cool in a fuel rich environment is experimentally demonstrated.

Solution Exchange Lithography: A Versatile Tool for Sequential Surface Engineering

NASA Astrophysics Data System (ADS)

Pester, Christian; Mattson, Kaila; Bothman, David; Klinger, Daniel; Lee, Kenneth; Discekici, Emre; Narupai, Benjaporn; Hawker, Craig

The covalent attachment of polymers has emerged as a viable strategy for the preparation of multi-functional surfaces. Patterned, surface-grafted polymer brushes provide spatial control over wetting, mechanical, biological or electronic properties, and allow fabrication of `intelligent' substrates which selectively adapt to their environment. However, the route towards patterned polymer brush surfaces often remains challenging, creating a demand for more efficient and less complicated fabrication strategies. We describe the design and application of a novel experimental setup to combine light-mediated and flow chemistry for the fabrication of hierarchical surface-grafted polymer brushes. Using light-mediated, surface initiated controlled radical polymerization and post-functionalization via well-established, and highly efficient chemistries, polymer brush films of previously unimaginable complexity are now shown to be accessible. This methodology allows full flexibility to exchange both lithographic photomasks and chemical environments in-situ, readily affording multidimensional thin film architectures, all from uniformly functionalized substrates.

Coupling surface and mantle dynamics: A novel experimental approach

NASA Astrophysics Data System (ADS)

Kiraly, Agnes; Faccenna, Claudio; Funiciello, Francesca; Sembroni, Andrea

2015-05-01

Recent modeling shows that surface processes, such as erosion and deposition, may drive the deformation of the Earth's surface, interfering with deeper crustal and mantle signals. To investigate the coupling between the surface and deep process, we designed a three-dimensional laboratory apparatus, to analyze the role of erosion and sedimentation, triggered by deep mantle instability. The setup is constituted and scaled down to natural gravity field using a thin viscous sheet model, with mantle and lithosphere simulated by Newtonian viscous glucose syrup and silicon putty, respectively. The surface process is simulated assuming a simple erosion law producing the downhill flow of a thin viscous material away from high topography. The deep mantle upwelling is triggered by the rise of a buoyant sphere. The results of these models along with the parametric analysis show how surface processes influence uplift velocity and topography signals.

Formation and metrology of dual scale nano-morphology on SF(6) plasma etched silicon surfaces.

PubMed

Boulousis, G; Constantoudis, V; Kokkoris, G; Gogolides, E

2008-06-25

Surface roughness and nano-morphology in SF(6) plasma etched silicon substrates are investigated in a helicon type plasma reactor as a function of etching time and process parameters. The plasma etched surfaces are analyzed by atomic force microscopy. It is found that dual scale nano-roughness is formatted on the silicon surface comprising an underlying nano-roughness and superimposed nano-mounds. Detailed metrological quantification is proposed for the characterization of dual scale surface morphology. As etching proceeds, the mounds become higher, fewer and wider, and the underlying nano-roughness also increases. Increase in wafer temperature leads to smoother surfaces with lower, fewer and wider nano-mounds. A mechanism based on the deposition of etch inhibiting particles during the etching process is proposed for the explanation of the experimental behavior. In addition, appropriately designed experiments are conducted, and they confirm the presence of this mechanism.

The contact sport of rough surfaces

NASA Astrophysics Data System (ADS)

Carpick, Robert W.

2018-01-01

Describing the way two surfaces touch and make contact may seem simple, but it is not. Fully describing the elastic deformation of ideally smooth contacting bodies, under even low applied pressure, involves second-order partial differential equations and fourth-rank elastic constant tensors. For more realistic rough surfaces, the problem becomes a multiscale exercise in surface-height statistics, even before including complex phenomena such as adhesion, plasticity, and fracture. A recent research competition, the “Contact Mechanics Challenge” (1), was designed to test various approximate methods for solving this problem. A hypothetical rough surface was generated, and the community was invited to model contact with this surface with competing theories for the calculation of properties, including contact area and pressure. A supercomputer-generated numerical solution was kept secret until competition entries were received. The comparison of results (2) provides insights into the relative merits of competing models and even experimental approaches to the problem.

A New Look at Factors Affecting Microbial Silicification: Effects of Microbe to Solution Ratio, Al and Fe on Silica Accumulation on B. subtilis Surfaces

NASA Astrophysics Data System (ADS)

Tenesch, A. C.; Hinman, N. W.; Blank, C. E.

2006-12-01

In this investigation, we aim to constrain the geochemical conditions that favor siliceous microfossil formation. This work will provide a framework for assessing the biogenic origin of putative microfossils in siliceous hydrothermal deposits on early Earth, and potentially, on Mars. Previous work on silicification of microbial cells has been done under unnatural conditions or when cells were physiological stressed. Here, we attempt to reduce the amount reduce the amount of physiological stress on the organisms and to better emulate the natural environment. Silicification experiments involving the gram-positive bacterium, Bacillus subtilis, have been conducted under different experimental conditions to provide insight into the processes that affect silicification of microorganisms. Experiments were conducted with silica stock solution at an initial pH of 8, and with and without added Al and Fe, in two different experimental designs. The first experimental design represented a silica-limited environment in which the ratio of exponentially growing culture (O.D.600 = 0.2) to silica-rich stock solution was very high (1:1 v/v). Silica concentrations declined likely due to nucleation and precipitation mediated by microbial surfaces, and the pH dropped from 8.0 to 6.5. The presence of Fe and Al resulted in lower dissolved silica concentrations, suggesting additional effects of these ions on nucleation and precipitation. The second experimental design used a lower ratio of exponentially growing culture (O.D.600 = .2) to silica-rich stock solution (0.004:1 v/v) resulting in a stable concentration of silica, which was also accompanied by a slight decline in pH. This latter design is more similar to the cell:silica ratios found in natural environments. B. subtilis cells were examined using scanning electron microscopy (SEM) accompanied by energy dispersive spectrometry (EDS). Cells exhibited silica crystallites under SEM and yet continued to undergo cell division in an environment of limited resources. Silicification in the low-ratio experiments appeared to be more efficient as cells were more encrusted with Si than cells in the high-ratio experiments. Further, sporulation was more efficient in the low-ratio experiments.

Ultra wideband surface wave communications

NASA Astrophysics Data System (ADS)

Lacomb, Julie Anne

Ultra Wideband (UWB), an impulse carrier waveform, was applied at HF-VHF frequencies to utilize surface wave propagation. UWB involves the propagation of transient pulses rather than continuous waves which makes the system easier to implement, inexpensive, low power and small. Commercial UWB for wireless personal area networks is 3.1 to 10.6 GHz band as approved by the FCC with ranges up to 12 ft. The use of surface wave propagation (instead of commercial SHF UWB) extends the communication range. Surface wave is a means of propagation where the wave is guided by the surface of the Earth. Surface wave is efficient at low frequencies, VLF to HF. The UWB HF channel was modeled and also experimentally characterized. The Federal Communications Commission (FCC) defines UWB as a signal with either a fractional bandwidth of 20% of the center frequency or a bandwidth of 500MHz. Designing an antenna to operate over the 20% bandwidth requirement of UWB is one of the greatest challenges. Two different antenna designs are presented, a spoke top antenna and a traveling wave antenna with photonic bandgap. These designs were implemented at the commercial UWB frequencies (3.1--10.6 GHz) due to availability of modeling tools for the higher frequencies, the reduced antenna size and the availability of measurement facilities. The spoke top was optimum for replication of the time domain input signal. The traveling wave antenna with photonic bandgap demonstrated increased impedance bandwidth of the antenna.

Thermophysical fundamentals of cyclonic recirculating heating devices

NASA Astrophysics Data System (ADS)

Karpov, S. V.; Zagoskin, A. A.

2017-10-01

This report presents the results of experimental and theoretical research of aerodynamics and convective heat transfer in cyclone devices with the new system of external recirculation of heating gas under the influence of radial pressure gradient in a heat carrier’s swirling turbulent flow. The dynamic problem of tangential velocity distribution in a clearance volume is solved at various re-circulation ratio values including limiting quantities (kr = 0; 1) and variations in cyclonic combustion chamber’s design parameters and operating conditions (Rer); the integrated calculation ratios for fundamental aerodynamic characteristics of a recirculation device are derived. The first experimental and numerical studies of convective heat transfer on internal and external surfaces of a hollow shaft in a swirling recirculation flow are derived through the instrumentality of OpenFOAM, these studies are also conducted for a setting of several cylindrical solid inserts. The external surface heat problem of a hollow cylindrical insert is solved with integral and digital methods; generalized similarity equations for the internal and external surfaces extended in range of Reynolds number are derived. The experimental data is in reasonable agreement with the derived curves and the results of mathematic modelling of convective heat transfer. Calculation recommendations for optimal selection of kr values at various ratios of their geometric characteristics and products utilization rate are obtained.

In situ plasma removal of surface contaminants from ion trap electrodes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Haltli, Raymond A.

2015-05-01

In this thesis, the construction and implementation of an in situ plasma discharge designed to remove surface contaminants from electrodes in an ion trapping experimental system is presented with results. In recent years, many advances have been made in using ion traps for quantum information processing. All of the criteria defined by DiVincenzo for using ion traps for implementing a quantum computer have been individually demonstrated, and in particular surface traps provide a scalable platform for ions. In order to be used for quantum algorithms, trapped ions need to be cooled to their motional (quantum mechanical) ground state. One ofmore » the hurdles in integrating surface ion traps for a quantum computer is minimizing electric field noise, which causes the ion to heat out of its motional ground state and which increases with smaller ion-to-electrode distances realized with surface traps. Surface contamination of trap electrodes is speculated to be the primary source of electric field noise. The main goal achieved by this work was to implement an in situ surface cleaning solution for surface electrode ion traps, which would not modify the ion trap electrode surface metal. Care was taken in applying the RF power in order to localize a plasma near the trap electrodes. A method for characterizing the energy of the plasma ions arriving at the ion trap surface is presented and results for plasma ion energies are shown. Finally, a method for quantifying the effectiveness of plasma cleaning of trap electrodes, using the surface analysis technique of X-ray photoelectron spectroscopy for measuring the amount and kind of surface contaminants, is described. A significant advantage of the trap electrode surface cleaning method presented here is the minimal changes necessary for implementation on a working ion trap experimental system.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moritzer, E., E-mail: elmar.moritzer@ktp.upb.de; Leister, C., E-mail: elmar.moritzer@ktp.upb.de

The industrial use of atmospheric pressure plasmas in the plastics processing industry has increased significantly in recent years. Users of this treatment process have the possibility to influence the target values (e.g. bond strength or surface energy) with the help of kinematic and electrical parameters. Until now, systematic procedures have been used with which the parameters can be adapted to the process or product requirements but only by very time-consuming methods. For this reason, the relationship between influencing values and target values will be examined based on the example of a pretreatment in the bonding process with the help ofmore » statistical experimental design. Because of the large number of parameters involved, the analysis is restricted to the kinematic and electrical parameters. In the experimental tests, the following factors are taken as parameters: gap between nozzle and substrate, treatment velocity (kinematic data), voltage and duty cycle (electrical data). The statistical evaluation shows significant relationships between the parameters and surface energy in the case of polypropylene. An increase in the voltage and duty cycle increases the polar proportion of the surface energy, while a larger gap and higher velocity leads to lower energy levels. The bond strength of the overlapping bond is also significantly influenced by the voltage, velocity and gap. The direction of their effects is identical with those of the surface energy. In addition to the kinematic influences of the motion of an atmospheric pressure plasma jet, it is therefore especially important that the parameters for the plasma production are taken into account when designing the pretreatment processes.« less

A measurement of the angular distribution of 5 eV atomic oxygen scattered off a solid surface in earth orbit

NASA Technical Reports Server (NTRS)

Gregory, John C.; Peters, Palmer N.

1986-01-01

The angular distribution of 5 eV atomic oxygen scattered off a polished vitreous carbon surface was measured on a recent Space Shuttle flight. The experimental apparatus was of novel design, completely passive, and used thin silver films as the recording device for oxygen atoms. Most of the incident oxygen was contained in the reflected beam and remained in an active form and probably still atoms. Allowance was made for 12 percent loss of incident atoms which are converted to CO at the carbon surface. The scattered distribution which is wide lobular, peaking 15 deg in the forward direction, shows almost but not quite full accommodation.

Surface erosion caused on Mars from Viking descent engine plume

USGS Publications Warehouse

Hutton, R.E.; Moore, H.J.; Scott, R.F.; Shorthill, R.W.; Spitzer, C.R.

1980-01-01

During the Martian landings the descent engine plumes on Viking Lander 1 (VL-1) and Viking Lander 2 (VL-2) eroded the Martian surface materials. This had been anticipated and investigated both analytically and experimentally during the design phase of the Viking spacecraft. This paper presents data on erosion obtained during the tests of the Viking descent engine and the evidence for erosion by the descent engines of VL-1 and VL-2 on Mars. From these and other results, it is concluded that there are four distinct surface materials on Mars: (1) drift material, (2) crusty to cloddy material, (3) blocky material, and (4) rock. ?? 1980 D. Reidel Publishing Co.

How merging droplets jump off a superhydrophobic surface: Measurements and model

NASA Astrophysics Data System (ADS)

Mouterde, Timothée; Nguyen, Thanh-Vinh; Takahashi, Hidetoshi; Clanet, Christophe; Shimoyama, Isao; Quéré, David

2017-11-01

We investigate how drops merging on a nonwettable surface jump off this surface, for both symmetric and asymmetric coalescences. For this purpose, we design and build a microelectromechanical system sensor able to quantify forces down to the micro-Newton scale at a high acquisition rate (200 kHz). Using this device, we perform direct force measurements of self-propelled droplets coupled to high-speed imaging. Experimental data show that the total momentum of the drop after coalescence mainly depends on the size of the smaller drop. Exploiting this finding, we quantitatively predict the takeoff speed of jumping drop pairs and show how to correct the usual argument based on energy conservation.

Parametric Optimization of Wire Electrical Discharge Machining of Powder Metallurgical Cold Worked Tool Steel using Taguchi Method

NASA Astrophysics Data System (ADS)

Sudhakara, Dara; Prasanthi, Guvvala

2017-04-01

Wire Cut EDM is an unconventional machining process used to build components of complex shape. The current work mainly deals with optimization of surface roughness while machining P/M CW TOOL STEEL by Wire cut EDM using Taguchi method. The process parameters of the Wire Cut EDM is ON, OFF, IP, SV, WT, and WP. L27 OA is used for to design of the experiments for conducting experimentation. In order to find out the effecting parameters on the surface roughness, ANOVA analysis is engaged. The optimum levels for getting minimum surface roughness is ON = 108 µs, OFF = 63 µs, IP = 11 A, SV = 68 V and WT = 8 g.

Characterizing the Role of Nanoparticle Design on Tumor Transport and Stability in the Extracellular Environment

NASA Astrophysics Data System (ADS)

Albanese, Alexandre

Nanotechnology has emerged as an exciting strategy for the delivery of diagnostic and therapeutic agents into established tumors. Advancements in nanomaterial synthesis have generated an extensive number of nanoparticle designs made from different materials. Unfortunately, it remains impossible to predict a design's effectiveness for in vivo tumor accumulation. Little is known about how a nanoparticle's morphology and surface chemistry affect its interactions with cells and proteins inside the tumor tissue. This thesis focuses on the development of in vitro experimental tools to evaluate how nanoparticle design affects transport in a three-dimensional tumor tissue and stability in the tumor microenvironment. Nanoparticle transport was evaluated using a novel 'tumor-on-a-chip' system where multicellular tumor spheroids were immobilized in a microfluidic channel. This setup created a three-dimensional tumor environment displaying physiological cell density, extracellular matrix organization, and interstitial flow rates. The tumor-on-a-chip demonstrated that accumulation of nanoparticles was limited to diameters below 110 nm and was improved by receptor targeting. Nanoparticle stability in the tumor microenvironment was evaluated using media isolated from different tumor cell lines. Nanoparticle diameter and surface chemistry were important determinants of stability in cancer cell-conditioned media. Small nanoparticles with unstable surface chemistries adsorbed cellular proteins on their surface and were prone to aggregation. Nanoparticle aggregation altered cellular interactions leading to changes in cell uptake. Using a novel technique to generate different aggregate sizes possessing a uniform surface composition, it was determined that aggregation can change receptor affinity, cell internalization mechanisms and sub-cellular sequestration patterns. Data from this thesis characterize the behavior of nanoparticles within modeled tumor environments and provide some preliminary design guidelines for maximizing nanoparticle tumor accumulation. This work highlights the importance of characterizing nano-bio interactions for engineering successful nanomaterial-based delivery systems.

Thermoelectric Power Generation System for Future Hybrid Vehicles Using Hot Exhaust Gas

NASA Astrophysics Data System (ADS)

Kim, Sun-Kook; Won, Byeong-Cheol; Rhi, Seok-Ho; Kim, Shi-Ho; Yoo, Jeong-Ho; Jang, Ju-Chan

2011-05-01

The present experimental and computational study investigates a new exhaust gas waste heat recovery system for hybrid vehicles, using a thermoelectric module (TEM) and heat pipes to produce electric power. It proposes a new thermoelectric generation (TEG) system, working with heat pipes to produce electricity from a limited hot surface area. The current TEG system is directly connected to the exhaust pipe, and the amount of electricity generated by the TEMs is directly proportional to their heated area. Current exhaust pipes fail to offer a sufficiently large hot surface area for the high-efficiency waste heat recovery required. To overcome this, a new TEG system has been designed to have an enlarged hot surface area by the addition of ten heat pipes, which act as highly efficient heat transfer devices and can transmit the heat to many TEMs. As designed, this new waste heat recovery system produces a maximum 350 W when the hot exhaust gas heats the evaporator surface of the heat pipe to 170°C; this promises great possibilities for application of this technology in future energy-efficient hybrid vehicles.

Optimum BET surface areas for activated carbon produced from textile sewage sludges and its application as dye removal.

PubMed

Kacan, Erdal

2016-01-15

The purpose of this experimental study is to determine optimum preparation conditions for activated carbons obtained from textile sewage sludge (TSS) for removal of dyes from aqueous solutions. The textile sewage sludge activated carbon (TSSAC) was prepared by chemical activation with potassium hydroxide using Response Surface Methodology (RSM). The most influential factor on each experimental design responses was identified via ANNOVA analysis. Based on the central composite design (CCD), quadratic model was developed to correlate the preparation variables for one response which is the Brunauer-Emmelt-Teller (BET) surface area. RSM based on a three-variable CCD was used to determine the effect of pyrolyzed temperature (400-700 °C), carbonization time (45-180 min) and KOH: weight of TSS (wt%) impregnation ratio (0.5:1-1.5:1) on BET surface area. According to the results, pyrolyzed temperature and impregnation ratio were found as the significant factors for maximizing the BET surface area. The major effect which influences the BET surface area was found as pyrolyzed temperature. Both carbonization time and impregnation ratio of KOH had no significant effect. The optimum conditions for preparing TSSAC, based on response surface and contour plots, were found as follows: pyrolyzed temperature 700 °C, carbonization time of 45 min and chemical impregnation ratio of 0.5. The maximum and optimum BET surface area of TSSAC were found as 336 m(2)/g and 310.62 m(2)/g, respectively. Synozol Blue reactive (RSB) and Setapers Yellow-Brown (P2RFL) industrial textile dyes adsorption capacities were investigated. As expected the TSSAC which has the biggest BET surface area (336 m(2)/g) adsorbed dye best. The maximum (RSB) and (P2RFL) uptake capacities were found as 8.5383 mg/g and 5.4 mg/g, respectively. The results of this study indicated the applicability of TSSAC for removing industrial dyes from aqueous solution. Copyright © 2015 Elsevier Ltd. All rights reserved.

Why Do Elephants Flap Their Ears?

NASA Astrophysics Data System (ADS)

Koffi, Moise; Jiji, Latif; Andreopoulos, Yiannis

2009-11-01

It is estimated that a 4200 kg elephant generates as much as 5.12 kW of heat. How the elephant dissipates its metabolic heat and regulates its body temperature has been investigated during the past seven decades. Findings and conclusions differ sharply. The high rate of metabolic heat coupled with low surface area to volume ratio and the absence of sweat glands eliminate surface convection as the primary mechanism for heat removal. Noting that the elephant ears have high surface area to volume ratio and an extensive vascular network, ear flapping is thought to be the principal thermoregulatory mechanism. A computational and experimental program is carried out to examine flow and heat transfer characteristics. The ear is modeled as a uniformly heated oscillating rectangular plate. Our computational work involves a three-dimensional time dependent CFD code with heat transfer capabilities to obtain predictions of the flow field and surface temperature distributions. This information was used to design an experimental setup with a uniformly heated plate of size 0.2m x 0.3m oscillating at 1.6 cycles per second. Results show that surface temperature increases and reaches a steady periodic oscillation after a period of transient oscillation. The role of the vortices shed off the plate in heat transfer enhancement will be discussed.