Measuring surface topography by scanning electron microscopy. II. Analysis of three estimators of surface roughness in second dimension and third dimension.

PubMed

Bonetto, Rita Dominga; Ladaga, Juan Luis; Ponz, Ezequiel

2006-04-01

Scanning electron microscopy (SEM) is widely used in surface studies and continuous efforts are carried out in the search of estimators of different surface characteristics. By using the variogram, we developed two of these estimators that were used to characterize the surface roughness from the SEM image texture. One of the estimators is related to the crossover between fractal region at low scale and the periodic region at high scale, whereas the other estimator characterizes the periodic region. In this work, a full study of these estimators and the fractal dimension in two dimensions (2D) and three dimensions (3D) was carried out for emery papers. We show that the obtained fractal dimension with only one image is good enough to characterize the roughness surface because its behavior is similar to those obtained with 3D height data. We show also that the estimator that indicates the crossover is related to the minimum cell size in 2D and to the average particle size in 3D. The other estimator has different values for the three studied emery papers in 2D but it does not have a clear meaning, and these values are similar for those studied samples in 3D. Nevertheless, it indicates the formation tendency of compound cells. The fractal dimension values from the variogram and from an area versus step log-log graph were studied with 3D data. Both methods yield different values corresponding to different information from the samples.

Measurement and image processing evaluation of surface modifications of dental implants G4 pure titanium created by different techniques

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bulutsuz, A. G., E-mail: asligunaya@gmail.com; Demircioglu, P., E-mail: pinar.demircioglu@adu.edu.tr; Bogrekci, I., E-mail: ismail.bogrekci@adu.edu.tr

Foreign substances and organic tissue interaction placed into the jaw in order to eliminate tooth loss involves a highly complex process. Many biological reactions take place as well as the biomechanical forces that influence this formation. Osseointegration denotes to the direct structural and functional association between the living bone and the load-bearing artificial implant's surface. Taking into consideration of the requirements in the manufacturing processes of the implants, surface characterizations with high precise measurement techniques are investigated and thus long-term success of dental implant is emphasized on the importance of these processes in this study. In this research, the detailedmore » surface characterization was performed to identify the dependence of the manufacturing techniques on the surface properties by using the image processing methods and using the scanning electron microscope (SEM) for morphological properties in 3D and Taylor Hobson stylus profilometer for roughness properties in 2D. Three implant surfaces fabricated by different manufacturing techniques were inspected, and a machined surface was included into the study as a reference specimen. The results indicated that different surface treatments were strongly influenced surface morphology. Thus 2D and 3D precise inspection techniques were highlighted on the importance for surface characterization. Different image analyses techniques such as Dark-light technique were used to verify the surface measurement results. The computational phase was performed using image processing toolbox in Matlab with precise evaluation of the roughness for the implant surfaces. The relationship between the number of black and white pixels and surface roughness is presented. FFT image processing and analyses results explicitly imply that the technique is useful in the determination of surface roughness. The results showed that the number of black pixels in the image increases with increase in surface roughness.« less

Surface Roughness Optimization Using Taguchi Method of High Speed End Milling For Hardened Steel D2

NASA Astrophysics Data System (ADS)

Hazza Faizi Al-Hazza, Muataz; Ibrahim, Nur Asmawiyah bt; Adesta, Erry T. Y.; Khan, Ahsan Ali; Abdullah Sidek, Atiah Bt.

2017-03-01

The main challenge for any manufacturer is to achieve higher quality of their final products with maintains minimum machining time. In this research final surface roughness analysed and optimized with maximum 0.3 mm flank wear length. The experiment was investigated the effect of cutting speed, feed rate and depth of cut on the final surface roughness using D2 as a work piece hardened to 52-56 HRC, and coated carbide as cutting tool with higher cutting speed 120-240 mm/min. The experiment has been conducted using L9 design of Taguchi collection. The results have been analysed using JMP software.

Full-wave Characterization of Rough Terrain Surface Effects for Forward-looking Radar Applications: A Scattering and Imaging Study from the Electromagnetic Perspective

DTIC Science & Technology

2011-09-01

and Imaging Framework First, the parallelized 3-D FDTD algorithm is applied to simulate composite scattering from targets in a rough ground...solver as pertinent to forward-looking radar sensing , the effects of surface clutter on multistatic target imaging are illustrated with large-scale...Full-wave Characterization of Rough Terrain Surface Effects for Forward-looking Radar Applications: A Scattering and Imaging Study from the

Dust lifting in GEM-Mars using a roughness length map

NASA Astrophysics Data System (ADS)

Daerden, F.; Neary, L.; Whiteway, J. A.; Hébrard, E.

2013-09-01

Lifting of size distributed dust due to surface wind stress and dust devils has been implemented in the GEM-Mars 3D-GCM. It turned out that a detailed surface roughness length map was necessary to bring the simulated dust opacities in accordance with observations.

Sputtering of rough surfaces: a 3D simulation study

NASA Astrophysics Data System (ADS)

von Toussaint, U.; Mutzke, A.; Manhard, A.

2017-12-01

The lifetime of plasma-facing components is critical for future magnetic confinement fusion power plants. A key process limiting the lifetime of the first-wall is sputtering by energetic ions. To provide a consistent modeling of the sputtering process of realistic geometries, the SDTrimSP-code has been extended to enable the processing of analytic as well as measured arbitrary 3D surface morphologies. The code has been applied to study the effect of varying the impact angle of ions on rough surfaces on the sputter yield as well as the influence of the aspect ratio of surface structures on the 2D distribution of the local sputtering yields. Depending on the surface morphologies reductions of the effective sputter yields to less than 25% have been observed in the simulation results.

Experiments on Hypersonic Roughness Induced Transition by Means of Infrared Thermography

NASA Astrophysics Data System (ADS)

Schrijer, F. F. J.; Scarano, F.; van Oudheusden, B. W.; Bannink, W. J.

2005-02-01

Roughness induced boundary layer transition is experimentally investigated in the hypersonic flow regime at M = 9. The primary interest is the possible effect of stepwise geometry imperfections (2D isolated roughness) on (boundary layer) transition which may be caused on the EXPERT vehicle by the difference in thermal expansion due to the different materials used in the vehicle-nose construction. Also 3D isolated and 3D distributed roughness configurations were studied. Quantitative Infra-Red Thermography (QIRT) is used as primary diagnostic technique to measure the surface convective heat transfer and to detect boundary layer laminar-to-turbulent transition. The investigation shows that for a given height of the roughness element, the boundary layer is least sensitive to a step-like disturbance, whereas distributed 3D roughness was found to be effective in triggering transition. The experimental results have been compared to existing hypersonic transition correlations (PANT and Shuttle). Finally a transition criterion is evaluated which is based on the critical roughness height Reynolds number. Usage of this criterion enables a straightforward extrapolation to flight. Key words: hypersonic flow, boundary layer transition.

a Predictive Model of Permeability for Fractal-Based Rough Rock Fractures during Shear

NASA Astrophysics Data System (ADS)

Huang, Na; Jiang, Yujing; Liu, Richeng; Li, Bo; Zhang, Zhenyu

This study investigates the roles of fracture roughness, normal stress and shear displacement on the fluid flow characteristics through three-dimensional (3D) self-affine fractal rock fractures, whose surfaces are generated using the modified successive random additions (SRA) algorithm. A series of numerical shear-flow tests under different normal stresses were conducted on rough rock fractures to calculate the evolutions of fracture aperture and permeability. The results show that the rough surfaces of fractal-based fractures can be described using the scaling parameter Hurst exponent (H), in which H = 3 - Df, where Df is the fractal dimension of 3D single fractures. The joint roughness coefficient (JRC) distribution of fracture profiles follows a Gauss function with a negative linear relationship between H and average JRC. The frequency curves of aperture distributions change from sharp to flat with increasing shear displacement, indicating a more anisotropic and heterogeneous flow pattern. Both the mean aperture and permeability of fracture increase with the increment of surface roughness and decrement of normal stress. At the beginning of shear, the permeability increases remarkably and then gradually becomes steady. A predictive model of permeability using the mean mechanical aperture is proposed and the validity is verified by comparisons with the experimental results reported in literature. The proposed model provides a simple method to approximate permeability of fractal-based rough rock fractures during shear using fracture aperture distribution that can be easily obtained from digitized fracture surface information.

Quantitative evaluation of performance of 3D printed lenses

PubMed Central

Gawedzinski, John; Pawlowski, Michal E.; Tkaczyk, Tomasz S.

2017-01-01

We present an analysis of the shape, surface quality, and imaging capabilities of custom 3D printed lenses. 3D printing technology enables lens prototypes to be fabricated without restrictions on surface geometry. Thus, spherical, aspherical and rotationally non-symmetric lenses can be manufactured in an integrated production process. This technique serves as a noteworthy alternative to multistage, labor-intensive, abrasive processes such as grinding, polishing and diamond turning. Here, we evaluate the quality of lenses fabricated by Luxexcel using patented Printoptical© technology that is based on an inkjet printing technique by comparing them to lenses made with traditional glass processing technologies (grinding, polishing etc.). The surface geometry and roughness of the lenses were evaluated using white-light and Fizeau interferometers. We have compared peak-to-valley wavefront deviation, root-mean-squared wavefront error, radii of curvature and the arithmetic average of the roughness profile (Ra) of plastic and glass lenses. Additionally, the imaging performance of selected pairs of lenses was tested using 1951 USAF resolution target. The results indicate performance of 3D printed optics that could be manufactured with surface roughness comparable to that of injection molded lenses (Ra < 20 nm). The RMS wavefront error of 3D printed prototypes was at a minimum 18.8 times larger than equivalent glass prototypes for a lens with a 12.7 mm clear aperture, but when measured within 63% of its clear aperture, 3D printed components’ RMS wavefront error was comparable to glass lenses. PMID:29238114

Comparison of Predicted and Measured Turbine Vane Rough Surface Heat Transfer

NASA Technical Reports Server (NTRS)

Boyle, R. J.; Spuckler, C. M.; Lucci, B. L.

2000-01-01

The proposed paper compares predicted turbine vane heat transfer for a rough surface over a wide range of test conditions with experimental data. Predictions were made for the entire vane surface. However, measurements were made only over the suction surface of the vane, and the leading edge region of the pressure surface. Comparisons are shown for a wide range of test conditions. Inlet pressures varied between 3 and 15 psia, and exit Mach numbers ranged between 0.3 and 0.9. Thus, while a single roughened vane was used for the tests, the effective rougness,(k(sup +)), varied by more than a factor of ten. Results were obtained for freestream turbulence levels of 1 and 10%. Heat transfer predictions were obtained using the Navier-Stokes computer code RVCQ3D. Two turbulence models, suitable for rough surface analysis, are incorporated in this code. The Cebeci-Chang roughness model is part of the algebraic turbulence model. The k-omega turbulence model accounts for the effect of roughness in the application of the boundary condition. Roughness causes turbulent flow over the vane surface. Even after accounting for transition, surface roughness significantly increased heat transfer compared to a smooth surface. The k-omega results agreed better with the data than the Cebeci-Chang model. However, the low Reynolds number k-omega model did not accurately account for roughness when the freestream turbulence level was low. The high Reynolds number version of this model was more suitable when the freestream turbulence was low.

Effect of ion-implantation on surface characteristics of nickel titanium and titanium molybdenum alloy arch wires.

PubMed

Krishnan, Manu; Saraswathy, Seema; Sukumaran, Kalathil; Abraham, Kurian Mathew

2013-01-01

To evaluate the changes in surface roughness and frictional features of 'ion-implanted nickel titanium (NiTi) and titanium molybdenum alloy (TMA) arch wires' from its conventional types in an in-vitro laboratory set up. 'Ion-implanted NiTi and low friction TMA arch wires' were assessed for surface roughness with scanning electron microscopy (SEM) and 3 dimensional (3D) optical profilometry. Frictional forces were studied in a universal testing machine. Surface roughness of arch wires were determined as Root Mean Square (RMS) values in nanometers and Frictional Forces (FF) in grams. Mean values of RMS and FF were compared by Student's 't' test and one way analysis of variance (ANOVA). SEM images showed a smooth topography for ion-implanted versions. 3D optical profilometry demonstrated reduction of RMS values by 58.43% for ion-implanted NiTi (795.95 to 330.87 nm) and 48.90% for TMA groups (463.28 to 236.35 nm) from controls. Nonetheless, the corresponding decrease in FF was only 29.18% for NiTi and 22.04% for TMA, suggesting partial correction of surface roughness and disproportionate reduction in frictional forces with ion-implantation. Though the reductions were highly significant at P < 0.001, relations between surface roughness and frictional forces remained non conclusive even after ion-implantation. The study proved that ion-implantation can significantly reduce the surface roughness of NiTi and TMA wires but could not make a similar reduction in frictional forces. This can be attributed to the inherent differences in stiffness and surface reactivity of NiTi and TMA wires when used in combination with stainless steel brackets, which needs further investigations.

2D scaling behavior of nanotextured GaN surfaces: A case study of hillocked and terraced surfaces

NASA Astrophysics Data System (ADS)

Mutta, Geeta Rani; Carapezzi, Stefania

2018-07-01

The 2D scaling properties of GaN surfaces have been studied by means of the 2D height-height correlation function (HHCF). The GaN layers under investigation presented exemplar morphologies, generated by distinct growth methods: a molecular beam epitaxy (MBE) grown surface decorated by hillocks and a metal organic vapor phase epitaxy (MOVPE) grown surface with terraced structure. The 2D statistical analysis of these surfaces has allowed assessing quantitatively the degree of morphological variability along all the different directions across each surface, their corresponding roughness exponents and correlation lengths. A scaling anisotropy as well as correlation length anisotropy has been detected for both hillocked and terraced surfaces. Especially, a marked dependence of correlation length from the direction across the terraced surface has been observed. Additionally, the terraced surfaces showed the lower root mean square (RMS) roughness value and at the same time, the lower roughness exponent value. This could appear as a contradiction, given that a low RMS value is associated to a smooth surface, and usually the roughness exponent is interpreted as a "measure" of the smoothness of the surface, the smoother the surface, the higher (approaching the unity) is the roughness exponent. Our case study is an experimental demonstration in which the roughness exponent should be, more appropriately, interpreted as a quantification of how the roughness changes with length scale.

Flow transition with 2-D roughness elements in a 3-D channel

NASA Technical Reports Server (NTRS)

Liu, Zhining; Liu, Chaoquin; Mccormick, Stephen F.

1993-01-01

We develop a new numerical approach to study the spatially evolving instability of the streamwise dominant flow in the presence of roughness elements. The difficulty in handling the flow over the boundary surface with general geometry is removed by using a new conservative form of the governing equations and an analytical mapping. The numerical scheme uses second-order backward Euler in time, fourth-order central differences in all three spatial directions, and boundary-fitted staggered grids. A three-dimensional channel with multiple two-dimensional-type roughness elements is employed as the test case. Fourier analysis is used to decompose different Fourier modes of the disturbance. The results show that surface roughness leads to transition at lower Reynolds number than for smooth channels.

Adsorption of silica colloids onto like-charged silica surfaces of different roughness

DOE PAGES

Dylla-Spears, R.; Wong, L.; Shen, N.; ...

2017-01-17

Particle adsorption was explored in a model optical polishing system, consisting of silica colloids and like-charged silica surfaces. The adsorption was monitored in situ under various suspension conditions, in the absence of surfactants or organic modifiers, using a quartz crystal microbalance with dissipation monitoring (QCM-D). Changes in surface coverage with particle concentration, particle size, pH, ionic strength and ionic composition were quantified by QCM-D and further characterized ex situ by atomic force microscopy (AFM). A Monte Carlo model was used to describe the kinetics of particle deposition and provide insights on scaling with particle concentration. Transitions from near-zero adsorption tomore » measurable adsorption were compared with equilibrium predictions made using the Deraguin-Verwey-Landau-Overbeek (DLVO) theory. In addition, the impact of silica surface roughness on the propensity for particle adsorption was studied on various spatial scale lengths by intentionally roughening the QCM sensor surface using polishing methods. It was found that a change in silica surface roughness at the AFM scale from 1.3 nm root-mean-square (rms) to 2.7 nm rms resulted in an increase in silica particle adsorption of 3-fold for 50-nm diameter particles and 1.3-fold for 100-nm diameter particles—far exceeding adsorption observed by altering suspension conditions alone, potentially because roughness at the proper scale reduces the total separation distance between particle and surface.« less

Surface roughness analysis after laser assisted machining of hard to cut materials

NASA Astrophysics Data System (ADS)

Przestacki, D.; Jankowiak, M.

2014-03-01

Metal matrix composites and Si3N4 ceramics are very attractive materials for various industry applications due to extremely high hardness and abrasive wear resistance. However because of these features they are problematic for the conventional turning process. The machining on a classic lathe still requires special polycrystalline diamond (PCD) or cubic boron nitride (CBN) cutting inserts which are very expensive. In the paper an experimental surface roughness analysis of laser assisted machining (LAM) for two tapes of hard-to-cut materials was presented. In LAM, the surface of work piece is heated directly by a laser beam in order to facilitate, the decohesion of material. Surface analysis concentrates on the influence of laser assisted machining on the surface quality of the silicon nitride ceramic Si3N4 and metal matrix composite (MMC). The effect of the laser assisted machining was compared to the conventional machining. The machining parameters influence on surface roughness parameters was also investigated. The 3D surface topographies were measured using optical surface profiler. The analysis of power spectrum density (PSD) roughness profile were analyzed.

A Rough Energy Landscape to Describe Surface-Linked Antibody and Antigen Bond Formation

NASA Astrophysics Data System (ADS)

Limozin, Laurent; Bongrand, Pierre; Robert, Philippe

2016-10-01

Antibodies and B cell receptors often bind their antigen at cell-cell interface while both molecular species are surface-bound, which impacts bond kinetics and function. Despite the description of complex energy landscapes for dissociation kinetics which may also result in significantly different association kinetics, surface-bound molecule (2D) association kinetics usually remain described by an on-rate due to crossing of a single free energy barrier, and few experimental works have measured association kinetics under conditions implying force and two-dimensional relative ligand-receptor motion. We use a new laminar flow chamber to measure 2D bond formation with systematic variation of the distribution of encounter durations between antigen and antibody, in a range from 0.1 to 10 ms. Under physiologically relevant forces, 2D association is 100-fold slower than 3D association as studied by surface plasmon resonance assays. Supported by brownian dynamics simulations, our results show that a minimal encounter duration is required for 2D association; an energy landscape featuring a rough initial part might be a reasonable way of accounting for this. By systematically varying the temperature of our experiments, we evaluate roughness at 2kBT, in the range of previously proposed rough parts of landscapes models during dissociation.

A Rough Energy Landscape to Describe Surface-Linked Antibody and Antigen Bond Formation

PubMed Central

Limozin, Laurent; Bongrand, Pierre; Robert, Philippe

2016-01-01

Antibodies and B cell receptors often bind their antigen at cell-cell interface while both molecular species are surface-bound, which impacts bond kinetics and function. Despite the description of complex energy landscapes for dissociation kinetics which may also result in significantly different association kinetics, surface-bound molecule (2D) association kinetics usually remain described by an on-rate due to crossing of a single free energy barrier, and few experimental works have measured association kinetics under conditions implying force and two-dimensional relative ligand-receptor motion. We use a new laminar flow chamber to measure 2D bond formation with systematic variation of the distribution of encounter durations between antigen and antibody, in a range from 0.1 to 10 ms. Under physiologically relevant forces, 2D association is 100-fold slower than 3D association as studied by surface plasmon resonance assays. Supported by brownian dynamics simulations, our results show that a minimal encounter duration is required for 2D association; an energy landscape featuring a rough initial part might be a reasonable way of accounting for this. By systematically varying the temperature of our experiments, we evaluate roughness at 2kBT, in the range of previously proposed rough parts of landscapes models during dissociation. PMID:27731375

A Rough Energy Landscape to Describe Surface-Linked Antibody and Antigen Bond Formation.

PubMed

Limozin, Laurent; Bongrand, Pierre; Robert, Philippe

2016-10-12

Antibodies and B cell receptors often bind their antigen at cell-cell interface while both molecular species are surface-bound, which impacts bond kinetics and function. Despite the description of complex energy landscapes for dissociation kinetics which may also result in significantly different association kinetics, surface-bound molecule (2D) association kinetics usually remain described by an on-rate due to crossing of a single free energy barrier, and few experimental works have measured association kinetics under conditions implying force and two-dimensional relative ligand-receptor motion. We use a new laminar flow chamber to measure 2D bond formation with systematic variation of the distribution of encounter durations between antigen and antibody, in a range from 0.1 to 10 ms. Under physiologically relevant forces, 2D association is 100-fold slower than 3D association as studied by surface plasmon resonance assays. Supported by brownian dynamics simulations, our results show that a minimal encounter duration is required for 2D association; an energy landscape featuring a rough initial part might be a reasonable way of accounting for this. By systematically varying the temperature of our experiments, we evaluate roughness at 2k B T, in the range of previously proposed rough parts of landscapes models during dissociation.

Quantitative evaluation of performance of three-dimensional printed lenses

NASA Astrophysics Data System (ADS)

Gawedzinski, John; Pawlowski, Michal E.; Tkaczyk, Tomasz S.

2017-08-01

We present an analysis of the shape, surface quality, and imaging capabilities of custom three-dimensional (3-D) printed lenses. 3-D printing technology enables lens prototypes to be fabricated without restrictions on surface geometry. Thus, spherical, aspherical, and rotationally nonsymmetric lenses can be manufactured in an integrated production process. This technique serves as a noteworthy alternative to multistage, labor-intensive, abrasive processes, such as grinding, polishing, and diamond turning. Here, we evaluate the quality of lenses fabricated by Luxexcel using patented Printoptical©; technology that is based on an inkjet printing technique by comparing them to lenses made with traditional glass processing technologies (grinding, polishing, etc.). The surface geometry and roughness of the lenses were evaluated using white-light and Fizeau interferometers. We have compared peak-to-valley wavefront deviation, root mean square (RMS) wavefront error, radii of curvature, and the arithmetic roughness average (Ra) profile of plastic and glass lenses. In addition, the imaging performance of selected pairs of lenses was tested using 1951 USAF resolution target. The results indicate performance of 3-D printed optics that could be manufactured with surface roughness comparable to that of injection molded lenses (Ra<20 nm). The RMS wavefront error of 3-D printed prototypes was at a minimum 18.8 times larger than equivalent glass prototypes for a lens with a 12.7 mm clear aperture, but, when measured within 63% of its clear aperture, the 3-D printed components' RMS wavefront error was comparable to glass lenses.

Diversity of dermal denticle structure in sharks: Skin surface roughness and three-dimensional morphology.

PubMed

Ankhelyi, Madeleine V; Wainwright, Dylan K; Lauder, George V

2018-05-29

Shark skin is covered with numerous placoid scales or dermal denticles. While previous research has used scanning electron microscopy and histology to demonstrate that denticles vary both around the body of a shark and among species, no previous study has quantified three-dimensional (3D) denticle structure and surface roughness to provide a quantitative analysis of skin surface texture. We quantified differences in denticle shape and size on the skin of three individual smooth dogfish sharks (Mustelus canis) using micro-CT scanning, gel-based surface profilometry, and histology. On each smooth dogfish, we imaged between 8 and 20 distinct areas on the body and fins, and obtained further comparative skin surface data from leopard, Atlantic sharpnose, shortfin mako, spiny dogfish, gulper, angel, and white sharks. We generated 3D images of individual denticles and measured denticle volume, surface area, and crown angle from the micro-CT scans. Surface profilometry was used to quantify metrology variables such as roughness, skew, kurtosis, and the height and spacing of surface features. These measurements confirmed that denticles on different body areas of smooth dogfish varied widely in size, shape, and spacing. Denticles near the snout are smooth, paver-like, and large relative to denticles on the body. Body denticles on smooth dogfish generally have between one and three distinct ridges, a diamond-like surface shape, and a dorsoventral gradient in spacing and roughness. Ridges were spaced on average 56 µm apart, and had a mean height of 6.5 µm, comparable to denticles from shortfin mako sharks, and with narrower spacing and lower heights than other species measured. We observed considerable variation in denticle structure among regions on the pectoral, dorsal, and caudal fins, including a leading-to-trailing edge gradient in roughness for each region. Surface roughness in smooth dogfish varied around the body from 3 to 42 microns. © 2018 Wiley Periodicals, Inc.

Multigrid methods for flow transition in three-dimensional boundary layers with surface roughness

NASA Technical Reports Server (NTRS)

Liu, Chaoqun; Liu, Zhining; Mccormick, Steve

1993-01-01

The efficient multilevel adaptive method has been successfully applied to perform direct numerical simulations (DNS) of flow transition in 3-D channels and 3-D boundary layers with 2-D and 3-D isolated and distributed roughness in a curvilinear coordinate system. A fourth-order finite difference technique on stretched and staggered grids, a fully-implicit time marching scheme, a semi-coarsening multigrid method associated with line distributive relaxation scheme, and an improved outflow boundary-condition treatment, which needs only a very short buffer domain to damp all order-one wave reflections, are developed. These approaches make the multigrid DNS code very accurate and efficient. This allows us not only to be able to do spatial DNS for the 3-D channel and flat plate at low computational costs, but also to do spatial DNS for transition in the 3-D boundary layer with 3-D single and multiple roughness elements, which would have extremely high computational costs with conventional methods. Numerical results show good agreement with the linear stability theory, the secondary instability theory, and a number of laboratory experiments. The contribution of isolated and distributed roughness to transition is analyzed.

Critical surface roughness for wall bounded flow of viscous fluids in an electric submersible pump

NASA Astrophysics Data System (ADS)

Deshmukh, Dhairyasheel; Siddique, Md Hamid; Kenyery, Frank; Samad, Abdus

2017-11-01

Surface roughness plays a vital role in the performance of an electric submersible pump (ESP). A 3-D numerical analysis has been carried out to find the roughness effect on ESP. The performance of pump for steady wall bounded turbulent flows is evaluated at different roughness values and compared with smooth surface considering a non-dimensional roughness factor K. The k- ω SST turbulence model with fine mesh at near wall region captures the rough wall effects accurately. Computational results are validated with experimental results of water (1 cP), at a design speed (3000 RPM). Maximum head is observed for a hydraulically smooth surface (K=0). When roughness factor is increased, the head decreases till critical roughness factor (K=0.1) due to frictional loss. Further increase in roughness factor (K>0.1) increases the head due to near wall turbulence. The performance of ESP is analyzed for turbulent kinetic energy and eddy viscosity at different roughness values. The wall disturbance over the rough surface affects the pressure distribution and velocity field. The roughness effect is predominant for high viscosity oil (43cP) as compared to water. Moreover, the study at off-design conditions showed that Reynolds number influences the overall roughness effect.

Combined Effect of Surface Roughness and Wake Splitter Plate on the Aerodynamic Characteristics of a Circular Cylinder

NASA Astrophysics Data System (ADS)

Saisanthosh, Iyer; Arunkumar, K.; Ajithkumar, R.; Srikrishnan, A. R.

2017-09-01

This paper is focussed on numerical investigation of flow around a stationary circular cylinder (diameter, D) with selectively applied surface roughness (roughness strips with thickness ‘k’) in the presence of a wake splitter plate (length, L). The plate leading edge is at a distance of ‘G’ from the cylinder base. For this study, the commercial software ANSYS Fluent is used. Fluid considered is water. Study was conducted the following cases (a) plain cylinder (b) cylinder with surface roughness (without splitter plate) (c) Cylinder with splitter plate (without surface roughness) and (d) cylinder with both roughness and splitter plate employed. The study Reynolds number (based on D) is 17,000 and k/δ = 1.25 (in all cases). Results indicate that, for cylinder with splitter plate (no roughness), lift coefficient gradually drops till G/D=1.5 further to which it sharply increases. Whereas, drag coefficient and Strouhal number undergoes slight reduction till G/D=1.0 and thereafter, gradually increase. Circumferential location of strip (α) does not influence the aerodynamic parameters significantly. With roughness alone, drag is magnified by about 1.5 times and lift, by about 2.7 times that of the respective values of the smooth cylinder. With splitter plate, for roughness applied at all ‘α’ values, drag and lift undergoes substantial reduction with the lowest value attained at G/D=1.0.

Relating surface roughness and magnetic domain structure to giant magneto-impedance of Co-rich melt-extracted microwires

DOE PAGES

Jiang, S. D.; Eggers, T.; Thiabgoh, O.; ...

2017-04-11

Understanding the relationship between the surface conditions and giant magneto-impedance (GMI) in Co-rich melt-extracted microwires is key to optimizing their magnetic responses for magnetic sensor applications. The surface magnetic domain structure (SMDS) parameters of ~45 μm diameter Co 69.25Fe 4.25Si 13B 13.5-xZr x (x = 0, 1, 2, 3) microwires, including the magnetic domain period (d) and surface roughness (Rq) as extracted from the magnetic force microscopy (MFM) images, have been correlated with GMI in the range 1–1000 MHz. It was found that substitution of B with 1 at. % Zr increased d of the base alloy from 729 tomore » 740 nm while retaining Rq from ~1 nm to ~3 nm. A tremendous impact on the GMI ratio was found, increasing the ratio from ~360% to ~490% at an operating frequency of 40 MHz. Further substitution with Zr decreased the high frequency GMI ratio, which can be understood by the significant increase in surface roughness evident by force microscopy. Lastly, this study demonstrates the application of the domain period and surface roughness found by force microscopy to the interpretation of the GMI in Co-rich microwires.« less

Simulation of RBS spectra with known 3D sample surface roughness

NASA Astrophysics Data System (ADS)

Malinský, Petr; Siegel, Jakub; Hnatowicz, Vladimir; Macková, Anna; Švorčík, Václav

2017-09-01

The Rutherford Backscattering Spectrometry (RBS) is a technique for elemental depth profiling with a nanometer depth resolution. Possible surface roughness of analysed samples can deteriorate the RBS spectra and makes their interpretation more difficult and ambiguous. This work describes the simulation of RBS spectra which takes into account real 3D morphology of the sample surface obtained by AFM method. The RBS spectrum is calculated as a sum of the many particular spectra obtained for randomly chosen particle trajectories over sample 3D landscape. The spectra, simulated for different ion beam incidence angles, are compared to the experimental ones measured with 2.0 MeV 4He+ ions. The main aim of this work is to obtain more definite information on how a particular surface morphology and measuring geometry affects the RBS spectra and derived elemental depth profiles. A reasonable agreement between the measured and simulated spectra was found and the results indicate that the AFM data on the sample surface can be used for the simulation of RBS spectra.

Virtual rough samples to test 3D nanometer-scale scanning electron microscopy stereo photogrammetry.

PubMed

Villarrubia, J S; Tondare, V N; Vladár, A E

2016-01-01

The combination of scanning electron microscopy for high spatial resolution, images from multiple angles to provide 3D information, and commercially available stereo photogrammetry software for 3D reconstruction offers promise for nanometer-scale dimensional metrology in 3D. A method is described to test 3D photogrammetry software by the use of virtual samples-mathematical samples from which simulated images are made for use as inputs to the software under test. The virtual sample is constructed by wrapping a rough skin with any desired power spectral density around a smooth near-trapezoidal line with rounded top corners. Reconstruction is performed with images simulated from different angular viewpoints. The software's reconstructed 3D model is then compared to the known geometry of the virtual sample. Three commercial photogrammetry software packages were tested. Two of them produced results for line height and width that were within close to 1 nm of the correct values. All of the packages exhibited some difficulty in reconstructing details of the surface roughness.

Influence of Surface Roughness on the Second Order Transport of Turbulence in Non-Equilibrium Boundary Layers

DTIC Science & Technology

2006-10-08

FINAL REPORT to Air Force Office of Scientific Research (AFOSR) Project Title Influence of Surface Roughness on the Second Order Transport of...large amount of research has been performed to quantify the effects of Mach number, roughness, and wall curvature on turbulent boundary layers. However...18 a) b) c) Figure 3: a) A. D. Smith high pressure storage tank. b) Morin B series actuator controlling Virgo Engineers Trunion Mounted Ball Valve. c

Smooth polishing of femtosecond laser induced craters on cemented carbide by ultrasonic vibration method

NASA Astrophysics Data System (ADS)

Wang, H. P.; Guan, Y. C.; Zheng, H. Y.

2017-12-01

Rough surface features induced by laser irradiation have been a challenging for the fabrication of micro/nano scale features. In this work, we propose hybrid ultrasonic vibration polishing method to improve surface quality of microcraters produced by femtosecond laser irradiation on cemented carbide. The laser caused rough surfaces are significantly smoothened after ultrasonic vibration polishing due to the strong collision effect of diamond particles on the surfaces. 3D morphology, SEM and AFM analysis has been conducted to characterize surface morphology and topography. Results indicate that the minimal surface roughness of Ra 7.60 nm has been achieved on the polished surfaces. The fabrication of microcraters with smooth surfaces is applicable to molding process for mass production of micro-optical components.

Roughness based perceptual analysis towards digital skin imaging system with haptic feedback.

PubMed

Kim, K

2016-08-01

To examine psoriasis or atopic eczema, analyzing skin roughness by palpation is essential to precisely diagnose skin diseases. However, optical sensor based skin imaging systems do not allow dermatologists to touch skin images. To solve the problem, a new haptic rendering technology that can accurately display skin roughness must be developed. In addition, the rendering algorithm must be able to filter spatial noises created during 2D to 3D image conversion without losing the original roughness on the skin image. In this study, a perceptual way to design a noise filter that will remove spatial noises and in the meantime recover maximized roughness is introduced by understanding human sensitivity on surface roughness. A visuohaptic rendering system that can provide a user with seeing and touching digital skin surface roughness has been developed including a geometric roughness estimation method from a meshed surface. In following, a psychophysical experiment was designed and conducted with 12 human subjects to measure human perception with the developed visual and haptic interfaces to examine surface roughness. From the psychophysical experiment, it was found that touch is more sensitive at lower surface roughness, and vice versa. Human perception with both senses, vision and touch, becomes less sensitive to surface distortions as roughness increases. When interact with both channels, visual and haptic interfaces, the performance to detect abnormalities on roughness is greatly improved by sensory integration with the developed visuohaptic rendering system. The result can be used as a guideline to design a noise filter that can perceptually remove spatial noises while recover maximized roughness values from a digital skin image obtained by optical sensors. In addition, the result also confirms that the developed visuohaptic rendering system can help dermatologists or skin care professionals examine skin conditions by using vision and touch at the same time. © 2015 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

Electromagnetic Scattering by an Exponentially Distributed Rough Surface with the Introduction of a Rough Surface Generation Technique

DTIC Science & Technology

1987-12-01

d integer corrow, corcol , refrow, refcol C Create lower triangle of corr. matrix (symetric matrix) do 33 i~l,n2 C calculate the row point (i) is in...reference Fig.(21)) corrow = (((i-l)/n)+1) C claculate the column point (i) is in corcol = i-(corrow-l)*n) write(6,*) i do 31 jl,i C calculate the row...refrow)*space C the horizontal distance (b) b = ( corcol -refcol)*space 14 d = sqrt(a**2+b**2) S coeff(i,j) = e%-P(-d**2) 31 ]i<ontiinue .3 crnt inue

Optimization of Machining Process Parameters for Surface Roughness of Al-Composites

NASA Astrophysics Data System (ADS)

Sharma, S.

2013-10-01

Metal matrix composites (MMCs) have become a leading material among the various types of composite materials for different applications due to their excellent engineering properties. Among the various types of composites materials, aluminum MMCs have received considerable attention in automobile and aerospace applications. These materials are known as the difficult-to-machine materials because of the hardness and abrasive nature of reinforcement element-like silicon carbide particles. In the present investigation Al-SiC composite was produced by stir casting process. The Brinell hardness of the alloy after SiC addition had increased from 74 ± 2 to 95 ± 5 respectively. The composite was machined using CNC turning center under different machining parameters such as cutting speed (S), feed rate (F), depth of cut (D) and nose radius (R). The effect of machining parameters on surface roughness (Ra) was studied using response surface methodology. Face centered composite design with three levels of each factor was used for surface roughness study of the developed composite. A response surface model for surface roughness was developed in terms of main factors (S, F, D and R) and their significant interactions (SD, SR, FD and FR). The developed model was validated by conducting experiments under different conditions. Further the model was optimized for minimum surface roughness. An error of 3-7 % was observed in the modeled and experimental results. Further, it was fond that the surface roughness of Al-alloy at optimum conditions is lower than that of Al-SiC composite.

Effect of sound on boundary layer stability

NASA Technical Reports Server (NTRS)

Saric, William S. (Principal Investigator); Spencer, Shelly Anne

1993-01-01

Experiments are conducted in the Arizona State University Unsteady Wind Tunnel with a zero-pressure-gradient flat-plate model that has a 67:1 elliptical leading edge. Boundary-layer measurements are made of the streamwise fluctuating-velocity component in order to identify the amplified T-S waves that are forced by downstream-travelling, sound waves. Measurements are taken with circular 3-D roughness elements placed at the Branch 1 neutral stability point for the frequency under consideration, and then with the roughness element downstream of Branch 1. These roughness elements have a principal chord dimension equal to 2(lambda)(sub TS)/pi, of the T-S waves under study and are 'stacked' in order to resemble a Gaussian height distribution. Measurements taken just downstream of the roughness (with leading-edge T-S waves, surface roughness T-S waves, instrumentation sting vibrations and the Stokes wave subtracted) show the generation of 3-D-T-S waves, but not in the characteristic heart-shaped disturbance field predicted by 3-D asymptotic theory. Maximum disturbance amplitudes are found on the roughness centerline. However, some near-field characteristics predicted by numerical modelling are observed.

Effect of sound on boundary layer stability

NASA Technical Reports Server (NTRS)

Saric, William S.; Spencer, Shelly Anne

1993-01-01

Experiments are conducted in the Arizona State University Unsteady Wind Tunnel with a zero-pressure-gradient flat-plate model that has a 67:1 elliptical leading edge. Boundary-layer measurements are made of the streamwise fluctuating-velocity component in order to identify the amplified T-S waves that are forced by downstream-traveling sound waves. Measurements are taken with circular 3-D roughness elements placed at the Branch 1 neutral stability point for the frequency under consideration, and then with the roughness element downstream of Branch 1. These roughness elements have a principal chord dimension equal to 2 lambda(sub TS)/pi of the T-S waves under study and are 'stacked' in order to resemble a Gaussian height distribution. Measurements taken just downstream of the roughness (with leading-edge T-S waves, surface roughness T-S waves, instrumentation sting vibrations, and the Stokes wave subtracted) show the generation of 3-D T-S waves, but not in the characteristic heart-shaped disturbance field predicted by 3-D asymptotic theory. Maximum disturbance amplitudes are found on the roughness centerline. However, some near-field characteristics predicted by numerical modeling are observed.

Preparation of poly(L-lactic acid) nanofiber scaffolds with a rough surface by phase inversion using supercritical carbon dioxide.

PubMed

Yang, Ding-Zhu; Chen, Ai-Zheng; Wang, Shi-Bin; Li, Yi; Tang, Xiao-Lin; Wu, Yong-Jing

2015-06-24

Phase inversion using supercritical carbon dioxide (SC-CO2) has been widely used in the development of tissue engineering scaffolds, and particular attention has been given to obtaining desired morphology without additional post-treatments. However, the main challenge of this technique is the difficulty in generating a three-dimensional (3D) nanofiber structure with a rough surface in one step. Here, a poly(L-lactic acid) (PLLA) 3D nanofiber scaffold with a rough surface is obtained via phase inversion using SC-CO2 by carefully choosing fabrication conditions and porogens. It is found that this method can effectively modulate the structure morphology, promote the crystallization process of semicrystalline polymer, and induce the formation of rough structures on the surface of nanofibers. Meanwhile, the porogen of ammonium bicarbonate (AB) can produce a 3D structure with large pores, and porogen of menthol can improve the interconnectivity between the micropores of nanofibers. A significant increase in the fiber diameter is observed as the menthol content increases. Furthermore, the menthol may affect the mutual transition between the α' and α crystals of PLLA during the phase separation process. In addition, the results of protein adsorption, cell adhesion, and proliferation assays indicate that cells tend to have higher viability on the nanofiber scaffold. This process combines the characteristic properties of SC-CO2 and the solubility of menthol to tailor the morphology of polymeric scaffolds, which may have potential applications in tissue engineering.

A Synthesis and Comparison of Approaches for Quantifying Coral Reef Structure

NASA Astrophysics Data System (ADS)

Duvall, M. S.; Hench, J. L.

2016-02-01

The complex physical structures of coral reefs provide substrate for benthic organisms, surface area for material fluxes, and have been used as a predictor of reef-fish biomass and biodiversity. Coral reef topography has a first order effect on reef hydrodynamics by imposing drag forces and increasing momentum and scalar dispersion. Despite its importance, quantifying reef topography remains a challenge, as it is patchy and discontinuous while also varying over orders of magnitude in spatial scale. Previous studies have quantified reef structure using a range of 1D and 2D metrics that estimate vertical roughness, which is the departure from a flat geometric profile or surface. However, there is no general mathematical or conceptual framework by which to apply or compare these roughness metrics. While the specific calculations of different metrics vary, we propose that they can be classified into four categories based on: 1) vertical relief relative to a reference height; 2) gradients in vertical relief; 3) surface contour distance; or 4) variations in roughness with scale. We apply metrics from these four classes to idealized reef topography as well as natural reef topography data from Moorea, French Polynesia. Through the use of idealized profiles, we demonstrate the potential for reefs with different morphologies to possess the same value for some scale-dependent metrics (i.e. classes 1-3). Due to the superposition of variable-scale roughness elements in reef topography, we find that multi-scale metrics (i.e. class 4) can better characterize structural complexity by capturing surface roughness across a range of spatial scales. In particular, we provide evidence of the ability of 1D continuous wavelet transforms to detect changes in dominant roughness scales on idealized topography as well as within real reef systems.

New horizons in selective laser sintering surface roughness characterization

NASA Astrophysics Data System (ADS)

Vetterli, M.; Schmid, M.; Knapp, W.; Wegener, K.

2017-12-01

Powder-based additive manufacturing of polymers and metals has evolved from a prototyping technology to an industrial process for the fabrication of small to medium series of complex geometry parts. Unfortunately due to the processing of powder as a basis material and the successive addition of layers to produce components, a significant surface roughness inherent to the process has been observed since the first use of such technologies. A novel characterization method based on an elastomeric pad coated with a reflective layer, the Gelsight, was found to be reliable and fast to characterize surfaces processed by selective laser sintering (SLS) of polymers. With help of this method, a qualitative and quantitative investigation of SLS surfaces is feasible. Repeatability and reproducibility investigations are performed for both 2D and 3D areal roughness parameters. Based on the good results, the Gelsight is used for the optimization of vertical SLS surfaces. A model built on laser scanning parameters is proposed and after confirmation could achieve a roughness reduction of 10% based on the S q parameter. The Gelsight could be successfully identified as a fast, reliable and versatile surface topography characterization method as it applies to all kind of surfaces.

Acoustic Receptivity of a Blasius Boundary Layer with 2-D and Oblique Surface Waviness

NASA Technical Reports Server (NTRS)

King, Rudolph A.; Breuer, Kenneth S.

2000-01-01

An experimental investigation was conducted to examine acoustic receptivity and subsequent boundary-layer instability evolution for a Blasius boundary layer formed on a flat plate in the presence of two-dimensional (2-D) and oblique (3-D) surface waviness. The effect of the non-localized surface roughness geometry and acoustic wave amplitude on the receptivity process was explored. The surface roughness had a well defined wavenumber spectrum with fundamental wavenumber k (sub w). A planar downstream traveling acoustic wave was created to temporally excite the flow near the resonance frequency of an unstable eigenmode corresponding to k (sub ts) = k (sub w). The range of acoustic forcing levels, epsilon, and roughness heights, DELTA h, examined resulted in a linear dependence of receptivity coefficients; however, the larger values of the forcing combination epsilon dot DELTA h resulted in subsequent nonlinear development of the Tollmien-Schlichting (T-S) wave. This study provided the first experimental evidence of a marked increase in the receptivity coefficient with increasing obliqueness of the surface waviness in excellent agreement with theory. Detuning of the 2-D and oblique disturbances was investigated by varying the streamwise wall-roughness wavenumber a,, and measuring the T-S response. For the configuration where laminar-to-turbulent breakdown occurred, the breakdown process was found to be dominated by energy at the fundamental and harmonic frequencies, indicative of K-type breakdown.

Laser-Sintered Constructs with Bio-inspired Porosity and Surface Micro/Nano-Roughness Enhance Mesenchymal Stem Cell Differentiation and Matrix Mineralization In Vitro.

PubMed

Cheng, Alice; Cohen, David J; Boyan, Barbara D; Schwartz, Zvi

2016-12-01

Direct metal laser sintering can produce porous Ti-6Al-4V orthopedic and dental implants. The process requires reduced resources and time and can provide greater structural control than machine manufacturing. Implants in bone are colonized by mesenchymal stem cells (MSCs), which can differentiate into osteoblasts and contribute to osseointegration. This study examined osteoblast differentiation and matrix mineralization of human MSCs cultured on laser-sintered Ti-6Al-4V constructs with varying porosity and at different time scales. 2D solid disks and low, medium and high porosity (LP, MP, and HP) 3D constructs based on a human trabecular bone template were laser sintered from Ti-6Al-4V powder and further processed to have micro- and nanoscale roughness. hMSCs exhibited greater osteoblastic differentiation and local factor production on all 3D porous constructs compared to 2D surfaces, which was sustained for 9 days without use of exogenous factors. hMSCs cultured for 8 weeks on MP constructs in osteogenic medium (OM), OM supplemented with BMP2 or collagen-coated MP constructs in OM exhibited bone-like extracellular matrix mineralization. Use of bio-inspired porosity for the 3D architecture of additively manufactured Ti-6Al-4V enhanced osteogenic differentiation of hMSCs beyond surface roughness alone. This study suggests that a 3D architecture may enhance the osseointegration of orthopedic and dental implants in vivo.

In vitro study of 3D PLGA/n-HAp/β-TCP composite scaffolds with etched oxygen plasma surface modification in bone tissue engineering

NASA Astrophysics Data System (ADS)

Roh, Hee-Sang; Jung, Sang-Chul; Kook, Min-Suk; Kim, Byung-Hoon

2016-12-01

Three-dimensional (3D) scaffolds have many advantageous properties for bone tissue engineering application, due to its controllable properties such as pore size, structural shape and interconnectivity. In this study, effects on oxygen plasma surface modification and adding of nano-hydroxyapatite (n-HAp) and β-tricalcium phosphate (β-TCP) on the 3D PLGA/n-HAp/β-TCP scaffolds for improving preosteoblast cell (MC3T3-E1) adhesion, proliferation and differentiation were investigated. The 3D PLGA/n-HAp/β-TCP scaffolds were fabricated by 3D Bio-Extruder equipment. The 3D scaffolds were prepared with 0°/90° architecture and pore size of approximately 300 μm. In addition 3D scaffolds surface were etched by oxygen plasma to enhance the hydrophilic property and surface roughness. After oxygen plasma treatment, the surface chemistry and morphology were investigated by Fourier transform infrared spectroscopy, scanning electron microscopy, and atomic force microscopy. And also hydrophilic property was measured by contact angle. The MC3T3-E1 cell proliferation and differentiation were investigated by MTT assay and ALP activity. In present work, the 3D PLGA/HAp/beta-TCP composite scaffold with suitable structure for the growth of osteoblast cells was successfully fabricated by 3D rapid prototyping technique. The surface hydrophilicity and roughness of 3D scaffold increased by oxygen plasma treatment had a positive effect on cell adhesion, proliferation, and differentiation. Furthermore, the differentiation of MC3T3-E1 cell was significantly enhanced by adding of n-HAp and β-TCP on 3D PLGA scaffold. As a result, combination of bioceramics and oxygen plasma treatment showed a synergistic effect on biocompatibility of 3D scaffolds. This result confirms that this technique was useful tool for improving the biocompatibility in bone tissue engineering application.

Influence of surface roughness on cetyltrimethylammonium bromide adsorption from aqueous solution.

PubMed

Wu, Shuqing; Shi, Liu; Garfield, Lucas B; Tabor, Rico F; Striolo, Alberto; Grady, Brian P

2011-05-17

The influence of surface roughness on surfactant adsorption was studied using a quartz crystal microbalance with dissipation (QCM-D). The sensors employed had root-mean-square (R) roughness values of 2.3, 3.1, and 5.8 nm, corresponding to fractal-calculated surface area ratios (actual/nominal) of 1.13, 1.73, and 2.53, respectively. Adsorption isotherms measured at 25 °C showed that adsorbed mass of cetyltrimethylammonium bromide per unit of actual surface area below 0.8 cmc, or above 1.2 cmc, decreases as the surface roughness increases. At the cmc, both the measured adsorbed amount and the measured dissipation increased dramatically on the rougher surfaces. These results are consistent with the presence of impurities, suggesting that roughness exacerbates well-known phenomena reported in the literature of peak impurity-related adsorption at the cmc. The magnitude of the increase, especially in dissipation, suggests that changes in adsorbed amount may not be the only reason for the observed results, as aggregates at the cmc on rougher surfaces are more flexible and likely contain larger amounts of solvent. Differences in adsorption kinetics were also found as a function of surface roughness, with data showing a second, slower adsorption rate after rapid initial adsorption. A two-rate Langmuir model was used to further examine this effect. Although adsorption completes faster on the smoother surfaces, initial adsorption at zero surface coverage is faster on the rougher surfaces, suggesting the presence of more high-energy sites on the rougher surfaces.

MC3T3-E1 cell response to stainless steel 316L with different surface treatments.

PubMed

Zhang, Hongyu; Han, Jianmin; Sun, Yulong; Huang, Yongling; Zhou, Ming

2015-11-01

In the present study, stainless steel 316L samples with polishing, aluminum oxide blasting, and hydroxyapatite (HA) coating were prepared and characterized through a scanning electron microscope (SEM), optical interferometer (surface roughness, Sq), contact angle, surface composition and phase composition analyses. Osteoblast-like MC3T3-E1 cell adhesion on the samples was investigated by cell morphology using a SEM (4h, 1d, 3d, 7d), and cell proliferation was assessed by MTT method at 1d, 3d, and 7d. In addition, adsorption of bovine serum albumin on the samples was evaluated at 1h. The polished sample was smooth (Sq: 1.8nm), and the blasted and HA coated samples were much rougher (Sq: 3.2μm and 7.8μm). Within 1d of incubation, the HA coated samples showed the best cell morphology (e.g., flattened shape and complete spread), but there was no significant difference after 3d and 7d of incubation for all the samples. The absorbance value for the HA coated samples was the highest after 1d and 3d of incubation, indicating better cell viability. However, it reduced to the lowest value at 7d. Protein adsorption on the HA coated samples was the highest at 1h. The results indicate that rough stainless steel surface improves cell adhesion and morphology, and HA coating contributes to superior cell adhesion, but inhibits cell proliferation. Copyright © 2015. Published by Elsevier B.V.

Benchmarking surface selective vacuum ultraviolet and thermal postprocessing of thermoplastics for ultrasmooth 3-D-printed micro-optics

NASA Astrophysics Data System (ADS)

Kirchner, Robert; Chidambaram, Nachiappan; Schift, Helmut

2018-04-01

State-of-the-art, polymeric, refractive micro-optics simultaneously require an ultrasmooth three-dimensional (3-D) surface and a precise geometry for excellent optical performance with minimal stray light. In earlier work, we have established a surface finishing process for thermoplastic polymer master structures that is only effective on the surface and does not affect the designed optical geometry, thus enabling polishing without touching. Therewith, the high curvature corners of a 50-μm-tall optical diffuser device were maintained while the surface roughness was reduced to about 10-nm root mean square. For this, 3-D master structures were first fabricated by direct write laser-lithography with two-photon polymerization. The master structures were replicated into poly(methyl methacrylate) through a poly(dimethyl siloxane) intermediate replication stamp. Finally, all structures were surface-polished by selective high-energy photon exposure and thermal postprocessing. In this work, we focus on the comparison of the surface smoothening using either postprocessing or dedicated direct writing strategies. For this comparison, strategies for modifying the exposed voxel size and the writing discretization being the primary source of roughness were tested by sweeping the laser exposure dose for two different resist materials and objectives. In conclusion, the postprocessing smoothening resulted in a lower roughness compared to a direct writing strategy-even when 50-nm vertical discretization steps were used-and still enabled 10 times shorter writing times.

Influence of Si wafer thinning processes on (sub)surface defects

NASA Astrophysics Data System (ADS)

Inoue, Fumihiro; Jourdain, Anne; Peng, Lan; Phommahaxay, Alain; De Vos, Joeri; Rebibis, Kenneth June; Miller, Andy; Sleeckx, Erik; Beyne, Eric; Uedono, Akira

2017-05-01

Wafer-to-wafer three-dimensional (3D) integration with minimal Si thickness can produce interacting multiple devices with significantly scaled vertical interconnections. Realizing such a thin 3D structure, however, depends critically on the surface and subsurface of the remaining backside Si after the thinning processes. The Si (sub)surface after mechanical grinding has already been characterized fruitfully for a range of few dozen of μm. Here, we expand the characterization of Si (sub)surface to 5 μm thickness after thinning process on dielectric bonded wafers. The subsurface defects and damage layer were investigated after grinding, chemical mechanical polishing (CMP), wet etching and plasma dry etching. The (sub)surface defects were characterized using transmission microscopy, atomic force microscopy, and positron annihilation spectroscopy. Although grinding provides the fastest removal rate of Si, the surface roughness was not compatible with subsequent processing. Furthermore, mechanical damage such as dislocations and amorphous Si cannot be reduced regardless of Si thickness and thin wafer handling systems. The CMP after grinding showed excellent performance to remove this grinding damage, even though the removal amount is 1 μm. For the case of Si thinning towards 5 μm using grinding and CMP, the (sub)surface is atomic scale of roughness without vacancy. For the case of grinding + dry etch, vacancy defects were detected in subsurface around 0.5-2 μm. The finished surface after wet etch remains in the nm scale in the strain region. By inserting a CMP step in between grinding and dry etch it is possible to significantly reduce not only the roughness, but also the remaining vacancies at the subsurface. The surface of grinding + CMP + dry etching gives an equivalent mono vacancy result as to that of grinding + CMP. This combination of thinning processes allows development of extremely thin 3D integration devices with minimal roughness and vacancy surface.

Direct laser writing of microstructures on optically opaque and reflective surfaces

NASA Astrophysics Data System (ADS)

Rekštytė, S.; Jonavičius, T.; Malinauskas, M.

2014-02-01

Direct laser writing (DLW) based on ultra-localized polymerization is an efficient way to produce three-dimensional (3D) micro/nano-structures for diverse applications in science and industry. It is attractive for its flexibility to materialize CAD models out of wide spectrum of materials on the desired substrates. In case of direct laser lithography, photo-crosslinking can be achieved by tightly focusing ultrashort laser pulses to a photo- or thermo-polymers. Selectively exposing material to laser radiation allows creating fully 3D structures with submicrometer spatial resolution. In this paper we present DLW results of hybrid organic-inorganic material SZ2080 on optically opaque and reflective surfaces, such as silicon and various metals (Cr, Ti, Au). Our studies prove that one can precisely fabricate 2D and 3D structures with lower than 1 μm spatial resolution even on glossy or rough surfaces (surface roughness rms 0.068-0.670 μm) using sample translation velocities of up to 1 mm/s. Using femtosecond high pulse repetition rate laser, sample translation velocity can reach over 1 mm/s ensuring repeatable submicrometer structuring resolution.

Understanding the mechanisms of solid-water reactions through analysis of surface topography.

PubMed

Bandstra, Joel Z; Brantley, Susan L

2015-12-01

The topography of a reactive surface contains information about the reactions that form or modify the surface and, therefore, it should be possible to characterize reactivity using topography parameters such as surface area, roughness, or fractal dimension. As a test of this idea, we consider a two-dimensional (2D) lattice model for crystal dissolution and examine a suite of topography parameters to determine which may be useful for predicting rates and mechanisms of dissolution. The model is based on the assumption that the reactivity of a surface site decreases with the number of nearest neighbors. We show that the steady-state surface topography in our model system is a function of, at most, two variables: the ratio of the rate of loss of sites with two neighbors versus three neighbors (d(2)/d(3)) and the ratio of the rate of loss of sites with one neighbor versus three neighbors (d(1)/d(3)). This means that relative rates can be determined from two parameters characterizing the topography of a surface provided that the two parameters are independent of one another. It also means that absolute rates cannot be determined from measurements of surface topography alone. To identify independent sets of topography parameters, we simulated surfaces from a broad range of d(1)/d(3) and d(2)/d(3) and computed a suite of common topography parameters for each surface. Our results indicate that the fractal dimension D and the average spacing between steps, E[s], can serve to uniquely determine d(1)/d(3) and d(2)/d(3) provided that sufficiently strong correlations exist between the steps. Sufficiently strong correlations exist in our model system when D>1.5 (which corresponds to D>2.5 for real 3D reactive surfaces). When steps are uncorrelated, surface topography becomes independent of step retreat rate and D is equal to 1.5. Under these conditions, measures of surface topography are not independent and any single topography parameter contains all of the available mechanistic information about the surface. Our results also indicate that root-mean-square roughness cannot be used to reliably characterize the surface topography of fractal surfaces because it is an inherently noisy parameter for such surfaces with the scale of the noise being independent of length scale.

Skin friction measurements of mathematically generated roughness in the transitionally- to fully-rough regimes

NASA Astrophysics Data System (ADS)

Barros, Julio; Schultz, Michael; Flack, Karen

2016-11-01

Engineering systems are affected by surface roughness which cause an increase in drag leading to significant performance penalties. One important question is how to predict frictional drag purely based upon surface topography. Although significant progress has been made in recent years, this has proven to be challenging. The present work takes a systematic approach by generating surface roughness in which surfaces parameters, such as rms , skewness, can be controlled. Surfaces were produced using the random Fourier modes method with enforced power-law spectral slopes. The surfaces were manufactured using high resolution 3D-printing. In this study three surfaces with constant amplitude and varying slope, P, were investigated (P = - 0 . 5 , - 1 . 0 , - 1 . 5). Skin-friction measurements were conducted in a high Reynolds number turbulent channel flow facility, covering a wide range of Reynolds numbers, from hydraulic-smooth to fully-rough regimes. Results show that some long wavelength roughness scales do not contribute significantly to the frictional drag, thus highlighting the need for filtering in the calculation of surface statistics. Upon high-pass filtering, it was found that krms is highly correlated with the measured ks.

Tribological Properties of PVD Ti/C-N Nanocoatnigs

NASA Astrophysics Data System (ADS)

Leitans, A.; Lungevics, J.; Rudzitis, J.; Filipovs, A.

2017-04-01

The present paper discusses and analyses tribological properties of various coatings that increase surface wear resistance. Four Ti/C-N nanocoatings with different coating deposition settings are analysed. Tribological and metrological tests on the samples are performed: 2D and 3D parameters of the surface roughness are measured with modern profilometer, and friction coefficient is measured with CSM Instruments equipment. Roughness parameters Ra, Sa, Sz, Str, Sds, Vmp, Vmc and friction coefficient at 6N load are determined during the experiment. The examined samples have many pores, which is the main reason for relatively large values of roughness parameter. A slight wear is identified in all four samples as well; its friction coefficient values range from 0,.21 to 0.29. Wear rate values are not calculated for the investigated coatings, as no expressed tribotracks are detected on the coating surface.

Correlation of bond strength with surface roughness using a new roughness measurement technique.

PubMed

Winkler, M M; Moore, B K

1994-07-01

The correlation between shear bond strength and surface roughness was investigated using new surface measurement methods. Bonding agents and associated resin composites were applied to set amalgam after mechanically roughening its surface. Surface treatments were noe (as set against glass), 80 grit, and 600 grit abrasive paper. Surface roughness (R(a) as measured parallel and perpendicular (+) to the direction of the polishing scratches and true profile length were measured. A knife-edge was applied (rate = 2.54 mm/min) at the bonding agent/amalgam interface of each sample until failure. Coefficients of determination for mean bond strength vs either roughness (R(a), of profile length were significantly higher for measurements in parallel directions than for those measurements in (+) directions. The shear bond strength to set amalgam for a PENTA-containing adhesives system (L.D. Caulk Division) was not significantly different from that of a PENTA-free adhesive (3M Dental Products Division), even though PENTA has been reported to increase bond strength to nonprecious metals. The shear bond strength of resin composite to amalgam is correlated to surface roughness when it is measured parallel to the polishing scratches. This correlation is significantly lower when surface roughness is measured in the typical manner, perpendicular to the polishing scratches.

The research on surface characteristics of optical lens by 3D printing technique and precise diamond turning technique

NASA Astrophysics Data System (ADS)

Huang, Chien-Yao; Chang, Chun-Ming; Ho, Cheng-Fong; Lee, Tai-Wen; Lin, Ping-Hung; Hsu, Wei-Yao

2017-06-01

The advantage of 3D printing technique is flexible in design and fabrication. Using 3D printing technique, the traditional manufacturing limitations are not considered. The optical lens is the key component in an optical system. The traditional process to manufacture optical plastic lens is injection molding. However injection molding is only suitable for plastics lens, it cannot fabricate optical and mechanical components at same time. The assembly error of optical system can be reduced effectively with fabricating optical and mechanical components at same time. The process of printing optical and mechanical components simultaneously is proposed in previous papers, but the optical surface of printing components is not transparent. If we increase the transmittance of the optical surface, the printing components which fabricated by 3D printing process could be high transmission. Therefore, precise diamond turning technique has been used to turning the surface of 3D printing optical lens in this paper. The precise diamond turning techniques could process surfaces of components to meet the requirements of optical system. A 3D printing machine, Stratasys Connex 500, and a precise diamond turning machine, Precitech Freeform705XG, have been used in this paper, respectively. The dimension, roughness, transmission and printing types of 3D printing components have been discussed in this paper. After turning and polishing process, the roughness of 3D printing component is below 0.05 μm and the transmittance increase above 80 %. This optical module can be used in hand-held telescope and other system which need lens and special mechanical structure fabricated simultaneously.

A dimensional comparison between embedded 3D-printed and silicon microchannels

NASA Astrophysics Data System (ADS)

O'Connor, J.; Punch, J.; Jeffers, N.; Stafford, J.

2014-07-01

The subject of this paper is the dimensional characterization of embedded microchannel arrays created using contemporary 3D-printing fabrication techniques. Conventional microchannel arrays, fabricated using deep reactive ion etching techniques (DRIE) and wet-etching (KOH), are used as a benchmark for comparison. Rectangular and trapezoidal cross-sectional shapes were investigated. The channel arrays were 3D-printed in vertical and horizontal directions, to examine the influence of print orientation on channel characteristics. The 3D-printed channels were benchmarked against Silicon channels in terms of the following dimensional characteristics: cross-sectional area (CSA), perimeter, and surface profiles. The 3D-printed microchannel arrays demonstrated variances in CSA of 6.6-20% with the vertical printing approach yielding greater dimensional conformity than the horizontal approach. The measured CSA and perimeter of the vertical channels were smaller than the nominal dimensions, while the horizontal channels were larger in both CSA and perimeter due to additional side-wall roughness present throughout the channel length. This side-wall roughness caused significant shape distortion. Surface profile measurements revealed that the base wall roughness was approximately the resolution of current 3D-printers. A spatial periodicity was found along the channel length which appeared at different frequencies for each channel array. This paper concludes that vertical 3D-printing is superior to the horizontal printing approach, in terms of both dimensional fidelity and shape conformity and can be applied in microfluidic device applications.

Surface roughness effects on turbulent Couette flow

NASA Astrophysics Data System (ADS)

Lee, Young Mo; Lee, Jae Hwa

2017-11-01

Direct numerical simulation of a turbulent Couette flow with two-dimensional (2-D) rod roughness is performed to examine the effects of the surface roughness. The Reynolds number based on the channel centerline laminar velocity (Uco) and channel half height (h) is Re =7200. The 2-D rods are periodically arranged with a streamwise pitch of λ = 8 k on the bottom wall, and the roughness height is k = 0.12 h. It is shown that the wall-normal extent for the logarithmic layer is significantly shortened in the rough-wall turbulent Couette flow, compared to a turbulent Couette flow with smooth wall. Although the Reynolds stresses are increased in a turbulent channel flow with surface roughness in the outer layer due to large-scale ejection motions produced by the 2-D rods, those of the rough-wall Couette flow are decreased. Isosurfaces of the u-structures averaged in time suggest that the decrease of the turbulent activity near the centerline is associated with weakened large-scale counter-rotating roll modes by the surface roughness. This research was supported by the National Research Foundation of Korea (NRF) funded by the Ministry of Education (NRF-2017R1D1A1A09000537) and the Ministry of Science, ICT & Future Planning (NRF-2017R1A5A1015311).

Precision of 655nm Confocal Laser Profilometry for 3D surface texture characterisation of natural human enamel undergoing dietary acid mediated erosive wear.

PubMed

Mullan, F; Mylonas, P; Parkinson, C; Bartlett, D; Austin, R S

2018-03-01

To assess the precision of optical profilometry for characterising the 3D surface roughness of natural and polished human enamel in order to reliably quantify acid mediated surface roughness changes in human enamel. Forty-two enamel samples were prepared from extracted human molars and either polished flat or left unmodified. To investigate precision, the variability of thirty repeated measurements of five areas of one polished and one natural enamel sample was assessed using 655nm Confocal Laser Profilometry. Remaining samples were subjected to forty-five minutes orange juice erosion and microstructural changes were analysed using Sa roughness change (μm) and qualitatively using surface/subsurface confocal microscopy. Enamel surface profilometry from the selected areas revealed maximal precision of 5nm for polished enamel and 23nm for natural enamel. After erosion, the polished enamel revealed a 48% increase in mean (SD) Sa roughness of 0.10 (0.07)μm (P<0.05), whereas in contrast the natural enamel revealed a 45% decrease in mean (SD) roughness of -0.32 (0.42)μm (P<0.05). These data were supported by qualitative confocal images of the surface/subsurface enamel. This study demonstrates a method for precise surface texture measurement of natural human enamel. Measurement precision was superior for polished flat enamel in contrast to natural enamel however, natural enamel responds very differently to polished enamel when exposed to erosion challenges. Therefore, thus future studies characterising enamel surface changes following erosion on natural enamel may provide more clinically relevant responses in comparison to polished enamel. Copyright © 2017 The Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Surface changes of metal alloys and high-strength ceramics after ultrasonic scaling and intraoral polishing.

PubMed

Yoon, Hyung-In; Noh, Hyo-Mi; Park, Eun-Jin

2017-06-01

This study was to evaluate the effect of repeated ultrasonic scaling and surface polishing with intraoral polishing kits on the surface roughness of three different restorative materials. A total of 15 identical discs were fabricated with three different materials. The ultrasonic scaling was conducted for 20 seconds on the test surfaces. Subsequently, a multi-step polishing with recommended intraoral polishing kit was performed for 30 seconds. The 3D profiler and scanning electron microscopy were used to investigate surface integrity before scaling (pristine), after scaling, and after surface polishing for each material. Non-parametric Friedman and Wilcoxon signed rank sum tests were employed to statistically evaluate surface roughness changes of the pristine, scaled, and polished specimens. The level of significance was set at 0.05. Surface roughness values before scaling (pristine), after scaling, and polishing of the metal alloys were 3.02±0.34 µm, 2.44±0.72 µm, and 3.49±0.72 µm, respectively. Surface roughness of lithium disilicate increased from 2.35±1.05 µm (pristine) to 28.54±9.64 µm (scaling), and further increased after polishing (56.66±9.12 µm, P <.05). The zirconia showed the most increase in roughness after scaling (from 1.65±0.42 µm to 101.37±18.75 µm), while its surface roughness decreased after polishing (29.57±18.86 µm, P <.05). Ultrasonic scaling significantly changed the surface integrities of lithium disilicate and zirconia. Surface polishing with multi-step intraoral kit after repeated scaling was only effective for the zirconia, while it was not for lithium disilicate.

Surface changes of metal alloys and high-strength ceramics after ultrasonic scaling and intraoral polishing

PubMed Central

Noh, Hyo-Mi

2017-01-01

PURPOSE This study was to evaluate the effect of repeated ultrasonic scaling and surface polishing with intraoral polishing kits on the surface roughness of three different restorative materials. MATERIALS AND METHODS A total of 15 identical discs were fabricated with three different materials. The ultrasonic scaling was conducted for 20 seconds on the test surfaces. Subsequently, a multi-step polishing with recommended intraoral polishing kit was performed for 30 seconds. The 3D profiler and scanning electron microscopy were used to investigate surface integrity before scaling (pristine), after scaling, and after surface polishing for each material. Non-parametric Friedman and Wilcoxon signed rank sum tests were employed to statistically evaluate surface roughness changes of the pristine, scaled, and polished specimens. The level of significance was set at 0.05. RESULTS Surface roughness values before scaling (pristine), after scaling, and polishing of the metal alloys were 3.02±0.34 µm, 2.44±0.72 µm, and 3.49±0.72 µm, respectively. Surface roughness of lithium disilicate increased from 2.35±1.05 µm (pristine) to 28.54±9.64 µm (scaling), and further increased after polishing (56.66±9.12 µm, P<.05). The zirconia showed the most increase in roughness after scaling (from 1.65±0.42 µm to 101.37±18.75 µm), while its surface roughness decreased after polishing (29.57±18.86 µm, P<.05). CONCLUSION Ultrasonic scaling significantly changed the surface integrities of lithium disilicate and zirconia. Surface polishing with multi-step intraoral kit after repeated scaling was only effective for the zirconia, while it was not for lithium disilicate. PMID:28680550

Nanoimprint Lithography on curved surfaces prepared by fused deposition modelling

NASA Astrophysics Data System (ADS)

Köpplmayr, Thomas; Häusler, Lukas; Bergmair, Iris; Mühlberger, Michael

2015-06-01

Fused deposition modelling (FDM) is an additive manufacturing technology commonly used for modelling, prototyping and production applications. The achievable surface roughness is one of its most limiting aspects. It is however of great interest to create well-defined (nanosized) patterns on the surface for functional applications such as optical effects, electronics or bio-medical devices. We used UV-curable polymers of different viscosities and flexible stamps made of poly(dimethylsiloxane) (PDMS) to perform Nanoimprint Lithography (NIL) on FDM-printed curved parts. Substrates with different roughness and curvature were prepared using a commercially available 3D printer. The nanoimprint results were characterized by optical light microscopy, profilometry and atomic force microscopy (AFM). Our experiments show promising results in creating well-defined microstructures on the 3D-printed parts.

Roughness of stylolites: implications of 3D high resolution topography measurements.

PubMed

Schmittbuhl, J; Renard, F; Gratier, J P; Toussaint, R

2004-12-03

Stylolites are natural pressure-dissolution surfaces in sedimentary rocks. We present 3D high resolution measurements at laboratory scales of their complex roughness. The topography is shown to be described by a self-affine scaling invariance. At large scales, the Hurst exponent is zeta(1) approximately 0.5 and very different from that at small scales where zeta(2) approximately 1.2. A crossover length scale at around L(c)=1 mm is well characterized. Measurements are consistent with a Langevin equation that describes the growth of a stylolitic interface as a competition between stabilizing long range elastic interactions at large scales or local surface tension effects at small scales and a destabilizing quenched material disorder.

Comparison of two metrological approaches for the prediction of human haptic perception

NASA Astrophysics Data System (ADS)

Neumann, Annika; Frank, Daniel; Vondenhoff, Thomas; Schmitt, Robert

2016-06-01

Haptic perception is regarded as a key component of customer appreciation and acceptance for various products. The prediction of customers’ haptic perception is of interest both during product development and production phases. This paper presents the results of a multivariate analysis between perceived roughness and texture related surface measurements, to examine whether perceived roughness can be accurately predicted using technical measurements. Studies have shown that standardized measurement parameters, such as the roughness coefficients (e.g. Rz or Ra), do not show a one-dimensional linear correlation with the human perception (of roughness). Thus, an alternative measurement method was compared to standard measurements of roughness, in regard to its capability of predicting perceived roughness through technical measurements. To estimate perceived roughness, an experimental study was conducted in which 102 subjects evaluated four sets of 12 different geometrical surface structures regarding their relative perceived roughness. The two different metrological procedures were examined in relation to their capability to predict the perceived roughness of the subjects stated within the study. The standardized measurements of the surface roughness were made using a structured light 3D-scanner. As an alternative method, surface induced vibrations were measured by a finger-like sensor during robot-controlled traverse over a surface. The presented findings provide a better understanding of the predictability of human haptic perception using technical measurements.

Validation of SMAP Radar Vegetation Data Cubes from Agricultural Field Measurements

NASA Astrophysics Data System (ADS)

Tsang, L.; Xu, X.; Liao, T.; Kim, S.; Njoku, E. G.

2012-12-01

The NASA Soil Moisture Active/Passive (SMAP) Mission will be launched in October 2014. The objective of the SMAP mission is to provide global measurements of soil moisture and its freeze/thaw state. These measurements will be used to enhance understanding of processes that link the water, energy and carbon cycles, and to extend the capabilities of weather and climate prediction models. In the active algorithm, the retrieval is performed based on the backscattering data cube, which are characterized by two surface parameters, which are soil moisture and soil surface rms height, and one vegetation parameter, the vegetation water content. We have developed a physical-based forward scattering model to generate the data cube for agricultural fields. To represent the agricultural crops, we include a layer of cylinders and disks on top of the rough surface. The scattering cross section of the vegetation layer and its interaction with the underground soil surface were calculated by the distorted Born approximation, which give explicitly three scattering mechanisms. A) The direct volume scattering B) The double bounce effect as, and C) The double bouncing effects. The direct volume scattering is calculated by using the Body of Revolution code. The double bounce effects, exhibited by the interaction of rough surface with the vegetation layer is considered by modifying the rough surface reflectivity using the coherent wave as computed by Numerical solution of Maxwell equations of 3 Dimensional simulations (NMM3D) of bare soil scattering. The rough surface scattering of the soil was calculated by NMM3D. We have compared the physical scattering models with field measurements. In the field campaign, the measurements were made on soil moisture, rough surface rms heights and vegetation water content as well as geometric parameters of vegetation. The three main crops lands are grassland, cornfield and soybean fields. The corresponding data cubes are validated using SGP99, SMEX02 and SMEX 08 field experiments.

3D Micro-topography of Transferred Laboratory and Natural Ice Crystal Surfaces Imaged by Cryo and Environmental Scanning Electron Microscopy

NASA Astrophysics Data System (ADS)

Magee, N. B.; Boaggio, K.; Bancroft, L.; Bandamede, M.

2015-12-01

Recent work has highlighted micro-scale roughness on the surfaces of ice crystals grown and imaged in-situ within the chambers of environmental scanning electron microscopes (ESEM). These observations appear to align with theoretical and satellite observations that suggest a prevalence of rough ice in cirrus clouds. However, the atmospheric application of the lab observations are indeterminate because the observations have been based only on crystals grown on substrates and in pure-water vapor environments. In this work, we present details and results from the development of a transfer technique which allows natural and lab-grown ice and snow crystals to be captured, preserved, and transferred into the ESEM for 3D imaging. Ice crystals were gathered from 1) natural snow, 2) a balloon-borne cirrus particle capture device, and 3) lab-grown ice crystals from a diffusion chamber. Ice crystals were captured in a pre-conditioned small-volume (~1 cm3) cryo-containment cell. The cell was then sealed closed and transferred to a specially-designed cryogenic dewer (filled with liquid nitrogen or crushed dry ice) for transport to a new Hitachi Field Emission, Variable Pressure SEM (SU-5000). The cryo-cell was then removed from the dewer and quickly placed onto the pre-conditioned cryo transfer stage attached to the ESEM (Quorum 3010T). Quantitative 3D topographical digital elevation models of ice surfaces are reported from SEM for the first time, including a variety of objective measures of statistical surface roughness. The surfaces of the transported crystals clearly exhibit signatures of mesoscopic roughening that are similar to examples of roughness seen in ESEM-grown crystals. For most transported crystals, the habits and crystal edges are more intricate that those observed for ice grown directly on substrates within the ESEM chamber. Portions of some crystals do appear smooth even at magnification greater than 1000x, a rare observation in our ESEM-grown crystals. The transported crystals hint at some significant differences in roughness morphology, but they do provide evidence that crystals grown in air/water mixtures and with minimal substrate influence also exhibit mesoscopic roughness with similarity to that observed in ESEM-grown crystals.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jiang, S. D.; Eggers, T.; Thiabgoh, O.

Understanding the relationship between the surface conditions and giant magneto-impedance (GMI) in Co-rich melt-extracted microwires is key to optimizing their magnetic responses for magnetic sensor applications. The surface magnetic domain structure (SMDS) parameters of ~45 μm diameter Co 69.25Fe 4.25Si 13B 13.5-xZr x (x = 0, 1, 2, 3) microwires, including the magnetic domain period (d) and surface roughness (Rq) as extracted from the magnetic force microscopy (MFM) images, have been correlated with GMI in the range 1–1000 MHz. It was found that substitution of B with 1 at. % Zr increased d of the base alloy from 729 tomore » 740 nm while retaining Rq from ~1 nm to ~3 nm. A tremendous impact on the GMI ratio was found, increasing the ratio from ~360% to ~490% at an operating frequency of 40 MHz. Further substitution with Zr decreased the high frequency GMI ratio, which can be understood by the significant increase in surface roughness evident by force microscopy. Lastly, this study demonstrates the application of the domain period and surface roughness found by force microscopy to the interpretation of the GMI in Co-rich microwires.« less

Growth of porous anodized alumina on the sputtered aluminum films with 2D-3D morphology for high specific surface area

NASA Astrophysics Data System (ADS)

Liao, M. W.; Chung, C. K.

2014-08-01

The porous anodic aluminum oxide (AAO) with high-aspect-ratio pore channels is widely used as a template for fabricating nanowires or other one-dimensional (1D) nanostructures. The high specific surface area of AAO can also be applied to the super capacitor and the supporting substrate for catalysis. The rough surface could be helpful to enhance specific surface area but it generally results in electrical field concentration even to ruin AAO. In this article, the aluminum (Al) films with the varied 2D-3D morphology on Si substrates were prepared using magnetron sputtering at a power of 50 W-185 W for 1 h at a working pressure of 2.5 × 10-1 Pa. Then, AAO was fabricated from the different Al films by means of one-step hybrid pulse anodizing (HPA) between the positive 40 V and the negative -2 V (1 s:1 s) for 3 min in 0.3 M oxalic acid at a room temperature. The microstructure and morphology of Al films were characterized by X-ray diffraction, scanning electron microscope and atomic force microscope, respectively. Some hillocks formed at the high target power could be attributed to the grain texture growth in the normal orientation of Al(1 1 1). The 3D porous AAO structure which is different from the conventional 2D planar one has been successfully demonstrated using HPA on the film with greatly rough hillock-surface formed at the highest power of 185 W. It offers a potential application of the new 3D AAO to high specific surface area devices.

Roughness, surface energy, and superficial damages of CAD/CAM materials after surface treatment.

PubMed

Strasser, Thomas; Preis, Verena; Behr, Michael; Rosentritt, Martin

2018-02-05

The aim of this study was to examine the effects of surface pre-treatment on CAD/CAM materials including ceramics, zirconia, resin-infiltrated ceramic, and resin-based composite. Specimens were made of ten CAD/CAM materials (Celtra Duo, Degudent, D; Vita Suprinity, Vita, D; E.max CAD, Ivoclar-Vivadent, FL; E.max ZirCAD, Ivoclar-Vivadent, FL; Vita Enamic, Vita, D; Cerasmart, GC, B; LAVA Ultimate, 3M, D; SHOFU Block HC, SHOFU, US; Grandio Blocs, VOCO, D; BRILLIANT Crios, Coltene, CH) and pretreated to represent clinical procedures (Hf 20 s/5%; phosphoric acid 20 s/37%; Monobond etch and prime (Ivoclar-Vivadent, FL); water-cooled diamond bur (80 μm; 4 μm); Al 2 O 3 -blasting (50 μm/1 bar, 50 μm/2 bar, 120 μm/1 bar, 120 μm/2 bar); untreated; manufacturer's instructions). SEM-analysis (Phenom, FEI, NL) of the surfaces was performed (magnifications ≤ 10,000×). Roughness values R a , R z (KJ 3D, Keyence, J), and surface energy SE (OCA15 plus, SCA20, DataPhysics, D) were determined (statistics: non-parametric Mann-Whitney U test/Kruskal-Wallis test for independent specimen, α = 0.05). Kruskal-Wallis revealed significant (p < 0.001) differences for all materials with different surface treatments. Roughness ranged from R a  = 0.05 μm (VS; D4)/R z  = 0.41 μm (VS; D4) to R a  = 1.82 μm (EMA; SB120/2)/R z  = 12.05 μm (CS; SB 120/2), SE from 22.7 mN/m (VE; M) to 52.8 mN/m (CD; M). SEM analysis showed material-dependent damages after pre-treatment. Different CAD/CAM materials require individual pre-treatment for optimized and protective surface activation. Cementation is a key factor for clinical success. Given the variety of available CAD/CAM materials, specific procedures are needed.

Micromorphological characterization of zinc/silver particle composite coatings.

PubMed

Méndez, Alia; Reyes, Yolanda; Trejo, Gabriel; StĘpień, Krzysztof; Ţălu, Ştefan

2015-12-01

The aim of this study was to evaluate the three-dimensional (3D) surface micromorphology of zinc/silver particles (Zn/AgPs) composite coatings with antibacterial activity prepared using an electrodeposition technique. These 3D nanostructures were investigated over square areas of 5 μm × 5 μm by atomic force microscopy (AFM), fractal, and wavelet analysis. The fractal analysis of 3D surface roughness revealed that (Zn/AgPs) composite coatings have fractal geometry. Triangulation method, based on the linear interpolation type, applied for AFM data was employed in order to characterise the surfaces topographically (in amplitude, spatial distribution and pattern of surface characteristics). The surface fractal dimension Df , as well as height values distribution have been determined for the 3D nanostructure surfaces. © 2015 The Authors published by Wiley Periodicals, Inc.

Evaluation of the Effect of Surface Polishing, Oral Beverages and Food Colorants on Color Stability and Surface Roughness of Nanocomposite Resins

PubMed Central

Kumari, R Veena; Nagaraj, Hema; Siddaraju, Kishore; Poluri, Ramya Krishna

2015-01-01

Background: It is beyond doubt that finishing and polishing of a composite restoration enhance its esthetics and, is also essential for the health of the periodontium. A variety of instruments are commonly used for finishing and polishing tooth-colored restorative materials Thus, it is important to understand which type of surface finishing treatments would significantly affect the staining and surface irregularities of the composite resin restoration. Still one of the properties of the composite resins that have to pass the test of time is its color stability. In modern day dentistry, a large emphasis is laid over esthetics. Hence, it is important to understand the various agents capable of adversely affecting the esthetics of a restoration due to its staining capacity. Thus, the aim of this in vitro study was to evaluate the effect of surface polishing, oral beverages and food colorants on the color stability and surface roughness of nanocomposite resins. Materials and Methods: 90 Disks of nanocomposites resin (Filtek Z350 XT) measuring 8 mm in diameter and 2 mm in thickness were fabricated using a custom made silicon mold. Pre-polishing surface roughness (Ra1) of all the 90 samples were measured using a Surface Profilometer. The nano-composite disks were then randomly divided into 3 groups with 30 samples in each group. Group I: Control group: The samples were not subjected to any polishing procedures. Group II: Sof-Lex group: Samples subjected to polishing using different grits of Sof-Lex disks. Group III: Diamond polishing paste group: Samples were subjected with a polishing paste consisting of diamond particles. Following polishing procedures, the surface roughness of all samples were measured again to obtain change in surface roughness due to polishing procedures (Ra2), pre immersion spectrophotometric value (ΔE1) was also recorded for baseline color of the samples. The samples were then divided into subgroups (A, B, C, D, E), by including every first sample in Subgroup A, second in Subgroup B, third in Subgroup C, fourth in Subgroup D, and fifth in Subgroup E. Each was immersed in the respective test solution for 10 min, twice a day for 30 days. Group A - Tea, Group B - Coffee, Group C - Cola, Group D - Turmeric, Group E - Control (artificial saliva). Post immersion profilometric value was recorded to evaluate roughness bought about by the solutions (Ra3) and spectrophotometric value was recorded to evaluate the color change in samples (ΔE2). Results were statistically analyzed using ANOVA. Results: Higher mean roughness (Ra2-Ra1) value was recorded in Sof-Lex, followed by Diamond polishing paste and Control group. Comparison of surface roughness caused due to beverages and food colorant solution showed subgroup C (Coca Cola) increased surface roughness in all groups (Group I, II, III). Subgroup D (Turmeric) had the highest discoloration potential (P < 0001) in all groups, followed by coffee, tea, coca-cola and artificial saliva. Sof-Lex polishing System showed most color stability. Conclusion: Polishing procedures significantly roughen the surface of the restoration compared to the unpolished Mylar controls. One-step polishing system (diamond polishing paste) produces a smoother surface compared to a multi-step system (Sof-Lex polishing disks). Turmeric solution caused maximum staining of the samples, to a visually perceptible level. PMID:26229373

Evaluation of the Effect of Surface Polishing, Oral Beverages and Food Colorants on Color Stability and Surface Roughness of Nanocomposite Resins.

PubMed

Kumari, R Veena; Nagaraj, Hema; Siddaraju, Kishore; Poluri, Ramya Krishna

2015-07-01

It is beyond doubt that finishing and polishing of a composite restoration enhance its esthetics and, is also essential for the health of the periodontium. A variety of instruments are commonly used for finishing and polishing tooth-colored restorative materials Thus, it is important to understand which type of surface finishing treatments would significantly affect the staining and surface irregularities of the composite resin restoration. Still one of the properties of the composite resins that have to pass the test of time is its color stability. In modern day dentistry, a large emphasis is laid over esthetics. Hence, it is important to understand the various agents capable of adversely affecting the esthetics of a restoration due to its staining capacity. Thus, the aim of this in vitro study was to evaluate the effect of surface polishing, oral beverages and food colorants on the color stability and surface roughness of nanocomposite resins. 90 Disks of nanocomposites resin (Filtek Z350 XT) measuring 8 mm in diameter and 2 mm in thickness were fabricated using a custom made silicon mold. Pre-polishing surface roughness (Ra1) of all the 90 samples were measured using a Surface Profilometer. The nano-composite disks were then randomly divided into 3 groups with 30 samples in each group. Group I: The samples were not subjected to any polishing procedures. Group II: Sof-Lex group: Samples subjected to polishing using different grits of Sof-Lex disks. Group III: Diamond polishing paste group: Samples were subjected with a polishing paste consisting of diamond particles. Following polishing procedures, the surface roughness of all samples were measured again to obtain change in surface roughness due to polishing procedures (Ra2), pre immersion spectrophotometric value (ΔE1) was also recorded for baseline color of the samples. The samples were then divided into subgroups (A, B, C, D, E), by including every first sample in Subgroup A, second in Subgroup B, third in Subgroup C, fourth in Subgroup D, and fifth in Subgroup E. Each was immersed in the respective test solution for 10 min, twice a day for 30 days. Group A - Tea, Group B - Coffee, Group C - Cola, Group D - Turmeric, Group E - Control (artificial saliva). Post immersion profilometric value was recorded to evaluate roughness bought about by the solutions (Ra3) and spectrophotometric value was recorded to evaluate the color change in samples (ΔE2). Results were statistically analyzed using ANOVA. Higher mean roughness (Ra2-Ra1) value was recorded in Sof-Lex, followed by Diamond polishing paste and Control group. Comparison of surface roughness caused due to beverages and food colorant solution showed subgroup C (Coca Cola) increased surface roughness in all groups (Group I, II, III). Subgroup D (Turmeric) had the highest discoloration potential (P < 0001) in all groups, followed by coffee, tea, coca-cola and artificial saliva. Sof-Lex polishing System showed most color stability. Polishing procedures significantly roughen the surface of the restoration compared to the unpolished Mylar controls. One-step polishing system (diamond polishing paste) produces a smoother surface compared to a multi-step system (Sof-Lex polishing disks). Turmeric solution caused maximum staining of the samples, to a visually perceptible level.

Acoustic imaging in application to reconstruction of rough rigid surface with airborne ultrasound waves

NASA Astrophysics Data System (ADS)

Krynkin, A.; Dolcetti, G.; Hunting, S.

2017-02-01

Accurate reconstruction of the surface roughness is of high importance to various areas of science and engineering. One important application of this technology is for remote monitoring of open channel flows through observing its dynamic surface roughness. In this paper a novel airborne acoustic method of roughness reconstruction is proposed and tested with a static rigid rough surface. This method is based on the acoustic holography principle and Kirchhoff approximation which make use of acoustic pressure data collected at multiple receiver points spread along an arch. The Tikhonov regularisation and generalised cross validation technique are used to solve the underdetermined system of equations for the acoustic pressures. The experimental data are collected above a roughness created with a 3D printer. For the given surface, it is shown that the proposed method works well with the various number of receiver positions. In this paper, the tested ratios between the number of surface points at which the surface elevation can be reconstructed and number of receiver positions are 2.5, 5, and 7.5. It is shown that, in a region comparable with the projected size of the main directivity lobe, the method is able to reconstruct the spatial spectrum density of the actual surface elevation with the accuracy of 20%.

Acoustic imaging in application to reconstruction of rough rigid surface with airborne ultrasound waves.

PubMed

Krynkin, A; Dolcetti, G; Hunting, S

2017-02-01

Accurate reconstruction of the surface roughness is of high importance to various areas of science and engineering. One important application of this technology is for remote monitoring of open channel flows through observing its dynamic surface roughness. In this paper a novel airborne acoustic method of roughness reconstruction is proposed and tested with a static rigid rough surface. This method is based on the acoustic holography principle and Kirchhoff approximation which make use of acoustic pressure data collected at multiple receiver points spread along an arch. The Tikhonov regularisation and generalised cross validation technique are used to solve the underdetermined system of equations for the acoustic pressures. The experimental data are collected above a roughness created with a 3D printer. For the given surface, it is shown that the proposed method works well with the various number of receiver positions. In this paper, the tested ratios between the number of surface points at which the surface elevation can be reconstructed and number of receiver positions are 2.5, 5, and 7.5. It is shown that, in a region comparable with the projected size of the main directivity lobe, the method is able to reconstruct the spatial spectrum density of the actual surface elevation with the accuracy of 20%.

New surface smoothing technologies for manufacturing of complex shaped glass components

NASA Astrophysics Data System (ADS)

Henkel, Sebastian; Schwager, Anne-Marie; Bliedtner, Jens; Götze, Kerstin; Rädlein, Edda; Schulze, Christian; Gerhardt, Martin; Fuhr, Michael

2017-10-01

The production of complex glass components with 2.5D or 3D-structures involves great effort and the need for advanced CNC-technology. Especially the final surface treatment, for generation of transparent surfaces, represents a timeconsuming and costly process. The ultrasonic-assisted grinding procedure is used to generate arbitrary shaped components and freeform-surfaces. The special kinematic principle, containing a high-frequency tool oscillation, enables efficient manufacturing processes. Surfaces produced in this way allow for application of novel smoothing methods, providing considerable advantages compared to classic polishing. It is shown, that manufacturing of transparent glass surfaces with low roughness down to Rq = 10 nm is possible, using an ultra-fine grinding process. By adding a CO2-laser polishing process, roughness can be reduced even further with a very short polishing time.

3D surface topography study of the biofunctionalized nanocrystalline Ti-6Zr-4Nb/Ca-P

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jakubowicz, J., E-mail: jaroslaw.jakubowicz@put.poznan.pl; Adamek, G.; Jurczyk, M.U.

2012-08-15

In this work surface of the sintered Ti-6Zr-4Nb nanocrystalline alloy was electrochemically biofunctionalized. The porous surface was produced by anodic oxidation in 1 M H{sub 3}PO{sub 4} + 2%HF electrolyte at 10 V for 30 min. Next the calcium-phosphate (Ca-P) layer was deposited, onto the formed porous surface, using cathodic potential - 5 V kept for 60 min in 0.042 M Ca(NO{sub 3}){sub 2} + 0.025 M (NH{sub 4}){sub 2}HPO{sub 4} + 0.1 M HCl electrolyte. The deposited Ca-P layer anchored in the pores. The biofunctionalized surface was studied by XRD, SEM and EDS. In vitro tests culture of normalmore » human osteoblast (NHOst) cells showed very good cells proliferation, colonization and multilayering. Using optical profiler, roughness and hybrid 3D surface topography parameters were estimated. Correlation between surface composition, morphology, roughness and biocompatibility results was done. It has been shown by us that surface with appropriate chemical composition and topography, after combined electrochemical anodic and cathodic surface treatment, supports osteoblast adhesion and proliferation. 3D topography measurements using optical profiler play a key role in the biomaterials surface analysis. - Highlights: Black-Right-Pointing-Pointer Nanocrystalline Ti-6Zr-4Nb/Ca-P material was produced for hard tissue implant applications. Black-Right-Pointing-Pointer Calcium-phosphate results in surface biofunctionalization. Black-Right-Pointing-Pointer The biofunctionalized surface shows good in-vitro behavior.« less

The Effects of Acid Etching on the Nanomorphological Surface Characteristics and Activation Energy of Titanium Medical Materials.

PubMed

Hung, Kuo-Yung; Lin, Yi-Chih; Feng, Hui-Ping

2017-10-11

The purpose of this study was to characterize the etching mechanism, namely, the etching rate and the activation energy, of a titanium dental implant in concentrated acid and to construct the relation between the activation energy and the nanoscale surface topographies. A commercially-pure titanium (CP Ti) and Ti-6Al-4V ELI surface were tested by shot blasting (pressure, grain size, blasting distance, blasting angle, and time) and acid etching to study its topographical, weight loss, surface roughness, and activation energy. An Arrhenius equation was applied to derive the activation energy for the dissolution of CP Ti/Ti-6Al-4V ELI in sulfuric acid (H₂SO₄) and hydrochloric acid (HCl) at different temperatures. In addition, white-light interferometry was applied to measure the surface nanomorphology of the implant to obtain 2D or 3D roughness parameters (Sa, Sq, and St). The nanopore size that formed after etching was approximately 100-500 nm. The surface roughness of CP Ti and Ti-6Al-4V ELI decreased as the activation energy decreased but weight loss increased. Ti-6Al-4V ELI has a higher level of activation energy than Ti in HCl, which results in lower surface roughness after acid etching. This study also indicates that etching using a concentrated hydrochloric acid provided superior surface modification effects in titanium compared with H₂SO₄.

A novel method of creation capillary structures in metal parts based on using selective laser melting methid of 3D printing technology and surface roughness

NASA Astrophysics Data System (ADS)

Ivanov, Roman A.; Melkikh, Alexey V.

2017-09-01

It has been experimentally proved that it is possible to produce a metal capillary structure with significant capillary action and free shape configuration using selective laser melting. Capillaries are created by dividing the solid detail volume into micro-sized parallel walls with roughness as a result of SLM 3D printing. Experiments are conducted on aluminum powder with particle size in the range of 10-40 µm (,) and distances in 3D model between surfaces incapillary generation zone in the range of 50-200 µm. It is showed that products produced from model with 100 µm gaps have the greatest efficiency of fluid lifting as a result of obtaining stable arrays of capillaries of 20-40 µm in size. Change in the direction of (growing) printingthe product doesn't significantly influence on capillary geometry, but it affects on safety of the structure.

The influence of surface roughness and solution concentration on pool boiling process in Diethanolamine aqueous solution

NASA Astrophysics Data System (ADS)

Khoshechin, Mohsen; Salimi, Farhad; Jahangiri, Alireza

2018-04-01

In this research, the effect of surface roughness and concentration of solution on bubble departing frequency and nucleation site density for pool boiling of water/diethanolamine (DEA) binary solution were investigated experimentally. In this investigation, boiling heat transfer coefficient, bubble departing frequency and nucleation site density have been experimentally investigated in various concentrations and heat fluxes. Microstructured surfaces with a wide range of well-defined surface roughness were fabricated, and a heat flux between 1.5-86 kW/m2 was achieved under atmospheric conditions. The Results indicated that surface roughness and concentration of solution increase the bubble departing frequency and nucleation site density with increasing heat flux. The boiling heat transfer coefficient in mixtures of water/DEA increases with increasing concentration of DEA in water. The experimental results were compared with predictions of several used correlations in the literatures. Results showed that the boiling heat transfer coefficients of this case study are much higher than the predicted values by major existing correlations and models. The excellent agreement for bubble departing frequency found between the models of Jackob and Fritz (1966) and experimental data and also the nucleation site density were in close agreement with the model of Paul (1983) data. f bubble departure frequency, 1/s or Hz N Number of nucleation sites per area per time R c Minimum cavity size, m D c critical diameter, m g gravitational acceleration, m/s2 ρ density, kg/m3 T temperature, °c ΔT temperature difference, °c d d vapor bubble diameter, m h fg enthalpy of vaporization, J/kg R Roughness, μm Ja Jakob number cp specific heat, J/kg °c Pr Prandtl number Ar Archimedes number h Heat transfer coefficient, J/(m2 °c) tg time it takes to grow a bubble, s q/A heat flux (kW/m2) tw time required to heat the layer, s gc Correction coefficient of incompatible units R a Surface roughness A heated surface area d departure ONB onset of nucleate boiling w surface wall s saturation v vapor l liquid θ groove angle (o) γ influence parameter of heating surface material σ surface tension, N/m.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dylla-Spears, R.; Wong, L.; Shen, N.

Particle adsorption was explored in a model optical polishing system, consisting of silica colloids and like-charged silica surfaces. The adsorption was monitored in situ under various suspension conditions, in the absence of surfactants or organic modifiers, using a quartz crystal microbalance with dissipation monitoring (QCM-D). Changes in surface coverage with particle concentration, particle size, pH, ionic strength and ionic composition were quantified by QCM-D and further characterized ex situ by atomic force microscopy (AFM). A Monte Carlo model was used to describe the kinetics of particle deposition and provide insights on scaling with particle concentration. Transitions from near-zero adsorption tomore » measurable adsorption were compared with equilibrium predictions made using the Deraguin-Verwey-Landau-Overbeek (DLVO) theory. In addition, the impact of silica surface roughness on the propensity for particle adsorption was studied on various spatial scale lengths by intentionally roughening the QCM sensor surface using polishing methods. It was found that a change in silica surface roughness at the AFM scale from 1.3 nm root-mean-square (rms) to 2.7 nm rms resulted in an increase in silica particle adsorption of 3-fold for 50-nm diameter particles and 1.3-fold for 100-nm diameter particles—far exceeding adsorption observed by altering suspension conditions alone, potentially because roughness at the proper scale reduces the total separation distance between particle and surface.« less

Investigation Into the Accuracy of 3D Surface Roughness Characteristics

NASA Astrophysics Data System (ADS)

Kumermanis, M.; Rudzitis, J.; Mozga, N.; Ancans, A.; Grislis, A.

2014-04-01

The existing standards for surface roughness cover only two dimensions, while in reality this is three-dimensional (3D). In particular, the 3D surface roughness parameters are important for solving the contact surface mechanics problems as related to the accuracy of 3D surface roughness characteristics. One of the most important factors for determination of 3D characteristics is the number of data points (NDP) on the x- and y-axes (i.e. in cut-off length). The NDP has a profound effect on the accuracy of measurement results, measuring time and volume of the output data (especially along the y-axis, where the NDP is identical to the number of parallel profiles). At a too small NDP the results will be incorrect and with too broad scatter, while a too large NDP - though not enlarging the range of basic information - considerably increases the measuring time. Therefore, the aim of the work was to find the optimal NDP for such surface processing methods as grinding, spark erosion and shot methods of surface treatment. Eksistējošie virsmas raupjuma standarti apskata virsmas raupjumu tikai divās dimensijās. Tomēr reālais virsmas raupjums pēc savas dabas ir trīsdimensiju (3D) objekts. Līdz ar to virsmas raupjums ir jāraksturo ar 3D parametriem. Un no šo parametru noteikšanas precizitātes ir atkarīgi tālākie virsmas aprēķini, piemēram, virsmu kontaktēšanās process. Viens no svarīgākajiem faktoriem, raksturojot virsmas raupjumu 3D, pielietojot kontakta tipa mēriekārtas, ir datu punktu skaits pa abām mērīšanas asīm x un y. Ar datu punktu skaitu mēs saprotam to skaitu mērīšanas bāzes garumā. Datu punktu skaits būtiski ietekmē sagaidāmo mērījumu rezultātu precizitāti, mērīšanai nepieciešamo laiku un izejas datu faila izmērus (sevišķi y-ass virzienā, kur katrs datu punkts ir paralēls profils). Datu punktu skaitam ir jābūt optimālam. Pārāk mazs punktu skaits noved pie neprecīziem rezultātiem un lielas to izkliedes, savukārt pārāk liels punktu skaits nedod būtisku informācijas pieaugumu, bet palielina mērījumam nepieciešamo laiku. Līdz ar to, mums ir jāatrod optimālākais datu punktu skaits katrai virsmas apstrādes metodei vai to grupai.

Assessment of morphology, topography and chemical composition of water-repellent films based on polystyrene/titanium dioxide nanocomposites

NASA Astrophysics Data System (ADS)

Bolvardi, Beleta; Seyfi, Javad; Hejazi, Iman; Otadi, Maryam; Khonakdar, Hossein Ali; Drechsler, Astrid; Holzschuh, Matthias

2017-02-01

In this study, polystyrene (PS)/titanium dioxide (TiO2) films were fabricated through simple solution casting technique via a modified phase separation process. The presented approach resulted in a remarkable reduction in the required amount of nanoparticles for achieving superhydrophobicity. Scanning electron microscopy (SEM) and 3D confocal microscopy were utilized to characterize surface morphology and topography of samples, respectively. An attempt was made to give an in-depth analysis on the surface rough structure using 3D roughness profiles. It was found that high inclusions of non-solvent and nanoparticles resulted in a stable self-cleaning behavior due to the strong presence of hydrophobic TiO2 nanoparticles on the surface. Quite unexpectedly, low inclusions of nanoparticles and non-solvent also resulted in superhydrophobic property mainly due to the proper level of induced surface roughness. XPS analysis was also utilized to determine the chemical composition of the films' surfaces. The results of falling drop experiments showed that the sample containing a higher level of nanoparticles had a much lower mechanical resistance against the induced harsh conditions. All in all, the presented method has shown promising potential in fabrication of superhydrophobic surfaces with self-cleaning behavior using the lowest content of nanoparticles.

Evaluation of the surface roughness of three heat-cured acrylic denture base resins with different conventional lathe polishing techniques: A comparative study.

PubMed

Rao, Duggineni Chalapathi; Kalavathy, N; Mohammad, H S; Hariprasad, A; Kumar, C Ravi

2015-01-01

Surface roughness promotes adhesion and colonization of denture plaque. Therefore, it is important to know the effects of polishing and finishing on the surface roughness of various acrylic resin materials. To evaluate and compare the effects of different conventional lathe polishing techniques on heat cured acrylic resins in producing surface roughness. Three different commercially available heat-cured acrylic resin materials namely DPI, Meliodent and Trevalon Hi were selected. 30 Specimens of each acrylic material (30 x 3 = 90, 10 x 60 x 2mm) were prepared and divided into 5 groups, each group consisted of 6 Nos. of specimens per material(6x3=18) and were grouped as Group A(unfinished), Group B (finished), Group C (Polishing Paste), Group D (Polishing Cake) and Group E (Pumice and Gold rouge). The resulted surface roughness (μm) was measured using Perthometer and observed under Scanning Electron Microscope. The values obtained were subjected statistical analyses. Among the materials tested, better results were obtained with Trevalon Hi followed by Meliodent and DPI. Among the polishing methods used, superior results were obtained with universal polishing paste followed by polishing cake; Pumice and Gold rouge. Although Pumice and Gold rouge values produced greater roughness value, they were well within the threshold value of 0.2 mm.

Influence of Additional Leading-Edge Surface Roughness on Performances in Highly Loaded Compressor Cascade

NASA Astrophysics Data System (ADS)

Chen, Shaowen; Xu, Hao; Sun, Shijun; Zhang, Longxin; Wang, Songtao

2015-05-01

Experimental research has been carried out at low speed to investigate the effect of additional leading-edge surface roughness on a highly-loaded axial compressor cascade. A 5-hole aerodynamic probe has been traversed across one pitch to obtain the distribution of total pressure loss coefficient, secondary flow vector, flow angles and other aerodynamic parameters at the exit section. Meanwhile, ink-trace flow visualization has been used to measure the flow fields on the walls of cascades and a detailed topology structure of the flow on the walls has been obtained. Aerodynamic parameters and flow characteristics are compared by arranging different levels of roughness on various parts of the leading edge. The results show that adding surface roughness at the leading edge and on the suction side obviously influences cascade performance. Aggravated 3-D flow separation significantly increases the loss in cascades, and the loss increases till 60% when the level of emery paper is 80 mm. Even there is the potential to improve cascade performance in local area of cascade passage. The influence of the length of surface roughness on cascade performance is not always adverse, and which depends on the position of surface roughness.

Oxygen Plasma Treatment on 3D-Printed Chitosan/Gelatin/Hydroxyapatite Scaffolds for Bone Tissue Engineering.

PubMed

Lee, Chang-Min; Yang, Seong-Won; Jung, Sang-Chul; Kim, Byung-Hoon

2017-04-01

The 3D hydroxyapatite/gelatin/chitosan composite scaffolds were fabricated by 3D printing technique. The scaffolds were treated by oxygen plasma to improve the bioactivity and its surface characterization and in vitro cell culture were investigated. The scaffolds exhibited the good porosity and interconnectivity of pores. After oxygen plasma etching, roughness and wettability on the scaffolds surface are increased. Plasma treated scaffolds showed higher proliferation than that of untreated scaffolds. Oxygen plasma treatment could be used as potential tool to enhance the biocompatibility on the 3D composite scaffolds.

Investigation on wide-band scattering of a 2-D target above 1-D randomly rough surface by FDTD method.

PubMed

Li, Juan; Guo, Li-Xin; Jiao, Yong-Chang; Li, Ke

2011-01-17

Finite-difference time-domain (FDTD) algorithm with a pulse wave excitation is used to investigate the wide-band composite scattering from a two-dimensional(2-D) infinitely long target with arbitrary cross section located above a one-dimensional(1-D) randomly rough surface. The FDTD calculation is performed with a pulse wave incidence, and the 2-D representative time-domain scattered field in the far zone is obtained directly by extrapolating the currently calculated data on the output boundary. Then the 2-D wide-band scattering result is acquired by transforming the representative time-domain field to the frequency domain with a Fourier transform. Taking the composite scattering of an infinitely long cylinder above rough surface as an example, the wide-band response in the far zone by FDTD with the pulsed excitation is computed and it shows a good agreement with the numerical result by FDTD with the sinusoidal illumination. Finally, the normalized radar cross section (NRCS) from a 2-D target above 1-D rough surface versus the incident frequency, and the representative scattered fields in the far zone versus the time are analyzed in detail.

Development of Fractal Dimension and Characteristic Roughness Models for Turned Surface of Carbon Steels

NASA Astrophysics Data System (ADS)

Zuo, Xue; Zhu, Hua; Zhou, Yuankai; Ding, Cong; Sun, Guodong

2016-08-01

Relationships between material hardness, turning parameters (spindle speed and feed rate) and surface parameters (surface roughness Ra, fractal dimension D and characteristic roughness τ∗) are studied and modeled using response surface methodology (RSM). The experiments are carried out on a CNC lathe for six carbon steel material AISI 1010, AISI 1020, AISI 1030, AISI 1045, AISI 1050 and AISI 1060. The profile of turned surface and the surface roughness value are measured by a JB-5C profilometer. Based on the profile data, D and τ∗ are computed through the root-mean-square method. The analysis of variance (ANOVA) reveals that spindle speed is the most significant factors affecting Ra, while material hardness is the most dominant parameter affecting τ∗. Material hardness and spindle speed have the same influence on D. Feed rate has less effect on three surface parameters than spindle speed and material hardness. The second-order models of RSM are established for estimating Ra, D and τ∗. The validity of the developed models is approximately 80%. The response surfaces show that a surface with small Ra and large D and τ∗ can be obtained by selecting a high speed and a large hardness material. According to the established models, Ra, D and τ∗ of six carbon steels surfaces can be predicted under cutting conditions studied in this paper. The results have an instructive meaning to estimate the surface quality before turning.

Scattering by inhomogeneous systems with rough internal surfaces: Porous solids and random-field Ising systems

NASA Astrophysics Data System (ADS)

Wong, Po-Zen

1985-12-01

For a two-component inhomogeneous system consisting of compact domains of characteristic size R, I show that if the domain walls are ``rough'' and their root-mean-square fluctuation w over a distance r obeys a power law w=b(r/a)x (a is the lattice constant and x>0), then the geometrical correlation function γ(r) has leading terms proportional to rx and r for r<>R-1, where d is the dimension of the system. Two possible applications of this result are discussed. (i) In granular porous solids which have a minimum grain size Rmin, the above result implies that surface roughness can cause I(q) to fall off like 1/qα for q>>Rmin-1, where α=3+x>3 for d=3. In particular, when x>1, the surface becomes a fractal with dimension D=1+x=α-2, which can be extracted from the scattering data. On the other hand, if the grains are smooth and their size distribution obeys a power law dN(R)/dR~R-β over a range Rmin

Fusion of cone-beam CT and 3D photographic images for soft tissue simulation in maxillofacial surgery

NASA Astrophysics Data System (ADS)

Chung, Soyoung; Kim, Joojin; Hong, Helen

2016-03-01

During maxillofacial surgery, prediction of the facial outcome after surgery is main concern for both surgeons and patients. However, registration of the facial CBCT images and 3D photographic images has some difficulties that regions around the eyes and mouth are affected by facial expressions or the registration speed is low due to their dense clouds of points on surfaces. Therefore, we propose a framework for the fusion of facial CBCT images and 3D photos with skin segmentation and two-stage surface registration. Our method is composed of three major steps. First, to obtain a CBCT skin surface for the registration with 3D photographic surface, skin is automatically segmented from CBCT images and the skin surface is generated by surface modeling. Second, to roughly align the scale and the orientation of the CBCT skin surface and 3D photographic surface, point-based registration with four corresponding landmarks which are located around the mouth is performed. Finally, to merge the CBCT skin surface and 3D photographic surface, Gaussian-weight-based surface registration is performed within narrow-band of 3D photographic surface.

The SIR-B observations of microwave backscatter dependence on soil moisture, surface roughness, and vegetation covers

NASA Technical Reports Server (NTRS)

Wang, J. R.; Shiue, J. C.; Engman, E. T.; Rusek, M.; Steinmeier, C.

1986-01-01

An experiment was conducted from an L-band SAR aboard Space Shuttle Challenger in October 1984 to study the microwave backscatter dependence on soil moisture, surface roughness, and vegetation cover. The results based on the analyses of an image obtained at 21-deg incidence angle show a positive correlatlion between scattering coefficient and soil moisture content, with a sensitivity comparable to that derived from the ground radar measurements reported by Ulaby et al. (1978). The surface roughness strongly affects the microwave backscatter. A factor of two change in the standard deviation of surface roughness height gives a corresponding change of about 8 dB in the scattering coefficient. The microwave backscatter also depends on the vegetation types. Under the dry soil conditions, the scattering coefficient is observed to change from about -24 dB for an alfalfa or lettuce field to about -17 dB for a mature corn field. These results suggest that observations with a SAR system of multiple frequencies and polarizations are required to unravel the effects of soil moisture, surface roughness, and vegetation cover.

Fundamental studies of nanoarchitectured dye-sensitized solar cells

NASA Astrophysics Data System (ADS)

Yang, Zhenzhen

2011-12-01

Dye-sensitized solar cells (DSSCs) are a promising candidate for next-generation photovoltaic panels due to their low cost, easy fabrication processes and relatively high efficiency. Despite the considerable effort on the advancement of DSSCs, the efficiency of DSSCs has been stalled for nearly two decades due to the complex interplay among various DSSC parameters. Particularly, in a conventional DSSC, a thicker semiconductor photovoltaic (PV) layer, i.e., a dye-sensitized TiO2 nanoparticle layer, is required to accommodate more light-induced charge separation centers to enhance light harvesting efficiency. However, a thicker PV layer concurrently increases the charge transport distance in the PV layer; so the system suffers from more charge recombination, leading to significant deterioration in charge collection efficiency. The conflicting demands on the thickness of PV layer by these two critical elementary photoelectrochemical processes becomes a fundamental limitation for further advancement in DSSCs and limits the choice of redox mediators and electrode materials in DSSCs. Hence, the focus of this dissertation research work is to systematically explore a transformative way to fundamentally resolve the conflicting interplay between light harvesting and charge transport. First, our strategy is to allocate part of the roughness factor to the collecting anode instead of imparting all the roughness factors onto the semiconductor PV layer attached to the anode. As a proof of concept, we first synthesized and characterized a microscopically rough Zn collecting anode, on which ZnO nanotips are grown. For the same surface roughness factor, the length of the ZnO nanotips supported on such a rough Zn anode can be much shorter than that of the ZnO nanowires supported on a planar anode. Our Zn-microtip|ZnO-nanotip DSSCs exhibit enhanced fill factor, Voc and Jsc. The investigation of kinetics indicates that the electron collection time is much faster than the electron lifetime due to the short electron transport distance. Apparently, in contrast to the surface roughness factor of a TiO 2 nanoparticulate film, typically well above 1000, the surface roughness factor of our Zn-microtip|ZnO-nanotip electrode is still very low. Thus, we integrated the above idea in the conventional TiO2-based DSSCs such that the advantage of high surface roughness in conventional NP-based DSSC can be retained. We designed and fabricated an array of metal micropillars by a lithographic method as additional electron collection pathways on a planar TCO anode. The surface roughness is distributed between the collecting electrode and the semiconductor layer. The electron transport kinetics was insightfully studied by electrochemical impedance technique, which suggests that the charge collection efficiency can be enhanced without sacrificing the thickness of TiO2 nanoparticle layer. Furthermore, novel TCO nanoarchitectures were explored by converting the 2-D planar TCO to 3-D structure with intentional incorporation of functional optical structures, e.g., photonic crystals in the cell, to synergistically enhance light harvesting efficiency by light trapping effect, while still keep the short charge transport path length at the TCO/semiconductor interface. A novel 3-D nanophotonic crystal TCO electrode was synthesized using a 3-D template-assisted and solution-chemistry-based method. The optical and electrical properties of the 3-D photonic crystal FTO electrodes are studied by UV-Vis transmittance spectroscopy, Hall effect and sheet resistance measurement. In addition, an ultrathin TiO2 layer is coated on all surfaces of the IO-FTO electrodes using the atomic layer deposition technique. Cyclic voltammetry study indicates that the resulting TiO2-coated 3-D FTO shows excellent potentials as electrodes for electrolyte-based DSSCs.

Micromorphological characterization of zinc/silver particle composite coatings

PubMed Central

Méndez, Alia; Reyes, Yolanda; Trejo, Gabriel; StĘpień, Krzysztof

2015-01-01

ABSTRACT The aim of this study was to evaluate the three‐dimensional (3D) surface micromorphology of zinc/silver particles (Zn/AgPs) composite coatings with antibacterial activity prepared using an electrodeposition technique. These 3D nanostructures were investigated over square areas of 5 μm × 5 μm by atomic force microscopy (AFM), fractal, and wavelet analysis. The fractal analysis of 3D surface roughness revealed that (Zn/AgPs) composite coatings have fractal geometry. Triangulation method, based on the linear interpolation type, applied for AFM data was employed in order to characterise the surfaces topographically (in amplitude, spatial distribution and pattern of surface characteristics). The surface fractal dimension D f, as well as height values distribution have been determined for the 3D nanostructure surfaces. Microsc. Res. Tech. 78:1082–1089, 2015. © 2015 The Authors published by Wiley Periodicals, Inc. PMID:26500164

Transport Theory for Propagation and Reverberation

DTIC Science & Technology

2016-07-20

mentioned that our transport theory method is essentially 2-D (range and depth), so that out-of- plane forward scattering (a 3-D effect) is not treated...roughness spectrum, it is useful to consider scattering based on perturbation theory in some detail with a plane wave incident on the rough surface. The...the wave vector for the water wave. Let an incident acoustic plane wave have wave vector ki = kiH + kiz, where kiH denotes the horizontal component

Single-scatter vector-wave scattering from surfaces with infinite slopes using the Kirchhoff approximation.

PubMed

Bruce, Neil C

2008-08-01

This paper presents a new formulation of the 3D Kirchhoff approximation that allows calculation of the scattering of vector waves from 2D rough surfaces containing structures with infinite slopes. This type of surface has applications, for example, in remote sensing and in testing or imaging of printed circuits. Some preliminary calculations for rectangular-shaped grooves in a plane are presented for the 2D surface method and are compared with the equivalent 1D surface calculations for the Kirchhoff and integral equation methods. Good agreement is found between the methods.

Resistivity scaling due to electron surface scattering in thin metal layers

NASA Astrophysics Data System (ADS)

Zhou, Tianji; Gall, Daniel

2018-04-01

The effect of electron surface scattering on the thickness-dependent electrical resistivity ρ of thin metal layers is investigated using nonequilibrium Green's function density functional transport simulations. Cu(001) thin films with thickness d =1 -2 nm are used as a model system, employing a random one-monolayer-high surface roughness and frozen phonons to cause surface and bulk scattering, respectively. The zero-temperature resistivity increases from 9.7 ±1.0 μ Ω cm at d =1.99 nm to 18.7 ±2.6 μ Ω cm at d =0.9 0 nm, contradicting the asymptotic T =0 prediction from the classical Fuchs-Sondheimer model. At T =9 00 K, ρ =5.8 ±0.1 μ Ω cm for bulk Cu and ρ =13.4 ±1.1 and 22.5 ±2.4 μ Ω cm for layers with d =1.99 and 0.90 nm, respectively, indicating an approximately additive phonon contribution which, however, is smaller than for bulk Cu or atomically smooth layers. The overall data indicate that the resistivity contribution from surface scattering is temperature-independent and proportional to 1 /d , suggesting that it can be described using a surface-scattering mean-free path λs for 2D transport which is channel-independent and proportional to d . Data fitting indicates λs=4 ×d for the particular simulated Cu(001) surfaces with a one-monolayer-high surface roughness. The 1 /d dependence deviates considerably from previous 1 /d2 predictions from quantum models, indicating that the small-roughness approximation in these models is not applicable to very thin (<2 nm) layers, where the surface roughness is a considerable fraction of d .

The effects of surface gloss and roughness on color constancy for real 3-D objects.

PubMed

Granzier, Jeroen J M; Vergne, Romain; Gegenfurtner, Karl R

2014-02-21

Color constancy denotes the phenomenon that the appearance of an object remains fairly stable under changes in illumination and background color. Most of what we know about color constancy comes from experiments using flat, matte surfaces placed on a single plane under diffuse illumination simulated on a computer monitor. Here we investigate whether material properties (glossiness and roughness) have an effect on color constancy for real objects. Subjects matched the color and brightness of cylinders (painted red, green, or blue) illuminated by simulated daylight (D65) or by a reddish light with a Munsell color book illuminated by a tungsten lamp. The cylinders were either glossy or matte and either smooth or rough. The object was placed in front of a black background or a colored checkerboard. We found that color constancy was significantly higher for the glossy objects compared to the matte objects, and higher for the smooth objects compared to the rough objects. This was independent of the background. We conclude that material properties like glossiness and roughness can have significant effects on color constancy.

Analysis of Flatness Deviations for Austenitic Stainless Steel Workpieces after Efficient Surface Machining

NASA Astrophysics Data System (ADS)

Nadolny, K.; Kapłonek, W.

2014-08-01

The following work is an analysis of flatness deviations of a workpiece made of X2CrNiMo17-12-2 austenitic stainless steel. The workpiece surface was shaped using efficient machining techniques (milling, grinding, and smoothing). After the machining was completed, all surfaces underwent stylus measurements in order to obtain surface flatness and roughness parameters. For this purpose the stylus profilometer Hommel-Tester T8000 by Hommelwerke with HommelMap software was used. The research results are presented in the form of 2D surface maps, 3D surface topographies with extracted single profiles, Abbott-Firestone curves, and graphical studies of the Sk parameters. The results of these experimental tests proved the possibility of a correlation between flatness and roughness parameters, as well as enabled an analysis of changes in these parameters from shaping and rough grinding to finished machining. The main novelty of this paper is comprehensive analysis of measurement results obtained during a three-step machining process of austenitic stainless steel. Simultaneous analysis of individual machining steps (milling, grinding, and smoothing) enabled a complementary assessment of the process of shaping the workpiece surface macro- and micro-geometry, giving special consideration to minimize the flatness deviations

The influence of surface roughness and turbulence on heat fluxes from an oil palm plantation in Jambi, Indonesia

NASA Astrophysics Data System (ADS)

June, Tania; Meijide, Ana; Stiegler, Christian; Purba Kusuma, Alan; Knohl, Alexander

2018-05-01

Oil palm plantations are expanding vastly in Jambi, resulted in altered surface roughness and turbulence characteristics, which may influence exchange of heat and mass. Micrometeorological measurements above oil palm canopy were conducted for the period 2013–2015. The oil palms were 12.5 years old, canopy height 13 meters and 1.5 years old canopy height 2.5 m. We analyzed the influence of surface roughness and turbulence strenght on heat (sensible and latent) fluxes by investigating the profiles and gradient of wind speed, and temperature, surface roughness (roughness length, zo, and zero plane displacement, d), and friction velocity u*. Fluxes of heat were calculated using profile similarity methods taking into account atmospheric stability calculated using Richardson number Ri and the generalized stability factor ζ. We found that roughness parameters (zo, d, and u*) directly affect turbulence in oil palm canopy and hence heat fluxes; they are affected by canopy height, wind speed and atmospheric stability. There is a negative trend of d towards air temperature above the oil palm canopy, indicating the effect of plant volume and height in lowering air temperature. We propose studying the relation between zero plane displacement d with a remote sensing vegetation index for scaling up this point based analysis.

Scattering of electromagnetic waves from a body over a random rough surface

NASA Astrophysics Data System (ADS)

Ripoll, J.; Madrazo, A.; Nieto-Vesperinas, M.

1997-02-01

A numerical study is made of the effect on the angular distribution of mean far field intensity due to the presence of an arbitrary body located over a random rough surface. It is found that the presence of the body decreases the coherent backscattering peak produced by the surface roughness. Also, for low dielectric constants, the reflected intensity is practically equal to the sum of the individual reflected intensities of the body and the surface respectively, namely, interaction between both bodies is almost negligible. The full interaction between object and surface only appears when both bodies are highly reflective. Results are compared with the case when the body is buried beneath the surface, and are illustrated with a 2-D calculation of a cylinder either partially immersed or above a 2-D rough profile.

Surface modification by electrolytic plasma processing for high Nb-TiAl alloys

NASA Astrophysics Data System (ADS)

Gui, Wanyuan; Hao, Guojian; Liang, Yongfeng; Li, Feng; Liu, Xiao; Lin, Junpin

2016-12-01

Metal surface modification by electrolytic plasma processing (EPP) is an innovative treatment widely commonly applied to material processing and pretreatment process of coating and galvanization. EPP involves complex processes and a great deal of parameters, such as preset voltage, current, solution temperature and processing time. Several characterization methods are presented in this paper for evaluating the micro-structure surfaces of Ti45Al8Nb alloys: SEM, EDS, XRD and 3D topography. The results showed that the oxide scale and other contaminants on the surface of Ti45Al8Nb alloys can be effectively removed via EPP. The typical micro-crater structure of the surface of Ti45Al8Nb alloys were observed by 3D topography after EPP to find that the mean diameter of the surface structure and roughness value can be effectively controlled by altering the processing parameters. The mechanical properties of the surface according to nanomechanical probe testing exhibited slight decrease in microhardness and elastic modulus after EPP, but a dramatic increase in surface roughness, which is beneficial for further processing or coating.

Excitation of Crossflow Instabilities in a Swept Wing Boundary Layer

NASA Technical Reports Server (NTRS)

Carpenter, Mark H.; Choudhari, Meelan; Li, Fei; Streett, Craig L.; Chang, Chau-Lyan

2010-01-01

The problem of crossflow receptivity is considered in the context of a canonical 3D boundary layer (viz., the swept Hiemenz boundary layer) and a swept airfoil used recently in the SWIFT flight experiment performed at Texas A&M University. First, Hiemenz flow is used to analyze localized receptivity due to a spanwise periodic array of small amplitude roughness elements, with the goal of quantifying the effects of array size and location. Excitation of crossflow modes via nonlocalized but deterministic distribution of surface nonuniformity is also considered and contrasted with roughness induced acoustic excitation of Tollmien-Schlichting waves. Finally, roughness measurements on the SWIFT model are used to model the effects of random, spatially distributed roughness of sufficiently small amplitude with the eventual goal of enabling predictions of initial crossflow disturbance amplitudes as functions of surface roughness parameters.

Analyzing the Deposition of Titanium Dioxide Nanoparticles at Model Rough Mineral Surfaces Using a Quartz Crystal Microbalance with Dissipation Monitoring

NASA Astrophysics Data System (ADS)

Li, Y.; Kananizadeh, N.; Rodenhausen, K. B.; Schubert, M.; Bartelt-Hunt, S.

2015-12-01

Titanium dioxide nanoparticles (nTiO2) is the most extensively manufactured engineered materials. nTiO2 from sunscreens was found to enter sediments after released into a lake. nTiO2 may also enter the subsurface via irrigation using effluents from wastewater treatment plants. Interaction of nTiO2 with soils and sediments will largely influence their fate, transport, and ecotoxicity. Measuring the interaction between nTiO2 and natural substrates (e.g. such as sands) is particularly challenging due to highly heterogeneous and rough natural sand surfaces. In this study, an engineered controllable rough surface known as three dimensional nanostructured sculptured columnar thin films (SCTFs) has been used to mimic surface roughness. SCTFs were fabricated by glancing angle deposition (GLAD), a physical vapor deposition technique facilitated by electron beam evaporation. Interaction between nTiO2 and SCTF coated surfaces was investigated using a quartz crystal microbalance with dissipation monitoring (QCM-D). In parallel, a Generalized Ellipsometry (GE) was coupled with the QCM-D to measure the deposition of nTiO2. We found that the typical QCM-D modeling approach, e.g. viscoelastic model, would largely overestimate the mass of deposited nTiO2, because the frequency drops due to particle deposition or water entrapment in rough areas were not differentiated. Here, we demonstrate a new approach to model QCM-D data for nTiO2 deposition on rough surfaces, which couples the viscoelastic model with a model of flow on the non-uniform surface.

Effect of surface treatment on stress distribution in immediately loaded dental implants--a 3D finite element analysis.

PubMed

Bahrami, Babak; Shahrbaf, Shirin; Mirzakouchaki, Behnam; Ghalichi, Farzan; Ashtiani, Mohammed; Martin, Nicolas

2014-04-01

To investigate, by means of FE analysis, the effect of surface roughness treatments on the distribution of stresses at the bone-implant interface in immediately loaded mandibular implants. An accurate, high resolution, digital replica model of bone structure (cortical and trabecular components) supporting an implant was created using CT scan data and image processing software (Mimics 13.1; Materialize, Leuven, Belgium). An anatomically accurate 3D model of a mandibular-implant complex was created using a professional 3D-CAD modeller (SolidWorks, DassaultSystèmes Solid Works Corp; 2011). Finite element models were created with one of the four roughness treatments on the implant fixture surface. Of these, three were surface treated to create a uniform coating determined by the coefficient of friction (μ); these were either (1) plasma sprayed or porous-beaded (μ=1.0), (2) sandblasted (μ=0.68) or (3) polished (μ=0.4). The fourth implant had a novel two-part surface roughness consisting of a coronal polished component (μ=0.4) interfacing with the cortical bone, and a body plasma treated surface component (μ=1) interfacing with the trabecular bone. Finite element stress analysis was carried out under vertical and lateral forces. This investigation showed that the type of surface treatment on the implant fixture affects the stress at the bone-implant interface of an immediately loaded implant complex. Von Mises stress data showed that the two-part surface treatment created the better stress distribution at the implant-bone interface. The results from this FE computational analysis suggest that the proposed two-part surface treatment for IL implants creates lower stresses than single uniform treatments at the bone-implant interface, which might decrease peri-implant bone loss. Future investigations should focus on mechanical and clinical validation of these FE results. Copyright © 2014 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Feather roughness reduces flow separation during low Reynolds number glides of swifts.

PubMed

van Bokhorst, Evelien; de Kat, Roeland; Elsinga, Gerrit E; Lentink, David

2015-10-01

Swifts are aerodynamically sophisticated birds with a small arm and large hand wing that provides them with exquisite control over their glide performance. However, their hand wings have a seemingly unsophisticated surface roughness that is poised to disturb flow. This roughness of about 2% chord length is formed by the valleys and ridges of overlapping primary feathers with thick protruding rachides, which make the wing stiffer. An earlier flow study of laminar-turbulent boundary layer transition over prepared swift wings suggested that swifts can attain laminar flow at a low angle of attack. In contrast, aerodynamic design theory suggests that airfoils must be extremely smooth to attain such laminar flow. In hummingbirds, which have similarly rough wings, flow measurements on a 3D printed model suggest that the flow separates at the leading edge and becomes turbulent well above the rachis bumps in a detached shear layer. The aerodynamic function of wing roughness in small birds is, therefore, not fully understood. Here, we performed particle image velocimetry and force measurements to compare smooth versus rough 3D-printed models of the swift hand wing. The high-resolution boundary layer measurements show that the flow over rough wings is indeed laminar at a low angle of attack and a low Reynolds number, but becomes turbulent at higher values. In contrast, the boundary layer over the smooth wing forms open laminar separation bubbles that extend beyond the trailing edge. The boundary layer dynamics of the smooth surface varies non-linearly as a function of angle of attack and Reynolds number, whereas the rough surface boasts more consistent turbulent boundary layer dynamics. Comparison of the corresponding drag values, lift values and glide ratios suggests, however, that glide performance is equivalent. The increased structural performance, boundary layer robustness and equivalent aerodynamic performance of rough wings might have provided small (proto) birds with an evolutionary window to high glide performance. © 2015. Published by The Company of Biologists Ltd.

Roughness and pH changes of enamel surface induced by soft drinks in vitro-applications of stylus profilometry, focus variation 3D scanning microscopy and micro pH sensor.

PubMed

Fujii, Mie; Kitasako, Yuichi; Sadr, Alireza; Tagami, Junji

2011-01-01

This study aimed to evaluate enamel surface roughness (Ra) and pH before and after erosion by soft drinks. Enamel was exposed to a soft drink (cola, orange juice or green tea) for 1, 5 or 60 min; Ra was measured using contact-stylus surface profilometry (SSP) and non-contact focus variation 3D microscope (FVM). Surface pH was measured using a micro pH sensor. Data were analyzed at significance level of alpha=0.05. There was a significant correlation in Ra between SSP and FVM. FVM images showed no changes in the surface morphology after various periods of exposure to green tea. Unlike cola and orange juice, exposure to green tea did not significantly affect Ra or pH. A significant correlation was observed between surface pH and Ra change after exposure to the drinks. Optical surface analysis and micro pH sensor may be useful tools for non-damaging, quantitative assessment of soft drinks erosion on enamel.

Profilometric analysis of two composite resins' surface repolished after tooth brush abrasion with three polishing systems.

PubMed

Uppal, Mudit; Ganesh, Arathi; Balagopal, Suresh; Kaur, Gurleen

2013-07-01

To evaluate the effect of three polishing protocols that could be implemented at recall on the surface roughness of two direct esthetic restorative materials. Specimens (n = 40) measuring 8 mm (length) × 5 mm (width) × 4 mm (height) were fabricated in an acrylic mold using two light-cured resin-based materials (microfilled composite and microhybrid composite). After photopolymerization, all specimens were finished and polished with one of three polishing protocols (Enhance, One Gloss, and Sof-Lex polishing systems). The average surface roughness of each treated specimen was determined using 3D optical profilometer. Next all specimens were brushed 60,000 times with nylon bristles at 7200 rpm using crosshead brushing device with equal parts of toothpaste and water used as abrasive medium. The surface roughness of each specimen was measured after brushing followed by repolishing with one of three polishing protocols, and then, the final surface roughness values were determined. The data were analyzed using one-way and two-factor analysis of variance (ANOVA) and Tukey's honestly significant difference (HSD). Significant difference (P < 0.05) in surface roughness was observed. Simulated brushing following initial polishing procedure significantly roughened the surface of restorative material (P < 0.05). Polishing protocols can be used to restore a smooth surface on esthetic restorative materials following simulated tooth brushing.

Near-field flow structures about subcritical surface roughness

NASA Astrophysics Data System (ADS)

Doolittle, Charles J.; Drews, Scott D.; Goldstein, David B.

2014-12-01

Laminar flow over a periodic array of cylindrical surface roughness elements is simulated with an immersed boundary spectral method both to validate the method for subsequent studies and to examine how persistent streamwise vortices are introduced by a low Reynolds number roughness element. Direct comparisons are made with prior studies at a roughness-based Reynolds number Rek (=U(k) k/ν) of 205 and a diameter to spanwise spacing ratio d/λ of 1/3. Downstream velocity contours match present and past experiments very well. The shear layer developed over the top of the roughness element produces the downstream velocity deficit. Upstream of the roughness element, the vortex topology is found to be consistent with juncture flow experiments, creating three cores along the recirculation line. Streamtraces stemming from these upstream cores, however, have unexpectedly little effect on the downstream flowfield as lateral divergence of the boundary layer quickly dissipates their vorticity. Long physical relaxation time of the recirculating wake behind the roughness remains a prominent issue for simulating this type of flowfield.

The Effects of Acid Etching on the Nanomorphological Surface Characteristics and Activation Energy of Titanium Medical Materials

PubMed Central

Hung, Kuo-Yung; Lin, Yi-Chih; Feng, Hui-Ping

2017-01-01

The purpose of this study was to characterize the etching mechanism, namely, the etching rate and the activation energy, of a titanium dental implant in concentrated acid and to construct the relation between the activation energy and the nanoscale surface topographies. A commercially-pure titanium (CP Ti) and Ti-6Al-4V ELI surface were tested by shot blasting (pressure, grain size, blasting distance, blasting angle, and time) and acid etching to study its topographical, weight loss, surface roughness, and activation energy. An Arrhenius equation was applied to derive the activation energy for the dissolution of CP Ti/Ti-6Al-4V ELI in sulfuric acid (H2SO4) and hydrochloric acid (HCl) at different temperatures. In addition, white-light interferometry was applied to measure the surface nanomorphology of the implant to obtain 2D or 3D roughness parameters (Sa, Sq, and St). The nanopore size that formed after etching was approximately 100–500 nm. The surface roughness of CP Ti and Ti-6Al-4V ELI decreased as the activation energy decreased but weight loss increased. Ti-6Al-4V ELI has a higher level of activation energy than Ti in HCl, which results in lower surface roughness after acid etching. This study also indicates that etching using a concentrated hydrochloric acid provided superior surface modification effects in titanium compared with H2SO4. PMID:29019926

Evaluation of Rock Surface Characterization by Means of Temperature Distribution

NASA Astrophysics Data System (ADS)

Seker, D. Z.; Incekara, A. H.; Acar, A.; Kaya, S.; Bayram, B.; Sivri, N.

2017-12-01

Rocks have many different types which are formed over many years. Close range photogrammetry is a techniques widely used and preferred rather than other conventional methods. In this method, the photographs overlapping each other are the basic data source of the point cloud data which is the main data source for 3D model that provides analysts automation possibility. Due to irregular and complex structures of rocks, representation of their surfaces with a large number points is more effective. Color differences caused by weathering on the rock surfaces or naturally occurring make it possible to produce enough number of point clouds from the photographs. Objects such as small trees, shrubs and weeds on and around the surface also contribute to this. These differences and properties are important for efficient operation of pixel matching algorithms to generate adequate point cloud from photographs. In this study, possibilities of using temperature distribution for interpretation of roughness of rock surface which is one of the parameters representing the surface, was investigated. For the study, a small rock which is in size of 3 m x 1 m, located at ITU Ayazaga Campus was selected as study object. Two different methods were used. The first one is production of producing choropleth map by interpolation using temperature values of control points marked on object which were also used in 3D model. 3D object model was created with the help of terrestrial photographs and 12 control points marked on the object and coordinated. Temperature value of control points were measured by using infrared thermometer and used as basic data source in order to create choropleth map with interpolation. Temperature values range from 32 to 37.2 degrees. In the second method, 3D object model was produced by means of terrestrial thermal photographs. Fort this purpose, several terrestrial photographs were taken by thermal camera and 3D object model showing temperature distribution was created. The temperature distributions in both applications are almost identical in position. The areas on the rock surface that roughness values are higher than the surroundings can be clearly identified. When the temperature distributions produced by both methods are evaluated, it is observed that as the roughness on the surface increases, the temperature increases.

Deviation characteristics of specular reflectivity of micro-rough surface from Fresnel's equation

NASA Astrophysics Data System (ADS)

Zhang, W. J.; Qiu, J.; Liu, L. H.

2015-07-01

Specular reflectivity is an important radiative property in thermal engineering applications and reflection-based optical constant determinations, yet it will be influenced by surface micro-roughness which cannot be completely removed during the polishing process. In this work, we examined the deviation characteristics of the specular reflectivity of micro-rough surfaces from that predicted by the Fresnel's equation under the assumption of smooth surface. The effects of incident angle and relative roughness were numerically investigated for both 1D and 2D micro randomly rough surfaces using full wave analysis under the condition that the relative roughness is smaller than 0.05. For transverse magnetic (TM) wave incidence, it is observed that the deviation of specular reflectivity dramatically rises as the incident angle approaches to the pseudo Brewster's angle, which violates the prediction based on Rayleigh criterion. While for the transverse electric (TE) wave incidence, the deviation of the specular reflectivity is much smaller and decreases monotonically with the increase of incident angle, which agrees with the predication from Rayleigh criterion. Generally, the deviation of specular reflectivity for both TM and TE increases with the relative roughness as commonly expected.

Laser polishing of additive manufactured Ti alloys

NASA Astrophysics Data System (ADS)

Ma, C. P.; Guan, Y. C.; Zhou, W.

2017-06-01

Laser-based additive manufacturing has attracted much attention as a promising 3D printing method for metallic components in recent years. However, surface roughness of additive manufactured components has been considered as a challenge to achieve high performance. In this work, we demonstrate the capability of fiber laser in polishing rough surface of additive manufactured Ti-based alloys as Ti-6Al-4V and TC11. Both as-received surface and laser-polished surfaces as well as cross-section subsurfaces were analyzed carefully by White-Light Interference, Confocal Microscope, Focus Ion Beam, Scanning Electron Microscopy, Energy Dispersive Spectrometer, and X-ray Diffraction. Results revealed that as-received Ti-based alloys with surface roughness more than 5 μm could be reduce to less than 1 μm through laser polishing process. Moreover, microstructure, microhardness and wear resistance of laser-polished zone was investigated in order to examine the thermal effect of laser polishing processing on the substrate of additive manufactured Ti alloys. This proof-of-concept process has the potential to effectively improve the surface roughness of additive manufactured metallic alloy by local polishing method without damage to the substrate.

Effects of plaque lengths on stent surface roughness.

PubMed

Syaifudin, Achmad; Takeda, Ryo; Sasaki, Katsuhiko

2015-01-01

The physical properties of the stent surface influence the effectiveness of vascular disease treatment after stent deployment. During the expanding process, the stent acquires high-level deformation that could alter either its microstructure or the magnitude of surface roughness. This paper constructed a finite element simulation to observe the changes in surface roughness during the stenting process. Structural transient dynamic analysis was performed using ANSYS, to identify the deformation after the stent is placed in a blood vessel. Two types of bare metal stents are studied: a Palmaz type and a Sinusoidal type. The relationship between plaque length and the changes in surface roughness was investigated by utilizing three different length of plaque; plaque length longer than the stent, shorter than the stent and the same length as the stent. In order to reduce computational time, 3D cyclical and translational symmetry was implemented into the FE model. The material models used was defined as a multilinear isotropic for stent and hyperelastic for the balloon, plaque and vessel wall. The correlation between the plastic deformation and the changes in surface roughness was obtained by intermittent pure tensile test using specimen whose chemical composition was similar to that of actual stent material. As the plastic strain is achieved from FE simulation, the surface roughness can be assessed thoroughly. The study found that the plaque size relative to stent length significantly influenced the critical changes in surface roughness. It was found that the length of stent which is equal to the plaque length was preferable due to the fact that it generated only moderate change in surface roughness. This effect was less influential to the Sinusoidal stent.

The Effect of Humidity and Particle Characteristics on Friction and Stick-slip Instability in Granular Fault Gouge

NASA Astrophysics Data System (ADS)

Anthony, J. L.; Marone, C. J.

2003-12-01

Previous studies have shown that particle characteristics such as shape, dimension, and roughness affect friction in granular shear zones. Other work shows that humidity plays a key role in frictional healing and rate/state dependence within granular gouge. In order to improve our understanding of grain-scale deformation mechanisms within fault gouge, we performed laboratory experiments using a double-direct-shear testing apparatus. This assembly includes three rigid forcing blocks with two gouge layers sandwiched between rough or smooth surfaces. Roughened surfaces were triangular grooves 0.8 mm deep and 1 mm wavelength. These promote distributed shear throughout the layer undergoing cataclastic deformation. Smooth surfaces were mirror-finished hardened steel and were used to promote and isolate grain boundary sliding. The center block is forced at controlled displacement rate between the two side blocks to create frictional shear. We studied gouge layers 3-7 mm thick, consisting of either quartz rods sheared in 1-D and 2-D configurations and smooth glass beads mixed with varying amounts of rough sand particles. We report on particle diameters that range from 0.050-0.210 mm, and quartz rods 1 mm in diameter and 100 mm long. The experiments are run at room temperature, controlled relative humidity ranging from 5 to 100%, and shear displacement rates from 0.1 to 300 microns per second. Experiments are carried out under a normal stress of 5 MPa, a non-fracture loading regime where sliding friction for smooth spherical particles is measurably lower than for rough angular particles. We compare results from shear between smooth boundaries, where we hypothesize that grain boundary sliding is the mechanism influencing granular friction, to rough sample experiments where shear undergoes a transition from distributed, pervasive shear to progressively localized as a function of increasing strain. For shear within rough surfaces, stick-slip instability occurs in gouge that consists of less than 30% angular grains and begins once the coefficient of friction (shear stress divided by normal stress) reaches a value of 0.35-0.40. Peak friction during stick-slip cycles is 0.40-0.45. Each stick-slip event involves a small amount of quasi-static displacement prior to failure, which we refer to as pre-seismic slip. For unstable sliding regimes, we measure the amount of pre-seismic slip and the magnitude of dynamic stress drop. These parameters vary systematically with sliding velocity, particle characteristics, and bounding roughness. For shear within smooth surfaces, friction is very low (0.15-0.16 for spherical particles) and sliding is stable, without stick-slip instability. As more angular grains are mixed with spherical beads the coefficient of friction increases. This holds true for both the rough and smooth sample experiments. We expand on previous work done by Frye and Marone 2002 (JGR) to study the effect of humidity on 1-D, 2-D, and 3-D gouge layer configurations. Our data show that humidity has a significant effect on frictional strength and stability and that this effect is observed for both smooth surfaces, where grain boundary sliding is the dominant deformation mechanisms, and for shear within rough surfaces where gouge deformation occurs by rolling, dilation, compaction, and grain boundary sliding.

Surface wettability of silicon substrates enhanced by laser ablation

NASA Astrophysics Data System (ADS)

Tseng, Shih-Feng; Hsiao, Wen-Tse; Chen, Ming-Fei; Huang, Kuo-Cheng; Hsiao, Sheng-Yi; Lin, Yung-Sheng; Chou, Chang-Pin

2010-11-01

Laser-ablation techniques have been widely applied for removing material from a solid surface using a laser-beam irradiating apparatus. This paper presents a surface-texturing technique to create rough patterns on a silicon substrate using a pulsed Nd:YAG laser system. The different degrees of microstructure and surface roughness were adjusted by the laser fluence and laser pulse duration. A scanning electron microscope (SEM) and a 3D confocal laser-scanning microscope are used to measure the surface micrograph and roughness of the patterns, respectively. The contact angle variations between droplets on the textured surface were measured using an FTA 188 video contact angle analyzer. The results indicate that increasing the values of laser fluence and laser pulse duration pushes more molten slag piled around these patterns to create micro-sized craters and leads to an increase in the crater height and surface roughness. A typical example of a droplet on a laser-textured surface shows that the droplet spreads very quickly and almost disappears within 0.5167 s, compared to a contact angle of 47.9° on an untextured surface. This processing technique can also be applied to fabricating Si solar panels to increase the absorption efficiency of light.

Pre-polishing on a CNC platform with bound abrasive contour tools

NASA Astrophysics Data System (ADS)

Schoeffer, Adrienne E.

2003-05-01

Deterministic micorgrinding (DMG) of optical glasses and ceramics is the commercial manufacturing process of choice to shape glass surfaces prior to final finishing. This process employs rigid bound matrix diamond tooling resulting in surface roughness values of 3-51.tm peak to valley and 100-400nm rms, as well as mid-spatial frequency tool marks that require subsequent removal in secondary finishing steps. The ability to pre-polish optical surfaces within the grinding platform would reduce final finishing process times. Bound abrasive contour wheels containing cerium oxide, alumina or zirconia abrasives were constructed with an epoxy matrix. The effects of abrasive type, composition, and erosion promoters were examined for tool hardness (Shore D), and tested with commercial optical glasses in an OptiproTM CNC grinding platform. Metrology protocols were developed to examine tool wear and subsequent surface roughness. Work is directed to demonstrating effective material removal, improved surface roughness and cutter mark removal.

Prepolishing on a CNC platform with bound abrasive contour tools

NASA Astrophysics Data System (ADS)

Schoeffler, Adrienne E.; Gregg, Leslie L.; Schoen, John M.; Fess, Edward M.; Hakiel, Michael; Jacobs, Stephen D.

2003-05-01

Deterministic microgrinding (DMG) of optical glasses and ceramics is the commercial manufacturing process of choice to shape glass surfaces prior to final finishing. This process employs rigid bound matrix diamond tooling resulting in surface roughness values of 3-5μm peak to valley and 100-400nm rms, as well as mid-spatial frequency tool marks that require subsequent removal in secondary finishing steps. The ability to pre-polish optical surfaces within the grinding platform would reduce final finishing process times. Bound abrasive contour wheels containing cerium oxide, alumina or zirconia abrasives were constructed with an epoxy matrix. The effects of abrasive type, composition, and erosion promoters were examined for tool hardness (Shore D), and tested with commercial optical glasses in an Optipro CNC grinding platform. Metrology protocols were developed to examine tool wear and subsequent surface roughness. Work is directed to demonstrating effective material removal, improved surface roughness and cutter mark removal.

Lotus LADM Based Self-Decontaminating Surfaces

DTIC Science & Technology

2007-05-01

nylon composite was examined with a scanning electron microscope (SEM), Hitachi S -3200N, operated at 10kV and magnifications from 50x to 2000x. For...cos1( HL H S p L p S d L d SeL γγγγγγθγ ⋅+⋅+⋅=+ (1) To make the nylon film surface hydrophobic, we need to attach a low surface tension material to...views of roughness pattern. For this rough surface, r and ФS are defined as: ( ) 1 2 2 2 ++ = dR Rhr π (4) ( )2 2 2 dR R S + =Φ π (5

Near Wall measurement in Turbulent Flow over Rough Wall using microscopic HPIV

NASA Astrophysics Data System (ADS)

Talapatra, Siddharth; Hong, Jiarong; Katz, Joseph

2009-11-01

Using holographic PIV, 3D velocity measurements are being performed in a turbulent rough wall channel flow. Our objective is to examine the contribution of coherent structures to the flow dynamics, momentum and energy fluxes in the roughness sublayer. The 0.45mm high, pyramid-shaped roughness is uniformly distributed on the top and bottom surfaces of a 5X20cm rectangular channel flow, where the Reτ is 3400. To facilitate recording of holograms through a rough plate, the working fluid is a concentrated solution of NaI in water, whose optical refractive index is matched with that of the acrylic rough plates. The test section is illuminated by a collimated laser beam from the top, and the sample volume extends from the bottom wall up to 7 roughness heights. After passing through the sample volume, the in-line hologram is magnified and recorded on a 4864X3248 pixels camera at a resolution of 0.74μm/pixel. The flow is locally seeded with 2μm particles. Reconstruction, spatial filtering and particle tracking provide the 3D velocity field. This approach has been successfully implemented recently, as preliminary data demonstrate.

Development of 70/30 Poly-L-DL-Lactic Acid Filaments for 3D Printers (Part 2): Mechanical and Surface Properties of Bioabsorbable Printed Plates for Biomedical Applications

NASA Astrophysics Data System (ADS)

Fernandes, Daniel J.; Vidal, Rafael; Assayag, Ariel; de Biasi, Ronaldo S.; Elias, Carlos N.

2017-01-01

The mechanical, chemical, roughness and wettability properties of 70/30 poly (L,DL-lactide acid) three-dimensional (3D)-printed surgical plates made with extruded polymer filaments developed in the first part of this work were investigated. The plates were printed with horizontal (HRZ) and vertical (VRT) running layer orientations and evaluated by tensile, Fourier transform infrared (FTIR), optical perfilometry and wettability tests before and after degradation in simulated body fluid (SBF) for 21 days. The results show that the ultimate tensile strength (UTS) of HRZ plates before immersion in SBF was higher (34.1 MPa) than that of VRT plates (31.8 MPa). The Young's modulus ( E) of HRZ plates and VRT plates are similar (4 GPa). After immersion in SBF, the UTS of HRZ plates dropped to 20.5 MPa and E decreased to 3.3 GPa. VRT were not tested after SBF immersion due to the large degradation. FTIR analysis showed no evidence of chemical change in the plates after immersion in SBF. The roughness parameter R3z of VRT surfaces (19.54 µm) was higher than that of the HRZ surfaces (12.80 µm). The roughness parameters increased after degradation in SBF ( p = 0.7048). The contact angles of HRZ surfaces before immersion in SBF (66.28°) were higher than after immersion in SBF (18.12°); the same behavior was also observed in VRT plates.

Oxygen and nitrogen plasma etching of three-dimensional hydroxyapatite/chitosan scaffolds fabricated by additive manufacturing

NASA Astrophysics Data System (ADS)

Myung, Sung-Woon; Kim, Byung-Hoon

2016-01-01

Three-dimensional (3D) chitosan and hydroxyapatite (HAp)/chitosan (CH) scaffolds were fabricated by additive manufacturing, then their surfaces were etched with oxygen (O2) and nitrogen (N2) plasma. O2 and N2 plasma etching was performed to increase surface properties such as hydrophilicity, roughness, and surface chemistry on the scaffolds. After etching, hydroxyapatite was exposed on the surface of 3D HAp/CH scaffolds. The surface morphology and chemical properties were characterized by contact angle measurement, scanning electron microscopy, X-ray diffraction, and attenuated total reflection Fourier infrared spectroscopy. The cell viability of 3D chitosan scaffolds was examined by 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide assay. The differentiation of preosteoblast cells was evaluated by alkaline phosphatase assay. The cell viability was improved by O2 and N2 plasma etching of 3D chitosan scaffolds. The present fabrication process for 3D scaffolds might be applied to a potential tool for preparing biocompatible scaffolds.

3D-printing zirconia implants; a dream or a reality? An in-vitro study evaluating the dimensional accuracy, surface topography and mechanical properties of printed zirconia implant and discs.

PubMed

Osman, Reham B; van der Veen, Albert J; Huiberts, Dennis; Wismeijer, Daniel; Alharbi, Nawal

2017-11-01

The aim of this study was to evaluate the dimensional accuracy, surface topography of a custom designed, 3D-printed zirconia dental implant and the mechanical properties of printed zirconia discs. A custom designed implant was 3D-printed in zirconia using digital light processing technique (DLP). The dimensional accuracy was assessed using the digital-subtraction technique. The mechanical properties were evaluated using biaxial flexure strength test. Three different build angles were adopted to print the specimens for the mechanical test; 0°(Vertical), 45° (Oblique) and 90°(Horizontal) angles. The surface topography, crystallographic phase structure and surface roughness were evaluated using scanning electron microscopy analysis (SEM), X-ray diffractometer and confocal microscopy respectively. The printed implant was dimensionally accurate with a root mean square (RMSE) value of 0.1mm. The Weibull analysis revealed a statistically significant higher characteristic strength (1006.6MPa) of 0° printed specimens compared to the other two groups and no significant difference between 45° (892.2MPa) and 90° (866.7MPa) build angles. SEM analysis revealed cracks, micro-porosities and interconnected pores ranging in size from 196nm to 3.3µm. The mean Ra (arithmetic mean roughness) value of 1.59µm (±0.41) and Rq (root mean squared roughness) value of 1.94µm (±0.47) was found. A crystallographic phase of primarily tetragonal zirconia typical of sintered Yttria tetragonal stabilized zirconia (Y-TZP) was detected. DLP prove to be efficient for printing customized zirconia dental implants with sufficient dimensional accuracy. The mechanical properties showed flexure strength close to those of conventionally produced ceramics. Optimization of the 3D-printing process parameters is still needed to improve the microstructure of the printed objects. Copyright © 2017 Elsevier Ltd. All rights reserved.

Slippery surfaces of pitcher plants: Nepenthes wax crystals minimize insect attachment via microscopic surface roughness.

PubMed

Scholz, I; Bückins, M; Dolge, L; Erlinghagen, T; Weth, A; Hischen, F; Mayer, J; Hoffmann, S; Riederer, M; Riedel, M; Baumgartner, W

2010-04-01

Pitcher plants of the genus Nepenthes efficiently trap and retain insect prey in highly specialized leaves. Besides a slippery peristome which inhibits adhesion of insects they employ epicuticular wax crystals on the inner walls of the conductive zone of the pitchers to hamper insect attachment by adhesive devices. It has been proposed that the detachment of individual crystals and the resulting contamination of adhesive organs is responsible for capturing insects. However, our results provide evidence in favour of a different mechanism, mainly based on the stability and the roughness of the waxy surface. First, we were unable to detect a large quantity of crystal fragments on the pads of insects detached from mature pitcher surfaces of Nepenthes alata. Second, investigation of the pitcher surface by focused ion beam treatment showed that the wax crystals form a compact 3D structure. Third, atomic force microscopy of the platelet-shaped crystals revealed that the crystals are mechanically stable, rendering crystal detachment by insect pads unlikely. Fourth, the surface profile parameters of the wax layer showed striking similarities to those of polishing paper with low grain size. By measuring friction forces of insects on this artificial surface we demonstrate that microscopic roughness alone is sufficient to minimize insect attachment. A theoretical model shows that surface roughness within a certain length scale will prevent adhesion by being too rough for adhesive pads but not rough enough for claws.

Dwell Time and Surface Parameter Effects on Removal of Silicone Oil From D6ac Steel Using TCA

NASA Technical Reports Server (NTRS)

Boothe, R. E.

2003-01-01

This study was conducted to evaluate the impact of dwell time, surface roughness, and the surface activation state on 1,1,1-trichloroethane's (TCA's) effectiveness for removing silicone oil from D6ac steel. Silicone-contaminated test articles were washed with TCA solvent, and then the surfaces were analyzed for residue, using Fourier transform infrared spectroscopy. The predominant factor affecting the ability to remove the silicone oil was surface roughness.

Multiscale analysis of replication technique efficiency for 3D roughness characterization of manufactured surfaces

NASA Astrophysics Data System (ADS)

Jolivet, S.; Mezghani, S.; El Mansori, M.

2016-09-01

The replication of topography has been generally restricted to optimizing material processing technologies in terms of statistical and single-scale features such as roughness. By contrast, manufactured surface topography is highly complex, irregular, and multiscale. In this work, we have demonstrated the use of multiscale analysis on replicates of surface finish to assess the precise control of the finished replica. Five commercial resins used for surface replication were compared. The topography of five standard surfaces representative of common finishing processes were acquired both directly and by a replication technique. Then, they were characterized using the ISO 25178 standard and multiscale decomposition based on a continuous wavelet transform, to compare the roughness transfer quality at different scales. Additionally, atomic force microscope force modulation mode was used in order to compare the resins’ stiffness properties. The results showed that less stiff resins are able to replicate the surface finish along a larger wavelength band. The method was then tested for non-destructive quality control of automotive gear tooth surfaces.

Effect of Experimental Variables of Abrasive Wear on 3D Surface Roughness and Wear Rate of Al-4.5 % Cu Alloy

NASA Astrophysics Data System (ADS)

Ghosh, Debashis; Mallik, Manab; Mandal, Nilrudra; Dutta, Samik; Roy, Himadri; Lohar, Aditya Kumar

2017-04-01

This investigation was primarily carried out to examine the abrasive wear behavior of as cast Al-4.5 % Cu alloy. Wear tests have been carried out using an abrasive wear machine with emery paper embedded with SiC particles acting as abrasive medium. The experiments were planned using central composite design, with, load, cycle and grit size as input variables, whereas wear rate and 3D roughness were considered as output variable. Analysis of variance was applied to check the adequacy of the mathematical model and their respective parameters. Microstructural investigations of the worn surfaces have been carried out to explain the observed results and to understand the wear micro-mechanisms as per the planned experiments. Desirability function optimization technique was finally employed to optimize the controlling factors. The observed results revealed that, grit size plays a significant role in the variation of wear rate and 3D roughness as compared to load and cycles. Based on the significance of interactions, the regression equations were derived and verified further with a number of confirmation runs to assess the adequacy of the model. A close agreement (±10 %) between the predicted and experimentally measured results was obtained from this investigation.

Radiative Transfer Model for Contaminated Rough Surfaces

DTIC Science & Technology

2013-02-01

grey). Right: reconstructed 3D BRDF . ........................................................ 14 Figure 6. Results of fitting the decay model to...in Section 3.2.5 and 4.2.2 that the decay model can allow the use of auxiliary H0 measurements. 2.2 RESULTS 2.2.1 BRDF FOR GOLD AND ALUMINUM Our...Reflectance Angle () R ef le ct an ce Meas. BRDF Lambertian 15 Figure 6. Results of fitting the decay model to angular reflectance for rough aluminum

The effect of bed roughness on the free surface of an open channel flow and implications for remotely monitoring river discharge

NASA Astrophysics Data System (ADS)

Johnson, Erika; Cowen, Edwin

2013-11-01

The effect of increased bed roughness on the free surface turbulence signature of an open channel flow is investigated with the goal of incorporating the findings into a methodology to remotely monitor volumetric flow rates. Half of a wide (B = 2 m) open channel bed is covered with a 3 cm thick layer of loose gravel (D50 = 0.6 cm). Surface PIV (particle image velocimetry) experiments are conducted for a range of flow depths (B/H = 10-30) and Reynolds numbers (ReH = 10,000-60,000). It is well established that bed roughness in wall-bounded flows enhances the vertical velocity fluctuations (e.g. Krogstad et al. 1992). When the vertical velocity fluctuations approach the free surface they are redistributed (e.g. Cowen et al. 1995) to the surface parallel component directions. It is anticipated and confirmed that the interaction of these two phenomena result in enhanced turbulence at the free surface. The effect of the rough bed on the integral length scales and the second order velocity structure functions calculated at the free surface are investigated. These findings have important implications for developing new technologies in stream gaging.

The effect of glazing and aging on the surface properties of CAD/CAM resin blocks

PubMed Central

Tuncer, Safa; Kara, Dilan; Demirci, Mustafa

2018-01-01

PURPOSE To investigate the effect of accelerated aging on surface properties of glazed CAD/CAM resin blocks using a 2D surface profilometer and a 3D non-contact optical profilometer. MATERIALS AND METHODS Three types of CAD/CAM resin restorative materials, LAVA Ultimate (3M ESPE, St Paul, MN, USA), VITA Enamic (Vita Zahnfabrik H. Rauter, Bad Säckingen, Germany), and Cerasmart (GC Corparation, Tokyo, Japan) were used for this study. CAD/CAM blocks were cut in 3-mm thickness slabs and divided into three groups; Group 1: control group (specimens polished with 600 grit SCI paper); Group 2: specimens sandblasted, silanized, and glazed with Optiglaze Color (GC); Group 3: glazed specimens subjected to 5000 thermocycles (n=15). The surface roughness (Ra and Rz) was evaluated using a profilometer and a 3D scanning instrument. Data were analyzed using two-way ANOVA and Tukey's post-hoc test (P<.05). RESULTS LAVA, VITA, and Cerasmart exhibited statistically similar Ra and Rz values for each group (P>.05). For VITA and Cerasmart, the specimens in Group 1 exhibited significantly higher Ra values than Group 2 (P<.05). Group 1 (0.502 Ra), Group 2 (0.384 Ra), and Group 3 (0.431 Ra) exhibited statistically similar Ra values for LAVA (P=.062). After 5000 thermocycles, surface roughness values did not change significantly for glazed LAVA, VITA, and Cerasmart (P>.05). CONCLUSION Glaze material Optiglaze Color makes CAD/CAM resin surfaces smooth and glazed CAD/CAM surfaces seem resistant to deterioration under 5000 thermocycles. PMID:29503714

The effect of glazing and aging on the surface properties of CAD/CAM resin blocks.

PubMed

Tekçe, Neslihan; Fidan, Sinan; Tuncer, Safa; Kara, Dilan; Demirci, Mustafa

2018-02-01

To investigate the effect of accelerated aging on surface properties of glazed CAD/CAM resin blocks using a 2D surface profilometer and a 3D non-contact optical profilometer. Three types of CAD/CAM resin restorative materials, LAVA Ultimate (3M ESPE, St Paul, MN, USA), VITA Enamic (Vita Zahnfabrik H. Rauter, Bad Säckingen, Germany), and Cerasmart (GC Corparation, Tokyo, Japan) were used for this study. CAD/CAM blocks were cut in 3-mm thickness slabs and divided into three groups; Group 1: control group (specimens polished with 600 grit SCI paper); Group 2: specimens sandblasted, silanized, and glazed with Optiglaze Color (GC); Group 3: glazed specimens subjected to 5000 thermocycles (n=15). The surface roughness (R a and R z ) was evaluated using a profilometer and a 3D scanning instrument. Data were analyzed using two-way ANOVA and Tukey's post-hoc test ( P <.05). LAVA, VITA, and Cerasmart exhibited statistically similar R a and R z values for each group ( P >.05). For VITA and Cerasmart, the specimens in Group 1 exhibited significantly higher R a values than Group 2 ( P <.05). Group 1 (0.502 R a ), Group 2 (0.384 R a ), and Group 3 (0.431 R a ) exhibited statistically similar R a values for LAVA ( P =.062). After 5000 thermocycles, surface roughness values did not change significantly for glazed LAVA, VITA, and Cerasmart ( P >.05). Glaze material Optiglaze Color makes CAD/CAM resin surfaces smooth and glazed CAD/CAM surfaces seem resistant to deterioration under 5000 thermocycles.

Combined active and passive microwave remote sensing of vegetated surfaces at l-band

USDA-ARS?s Scientific Manuscript database

In previous work the distorted Born approximation (DBA) of volume scattering was combined with the numerical solutions of Maxwell equations (NMM3D) for a rough surface to calculate the radar backscattering coefficient for the Soil Moisture Active Passive (SMAP) mission. The model results were valida...

Collisions of ideal gas molecules with a rough/fractal surface. A computational study.

PubMed

Panczyk, Tomasz

2007-02-01

The frequency of collisions of ideal gas molecules (argon) with a rough surface has been studied. The rough/fractal surface was created using random deposition technique. By applying various depositions, the roughness of the surface was controlled and, as a measure of the irregularity, the fractal dimensions of the surfaces were determined. The surfaces were next immersed in argon (under pressures 2 x 10(3) to 2 x 10(5) Pa) and the numbers of collisions with these surfaces were counted. The calculations were carried out using a simplified molecular dynamics simulation technique (only hard core repulsions were assumed). As a result, it was stated that the frequency of collisions is a linear function of pressure for all fractal dimensions studied (D = 2, ..., 2.5). The frequency per unit pressure is quite complex function of the fractal dimension; however, the changes of that frequency with the fractal dimension are not strong. It was found that the frequency of collisions is controlled by the number of weakly folded sites on the surfaces and there is some mapping between the shape of adsorption energy distribution functions and this number of weakly folded sites. The results for the rough/fractal surfaces were compared with the prediction given by the Langmuir-Hertz equation (valid for smooth surface), generally the departure from the Langmuir-Hertz equation is not higher than 48% for the studied systems (i.e. for the surfaces created using the random deposition technique).

Analysis of turbulent heat and momentum transfer in a transitionally rough turbulent boundary layer

NASA Astrophysics Data System (ADS)

Doosttalab, Ali; Dharmarathne, Suranga; Tutkun, Murat; Adrian, Ronald; Castillo, Luciano

2016-11-01

A zero-pressure-gradient (ZPG) turbulent boundary layer over a transitionally rough surface is studied using direct numerical simulation (DNS). The rough surface is modeled as 24-grit sandpaper which corresponds to k+ 11 , where k+ is roughness height. Reynolds number based on momentum thickness is approximately 2400. The walls are isothermal and turbulent flow Prandtl number is 0.71. We simulate temperature as passive scalar. We compute the inner product of net turbulent force (d (u1ui) / dxi) and net turbulent heat flux (d (ui θ / dxi)) in order to investigate (i) the correlation between these vectorial quantities, (II) size of the projection of these fields on each other and (IIi) alignment of momentum and hear flux. The inner product in rough case results in larger projection and better alignment. In addition, our study on the vortices shows that surface roughness promotes production of vortical structures which affects the thermal transport near the wall.

Joint properties of a tool machining process to guarantee fluid-proof abilities

NASA Astrophysics Data System (ADS)

Bataille, C.; Deltombe, R.; Jourani, A.; Bigerelle, M.

2017-12-01

This study addressed the impact of rod surface topography in contact with reciprocating seals. Rods were tooled with and without centreless grinding. All rods tooled with centreless grinding were fluid-proof, in contrast to rods tooled without centreless grinding that either had leaks or were fluid-proof. A method was developed to analyse the machining signature, and the software Mesrug™ was used in order to discriminate roughness parameters that can be used to characterize the sealing functionality. According to this surface roughness analysis, a fluid-proof rod tooled without centreless grinding presents aperiodic large plateaus, and the relevant roughness parameter for characterizing the sealing functionality is the density of summits S DS. Increasing the density of summits counteracts leakage, which may be because motif decomposition integrates three topographical components: circularity (perpendicular long-wave roughness), longitudinal waviness, and roughness thanks to the Wolf pruning algorithm. A 3D analytical contact model was applied to analyse the contact area of each type of sample with the seal surface. This model provides a leakage probability, and the results were consistent with the interpretation of the topographical analysis.

High-Speed 3D Printing of Millimeter-Size Customized Aspheric Imaging Lenses with Sub 7 nm Surface Roughness.

PubMed

Chen, Xiangfan; Liu, Wenzhong; Dong, Biqin; Lee, Jongwoo; Ware, Henry Oliver T; Zhang, Hao F; Sun, Cheng

2018-05-01

Advancements in three-dimensional (3D) printing technology have the potential to transform the manufacture of customized optical elements, which today relies heavily on time-consuming and costly polishing and grinding processes. However the inherent speed-accuracy trade-off seriously constrains the practical applications of 3D-printing technology in the optical realm. In addressing this issue, here, a new method featuring a significantly faster fabrication speed, at 24.54 mm 3 h -1 , without compromising the fabrication accuracy required to 3D-print customized optical components is reported. A high-speed 3D-printing process with subvoxel-scale precision (sub 5 µm) and deep subwavelength (sub 7 nm) surface roughness by employing the projection micro-stereolithography process and the synergistic effects from grayscale photopolymerization and the meniscus equilibrium post-curing methods is demonstrated. Fabricating a customized aspheric lens 5 mm in height and 3 mm in diameter is accomplished in four hours. The 3D-printed singlet aspheric lens demonstrates a maximal imaging resolution of 373.2 lp mm -1 with low field distortion less than 0.13% across a 2 mm field of view. This lens is attached onto a cell phone camera and the colorful fine details of a sunset moth's wing and the spot on a weevil's elytra are captured. This work demonstrates the potential of this method to rapidly prototype optical components or systems based on 3D printing. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Quantification of tillage, plant cover, and cumulative rainfall effects on soil surface microrelief by statistical, geostatistical and fractal indices

NASA Astrophysics Data System (ADS)

Paz-Ferreiro, J.; Bertol, I.; Vidal Vázquez, E.

2008-07-01

Changes in soil surface microrelief with cumulative rainfall under different tillage systems and crop cover conditions were investigated in southern Brazil. Surface cover was none (fallow) or the crop succession maize followed by oats. Tillage treatments were: 1) conventional tillage on bare soil (BS), 2) conventional tillage (CT), 3) minimum tillage (MT) and 4) no tillage (NT) under maize and oats. Measurements were taken with a manual relief meter on small rectangular grids of 0.234 and 0.156 m2, throughout growing season of maize and oats, respectively. Each data set consisted of 200 point height readings, the size of the smallest cells being 3×5 cm during maize and 2×5 cm during oats growth periods. Random Roughness (RR), Limiting Difference (LD), Limiting Slope (LS) and two fractal parameters, fractal dimension (D) and crossover length (l) were estimated from the measured microtopographic data sets. Indices describing the vertical component of soil roughness such as RR, LD and l generally decreased with cumulative rain in the BS treatment, left fallow, and in the CT and MT treatments under maize and oats canopy. However, these indices were not substantially affected by cumulative rain in the NT treatment, whose surface was protected with previous crop residues. Roughness decay from initial values was larger in the BS treatment than in CT and MT treatments. Moreover, roughness decay generally tended to be faster under maize than under oats. The RR and LD indices decreased quadratically, while the l index decreased exponentially in the tilled, BS, CT and MT treatments. Crossover length was sensitive to differences in soil roughness conditions allowing a description of microrelief decay due to rainfall in the tilled treatments, although better correlations between cumulative rainfall and the most commonly used indices RR and LD were obtained. At the studied scale, parameters l and D have been found to be useful in interpreting the configuration properties of the soil surface microrelief.

Effects of hydraulic roughness on surface textures of gravel‐bed rivers

USGS Publications Warehouse

Buffington, John M.; Montgomery, David R.

1999-01-01

Field studies of forest gravel‐bed rivers in northwestern Washington and southeastern Alaska demonstrate that bed‐surface grain size is responsive to hydraulic roughness caused by bank irregularities, bars, and wood debris. We evaluate textural response by comparing reach‐average median grain size (D50) to that predicted from the total bank‐full boundary shear stress (т0bf), representing a hypothetical reference condition of low hydraulic roughness. For a given т0bf, channels with progressively greater hydraulic roughness have systematically finer bed surfaces, presumably due to reduced bed shear stress, resulting in lower channel competence and diminished bed load transport capacity, both of which promote textural fining. In channels with significant hydraulic roughness, observed values D50 can be up to 90% smaller than those predicted from т0bf. We find that wood debris plays an important role at our study sites, not only providing hydraulic roughness but also influencing pool spacing, frequency of textural patches, and the amplitude and wavelength of bank and bar topography and their consequent roughness. Our observations also have biological implications. We find that textural fining due to hydraulic roughness can create usable salmonid spawning gravels in channels that otherwise would be too coarse.

ANN-PSO Integrated Optimization Methodology for Intelligent Control of MMC Machining

NASA Astrophysics Data System (ADS)

Chandrasekaran, Muthumari; Tamang, Santosh

2017-08-01

Metal Matrix Composites (MMC) show improved properties in comparison with non-reinforced alloys and have found increased application in automotive and aerospace industries. The selection of optimum machining parameters to produce components of desired surface roughness is of great concern considering the quality and economy of manufacturing process. In this study, a surface roughness prediction model for turning Al-SiCp MMC is developed using Artificial Neural Network (ANN). Three turning parameters viz., spindle speed ( N), feed rate ( f) and depth of cut ( d) were considered as input neurons and surface roughness was an output neuron. ANN architecture having 3 -5 -1 is found to be optimum and the model predicts with an average percentage error of 7.72 %. Particle Swarm Optimization (PSO) technique is used for optimizing parameters to minimize machining time. The innovative aspect of this work is the development of an integrated ANN-PSO optimization method for intelligent control of MMC machining process applicable to manufacturing industries. The robustness of the method shows its superiority for obtaining optimum cutting parameters satisfying desired surface roughness. The method has better convergent capability with minimum number of iterations.

TOPSIS based parametric optimization of laser micro-drilling of TBC coated nickel based superalloy

NASA Astrophysics Data System (ADS)

Parthiban, K.; Duraiselvam, Muthukannan; Manivannan, R.

2018-06-01

The technique for order of preference by similarity ideal solution (TOPSIS) approach was used for optimizing the process parameters of laser micro-drilling of nickel superalloy C263 with Thermal Barrier Coating (TBC). Plasma spraying was used to deposit the TBC and a pico-second Nd:YAG pulsed laser was used to drill the specimens. Drilling angle, laser scan speed and number of passes were considered as input parameters. Based on the machining conditions, Taguchi L8 orthogonal array was used for conducting the experimental runs. The surface roughness and surface crack density (SCD) were considered as the output measures. The surface roughness was measured using 3D White Light Interferometer (WLI) and the crack density was measured using Scanning Electron Microscope (SEM). The optimized result achieved from this approach suggests reduced surface roughness and surface crack density. The holes drilled at an inclination angle of 45°, laser scan speed of 3 mm/s and 400 number of passes found to be optimum. From the Analysis of variance (ANOVA), inclination angle and number of passes were identified as the major influencing parameter. The optimized parameter combination exhibited a 19% improvement in surface finish and 12% reduction in SCD.

Post-processing of 3D-printed parts using femtosecond and picosecond laser radiation

NASA Astrophysics Data System (ADS)

Mingareev, Ilya; Gehlich, Nils; Bonhoff, Tobias; Meiners, Wilhelm; Kelbassa, Ingomar; Biermann, Tim; Richardson, Martin C.

2014-03-01

Additive manufacturing, also known as 3D-printing, is a near-net shape manufacturing approach, delivering part geometry that can be considerably affected by various process conditions, heat-induced distortions, solidified melt droplets, partially fused powders, and surface modifications induced by the manufacturing tool motion and processing strategy. High-repetition rate femtosecond and picosecond laser radiation was utilized to improve surface quality of metal parts manufactured by laser additive techniques. Different laser scanning approaches were utilized to increase the ablation efficiency and to reduce the surface roughness while preserving the initial part geometry. We studied post-processing of 3D-shaped parts made of Nickel- and Titanium-base alloys by utilizing Selective Laser Melting (SLM) and Laser Metal Deposition (LMD) as additive manufacturing techniques. Process parameters such as the pulse energy, the number of layers and their spatial separation were varied. Surface processing in several layers was necessary to remove the excessive material, such as individual powder particles, and to reduce the average surface roughness from asdeposited 22-45 μm to a few microns. Due to the ultrafast laser-processing regime and the small heat-affected zone induced in materials, this novel integrated manufacturing approach can be used to post-process parts made of thermally and mechanically sensitive materials, and to attain complex designed shapes with micrometer precision.

Additively manufactured 3D porous Ti-6Al-4V constructs mimic trabecular bone structure and regulate osteoblast proliferation, differentiation and local factor production in a porosity and surface roughness dependent manner.

PubMed

Cheng, Alice; Humayun, Aiza; Cohen, David J; Boyan, Barbara D; Schwartz, Zvi

2014-10-07

Additive manufacturing by laser sintering is able to produce high resolution metal constructs for orthopedic and dental implants. In this study, we used a human trabecular bone template to design and manufacture Ti-6Al-4V constructs with varying porosity via laser sintering. Characterization of constructs revealed interconnected porosities ranging from 15-70% with compressive moduli of 2579-3693 MPa. These constructs with macro porosity were further surface-treated to create a desirable multi-scale micro-/nano-roughness, which has been shown to enhance the osseointegration process. Osteoblasts (MG63 cells) exhibited high viability when grown on the constructs. Proliferation (DNA) and alkaline phosphatase specific activity, an early differentiation marker, decreased as porosity increased, while osteocalcin, a late differentiation marker, as well as osteoprotegerin, vascular endothelial growth factor and bone morphogenetic proteins 2 and 4 increased with increasing porosity. Three-dimensional (3D) constructs with the highest porosity and surface modification supported the greatest osteoblast differentiation and local factor production. These results indicate that additively manufactured 3D porous constructs mimicking human trabecular bone and produced with additional surface treatment can be customized for increased osteoblast response. Increased factors for osteoblast maturation and differentiation on high porosity constructs suggest the enhanced performance of these surfaces for increasing osseointegration in vivo.

Assessing the performance of structure-from-motion photogrammetry and terrestrial lidar 1 at reconstructing soil surface microtopography of naturally vegetated plots

USDA-ARS?s Scientific Manuscript database

Soil microtopography or soil roughness is a property of critical importance in many earth surface processes but is often difficult to measure. Advances in computer vision technologies have made image-based 3D depiction of the soil surface or Structure-from-Motion (SfM) available to many scientists ...

Analysis of the influence of chemical treatment to the strength and surface roughness of FDM

NASA Astrophysics Data System (ADS)

Hambali, R. H.; Cheong, K. M.; Azizan, N.

2017-06-01

The applications of Additive Manufacturing (AM) technology have a greater functionality and wider range of application beyond an intention of prototyping. AM is the process of joining materials to form objects from Computer-Aided Design (CAD) models via layer upon layer process. One of AM technologies is the Fused Deposition Modelling (FDM), which use an extrusion method to create a part. FDM has been applied in many manufacturing applications includes an end-used parts. However, FDM tends to have bad surface quality due to staircase effect and post treatment is required. This chemical treatment is one of a way to improve the surface roughness of FDM fabricated parts. This method is one of economical and faster method. In order to enhance the surface finish of Acrylonitrile-Butadiene-Styrene (ABS) FDM parts by performing chemical treatment in an acetone solution as acetone has very low toxicity, high diffusion and low cost chemical solution. Therefore, the aim of this research is to investigate the influence of chemical treatment to the FDM used part in terms of surface roughness as well as the strength. In this project, ten specimens of standard ASTM D638 dogbone specimens have been fabricated using MOJO 3D printer. Five specimens from the dogbone were tested for surface roughness and tensile testing while another five were immersed in the chemical solution before the same testing. Based on results, the surface roughness of chemically treated dogbone has dramatically improved, compared to untreated dogbone with 97.2% of improvement. However, in term of strength, the tensile strength of dogbone is reduced 42.58% due to the rearrange of material properties and chemical effects to the joining of the filaments. In conclusion, chemical treatment is an economical and sustainable approach to enhance the surface quality of AM parts.

3-D Acoustic Scattering from 2-D Rough Surfaces Using A Parabolic Equation Model

DTIC Science & Technology

2013-12-01

Frequency Acoustic Propagation in Shallow Water.” Journal of Oceanic Engineering, September 2011: 1–10. Liu, Jin Yuan, Chen Fen Huang, and Ping Chang...loss values at a constant depth. .............................52  xi LIST OF ACRONYMS AND ABBREVIATIONS FD Finite Difference MMPE Monterey...2013). First, at each range step ( xi ), the 3-D field is transformed from cross-range spatial variable (y) to cross-range wavenumber variable (ky

3D-profile measurement of advanced semiconductor features by using FIB as reference metrology

NASA Astrophysics Data System (ADS)

Takamasu, Kiyoshi; Iwaki, Yuuki; Takahashi, Satoru; Kawada, Hiroki; Ikota, Masami

2017-03-01

A novel method of sub-nanometer uncertainty for the 3D-profile measurement and LWR (Line Width Roughness) measurement by using FIB (Focused Ion Beam) processing, and TEM (Transmission Electron Microscope) and CD-SEM (Critical Dimension Scanning Electron Microscope) images measurement is proposed to standardize 3D-profile measurement through reference metrology. In this article, we apply the methodology to line profile measurements and roughness measurement of advanced FinFET (Fin-shaped Field-Effect Transistor) features. The FinFET features are horizontally sliced as a thin specimen by FIB micro sampling system. Horizontally images of the specimens are obtained then by a planar TEM. LWR is calculated from the edges positions on TEM images. Moreover, we already have demonstrated the novel on-wafer 3D-profile metrology as "FIB-to-CDSEM method" with FIB slope cut and CD-SEM measuring. Using the method, a few micrometers wide on a wafer is coated and cut by 45-degree slope using FIB tool. Then, the wafer is transferred to CD-SEM to measure the cross section image by top down CD-SEM measurement. We applied FIB-to-CDSEM method to a CMOS image sensor feature. The 45-degree slope cut surface is observed using AFM. The surface profile of slope cut surface and line profiles are analyzed for improving the accuracy of FIB-to-CDSEM method.

Novel fabrication method for 3D microstructures using surface-activated bonding and its application to micro-mechanical parts

NASA Astrophysics Data System (ADS)

Yamada, Takayuki; Takahashi, Mutsuya; Ozawa, Takashi; Tawara, Satoshi; Goto, Takayuki

2002-11-01

The purpose of this work is to demonstrate that a novel fabrication method for 3-D microstructures (FORMULA) is applicable to fabrication of micro mechanical parts with a large flexibility. This method is a kind of layer manufacturing method of thin films for metallic or dielectric microstructures using surface-activated bonding (SAB). The bonding interfaces of thin films are investigated by transmission electron microscope (TEM). Voids were observed at the interfaces of both pure aluminum films and Al-Cu alloy films. The ratio of void on the Al-Cu/Al-Cu interface is much larger than that of Al/Al interface, although the films have the same surface roughness of 3nm in Ra (average roughness). And approximately 10nm-thick amorphous intermediate layers were found at the interfaces. Furthermore, we have fabricated a micro gear of 900μm in diameter and 200μm in height, which is about ten times as large as our previous test pieces. Overhung structures such as a bridge structure and a cantilever were also fabricated without supporting layers beneath them.

Laser-treated stainless steel mini-screw implants: 3D surface roughness, bone-implant contact, and fracture resistance analysis

PubMed Central

Kang, He-Kyong; Chu, Tien-Min; Dechow, Paul; Stewart, Kelton; Kyung, Hee-Moon

2016-01-01

Summary Background/Objectives: This study investigated the biomechanical properties and bone-implant intersurface response of machined and laser surface-treated stainless steel (SS) mini-screw implants (MSIs). Material and Methods: Forty-eight 1.3mm in diameter and 6mm long SS MSIs were divided into two groups. The control (machined surface) group received no surface treatment; the laser-treated group received Nd-YAG laser surface treatment. Half in each group was used for examining surface roughness (Sa and Sq), surface texture, and facture resistance. The remaining MSIs were placed in the maxilla of six skeletally mature male beagle dogs in a randomized split-mouth design. A pair with the same surface treatment was placed on the same side and immediately loaded with 200g nickel–titanium coil springs for 8 weeks. After killing, the bone-implant contact (BIC) for each MSI was calculated using micro computed tomography. Analysis of variance model and two-sample t test were used for statistical analysis with a significance level of P <0.05. Results: The mean values of Sa and Sq were significantly higher in the laser-treated group compared with the machined group (P <0.05). There were no significant differences in fracture resistance and BIC between the two groups. Limitation: animal study Conclusions/Implications: Laser treatment increased surface roughness without compromising fracture resistance. Despite increasing surface roughness, laser treatment did not improve BIC. Overall, it appears that medical grade SS has the potential to be substituted for titanium alloy MSIs. PMID:25908868

AFM surface imaging of AISI D2 tool steel machined by the EDM process

NASA Astrophysics Data System (ADS)

Guu, Y. H.

2005-04-01

The surface morphology, surface roughness and micro-crack of AISI D2 tool steel machined by the electrical discharge machining (EDM) process were analyzed by means of the atomic force microscopy (AFM) technique. Experimental results indicate that the surface texture after EDM is determined by the discharge energy during processing. An excellent machined finish can be obtained by setting the machine parameters at a low pulse energy. The surface roughness and the depth of the micro-cracks were proportional to the power input. Furthermore, the AFM application yielded information about the depth of the micro-cracks is particularly important in the post treatment of AISI D2 tool steel machined by EDM.

The effect of brushing with toothpaste containing nano calcium carbonate upon nanofill composite resin surface roughness

NASA Astrophysics Data System (ADS)

Ramadhani, A. M.; Herda, E.; Triaminingsih, S.

2017-08-01

This study aims to determine the effect of brushing with toothpaste containing nanocalcium carbonate on the roughness of nanofill composite resin surface. Brushing was conducted with 3 types of materials for 3 consecutive brushing periods of 10 minutes each. Surface roughness was measured using a surface-roughness tester and the results were analyzed using the repeated ANOVA and the one-way ANOVA test. The surface morphology was observed using SEM after 3 months’ worth of brushing with the 3 materials. It was found that the nanofill composite resin surface-roughness value increased significantly (p<0.005) after brushing with toothpaste containing nano calcium carbonate for 3 months, but the value was not as high as that obtained when brushing with other types of toothpaste.

Optical stent inspection of surface texture and coating thickness

NASA Astrophysics Data System (ADS)

Bermudez, Carlos; Laguarta, Ferran; Cadevall, Cristina; Matilla, Aitor; Ibañez, Sergi; Artigas, Roger

2017-02-01

Stent quality control is a critical process. Coronary stents have to be inspected 100% so no defective stent is implanted into a human body. We have developed a high numerical aperture optical stent inspection system able to acquire both 2D and 3D images. Combining a rotational stage, an area camera with line-scan capability and a triple illumination arrangement, unrolled sections of the outer, inner, and sidewalls surfaces are obtained with high resolution. During stent inspection, surface roughness and coating thickness uniformity is of high interest. Due to the non-planar shape of the surface of the stents, the thickness values of the coating need to be corrected with the 3D surface local slopes. A theoretical model and a simulation are proposed, and a measurement with white light interferometry is shown. Confocal and spectroscopic reflectometry showed to be limited in this application due to stent surface roughness. Due to the high numerical aperture of the optical system, only certain parts of the stent are in focus, which is a problem for defect detection, specifically on the sidewalls. In order to obtain fully focused 2D images, an extended depth of field algorithm has been implemented. A comparison between pixel variance and Laplacian filtering is shown. To recover the stack image, two different methods are proposed: maximum projection and weighted intensity. Finally, we also discuss the implementation of the processing algorithms in both the CPU and GPU, targeting real-time 2-Million pixel image acquisition at 50 frames per second.

Surface characterization of nickel titanium orthodontic arch wires

PubMed Central

Krishnan, Manu; Seema, Saraswathy; Tiwari, Brijesh; Sharma, Himanshu S.; Londhe, Sanjay; Arora, Vimal

2015-01-01

Background Surface roughness of nickel titanium orthodontic arch wires poses several clinical challenges. Surface modification with aesthetic/metallic/non metallic materials is therefore a recent innovation, with clinical efficacy yet to be comprehensively evaluated. Methods One conventional and five types of surface modified nickel titanium arch wires were surface characterized with scanning electron microscopy, energy dispersive analysis, Raman spectroscopy, Atomic force microscopy and 3D profilometry. Root mean square roughness values were analyzed by one way analysis of variance and post hoc Duncan's multiple range tests. Results Study groups demonstrated considerable reduction in roughness values from conventional in a material specific pattern: Group I; conventional (578.56 nm) > Group V; Teflon (365.33 nm) > Group III; nitride (301.51 nm) > Group VI (i); rhodium (290.64 nm) > Group VI (ii); silver (252.22 nm) > Group IV; titanium (229.51 nm) > Group II; resin (158.60 nm). It also showed the defects with aesthetic (resin/Teflon) and nitride surfaces and smooth topography achieved with metals; titanium/silver/rhodium. Conclusions Resin, Teflon, titanium, silver, rhodium and nitrides were effective in decreasing surface roughness of nickel titanium arch wires albeit; certain flaws. Findings have clinical implications, considering their potential in lessening biofilm adhesion, reducing friction, improving corrosion resistance and preventing nickel leach and allergic reactions. PMID:26843749

On Surface Losses in Direct Metal Laser Sintering Printed Millimeter and Submillimeter Waveguides

NASA Astrophysics Data System (ADS)

Holmberg, Max; Dancila, Dragos; Rydberg, Anders; Hjörvarsson, Björgvin; Jansson, Ulf; Marattukalam, Jithin James; Johansson, Niklas; Andersson, Joakim

2018-02-01

Different lengths of WR3 (220-330 GHz) and WR10 (75-110 GHz) waveguides are fabricated through direct metal laser sintering (DMLS). The losses in these waveguides are measured and modelled using the Huray surface roughness model. The losses in WR3 are around 0.3 dB/mm and in WR10 0.05 dB/mm. The Huray equation model is accounting relatively good for the attenuation in the WR10 waveguide but deviates more in the WR3 waveguide. The model is compared to finite element simulations of the losses assuming an approximate surface structure similar to the resulting one from the DMLS process.

On Surface Losses in Direct Metal Laser Sintering Printed Millimeter and Submillimeter Waveguides

NASA Astrophysics Data System (ADS)

Holmberg, Max; Dancila, Dragos; Rydberg, Anders; Hjörvarsson, Björgvin; Jansson, Ulf; Marattukalam, Jithin James; Johansson, Niklas; Andersson, Joakim

2018-06-01

Different lengths of WR3 (220-330 GHz) and WR10 (75-110 GHz) waveguides are fabricated through direct metal laser sintering (DMLS). The losses in these waveguides are measured and modelled using the Huray surface roughness model. The losses in WR3 are around 0.3 dB/mm and in WR10 0.05 dB/mm. The Huray equation model is accounting relatively good for the attenuation in the WR10 waveguide but deviates more in the WR3 waveguide. The model is compared to finite element simulations of the losses assuming an approximate surface structure similar to the resulting one from the DMLS process.

Influence of wall roughness and thermal coductivity on turbulent natural convection

NASA Astrophysics Data System (ADS)

Orlandi, Paolo; Pirozzoli, Sergio; Bernardini, Matteo

2015-11-01

We study turbulent natural convection in enclosures with conjugate heat transfer. The simplest way to increase the heat transfer in this flow is through rough surfaces. In numerical simulations often constant temperatures are assigned on the walls, but this is an unrealistic condition in laboratory experiments. Therefore, in the DNS, to be of help to experimentalists, it is necessary to solve the heat conduction in the solid walls together with the turbulent flow between the hot and the cold walls. Here the cold wall, 0 . 5 h tick is smooth, and the hot wall has 2D and 3D rough elements of thickness 0 . 2 h above a solid layer 0 . 3 h tick. The simulation is performed in a bi-periodic domain 4 h wide. The Rayleigh number varies from 106 to 108. Two values of the thermal conductivity, one corresponding to copper and the other ten times higher were assumed. It has been found that the Nusselt number behaves as Nu = αRaγ , with α increasing with the solid conductivity and depending of the roughness shape. 3D elements produce a heat transfer greater than 2D elements. An imprinting of the flow structures on the thermal field inside the walls is observed. The one-dimensional spectra at the center, one decade wide, agree with those of forced isotropic turbulence.

Effects of Wet and Dry Finishing and Polishing on Surface Roughness and Microhardness of Composite Resins

PubMed Central

Nasoohi, Negin; Hoorizad, Maryam

2017-01-01

Objectives: This study aimed to assess the effect of wet and dry finishing and polishing on microhardness and roughness of microhybrid and nanohybrid composites. Materials and Methods: Thirty samples were fabricated of each of the Polofil Supra and Aelite Aesthetic All-Purpose Body microhybrid and Grandio and Aelite Aesthetic Enamel nanohybrid composite resins. Each group (n=30) was divided into three subgroups of D, W and C (n=10). Finishing and polishing were performed dry in group D and under water coolant in group W. Group C served as the control group and did not receive finishing and polishing. Surface roughness of samples was measured by a profilometer and their hardness was measured by a Vickers hardness tester. Data were analyzed using two-way ANOVA (P<0.05). Results: The smoothest surfaces with the lowest microhardness were obtained under Mylar strip without finishing/polishing for all composites (P<0.0001). The highest surface roughness was recorded for dry finishing/polishing for all composites (P<0.0001). Dry finishing/polishing increased the microhardness of all composites (P<0.0001). Conclusions: Dry finishing and polishing increases the microhardness and surface roughness of microhybrid and nanohybrid composite resins. PMID:29104597

The effect of polishing technique on 3-D surface roughness and gloss of dental restorative resin composites.

PubMed

Ereifej, N S; Oweis, Y G; Eliades, G

2013-01-01

The aim of this study was to compare surface roughness and gloss of resin composites polished using different polishing systems. Five resin composites were investigated: Filtek Silorane (FS), IPS Empress Direct (IP), Clearfil Majesty Posterior (CM), Premise (PM), and Estelite Sigma (ES). Twenty-five disk specimens were prepared from each material, divided into five groups, each polished with one of the following methods: Opti1Step (OS), OptiDisc (OD), Kenda CGI (KD), Pogo (PG), or metallurgical polishing (ML). Gloss and roughness parameters (Sa, Sz, Sq, and St) were evaluated by 60°-angle glossimetry and white-light interferometric profilometry. Two-way analysis of variance was used to detect differences in different materials and polishing techniques. Regression and correlation analyses were performed to examine correlations between roughness and gloss. Significant differences in roughness parameters and gloss were found according to the material, type of polishing, and material/polishing technique (p< 0.05). The highest roughness was recorded when KD was used (Sa: 581.8 [62.1] for FS/KD, Sq: 748.7 [55.6] for FS/KD, Sz: 17.7 [2.7] for CM/KD, and St: 24.6 [6.8] for FS/KD), while the lowest was recorded after ML (Sa: 133.6 [68.9] for PM/ML, Sq: 256.5 [53.5] for ES/ML, Sz: 4.0 [1.3] for ES/ML, and St: 7.1 [0.7] for ES/ML). The highest gloss was recorded for PM/ML (88.4 [2.3]) and lowest for FS/KD (30.3 [5.7]). All roughness parameters were significantly correlated with gloss (r= 0.871, 0.846, 0.713, and 0.707 for Sa, Sq, Sz, St, and gloss, respectively). It was concluded that the polishing procedure and the type of composite can have significant impacts on surface roughness and gloss of resin composites.

Investigation of surface wave amplitudes in 3-D velocity and 3-D Q models

NASA Astrophysics Data System (ADS)

Ruan, Y.; Zhou, Y.

2010-12-01

It has been long recognized that seismic amplitudes depend on both wave speed structures and anelasticity (Q) structures. However, the effects of lateral heterogeneities in wave speed and Q structures on seismic amplitudes has not been well understood. We investigate the effects of 3-D wave speed and 3-D anelasticity (Q) structures on surface-wave amplitudes based upon wave propagation simulations of twelve globally-distributed earthquakes and 801 stations in Earth models with and without lateral heterogeneities in wave speed and anelasticity using a Spectral Element Method (SEM). Our tomographic-like 3-D Q models are converted from a velocity model S20RTS using a set of reasonable mineralogical parameters, assuming lateral perturbations in both velocity and Q are due to temperature perturbations. Surface-wave amplitude variations of SEM seismograms are measured in the period range of 50--200 s using boxcar taper, cosine taper and Slepian multi-tapers. We calculate ray-theoretical predictions of surface-wave amplitude perturbations due to elastic focusing, attenuation, and anelastic focusing which respectively depend upon the second spatial derivative (''roughness'') of perturbations in phase velocity, 1/Q, and the roughness of perturbations in 1/Q. Both numerical experiments and theoretical calculations show that (1) for short-period (~ 50 s) surface waves, the effects of amplitude attenuation due to 3-D Q structures are comparable with elastic focusing effects due to 3-D wave speed structures; and (2) for long-period (> 100 s) surface waves, the effects of attenuation become much weaker than elastic focusing; and (3) elastic focusing effects are correlated with anelastic focusing at all periods due to the correlation between velocity and Q models; and (4) amplitude perturbations are depend on measurement techniques and therefore cannot be directly compared with ray-theoretical predictions because ray theory does not account for the effects of measurement techniques. We calculate 3-D finite-frequency sensitivity of surface-wave amplitude to perturbations in wave speed and anelasticity (Q) which fully account for the effects of elastic focusing, attenuation, anelastic focusing as well as measurement techniques. We show that amplitude perturbations calculated using wave speed and Q sensitivity kernels agree reasonably well with SEM measurements and therefore the sensitivity kernels can be used in a joint inversion of seismic phase delays and amplitudes to simultaneously image high resolution 3-D wave speed and 3-D Q structures in the upper mantle.

Describing soil surface microrelief by crossover length and fractal dimension

NASA Astrophysics Data System (ADS)

Vidal Vázquez, E.; Miranda, J. G. V.; Paz González, A.

2007-05-01

Accurate description of soil surface topography is essential because different tillage tools produce different soil surface roughness conditions, which in turn affects many processes across the soil surface boundary. Advantages of fractal analysis in soil microrelief assessment have been recognised but the use of fractal indices in practice remains challenging. There is also little information on how soil surface roughness decays under natural rainfall conditions. The objectives of this work were to investigate the decay of initial surface roughness induced by natural rainfall under different soil tillage systems and to compare the performances of a classical statistical index and fractal microrelief indices. Field experiments were performed on an Oxisol at Campinas, São Paulo State (Brazil). Six tillage treatments, namely, disc harrow, disc plow, chisel plow, disc harrow + disc level, disc plow + disc level and chisel plow + disc level were tested. Measurements were made four times, firstly just after tillage and subsequently with increasing amounts of natural rainfall. Duplicated measurements were taken per treatment and date, yielding a total of 48 experimental surfaces. The sampling scheme was a square grid with 25×25 mm point spacing and the plot size was 1350×1350 mm, so that each data set consisted of 3025 individual elevation points. Statistical and fractal indices were calculated both for oriented and random roughness conditions, i.e. after height reading have been corrected for slope and for slope and tillage tool marks. The main drawback of the standard statistical index random roughness, RR, lies in its no spatial nature. The fractal approach requires two indices, fractal dimension, D, which describes how roughness changes with scale, and crossover length, l, specifying the variance of surface microrelief at a reference scale. Fractal parameters D and l, were estimated by two independent self-affine models, semivariogram (SMV) and local root mean square (RMS). Both algorithms, SMV and RMS, gave equivalent results for D and l indices, irrespective of trend removal procedure, even if some bias was present which is in accordance with previous work. Treatments with two tillage operations had the greatest D values, irrespective of evolution stage under rainfall and trend removal procedure. Primary tillage had the greatest initial values of RR and l. Differences in D values between treatments with primary tillage and those with two successive tillage operations were significant for oriented but not for random conditions. The statistical index RR and the fractal indices l and D decreased with increasing cumulative rainfall following different patterns. The l and D decay from initial value was very sharp after the first 24.4 mm cumulative rainfall. For five out of six tillage treatments a significant relationship between D and l was found for the random microrelief conditions allowing a covariance analysis. It was concluded that using RR or l together with D best allow joint description of vertical and horizontal soil roughness variations.

Evolutionary computation applied to the reconstruction of 3-D surface topography in the SEM.

PubMed

Kodama, Tetsuji; Li, Xiaoyuan; Nakahira, Kenji; Ito, Dai

2005-10-01

A genetic algorithm has been applied to the line profile reconstruction from the signals of the standard secondary electron (SE) and/or backscattered electron detectors in a scanning electron microscope. This method solves the topographical surface reconstruction problem as one of combinatorial optimization. To extend this optimization approach for three-dimensional (3-D) surface topography, this paper considers the use of a string coding where a 3-D surface topography is represented by a set of coordinates of vertices. We introduce the Delaunay triangulation, which attains the minimum roughness for any set of height data to capture the fundamental features of the surface being probed by an electron beam. With this coding, the strings are processed with a class of hybrid optimization algorithms that combine genetic algorithms and simulated annealing algorithms. Experimental results on SE images are presented.

Effect of leading-edge roughness on stability and transition of wind turbine blades

NASA Astrophysics Data System (ADS)

Kutz, Douglas; Freels, Justin; Hidore, John; White, Edward

2011-11-01

Over time, wind turbine blades erode due to impacts with sand and other debris. The resulting surface roughness degrades the blades' aerodynamic performance. Experimental studies conducted at the Texas A&M University Low-Speed Wind Tunnel examine roughness effects using a 2D NACA 63-418 airfoil with interchangeable leading edges of varying roughness at chord Reynolds numbers up to 3 . 0 ×106 . These data reveal decreased CL , max and increased CD , min as roughness increases. At very high roughness levels, even the lift curve slope is reduced. To better understand these findings and improve modeling of roughness effects, extensive boundary layer measurements including surface-mounted hotfilms and boundary-layer velocity profiles are used to assess how laminar-to-turbulent transition is promoted by roughness. As expected, roughness accelerates transition. Tollmien-Schlichting (TS) transition is observed only for a smooth leading edge while bypass transition is observed for the moderate and high roughness levels. Results are compared to N-factor transition predictions generated with software used by the wind industry. Predictions are successful for the smooth leading edge but even the low roughness level prevents correct transition prediction using TS-based methods. Support for this work by Vestas Technology Americas, Inc., is gratefully acknowledged as is the support of the wind-energy research group and the Low-Speed Wind Tunnel staff.

Investigation of wall-bounded turbulence over regularly distributed roughness

NASA Astrophysics Data System (ADS)

Placidi, Marco; Ganapathisubramani, Bharathram

2012-11-01

The effects of regularly distributed roughness elements on the structure of a turbulent boundary layer are examined by performing a series of Planar (high resolution l+ ~ 30) and Stereoscopic Particle Image Velocimetry (PIV) experiments in a wind tunnel. An adequate description of how to best characterise a rough wall, especially one where the density of roughness elements is sparse, is yet to be developed. In this study, rough surfaces consisting of regularly and uniformly distributed LEGO® blocks are used. Twelve different patterns are adopted in order to systematically examine the effects of frontal solidity (λf, frontal area of the roughness elements per unit wall-parallel area) and plan solidity (λp, plan area of roughness elements per unit wall-parallel area), on the turbulence structure. The Karman number, Reτ , is approximately 4000 across the different cases. Spanwise 3D vector fields at two different wall-normal locations (top of the canopy and within the log-region) are also compared to examine the spanwise homogeneity of the flow across different surfaces. In the talk, a detailed analysis of mean and rms velocity profiles, Reynolds stresses, and quadrant decomposition for the different patterns will be presented.

Defect inspection in hot slab surface: multi-source CCD imaging based fuzzy-rough sets method

NASA Astrophysics Data System (ADS)

Zhao, Liming; Zhang, Yi; Xu, Xiaodong; Xiao, Hong; Huang, Chao

2016-09-01

To provide an accurate surface defects inspection method and make the automation of robust image region of interests(ROI) delineation strategy a reality in production line, a multi-source CCD imaging based fuzzy-rough sets method is proposed for hot slab surface quality assessment. The applicability of the presented method and the devised system are mainly tied to the surface quality inspection for strip, billet and slab surface etcetera. In this work we take into account the complementary advantages in two common machine vision (MV) systems(line array CCD traditional scanning imaging (LS-imaging) and area array CCD laser three-dimensional (3D) scanning imaging (AL-imaging)), and through establishing the model of fuzzy-rough sets in the detection system the seeds for relative fuzzy connectedness(RFC) delineation for ROI can placed adaptively, which introduces the upper and lower approximation sets for RIO definition, and by which the boundary region can be delineated by RFC region competitive classification mechanism. For the first time, a Multi-source CCD imaging based fuzzy-rough sets strategy is attempted for CC-slab surface defects inspection that allows an automatic way of AI algorithms and powerful ROI delineation strategies to be applied to the MV inspection field.

Change in surface roughness of esthetic restorative materials after exposure to different immersion regimes in a cola drink.

PubMed

Bajwa, Navroop Kaur; Pathak, Anuradha

2014-01-01

Context. An in vitro study carried out to evaluate and compare the effect of Cola drink on surface roughness of esthetic restorative materials. Purpose. To compare the effect of different immersion regimes in a Cola drink on surface roughness of esthetic restorative materials. Method. Two hundred samples were grouped into 4 equal groups of 50 samples each: Group I: conventional glass ionomer, Group II: resin modified glass ionomer, Group III: polyacid-modified resin composite, Group IV: Composite resin. Each group was further subdivided into 5 subgroups of 10 samples each. Subgroup A (Control Subgroup). Samples were kept immersed in artificial saliva. Subgroup B. Samples were immersed in Cola drink once a day. Subgroup C. Samples were immersed in Cola drink, 3 times a day. Subgroup D. Samples were immersed in Cola drink 5 times a day. Subgroup E. Samples were immersed in Cola drink 10 times a day. Each immersion lasted 5 minutes. The immersion protocol was repeated for 7 days. Results. Maximum surface roughness was seen in Group I conventional glass ionomer cement, followed by Group II resin modified glass ionomer, Group III polyacid modified resin composite, and Group IV composite resin samples. Conclusion. Resistance to change in surface roughness is more in resin based restorative materials as compared to glass ionomer based materials.

Change in Surface Roughness of Esthetic Restorative Materials after Exposure to Different Immersion Regimes in a Cola Drink

PubMed Central

Bajwa, Navroop Kaur; Pathak, Anuradha

2014-01-01

Context. An in vitro study carried out to evaluate and compare the effect of Cola drink on surface roughness of esthetic restorative materials. Purpose. To compare the effect of different immersion regimes in a Cola drink on surface roughness of esthetic restorative materials. Method. Two hundred samples were grouped into 4 equal groups of 50 samples each: Group I: conventional glass ionomer, Group II: resin modified glass ionomer, Group III: polyacid-modified resin composite, Group IV: Composite resin. Each group was further subdivided into 5 subgroups of 10 samples each. Subgroup A (Control Subgroup). Samples were kept immersed in artificial saliva. Subgroup B. Samples were immersed in Cola drink once a day. Subgroup C. Samples were immersed in Cola drink, 3 times a day. Subgroup D. Samples were immersed in Cola drink 5 times a day. Subgroup E. Samples were immersed in Cola drink 10 times a day. Each immersion lasted 5 minutes. The immersion protocol was repeated for 7 days. Results. Maximum surface roughness was seen in Group I conventional glass ionomer cement, followed by Group II resin modified glass ionomer, Group III polyacid modified resin composite, and Group IV composite resin samples. Conclusion. Resistance to change in surface roughness is more in resin based restorative materials as compared to glass ionomer based materials. PMID:25006464

Development of the Improving Process for the 3D Printed Structure

NASA Astrophysics Data System (ADS)

Takagishi, Kensuke; Umezu, Shinjiro

2017-01-01

The authors focus on the Fused Deposition Modeling (FDM) 3D printer because the FDM 3D printer can print the utility resin material. It can print with low cost and therefore it is the most suitable for home 3D printer. The FDM 3D printer has the problem that it produces layer grooves on the surface of the 3D printed structure. Therefore the authors developed the 3D-Chemical Melting Finishing (3D-CMF) for removing layer grooves. In this method, a pen-style device is filled with a chemical able to dissolve the materials used for building 3D printed structures. By controlling the behavior of this pen-style device, the convex parts of layer grooves on the surface of the 3D printed structure are dissolved, which, in turn, fills the concave parts. In this study it proves the superiority of the 3D-CMF than conventional processing for the 3D printed structure. It proves utilizing the evaluation of the safety, selectively and stability. It confirms the improving of the 3D-CMF and it is confirmed utilizing the data of the surface roughness precision and the observation of the internal state and the evaluation of the mechanical characteristics.

Development of the Improving Process for the 3D Printed Structure

PubMed Central

Takagishi, Kensuke; Umezu, Shinjiro

2017-01-01

The authors focus on the Fused Deposition Modeling (FDM) 3D printer because the FDM 3D printer can print the utility resin material. It can print with low cost and therefore it is the most suitable for home 3D printer. The FDM 3D printer has the problem that it produces layer grooves on the surface of the 3D printed structure. Therefore the authors developed the 3D-Chemical Melting Finishing (3D-CMF) for removing layer grooves. In this method, a pen-style device is filled with a chemical able to dissolve the materials used for building 3D printed structures. By controlling the behavior of this pen-style device, the convex parts of layer grooves on the surface of the 3D printed structure are dissolved, which, in turn, fills the concave parts. In this study it proves the superiority of the 3D-CMF than conventional processing for the 3D printed structure. It proves utilizing the evaluation of the safety, selectively and stability. It confirms the improving of the 3D-CMF and it is confirmed utilizing the data of the surface roughness precision and the observation of the internal state and the evaluation of the mechanical characteristics. PMID:28054558

Development of the Improving Process for the 3D Printed Structure.

PubMed

Takagishi, Kensuke; Umezu, Shinjiro

2017-01-05

The authors focus on the Fused Deposition Modeling (FDM) 3D printer because the FDM 3D printer can print the utility resin material. It can print with low cost and therefore it is the most suitable for home 3D printer. The FDM 3D printer has the problem that it produces layer grooves on the surface of the 3D printed structure. Therefore the authors developed the 3D-Chemical Melting Finishing (3D-CMF) for removing layer grooves. In this method, a pen-style device is filled with a chemical able to dissolve the materials used for building 3D printed structures. By controlling the behavior of this pen-style device, the convex parts of layer grooves on the surface of the 3D printed structure are dissolved, which, in turn, fills the concave parts. In this study it proves the superiority of the 3D-CMF than conventional processing for the 3D printed structure. It proves utilizing the evaluation of the safety, selectively and stability. It confirms the improving of the 3D-CMF and it is confirmed utilizing the data of the surface roughness precision and the observation of the internal state and the evaluation of the mechanical characteristics.

Small-Scale Surf Zone Geometric Roughness

DTIC Science & Technology

2017-12-01

and an image of the tie points can be seen (Figure 6). 23 Figure 6. Screen Shot of Alignment Process On the left side is the workspace which...rest of the points, producing the 3D surface. 24 Figure 7. Screen Shot of Dense Cloud Process On the left side is the workspace which...maximum 200 words) Measurements of small-scale (O(mm)) geometric roughness (kf) associated with breaking wave foam were obtained within the surf zone on

Investigation of ellipsometric parameters of 2D microrough surfaces by FDTD.

PubMed

Qiu, J; Ran, D F; Liu, Y B; Liu, L H

2016-07-10

Ellipsometry is a powerful method for measuring the optical constants of materials and is very sensitive to surface roughness. In previous ellipsometric measurement of optical constants of solid materials with rough surfaces, researchers frequently used effective medium approximation (EMA) with roughness already known to fit the complex refractive index of the material. However, the ignored correlation length, the other important parameter of rough surfaces, will definitely result in fitting errors. Hence it is necessary to consider the influence of surface roughness and correlation length on the ellipsometric parameters Δ (phase difference) and Ψ (azimuth) characterizing practical systems. In this paper, the influence of roughness of two-dimensional randomly microrough surfaces (relative roughness σ/λ ranges from 0.001 to 0.025) of silicon on ellipsometric parameters was simulated by the finite-difference time-domain method which was validated with experimental results. The effects of incident angle, relative roughness, and correlation length were numerically investigated for two-dimensional Gaussian distributed randomly microrough surfaces, respectively. The simulated results showed that compared with the smooth surface, only tiny changes of the ellipsometric parameter Δ could be observed for microrough silicon surface in the vicinity of the Brewster angle, but obviously changes of Ψ occur especially in the vicinity of the Brewster angle. More differences between the ellipsometric parameters of the rough surface and smooth surface can been seen especially in the vicinity of the Brewster angle as the relative roughness σ/λ increases or correlation length τ decreases. The results reveal that when we measure the optical constants of solid materials by ellipsometry, the smaller roughness, larger correlation length and larger incident wavelength will lead to the higher precision of measurements.

Superficial physicochemical properties of polyurethane biomaterials as osteogenic regulators in human mesenchymal stem cells fates.

PubMed

Shahrousvand, Mohsen; Sadeghi, Gity Mir Mohamad; Shahrousvand, Ehsan; Ghollasi, Marzieh; Salimi, Ali

2017-08-01

All of the cells' interactions are done through their surfaces. Evaluation of surface physicochemical scaffolds along with other factors is important and determines the fate of stem cells. In this work, biodegradable and biocompatible polyester/polyether based polyurethanes (PUs) were synthesized by polycaprolactone diol (PCL) and poly (tetra methylene ether) glycol (PTMEG) as the soft segment. To assess better the impact of surface parameters such as stiffness and roughness effects on osteogenic differentiation of the human mesenchymal stem cell (hMSC), the dimension effect of substrates was eliminated and two-dimensional membranes were produced by synthesized polyurethane. Surface and bulk properties of prepared 2D membranes such as surface chemistry, roughness, stiffness and tensile behavior were evaluated by Attenuated total reflectance Fourier transform infrared (ATR-FTIR), atomic force microscopy (AFM) and tensile behavior. The prepared 2D PU films had suitable hydrophilicity, biodegradability, water absorption, surface roughness and bulk strength. The hMSCs showed greater osteogenesis expression in PU substrates with more roughness and stiffness than others. The results demonstrated that surface parameters along with other differentiation cues have a synergistic effect on stem cells fates. Copyright © 2017 Elsevier B.V. All rights reserved.

Comparison of two-step versus four-step composite finishing/polishing disc systems: evaluation of a new two-step composite polishing disc system.

PubMed

da Costa, Juliana B; Goncalves, Flavia; Ferracane, Jack L

2011-01-01

The purpose of this study was to evaluate surface finish and gloss of a two-step composite finishing/polishing (F/P) disc system compared with two multistep systems on five composites. Seventy-five disc-shaped composite specimens (D=10.0 mm, 2 mm thick, n=15 per composite) were made of microfill (Durafill-D), nanofill (Filtek Supreme-FS), nanohybrid (Premise-PR), and microhybrids (Filtek Z250-FZ, Esthet-EX). One side of each specimen was initially finished with a carbide bur. Five specimens of each resin composite were randomly assigned to receive full F/P by each of the disc systems: two-step (Enhance Flex NST-EF) and four-step (Sof-Lex-SL, Super-Snap-SS). Surface gloss was measured with a glossmeter and surface roughness was measured with a profilometer. Results were analyzed by two-way analysis of variance (ANOVA)/Tukey's (α<0.05). No difference in gloss was noted among the three F/P systems when used with D and EX; no difference between SL and EF when used with any composite, except for FS; and no difference between SL and SS when used with any composite. SL and EF showed similar surface roughness when used on all composites, except for EX. EF and SS showed similar surface roughness on PR. SL and SS showed similar surface roughness values on every composite, except for FZ. EF was capable of providing similar gloss and surface roughness to SL on four composites evaluated but was not able to produce as glossy or as smooth a surface as SS for three of the five composites.

Roughness and temperature effects on the filter media of a trickling filter for nitrification.

PubMed

Kishimoto, Naoyuki; Ohara, Tetsuya; Hinobayashi, Jouji; Hashimoto, Tsutomu

2014-01-01

The performance of trickling filters using two types of plastic media with the same material, the same shape and different roughness was evaluated during a temperature-decreasing period to understand the roughness and temperature effects on the filter media. Real restaurant wastewater was used for the experiments. The chemical oxygen demand (COD) removal and nitrification performance of plastic media with a rough surface (LT-15) was superior to that with a smooth surface (KT-15). Because the biomass of microorganisms attached on the LT-15 was twice that attached on the KT-15, the larger biomass attached on the LT-15 was thought to be responsible for the higher performance. During the operation, the COD loading and water temperature varied in the range from 0.37 to 1.9 kg m(-3) d(-1) and 17.0--10.0 degrees C, respectively. However, the COD removal performance was not dependent on the COD loading or water temperature. On the contrary, the COD loading and the water temperature influenced the nitrification performance. Although a nitrification efficiency of 100% was recorded at a COD loading of 0.37 kg m(-3) d(-1), it deteriorated to 17-28% at higher COD loading. Moreover, a decline in the water temperature decreased the nitrification performance. The temperature-activity coefficient for nitrification was estimated to be 1.096. Based on this value, it was inferred that the COD loading should be set at less than 0.20 kg m(-3) d(-1) for the complete nitrification of the restaurant wastewater in winter, when the water temperature usually drops to around 10 degrees C.

Cement paste surface roughness analysis using coherence scanning interferometry and confocal microscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Apedo, K.L., E-mail: apedo@unistra.fr; Munzer, C.; He, H.

2015-02-15

Scanning electron microscopy and scanning probe microscopy have been used for several decades to better understand the microstructure of cementitious materials. Very limited work has been performed to date to study the roughness of cementitious materials by optical microscopy such as coherence scanning interferometry (CSI) and chromatic confocal sensing (CCS). The objective of this paper is to better understand how CSI can be used as a tool to analyze surface roughness and topography of cement pastes. Observations from a series of images acquired using this technique on both polished and unpolished samples are described. The results from CSI are comparedmore » with those from a STIL confocal microscopy technique (SCM). Comparison between both optical techniques demonstrates the ability of CSI to measure both polished and unpolished cement pastes. - Highlights: • Coherence scanning interferometry (CSI) was used to analyze cement paste surfaces. • The results from the CSI were compared with those from a confocal microscopy. • 3D roughness parameters were obtained using the window resizing method. • Polished and unpolished cement pastes were studied.« less

Toward a better integration of roughness in rockfall simulations - a sensitivity study with the RockyFor3D model

NASA Astrophysics Data System (ADS)

Monnet, Jean-Matthieu; Bourrier, Franck; Milenkovic, Milutin

2017-04-01

Advances in numerical simulation and analysis of real-size field experiments have supported the development of process-based rockfall simulation models. Availability of high resolution remote sensing data and high-performance computing now make it possible to implement them for operational applications, e.g. risk zoning and protection structure design. One key parameter regarding rock propagation is the surface roughness, sometimes defined as the variation in height perpendicular to the slope (Pfeiffer and Bowen, 1989). Roughness-related input parameters for rockfall models are usually determined by experts on the field. In the RockyFor3D model (Dorren, 2015), three values related to the distribution of obstacles (deposited rocks, stumps, fallen trees,... as seen from the incoming rock) relatively to the average slope are estimated. The use of high resolution digital terrain models (DTMs) questions both the scale usually adopted by experts for roughness assessment and the relevance of modeling hypotheses regarding the rock / ground interaction. Indeed, experts interpret the surrounding terrain as obstacles or ground depending on the overall visibility and on the nature of objects. Digital models represent the terrain with a certain amount of smoothing, depending on the sensor capacities. Besides, the rock rebound on the ground is modeled by changes in the velocities of the gravity center of the block due to impact. Thus, the use of a DTM with resolution smaller than the block size might have little relevance while increasing computational burden. The objective of this work is to investigate the issue of scale relevance with simulations based on RockyFor3D in order to derive guidelines for roughness estimation by field experts. First a sensitivity analysis is performed to identify the combinations of parameters (slope, soil roughness parameter, rock size) where the roughness values have a critical effect on rock propagation on a regular hillside. Second, a more complex hillside is simulated by combining three components: a) a global trend (planar surface), b) local systematic components (sine waves), c) random roughness (Gaussian, zero-mean noise). The parameters for simulating these components are estimated for three typical scenarios of rockfall terrains: soft soil, fine scree and coarse scree, based on expert knowledge and available airborne and terrestrial laser scanning data. For each scenario, the reference terrain is created and used to compute input data for RockyFor3D simulations at different scales, i.e. DTMs with resolutions from 0.5 m to 20 m and associated roughness parameters. Subsequent analysis mainly focuses on the sensitivity of simulations both in terms of run-out envelope and kinetic energy distribution. Guidelines drawn from the results are expected to help experts handle the scale issue while integrating remote sensing data and field measurements of roughness in rockfall simulations.

Additively Manufactured 3D Porous Ti-6Al-4V Constructs Mimic Trabecular Bone Structure and Regulate Osteoblast Proliferation, Differentiation and Local Factor Production in a Porosity and Surface Roughness Dependent Manner

PubMed Central

Cheng, Alice; Humayun, Aiza; Cohen, David J.; Boyan, Barbara D.; Schwartz, Zvi

2014-01-01

Additive manufacturing by laser sintering is able to produce high resolution metal constructs for orthopaedic and dental implants. In this study, we used a human trabecular bone template to design and manufacture Ti-6Al-4V constructs with varying porosity via laser sintering. Characterization of constructs revealed interconnected porosities ranging from 15–70% with compressive moduli of 2063–2954 MPa. These constructs with macro porosity were further surface-treated to create a desirable multi-scale micro-/nano-roughness, which has been shown to enhance the osseointegration process. Osteoblasts (MG63 cells) exhibited high viability when grown on the constructs. Proliferation (DNA) and alkaline phosphatase specific activity (ALP), an early differentiation marker, decreased as porosity increased, while osteocalcin (OCN), a late differentiation marker, as well as osteoprotegerin (OPG), vascular endothelial growth factor (VEGF) and bone morphogenetic proteins 2 and 4 (BMP2, BMP4) increased with increasing porosity. 3D constructs with the highest porosity and surface modification supported the greatest osteoblast differentiation and local factor production. These results indicate that additively manufactured 3D porous constructs mimicking human trabecular bone and produced with additional surface treatment can be customized for increased osteoblast response. Increased factors for osteoblast maturation and differentiation on high porosity constructs suggest the enhanced performance of these surfaces for increasing osseointegration in vivo. PMID:25287305

Atmospheric stability analysis over statically and dynamically rough surfaces

NASA Astrophysics Data System (ADS)

Maric, Emina; Metzger, Meredith; Singha, Arindam; Sadr, Reza

2011-11-01

The ratio of buoyancy flux to turbulent kinetic energy production in the atmospheric surface layer is investigated experimentally for air flow over two types of surfaces characterized by static and dynamic roughness. In this study, ``static'' refers to the time-invariant nature of naturally-occurring roughness over a mud/salt playa; while, ``dynamic'' refers to the behavior of water waves along an air-water interface. In both cases, time-resolved measurements of the momentum and heat fluxes were acquired from synchronized 3D sonic anemometers mounted on a vertical tower. Field campaigns were conducted at two sites, representing the ``statically'' and ``dynamically'' rough surfaces, respectively: (1) the SLTEST facility in Utah's western desert, and (2) the new Doha airport in Qatar under construction along the coast of the Persian Gulf. Note, at site 2, anemometers were located directly above the water by extension from a tower secured to the end of a 1 km-long pier. Comparisons of the Monin-Obukhov length, flux Richardson number, and gradient Richardson number are presented, and discussed in the context of the observed evolution of the turbulent spectra in response to diurnal variations of atmospheric stability. Supported by the Qatar National Research Fund.

Numerical simulation of electroosmotic flow in rough microchannels using the lattice Poisson-Nernst-Planck methods

NASA Astrophysics Data System (ADS)

Kamali, Reza; Soloklou, Mohsen Nasiri; Hadidi, Hooman

2018-05-01

In this study, coupled Lattice Boltzmann method is applied to solve the dynamic model for an electroosmotic flow and investigate the effects of roughness in a 2-D flat microchannel. In the present model, the Poisson equation is solved for the electrical potential, the Nernst- Planck equation is solved for the ion concentration. In the analysis of electroosmotic flows, when the electric double layers fully overlap or the convective effects are not negligible, the Nernst-Planck equation must be used to find the ionic distribution throughout the microchannel. The effects of surface roughness height, roughness interval spacing and roughness surface potential on flow conditions are investigated for two different configurations of the roughness, when the EDL layers fully overlap through the microchannel. The results show that in both arrangements of roughness in homogeneously charged rough channels, the flow rate decreases by increasing the roughness height. A discrepancy in the mass flow rate is observed when the roughness height is about 0.15 of the channel width, which its average is higher for the asymmetric configuration and this difference grows by increasing the roughness height. In the symmetric roughness arrangement, the mass flow rate increases until the roughness interval space is almost 1.5 times the roughness width and it decreases for higher values of the roughness interval space. For the heterogeneously charged rough channel, when the roughness surface potential ψr is less than channel surface potential ψs , the net charge density increases by getting far from the roughness surface, while in the opposite situation, when ψs is more than ψr , the net charge density decreases from roughness surface to the microchannel middle center. Increasing the roughness surface potential induces stronger electric driving force on the fluid which results in larger velocities in the flow.

Comparing Vesta's Surface Roughness to the Moon Using Bistatic Radar Observations by the Dawn Mission

NASA Astrophysics Data System (ADS)

Palmer, E. M.; Heggy, E.; Kofman, W. W.; Moghaddam, M.

2015-12-01

The first orbital bistatic radar (BSR) observations of a small body have been conducted opportunistically by NASA's Dawn spacecraft at Asteroid Vesta using the telecommunications antenna aboard Dawn to transmit and the Deep Space Network 70-meter antennas on Earth to receive. Dawn's high-gain communications antenna continuously transmitted right-hand circularly polarized radio waves (4-cm wavelength), and due to the opportunistic nature of the experiment, remained in a fixed orientation pointed toward Earth throughout each BSR observation. As a consequence, Dawn's transmitted radio waves scattered from Vesta's surface just before and after each occultation of the Dawn spacecraft behind Vesta, resulting in surface echoes at highly oblique incidence angles of greater than 85 degrees, and a small Doppler shift of ~2 Hz between the carrier signal and surface echoes from Vesta. We analyze the power and Doppler spreading of Vesta's surface echoes to assess surface roughness, and find that Vesta's area-normalized radar cross section ranges from -8 to -17 dB, which is notably much stronger than backscatter radar cross section values reported for the Moon's limbs (-20 to -35 dB). However, our measurements correspond to the forward scattering regime--such that at high incidence, radar waves are expected to scatter more weakly from a rough surface in the backscatter direction than that which is scattered forward. Using scattering models of rough surfaces observed at high incidence, we report on the relative roughness of Vesta's surface as compared to the Moon and icy Galilean satellites. Through this, we assess the dominant processes that have influenced Vesta's surface roughness at centimeter and decimeter scales, which are in turn applicable to assisting future landing, sampling and orbital missions of other small bodies.

Haptic augmented skin surface generation toward telepalpation from a mobile skin image.

PubMed

Kim, K

2018-05-01

Very little is known about the methods of integrating palpation techniques to existing mobile teleskin imaging that delivers low quality tactile information (roughness) for telepalpation. However, no study has been reported yet regarding telehaptic palpation using mobile phone images for teledermatology or teleconsultations of skincare. This study is therefore aimed at introducing a new algorithm accurately reconstructing a haptic augmented skin surface for telehaptic palpation using a low-cost clip-on microscope simply attached to a mobile phone. Multiple algorithms such as gradient-based image enhancement, roughness-adaptive tactile mask generation, roughness-enhanced 3D tactile map building, and visual and haptic rendering with a three-degrees-of-freedom (DOF) haptic device were developed and integrated as one system. Evaluation experiments have been conducted to test the performance of 3D roughness reconstruction with/without the tactile mask. The results confirm that reconstructed haptic roughness with the tactile mask is superior to the reconstructed haptic roughness without the tactile mask. Additional experiments demonstrate that the proposed algorithm is robust against varying lighting conditions and blurring. In last, a user study has been designed to see the effect of the haptic modality to the existing visual only interface and the results attest that the haptic skin palpation can significantly improve the skin exam performance. Mobile image-based telehaptic palpation technology was proposed, and an initial version was developed. The developed technology was tested with several skin images and the experimental results showed the superiority of the proposed scheme in terms of the performance of haptic augmentation of real skin images. © 2017 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

Fractal Properties of Some Machined Surfaces

NASA Astrophysics Data System (ADS)

Thomas, T. R.; Rosén, B.-G.

Many surface profiles are self-affine fractals defined by fractal dimension D and topothesy Λ. Traditionally these parameters are derived laboriously from the slope and intercept of the profile's structure function. Recently a quicker and more convenient derivation from standard roughness parameters has been suggested. Based on this derivation, it is shown that D and Λ depend on two dimensionless numbers: the ratio of the mean peak spacing to the rms roughness, and the ratio of the mean local peak spacing to the sampling interval. Using this approach, values of D and Λ are calculated for 125 profiles produced by polishing, plateau honing and various single-point machining processes. Different processes are shown to occupy different regions in D-Λ space, and polished surfaces show a relationship between D and Λ which is independent of the surface material.

Controlled implant/soft tissue interaction by nanoscale surface modifications of 3D porous titanium implants.

PubMed

Rieger, Elisabeth; Dupret-Bories, Agnès; Salou, Laetitia; Metz-Boutigue, Marie-Helene; Layrolle, Pierre; Debry, Christian; Lavalle, Philippe; Vrana, Nihal Engin

2015-06-07

Porous titanium implants are widely employed in the orthopaedics field to ensure good bone fixation. Recently, the use of porous titanium implants has also been investigated in artificial larynx development in a clinical setting. Such uses necessitate a better understanding of the interaction of soft tissues with porous titanium structures. Moreover, surface treatments of titanium have been generally evaluated in planar structures, while the porous titanium implants have complex 3 dimensional (3D) architectures. In this study, the determining factors for soft tissue integration of 3D porous titanium implants were investigated as a function of surface treatments via quantification of the interaction of serum proteins and cells with single titanium microbeads (300-500 μm in diameter). Samples were either acid etched or nanostructured by anodization. When the samples are used in 3D configuration (porous titanium discs of 2 mm thickness) in vivo (in subcutis of rats for 2 weeks), a better integration was observed for both anodized and acid etched samples compared to the non-treated implants. If the implants were also pre-treated with rat serum before implantation, the integration was further facilitated. In order to understand the underlying reasons for this effect, human fibroblast cell culture tests under several conditions (directly on beads, beads in suspension, beads encapsulated in gelatin hydrogels) were conducted to mimic the different interactions of cells with Ti implants in vivo. Physical characterization showed that surface treatments increased hydrophilicity, protein adsorption and roughness. Surface treatments also resulted in improved adsorption of serum albumin which in turn facilitated the adsorption of other proteins such as apolipoprotein as quantified by protein sequencing. The cellular response to the beads showed considerable difference with respect to the cell culture configuration. When the titanium microbeads were entrapped in cell-laden gelatin hydrogels, significantly more cells migrated towards the acid etched beads. In conclusion, the nanoscale surface treatment of 3D porous titanium structures can modulate in vivo integration by the accumulative effect of the surface treatment on several physical factors such as protein adsorption, surface hydrophilicity and surface roughness. The improved protein adsorption capacity of the treated implants can be further exploited by a pre-treatment with autologous serum to render the implant surface more bioactive. Titanium microbeads are a good model system to observe these effects in a 3D microenvironment and provide a better representation of cellular responses in 3D.

Evaluation of Surface Roughness by Image Processing of a Shot-Peened, TIG-Welded Aluminum 6061-T6 Alloy: An Experimental Case Study

PubMed Central

Rawashdeh, Nathir A.

2018-01-01

Visual inspection through image processing of welding and shot-peened surfaces is necessary to overcome equipment limitations, avoid measurement errors, and accelerate processing to gain certain surface properties such as surface roughness. Therefore, it is important to design an algorithm to quantify surface properties, which enables us to overcome the aforementioned limitations. In this study, a proposed systematic algorithm is utilized to generate and compare the surface roughness of Tungsten Inert Gas (TIG) welded aluminum 6061-T6 alloy treated by two levels of shot-peening, high-intensity and low-intensity. This project is industrial in nature, and the proposed solution was originally requested by local industry to overcome equipment capabilities and limitations. In particular, surface roughness measurements are usually only possible on flat surfaces but not on other areas treated by shot-peening after welding, as in the heat-affected zone and weld beads. Therefore, those critical areas are outside of the measurement limitations. Using the proposed technique, the surface roughness measurements were possible to obtain for weld beads, high-intensity and low-intensity shot-peened surfaces. In addition, a 3D surface topography was generated and dimple size distributions were calculated for the three tested scenarios: control sample (TIG-welded only), high-intensity shot-peened, and low-intensity shot-peened TIG-welded Al6065-T6 samples. Finally, cross-sectional hardness profiles were measured for the three scenarios; in all scenarios, lower hardness measurements were obtained compared to the base metal alloy in the heat-affected zone and in the weld beads even after shot-peening treatments. PMID:29748520

Evaluation of Surface Roughness by Image Processing of a Shot-Peened, TIG-Welded Aluminum 6061-T6 Alloy: An Experimental Case Study.

PubMed

Atieh, Anas M; Rawashdeh, Nathir A; AlHazaa, Abdulaziz N

2018-05-10

Visual inspection through image processing of welding and shot-peened surfaces is necessary to overcome equipment limitations, avoid measurement errors, and accelerate processing to gain certain surface properties such as surface roughness. Therefore, it is important to design an algorithm to quantify surface properties, which enables us to overcome the aforementioned limitations. In this study, a proposed systematic algorithm is utilized to generate and compare the surface roughness of Tungsten Inert Gas (TIG) welded aluminum 6061-T6 alloy treated by two levels of shot-peening, high-intensity and low-intensity. This project is industrial in nature, and the proposed solution was originally requested by local industry to overcome equipment capabilities and limitations. In particular, surface roughness measurements are usually only possible on flat surfaces but not on other areas treated by shot-peening after welding, as in the heat-affected zone and weld beads. Therefore, those critical areas are outside of the measurement limitations. Using the proposed technique, the surface roughness measurements were possible to obtain for weld beads, high-intensity and low-intensity shot-peened surfaces. In addition, a 3D surface topography was generated and dimple size distributions were calculated for the three tested scenarios: control sample (TIG-welded only), high-intensity shot-peened, and low-intensity shot-peened TIG-welded Al6065-T6 samples. Finally, cross-sectional hardness profiles were measured for the three scenarios; in all scenarios, lower hardness measurements were obtained compared to the base metal alloy in the heat-affected zone and in the weld beads even after shot-peening treatments.

Factors influencing optical 3D scanning of vinyl polysiloxane impression materials.

PubMed

DeLong, R; Pintado, M R; Ko, C C; Hodges, J S; Douglas, W H

2001-06-01

Future growth in dental practice lies in digital imaging enhancing many chairside procedures and functions. This revolution requires the fast, accurate, and 3D digitizing of clinical records. One such clinical record is the chairside impression. This study investigated how surface angle and surface roughness affect the digitizing of vinyl polysiloxane impression materials. Seventeen vinyl polysiloxane impression materials were digitized with a white light optical digitizing system. Each sample was digitized at 3 different angles: 0 degrees, 22.5 degrees, and 45 degrees, and 2 digitizer camera f-stops. The digitized images were rendered on a computer monitor using custom software developed under NIH/NIDCR grant DE12225. All the 3D images were rotated to the 0 degrees position, cropped using Corel Photo-Paint 8 (Corel Corp, Ottawa, Ontario, Canada), then saved in the TIFF file format. The impression material area that was successfully digitized was calculated as a percentage of the total sample area, using Optimas 5.22 image processing software (Media Cybernetics, LP, Silver Spring, MD). The dependent variable was a Performance Value calculated for each material by averaging the percentage of area that digitized over the 3 angles. New samples with smooth and rough surfaces were made using the 7 impression materials with the largest Performance Values. These samples were tested as before, but with the additional angle of 60 degrees. Silky-Rock die stone (Whip Mix Corp, Louisville, KY) was used as a control. The Performance Values for the 17 impression materials ranged from 0% to 100%. The Performance Values for the 7 best materials were equivalent to the control at f/11 out to a surface angle of 45 degrees; however, only Examix impression material (GC America Inc, Alsip, IL) was equivalent to the control at f/11/\\16. At the 60 degrees surface angle with f/11/\\16, the Performance Values were 0% for all the impression materials, whereas that for the control was 90%. The difference in the Performance Values for the smooth and rough surface textures was 7%, which was not significant. The digitizing performance of vinyl polysiloxane impression materials is highly material and surface angle-dependent and is significantly lower than the die stone control when angles to 60 degrees are included. It is affected to a lesser extent by surface texture. Copyright 2001 by The American College of Prosthodontists.

Plant surfaces with cuticular folds are slippery for beetles

PubMed Central

Prüm, Bettina; Seidel, Robin; Bohn, Holger Florian; Speck, Thomas

2012-01-01

Plant surfaces covered with three-dimensional (3D) waxes are known to strongly reduce insect adhesion, leading to slippery surfaces. Besides 3D epicuticular waxes, cuticular folds are a common microstructure found on plant surfaces, which have not been quantitatively investigated with regard to their influence on insect adhesion. We performed traction experiments with Colorado potato beetles on five plant surfaces with cuticular folds of different magnitude. For comparison, we also tested (i) smooth plant surfaces and (ii) plant surfaces possessing 3D epicuticular waxes. Traction forces on surfaces with medium cuticular folds, of about 0.5 µm in both height and thickness and a spacing of 0.5–1.5 µm, were reduced by an average of 88 per cent in comparison to smooth plant surfaces. Traction forces were reduced by the same order of magnitude as on plant surfaces covered with 3D epicuticular waxes. For surface characterization, we performed static contact angle measurements, which proved a strong effect of cuticular folds also on surface wettability. Surfaces possessing cuticular folds of greater magnitude showed higher contact angles up to superhydrophobicity. We hypothesize that cuticular folds reduce insect adhesion mainly due to a critical roughness, reducing the real contact area between the surface and the insect's adhesive devices. PMID:21642366

Thin film growth by 3D multi-particle diffusion limited aggregation model: Anomalous roughening and fractal analysis

NASA Astrophysics Data System (ADS)

Nasehnejad, Maryam; Nabiyouni, G.; Gholipour Shahraki, Mehran

2018-03-01

In this study a 3D multi-particle diffusion limited aggregation method is employed to simulate growth of rough surfaces with fractal behavior in electrodeposition process. A deposition model is used in which the radial motion of the particles with probability P, competes with random motions with probability 1 - P. Thin films growth is simulated for different values of probability P (related to the electric field) and thickness of the layer(related to the number of deposited particles). The influence of these parameters on morphology, kinetic of roughening and the fractal dimension of the simulated surfaces has been investigated. The results show that the surface roughness increases with increasing the deposition time and scaling exponents exhibit a complex behavior which is called as anomalous scaling. It seems that in electrodeposition process, radial motion of the particles toward the growing seeds may be an important mechanism leading to anomalous scaling. The results also indicate that the larger values of probability P, results in smoother topography with more densely packed structure. We have suggested a dynamic scaling ansatz for interface width has a function of deposition time, scan length and probability. Two different methods are employed to evaluate the fractal dimension of the simulated surfaces which are "cube counting" and "roughness" methods. The results of both methods show that by increasing the probability P or decreasing the deposition time, the fractal dimension of the simulated surfaces is increased. All gained values for fractal dimensions are close to 2.5 in the diffusion limited aggregation model.

Segmenting the Femoral Head and Acetabulum in the Hip Joint Automatically Using a Multi-Step Scheme

NASA Astrophysics Data System (ADS)

Wang, Ji; Cheng, Yuanzhi; Fu, Yili; Zhou, Shengjun; Tamura, Shinichi

We describe a multi-step approach for automatic segmentation of the femoral head and the acetabulum in the hip joint from three dimensional (3D) CT images. Our segmentation method consists of the following steps: 1) construction of the valley-emphasized image by subtracting valleys from the original images; 2) initial segmentation of the bone regions by using conventional techniques including the initial threshold and binary morphological operations from the valley-emphasized image; 3) further segmentation of the bone regions by using the iterative adaptive classification with the initial segmentation result; 4) detection of the rough bone boundaries based on the segmented bone regions; 5) 3D reconstruction of the bone surface using the rough bone boundaries obtained in step 4) by a network of triangles; 6) correction of all vertices of the 3D bone surface based on the normal direction of vertices; 7) adjustment of the bone surface based on the corrected vertices. We evaluated our approach on 35 CT patient data sets. Our experimental results show that our segmentation algorithm is more accurate and robust against noise than other conventional approaches for automatic segmentation of the femoral head and the acetabulum. Average root-mean-square (RMS) distance from manual reference segmentations created by experienced users was approximately 0.68mm (in-plane resolution of the CT data).

Measuring surface topography with scanning electron microscopy. I. EZEImage: a program to obtain 3D surface data.

PubMed

Ponz, Ezequiel; Ladaga, Juan Luis; Bonetto, Rita Dominga

2006-04-01

Scanning electron microscopy (SEM) is widely used in the science of materials and different parameters were developed to characterize the surface roughness. In a previous work, we studied the surface topography with fractal dimension at low scale and two parameters at high scale by using the variogram, that is, variance vs. step log-log graph, of a SEM image. Those studies were carried out with the FERImage program, previously developed by us. To verify the previously accepted hypothesis by working with only an image, it is indispensable to have reliable three-dimensional (3D) surface data. In this work, a new program (EZEImage) to characterize 3D surface topography in SEM has been developed. It uses fast cross correlation and dynamic programming to obtain reliable dense height maps in a few seconds which can be displayed as an image where each gray level represents a height value. This image can be used for the FERImage program or any other software to obtain surface topography characteristics. EZEImage also generates anaglyph images as well as characterizes 3D surface topography by means of a parameter set to describe amplitude properties and three functional indices for characterizing bearing and fluid properties.

Determining the Effect of Material Hardness During the Hard Turning of AISI4340 Steel

NASA Astrophysics Data System (ADS)

Kambagowni, Venkatasubbaiah; Chitla, Raju; Challa, Suresh

2018-05-01

In the present manufacturing industries hardened steels are most widely used in the applications like tool design and mould design. It enhances the application range of hard turning of hardened steels in manufacturing industries. This study discusses the impact of workpiece hardness, feed and depth of cut on Arithmetic mean roughness (Ra), root mean square roughness (Rq), mean depth of roughness (Rz) and total roughness (Rt) during the hard turning. Experiments have been planned according to the Box-Behnken design and conducted on hardened AISI4340 steel at 45, 50 and 55 HRC with wiper ceramic cutting inserts. Cutting speed is kept constant during this study. The analysis of variance was used to determine the effects of the machining parameters. 3-D response surface plots drawn based on RSM were utilized to set up the input-output relationships. The results indicated that the feed rate has the most significant parameter for Ra, Rq and Rz and hardness has the most critical parameter for the Rt. Further, hardness shows its influence over all the surface roughness characteristics.

Estimating the age of arid-zone alluvial fan surfaces using roughness measurements from spaceborne radar backscatter

NASA Astrophysics Data System (ADS)

Hetz, G.; Mushkin, A.; Blumberg, D. G.; Baer, G.; Trabelsky, E.

2012-12-01

Alluvial fan surfaces respond to geologic and climate changes as they record the deposition and erosion processes that govern their evolution, which amongst others is manifested in the micro and meso scale topography of the surface. Remote sensing provides a regional view that is very useful for mapping. Some previous publications have demonstrated that relative dating can also be achieved by remote sensing using techniques common in planetary geology such as overlap relationships. This work focuses on the use of radar backscatter as suggested originally by Evans et al., (1992) to map ages but here we will try to provide an absolute geologic age. The objective of this paper is to demonstrate the use of radar backscatter to constrain surface roughness as a calibrated proxy for estimating age of alluvial surfaces. With the unique regional spatial perspective provided by spaceborne imaging, we aim at providing a new and complementary regional perspective for studying neotectonic and recent landscape evolution processes as well as paleoclimate. Moreover, the method (by radar backscattering measure) can be applied to the geomorphology of other planets. The current study is located in the southeastern part of the Negev desert, Israel on the late Pleistocene - Holocene Shehoret alluvial fan sequence. High resolution (0.5 cm) 3D roughness measurements were collected using a ground-based LIDAR (Leica HDS 3000) and these show a robust relationship between independently obtained OSL surface age and surface roughness; the fan surfaces become smoother with time over 103-105 yr timescales. Spaceborne backscatter radar data respond primarily to surface slope, roughness at a scale comparable to the radar wavelength, and other parameters such as dielectric properties of the surface. Therefore, radar can provide a good quantitative indication of surface roughness in arid zones, where vegetation cover is low. Preliminary results show a relationship between surface age and roughness and the radar cross section extracted from polarimetric spaceborne data. The best result is found in cross polarization (HV), L-band measured at an incidence angle of 38°.

Influence of Nitrogen Flow Rate on Friction Coefficient and Surface Roughness of TiN Coatings Deposited on Tool Steel Using Arc Method

NASA Astrophysics Data System (ADS)

Hamzah, Esah; Ourdjini, Ali; Ali, Mubarak; Akhter, Parvez; Hj. Mohd Toff, Mohd Radzi; Abdul Hamid, Mansor

In the present study, the effect of various N2 gas flow rates on friction coefficient and surface roughness of TiN-coated D2 tool steel was examined by a commercially available cathodic arc physical vapor deposition (CAPVD) technique. A Pin-on-Disc test was carried out to study the Coefficient of friction (COF) versus sliding distance. A surface roughness tester measured the surface roughness parameters. The minimum values for the COF and surface roughness were recorded at a N2 gas flow rate of 200 sccm. The increase in the COF and surface roughness at a N2 gas flow rate of 100 sccm was mainly attributed to an increase in both size and number of titanium particles, whereas the increase at 300 sccm was attributed to a larger number of growth defects generated during the coating process. These ideas make it possible to optimize the coating properties as a function of N2 gas flow rate for specific applications, e.g. cutting tools for automobiles, aircraft, and various mechanical parts.

Fabrication of PLA Filaments and its Printable Performance

NASA Astrophysics Data System (ADS)

Liu, Wenjie; Zhou, Jianping; Ma, Yuming; Wang, Jie; Xu, Jie

2017-12-01

Fused deposition modeling (FDM) is a typical 3D printing technology and preparation of qualified filaments is the basis. In order to prepare polylactic acid (PLA) filaments suitable for personalized FDM 3D printing, this article investigated the effect of factors such as extrusion temperature and screw speed on the diameter, surface roughness and ultimate tensile stress of the obtained PLA filaments. The optimal process parameters for fabrication of qualified filaments were determined. Further, the printable performance of the obtained PLA filaments for 3D objects was preliminarily explored.

Residual Stress Distribution and Microstructure of a Multiple Laser-Peened Near-Alpha Titanium Alloy

NASA Astrophysics Data System (ADS)

Umapathi, A.; Swaroop, S.

2018-04-01

Laser peening without coating (LPwC) was performed on a Ti-2.5 Cu alloy with multiple passes (1, 3 and 5), using a Nd:YAG laser (1064 nm) at a constant overlap rate of 70% and power density of 6.7 GW cm-2. Hardness and residual stress profiles indicated thermal softening near the surface (< 100 μm) and bulk softening due to adiabatic heating. Maximum hardness (235 HV at 500 μm) and maximum residual stress (- 890 MPa at 100 μm) were observed for LPwC with 1 pass. Surface roughness and surface 3-D topography imaging showed that the surface roughness increased with the increase in the number of passes. XRD results indicated no significant β phases. However, peak shifts, broadening and asymmetry were observed and interpreted based on dislocation activity. Microstructures indicated no melting or resolidification or refinement of grains at the surface. Twin density was found to increase with the increase in the number of passes.

Residual Stress Distribution and Microstructure of a Multiple Laser-Peened Near-Alpha Titanium Alloy

NASA Astrophysics Data System (ADS)

Umapathi, A.; Swaroop, S.

2018-05-01

Laser peening without coating (LPwC) was performed on a Ti-2.5 Cu alloy with multiple passes (1, 3 and 5), using a Nd:YAG laser (1064 nm) at a constant overlap rate of 70% and power density of 6.7 GW cm-2. Hardness and residual stress profiles indicated thermal softening near the surface (< 100 μm) and bulk softening due to adiabatic heating. Maximum hardness (235 HV at 500 μm) and maximum residual stress (- 890 MPa at 100 μm) were observed for LPwC with 1 pass. Surface roughness and surface 3-D topography imaging showed that the surface roughness increased with the increase in the number of passes. XRD results indicated no significant β phases. However, peak shifts, broadening and asymmetry were observed and interpreted based on dislocation activity. Microstructures indicated no melting or resolidification or refinement of grains at the surface. Twin density was found to increase with the increase in the number of passes.

Micro-topography, rock surface modelling and minerology of notches in Mount Carmel

NASA Astrophysics Data System (ADS)

Brook, Anna; Ben-Binyamin, Atzmon; Shtober-Zisu, Nurit

2016-04-01

Notches are defined as horizontal concaved indentations developed on slopes or cliffs in a basic "C" shape regardless of their location or formation process. Many studies have proclaimed that notches are associated with coastal processes where rocky shore faces are back carved, parallel to sea level by a combination of physical and biological abrasion, and by chemical and biological dissolution. The notches morphologies are various and depend on the lithology, climate, and environment history. These changes involve complex volumetric effects such as weathering and surface mineral dissolution. The main impetus for the present paper is to advance the modeling and the 3D complex pattern reconstruction of notch's cavity surface and detailed shapes and to assess the association between the morphological structures observed upon the notch parts and the fine scale mineralogical composition of the rock. The reconstruction of 3D surfaces using point clouds scanned data is a known problem in computer graphics. Several approaches are based on combinatorial structures, such as Delaunay triangulations, alpha shapes, or Voronoi diagrams. These schemes typically create a triangle mesh that interpolates all or most of the points. In the presence of noisy data, resulting surface is often jagged, and is therefore smoothed or refit to the points in subsequent processing. Fast Fourier Transform (FFT) is a common technique for solving dense, periodic Poisson systems. However, the FFT requires longer time and larger space, quickly becoming prohibitive for fine resolutions. The Poisson approach's key element is the observation that inward normal field of the boundary can be inferred as the gradient of a three dimensional solid indicator function. Thus, the generation of a watertight mesh can be obtained by: (1) transforming the oriented point samples into a continuous vector field referred to as the relationship between the gradient of the indicator function and an integral of surface normals. The computation of the indicator function is reduced to (2) finding a scalar function whose gradients best match the vector field. Point cloud input gives enough information for the approximation of the surface integral with discrete summation. A set of points used for the portioning of the whole scene into distinct patches and also for the surface integral scaled by the patch's area. (3) Extracting the appropriate iso-surface. The roughness spatial variation was calculated according to: 1) removal of the regional slope effect is a pre-step for the surface roughness indices calculation (regression surface is reduced from the original iso-surface model to produce residuals features, surface roughness, from which it possible to calculate the variogram of the residuals), 2) Semivariogram is used to determine the optimal window size for image texture analysis. Mineral composition and structure of the different patches and components define its solubility implying thus upon the micro-morphological differences. Spectral measurements taken in the field and in the lab will be constructed to spectral libraries representing the notch's visor, cavity and floor. The VIS-NIR, SWIR and MIR reflectance data measured by the different types of spectrometers will not be mixed for future evaluation of mineral identification. The constructed spectral libraries was analyzed and processed for the characterization of spectral features of samples. The spectral features were compared with various well characterized resampled mineral spectral libraries for identification of the forming minerals. The mineral composition is defined by spectroscopy and used to capture the areas corresponding to different patterns of micro roughness along the notch's surface. The suggested roughness and 3D surface reconstruction employ real data acquired by the Terrestrial Light and Range Detection (t-LiDAR) scanner. The project stresses an interdisciplinary approach to map the mineral variations along the notch's different components corresponding to the roughness surface changes.

The study on surface characteristics of high transmission components by 3D printing technique

NASA Astrophysics Data System (ADS)

Kuo, Hui-Jean; Huang, Chien-Yao; Wang, Wan-Hsuan; Lin, Ping-Hung; Tsay, Ho-Lin; Hsu, Wei-Yao

2017-06-01

3D printing is a high freedom fabrication technique. Any components, which designed by 3D design software or scanned from real parts, can be printed. The printing materials include metals, plastics and biocompatible materials etc. Especially for those high transmission components used in optical system or biomedical field can be printed, too. High transmission lens increases the performances of optical system. And high transmission cover or shell using in biomedical field helps observers to see the structures inside, such as brain, bone, and vessels. But the surface of printed components is not transparent, even the inside layer is transparent. If we increase the transmittance of surface, the components which fabricated by 3D printing process could have high transmission. In this paper, we using illuminating and polishing methods to improve the transmittance of printing surface. The illuminating time is the experiment parameters in illuminating method. The roughness and transmission of printing components are the evaluating targets. A 3D printing machine, Stratasys Connex 500, has been used to print high transmittance components in this paper. The surface transmittance of printing components is increasing above 80 % by polishing method.

Helicopter rotor noise investigation during ice accretion

NASA Astrophysics Data System (ADS)

Cheng, Baofeng

An investigation of helicopter rotor noise during ice accretion is conducted using experimental, theoretical, and numerical methods. This research is the acoustic part of a joint helicopter rotor icing physics, modeling, and detection project at The Pennsylvania State University Vertical Lift Research Center of Excellence (VLRCOE). The current research aims to provide acoustic insight and understanding of the rotor icing physics and investigate the feasibility of detecting rotor icing through noise measurements, especially at the early stage of ice accretion. All helicopter main rotor noise source mechanisms and their change during ice accretion are discussed. Changes of the thickness noise, steady loading noise, and especially the turbulent boundary layer - trailing edge (TBL-TE) noise due to ice accretion are identified and studied. The change of the discrete frequency noise (thickness noise and steady loading noise) due to ice accretion is calculated by using PSU-WOPWOP, an advanced rotorcraft acoustic prediction code. The change is noticeable, but too small to be used in icing detection. The small thickness noise change is due to the small volume of the accreted ice compared to that of the entire blade, although a large iced airfoil shape is used. For the loading noise calculation, two simplified methods are used to generate the loading on the rotor blades, which is the input for the loading noise calculation: 1) compact loading from blade element momentum theory, icing effects are considered by increasing the drag coefficient; and 2) pressure loading from the 2-D CFD simulation, icing effects are considered by using the iced airfoil shape. Comprehensive rotor broadband noise measurements are carried out on rotor blades with different roughness sizes and rotation speeds in two facilities: the Adverse Environment Rotor Test Stand (AERTS) facility at The Pennsylvania State University, and The University of Maryland Acoustic Chamber (UMAC). In both facilities the measured high-frequency broadband noise increases significantly with increasing surface roughness heights, which indicates that it is feasible to quantify helicopter rotor ice-induced surface roughness through acoustic measurements. Comprehensive broadband noise measurements based on different accreted ice roughness at AERTS are then used to form the data base from which a correlation between the ice-induced surface roughness and the broadband noise level is developed. Two parameters, the arithmetic average roughness height, Ra, and the averaged roughness height, based on the integrated ice thickness at the blade tip, are introduced to describe the ice-induced surface roughness at the early stage of the ice accretion. The ice roughness measurements are correlated to the measured broadband noise level. Strong correlations (absolute mean deviations of 9.3% and 11.2% for correlation using Ra and the averaged roughness height respectively) between the ice roughness and the broadband noise level are obtained, which can be used as a tool to determine the accreted ice roughness in the AERTS facility through acoustic measurement. It might be possible to use a similar approach to develop an early ice accretion detection tool for helicopters, as well as to quantify the ice-induced roughness at the early stage of rotor ice accretion. Rotor broadband noise source identification is conducted and the broadband noise related to ice accretion is argued to be turbulent boundary layer - trailing edge (TBL-TE) noise. Theory suggests TBL-TE noise scales with Mach number to the fifth power, which is also observed in the experimental data. The trailing edge noise theories developed by Ffowcs Williams and Hall, and Howe both identify two important parameters: boundary layer thickness and turbulence intensity. Numerical studies of 2-D airfoils with different ice-induced surface roughness heights are conducted to investigate the extent that surface roughness impacts the boundary layer thickness and turbulence intensity (and ultimately the TBL-TE noise). The results show that boundary layer thickness and turbulence intensity at the trailing edge increase with the increased roughness height. Using Howe's trailing edge noise model, the increased sound pressure level (SPL) of the trailing edge noise due to the increased displacement thickness and normalized integrated turbulence intensity are 6.2 dB and 1.6 dB for large and small accreted ice roughness heights, respectively. The estimated increased SPL values agree well with the experimental results, which are 5.8 dB and 2.6 dB for large and small roughness height, respectively. Finally a detailed broadband noise spectral scaling for all measured broadband noise in both AERTS and UMAC facilities is conducted. The magnitude and the frequency spectrum of the measured broadband noise are scaled on characteristic velocity and length. The peak of the laminar boundary layer - vortex shedding (LBL-VS) noise coalesces well on the Strouhal scaling in those cases. For the measured broadband noise from a rotor with relatively large roughness heights, no contribution of the LBL-VS noise is observed. The velocity scaling shows that the TBL-TE noise, which is the dominant source mechanism, scales with Mach number to the fifth power based on the absolute frequency. The length scaling shows that the TBL-TE noise scales well on the absolute roughness height based on Howe's TE noise theory.

Surface Features Parameterization and Equivalent Roughness Height Estimation of a Real Subglacial Conduit in the Arctic

NASA Astrophysics Data System (ADS)

Chen, Y.; Liu, X.; Mankoff, K. D.; Gulley, J. D.

2016-12-01

The surfaces of subglacial conduits are very complex, coupling multi-scale roughness, large sinuosity, and cross-sectional variations together. Those features significantly affect the friction law and drainage efficiency inside the conduit by altering velocity and pressure distributions, thus posing considerable influences on the dynamic development of the conduit. Parameterizing the above surface features is a first step towards understanding their hydraulic influences. A Matlab package is developed to extract the roughness field, the conduit centerline, and associated area and curvature data from the conduit surface, acquired from 3D scanning. By using those data, the characteristic vertical and horizontal roughness scales are then estimated based on the structure functions. The centerline sinuosities, defined through three concepts, i.e., the traditional definition of a fluvial river, entropy-based sinuosity, and curvature-based sinuosity, are also calculated and compared. The cross-sectional area and equivalent circular diameter along the centerline are also calculated. Among those features, the roughness is especially important due to its pivotal role in determining the wall friction, and thus an estimation of the equivalent roughness height is of great importance. To achieve such a goal, the original conduit is firstly simplified into a straight smooth pipe with the same volume and centerline length, and the roughness field obtained above is then reconstructed into the simplified pipe. An OpenFOAM-based Large-eddy-simulation (LES) is then performed based on the reconstructed pipe. Considering that the Reynolds number is of the order 106, and the relative roughness is larger than 5% for 60% of the conduit, we test the validity of the resistance law for completely rough pipe. The friction factor is calculated based on the pressure drop and mean velocity in the simulation. Working together, the equivalent roughness height can be calculated. However, whether the assumption is applicable for the current case, i.e., high relative roughness, is a question. Two other roughness heights, i.e., the vertical roughness scale based on structure functions and viscous sublayer thickness determined from the wall boundary layer are also calculated and compared with the equivalent roughness height.

Soft X-ray multilayers produced by sputtering and molecular beam epitaxy (MBE) - Substrate and interfacial roughness

NASA Astrophysics Data System (ADS)

Kearney, Patrick A.; Slaughter, J. M.; Powers, K. D.; Falco, Charles M.

1988-01-01

Roughness measurements were made on uncoated silicon wafers and float glass using a WYKO TOPO-3D phase shifting interferometry, and the results are reported. The wafers are found to be slightly smoother than the flat glass. The effects of different cleaning methods and of the deposition of silicon 'buffer layers' on substrate roughness are examined. An acid cleaning method is described which gives more consistent results than detergent cleaning. Healing of the roughness due to sputtered silicon buffer layers was not observed on the length scale probed by the WYKO. Sputtered multilayers are characterized using both the WYKO interferometer and low-angle X-ray diffraction in order to yield information about the roughness of the top surface and of the multilayer interfaces. Preliminary results on film growth using molecular beam epitaxy are also presented.

Rough-Surface-Enabled Capacitive Pressure Sensors with 3D Touch Capability.

PubMed

Lee, Kilsoo; Lee, Jaehong; Kim, Gwangmook; Kim, Youngjae; Kang, Subin; Cho, Sungjun; Kim, SeulGee; Kim, Jae-Kang; Lee, Wooyoung; Kim, Dae-Eun; Kang, Shinill; Kim, DaeEun; Lee, Taeyoon; Shim, Wooyoung

2017-11-01

Fabrication strategies that pursue "simplicity" for the production process and "functionality" for a device, in general, are mutually exclusive. Therefore, strategies that are less expensive, less equipment-intensive, and consequently, more accessible to researchers for the realization of omnipresent electronics are required. Here, this study presents a conceptually different approach that utilizes the inartificial design of the surface roughness of paper to realize a capacitive pressure sensor with high performance compared with sensors produced using costly microfabrication processes. This study utilizes a writing activity with a pencil and paper, which enables the construction of a fundamental capacitor that can be used as a flexible capacitive pressure sensor with high pressure sensitivity and short response time and that it can be inexpensively fabricated over large areas. Furthermore, the paper-based pressure sensors are integrated into a fully functional 3D touch-pad device, which is a step toward the realization of omnipresent electronics. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Influence of surface roughness on the oxidation behavior of a Ni-4.0Cr-5.7Al single crystal superalloy

NASA Astrophysics Data System (ADS)

Pei, Haiqing; Wen, Zhixun; Li, Zhenwei; Zhang, Yamin; Yue, Zhufeng

2018-05-01

The high-temperature oxidation dynamics and mechanisms of a Ni-based single crystal superalloy with four kinds of surface roughnesses were investigated by virtue of XRD, OM, SEM and EDS at 1000 °C. In the initial oxidation stage, outer (Ni, Co)O was mainly produced on the surfaces of the samples with Ra = 90 nm and 19 nm. Correspondingly, outer Cr2O3 and transient θ-Al2O3 were mainly formed on the surfaces with Ra = 509 nm and 182 nm. After 180 min oxidation, the values of instantaneous parabolic mass gain coefficients (kp) of the samples with all surface roughnesses were gradually consistent with the data of the growth parabolic coefficient of α-Al2O3. The oxidation mechanisms of Ni-based superalloy with different surface roughnesses were discussed by a model. The external diffusion flux of Al (DAl) increases with the increases of surface roughness. Thus, the required Al concentration decreases with the increases of surface roughness when the selective oxidation of Al occurrs to form a protective single α-Al2O3 film.

A one-dimensional free energy surface does not account for two-probe folding kinetics of protein alpha(3)D.

PubMed

Liu, Feng; Dumont, Charles; Zhu, Yongjin; DeGrado, William F; Gai, Feng; Gruebele, Martin

2009-02-14

We present fluorescence-detected measurements of the temperature-jump relaxation kinetics of the designed three-helix bundle protein alpha(3)D taken under solvent conditions identical to previous infrared-detected kinetics. The fluorescence-detected rate is similar to the IR-detected rate only at the lowest temperature where we could measure it (326 K). The fluorescence-detected rate decreases by a factor of 3 over the 326-344 K temperature range, whereas the IR-detected rate remains nearly constant over the same range. To investigate this probe dependence, we tested an extensive set of physically reasonable one-dimensional (1D) free energy surfaces by Langevin dynamics simulation. The simulations included coordinate- and temperature-dependent roughness, diffusion coefficients, and IR/fluorescence spectroscopic signatures. None of these can reproduce the IR and fluorescence data simultaneously, forcing us to the conclusion that a 1D free energy surface cannot accurately describe the folding of alpha(3)D. This supports the hypothesis that alpha(3)D has a multidimensional free energy surface conducive to downhill folding at 326 K, and that it is already an incipient downhill folder with probe-dependent kinetics near its melting point.

Development of the Navy’s Next-Generation Nonhydrostatic Modeling System

DTIC Science & Technology

2013-09-30

e.g. surface roughness, land- sea mask, surface albedo ) are needed by physical parameterizations. The surface values will be read and interpolated...characteristics (e.g. albedo , surface roughness) is now available to the model during the initialization stage. We have added infrastructure to the...six faces (Fig 3). 4 Figure 3: Topography (top left, in meters), surface roughness (top right, in meters), albedo (bottom left, no units

Radiographic evaluation of marginal bone level around implants with different neck designs after 1 year.

PubMed

Shin, Young-Kyu; Han, Chong-Hyun; Heo, Seong-Joo; Kim, Sunjai; Chun, Heoung-Jae

2006-01-01

To evaluate the influence of macro- and microstructure of the implant surface at the marginal bone level after functional loading. Sixty-eight patients were randomly assigned to 1 of 3 groups. The first group received 35 implants with a machined neck (Ankylos); the second group, 34 implants with a rough-surfaced neck (Stage 1); and the third, 38 implants with a rough-surfaced neck with microthreads (Oneplant). Clinical and radiographic examinations were conducted at baseline (implant loading) and 3, 6, and 12 months postloading. Two-way repeated analysis of variance (ANOVA) was used to test the significance of marginal bone change of each tested group at baseline, 3, 6, and 12 month follow-ups and 1-way ANOVA was also used to compare the bone loss of each time interval within the same implant group (P < .05). At 12 months, significant differences were noted in the amount of alveolar bone loss recorded for the 3 groups (P < .05). The group with the rough-surfaced microthreaded neck had a mean crestal bone loss of 0.18 +/- 0.16 mm; the group with the rough-surfaced neck, 0.76 +/- 0.21 mm; and the group with the machined neck, 1.32 +/- 0.27 mm. In the rough-surfaced group and the rough-surfaced microthreaded group, no statistically significant changes were observed after 3 months, whereas the machined-surface group showed significant bone loss for every interval (P < .05). To minimize marginal bone loss, in addition to the use of a rough surface at the marginal bone level, a macroscopic modification such as the addition of microthreads could be recommended. A rough surface and microthreads at the implant neck not only reduce crestal bone loss but also help with early biomechanical adaptation against loading in comparison to the machined neck design. A rough surface with microthreads at the implant neck was the most effective design to maintain the marginal bone level against functional loading.

Effect finishing and polishing procedures on the surface roughness of IPS Empress 2 ceramic.

PubMed

Boaventura, Juliana Maria Capelozza; Nishida, Rodrigo; Elossais, André Afif; Lima, Darlon Martins; Reis, José Mauricio Santos Nunes; Campos, Edson Alves; de Andrade, Marcelo Ferrarezi

2013-01-01

To evaluate the surface roughness of IPS Empress 2 ceramic when treated with different finishing/polishing protocols. Sixteen specimens of IPS Empress 2 ceramic were made from wax patterns obtained using a stainless steel split mold. The specimens were glazed (Stage 0-S0, control) and divided into two groups. The specimens in Group 1 (G1) were finished/polished with a KG Sorensen diamond point (S1), followed by KG Sorensen siliconized points (S2) and final polishing with diamond polish paste (S3). In Group 2 (G2), the specimens were finished/polished using a Shofu diamond point (S1), as well as Shofu siliconized points (S2) and final polishing was performed using Porcelize paste (S3). After glazing (S0) and following each polishing procedure (S1, S2 or S3), the surface roughness was measured using TALYSURF Series 2. The average surface roughness results were analyzed using ANOVA followed by Tukey post-hoc tests (α = 0.01) RESULTS: All of the polishing procedures yielded higher surface roughness values when compared to the control group (S0). S3 yielded lower surface roughness values when compared to S1 and S2. The proposed treatments negatively affected the surface roughness of the glazed IPS Empress 2 ceramic.

Surface degradation of glass ceramics after exposure to acidulated phosphate fluoride.

PubMed

Ccahuana, Vanessa Zulema S; Ozcan, Mutlu; Mesquita, Alfredo Mikail Melo; Nishioka, Renato Sussumo; Kimpara, Estevão Tomomitsu; Bottino, Marco Antonio

2010-01-01

This study evaluated the surface degradation effect of acidulated phosphate fluoride (APF) gel exposure on the glassy matrix ceramics as a function of time. Disc-shaped ceramic specimens (N = 120, 10/per ceramic material) were prepared in stainless steel molds (inner diameter: 5 mm, height: 2 mm) using 6 dental ceramics: 3 indicated for ceramic-fused-to-metal (Vita Omega 900, Carmen and Vita Titankeramik), 2 for all-ceramic (Vitadur Alpha and Finesse Low Fusing) and 1 for both types of restorations (IPS d.SIGN). The specimens were wet ground finished, ultrasonically cleaned and auto-glazed. All specimens were subjected to calculation of percentage of mass loss, surface roughness analysis and topographical description by scanning electron microscopy (SEM) before (0 min) and after exposure to 1.23 % APF gel for 4 min and 60 min representing short- and long-term etching effect, respectively. The data were analyzed using two-way ANOVA with repeated measures and Tukey's test (a=0.05). Significant effect of the type of the ceramics (p=0.0000, p=0.0031) and exposure time (p=0.0000) was observed in both surface roughness and percentage of mass loss values, respectively. The interaction factor between both parameters was also significant for both parameters (p=0.0904, p=0.0258). Both 4 min (0.44+/-0.1 - 0.81+/-0.2 microm) and 60 min (0.66+/-0.1 - 1.04+/-0.3 microm) APF gel exposure created significantly more surface roughness for all groups when compared to the control groups (0.33+/-0.2 - 0.68+/-0.2 microm) (p<0.05). There were no significant differences in percentage of mass loss between the ceramics at 4 min (p>0.05) but at 60 min exposure, IPS d.SIGN showed the highest percentage of mass loss (0.1151+/-0.11). The mean surface roughness for Vita Titankeramik (0.84+/-0.2 microm) and Finesse Low Fusing (0.74.+/-0.2 microm) was significantly higher than those of the other ceramics (0.59+/-0.1 microm - 0.49+/-0.1 microm) and Vita Titankeramik (p<0.05) regardless of the exposure time. A positive correlation was found between surface roughness and percentage of mass loss for all ceramic materials [(r=0.518 (Vitadur Alpha), r=0.405 (Vita Omega 900), r=0.580 (Carmen), r=0.687 (IPS d.SIGN), r=0.442 (Finesse Low Fusing), r=0.572 (Vita Titankeramik), Pearson's correlation coefficient)]. The qualitative SEM analysis showed evidence of corrosive attack on all of ceramics at varying degrees. The ceramics indicated for either metal-ceramic or all-ceramic restorations were all vulnerable to surface texture changes and mass loss after short-term and long-term APF gel exposure.

Plume Dispersion over Idealized Urban-liked Roughness with Height Variation: an LES Approach

NASA Astrophysics Data System (ADS)

Wong, Colman Ching Chi; Liu, Chun-Ho

2013-04-01

Human activities (e.g. vehicular emission) are the primary pollutant sources affecting the health and living quality of stakeholders in modern compact cities. Gaussian plume dispersion model is commonly used for pollutant distribution estimate that works well over rural areas with flat terrain. However, its major parameters, dispersion coefficients, exclude the effect of surface roughness that unavoidably prone to error handling the pollutant transport in the urban boundary layer (UBL) over building roughness. Our recent large-eddy simulation (LES) has shown that urban surfaces affect significantly the pollutant dispersion over idealized, identical two-dimensional (2D) street canyons of uniform height. As an extension to our on-going effort, this study is conceived to investigate how rough urban surfaces, which are constructed by 2D street canyons of non-uniform height, modify the UBL pollutant dispersion . A series of LESs with idealized roughness elements of non-uniform heights were performed in neutral stratification. Building models with two different heights were placed alternatively in the computational domain to construct 2D street canyons in cross flows. The plume dispersion from a ground-level passive pollutant source over more realistic urban areas was then examined. Along with the existing building-height-to-street-width (aspect) ratio (AR), a new parameter, building-height variability (BHV), is used to measure the building height unevenness. Four ARs (1, 0.5, 0.25 and 0.125) and three BHVs (20%, 40% and 60%) were considered in this study. Preliminary results show that BHV greatly increases the aerodynamic roughness of the hypothetical urban surfaces for narrow street canyons. Analogous to our previous findings, the air exchange rate (ACH) of street canyons increases with increasing friction factor, implying that street-level ventilation could be improved by increasing building roughness via BHV. In addition, the parameters used in dispersion coefficient estimates are related to the friction factor in the way similar to that of uniform street canyons, i.e. they are linear functions of friction factor when the roughness is small and become insensitive to friction factor thereafter over very rough surfaces. It is thus suggested that aerodynamic resistance is the key factor affecting the air quality in urban areas. Moreover, the friction factor could be used to parameterize the dispersion coefficients over different roughness elements.

Understanding the creation of & reducing surface microroughness during polishing & post-processing of glass optics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Suratwala, Tayyab

2016-09-22

In the follow study, we have developed a detailed understanding of the chemical and mechanical microscopic interactions that occur during polishing affecting the resulting surface microroughness of the workpiece. Through targeted experiments and modeling, the quantitative relationships of many important polishing parameters & characteristics affecting surface microroughness have been determined. These behaviors and phenomena have been described by a number of models including: (a) the Ensemble Hertzian Multi Gap (EHMG) model used to predict the removal rate and roughness at atomic force microscope (AFM) scale lengths as a function of various polishing parameters, (b) the Island Distribution Gap (IDG) modelmore » used to predict the roughness at larger scale lengths, (c) the Deraguin-Verwey-Landau-Overbeek (DLVO) 3-body electrostatic colloidal model used to predict the interaction of slurry particles at the interface and roughness behavior as a function of pH, and (d) a diffusion/chemical reaction rate model of the incorporation of impurities species into the polishing surface layer (called the Bielby layer). Based on this improved understanding, novel strategies to polish the workpiece have been developed simultaneously leading to both ultrasmooth surfaces and high material removal rates. Some of these strategies include: (a) use of narrow PSD slurries, (b) a novel diamond conditioning recipe of the lap to increase the active contact area between the workpiece and lap without destroying its surface figure, (c) proper control of pH for a given glass type to allow for a uniform distribution of slurry particles at the interface, and (d) increase in applied load just up to the transition between molecular to plastic removal regime for a single slurry particle. These techniques have been incorporated into a previously developed finishing process called Convergent Polishing leading to not just economical finishing process with improved surface figure control, but also simultaneously leading to low roughness surface with high removal rates.« less

3D-Printed Biomimetic Super-Hydrophobic Structure for Microdroplet Manipulation and Oil/Water Separation.

PubMed

Yang, Yang; Li, Xiangjia; Zheng, Xuan; Chen, Zeyu; Zhou, Qifa; Chen, Yong

2018-03-01

Biomimetic functional surfaces are attracting increasing attention for various technological applications, especially the superhydrophobic surfaces inspired by plant leaves. However, the replication of the complex hierarchical microstructures is limited by the traditional fabrication techniques. In this paper, superhydrophobic micro-scale artificial hairs with eggbeater heads inspired by Salvinia molesta leaf was fabricated by the Immersed surface accumulation three dimensional (3D) printing process. Multi-walled carbon nanotubes were added to the photocurable resins to enhance the surface roughness and mechanical strength of the microstructures. The 3D printed eggbeater surface reveals interesting properties in terms of superhydrophobilicity and petal effect. The results show that a hydrophilic material can macroscopically behave as hydrophobic if a surface has proper microstructured features. The controllable adhesive force (from 23 μN to 55 μN) can be easily tuned with different number of eggbeater arms for potential applications such as micro hand for droplet manipulation. Furthermore, a new energy-efficient oil/water separation solution based on our biomimetic structures was demonstrated. The results show that the 3D-printed eggbeater structure could have numerous applications, including water droplet manipulation, 3D cell culture, micro reactor, oil spill clean-up, and oil/water separation. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Hydrodynamic instability growth of three-dimensional modulations in radiation-driven implosions with “low-foot” and “high-foot” drives at the National Ignition Facility

DOE Office of Scientific and Technical Information (OSTI.GOV)

Smalyuk, V. A.; Weber, C. R.; Robey, H. F.

Hydrodynamic instability growth has been studied using three-dimensional (3-D) broadband modulations by comparing “high-foot” and “low-foot” spherical plastic (CH) capsule implosions at the National Ignition Facility (NIF). The initial perturbations included capsule outer-surface roughness and capsule-mounting membranes (“tents”) that were similar to those used in a majority of implosions on NIF. The tents with thicknesses of 31-nm, 46-nm, and 109-nm were used in the experiments. The outer-surface roughness in the “low-foot” experiment was similar to the standard specification, while it was increased by ~4 times in the “high-foot” experiment to compensate for the reduced growth. The ablation-front instability growth wasmore » measured using a Hydrodynamic Growth Radiography platform at a convergence ratio of 3. The dominant capsule perturbations, generated by the tent mountings, had measured perturbation amplitudes comparable to the capsule thickness with the “low-foot” drive. These tent perturbations were reduced by ~3 to 10 times in implosions with the “high-foot” drive. Unexpectedly, the measured perturbations with initially thinner tents were either larger or similar to the measured perturbations with thicker tents for both “high-foot” and “low-foot” drives. While the measured instability growth of 3-D broadband perturbations was also significantly reduced by ~5 to 10 times with the “high-foot” drive, compared to the “low-foot” drive, the growth mitigation was stronger than expected based on previous “growth-factor” results measured with two-dimensional modulations. Lastly, one of the hypotheses to explain the results is based on the 3-D modulations of the oxygen content in the bulk of the capsule having a stronger effect on the overall growth of capsule perturbations than the outer-surface capsule roughness.« less

Hydrodynamic instability growth of three-dimensional modulations in radiation-driven implosions with “low-foot” and “high-foot” drives at the National Ignition Facility

DOE PAGES

Smalyuk, V. A.; Weber, C. R.; Robey, H. F.; ...

2017-04-11

Hydrodynamic instability growth has been studied using three-dimensional (3-D) broadband modulations by comparing “high-foot” and “low-foot” spherical plastic (CH) capsule implosions at the National Ignition Facility (NIF). The initial perturbations included capsule outer-surface roughness and capsule-mounting membranes (“tents”) that were similar to those used in a majority of implosions on NIF. The tents with thicknesses of 31-nm, 46-nm, and 109-nm were used in the experiments. The outer-surface roughness in the “low-foot” experiment was similar to the standard specification, while it was increased by ~4 times in the “high-foot” experiment to compensate for the reduced growth. The ablation-front instability growth wasmore » measured using a Hydrodynamic Growth Radiography platform at a convergence ratio of 3. The dominant capsule perturbations, generated by the tent mountings, had measured perturbation amplitudes comparable to the capsule thickness with the “low-foot” drive. These tent perturbations were reduced by ~3 to 10 times in implosions with the “high-foot” drive. Unexpectedly, the measured perturbations with initially thinner tents were either larger or similar to the measured perturbations with thicker tents for both “high-foot” and “low-foot” drives. While the measured instability growth of 3-D broadband perturbations was also significantly reduced by ~5 to 10 times with the “high-foot” drive, compared to the “low-foot” drive, the growth mitigation was stronger than expected based on previous “growth-factor” results measured with two-dimensional modulations. Lastly, one of the hypotheses to explain the results is based on the 3-D modulations of the oxygen content in the bulk of the capsule having a stronger effect on the overall growth of capsule perturbations than the outer-surface capsule roughness.« less

Determining efficacy of monitoring devices on ceramic bond to resin composite

PubMed Central

Osorio, Estrella; Aguilera, Fátima S.; Osorio, Raquel; García-Godoy, Franklin; Cabrerizo-Vilchez, Miguel A.; Toledano, Manuel

2012-01-01

Objectives: This paper aims to assess the effectiveness of 3D nanoroughness and 2D microroughness evaluations, by their correlation with contact angle measurements and shear bond strength test, in order to evaluate the effect of two different acids conditioning on the bonding efficacy of a leucite-based glass-ceramic to a composite resin. Study Design: Ceramic (IPS Empress) blocks were treated as follows: 1) no treatment, 2) 37% phosphoric acid (H3PO4), 15 s, 3) 9% hydrofluoric acid (HF), 5 min. Micro- and nano-roughness were assessed with a profilometer and by means of an atomic force microscopy (AFM). Water contact angle (CA) measurements were determined to assess wettability of the ceramic surfaces with the asixymetric drop shape analysis contact diameter technique. Shear bond strength (SBS) was tested to a resin composite (Z100) with three different adhesive systems (Scotchbond Multipurpose Plus, Clearfil New Bond, ProBOND). Scanning electron microscopy (SEM) images were performed. Results: Nanoroughness values assessed in 50x50 μm areas were higher for the HF group, these differences were not detected by profilometric analysis. HF treatment created the nano- roughest surfaces and the smallest CA (p<0.05), producing the highest SBS to the composite resin with all tested adhesive systems (p<0.05). No differences existed between the SBS produced by the adhesive systems evaluated with any of the surface treatments tested. Conclusions: Nano-roughness obtained in a 50x50 µm scan size areas was the most reliable data to evaluate the topographical changes produced by the different acid treatments on ceramic surfaces. Key words:Dental ceramic, acid etching, bonding efficacy, resin composite, adhesive systems, contact angle, roughness. PMID:22549693

Skin friction related behaviour of artificial turf systems.

PubMed

Tay, Sock Peng; Fleming, Paul; Hu, Xiao; Forrester, Steph

2017-08-01

The occurrence of skin friction related injuries is an issue for artificial turf sports pitches and remains a barrier to their acceptance. The purpose of this study was to evaluate the current industry standard Securisport® Sports Surface Tester that measures skin surface related frictional behaviour of artificial turf. Little research has been published about the device and its efficacy, despite its widespread use as a standard FIFA test instrument. To achieve a range of frictional behaviours, several "third generation" (3G) carpet and infill combinations were investigated; friction time profiles throughout the Securisport rotations were assessed in combination with independent measurements of skin roughness before and after friction testing via 3D surface scanning. The results indicated that carpets without infill had greatest friction (coefficients of friction 0.97-1.20) while those completely filled with sand or rubber had similar and lower values independent of carpet type (coefficient of friction (COF) ≈0.57). Surface roughness of a silicone skin (s-skin) decreased after friction testing, with the largest change on sand infilled surfaces, indicating an "abrasive" polishing effect. The combined data show that the s-skin is damaged in a surface-specific manner, thus the Securisport COF values appear to be a poor measure of the potential for skin abrasion. It is proposed that the change in s-skin roughness improves assessment of the potential for skin damage when players slide on artificial turf.

The electrical resistivity of rough thin films: A model based on electron reflection at discrete step edges

NASA Astrophysics Data System (ADS)

Zhou, Tianji; Zheng, Pengyuan; Pandey, Sumeet C.; Sundararaman, Ravishankar; Gall, Daniel

2018-04-01

The effect of the surface roughness on the electrical resistivity of metallic thin films is described by electron reflection at discrete step edges. A Landauer formalism for incoherent scattering leads to a parameter-free expression for the resistivity contribution from surface mound-valley undulations that is additive to the resistivity associated with bulk and surface scattering. In the classical limit where the electron reflection probability matches the ratio of the step height h divided by the film thickness d, the additional resistivity Δρ = √{3 /2 } /(g0d) × ω/ξ, where g0 is the specific ballistic conductance and ω/ξ is the ratio of the root-mean-square surface roughness divided by the lateral correlation length of the surface morphology. First-principles non-equilibrium Green's function density functional theory transport simulations on 1-nm-thick Cu(001) layers validate the model, confirming that the electron reflection probability is equal to h/d and that the incoherent formalism matches the coherent scattering simulations for surface step separations ≥2 nm. Experimental confirmation is done using 4.5-52 nm thick epitaxial W(001) layers, where ω = 0.25-1.07 nm and ξ = 10.5-21.9 nm are varied by in situ annealing. Electron transport measurements at 77 and 295 K indicate a linear relationship between Δρ and ω/(ξd), confirming the model predictions. The model suggests a stronger resistivity size effect than predictions of existing models by Fuchs [Math. Proc. Cambridge Philos. Soc. 34, 100 (1938)], Sondheimer [Adv. Phys. 1, 1 (1952)], Rossnagel and Kuan [J. Vac. Sci. Technol., B 22, 240 (2004)], or Namba [Jpn. J. Appl. Phys., Part 1 9, 1326 (1970)]. It provides a quantitative explanation for the empirical parameters in these models and may explain the recently reported deviations of experimental resistivity values from these models.

Lunar textural analysis based on WAC-derived kilometer-scale roughness and entropy maps

NASA Astrophysics Data System (ADS)

Li, Bo; Wang, XueQiang; Zhang, Jiang; Chen, Jian; Ling, Zongcheng

2016-06-01

In general, textures are thought to be some complicated repeated patterns formed by elements, or primitives which are sorted in certain rules. Lunar surfaces record the interactions between its outside environment and itself, thus, based on high-resolution DEM model or image data, there are some topographic features which have different roughness and entropy values or signatures on lunar surfaces. Textures of lunar surfaces can help us to concentrate on typical topographic and photometric variations and reveal the relationships between obvious features (craters, impact basins, sinuous rilles (SRs) and ridges) with resurfacing processes on the Moon. In this paper, the term surface roughness is an expression of the variability of a topographic or photometric surface at kilometer scale, and the term entropy can characterize the variability inherent in a geological and topographic unit and evaluate the uncertainty of predictions made by a given geological process. We use the statistical moments of gray-level histograms in different-sized neighborhoods (e.g., 3, 5, 10, 20, 40 and 80 pixels) to compute the kilometer-scale roughness and entropy values, using the mosaic image from 70°N to 70°S obtained by Lunar Reconnaissance Orbiter (LRO) Wide Angle Camera (WAC). Large roughness and entropy signatures were only found in the larger scale maps, while the smallest 3-pixel scale map had more disorderly and unsystematic textures. According to the entropy values in 10-pixel scale entropy map, we made a frequency curve and categorized lunar surfaces into three types, shadow effects, maria and highlands. A 2D scatter plot of entropy versus roughness values was produced and we found that there were two point clusters corresponding to the highlands and maria, respectively. In the last, we compared the topographic and photometric signatures derived from Lunar Orbiter Laser Altimeter (LOLA) data and WAC mosaic image. On the lunar surfaces, the ridges have obvious multilevel topographic textures which are sensitive to the topographic changes, while the ejecta deposits of fresh craters appear obvious photometric textures which are sensitive to the brightness variations.

Comparison of tool life and surface roughness with MQL, flood cooling, and dry cutting conditions with P20 and D2 steel

NASA Astrophysics Data System (ADS)

Senevirathne, S. W. M. A. I.; Punchihewa, H. K. G.

2017-09-01

Minimum quantity lubrication (MQL) is a cutting fluid (CF) application method that has given promising results in improving machining performances. It has shown that, the performance of cutting systems, depends on the work and tool materials used. AISI P20, and D2 are popular in tool making industry. However, the applicability of MQL in machining these two steels has not been studied previously. This experimental study is focused on evaluating performances of MQL compared to dry cutting, and conventional flood cooling method. Trials were carried out with P20, and D2 steels, using coated carbides as tool material, emulsion cutting oil as the CF. Tool nose wear, and arithmetic average surface roughness (Ra) were taken as response variables. Results were statistically analysed for differences in response variables. Although many past literature has suggested that MQL causes improvements in tool wear, and surface finish, this study has found contradicting results. MQL has caused nearly 200% increase in tool nose wear, and nearly 11-13% increase in surface roughness compared flood cooling method with both P20 and D2. Therefore, this study concludes that MQL affects adversely in machining P20, and D2 steels.

Unpolarized emissivity with shadow and multiple reflections from random rough surfaces with the geometric optics approximation: application to Gaussian sea surfaces in the infrared band.

PubMed

Bourlier, Christophe

2006-08-20

The emissivity from a stationary random rough surface is derived by taking into account the multiple reflections and the shadowing effect. The model is applied to the ocean surface. The geometric optics approximation is assumed to be valid, which means that the rough surface is modeled as a collection of facets reflecting locally the light in the specular direction. In particular, the emissivity with zero, single, and double reflections are analytically calculated, and each contribution is studied numerically by considering a 1D sea surface observed in the near infrared band. The model is also compared with results computed from a Monte Carlo ray-tracing method.

Subgap in the Surface Bound States Spectrum of Superfluid (3) 3 He-B with Rough Surface

NASA Astrophysics Data System (ADS)

Nagato, Y.; Higashitani, S.; Nagai, K.

2018-03-01

The subgap structure in the surface bound states spectrum of superfluid ^3He-B with rough surface is discussed. The subgap is formed by the level repulsion between the surface bound state and the continuum states in the course of multiple scattering by the surface roughness. We show that the level repulsion is originated from the nature of the wave function of the surface bound state that is now recognized as Majorana fermion. We study the superfluid ^3He-B with a rough surface and in a magnetic field perpendicular to the surface using the quasi-classical Green function together with a random S-matrix model. We calculate the self-consistent order parameters, the spin polarization density and the surface density of states. It is shown that the subgap is found also in a magnetic field perpendicular to the surface. The magnetic field dependence of the transverse acoustic impedance is also discussed.

Analysis of Surface Roughness at Overlapping Laser Shock Peening

NASA Astrophysics Data System (ADS)

Dai, F. Z.; Zhang, Z. D.; Zhou, J. Z.; Lu, J. Z.; Zhang, Y. K.

2016-02-01

The overlapping effects on surface roughness are studied when samples are treated by laser shock peening (LSP). Surface roughness of overlapped circular laser spot is calculated by ISO 25178 height parameters. The usually used overlapping styles namely isosceles-right-triangle-style (AAP) and equilateral-triangle-style (AAA) are carefully investigated when the overlapping degree in x-axis (ηx) is below 50%. Surface roughness of isosceles-right-triangle-style attains its minimum value at ηx of 29.3%, and attains its maximum value at ηx of 43.6%. Surface roughness of equilateral-triangle-style attains its minimum value at ηx of 42.3%, and attains its maximum value at ηx of 32%. Experimental results are well consistent with theoretical analysis.

Understanding EUV mask blank surface roughness induced LWR and associated roughness requirement

NASA Astrophysics Data System (ADS)

Yan, Pei-Yang; Zhang, Guojing; Gullikson, Eric M.; Goldberg, Ken A.; Benk, Markus P.

2015-03-01

Extreme ultraviolet lithography (EUVL) mask multi-layer (ML) blank surface roughness specification historically comes from blank defect inspection tool requirement. Later, new concerns on ML surface roughness induced wafer pattern line width roughness (LWR) arise. In this paper, we have studied wafer level pattern LWR as a function of EUVL mask surface roughness via High-NA Actinic Reticle Review Tool. We found that the blank surface roughness induced LWR at current blank roughness level is in the order of 0.5nm 3σ for NA=0.42 at the best focus. At defocus of ±40nm, the corresponding LWR will be 0.2nm higher. Further reducing EUVL mask blank surface roughness will increase the blank cost with limited benefit in improving the pattern LWR, provided that the intrinsic resist LWR is in the order of 1nm and above.

3D-shape recognition and size measurement of irregular rough particles using multi-views interferometric out-of-focus imaging.

PubMed

Ouldarbi, L; Talbi, M; Coëtmellec, S; Lebrun, D; Gréhan, G; Perret, G; Brunel, M

2016-11-10

We realize simplified-tomography experiments on irregular rough particles using interferometric out-of-focus imaging. Using two angles of view, we determine the global 3D-shape, the dimensions, and the 3D-orientation of irregular rough particles whose morphologies belong to families such as sticks, plates, and crosses.

Effect of resin infiltration and microabrasion on the microhardness, surface roughness and morphology of incipient carious lesions.

PubMed

Yazkan, Basak; Ermis, R Banu

2018-02-15

The effects of resin infiltration and microabrasion on incipient carious lesions by surface microhardness, roughness and morphological assessments, and resistance to further acid attack of treated lesions were evaluated. Eighty artificially-induced incipient lesions were randomly divided into five groups (n = 16): resin infiltration with an adhesive resin (Excite F, Ivoclar Vivadent, Schaan, Liechtenstein), resin infiltration with a resin infiltrant (Icon, DMG, Hamburg, Germany), microabrasion without polishing (Opalustre, Ultradent, South Jordan, UT, USA), microabrasion with polishing (Opalustre, Ultradent, Diamond Excel, FGM, Joinville, SC, Brazil), and distilled water (control group). All specimens were exposed to demineralization for another 10 d. Microhardness, roughness and morphological assessments were done at baseline, following initial demineralization, treatment and further demineralization. Data were analysed by the Kruskal-Wallis, Friedman's and Bonferroni tests (p < .05). Enamel lesions treated with resin infiltrant and microabrasion demonstrated similar hardness values, with a nonsignificant difference compared with sound enamel. Resin infiltration demonstrated lower roughness values than those of microabrasion, and the values did not reach the values of sound enamel. Further demineralization for 10 d did not affect the hardness but increased the roughness of infiltrated and microabraded enamel surfaces. Polishing did not influence the roughness of microabraded enamel surfaces. After resin infiltration, porosities on enamel were sealed completely. The surface structure was similar to that of the enamel conditioning pattern for microabraded enamel lesions. Within the limitations of this study, the icon infiltration and microabrasion technique appeared to be effective for improving microhardness. Icon appeared to provide reduced roughness, although not equal to sound enamel. Further research is needed to elucidate their clinical relevance.

Effects of hydraulic roughness on surface textures of gravel-bed rivers

Treesearch

John M. Buffington; David R. Montgomery

1999-01-01

Field studies of forest gravel-bed rivers in northwestern Washington and southeastern Alaska demonstrate that bed-surface grain size is responsive to hydraulic roughness caused by bank irregularities, bars, and wood debris. We evaluate textural response by comparing reach-average median grain size (D50) to that predicted from the total bank-full boundary shear stress (...

Specular Scattering of Acoustic Waves from a Rough Surface in the Fraunhofer and Fresnel Approximations

DTIC Science & Technology

1969-01-01

ted in Fi g 4v er •it the te nt ti t ~ ~ ~ ~ ~ ~ ~ ~ o teslt obrnd y(ulnad ay he (1962) , who scatee Eou4d siWnal .4 frtn th surfac of the oea TheirW...and11 NT YPy’hik, Thbiz-_ :17 Nti-rlý Sr t z ciPout, AfzaimiQ PreNis !w Trýc, ( Wun . F.. P., "Antp1 4tudA ncA Phstocd Fluictuft-d.0on of at 3%Iund WfAve

Effect finishing and polishing procedures on the surface roughness of IPS Empress 2 ceramic

PubMed Central

Nishida, Rodrigo; Elossais, André Afif; Lima, Darlon Martins; Reis, José Mauricio Santos Nunes; Campos, Edson Alves; de Andrade, Marcelo Ferrarezi

2013-01-01

Objective. To evaluate the surface roughness of IPS Empress 2 ceramic when treated with different finishing/polishing protocols. Materials and methods. Sixteen specimens of IPS Empress 2 ceramic were made from wax patterns obtained using a stainless steel split mold. The specimens were glazed (Stage 0–S0, control) and divided into two groups. The specimens in Group 1 (G1) were finished/polished with a KG Sorensen diamond point (S1), followed by KG Sorensen siliconized points (S2) and final polishing with diamond polish paste (S3). In Group 2 (G2), the specimens were finished/polished using a Shofu diamond point (S1), as well as Shofu siliconized points (S2) and final polishing was performed using Porcelize paste (S3). After glazing (S0) and following each polishing procedure (S1, S2 or S3), the surface roughness was measured using TALYSURF Series 2. The average surface roughness results were analyzed using ANOVA followed by Tukey post-hoc tests (α = 0.01) Results. All of the polishing procedures yielded higher surface roughness values when compared to the control group (S0). S3 yielded lower surface roughness values when compared to S1 and S2. Conclusions. The proposed treatments negatively affected the surface roughness of the glazed IPS Empress 2 ceramic. PMID:22724660

Laser polishing of 3D printed mesoscale components

NASA Astrophysics Data System (ADS)

Bhaduri, Debajyoti; Penchev, Pavel; Batal, Afif; Dimov, Stefan; Soo, Sein Leung; Sten, Stella; Harrysson, Urban; Zhang, Zhenxue; Dong, Hanshan

2017-05-01

Laser polishing of various engineered materials such as glass, silica, steel, nickel and titanium alloys, has attracted considerable interest in the last 20 years due to its superior flexibility, operating speed and capability for localised surface treatment compared to conventional mechanical based methods. The paper initially reports results from process optimisation experiments aimed at investigating the influence of laser fluence and pulse overlap parameters on resulting workpiece surface roughness following laser polishing of planar 3D printed stainless steel (SS316L) specimens. A maximum reduction in roughness of over 94% (from ∼3.8 to ∼0.2 μm Sa) was achieved at the optimised settings (fluence of 9 J/cm2 and overlap factors of 95% and 88-91% along beam scanning and step-over directions respectively). Subsequent analysis using both X-ray photoelectron spectroscopy (XPS) and glow discharge optical emission spectroscopy (GDOES) confirmed the presence of surface oxide layers (predominantly consisting of Fe and Cr phases) up to a depth of ∼0.5 μm when laser polishing was performed under normal atmospheric conditions. Conversely, formation of oxide layers was negligible when operating in an inert argon gas environment. The microhardness of the polished specimens was primarily influenced by the input thermal energy, with greater sub-surface hardness (up to ∼60%) recorded in the samples processed with higher energy density. Additionally, all of the polished surfaces were free of the scratch marks, pits, holes, lumps and irregularities that were prevalent on the as-received stainless steel samples. The optimised laser polishing technology was consequently implemented for serial finishing of structured 3D printed mesoscale SS316L components. This led to substantial reductions in areal Sa and St parameters by 75% (0.489-0.126 μm) and 90% (17.71-1.21 μm) respectively, without compromising the geometrical accuracy of the native 3D printed samples.

Physics and Designs of Ignition Capsules Using High-Density Carbon (HDC) Ablators: Robust Designs, Stability, and Shock Mergers

NASA Astrophysics Data System (ADS)

Ho, D.; Salmonson, J.; Haan, S.; Clark, D.; Lindl, J.; Meezan, N.; Thomas, C.

2015-11-01

We present six ignition designs using W-doped HDC ablators with, respectively, 2, 3, and 4-step increases in Tr. Fuel adiabat α ranges between 1.5 and 4. The 4-step design has the lowest α of 1.5 but has the highest ablation front Rayleigh-Taylor (RT) growth. Consequently, the overall robustness of the 4-step design is inferior to the intermediate- α 3-step design, assuming typical currently measured surface roughness spectrum. As the foot level is increased further and the shocks merge inside the fuel, the fuel adiabat is raised to 4. The RT growth and mix are reduced but the 1D margin is decreased making it overall more susceptible to surface roughness. The 2-step α = 2.5 design turns out to be the most robust against surface roughness and still can deliver very high 1D yield of 14.5 MJ. Systematic evaluation of the robustness of these capsules with respect to low-mode radiation asymmetries, will also be discussed. Different paths to achieve low-convergence-ratio implosions (i.e. high velocity and high α as one option versus low velocity and low α as another option), while still giving respectable neutron yield will be presented. Finally, we discuss how the performance of these doped capsules changes; if the Au wall of the hohlraum is replaced by U. Work performed under auspices of U.S. DOE by LLNL under DE-AC52-07NA27344.

Possible Applications of 3D Printing Technology on Textile Substrates

NASA Astrophysics Data System (ADS)

Korger, M.; Bergschneider, J.; Lutz, M.; Mahltig, B.; Finsterbusch, K.; Rabe, M.

2016-07-01

3D printing is a rapidly emerging additive manufacturing technology which can offer cost efficiency and flexibility in product development and production. In textile production 3D printing can also serve as an add-on process to apply 3D structures on textiles. In this study the low-cost fused deposition modeling (FDM) technique was applied using different thermoplastic printing materials available on the market with focus on flexible filaments such as thermoplastic elastomers (TPE) or Soft PLA. Since a good adhesion and stability of the 3D printed structures on textiles are essential, separation force and abrasion resistance tests were conducted with different kinds of printed woven fabrics demonstrating that a sufficient adhesion can be achieved. The main influencing factor can be attributed to the topography of the textile surface affected by the weave, roughness and hairiness offering formlocking connections followed by the wettability of the textile surface by the molten polymer, which depends on the textile surface energy and can be specifically controlled by washing (desizing), finishing or plasma treatment of the textile before the print. These basic adhesion mechanisms can also be considered crucial for 3D printing on knitwear.

Model-based recognition of 3D articulated target using ladar range data.

PubMed

Lv, Dan; Sun, Jian-Feng; Li, Qi; Wang, Qi

2015-06-10

Ladar is suitable for 3D target recognition because ladar range images can provide rich 3D geometric surface information of targets. In this paper, we propose a part-based 3D model matching technique to recognize articulated ground military vehicles in ladar range images. The key of this approach is to solve the decomposition and pose estimation of articulated parts of targets. The articulated components were decomposed into isolate parts based on 3D geometric properties of targets, such as surface point normals, data histogram distribution, and data distance relationships. The corresponding poses of these separate parts were estimated through the linear characteristics of barrels. According to these pose parameters, all parts of the target were roughly aligned to 3D point cloud models in a library and fine matching was finally performed to accomplish 3D articulated target recognition. The recognition performance was evaluated with 1728 ladar range images of eight different articulated military vehicles with various part types and orientations. Experimental results demonstrated that the proposed approach achieved a high recognition rate.

Interfacial contact stiffness of fractal rough surfaces.

PubMed

Zhang, Dayi; Xia, Ying; Scarpa, Fabrizio; Hong, Jie; Ma, Yanhong

2017-10-09

In this work we describe a theoretical model that predicts the interfacial contact stiffness of fractal rough surfaces by considering the effects of elastic and plastic deformations of the fractal asperities. We also develop an original test rig that simulates dovetail joints for turbo machinery blades, which can fine tune the normal contact load existing between the contacting surfaces of the blade root. The interfacial contact stiffness is obtained through an inverse identification method in which finite element simulations are fitted to the experimental results. Excellent agreement is observed between the contact stiffness predicted by the theoretical model and by the analogous experimental results. We demonstrate that the contact stiffness is a power law function of the normal contact load with an exponent α within the whole range of fractal dimension D(1 < D < 2). We also show that for 1 < D < 1.5 the Pohrt-Popov behavior (α = 1/(3 - D)) is valid, however for 1.5 < D < 2, the exponent α is different and equal to 2(D - 1)/D. The diversity between the model developed in the work and the Pohrt-Popov one is explained in detail.

3D skin surface reconstruction from a single image by merging global curvature and local texture using the guided filtering for 3D haptic palpation.

PubMed

Lee, K; Kim, M; Kim, K

2018-05-11

Skin surface evaluation has been studied using various imaging techniques. However, all these studies had limited impact because they were performed using visual exam only. To improve on this scenario with haptic feedback, we propose 3D reconstruction of the skin surface using a single image. Unlike extant 3D skin surface reconstruction algorithms, we utilize the local texture and global curvature regions, combining the results for reconstruction. The first entails the reconstruction of global curvature, achieved by bilateral filtering that removes noise on the surface while maintaining the edge (ie, furrow) to obtain the overall curvature. The second entails the reconstruction of local texture, representing the fine wrinkles of the skin, using an advanced form of bilateral filtering. The final image is then composed by merging the two reconstructed images. We tested the curvature reconstruction part by comparing the resulting curvatures with measured values from real phantom objects while local texture reconstruction was verified by measuring skin surface roughness. Then, we showed the reconstructed result of our proposed algorithm via the reconstruction of various real skin surfaces. The experimental results demonstrate that our approach is a promising technology to reconstruct an accurate skin surface with a single skin image. We proposed 3D skin surface reconstruction using only a single camera. We highlighted the utility of global curvature, which has not been considered important in the past. Thus, we proposed a new method for 3D reconstruction that can be used for 3D haptic palpation, dividing the concepts of local and global regions. © 2018 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

Flow over a Biomimetic Surface Roughness Microgeometry

NASA Astrophysics Data System (ADS)

Warncke Lang, Amy; Hidalgo, Pablo; Westcott, Matthew

2006-11-01

Certain species of sharks (e.g. shortfin mako and common hammerhead) have a skin structure that could result in a bristling of their denticles (scales) during increased swimming speeds (Bechert, D. W., Bruse, M., Hage, W. and Meyer, R. 2000, Fluid mechanics of biological surfaces and their technological application. Naturwissenschaften 80:157-171). This unique surface geometry results in a three-dimensional array of cavities* (d-type roughness geometry) forming within the surface and has been given the acronym MAKO (Micro-roughness Array for Kinematic Optimization). Possible mechanisms leading to drag reduction over the shark's body by this unique roughness geometry include separation control thereby reducing pressure drag, skin friction reduction (via the `micro-air bearing' effect first proposed by Bushnell (AIAA 83-0227)), as well as possible transition delay in the boundary layer. Initial work is confined to scaling up the geometry from 0.2 mm on the shark skin to 2 cm, with a scaling down in characteristic velocity from 10 - 20 m/s to 10 - 20 cm/s for laminar flow boundary layer water tunnel studies. Support for this research by NSF SGER grant CTS-0630489 and a University of Alabama RAC grant is gratefully acknowledged. * Patent pending.

Accelerated aging effects on surface hardness and roughness of lingual retainer adhesives.

PubMed

Ramoglu, Sabri Ilhan; Usumez, Serdar; Buyukyilmaz, Tamer

2008-01-01

To test the null hypothesis that accelerated aging has no effect on the surface microhardness and roughness of two light-cured lingual retainer adhesives. Ten samples of light-cured materials, Transbond Lingual Retainer (3M Unitek) and Light Cure Retainer (Reliance) were cured with a halogen light for 40 seconds. Vickers hardness and surface roughness were measured before and after accelerated aging of 300 hours in a weathering tester. Differences between mean values were analyzed for statistical significance using a t-test. The level of statistical significance was set at P < .05. The mean Vickers hardness of Transbond Lingual Retainer was 62.8 +/- 3.5 and 79.6 +/- 4.9 before and after aging, respectively. The mean Vickers hardness of Light Cure Retainer was 40.3 +/- 2.6 and 58.3 +/- 4.3 before and after aging, respectively. Differences in both groups were statistically significant (P < .001). Following aging, mean surface roughness was changed from 0.039 microm to 0.121 microm and from 0.021 microm to 0.031 microm for Transbond Lingual Retainer and Light Cure Retainer, respectively. The roughening of Transbond Lingual Retainer with aging was statistically significant (P < .05), while the change in the surface roughness of Light Cure Retainer was not (P > .05). Accelerated aging significantly increased the surface microhardness of both light-cured retainer adhesives tested. It also significantly increased the surface roughness of the Transbond Lingual Retainer.

Surface roughness in XeF{sub 2} etching of a-Si/c-Si(100)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stevens, A.A.E.; Beijerinck, H.C.W.

2005-01-01

Single wavelength ellipsometry and atomic force microscopy (AFM) have been applied in a well-calibrated beam-etching experiment to characterize the dynamics of surface roughening induced by chemical etching of a {approx}12 nm amorphous silicon (a-Si) top layer and the underlying crystalline silicon (c-Si) bulk. In both the initial and final phase of etching, where either only a-Si or only c-Si is exposed to the XeF{sub 2} flux, we observe a similar evolution of the surface roughness as a function of the XeF{sub 2} dose proportional to D(XeF{sub 2}){sup {beta}} with {beta}{approx_equal}0.2. In the transition region from the pure amorphous to themore » pure crystalline silicon layer, we observe a strong anomalous increase of the surface roughness proportional to D(XeF{sub 2}){sup {beta}} with {beta}{approx_equal}1.5. Not only the growth rate of the roughness increases sharply in this phase, also the surface morphology temporarily changes to a structure that suggests a cusplike shape. Both features suggest that the remaining a-Si patches on the surface act effectively as a capping layer which causes the growth of deep trenches in the c-Si. The ellipsometry data on the roughness are corroborated by the AFM results, by equating the thickness of the rough layer to 6 {sigma}, with {sigma} the root-mean-square variation of the AFM's distribution function of height differences. In the AFM data, the anomalous behavior is reflected in a too small value of {sigma} which again suggests narrow and deep surface features that cannot be tracked by the AFM tip. The final phase morphology is characterized by an effective increase in surface area by a factor of two, as derived from a simple bilayer model of the reaction layer, using the experimental etch rate as input. We obtain a local reaction layer thickness of 1.5 monolayer consistent with the 1.7 ML value of Lo et al. [Lo et al., Phys. Rev. B 47, 648 (1993)] that is also independent of surface roughness.« less

A Two-stage Improvement Method for Robot Based 3D Surface Scanning

NASA Astrophysics Data System (ADS)

He, F. B.; Liang, Y. D.; Wang, R. F.; Lin, Y. S.

2018-03-01

As known that the surface of unknown object was difficult to measure or recognize precisely, hence the 3D laser scanning technology was introduced and used properly in surface reconstruction. Usually, the surface scanning speed was slower and the scanning quality would be better, while the speed was faster and the quality would be worse. In this case, the paper presented a new two-stage scanning method in order to pursuit the quality of surface scanning in a faster speed. The first stage was rough scanning to get general point cloud data of object’s surface, and then the second stage was specific scanning to repair missing regions which were determined by chord length discrete method. Meanwhile, a system containing a robotic manipulator and a handy scanner was also developed to implement the two-stage scanning method, and relevant paths were planned according to minimum enclosing ball and regional coverage theories.

Capillary-induced crack healing between surfaces of nanoscale roughness.

PubMed

Soylemez, Emrecan; de Boer, Maarten P

2014-10-07

Capillary forces are important in nature (granular materials, insect locomotion) and in technology (disk drives, adhesion). Although well studied in equilibrium state, the dynamics of capillary formation merit further investigation. Here, we show that microcantilever crack healing experiments are a viable experimental technique for investigating the influence of capillary nucleation on crack healing between rough surfaces. The average crack healing velocity, v̅, between clean hydrophilic polycrystalline silicon surfaces of nanoscale roughness is measured. A plot of v̅ versus energy release rate, G, reveals log-linear behavior, while the slope |d[log(v̅)]/dG| decreases with increasing relative humidity. A simplified interface model that accounts for the nucleation time of water bridges by an activated process is developed to gain insight into the crack healing trends. This methodology enables us to gain insight into capillary bridge dynamics, with a goal of attaining a predictive capability for this important microelectromechanical systems (MEMS) reliability failure mechanism.

Bottom-up Fabrication of Multilayer Stacks of 3D Photonic Crystals from Titanium Dioxide.

PubMed

Kubrin, Roman; Pasquarelli, Robert M; Waleczek, Martin; Lee, Hooi Sing; Zierold, Robert; do Rosário, Jefferson J; Dyachenko, Pavel N; Montero Moreno, Josep M; Petrov, Alexander Yu; Janssen, Rolf; Eich, Manfred; Nielsch, Kornelius; Schneider, Gerold A

2016-04-27

A strategy for stacking multiple ceramic 3D photonic crystals is developed. Periodically structured porous films are produced by vertical convective self-assembly of polystyrene (PS) microspheres. After infiltration of the opaline templates by atomic layer deposition (ALD) of titania and thermal decomposition of the polystyrene matrix, a ceramic 3D photonic crystal is formed. Further layers with different sizes of pores are deposited subsequently by repetition of the process. The influence of process parameters on morphology and photonic properties of double and triple stacks is systematically studied. Prolonged contact of amorphous titania films with warm water during self-assembly of the successive templates is found to result in exaggerated roughness of the surfaces re-exposed to ALD. Random scattering on rough internal surfaces disrupts ballistic transport of incident photons into deeper layers of the multistacks. Substantially smoother interfaces are obtained by calcination of the structure after each infiltration, which converts amorphous titania into the crystalline anatase before resuming the ALD infiltration. High quality triple stacks consisting of anatase inverse opals with different pore sizes are demonstrated for the first time. The elaborated fabrication method shows promise for various applications demanding broadband dielectric reflectors or titania photonic crystals with a long mean free path of photons.

Changes to Glazed Dental Ceramic Shade, Roughness, and Microhardness after Bleaching and Simulated Brushing.

PubMed

Rodrigues, Carlos Roberto Teixeira; Turssi, Cecilia Pedroso; Amaral, Flávia Lucisano Botelho; Basting, Roberta Tarkany; França, Fabiana Mantovani Gomes

2017-09-05

To evaluate shade stability, surface roughness, microhardness, and compressive strength of a glazed feldspathic ceramic subjected to bleaching and simulated brushing. Eighty-eight glazed feldspathic ceramic specimens were made from microparticulate leucite and divided into eight groups (n = 10). The whitening products used were: Opalescence Trèswhite Supreme (Ultradent), Opalescence®\\ PF 15% (Ultradent), and Oral-B 3D White Whitestrips. All substances for whitening were used for 4 hours/day for a period of 14 days; the control group was not bleached. Next, half of the specimens were individually brushed. Microhardness and surface roughness data were subjected to three-way ANOVA and Tukey test. The diametrical tensile strength data were subjected to two-way ANOVA. The shade change data were analyzed using Kruskal-Wallis, Mann-Whitney, and the Student-Newman-Keuls test. The significance level was set at 5%. Glazed feldspathic ceramic surface microhardness was significantly affected by bleaching agents (p = 0.007). Initially, glazed ceramic microhardness was significantly higher than that observed after contact with the bleaching agents, whether or not brushing was performed. The specimens submitted to bleaching in preloaded trays presented lower surface roughness values after brushing (p = 0.037). The surface roughness was significantly lower in the brushed specimens (p = 0.044). The diametrical tensile strength was not significantly affected by the application of bleaching agents (p = 0.563) or by brushing (p = 0.477). When the specimens were brushed, however, shade change was significantly influenced by the bleaching agent used (p = 0.041). Bleaching agents associated with brushing cycles can alter surface properties and shade stability of glazed feldspathic ceramics, though such findings may not reflect the performance of unglazed feldspathic ceramics. © 2017 by the American College of Prosthodontists.

Quantitative analysis of fracture surface by roughness and fractal method

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, X.W.; Tian, J.F.; Kang, Y.

1995-09-01

In recent years there has been extensive research and great development in Quantitative Fractography, which acts as an integral part of fractographic analysis. A prominent technique for studying the fracture surface is based on fracture profile generation and the major means for characterizing the profile quantitatively are roughness and fractal methods. By this way, some quantitative indexes such as the roughness parameters R{sub L} for profile and R{sub S} for surface, fractal dimensions D{sub L} for profile and D{sub S} for surface can be measured. Given the relationships between the indexes and the mechanical properties of materials, it is possiblemore » to achieve the goal of protecting materials from fracture. But, as the case stands, the theory and experimental technology of quantitative fractography are still imperfect and remain to be studied further. Recently, Gokhale and Underwood et al have proposed an assumption-free method for estimating the surface roughness by vertically sectioning the fracture surface with sections at an angle of 120 deg with each other, which could be expressed as follows: R{sub S} = {ovr R{sub L}{center_dot}{Psi}} where {Psi} is the profile structure factor. This method is based on the classical sterological principles and verified with the aid of computer simulations for some ruled surfaces. The results are considered to be applicable to fracture surfaces with any arbitrary complexity and anisotropy. In order to extend the detail applications to this method in quantitative fractography, the authors made a study on roughness and fractal methods dependent on this method by performing quantitative measurements on some typical low-temperature impact fractures.« less

Light transmittance and surface roughness of a feldspathic ceramic CAD-CAM material as a function of different surface treatments.

PubMed

Ural, Çağrı; Duran, İbrahim; Evmek, Betül; Kavut, İdris; Cengiz, Seda; Yuzbasioglu, Emir

2016-07-15

The aim of the present study was to determine the effect of different surface treatments on light transmission of aesthetic feldspathic ceramics used in CAD-CAM chairside restorations. Forty eight feldspatic ceramic test specimens were prepared from prefabricated CAD-CAM blocks by using a slow speed diamond saw. Test specimens were prepared and divided into 4 groups (n = 12). In the control group, no surface treatments were applied on the feldspathic ceramic surfaces. In the hydrofluoric acid group, the bonding surfaces of feldspathic ceramics were etched with 9.5 % hydrofluoric acid. In the sandblasting group the feldspathic ceramic surfaces were air-abraded with 30-μm alumium oxide (Al2O3) particles and Er:YAG laser was used to irradiate the ceramic surfaces. The incident light power given by the LED device and the transmitted light power through each ceramic sample was registered using a digital LED radiometer device. Each polymerization light had a light guide with 8-mm-diameter tips. Light transmission of feldspathic ceramic samples was determined by placing it on the radiometer and irradiating the specimen for 10 s at the highest setting for each light polymerization. All specimens were coated with gold using a sputter coater and examined under a field emission scanning electron microscope. Surface roughness measurement each group were evaluated with 3D optical surface and tactile profilometers. One-way ANOVA test results revealed that both surface conditioning method significantly affect the light transmittance (F:412.437; p < 0.001) and the surface roughness values (F:16.386; p < 0.001). Al2O3 and Er-YAG laser application reduced the light transmission significantly (p < 0.05). The laser and Al2O3 applications reduced the light transmission of 1.5 mm thickness feldspathic ceramic material below the value of 400 mW/cm(2) which is critical limit for safe polymerization.

Surface modification and deuterium retention in reduced-activation steels under low-energy deuterium plasma exposure. Part I: undamaged steels

NASA Astrophysics Data System (ADS)

Ogorodnikova, O. V.; Zhou, Z.; Sugiyama, K.; Balden, M.; Gasparyan, Yu.; Efimov, V.

2017-03-01

In this paper, reduced-activation ferritic/martensitic (RAFM) steels including Eurofer (9Cr) and oxide dispersion strengthening (ODS) steels by the addition of Y2O3 particles with different amounts of Cr, namely, (9-16)Cr were exposed to low energy deuterium (D) plasma (~20-200 eV per D) up to a fluence of 2.9  ×  1025 D m-2 in the temperature range from 290 K to 700 K. The depth profile of D in steels was measured up to 8 µm depth by nuclear reaction analysis (NRA) and the total retained amount of D in those materials was determined by thermal desorption spectroscopy (TDS). It was found that the D retention in ODS steels is higher compared to Eurofer due to the much higher density of fine dispersoids and finer grain size. This work shows that in addition to the sintering temperature and time, the type, size and concentration of the doping particles have an enormous effect on the increase in the D retention. The D retention in undamaged ODS steels strongly depends on the Cr content: ODS with 12Cr has a minimum and the D retention in the case of ODS with (14-16)Cr is higher compared to (9-12)Cr. The replacing of Ti by Al in ODS-14Cr steels reduces the D retention. The formation of nano-structure surface roughness enriched in W or Ta due to combination of preferential sputtering of light elements and radiation-induced segregation was observed at incident D ion energy of 200 eV for both Eurofer and ODS steels. Both the surface roughness and the eroded layer enhance with increasing the temperature. The surface modifications result in a reduction of the D retention near the surface due to increasing the desorption flux and can reduce the overall D retention.

Microscopic Holography for flow over rough plate

NASA Astrophysics Data System (ADS)

Talapatra, Siddharth; Hong, Jiarong; Lu, Yuan; Katz, Joseph

2008-11-01

Our objective is to measure the near wall flow structures in a turbulent channel flow over a rough wall. In-line microscopic holographic PIV can resolve the 3-D flow field in a small sample volume, but recording holograms through a rough surface is a challenge. To solve this problem, we match the refractive indices of the fluid with that of the wall. Proof of concept tests involve an acrylic plate containing uniformly distributed, closely packed 0.45mm high pyramids with slope angle of 22^^o located within a concentrated sodium iodide solution. Holograms recorded by a 4864 x 3248 pixel digital camera at 10X magnification provide a field of view of 3.47mm x 2.32mm and pixel resolution of 0.714 μm. Due to index matching, reconstructed seed particles can be clearly seen over the entire volume, with only faint traces with the rough wall that can be removed. Planned experiments will be performed in a 20 x 5 cm rectangular channel with the top and bottom plates having the same roughness as the sample plate.

The improvement of surface roughness by polishing method of arcylic door panel at Taishi Tech Sdn Bhd

NASA Astrophysics Data System (ADS)

Basirin, Hammadi bin Mohd; Nawi, Ismail bin Haji Mohd

2017-04-01

This research is an approach to improve the surface roughness for acrylic door panel by using polishing process. The polishing process involve is sanding process by 3 types of sand paper. The sanding process used to improve the surface roughness by using the different grit sizes of sand paper. The experiment was done by using two types of material s, that is plywood and medium density board (MDF). These two materials are the main materials in producing the arcrylic door panel. The surface roughness of these two materials affects the qualities and quantities of the acrylic door panel. The surface structure was measured by using Optical Microscope and Scanning Electron Microscope (SEM) and the surface roughness was measured by using Mitutoyo surfest SJ 400 Tester. Results indicates that using the different types of grit are influence the surface roughness of the material. When the higher types of grit sizes had been used, the average roughness of the surface are decrease. In summary, a good surface roughness condition produced when using the higher types of grit sizes sand paper.

A novel approach of magnetorheological abrasive fluid finishing with swirling-assisted inlet flow

NASA Astrophysics Data System (ADS)

Kheradmand, Saeid; Esmailian, Mojtaba; Fatahy, A.

Abrasive flow machining has been the pioneer of new finishing processes. Rotating workpiece and imposing a magnetic field using magnetorheological working medium are some assisting manipulations to improve surface finishing, because they can increase the forces on the workpiece surface. Similarly, swirling the inlet flow using stationary swirler vanes, as a novel idea, may also increase forces on the surface, and then raise the material removal, with a lower expense and energy consumption compared with the case of workpiece rotation. Thus, in this paper, surface roughness improvement is studied in a pipe with rotating inlet flow of a magnetorheological finishing medium under imposing a magnetic field. The results are compared with the case of rotating workpiece, using 3D numerical simulation. The governing hydrodynamic parameters are investigated in both cases to monitor the flow variations. It is shown that surface roughness is improved by rotating inlet flow. However, it is found that finishing in the entrance length of swirling-assisted inlet flow can be so economical for short length workpieces, compared with the case of rotating workpiece, with very near Ra values. By comparison of the numerical results and published experimental data, current study also shows the ability of the numerical simulation, as an inexpensive and efficient tool, to predict the surface roughness changes in finishing processes.

The machined surface of magnesium AZ31 after rotary turning at air cooling condition

NASA Astrophysics Data System (ADS)

Akhyar, G.; Purnomo, B.; Hamni, A.; Harun, S.; Burhanuddin, Y.

2018-04-01

Magnesium is a lightweight metal that is widely used as an alternative to iron and steel. Magnesium has been applied in the automotive industry to reduce the weight of a component, but the machining process has the disadvantage that magnesium is highly flammable because it has a low flash point. High temperature can cause the cutting tool wear and contributes to the quality of the surface roughness. The purpose of this study is to obtain the value of surface roughness and implement methods of rotary cutting tool and air cooling output vortex tube cooler to minimize the surface roughness values. Machining parameters that is turning using rotary cutting tool at speed the workpiece of (Vw) 50, 120, 160 m/min, cutting speed of rotary tool of (Vt) 25, 50, 75 m/min, feed rate of (f) 0.1, 0.15, 0.2 mm/rev, and depth of cut of 0.3 mm. Type of tool used is a carbide tool diameter of 16 mm and air cooling pressure of 6 bar. The results show the average value of the lowest surface roughness on the speed the workpiece of 80 m/min, cutting speed of rotary tool of 50 m/min, feed rate of 0.2 mm/rev, and depth of cut of 0.3 mm. While the average value of the highest surface roughness on the speed the workpiece of 160 m/min, cutting speed of rotary tool of 50 m/min, feed rate of 0.2 mm/rev, and depth of cut of 0.3 mm. The influence of machining parameters concluded the higher the speed of the workpiece the surface roughness value higher. Otherwise the higher cutting speed of rotary tool then the lower the surface roughness value. The observation on the surface of the rotary tool, it was found that no uniform tool wear which causes non-uniform surface roughness. The use of rotary cutting tool contributing to lower surface roughness values generated.

Etidronate from Medicine to Endodontics: effects of different irrigation regimes on root dentin roughness

PubMed Central

TARTARI, Talita; DUARTE JUNIOR, Anivaldo Pereira; SILVA JÚNIOR, José Otávio Carrera; KLAUTAU, Eliza Burlamaqui; SILVA E SOUZA JUNIOR, Mario Honorato; SILVA E SOUZA, Patrícia de Almeida Rodrigues

2013-01-01

An increase in dentin roughness, associated with surface composition, contributes to bacterial adherence in recontaminations. Surface roughness is also important for micromechanical interlocking of dental materials to dentin, and understanding the characteristics of the surface is essential to obtain the adhesion of root canal sealers that have different physico-chemical characteristics. Objectives To evaluate the effects of sodium hypochlorite (NaOCl), ethylenediaminetetraacetic (EDTA), etidronic (HEBP), and citric acid (CA) associated with different irrigation regimens on root dentin roughness. Material and Methods Forty-five root halves of anterior teeth were used. The root parts were sectioned in thirds, embedded in acrylic resin and polished to a standard surface roughness. Initially, the samples of each third were randomly assigned into 3 groups and treated as follows: G1 - saline solution (control); G2 - 5% NaOCl+18% HEBP mixed in equal parts; and G3 - 2.5% NaOCl. After initial measuments, the G3 samples were distributed into subgroups G4, G5 and G6, which were subjected to 17% EDTA, 10% CA and 9% HEBP, respectively. Following the new measuments, these groups received a final flush with 2.5% NaOCl, producing G7, G8 and G9. The dentin surface roughness (Ra) was determined before and after treatments using a profilometer. The Wilcoxon test (α<0.05) was used to compare the values before and after treatments, and the Friedman test (α<0.05) to detect any differences among root thirds. Results (i) NaOCl did not affect the surface roughness; (ii) there was a significant increase in roughness after the use of chelating agents (P<0.01); and (iii) only the G3 group showed a difference in surface roughness between apical third and other thirds of the teeth (P<0.0043). Conclusion Only the irrigation regimens that used chelating agents altered the roughness of root dentin. PMID:24212986

Etidronate from medicine to endodontics: effects of different irrigation regimes on root dentin roughness.

PubMed

Tartari, Talita; Duarte Junior, Anivaldo Pereira; Silva Júnior, José Otávio Carrera; Klautau, Eliza Burlamaqui; Silva E Souza Junior, Mario Honorato; Silva E Souza Junior, Patrícia de Almeida Rodrigues

2013-01-01

An increase in dentin roughness, associated with surface composition, contributes to bacterial adherence in recontaminations. Surface roughness is also important for micromechanical interlocking of dental materials to dentin, and understanding the characteristics of the surface is essential to obtain the adhesion of root canal sealers that have different physico-chemical characteristics. To evaluate the effects of sodium hypochlorite (NaOCl), ethylenediaminetetraacetic (EDTA), etidronic (HEBP), and citric acid (CA) associated with different irrigation regimens on root dentin roughness. Forty-five root halves of anterior teeth were used. The root parts were sectioned in thirds, embedded in acrylic resin and polished to a standard surface roughness. Initially, the samples of each third were randomly assigned into 3 groups and treated as follows: G1 - saline solution (control); G2 - 5% NaOCl+18% HEBP mixed in equal parts; and G3 - 2.5% NaOCl. After initial measuments, the G3 samples were distributed into subgroups G4, G5 and G6, which were subjected to 17% EDTA, 10% CA and 9% HEBP, respectively. Following the new measuments, these groups received a final flush with 2.5% NaOCl, producing G7, G8 and G9. The dentin surface roughness (Ra) was determined before and after treatments using a profilometer. The Wilcoxon test (α<0.05) was used to compare the values before and after treatments, and the Friedman test (α<0.05) to detect any differences among root thirds. (i) NaOCl did not affect the surface roughness; (ii) there was a significant increase in roughness after the use of chelating agents (P<0.01); and (iii) only the G3 group showed a difference in surface roughness between apical third and other thirds of the teeth (P<0.0043). Only the irrigation regimens that used chelating agents altered the roughness of root dentin.

Surface degradation of glass ceramics after exposure to acidulated phosphate fluoride

PubMed Central

CCAHUANA, Vanessa Zulema S.; ÖZCAN, Mutlu; MESQUITA, Alfredo Mikail Melo; NISHIOKA, Renato Sussumo; KIMPARA, Estevão Tomomitsu; BOTTINO, Marco Antonio

2010-01-01

Objective This study evaluated the surface degradation effect of acidulated phosphate fluoride (APF) gel exposure on the glassy matrix ceramics as a function of time. Material and methods Disc-shaped ceramic specimens (N = 120, 10/per ceramic material) were prepared in stainless steel molds (inner diameter: 5 mm, height: 2 mm) using 6 dental ceramics: 3 indicated for ceramic-fused-to-metal (Vita Omega 900, Carmen and Vita Titankeramik), 2 for all-ceramic (Vitadur Alpha and Finesse® Low Fusing) and 1 for both types of restorations (IPS d.SIGN). The specimens were wet ground finished, ultrasonically cleaned and auto-glazed. All specimens were subjected to calculation of percentage of mass loss, surface roughness analysis and topographical description by scanning electron microscopy (SEM) before (0 min) and after exposure to 1.23 % APF gel for 4 min and 60 min representing short- and long-term etching effect, respectively. The data were analyzed using two-way ANOVA with repeated measures and Tukey`s test (α=0.05). Results Significant effect of the type of the ceramics (p=0.0000, p=0.0031) and exposure time (p=0.0000) was observed in both surface roughness and percentage of mass loss values, respectively. The interaction factor between both parameters was also significant for both parameters (p=0.0904, p=0.0258). Both 4 min (0.44±0.1 - 0.81±0.2 µm) and 60 min (0.66±0.1 - 1.04±0.3 µm) APF gel exposure created significantly more surface roughness for all groups when compared to the control groups (0.33±0.2 - 0.68±0.2 µm) (p<0.05). There were no significant differences in percentage of mass loss between the ceramics at 4 min (p>0.05) but at 60 min exposure, IPS d.SIGN showed the highest percentage of mass loss (0.1151±0.11). The mean surface roughness for Vita Titankeramik (0.84±0.2 µm) and Finesse® Low Fusing (0.74.±0.2 µm) was significantly higher than those of the other ceramics (0.59±0.1 µm - 0.49±0.1 µm) and Vita Titankeramik (p<0.05) regardless of the exposure time. A positive correlation was found between surface roughness and percentage of mass loss for all ceramic materials [(r=0.518 (Vitadur Alpha), r=0.405 (Vita Omega 900), r=0.580 (Carmen), r=0.687 (IPS d.SIGN), r=0.442 (Finesse® Low Fusing), r=0.572 (Vita Titankeramik), Pearson`s correlation coefficient)]. The qualitative SEM analysis showed evidence of corrosive attack on all of ceramics at varying degrees. Conclusions The ceramics indicated for either metal-ceramic or all-ceramic restorations were all vulnerable to surface texture changes and mass loss after short-term and long-term APF gel exposure. PMID:20485927

Generalizing roughness: experiments with flow-oriented roughness

NASA Astrophysics Data System (ADS)

Trevisani, Sebastiano

2015-04-01

Surface texture analysis applied to High Resolution Digital Terrain Models (HRDTMs) improves the capability to characterize fine-scale morphology and permits the derivation of useful morphometric indexes. An important indicator to be taken into account in surface texture analysis is surface roughness, which can have a discriminant role in the detection of different geomorphic processes and factors. The evaluation of surface roughness is generally performed considering it as an isotropic surface parameter (e.g., Cavalli, 2008; Grohmann, 2011). However, surface texture has often an anisotropic character, which means that surface roughness could change according to the considered direction. In some applications, for example involving surface flow processes, the anisotropy of roughness should be taken into account (e.g., Trevisani, 2012; Smith, 2014). Accordingly, we test the application of a flow-oriented directional measure of roughness, computed considering surface gravity-driven flow. For the calculation of flow-oriented roughness we use both classical variogram-based roughness (e.g., Herzfeld,1996; Atkinson, 2000) as well as an ad-hoc developed robust modification of variogram (i.e. MAD, Trevisani, 2014). The presented approach, based on a D8 algorithm, shows the potential impact of considering directionality in the calculation of roughness indexes. The use of flow-oriented roughness could improve the definition of effective proxies of impedance to flow. Preliminary results on the integration of directional roughness operators with morphometric-based models, are promising and can be extended to more complex approaches. Atkinson, P.M., Lewis, P., 2000. Geostatistical classification for remote sensing: an introduction. Computers & Geosciences 26, 361-371. Cavalli, M. & Marchi, L. 2008, "Characterization of the surface morphology of an alpine alluvial fan using airborne LiDAR", Natural Hazards and Earth System Science, vol. 8, no. 2, pp. 323-333. Grohmann, C.H., Smith, M.J., Riccomini, C., 2011. Multiscale Analysis of Topographic Surface Roughness in the Midland Valley, Scotland. IEEE Transactions on Geoscience and Remote Sensing 49, 1220-1213. Herzfeld, U.C., Higginson, C.A., 1996. Automated geostatistical seafloor classification - Principles, parameters, feature vectors, and discrimination criteria. Computers and Geosciences, 22 (1), pp. 35-52. Smith, M.W. 2014, "Roughness in the Earth Sciences", Earth-Science Reviews, vol. 136, pp. 202-225. Trevisani, S., Cavalli, M. & Marchi, L. 2012, "Surface texture analysis of a high-resolution DTM: Interpreting an alpine basin", Geomorphology, vol. 161-162, pp. 26-39. Trevisani S., Rocca M., 2014. Geomorphometric analysis of fine-scale morphology for extensive areas: a new surface-texture operator. Geophysical Research Abstracts, Vol. 16, EGU2014-5612, 2014. EGU General Assembly 2014.

Nanoscale Roughness and Morphology Affect the IsoElectric Point of Titania Surfaces

PubMed Central

Borghi, Francesca; Vyas, Varun; Podestà, Alessandro; Milani, Paolo

2013-01-01

We report on the systematic investigation of the role of surface nanoscale roughness and morphology on the charging behaviour of nanostructured titania (TiO2) surfaces in aqueous solutions. IsoElectric Points (IEPs) of surfaces have been characterized by direct measurement of the electrostatic double layer interactions between titania surfaces and the micrometer-sized spherical silica probe of an atomic force microscope in NaCl aqueous electrolyte. The use of a colloidal probe provides well-defined interaction geometry and allows effectively probing the overall effect of nanoscale morphology. By using supersonic cluster beam deposition to fabricate nanostructured titania films, we achieved a quantitative control over the surface morphological parameters. We performed a systematical exploration of the electrical double layer properties in different interaction regimes characterized by different ratios of characteristic nanometric lengths of the system: the surface rms roughness Rq, the correlation length ξ and the Debye length λD. We observed a remarkable reduction by several pH units of IEP on rough nanostructured surfaces, with respect to flat crystalline rutile TiO2. In order to explain the observed behavior of IEP, we consider the roughness-induced self-overlap of the electrical double layers as a potential source of deviation from the trend expected for flat surfaces. PMID:23874708

Surface thermophysical properties on the potentially hazardous asteroid (99942) Apophis

NASA Astrophysics Data System (ADS)

Yu, Liang-Liang; Ji, Jianghui; Ip, Wing-Huen

2017-07-01

We investigate the surface thermophysical properties (thermal emissivity, thermal inertia, roughness fraction and geometric albedo) of asteroid (99942) Apophis, using the currently available mid-infrared observations from CanariCam on Gran Telescopio CANARIAS and far-infrared data from PACS on Herschel, based on the Advanced Thermophysical Model. We show that the thermal emissivity of Apophis should be wavelength dependent from 8.70 μm to 160 μm, and the maximum emissivity may appear around 20 μm, similar to that of Vesta. Moreover, we further derive the thermal inertia, roughness fraction, geometric albedo and effective diameter of Apophis within a possible 1σ scale of Γ ={100}-52+100{{{Jm}}}{{-}2} {{{s}}}{{-}0.{{5}}} {{{K}}}{{-}1}, {f}{{r}}=0.78˜ 1.0, {p}{{v}}={0.286}-0.026+0.030 and {D}{{eff}}={378}-25+19{{m}}, and 3σ scale of Γ ={100}-100+240 {{{Jm}}}{{-}2} {{{s}}}{{-}0.{{5}}} {{{K}}}{{-}1}, {f}{{r}}=0.2˜ 1.0, {p}{{v}}={0.286}-0.029+0.039 and {D}{{eff}}={378}-29+27{{m}}. The derived low thermal inertia but high roughness fraction may imply that Apophis could have regolith on its surface, where stronger space weathering but weaker regolith migration has happened in comparison with asteroid Itokawa. Our results show that small-size asteroids could also have fine regolith on the surface, and further infer that Apophis may have been delivered from the Main Belt by the Yarkovsky effect.

Phase-field study of grain boundary tracking behavior in crack-seal microstructures

NASA Astrophysics Data System (ADS)

Ankit, Kumar; Nestler, Britta; Selzer, Michael; Reichardt, Mathias

2013-12-01

In order to address the growth of crystals in veins, a multiphase-field model is used to capture the dynamics of crystals precipitating from a super-saturated solution. To gain a detailed understanding of the polycrystal growth phenomena in veins, we investigate the influence of various boundary conditions on crystal growth. In particular, we analyze the formation of vein microstructures resulting from the free growth of crystals as well as crack-sealing processes. We define the crystal symmetry by considering the anisotropy in surface energy to simulate crystals with flat facets and sharp corners. The resulting growth competition of crystals with different orientations is studied to deduce a consistent orientation selection rule in the free-growth regime. Using crack-sealing simulations, we correlate the grain boundary tracking behavior depending on the relative rate of crack opening, opening trajectory, initial grain size, and wall roughness. Further, we illustrate how these parameters induce the microstructural transition between blocky (crystals growing anisotropically) to fibrous morphology (isotropic) and formation of grain boundaries. The phase-field simulations of crystals in the free-growth regime (in 2D and 3D) indicate that the growth or consumption of a crystal is dependent on the orientation difference with neighboring crystals. The crack-sealing simulation results (in 2D and 3D) reveal that crystals grow isotropically and grain boundaries track the opening trajectory if the wall roughness is high, opening increments are small, and crystals touch the wall before the next crack increment starts. Further, we find that within the complete crack-seal regime, anisotropy in surface energy results in the formation of curved/oscillating grain boundaries (instead of straight) when the crack-opening velocity is increased and wall roughness is not sufficiently high. Additionally, the overall capability of phase-field method to simulate large-scale polycrystal growth in veins (in 3D) is demonstrated enumerating the main advantages of adopting the novel approach.

An effective medium approach to predict the apparent contact angle of drops on super-hydrophobic randomly rough surfaces.

PubMed

Bottiglione, F; Carbone, G

2015-01-14

The apparent contact angle of large 2D drops with randomly rough self-affine profiles is numerically investigated. The numerical approach is based upon the assumption of large separation of length scales, i.e. it is assumed that the roughness length scales are much smaller than the drop size, thus making it possible to treat the problem through a mean-field like approach relying on the large-separation of scales. The apparent contact angle at equilibrium is calculated in all wetting regimes from full wetting (Wenzel state) to partial wetting (Cassie state). It was found that for very large values of the roughness Wenzel parameter (r(W) > -1/ cos θ(Y), where θ(Y) is the Young's contact angle), the interface approaches the perfect non-wetting condition and the apparent contact angle is almost equal to 180°. The results are compared with the case of roughness on one single scale (sinusoidal surface) and it is found that, given the same value of the Wenzel roughness parameter rW, the apparent contact angle is much larger for the case of a randomly rough surface, proving that the multi-scale character of randomly rough surfaces is a key factor to enhance superhydrophobicity. Moreover, it is shown that for millimetre-sized drops, the actual drop pressure at static equilibrium weakly affects the wetting regime, which instead seems to be dominated by the roughness parameter. For this reason a methodology to estimate the apparent contact angle is proposed, which relies only upon the micro-scale properties of the rough surface.

Simulation of an oil film at the sea surface and its radiometric properties in the SWIR

NASA Astrophysics Data System (ADS)

Schwenger, Frédéric; Van Eijk, Alexander M. J.

2017-10-01

The knowledge of the optical contrast of an oil layer on the sea under various surface roughness conditions is of great interest for oil slick monitoring techniques. This paper presents a 3D simulation of a dynamic sea surface contaminated by a floating oil film. The simulation considers the damping influence of oil on the ocean waves and its physical properties. It calculates the radiance contrast of the sea surface polluted by the oil film in relation to a clean sea surface for the SWIR spectral band. Our computer simulation combines the 3D simulation of a maritime scene (open clear sea/clear sky) with an oil film at the sea surface. The basic geometry of a clean sea surface is modeled by a composition of smooth wind driven gravity waves. Oil on the sea surface attenuates the capillary and short gravity waves modulating the wave power density spectrum of these waves. The radiance of the maritime scene is calculated in the SWIR spectral band with the emitted sea surface radiance and the specularly reflected sky radiance as components. Wave hiding and shadowing, especially occurring at low viewing angles, are considered. The specular reflection of the sky radiance at the clean sea surface is modeled by an analytical statistical bidirectional reflectance distribution function (BRDF) of the sea surface. For oil at the sea surface, a specific BRDF is used influenced by the reduced surface roughness, i.e., the modulated wave density spectrum. The radiance contrast of an oil film in relation to the clean sea surface is calculated for different viewing angles, wind speeds, and oil types characterized by their specific physical properties.

Evaluating the Whitening and Microstructural Effects of a Novel Whitening Strip on Porcelain and Composite Dental Materials

PubMed Central

Takesh, Thair; Sargsyan, Anik; Lee, Matthew; Anbarani, Afarin; Ho, Jessica; Wilder-Smith, Petra

2017-01-01

Aims The aim of this project was to evaluate the effects of 2 different whitening strips on color, microstructure and roughness of tea stained porcelain and composite surfaces. Methods 54 porcelain and 72 composite chips served as samples for timed application of over-the-counter (OTC) test or control dental whitening strips. Chips were divided randomly into three groups of 18 porcelain and 24 composite chips each. Of these groups, 1 porcelain and 1 composite set served as controls. The remaining 2 groups were randomized to treatment with either Oral Essentials® Whitening Strips or Crest® 3D White Whitestrips™. Sample surface structure was examined by light microscopy, profilometry and Scanning Electron Microscopy (SEM). Additionally, a reflectance spectrophotometer was used to assess color changes in the porcelain and composite samples over 24 hours of whitening. Data points were analyzed at each time point using ANOVA. Results In the light microscopy and SEM images, no discrete physical defects were observed in any of the samples at any time points. However, high-resolution SEM images showed an appearance of increased surface roughness in all composite samples. Using profilometry, significantly increased post-whitening roughness was documented in the composite samples exposed to the control bleaching strips. Composite samples underwent a significant and equivalent shift in color following exposure to Crest® 3D White Whitestrips™ and Oral Essentials® Whitening Strips. Conclusions A novel commercial tooth whitening strip demonstrated a comparable beaching effect to a widely used OTC whitening strip. Neither whitening strip caused physical defects in the sample surfaces. However, the control strip caused roughening of the composite samples whereas the test strip did not. PMID:29226023

Topological and morphological analysis of gamma rays irradiated chitosan-poly (vinyl alcohol) blends using atomic force microscopy

NASA Astrophysics Data System (ADS)

Bhatt, Rinkesh; Bisen, D. S.; Bajpai, R.; Bajpai, A. K.

2017-04-01

In the present communication, binary blends of poly (vinyl alcohol) (PVA) and chitosan (CS) were prepared by solution cast method and the roughness parameters of PVA, native CS and CS-PVA blend films were determined using atomic force microscopy (AFM). Moreover, the changes in the morphology of the samples were also investigated after irradiation of gamma rays at absorbed dose of 1 Mrad and 10 Mrad for the scanning areas of 5×5 μm2, 10×10 μm2 and 20×20 μm2. Amplitude, statistical and spatial parameters, including line, 3D and 2D image profiles of the experimental surfaces were examined and compared to un-irradiated samples. For gamma irradiated CS-PVA blends the larger waviness over the surface was found as compared to un-irradiated CS-PVA blends but the values of average roughness for both the films were found almost same. The coefficient of skewness was positive for gamma irradiated CS-PVA blends which revealed the presence of more peaks than valleys on the blend surfaces.

Flow Measurements over a Biomimetic Surface Roughness Microgeometry

NASA Astrophysics Data System (ADS)

Lang, Amy; Hidalgo, Pablo; Westcott, Matthew

2007-11-01

Certain species of sharks (e.g. shortfin mako) have a skin structure that results in a bristling of their denticles (scales) during increased swimming speeds. This unique surface geometry results in the formation of a 3D array of cavities* (d-type roughness geometry) within the shark skin, thus causing it to potentially act as a means of boundary layer control. Initial work is confined to scaling up the geometry from 0.2 mm on the shark skin to 2 cm, with a scaling down in characteristic velocity from 10 - 20 m/s to 10 - 20 cm/s for laminar flow boundary layer water tunnel studies over a shark skin model. The hypothesized formation of cavity vortices within the shark skin replica has been measured using DPIV. We have also shown that with the sufficient growth of a boundary layer upstream of the model (local Re = 200,000), transition is not tripped by the surface and the flow skips over the cavities. Support for this research by a NSF SGER grant (CTS-0630489), Lindbergh Foundation Grant and a University of Alabama RAC grant is gratefully acknowledged. * Patent pending.

Evaluating the Surface Topography of Pyrolytic Carbon Finger Prostheses through Measurement of Various Roughness Parameters

PubMed Central

Naylor, Andrew; Talwalkar, Sumedh C.; Trail, Ian A.; Joyce, Thomas J.

2016-01-01

The articulating surfaces of four different sizes of unused pyrolytic carbon proximal interphalangeal prostheses (PIP) were evaluated though measuring several topographical parameters using a white light interferometer: average roughness (Sa); root mean-square roughness (Sq); skewness (Ssk); and kurtosis (Sku). The radii of the articulating surfaces were measured using a coordinate measuring machine, and were found to be: 2.5, 3.3, 4.2 and 4.7 mm for proximal, and 4.0, 5.1, 5.6 and 6.3 mm for medial components. ANOVA was used to assess the relationship between the component radii and each roughness parameter. Sa, Sq and Ssk correlated negatively with radius (p = 0.001, 0.001, 0.023), whilst Sku correlated positively with radius (p = 0.03). Ergo, the surfaces with the largest radii possessed the better topographical characteristics: low roughness, negative skewness, high kurtosis. Conversely, the surfaces with the smallest radii had poorer topographical characteristics. PMID:27089375

Quantitative Three-Dimensional Characterization of Block Copolymer Directed Self-Assembly on Combined Chemical and Topographical Prepatterned Templates.

PubMed

Segal-Peretz, Tamar; Ren, Jiaxing; Xiong, Shisheng; Khaira, Gurdaman; Bowen, Alec; Ocola, Leonidas E; Divan, Ralu; Doxastakis, Manolis; Ferrier, Nicola J; de Pablo, Juan; Nealey, Paul F

2017-02-28

Characterization of the three-dimensional (3D) structure in directed self-assembly (DSA) of block copolymers is crucial for understanding the complex relationships between the guiding template and the resulting polymer structure so DSA could be successfully implemented for advanced lithography applications. Here, we combined scanning transmission electron microscopy (STEM) tomography and coarse-grain simulations to probe the 3D structure of P2VP-b-PS-b-P2VP assembled on prepatterned templates using solvent vapor annealing. The templates consisted of nonpreferential background and raised guiding stripes that had PS-preferential top surfaces and P2VP-preferential sidewalls. The full 3D characterization allowed us to quantify the shape of the polymer domains and the interface between domains as a function of depth in the film and template geometry and offered important insights that were not accessible with 2D metrology. Sidewall guiding was advantageous in promoting the alignment and lowering the roughness of the P2VP domains over the sidewalls, but incommensurate confinement from the increased topography could cause roughness and intermittent dislocations in domains over the background region at the bottom of the film. The 3D characterization of bridge structures between domains over the background and breaks within domains on guiding lines sheds light on possible origins of common DSA defects. The positional fluctuations of the PS/P2VP interface between domains showed a depth-dependent behavior, with high levels of fluctuations near both the free surface of the film and the substrate and lower fluctuation levels in the middle of the film. This research demonstrates how 3D characterization offers a better understanding of DSA processes, leading to better design and fabrication of directing templates.

Quantitative three-dimensional characterization of block copolymer directed self-assembly on combined chemical and topographical prepatterned templates

DOE PAGES

Segal-Peretz, Tamar; Ren, Jiaxing; Xiong, Shisheng; ...

2016-12-22

Characterization of the three-dimensional (3D) structure in directed self-assembly (DSA) of block copolymers is crucial for understanding the complex relationships between the guiding template and the resulting polymer structure so DSA could be successfully implemented for advanced lithography applications. Here, we combined scanning transmission electron microscopy (STEM) tomography and coarse-grain simulations to probe the 3D structure of P2VP- b-PS- b-P2VP assembled on prepatterned templates using solvent vapor annealing. The templates consisted of nonpreferential background and raised guiding stripes that had PS-preferential top surfaces and P2VP-preferential sidewalls. The full 3D characterization allowed us to quantify the shape of the polymer domainsmore » and the interface between domains as a function of depth in the film and template geometry and offered important insights that were not accessible with 2D metrology. Sidewall guiding was advantageous in promoting the alignment and lowering the roughness of the P2VP domains over the sidewalls, but incommensurate confinement from the increased topography could cause roughness and intermittent dislocations in domains over the background region at the bottom of the film. The 3D characterization of bridge structures between domains over the background and breaks within domains on guiding lines sheds light on possible origins of common DSA defects. The positional fluctuations of the PS/P2VP interface between domains showed a depth-dependent behavior, with high levels of fluctuations near both the free surface of the film and the substrate and lower fluctuation levels in the middle of the film. As a result, this research demonstrates how 3D characterization offers a better understanding of DSA processes, leading to better design and fabrication of directing templates.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yan, Pei-Yang; Zhang, Guojing; Gullickson, Eric M.

Extreme ultraviolet lithography (EUVL) mask multi-layer (ML) blank surface roughness specification historically comes from blank defect inspection tool requirement. Later, new concerns on ML surface roughness induced wafer pattern line width roughness (LWR) arise. In this paper, we have studied wafer level pattern LWR as a function of EUVL mask surface roughness via High-NA Actinic Reticle Review Tool. We found that the blank surface roughness induced LWR at current blank roughness level is in the order of 0.5nm 3σ for NA=0.42 at the best focus. At defocus of ±40nm, the corresponding LWR will be 0.2nm higher. Further reducing EUVL maskmore » blank surface roughness will increase the blank cost with limited benefit in improving the pattern LWR, provided that the intrinsic resist LWR is in the order of 1nm and above.« less

How To Functionalize Ceramics by Perfluoroalkylsilanes for Membrane Separation Process? Properties and Application of Hydrophobized Ceramic Membranes.

PubMed

Kujawa, Joanna; Cerneaux, Sophie; Kujawski, Wojciech; Bryjak, Marek; Kujawski, Jan

2016-03-23

The combination of microscopic (atomic force microscopy and scanning electron microscopy) and goniometric (static and dynamic measurements) techniques, and surface characterization (surface free energy determination, critical surface tension, liquid entry pressure, hydraulic permeability) was implemented to discuss the influence of perfluoroalkylsilanes structure and grafting time on the physicochemistry of the created hydrophobic surfaces on the titania ceramic membranes of 5 kD and 300 kD. The impact of molecular structure of perfluoroalkylsilanes modifiers (possessing from 6 to 12 carbon atoms in the fluorinated part of the alkyl chain) and the time of the functionalization process in the range of 5 to 35 h was studied. Based on the scanning electron microscopy with energy-dispersive X-ray spectroscopy, it was found that the localization of grafting molecules depends on the membrane pore size (5 kD or 300 kD). In the case of 5 kD titania membranes, modifiers are attached mainly on the surface and only partially inside the membrane pores, whereas, for 300 kD membranes, the perfluoroalkylsilanes molecules are present within the whole porous structure of the membranes. The application of 4 various types of PFAS molecules enabled for interesting observations and remarks. It was explained how to obtain ceramic membrane surfaces with controlled material (contact angle, roughness, contact angle hysteresis) and separation properties. Highly hydrophobic surfaces with low values of contact angle hysteresis and low roughness were obtained. These surfaces possessed also low values of critical surface tension, which means that surfaces are highly resistant to wetting. This finding is crucial in membrane applicability in separation processes. The obtained and characterized hydrophobic membranes were subsequently applied in air-gap membrane distillation processes. All membranes were very efficient in MD processes, showing good transport and selective properties (∼99% of NaCl salt rejection). Depending on the membrane pore size and used modifiers, the permeate flux was in the range of 0.5-4.5 kg·m(-2)·h(-1) and 0.3-4.2 kg·m(-2)·h(-1) for 5 kD and 300 kD membranes, respectively.

Sub ablative Er: YAG laser irradiation on surface roughness of eroded dental enamel.

PubMed

Curylofo-Zotti, Fabiana Almeida; Lepri, Taísa Penazzo; Colucci, Vivian; Turssi, Cecília Pedroso; Corona, Silmara Aparecida Milori

2015-11-01

This study evaluated the effects of Er:YAG laser irradiation applied at varying pulse repetition rate on the surface roughness of eroded enamel. Bovine enamel slabs (n = 10) were embedded in polyester resin, ground, and polished. To erosive challenges, specimens were immersed two times per day in 20mL of concentrated orange juice (pH = 3.84) under agitation, during a two-day period. Specimens were randomly assigned to irradiation with the Er:YAG laser (focused mode, pulse energy of 60 mJ and energy density of 3.79 J/cm(2) ) operating at 1, 2, 3, or 4 Hz. The control group was left nonirradiated. Surface roughness measurements were recorded post erosion-like formation and further erosive episodes by a profilometer and observed through atomic force microscopy (AFM). Analysis of variance revealed that the control group showed the lowest surface roughness, while laser-irradiated substrates did not differ from each other following post erosion-like lesion formation. According to analysis of covariance, at further erosive episodes, the control group demonstrated lower surface roughness (P > 0.05), than any of the irradiated groups (P < 0.05). The pulse repetition rate of the Er:YAG laser did not affect roughness of dental enamel eroded. The AFM images showed that the specimens irradiated by the Er:YAG laser at 1 Hz presented a less rough surface than those irradiated at 2, 3, and 4 Hz. © 2015 Wiley Periodicals, Inc.

Surface deterioration of dental materials after simulated toothbrushing in relation to brushing time and load.

PubMed

Heintze, S D; Forjanic, M; Ohmiti, K; Rousson, V

2010-04-01

(1) To evaluate the changes in surface roughness and gloss after simulated toothbrushing of 9 composite materials and 2 ceramic materials in relation to brushing time and load in vitro; (2) to assess the relationship between surface gloss and surface roughness. Eight flat specimens of composite materials (microfilled: Adoro, Filtek Supreme, Heliomolar; microhybrid: Four Seasons, Tetric EvoCeram; hybrid: Compoglass F, Targis, Tetric Ceram; macrohybrid: Grandio), two ceramic materials (IPS d.SIGN and IPS Empress polished) were fabricated according to the manufacturer's instructions and optimally polished with up to 4000 grit SiC. The specimens were subjected to a toothbrushing (TB) simulation device (Willytec) with rotating movements, toothpaste slurry and at three different loads (100g/250g/350g). At hourly intervals from 1h to 10h TB, mean surface roughness Ra was measured with an optical sensor and the surface gloss (Gl) with a glossmeter. Statistical analysis was performed for log-transformed Ra data applying two-way ANOVA to evaluate the interaction between load and material and load and brushing time. There was a significant interaction between material and load as well as between load and brushing time (p<0.0001). The microhybrid and hybrid materials demonstrated more surface deterioration with higher loads, whereas with the microfilled resins Heliomolar and Adoro it was vice versa. For ceramic materials, no or little deterioration was observed over time and independent of the load. The ceramic materials and 3 of the composite materials (roughness) showed no further deterioration after 5h of toothbrushing. Mean surface gloss was the parameter which discriminated best between the materials, followed by mean surface roughness Ra. There was a strong correlation between surface gloss and surface roughness for all the materials except the ceramics. The evaluation of the deterioration curves of individual specimens revealed a more or less synchronous course suspecting hinting specific external conditions and not showing the true variability in relation to the tested material. The surface roughness and gloss of dental materials changes with brushing time and load and thus results in different material rankings. Apart from Grandio, the hybrid composite resins were more prone to surface changes than microfilled composites. The deterioration potential of a composite material can be quickly assessed by measuring surface gloss. For this purpose, a brushing time of 10h (=72,000 strokes) is needed. In further comparative studies, specimens of different materials should be tested in one series to estimate the true variability. Copyright (c) 2009 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Combined registration of 3D tibia and femur implant models in 3D magnetic resonance images

NASA Astrophysics Data System (ADS)

Englmeier, Karl-Hans; Siebert, Markus; von Eisenhart-Rothe, Ruediger; Graichen, Heiko

2008-03-01

The most frequent reasons for revision of total knee arthroplasty are loosening and abnormal axial alignment leading to an unphysiological kinematic of the knee implant. To get an idea about the postoperative kinematic of the implant, it is essential to determine the position and orientation of the tibial and femoral prosthesis. Therefore we developed a registration method for fitting 3D CAD-models of knee joint prostheses into an 3D MR image. This rigid registration is the basis for a quantitative analysis of the kinematics of knee implants. Firstly the surface data of the prostheses models are converted into a voxel representation; a recursive algorithm determines all boundary voxels of the original triangular surface data. Secondly an initial preconfiguration of the implants by the user is still necessary for the following step: The user has to perform a rough preconfiguration of both remaining prostheses models, so that the fine matching process gets a reasonable starting point. After that an automated gradient-based fine matching process determines the best absolute position and orientation: This iterative process changes all 6 parameters (3 rotational- and 3 translational parameters) of a model by a minimal amount until a maximum value of the matching function is reached. To examine the spread of the final solutions of the registration, the interobserver variability was measured in a group of testers. This variability, calculated by the relative standard deviation, improved from about 50% (pure manual registration) to 0.5% (rough manual preconfiguration and subsequent fine registration with the automatic fine matching process).

The effect of various dentifrices on surface roughness and gloss of resin composites.

PubMed

da Costa, Juliana; Adams-Belusko, Anne; Riley, Kelly; Ferracane, Jack L

2010-01-01

The purpose of this study was to evaluate the effect of different levels of abrasiveness (RDA) of dentifrices on the gloss and surface roughness of resin composites after toothbrushing. Sixty disk-shaped composite specimens (D=10.0mm, 2-mm thick, n=15 per material) were made of: microfill (Durafill), nanofill (Filtek Supreme), minifill hybrid (Filtek 250), and nanohybrid (Premise). One side of each specimen was finished with a carbide bur and polished with Enhance and Pogo. Five specimens of each composite were randomly assigned to one of the dentifrices, Colgate Total (CT; RDA 70), Colgate baking soda & peroxide whitening (CBS; RDA 145), and Colgate tartar control & whitening (CTW; RDA 200). Surface gloss was measured with a glossmeter and surface roughness with a profilometer before and after toothbrushing with a 1:2 slurry (dentifrice/deionised water) at 5760 strokes in a brushing machine (approximately 1Hz). Results were analyzed by three-way ANOVA/Tukey's (p<0.05). There was a significant reduction in gloss and increase in surface roughness after brushing with all dentifrices. There was no significant difference in gloss when Durafill was brushed with any dentifrice; the other composites showed less gloss reduction when brushed with CT. Durafill, Supreme and Premise did not show significantly different surface roughness results and CBS and CTW did not produce significantly different results. Dentifrices of lower abrasivity promote less reduction in gloss and surface roughness for composites of different particle sizes after brushing. Composites containing smaller average fillers showed less reduction in gloss and less increase in surface roughness than ones with larger fillers. Published by Elsevier Ltd.

Surface characteristics and biocompatibility of cranioplasty titanium implants following different surface treatments.

PubMed

Hatamleh, Muhanad M; Wu, Xiaohong; Alnazzawi, Ahmad; Watson, Jason; Watts, David

2018-04-01

Surface and mechanical properties of titanium alloys are integral for their use in restoring bone defects of skull and face regions. These properties are affected by the method of constructing and surface treatment of the titanium implant. This study aimed to investigate the effects of titanium finishing protocols on the surface morphology, hardness and biocompatibility of TiAl6V4. Square shaped TiAl6V4 specimens (ASTM F68) (10×10×0.5mm) were divided into seven groups of different surface treatments (n=10). The treatments included mechanical polishing, sandblasting with AL 2 O 3 (50μm), immersion in different acids, and/or electro-chemical anodization. Weight loss %; 3D micro-roughness; Knoop micro-hardness, and osteoblast cell attachment and proliferation (after 3 days) were determined for each specimen. Data was analysed using one way ANOVA and Dunett T3 post-hoc tests, and t-test (p<0.05). Weight loss % was in the range of 1.70-5.60 as mechanical polishing produced the highest weight loss, followed by sandblasting, and combined protocol of mechanical polishing and acid treatment (p<0.05). Micro-roughness values (μm) were in the range of 2.81-16.68. It was the highest for control specimens (p<0.05), and smoothest surfaces after combined mechanical polishing and acid treatment; or after electro-chemical treatment (p<0.05). Micro-hardness values (MPa) ranged 170.90-442.15 as sandblasting with/without acid treatment caused statically significantly the highest values (p<0.05) while control and mechanically polished specimens had the lowest values (p<0.05). All treatments produced equally biocompatible surfaces (p>0.05) after 1h or 3 days. Furthermore, osteoblast cell proliferation statistically significantly increased after 3days among each surface treatment (p<0.05). Different finishing treatments have variable effect on cranioplasty titanium surface loss, micro-roughness and micro-hardness but constant improved biocompatibility effect. Electro-chemical treatment caused less material loss and produced biocompatible smoothest surface of comparable hardness; hence it can be suitable for cranioplasty titanium surface finishing. Copyright © 2018 The Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Do pediatric medicines induce topographic changes in dental enamel?

PubMed

Alexandria, Adílis Kalina; Meckelburg, Nicolli de Araujo; Puetter, Ursula Tavares; Salles, Jordan Trugilho; Souza, Ivete Pomarico Ribeiro; Maia, Lucianne Cople

2016-01-01

The purpose of the present study was to evaluate the effect of common pediatric liquid medicines on surface roughness and tooth structure loss and to evaluate the pH values of these medicines at room and cold temperatures in vitro. Eighty-four bovine enamel blocks were divided into seven groups (n = 12): G1-Alivium®, G2-Novalgina®, G3-Betamox®, G4-Clavulin®, G5-Claritin®, G6-Polaramine® and G7-Milli-Q water (negative control). The pH was determined and the samples were immersed in each treatment 3x/day for 5 min. 3D non-contact profilometry was used to determine surface roughness (linear Ra, volumetric Sa) and the Gap formed between treated and control areas in each block. Scanning electron microscopy (SEM) and energy dispersive spectrometry (EDS) were also performed. The majority of liquid medicines had pH ≤ 5.50. G1, G4, and G5 showed alterations in Ra when compared with G7 (p < 0.05). According to Sa and Gap results, only G5 was different from G7 (p < 0.05). Alteration in surface was more evident in G5 SEM images. EDS revealed high concentrations of carbon, oxygen, phosphorus, and calcium in all tested groups. Despite the low pH values of all evaluated medicines, only Alivium®, Clavulin®, and Claritin® increased linear surface roughness, and only Claritin® demonstrated the in vitro capacity to produce significant tooth structure loss.

The effect of cutting parameters on the performance of ZTA-MgO cutting tool

NASA Astrophysics Data System (ADS)

Ali, A. M.; Hamidon, N. E.; Zaki, N. K. M.; Mokhtar, S.; Azhar, A. Z. A.; Bahar, R.; Ahmad, Z. A.

2018-01-01

The effect of cutting parameters on the performances of ZTA-MgO ceramic cutting tool investigated. The aim of this project is to discover the effect of cutting speed and feedrate on the performance of the ZTA-MgO cutting tool via wear and surface roughness measurement. CNC turning machining performed using the cutting speed, Vc range from 354 to 471 m/min and the feed rate, f 0.1, 0.3 and 0.5 mm/rev while the depth of cut, d is kept constant at 0.2 mm. The flank wear, crater wear, and chipping were measured accordingly using optical microscope, Matlab programming and SEM. Surface roughness of machined stainless steel 316L surface were measured using the surface roughness tester (Mitutoyo MTR097-8. The result showing the increment trend of flank wear with increment of cutting speed and feed rate with the lowest value of flank wear, 0.061 mm achieved at Vc = 354 m/min and f = 0.1 mm/rev while the highest flank wear is 0.480 mm at Vc = 471 m/min and f = 0.5 mm/rev. The increasing pattern also observed in the crater wear results. The lowest area of crater wear is 2.2736 mm2 at Vc = 354 m/min and f = 0.1 mm/rev while the highest value is 4.8524 mm2 at Vc = 471 m/min and f = 0.5 mm/rev. As for the surface roughness, the higher the cutting speed, the lower the average roughness (Ra) value. Cutting speed, Vc = 471 m/min with f = 0.1 mm/rev has the lowest value of Ra which is 0.72µm.

Thermophysical Characteristics of OSIRIS-REx Target Asteroid (101955) Bennu

NASA Astrophysics Data System (ADS)

Yu, Liangliang; Ji, Jianghui

2016-01-01

In this work, we investigate the thermophysical properties, including thermal inertia, roughness fraction and surface grain size of OSIRIS-REx target asteroid (101955) Bennu by using a thermophysical model with the recently updated 3D radar-derived shape model (Nolan et al., 2013) and mid-infrared observations (Müller et al. 2012, Emery et al., 2014). We find that the asteroid bears an effective diameter of 510+6 -40 m, a geometric albedo of 0.047+0.0083 -0.0011, a roughness fraction of 0.04+0.26 -0.04, and thermal inertia of 240+440 -60 Jm-2s-0.5K-1 for our best-fit solution. The best-estimate thermal inertia suggests that fine-grained regolith may cover a large portion of Bennu's surface, where a grain size may vary from 1.3 to 31 mm. Our outcome suggests that Bennu is suitable for the OSIRIS-REx mission to return samples to Earth.

Characterizing low-Z erosion and deposition in the DIII-D divertor using aluminum

DOE PAGES

Chrobak, Chris P.; Doerner, R. P.; Stangeby, Peter C.; ...

2017-01-28

Here, we present measurements and modeling of aluminum erosion and redeposition experiments in separate helium and deuterium low power, low density L-mode plasmas at the outer divertor strike point of DIII-D to provide a low-Z material benchmark dataset for tokamak erosion-deposition modeling codes. Coatings of Al ~100nm thick were applied to ideal (smooth) and realistic (rough) surfaces and exposed to repeat plasma discharges using the DiMES probe. Redeposition and re-erosion in all cases was primarily in the downstream toroidal field direction, evident from both in-situ spectroscopic and post-mortem non spectroscopic measurements. The gross Al erosion yield estimated from both Hemore » and D plasma exposures was ~40-70% of the expected erosion yield based on theoretical physical sputtering yields. However, the multi-step redeposition and re-erosion process, and hence the measured net erosion yield and material migration, was found to be influenced by the surface roughness and/or porosity. On rough surfaces, the fraction of the eroded Al coating found redeposited outside the original coating area was 25x higher than on smooth surfaces. The amount of Al found redeposited on the rough substrate was in fact proportional to the net eroded Al, suggesting an accumulation of deposited Al in surface pores and other areas shadowed from re-erosion. In order to determine the fraction and distribution of eroded Al returning to the surface, a simple model for erosion and redeposition was developed and fitted to the measurements. The model presented here reproduces many of the observed results in these experiments by using theoretically calculated sputtering yields, calculating surface composition changes and erosion rates in time, assuming a spatial distribution function for redepositing atoms, and accounting for deposit trapping in pores. The results of the model fits reveal that total redeposition fraction increases with higher plasma temperature (~30% for 15-18eV plasmas, and ~45% for 25-30eV plasmas), and that 50% of the atoms redepositing on rough surfaces accumulated in shadowed areas.« less

The recent development and applications of fluidic channels by 3D printing.

PubMed

Zhou, Yufeng

2017-10-18

The technology of "Lab-on-a-Chip" allows the synthesis and analysis of chemicals and biological substance within a portable or handheld device. The 3D printed structures enable precise control of various geometries. The combination of these two technologies in recent years makes a significant progress. The current approaches of 3D printing, such as stereolithography, polyjet, and fused deposition modeling, are introduced. Their manufacture specifications, such as surface roughness, resolution, replication fidelity, cost, and fabrication time, are compared with each other. Finally, novel application of 3D printed channel in biology are reviewed, including pathogenic bacteria detection using magnetic nanoparticle clusters in a helical microchannel, cell stimulation by 3D chemical gradients, perfused functional vascular channels, 3D tissue construct, organ-on-a-chip, and miniaturized fluidic "reactionware" devices for chemical syntheses. Overall, the 3D printed fluidic chip is becoming a powerful tool in the both medical and chemical industries.

Surface roughness of flowable resin composites eroded by acidic and alcoholic drinks

PubMed Central

Poggio, Claudio; Dagna, Alberto; Chiesa, Marco; Colombo, Marco; Scribante, Andrea

2012-01-01

Aim: The aim of this study is to evaluate the surface roughness of four flowable resin composites following exposure to acidic and alcoholic drinks. Materials and Methods: SureFil SDR flow, TetricEvoFlow, Esthet-X Flow and Amaris Flow HT samples were immersed in artificial saliva, Coca Cola and Chivas Regal Whisky. Each specimen was examined using a Leica DCM 3D microscope: Arithmetical mean height of the surface profiles was measured (Sa). Results: Kruskal-Wallis test showed significant differences among various groups (P<0,001). Mann Whitney test was applied and control groups showed significantly lower Sa values than other groups (P=0,008). Coca Cola groups showed highest Sa values (P<0,021). No significant differences (P=0,14) in surface texture were found among the specimens of the different materials. No significant differences were found among TetricEvoFlow, Esthet-X Flow and Amaris Flow under control conditions nor after Coca Cola application. Under control condition and after Coca Cola application SureFil SDR flow showed significantly higher Sa values. Moreover, after whisky application Amaris Flow showed significantly lower Sa values then the other three groups that showed no significant differences among them. Conclusions: Acidic and alcoholic drinks eroded the surface roughness of all evaluated flowable resin composites. PMID:22557811

Measurement uncertainty associated with chromatic confocal profilometry for 3D surface texture characterization of natural human enamel.

PubMed

Mullan, F; Bartlett, D; Austin, R S

2017-06-01

To investigate the measurement performance of a chromatic confocal profilometer for quantification of surface texture of natural human enamel in vitro. Contributions to the measurement uncertainty from all potential sources of measurement error using a chromatic confocal profilometer and surface metrology software were quantified using a series of surface metrology calibration artifacts and pre-worn enamel samples. The 3D surface texture analysis protocol was optimized across 0.04mm 2 of natural and unpolished enamel undergoing dietary acid erosion (pH 3.2, titratable acidity 41.3mmolOH/L). Flatness deviations due to the x, y stage mechanical movement were the major contribution to the measurement uncertainty; with maximum Sz flatness errors of 0.49μm. Whereas measurement noise; non-linearity's in x, y, z and enamel sample dimensional instability contributed minimal errors. The measurement errors were propagated into an uncertainty budget following a Type B uncertainty evaluation in order to calculate the Standard Combined Uncertainty (u c ), which was ±0.28μm. Statistically significant increases in the median (IQR) roughness (Sa) of the polished samples occurred after 15 (+0.17 (0.13)μm), 30 (+0.12 (0.09)μm) and 45 (+0.18 (0.15)μm) min of erosion (P<0.001 vs. baseline). In contrast, natural unpolished enamel samples revealed a statistically significant decrease in Sa roughness of -0.14 (0.34) μm only after 45min erosion (P<0.05s vs. baseline). The main contribution to measurement uncertainty using chromatic confocal profilometry was from flatness deviations however by optimizing measurement protocols the profilometer successfully characterized surface texture changes in enamel from erosive wear in vitro. Copyright © 2017 The Academy of Dental Materials. All rights reserved.

RANS Based Methodology for Predicting the Influence of Leading Edge Erosion on Airfoil Performance

DOE Office of Scientific and Technical Information (OSTI.GOV)

Langel, Christopher M.; Chow, Raymond C.; van Dam, C. P.

The impact of surface roughness on flows over aerodynamically designed surfaces is of interested in a number of different fields. It has long been known the surface roughness will likely accelerate the laminar- turbulent transition process by creating additional disturbances in the boundary layer. However, there are very few tools available to predict the effects surface roughness will have on boundary layer flow. There are numerous implications of the premature appearance of a turbulent boundary layer. Increases in local skin friction, boundary layer thickness, and turbulent mixing can impact global flow properties compounding the effects of surface roughness. With thismore » motivation, an investigation into the effects of surface roughness on boundary layer transition has been conducted. The effort involved both an extensive experimental campaign, and the development of a high fidelity roughness model implemented in a R ANS solver. Vast a mounts of experimental data was generated at the Texas A&M Oran W. Nicks Low Speed Wind Tunnel for the calibration and validation of the roughness model described in this work, as well as future efforts. The present work focuses on the development of the computational model including a description of the calibration process. The primary methodology presented introduces a scalar field variable and associated transport equation that interacts with a correlation based transition model. The additional equation allows for non-local effects of surface roughness to be accounted for downstream of rough wall sections while maintaining a "local" formulation. The scalar field is determined through a boundary condition function that has been calibrated to flat plate cases with sand grain roughness. The model was initially tested on a NACA 0012 airfoil with roughness strips applied to the leading edge. Further calibration of the roughness model was performed using results from the companion experimental study on a NACA 63 3 -418 airfoil. The refined model demonstrates favorable agreement predicting changes to the transition location, as well as drag, for a number of different leading edge roughness configurations on the NACA 63 3-418 airfoil. Additional tests were conducted on a thicker S814 airfoil, with similar roughness configurations to the NACA 63 3-418. Simulations run with the roughness model compare favorably with the results obtained in the experimental study for both airfoils.« less

Wettability of Y2O3: A Relative Analysis of Thermally Oxidized, Reactively Sputtered and Template Assisted Nanostructured Coatings

PubMed Central

Barshilia, Harish C.; Chaudhary, Archana; Kumar, Praveen; Manikandanath, Natarajan T.

2012-01-01

The wettability of reactively sputtered Y2O3, thermally oxidized Y-Y2O3 and Cd-CdO template assisted Y2O3 coatings has been studied. The wettability of as-deposited Y2O3 coatings was determined by contact angle measurements. The water contact angles for reactively sputtered, thermally oxidized and template assisted Y2O3 nanostructured coatings were 99°, 117° and 155°, respectively. The average surface roughness values of reactively sputtered, thermally oxidized and template assisted Y2O3 coatings were determined by using atomic force microscopy and the corresponding values were 3, 11 and 180 nm, respectively. The low contact angle of the sputter deposited Y2O3 and thermally oxidized Y-Y2O3 coatings is attributed to a densely packed nano-grain like microstructure without any void space, leading to low surface roughness. A water droplet on such surfaces is mostly in contact with a solid surface relative to a void space, leading to a hydrophobic surface (low contact angle). Surface roughness is a crucial factor for the fabrication of a superhydrophobic surface. For Y2O3 coatings, the surface roughness was improved by depositing a thin film of Y2O3 on the Cd-CdO template (average roughness = 178 nm), which resulted in a contact angle greater than 150°. The work of adhesion of water was very high for the reactively sputtered Y2O3 (54 mJ/m2) and thermally oxidized Y-Y2O3 coatings (43 mJ/m2) compared to the Cd-CdO template assisted Y2O3 coating (7 mJ/m2). PMID:28348296

Does the low hole transport mass in <110> and <111> Si nanowires lead to mobility enhancements at high field and stress: A self-consistent tight-binding study

NASA Astrophysics Data System (ADS)

Kotlyar, R.; Linton, T. D.; Rios, R.; Giles, M. D.; Cea, S. M.; Kuhn, K. J.; Povolotskyi, Michael; Kubis, Tillmann; Klimeck, Gerhard

2012-06-01

The hole surface roughness and phonon limited mobility in the silicon <100>, <110>, and <111> square nanowires under the technologically important conditions of applied gate bias and stress are studied with the self-consistent Poisson-sp3d5s*-SO tight-binding bandstructure method. Under an applied gate field, the hole carriers in a wire undergo a volume to surface inversion transition diminishing the positive effects of the high <110> and <111> valence band nonparabolicities, which are known to lead to the large gains of the phonon limited mobility at a zero field in narrow wires. Nonetheless, the hole mobility in the unstressed wires down to the 5 nm size remains competitive or shows an enhancement at high gate field over the large wire limit. Down to the studied 3 nm sizes, the hole mobility is degraded by strong surface roughness scattering in <100> and <110> wires. The <111> channels are shown to experience less surface scattering degradation. The physics of the surface roughness scattering dependence on wafer and channel orientations in a wire is discussed. The calculated uniaxial compressive channel stress gains of the hole mobility are found to reduce in the narrow wires and at the high field. This exacerbates the stressed mobility degradation with size. Nonetheless, stress gains of a factor of 2 are obtained for <110> wires down to 3 nm size at a 5×1012 cm-2 hole inversion density per gate area.

Improvement of the Correlative AFM and ToF-SIMS Approach Using an Empirical Sputter Model for 3D Chemical Characterization.

PubMed

Terlier, T; Lee, J; Lee, K; Lee, Y

2018-02-06

Technological progress has spurred the development of increasingly sophisticated analytical devices. The full characterization of structures in terms of sample volume and composition is now highly complex. Here, a highly improved solution for 3D characterization of samples, based on an advanced method for 3D data correction, is proposed. Traditionally, secondary ion mass spectrometry (SIMS) provides the chemical distribution of sample surfaces. Combining successive sputtering with 2D surface projections enables a 3D volume rendering to be generated. However, surface topography can distort the volume rendering by necessitating the projection of a nonflat surface onto a planar image. Moreover, the sputtering is highly dependent on the probed material. Local variation of composition affects the sputter yield and the beam-induced roughness, which in turn alters the 3D render. To circumvent these drawbacks, the correlation of atomic force microscopy (AFM) with SIMS has been proposed in previous studies as a solution for the 3D chemical characterization. To extend the applicability of this approach, we have developed a methodology using AFM-time-of-flight (ToF)-SIMS combined with an empirical sputter model, "dynamic-model-based volume correction", to universally correct 3D structures. First, the simulation of 3D structures highlighted the great advantages of this new approach compared with classical methods. Then, we explored the applicability of this new correction to two types of samples, a patterned metallic multilayer and a diblock copolymer film presenting surface asperities. In both cases, the dynamic-model-based volume correction produced an accurate 3D reconstruction of the sample volume and composition. The combination of AFM-SIMS with the dynamic-model-based volume correction improves the understanding of the surface characteristics. Beyond the useful 3D chemical information provided by dynamic-model-based volume correction, the approach permits us to enhance the correlation of chemical information from spectroscopic techniques with the physical properties obtained by AFM.

Laser Sintered Porous Ti-6Al-4V Implants Stimulate Vertical Bone Growth.

PubMed

Cheng, Alice; Cohen, David J; Kahn, Adrian; Clohessy, Ryan M; Sahingur, Kaan; Newton, Joseph B; Hyzy, Sharon L; Boyan, Barbara D; Schwartz, Zvi

2017-08-01

The objective of this study was to examine the ability of 3D implants with trabecular-bone-inspired porosity and micro-/nano-rough surfaces to enhance vertical bone ingrowth. Porous Ti-6Al-4V constructs were fabricated via laser-sintering and processed to obtain micro-/nano-rough surfaces. Male and female human osteoblasts were seeded on constructs to analyze cell morphology and response. Implants were then placed on rat calvaria for 10 weeks to assess vertical bone ingrowth, mechanical stability and osseointegration. All osteoblasts showed higher levels of osteocalcin, osteoprotegerin, vascular endothelial growth factor and bone morphogenetic protein 2 on porous constructs compared to solid laser-sintered controls. Porous implants placed in vivo resulted in an average of 3.1 ± 0.6 mm 3 vertical bone growth and osseointegration within implant pores and had significantly higher pull-out strength values than solid implants. New bone formation and pull-out strength was not improved with the addition of demineralized bone matrix putty. Scanning electron images and histological results corroborated vertical bone growth. This study indicates that Ti-6Al-4V implants fabricated by additive manufacturing to have porosity based on trabecular bone and post-build processing to have micro-/nano-surface roughness can support vertical bone growth in vivo, and suggests that these implants may be used clinically to increase osseointegration in challenging patient cases.

The evolution of slip surface roughness during earthquake propagation in carbonate faults

NASA Astrophysics Data System (ADS)

Zhu, B.; De Paola, N.; Llewellin, E. W.; Holdsworth, R.

2014-12-01

Slip surface roughness is understood to control the dynamics of earthquake propagation. Quantifying the micro- and nano-scale roughness of slip surfaces can give insight into the grain-scale processes controlling the strength of faults during earthquake propagation. Friction experiments were performed on fine-grained calcite gouges, at speed 1 ms-1, normal stress 18 MPa, displacements 0.009-1.46 m, and room temperature and humidity. Results show a two stage-evolution (S1-2) of the fault strength, with an initial increase up to peak value 0.82 (S1), followed by a sudden decrease to a low, steady-state value 0.18 (S2). Samples retrieved at the end of S1 show the development of a cohesive slip zone (SZ), made of micron-scale, angular clasts formed by brittle fracturing and cataclasis. The SZ of samples deformed up to S2, is composed of nanograin aggregates which exhibit polygonal grain boundaries indicating high temperature grain boundary sliding creep deformation. In both cases, the SZ is bounded by a sharply defined slip surface. The 3-D geometry of seven experimental slip surfaces (40μm×40μm) has been reconstructed by digital processing of sets of 1800 images of SZ cross sections acquired at 20 nm intervals perpendicular to the slip direction, using a slicing (Focussed Ion Beam) and viewing (Field Emission Scanning Electron Microscope) technique. Spectrum power density analyses show that nano- and micron-scale slip surface roughness is anisotropic for both S1 and S2 slip surfaces. At the nano- and micron-scale, root mean square values decrease with length for S1 slip surfaces, but only slightly for S2 surfaces, and are anisotropic in the slip-normal and slip-parallel directions. The anisotropy is reduced at the nano-scale, although S2 slip surfaces are still smoother parallel to slip than normal to slip. Hurst exponents vary through scales, and are anisotropic in the directions parallel and normal to slip. Variable Hurst exponents indicate that slip surface roughness is scale-dependent with anisotropic, not self-affine behaviour at the micro/nano-scale, in contrast to the self-affine behaviour inferred at the mm to km scales. Dynamic weakening and creep deformation, observed during S2, coincide with an evolution towards less anisotropic and scale-dependent slip surface roughness at the nanoscale.

Quantitative fractography by digital image processing: NIH Image macro tools for stereo pair analysis and 3-D reconstruction.

PubMed

Hein, L R

2001-10-01

A set of NIH Image macro programs was developed to make qualitative and quantitative analyses from digital stereo pictures produced by scanning electron microscopes. These tools were designed for image alignment, anaglyph representation, animation, reconstruction of true elevation surfaces, reconstruction of elevation profiles, true-scale elevation mapping and, for the quantitative approach, surface area and roughness calculations. Limitations on time processing, scanning techniques and programming concepts are also discussed.

The physics of water droplets on surfaces: exploring the effects of roughness and surface chemistry

NASA Astrophysics Data System (ADS)

Eid, K. F.; Panth, M.; Sommers, A. D.

2018-03-01

This paper explores the fluid property commonly called surface tension, its effect on droplet shape and contact angle, and the major influences of contact angle behaviour (i.e. surface roughness and surface chemistry). Images of water droplets placed on treated copper surfaces are used to measure the contact angles between the droplets and the surface. The surface wettability is manipulated either by growing a self-assembled monolayer on the surface to make it hydrophobic or by changing the surface roughness. The main activities in this experiment, then, are (1) preparing and studying surfaces with different surface wettability and roughness; (2) determining the shape and contact angles of water droplets on these surfaces; and (3) demonstrating the spontaneous motion of water droplets using surface tension gradients.

Effect of oxygen plasma etching on pore size-controlled 3D polycaprolactone scaffolds for enhancing the early new bone formation in rabbit calvaria.

PubMed

Kook, Min-Suk; Roh, Hee-Sang; Kim, Byung-Hoon

2018-05-02

This study was to investigate the effects of O 2 plasma-etching of the 3D polycaprolactone (PCL) scaffold surface on preosteoblast cell proliferation and differentiation, and early new bone formation. The PCL scaffolds were fabricated by 3D printing technique. After O 2 plasma treatment, surface characterizations were examined by scanning electron microscopy, atomic force microscopy, and contact angle. MTT assay was used to determine cell proliferation. To investigate the early new bone formation, rabbits were sacrificed at 2 weeks for histological analyses. As the O 2 plasma etching time is increased, roughness and hydrophilicity of the PCL scaffold surface increased. The cell proliferation and differentiation on plasma-etched samples was significantly increased than on untreated samples. At 2 weeks, early new bone formation in O 2 plasma-etched PCL scaffolds was the higher than that of untreated scaffolds. The O 2 plasma-etched PCL scaffolds showed increased preosteoblast differentiation as well as increased new bone formation.

Aerodynamics of a finite wing with simulated ice

NASA Technical Reports Server (NTRS)

Bragg, M. B.; Khodadoust, A.; Kerho, M.

1992-01-01

The effect of a simulated glaze ice accretion on the aerodynamic performance of a three-dimensional wing is studied experimentally. Results are reviewed from earlier two-dimensional tests which show the character of the large leading-edge separation bubbles caused by the simulated ice accretion. The 2-D bubbles are found to closely resemble well known airfoil laminar separation bubbles. For the 3-D experiments a semispan wing of effective aspect ratio five was mounted from the sidewall of the UIUC subsonic wind tunnel. The model uses a NACA 0012 airfoil section on a rectangular planform with interchangeable tip and root sections to allow for 0- and 30-degree sweep. A three-component sidewall balance was used to measure lift, drag and pitching moment on the clean and iced model. Fluorescent oil flow visualization has been performed on the iced model and reveals extensive spanwise and vortical flow in the separation bubble aft of the upper surface horn. Sidewall interaction and spanwise nonuniformity are also seen on the unswept model. Comparisons to the computed flow fields are shown. Results are also shown for roughness effects on the straight wing. Sand grain roughness on the ice shape is seen to have a different effect than isolated 3-D roughness elements.

Rough Interface Effects on N-S Proximity-Contact Systems

NASA Astrophysics Data System (ADS)

Nagato, Yasushi; Nagai, Katsuhiko

2003-03-01

We discuss the influence of atomic scale roughness of the interface on the properties of the N-S contact systems. To treat the interface roughness effects we extend our previous quasi-classical theory of the rough surface effect and construct a formal solution for the quasi-classical Green's function. We apply the formulation to N-S systems with two-dimensional anisotropic dx2-y2 superconductor and calculate the self-consistent pair potential and the density of states at the interface.

The effect of heterogeneity and surface roughness on soil hydrophobicity

NASA Astrophysics Data System (ADS)

Hallin, I.; Bryant, R.; Doerr, S. H.; Douglas, P.

2010-05-01

Soil water repellency, or hydrophobicity, can develop under both natural and anthropogenic conditions. Forest fires, vegetation decomposition, microbial activity and oil spills can all promote hydrophobic behaviour in surrounding soils. Hydrophobicity can stabilize soil organic matter pools and decrease evapotranspiration, but there are many negative impacts of hydrophobicity as well: increased erosion of topsoil, an increasingly scarce resource; increased runoff, which can lead to flooding; and decreased infiltration, which directly affects plant health. The degree of hydrophobicity expressed by soil can vary greatly within a small area, depending partly on the type and severity of the disturbance as well as on temporal factors such as water content and microbial activity. To date, many laboratory investigations into soil hydrophobicity have focused on smooth particle surfaces. As a result, our understanding of how hydrophobicity develops on rough surfaces of macro, micro and nano-particulates is limited; we are unable to predict with certainty how these soil particles will behave on contact with water. Surface chemistry is the main consideration when predicting hydrophobic behaviour of smooth solids, but for particles with rough surfaces, hydrophobicity is believed to develop as a combination of surface chemistry and topography. Topography may reflect both the arrangement (aggregation) of soil particles and the distribution of materials adsorbed on particulate surfaces. Patch-wise or complete coverage of rough soil particles by hydrophobic material may result in solid/water contact angles ≥150° , at which point the soil may be classified as super-hydrophobic. Here we present a critical review of the research to date on the effects of heterogeneity and surface roughness on soil hydrophobicity in which we discuss recent advances, current trends, and future research areas. References: Callies, M., Y. Chen, F. Marty, A. Pépin and D. Quéré. 2005. Microfabricated textured surfaces for super-hydrophobicity investigations. Microelectronic Engineering. 78-79:100-105. Doerr, S.H. C.J. Ritsema, L.W. Dekker, D.F. Scott and D. Carter. 2007. Water repellence of soils: new insights and emerging research needs. Hydrological Processes. 21:2223-2228. Doerr, S.H., R.A. Shakesby and R.P.D. Walsh. 2000. Soil water repellency: its causes, characteristics and hydro-geomorphological significance. Earth-Science Reviews. 51:33-65. McHale, G. N.J. Shirtcliffe, M.I. Newton, F.B. Pyatt and S.H. Doerr. 2007. Self-organization of hydrophobic soil and granular surfaces. Applied Physics Letters. 90. 054110.

Experimental validation of a 2D overland flow model using high resolution water depth and velocity data

NASA Astrophysics Data System (ADS)

Cea, L.; Legout, C.; Darboux, F.; Esteves, M.; Nord, G.

2014-05-01

This paper presents a validation of a two-dimensional overland flow model using empirical laboratory data. Unlike previous publications in which model performance is evaluated as the ability to predict an outlet hydrograph, we use high resolution 2D water depth and velocity data to analyze to what degree the model is able to reproduce the spatial distribution of these variables. Several overland flow conditions over two impervious surfaces of the order of one square meter with different micro and macro-roughness characteristics are studied. The first surface is a simplified representation of a sinusoidal terrain with three crests and furrows, while the second one is a mould of a real agricultural seedbed terrain. We analyze four different bed friction parameterizations and we show that the performance of formulations which consider the transition between laminar, smooth turbulent and rough turbulent flow do not improve the results obtained with Manning or Keulegan formulas for rough turbulent flow. The simulations performed show that using Keulegan formula with a physically-based definition of the bed roughness coefficient, a two-dimensional shallow water model is able to reproduce satisfactorily the flow hydrodynamics. It is shown that, even if the resolution of the topography data and numerical mesh are high enough to include all the small scale features of the bed surface, the roughness coefficient must account for the macro-roughness characteristics of the terrain in order to correctly reproduce the flow hydrodynamics.

Copper foils with gradient structure in thickness direction and different roughnesses on two surfaces fabricated by double rolling

NASA Astrophysics Data System (ADS)

Wang, Xi-yong; Liu, Xue-feng; Zou, Wen-jiang; Xie, Jian-xin

2013-12-01

Copper foils with gradient structure in thickness direction and different roughnesses on two surfaces were fabricated by double rolling. The two surface morphologies of double-rolled copper foils are quite different, and the surface roughness values are 61 and 1095 nm, respectively. The roughness value of matt surface can meet the requirement for bonding the resin matrix with copper foils used for flexible printed circuit boards, thus may omit traditional roughening treatment; the microstructure of double-rolled copper foils demonstrates an obviously asymmetric gradient feature. From bright surface to matt surface in thickness direction, the average grain size first increases from 2.3 to 7.4 μm and then decreases to 3.6 μm; compared with conventional rolled copper foils, the double-rolled copper foils exhibit a remarkably increased bending fatigue life, and the increased range is about 16.2%.

Spatial characteristics of secondary flow in a turbulent boundary layer over longitudinal surface roughness

NASA Astrophysics Data System (ADS)

Hwang, Hyeon Gyu; Lee, Jae Hwa

2017-11-01

Direct numerical simulations of turbulent boundary layers (TBLs) over spanwise heterogeneous surface roughness are performed to investigate the characteristics of secondary flow. The longitudinal surface roughness, which features lateral change in bed elevation, is described by immersed boundary method. The Reynolds number based on the momentum thickness is varied in the range of Reθ = 300-900. As the TBLs over the roughness elements spatially develop in the streamwise direction, a secondary flow emerges in a form of counter-rotating vortex pair. As the spanwise spacing between the roughness elements and roughness width vary, it is shown that the size of the secondary flow is determined by the valley width between the roughness elements. In addition, the strength of the secondary flow is mostly affected by the spanwise distance between the cores of the secondary flow. Analysis of the Reynolds-averaged turbulent kinetic energy transport equation reveals that the energy redistribution terms in the TBLs over-the ridge type roughness play an important role to derive low-momentum pathways with upward motion over the roughness crest, contrary to the previous observation with the strip-type roughness. This research was supported by the National Research Foundation of Korea (NRF) funded by the Ministry of Education (NRF-2017R1D1A1A09000537) and the Ministry of Science, ICT & Future Planning (NRF-2017R1A5A1015311).

Full-dimensional quantum calculations of the dissociation energy, zero-point, and 10 K properties of H7+/D7+ clusters using an ab initio potential energy surface.

PubMed

Barragán, Patricia; Pérez de Tudela, Ricardo; Qu, Chen; Prosmiti, Rita; Bowman, Joel M

2013-07-14

Diffusion Monte Carlo (DMC) and path-integral Monte Carlo computations of the vibrational ground state and 10 K equilibrium state properties of the H7 (+)/D7 (+) cations are presented, using an ab initio full-dimensional potential energy surface. The DMC zero-point energies of dissociated fragments H5 (+)(D5 (+))+H2(D2) are also calculated and from these results and the electronic dissociation energy, dissociation energies, D0, of 752 ± 15 and 980 ± 14 cm(-1) are reported for H7 (+) and D7 (+), respectively. Due to the known error in the electronic dissociation energy of the potential surface, these quantities are underestimated by roughly 65 cm(-1). These values are rigorously determined for first time, and compared with previous theoretical estimates from electronic structure calculations using standard harmonic analysis, and available experimental measurements. Probability density distributions are also computed for the ground vibrational and 10 K state of H7 (+) and D7 (+). These are qualitatively described as a central H3 (+)/D3 (+) core surrounded by "solvent" H2/D2 molecules that nearly freely rotate.

Micro PIV measurements of turbulent flow over 2D structured roughness

NASA Astrophysics Data System (ADS)

Hartenberger, Joel; Perlin, Marc

2015-11-01

We investigate the turbulent boundary layer over surfaces with 2D spanwise square and triangular protrusions having nominal heights of 100 - 300 microns for Reynolds numbers ranging from Reτ ~ 1500 through Reτ ~ 4500 using a high speed, high magnification imaging system. Micro PIV analysis gives finely resolved velocity fields of the flow (on the order of 10 microns between vectors) enabling a detailed look at the inner region as well as the flow in the immediate vicinity of the roughness elements. Additionally, planar PIV with lower resolution is performed to capture the remainder of the boundary layer to the freestream flow. Varying the streamwise distance between individual roughness elements from one to ten times the nominal heights allows investigation of k-type and d-type roughness in both the transitionally rough and fully rough regimes. Preliminary results show a shift in the mean velocity profile similar to the results of previous studies. Turbulent statistics will be presented also. The authors would like to acknowledge the support of NAVSEA which funded this project through the Naval Engineering Education Center (NEEC).

Elemental and topographical imaging of microscopic variations in deposition on NSTX-U and DIII-D samples

NASA Astrophysics Data System (ADS)

Skinner, C. H.; Kaita, R.; Koel, B. E.; Chrobak, C. P.; Wampler, W. R.

2017-10-01

Tokamak plasma facing components (PFCs) have surface roughness that can cause microscopic spatial variations in erosion and deposition and hence influence material migration. Previous RBS measurements showed indirect evidence for this but the spatial (0.5mm) resolution was insufficient for direct imaging. We will present elemental images at sub-micron resolution of deposition on NSTX-U and DiMES samples that show strong microscopic variations and correlate this with 3D topographical maps of surface irregularities. The elemental imaging is performed with a Scanning Auger Microprobe (SAM) that measures element-specific Auger electrons excited by an SEM electron beam. 3D topographical maps of the samples are performed with a Leica DCM 3D confocal light microscope and compared to the elemental deposition pattern. The initial results appear consistent with erosion at the downstream edges of the surface pores exposed to the incident ion flux, whereas the deeper regions are shadowed and serve as deposition traps. Support was provided through DOE Contract Numbers DE-AC02-09CH11466, DE-FC02-04ER54698 and DE-NA0003525.

Effect of different polishing systems on the surface roughness of nano-hybrid composites.

PubMed

Patel, Brijesh; Chhabra, Naveen; Jain, Disha

2016-01-01

The study aimed to investigate the influence of different polishing systems on the surface roughness of nano-hybrid composite resins. Different shapes of polishing systems are available according to the site of work. To minimize variability, a new system with single shape is developed that can be utilized in both anterior as well as posterior teeth. Seventy composite discs were fabricated using Teflon well (10 mm × 3 mm). Two main group of nano-hybrid composite Group I - Filtek Z350 and Group II - Tetric N-Ceram were used (n = 35 for each group). Both groups were further divided into four subgroups. Subgroup a - OneGloss (n = 10), Subgroup b - PoGo (n = 10), Subgroup c - Sof-Lex spiral (n = 10), Subgroup d - Mylar strip (control, n = 5). Samples were polished according to the manufacturer's recommendations. Surface roughness test was performed using contact profilometer. The obtained data were analyzed using the one-way analysis of variance test. Tetric N-Ceram produced smoother surfaces than Filtek Z350 (P < 0.05). Mylar strip and "PoGo" created equally smooth surfaces, while significantly rougher surfaces were obtained after applications of "Sof-Lex spiral" and "OneGloss" (P < 0.05). Polishing ability of Tetric N-Ceram is better than Filtek Z350 XT. "PoGo" seems to be a better polishing system than "OneGloss" and "Sof-Lex Spiral."

Ternary composite scaffolds with tailorable degradation rate and highly improved colonization by human bone marrow stromal cells.

PubMed

Idaszek, J; Bruinink, A; Święszkowski, W

2015-07-01

Poly(ε-caprolactone), PCL, is of great interest for fabrication of biodegradable scaffolds due to its high compatibility with various manufacturing techniques, especially Fused Deposition Modeling (FDM). However, slow degradation and low strength make application of PCL limited only to longer-term bioresorbable and non-load bearing implants. To overcome latter drawbacks, ternary PCL-based composite fibrous scaffolds consisting of 70-95 wt % PCL, 5 wt % Tricalcium Phosphate (TCP) and 0-25 wt % poly(lactide-co-glycolide) (PLGA) were fabricated using FDM. In the present study, the effect of composition of the scaffolds on their mechanical properties, degradation kinetics, and surface properties (wettability, surface energy, and roughness) was investigated and correlated with response of human bone marrow mesenchymal stromal cells (HBMC). The presence of PLGA increased degradation kinetics, surface roughness and significantly improved scaffold colonization. Of the evaluated surface properties only the wettability was correlated with the surface area colonized by HBMC. This study demonstrates that introduction of PLGA into PCL-TCP binary composite could largely abolish the disadvantages of the PCL matrix and improve biocompatibility by increasing wettability and polar interactions rather than surface roughness. Additionally, we showed great potential of multicellular spheroids as a sensitive in vitro tool for detection of differences in chemistry of 3D scaffolds. © 2014 Wiley Periodicals, Inc.

Synergistic effect of wire bending and salivary pH on surface properties and mechanical properties of orthodontic stainless steel archwires.

PubMed

Hobbelink, Marieke G; He, Yan; Xu, Jia; Xie, Huixu; Stoll, Richard; Ye, Qingsong

2015-01-01

The aim of this study was to investigate the corrosive behaviour of stainless steel archwires in a more clinically relevant way by bending and exposing to various pH. One hundred and twenty pieces of rectangular stainless steel wires (0.43 × 0.64 mm) were randomly assigned into four groups. In each group, there were 15 pieces of bent wires and 15 straight ones. Prior to measurements of the wires, as individual experimental groups (group 1, 2, and 3), the wires were exposed to artificial saliva for 4 weeks at pH 5.6, 6.6, and 7.6, respectively. A control group of wires (group 4) remained in air for the same period of time before sent for measurements. Surface roughness (Ra-value) was measured by a profilometer. Young's modulus and maximum force were determined by a four-point flexural test apparatus. Scanning electron microscopy was used to observe the surface morphology of straight wire. Differences between groups were examined using a two-way analysis of variance (ANOVA). Mean surface roughness values, flexural Young's moduli, and maximum force values of bent wires are significantly different from those of the straight wires, which was the main effect of wire bending, ignoring the influence of pH. A significant effect was found between Ra-values regarding the main effect of pH, ignoring the influence of shape. There was a significant interaction effect of bending and pH on flexural Young's moduli of stainless steel archwires, while pH did not show much impact on the maximum force values of those stainless steel wires. Bigger surface irregularities were seen on SEM images of straight wires immersed in artificial saliva at pH 5.6 compared to artificial saliva at other pH values. Surface depth (Rz) was more sensitive than Ra in revealing surface roughness, both measured from 3D reconstructed SEM images. Ra showed a comparable result of surface roughness to Ra-value measured by the profilometer. Bending has a significant influence on surface roughness and mechanical properties of rectangular SS archwires. pH plays a synergistic effect on the change of mechanical properties of stainless steel (SS) wires along with wire bending.

Effects of fracture surface roughness and shear displacement on geometrical and hydraulic properties of three-dimensional crossed rock fracture models

NASA Astrophysics Data System (ADS)

Huang, Na; Liu, Richeng; Jiang, Yujing; Li, Bo; Yu, Liyuan

2018-03-01

While shear-flow behavior through fractured media has been so far studied at single fracture scale, a numerical analysis of the shear effect on the hydraulic response of 3D crossed fracture model is presented. The analysis was based on a series of crossed fracture models, in which the effects of fracture surface roughness and shear displacement were considered. The rough fracture surfaces were generated using the modified successive random additions (SRA) algorithm. The shear displacement was applied on one fracture, and at the same time another fracture shifted along with the upper and lower surfaces of the sheared fracture. The simulation results reveal the development and variation of preferential flow paths through the model during the shear, accompanied by the change of the flow rate ratios between two flow planes at the outlet boundary. The average contact area accounts for approximately 5-27% of the fracture planes during shear, but the actual calculated flow area is about 38-55% of the fracture planes, which is much smaller than the noncontact area. The equivalent permeability will either increase or decrease as shear displacement increases from 0 to 4 mm, depending on the aperture distribution of intersection part between two fractures. When the shear displacement continuously increases by up to 20 mm, the equivalent permeability increases sharply first, and then keeps increasing with a lower gradient. The equivalent permeability of rough fractured model is about 26-80% of that calculated from the parallel plate model, and the equivalent permeability in the direction perpendicular to shear direction is approximately 1.31-3.67 times larger than that in the direction parallel to shear direction. These results can provide a fundamental understanding of fluid flow through crossed fracture model under shear.

Surface Roughness of the Moon Derived from Multi-frequency Radar Data

NASA Astrophysics Data System (ADS)

Fa, W.

2011-12-01

Surface roughness of the Moon provides important information concerning both significant questions about lunar surface processes and engineering constrains for human outposts and rover trafficabillity. Impact-related phenomena change the morphology and roughness of lunar surface, and therefore surface roughness provides clues to the formation and modification mechanisms of impact craters. Since the Apollo era, lunar surface roughness has been studied using different approaches, such as direct estimation from lunar surface digital topographic relief, and indirect analysis of Earth-based radar echo strengths. Submillimeter scale roughness at Apollo landing sites has been studied by computer stereophotogrammetry analysis of Apollo Lunar Surface Closeup Camera (ALSCC) pictures, whereas roughness at meter to kilometer scale has been studied using laser altimeter data from recent missions. Though these studies shown lunar surface roughness is scale dependent that can be described by fractal statistics, roughness at centimeter scale has not been studied yet. In this study, lunar surface roughnesses at centimeter scale are investigated using Earth-based 70 cm Arecibo radar data and miniature synthetic aperture radar (Mini-SAR) data at S- and X-band (with wavelengths 12.6 cm and 4.12 cm). Both observations and theoretical modeling show that radar echo strengths are mostly dominated by scattering from the surface and shallow buried rocks. Given the different penetration depths of radar waves at these frequencies (< 30 m for 70 cm wavelength, < 3 m at S-band, and < 1 m at X-band), radar echo strengths at S- and X-band will yield surface roughness directly, whereas radar echo at 70-cm will give an upper limit of lunar surface roughness. The integral equation method is used to model radar scattering from the rough lunar surface, and dielectric constant of regolith and surface roughness are two dominate factors. The complex dielectric constant of regolith is first estimated globally using the regolith composition and the relation among the dielectric constant, bulk density, and regolith composition. The statistical properties of lunar surface roughness are described by the root mean square (RMS) height and correlation length, which represent the vertical and horizontal scale of the roughness. The correlation length and its scale dependence are studied using the topography data from laser altimeter observations from recent lunar missions. As these two parameters are known, surface roughness (RMS slope) can be estimated by minimizing the difference between the observed and modeled radar echo strength. Surface roughness of several regions over Oceanus Procellarum and southeastern highlands on lunar nearside are studied, and preliminary results show that maira is smoother than highlands at 70 cm scale, whereas the situation turns opposite at 12 and 4 cm scale. Surface roughness of young craters is in general higher than that of maria and highlands, indicating large rock population produced during impacting process.

The effect of toothbrush bristle stiffness on nanohybrid surface roughness

NASA Astrophysics Data System (ADS)

Zairani, O.; Irawan, B.; Damiyanti, M.

2017-08-01

The surface of a restoration can be affected by toothpaste containing abrasive agents and the stiffness of toothbrush bristles. Objective: To identify the effect of toothbrush bristle stiffness on nanohybrid surface roughness. Methods: Sixteen nanohybrid specimens were separated into two groups. The first group was brushed using soft-bristle toothbrushes, and the second group was brushed using medium-bristle toothbrushes. Media such as aqua bides was used for brushing in both groups. Brushing was done 3 times for 5 minutes. Surface roughness was measured initially and at 5, 10, and 15 minutes using a surface roughness tester. Results: The results, tested with One-Way ANOVA and Independent Samples t Test, demonstrated that after brushing for 15 minutes, the soft-bristle toothbrush group showed a significantly different value (p < 0.05) of nanohybrid surface roughness. The group using medium-bristle toothbrushes showed the value of nano hybrid surface roughness significant difference after brushing for 10 minutes. Conclusion: Roughness occurs more rapidly when brushing with medium-bristle tooth brushes than when brushing with soft-bristle toothbrushes.

A lattice Boltzmann simulation of coalescence-induced droplet jumping on superhydrophobic surfaces with randomly distributed structures

NASA Astrophysics Data System (ADS)

Zhang, Li-Zhi; Yuan, Wu-Zhi

2018-04-01

The motion of coalescence-induced condensate droplets on superhydrophobic surface (SHS) has attracted increasing attention in energy-related applications. Previous researches were focused on regularly rough surfaces. Here a new approach, a mesoscale lattice Boltzmann method (LBM), is proposed and used to model the dynamic behavior of coalescence-induced droplet jumping on SHS with randomly distributed rough structures. A Fast Fourier Transformation (FFT) method is used to generate non-Gaussian randomly distributed rough surfaces with the skewness (Sk), kurtosis (K) and root mean square (Rq) obtained from real surfaces. Three typical spreading states of coalesced droplets are observed through LBM modeling on various rough surfaces, which are found to significantly influence the jumping ability of coalesced droplet. The coalesced droplets spreading in Cassie state or in composite state will jump off the rough surfaces, while the ones spreading in Wenzel state would eventually remain on the rough surfaces. It is demonstrated that the rough surfaces with smaller Sks, larger Rqs and a K at 3.0 are beneficial to coalescence-induced droplet jumping. The new approach gives more detailed insights into the design of SHS.

Morphological Properties of Siloxane-Hydrogel Contact Lens Surfaces.

PubMed

Stach, Sebastian; Ţălu, Ştefan; Trabattoni, Silvia; Tavazzi, Silvia; Głuchaczka, Alicja; Siek, Patrycja; Zając, Joanna; Giovanzana, Stefano

2017-04-01

The aim of this study was to quantitatively characterize the micromorphology of contact lens (CL) surfaces using atomic force microscopy (AFM) and multifractal analysis. AFM and multifractal analysis were used to characterize the topography of new and worn siloxane-hydrogel CLs made of Filcon V (I FDA group). CL surface roughness was studied by AFM in intermittent-contact mode, in air, on square areas of 25 and 100 μm 2 , by using a Nanoscope V MultiMode (Bruker). Detailed surface characterization of the surface topography was obtained using statistical parameters of 3-D (three-dimensional) surface roughness, in accordance with ISO 25178-2: 2012. Before wear, the surface was found to be characterized by out-of-plane and sharp structures, whilst after a wear of 8 h, two typical morphologies were observed. One morphology (sharp type) has a similar aspect as the unworn CLs and the other morphology (smooth type) is characterized by troughs and bumpy structures. The analysis of the AFM images revealed a multifractal geometry. The generalized dimension D q and the singularity spectrum f(α) provided quantitative values that characterize the local scale properties of CL surface geometry at nanometer scale. Surface statistical parameters deduced by multifractal analysis can be used to assess the CL micromorphology and can be used by manufacturers in developing CLs with improved surface characteristics. These parameters can also be used in understanding the tribological interactions of the back surface of the CL with the corneal surface and the front surface of the CL with the under-surface of the eyelid (friction, wear, and micro-elastohydrodynamic lubrication at a nanometer scale).

Surface Forces Apparatus Measurements of Interactions between Rough and Reactive Calcite Surfaces.

PubMed

Dziadkowiec, Joanna; Javadi, Shaghayegh; Bratvold, Jon E; Nilsen, Ola; Røyne, Anja

2018-06-26

nm-Range forces acting between calcite surfaces in water affect macroscopic properties of carbonate rocks and calcite-based granular materials and are significantly influenced by calcite surface recrystallization. We suggest that the repulsive mechanical effects related to nm-scale surface recrystallization of calcite in water could be partially responsible for the observed decrease of cohesion in calcitic rocks saturated with water. Using the surface forces apparatus, we simultaneously followed the calcite reactivity and measured the forces in water in two surface configurations: between two rough calcite surfaces (CC) and between rough calcite and a smooth mica surface (CM). We used nm-scale rough, polycrystalline calcite films prepared by atomic layer deposition. We measured only repulsive forces in CC in CaCO 3 -saturated water, which was related to roughness and possibly to repulsive hydration effects. Adhesive or repulsive forces were measured in CM in CaCO 3 -saturated water depending on calcite roughness, and the adhesion was likely enhanced by electrostatic effects. The pull-off adhesive force in CM became stronger with time, and this increase was correlated with a decrease of roughness at contacts, the parameter which could be estimated from the measured force-distance curves. That suggested a progressive increase of real contact areas between the surfaces, caused by gradual pressure-driven deformation of calcite surface asperities during repeated loading-unloading cycles. Reactivity of calcite was affected by mass transport across nm- to μm-thick gaps between the surfaces. Major roughening was observed only for the smoothest calcite films, where gaps between two opposing surfaces were nm-thick over μm-sized areas and led to force of crystallization that could overcome confining pressures of the order of MPa. Any substantial roughening of calcite caused a significant increase of the repulsive mechanical force contribution.

Gas discharge plasma treatment of poly(ethylene glycol-co-1,3/1,4 cyclohexanedimethanol terephthalate) for enhanced paint adhesion

DOE Office of Scientific and Technical Information (OSTI.GOV)

Salapare, Hernando S., E-mail: hssalapare@up.edu.ph; Department of Physical Sciences and Mathematics, College of Arts and Sciences, University of the Philippines Manila, Manila City 1000; College of Science, Pamantasan ng Lungsod ng Maynila, Intramuros, Manila City 1002

Low-energy hydrogen-ions and tetrafluoromethane-ions produced from a gas discharge ion source were irradiated to poly(ethylene glycol-co-1,3/1,4 cyclohexanedimethanol terephthalate) (PETG) sheets for enhancing paint adhesion. The ion beams were characterized using a cast steel mass spectrometer, while the untreated and treated samples were characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, contact angle measurements, and profilometry. The paint adhesion was determined by using the standard method for evaluating adhesion by knife [ASTM D6677-07, Standard Test Method for Evaluating Adhesion by Knife (ASTM International, West Conshohocken, PA, 2012)] and was correlated with the calculation of the work of adhesion derived frommore » the Young–Dupré equation. After plasma treatment, a significant decrease in the contact angle was observed in all samples, except for the CF{sub 4} ion-treated samples with the discharge current of 3 mA and an irradiation time of 30 min. At longer irradiation times, the treated samples showed lesser changes in the contact angle measurement. The increase in the average and root-mean-square surface roughness was observed on the samples after plasma treatment. The samples treated with either H{sub 2} or CF{sub 4} ions for 15 min showed a direct correlation between the discharge current and surface roughness. The samples treated for 30 min showed no significant correlation between the surface roughness and discharge current, which can be attributed to the possible melting of the samples since PETG has a low melting point. The observation made in this study on the relationship of wettability and surface roughness is consistent with the Wenzel wetting mode. Scanning electron micrographs showed surface etching on the hydrogen ion-treated samples while no significant surface changes were observed for the CF{sub 4} ion-treated samples. In general, paint adhesion was stronger for samples that exhibited enhanced wettability and high work of adhesion. The optimal work of adhesion to double the paint adhesion performance was at least 84.79 mN/m. The increase in the surface roughness after the treatment provided an increased friction between the paint and the PETG surface. The increase in the paint adhesion was also due to the covalent, hydrogen, and van der Waals bonding that are typically observed for highly wettable surfaces.« less

Mechanical properties and cell-culture characteristics of a polycaprolactone kagome-structure scaffold fabricated by a precision extruding deposition system.

PubMed

Lee, Se-Hwan; Cho, Yong Sang; Hong, Myoung Wha; Lee, Bu-Kyu; Park, Yongdoo; Park, Sang-Hyug; Kim, Young Yul; Cho, Young-Sam

2017-09-13

To enhance the mechanical properties of three-dimensional (3D) scaffolds used for bone regeneration in tissue engineering, many researchers have studied their structure and chemistry. In the structural engineering field, the kagome structure has been known to have an excellent relative strength. In this study, to enhance the mechanical properties of a synthetic polymer scaffold used for tissue engineering, we applied the 3D kagome structure to a porous scaffold for bone regeneration. Prior to fabricating the biocompatible-polymer scaffold, the ideal kagome structure, which was manufactured by a 3D printer of the digital light processing type, was compared with a grid-structure, which was used as the control group, using a compressive experiment. A polycaprolactone (PCL) kagome-structure scaffold was successfully fabricated by additive manufacturing using a 3D printer with a precision extruding deposition head. To assess the physical characteristics of the fabricated PCL-kagome-structure scaffold, we analyzed its porosity, pore size, morphological structure, surface roughness, compressive stiffness, and mechanical bending properties. The results showed that, the mechanical properties of proposed kagome-structure scaffold were superior to those of a grid-structure scaffold. Moreover, Sarcoma osteogenic (Saos-2) cells were used to evaluate the characteristics of in vitro cell proliferation. We carried out cell counting kit-8 (CCK-8) and DNA contents assays. Consequently, the cell proliferation of the kagome-structure scaffold was increased; this could be because the surface roughness of the kagome-structure scaffold enhances initial cell attachment.

Theory of Space Charge Limited Current in Fractional Dimensional Space

NASA Astrophysics Data System (ADS)

Zubair, Muhammad; Ang, L. K.

The concept of fractional dimensional space has been effectively applied in many areas of physics to describe the fractional effects on the physical systems. We will present some recent developments of space charge limited (SCL) current in free space and solid in the framework of fractional dimensional space which may account for the effect of imperfectness or roughness of the electrode surface. For SCL current in free space, the governing law is known as the Child-Langmuir (CL) law. Its analogy in a trap-free solid (or dielectric) is known as Mott-Gurney (MG) law. This work extends the one-dimensional CL Law and MG Law for the case of a D-dimensional fractional space with 0 < D <= 1 where parameter D defines the degree of roughness of the electrode surface. Such a fractional dimensional space generalization of SCL current theory can be used to characterize the charge injection by the imperfectness or roughness of the surface in applications related to high current cathode (CL law), and organic electronics (MG law). In terms of operating regime, the model has included the quantum effects when the spacing between the electrodes is small.

[Influence of different surface roughness of opaque porcelain on reflectance and L* value of porcelain fused to metal].

PubMed

Wang, Hui; Xiong, Fang; Yu, Hai-yang; Luo, Zhen-hua

2009-08-01

The purpose of this study was to investigate how different surface roughness of opaque porcelain influence reflectance and CIE L* value of porcelain fused to metal (PFM) restorations. 48 casted Ni-Cr alloy metal specimens (12.0 mm x 1.0 mm) were fabricated with ShoFu Vintage Halo porcelain and divided into six groups, eight pieces for each group. The specimens in the first group without polishing were used as control. Other groups were polished against 200-, 400-, 600-, 800-, and 1000-grit sandpaper after sintered, respectively. Surface roughness and color parameters of the specimens were measured with a Surface Roughometer EX2154-13 and a spectrocolorimeter, respectively. Ra (arithmetical mean deviation of the profile) was the main standard value to describe the surface roughness of many kinds of meatal or porcelain materials, and here we used it to express surface roughness of opaque porcelain. The data were statistically analyzed by one-way analysis of variance (alpha = 0.05) in SPSS 13.0. The reflectance value increased from 72.386 +/- 3.953 to 78.671 +/- 3.408, and CIE L* value from 90.189 +/- 1.200 to 93.496 +/- 1.070 with the increasing of surface roughness (Ra) of opaque porcelain from (0.226 +/- 0.069) microm to (0.706 +/- 0.082) microm. The same magnitude were also observed after body porcelain and enamel porcelain were sintered on with reflectance increased from 76.301 +/- 3.097 to 81.529 +/- 4.028, and CIE L* value from 80.694 +/- 1.564 to 84.604 +/- 2.964. The surface roughness of opaque porcelain had effects on the reflectance and value of PFM restorations. Within the limitation of this study, the recommended Ra range of opaque porcelain was 0.23-0.50 microm.

Nd:YAG-laser-based time-domain reflectometry measurements of the intrinsic reflection signature from PMMA fiber splices

NASA Astrophysics Data System (ADS)

Lawson, Christopher M.; Michael, Robert R., Jr.; Dressel, Earl M.; Harmony, David W.

1991-12-01

Optical time domain reflectometry (OTDR) measurements have been performed on polished polymethylmethacrylate (PMMA) plastic fiber splices. After the dominant splice reflection sources due to surface roughness, inexact index matching, and fiber core misalignment were eliminated, an intrinsic OTDR signature 3 - 8 dB above the Rayleigh backscatter floor remained with all tested fibers. This minimum splice reflectivity exhibits characteristics that are consistent with sub-surface polymer damage and can be used for detection of PMMA fiber splices.

Message-passing-interface-based parallel FDTD investigation on the EM scattering from a 1-D rough sea surface using uniaxial perfectly matched layer absorbing boundary.

PubMed

Li, J; Guo, L-X; Zeng, H; Han, X-B

2009-06-01

A message-passing-interface (MPI)-based parallel finite-difference time-domain (FDTD) algorithm for the electromagnetic scattering from a 1-D randomly rough sea surface is presented. The uniaxial perfectly matched layer (UPML) medium is adopted for truncation of FDTD lattices, in which the finite-difference equations can be used for the total computation domain by properly choosing the uniaxial parameters. This makes the parallel FDTD algorithm easier to implement. The parallel performance with different processors is illustrated for one sea surface realization, and the computation time of the parallel FDTD algorithm is dramatically reduced compared to a single-process implementation. Finally, some numerical results are shown, including the backscattering characteristics of sea surface for different polarization and the bistatic scattering from a sea surface with large incident angle and large wind speed.

Evolutionary grinding model for nanometric control of surface roughness for aspheric optical surfaces.

PubMed

Han, Jeong-Yeol; Kim, Sug-Whan; Han, Inwoo; Kim, Geon-Hee

2008-03-17

A new evolutionary grinding process model has been developed for nanometric control of material removal from an aspheric surface of Zerodur substrate. The model incorporates novel control features such as i) a growing database; ii) an evolving, multi-variable regression equation; and iii) an adaptive correction factor for target surface roughness (Ra) for the next machine run. This process model demonstrated a unique evolutionary controllability of machining performance resulting in the final grinding accuracy (i.e. averaged difference between target and measured surface roughness) of -0.2+/-2.3(sigma) nm Ra over seven trial machine runs for the target surface roughness ranging from 115 nm to 64 nm Ra.

Impact of the ongoing Amazonian deforestation on local precipitation: A GCM simulation study

NASA Technical Reports Server (NTRS)

Walker, G. K.; Sud, Y. C.; Atlas, R.

1995-01-01

Numerical simulation experiments were conducted to delineate the influence of in situ deforestation data on episodic rainfall by comparing two ensembles of five 5-day integrations performed with a recent version of the Goddard Laboratory for Atmospheres General Circulation Model (GCM) that has a simple biosphere model (SiB). The first set, called control cases, used the standard SiB vegetation cover (comprising 12 biomes) and assumed a fully forested Amazonia, while the second set, called deforestation cases, distinguished the partially deforested regions of Amazonia as savanna. Except for this difference, all other initial and prescribed boundary conditions were kept identical in both sets of integrations. The differential analyses of these five cases show the following local effects of deforestation. (1) A discernible decrease in evapotranspiration of about 0.80 mm/d (roughly 18%) that is quite robust in the averages for 1-, 2-, and 5-day forecasts. (2) A decrease in precipitation of about 1.18 mm/d (roughly 8%) that begins to emerge even in 1-2 day averages and exhibits complex evolution that extends downstream with the winds. (3) A significant decrease in the surface drag force (as a consequence of reduced surface roughness of deforested regions) that, in turn, affects the dynamical structure of moisture convergence and circulation. The surface winds increase significantly during the first day, and thereafter the increase is well maintained even in the 2- and 5-day averages.

Rolling viscous drops on a non-wettable surface containing both micro- and macro-scale roughness

NASA Astrophysics Data System (ADS)

Abolghasemibizaki, Mehran; Robertson, Connor J.; Fergusson, Christian P.; McMasters, Robert L.; Mohammadi, Reza

2018-02-01

It has previously been shown that when a liquid drop of high viscosity is placed on a non-wettable inclined surface, it rolls down at a constant descent velocity determined by the balance between viscous dissipation and the reduction rate of its gravitational potential energy. Since increasing the roughness of the surface boosts its non-wetting property, the drop should move faster on a surface structured with macrotextures (ribbed surface). Such a surface was obtained from a superhydrophobic soot coating on a solid specimen printed with an extruder-type 3D printer. The sample became superoleophobic after a functionalization process. The descent velocity of glycerol drops of different radii was then measured on the prepared surface for varied tilting angles. Our data show that the drops roll down on the ribbed surface approximately 27% faster (along the ridges) than on the macroscopically smooth counterpart. This faster velocity demonstrates that ribbed surfaces can be promising candidates for drag-reduction and self-cleaning applications. Moreover, we came up with a modified scaling model to predict the descent velocity of viscous rolling drops more accurately than what has previously been reported in the literature.

Osteoblast response to magnesium ion-incorporated nanoporous titanium oxide surfaces.

PubMed

Park, Jin-Woo; Kim, Youn-Jeong; Jang, Je-Hee; Song, Hwangjun

2010-11-01

This study investigated the surface characteristics and in vitro osteoconductivity of a titanium (Ti) surface incorporated with the magnesium ions (Mg) produced by hydrothermal treatment for future application as an endosseous implant surface. Mg-incorporated Ti oxide surfaces were produced by hydrothermal treatment using Mg-containing solution on two different microstructured surfaces--abraded minimally rough (Ma) or grit-blasted moderately rough (RBM) samples. The surface characteristics were evaluated using scanning electron microscopy, thin-film X-ray diffractometry, X-ray photoelectron spectroscopy, optical profilometry, and inductively coupled plasma atomic emission spectroscopy (ICP-AES). MC3T3-E1 pre-osteoblast cell attachment, proliferation, alkaline phosphatase (ALP) activity, and quantitative analysis of osteoblastic gene expression on Ma, RBM, Mg-incorporated Ma (Mg), and Mg-incorporated grit-blasted (RBM/Mg) Ti surfaces were evaluated. Hydrothermal treatment produced an Mg-incorporated Ti oxide layer with nanoporous surface structures. Mg-incorporated surfaces showed surface morphologies and surface roughness values almost identical to those of untreated smooth or micro-rough surfaces at the micron scale. ICP-AES analysis showed Mg ions released from treated surfaces into the solution. Mg incorporation significantly increased cellular attachment (P=0 at 0.5 h, P=0.01 at 1 h) on smooth surfaces, but no differences were found on micro-rough surfaces. Mg incorporation further increased ALP activity in cells grown on both smooth and micro-rough surfaces at 7 and 14 days of culture (P=0). Real-time polymerase chain reaction analysis showed higher mRNA expressions of the osteoblast transcription factor gene (Dlx5), various integrins, and the osteoblast phenotype genes (ALP, bone sialoprotein and osteocalcin) in cells grown on micro-rough (RBM) and Mg-incorporated (Mg and RBM/Mg) surfaces than those on Ma surfaces. Mg incorporation further increased the mRNA expressions of key osteoblast genes and integrins (α1, α2, α5, and β1) in cells grown on both the smooth and the micro-rough surfaces. These results indicate that an Mg-incorporated nanoporous Ti oxide surface produced by hydrothermal treatment may improve implant bone healing by enhancing the attachment and differentiation of osteoblastic cells. © 2010 John Wiley & Sons A/S.

Visual and digital comparative tooth colour assessment methods and atomic force microscopy surface roughness.

PubMed

Grundlingh, A A; Grossman, E S; Shrivastava, S; Witcomb, M J

2013-10-01

This study compared digital and visual colour tooth colour assessment methods in a sample of 99 teeth consisting of incisors, canines and pre-molars. The teeth were equally divided between Control, Ozicure Oxygen Activator bleach and Opalescence Quick bleach and subjected to three treatments. Colour readings were recorded at nine intervals by two assessment methods, VITA Easyshade and VITAPAN 3D MASTER TOOTH GUIDE, giving a total of 1782 colour readings. Descriptive and statistical analysis was undertaken using a GLM test for Analysis of Variance for a Fractional Design set at a significance of P < 0.05. Atomic force micros copy was used to examine treated ename surfaces and establish surface roughness. Visual tooth colour assessment showed significance for the independent variables of treatment, number of treatments, tooth type and the combination tooth type and treatment. Digital colour assessment indicated treatment and tooth type to be of significance in tooth colour change. Poor agreement was found between visual and digital colour assessment methods for Control and Ozicure Oxygen Activator treatments. Surface roughness values increased two-fold for Opalescence Quick specimens over the two other treatments, implying that increased light scattering improved digital colour reading. Both digital and visual colour matching methods should be used in tooth bleaching studies to complement each other and to compensate for deficiencies.

Increasing component functionality via multi-process additive manufacturing

NASA Astrophysics Data System (ADS)

Coronel, Jose L.; Fehr, Katherine H.; Kelly, Dominic D.; Espalin, David; Wicker, Ryan B.

2017-05-01

Additively manufactured components, although extensively customizable, are often limited in functionality. Multi-process additive manufacturing (AM) grants the ability to increase the functionality of components via subtractive manufacturing, wire embedding, foil embedding and pick and place. These processes are scalable to include several platforms ranging from desktop to large area printers. The Multi3D System is highlighted, possessing the capability to perform the above mentioned processes, all while transferring a fabricated component with a robotic arm. Work was conducted to fabricate a patent inspired, printed missile seeker. The seeker demonstrated the advantage of multi-process AM via introduction of the pick and place process. Wire embedding was also explored, with the successful interconnect of two layers of embedded wires in different planes. A final demonstration of a printed contour bracket, served to show the reduction of surface roughness on a printed part is 87.5% when subtractive manufacturing is implemented in tandem with AM. Functionality of the components on all the cases was improved. Results included optical components embedded within the printed housing, wires embedded with interconnection, and reduced surface roughness. These results highlight the improved functionality of components through multi-process AM, specifically through work conducted with the Multi3D System.

Effect of Oxide Interface Roughness on the Threshold Voltage Fluctuations in Decanano MOSFETs with Ultrathin Gate Oxides

NASA Technical Reports Server (NTRS)

Asenov, Asen; Kaya, S.

2000-01-01

In this paper we use the Density Gradient (DG) simulation approach to study, in 3-D, the effect of local oxide thickness fluctuations on the threshold voltage of decanano MOSFETs on a statistical scale. The random 2-D surfaces used to represent the interface are constructed using the standard assumptions for the auto-correlation function of the interface. The importance of the Quantum Mechanical effects when studying oxide thickness fluctuations are illustrated in several simulation examples.

Prostaglandin E2 Receptor Expression by Osteoblasts is Modulated by Implant Surface Roughness and Prostaglandin E2

DTIC Science & Technology

2006-05-01

al. 1996; Trancik et al. 1989). Thus, it is of vital importance to the field of dental implantology to investigate how prostaglandins mediate their...of Texas Graduate School of Biomedical Sciences at San Antonio Supervising Professor: David D. Dean, Ph.D. While the predictability of dental implants...control media lacking PGE2. Cells were incubated for an additional 3, 6, or 120 hrs to simulate the early response after dental implant placement, after

Influence of Wire Electrical Discharge Machining (WEDM) process parameters on surface roughness

NASA Astrophysics Data System (ADS)

Yeakub Ali, Mohammad; Banu, Asfana; Abu Bakar, Mazilah

2018-01-01

In obtaining the best quality of engineering components, the quality of machined parts surface plays an important role. It improves the fatigue strength, wear resistance, and corrosion of workpiece. This paper investigates the effects of wire electrical discharge machining (WEDM) process parameters on surface roughness of stainless steel using distilled water as dielectric fluid and brass wire as tool electrode. The parameters selected are voltage open, wire speed, wire tension, voltage gap, and off time. Empirical model was developed for the estimation of surface roughness. The analysis revealed that off time has a major influence on surface roughness. The optimum machining parameters for minimum surface roughness were found to be at a 10 V open voltage, 2.84 μs off time, 12 m/min wire speed, 6.3 N wire tension, and 54.91 V voltage gap.

The evolution of fracture surface roughness and its dependence on slip

NASA Astrophysics Data System (ADS)

Wells, Olivia L.

Under effective compression, impingement of opposing rough surfaces of a fracture can force the walls of the fracture apart during slip. Therefore, a fracture's surface roughness exerts a primary control on the amount of dilation that can be sustained on a fracture since the opposing surfaces need to remain in contact. Previous work has attempted to characterize fracture surface roughness through topographic profiles and power spectral density analysis, but these metrics describing the geometry of a fracture's surface are often non-unique when used independently. However, when combined these metrics are affective at characterizing fracture surface roughness, as well as the mechanisms affecting changes in roughness with increasing slip, and therefore changes in dilation. These mechanisms include the influence of primary grains and pores on initial fracture roughness, the effect of linkage on locally increasing roughness, and asperity destruction that limits the heights of asperities and forms gouge. This analysis reveals four essential stages of dilation during the lifecycle of a natural fracture, whereas previous slip-dilation models do not adequately address the evolution of fracture surface roughness: (1) initial slip companied by small dilation is mediated by roughness controlled by the primary grain and pore dimensions; (2) rapid dilation during and immediately following fracture growth by linkage of formerly isolated fractures; (3) wear of the fracture surface and gouge formation that minimizes dilation; and (4) between slip events cementation that modifies the mineral constituents in the fracture. By identifying these fundamental mechanisms that influence fracture surface roughness, this new conceptual model relating dilation to slip has specific applications to Enhanced Geothermal Systems (EGS), which attempt to produce long-lived dilation in natural fractures by inducing slip.

Long-Wavelength Elastic Wave Propagation Across Naturally Fractured Rock Masses

NASA Astrophysics Data System (ADS)

Mohd-Nordin, Mohd Mustaqim; Song, Ki-Il; Cho, Gye-Chun; Mohamed, Zainab

2014-03-01

Geophysical site investigation techniques based on elastic waves have been widely used to characterize rock masses. However, characterizing jointed rock masses by using such techniques remains challenging because of a lack of knowledge about elastic wave propagation in multi-jointed rock masses. In this paper, the roughness of naturally fractured rock joint surfaces is estimated by using a three-dimensional (3D) image-processing technique. The classification of the joint roughness coefficient (JRC) is enhanced by introducing the scan line technique. The peak-to-valley height is selected as a key indicator for JRC classification. Long-wavelength P-wave and torsional S-wave propagation across rock masses containing naturally fractured joints are simulated through the quasi-static resonant column (QSRC) test. In general, as the JRC increases, the S-wave velocity increases within the range of stress levels considered in this paper, whereas the P-wave velocity and the damping ratio of the shear wave decrease. In particular, the two-dimensional joint specimen underestimates the S-wave velocity while overestimating the P-wave velocity. This suggests that 3D joint surfaces should be implicated to obtain the reliable elastic wave velocity in jointed rock masses. The contact characteristic and degree of roughness and waviness of the joint surface are identified as a factor influencing P-wave and S-wave propagation in multi-jointed rock masses. The results indicate a need for a better understanding of the sensitivity of contact area alterations to the elastic wave velocity induced by changes in normal stress. This paper's framework can be a reference for future research on elastic wave propagation in naturally multi-jointed rock masses.

Fibronectin and bovine serum albumin adsorption and conformational dynamics on inherently conducting polymers: a QCM-D study.

PubMed

Molino, Paul J; Higgins, Michael J; Innis, Peter C; Kapsa, Robert M I; Wallace, Gordon G

2012-06-05

Quartz crystal microbalance with dissipation monitoring (QCM-D) was employed to characterize the adsorption of the model proteins, bovine serum albumin (BSA) and fibronectin (FN), to polypyrrole doped with dextran sulfate (PPy-DS) as a function of DS loading and surface roughness. BSA adsorption was greater on surfaces of increased roughness and was above what could be explained by the increase in surface area alone. Furthermore, the additional mass adsorbed on the rough films was concomitant with an increase in the rigidity of the protein layer. Analysis of the dynamic viscoelastic properties of the protein adlayer reveal BSA adsorption on the rough films occurs in two phases: (1) arrival and initial adsorption of protein to the polymer surface and (2) postadsorption molecular rearrangement to a more dehydrated and compact conformation that facilitates further recruitment of protein to the polymer interface, likely forming a multilayer. In contrast, FN adsorption was independent of surface roughness. However, films prepared from solutions containing the highest concentration of DS (20 mg/mL) demonstrated both an increase in adsorbed mass and adlayer viscoelasticity. This is attributed to the higher DS loading in the conducting polymer film resulting in presentation of a more hydrated molecular structure indicative of a more unfolded and bioactive conformation. Modulating the redox state of the PPy-DS polymers was shown to modify both the adsorbed mass and viscoelastic nature of FN adlayers. An oxidizing potential increased both the total adsorbed mass and the adlayer viscoelasticity. Our findings demonstrate that modification of polymer physicochemical and redox condition alters the nature of protein-polymer interaction, a process that may be exploited to tailor the bioactivity of protein through which interactions with cells and tissues may be controlled.

Ultra small angle x-ray scattering in complex mixtures of triacylglycerols

NASA Astrophysics Data System (ADS)

Peyronel, Fernanda; Quinn, Bonnie; Marangoni, Alejandro G.; Pink, David A.

2014-11-01

Ultra-small angle x-ray scattering (USAXS) has been used to elucidate, in situ, the aggregation structure of unsheared model edible oils. Each system comprised one or two solid lipids and a combination of liquid lipids. The 3D nano- to micro-structures of each system were characterized. The length scale investigated, using the Bonse-Hart camera at beamline ID-15D at the Advanced Photon Source, ANL, ranged from 300 Å-10 µm. Using the Unified Fit model, level-1 analysis showed that the scatterers were 2D objects with either a smooth, a rough, or a diffuse surface. These 2D objects had an average radius of gyration Rg1 between 200-1500 Å. Level-2 analysis displayed a slope between -1 and -2. Use of the Guinier-Porod model gave s ≈ 1 thus showing that it was cylinders (TAGwoods) aggregating with fractal dimension 1 ≤ D2 ≤ 2. D2 = 1 is consistent with 1D structures formed from TAGwoods, while D2 = 2 implies that the TAGwoods had formed structures characteristic of diffusion or reaction limited cluster-cluster aggregation (DLCA/RLCA). These aggregates exhibited radii of gyration, Rg2, between 2500 and 6500 Å. Level-3 analyses showed diffuse surfaces, for most of the systems. These interpretations are in accord with theoretical models which studied crystalline nano-platelets (CNPs) coated with nano-scale layers arising from phase separation at the CNP surfaces. These layers could be due to either liquid-liquid phase separation with the CNPs coated, uniformly or non-uniformly, by a diffuse layer of TAGs, or solid-liquid phase separation with the CNPs coated by a rough layer of crystallites. A fundamental understanding of the self-organizing structures arising in these systems helps advance the characterization of fat crystal networks from nanometres to micrometres. This research can be used to design novel fat structures that use healthier fats via nano- and meso-scale structural engineering.

Evaluation of modified titanium surfaces physical and chemical characteristics

NASA Astrophysics Data System (ADS)

Lukaszewska-Kuska, Magdalena; Leda, Bartosz; Gajdus, Przemyslaw; Hedzelek, Wieslaw

2017-11-01

Development of dental implantology is focused, among other things, on devising active surface of the implant, conditioning acceleration of the implant's integration with the bone. Increased roughness, characteristic for group of implants with developed surface, altered topography and chemically modified implant's surface determines increased implants stability. In this study four different titanium surfaces modifications: turned (TS); aluminium oxide-blasted (Al2O3); resorbable material blasted (RBM); sandblast and then etched with a mixture of acids (SAE), were evaluated in terms of surfaces topography and chemical composition prior to in vivo analysis. Topography analysis revealed two groups: one with smooth, anisotropic, undeveloped TS surface and the second group with remaining surfaces presenting rough, isotropic, developed surfaces with added during blasting procedure aluminium for Al2O3 and calcium and phosphorus for RBM. Physical and chemical modifications of titanium surface change its microstructure (typical for SAE) and increase its roughness (highest for Al2O3-blasted and RBM surfaces). The introduced modifications develop titanium surface - 10 times for SAE surfaces, 16 times for Al2O3-blasted surfaces, and 20 times for RBM surfaces.

Effects of tooth-brushing force with a desensitising dentifrice on dentine tubule patency and surface roughness.

PubMed

Mullan, F; Paraskar, S; Bartlett, D W; Olley, R C

2017-05-01

To investigate the effects of a 5% NovaMin containing dentifrice on dentine tubule patency and surface roughness at 100g and 400g tooth brush abrasion forces. 75 polished human dentine samples were prepared and randomly allocated into one of five groups; control (1), Na 2 PFO 3 100g abrasion force (2), NovaMin 100g (3), Na 2 PFO 3 400g (4) and NovaMin 400g (5). The control group underwent two 2-min cycles of artificial saliva (AS), one 2-min erosion cycle; the rest underwent two toothbrush abrasion cycles in an AS/dentifrice slurry and one 2-min erosion cycle. All samples were imaged at baseline and post intervention using Tandem Scanning Microscopy and Profilometry to analyse tubule patency and roughness. Mean tubule patency increased significantly between baseline and post intervention in groups 1,2 and 4 and decreased significantly post intervention in groups 3 and 5 (p<0.01). Post intervention, there were statistically significant differences in mean patent tubules between NovaMin and the Na 2 PFO 3 and control groups (p<0.001). Surface roughness increased for all groups between baseline and post interventions (P<0.001); mean (SD) roughness increases for groups 1, 2, 3, 4 and 5 were 0.14 (0.05) μm, 0.18 (0.04) μm, 0.16 (0.06) μm, 0.19 (0.07) μm and 0.21 (0.02) μm respectively. Differences between group 1 and 5 were significant (p<0.01). Brushing with NovaMin resulted in significant dentine tubule occlusion at 100g and 400g, but brushing with Na 2 PFO 3 resulted in increased tubule patency. Surface roughness increased significantly at 400g brushing with NovaMin. There was no correlation between tubule patency and surface roughness. A NovaMin desensitising dentifrice resulted in tubule occlusion even at high brushing forces. There was minimal increase in surface roughness at the lower (100g) brushing force. Copyright © 2017 Elsevier Ltd. All rights reserved.

Gradual surface degradation of restorative materials by acidic agents.

PubMed

Hengtrakool, Chanothai; Kukiattrakoon, Boonlert; Kedjarune-Leggat, Ureporn

2011-01-01

The aim of this study was to investigate the effect of acidic agents on surface roughness and characteristics of four restorative materials. Fifty-two discs were created from each restorative material: metal-reinforced glass ionomer cement (Ketac-S), resin-modified glass ionomer cement (Fuji II LC), resin composite (Filtek Z250), and amalgam (Valiant-PhD); each disc was 12 mm in diameter and 2.5 mm thick. The specimens were divided into four subgroups (n=13) and immersed for 168 hours in four storage media: deionized water (control); citrate buffer solution; green mango juice; and pineapple juice. Surface roughness measurements were performed with a profilometer, both before and after storage media immersion. Surface characteristics were examined using scanning electron microscopy (SEM). Statistical significance among each group was analyzed using two-way repeated ANOVA and Tukey's tests. Ketac-S demonstrated the highest roughness changes after immersion in acidic agents (p<0.05), followed by Fuji II LC. Valiant-PhD and Filtek Z250 illustrated some minor changes over 168 hours. The mango juice produced the greatest degradation effect of all materials tested (p<0.05). SEM photographs demonstrated gradual surface changes of all materials tested after immersions. Of the materials evaluated, amalgam and resin composite may be the most suitable for restorations for patients with tooth surface loss.

Effects of boundary layer forcing on wing-tip vortices

NASA Astrophysics Data System (ADS)

Shaw-Ward, Samantha

The nature of turbulence within wing-tip vortices has been a topic of research for decades, yet accurate measurements of Reynolds stresses within the core are inherently difficult due to the bulk motion wandering caused by initial and boundary conditions in wind tunnels. As a result, characterization of a vortex as laminar or turbulent is inconclusive and highly contradicting. This research uses several experimental techniques to study the effects of broadband turbulence, introduced within the wing boundary layer, on the development of wing-tip vortices. Two rectangular wings with a NACA 0012 profile were fabricated for the use of this research. One wing had a smooth finish and the other rough, introduced by P80 grade sandpaper. Force balance measurements showed a small reduction in wing performance due to surface roughness for both 2D and 3D configurations, although stall characteristics remained relatively unchanged. Seven-hole probes were purpose-built and used to assess the mean velocity profiles of the vortices five chord lengths downstream of the wing at multiple angles of attack. Above an incidence of 4 degrees, the vortices were nearly axisymmetric, and the wing roughness reduced both velocity gradients and peak velocity magnitudes within the vortex. Laser Doppler velocimetry was used to further assess the time-resolved vortex at an incidence of 5 degrees. Evidence of wake shedding frequencies and wing shear layer instabilities at higher frequencies were seen in power spectra within the vortex. Unlike the introduction of freestream turbulence, wing surface roughness did not appear to increase wandering amplitude. A new method for removing the effects of vortex wandering is proposed with the use of carefully selected high-pass filters. The filtered data revealed that the Reynolds stress profiles of the vortex produced by the smooth and rough wing were similar in shape, with a peak occurring away from the vortex centre but inside of the core. Single hot-wire measurements in the 2D wing wake revealed the potential origin of dominant length-scales observed in the vortex power spectra. At angles above 5 degrees, the 2D wing wake had both higher velocity deficits and higher levels of total wake kinetic energy for the rough wing as compared to the smooth wing.

Biologically Inspired Model for Inference of 3D Shape from Texture

PubMed Central

Gomez, Olman; Neumann, Heiko

2016-01-01

A biologically inspired model architecture for inferring 3D shape from texture is proposed. The model is hierarchically organized into modules roughly corresponding to visual cortical areas in the ventral stream. Initial orientation selective filtering decomposes the input into low-level orientation and spatial frequency representations. Grouping of spatially anisotropic orientation responses builds sketch-like representations of surface shape. Gradients in orientation fields and subsequent integration infers local surface geometry and globally consistent 3D depth. From the distributions in orientation responses summed in frequency, an estimate of the tilt and slant of the local surface can be obtained. The model suggests how 3D shape can be inferred from texture patterns and their image appearance in a hierarchically organized processing cascade along the cortical ventral stream. The proposed model integrates oriented texture gradient information that is encoded in distributed maps of orientation-frequency representations. The texture energy gradient information is defined by changes in the grouped summed normalized orientation-frequency response activity extracted from the textured object image. This activity is integrated by directed fields to generate a 3D shape representation of a complex object with depth ordering proportional to the fields output, with higher activity denoting larger distance in relative depth away from the viewer. PMID:27649387

The effect of piezoelectric ultrasonic instrumentation on titanium discs: a microscopy and trace elemental analysis in vitro study.

PubMed

Tawse-Smith, A; Atieh, M A; Tompkins, G; Duncan, W J; Reid, M R; Stirling, C H

2016-08-01

To evaluate in vitro topographical and composition changes by piezoelectric ultrasonic instrumentation with metallic and plastic tips on machined and moderately roughened titanium surfaces. Twenty machined and moderately roughened laser-marked titanium discs were ultrasonically instrumented with metallic and plastic tips. Surface instrumentation was carried out with controlled pressure for 20 and 30 seconds at two power settings. For each time and power setting, instrumentation was repeated four times with one instrumentation per disc quadrant. Surface topography analysis was performed using scanning electron microscopy (SEM) and confocal laser scanning microscopy (CLSM). Surface roughness measurements were compared between instrumented and non-instrumented surfaces. Surface element composition and rinsing solutions were evaluated using energy-dispersive spectroscopy (EDS) and trace elemental analysis using inductively coupled plasma mass spectrometry (ICPMS), respectively. SEM photomicrographs and CLSM 3D surface plot images of instrumented machined and moderately roughened surfaces demonstrated severe surface topographical alterations with metallic tips and mild to moderate changes for plastic tip instrumented sites. ICPMS analysis of the rinsing solutions identified titanium and other metal traces with the use of metallic tips, and mainly titanium and carbon when plastic tips were used. Surface EDS analysis showed elemental traces of the ultrasonic tips. Ultrasonic instrumentation with metallic or plastic tips created surface topographical and compositional changes. Different changes in surface topography were noted between the surfaces, as the roughness of the machined surfaces increased while the extent of roughness of the moderately roughened surfaces decreased. The clinical relevance of these changes is yet to be determined. © 2015 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

Intense deformation field at oceanic front inferred from directional sea surface roughness observations

NASA Astrophysics Data System (ADS)

Rascle, Nicolas; Molemaker, Jeroen; Marié, Louis; Nouguier, Frédéric; Chapron, Bertrand; Lund, Björn; Mouche, Alexis

2017-06-01

Fine-scale current gradients at the ocean surface can be observed by sea surface roughness. More specifically, directional surface roughness anomalies are related to the different horizontal current gradient components. This paper reports results from a dedicated experiment during the Lagrangian Submesoscale Experiment (LASER) drifter deployment. A very sharp front, 50 m wide, is detected simultaneously in drifter trajectories, sea surface temperature, and sea surface roughness. A new observational method is applied, using Sun glitter reflections during multiple airplane passes to reconstruct the multiangle roughness anomaly. This multiangle anomaly is consistent with wave-current interactions over a front, including both cross-front convergence and along-front shear with cyclonic vorticity. Qualitatively, results agree with drifters and X-band radar observations. Quantitatively, the sharpness of roughness anomaly suggests intense current gradients, 0.3 m s-1 over the 50 m wide front. This work opens new perspectives for monitoring intense oceanic fronts using drones or satellite constellations.

Influence of polishing on surface roughness following toothbrushing wear of composite resins.

PubMed

Dalla-Vecchia, Karine Battestin; Taborda, Talita Damas; Stona, Deborah; Pressi, Heloísa; Burnett Júnior, Luiz Henrique; Rodrigues-Junior, Sinval Adalberto

2017-01-01

This study aimed to evaluate the influence of different polishing systems on the surface roughness of composite resins following procedures to simulate the effects of toothbrushing over time. Four currently available commercial composites were used to make 128 cylindrical specimens. The specimens were randomly allocated to polishing with a 1-step polisher or 1 of 3 multistep polishers (n = 8 per group). The baseline surface roughness was measured, and the specimens were submitted to 5000, 10,000, and 20,000 brushing cycles to represent toothbrushing throughout 6, 12, and 24 months, respectively. Results showed that surface roughness was influenced by the type of composite and polishing system and was not influenced by the simulated toothbrushing time. However, the surface roughness, as challenged by toothbrushing wear, was affected by the interaction among the composite, the polisher, and the toothbrushing time. The 1-step polisher produced the highest surface roughness and influenced toothbrushing wear resistance of some composites.

Effects of Structural Properties of Electrospun TiO2 Nano-fiber Meshes on their Osteogenic Potential

PubMed Central

Wang, Xiaokun; Gittens, Rolando A.; Song, Rosemary; Tannenbaum, Rina; Olivares-Navarrete, Rene; Schwartz, Zvi; Chen, Haifeng; Boyan, Barbara D.

2011-01-01

Ideal outcomes in the field of tissue engineering and regenerative medicine involve biomaterials that can enhance cell differentiation and production of local factors for natural tissue regeneration without the use of systemic drugs. Biomaterials typically used in tissue engineering applications include polymeric scaffolds that mimic the 3-D structural environment of the native tissue, but these are often functionalized with proteins or small peptides to improve their biological performance. For bone applications, titanium (Ti) implants, or more appropriately the titania (TiO2) passive oxide layer formed on their surface, have been shown to enhance osteoblast differentiation in vitro and to promote osseointegration in vivo. In this study we evaluated the effect on osteoblast differentiation of pure TiO2 nano-fiber meshes with different surface micro-roughness and nano-fiber diameters, prepared by the electrospinning method. MG63 cells were seeded on TiO2 meshes, and cell number, differentiation markers and local factor production were analyzed. The results showed that cells grew throughout the entire surfaces and with similar morphology in all groups. Cell number was sensitive to surface micro-roughness, whereas cell differentiation and local factor production was regulated by both surface roughness and nano-fiber diameter. These results indicate that scaffold structural cues alone can be used to drive cell differentiation and create an osteogenic environment without the use of exogenous factors. PMID:22075122

Diamond thin film temperature and heat-flux sensors

NASA Technical Reports Server (NTRS)

Aslam, M.; Yang, G. S.; Masood, A.; Fredricks, R.

1995-01-01

Diamond film temperature and heat-flux sensors are developed using a technology compatible with silicon integrated circuit processing. The technology involves diamond nucleation, patterning, doping, and metallization. Multi-sensor test chips were designed and fabricated to study the thermistor behavior. The minimum feature size (device width) for 1st and 2nd generation chips are 160 and 5 micron, respectively. The p-type diamond thermistors on the 1st generation test chip show temperature and response time ranges of 80-1270 K and 0.29-25 microseconds, respectively. An array of diamond thermistors, acting as heat flux sensors, was successfully fabricated on an oxidized Si rod with a diameter of 1 cm. Some problems were encountered in the patterning of the Pt/Ti ohmic contacts on the rod, due mainly to the surface roughness of the diamond film. The use of thermistors with a minimum width of 5 micron (to improve the spatial resolution of measurement) resulted in lithographic problems related to surface roughness of diamond films. We improved the mean surface roughness from 124 nm to 30 nm by using an ultra high nucleation density of 10(exp 11)/sq cm. To deposit thermistors with such small dimensions on a curved surface, a new 3-D diamond patterning technique is currently under development. This involves writing a diamond seed pattern directly on the curved surface by a computer-controlled nozzle.

Role of Integrin Subunits in Mesenchymal Stem Cell Differentiation and Osteoblast Maturation on Graphitic Carbon-coated Microstructured Surfaces

PubMed Central

Olivares-Navarrete, Rene; Rodil, Sandra E.; Hyzy, Sharon L.; Dunn, Ginger R.; Almaguer-Flores, Argelia; Schwartz, Zvi; Boyan, Barbara D.

2015-01-01

Surface roughness, topography, chemistry, and energy promote osteoblast differentiation and increase osteogenic local factor production in vitro and bone-to-implant contact in vivo, but the mechanisms involved are not well understood. Knockdown of integrin heterodimer alpha2beta1 (α2β1) blocks the osteogenic effects of the surface, suggesting signaling by this integrin homodimer is required. The purpose of the present study was to separate effects of surface chemistry and surface structure on integrin expression by coating smooth or rough titanium (Ti) substrates with graphitic carbon, retaining surface morphology but altering surface chemistry. Ti surfaces (smooth [Ra<0.4μm], rough [Ra≥3.4μm]) were sputter-coated using a magnetron sputtering system with an ultrapure graphite target, producing a graphitic carbon thin film. Human mesenchymal stem cells and MG63 osteoblast-like cells had higher mRNA for integrin subunits α1, α2, αv, and β1 on rough surfaces in comparison to smooth, and integrin αv on graphitic-carbon-coated rough surfaces in comparison to Ti. Osteogenic differentiation was greater on rough surfaces in comparison to smooth, regardless of chemistry. Silencing integrins β1, α1, or α2 decreased osteoblast maturation on rough surfaces independent of surface chemistry. Silencing integrin αv decreased maturation only on graphitic carbon-coated surfaces, not on Ti. These results suggest a major role of the integrin β1 subunit in roughness recognition, and that integrin alpha subunits play a major role in surface chemistry recognition. PMID:25770999

A Scale-up Approach for Film Coating Process Based on Surface Roughness as the Critical Quality Attribute.

PubMed

Yoshino, Hiroyuki; Hara, Yuko; Dohi, Masafumi; Yamashita, Kazunari; Hakomori, Tadashi; Kimura, Shin-Ichiro; Iwao, Yasunori; Itai, Shigeru

2018-04-01

Scale-up approaches for film coating process have been established for each type of film coating equipment from thermodynamic and mechanical analyses for several decades. The objective of the present study was to establish a versatile scale-up approach for film coating process applicable to commercial production that is based on critical quality attribute (CQA) using the Quality by Design (QbD) approach and is independent of the equipment used. Experiments on a pilot scale using the Design of Experiment (DoE) approach were performed to find a suitable CQA from surface roughness, contact angle, color difference, and coating film properties by terahertz spectroscopy. Surface roughness was determined to be a suitable CQA from a quantitative appearance evaluation. When surface roughness was fixed as the CQA, the water content of the film-coated tablets was determined to be the critical material attribute (CMA), a parameter that does not depend on scale or equipment. Finally, to verify the scale-up approach determined from the pilot scale, experiments on a commercial scale were performed. The good correlation between the surface roughness (CQA) and the water content (CMA) identified at the pilot scale was also retained at the commercial scale, indicating that our proposed method should be useful as a scale-up approach for film coating process.

Experimental Investigation of Turbine Vane Heat Transfer for Alternative Fuels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nix, Andrew Carl

The focus of this program was to experimentally investigate advanced gas turbine cooling schemes and the effects of and factors that contribute to surface deposition from particulate matter found in coal syngas exhaust flows on turbine airfoil heat transfer and film cooling, as well as to characterize surface roughness and determine the effects of surface deposition on turbine components. The program was a comprehensive, multi-disciplinary collaborative effort between aero-thermal and materials faculty researchers and the Department of Energy, National Energy Technology Laboratory (NETL). The primary technical objectives of the program were to evaluate the effects of combustion of syngas fuelsmore » on heat transfer to turbine vanes and blades in land-based power generation gas turbine engines. The primary questions to be answered by this investigation were; What are the factors that contribute to particulate deposition on film cooled gas turbine components? An experimental program was performed in a high-temperature and pressure combustion rig at the DOE NETL; What is the effect of coal syngas combustion and surface deposition on turbine airfoil film cooling? Deposition of particulate matter from the combustion gases can block film cooling holes, decreasing the flow of the film coolant and the film cooling effectiveness; How does surface deposition from coal syngas combustion affect turbine surface roughness? Increased surface roughness can increase aerodynamic losses and result in decreased turbine hot section efficiency, increasing engine fuel consumption to maintain desired power output. Convective heat transfer is also greatly affected by the surface roughness of the airfoil surface; Is there any significant effect of surface deposition or erosion on integrity of turbine airfoil thermal barrier coatings (TBC) and do surface deposits react with the TBC in any way to decrease its thermal insulating capability? Spallation and erosion of TBC is a persistent problem in modern turbine engines; and What advancements in film cooling hole geometry and design can increase effectiveness of film cooling in turbines burning high-hydrogen coal syngas due to the higher heat loads and mass flow rates of the core flow? Experimental and numerical investigations of advanced cooling geometries that can improve resistance to surface deposition were performed. The answers to these questions were investigated through experimental measurements of turbine blade surface temperature and coolant coverage (via infrared camera images and thermocouples) and time-varying surface roughness in the NETL high-pressure combustion rig with accelerated, simulated surface deposition and advanced cooling hole concepts, coupled with detailed materials analysis and characterization using conventional methods of Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), X-Ray Diffraction (XRD), 3-D Surface Topography (using a 3-D stylus profilometer). Detailed surface temperatures and cooling effectiveness could not be measured due to issues with the NETL infrared camera system. In collaboration with faculty startup funding from the principal investigator, experimental and numerical investigations were performed of an advanced film cooling hole geometry, the anti-vortex hole (AVH), focusing on improving cooling effectiveness and decreasing the counter-rotating vortex of conventional cooling holes which can entrain mainstream particulate matter to the surface. The potential benefit of this program is in gaining a fundamental understanding of how the use of alternative fuels will effect the operation of modern gas turbine engines, providing valuable data for more effective cooling designs for future turbine systems utilizing alternative fuels.« less

Effect of grit-blasting on substrate roughness and coating adhesion

NASA Astrophysics Data System (ADS)

Varacalle, Dominic J.; Guillen, Donna Post; Deason, Douglas M.; Rhodaberger, William; Sampson, Elliott

2006-09-01

Statistically designed experiments were performed to compare the surface roughness produced by grit blasting A36/1020 steel using different abrasives. Grit blast media, blast pressure, and working distance were varied using a Box-type statistical design of experiment (SDE) approach. The surface textures produced by four metal grits (HG16, HG18, HG25, and HG40) and three conventional grits (copper slag, coal slag, and chilled iron) were compared. Substrate roughness was measured using surface profilometry and correlated with operating parameters. The HG16 grit produced the highest surface roughness of all the grits tested. Aluminum and zinc-aluminum coatings were deposited on the grit-blasted substrates using the twin-wire electric are (TWEA) process. Bond strength of the coatings was measured with a portable adhesion tester in accordance with ASTM standard D 4541. The coatings on substrates roughened with steel grit exhibit superior bond strength to those prepared with conventional grit. For aluminum coatings sprayed onto surfaces prepared with the HG16 grit, the bond strength was most influenced by current, spray distance, and spray gun pressure (in that order). The highest bond strength for the zinc-aluminum coatings was attained on surfaces prepared using the metal grits.

Comparison of roadway roughness derived from LIDAR and SFM 3D point clouds.

DOT National Transportation Integrated Search

2015-10-01

This report describes a short-term study undertaken to investigate the potential for using dense three-dimensional (3D) point : clouds generated from light detection and ranging (LIDAR) and photogrammetry to assess roadway roughness. Spatially : cont...

The effect of glycerin solution density and viscosity on vibration amplitude of oblique different piezoelectric MC near the surface in 3D modeling

NASA Astrophysics Data System (ADS)

Korayem, A. H.; Abdi, M.; Korayem, M. H.

2018-06-01

The surface topography in nanoscale is one of the most important applications of AFM. The analysis of piezoelectric microcantilevers vibration behavior is essential to improve the AFM performance. To this end, one of the appropriate methods to simulate the dynamic behavior of microcantilever (MC) is a numerical solution with FEM in the 3D modeling using COMSOL software. The present study aims to simulate different geometries of the four-layered AFM piezoelectric MCs in 2D and 3D modeling in a liquid medium using COMSOL software. The 3D simulation was done in a spherical container using FSI domain in COMSOL. In 2D modeling by applying Hamilton's Principle based on Euler-Bernoulli Beam theory, the governing motion equation was derived and discretized with FEM. In this mode, the hydrodynamic force was assumed with a string of spheres. The effect of this force along with the squeezed-film force was considered on MC equations. The effect of fluid density and viscosity on the MC vibrations that immersed in different glycerin solutions was investigated in 2D and 3D modes and the results were compared with the experimental results. The frequencies and time responses of MC close to the surface were obtained considering tip-sample forces. The surface topography of MCs different geometries were compared in the liquid medium and the comparison was done in both tapping and non-contact mode. Various types of surface roughness were considered in the topography for MC different geometries. Also, the effect of geometric dimensions on the surface topography was investigated. In liquid medium, MC is installed at an oblique position to avoid damaging the MC due to the squeezed-film force in the vicinity of MC surface. Finally, the effect of MC's angle on surface topography and time response of the system was investigated.

Effect of grinding and polishing on roughness and strength of zirconia.

PubMed

Khayat, Waad; Chebib, Najla; Finkelman, Matthew; Khayat, Samer; Ali, Ala

2018-04-01

The clinical applications of high-translucency monolithic zirconia restorations have increased. Chairside and laboratory adjustments of these restorations are inevitable, which may lead to increased roughness and reduced strength. The influence of grinding and polishing on high-translucency zirconia has not been investigated. The purpose of this in vitro study was to compare the roughness averages (Ra) of ground and polished zirconia and investigate whether roughness influenced strength after aging. High-translucency zirconia disks were milled, sintered, and glazed according to the manufacturer's recommendations. Specimens were randomized to 4 equal groups. Group G received only grinding; groups GPB and GPK received grinding and polishing with different polishing systems; and group C was the (unground) control group. All specimens were subjected to hydrothermal aging in an autoclave at 134°C at 200 kPa for 3 hours. Roughness average was measured using a 3-dimensional (3D) optical interferometer at baseline (Ra1), after grinding and polishing (Ra2), and after aging (Ra3). A biaxial flexural strength test was performed at a rate of 0.5 mm/min. Statistical analyses were performed using commercial software (α=.05). Group G showed a significantly higher mean value of Ra3 (1.96 ±0.32 μm) than polished and glazed groups (P<.001), which showed no statistically significant difference among them (GPB, 1.12 ±0.31 µm; GPK, 0.88 ±0.31 µm; C: 0.87 ±0.25 μm) (P>.05). Compared with baseline, the roughness of groups G and GPB increased significantly after surface treatments and after aging, whereas aging did not significantly influence the roughness of groups GPK or C. Group G showed the lowest mean value of biaxial flexural strength (879.01 ±157.99 MPa), and the highest value was achieved by group C (962.40 ±113.84 MPa); no statistically significant differences were found among groups (P>.05). Additionally, no significant correlation was detected between the Ra and flexural strength of zirconia. Grinding increased the roughness of zirconia restorations, whereas proper polishing resulted in smoothness comparable with glazed surfaces. The results provide no evidence that grinding and polishing affect the flexural strength of zirconia after aging. Copyright © 2017 Editorial Council for the Journal of Prosthetic Dentistry. Published by Elsevier Inc. All rights reserved.

Roughness threshold for cell attachment and proliferation on plasma micro-nanotextured polymeric surfaces: the case of primary human skin fibroblasts and mouse immortalized 3T3 fibroblasts

NASA Astrophysics Data System (ADS)

Bourkoula, A.; Constantoudis, V.; Kontziampasis, D.; Petrou, P. S.; Kakabakos, S. E.; Tserepi, A.; Gogolides, E.

2016-08-01

Poly(methyl methacrylate) surfaces have been micro-nanotextured in oxygen plasmas with increasing ion energy, leading to micro-nanotopography characterized by increased root mean square roughness, correlation length and fractal dimension. Primary human skin fibroblasts and mouse immortalized 3T3 fibroblasts were cultured on these surfaces and the number of adhering cells, their proliferation rate and morphology (cytoplasm and nucleus area) were evaluated as a function of roughness height, correlation length, and fractal dimension. A roughness threshold behavior was observed for both types of cells leading to dramatic cell number decrease above this threshold, which is almost similar for the two types of cells, despite their differences in size and stiffness. The results are discussed based on two theoretical models, which are reconciled and unified when the elastic moduli and the size of the cells are taken into account.

Wear resistance of packable resin composites after simulated toothbrushing test.

PubMed

Wang, Linda; Garcia, Fernanda Cristina Pimentel; Amarante de Araújo, Paulo; Franco, Eduardo Batista; Mondelli, Rafael Francisco Lia

2004-01-01

The purpose of this study was to determine the wear resistance of five different packable composites versus two different composite controls using a laboratory toothbrushing simulation test. Twelve samples measuring 5 mm in diameter and 3 mm thick were prepared from the following resin composites: Packable resin composites SureFil (Dentsply Ind. Com. Ltda, Petrópolis, Rio de Janeiro, Brazil), Alert (Jeneric Pentron Incorporated, Wallingford, CT, USA), Filtek P60 (3M ESPE Dental Products, St. Paul, MN, USA), Prodigy Condensable (sds Kerr, Orange CA, USA), Solitaire (Heraeus Kulzer GmbH, Wehrheim, Germany), and control resin composites Z100 Restorative (3M ESPE) and Silux Plus (3M ESPE). Finishing and polishing were conducted with Sof-Lex disks (3M ESPE), and baseline weight (grams) and surface roughness (measured with Hommel Tester T 1000, Hommelwerke, GmbH, Alte Tuttinger Strebe 20. D-7730 VS-Schwenningen, Germany) were recorded. Specimens were aged for 2 weeks until they reached a weight that remained constant for 5 consecutive days, and then were subjected to 100,000 cycles of brushing (representative of 4.2 yr) using a toothbrushing testing machine. Toothbrush heads with soft bristle tips (Colgate Classic, Colgate-Palmolive Co., Osasco, São Paulo, Brazil) with dentifrice suspension (Colgate MFP, Colgate-Palmolive Co.) in deionized water were used under a 200 g load. Changes in weight and surface roughness were determined after toothbrushing cycles. Significant differences of weight loss and surface roughness were found (paired t-test, p < .05). Weight loss percentage (mean [SD]) ranged from 0.38 to 1.69% (analysis of variance and Tukey's least significant difference, p < .05); the weight loss of the materials ranked from least to most as follows: SureFil (0.38 [0.56]), Alert (0.52 [0.18]), Z100 (1.16 [0.27]), Filtek P60 (1.31 [0.17]), Solitaire (1.51 [0.45]), Prodigy Condensable (1.55 [0.471), and Silux Plus (1.69 [0.66]). Regarding surface roughness, Prodigy Condensable (0.19 [0.08]), Solitaire (0.28 [0.06]), and Z100 (0.30 [0.07]) became less rough after toothbrushing, whereas all the others were rendered rougher: Alert (0.49 [0.29]), Filtek P60 (0.28 [0.08]), Silux Plus (0.39 [0.091), and SureFil (0.81 [0.32]). SureFil and Alert were statistically more resistant to wear (less weight loss) than were the other materials. SureFil became significantly rougher than did all the others. Overal, packable resin composites are unlikely to show superior wear resistance with regard to weight loss and surface roughness compared with current resin composites also indicated for posterior restorations.

A numerical investigation of the crystallographic texture effect on the surface roughening in aluminum polycrystals

NASA Astrophysics Data System (ADS)

Romanova, V.; Balokhonov, R.; Batukhtina, E.; Zinovieva, O.; Bezmozgiy, I.

2015-10-01

The results of a numerical analysis of the mesoscale surface roughening in a polycrystalline aluminum alloy exposed to uniaxial tension are presented. A 3D finite-element model taking an explicit account of grain structure is developed. The model describes a constitutive behavior of the material on the grain scale, using anisotropic elasticity and crystal plasticity theory. The effects of the grain shape and texture on the deformation-induced roughening are investigated. Calculation results have shown that surface roughness is much higher and develops at the highest rate in a polycrystal with equiaxed grains where both the micro- and mesoscale surface displacements are observed.

A hybrid 3D SEM reconstruction method optimized for complex geologic material surfaces.

PubMed

Yan, Shang; Adegbule, Aderonke; Kibbey, Tohren C G

2017-08-01

Reconstruction methods are widely used to extract three-dimensional information from scanning electron microscope (SEM) images. This paper presents a new hybrid reconstruction method that combines stereoscopic reconstruction with shape-from-shading calculations to generate highly-detailed elevation maps from SEM image pairs. The method makes use of an imaged glass sphere to determine the quantitative relationship between observed intensity and angles between the beam and surface normal, and the detector and surface normal. Two specific equations are derived to make use of image intensity information in creating the final elevation map. The equations are used together, one making use of intensities in the two images, the other making use of intensities within a single image. The method is specifically designed for SEM images captured with a single secondary electron detector, and is optimized to capture maximum detail from complex natural surfaces. The method is illustrated with a complex structured abrasive material, and a rough natural sand grain. Results show that the method is capable of capturing details such as angular surface features, varying surface roughness, and surface striations. Copyright © 2017 Elsevier Ltd. All rights reserved.

Chemically Accelerated Vibratory Surface Finishing (CAVSF)

DTIC Science & Technology

2009-02-01

media) • End-roughness and micro structure of different C- steels • Material removal and roughness changes versus the amount of treatment solution in...surface finishing (CAVSF) Visual appearance of strip steel test pieces during the CAVSF process. 0-120 minutes = acid treatment 120-135 minutes = water... steel during the super-finishing process 0 50 100 150 200 250 300 350 0 50 100 150 200 250 Time minutes R e m o v e d m a t e r i a l m i c r

3D Finite Element Modelling of Cutting Forces in Drilling Fibre Metal Laminates and Experimental Hole Quality Analysis

NASA Astrophysics Data System (ADS)

Giasin, Khaled; Ayvar-Soberanis, Sabino; French, Toby; Phadnis, Vaibhav

2017-02-01

Machining Glass fibre aluminium reinforced epoxy (GLARE) is cumbersome due to distinctively different mechanical and thermal properties of its constituents, which makes it challenging to achieve damage-free holes with the acceptable surface quality. The proposed work focuses on the study of the machinability of thin ( 2.5 mm) GLARE laminate. Drilling trials were conducted to analyse the effect of feed rate and spindle speed on the cutting forces and hole quality. The resulting hole quality metrics (surface roughness, hole size, circularity error, burr formation and delamination) were assessed using surface profilometry and optical scanning techniques. A three dimensional (3D) finite-element (FE) model of drilling GLARE laminate was also developed using ABAQUS/Explicit to help understand the mechanism of drilling GLARE. The homogenised ply-level response of GLARE laminate was considered in the FE model to predict cutting forces in the drilling process.

Cryo-Scanning Electron Microscopy of Captured Cirrus Ice Particles

NASA Astrophysics Data System (ADS)

Magee, N. B.; Boaggio, K.; Bandamede, M.; Bancroft, L.; Hurler, K.

2016-12-01

We present the latest collection of high-resolution cryo-scanning electron microscopy images and microanalysis of cirrus ice particles captured by high-altitude balloon (ICE-Ball, see abstracts by K. Boaggio and M. Bandamede). Ice particle images and sublimation-residues are derived from particles captured during approximately 15 balloon flights conducted in Pennsylvania and New Jersey over the past 12 months. Measurements include 3D digital elevation model reconstructions of ice particles, and associated statistical analyses of entire particles and particle sub-facets and surfaces. This 3D analysis reveals that morphologies of most ice particles captured deviate significantly from ideal habits, and display geometric complexity and surface roughness at multiple measureable scales, ranging from 100's nanometers to 100's of microns. The presentation suggests potential a path forward for representing scattering from a realistically complex array of ice particle shapes and surfaces.

On the sensitivity of mesoscale models to surface-layer parameterization constants

NASA Astrophysics Data System (ADS)

Garratt, J. R.; Pielke, R. A.

1989-09-01

The Colorado State University standard mesoscale model is used to evaluate the sensitivity of one-dimensional (1D) and two-dimensional (2D) fields to differences in surface-layer parameterization “constants”. Such differences reflect the range in the published values of the von Karman constant, Monin-Obukhov stability functions and the temperature roughness length at the surface. The sensitivity of 1D boundary-layer structure, and 2D sea-breeze intensity, is generally less than that found in published comparisons related to turbulence closure schemes generally.

Effect of bleaching agents and whitening dentifrices on the surface roughness of human teeth enamel.

PubMed

Özkan, Pelin; Kansu, Gülay; Özak, Sule Tuğba; Kurtulmuş-Yilmaz, Sevcan; Kansu, Pelin

2013-01-01

The aim of this in vitro study was to evaluate the surface roughness of human enamel bleached with 10% carbamide peroxide or 10% hydrogen peroxide bleaching agents at different times and also subjected to different superficial cleaning treatments. One hundred and forty flat enamel samples were divided into 14 groups, Group 1-Group 14 (G1-G14). G1-G7 were treated with 10% carbamide peroxide and different dentifrices, G8-G14 were treated with 10% hydrogen peroxide and different dentifrices (G1 and G8: not brushed as control groups; G2 and G9: brushed with Ipana® toothpaste; G3 and G10: brushed with Clinomyn® toothpaste; G4 and G11: brushed with Moos Dent® toothpaste; G5 and G12: brushed with Signal® toothpaste; G6 and G13: brushed with Colgate® toothpaste; G7 and G14: brushed without dentifrice). A profilometer was used to measure average roughness values of the initial surface roughness and at each 7-day-interval. The bleaching was performed for 6 h a day and the surface cleaning treatment was performed 3-times a day, 2 min each time, for 4 weeks. The samples were stored in distilled water during the test period. Statistical analysis revealed significant differences in surface roughness values over time for all groups except G1 and G8 (not brushed). The results of the surface roughness of all groups were nearly the same. The bleaching with 10% hydrogen peroxide and 10% carbamide peroxide did not alter the enamel surface roughness, but when the bleaching treatment was performed combined with abrasive dentifrices, a significant increase in roughness values was observed.

Identification of superficial defects in reconstructed 3D objects using phase-shifting fringe projection

NASA Astrophysics Data System (ADS)

Madrigal, Carlos A.; Restrepo, Alejandro; Branch, John W.

2016-09-01

3D reconstruction of small objects is used in applications of surface analysis, forensic analysis and tissue reconstruction in medicine. In this paper, we propose a strategy for the 3D reconstruction of small objects and the identification of some superficial defects. We applied a technique of projection of structured light patterns, specifically sinusoidal fringes and an algorithm of phase unwrapping. A CMOS camera was used to capture images and a DLP digital light projector for synchronous projection of the sinusoidal pattern onto the objects. We implemented a technique based on a 2D flat pattern as calibration process, so the intrinsic and extrinsic parameters of the camera and the DLP were defined. Experimental tests were performed in samples of artificial teeth, coal particles, welding defects and surfaces tested with Vickers indentation. Areas less than 5cm were studied. The objects were reconstructed in 3D with densities of about one million points per sample. In addition, the steps of 3D description, identification of primitive, training and classification were implemented to recognize defects, such as: holes, cracks, roughness textures and bumps. We found that pattern recognition strategies are useful, when quality supervision of surfaces has enough quantities of points to evaluate the defective region, because the identification of defects in small objects is a demanding activity of the visual inspection.

Comparison of Self-Etch Primers with Conventional Acid Etching System on Orthodontic Brackets

PubMed Central

Zope, Amit; Zope-Khalekar, Yogita; Chitko, Shrikant S.; Kerudi, Veerendra V.; Patil, Harshal Ashok; Jaltare, Pratik; Dolas, Siddhesh G

2016-01-01

Introduction The self-etching primer system consists of etchant and primer dispersed in a single unit. The etching and priming are merged as a single step leading to fewer stages in bonding procedure and reduction in the number of steps that also reduces the chance of introduction of error, resulting in saving time for the clinician. It also results in smaller extent of enamel decalcification. Aim To compare the Shear Bond Strength (SBS) of orthodontic bracket bonded with Self-Etch Primers (SEP) and conventional acid etching system and to study the surface appearance of teeth after debonding; etching with conventional acid etch and self-etch priming, using stereomicroscope. Materials and Methods Five Groups (n=20) were created randomly from a total of 100 extracted premolars. In a control Group A, etching of enamel was done with 37% phosphoric acid and bonding of stainless steel brackets with Transbond XT (3M Unitek, Monrovia, California). Enamel conditioning in left over four Groups was done with self-etching primers and adhesives as follows: Group B-Transbond Plus (3M Unitek), Group C Xeno V+ (Dentsply), Group D-G-Bond (GC), Group E-One-Coat (Coltene). The Adhesive Remnant Index (ARI) score was also evaluated. Additionally, the surface roughness using profilometer were observed. Results Mean SBS of Group A was 18.26±7.5MPa, Group B was 10.93±4.02MPa, Group C was 6.88±2.91MPa while of Group D was 7.78±4.13MPa and Group E was 10.39±5.22MPa respectively. In conventional group ARI scores shows that over half of the adhesive was remaining on the surface of tooth (score 1 to 3). In self-etching primer groups ARI scores show that there was no or minor amount of adhesive remaining on the surface of tooth (score 4 and 5). SEP produces a lesser surface roughness on the enamel than conventional etching. However, statistical analysis shows significant correlation (p<0.001) of bond strength with surface roughness of enamel. Conclusion All groups might show clinically useful SBS values and Transbond XT can be successfully used for bracket bonding after enamel conditioning with any of the SEPs tested. The SEPs used in Groups C (Xeno V+) and D (G-Bond) have significantly lowered SBS. Although, the values might still be clinically acceptable. PMID:28208997

Bacterial plaque retention on oral hard materials: effect of surface roughness, surface composition, and physisorbed polycarboxylate.

PubMed

McConnell, Marla D; Liu, Yu; Nowak, Andrew P; Pilch, Shira; Masters, James G; Composto, Russell J

2010-03-15

Bacterial adhesion to oral hard materials is dependent on various factors, for example, surface roughness and surface composition. In this study, bacteria retention on three oral hard substrates, hydroxyapatite (HAP), enamel, and polished enamel (p-enamel) were investigated. The surface morphology and roughness of the three substrates were measured by scanning probe microscopy. HAP had the roughest surface, followed by enamel and polished enamel. For each individual substrate type, the roughness was shown to increase with scan size up to 50 microm x 50 microm. For HAP and enamel, roughness decreased considerably after formation of a pellicle, while addition of polymer coating to the pellicle layer reduced roughness much less in comparison. Bacterial surface coverage was measured at 30 min, 3 h, and 24 h on both native and surface-modified substrates, which were coated with two different polycarboxylate-based polymers, Gantrez S97 and Carbopol 940. As a result, the polymer coated surfaces had reduced bacteria coverage compared with the native surfaces over all time points and substrates measured. The reduction is the combined effect of electrostatic repulsion and sequestering of Ca(2+) ions at the surface, which plays a key role in the initial adhesion of bacteria to enamel surfaces in models of plaque formation. (c) 2009 Wiley Periodicals, Inc.

Three-dimensional online surface reconstruction of augmented fluorescence lifetime maps using photometric stereo (Conference Presentation)

NASA Astrophysics Data System (ADS)

Unger, Jakob; Lagarto, Joao; Phipps, Jennifer; Ma, Dinglong; Bec, Julien; Sorger, Jonathan; Farwell, Gregory; Bold, Richard; Marcu, Laura

2017-02-01

Multi-Spectral Time-Resolved Fluorescence Spectroscopy (ms-TRFS) can provide label-free real-time feedback on tissue composition and pathology during surgical procedures by resolving the fluorescence decay dynamics of the tissue. Recently, an ms-TRFS system has been developed in our group, allowing for either point-spectroscopy fluorescence lifetime measurements or dynamic raster tissue scanning by merging a 450 nm aiming beam with the pulsed fluorescence excitation light in a single fiber collection. In order to facilitate an augmented real-time display of fluorescence decay parameters, the lifetime values are back projected to the white light video. The goal of this study is to develop a 3D real-time surface reconstruction aiming for a comprehensive visualization of the decay parameters and providing an enhanced navigation for the surgeon. Using a stereo camera setup, we use a combination of image feature matching and aiming beam stereo segmentation to establish a 3D surface model of the decay parameters. After camera calibration, texture-related features are extracted for both camera images and matched providing a rough estimation of the surface. During the raster scanning, the rough estimation is successively refined in real-time by tracking the aiming beam positions using an advanced segmentation algorithm. The method is evaluated for excised breast tissue specimens showing a high precision and running in real-time with approximately 20 frames per second. The proposed method shows promising potential for intraoperative navigation, i.e. tumor margin assessment. Furthermore, it provides the basis for registering the fluorescence lifetime maps to the tissue surface adapting it to possible tissue deformations.

Effect of different polishing systems on the surface roughness of nano-hybrid composites

PubMed Central

Patel, Brijesh; Chhabra, Naveen; Jain, Disha

2016-01-01

Objective: The study aimed to investigate the influence of different polishing systems on the surface roughness of nano-hybrid composite resins. Background: Different shapes of polishing systems are available according to the site of work. To minimize variability, a new system with single shape is developed that can be utilized in both anterior as well as posterior teeth. Materials and Methods: Seventy composite discs were fabricated using Teflon well (10 mm × 3 mm). Two main group of nano-hybrid composite Group I — Filtek Z350 and Group II — Tetric N-Ceram were used (n = 35 for each group). Both groups were further divided into four subgroups. Subgroup a — OneGloss (n = 10), Subgroup b - PoGo (n = 10), Subgroup c — Sof-Lex spiral (n = 10), Subgroup d - Mylar strip (control, n = 5). Samples were polished according to the manufacturer's recommendations. Surface roughness test was performed using contact profilometer. The obtained data were analyzed using the one-way analysis of variance test. Result: Tetric N-Ceram produced smoother surfaces than Filtek Z350 (P < 0.05). Mylar strip and “PoGo” created equally smooth surfaces, while significantly rougher surfaces were obtained after applications of “Sof-Lex spiral” and “OneGloss” (P < 0.05). Conclusion: Polishing ability of Tetric N-Ceram is better than Filtek Z350 XT. “PoGo” seems to be a better polishing system than “OneGloss” and “Sof-Lex Spiral.” PMID:26957791

DPSC colonization of functionalized 3D textiles.

PubMed

Ortiz, Marine; Rosales-Ibáñez, Raúl; Pozos-Guillén, Amaury; De Bien, Charlotte; Toye, Dominique; Flores, Héctor; Grandfils, Christian

2017-05-01

Fiber scaffolds are attractive materials for mimicking, within a 3D in vitro system, any living environment in which animal cells can adhere and proliferate. In three dimensions, cells have the ability to communicate and organize into complex architectures similar to those found in their natural environments. The aim of this study was to evaluate, in terms of cell reactivity, a new in vitro cell model: dental pulp stem cells (DPSCs) in a 3D polymeric textile. Scaffolds were knitted from polyglycolic acid (PGA) or polydioxanone (PDO) fibers differing in surface roughness. To promote cell adhesion, these hydrophobic fabrics were also functionalized with either chitosan or the peptide arginine-glycine-aspartic acid (RGD). Cell behavior was examined 1, 10, and 21 days post-seeding with a LIVE/DEAD ® Kit. Confocal laser scanning microscopy (CLSM) highlighted the biocompatibility of these materials (cell survival rate: 94% to 100%). Fiber roughness was found to influence cell adhesion and viability significantly and favorably. A clear benefit of polymeric textile functionalization with chitosan or RGD was demonstrated in terms of cell adhesion and viability. © 2016 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 105B: 785-794, 2017. © 2016 Wiley Periodicals, Inc.

Dual-Doppler lidar observation of horizontal convective rolls and near-surface streaks

NASA Astrophysics Data System (ADS)

Iwai, Hironori; Ishii, Shoken; Tsunematsu, Nobumitsu; Mizutani, Kohei; Murayama, Yasuhiro; Itabe, Toshikazu; Yamada, Izumi; Matayoshi, Naoki; Matsushima, Dai; Weiming, Sha; Yamazaki, Takeshi; Iwasaki, Toshiki

2008-07-01

Dual-Doppler lidar and heliborne sensors were used to investigate the three-dimensional (3D) structure of the wind field over Sendai Airport in June 2007. The 3D structures of several-hundred-meter-scale horizontal convective rolls (HCRs) in the sea-breeze layer were observed by the dual-Doppler lidar. The scale of the HCRs determined by the heliborne sensors roughly agreed with that determined by the dual-Doppler lidar. Analysis of the dual-Doppler lidar data showed that the region of upward flow in the HCRs originated in near-surface low-speed streaks. This structure is consistent with the results of large-eddy simulations of the atmospheric boundary layer. The aspect ratios of the HCRs were close to those predicted by linear theories.

Design and optimization of G-band extended interaction klystron with high output power

NASA Astrophysics Data System (ADS)

Li, Renjie; Ruan, Cunjun; Zhang, Huafeng

2018-03-01

A ladder-type Extended Interaction Klystron (EIK) with unequal-length slots in the G-band is proposed and designed. The key parameters of resonance cavities working in the π mode are obtained based on the theoretical analysis and 3D simulation. The influence of the device fabrication tolerance on the high-frequency performance is analyzed in detail, and it is found that at least 5 μm of machining precision is required. Thus, the dynamic tuning is required to compensate for the frequency shift and increase the bandwidth. The input and output coupling hole dimensions are carefully designed to achieve high output power along with a broad bandwidth. The effect of surface roughness of the metallic material on the output power has been investigated, and it is proposed that lower surface roughness leads to higher output power. The focusing magnetic field is also optimized to 0.75 T in order to maintain the beam transportation and achieve high output power. With 16.5 kV operating voltage and 0.30 A beam current, the output power of 360 W, the efficiency of 7.27%, the gain of 38.6 dB, and the 3 dB bandwidth of 500 MHz are predicted. The output properties of the EIK show great stability with the effective suppression of oscillation and mode competition. Moreover, small-signal theory analysis and 1D code AJDISK calculations are carried out to verify the results of 3D PIC simulations. A close agreement among the three methods proves the relative validity and the reliability of the designed EIK. Thus, it is indicated that the EIK with unequal-length slots has potential for power improvement and bandwidth extension.

Roughness effects on thermal-infrared emissivities estimated from remotely sensed images

NASA Astrophysics Data System (ADS)

Mushkin, Amit; Danilina, Iryna; Gillespie, Alan R.; Balick, Lee K.; McCabe, Matthew F.

2007-10-01

Multispectral thermal-infrared images from the Mauna Loa caldera in Hawaii, USA are examined to study the effects of surface roughness on remotely retrieved emissivities. We find up to a 3% decrease in spectral contrast in ASTER (Advanced Spaceborne Thermal Emission and Reflection Radiometer) 90-m/pixel emissivities due to sub-pixel surface roughness variations on the caldera floor. A similar decrease in spectral contrast of emissivities extracted from MASTER (MODIS/ASTER Airborne Simulator) ~12.5-m/pixel data can be described as a function of increasing surface roughness, which was measured remotely from ASTER 15-m/pixel stereo images. The ratio between ASTER stereo images provides a measure of sub-pixel surface-roughness variations across the scene. These independent roughness estimates complement a radiosity model designed to quantify the unresolved effects of multiple scattering and differential solar heating due to sub-pixel roughness elements and to compensate for both sub-pixel temperature dispersion and cavity radiation on TIR measurements.

Scale Effects in the Flow of a Shear-Thinning Fluid in Geological Fractures

NASA Astrophysics Data System (ADS)

Meheust, Y.; Roques, C.; Le Borgne, T.; Selker, J. S.

2017-12-01

Subsurface flow processes involving non-Newtonian fluids play a major role in many engineering applications, from in-situ remediation to enhanced oil recovery. The fluids of interest in such applications (f.e., polymers in remediation) often present shear-thinning properties, i.e., their viscosity decreases as a function of the local shear rate. We investigate how fracture wall roughness impacts the flow of a shear-thinning fluid. Numerical simulations of flow in 3D geological fractures are carried out by solving a modified Navier-Stokes equation incorporating the Carreau viscous-shear model. The numerical fractures consist of two isotropic self-affine surfaces which are correlated with each other above a characteristic scale (thecorrelation length of Méheust et al. PAGEOPH 2003). Perfect plastic closing is assumed when the surfaces are in contact. The statistical parameters describing a fracture are the standard deviation of the wall roughness, the mean aperture, the correlation length, and the fracture length, the Hurst exponent being fixed (equal to 0.8). The objective is to investigate how varying the correlation length impacts the flow behavior, for different degrees of closure, and how this behavior diverges from what is known for Newtonian fluids. The results from the 3D simulations are also compared to 2D simulations based on the lubrication theory, which we have developed as an extension of the Reynolds equation for Newtonian fluids. These 2D simulations run orders of magnitude faster, which allows considering a significant statistics of fractures of identical statistical parameters, and therefore draw general conclusions despite the large stochasticity of the media. We also discuss the implications of our results for solute transport by such flows. References:Méheust, Y., & Schmittbuhl, J. (2003). Scale effects related to flow in rough fractures. Pure and Applied Geophysics, 160(5-6), 1023-1050.

Texture descriptions of lunar surface derived from LOLA data: Kilometer-scale roughness and entropy maps

NASA Astrophysics Data System (ADS)

Li, Bo; Ling, Zongcheng; Zhang, Jiang; Chen, Jian; Wu, Zhongchen; Ni, Yuheng; Zhao, Haowei

2015-11-01

The lunar global texture maps of roughness and entropy are derived at kilometer scales from Digital Elevation Models (DEMs) data obtained by Lunar Orbiter Laser Altimeter (LOLA) aboard on Lunar Reconnaissance Orbiter (LRO) spacecraft. We use statistical moments of a gray-level histogram of elevations in a neighborhood to compute the roughness and entropy value. Our texture descriptors measurements are shown in global maps at multi-sized square neighborhoods, whose length of side is 3, 5, 10, 20, 40 and 80 pixels, respectively. We found that large-scale topographical changes can only be displayed in maps with longer side of neighborhood, but the small scale global texture maps are more disorderly and unsystematic because of more complicated textures' details. Then, the frequency curves of texture maps are made out, whose shapes and distributions are changing as the spatial scales increases. Entropy frequency curve with minimum 3-pixel scale has large fluctuations and six peaks. According to this entropy curve we can classify lunar surface into maria, highlands, different parts of craters preliminarily. The most obvious textures in the middle-scale roughness and entropy maps are the two typical morphological units, smooth maria and rough highlands. For the impact crater, its roughness and entropy value are characterized by a multiple-ring structure obviously, and its different parts have different texture results. In the last, we made a 2D scatter plot between the two texture results of typical lunar maria and highlands. There are two clusters with largest dot density which are corresponded to the lunar highlands and maria separately. In the lunar mare regions (cluster A), there is a high correlation between roughness and entropy, but in the highlands (Cluster B), the entropy shows little change. This could be subjected to different geological processes of maria and highlands forming different landforms.

Statistical characterization of surface features from tungsten-coated divertor inserts in the DIII-D Metal Rings Campaign

NASA Astrophysics Data System (ADS)

Adams, Jacob; Unterberg, Ezekial; Chrobak, Christopher; Stahl, Brian; Abrams, Tyler

2017-10-01

Continuing analysis of tungsten-coated inserts from the recent DIII-D Metal Rings Campaign utilizes a statistical approach to study carbon migration and deposition on W surfaces and to characterize the pre- versus post-exposure surface morphology. A TZM base was coated with W using both CVD and PVD and allowed for comparison between the two coating methods. The W inserts were positioned in the lower DIII-D divertor in both the upper (shelf) region and lower (floor) region and subjected to multiple plasma shots, primarily in H-mode. Currently, the post-exposure W inserts are being characterized using SEM/EDX to qualify the surface morphology and to quantify the surface chemical composition. In addition, profilometry is being used to measure the surface roughness of the inserts both before and after plasma exposure. Preliminary results suggest a correlation between the pre-exposure surface roughness and the level of carbon deposited on the surface. Furthermore, ongoing in-depth analysis may reveal insights into the formation mechanism of nanoscale bumps found in the carbon-rich regions of the W surfaces that have not yet been explained. Work supported in part by US DoE under the Science Undergraduate Laboratory Internship (SULI) program and under DE-FC02-04ER54698.

Effect of prophylactic polishing protocols on the surface roughness of esthetic restorative materials.

PubMed

Neme, A L; Frazier, K B; Roeder, L B; Debner, T L

2002-01-01

Many polishing protocols have been evaluated in vitro for their effect on the surface roughness of restorative materials. These results have been useful in establishing protocols for in vivo application. However, limited research has focused on the subsequent care and maintenance of esthetic restorations following their placement. This investigation evaluated the effect of five polishing protocols that could be implemented at recall on the surface roughness of five direct esthetic restorative materials. Specimens (n=25) measuring 8 mm diameter x 3 mm thick were fabricated in an acrylic mold using five light-cured resin-based materials (hybrid composite, microfilled composite, packable composite, compomer and resin-modified glass ionomer). After photopolymerization, all specimens were polished with Sof-Lex Disks to produce an initial (baseline) surface finish. All specimens were then polished with one of five prophylactic protocols (Butler medium paste, Butler coarse paste, OneGloss, SuperBuff or OneGloss & SuperBuff). The average surface roughness of each treated specimen was determined from three measurements with a profilometer (Surface 1). Next, all specimens were brushed 60,000 times at 1.5 Hz using a brush-head force of 2 N on a Manly V-8 cross-brushing machine in a 50:50 (w/w) slurry of toothpaste and water. The surface roughness of each specimen was measured after brushing (Surface 2) followed by re-polishing with one of five protocols, then final surface roughness values were determined (Surface 3). The data were analyzed using repeated measures ANOVA. Significant differences (p=0.05) in surface roughness were observed among restorative materials and polishing protocols. The microfilled and hybrid resin composite yielded significantly rougher surfaces than the other three materials following tooth brushing. Prophylactic polishing protocols can be used to restore a smooth surface on resin-based esthetic restorative materials following simulated tooth brushing.

An Experimental Study of Momentum and Thermal Transport in Flow through Smooth- and Rough-Wall Microchannels

ERIC Educational Resources Information Center

Natrajan, Vinay Kumar

2009-01-01

The impact of surface roughness on momentum and thermal transport in microscale flow passages of hydraulic diameter D[subscript h] = 600 micrometer is investigated in the laminar, transitional and turbulent flow regimes using microscopic PIV, two-color LIF thermometry and pressure-drop measurements. In addition to smooth-wall flow, two different…

The effect of row structure on soil moisture retrieval accuracy from passive microwave data.

PubMed

Xingming, Zheng; Kai, Zhao; Yangyang, Li; Jianhua, Ren; Yanling, Ding

2014-01-01

Row structure causes the anisotropy of microwave brightness temperature (TB) of soil surface, and it also can affect soil moisture retrieval accuracy when its influence is ignored in the inversion model. To study the effect of typical row structure on the retrieved soil moisture and evaluate if there is a need to introduce this effect into the inversion model, two ground-based experiments were carried out in 2011. Based on the observed C-band TB, field soil and vegetation parameters, row structure rough surface assumption (Q p model and discrete model), including the effect of row structure, and flat rough surface assumption (Q p model), ignoring the effect of row structure, are used to model microwave TB of soil surface. Then, soil moisture can be retrieved, respectively, by minimizing the difference of the measured and modeled TB. The results show that soil moisture retrieval accuracy based on the row structure rough surface assumption is approximately 0.02 cm(3)/cm(3) better than the flat rough surface assumption for vegetated soil, as well as 0.015 cm(3)/cm(3) better for bare and wet soil. This result indicates that the effect of row structure cannot be ignored for accurately retrieving soil moisture of farmland surface when C-band is used.

Geometric effects on surface states in topological insulator Bi2Te3 nanowire

NASA Astrophysics Data System (ADS)

Sengupta, Parijat; Kubis, Tillman; Povolotskyi, Michael; Klimeck, Gerhard

2012-02-01

Bismuth Telluride (BT) is a 3D topological insulator (TI) with surface states that have energy dispersion linear in momentum and forms a Dirac cone at low energy. In this work we investigate the surface properties of a BT nanowire and demonstrate the existence of TI states. We also show how such states vanish under certain geometric conditions. An atomistic model (sp3d5s* TB) is used to compute the energy dispersion in a BT nanowire. Penetration depth of the surface states is estimated by ratio of Fermi velocity and band-gap. BT possesses a tiny band-gap, which creates small localization of surface states and greater penetration in to the bulk. To offset this large spatial penetration, which is undesirable to avoid a direct coupling between surfaces, we expect that bigger cross-sections of BT nanowires would be needed to obtain stable TI states. Our numerical work validates this prediction. Furthermore, geometry of the nanowire is shown to influence the TI states. Using a combined analytical and numerical approach our results reveal that surface roughness impact electronic structure leading to Rashba type splits along z-direction. Cylindrical and square cross-sections are given as illustrative examples.

Surface topography characterization using 3D stereoscopic reconstruction of SEM images

NASA Astrophysics Data System (ADS)

Vedantha Krishna, Amogh; Flys, Olena; Reddy, Vijeth V.; Rosén, B. G.

2018-06-01

A major drawback of the optical microscope is its limitation to resolve finer details. Many microscopes have been developed to overcome the limitations set by the diffraction of visible light. The scanning electron microscope (SEM) is one such alternative: it uses electrons for imaging, which have much smaller wavelength than photons. As a result high magnification with superior image resolution can be achieved. However, SEM generates 2D images which provide limited data for surface measurements and analysis. Often many research areas require the knowledge of 3D structures as they contribute to a comprehensive understanding of microstructure by allowing effective measurements and qualitative visualization of the samples under study. For this reason, stereo photogrammetry technique is employed to convert SEM images into 3D measurable data. This paper aims to utilize a stereoscopic reconstruction technique as a reliable method for characterization of surface topography. Reconstructed results from SEM images are compared with coherence scanning interferometer (CSI) results obtained by measuring a roughness reference standard sample. This paper presents a method to select the most robust/consistent surface texture parameters that are insensitive to the uncertainties involved in the reconstruction technique itself. Results from the two-stereoscopic reconstruction algorithms are also documented in this paper.

Process Characterization of Electrical Discharge Machining of Highly Doped Silicon

DTIC Science & Technology

2012-06-01

EEE .! E# EEE @! E#EEEI! E#EEEJ! E# EE "! E# EE ".! E# EE "@! E# EE "I! E# EE "J! $L! $U! 07$(L<--B(L$B(F-O(D1$(ZL]\\(E[( GMU! GML! 64... EE ! LFE# EE ! L@F# EE ! L@E# EE ! L<F# EE ! L<E# EE ! L.F# EE ! &*6)! M! NDO! D! %A! DP! N5P! /G! G! LY > (Z B ; [( G&’=41416(D1ɟ$(H&%&C-$-%( IEFG(N.76=416(LY...roughing experiment. Surface roughness measurements ranged from just over 24

Introductory review on `Flying Triangulation': a motion-robust optical 3D measurement principle

NASA Astrophysics Data System (ADS)

Ettl, Svenja

2015-04-01

'Flying Triangulation' (FlyTri) is a recently developed principle which allows for a motion-robust optical 3D measurement of rough surfaces. It combines a simple sensor with sophisticated algorithms: a single-shot sensor acquires 2D camera images. From each camera image, a 3D profile is generated. The series of 3D profiles generated are aligned to one another by algorithms, without relying on any external tracking device. It delivers real-time feedback of the measurement process which enables an all-around measurement of objects. The principle has great potential for small-space acquisition environments, such as the measurement of the interior of a car, and motion-sensitive measurement tasks, such as the intraoral measurement of teeth. This article gives an overview of the basic ideas and applications of FlyTri. The main challenges and their solutions are discussed. Measurement examples are also given to demonstrate the potential of the measurement principle.

Effect of surface roughness on the in vitro degradation behaviour of a biodegradable magnesium-based alloy

NASA Astrophysics Data System (ADS)

Walter, R.; Kannan, M. Bobby; He, Y.; Sandham, A.

2013-08-01

In this study, the in vitro degradation behaviour of AZ91 magnesium alloy with two different surface finishes was investigated using electrochemical impedance spectroscopy (EIS) in simulated body fluid (SBF). The polarisation resistance (Rp) of the rough surface alloy immersed in SBF for 3 h was ~30% lower as compared to that of the smooth surface alloy. After 12 h immersion in SBF, the Rp values for both the surface finishes decreased and were also similar. However, localised degradation occurred sooner, and to a noticeably higher severity in the rough surface alloy as compared to the smooth surface alloy.

Hydrodynamic instability experiments with three-dimensional modulations at the National Ignition Facility

DOE PAGES

Smalyuk, V. A.; Weber, S. V.; Casey, D. T.; ...

2015-06-18

The first hydrodynamic instability growth measurements with three-dimensional (3D) surface-roughness modulations were performed on CH shell spherical implosions at the National Ignition Facility (NIF) [G. H. Miller, E. I. Moses, and C. R. Wuest, Opt. Eng. 43, 2841 (2004)]. The initial capsule outer-surface amplitudes were increased approximately four times, compared with the standard specifications, to increase the signal-to-noise ratio, helping to qualify a technique for measuring small 3D modulations. The instability growth measurements were performed using x-ray through-foil radiography based on time-resolved pinhole imaging. Averaging over 15 similar images significantly increased the signal-to-noise ratio, making possible a comparison with 3Dmore » simulations. At a convergence ratio of ~2.4, the measured modulation levels were ~3 times larger than those simulated based on the growth of the known imposed initial surface modulations. Several hypotheses are discussed, including increased instability growth due to modulations of the oxygen content in the bulk of the capsule. In conclusion, future experiments will be focused on measurements with standard 3D ‘native-roughness’ capsules as well as with deliberately imposed oxygen modulations.« less

The influence of machining condition and cutting tool wear on surface roughness of AISI 4340 steel

NASA Astrophysics Data System (ADS)

Natasha, A. R.; Ghani, J. A.; Che Haron, C. H.; Syarif, J.

2018-01-01

Sustainable machining by using cryogenic coolant as the cutting fluid has been proven to enhance some machining outputs. The main objective of the current work was to investigate the influence of machining conditions; dry and cryogenic, as well as the cutting tool wear on the machined surface roughness of AISI 4340 steel. The experimental tests were performed using chemical vapor deposition (CVD) coated carbide inserts. The value of machined surface roughness were measured at 3 cutting intervals; beginning, middle, and end of the cutting based on the readings of the tool flank wear. The results revealed that cryogenic turning had the greatest influence on surface roughness when machined at lower cutting speed and higher feed rate. Meanwhile, the cutting tool wear was also found to influence the surface roughness, either improving it or deteriorating it, based on the severity and the mechanism of the flank wear.

Addressing scale dependence in roughness and morphometric statistics derived from point cloud data.

NASA Astrophysics Data System (ADS)

Buscombe, D.; Wheaton, J. M.; Hensleigh, J.; Grams, P. E.; Welcker, C. W.; Anderson, K.; Kaplinski, M. A.

2015-12-01

The heights of natural surfaces can be measured with such spatial density that almost the entire spectrum of physical roughness scales can be characterized, down to the morphological form and grain scales. With an ability to measure 'microtopography' comes a demand for analytical/computational tools for spatially explicit statistical characterization of surface roughness. Detrended standard deviation of surface heights is a popular means to create continuous maps of roughness from point cloud data, using moving windows and reporting window-centered statistics of variations from a trend surface. If 'roughness' is the statistical variation in the distribution of relief of a surface, then 'texture' is the frequency of change and spatial arrangement of roughness. The variance in surface height as a function of frequency obeys a power law. In consequence, roughness is dependent on the window size through which it is examined, which has a number of potential disadvantages: 1) the choice of window size becomes crucial, and obstructs comparisons between data; 2) if windows are large relative to multiple roughness scales, it is harder to discriminate between those scales; 3) if roughness is not scaled by the texture length scale, information on the spacing and clustering of roughness `elements' can be lost; and 4) such practice is not amenable to models describing the scattering of light and sound from rough natural surfaces. We discuss the relationship between roughness and texture. Some useful parameters which scale vertical roughness to characteristic horizontal length scales are suggested, with examples of bathymetric point clouds obtained using multibeam from two contrasting riverbeds, namely those of the Colorado River in Grand Canyon, and the Snake River in Hells Canyon. Such work, aside from automated texture characterization and texture segmentation, roughness and grain size calculation, might also be useful for feature detection and classification from point clouds.

Fluorescence Enhancement on Large Area Self-Assembled Plasmonic-3D Photonic Crystals.

PubMed

Chen, Guojian; Wang, Dongzhu; Hong, Wei; Sun, Lu; Zhu, Yongxiang; Chen, Xudong

2017-03-01

Discontinuous plasmonic-3D photonic crystal hybrid structures are fabricated in order to evaluate the coupling effect of surface plasmon resonance and the photonic stop band. The nanostructures are prepared by silver sputtering deposition on top of hydrophobic 3D photonic crystals. The localized surface plasmon resonance of the nanostructure has a symbiotic relationship with the 3D photonic stop band, leading to highly tunable characteristics. Fluorescence enhancements of conjugated polymer and quantum dot based on these hybrid structures are studied. The maximum fluorescence enhancement for the conjugated polymer of poly(5-methoxy-2-(3-sulfopropoxy)-1,4-phenylenevinylene) potassium salt by a factor of 87 is achieved as compared with that on a glass substrate due to the enhanced near-field from the discontinuous plasmonic structures, strong scattering effects from rough metal surface with photonic stop band, and accelerated decay rates from metal-coupled excited state of the fluorophore. It is demonstrated that the enhancement induced by the hybrid structures has a larger effective distance (optimum thickness ≈130 nm) than conventional plasmonic systems. It is expected that this approach has tremendous potential in the field of sensors, fluorescence-imaging, and optoelectronic applications. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

3D fault curvature and fractal roughness: Insights for rupture dynamics and ground motions using a Discontinous Galerkin method

NASA Astrophysics Data System (ADS)

Ulrich, Thomas; Gabriel, Alice-Agnes

2017-04-01

Natural fault geometries are subject to a large degree of uncertainty. Their geometrical structure is not directly observable and may only be inferred from surface traces, or geophysical measurements. Most studies aiming at assessing the potential seismic hazard of natural faults rely on idealised shaped models, based on observable large-scale features. Yet, real faults are wavy at all scales, their geometric features presenting similar statistical properties from the micro to the regional scale. Dynamic rupture simulations aim to capture the observed complexity of earthquake sources and ground-motions. From a numerical point of view, incorporating rough faults in such simulations is challenging - it requires optimised codes able to run efficiently on high-performance computers and simultaneously handle complex geometries. Physics-based rupture dynamics hosted by rough faults appear to be much closer to source models inverted from observation in terms of complexity. Moreover, the simulated ground-motions present many similarities with observed ground-motions records. Thus, such simulations may foster our understanding of earthquake source processes, and help deriving more accurate seismic hazard estimates. In this presentation, the software package SeisSol (www.seissol.org), based on an ADER-Discontinuous Galerkin scheme, is used to solve the spontaneous dynamic earthquake rupture problem. The usage of tetrahedral unstructured meshes naturally allows for complicated fault geometries. However, SeisSol's high-order discretisation in time and space is not particularly suited for small-scale fault roughness. We will demonstrate modelling conditions under which SeisSol resolves rupture dynamics on rough faults accurately. The strong impact of the geometric gradient of the fault surface on the rupture process is then shown in 3D simulations. Following, the benefits of explicitly modelling fault curvature and roughness, in distinction to prescribing heterogeneous initial stress conditions on a planar fault, is demonstrated. Furthermore, we show that rupture extend, rupture front coherency and rupture speed are highly dependent on the initial amplitude of stress acting on the fault, defined by the normalized prestress factor R, the ratio of the potential stress drop over the breakdown stress drop. The effects of fault complexity are particularly pronounced for lower R. By low-pass filtering a rough fault at several cut-off wavelengths, we then try to capture rupture complexity using a simplified fault geometry. We find that equivalent source dynamics can only be obtained using a scarcely filtered fault associated with a reduced stress level. To investigate the wavelength-dependent roughness effect, the fault geometry is bandpass-filtered over several spectral ranges. We show that geometric fluctuations cause rupture velocity fluctuations of similar length scale. The impact of fault geometry is especially pronounced when the rupture front velocity is near supershear. Roughness fluctuations significantly smaller than the rupture front characteristic dimension (cohesive zone size) affect only macroscopic rupture properties, thus, posing a minimum length scale limiting the required resolution of 3D fault complexity. Lastly, the effect of fault curvature and roughness on the simulated ground-motions is assessed. Despite employing a simple linear slip weakening friction law, the simulated ground-motions compare well with estimates from ground motions prediction equations, even at relatively high frequencies.

Evaluation of surface roughness of enamel after various bonding and clean-up procedures on enamel bonded with three different bonding agents: An in-vitro study

PubMed Central

Goel, Amit; Singh, Atul; Gupta, Tarun

2017-01-01

Background The purpose of this study was to analyze and compare the enamel surface roughness before bonding and after debonding, to find correlation between the adhesive remnant index and its effect on enamel surface roughness and to evaluate which clean-up method is most efficient to provide a smoother enamel surface. Material and Methods 135 premolars were divided into 3 groups containing 45 premolars in each group. Group I was bonded by using moisture insensitive primer, Group II by using conventional orthodontic adhesive and Group III by using self-etching primer. Each group was divided into 3 sub-groups on the basis of type of clean-up method applied i,e scaling followed by polishing, tungsten carbide bur and Sof-Lex disc. Enamel surface roughness was measured and compared before bonding and after clean-up. Results Evaluation of pre bonding and post clean-up enamel surface roughness (Ra value) with the t test showed that Post clean-up Ra values were greater than Pre bonding Ra values in all the groups except in teeth bonded with self-etching primer cleaned with Sof-Lex disc. Reliability of ARI score taken at different time interval tested with Kruskal Wallis test suggested that all the readings were reliable. Conclusions No clean-up procedure was able to restore the enamel to its original smoothness. Self-etching primer and Sof-Lex disc clean-up method combination restored the enamel surface roughness (Ra value) closest to its pre-treatment value. Key words:Enamel surface roughness, clean-up method, adhesive remnant index. PMID:28512535

Radiative transfer simulations of the two-dimensional ocean glint reflectance and determination of the sea surface roughness.

PubMed

Lin, Zhenyi; Li, Wei; Gatebe, Charles; Poudyal, Rajesh; Stamnes, Knut

2016-02-20

An optimized discrete-ordinate radiative transfer model (DISORT3) with a pseudo-two-dimensional bidirectional reflectance distribution function (BRDF) is used to simulate and validate ocean glint reflectances at an infrared wavelength (1036 nm) by matching model results with a complete set of BRDF measurements obtained from the NASA cloud absorption radiometer (CAR) deployed on an aircraft. The surface roughness is then obtained through a retrieval algorithm and is used to extend the simulation into the visible spectral range where diffuse reflectance becomes important. In general, the simulated reflectances and surface roughness information are in good agreement with the measurements, and the diffuse reflectance in the visible, ignored in current glint algorithms, is shown to be important. The successful implementation of this new treatment of ocean glint reflectance and surface roughness in DISORT3 will help improve glint correction algorithms in current and future ocean color remote sensing applications.

Radiative Transfer Simulations of the Two-Dimensional Ocean Glint Reflectance and Determination of the Sea Surface Roughness

NASA Technical Reports Server (NTRS)

Lin, Zhenyi; Li, Wei; Gatebe, Charles; Poudyal, Rajesh; Stamnes, Knut

2016-01-01

An optimized discrete-ordinate radiative transfer model (DISORT3) with a pseudo-two-dimensional bidirectional reflectance distribution function (BRDF) is used to simulate and validate ocean glint reflectances at an infrared wavelength (1036 nm) by matching model results with a complete set of BRDF measurements obtained from the NASA cloud absorption radiometer (CAR) deployed on an aircraft. The surface roughness is then obtained through a retrieval algorithm and is used to extend the simulation into the visible spectral range where diffuse reflectance becomes important. In general, the simulated reflectances and surface roughness information are in good agreement with the measurements, and the diffuse reflectance in the visible, ignored in current glint algorithms, is shown to be important. The successful implementation of this new treatment of ocean glint reflectance and surface roughness in DISORT3 will help improve glint correction algorithms in current and future ocean color remote sensing applications.

Evidence of a metal-rich surface for the Asteroid (16) Psyche from interferometric observations in the thermal infrared

NASA Astrophysics Data System (ADS)

Matter, Alexis; Delbo, Marco; Carry, Benoit; Ligori, Sebastiano

2013-09-01

We describe the first determination of thermal properties and size of the M-type Asteroid (16) Psyche from interferometric observations obtained with the Mid-Infrared Interferometric Instrument (MIDI) of the Very Large Telescope Interferometer. We used a thermophysical model to interpret our interferometric data. Our analysis shows that Psyche has a low macroscopic surface roughness. Using a convex 3-D shape model obtained by Kaasalainen et al. (Kaasalainen, M., Torppa, J., Piironen, J. [2002]. Icarus 159, 369-395), we derived a volume-equivalent diameter for (16) Psyche of 247 ± 25 km or 238 ± 24 km, depending on the possible values of surface roughness. Our corresponding thermal inertia estimates are 133 or 114 J m-2 s-0.5 K-1, with a total uncertainty estimated at 40 J m-2 s-0.5 K-1. They are among the highest thermal inertia values ever measured for an asteroid of this size. We consider this as a new evidence of a metal-rich surface for the Asteroid (16) Psyche.

Impact of cleaning methods on the structural properties and morphology of SrTiO3 surface

NASA Astrophysics Data System (ADS)

Arnay, Iciar; Rubio-Zuazo, Juan; Castro, German R.

2018-01-01

SrTiO3 is a widely used substrate for the epitaxial growth of complex systems. Nevertheless, in order to get good quality interface and avoid the formation of defects in the adsorbed layer it is essential to prepare the surface of the substrate prior to the deposition. Thermal and chemical treatments are mostly used to eliminate superficial contamination and improve the surface quality. However, there is a lack of information regarding the impact of these treatments on the formation of structural defects at the SrTiO3 surface. In this work we present a detailed characterization of the SrTiO3 surface for the different cleaning methods paying special attention to the formation of oxygen vacancies, large surface mosaicity and roughness. We prove that thermal treatment induces large surface roughness and that chemical etching produces important structural defects at the surface. Our results show that mechanical polishing provided the best compromise in terms of large surface domains, low roughness, absence of oxygen vacancies and absence of atomic structure modification, although with the presence of low level of contaminants at the SrTiO3 surface.

Shear bond, wettability and AFM evaluations on CO2 laser-irradiated CAD/CAM ceramic surfaces.

PubMed

El Gamal, Ahmed; Medioni, Etienne; Rocca, Jean Paul; Fornaini, Carlo; Muhammad, Omid H; Brulat-Bouchard, Nathalie

2017-05-01

The purpose of this study is to determine the CO 2 laser irradiation in comparison with sandblasting (Sb), hydrofluoric acid (Hf) and silane coupling agent (Si) on shear bond strength (SBS), roughness (Rg) and wettability (Wt) of resin cement to CAD/CAM ceramics. Sixty (CAD/CAM) ceramic discs were prepared and distributed into six different groups: group A, control lithium disilicate (Li); group B, control zirconia (Zr); group C, Li: CO 2 /HF/Si; group D, Li: HF/Si; group E, Zr: CO 2 /Sb/Si; group F, Zr: Sb/Si. Result showed significant difference between irradiated and non-irradiated in terms of shear bond strength for zirconia ceramics (p value = 0.014). Moreover, partial surface wettability for irradiated and non-irradiated ceramics. Irradiated surface demonstrated more rough surface in lithium disilicate than zirconia ceramics. CO 2 irradiation could increase shear bond strength, surface roughness and wettability for both CAD/CAM ceramics.

Estimation of effective aerodynamic roughness with altimeter measurements

NASA Technical Reports Server (NTRS)

Menenti, M.; Ritchie, J. C.

1992-01-01

A new method is presented for estimating the aerodynamic roughness length of heterogeneous land surfaces and complex landscapes using elevation measurements performed with an airborne laser altimeter and the Seasat radar altimeter. Land surface structure is characterized at increasing length scales by considering three basic landscape elements: (1) partial to complete canopies of herbaceous vegetation; (2) sparse obstacles (e.g., shrubs and trees); and (3) local relief. Measured parameters of land surface geometry are combined to obtain an effective aerodynamic roughness length which parameterizes the total atmosphere-land surface stress.

Impact of pre-incubation time of silk fibroin scaffolds in culture medium on cell proliferation and attachment.

PubMed

Amirikia, Mehdi; Shariatzadeh, Seyed Mohammad Ali; Jorsaraei, Seyed Gholam Ali; Soleimani Mehranjani, Malek

2017-12-01

Cell behaviours such as proliferation and attachment can be affected by the length of pre-incubation period of the scaffolds in the culture medium for long term. The aim of this study was to investigate the long term pre-incubation of 3D silk fibroin scaffolds in complete culture medium on cell attachment and proliferation. After the preparation of silk fibroin scaffolds by the technique of freeze drying, the scaffolds were pre-incubated in complete culture medium for 2 d, 6 d or 10 d before apical papilla stem cells (SCAP) seeding. Modifications of the scaffold surface and wettability were examined by FE-SEM and water contact angle, respectively. Results showed a decrease both in roughness and water contact angle as pre-incubation time increases. DNA measurement after 18h and 10 d cell seeding showed a significant increase of DNA concentration which represents better attachment and proliferation with pre-incubation time increase. Qualitative examination, live&dead assay or H&E staining method after 30h and 10 d cell seeding respectively, indicated that pre-incubation of scaffolds has time dependent effect on cell proliferation and attachment. This suggests that improvement of cell attachment and proliferation may be mediated by differences in the amount of wettability (decreased water contact angle) after exposure of scaffold to culture medium for long term which, in turn, causes more protein adsorption in the surface of silk fibroin scaffold (decreased roughness). Copyright © 2017. Published by Elsevier Ltd.

ICO Topical Meeting on Atmospheric, Volume and Surface Scattering and Propagation Held in Florence, Italy on 27-30 August 1991

DTIC Science & Technology

1991-01-01

66,207 (1976). 3. M. Abitbol, " Wavefront Sensing in Adaptive Optics System," Ph.d Thesis submited to the senat of the Hebrew University OCt. 1990... thesis , University of London (In preparation). 14. Cope, M. et al (1989) Adv. in Exp. Med. & Biol., 247, 33-40 15. Kottler, F. (1980) Journal of the...Ph.D. Thesis . University of llelsinki, (1990) (9] K. Muinonen and K. Lumme. subm. to Proc. 126th I[AU (olloquiin, Kyoto. (1990) 221 1~ roughness=0.0

Modeling photopolarimetric characteristics of comet dust as a polydisperse mixture of polyshaped rough spheroids

NASA Astrophysics Data System (ADS)

Kolokolova, L.; Das, H.; Dubovik, O.; Lapyonok, T.

2013-12-01

It is widely recognized now that the main component of comet dust is aggregated particles that consist of submicron grains. It is also well known that cometary dust obey a rather wide size distribution with abundant particles whose size reaches dozens of microns. However, numerous attempts of computer simulation of light scattering by comet dust using aggregated particles have not succeeded to consider particles larger than a couple of microns due to limitations in the memory and speed of available computers. Attempts to substitute aggregates by polydisperse solid particles (spheres, spheroids, cylinders) could not consistently reproduce observed angular and spectral characteristics of comet brightness and polarization even in such a general case as polyshaped (i.e. containing particles of a variety of aspect ratios) mixture of spheroids (Kolokolova et al., In: Photopolarimetry in Remote Sensing, Kluwer Acad. Publ., 431, 2004). In this study we are checking how well cometary dust can be modeled using modeling tools for rough spheroids. With this purpose we use the software package described in Dubovik et al. (J. Geophys. Res., 111, D11208, doi:10.1029/2005JD006619d, 2006) that allows for a substantial reduction of computer time in calculating scattering properties of spheroid mixtures by means of using pre-calculated kernels - quadrature coefficients employed in the numerical integration of spheroid optical properties over size and shape. The kernels were pre-calculated for spheroids of 25 axis ratios, ranging from 0.3 to 3, and 42 size bins within the size parameter range 0.01 - 625. This software package has been recently expanded with the possibility of simulating not only smooth but also rough spheroids that is used in present study. We consider refractive indexes of the materials typical for comet dust: silicate, carbon, organics, and their mixtures. We also consider porous particles accounting on voids in the spheroids through effective medium approach. The roughness of the spheroids is considered as a normal distribution of particle surface slopes and can be of different degree depending on the standard deviation of the distribution, σ, where σ=0 corresponds to smooth surface and σ=0.5 describes severely rough surface (see Young et al., J. Atm. Sci., 70, 330, 2012). We perform computations for two wavelengths, typical for blue (447nm) and red (640nm) cometary continuum filters. We compare phase angle dependence of polarization and brightness and their spectral change obtained with the rough-spheroid model with those observed for comets (e.g. Kolokolova et al., In: Comets 2, Arizona Press, 577, 2004) to see how well rough spheroids can reproduce cometary low albedo, red color, red polarimetric color, negative polarization at small phase angles and polarization maximum at medium phase angles.

Influence of the artificial saliva storage on 3-D surface texture characteristics of contemporary dental nanocomposites.

PubMed

Ţălu, Ştefan; Bramowicz, Miroslaw; Kulesza, Slawomir; Lainović, Tijana; Vilotić, Marko; Blažić, Larisa

2016-11-01

The aim of this study was to analyse the influence of the artificial saliva on a three-dimensional (3-D) surface texture of contemporary dental composites. The representatives of four composites types were tested: nanofilled (Filtek Ultimate Body, FUB), nanohybrid (Filtek Z550, FZ550), microfilled (Gradia Direct, GD) and microhybrid (Filtek Z250, FZ250). The specimens were polymerised and polished by the multistep protocol (SuperSnap, Shofu). Their surface was examined, before and after 3 weeks' exposure to artificial saliva storage. The surface texture was analysed using the atomic force microscope (AFM). The obtained images were processed to calculate the areal autocorrelation function (AACF), anisotropy ratio S tr (texture aspect ratio), and structure function (SF). The log-log plots of SF were used to calculate fractal properties, such as fractal dimension D, and pseudo-topothesy K. The analysis showed changes in surface anisotropy ratio S tr values, which became higher, whereas the S q roughness (root-mean-square) reduced after the artificial saliva storage. All the samples exhibited bifractal structure before the saliva treatment, but only half of them remained bifractal afterwards (GD, FZ250), whereas the other half turned into a monofractal (FUB, FZ550). The cube-count fractal dimension D cc was found to be material- and treatment-insensitive. © 2016 The Authors Journal of Microscopy © 2016 Royal Microscopical Society.

Comparative histomorphometry and resonance frequency analysis of implants with moderately rough surfaces in a loaded animal model.

PubMed

Al-Nawas, B; Groetz, K A; Goetz, H; Duschner, H; Wagner, W

2008-01-01

Test of favourable conditions for osseointegration with respect to optimum bone-implant contact (BIC) in a loaded animal model. The varied parameters were surface roughness and surface topography of commercially available dental implants. Thirty-two implants of six types of macro and microstructure were included in the study (total 196). The different types were: minimally rough control: Branemark machined Mk III; oxidized surface: TiUnite MkIII and MkIV; ZL Ticer; blasted and etched surface: Straumann SLA; rough control: titanium plasma sprayed (TPS). Sixteen beagle dogs were implanted with the whole set of the above implants. After a healing period of 8 weeks, implants were loaded for 3 months. For the evaluation of the BIC areas, adequately sectioned biopsies were visualized by subsurface scans with confocal laser scanning microscopy (CLSM). The primary statistical analysis testing BIC of the moderately rough implants (mean 56.1+/-13.0%) vs. the minimally rough and the rough controls (mean 53.9+/-11.2%) does not reveal a significant difference (P=0.57). Mean values of 50-70% BIC were found for all implant types. Moderately rough oxidized implants show a median BIC, which is 8% higher than their minimally rough turned counterpart. The intraindividual difference between the TPS and the blasted and etched counterparts revealed no significant difference. The turned and the oxidized implants show median values of the resonance frequency [implant stability quotients (ISQ)] over 60; the nonself-tapping blasted and etched and TPS implants show median values below 60. In conclusion, the benefit of rough surfaces relative to minimally rough ones in this loaded animal model was confirmed histologically. The comparison of different surface treatment modalities revealed no significant differences between the modern moderately rough surfaces. Resonance frequency analysis seems to be influenced in a major part by the transducer used, thus prohibiting the comparison of different implant systems.

Adhesion and proliferation of fibroblasts on RF plasma-deposited nanostructured fluorocarbon coatings: evidence of FAK activation.

PubMed

Rosso, Francesco; Marino, Gerardo; Muscariello, Livio; Cafiero, Gennaro; Favia, Pietro; D'Aloia, Erica; d'Agostino, Riccardo; Barbarisi, Alfonso

2006-06-01

We used combined plasma-deposition process to deposit smooth and nanostructured fluorocarbon coatings on polyethylenethereftalate (PET) substrates, to obtain surfaces with identical chemical composition and different roughness, and investigate the effect of surface nanostructures on adhesion and proliferation of 3T3 Swiss Albino Mouse fibroblasts. Untreated PET and polystyrene (PS) were used as controls for cell culture. We have found that the statistically significant increase of cell proliferation rate and FAK (a nonreceptor tyrosine kinase) activation detected on ROUGH fluorocarbon surfaces is due to the presence of nanostructures. Changes in cytoskeletal organization and phospho FAK (tyr 397) localization were evident after 60 min on cells adhering to ROUGH surfaces. This change was characterized by the formation of actin stress fibers along lamellar membrane protrusion instead of usual focal contacts. Also the morphology of the adhering fibroblasts (60 min) adhering on ROUGH surfaces was found quite different compared to cells adhering on smooth ones. Copyright 2006 Wiley-Liss, Inc.

Effects of uniform surface roughness on vortex-induced vibration of towed vertical cylinders

NASA Astrophysics Data System (ADS)

Kiu, K. Y.; Stappenbelt, B.; Thiagarajan, K. P.

2011-09-01

The present study was motivated by a desire to understand the vortex-induced vibration (VIV) of cylindrical offshore structures such as spars in strong currents. In particular, the consequences of marine growth on the surface as well as natural surface roughness that occurs with years in service are studied. Of special interest is the effect of surface roughness on the response amplitudes and the forces experienced by these structures while undergoing VIV. The experimental apparatus employed for the present study consisted of an elastically mounted rigid vertical cylinder with no end plates, towed along the length of a water tank. The cylinder was attached to a parallel linkage mechanism allowing motion in the transverse direction only. The cylinder surface was covered by sandpapers with known mean particle diameters, thus providing controlled values of roughness coefficient from 0.28×10 -3 to 1.38×10 -2. The tests covered the subcritical range of Reynolds number from 1.7×10 4 to 8.3×10 4, and a reduced velocity range from 4 to 16. It was found that as the roughness of the cylinder was increased the maximum response amplitude and the maximum mean drag coefficient decreased, levelling off to constant values. The onset of lock-in was progressively delayed for rougher cylinders, and the width of the lock-in region showed remarkable reduction at higher roughness values. The Strouhal number was found to display a modest increase with roughness. The dynamic mean drag of the rough cylinders was also found to be lower than that for a smooth cylinder. It is felt that uniform roughness such as caused in marine environments may act favorably to lower VIV incidence and effects in the range of Reynolds number tested.

Convective Enhancement of Icing Roughness Elements in Stagnation Region Flows

NASA Technical Reports Server (NTRS)

Hughes, Michael T.; McClain, Stephen T.; Vargas, Mario; Broeren, Andy

2015-01-01

To improve existing ice accretion simulation codes, more data regarding ice roughness and its effects on convective heat transfer are required. To build on existing research on this topic, this study used the Vertical Icing Studies Tunnel (VIST) at NASA Glenn Research to model realistic ice roughness in the stagnation region of a NACA 0012 airfoil. Using the VIST, a test plate representing the leading 2% chord of the airfoil was subjected to flows of 7.62 m/s (25 ft/s), 12.19 m/s (40 ft/s), and 16.76 m/s (55 ft/s). The test plate was fitted with 3 surfaces, each with a different representation of ice roughness: 1) a control surface with no ice roughness, 2) a surface with ice roughness with element height scaled by 10x and streamwise rough zone width from the stagnation point scaled by 10x, and 3) a surface with ice roughness with element height scaled by 10x and streamwise rough zone width from the stagnation point scaled by 25x. Temperature data from the tests were recorded using an infrared camera and thermocouples imbedded in the test plate. From the temperature data, a convective heat transfer coefficient map was created for each case. Additional testing was also performed to validate the VIST's flow quality. These tests included five-hole probe and hot-wire probe velocity traces to provide flow visualization and to study boundary layer formation on the various test surfaces. The knowledge gained during the experiments will help improve ice accretion codes by providing heat transfer coefficient validation data and by providing flow visualization data helping understand current and future experiments performed in the VIST.

3D displacement field measurement with correlation based on the micro-geometrical surface texture

NASA Astrophysics Data System (ADS)

Bubaker-Isheil, Halima; Serri, Jérôme; Fontaine, Jean-François

2011-07-01

Image correlation methods are widely used in experimental mechanics to obtain displacement field measurements. Currently, these methods are applied using digital images of the initial and deformed surfaces sprayed with black or white paint. Speckle patterns are then captured and the correlation is performed with a high degree of accuracy to an order of 0.01 pixels. In 3D, however, stereo-correlation leads to a lower degree of accuracy. Correlation techniques are based on the search for a sub-image (or pattern) displacement field. The work presented in this paper introduces a new correlation-based approach for 3D displacement field measurement that uses an additional 3D laser scanner and a CMM (Coordinate Measurement Machine). Unlike most existing methods that require the presence of markers on the observed object (such as black speckle, grids or random patterns), this approach relies solely on micro-geometrical surface textures such as waviness, roughness and aperiodic random defects. The latter are assumed to remain sufficiently small thus providing an adequate estimate of the particle displacement. The proposed approach can be used in a wide range of applications such as sheet metal forming with large strains. The method proceeds by first obtaining cloud points using the 3D laser scanner mounted on a CMM. These points are used to create 2D maps that are then correlated. In this respect, various criteria have been investigated for creating maps consisting of patterns, which facilitate the correlation procedure. Once the maps are created, the correlation between both configurations (initial and moved) is carried out using traditional methods developed for field measurements. Measurement validation was conducted using experiments in 2D and 3D with good results for rigid displacements in 2D, 3D and 2D rotations.

Surface roughness and bacterial adhesion on root dentin treated with diode laser and conventional desensitizing agents.

PubMed

Cury, Maiza S; Silva, Camilla B; Nogueira, Ruchele D; Campos, Michelle G D; Palma-Dibb, Regina G; Geraldo-Martins, Vinicius R

2018-02-01

The treatments for dentin hypersensitivity (DH) may change the surface roughness of the root dentin, which can lead to biofilm accumulation, increasing the risk of root caries. The aim was to compare the surface roughness of root dentin after different treatments of DH and the biofilm formation on those surfaces. After initial surface roughness (Sa) assessment, 50 bovine root fragments received the following treatments (n = 10): G 1-no treatment; G2-5% sodium fluoride varnish; G3-professional application of a desensitizing dentifrice; G4-toothbrushing with a desensitizing dentifrice; and G5-diode laser application (908 nm; 1.5 W, 20 s). The Sa was reevaluated after treatments. Afterward, all samples were incubated in a suspension of Streptococcus mutans at 37 °C for 24 h. The colony-forming units (CFU) were counted using a stereoscope, and the results were expressed in CFU/mL. The one-way ANOVA and the Tukey's tests compared the roughness data and the results obtained on the bacterial adhesion test (α = 5%). G2 (2.3 ± 1.67%) showed similar Sa variation than G1 (0.25 ± 0.41%) and G5 (5.69 ± 0.99%), but different from group G3 (9.05 ± 2.39%). Group 4 showed the highest Sa variation (30.02 ± 3.83%; p < 0.05). Bacterial adhesion was higher in G4 (2208 ± 211.9), suggesting that bacterial growth is greater on rougher surfaces. The diode laser and the conventional treatments for DH may change the surface roughness of the root dentin, but only brushing with desensitizing dentifrice induced a higher bacteria accumulation on root dentin surface.

Can high resolution 3D topographic surveys provide reliable grain size estimates in gravel bed rivers?

NASA Astrophysics Data System (ADS)

Pearson, E.; Smith, M. W.; Klaar, M. J.; Brown, L. E.

2017-09-01

High resolution topographic surveys such as those provided by Structure-from-Motion (SfM) contain a wealth of information that is not always exploited in the generation of Digital Elevation Models (DEMs). In particular, several authors have related sub-metre scale topographic variability (or 'surface roughness') to sediment grain size by deriving empirical relationships between the two. In fluvial applications, such relationships permit rapid analysis of the spatial distribution of grain size over entire river reaches, providing improved data to drive three-dimensional hydraulic models, allowing rapid geomorphic monitoring of sub-reach river restoration projects, and enabling more robust characterisation of riverbed habitats. However, comparison of previously published roughness-grain-size relationships shows substantial variability between field sites. Using a combination of over 300 laboratory and field-based SfM surveys, we demonstrate the influence of inherent survey error, irregularity of natural gravels, particle shape, grain packing structure, sorting, and form roughness on roughness-grain-size relationships. Roughness analysis from SfM datasets can accurately predict the diameter of smooth hemispheres, though natural, irregular gravels result in a higher roughness value for a given diameter and different grain shapes yield different relationships. A suite of empirical relationships is presented as a decision tree which improves predictions of grain size. By accounting for differences in patch facies, large improvements in D50 prediction are possible. SfM is capable of providing accurate grain size estimates, although further refinement is needed for poorly sorted gravel patches, for which c-axis percentiles are better predicted than b-axis percentiles.

Quasi-2D Unsteady Flow Procedure for Real Fluids (PREPRINT)

DTIC Science & Technology

2006-05-17

water /steam/ oil piping networks, refinery systems, gas-turbine secondary flow -path and cooling networks...friction factor, f, which is a function of the local Reynolds number and the wall surface roughness . For the viscous flow examples presented below, the...3.5 4 4.5 Time ( s ) V el oc ity (m / s ) Line 2 Inlet 25% 50% 75% Exit Velocity Figure 4. Water transient viscous pipe flow using

In situ effect of a CPP-ACP chewing gum on enamel erosion associated or not with abrasion.

PubMed

de Oliveira, Andressa Feitosa Bezerra; de Oliveira Diniz, Luciana Vilar; Forte, Franklin Delano Soares; Sampaio, Fabio Correia; Ccahuana-Vásquez, Renzo Alberto; Tochukwu Amaechi, Bennett

2017-01-01

The purpose of this study is to analyze the in situ effect of a casein phosphopeptide-stabilized amorphous calcium phosphate (CPP-ACP) chewing gum on human enamel erosion lesion associated or not with abrasion. A three-way crossover study of 7 days was conducted involving 10 volunteers subjected to the same protocol: (G1) CPP-ACP sugar-free chewing gum, (G2) regular sugar-free chewing gum without CPP-ACP, and (G3) saliva-no chewing gum. An abrasion test was included in each phase. A 3D non-contact profilometry measurement of lesion depth and surface roughness was obtained of sound and eroded surfaces. A salivary calcium concentration was determined for all volunteers. ANOVA followed by Tukey's test were used with a p < 0.05. The enamel depth and the enamel surface roughness of the CPP-ACP gum group were significantly lower than the others (ANOVA, p < 0.05). No significant differences were observed between the treatments when associated with abrasion (p > 0.05). A positive and significant correlation was seen between the lesion depth and enamel surface roughness for GI (r = 0.87, p = 0.00) and GIII (r = 0.79, p = 0.00) groups. The estimated total calcium presented in the saliva after the chewed CPP-ACP gum showed no statistical significance between the mean absorbance values at the different time collections (p > 0.05). It is demonstrated that the incorporation of the CPP-ACP into a sugar-free gum significantly increased the remineralization/protection of eroded enamel surface. The CPP-ACP added to gum may be a suitable alternative vehicle, to deliver calcium ions to saliva and therefore protecting enamel.

Formation of thin film like assembly of exfoliated C3N4 nanoflakes by solvent non-evaporative method using centrifuge

NASA Astrophysics Data System (ADS)

Tejasvi, Ravi; Basu, Suddhasatwa

2017-12-01

A simple method for depositing a thin film of nanomaterial on a substrate using centrifugation technique has been developed, whereby solvent evaporation is prevented and solvent reuse is possible. The centrifuge technique of deposition yields uniform, smooth thin film irrespective of substrate surface texture. The deposited TiO2/eC3N4 film studied, through field emission scanning electron microscope, atomic force microscope, and optical surface profilometer, shows variation in surface roughness on the basis of centrifugation speeds. Initially film coverage improves and surface roughness decreases with the increase in rpm of the centrifuge and the surface roughness slightly increases with further increase in rpm. The photoelectrochemical studies of TiO2/eC3N4 films suggest that the centrifuge technique forms better heterojunctions compared to that by spin coating technique leading to enhanced photoelectrochemical water splitting.

Perception-based 3D tactile rendering from a single image for human skin examinations by dynamic touch.

PubMed

Kim, K; Lee, S

2015-05-01

Diagnosis of skin conditions is dependent on the assessment of skin surface properties that are represented by more tactile properties such as stiffness, roughness, and friction than visual information. Due to this reason, adding tactile feedback to existing vision based diagnosis systems can help dermatologists diagnose skin diseases or disorders more accurately. The goal of our research was therefore to develop a tactile rendering system for skin examinations by dynamic touch. Our development consists of two stages: converting a single image to a 3D haptic surface and rendering the generated haptic surface in real-time. Converting to 3D surfaces from 2D single images was implemented with concerning human perception data collected by a psychophysical experiment that measured human visual and haptic sensibility to 3D skin surface changes. For the second stage, we utilized real skin biomechanical properties found by prior studies. Our tactile rendering system is a standalone system that can be used with any single cameras and haptic feedback devices. We evaluated the performance of our system by conducting an identification experiment with three different skin images with five subjects. The participants had to identify one of the three skin surfaces by using a haptic device (Falcon) only. No visual cue was provided for the experiment. The results indicate that our system provides sufficient performance to render discernable tactile rendering with different skin surfaces. Our system uses only a single skin image and automatically generates a 3D haptic surface based on human haptic perception. Realistic skin interactions can be provided in real-time for the purpose of skin diagnosis, simulations, or training. Our system can also be used for other applications like virtual reality and cosmetic applications. © 2014 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

Scale growth of structures in the turbulent boundary layer with a rod-roughened wall

NASA Astrophysics Data System (ADS)

Lee, Jin; Kim, Jung Hoon; Lee, Jae Hwa

2016-01-01

Direct numerical simulation of a turbulent boundary layer over a rod-roughened wall is performed with a long streamwise domain to examine the streamwise-scale growth mechanism of streamwise velocity fluctuating structures in the presence of two-dimensional (2-D) surface roughness. An instantaneous analysis shows that there is a slightly larger population of long structures with a small helix angle (spanwise inclinations relative to streamwise) and a large spanwise width over the rough-wall compared to that over a smooth-wall. Further inspection of time-evolving instantaneous fields clearly exhibits that adjacent long structures combine to form a longer structure through a spanwise merging process over the rough-wall; moreover, spanwise merging for streamwise scale growth is expected to occur frequently over the rough-wall due to the large spanwise scales generated by the 2-D roughness. Finally, we examine the influence of a large width and a small helix angle of the structures over the rough-wall with regard to spatial two-point correlation. The results show that these factors can increase the streamwise coherence of the structures in a statistical sense.

3D Powder Printed Bioglass and β-Tricalcium Phosphate Bone Scaffolds.

PubMed

Seidenstuecker, Michael; Kerr, Laura; Bernstein, Anke; Mayr, Hermann O; Suedkamp, Norbert P; Gadow, Rainer; Krieg, Peter; Hernandez Latorre, Sergio; Thomann, Ralf; Syrowatka, Frank; Esslinger, Steffen

2017-12-22

The use of both bioglass (BG) and β tricalcium phosphate (β-TCP) for bone replacement applications has been studied extensively due to the materials' high biocompatibility and ability to resorb when implanted in the body. 3D printing has been explored as a fast and versatile technique for the fabrication of porous bone scaffolds. This project investigates the effects of using different combinations of a composite BG and β-TCP powder for 3D printing of porous bone scaffolds. Porous 3D powder printed bone scaffolds of BG, β-TCP, 50/50 BG/β-TCP and 70/30 BG/β-TCP compositions were subject to a variety of characterization and biocompatibility tests. The porosity characteristics, surface roughness, mechanical strength, viability for cell proliferation, material cytotoxicity and in vitro bioactivity were assessed. The results show that the scaffolds can support osteoblast-like MG-63 cells growth both on the surface of and within the scaffold material and do not show alarming cytotoxicity; the porosity and surface characteristics of the scaffolds are appropriate. Of the two tested composite materials, the 70/30 BG/β-TCP scaffold proved to be superior in terms of biocompatibility and mechanical strength. The mechanical strength of the scaffolds makes them unsuitable for load bearing applications. However, they can be useful for other applications such as bone fillers.

Using Unmanned Aerial Vehicle (UAV) for spatio-temporal monitoring of soil erosion and roughness in Chania, Crete, Greece

NASA Astrophysics Data System (ADS)

Alexakis, Dimitrios; Seiradakis, Kostas; Tsanis, Ioannis

2016-04-01

This article presents a remote sensing approach for spatio-temporal monitoring of both soil erosion and roughness using an Unmanned Aerial Vehicle (UAV). Soil erosion by water is commonly known as one of the main reasons for land degradation. Gully erosion causes considerable soil loss and soil degradation. Furthermore, quantification of soil roughness (irregularities of the soil surface due to soil texture) is important and affects surface storage and infiltration. Soil roughness is one of the most susceptible to variation in time and space characteristics and depends on different parameters such as cultivation practices and soil aggregation. A UAV equipped with a digital camera was employed to monitor soil in terms of erosion and roughness in two different study areas in Chania, Crete, Greece. The UAV followed predicted flight paths computed by the relevant flight planning software. The photogrammetric image processing enabled the development of sophisticated Digital Terrain Models (DTMs) and ortho-image mosaics with very high resolution on a sub-decimeter level. The DTMs were developed using photogrammetric processing of more than 500 images acquired with the UAV from different heights above the ground level. As the geomorphic formations can be observed from above using UAVs, shadowing effects do not generally occur and the generated point clouds have very homogeneous and high point densities. The DTMs generated from UAV were compared in terms of vertical absolute accuracies with a Global Navigation Satellite System (GNSS) survey. The developed data products were used for quantifying gully erosion and soil roughness in 3D as well as for the analysis of the surrounding areas. The significant elevation changes from multi-temporal UAV elevation data were used for estimating diachronically soil loss and sediment delivery without installing sediment traps. Concerning roughness, statistical indicators of surface elevation point measurements were estimated and various parameters such as standard deviation of DTM, deviation of residual and standard deviation of prominence were calculated directly from the extracted DTM. Sophisticated statistical filters and elevation indices were developed to quantify both soil erosion and roughness. The applied methodology for monitoring both soil erosion and roughness provides an optimum way of reducing the existing gap between field scale and satellite scale. Keywords : UAV, soil, erosion, roughness, DTM

Surface roughness of composite resins subjected to hydrochloric acid.

PubMed

Roque, Ana Carolina Cabral; Bohner, Lauren Oliveira Lima; de Godoi, Ana Paula Terossi; Colucci, Vivian; Corona, Silmara Aparecida Milori; Catirse, Alma Blásida Concepción Elizaur Benitez

2015-01-01

The purpose of this study was to determine the influence of hydrochloric acid on surface roughness of composite resins subjected to brushing. Sixty samples measuring 2 mm thick x 6 mm diameter were prepared and used as experimental units. The study presented a 3x2 factorial design, in which the factors were composite resin (n=20), at 3 levels: microhybrid composite (Z100), nanofilled composite (FiltekTM Supreme), nanohybrid composite (Ice), and acid challenge (n=10) at 2 levels: absence and presence. Acid challenge was performed by immersion of specimens in hydrochloric acid (pH 1.2) for 1 min, 4 times per day for 7 days. The specimens not subjected to acid challenge were stored in 15 mL of artificial saliva at 37 oC. Afterwards, all specimens were submitted to abrasive challenge by a brushing cycle performed with a 200 g weight at a speed of 356 rpm, totaling 17.8 cycles. Surface roughness measurements (Ra) were performed and analyzed by ANOVA and Tukey test (p≤0.05). Surface roughness values were higher in the presence (1.07±0.24) as compared with the absence of hydrochloric acid (0.72±0.04). Surface roughness values were higher for microhybrid (1.01±0.27) compared with nanofilled (0.68 ±0.09) and nanohybrid (0.48±0.15) composites when the specimens were not subjects to acid challenge. In the presence of hydrochloric acid, microhybrid (1.26±0.28) and nanofilled (1.18±0,30) composites presents higher surface roughness values compared with nanohybrid (0.77±0.15). The hydrochloric acid affected the surface roughness of composite resin subjected to brushing.

Novel MRF fluid for ultra-low roughness optical surfaces

NASA Astrophysics Data System (ADS)

Dumas, Paul; McFee, Charles

2014-08-01

Over the past few years there have been an increasing number of applications calling for ultra-low roughness (ULR) surfaces. A critical demand has been driven by EUV optics, EUV photomasks, X-Ray, and high energy laser applications. Achieving ULR results on complex shapes like aspheres and X-Ray mirrors is extremely challenging with conventional polishing techniques. To achieve both tight figure and roughness specifications, substrates typically undergo iterative global and local polishing processes. Typically the local polishing process corrects the figure or flatness but cannot achieve the required surface roughness, whereas the global polishing process produces the required roughness but degrades the figure. Magnetorheological Finishing (MRF) is a local polishing technique based on a magnetically-sensitive fluid that removes material through a shearing mechanism with minimal normal load, thus removing sub-surface damage. The lowest surface roughness produced by current MRF is close to 3 Å RMS. A new ULR MR fluid uses a nano-based cerium as the abrasive in a proprietary aqueous solution, the combination of which reliably produces under 1.5Å RMS roughness on Fused Silica as measured by atomic force microscopy. In addition to the highly convergent figure correction achieved with MRF, we show results of our novel MR fluid achieving <1.5Å RMS roughness on fused silica and other materials.

Real-time spectro-ellipsometric approach to distinguish between two-dimensional Ge layer growth and Ge dot formation on SiO2 substrates

NASA Astrophysics Data System (ADS)

Akazawa, Housei

2018-04-01

Morphological evolution of Ge layers on SiO2 substrates grown by photo-excited chemical vapor deposition from GeH4 was monitored in real time by recording (Ψ, Δ) angles of spectroscopic ellipsometry and ex-situ analyzed by atomic force microscopy (AFM). Distinct Ψ-Δ trajectory shapes were demonstrated to discriminate the two-dimensional (2D) and three-dimensional (3D) growth modes. While the trajectory of 2D growth is characterized by a one-turn spiral, that of 3D growth consisted of three sections corresponding to initial wetting of the SiO2 surface, creation of nucleation centers, and dot growth. The critical point where the system turns into 2D or 3D growth can be in situ identified in terms of the directions of the Ψ-Δ trajectories. AFM images revealed characteristic changes in the microstructure, including self-assembling dots and dots merging with one another. While the root-mean-square surface roughness increased linearly against film thickness, the maximum peak-to-valley height deviated once from linear dependence and later returned back to it, which reflected coarsening of dots and embedding of valleys between dots.

Real-time and post-plasma studies of influence of low levels of tungsten on carbon erosion and surface evolution behaviour in D2 plasma

NASA Astrophysics Data System (ADS)

Weilnboeck, F.; Fox-Lyon, N.; Oehrlein, G. S.; Doerner, R. P.

2010-02-01

A profound influence of monolayer tungsten coverage of hard carbon films on the evolution of carbon surface erosion behaviour, surface chemistry and morphology in D2 plasma has been established by real-time ellipsometry, x-ray photoelectron spectroscopy and atomic force microscopy measurements. The erosion of tungsten-covered carbon showed two distinct stages of plasma material interactions: rapid tungsten removal during the initial erosion period and steady-state amorphous carbon removal accompanied by large-scale surface roughness development. The initial removal of tungsten takes place at a rate that significantly exceeds typical sputter yields at the ion energies used here and is attributed to elimination of weakly bonded tungsten from the surface. The tungsten remaining on the a-C : H film surface causes surface roughness development of the eroding carbon surface by a masking effect, and simultaneously leads to a seven fold reduction of the steady-state carbon erosion rate for long plasma surface interaction times (~100 s). Results presented are of direct relevance for material transport and re-deposition, and the interaction of those films with plasma in the divertor region and on mirror surfaces of fusion devices.

Surface roughness control by extreme ultraviolet (EUV) radiation

NASA Astrophysics Data System (ADS)

Ahad, Inam Ul; Obeidi, Muhannad Ahmed; Budner, Bogusław; Bartnik, Andrzej; Fiedorowicz, Henryk; Brabazon, Dermot

2017-10-01

Surface roughness control of polymeric materials is often desirable in various biomedical engineering applications related to biocompatibility control, separation science and surface wettability control. In this study, Polyethylene terephthalate (PET) polymer films were irradiated with Extreme ultraviolet (EUV) photons in nitrogen environment and investigations were performed on surface roughness modification via EUV exposure. The samples were irradiated at 3 mm and 4 mm distance from the focal spot to investigate the effect of EUV fluence on topography. The topography of the EUV treated PET samples were studied by AFM. The detailed scanning was also performed on the sample irradiated at 3 mm. It was observed that the average surface roughness of PET samples was increased from 9 nm (pristine sample) to 280 nm and 253 nm for EUV irradiated samples. Detailed AFM studies confirmed the presence of 1.8 mm wide period U-shaped channels in EUV exposed PET samples. The walls of the channels were having FWHM of about 0.4 mm. The channels were created due to translatory movements of the sample in horizontal and transverse directions during the EUV exposure. The increased surface roughness is useful for many applications. The nanoscale channels fabricated by EUV exposure could be interesting for microfluidic applications based on lab-on-a-chip (LOC) devices.

A fast and flexible method for manufacturing 3D molded interconnect devices by the use of a rapid prototyping technology

NASA Astrophysics Data System (ADS)

Amend, P.; Pscherer, C.; Rechtenwald, T.; Frick, T.; Schmidt, M.

This paper presents experimental results of manufacturing MID-prototypes by means of SLS, laser structuring and metallization. Therefore common SLS powder (PA12) doped with laser structuring additives is used. First of all the influence of the additives on the characteristic temperatures of melting and crystallization is analyzed by means of DSC. Afterwards the sintering process is carried out and optimized by experiments. Finally the generated components are qualified regarding their density, mechanical properties and surface roughness. Especially the surface quality is important for the metallization process. Therefore surface finishing techniques are investigated.

The Effect of Surface Irregularities on Wing Drag. 3; Roughness

NASA Technical Reports Server (NTRS)

Hood, Manley J.

1938-01-01

Tests have been made in the N.A.C.A. 8-foot high-speed wind tunnel of the drag caused by roughness on the surface of an airfoil of N.A.C.A. 23012 section and 5-foot chord. The tests were made at speeds from 80 t o 500 miles per hour at lift coefficients from 0 to 0.30. For conditions corresponding to high-speed flight, the increase in the drag was 30 percent of the profile drag of the smooth airfoil for the roughness produced by spray painting and 63 percent for the roughness produced. by 0.0037-inch carborundum grains. About one-half the drag increase was caused by the roughness on the forward one-fourth of the airfoil. Sandpapering the painted surface with No. 400 sandpaper made it sufficiently smooth that the drag was no greater than when the surface was polished. In the lower part of the range investigated the drag due to roughness increased rapidly with Reynolds Number.

Effect of whitening dentifrices on the surface roughness of a nanohybrid composite resin

PubMed Central

da Rosa, Gabriela Migliorin; da Silva, Luciana Mendonça; de Menezes, Márcio; do Vale, Hugo Felipe; Regalado, Diego Ferreira; Pontes, Danielson Guedes

2016-01-01

Objectives: The present study verified the influence of whitening dentifrices on the surface roughness of a nanohybrid composite resin. Materials and Methods: Thirty-two specimens were prepared with Filtek™ Z350 XT (3M/ESPE) and randomly divided into four groups (n = 08) that were subjected to brushing simulation equivalent to the period of 1 month. The groups assessed were a control group with distilled water (G1), Colgate Total 12 Professional Clean (G2), Sensodyne Extra Whitener Extra Fresh (G3), and Colgate Luminous White (G4). A sequence of 90 cycles was performed for all the samples. The initial roughness of each group was analyzed by the Surface Roughness Tester (TR 200-TIME Group Inc., CA, USA). After the brushing period, the final roughness was measured, and the results were statistically analyzed using nonparametric Kruskal–Wallis and Dunn tests for intergroup roughness comparison in the time factor. For intragroup and “Δ Final − Initial” comparisons, the Wilcoxon test and (one-way) ANOVA were, respectively, performed (α = 0.05). Results: The roughness mean values before and after brushing showed no statistically significant difference when the different dentifrices were used. None of the dentifrices analyzed increased significantly the nanohybrid composite resin surface roughness in a 1 month of tooth brushing simulation. Conclusions: These results suggest that no hazardous effect on the roughness of nanohybrid composite resin can be expected when whitening dentifrices are used for a short period. Similar studies should be conducted to analyze other esthetic composite materials. PMID:27095891

Surface energy changes produced by ultraviolet-ozone irradiation of poly(methylmethacrylate), polycarbone and polytetrafluoroethylene

NASA Technical Reports Server (NTRS)

Ponter, A. B.; Jones, W. R., Jr.; Jansen, R. H.

1994-01-01

Contact angles of water and methylene iodide were measured as a function of UV/O3 treatment time for three polymers: poly(methylmethacrylate) (PMMA), polycarbonate, and polytetrafluoroethylene (PTFE). Surface roughnesses were also measured. Surface free energies were then calculated using relationships developed by Kaelble and Neumann. The surface energy of polycarbonate was found to increase (60 percent) during UV/O3 treatment. However, calculations on PMMA were hampered by the formation of a water soluble surface product. On PTFE surfaces, the UV/O3 treatment etched the surface causing large increases in surface roughness, rendering contact angle measurements impossible. It is concluded that care must be taken in interpreting contact angle measurements and surface energy calculations on UV/O3 treated polymer surfaces.

Comparison of aerodynamically and model-derived roughness lengths (zo) over diverse surfaces, central Mojave Desert, California, USA

USGS Publications Warehouse

MacKinnon, D.J.; Clow, G.D.; Tigges, R.K.; Reynolds, R.L.; Chavez, P.S.

2004-01-01

The vulnerability of dryland surfaces to wind erosion depends importantly on the absence or the presence and character of surface roughness elements, such as plants, clasts, and topographic irregularities that diminish wind speed near the surface. A model for the friction velocity ratio has been developed to account for wind sheltering by many different types of co-existing roughness elements. Such conditions typify a monitored area in the central Mojave Desert, California, that experiences frequent sand movement and dust emission. Two additional models are used to convert the friction velocity ratio to the surface roughness length (zo) for momentum. To calculate roughness lengths from these models, measurements were made at 11 sites within the monitored area to characterize the surface roughness element. Measurements included (1) the number of roughness species (e.g., plants, small-scale topography, clasts), and their associated heights and widths, (2) spacing among species, and (3) vegetation porosity (a measurement of the spatial distribution of woody elements of a plant). Documented or estimated values of drag coefficients for different species were included in the modeling. At these sites, wind-speed profiles were measured during periods of neutral atmospheric stability using three 9-m towers with three or four calibrated anemometers on each. Modeled roughness lengths show a close correspondence (correlation coefficient, 0.84-0.86) to the aerodynamically determined values at the field sites. The geometric properties of the roughness elements in the model are amenable to measurement at much higher temporal and spatial resolutions using remote-sensing techniques than can be accomplished through laborious ground-based methods. A remote-sensing approach to acquire values of the modeled roughness length is particularly important for the development of linked surface/atmosphere wind-erosion models sensitive to climate variability and land-use changes in areas such as the southwestern United States, where surface roughness has large spatial and temporal variations. ?? 2004 Elsevier B.V. All rights reserved.

Fabrication of 3D polypyrrole microstructures and their utilization as electrodes in supercapacitors

NASA Astrophysics Data System (ADS)

Ho, Vinh; Zhou, Cheng; Kulinsky, Lawrence; Madou, Marc

2013-12-01

We present a novel fabrication method for constructing three-dimensional (3D) conducting microstructures based on the controlled-growth of electrodeposited polypyrrole (PPy) within a lithographically patterned photoresist layer. PPy thin films, post arrays, suspended planes supported by post arrays and multi-layered PPy structures were fabricated. The performance of supercapacitors based on 3D PPy electrodes doped with dodecylbenzene sulfonate (DBS-) and perchlorate (ClO4-) anions was studied using cyclic voltammetry and galvanostatic charge/discharge tests. The highest specific capacitance obtained from the multi-layered PPy(ClO4) electrodes was 401 ± 18 mF cm-2, which is roughly twice as high as the highest specific capacitance of PPy-based supercapacitor reported thus far. The increase in capacitance is the result of higher surface area per unit footprint achieved through the fabrication of multi-layered 3D electrodes.

Toward fully three-dimensional-printed miniaturized confocal imager

NASA Astrophysics Data System (ADS)

Savaş, Janset; Khayatzadeh, Ramin; Çivitçi, Fehmi; Gökdel, Yiğit Dağhan; Ferhanoğlu, Onur

2018-04-01

We present a disposable miniaturized confocal imager, consisting mostly of three-dimensional (3-D)-printed components. A 3-D printed laser scanner with 10×10 mm2 frame size is employed for Lissajous scan, with 180 and 315 Hz frequencies in orthogonal directions corresponding to ±8 deg and ±4 deg optical scan angles, respectively. The actuation is done electromagnetically via a magnet attached to the scanner and an external coil. A miniaturized lens with 6-mm clear aperture and 10-mm focal length is 3-D printed and postprocessed to obtain desired (≤λ/5 surface roughness) performance. All components are press-fitted into a 3-D-printed housing having 17 mm width, which is comparable to many of the MEMS-based scanning imagers. Finally, line-scan from a resolution target and two-dimensional scanning in the sample location were demonstrated with the integrated device.

Effects of Nanowire Length and Surface Roughness on the Electrochemical Sensor Properties of Nafion-Free, Vertically Aligned Pt Nanowire Array Electrodes

PubMed Central

Li, Zhiyang; Leung, Calvin; Gao, Fan; Gu, Zhiyong

2015-01-01

In this paper, vertically aligned Pt nanowire arrays (PtNWA) with different lengths and surface roughnesses were fabricated and their electrochemical performance toward hydrogen peroxide (H2O2) detection was studied. The nanowire arrays were synthesized by electroplating Pt in nanopores of anodic aluminum oxide (AAO) template. Different parameters, such as current density and deposition time, were precisely controlled to synthesize nanowires with different surface roughnesses and various lengths from 3 μm to 12 μm. The PtNWA electrodes showed better performance than the conventional electrodes modified by Pt nanowires randomly dispersed on the electrode surface. The results indicate that both the length and surface roughness can affect the sensing performance of vertically aligned Pt nanowire array electrodes. Generally, longer nanowires with rougher surfaces showed better electrochemical sensing performance. The 12 μm rough surface PtNWA presented the largest sensitivity (654 μA·mM−1·cm−2) among all the nanowires studied, and showed a limit of detection of 2.4 μM. The 12 μm rough surface PtNWA electrode also showed good anti-interference property from chemicals that are typically present in the biological samples such as ascorbic, uric acid, citric acid, and glucose. The sensing performance in real samples (river water) was tested and good recovery was observed. These Nafion-free, vertically aligned Pt nanowires with surface roughness control show great promise as versatile electrochemical sensors and biosensors. PMID:26404303

Automatic generation of endocardial surface meshes with 1-to-1 correspondence from cine-MR images

NASA Astrophysics Data System (ADS)

Su, Yi; Teo, S.-K.; Lim, C. W.; Zhong, L.; Tan, R. S.

2015-03-01

In this work, we develop an automatic method to generate a set of 4D 1-to-1 corresponding surface meshes of the left ventricle (LV) endocardial surface which are motion registered over the whole cardiac cycle. These 4D meshes have 1- to-1 point correspondence over the entire set, and is suitable for advanced computational processing, such as shape analysis, motion analysis and finite element modelling. The inputs to the method are the set of 3D LV endocardial surface meshes of the different frames/phases of the cardiac cycle. Each of these meshes is reconstructed independently from border-delineated MR images and they have no correspondence in terms of number of vertices/points and mesh connectivity. To generate point correspondence, the first frame of the LV mesh model is used as a template to be matched to the shape of the meshes in the subsequent phases. There are two stages in the mesh correspondence process: (1) a coarse matching phase, and (2) a fine matching phase. In the coarse matching phase, an initial rough matching between the template and the target is achieved using a radial basis function (RBF) morphing process. The feature points on the template and target meshes are automatically identified using a 16-segment nomenclature of the LV. In the fine matching phase, a progressive mesh projection process is used to conform the rough estimate to fit the exact shape of the target. In addition, an optimization-based smoothing process is used to achieve superior mesh quality and continuous point motion.

Determination and interpretation of the optical constants for solar cell materials

NASA Astrophysics Data System (ADS)

Fujiwara, Hiroyuki; Fujimoto, Shohei; Tamakoshi, Masato; Kato, Masato; Kadowaki, Hideyuki; Miyadera, Tetsuhiko; Tampo, Hitoshi; Chikamatsu, Masayuki; Shibata, Hajime

2017-11-01

Solar cell materials in thin film form often exhibit quite rough surface, which makes the accurate determination of the optical constants using spectroscopic ellipsometry (SE) quite difficult. In this study, we investigate the effect of the rough surface on the SE analysis and establish an analysis procedure, which is quite helpful for the correction of the underestimated roughness contribution. As examples, the roughness analyses for CuInSe2 and CH3NH3PbI3 hybrid-perovskite thin films are presented. Moreover, to interpret the dielectric functions of emerging solar cell materials, such as CH3NH3PbI3 and Cu2ZnSnSe4, the optical transition analyses are performed based on density functional theory (DFT). The excellent agreement observed between the experimental and DFT results allows the detailed assignment of the transition peaks, confirming the importance of DFT for revealing fundamental optical characteristics.

Superficial roughness on composite surface, composite-enamel and composite-dentin junctions after different finishing and polishing procedures. Part II: roughness with diamond finishing and differences between enamel composite vs body composite.

PubMed

Ferraris, Federico; Conti, Alessandro

2014-01-01

The following study asks three principle questions relative to composite finishing and composite polishing: 1) Will the superficial roughness of different restoration surfaces have different values, utilizing the same polishing system (multistep), after finishing with the tungsten carbide or diamond bur? 2) Under the same conditions of finishing and polishing sequences, will the composite surfaces (C), the composite-enamel (CE) and composite-dentin (CD) interfaces show different roughness values? 3) Will the surface roughness of composites of different translucency in the various phases of finishing and polishing, and on different interfaces, have different results? The null hypothesis is represented by the fact that there are no significant differences on roughness of composite restorations when polishing, after finishing with tungsten carbide or diamond burs. Furthermore, the null hypothesis is that there are no significant differences on roughness between polishing on composite surface, composite-enamel and composite-dentin interfaces, and finally there are no differences on roughness after finishing and polishing of two composite with different translucency. For the study, 56 class V cavities were prepared on extracted teeth. Restorations were done in nanofilled composite Filtek XTE (3M Espe) in a standard fashion, and then finished and polished. The 28 buccal cavities were restored on the surface with composite enamel and the 28 palatals with composite body. Finishing was done with fine toothing burs in tungsten carbide (16 blades) or fine grit diamond burs (46 μm), and made by the same manufacturer (Komet). The second phase of finishing was done with burs (with the same form as already mentioned) ultrafine toothing tungsten carbide (30 blades) or with extra and ultrafine grit diamond (25 and 8 μm). The polishing phase for both of the earlier sequences was done with the application of three rubber tips with decreasing abrasiveness and an application with a self-polishing brush. All measurements were taken from surfaces C, and interfaces CE and CD. Statistical analyses were carried out with c2 test (a = 0.05). 1) There were no relevant differences of surface roughness on the different surfaces if the polishing was done after finishing with tungsten carbide or diamond burs. 2) Keeping the same sequence of finishing and polishing, a difference was noticed between C, CE and CD, where the latter showed greater roughness. 3) Analyzing the data in all the phases of finishing and polishing on every interface, it can be concluded that the composite enamel and the composite body did not show different levels of superficial roughness. The clinical relevance could be resumed as follows: no difference after polishing, which is preceded by tungsten carbide or diamond finishing burs. The less favorable interface to be polished is CD, compared to CE and C. Considering two composites with different translucency, no difference on roughness after finishing and polishing were detected.

Surface roughness estimation of MBE grown CdTe/GaAs(211)B by ex-situ spectroscopic ellipsometry

DOE Office of Scientific and Technical Information (OSTI.GOV)

Karakaya, Merve, E-mail: mervegunnar@iyte.edu.tr; Bilgilisoy, Elif; Arı, Ozan

Spectroscopic ellipsometry (SE) ranging from 1.24 eV to 5.05 eV is used to obtain the film thickness and optical properties of high index (211) CdTe films. A three-layer optical model (oxide/CdTe/GaAs) was chosen for the ex-situ ellipsometric data analysis. Surface roughness cannot be determined by the optical model if oxide is included. We show that roughness can be accurately estimated, without any optical model, by utilizing the correlation between SE data (namely the imaginary part of the dielectric function, or phase angle, ψ) and atomic force microscopy (AFM) roughness. and ψ values at 3.31 eV, which corresponds to E{sub 1}more » critical transition energy of CdTe band structure, are chosen for the correlation since E{sub 1} gives higher resolution than the other critical transition energies. On the other hand, due to the anisotropic characteristic of (211) oriented CdTe surfaces, SE data ( and ψ) shows varieties for different azimuthal angle measurements. For this reason, in order to estimate the surface roughness by considering these correlations, it is shown that SE measurements need to be taken at the same surface azimuthal angle. Estimating surface roughness in this manner is an accurate way to eliminate cumbersome surface roughness measurement by AFM.« less

Effect of sodium hypochlorite and peracetic acid on the surface roughness of acrylic resin polymerized by heated water for short and long cycles.

PubMed

Sczepanski, Felipe; Sczepanski, Claudia Roberta Brunnquell; Berger, Sandrine Bittencourt; Consani, Rafael Leonardo Xediek; Gonini-Júnior, Alcides; Guiraldo, Ricardo Danil

2014-10-01

To evaluate the surface roughness of acrylic resin submitted to chemical disinfection via 1% sodium hypochlorite (NaClO) or 1% peracetic acid (C2H4O3). The disc-shaped resin specimens (30 mm diameter ×4 mm height) were polymerized by heated water using two cycles (short cycle: 1 h at 74°C and 30 min at 100°C; conventional long cycle: 9 h at 74°C). The release of substances by these specimens in water solution was also quantified. Specimens were fabricated, divided into four groups (n = 10) depending on the polymerization time and disinfectant. After polishing, the specimens were stored in distilled deionized water. Specimens were immersed in 1% NaClO or 1% C2H4O3 for 30 min, and then were immersed in distilled deionized water for 20 min. The release of C2H4O3 and NaClO was measured via visual colorimetric analysis. Roughness was measured before and after disinfection. Roughness data were subjected to two-way ANOVA and Tukey's test. There was no interaction between polymerization time and disinfectant in influencing the average surface roughness (Ra, P = 0.957). Considering these factors independently, there were significant differences between short and conventional long cycles (P = 0.012), but no significant difference between the disinfectants hypochlorite and C2H4O3 (P = 0.366). Visual colorimetric analysis did not detect release of substances. It was concluded that there was the difference in surface roughness between short and conventional long cycles, and disinfection at acrylic resins polymerized by heated water using a short cycle modified the properties of roughness.

Effect of sodium hypochlorite and peracetic acid on the surface roughness of acrylic resin polymerized by heated water for short and long cycles

PubMed Central

Sczepanski, Felipe; Sczepanski, Claudia Roberta Brunnquell; Berger, Sandrine Bittencourt; Consani, Rafael Leonardo Xediek; Gonini-Júnior, Alcides; Guiraldo, Ricardo Danil

2014-01-01

Objective: To evaluate the surface roughness of acrylic resin submitted to chemical disinfection via 1% sodium hypochlorite (NaClO) or 1% peracetic acid (C2H4O3). Materials and Methods: The disc-shaped resin specimens (30 mm diameter ×4 mm height) were polymerized by heated water using two cycles (short cycle: 1 h at 74°C and 30 min at 100°C; conventional long cycle: 9 h at 74°C). The release of substances by these specimens in water solution was also quantified. Specimens were fabricated, divided into four groups (n = 10) depending on the polymerization time and disinfectant. After polishing, the specimens were stored in distilled deionized water. Specimens were immersed in 1% NaClO or 1% C2H4O3 for 30 min, and then were immersed in distilled deionized water for 20 min. The release of C2H4O3 and NaClO was measured via visual colorimetric analysis. Roughness was measured before and after disinfection. Roughness data were subjected to two-way ANOVA and Tukey's test. Results: There was no interaction between polymerization time and disinfectant in influencing the average surface roughness (Ra, P = 0.957). Considering these factors independently, there were significant differences between short and conventional long cycles (P = 0.012), but no significant difference between the disinfectants hypochlorite and C2H4O3 (P = 0.366). Visual colorimetric analysis did not detect release of substances. Conclusion: It was concluded that there was the difference in surface roughness between short and conventional long cycles, and disinfection at acrylic resins polymerized by heated water using a short cycle modified the properties of roughness. PMID:25512737

Impact of low-pressure glow-discharge-pulsed plasma polymerization on properties of polyaniline thin films

NASA Astrophysics Data System (ADS)

Jatratkar, Aviraj A.; Yadav, Jyotiprakash B.; Deshmukh, R. R.; Barshilia, Harish C.; Puri, Vijaya; Puri, R. K.

2016-12-01

This study reports on polyaniline thin films deposited on a glass substrate using a low-pressure glow-discharge-pulsed plasma polymerization method. The polyaniline thin film obtained by pulsed plasma polymerization has been successfully demonstrated as an optical waveguide with a transmission loss of 3.93 dB cm-1, and has the potential to be employed in integrated optics. An attempt has been made to investigate the effect of plasma OFF-time on the structural, optical as well as surface properties of polyaniline thin film. The plasma ON-time has been kept constant and the plasma OFF-time has been varied throughout the work. The plasma OFF-time strongly influenced the properties of the polyaniline thin film, and a nanostructured and compact surface was revealed in the morphological studies. The plasma OFF-time was found to enhance film thickness, roughness, refractive index and optical transmission loss, whereas it reduced the optical band gap of the polyaniline thin films. Retention in the aromatic structure was confirmed by FTIR results. Optical studies revealed a π-π* electronic transition at about 317 nm as well as the formation of a branched structure. As compared with continuous wave plasma, pulsed plasma polymerization shows better properties. Pulsed plasma polymerization reduced the roughness of the film from 1.2 nm to 0.42 nm and the optical transmission loss from 6.56 dB cm-1 to 3.39 dB cm-1.

Experimental and Numerical Investigation of Pressure Drop in Silicon Carbide Fuel Rod for Application in Pressurized Water Reactors

NASA Astrophysics Data System (ADS)

Abir, Ahmed Musafi

Spacer grids are used in Pressurized Water Reactors (PWRs) fuel assemblies which enhances heat transfer from fuel rods. However, there remain regions of low turbulence in between the spacer grids. To enhance turbulence in these regions surface roughness is applied on the fuel rod walls. Meyer [1] used empirical correlations to predict heat transfer and friction factor for artificially roughened fuel rod bundles at High Performance Light Water Reactors (LWRs). Their applicability was tested by Carrilho at University of South Carolina's (USC) Single Heated Element Loop Tester (SHELT). He attained a heat transfer and friction factor enhancement of 50% and 45% respectively, using Inconel nuclear fuel rods with square transverse ribbed surface. Following him Najeeb conducted a similar study due to three dimensional diamond shaped blocks in turbulent flow. He recorded a maximum heat transfer enhancement of 83%. At present, several types of materials are being used for fuel rod cladding including Zircaloy, Uranium oxide, etc. But researchers are actively searching for new material that can be a more practical alternative. Silicon Carbide (SiC) has been identified as a material of interest for application as fuel rod cladding [2]. The current study deals with the experimental investigation to find out the friction factor increase of a SiC fuel rod with 3D surface roughness. The SiC rod was tested at USC's SHELT loop. The experiment was conducted in turbulent flowing Deionized (DI) water at steady state conditions. Measurements of Flow rate and pressure drop were made. The experimental results were also validated by Computational Fluid Dynamics (CFD) analysis in ANSYS Fluent. To simplify the CFD analysis and to save computational resources the 3D roughness was approximated as a 2D one. The friction factor results of the CFD investigation was found to lie within +/-8% of the experimental results. A CFD model was also run with the energy equation turned on, and a heat generation of 8 kW applied to the rod. A maximum heat transfer enhancement of 18.4% was achieved at the highest flow rate investigated (i.e. Re=109204).

An In Vitro Evaluation of Alumina, Zirconia, and Lithium Disilicate Surface Roughness Caused by Two Scaling Instruments.

PubMed

Vigolo, Paolo; Buzzo, Ottavia; Buzzo, Maurizio; Mutinelli, Sabrina

2017-02-01

Plaque control is crucial for the prevention of inflammatory periodontal disease. Hand scaling instruments have been shown to be efficient for the removal of plaque; however, routine periodontal prophylactic procedures may modify the surface profile of restorative materials. The purpose of this study was to assess in vitro the changes in roughness of alumina, zirconia, and lithium disilicate surfaces treated by two hand scaling instruments. Forty-eight alumina specimens, 48 zirconia specimens, and 48 lithium disilicate specimens, were selected. All specimens were divided into three groups of 16 each; one group for each material was considered the control group and no scaling procedures were performed; the second group of each material was exposed to scaling with steel curettes simulating standard clinical conditions; the third group of each material was exposed to scaling with titanium curettes. After scaling, the surface roughness of the specimens was evaluated with a profilometer. First, a statistical test was carried out to evaluate the difference in surface roughness before the scaling procedure of the three materials was effected (Kruskal-Wallis test). Subsequently, the effect of curette material (steel and titanium) on roughness difference and roughness ratio was analyzed throughout the entire sample and within each material group, and a nonparametric test for dependent values was conducted (Wilcoxon signed-rank test). Finally, the roughness ratios of the three material groups were compared by means of a Kruskal-Wallis test and a Wilcoxon signed-rank test. Upon completion of profilometric evaluation, representative specimens from each group were prepared for SEM evaluation to evaluate the effects of the two scaling systems on the different surfaces qualitatively. After scaling procedure, the roughness profile value increased in all disks. Classifying the full sample according to curette used, the roughness of the disks treated with a steel curette reached a higher median value than that of the titanium group. Zirconia demonstrated the least significant increase in surface roughness. The result was 3.9 times of the initial value as compared to 4.3 times for alumina and 4.6 times for lithium disilicate. Comparison of profilometer readings before and after instrumentation, carried out with different hand scaling instruments, highlighted both a statistically and clinically relevant increase in material roughness. © 2015 by the American College of Prosthodontists.

Effect of professional dental prophylaxis on the surface gloss and roughness of CAD/CAM restorative materials.

PubMed

Sugiyama, Toshiko; Kameyama, Atsushi; Enokuchi, Tomoka; Haruyama, Akiko; Chiba, Aoi; Sugiyama, Setsuko; Hosaka, Makoto; Takahashi, Toshiyuki

2017-06-01

This study aimed to evaluate the effect of dental prophylaxis on the surface gloss and roughness of different indirect restorative materials for computer-aided design/computer-aided manufacturing (CAD/CAM): two types of CAD/CAM composite resin blocks (Shofu Block HC and Estelite Block) and two types of CAD/CAM ceramic blocks (IPS Empress CAD and Celtra DUO). After polishing the CAD/CAM blocks and applying prophylaxis pastes, professional dental prophylaxis was performed using four different experimental protocols (n = 5 each): mechanical cleaning with Merssage Regular for 10 s four times (Group 1); four cycles of mechanical cleaning with Merssage Regular for 10 s and Merssage Fine for 10 s (Group 2); four cycles of mechanical cleaning with Merssage Regular for 10 s and Merssage Fine for 30 s (Group 3); and mechanical cleaning with Merssage Fine for 10 s four times (Group 4). A glossmeter was used to measure surface gloss before and after mechanical cleaning, and a contact stylus profilometer was used to measure surface roughness (Ra). Polishing with prophylactic paste led to a significant reduction in surface gloss and increase in surface roughness among resin composite blocks, whereas the polishing-related change in surface gloss or roughness was smaller in Celtra DUO, a zirconia-reinforced lithium silicate block. Changes in surface gloss and roughness due to polishing with a prophylactic paste containing large particles were not improved by subsequent polishing with a prophylactic paste containing fine particles. Key words: CAD/CAM, professional dental prophylaxis, prophylactic paste, surface gloss, surface roughness.

Effect of professional dental prophylaxis on the surface gloss and roughness of CAD/CAM restorative materials

PubMed Central

Sugiyama, Toshiko; Enokuchi, Tomoka; Haruyama, Akiko; Chiba, Aoi; Sugiyama, Setsuko; Hosaka, Makoto; Takahashi, Toshiyuki

2017-01-01

Background This study aimed to evaluate the effect of dental prophylaxis on the surface gloss and roughness of different indirect restorative materials for computer-aided design/computer-aided manufacturing (CAD/CAM): two types of CAD/CAM composite resin blocks (Shofu Block HC and Estelite Block) and two types of CAD/CAM ceramic blocks (IPS Empress CAD and Celtra DUO). Material and Methods After polishing the CAD/CAM blocks and applying prophylaxis pastes, professional dental prophylaxis was performed using four different experimental protocols (n = 5 each): mechanical cleaning with Merssage Regular for 10 s four times (Group 1); four cycles of mechanical cleaning with Merssage Regular for 10 s and Merssage Fine for 10 s (Group 2); four cycles of mechanical cleaning with Merssage Regular for 10 s and Merssage Fine for 30 s (Group 3); and mechanical cleaning with Merssage Fine for 10 s four times (Group 4). A glossmeter was used to measure surface gloss before and after mechanical cleaning, and a contact stylus profilometer was used to measure surface roughness (Ra). Results Polishing with prophylactic paste led to a significant reduction in surface gloss and increase in surface roughness among resin composite blocks, whereas the polishing-related change in surface gloss or roughness was smaller in Celtra DUO, a zirconia-reinforced lithium silicate block. Conclusions Changes in surface gloss and roughness due to polishing with a prophylactic paste containing large particles were not improved by subsequent polishing with a prophylactic paste containing fine particles. Key words:CAD/CAM, professional dental prophylaxis, prophylactic paste, surface gloss, surface roughness. PMID:28638554

[Influence of surface roughness on degree of polarization of biotite plagioclase gneiss varying with viewing angle].

PubMed

Xiang, Yun; Yan, Lei; Zhao, Yun-sheng; Gou, Zhi-yang; Chen, Wei

2011-12-01

Polarized reflectance is influenced by such factors as its physical and chemical properties, the viewing geometry composed of light incident zenith, viewing zenith and viewing azimuth relative to light incidence, surface roughness and texture, surface density, detection wavelengths, polarization phase angle and so on. In the present paper, the influence of surface roughness on the degree of polarization (DOP) of biotite plagioclase gneiss varying with viewing angle was inquired and analyzed quantitatively. The polarized spectra were measured by ASD FS3 spectrometer on the goniometer located in Northeast Normal University. When the incident zenith angle was fixed at 50 degrees, it was showed that on the rock surfaces with different roughness, in the specular reflection direction, the DOP spectrum within 350-2500 nm increased to the highest value first, and then began to decline varying with viewing zenith angle from 0 degree to 80 degrees. The characterized band (520 +/- 10) nm was picked out for further analysis. The correlation analysis between the peak DOP value of zenith and surface roughness showed that they are in a power function relationship, with the regression equation: y = 0.604x(-0.297), R2 = 0.985 4. The correlation model of the angle where the peak is in and the surface roughness is y = 3.4194x + 51.584, y < 90 degrees , R2 = 0.8177. With the detecting azimuth farther away from 180 degrees azimuth where the maximum DOP exists, the DOP lowers gradually and tends to 0. In the detection azimuth 180 dgrees , the correlation analysis between the peak values of DOP on the (520 =/- 10) nm band for five rocks and their surface roughness indicates a power function, with the regression equation being y = 0.5822x(-0.333), R2 = 0.9843. F tests of the above regression models indicate that the peak value and its corresponding viewing angle correlate much with surface roughness. The study provides a theoretical base for polarization remote sensing, and impels the rock and city architecture discrimination and minerals mapping.

Measuring vibrational motion in the presence of speckle using off-axis holography.

PubMed

Redding, Brandon; Davis, Allen; Kirkendall, Clay; Dandridge, Anthony

2016-02-20

We present a holographic laser vibrometer designed to mitigate the effects of speckle noise when measuring the vibrational motion of a rough object. We show that multiplexing the interferometric measurement across 10⁵ pixels provides a 50 dB reduction in the incoherent noise. Using a high-speed camera, this enables a displacement sensitivity of 50  fm/√Hz with a bandwidth of 12.5 kHz when measuring rough objects, representing a 20 dB improvement compared with a commercially available single-detector-based laser vibrometer. Finally, we show that the holographic vibrometer system is capable of stand-off acoustic sensing by measuring the acoustic-induced vibrations of a piece of paper with sensitivity as low as 10 dB (re 20 μPa). The ability to sensitively and noninvasively measure the vibrations of arbitrary rough surfaces could enable new applications in laser vibrometry.

Gloss and surface roughness produced by polishing kits on resin composites.

PubMed

Sadidzadeh, Ramtin; Cakir, Deniz; Ramp, Lance C; Burgess, John O

2010-08-01

To compare in vitro the surface roughness (Ra) and gloss (G) produced by three conventional and one experimental polishing kits on four resin composites. 24 discs were prepared (d = 12 mm, t = 4 mm) for each resin composite: Filtek Supreme Plus Body/A2 (FSB), Yellow Translucent (FST), Heliomolar/A2 (HM), and EsthetX/A2 (EX) following the manufacturers' instructions. They were finished with 320 grit silicon carbide paper for 80 seconds each. Polishing systems: Sof-Lex, Enhance-Pogo, Astropol and Experimental Discs/EXL-695, were applied following manufacturers' instructions. Each specimen was ultrasonically cleaned with distilled water and dried. Gloss and Ra were measured with a small area glossmeter (Novo-curve) and non-contact profilometer (Proscan 2000) following ISO 4288, respectively. The results were evaluated by two-way ANOVA followed by separate one-way ANOVA and Tukey/Kramer test (P = 0.05). There was a significant interaction of surface roughness and gloss between the composites and polishing systems (P < 0.05). The lowest surface roughness was recorded for FST polished with the Experimental kit. The highest gloss was obtained for FSB composite polished with the Experimental kit. The experimental polishing system produced smoothest surfaces (P < 0.05). The Enhance-Pogo and the experimental polishing kit produced highest gloss (P < 0.05).

Study of 3-D Dynamic Roughness Effects on Flow Over a NACA 0012 Airfoil Using Large Eddy Simulations at Low Reynolds Numbers

NASA Astrophysics Data System (ADS)

Guda, Venkata Subba Sai Satish

There have been several advancements in the aerospace industry in areas of design such as aerodynamics, designs, controls and propulsion; all aimed at one common goal i.e. increasing efficiency --range and scope of operation with lesser fuel consumption. Several methods of flow control have been tried. Some were successful, some failed and many were termed as impractical. The low Reynolds number regime of 104 - 105 is a very interesting range. Flow physics in this range are quite different than those of higher Reynolds number range. Mid and high altitude UAV's, MAV's, sailplanes, jet engine fan blades, inboard helicopter rotor blades and wind turbine rotors are some of the aerodynamic applications that fall in this range. The current study deals with using dynamic roughness as a means of flow control over a NACA 0012 airfoil at low Reynolds numbers. Dynamic 3-D surface roughness elements on an airfoil placed near the leading edge aim at increasing the efficiency by suppressing the effects of leading edge separation like leading edge stall by delaying or totally eliminating flow separation. A numerical study of the above method has been carried out by means of a Large Eddy Simulation, a mathematical model for turbulence in Computational Fluid Dynamics, owing to the highly unsteady nature of the flow. A user defined function has been developed for the 3-D dynamic roughness element motion. Results from simulations have been compared to those from experimental PIV data. Large eddy simulations have relatively well captured the leading edge stall. For the clean cases, i.e. with the DR not actuated, the LES was able to reproduce experimental results in a reasonable fashion. However DR simulation results show that it fails to reattach the flow and suppress flow separation compared to experiments. Several novel techniques of grid design and hump creation are introduced through this study.

Effects of toothbrushing with fluoride abrasive and whitening dentifrices on both unbleached and bleached human enamel surface in terms of roughness and hardness: an in vitro study.

PubMed

Bolay, Sukran; Cakir, Filiz Yalcin; Gurgan, Sevil

2012-09-01

The aim of this in vitro study was to evaluate the surface roughness and hardness of both unbleached and bleached (opalescence; 10% carbamide peroxide) human enamel brushed with water (without dentifrice), fluoride abrasive dentifrice (Colgate Total) and whitening dentifrice (Natural White). Human enamel samples were obtained from third molars and randomly divided into five groups (n = 8): G1 - Control (brushed with water without dentifrice), G2 - Colgate Total (fluoride abrasive dentifrice), G3 - Natural White (whitening dentifrice), G4 - Opalescence (10% carbamide peroxide) and then brushed with Colgate Total, G5 - Opalescence (10% carbamide peroxide) and then brushed with Natural White. Bleaching regimen was applied according to manufacturers' instructions. The brushing process was performed with a modified Nyffenegger's brushing machine. Surface roughness was analyzed with a profilometer. Microhardness testing was performed with a Brinell hardness tester. Results were statistically analyzed by Kruskal-Wallis, one-way ANOVA analysis and Mann-Whitney U, Wilcoxon matched-pairs signed-ranks tests. There were significant differences in surface roughness values for all groups, which showed an increase in roughness (p < 0.05). When the bleaching treatment combined with brushing with whitening dentifrice was performed (G5), there was a significant decrease in hardness values (p < 0.05). The other groups (G1, G2, G3, G4) showed no significant hardness differences (p > 0.05). It was concluded that toothbrushing procedures increased the enamel surface roughness, and that bleaching regimen performed with cleaning treatment, through brushing with whitening dentifrice decreased hardness values. When applied together, bleaching and cleaning treatments may alter the enamel surface roughness and hardness values.

Abrasive wear of resin composites as related to finishing and polishing procedures.

PubMed

Turssi, Cecilia P; Ferracane, Jack L; Serra, Mônica C

2005-07-01

Finishing and polishing procedures may cause topographical changes and introduce subsurface microcracks in dental composite restoratives. Since both of these effects may contribute toward the kinetics of wear, the purpose of this study was to assess and correlate the wear and surface roughness of minifilled and nanofilled composites finished and polished by different methods. Specimens (n=10) made of a minifilled and a nanofilled composite were finished and polished with one of the four sequences: (1) tungsten carbide burs plus Al(2)O(3)-impregnated brush (CbBr) or (2) tungsten carbide burs plus diamond-impregnated cup (CbCp), (3) diamond burs plus brush (DmBr) or (4) diamond burs plus cup (DmCp). As a control, abrasive papers were used. After surface roughness had been quantified, three-body abrasion was simulated using the OHSU wear machine. The wear facets were then scanned to measure wear depth and post-testing roughness. All sets of data were subjected to ANOVA and Tukey's tests (alpha=0.05). Pearson's correlation test was applied to check for the existence of a relationship between pre-testing roughness and wear. Significantly smoother surfaces were attained with the sequences CbBr and CbCp, whereas DmCp yielded the roughest surface. Regardless of the finishing/polishing technique, the nanofilled composite exhibited the lowest pre-testing roughness and wear. There was no correlation between the surface roughness achieved after finishing/polishing procedures and wear (p=0.3899). Nano-sized materials may have improved abrasive wear resistance over minifilled composites. The absence of correlation between wear and surface roughness produced by different finishing/polishing methods suggests that the latter negligibly influences material loss due to three-body abrasion.

The effect of different polishing systems on surface roughness and gloss of various resin composites.

PubMed

Da Costa, Juliana; Ferracane, Jack; Paravina, Rade D; Mazur, Rui Fernando; Roeder, Leslie

2007-01-01

The purpose of this in vitro study was to evaluate the surface finish and gloss of five direct resin composites polished with six polishing systems. One hundred and fifty disk-shaped composite specimens (D=10.0 mm, 2-mm-thick, N=30 per material) were made. One side of each specimen was finished with a 16-fluted carbide finishing bur and then polished. Five specimens of each resin composite were randomly assigned to one of the six polishing systems. The surface roughness and gloss were measured with a surface profilometer and a glossmeter. The results were analyzed by two-way analysis of variance and Tukey's t-test (p

Mapping lava flow textures using three-dimensional measures of surface roughness

NASA Astrophysics Data System (ADS)

Mallonee, H. C.; Kobs-Nawotniak, S. E.; McGregor, M.; Hughes, S. S.; Neish, C.; Downs, M.; Delparte, D.; Lim, D. S. S.; Heldmann, J. L.

2016-12-01

Lava flow emplacement conditions are reflected in the surface textures of a lava flow; unravelling these conditions is crucial to understanding the eruptive history and characteristics of basaltic volcanoes. Mapping lava flow textures using visual imagery alone is an inherently subjective process, as these images generally lack the resolution needed to make these determinations. Our team has begun mapping lava flow textures using visual spectrum imagery, which is an inherently subjective process involving the challenge of identifying transitional textures such as rubbly and slabby pāhoehoe, as these textures are similar in appearance and defined qualitatively. This is particularly problematic for interpreting planetary lava flow textures, where we have more limited data. We present a tool to objectively classify lava flow textures based on quantitative measures of roughness, including the 2D Hurst exponent, RMS height, and 2D:3D surface area ratio. We collected aerial images at Craters of the Moon National Monument (COTM) using Unmanned Aerial Vehicles (UAVs) in 2015 and 2016 as part of the FINESSE (Field Investigations to Enable Solar System Science and Exploration) and BASALT (Biologic Analog Science Associated with Lava Terrains) research projects. The aerial images were stitched together to create Digital Terrain Models (DTMs) with resolutions on the order of centimeters. The DTMs were evaluated by the classification tool described above, with output compared against field assessment of the texture. Further, the DTMs were downsampled and reevaluated to assess the efficacy of the classification tool at data resolutions similar to current datasets from other planetary bodies. This tool allows objective classification of lava flow texture, which enables more accurate interpretations of flow characteristics. This work also gives context for interpretations of flows with comparatively low data resolutions, such as those on the Moon and Mars. Textural maps based on quantitative measures of roughness are a valuable asset for studies of lava flows on Earth and other planetary bodies.

Sea ice roughness: the key for predicting Arctic summer ice albedo

NASA Astrophysics Data System (ADS)

Landy, J.; Ehn, J. K.; Tsamados, M.; Stroeve, J.; Barber, D. G.

2017-12-01

Although melt ponds on Arctic sea ice evolve in stages, ice with smoother surface topography typically allows the pond water to spread over a wider area, reducing the ice-albedo and accelerating further melt. Building on this theory, we simulated the distribution of meltwater on a range of statistically-derived topographies to develop a quantitative relationship between premelt sea ice surface roughness and summer ice albedo. Our method, previously applied to ICESat observations of the end-of-winter sea ice roughness, could account for 85% of the variance in AVHRR observations of the summer ice-albedo [Landy et al., 2015]. Consequently, an Arctic-wide reduction in sea ice roughness over the ICESat operational period (from 2003 to 2008) explained a drop in ice-albedo that resulted in a 16% increase in solar heat input to the sea ice cover. Here we will review this work and present new research linking pre-melt sea ice surface roughness observations from Cryosat-2 to summer sea ice albedo over the past six years, examining the potential of winter roughness as a significant new source of sea ice predictability. We will further evaluate the possibility for high-resolution (kilometre-scale) forecasts of summer sea ice albedo from waveform-level Cryosat-2 roughness data in the landfast sea ice zone of the Canadian Arctic. Landy, J. C., J. K. Ehn, and D. G. Barber (2015), Albedo feedback enhanced by smoother Arctic sea ice, Geophys. Res. Lett., 42, 10,714-10,720, doi:10.1002/2015GL066712.

Impact of the ongoing Amazonian deforestation on local precipitation: A GCM simulation study

DOE Office of Scientific and Technical Information (OSTI.GOV)

Walker, G.K.; Sud, Y.C.; Atlas, R.

1995-03-01

Numerical simulation experiments were conducted to delineate the influence of in situ deforestation data on episodic rainfall by comparing two ensembles of five 5-day integrations performed with a recent version of the Goddard Laboratory for Atmospheres GCM that has a simple biosphere model (SiB). The first set, called control cases, used the standard SiB vegetation cover (comprising 12 biomes) and assumed a fully forested Amazonia, while the second set, called deforestation cases, distinguished the partially deforested regions of Amazonia as savanna. Except for this difference, all other initial and prescribed boundary conditions were kept identical in both sets of integrations.more » The differential analyses of these five cases show the following local effects of deforestation. (1) A discernible decrease in evapotranspiration of about 0.80 mm d{sup {minus}1} (roughly 18%) that is quite robust in the averages for 1-, 2-, and 5-day forecasts. (2) A decrease in precipitation of about 1.18 mm d{sup {minus}1} (roughly 8%) that begins to emerge even in 1-2-day averages and exhibits complex evolution that extends downstream with the winds. A larger decrease in precipitation as compared to evapotranspiration produces some drying and warming. The precipitation differences are consistent with the decrease in atmospheric moisture flux convergence and are consistent with earlier simulation studies of local climate change due to large-scale deforestation. (3) A significant decrease in the surface drag force (as a consequence of reduced surface roughness of deforested regions) that, in turn, affects the dynamical structure of moisture convergence and circulation. The surface winds increase significantly during the first day, and thereafter the increase is well maintained even in the 2- and 5-day averages. 34 refs., 9 figs., 2 tabs.« less

Design of low surface roughness-low residual stress-high optoelectronic merit a-IZO thin films for flexible OLEDs

DOE PAGES

Kumar, Naveen; Wilkinson, Taylor M.; Packard, Corinne E.; ...

2016-06-08

The development of efficient and reliable large-area flexible optoelectronic devices demands low surface roughness-low residual stress-high optoelectronic merit transparent conducting oxide (TCO) thin films. Here, we correlate surface roughness-residual stress-optoelectronic properties of sputtered amorphous indium zinc oxide (a-IZO) thin films using a statistical design of experiment (DOE) approach and find a common growth space to achieve a smooth surface in a stress-free and high optoelectronic merit a-IZO thin film. The sputtering power, growth pressure, oxygen partial pressure, and RF/(RF+DC) are varied in a two-level system with a full factorial design, and results are used to deconvolve the complex growth space,more » identifying significant control growth parameters and their possible interactions. The surface roughness of a-IZO thin film varies over 0.19 nm to 3.97 nm, which is not in line with the general assumption of low surface roughness in a-IZO thin films. The initial regression model and analysis of variance reveal no single optimum growth sub-space to achieve low surface roughness (=0.5 nm), low residual stress (-1 to 0 GPa), and industrially acceptable electrical conductivity (>1000 S/cm) for a-IZO thin films. The extrapolation of growth parameters in light of the current results and previous knowledge leads to a new sub-space, resulting in a low residual stress of -0.52 +/- 0.04 GPa, a low surface roughness of 0.55 +/- 0.03 nm, and moderate electrical conductivity of 1962 +/- 3.84 S/cm in a-IZO thin films. Lastly, these results demonstrate the utility of the DOE approach to multi-parameter optimization, which provides an important tool for the development of flexible TCOs for the next-generation flexible organic light emitting diodes applications.« less

Design of low surface roughness-low residual stress-high optoelectronic merit a-IZO thin films for flexible OLEDs

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kumar, Naveen; Kumar, Mukesh, E-mail: mkumar@iitrpr.ac.in, E-mail: cpackard@mines.edu; Wilkinson, Taylor M.

2016-06-14

The development of efficient and reliable large-area flexible optoelectronic devices demands low surface roughness-low residual stress-high optoelectronic merit transparent conducting oxide (TCO) thin films. Here, we correlate surface roughness-residual stress-optoelectronic properties of sputtered amorphous indium zinc oxide (a-IZO) thin films using a statistical design of experiment (DOE) approach and find a common growth space to achieve a smooth surface in a stress-free and high optoelectronic merit a-IZO thin film. The sputtering power, growth pressure, oxygen partial pressure, and RF/(RF+DC) are varied in a two-level system with a full factorial design, and results are used to deconvolve the complex growth space,more » identifying significant control growth parameters and their possible interactions. The surface roughness of a-IZO thin film varies over 0.19 nm to 3.97 nm, which is not in line with the general assumption of low surface roughness in a-IZO thin films. The initial regression model and analysis of variance reveal no single optimum growth sub-space to achieve low surface roughness (≤0.5 nm), low residual stress (−1 to 0 GPa), and industrially acceptable electrical conductivity (>1000 S/cm) for a-IZO thin films. The extrapolation of growth parameters in light of the current results and previous knowledge leads to a new sub-space, resulting in a low residual stress of −0.52±0.04 GPa, a low surface roughness of 0.55±0.03 nm, and moderate electrical conductivity of 1962±3.84 S/cm in a-IZO thin films. These results demonstrate the utility of the DOE approach to multi-parameter optimization, which provides an important tool for the development of flexible TCOs for the next-generation flexible organic light emitting diodes applications.« less

Polishing parameter optimization for end-surface of chalcogenide glass fiber connector

NASA Astrophysics Data System (ADS)

Guo, Fangxia; Dai, Shixun; Tang, Junzhou; Wang, Xunsi; Li, Xing; Xu, Yinsheng; Wu, Yuehao; Liu, Zijun

2017-11-01

We have investigated the optimization parameters for polishing end-surface of chalcogenide glass fiber connector in the paper. Six SiC abrasive particles of different sizes were used to polish the fiber in order of size from large to small. We analyzed the effects of polishing parameters such as particle sizes, grinding speeds and polishing durations on the quality of the fiber end surface and determined the optimized polishing parameters. We found that, high-quality fiber end surface can be achieved using only three different SiC abrasives. The surface roughness of the final ChG fiber end surface is about 48 nm without any scratches, spots and cracks. Such polishing processes could reduce the average insertion loss of the connector to about 3.4 dB.

Artificial Roughness Encoding with a Bio-inspired MEMS- based Tactile Sensor Array

PubMed Central

Oddo, Calogero Maria; Beccai, Lucia; Felder, Martin; Giovacchini, Francesco; Carrozza, Maria Chiara

2009-01-01

A compliant 2×2 tactile sensor array was developed and investigated for roughness encoding. State of the art cross shape 3D MEMS sensors were integrated with polymeric packaging providing in total 16 sensitive elements to external mechanical stimuli in an area of about 20 mm2, similarly to the SA1 innervation density in humans. Experimental analysis of the bio-inspired tactile sensor array was performed by using ridged surfaces, with spatial periods from 2.6 mm to 4.1 mm, which were indented with regulated 1N normal force and stroked at constant sliding velocity from 15 mm/s to 48 mm/s. A repeatable and expected frequency shift of the sensor outputs depending on the applied stimulus and on its scanning velocity was observed between 3.66 Hz and 18.46 Hz with an overall maximum error of 1.7%. The tactile sensor could also perform contact imaging during static stimulus indentation. The experiments demonstrated the suitability of this approach for the design of a roughness encoding tactile sensor for an artificial fingerpad. PMID:22412304

Numerical Modeling of Compressible Flow and Its Control

DTIC Science & Technology

2014-03-01

surface just outbound of the fin . This impinging jet is believed to be responsible for the high surface pressure, skin friction, and heat transfer in...and fine grid simulations over predict the heat transfer by roughly 13% for this case. E. LF12 Case, Sharp Fin at 12° In the LF12 case, a sharp...Dolling, D. S., and Knight, D. D., “An Experimental/Computational Study of Heat Transfer in Sharp Fin Induced Turbulent Interactions at Mach 5,” AIAA

Effects of short-term immersion and brushing with different denture cleansers on the roughness, hardness, and color of two types of acrylic resin.

PubMed

Panariello, Beatriz Helena Dias; Izumida, Fernanda Emiko; Moffa, Eduardo Buozi; Pavarina, Ana Claudia; Jorge, Janaina Habib; Giampaolo, Eunice Teresinha

2015-06-01

To investigate the cumulative effects of brushing (B) or immersion (I), using different cleansing agents, on the surface roughness, hardness and color stability of a heat-polymerized denture resin, Lucitone 550 (L), and a hard chairside reline resin, Tokuyama Rebase Fast II (T). A total of 316 specimens (10 x 2 mm) were fabricated. The specimens (n = 9) were divided into brushing or immersion groups according to the following agents: dentifrice/distilled water (D), 1% sodium hypochlorite (NaOCl), Corega Tabs (Pb), 1% chlorhexidine gluconate (Chx), and 0.2% peracetic acid (Ac). Brushing and immersion were tested independently. Assays were performed after 1, 3, 21, 45 and 90 brushing cycles or immersion of 10 seconds each. Data were evaluated statistically by repeated measures ANOVA. Tukey's honestly significant difference (HSD) post-hoc test was used to determine differences between means (α = 0.05). For L there was no statistically significant difference in roughness, except a significant decrease in roughness by brushing with D. T showed a significant effect on the roughness after 90 immersions with Ac. Hardness values decreased for L when specimens were immersed or brushed in NaOCl and Pb. The hardness of T decreased with increases in the repetitions (immersion or brushing), regardless of the cleaning method. Values of color stability for L resin showed significant color change after brushing with and immersion in Ac and Pb. Brushing with D exhibited a higher incidence of color change. For T there were no significant differences between cleaning agents and repetitions in immersion. A color change was noted after three brushings with the Ac, Chx, and D. Brushing with dentifrice decreased roughness of L. Immersion in or brushing with NaOCl and Pb decreased the hardness of L. For T, hardness decreased with increases in immersions or brushing. Color changes after the immersion in or brushing with cleaning agents were clinically acceptable according to National Bureau of Standards parameters for both resins.

Effects of surface-finishing protocols on the roughness, color change, and translucency of different ceramic systems.

PubMed

Akar, Gülcan Coşkun; Pekkan, Gürel; Çal, Ebru; Eskitaşçıoğlu, Gürcan; Özcan, Mutlu

2014-08-01

Surface-finishing protocols have a mechanical impact on ceramic surfaces that could eventually affect surface topography and light scattering. An optimum protocol is needed to avoid damaging the optical properties of ceramics. The purpose of this study was to determine the effects of different surface-finishing protocols on the surface roughness, color change, and translucency of ceramic and metal ceramic restorations. Standardized disk-shaped specimens (1.5 × 10 mm, n=128) were fabricated from 3 different ceramic core materials (aluminum oxide [Al2O3]-AL, zirconium oxide [ZrO2]-ZR, lithium disilicate [Li2Si2O5]-LIT), veneered (V) with dentin ceramics (n=32 per group), and placed in the following groups: ALV, ZRV, and LITV. The metal ceramic group acted as the control (n=32). Four different surface-finishing methods were tested. Airborne-particle abrasion with 50 μm Al2O3, polishing with adjustment kit, polishing with adjustment kit plus diamond polishing paste, and autoglazing (n=8 subgroup) were applied on the veneering ceramics. The specimens were analyzed with a profilometer for surface roughness, and color change and translucency were measured with a clinical spectrophotometer. Statistical analyses were performed with 1-way ANOVA and the Tukey honest significant difference tests (α=.05). Specimens treated with the airborne particle abrasion method showed significantly higher mean profilometer for surface roughness values in all groups (P<.05). The polishing with adjustment kit and autoglazing methods revealed statistically similar surface roughness values in all groups (P>.05). With the diamond polishing paste method, lower surface roughness values were achieved in the ZRV and metal ceramic groups acted as the control groups. Different surface-finishing methods affected the color change of the ceramic systems, except for ZRV. Surface-finishing protocols significantly affected the translucency values of the ALV, LITV, and metal ceramic groups (P<.05). No single surface-finishing protocol can be recommended to obtain the smoothest surface and the least color change without affecting translucency for the ceramics tested. The airborne-particle abrasion protocol created rougher surfaces and decreased translucency, and color change in zirconia was not affected by the finishing protocols. Copyright © 2014 Editorial Council for the Journal of Prosthetic Dentistry. Published by Elsevier Inc. All rights reserved.

Low-loss slot waveguides with silicon (111) surfaces realized using anisotropic wet etching

NASA Astrophysics Data System (ADS)

Debnath, Kapil; Khokhar, Ali; Boden, Stuart; Arimoto, Hideo; Oo, Swe; Chong, Harold; Reed, Graham; Saito, Shinichi

2016-11-01

We demonstrate low-loss slot waveguides on silicon-on-insulator (SOI) platform. Waveguides oriented along the (11-2) direction on the Si (110) plane were first fabricated by a standard e-beam lithography and dry etching process. A TMAH based anisotropic wet etching technique was then used to remove any residual side wall roughness. Using this fabrication technique propagation loss as low as 3.7dB/cm was realized in silicon slot waveguide for wavelengths near 1550nm. We also realized low propagation loss of 1dB/cm for silicon strip waveguides.

Establishing Antibacterial Multilayer Films on the Surface of Direct Metal Laser Sintered Titanium Primed with Phase-Transited Lysozyme

PubMed Central

Guan, Binbin; Wang, Haorong; Xu, Ruiqing; Zheng, Guoying; Yang, Jie; Liu, Zihao; Cao, Man; Wu, Mingyao; Song, Jinhua; Li, Neng; Li, Ting; Cai, Qing; Yang, Xiaoping; Li, Yanqiu; Zhang, Xu

2016-01-01

Direct metal laser sintering is a technology that allows the fabrication of titanium (Ti) implants with a functional gradation of porosity and surface roughness according to three-dimensional (3D) computer data. The surface roughness of direct metal laser sintered titanium (DMLS-Ti) implants may provide abundant binding sites for bacteria. Bacterial colonization and subsequent biofilm formation can cause unsatisfactory cell adhesion and implant-related infections. To prevent such infections, a novel phase-transited lysozyme (PTL) was utilized as an initial functional layer to simply and effectively prime DMLS-Ti surfaces for subsequent coating with antibacterial multilayers. The purpose of the present study was to establish a surface with dual biological functionality. The minocycline-loaded polyelectrolyte multilayers of hyaluronic acid (HA) and chitosan (CS) formed via a layer-by-layer (LbL) self-assembly technique on PTL-functionalized DMLS-Ti were designed to inhibit pathogenic microbial infections while allowing the DMLS-Ti itself and the modified coatings to retain acceptable biocompatibility. The experimental results indicate that the DMLS-Ti and the hydrogel treated surfaces can inhibit early bacterial adhesion while completely preserving osteoblast functions. This design is expected to gain considerable interest in the medical field and to have good potential for applications in multifunctional DMLS-Ti implants. PMID:27821857

Establishing Antibacterial Multilayer Films on the Surface of Direct Metal Laser Sintered Titanium Primed with Phase-Transited Lysozyme.

PubMed

Guan, Binbin; Wang, Haorong; Xu, Ruiqing; Zheng, Guoying; Yang, Jie; Liu, Zihao; Cao, Man; Wu, Mingyao; Song, Jinhua; Li, Neng; Li, Ting; Cai, Qing; Yang, Xiaoping; Li, Yanqiu; Zhang, Xu

2016-11-08

Direct metal laser sintering is a technology that allows the fabrication of titanium (Ti) implants with a functional gradation of porosity and surface roughness according to three-dimensional (3D) computer data. The surface roughness of direct metal laser sintered titanium (DMLS-Ti) implants may provide abundant binding sites for bacteria. Bacterial colonization and subsequent biofilm formation can cause unsatisfactory cell adhesion and implant-related infections. To prevent such infections, a novel phase-transited lysozyme (PTL) was utilized as an initial functional layer to simply and effectively prime DMLS-Ti surfaces for subsequent coating with antibacterial multilayers. The purpose of the present study was to establish a surface with dual biological functionality. The minocycline-loaded polyelectrolyte multilayers of hyaluronic acid (HA) and chitosan (CS) formed via a layer-by-layer (LbL) self-assembly technique on PTL-functionalized DMLS-Ti were designed to inhibit pathogenic microbial infections while allowing the DMLS-Ti itself and the modified coatings to retain acceptable biocompatibility. The experimental results indicate that the DMLS-Ti and the hydrogel treated surfaces can inhibit early bacterial adhesion while completely preserving osteoblast functions. This design is expected to gain considerable interest in the medical field and to have good potential for applications in multifunctional DMLS-Ti implants.

Establishing Antibacterial Multilayer Films on the Surface of Direct Metal Laser Sintered Titanium Primed with Phase-Transited Lysozyme

NASA Astrophysics Data System (ADS)

Guan, Binbin; Wang, Haorong; Xu, Ruiqing; Zheng, Guoying; Yang, Jie; Liu, Zihao; Cao, Man; Wu, Mingyao; Song, Jinhua; Li, Neng; Li, Ting; Cai, Qing; Yang, Xiaoping; Li, Yanqiu; Zhang, Xu

2016-11-01

Direct metal laser sintering is a technology that allows the fabrication of titanium (Ti) implants with a functional gradation of porosity and surface roughness according to three-dimensional (3D) computer data. The surface roughness of direct metal laser sintered titanium (DMLS-Ti) implants may provide abundant binding sites for bacteria. Bacterial colonization and subsequent biofilm formation can cause unsatisfactory cell adhesion and implant-related infections. To prevent such infections, a novel phase-transited lysozyme (PTL) was utilized as an initial functional layer to simply and effectively prime DMLS-Ti surfaces for subsequent coating with antibacterial multilayers. The purpose of the present study was to establish a surface with dual biological functionality. The minocycline-loaded polyelectrolyte multilayers of hyaluronic acid (HA) and chitosan (CS) formed via a layer-by-layer (LbL) self-assembly technique on PTL-functionalized DMLS-Ti were designed to inhibit pathogenic microbial infections while allowing the DMLS-Ti itself and the modified coatings to retain acceptable biocompatibility. The experimental results indicate that the DMLS-Ti and the hydrogel treated surfaces can inhibit early bacterial adhesion while completely preserving osteoblast functions. This design is expected to gain considerable interest in the medical field and to have good potential for applications in multifunctional DMLS-Ti implants.

Group D. Initiator paper. Implants--peri-implant (hard and soft tissue) interactions in health and disease: the impact of explosion of implant manufacturers.

PubMed

Ivanovski, Saso

2015-01-01

1. The best-documented implants have a threaded solid screw-type design and are manufactured from commercially pure (grade IV) titanium. There is good evidence to support implants ≥ 6 mm in length, and ≥ 3 mm in diameter. 2. Integrity of the seal between the abutment and the implant is important for several reasons, including minimization of mechanical and biological complications and maintaining marginal bone levels. Although the ideal design features of the implant-abutment connection have not been determined, an internal connection, micro-grooves at the implant collar, and horizontal offset of the implant-abutment junction (platform switch) appear to impart favorable properties. 3. Implants with moderately rough implant surfaces provide advantages over machined surfaces in terms of the speed and extent of osseointegration. While the favorable performances of both minimally and moderately rough surfaces are supported by long-term data, moderately rough surfaces provide superior outcomes in compromised sites, such as the posterior maxilla. 4. Although plaque is critical in the progression of peri-implantitis, the disease has a multi-factorial aetiology, and may be influenced by poor integrity of the abutment/implant connection. Iatrogenic factors, such as the introduction of a foreign body. (e.g., cement) below the mucosal margin, can be important contributors. 5. Clinicians should exercise caution when using a particular implant system, ensuring that the implant design is appropriate and supported by scientific evidence. Central to this is access to and participation in quality education on the impact that implant characteristics can have on clinical outcomes. Caution should be exercised in utilizing non-genuine restorative componentry that may lead to a poor implant-abutment fit and subsequent technical and biological complications.

Effects of 6 months of aging in water on hardness and surface roughness of two microhybrid dental composites.

PubMed

de Moraes, Rafael Ratto; Marimon, José Laurindo Machado; Schneider, Luis Felipe; Sinhoreti, Mário Alexandre Coelho; Correr-Sobrinho, Lourenço; Bueno, Márcia

2008-06-01

This study assessed the effect of 6 months of aging in water on surface roughness and surface/subsurface hardness of two microhybrid resin composites. Filtek Z250 and Charisma were tested. Cylindrical specimens were obtained and stored in distilled water for 24 hours or 6 months, at 37 degrees C. For Knoop hardness evaluation, the specimens were transversely wet-flattened, and indentations were made on surface and subsurface layers. Data were submitted to three-way ANOVA and Tukey's test (alpha < or = 0.05). Surface roughness baseline measurements were made at 24 hours and repeated after 6 months of storage. Data were submitted to repeated measures ANOVA and Tukey's test (alpha < or = 0.05). Surface hardness (KHN, kg/mm(2)) means (+/- standard deviation) ranged from 55 +/- 1 to 49 +/- 4 for Z250 and from 50 +/- 2 to 41 +/- 3 for Charisma, at 24 hours and 6 months, respectively. Subsurface means ranged from 58 +/- 2 to 61 +/- 3 for Z250 and from 50 +/- 1 to 54 +/- 2 for Charisma, at 24 hours and 6 months. For both composites, the aged specimens presented significantly softer surfaces (p < 0.01). For the subsurface hardness, alteration after storage was detected only for Charisma, which presented a significant rise in hardness (p < 0.01). Z250 presented significantly harder surface and subsurface layers in comparison with Charisma. Surface roughness (Ra, mum) means ranged from 0.07 +/- 0.00 to 0.07 +/- 0.01 for Z250 and from 0.06 +/- 0.01 to 0.07 +/- 0.01 for Charisma, at 24 hours and 6 months, respectively. For both composites, no significant roughness alteration was detected during the study (p= 0.386). The 6-month period of storage in water presented a significant softening effect on the surfaces of the composites, although no significant deleterious alteration was detected for the subsurface hardness. In addition, the storage period had no significant effect on the surface roughness of the materials.

Microwave remote sensing and its application to soil moisture detection

NASA Technical Reports Server (NTRS)

Newton, R. W. (Principal Investigator)

1977-01-01

The author has identified the following significant results. Experimental measurements were utilized to demonstrate a procedure for estimating soil moisture, using a passive microwave sensor. The investigation showed that 1.4 GHz and 10.6 GHz can be used to estimate the average soil moisture within two depths; however, it appeared that a frequency less than 10.6 GHz would be preferable for the surface measurement. Average soil moisture within two depths would provide information on the slope of the soil moisture gradient near the surface. Measurements showed that a uniform surface roughness similar to flat tilled fields reduced the sensitivity of the microwave emission to soil moisture changes. Assuming that the surface roughness was known, the approximate soil moisture estimation accuracy at 1.4 GHz calculated for a 25% average soil moisture and an 80% degree of confidence, was +3% and -6% for a smooth bare surface, +4% and -5% for a medium rough surface, and +5.5% and -6% for a rough surface.

Surface study of irradiated sapphires from Phrae Province, Thailand using AFM

NASA Astrophysics Data System (ADS)

Monarumit, N.; Jivanantaka, P.; Mogmued, J.; Lhuaamporn, T.; Satitkune, S.

2017-09-01

The irradiation is one of the gemstone enhancements for improving the gem quality. Typically, there are many varieties of irradiated gemstones in the gem market such as diamond, topaz, and sapphire. However, it is hard to identify the gemstones before and after irradiation. The aim of this study is to analyze the surface morphology for classifying the pristine and irradiated sapphires using atomic force microscope (AFM). In this study, the sapphire samples were collected from Phrae Province, Thailand. The samples were irradiated by high energy electron beam for a dose of ionizing radiation at 40,000 kGy. As the results, the surface morphology of pristine sapphires shows regular atomic arrangement, whereas, the surface morphology of irradiated sapphires shows the nano-channel observed by the 2D and 3D AFM images. The atomic step height and root mean square roughness have changed after irradiation due to the micro-structural defect on the sapphire surface. Therefore, this study is a frontier application for sapphire identification before and after irradiation.

Effect of plasma treatment (He/CH4) on glass surface for the reduction of powder flux adhesion in the spray drying process

NASA Astrophysics Data System (ADS)

Ramlan, Nadiah; Zamri, Nazirah Wahidah Mohd; Maskat, Mohd Yusof; Hoong, Chin Oi; Theng, Lau Yen; Zubairi, Saiful Irwan

2018-04-01

A 50Hz glow discharge He/CH4 plasma was generated and applied for the modification of glass surface to reduce powder adhesion on the wall of spray dryer. The hydrophobicity of the glass samples determined by the water droplet contact angle and adhesion weight on glass, dependent on the CH4 flow rate and plasma exposure time. There was a peak that appeared at 1470 cm-1 on the surface of treated glass indicating the presence of CH3 groups from ATR-FTIR data. Surface morphology analysis using scanning electron microscopy (SEM) showed changes of roughness in the surface-treated glass. The presence of alkyl group (CH3) that deposited on the glass surface is one of the factors that contribute to the increase in the surface roughness. The surface roughness will reflect the value of contact angle where hydrophobic surface are rougher compared to hydrophilic surface. The plasma treatment could enhance the value of the contact angle and thus reduced the adhesion on the spray dryer glass surface.

Effect of surface roughness on droplet splashing

NASA Astrophysics Data System (ADS)

Hao, Jiguang

2017-12-01

It is well known that rough surfaces trigger prompt splashing and suppress corona splashing on droplet impact. Upon water droplet impact, we experimentally found that a slightly rough substrate triggers corona splashing which is suppressed to prompt splashing by both further increase and further decrease of surface roughness. The nonmonotonic effect of surface roughness on corona splashing weakens with decreasing droplet surface tension. The threshold velocities for prompt splashing and corona splashing are quantified under different conditions including surface roughness, droplet diameter, and droplet surface tension. It is determined that slight roughness significantly enhances both prompt splashing and corona splashing of a water droplet, whereas it weakly affects low-surface-tension droplet splashing. Consistent with previous studies, high roughness triggers prompt splashing and suppresses corona splashing. Further experiments on droplet spreading propose that the mechanism of slight roughness enhancing water droplet splashing is due to the decrease of the wetted area with increasing surface roughness.

Structural properties 3,16-bis triisopropylsilylethynyl (pentacene) (TIPS-pentacene) thin films onto organic dielectric layer using slide coating method

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rusnan, Fara Naila; Mohamad, Khairul Anuar; Seria, Dzul Fahmi Mohd Husin

3,16-bis triisopropylsilylethynyl (Pentacene) (TIPS-Pentacene) compactable interface property is important in order to have a good arrangement of molecular structure. Comparison for TIPS-Pentacene deposited between two different surface layers conducted. 0.1wt% TIPS-Pentacene diluted in chloroform were deposited onto poly(methylmeaclyrate) (PMMA) layered transparent substrates using slide coating method. X-ray diffraction (XRD) used to determine crystallinity of thin films. Series of (00l) diffraction peaks obtained with sharp first peaks (001) for TIPS-Pentacene deposited onto PMMA layer at 5.35° and separation of 16.3 Å. Morphology and surface roughness were carried out using scanning electron microscope (SEM) and surface profilemeter LS500, respectively.TIPS-Pentacene deposited onto PMMAmore » layer formed needled-like-shape grains with 10.26 nm surface roughness. These properties were related as thin film formed and its surface roughness plays important role towards good mobility devices.« less

10.6 Micrometer Absorption in Molybdenum Mirrors

DTIC Science & Technology

1974-07-01

laser damage studies. Interferometric versus stylus instrument measurement of surface rough- ness is discussed. The polishing and coating procedures are...preliminary CW laser damage studies. Interferometric versus stylus instrument measurement of surface roughness is discussed. The polishing and coating...contrast ( Nomarski ) microscopic invescigations were made of th. surface. Figue 3 presents Nomarski photographs of mirrors M-107 through M-109. M-108

Effect of the Polishing Procedures on Color Stability and Surface Roughness of Composite Resins

PubMed Central

Schmitt, Vera Lucia; Puppin-Rontani, Regina Maria; Naufel, Fabiana Scarparo; Nahsan, Flávia Pardo Salata; Alexandre Coelho Sinhoreti, Mário; Baseggio, Wagner

2011-01-01

Objectives. To evaluate the polishing procedures effect on color stability and surface roughness of composite resins. Methods. Specimens were distributed into 6 groups: G1: Filtek Supreme XT + PoGo; G2: Filtek Supreme XT + Sof-Lex; G3: Filtek Supreme XT + no polishing; G4: Amelogen + PoGo; G5: Amelogen + Sof-Lex.; G6: Amelogen + no polishing. Initial color values were evaluated using the CIELab scale. After polishing, surface roughness was evaluated and the specimens were stored in coffee solution at 37°C for 7 days. The final color measurement and roughness were determined. Results. Sof-Lex resulted in lower staining. Amelogen showed the highest roughness values than Filtek Supreme on baseline and final evaluations regardless of the polishing technique. Filtek Supreme polished with PoGo showed the lowest roughness values. All groups presented discoloration after storage in coffee solution, regardless of the polishing technique. Conclusion. Multiple-step polishing technique provided lower degree of discoloration for both composite resins. The final surface texture is material and technique dependent. PMID:21991483

Enhanced Osteoblast Response to Porosity and Resolution of Additively Manufactured Ti-6Al-4V Constructs with Trabeculae-Inspired Porosity

PubMed Central

Cheng, Alice; Humayun, Aiza; Schwartz, Zvi

2016-01-01

Abstract The addition of porosity to the traditionally used solid titanium metal implants has been suggested to more closely mimic the natural mechanical properties of bone and increase osseointegration in dental and orthopedic implants. The objective of this study was to evaluate cellular response to three-dimensional (3D) porous Ti-6Al-4V constructs fabricated by additive manufacturing using laser sintering with low porosity (LP), medium porosity (MP), and high porosity (HP) with low resolution (LR) and high resolution (HR) based on a computed tomography scan of human trabecular bone. After surface processing, construct porosity ranged from 41.0% to 76.1%, but all possessed micro-/nanoscale surface roughness and similar surface chemistry containing mostly Ti, O, and C. Biological responses (osteoblast differentiation, maturation, and local factor production) by MG63 osteoblast-like cells and normal human osteoblasts favored 3D than two-dimensional (2D) solid constructs. First, MG63 cells were used to assess differences in cell response to 2D compared to LR and HR porous 3D constructs. MG63 cells were sensitive to porosity resolution and exhibited increased osteocalcin (OCN), vascular endothelial growth factor (VEGF), osteoprotegerin (OPG), and bone morphogenetic protein 2 (BMP2) on HR 3D constructs than on 2D and LR 3D constructs. MG63 cells also exhibited porosity-dependent responses on HR constructs, with up to a 6.9-fold increase in factor production on LP-HR and MP-HR constructs than on HP-HR constructs. NHOsts were then used to validate biological response on HR constructs. NHOsts exhibited decreased DNA content and alkaline phosphatase activity and up to a 2.9-fold increase in OCN, OPG, VEGF, BMP2, and BMP4 on 3D HR constructs than on 2D controls. These results indicate that osteoblasts prefer a 3D architecture than a 2D surface and that osteoblasts are sensitive to the resolution of trabecular detail and porosity parameters of laser-sintered 3D Ti-6Al-4V constructs. PMID:28804735

Enhanced Osteoblast Response to Porosity and Resolution of Additively Manufactured Ti-6Al-4V Constructs with Trabeculae-Inspired Porosity.

PubMed

Cheng, Alice; Humayun, Aiza; Boyan, Barbara D; Schwartz, Zvi

2016-03-01

The addition of porosity to the traditionally used solid titanium metal implants has been suggested to more closely mimic the natural mechanical properties of bone and increase osseointegration in dental and orthopedic implants. The objective of this study was to evaluate cellular response to three-dimensional (3D) porous Ti-6Al-4V constructs fabricated by additive manufacturing using laser sintering with low porosity (LP), medium porosity (MP), and high porosity (HP) with low resolution (LR) and high resolution (HR) based on a computed tomography scan of human trabecular bone. After surface processing, construct porosity ranged from 41.0% to 76.1%, but all possessed micro-/nanoscale surface roughness and similar surface chemistry containing mostly Ti, O, and C. Biological responses (osteoblast differentiation, maturation, and local factor production) by MG63 osteoblast-like cells and normal human osteoblasts favored 3D than two-dimensional (2D) solid constructs. First, MG63 cells were used to assess differences in cell response to 2D compared to LR and HR porous 3D constructs. MG63 cells were sensitive to porosity resolution and exhibited increased osteocalcin (OCN), vascular endothelial growth factor (VEGF), osteoprotegerin (OPG), and bone morphogenetic protein 2 (BMP2) on HR 3D constructs than on 2D and LR 3D constructs. MG63 cells also exhibited porosity-dependent responses on HR constructs, with up to a 6.9-fold increase in factor production on LP-HR and MP-HR constructs than on HP-HR constructs. NHOsts were then used to validate biological response on HR constructs. NHOsts exhibited decreased DNA content and alkaline phosphatase activity and up to a 2.9-fold increase in OCN, OPG, VEGF, BMP2, and BMP4 on 3D HR constructs than on 2D controls. These results indicate that osteoblasts prefer a 3D architecture than a 2D surface and that osteoblasts are sensitive to the resolution of trabecular detail and porosity parameters of laser-sintered 3D Ti-6Al-4V constructs.

Formation of organic layer on femtosecond laser-induced periodic surface structures

NASA Astrophysics Data System (ADS)

Yasumaru, Naoki; Sentoku, Eisuke; Kiuchi, Junsuke

2017-05-01

Two types of laser-induced periodic surface structures (LIPSS) formed on titanium by femtosecond (fs) laser pulses (λ = 800 nm, τ = 180 fs, ν = 1 kHz) in air were investigated experimentally. At a laser fluence F above the ablation threshold, LIPSS with a minimum mean spacing of D < λ⁄2 were observed perpendicular to the laser polarization direction. In contrast, for F slightly below than the ablation threshold, ultrafine LIPSS with a minimum value of D < λ/10 were formed parallel to the polarization direction. The surface roughness of the parallel-oriented LIPSS was almost the same as that of the non-irradiated surface, unlike the high roughness of the perpendicular-oriented LIPSS. In addition, although the surface state of the parallel-oriented LIPSS was the same as that of the non-irradiated surface, the perpendicular-oriented LIPSS were covered with an organic thin film similar to a cellulose derivative that cannot be easily formed by conventional chemical synthesis. The results of these surface analyses indicate that these two types of LIPSS are formed through different mechanisms. This fs-laser processing technique may become a new technology for the artificial synthesis of cellulose derivatives.

Porous texture of activated carbons prepared by phosphoric acid activation of woods

NASA Astrophysics Data System (ADS)

Díaz-Díez, M. A.; Gómez-Serrano, V.; Fernández González, C.; Cuerda-Correa, E. M.; Macías-García, A.

2004-11-01

Activated carbons (ACs) have been prepared using chestnut, cedar and walnut wood shavings from furniture industries located in the Comunidad Autónoma de Extremadura (SW Spain). Phosphoric acid (H3PO4) at different concentrations (i.e. 36 and 85 wt.%) has been used as activating agent. ACs have been characterized from the results obtained by N2 adsorption at 77 K. Moreover, the fractal dimension (D) has been calculated in order to determine the AC surface roughness degree. Optimal textural properties of ACs have been obtained by chemical activation with H3PO4 36 wt.%. This is corroborated by the slightly lower values of D for samples treated with H3PO4 85 wt.%.

Lacunarity study of speckle patterns produced by rough surfaces

NASA Astrophysics Data System (ADS)

Dias, M. R. B.; Dornelas, D.; Balthazar, W. F.; Huguenin, J. A. O.; da Silva, L.

2017-11-01

In this work we report on the study of Lacunarity of digital speckle patterns generated by rough surfaces. The study of Lacunarity of speckle patterns was performed on both static and moving rough surfaces. The results show that the Lacunarity is sensitive to the surface roughness, which suggests that it can be used to perform indirect measurement of surface roughness as well as to monitor defects, or variations of roughness, of metallic moving surfaces. Our results show the robustness of this statistical tool applied to speckle pattern in order to study surface roughness.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kafka, Kyle R. P.; Hoffman, Brittany N.; Papernov, Semyon

The laser-induced damage threshold of fused-silica samples processed via magnetorheological finishing is investigated for polishing compounds depending on the type of abrasive material and the post-polishing surface roughness. The effectiveness of laser conditioning is examined using a ramped pre-exposure with the same 351-nm, 3-ns Gaussian pulses. Lastly, we examine chemical etching of the surface and correlate the resulting damage threshold to the etching protocol. A combination of etching and laser conditioning is found to improve the damage threshold by a factor of ~3, while maintaining <1-nm surface roughness.

Nanoindentation and surface roughness profilometry of poly methyl methacrylate denture base materials.

PubMed

Zafar, Muhammad Sohail; Ahmed, Naseer

2014-01-01

Polymers have a wide range of applications in dentistry. Poly methyl methacrylate (PMMA) is the most popular for making orthodontic retainers, dentures as well as synthetic teeth. Prior to clinical applications, the appliances are polished in the dental laboratory to achieve smooth, polished and comfortable surfaces. The objective of this study was to analyze the surface roughness profiles of PMMA dentures polished using two different approaches. In addition, the effects of ultrasonication and sandblasting were also evaluated on the fitting surface of PMMA dentures. This was an in vitro study using non-contact mode surface roughness profilometer and nano-indenter. Samples were polished using two different techniques (Standard and modified). Both cold cure and heat cure PMMA denture surfaces were evaluated for roughness, nanohardness and elastic modulus. The absolute hardness was recorded 297.72±19.04 MPa and 229.93±18.53 MPa for heat cured PMMA and cold cured PMMA. Manufactured acrylic teeth were harder (319.20±12.58 MPa) with an elastic modulus of (4.34±1.86 GPa). Modified polishing techniques (group 3) produced smoother surface. It was concluded that elastic moduli of acrylic tooth and heat cure PMMA is not very different. Surface treatments such as ultrasonication or sandblasting do not affect the roughness profiles of denture fitting surfaces.

Surface correlations of hydrodynamic drag for transitionally rough engineering surfaces

NASA Astrophysics Data System (ADS)

Thakkar, Manan; Busse, Angela; Sandham, Neil

2017-02-01

Rough surfaces are usually characterised by a single equivalent sand-grain roughness height scale that typically needs to be determined from laboratory experiments. Recently, this method has been complemented by a direct numerical simulation approach, whereby representative surfaces can be scanned and the roughness effects computed over a range of Reynolds number. This development raises the prospect over the coming years of having enough data for different types of rough surfaces to be able to relate surface characteristics to roughness effects, such as the roughness function that quantifies the downward displacement of the logarithmic law of the wall. In the present contribution, we use simulation data for 17 irregular surfaces at the same friction Reynolds number, for which they are in the transitionally rough regime. All surfaces are scaled to the same physical roughness height. Mean streamwise velocity profiles show a wide range of roughness function values, while the velocity defect profiles show a good collapse. Profile peaks of the turbulent kinetic energy also vary depending on the surface. We then consider which surface properties are important and how new properties can be incorporated into an empirical model, the accuracy of which can then be tested. Optimised models with several roughness parameters are systematically developed for the roughness function and profile peak turbulent kinetic energy. In determining the roughness function, besides the known parameters of solidity (or frontal area ratio) and skewness, it is shown that the streamwise correlation length and the root-mean-square roughness height are also significant. The peak turbulent kinetic energy is determined by the skewness and root-mean-square roughness height, along with the mean forward-facing surface angle and spanwise effective slope. The results suggest feasibility of relating rough-wall flow properties (throughout the range from hydrodynamically smooth to fully rough) to surface parameters.

Effects of thermal cycling on surface roughness, hardness and flexural strength of polymethylmethacrylate and polyamide denture base resins.

PubMed

Ayaz, Elif Aydoğan; Bağış, Bora; Turgut, Sedanur

2015-10-16

The purpose of this study was to evaluate the effects of thermal cycling on the surface roughness, hardness and flexural strength of denture resins. Polyamide (PA; Deflex and Valplast) and polymethylmethacrylate (PMMA; QC-20 and Acron MC) denture materials were selected. A total of 180 specimens were fabricated and then divided into 3 groups. The first group (group 1) acted as a control and was not thermocycled. The second group (group 2) was subjected to thermocycling for 10,000 cycles in artificial saliva and 5,000 cycles in distilled water. The last group (group 3) was thermocycled for 20,000 cycles in artificial saliva and 10,000 cycles in distilled water. The surface roughness were measured with a profilometer. The hardness of the resins were measured with a Vickers Hardness Tester using a 100-gf load. The flexural strength test was performed using the universal test machine with a crosshead speed of 5 mm/min. Data were analyzed using statistical software. The results of the measurements in the 3 different tests were analyzed by Kruskal-Wallis test with Bonferroni correction. Multiple comparisons were made by Conover and Wilcoxon tests. There was a significant difference between the PMMA and PA groups in terms of surface roughness, hardness and transverse strength before and after thermal cycling (p<0.001). Thermal cycling did not change the surface roughness, hardness and flexural strength values of either the PMMA or PA group (p>0.001).

Roughness Effects on the Formation of a Leading Edge Vortex

NASA Astrophysics Data System (ADS)

Elliott, Cassidy; Lang, Amy; Wahidi, Redha; Wilroy, Jacob

2016-11-01

Microscopic scales cover the wings of Monarch butterflies, creating a patterned surface. This patterning is an important natural flow control mechanism that is thought to delay the growth of the leading edge vortex (LEV) produced by the flapping motion of a wing. The increased skin friction caused by the scales leads to a weaker LEV being shed into the butterfly's wake, lessening drag and increasing flight efficiency. To test this theory, a plate of random roughness was designed in SolidWorks and printed on the Objet 30 Pro 3D printer. A 2x3x5 cubic foot tow tank was used to test the rough plate at Reynold's numbers of 1500, 3000, and 6000 (velocities of 8, 16, and 32 mm/s) at an angle of attack of 45 degrees. Particle Image Velocimetry (PIV) captured images of the LEV generated by the plate when towed upwards through the particle-seeded flow. Codes written in MatLab were used to automatically track and determine the strength of the LEV. Circulation values for the randomly-rough plate were then compared to the same values generated in a previous experiment that used a smooth plate and a grooved plate to determine the effect of the patterning on vortex development. Funding provided by NSF REU site Grant EEC 1358991 and CBET 1628600.

50 kHz bottom backscattering measurements from two types of artificially roughened sandy bottoms

NASA Astrophysics Data System (ADS)

Son, Su-Uk; Cho, Sungho; Choi, Jee Woong

2016-07-01

Laboratory measurements of 50 kHz bottom backscattering strengths as a function of grazing angle were performed on the sandy bottom of a water tank; two types of bottom roughnesses, a relatively smooth interface and a rough interface, were created on the bottom surface. The roughness profiles of the two interface types were measured directly using an ultrasound arrival time difference of 5 MHz and then were Fourier transformed to obtain the roughness power spectra. The measured backscattering strengths increased from -29 to 0 dB with increasing grazing angle from 35 to 86°, which were compared to theoretical backscattering model predictions. The comparison results implied that bottom roughness is a key factor in accurately predicting bottom scattering for a sandy bottom.

Effect of implantoplasty on fracture resistance and surface roughness of standard diameter dental implants.

PubMed

Costa-Berenguer, Xavier; García-García, Marta; Sánchez-Torres, Alba; Sanz-Alonso, Mariano; Figueiredo, Rui; Valmaseda-Castellón, Eduard

2018-01-01

To assess the effect of implantoplasty on the fracture resistance, surface roughness, and macroscopic morphology of standard diameter (4.1 mm) external connection dental implants. An in vitro study was conducted in 20 screw-shaped titanium dental implants with an external connection. In 10 implants, the threads and surface were removed and polished with high-speed burs (implantoplasty), while the remaining 10 implants were used as controls. The final implant dimensions were recorded. The newly polished surface quality was assessed by scanning electron microscopy (SEM) and by 3D surface roughness analysis using a confocal laser microscope. Finally, all the implants were subjected to a mechanical pressure resistance test. A descriptive analysis of the data was made. Also, Student's t tests were employed to detect differences regarding the compression tests. Implantoplasty was carried out for a mean time of 10 min and 48 s (standard deviation (SD) of 1 min 22 s). Macroscopically, the resulting surface had a smooth appearance, although small titanium shavings and silicon debris were present. The final surface roughness (S a values 0.1 ± 0.02 μm) was significantly lower than that of the original (0.75 ± 0.08 μm S a ) (p = .005). There was minimal reduction in the implant's inner body diameter (0.19 ± 0.03 mm), and no statistically significant differences were found between the test and control implants regarding the maximum resistance force (896 vs 880 N, respectively). Implantoplasty, although technically demanding and time-consuming, does not seem to significantly alter fracture resistance of standard diameter external connection implants. A smooth surface with S a values below 0.1 μm can be obtained through the use of silicon polishers. A larger sample is required to confirm that implantoplasty does not significantly affect the maximum resistance force of standard diameter external connection implants. © 2017 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

Control of Stationary Cross-Flow Modes in a Mach 3.5 Boundary Layer Using Patterned Passive and Active Roughness

NASA Technical Reports Server (NTRS)

Schuele, Chan Yong

2011-01-01

Spanwise-periodic roughness designed to excite selected wavelengths of stationary cross- ow modes was investigated in a 3-D boundary layer at Mach 3.5. The test model was a sharp-tipped 14deg right-circular cone. The model and integrated sensor traversing system were placed in the Mach 3.5 Supersonic Low Disturbance Tunnel (SLDT) equipped with a "quiet design" nozzle at the NASA Langley Research Center. The model was oriented at a 4:2deg angle of attack to produce a mean cross-fl ow velocity component in the boundary layer over the cone. Five removable cone tips have been investigated. One has a smooth surface that is used to document the baseline ("natural") conditions. Two had minute (20 - 40 micron) "dimples" that are equally spaced around the circumference, at a streamwise location that is just upstream of the linear stability neutral growth branch for cross- ow modes. The azimuthal mode numbers of the dimpled tips were selected to either enhance the most amplified wave numbers, or to suppress the growth of the most amplified wave numbers. Two of the cone tips had an array of plasma streamwise vortex generators that were designed to simulate the disturbances produced by the passive patterned roughness. The results indicate that the stationary cross-fl ow modes were highly receptive to the patterned roughness of both passive and active types. The patterned passive roughness that was designed to suppress the growth of the most amplified modes had an azimuthal wavelength that was 66% smaller that that of the most amplified stationary cross- ow mode. This had the effect to increase the transition Reynolds number from 25% to 50% depending on the measurement technique. The application of the research is on turbulent transition control on swept wings of supersonic aircraft. The plasma-based roughness has the advantage over the passive roughness of being able to be adaptable to different conditions that would occur during a flight mission.

Effect of endodontic irrigating solutions on the microhardness and roughness of root canal dentin: an in vitro study.

PubMed

Patil, Chetan R; Uppin, Veerendra

2011-01-01

To evaluate the effect of widely used endodontic irrigating solutions on root dentin microhardness and surface roughness. One hundred twenty, non-carious extracted human permanent incisor teeth were selected. The crowns of the teeth were sectioned and the roots were separated longitudinally to get 240 specimens. These specimens were then divided into six groups according to the irrigating solutions used. The solutions used were 5% and 2.5% NaOCl solutions, 3% H2 O2 , 17% EDTA solution, 0.2% chlorhexidine gluconate, and distilled water. Then, the specimens were subjected to microhardness and roughness testing. The data were analyzed using ANOVA and Tukey's multiple comparison tests. The results of this study indicated that all irrigation solutions, except 0.2% chlorhexidine gluconate, decreased the microhardness of root dentin, and 3% H2 O2 and 0.2% chlorhexidine gluconate had no effect on surface roughness. Within the limitation of this study, it is concluded that 0.2% chlorhexidine gluconate seems to be an appropriate irrigation solution, because of its harmless effect on the microhardness and surface roughness of root canal dentin.

Noviodunum Roman Fortress. a Survey on a City Wall Section

NASA Astrophysics Data System (ADS)

Teodor, A.; Teodor, E. S.; Florea, M. S.; Popescu, M. A.

2011-09-01

The paper presents in detail the method used to acquire 2D and 3D representations for the Large Tower of the Roman fortress from Noviodunum (Isaccea, Tulcea County). The available implements were a total station, a digital camera and some software for handling data. The method is not new by any rate, but well fitted to the aims - recording archaeological data on ruined but massif walls, with rough surfaces - and with a limited budget. Lately considered as a low cost procedure, laser scanning is still costly and rare in some East-European countries. Our method, as simple as it is, provides reliable data as a 3D survey, along texture details, at the lowest price, on unfinished fieldwork, preserving and picturing a stage of knowledge about the site and the architectural bodies.

Fabrication of surface micro- and nanostructures for superhydrophobic surfaces in electric and electronic applications

NASA Astrophysics Data System (ADS)

Xiu, Yonghao

In our study, the superhydrophobic surface based on biomimetic lotus leave is explored to maintain the desired properties for self-cleaning. Parameters in controlling bead-up and roll-off characteristics of water droplets were investigated on different model surfaces. The governing equations were proposed. Heuristic study is performed. First, the fundamental understanding of the effect of roughness on superhydrophobicity is performed. The effect of hierarchical roughness, i.e., two scale roughness effect on roughness is investigated using systems of (1) monodisperse colloidal silica sphere (submicron) arrays and Au nanoparticle on top and (2) Si micrometer pyramids and Si nanostructures on top from KOH etching and metal assisted etching of Si. The relation between the contact area fraction and water droplet contact angles are derived based on Wenzel and Cassie-Baxter equation for the systems and the two scale effect is explained regarding the synergistic combination of two scales. Previously the microscopic three-phase-contact line is thought to be the key factor in determining contact angles and hystereses. In our study, Laplace pressure was brought up and related to the three-phase-contact line and taken as a key figure of merit in determining superhydrophobicity. In addition, we are one of the first to study the effect of tapered structures (wall inclination). Combining with a second scale roughness on the tapered structures, stable Cassie state for both water and low surface energy oil may be achieved. This is of great significance for designing both superhydrophobicity and superoleophobicity. Regarding the origin of contact angle hysteresis, study of superhydrophobicity on micrometer Si pillars was performed. The relation between the interface work of function and contact angle hysteresis was proposed and derived mathematically based on the Young-Dupre equation. The three-phase-contact line was further related to a secondary scale roughness induced. Based on our understanding of the roughness effect on superhydrophobicity (both contact angle and hysteresis), structured surfaces from polybutadiene, polyurethane, silica, and Si etc. were successfully prepared. For engineering applications of superhydrophobic surfaces, stability issues regarding UV, mechanical robustness and humid environment need to be investigated. Among these factors, UV stability is the first one to be studied. However, most polymer surfaces we prepared failed the purpose. Silica surfaces with excellent UV stability were prepared. This method consists of preparation of rough silica surfaces, thermal treatment and the following surface hydrophobization by fluoroalkyl silane treatment. Fluoroalkyl groups are UV stable and the underlying species are silica which is also UV stable (UV transparent). UV stability on the surface currently is 5,500 h according the standard test method of ASTM D 4329. No degradation on surface superhydrophobicity was observed. New methods for preparing superhydrophobic and transparent silica surfaces were investigated using urea-choline chloride eutectic liquid to generate fine roughness and reduce the cost for preparation of surface structures. Another possible application for self-cleaning in photovoltaic panels was investigated on Si surfaces by construction of the two-scale rough structures followed by fluoroalkyl silane treatment. Metal (Au) assisted etching was employed to fabricate nanostructures on micrometer pyramid surfaces. The light reflection on the prepared surfaces was investigated. After surface texturing using KOH etching for micrometer pyramids and the following nanostructure using metal assisted etching, surface light reflection reduced to a minimum value which shows that this surface texturing technique is highly promising for improving the photovoltaic efficiency while imparting photovoltaics the self-cleaning feature. This surface is also expected to be UV stable due to the same fluoroalkyl silane used. Regarding the mechanical robustness, epoxy-silica superhydrophobic surfaces were prepared by O2 plasma etching to generate enough surface roughness of silica spheres followed by fluoroalkyl silane treatment. A robustness test method was proposed and the test results showed that the surface is among the most robust surfaces for the superhydrophobic surfaces we prepared and currently reported in literature.

Thermal Effects of Lunar Surface Roughness: Application for the 2008 LRO Diviner Lunar Radiometer Experiment

NASA Astrophysics Data System (ADS)

Greenhagen, B.; Paige, D. A.

2007-12-01

It is well known that surface roughness affects spectral slope in the infrared. For the first time, we applied a three-dimensional thermal model to a high resolution lunar topography map to study the effects of surface roughness on lunar thermal emission spectra. We applied a numerical instrument model of the upcoming Diviner Lunar Radiometer Experiment (DLRE) to simulate the expected instrument response to surface roughness variations. The Diviner Lunar Radiometer Experiment (DLRE) will launch in late 2008 onboard the Lunar Reconnaissance Orbiter (LRO). DLRE is a nine-channel radiometer designed to study the thermal and petrologic properties of the lunar surface. DLRE has two solar channels (0.3-3.0 μm high/low sensitivity), three mid-infrared petrology channels (7.55-8.05, 8.10-8.40 8.40-8.70 μm), and four thermal infrared channels (12.5-25, 25-50, 50-100, and 100-200 μm). The topographic data we used was selected from a USGS Hadley Rille DEM (from Apollo 15 Panoramic Camera data) with 10 m resolution (M. Rosiek; personal communication). To remove large scale topographic features, we applied a 200 x 200 pixel boxcar high-pass filter to a relatively flat portion of the DEM. This "flattened" surface roughness map served as the basis for much of this study. We also examined the unaltered topography. Surface temperatures were calculated using a three-dimensional ray tracing thermal model. We created temperature maps at numerous solar incidence angles with nadir viewing geometry. A DLRE instrument model, which includes filter spectral responses and detector fields of view, was applied to the high resolution temperature maps. We studied both the thermal and petrologic effects of surface roughness. For the thermal study, the output of the optics model is a filter specific temperature, scaled to a DLRE footprint of < 500 m. For the petrologic study, we examined the effect of the surface roughness induced spectral slope on the DLRE's ability to locate the Christiansen Feature, which is a good compositional indicator. With multiple thermal infrared channels over a wide spectral range, DLRE will be well suited to measure temperature variations due to surface roughness. Any necessary compensation (e.g. correction for spectral slope) to the mid-infrared petrology data will be performed.

High Reynolds number rough wall turbulent boundary layer experiments using Braille surfaces

NASA Astrophysics Data System (ADS)

Harris, Michael; Monty, Jason; Nova, Todd; Allen, James; Chong, Min

2007-11-01

This paper details smooth, transitional and fully rough turbulent boundary layer experiments in the New Mexico State high Reynolds number rough wall wind tunnel. The initial surface tested was generated with a Braille printer and consisted of an uniform array of Braille points. The average point height being 0.5mm, the spacing between the points in the span was 0.5mm and the surface consisted of span wise rows separated by 4mm. The wavelength to peak ratio was 8:1. The boundary layer thickness at the measurement location was 190mm giving a large separation of roughness height to layer thickness. The maximum friction velocity was uτ=1.5m/s at Rex=3.8 x10^7. Results for the skin friction co-efficient show that this surface follows a Nikuradse type inflectional curve and that Townsends outer layer similarity hypothesis is valid for rough wall flows with a large separation of scales. Mean flow and turbulence statistics will be presented.

Stereo imaging and cytocompatibility of a model dental implant surface formed by direct laser fabrication.

PubMed

Mangano, Carlo; Raspanti, Mario; Traini, Tonino; Piattelli, Adriano; Sammons, Rachel

2009-03-01

Direct laser fabrication (DLF) allows solids with complex geometry to be produced by sintering metal powder particles in a focused laser beam. In this study, 10 Ti6Al4V alloy model dental root implants were obtained by DLF, and surface characterization was carried out using stereo scanning electron microscopy to produce 3D reconstructions. The surfaces were extremely irregular, with approximately 100 microm deep, narrow intercommunicating crevices, shallow depressions and deep, rounded pits of widely variable shape and size, showing ample scope for interlocking with the host bone. Roughness parameters were as follows: R(t), 360.8 microm; R(z), 358.4 microm; R(a), 67.4 microm; and R(q), 78.0 microm. Disc specimens produced by DLF with an identically prepared surface were used for biocompatibility studies with rat calvarial osteoblasts: After 9 days, cells had attached and spread on the DLF surface, spanning across the crevices, and voids. Cell density was similar to that on a commercial rough microtextured surface but lower than on commercial smooth machined and smooth-textured grit-blasted, acid-etched surfaces. Human fibrin clot extension on the DLF surface was slightly improved by inorganic acid etching to increase the microroughness. With further refinements, DLF could be an economical means of manufacturing implants from titanium alloys. (c) 2008 Wiley Periodicals, Inc.

Three-Dimensional (3D) Nanometrology Based on Scanning Electron Microscope (SEM) Stereophotogrammetry.

PubMed

Tondare, Vipin N; Villarrubia, John S; Vlada R, András E

2017-10-01

Three-dimensional (3D) reconstruction of a sample surface from scanning electron microscope (SEM) images taken at two perspectives has been known for decades. Nowadays, there exist several commercially available stereophotogrammetry software packages. For testing these software packages, in this study we used Monte Carlo simulated SEM images of virtual samples. A virtual sample is a model in a computer, and its true dimensions are known exactly, which is impossible for real SEM samples due to measurement uncertainty. The simulated SEM images can be used for algorithm testing, development, and validation. We tested two stereophotogrammetry software packages and compared their reconstructed 3D models with the known geometry of the virtual samples used to create the simulated SEM images. Both packages performed relatively well with simulated SEM images of a sample with a rough surface. However, in a sample containing nearly uniform and therefore low-contrast zones, the height reconstruction error was ≈46%. The present stereophotogrammetry software packages need further improvement before they can be used reliably with SEM images with uniform zones.

Venus surface roughness and Magellan stereo data

NASA Technical Reports Server (NTRS)

Maurice, Kelly E.; Leberl, Franz W.; Norikane, L.; Hensley, Scott

1994-01-01

Presented are results of some studies to develop tools useful for the analysis of Venus surface shape and its roughness. Actual work was focused on Maxwell Montes. The analyses employ data acquired by means of NASA's Magellan satellite. The work is primarily concerned with deriving measurements of the Venusian surface using Magellan stereo SAR. Roughness was considered by means of a theoretical analyses based on digital elevation models (DEM's), on single Magellan radar images combined with radiometer data, and on the use of multiple overlapping Magellan radar images from cycles 1, 2, and 3, again combined with collateral radiometer data.

Superlubricity of Graphite Induced by Multiple Transferred Graphene Nanoflakes.

PubMed

Li, Jinjin; Gao, Tianyang; Luo, Jianbin

2018-03-01

2D or 3D layered materials, such as graphene, graphite, and molybdenum disulfide, usually exhibit superlubricity properties when sliding occurs between the incommensurate interface lattices. This study reports the superlubricity between graphite and silica under ambient conditions, induced by the formation of multiple transferred graphene nanoflakes on the asperities of silica surfaces after the initial frictional sliding. The friction coefficient can be reduced to as low as 0.0003 with excellent robustness and is independent of the surface roughness, sliding velocities, and rotation angles. The superlubricity mechanism can be attributed to the extremely weak interaction and easy sliding between the transferred graphene nanoflakes and graphite in their incommensurate contact. This finding has important implications for developing approaches to achieve superlubricity of layered materials at the nanoscale by tribointeractions.

Predicting the Oxygen-Binding Properties of Platinum Nanoparticle Ensembles by Combining High-Precision Electron Microscopy and Density Functional Theory.

PubMed

Aarons, Jolyon; Jones, Lewys; Varambhia, Aakash; MacArthur, Katherine E; Ozkaya, Dogan; Sarwar, Misbah; Skylaris, Chris-Kriton; Nellist, Peter D

2017-07-12

Many studies of heterogeneous catalysis, both experimental and computational, make use of idealized structures such as extended surfaces or regular polyhedral nanoparticles. This simplification neglects the morphological diversity in real commercial oxygen reduction reaction (ORR) catalysts used in fuel-cell cathodes. Here we introduce an approach that combines 3D nanoparticle structures obtained from high-throughput high-precision electron microscopy with density functional theory. Discrepancies between experimental observations and cuboctahedral/truncated-octahedral particles are revealed and discussed using a range of widely used descriptors, such as electron-density, d-band centers, and generalized coordination numbers. We use this new approach to determine the optimum particle size for which both detrimental surface roughness and particle shape effects are minimized.

Superlubricity of Graphite Induced by Multiple Transferred Graphene Nanoflakes

PubMed Central

Gao, Tianyang; Luo, Jianbin

2018-01-01

Abstract 2D or 3D layered materials, such as graphene, graphite, and molybdenum disulfide, usually exhibit superlubricity properties when sliding occurs between the incommensurate interface lattices. This study reports the superlubricity between graphite and silica under ambient conditions, induced by the formation of multiple transferred graphene nanoflakes on the asperities of silica surfaces after the initial frictional sliding. The friction coefficient can be reduced to as low as 0.0003 with excellent robustness and is independent of the surface roughness, sliding velocities, and rotation angles. The superlubricity mechanism can be attributed to the extremely weak interaction and easy sliding between the transferred graphene nanoflakes and graphite in their incommensurate contact. This finding has important implications for developing approaches to achieve superlubricity of layered materials at the nanoscale by tribointeractions. PMID:29593965

Surface roughness: A review of its measurement at micro-/nano-scale

NASA Astrophysics Data System (ADS)

Gong, Yuxuan; Xu, Jian; Buchanan, Relva C.

2018-01-01

The measurement of surface roughness at micro-/nano-scale is of great importance to metrological, manufacturing, engineering, and scientific applications given the critical roles of roughness in physical and chemical phenomena. The surface roughness of materials can significantly change the way of how they interact with light, phonons, molecules, and so forth, thus surface roughness ultimately determines the functionality and property of materials. In this short review, the techniques of measuring micro-/nano-scale surface roughness are discussed with special focus on the limitations and capabilities of each technique. In addition, the calculations of surface roughness and their theoretical background are discussed to offer readers a better understanding of the importance of post-measurement analysis. Recent progress on fractal analysis of surface roughness is discussed to shed light on the future efforts in surface roughness measurement.

Study on influence of Surface roughness of Ni-Al2O3 nano composite coating and evaluation of wear characteristics

NASA Astrophysics Data System (ADS)

Raghavendra, C. R.; Basavarajappa, S.; Sogalad, Irappa

2018-02-01

Electrodeposition is one of the most technologically feasible and economically superior techniques for producing metallic coating. The advancement in the application of nano particles has grabbed the attention in all fields of engineering. In this present study an attempt has been made on the Ni-Al2O3nano particle composite coating on aluminium substrate by electrodeposition process. The aluminium surface requires a specific pre-treatment for better adherence of coating. In light of this a thin zinc layer is coated on the aluminium substrate by electroless process. In addition to this surface roughness is an important parameter for any coating method and material. In this work Ni-Al2O3 composite coating were successfully coated by varying the process parameters such as bath temperature, current density and particle loading. The experimentation was performed using central composite design based 20 trials of experiments. The effect of process parameters and surface roughness before and after coating is analyzed on wear rate and coating thickness. The results shown a better wear resistance of Ni-Al2O3 composite electrodeposited coating compared to Ni coating. The particle loading and interaction effect of current density with temperature has greater significant effect on wear rate. The surface roughness is significantly affected the wear behaviour and thickness of coating.

Nanostructures on fused silica surfaces produced by ion beam sputtering with Al co-deposition

NASA Astrophysics Data System (ADS)

Liu, Ying; Hirsch, Dietmar; Fechner, Renate; Hong, Yilin; Fu, Shaojun; Frost, Frank; Rauschenbach, Bernd

2018-01-01

The ion beam sputtering (IBS) of smooth mono-elemental Si with impurity co-deposition is extended to a pre-rippled binary compound surface of fused silica (SiO2). The dependence of the rms roughness and the deposited amount of Al on the distance from the Al source under Ar+ IBS with Al co-deposition was investigated on smooth SiO2, pre-rippled SiO2, and smooth Si surfaces, using atomic force microscopy and X-ray photoelectron spectroscopy. Although the amounts of Al deposited on these three surfaces all decreased with increasing distance from the Al target, the morphology and rms roughness of the smooth Si surface did not demonstrate a strong distance dependence. In contrast to smooth Si, the rms roughness of both the smooth and pre-rippled SiO2 surfaces exhibited a similar distance evolution trend of increasing, decreasing, and final stabilization at the distance where the results were similar to those obtained without Al co-deposition. However, the pre-rippled SiO2 surfaces showed a stronger modulation of rms roughness than the smooth surfaces. At the incidence angles of 60° and 70°, dot-decorated ripples and roof-tiles were formed on the smooth SiO2 surfaces, respectively, whereas nanostructures of closely aligned grains and blazed facets were generated on the pre-rippled SiO2, respectively. The combination of impurity co-deposition with pre-rippled surfaces was found to facilitate the formation of novel types of nanostructures and morphological growth. The initial ripples act as a template to guide the preferential deposition of Al on the tops of the ripples or the ripple sides facing the Al wedge, but not in the valleys between the ripples, leading to 2D grains and quasi-blazed grating, which offer significant promise in optical applications. The rms roughness enhancement is attributed not to AlSi, but to AlOxFy compounds originating mainly from the Al source.

14 CFR 25.1517 - Rough air speed, VRA.

Code of Federal Regulations, 2010 CFR

2010-01-01

... 14 Aeronautics and Space 1 2010-01-01 2010-01-01 false Rough air speed, VRA. 25.1517 Section 25... Limitations § 25.1517 Rough air speed, VRA. A rough air speed, VRA, for use as the recommended turbulence... specified in § 25.335(d); and (3) Is sufficiently less than VMO to ensure that likely speed variation during...

14 CFR 25.1517 - Rough air speed, VRA.

Code of Federal Regulations, 2011 CFR

2011-01-01

... 14 Aeronautics and Space 1 2011-01-01 2011-01-01 false Rough air speed, VRA. 25.1517 Section 25... Limitations § 25.1517 Rough air speed, VRA. A rough air speed, VRA, for use as the recommended turbulence... specified in § 25.335(d); and (3) Is sufficiently less than VMO to ensure that likely speed variation during...

Optical properties study of silicone polymer PDMS substrate surfaces modified by plasma treatment

NASA Astrophysics Data System (ADS)

Zahid, A.; Dai, B.; Hong, R.; Zhang, D.

2017-10-01

In this study, PDMS (polydimethylsiloxane) substrates with a half-plain, half-rough surface were prepared on a plain and rough fused silica glass substrate using a molding technique. The molded PDMS surface morphology was changed into a half-smooth and half-rough surface after peeling. The modified PDMS surfaces’ optical properties were inspected with and without treatment. The treatment is exposed by oxygen plasma (15 W) for 3 min in a vacuum, down to a pressure of six torr, using a vacuum pump. An atomic force microscope (AMF) and interferometer (white light) indicated that the plasma O2 treatment increased the formation of the plain surface and decreased the formation of the rough surface. The optical properties via a spectrophotometer (lambda) show the resonance from 300 nm to 1200 nm on the rough surface, which is considered to be a faithful reproduction for transmittance and reflectance. The Raman spectra and FDTD simulation results are in excellent agreement; not to be confused with metal local surface plasmon resonances (LSPRs). The Raman spectra peaks and hotspot are the results of the PDMS Si-O backbone. The PDMS substrate presented the diversity of the optical properties, which makes the substrate complementary to various optical applications.

Carbon buffer layers for smoothing superpolished glass surfaces as substrates for molybdenum /silicon multilayer soft-x-ray mirrors.

PubMed

Stock, H J; Hamelmann, F; Kleineberg, U; Menke, D; Schmiedeskamp, B; Osterried, K; Heidemann, K F; Heinzmann, U

1997-03-01

Zerodur and BK7 glass substrates (developed by Fa. Glaswerke Schott, D-55014 Mainz, Germany) from Carl Zeiss Oberkochen polished to a standard surface roughness of varsigma = 0.8 nm rms were coated with a C layer by electron-beam evaporation in the UHV. The roughness of the C-layer surfaces is reduced to 0.6 nm rms. A normal-incidence reflectance of 50% at a wavelength of 13 nm was measured for a Mo/Si multilayer soft-x-ray mirror with 30 double layers (N = 30) deposited onto the BK7/C substrate, whereas a similar Mo/Si multilayer (N = 30) evaporated directly onto the bare BK7 surface turned out to show a reflectance of only 42%.

Wind flow modulation due to variations of the water surface roughness

NASA Astrophysics Data System (ADS)

Shomina, Olga; Ermakov, Stanislav; Kapustin, Ivan; Lazareva, Tatiana

2016-04-01

Air-ocean interaction is a classical problem in atmosphere and ocean physics, which has important geophysical applications related to calculation of vertical and horizontal humidity, aerosol and gas fluxes, development of global climate models and weather forecasts. The structure of wind flow over fixed underlying surfaces, such as forestry, buildings, mountains, is well described, while the interaction between a rough water surface and turbulent wind is far more complicated because of the presence of wind waves with different wavelength and amplitudes and propagating with different velocities and directions. The aim of this study was to investigate experimentally the variability of the wind profile structure due to variations of wave characteristics. The surface roughness variations were produced using a) surfactant films (oleic acid) spread on the water surface and b) mechanically generated waves superimposed on wind waves. The first case is related to oil slicks on sea surface, the second one - to the sea swell, which propagates into zones with lower wind velocities and interacts with wind flow. Laboratory experiments were conducted in the Oval Wind Wave Tank (OWWT) at the Institute of Applied Physics, cross-section of the wind channel is 30 cm x30 cm. Wave amplitude and the spectrum of surface waves were measured by a wire wave gauge, the wind speed was measured using a hot-wire anemometer DISA and a Pitot tube. In the experiments with surfactants, two frequencies of dripping of the oleic acid were studied, so that low concentration films with the elasticity parameters of about 19 mN/m and the high concentration ("thick") films with the elasticity of 34 mN/m were formed. In the experiments with mechanically generated waves (MGW) different regimes were studied with MGW amplitude of 3.4 mm and of 4.4 mm, and with MGW frequencies of 3.3 Hz and 3.7 Hz. It was shown, that: a) the mean velocity of the wind flow in the presence of surfactant and MGW can be described by a logarithmic profile; b) in the presence of a surfactant film an increase of wind speed was revealed; the more elastic films was deployed on the surface - the stronger wind acceleration was detected; c) MGW result in deceleration of wind flow, the larger MGW amplitude the stronger wind flow reduction is; d) the wind deceleration effect is more pronounced for MGW with higher frequency, i.e. for slower propagating MGW. e) experimental dependencies of the logarithmic wind profile characteristics as functions of the rout mean square (RMS) wave height were obtained demonstrating the growth of the wind friction velocity and the roughness coefficient with RMS. The work has been supported by the Russian Foundation of Basic Research (Projects № 14-05-31535, 14-05-00876, 15-35-20992).

A multi-directional and multi-scale roughness filter to detect lineament segments on digital elevation models - analyzing spatial objects in R

NASA Astrophysics Data System (ADS)

Baumann, Sebastian; Robl, Jörg; Wendt, Lorenz; Willingshofer, Ernst; Hilberg, Sylke

2016-04-01

Automated lineament analysis on remotely sensed data requires two general process steps: The identification of neighboring pixels showing high contrast and the conversion of these domains into lines. The target output is the lineaments' position, extent and orientation. We developed a lineament extraction tool programmed in R using digital elevation models as input data to generate morphological lineaments defined as follows: A morphological lineament represents a zone of high relief roughness, whose length significantly exceeds the width. As relief roughness any deviation from a flat plane, defined by a roughness threshold, is considered. In our novel approach a multi-directional and multi-scale roughness filter uses moving windows of different neighborhood sizes to identify threshold limited rough domains on digital elevation models. Surface roughness is calculated as the vertical elevation difference between the center cell and the different orientated straight lines connecting two edge cells of a neighborhood, divided by the horizontal distance of the edge cells. Thus multiple roughness values depending on the neighborhood sizes and orientations of the edge connecting lines are generated for each cell and their maximum and minimum values are extracted. Thereby negative signs of the roughness parameter represent concave relief structures as valleys, positive signs convex relief structures as ridges. A threshold defines domains of high relief roughness. These domains are thinned to a representative point pattern by a 3x3 neighborhood filter, highlighting maximum and minimum roughness peaks, and representing the center points of lineament segments. The orientation and extent of the lineament segments are calculated within the roughness domains, generating a straight line segment in the direction of least roughness differences. We tested our algorithm on digital elevation models of multiple sources and scales and compared the results visually with shaded relief map of these digital elevation models. The lineament segments trace the relief structure to a great extent and the calculated roughness parameter represents the physical geometry of the digital elevation model. Modifying the threshold for the surface roughness value highlights different distinct relief structures. Also the neighborhood size at which lineament segments are detected correspond with the width of the surface structure and may be a useful additional parameter for further analysis. The discrimination of concave and convex relief structures perfectly matches with valleys and ridges of the surface.

The Design of 3D-Printed Lattice-Reinforced Thickness-Varying Shell Molds for Castings.

PubMed

Shangguan, Haolong; Kang, Jinwu; Yi, Jihao; Zhang, Xiaochuan; Wang, Xiang; Wang, Haibin; Huang, Tao

2018-03-30

3D printing technologies have been used gradually for the fabrication of sand molds and cores for castings, even though these molds and cores are dense structures. In this paper, a generation method for lattice-reinforced thickness-varying shell molds is proposed and presented. The first step is the discretization of the STL (Stereo Lithography) model of a casting into finite difference meshes. After this, a shell is formed by surrounding the casting with varying thickness, which is roughly proportional to the surface temperature distribution of the casting that is acquired by virtually cooling it in the environment. A regular lattice is subsequently constructed to support the shell. The outside surface of the shell and lattice in the cubic mesh format is then converted to STL format to serve as the external surface of the new shell mold. The internal surface of the new mold is the casting's surface with the normals of all of the triangles in STL format reversed. Experimental verification was performed on an Al alloy wheel hub casting. Its lattice-reinforced thickness-varying shell mold was generated by the proposed method and fabricated by the binder jetting 3D printing. The poured wheel hub casting was sound and of good surface smoothness. The cooling rate of the wheel hub casting was greatly increased due to the shell mold structure. This lattice-reinforced thickness-varying shell mold generation method is of great significance for mold design for castings to achieve cooling control.

The Design of 3D-Printed Lattice-Reinforced Thickness-Varying Shell Molds for Castings

PubMed Central

Shangguan, Haolong; Kang, Jinwu; Yi, Jihao; Zhang, Xiaochuan; Wang, Xiang; Wang, Haibin; Huang, Tao

2018-01-01

3D printing technologies have been used gradually for the fabrication of sand molds and cores for castings, even though these molds and cores are dense structures. In this paper, a generation method for lattice-reinforced thickness-varying shell molds is proposed and presented. The first step is the discretization of the STL (Stereo Lithography) model of a casting into finite difference meshes. After this, a shell is formed by surrounding the casting with varying thickness, which is roughly proportional to the surface temperature distribution of the casting that is acquired by virtually cooling it in the environment. A regular lattice is subsequently constructed to support the shell. The outside surface of the shell and lattice in the cubic mesh format is then converted to STL format to serve as the external surface of the new shell mold. The internal surface of the new mold is the casting’s surface with the normals of all of the triangles in STL format reversed. Experimental verification was performed on an Al alloy wheel hub casting. Its lattice-reinforced thickness-varying shell mold was generated by the proposed method and fabricated by the binder jetting 3D printing. The poured wheel hub casting was sound and of good surface smoothness. The cooling rate of the wheel hub casting was greatly increased due to the shell mold structure. This lattice-reinforced thickness-varying shell mold generation method is of great significance for mold design for castings to achieve cooling control. PMID:29601543

Site-specific ultrasound reflection properties and superficial collagen content of bovine knee articular cartilage

NASA Astrophysics Data System (ADS)

Laasanen, Mikko S.; Saarakkala, Simo; Töyräs, Juha; Rieppo, Jarno; Jurvelin, Jukka S.

2005-07-01

Previous quantitative 2D-ultrasound imaging studies have demonstrated that the ultrasound reflection measurement of articular cartilage surface sensitively detects degradation of the collagen network, whereas digestion of cartilage proteoglycans has no significant effect on the ultrasound reflection. In this study, the first aim was to characterize the ability of quantitative 2D-ultrasound imaging to detect site-specific differences in ultrasound reflection and backscattering properties of cartilage surface and cartilage-bone interface at visually healthy bovine knee (n = 30). As a second aim, we studied factors controlling ultrasound reflection properties of an intact cartilage surface. The ultrasound reflection coefficient was determined in time (R) and frequency domains (IRC) at medial femoral condyle, lateral patello-femoral groove, medial tibial plateau and patella using a 20 MHz ultrasound imaging instrument. Furthermore, cartilage surface roughness was quantified by calculating the ultrasound roughness index (URI). The superficial collagen content of the cartilage was determined using a FT-IRIS-technique. A significant site-dependent variation was shown in cartilage thickness, ultrasound reflection parameters, URI and superficial collagen content. As compared to R and IRC, URI was a more sensitive parameter in detecting differences between the measurement sites. Ultrasound reflection parameters were not significantly related to superficial collagen content, whereas the correlation between R and URI was high. Ultrasound reflection at the cartilage-bone interface showed insignificant site-dependent variation. The current results suggest that ultrasound reflection from the intact cartilage surface is mainly dependent on the cartilage surface roughness and the collagen content has a less significant role.

Kinematic ground motion simulations on rough faults including effects of 3D stochastic velocity perturbations

USGS Publications Warehouse

Graves, Robert; Pitarka, Arben

2016-01-01

We describe a methodology for generating kinematic earthquake ruptures for use in 3D ground‐motion simulations over the 0–5 Hz frequency band. Our approach begins by specifying a spatially random slip distribution that has a roughly wavenumber‐squared fall‐off. Given a hypocenter, the rupture speed is specified to average about 75%–80% of the local shear wavespeed and the prescribed slip‐rate function has a Kostrov‐like shape with a fault‐averaged rise time that scales self‐similarly with the seismic moment. Both the rupture time and rise time include significant local perturbations across the fault surface specified by spatially random fields that are partially correlated with the underlying slip distribution. We represent velocity‐strengthening fault zones in the shallow (<5  km) and deep (>15  km) crust by decreasing rupture speed and increasing rise time in these regions. Additional refinements to this approach include the incorporation of geometric perturbations to the fault surface, 3D stochastic correlated perturbations to the P‐ and S‐wave velocity structure, and a damage zone surrounding the shallow fault surface characterized by a 30% reduction in seismic velocity. We demonstrate the approach using a suite of simulations for a hypothetical Mw 6.45 strike‐slip earthquake embedded in a generalized hard‐rock velocity structure. The simulation results are compared with the median predictions from the 2014 Next Generation Attenuation‐West2 Project ground‐motion prediction equations and show very good agreement over the frequency band 0.1–5 Hz for distances out to 25 km from the fault. Additionally, the newly added features act to reduce the coherency of the radiated higher frequency (f>1  Hz) ground motions, and homogenize radiation‐pattern effects in this same bandwidth, which move the simulations closer to the statistical characteristics of observed motions as illustrated by comparison with recordings from the 1979 Imperial Valley earthquake.

Kinematic Ground-Motion Simulations on Rough Faults Including Effects of 3D Stochastic Velocity Perturbations

DOE PAGES

Graves, Robert; Pitarka, Arben

2016-08-23

Here, we describe a methodology for generating kinematic earthquake ruptures for use in 3D ground–motion simulations over the 0–5 Hz frequency band. Our approach begins by specifying a spatially random slip distribution that has a roughly wavenumber–squared fall–off. Given a hypocenter, the rupture speed is specified to average about 75%–80% of the local shear wavespeed and the prescribed slip–rate function has a Kostrov–like shape with a fault–averaged rise time that scales self–similarly with the seismic moment. Both the rupture time and rise time include significant local perturbations across the fault surface specified by spatially random fields that are partially correlatedmore » with the underlying slip distribution. We represent velocity–strengthening fault zones in the shallow (<5 km) and deep (>15 km) crust by decreasing rupture speed and increasing rise time in these regions. Additional refinements to this approach include the incorporation of geometric perturbations to the fault surface, 3D stochastic correlated perturbations to the P– and S–wave velocity structure, and a damage zone surrounding the shallow fault surface characterized by a 30% reduction in seismic velocity. We demonstrate the approach using a suite of simulations for a hypothetical Mw 6.45 strike–slip earthquake embedded in a generalized hard–rock velocity structure. The simulation results are compared with the median predictions from the 2014 Next Generation Attenuation–West2 Project ground–motion prediction equations and show very good agreement over the frequency band 0.1–5 Hz for distances out to 25 km from the fault. Additionally, the newly added features act to reduce the coherency of the radiated higher frequency (f>1 Hz) ground motions, and homogenize radiation–pattern effects in this same bandwidth, which move the simulations closer to the statistical characteristics of observed motions as illustrated by comparison with recordings from the 1979 Imperial Valley earthquake.« less