Effect of electric arc, gas oxygen torch and induction melting techniques on the marginal accuracy of cast base-metal and noble metal-ceramic crowns.

PubMed

Gómez-Cogolludo, Pablo; Castillo-Oyagüe, Raquel; Lynch, Christopher D; Suárez-García, María-Jesús

2013-09-01

The aim of this study was to identify the most appropriate alloy composition and melting technique by evaluating the marginal accuracy of cast metal-ceramic crowns. Seventy standardised stainless-steel abutments were prepared to receive metal-ceramic crowns and were randomly divided into four alloy groups: Group 1: palladium-gold (Pd-Au), Group 2: nickel-chromium-titanium (Ni-Cr-Ti), Group 3: nickel-chromium (Ni-Cr) and Group 4: titanium (Ti). Groups 1, 2 and 3 were in turn subdivided to be melted and cast using: (a) gas oxygen torch and centrifugal casting machine (TC) or (b) induction and centrifugal casting machine (IC). Group 4 was melted and cast using electric arc and vacuum/pressure machine (EV). All of the metal-ceramic crowns were luted with glass-ionomer cement. The marginal fit was measured under an optical microscope before and after cementation using image analysis software. All data was subjected to two-way analysis of variance (ANOVA). Duncan's multiple range test was run for post-hoc comparisons. The Student's t-test was used to investigate the influence of cementation (α=0.05). Uncemented Pd-Au/TC samples achieved the best marginal adaptation, while the worst fit corresponded to the luted Ti/EV crowns. Pd-Au/TC, Ni-Cr and Ti restorations demonstrated significantly increased misfit after cementation. The Ni-Cr-Ti alloy was the most predictable in terms of differences in misfit when either torch or induction was applied before or after cementation. Cemented titanium crowns exceeded the clinically acceptable limit of 120μm. The combination of alloy composition, melting technique, casting method and luting process influences the vertical seal of cast metal-ceramic crowns. An accurate use of the gas oxygen torch may overcome the results attained with the induction system concerning the marginal adaptation of fixed dental prostheses. Copyright © 2013 Elsevier Ltd. All rights reserved.

Vacuum Processing Technique for Development of Primary Standard Blackbodies

PubMed Central

Navarro, M.; Bruce, S. S.; Johnson, B. Carol; Murthy, A. V.; Saunders, R. D.

1999-01-01

Blackbody sources with nearly unity emittance that are in equilibrium with a pure freezing metal such as gold, silver, or copper are used as primary standard sources in the International Temperature Scale of 1990 (ITS-90). Recently, a facility using radio-frequency induction heating for melting and filling the blackbody crucible with the freeze metal under vacuum conditions was developed at the National Institute of Standards and Technology (NIST). The blackbody development under a vacuum environment eliminated the possibility of contamination of the freeze metal during the process. The induction heating, compared to a resistively heated convection oven, provided faster heating of crucible and resulted in shorter turn-around time of about 7 h to manufacture a blackbody. This paper describes the new facility and its application to the development of fixed-point blackbodies.

Solidification observations and sliding wear behavior of vacuum arc melting processed Ni-Al-TiC composites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Karantzalis, A.E., E-mail: akarantz@cc.uoi.gr; Lekatou, A.; Tsirka, K.

2012-07-15

Monolithic Ni{sub 3}Al and Ni-25 at.%Al intermetallic matrix TiC-reinforced composites were successfully produced by vacuum arc melting. TiC crystals were formed through a dissolution-reprecipitation mechanism and their final morphology is explained by means of a) Jackson's classical nucleation and growth phenomena and b) solidification rate considerations. The TiC presence altered the matrix microconstituents most likely due to specific melt-particle interactions and crystal plane epitaxial matching. TiC particles caused a significant decrease on the specific wear rate of the monolithic Ni{sub 3}Al alloy and the possible wear mechanisms are approached by means of a) surface oxidation, b) crack/flaws formation, c) materialmore » detachment and d) debris-counter surfaces interactions. - Highlights: Black-Right-Pointing-Pointer Vacuum arc melting (VAM) of Ni-Al based intermetallic matrix composite materials. Black-Right-Pointing-Pointer Solidification phenomena examination. Black-Right-Pointing-Pointer TiC crystal formation and growth mechanisms. Black-Right-Pointing-Pointer Sliding wear examination.« less

Ultra-high vacuum compatible preparation chain for intermetallic compounds

NASA Astrophysics Data System (ADS)

Bauer, A.; Benka, G.; Regnat, A.; Franz, C.; Pfleiderer, C.

2016-11-01

We report the development of a versatile material preparation chain for intermetallic compounds, which focuses on the realization of a high-purity growth environment. The preparation chain comprises an argon glovebox, an inductively heated horizontal cold boat furnace, an arc melting furnace, an inductively heated rod casting furnace, an optically heated floating-zone furnace, a resistively heated annealing furnace, and an inductively heated annealing furnace. The cold boat furnace and the arc melting furnace may be loaded from the glovebox by means of a load-lock permitting to synthesize compounds starting with air-sensitive elements while handling the constituents exclusively in an inert gas atmosphere. All furnaces are all-metal sealed, bakeable, and may be pumped to ultra-high vacuum. We find that the latter represents an important prerequisite for handling compounds with high vapor pressure under high-purity argon atmosphere. We illustrate the operational aspects of the preparation chain in terms of the single-crystal growth of the heavy-fermion compound CeNi2Ge2.

Numerical and Experimental Modeling of the Recirculating Melt Flow Inside an Induction Crucible Furnace

NASA Astrophysics Data System (ADS)

Asad, Amjad; Bauer, Katrin; Chattopadhyay, Kinnor; Schwarze, Rüdiger

2018-06-01

In the paper, a new water model of the turbulent recirculating flow in an induction furnace is introduced. The water model was based on the principle of the stirred vessel used in process engineering. The flow field in the water model was measured by means of particle image velocimetry in order to verify the model's performance. Here, it is indicated that the flow consists of two toroidal vortices similar to the flow in the induction crucible furnace. Furthermore, the turbulent flow in the water model is investigated numerically by adopting eddy-resolving turbulence modeling. The two toroidal vortices occur in the simulations as well. The numerical approaches provide identical time-averaged flow patterns. Moreover, a good qualitative agreement is observed on comparing the experimental and numerical results. In addition, a numerical simulation of the melt flow in a real induction crucible furnace was performed. The turbulent kinetic energy spectrum of the flow in the water model was compared to that of the melt flow in the induction crucible furnace to show the similarity in the nature of turbulence.

Ultra-high vacuum compatible induction-heated rod casting furnace

NASA Astrophysics Data System (ADS)

Bauer, A.; Neubauer, A.; Münzer, W.; Regnat, A.; Benka, G.; Meven, M.; Pedersen, B.; Pfleiderer, C.

2016-06-01

We report the design of a radio-frequency induction-heated rod casting furnace that permits the preparation of polycrystalline ingots of intermetallic compounds under ultra-high vacuum compatible conditions. The central part of the system is a bespoke water-cooled Hukin crucible supporting a casting mold. Depending on the choice of the mold, typical rods have a diameter between 6 mm and 10 mm and a length up to 90 mm, suitable for single-crystal growth by means of float-zoning. The setup is all-metal sealed and may be baked out. We find that the resulting ultra-high vacuum represents an important precondition for processing compounds with high vapor pressures under a high-purity argon atmosphere up to 3 bars. Using the rod casting furnace, we succeeded to prepare large high-quality single crystals of two half-Heusler compounds, namely, the itinerant antiferromagnet CuMnSb and the half-metallic ferromagnet NiMnSb.

Ultra-high vacuum compatible induction-heated rod casting furnace.

PubMed

Bauer, A; Neubauer, A; Münzer, W; Regnat, A; Benka, G; Meven, M; Pedersen, B; Pfleiderer, C

2016-06-01

We report the design of a radio-frequency induction-heated rod casting furnace that permits the preparation of polycrystalline ingots of intermetallic compounds under ultra-high vacuum compatible conditions. The central part of the system is a bespoke water-cooled Hukin crucible supporting a casting mold. Depending on the choice of the mold, typical rods have a diameter between 6 mm and 10 mm and a length up to 90 mm, suitable for single-crystal growth by means of float-zoning. The setup is all-metal sealed and may be baked out. We find that the resulting ultra-high vacuum represents an important precondition for processing compounds with high vapor pressures under a high-purity argon atmosphere up to 3 bars. Using the rod casting furnace, we succeeded to prepare large high-quality single crystals of two half-Heusler compounds, namely, the itinerant antiferromagnet CuMnSb and the half-metallic ferromagnet NiMnSb.

The Use of Induction Melting for the Treatment of Metal Radioactive Waste - 13088

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zherebtsov, Alexander; Pastushkov, Vladimir; Poluektov, Pavel

2013-07-01

The aim of the work is to assess the efficacy of induction melting metal for recycling radioactive waste in order to reduce the volume of solid radioactive waste to be disposed of, and utilization of the metal. (authors)

Study on the Removal of Gases in RH Refining Progress through Experiments Using Vacuum Induction Furnace

NASA Astrophysics Data System (ADS)

Niu, Deliang; Liu, Qingcai; Wang, Zhu; Ren, Shan; Lan, Yuanpei; Xu, Minren

Removal of gas is the major function of RH degasser. To optimize the RH refining craft in Chongqing Iron and Steel Co. Ltd, the degassing effect of RH degasser at different degrees of vacuum was investigated using a vacuum induction furnace. In addition, the effect of processing time on the gas content dissolved in molten steel was also studied. The results showed that degree of vacuum was one of the important factors that determined the degassing efficiency in RH refining process. High vacuum degree is helpful in the removal of gas, especially in the removal of [H] dissolved in molten steel. The processing time could be reduced from 25-30 min to 15 minutes and gas content could also meet the demand of RH refining.

Control of Vacuum Induction Brazing System for Sealing of Instrumentation Feedthrough

NASA Astrophysics Data System (ADS)

Ahn, Sung Ho; Hong, Jintae; Joung, Chang Young; Heo, Sung Ho

2017-04-01

The integrity of instrumentation cables is an important performance parameter in the brazing process, along with the sealing performance. In this paper, an accurate control scheme for brazing of the instrumentation feedthrough in a vacuum induction brazing system was developed. The experimental results show that the accurate brazing temperature control performance is achieved by the developed control scheme. It is demonstrated that the sealing performances of the instrumentation feedthrough and the integrity of the instrumentation cables are to be acceptable after brazing.

Vacuum ultraviolet photon fluxes in argon-containing inductively coupled plasmas

NASA Astrophysics Data System (ADS)

Radovanov, S. B.; Persing, H. M.; Wang, S.; Culver, C. L.; Boffard, J. B.; Lin, C. C.; Wendt, A. E.

2013-09-01

Vacuum ultraviolet (VUV) photons emitted from excited atomic states are ubiquitous in material processing plasmas. Damage of materials is induced by energy transfer from the VUV photons to the surface, causing disorder in the surface region, surface reactions, and affecting bonds in the material bulk. Monitoring of the surface flux of VUV photons from inductively coupled plasmas (ICP) and its dependence on discharge parameters is thus highly desirable. Results of non-invasive, direct windowless VUV detection using a photosensitive diode will be presented. Relative VUV fluxes were also obtained using a sodium salicylate coating on the inside of a vacuum window, converting VUV into visible light detected through the vacuum window. The coating is sensitive to wavelengths in the range 80-300 nm, while the photodiode is only sensitive to wavelengths below 120 nm. In argon the VUV emissions are primarily produced by spontaneous decay from 3p5 4 s resonance levels (1s2,1s4) and may be reabsorbed by ground state atoms. Real-time resonance level concentrations were measured and used to predict the VUV photon flux at the detector for a range of different ICP pressures, powers, and for various admixtures of Ar with N2, and H2. This work was supported in part by NSF grant PHY-1068670.

Analysis of four dental alloys following torch/centrifugal and induction/ vacuum-pressure casting procedures.

PubMed

Thompson, Geoffrey A; Luo, Qing; Hefti, Arthur

2013-12-01

Previous studies have shown casting methodology to influence the as-cast properties of dental casting alloys. It is important to consider clinically important mechanical properties so that the influence of casting can be clarified. The purpose of this study was to evaluate how torch/centrifugal and inductively cast and vacuum-pressure casting machines may affect the castability, microhardness, chemical composition, and microstructure of 2 high noble, 1 noble, and 1 base metal dental casting alloys. Two commonly used methods for casting were selected for comparison: torch/centrifugal casting and inductively heated/ vacuum-pressure casting. One hundred and twenty castability patterns were fabricated and divided into 8 groups. Four groups were torch/centrifugally cast in Olympia (O), Jelenko O (JO), Genesis II (G), and Liberty (L) alloys. Similarly, 4 groups were cast in O, JO, G, and L by an inductively induction/vacuum-pressure casting machine. Each specimen was evaluated for casting completeness to determine a castability value, while porosity was determined by standard x-ray techniques. Each group was metallographically prepared for further evaluation that included chemical composition, Vickers microhardness, and grain analysis of microstructure. Two-way ANOVA was used to determine significant differences among the main effects. Statistically significant effects were examined further with the Tukey HSD procedure for multiple comparisons. Data obtained from the castability experiments were non-normal and the variances were unequal. They were analyzed statistically with the Kruskal-Wallis rank sum test. Significant results were further investigated statistically with the Steel-Dwass method for multiple comparisons (α=.05). The alloy type had a significant effect on surface microhardness (P<.001). In contrast, the technique used for casting did not affect the microhardness of the test specimen (P=.465). Similarly, the interaction between the alloy and casting

Control of vacuum induction brazing system for sealing of instrumentation feed-through

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sung Ho Ahn; Jintae Hong; Chang Young Joung

2015-07-01

The integrity of instrumentation cables is an important performance parameter in addition to the sealing performance in the brazing process. An accurate brazing control was developed for the brazing of the instrumentation feed-through in the vacuum induction brazing system in this paper. The experimental results show that the accurate brazing temperature control performance is achieved by the developed control scheme. Consequently, the sealing performances of the instrumentation feed-through and the integrities of the instrumentation cables were satisfied after brazing. (authors)

Sulfur in vacuum - Sublimation effects on frozen melts, and applications to Io's surface and torus

NASA Astrophysics Data System (ADS)

Nash, D. B.

1987-10-01

The author has found from laboratory experiments that vacuum sublimation has a profound effect on the molecular composition, microtexture, bulk density (porosity), and the UV/visible spectral reflectance of the surface of solid sulfur samples, both when the sulfur is in the form of frozen or quenched melts and as laboratory-grade sulfur powder. These sublimation effects produce a unique surface material, the understanding of which may have important implications for deciphering the many enigmatic optical and textural properties of the surface of Jupiter's satellite Io. This planetary body is thought to have a surface greatly enriched in volcanically produced elemental sulfur and sulfur compounds and to have a surface atmospheric pressure with an upper limit of ≡10-7atm, comparable to a good laboratory vacuum, and surface hotspots at temperatures of about 300K covering about 0.3% of its global surface.

Induction heating pure vapor source of high temperature melting point materials on electron cyclotron resonance ion source.

PubMed

Kutsumi, Osamu; Kato, Yushi; Matsui, Yuuki; Kitagawa, Atsushi; Muramatsu, Masayuki; Uchida, Takashi; Yoshida, Yoshikazu; Sato, Fuminobu; Iida, Toshiyuki

2010-02-01

Multicharged ions that are needed are produced from solid pure material with high melting point in an electron cyclotron resonance ion source. We develop an evaporator by using induction heating (IH) with multilayer induction coil, which is made from bare molybdenum or tungsten wire without water cooling and surrounding the pure vaporized material. We optimize the shapes of induction coil and vaporized materials and operation of rf power supply. We conduct experiment to investigate the reproducibility and stability in the operation and heating efficiency. IH evaporator produces pure material vapor because materials directly heated by eddy currents have no contact with insulated materials, which are usually impurity gas sources. The power and the frequency of the induction currents range from 100 to 900 W and from 48 to 23 kHz, respectively. The working pressure is about 10(-4)-10(-3) Pa. We measure the temperature of the vaporized materials with different shapes, and compare them with the result of modeling. We estimate the efficiency of the IH vapor source. We are aiming at the evaporator's higher melting point material than that of iron.

Induction heating pure vapor source of high temperature melting point materials on electron cyclotron resonance ion sourcea)

NASA Astrophysics Data System (ADS)

Kutsumi, Osamu; Kato, Yushi; Matsui, Yuuki; Kitagawa, Atsushi; Muramatsu, Masayuki; Uchida, Takashi; Yoshida, Yoshikazu; Sato, Fuminobu; Iida, Toshiyuki

2010-02-01

Multicharged ions that are needed are produced from solid pure material with high melting point in an electron cyclotron resonance ion source. We develop an evaporator by using induction heating (IH) with multilayer induction coil, which is made from bare molybdenum or tungsten wire without water cooling and surrounding the pure vaporized material. We optimize the shapes of induction coil and vaporized materials and operation of rf power supply. We conduct experiment to investigate the reproducibility and stability in the operation and heating efficiency. IH evaporator produces pure material vapor because materials directly heated by eddy currents have no contact with insulated materials, which are usually impurity gas sources. The power and the frequency of the induction currents range from 100to900W and from 48to23kHz, respectively. The working pressure is about 10-4-10-3Pa. We measure the temperature of the vaporized materials with different shapes, and compare them with the result of modeling. We estimate the efficiency of the IH vapor source. We are aiming at the evaporator's higher melting point material than that of iron.

Inductance Jump at Melting of Vortex Lattice in Untwinned YBaCuO

NASA Astrophysics Data System (ADS)

Matl, P.; Wu, H.; Ong, N. P.; Gagnon, R.; Taillefer, L.

1997-03-01

We have measured the complex resistivity in an untwinned single crystal YBaCuO between 70K and 120K at a fixed magnetic field. As T increases towards the melting temperature Tm the inductance increases rapidly. At Tm the inductance undergoes a discontinuous jump, which we correlate with the collapse of the shear modulus c_66. We describe how the magnitude of the jump varies with temperature, field, and frequency. We have also extracted the viscosity of the vortex lattice from a Bardeen-Stephen fit to the low field complex resistivity measured at 1 to 15 MHz between 80K and T_c. We find that the viscosity decreases as 1.2x10-13 kg m-1 s-1 K-1 as the temperature approaches T_c.

Kinetics of the melting front movement in process of centrifugal induction surfacing of powder material with nanoscale modificaters

NASA Astrophysics Data System (ADS)

Sasnouski, I.; Kurylionak, A.

2018-03-01

For solving the problem of improving the powder coatings modified by nanostructure components obtained by induction surfacing method tribological characteristics it is necessary to study the kinetics of the powdered layer melting and define the minimum time of melting. For powdered layer predetermined temperature maintenance at sintering mode stage it is required to determine the temperature difference through blank thickness of the for one hundred-day of the define the warm-up swing on of the stocking up by solving the thermal conductivity stationary problem for quill (hollow) cylinder with internal heat source. Herewith, since in practice thickness of the cylinder wall is much less then its diameter and the temperature difference is comparatively small, the thermal conductivity dependence upon the temperature can be treated as negligible. As it was shown by our previous studies, in the induction heating process under powdered material centrifugal surfacing (i.e. before achieving the melting temperature) the temperature distribution in powdered layer thickness may be considered even. Hereinafter, considering the blank part induction heating process quasi-stationarity under Fo big values, it is possible to consider its internal surface heating as developing with constant velocity. As a result of development the melting front movement mathematical model in a powdered material with nanostructure modifiers the minimum surfacing time is defined. It allows to minimize negative impact of thermal influence on formation of applied coating structure, to raise productivity of the process, to lower power inputs and to ensure saving of nonferrous and high alloys by reducing the allowance for machining. The difference of developed mathematical model of melting front movement from previously known is that the surface temperature from which the heat transfer occures is a variable and varies with a time after the linear law.

Numerical investigation of melting and solidification processes in modified surface layers of metal at induction heating

NASA Astrophysics Data System (ADS)

Shchukin, V. G.; Popov, V. N.

2017-10-01

One of the perspective ways to improve the operational properties of parts of machines during induction treatment of their surfaces is the modification of the melt by specially prepared nanoscale particles of refractory compounds (carbides, nitrides, carbonitrides, etc.). This approach allows us to increase the number of crystallization centers and to refine the structural components of the solidified metal. The resulting high dispersity and homogeneity of crystalline grains favorably affect the quality of the treated surfaces. 3D numerical simulation of thermophysical processes in the modification of the surface layer of metal in a moving substrate was carried out. It is assumed that the surface of the substrate is covered with a layer of specially prepared nanoscale particles of a refractory compound, which, upon penetration into the melt, are uniformly distributed in it. The possibility of applying a high-frequency electromagnetic field of high power for heating and melting of a metal (iron) for the purpose of its subsequent modification is investigated. The distribution of electromagnetic energy in the metal is described by empirical formulas. Melting of the metal is considered in the Stefan approximation, and upon solidification it is assumed that all nanoparticles serve as centers for volume-sequential crystallization. Calculations were carried out with the following parameters: specific power p0 = 35 and 40 kW/cm2 at frequency f = 440 and 1200 kHz, the substrate velocity V = 0.5-2.5 cm/s, the nanoparticles' size is 50 nm and concentration Np = 2.0 . 109 cm-3. Based on the results obtained in a quasi-stationary formulation, the distribution of the temperature field, the dimensions of the melting and crystallization zones, the change in the solid fraction in the two-phase zone, the area of the treated substrate surface, depending on the speed of its movement and induction heating characteristics were estimated.

[Laser-induced breakdown spectroscopy system for elements analysis in high-temperature and vacuum environment].

PubMed

Pan, Cong-Yuan; Du, Xue-Wei; An, Ning; Han, Zhen-Yu; Wang, Sheng-Bo; Wei, Wei; Wang, Qiu-Ping

2013-12-01

Laser-induced breakdown spectroscopy (LIBS) is one of the most promising technologies to be applied to metallurgical composition online monitoring in these days. In order to study the spectral characters of LIBS spectrum and to investigate the quantitative analysis method of material composition under vacuum and high temperature environment, a LIBS measurement system was designed and set up which can be used for conducting experiments with high-temperature or molten samples in different vacuum environment. The system consists of a Q-switched Nd : YAG laser used as the light source, lens with different focus lengths used for laser focusing and spectrum signal collecting, a spectrometer used for detecting the signal of LIBS spectrums, and a vacuum system for holding and heating the samples while supplying a vacuum environment. The vacuum was achieved and maintained by a vacuum pump and an electric induction furnace was used for heating the system. The induction coil was integrated to the vacuum system by attaching to a ceramic sealing flange. The system was installed and testified, and the results indicate that the vacuum of the system can reach 1X 10(-4) Pa without heating, while the heating temperature could be about 1 600 degreeC, the system can be used for melting metal samples such as steel and aluminum and get the LIBS spectrum of the samples at the same time. Utilizing this system, LIBS experiments were conducted using standard steel samples under different vacuum or high-temperature conditions. Results of comparison between LIBS spectrums of solid steel samples under different vacuum were achieved, and so are the spectrums of molten and solid steel samples under vacuum environment. Through data processing and theoretical analyzing of these spectrums, the initial results of those experiments are in good agreement with the results that are presently reported, which indicates that the whole system functions well and is available for molten metal LIBS experiment

Dephosphorization of complexly alloyed nickel melts under vacuum induction melting conditions: II. Experimental results and their interpretation

NASA Astrophysics Data System (ADS)

Burtsev, V. T.; Anuchkin, S. N.; Sidorov, V. V.; Rigin, V. E.

2013-05-01

The activities of the components of BaO-BaF2-BaCl2-NiO and CaO-CaF2-CaCl2-NiO slags systems, which were considered as a phase having a collective electron system, are calculated, and it is shown that the barium, calcium, and oxygen activities at 1600°C are maximal in the BaO- and CaO-based systems depending on the main oxide content. The dephosphorization of three types of nickel-based melts by slags of 14 compositions in crucibles made of Al2O3, MgO, and MgO-Al2O3 (80-20 wt %) is experimentally studied, and the degree of dephosphorization is shown to depend on the phosphorus content in a metal, the slag composition, and the crucible material (degree of dephosphorization is maximal in Al2O3 crucibles). The forming slag is assimilated by Al2O3 and MgO-Al2O3 ceramics with a porosity of about 30%. If 4-10 wt % NiO are present in a slag, the wettability of the Al2O3 ceramic is significantly higher than that of the MgO-based ceramic.

Research on Melt Degassing Processes of High Conductivity Hard Drawn Aluminum Wire

NASA Astrophysics Data System (ADS)

Xu, Xuexia; Feng, Yanting; Wang, Qing; Li, Wenbin; Fan, Hui; Wang, Yong; Li, Guowei; Zhang, Daoqian

2018-03-01

Degassing effects of ultrasonic and vacuum processes on high conductivity hard drawn aluminum melt were studied. Results showed that the degassing efficiency improved with the increase of ultrasonic power within certain range, stabilizing at 70% with 240W. For vacuum degassing process, hydrogen content of aluminum melt decreased with the loading time and was linear with logarithm of vacuum degree. Comparison of degassing effects of ultrasonic, vacuum, vacuum-ultrasonic degassing process showed that vacuum-ultrasonic process presented optimal effect.

Influence of melting and casting methods and finish line design on the marginal discrepancy of nickel-chromium-titanium alloy crowns.

PubMed

Cogolludo, Pablo G; Suarez, María J; Peláez, Jesús; Lozano, José F L

2010-01-01

The aim of this study was to analyze the influence of melting and casting procedures and the cervical finish line design on the marginal fit of nickel-chromium-titanium alloy crowns. Sixty standardized specimens were prepared to receive metal-ceramic crowns and were divided into two groups according to the cervical finish line: chamfer or rounded shoulder. Three melting and casting procedures were analyzed: (1) induction-centrifuge (IC), (2) gas oxygen torch-centrifuge (TC), and (3) induction-vacuum/pressure (IP). The marginal fit was measured with an image analysis system. Significant differences (P =.005) were observed among the groups, with TC showing the lowest discrepancies (45.87 μm). No significant differences were observed between the two finish lines. The accuracy of fit achieved for the groups analyzed may be regarded as within the range of clinical acceptance.

Comparative microstructural and corrosion development of VCrNiCoFeCu equiatomic multicomponent alloy produced by induction melting and spark plasma sintering

NASA Astrophysics Data System (ADS)

Fazakas, É.; Heczel, A.; Molnár, D.; Varga, B.; Zadorozhnyy, V.; Vida, Á.

2018-03-01

The present study focuses on the corrosion behavior of a single-phase FCC high entropy alloy (VCrNiCoFeCu) casted by two different methods: induction melting and spark plasma sintering. The corrosion resistance has been evaluated using immersion tests in 3.5% NaCl solution, the potentiodynamic polarization measurements and the results are compared how is dependent the corrosion rate as a function of the production methods. Our results show that induction melted sample is stable in salty environment. On the other hand, based on the changes of polarization curves, there must be an evolution of oxide films on the SPSed sample until reaching the stable oxide layer.

Purifying Aluminum by Vacuum Distillation

NASA Technical Reports Server (NTRS)

Du Fresne, E. R.

1985-01-01

Proposed method for purifying aluminum employs one-step vacuum distillation. Raw material for process impure aluminum produced in electrolysis of aluminum ore. Impure metal melted in vacuum. Since aluminum has much higher vapor pressure than other constituents, boils off and condenses on nearby cold surfaces in proportions much greater than those of other constituents.

Laser Vacuum Furnace for Zone Refining

NASA Technical Reports Server (NTRS)

Griner, D. B.; Zurburg, F. W.; Penn, W. M.

1986-01-01

Laser beam scanned to produce moving melt zone. Experimental laser vacuum furnace scans crystalline wafer with high-power CO2-laser beam to generate precise melt zone with precise control of temperature gradients around zone. Intended for zone refining of silicon or other semiconductors in low gravity, apparatus used in normal gravity.

Simulation results of influence of constricted arc column on anode deformation and melting pool swirl in vacuum arcs with AMF contacts

NASA Astrophysics Data System (ADS)

Wang, Lijun; Zhang, Xiao; Huang, Xiaolong; Jia, Shenli

2017-11-01

In the process of vacuum arc breaking, the energy injected into the anode will cause anode melting, evaporation, and deformation, resulting in the formation of the anode melting pool. The anode activities have great influence on the arc behavior. When the arc current is large enough, even the influence of axial magnetic field is considered, the arc column still is in contraction state, which means the arc burns only on a part of the electrode. In this paper, the model of anode melting pool deformation and rotation is used, and the model includes anode melting and solidification module, magneto-hydro-dynamic module of the anode melting pool, the volume of fraction method, and the current continuity equation. In this paper, the diffuse arc area is selected as 100%, 75%, and 50%, respectively. The anode temperature and deformation, the anode melting layer thickness, and the rotational velocity of the anode melting pool are obtained. The results show that when the current is at 17.5 kA (rms) and the diffuse arc area is 100%, the anode's maximum temperature is 1477 K and the crater depth is 0.83 mm. But when the diffuse arc areas are 75% and 50%, the anode's maximum temperatures reach 1500 K and 1761 K, and the crater depths reach 1.2 mm and 3 mm, respectively. Arc contraction will lead to more serious anode deformation. A similar result is obtained when the simulation current is 12.5 kA. Under the similar situation, the simulation results in the crater depth, the residual melt layer thickness, the rotational speed of the melting pool, and the maximum temperature of the anode at current zero are in good agreement with the experimental results.

DWPF Melt Cell Crawler

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ward, C.R.

2003-04-08

On December 2, 2002, Remote and Specialty Equipment Systems (RSES) of the Savannah River Technology Center (SRTC) was requested to build a remotely operated crawler to assist in cleaning the Defense Waste Processing Facility (DWPF) melt cell floor of glass, tools, and other debris. The crawler was to assist a grapple and vacuum system in cleaning the cell. The crawler was designed to push glass and debris into piles so that the grapple could pick up the material and place it in waste bins. The crawler was also designed to maneuver the end of the vacuum hose, if needed. Inmore » addition, the crawler was designed to clean the area beneath the cell worktable that was inaccessible to the grapple and vacuum system. Originally, the system was to be ready for deployment by December 17. The date was moved up to December 12 to better utilize the available time for clean up. The crawler was designed and built in 10 days and completed cleaning the melt cell in 8 days. Due to initial problems with the grapple and vacuum system, the crawler completed essentially all of the cleanup tasks by itself. The crawler also cleaned an area on the west side of the cell that was not initially slated for cleaning.« less

Solubility of Nitrogen in Superaustenitic Stainless Steels During Air Induction Melting

NASA Astrophysics Data System (ADS)

Chandrasekar, A.; Anburaj, J.; Narayanan, R.; Balusamy, V.; Mohamed Nazirudeen, S. S.

2013-04-01

The amount of nitrogen contained in super austenitic stainless steels (SASS) influences their properties significantly. The effect of maximum amount of nitrogen in the highly alloyed Cr and Ni SASS containing further additions of Mo and Mn is studied. The calculated nitrogen contents of the experimental alloys are compared with the actual nitrogen contents obtained in the alloys produced using induction melting furnace. The actual nitrogen content of the alloys is always lower than the calculated value, and this discrepancy is due to the presence of positive interaction parameters of Ni, Cu, and Si in the alloy. However, the yield of nitrogen in the liquid SASS is improved significantly with additions of Mn and Mo contents. The construction of multicomponent phase diagrams for SASS is demonstrated using Thermo-Calc software. SASS containing more nitrogen exhibited a very high strength without loss of toughness.

Rolling-element fatigue life of AMS 5749 corrosion resistant, high temperature bearing steel

NASA Technical Reports Server (NTRS)

Parker, R. J.; Hodder, R. S.

1977-01-01

The rolling element fatigue lives of AMS 5749 and AISI M-50 were compared in tests run in the five ball fatigue tester and the rolling contact fatigue tester. The effects of double vacuum melting and retained austenite on the life of AMS 5749 were determined in five ball fatigue tests. The double vacuum melting process consisted of induction vacuum melting followed by vacuum arc remelting (VIM-VAR). In the five ball tests, VIM-VAR AMS 5749 gave lives at least six times that of VIM-VAR AISI M-50. Similar tests in the rolling contact fatigue tester showed no significant difference in the lives of the two materials. The rolling element fatigue life of VIM-VAR AMS 5749 was at least 14 times that of vacuum induction melted AMS 5749. A trend toward increased rolling element fatigue life with decreased retained austenite is apparent, but the confidence that all experimental differences are significant is not great.

Hot melt adhesive attachment pad

NASA Technical Reports Server (NTRS)

Fox, R. L.; Frizzill, A. W.; Little, B. D.; Progar, D. J.; Coultrip, R. H.; Couch, R. H.; Gleason, J. R.; Stein, B. A.; Buckley, J. D.; St.clair, T. L. (Inventor)

1984-01-01

A hot melt adhesive attachment pad for releasably securing distinct elements together is described which is particularly useful in the construction industry or a spatial vacuum environment. The attachment pad consists primarily of a cloth selectively impregnated with a charge of hot melt adhesive, a thermo-foil heater, and a thermo-cooler. These components are securely mounted in a mounting assembly. In operation, the operator activates the heating cycle transforming the hot melt adhesive to a substantially liquid state, positions the pad against the attachment surface, and activates the cooling cycle solidifying the adhesive and forming a strong, releasable bond.

Vacuum Powder Injector

NASA Technical Reports Server (NTRS)

Working, Dennis C.

1991-01-01

Method developed to provide uniform impregnation of bundles of carbon-fiber tow with low-solubility, high-melt-flow polymer powder materials to produce composite prepregs. Vacuum powder injector expands bundle of fiber tow, applies polymer to it, then compresses bundle to hold powder. System provides for control of amount of polymer on bundle. Crystallinity of polymer maintained by controlled melt on takeup system. All powder entrapped, and most collected for reuse. Process provides inexpensive and efficient method for making composite materials. Allows for coating of any bundle of fine fibers with powders. Shows high potential for making prepregs of improved materials and for preparation of high-temperature, high-modulus, reinforced thermoplastics.

The judgment of the All-melted-moment during using electron beam melting equipment to purify silicon

NASA Astrophysics Data System (ADS)

Han, Xiaojie; Meng, Jianxiong; Wang, Shuaiye; Jiang, Tonghao; Wang, Feng; Tan, Yi; Jiang, Dachuan

2017-06-01

Experiment has proved that the rate of impurity removal depends on the pressure and the temperature of the vacuum chamber during using electron beam to smelt silicon, and the amount of removed-impurity depends on time when other conditions are the same. In the actual production process, smelting time is a decisive factor of impurity removal amount while pressure and temperature of the vacuum chamber is certain due to a certain melting power. To avoiding the influence of human control and improving the quality of production, thinking of using cooling water temperature to estimate the state of material during metal smelting is considered. We try to use the change of cooling water temperature to judge that when silicon is all melted and to evaluate the effectiveness of this method.

Effect of Reduced Flux Iron Ore Pellets on Removal of Impurities from Pig Iron During Induction Melting: A New Phenomenon

NASA Astrophysics Data System (ADS)

Dishwar, Raj Kumar; Agrawal, Shavi; Mandal, A. K.; Mahobia, G. S.; Sinha, O. P.

2018-06-01

The present work represents a comparative study of impurity removal (sulfur, phosphorus, and carbon) from pig iron melt by the addition of lime powder and reduced fluxed iron ore pellets separately in a 5-kg-capacity induction melting furnace. Two types of reduced flux pellets (80% and 50%) of similar basicity ( 3.06) were charged separately into the pool to obtain the different oxidizing atmospheres of the bath. Results showed that the rate of impurity removal increases up to 6 min of exposure time and decreases afterward. Only lime powder charging, sulfur ( 77%), and a small fraction of carbon were removed from pig iron. Phosphorous ( 41%), sulfur ( 53%), and carbon ( 96%) were removed simultaneously when 80% reduced fluxed pellets were used. The present study indicates that the optimum removal of impurities is possible by charging 80% reduced flux iron ore pellets from the pig iron melt.

Vacuum Plasma Spraying Replaces Electrodeposition

NASA Technical Reports Server (NTRS)

Holmes, Richard R.; Power, Chris; Burns, David H.; Daniel, Ron; Mckechnie, Timothy N.

1992-01-01

Vacuum plasma spraying used to fabricate large parts with complicated contours and inner structures, without uninspectable welds. Reduces time, and expense of fabrication. Wall of combustion chamber built up inside of outer nickel-alloy jacket by plasma spraying. Particles of metal sprayed partially melted in plasma gun and thrown at supersonic speed toward deposition surface. Vacuum plasma-spray produces stronger bond between the grooves and covering layer completing channels and wall of combustion chamber. In tests, bond withstood pressure of 20 kpsi, three times allowable limit by old method.

A versatile approach to vacuum injection casting for materials research and development.

PubMed

Xu, Donghua; Xu, Yifan

2017-03-01

Vacuum injection casting (VIC) is important for research and development (R&D) of materials that are prone to oxidation at high temperatures, particularly metals and metallic alloys (e.g., metallic glasses and high entropy alloys). VIC in R&D laboratories often involves initial melting/alloying in a prior step, transporting the sample to a dedicated vacuum chamber, re-melting the sample in a quartz tube, and finally injecting the melt with an inert gas to a dedicated mold. Here we present a new approach to laboratory VIC that requires no sample transfer (for a variety of materials), no dedicated vacuum chamber/space nor dedicated mold, and hence provides more versatility and higher efficiency and yet lowers the capital equipment cost. Our approach takes advantage of the exceptional portability, thermal and chemical stability, and thermoplastic processability of quartz glass and uses quartz tubes for all the melting, re-melting, injection casting, and molding. In addition, our approach includes oxygen gettering to remove residual oxygen for all the steps and allows for slow or fast cooling (e.g., water quenching) upon injection. This paper focuses on the design, the procedures, and the versatile features of this new approach while also demonstrating the practical implementation of this approach and computational modeling of the heat transfer and the cooling rates for two exemplary cases. The new approach is expected to bring notable expedition to sample fabrication and materials discovery, as well as wider adoption of vacuum injection casting in materials science and condensed matter physics research laboratories.

A versatile approach to vacuum injection casting for materials research and development

NASA Astrophysics Data System (ADS)

Xu, Donghua; Xu, Yifan

2017-03-01

Vacuum injection casting (VIC) is important for research and development (R&D) of materials that are prone to oxidation at high temperatures, particularly metals and metallic alloys (e.g., metallic glasses and high entropy alloys). VIC in R&D laboratories often involves initial melting/alloying in a prior step, transporting the sample to a dedicated vacuum chamber, re-melting the sample in a quartz tube, and finally injecting the melt with an inert gas to a dedicated mold. Here we present a new approach to laboratory VIC that requires no sample transfer (for a variety of materials), no dedicated vacuum chamber/space nor dedicated mold, and hence provides more versatility and higher efficiency and yet lowers the capital equipment cost. Our approach takes advantage of the exceptional portability, thermal and chemical stability, and thermoplastic processability of quartz glass and uses quartz tubes for all the melting, re-melting, injection casting, and molding. In addition, our approach includes oxygen gettering to remove residual oxygen for all the steps and allows for slow or fast cooling (e.g., water quenching) upon injection. This paper focuses on the design, the procedures, and the versatile features of this new approach while also demonstrating the practical implementation of this approach and computational modeling of the heat transfer and the cooling rates for two exemplary cases. The new approach is expected to bring notable expedition to sample fabrication and materials discovery, as well as wider adoption of vacuum injection casting in materials science and condensed matter physics research laboratories.

Using laser-induced breakdown spectroscopy on vacuum alloys-production process for elements concentration analysis

NASA Astrophysics Data System (ADS)

Zhao, Tianzhuo; Fan, Zhongwei; Lian, Fuqiang; Liu, Yang; Lin, Weiran; Mo, Zeqiang; Nie, Shuzhen; Wang, Pu; Xiao, Hong; Li, Xin; Zhong, Qixiu; Zhang, Hongbo

2017-11-01

Laser-induced breakdown spectroscopy (LIBS) utilizing an echelle spectrograph-ICCD system is employed for on-line analysis of elements concentration in a vacuum induction melting workshop. Active temperature stabilization of echelle spectrometer is implemented specially for industrial environment applications. The measurement precision is further improved by monitoring laser parameters, such as pulse energy, spatial and temporal profiles, in real time, and post-selecting laser pulses with specific pulse energies. Experimental results show that major components of nickel-based alloys are stable, and can be well detected. By using internal standard method, calibration curves for chromium and aluminum are obtained for quantitative determination, with determination coefficient (relative standard deviation) to be 0.9559 (< 2.2%) and 0.9723 (< 2.8%), respectively.

Radioactive scrap metal decontamination technology assessment report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Buckentin, J.M.; Damkroger, B.K.; Schlienger, M.E.

1996-04-01

Within the DOE complex there exists a tremendous quantity of radioactive scrap metal. As an example, it is estimated that within the gaseous diffusion plants there exists in excess of 700,000 tons of contaminated stainless steel. At present, valuable material is being disposed of when it could be converted into a high quality product. Liquid metal processing represents a true recycling opportunity for this material. By applying the primary production processes towards the material`s decontamination and re-use, the value of the strategic resource is maintained while drastically reducing the volume of material in need of burial. Potential processes for themore » liquid metal decontamination of radioactively contaminated metal are discussed and contrasted. Opportunities and technology development issues are identified and discussed. The processes compared are: surface decontamination; size reduction, packaging and burial; melting technologies; electric arc melting; plasma arc centrifugal treatment; air induction melting; vacuum induction melting; and vacuum induction melting and electroslag remelting.« less

Silicon crystal growth in vacuum

NASA Technical Reports Server (NTRS)

Khattak, C. P.; Schmid, F.

1982-01-01

The most developed process for silicon crystal growth is the Czochralski (CZ) method which was in production for over two decades. In an effort to reduce cost of single crystal silicon for photovoltaic applications, a directional solidification technique, Heat Exchanger Method (HEM), was adapted. Materials used in HEM and CZ furnaces are quite similar (heaters, crucibles, insulation, etc.). To eliminate the cost of high purity argon, it was intended to use vacuum operation in HEM. Two of the major problems encountered in vacuum processing of silicon are crucible decomposition and silicon carbide formation in the melt.

Thermal sprayed composite melt containment tubular component and method of making same

DOEpatents

Besser, Matthew F.; Terpstra, Robert L.; Sordelet, Daniel J.; Anderson, Iver E.

2002-03-19

A tubular thermal sprayed melt containment component for transient containment of molten metal or alloy wherein the tubular member includes a thermal sprayed inner melt-contacting layer for contacting molten metal or alloy to be processed, a thermal sprayed heat-generating layer deposited on the inner layer, and an optional thermal sprayed outer thermal insulating layer. The thermal sprayed heat-generating layer is inductively heated as a susceptor of an induction field or electrical resistively heated by passing electrical current therethrough. The tubular thermal sprayed melt containment component can comprise an elongated melt pour tube of a gas atomization apparatus where the melt pour tube supplies molten material from a crucible to an underlying melt atomization nozzle.

SiO(x) nanoparticles synthesized by an evaporation and condensation process using induction melting of silicon and gas injection.

PubMed

Jang, Bo Yun; Lee, Jin Seok; Kim, Joon Soo

2013-05-01

SiO(x) nanoparticles were synthesized using a specially designed induction melting system equipped with a segmented graphite crucible. The graphite crucible with the segmented wall was the key to enhancing the evaporation rate due to the increase of the evaporation area and convection of the silicon melt. Injection of the gas mixture of oxygen (O2) and argon (Ar) on silicon (Si) melt caused the formation of SiO(x) nanoparticles. The evaporated SiO(x) nanoparticles were then cooled and condensed in a process chamber. The effects of the O2/Ar ratio in the injection gas on the microstructures of the SiO(x) nanoparticles were then investigated. Synthesized SiO(x) nanoparticles were proven to be of a homogeneous amorphous phase with average diameters of 30-35 nm. The microstructures were independent from the O2/Ar ratio of the injected gas. However, x increased from 1.36 to 1.84 as the O2/Ar ratio increased. The purity of the synthesized nanoparticles was about 99.9%. SiO(x) nanoparticles could be applied as the active anode material in a lithium (Li) ion secondary battery.

Recycling of waste lead storage battery by vacuum methods.

PubMed

Lin, Deqiang; Qiu, Keqiang

2011-07-01

Waste lead storage battery is the most important recyclable lead material not only in various European and other OECD countries but also in China. Pollution control of lead has become the focus of people's attention in the world. A vacuum process for recycling waste lead storage battery was developed in this work. The experimental results showed that all the valuable materials in waste lead storage battery could be satisfactorily recycled by vacuum technologies. The vacuum melting of lead grids and the vacuum reduction of lead pastes produce the lead bullion with the direct recovery ratio of 96.29% and 98.98%, respectively. The vacuum pyrolysis of plastics can produce pyrolysis oil with yield of more than 93 wt.%. These vacuum recycling technologies offer improvements in metallurgical and environmental performance. Copyright © 2011 Elsevier Ltd. All rights reserved.

Special features of changes in the structure and mechanical properties of oxygen-free pure and yttrium-alloyed copper after vacuum induction remelting

NASA Astrophysics Data System (ADS)

Kamyshanchenko, N. V.; Galtsev, A. V.; Durykhin, M. I.; Neklyudov, I. M.; Borts, B. V.; Shevchenko, S. V.

2011-03-01

Properties of oxygen-free copper with a microadditive of yttrium and without it are studied after vacuum induction remelting. The ingots are subjected to intense hot pressing and subsequent rolling to various degrees of reduction. The effects of the annealing temperature on the structure and of the anisotropy of the structure on the strength properties of the copper are determined. The properties of copper with an additive of yttrium and without it are compared.

Microstructure and magnetism of Co2FeAl Heusler alloy prepared by arc and induction melting compared with planar flow casting

NASA Astrophysics Data System (ADS)

Titov, A.; Jiraskova, Y.; Zivotsky, O.; Bursik, J.; Janickovic, D.

2018-04-01

This paper is devoted to investigations of the structural and magnetic properties of the Co2FeAl Heusler alloy produced by three technologies. The alloys prepared by arc and induction melting have resulted in coarse-grained samples in contrast to the fine-grained ribbon-type sample prepared by planar flow casting. Scanning electron microscopy completed by energy dispersive X-ray spectroscopy, X-ray diffraction, Mössbauer spectroscopy, and magnetic methods sensitive to both bulk and surface were applied. The chemical composition was slightly different from the nominal only for the ribbon sample. From the viewpoint of magnetic properties, the bulk coercivity and remnant magnetization have followed the structure influenced by the technology used. Saturation magnetization was practically the same for samples prepared by arc and induction melting, whereas the magnetization of ribbon is slightly lower due to a higher Al content at the expense of iron and cobalt. The surface magnetic properties were markedly influenced by anisotropy, grain size, and surface roughness of the samples. The surface roughness and brittleness of the ribbon-type sample did not make domain structure observation possible. The other two samples could be well polished and their highly smooth surface has enabled domain structure visualization by both magneto-optical Kerr microscopy and magnetic force microscopy.

Proceedings of the twenty sixth international symposium on discharges and electrical insulation in vacuum. V. 2

DOE Office of Scientific and Technical Information (OSTI.GOV)

NONE

2014-07-01

Vacuum science and technology has made vital contributions in high technology areas like space, high energy particle accelerators, plasma devices, pulse power, electronics, vacuum interrupters, thin films, melting and refining of metals/alloys, extraction and processing of advanced materials. Vacuum discharges, vacuum arc physics and technology and various applications towards vacuum interrupters, pulse power and particle accelerator are the main themes for this symposium. Papers relevant to INIS are indexed separately.

Proceedings of the twenty sixth international symposium on discharges and electrical insulation in vacuum. V. 1

DOE Office of Scientific and Technical Information (OSTI.GOV)

NONE

2014-07-01

Vacuum science and technology has made vital contributions in high technology areas like space, high energy particle accelerators, plasma devices, pulse power, electronics, vacuum interrupters, thin films, melting and refining of metals/alloys, extraction and processing of advanced materials. Vacuum discharges, vacuum arc physics and technology and various applications towards vacuum interrupters, pulse power and particle accelerator are the main themes for this symposium. Papers relevant to INIS are indexed separately.

Cold-Worked Inconel(R) 718 Bars

NASA Technical Reports Server (NTRS)

Montano, J. W.

1988-01-01

Cold working and double aging yield high strength without sacrifice of resistance to corrosion. Report presents data on mechanical properties and stress-corrosion resistance of triple-melted, solution-treated, work-strengthened, direct-double-aged Inconel(R) 718 alloy. Triple melting consists of vacuum induction melting, electro-slag remelting, and vacuum arm remelting. Data indicate advance in processing of large-diameter bars. New process increases yield strength without reducing the elongation, reduction of area, and grain size.

Linear induction accelerator

DOEpatents

Buttram, M.T.; Ginn, J.W.

1988-06-21

A linear induction accelerator includes a plurality of adder cavities arranged in a series and provided in a structure which is evacuated so that a vacuum inductance is provided between each adder cavity and the structure. An energy storage system for the adder cavities includes a pulsed current source and a respective plurality of bipolar converting networks connected thereto. The bipolar high-voltage, high-repetition-rate square pulse train sets and resets the cavities. 4 figs.

Collapse of the vortex-lattice inductance and shear modulus at the melting transition in untwinned YBa2Cu3O7

NASA Astrophysics Data System (ADS)

Matl, Peter; Ong, N. P.; Gagnon, R.; Taillefer, L.

2002-06-01

The complex resistivity ρ^(ω) of the vortex lattice in an untwinned crystal of 93-K YBa2Cu3O7 has been measured at frequencies ω/2π from 100 kHz to 20 MHz in a 2-T field H||c, using a four-probe rf transmission technique that enables continuous measurements versus ω and temperature T. As T is increased, the inductance Ls(ω)=Imρ^(ω)/ω increases steeply to a cusp at the melting temperature Tm, and then undergoes a steep collapse consistent with vanishing of the shear modulus c66. We discuss in detail the separation of the vortex-lattice inductance from the ``volume'' inductance, and other skin-depth effects. To analyze the spectra, we consider a weakly disordered lattice with a low pin density. Close fits are obtained to ρ1(ω) over 2 decades in ω. Values of the pinning parameter κ and shear modulus c66 obtained show that c66 collapses by over 4 decades at Tm, whereas κ remains finite.

Plates for vacuum thermal fusion

DOEpatents

Davidson, James C.; Balch, Joseph W.

2002-01-01

A process for effectively bonding arbitrary size or shape substrates. The process incorporates vacuum pull down techniques to ensure uniform surface contact during the bonding process. The essence of the process for bonding substrates, such as glass, plastic, or alloys, etc., which have a moderate melting point with a gradual softening point curve, involves the application of an active vacuum source to evacuate interstices between the substrates while at the same time providing a positive force to hold the parts to be bonded in contact. This enables increasing the temperature of the bonding process to ensure that the softening point has been reached and small void areas are filled and come in contact with the opposing substrate. The process is most effective where at least one of the two plates or substrates contain channels or grooves that can be used to apply vacuum between the plates or substrates during the thermal bonding cycle. Also, it is beneficial to provide a vacuum groove or channel near the perimeter of the plates or substrates to ensure bonding of the perimeter of the plates or substrates and reduce the unbonded regions inside the interior region of the plates or substrates.

Welding/sealing glass-enclosed space in a vacuum

DOEpatents

Tracy, C.E.; Benson, D.K.

1996-02-06

A method of welding and sealing the edges of two juxtaposed glass sheets together to seal a vacuum space between the sheets comprises the steps of positioning a radiation absorbent material, such as FeO, VO{sub 2}, or NiO, between the radiation transmissive glass sheets adjacent the edges and then irradiating the absorbent material, preferably with a laser beam, through at least one of the glass sheets. Heat produced by the absorbed radiation in the absorbent material melts glass in the portions of both glass sheets that are adjacent the absorbent material, and the melted glass from both sheets flows together to create the weld when the melted glass cools and hardens. The absorbent material can be dissolved and diffused into the melted glass to the extent that it no longer absorbs enough energy to keep the glass melted, thus, with appropriate proportioning of absorbent material to source energy power and welding heat needed, the process can be made self-stopping. 8 figs.

Welding/sealing glass-enclosed space in a vacuum

DOEpatents

Tracy, C. Edwin; Benson, David K.

1996-01-01

A method of welding and sealing the edges of two juxtaposed glass sheets together to seal a vacuum space between the sheets comprises the steps of positioning a radiation absorbant material, such as FeO, VO.sub.2, or NiO, between the radiation transmissive glass sheets adjacent the edges and then irradiating the absorbant material, preferably with a laser beam, through at least one of the glass sheets. Heat produced by the absorbed radiation in the absorbant material melts glass in the portions of both glass sheets that are adjacent the absorbant material, and the melted glass from both sheets flows together to create the weld when the melted glass cools and hardens. The absorbant material can be dissolved and diffused into the melted glass to the extent that it no longer absorbs enough energy to keep the glass melted, thus, with appropriate proportioning of absorbant material to source energy power and welding heat needed, the process can be made self-stopping.

Method of correcting eddy current magnetic fields in particle accelerator vacuum chambers

DOEpatents

Danby, Gordon T.; Jackson, John W.

1991-01-01

A method for correcting magnetic field aberrations produced by eddy currents induced in a particle accelerator vacuum chamber housing is provided wherein correction windings are attached to selected positions on the housing and the windings are energized by transformer action from secondary coils, which coils are inductively coupled to the poles of electro-magnets that are powered to confine the charged particle beam within a desired orbit as the charged particles are accelerated through the vacuum chamber by a particle-driving rf field. The power inductively coupled to the secondary coils varies as a function of variations in the power supplied by the particle-accelerating rf field to a beam of particles accelerated through the vacuum chamber, so the current in the energized correction coils is effective to cancel eddy current flux fields that would otherwise be induced in the vacuum chamber by power variations in the particle beam.

Butt Welding Joint of Aluminum Alloy by Space GHTA Welding Process in Vacuum

NASA Astrophysics Data System (ADS)

Suita, Yoshikazu; Shinike, Shuhei; Ekuni, Tomohide; Terajima, Noboru; Tsukuda, Yoshiyuki; Imagawa, Kichiro

Aluminum alloys have been used widely in constructing various space structures including the International Space Station (ISS) and launch vehicles. For space applications, welding experiments on aluminum alloy were performed using the GHTA (Gas Hollow Tungsten Arc) welding process using a filler wire feeder in a vacuum. We investigated the melting phenomenon of the base metal and filler wire, bead formation, and the effects of wire feed speed on melting characteristics. The melting mechanism in the base metal during the bead on a plate with wire feed was similar to that for the melt run without wire feed. We clarified the effects of wire feed speed on bead sizes and configurations. Furthermore, the butt welded joint welded using the optimum wire feed speed, and the joint tensile strengths were evaluated. The tensile strength of the square butt joint welded by the pulsed DC GHTA welding with wire feed in a vacuum is nearly equal to that of the same joint welded by conventional GTA (Gas Tungsten Arc) welding in air.

Development of vacuum ultraviolet absorption spectroscopy system for wide measurement range of number density using a dual-tube inductively coupled plasma light source

NASA Astrophysics Data System (ADS)

Kuwahara, Akira; Matsui, Makoto; Yamagiwa, Yoshiki

2012-12-01

A vacuum ultraviolet absorption spectroscopy system for a wide measurement range of atomic number densities is developed. Dual-tube inductively coupled plasma was used as a light source. The probe beam profile was optimized for the target number density range by changing the mass flow rate of the inner and outer tubes. This system was verified using cold xenon gas. As a result, the measurement number density range was extended from the conventional two orders to five orders of magnitude.

Investigation on the properties of nano copper matrix composite via vacuum arc melting method

NASA Astrophysics Data System (ADS)

Liu, Yi; Leng, Jinfeng; Wu, Qirui; Zhang, Shaochen; Teng, Xinying

2017-10-01

Copper and copper matrix composites (CMCs) are widely used as electrical contact materials in electrical switch systems due to their excellent electrical properties. Graphene has great mechanical, physical and electrical properties, which is competent as an attractive reinforcing material for fabricating CMCs. Therefore, graphene was added to CMCs to improve the mechanical properties. In this study, graphene-reinforced copper matrix composites (Gr/Cu composites) were obtained. The xGr/Cu (x  =  0, 0.1, 0.3 and 0.5 wt.%) composites were fabricated via the vacuum arc melting method and compared the performance of them. The mechanical properties and electrical properties were obtained by measuring the hardness and conductivity. The microstructure of Gr/Cu composites was observed by optical microscopy (OM) and scanning electron microscopy (SEM). With the addition of graphene from 0 wt.% to 0.5 wt.%, the densities of materials decreased from 97.0% to 95.7%. With the increasing of graphene content, the hardness of composites increased at beginning and then decreased. In this range of adding amount, the hardness of 0.3Gr/Cu composite was up to 66.8 HB and increased by 15.4% compared to Al2O3/Cu composites without graphene. With the addition of graphene powder, the international annealing copper standard IACS% of Gr/Cu composites decreased from 86.16 to 69.86. The range of decline and the percentage of decline range are middle and 18.9%, respectively.

Method of correcting eddy current magnetic fields in particle accelerator vacuum chambers

DOEpatents

Danby, G.T.; Jackson, J.W.

1990-03-19

A method for correcting magnetic field aberrations produced by eddy currents induced in a particle accelerator vacuum chamber housing is provided wherein correction windings are attached to selected positions on the housing and the windings are energized by transformer action from secondary coils, which coils are inductively coupled to the poles of electro-magnets that are powered to confine the charged particle beam within a desired orbit as the charged particles are accelerated through the vacuum chamber by a particle-driving rf field. The power inductively coupled to the secondary coils varies as a function of variations in the power supplied by the particle-accelerating rf field to a beam of particles accelerated through the vacuum chamber, so the current in the energized correction coils is effective to cancel eddy current flux fields that would otherwise be induced in the vacuum chamber by power variations (dB/dt) in the particle beam.

Local ice melting by an antifreeze protein.

PubMed

Calvaresi, Matteo; Höfinger, Siegfried; Zerbetto, Francesco

2012-07-09

Antifreeze proteins, AFP, impede freezing of bodily fluids and damaging of cellular tissues by low temperatures. Adsorption-inhibition mechanisms have been developed to explain their functioning. Using in silico Molecular Dynamics, we show that type I AFP can also induce melting of the local ice surface. Simulations of antifreeze-positive and antifreeze-negative mutants show a clear correlation between melting induction and antifreeze activity. The presence of local melting adds a function to type I AFPs that is unique to these proteins. It may also explain some apparently conflicting experimental results where binding to ice appears both quasipermanent and reversible.

Hydrogenation and interesterification effects on the oxidative stability and melting point of soybean oil.

PubMed

Daniels, Roger L; Kim, Hyun Jung; Min, David B

2006-08-09

Soybean oil with an iodine value of 136 was hydrogenated to have iodine values of 126 and 117. The soybean oils with iodine values of 136, 126, and 117 were randomly interesterified using sodium methoxide. The oxidative stabilities of the hydrogenated and/or interesterified soybean oils were evaluated by measuring the headspace oxygen content by gas chromatography, and the induction time was measured using Rancimat. The melting points of the oils were evaluated by differential scanning calorimetry. Duncan's multiple range test of the headspace oxygen and induction time showed that hydrogenation increased the headspace oxygen content and induction time at alpha = 0.05. Interesterification decreased the headspace oxygen and the induction time for the soybean oils with iodine values of 136, 126, and 117 at alpha = 0.05. Hydrogenation increased the melting points as the iodine value decreased from 136 and 126 to 117 at alpha = 0.05. The random interesterification increased the melting points of soybean oils with iodine values of 136, 126, and 117 at alpha = 0.05. The combined effects of hydrogenation and interesterification increased the oxidative stability of soybean oil at alpha = 0.05 and the melting point at alpha = 0.01. The optimum combination of hydrogenation and random interesterification can improve the oxidative stability and increase the melting point to expand the application of soybean oil in foods.

Recovery of materials from waste printed circuit boards by vacuum pyrolysis and vacuum centrifugal separation.

PubMed

Zhou, Yihui; Wu, Wenbiao; Qiu, Keqiang

2010-11-01

In this research, a two-step process consisting of vacuum pyrolysis and vacuum centrifugal separation was employed to treat waste printed circuit boards (WPCBs). Firstly, WPCBs were pyrolysed under vacuum condition at 600 °C for 30 min in a lab-scale reactor. Then, the obtained pyrolysis residue was heated under vacuum until the solder was melted, and then the molten solder was separated from the pyrolysis residue by the centrifugal force. The results of vacuum pyrolysis showed that the type-A of WPCBs (the base plates of which was made from cellulose paper reinforced phenolic resin) pyrolysed to form an average of 67.97 wt.% residue, 27.73 wt.% oil, and 4.30 wt.% gas; and pyrolysis of the type-B of WPCBs (the base plates of which was made from glass fiber reinforced epoxy resin) led to an average mass balance of 72.20 wt.% residue, 21.45 wt.% oil, and 6.35 wt.% gas. The results of vacuum centrifugal separation showed that the separation of solder was complete when the pyrolysis residue was heated at 400 °C, and the rotating drum was rotated at 1200 rpm for 10 min. The pyrolysis oil and gas can be used as fuel or chemical feedstock after treatment. The pyrolysis residue after solder separation contained various metals, glass fibers and other inorganic materials, which could be recycled for further processing. The recovered solder can be reused directly and it can also be a good resource of lead and tin for refining. Copyright © 2010 Elsevier Ltd. All rights reserved.

Vacuum fusion bonding of glass plates

DOEpatents

Swierkowski, Steve P.; Davidson, James C.; Balch, Joseph W.

2001-01-01

An improved apparatus and method for vacuum fusion bonding of large, patterned glass plates. One or both glass plates are patterned with etched features such as microstructure capillaries and a vacuum pumpout moat, with one plate having at least one hole therethrough for communication with a vacuum pumpout fixture. High accuracy alignment of the plates is accomplished by a temporary clamping fixture until the start of the fusion bonding heat cycle. A complete, void-free fusion bond of seamless, full-strength quality is obtained through the plates; because the glass is heated well into its softening point and because of a large, distributed force that is developed that presses the two plates together from the difference in pressure between the furnace ambient (high pressure) and the channeling and microstructures in the plates (low pressure) due to the vacuum drawn. The apparatus and method may be used to fabricate microcapillary arrays for chemical electrophoresis; for example, any apparatus using a network of microfluidic channels embedded between plates of glass or similar moderate melting point substrates with a gradual softening point curve, or for assembly of glass-based substrates onto larger substrates, such as in flat panel display systems.

Vacuum fusion bonding of glass plates

DOEpatents

Swierkowski, Steve P.; Davidson, James C.; Balch, Joseph W.

2000-01-01

An improved apparatus and method for vacuum fusion bonding of large, patterned glass plates. One or both glass plates are patterned with etched features such as microstructure capillaries and a vacuum pumpout moat, with one plate having at least one hole therethrough for communication with a vacuum pumpout fixture. High accuracy alignment of the plates is accomplished by a temporary clamping fixture until the start of the fusion bonding heat cycle. A complete, void-free fusion bond of seamless, full-strength quality is obtained through the plates; because the glass is heated well into its softening point and because of a large, distributed force that is developed that presses the two plates together from the difference in pressure between the furnace ambient (high pressure) and the channeling and microstructures in the plates (low pressure) due to the vacuum drawn. The apparatus and method may be used to fabricate microcapillary arrays for chemical electrophoresis; for example, any apparatus using a network of microfluidic channels embedded between plates of glass or similar moderate melting point substrates with a gradual softening point curve, or for assembly of glass-based substrates onto larger substrates, such as in flat panel display systems.

Interaction of exogenous refractory nanophases with antimony dissolved in liquid iron

NASA Astrophysics Data System (ADS)

Burtsev, V. T.; Anuchkin, S. N.; Samokhin, A. V.

2017-07-01

The heterophase interaction of Al2O3 refractory nanoparticles with a surfactant impurity (antimony) in the Fe-Sb (0.095 wt %)-O (0.008 wt %) system is studied. It is shown that the introduction of 0.06-0.18 wt % Al2O3 nanoparticles (25-83 nm) into a melt during isothermal holding for up to 1200 s leads to a decrease in the antimony content: the maximum degree of antimony removal is 26 rel %. The sessile drop method is used to investigate the surface tension and the density of Fe, Fe-Sb, and Fe-Sb-Al2O3 melts. The polytherms of the surface tension of these melts have a linear character, the removal of antimony from the Fe-Sb-Al2O3 melts depends on the time of melting in a vacuum induction furnace, and the experimental results obtained reveal the kinetic laws of the structure formation in the surface layers of the melts. The determined melt densities demonstrate that the introduction of antimony into the Fe-O melt causes an increase in its compression by 47 rel %. The structure of the Fe-Sb-O melt after the introduction of Al2O3 nanoparticles depends on the time of melting in a vacuum induction furnace.

Analysis of laser-induction hybrid cladding processing conditions

NASA Astrophysics Data System (ADS)

Huang, Yongjun; Zeng, Xiaoyan; Hu, Qianwu

2007-12-01

A new cladding approach based on laser-induction hybrid technique on flat sheets is presented in this paper. Coating is produced by means of 5kw cw CO II laser equipped with 100kw high frequent inductor, and the experiments set-up, involving a special machining-head, which can provide laser-induction hybrid heat resources simultaneously. The formation of thick NiCrSiB coating on a steel substrate by off-axial powder feeding is studied from an experimental point of view. A substrate melting energy model is developed to describe the energy relationship between laser-induction hybrid cladding and laser cladding alone quantitatively. By comparing the experimental results with the calculational ones, it is shown that the tendency of fusion zone height of theoretical calculation is in agreement with that of tests in laser-induction hybrid cladding. Via analyses and tests, the conclusions can be lead to that the fusion zone height can be increased easily and the good bond of cladding track can be achieved within wide cladding processing window in laser-induction hybrid processing. It shows that the induction heating has an obvious effect on substrate melting and metallurgical bond.

Removing antimony from waste lead storage batteries alloy by vacuum displacement reaction technology.

PubMed

Liu, Tiantian; Qiu, Keqiang

2018-04-05

With the wide application of lead acid battery, spent lead acid battery has become a serious problem to environmental protection and human health. Though spent battery can be a contaminant if not handled properly, it is also an important resource to obtain refined lead. Nowadays, the Sb-content in lead storage batteries is about 0.5-3 wt%, which is higher than the Sb-content in the crude lead. However, there are few reports about the process of removing antimony from high-antimony lead bullion. In this study, vacuum displacement reaction technology, a new process for removing antimony from high-antimony lead melts, was investigated. During this process, lead oxide was added to the system and antimony from lead melts was converted into antimony trioxide, which easily was evaporated under vacuum so that antimony was removed from lead melts. The experimental results demonstrated that Sb-content in lead melts decreased from 2.5% to 23 ppm under following conditions: mass ratio of PbO/lead bullion of 0.33, residual gas pressure of 30 Pa, melt temperature of 840 °C, reaction time of 60 min. The distillate gotten can be used as by-product to produce antimony white. Moreover, this study is of importance to recycling of waste lead storage batteries alloy. Copyright © 2018 Elsevier B.V. All rights reserved.

Interaction Studies of Ceramic Vacuum Plasma Spraying for the Melting Crucible Materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jong Hwan Kim; Hyung Tae Kim; Yoon Myung Woo

2013-10-01

Candidate coating materials for re-usable metallic nuclear fuel crucibles, TaC, TiC, ZrC, ZrO2, and Y2O3, were plasmasprayed onto a niobium substrate. The microstructure of the plasma-sprayed coatings and thermal cycling behavior were characterized, and U-Zr melt interaction studies were carried out. The TaC and Y2O3 coating layers had a uniform thickness, and high density with only a few small closed pores showing good consolidation, while the ZrC, TiC, and ZrO2 coatings were not well consolidated with a considerable amount of porosity. Thermal cycling tests showed that the adhesion of the TiC, ZrC, and ZrO2 coating layers with niobium was relativelymore » weak compared to the TaC and Y2O3 coatings. The TaC and Y2O3 coatings had better cycling characteristics with no interconnected cracks. In the interaction studies, ZrC and ZrO2 coated rods showed significant degradations after exposure to U-10 wt.% Zr melt at 1600 degrees C for 15 min., but TaC, TiC, and Y2O3 coatings showed good compatibility with U-Zr melt.« less

Thermal Diffusivity for III-VI Semiconductor Melts at Different Temperatures

NASA Technical Reports Server (NTRS)

Ban, H.; Li, C.; Lin, B.; Emoto, K.; Scripa, R. N.; Su, C.-H.; Lehoczky, S. L.

2004-01-01

The change of the thermal properties of semiconductor melts reflects the structural changes inside the melts, and a fundamental understanding of this structural transformation is essential for high quality semiconductor crystal growth process. This paper focused on the technical development and the measurement of thermal properties of III-VI semiconductor melts at high temperatures. Our previous work has improved the laser flash method for the specialized quartz sample cell. In this paper, we reported the results of our recent progress in further improvements of the measurement system by minimizing the free convection of the melt, adding a front IR detector, and placing the sample cell in a vacuum environment. The results for tellurium and selenium based compounds, some of which have never been reported in the literature, were obtained at different temperatures as a function of time. The data were compared with other measured thermophysical properties to shed light on the structural transformations of the melt.

Melt-gas phase equilibria and state diagrams of the selenium-tellurium system

NASA Astrophysics Data System (ADS)

Volodin, V. N.; Trebukhov, S. A.; Burabaeva, N. M.; Nitsenko, A. V.

2017-05-01

The partial pressures of saturated vapor of the components in the Se-Te system are determined and presented in the form of temperature-concentration dependences from which the boundaries of the melt-gas phase transition are calculated at atmospheric pressure and vacuums of 2000 and 100 Pa. The existence of azeotropic mixtures is revealed. It is found that the points of inseparably boiling melts correspond to 7.5 at % of Se and 995°C at 101325 Pa, 10.9 at % at 673°C and 19.5 at % at 522°C in vacuums of 2000 and 100 Pa, respectively. A complete state diagram is constructed, including the fields of gas-liquid equilibria at atmospheric and low pressures, the boundaries of which allow us to assess the behavior of selenium and tellurium upon distillation fractionation.

Vacuum fusion bonded glass plates having microstructures thereon

DOEpatents

Swierkowski, Steve P.; Davidson, James C.; Balch, Joseph W.

2001-01-01

An improved apparatus and method for vacuum fusion bonding of large, patterned glass plates. One or both glass plates are patterned with etched features such as microstructure capillaries and a vacuum pumpout moat, with one plate having at least one hole therethrough for communication with a vacuum pumpout fixture. High accuracy alignment of the plates is accomplished by a temporary clamping fixture until the start of the fusion bonding heat cycle. A complete, void-free fusion bond of seamless, full-strength quality is obtained through the plates; because the glass is heated well into its softening point and because of a large, distributed force that is developed that presses the two plates together from the difference in pressure between the furnace ambient (high pressure) and the channeling and microstructures in the plates (low pressure) due to the vacuum drawn. The apparatus and method may be used to fabricate microcapillary arrays for chemical electrophoresis; for example, any apparatus using a network of microfluidic channels embedded between plates of glass or similar moderate melting point substrates with a gradual softening point curve, or for assembly of glass-based substrates onto larger substrates, such as in flat panel display systems.

Experience of ALCOA-KOFEM with MHD induction stirrer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Petho, S.

1996-10-01

Every ingot cast shop makes an effort to reduce the costs and to increase the productivity. The MHD stirrer is an adequate tool to achieve a more economical production. The electromagnetic stirrer accelerates the melting rate of the charge, reduces the metal loss and improves the consistency of ingot quality. The Ingot Business Unit of ALCOA-KOFEM operates seven melting furnaces. Each furnace is equipped with a POTOK type MHD induction stirrer in order to achieve a more profitable melting operation. Magnetohydrodynamic stirrers were installed between 1988 and 1990 on melting furnaces ranging in capacity from 25 to 60 tons ofmore » molten metal.« less

Effects of Vegetable Oil Type and Lipophilic Emulsifiers on the Induction Period of Fat Crystallization.

PubMed

Miyagawa, Yayoi; Ogawa, Takenobu; Nakagawa, Kyuya; Adachi, Shuji

2015-01-01

The induction period of crystallization, which is defined as the time required for oil to start to crystallize, is useful indicator of the freeze-thaw stability of food emulsions such as mayonnaise. We investigated the induction period of vegetable oils with low melting points, such as rapeseed and soybean oils, which are commonly employed for mayonnaise production. The induction period was measured by monitoring the temperature of a specimen during storage at low temperature. The induction period depended on the type of oil and lipophilic emulsifier, emulsifier concentration, and storage temperature. The effect of the oil type on the induction period depended on the composition of the oil. Differential scanning calorimetry (DSC) analyses of the lipophilic emulsifiers suggested that the melting trend of the emulsifier is strongly related to the induction period.

Method for producing melt-infiltrated ceramic composites using formed supports

DOEpatents

Corman, Gregory Scot; Brun, Milivoj Konstantin; McGuigan, Henry Charles

2003-01-01

A method for producing shaped articles of ceramic composites provides a high degree of dimensional tolerance to these articles. A fiber preform is disposed on a surface of a stable formed support, a surface of which is formed with a plurality of indentations, such as grooves, slots, or channels. Precursors of ceramic matrix materials are provided to the fiber preform to infiltrate from both sides of the fiber preform. The infiltration is conducted under vacuum at a temperature not much greater than a melting point of the precursors. The melt-infiltrated composite article substantially retains its dimension and shape throughout the fabrication process.

[The induction current, an ideal resource for the smelting of dental alloys].

PubMed

Ionescu, G; Chiper, C; Teofănescu, L; Brezulianu, C

1996-01-01

The authors present an electrical furnace for melting dental alloys, made by the German company BEGO. This furnace uses electrical current of high frequency. The advantages of this melting method are the possibility of controlling the adequate melting temperature for a specific type of alloy, the fusion in a protective environment of rare gas and casting by associating the centrifugation with the vacuum. This leads to exact castings without any defects. The authors describe as a personal contribution an external cooling system capable of maintaining the furnace's parameters even when the water pressure is low.

Primary melt and fluid inclusions in regenerated crystals and phenocrysts of olivine from kimberlites of the Udachnaya-East Pipe, Yakutia: The problem of the kimberlite melt

NASA Astrophysics Data System (ADS)

Tomilenko, A. A.; Kuzmin, D. V.; Bul'bak, T. A.; Sobolev, N. V.

2017-08-01

The primary melt and fluid inclusions in regenerated zonal crystals of olivine and homogeneous phenocrysts of olivine from kimberlites of the Udachnaya-East pipe, were first studied by means of microthermometry, optic and scanning electron microscopy, electron and ion microprobe analysis (SIMS), inductively coupled plasma mass-spectrometry (ICP MSC), and Raman spectroscopy. It was established that olivine crystals were regenerated from silicate-carbonate melts at a temperature of 1100°C.

Dynamic polarizability of tungsten atoms reconstructed from fast electrical explosion of fine wires in vacuum

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sarkisov, G. S.; Rosenthal, S. E.; Struve, K. W.

For nanosecond electrical explosion of fine metal wires in vacuum generates calibrated, radially expanded gas cylinders of metal atoms are surrounded by low-density fast expanding plasma corona. Here, a novel integrated-phase technique, based on laser interferometry, provides the dynamic dipole polarizability of metal atoms. This data was previously unavailable for tungsten atoms. Furthermore, an extremely high melting temperature and significant pre-melt electronic emission make these measurements particularly complicated for this refractory metal.

Dynamic polarizability of tungsten atoms reconstructed from fast electrical explosion of fine wires in vacuum

DOE PAGES

Sarkisov, G. S.; Rosenthal, S. E.; Struve, K. W.

2016-10-12

For nanosecond electrical explosion of fine metal wires in vacuum generates calibrated, radially expanded gas cylinders of metal atoms are surrounded by low-density fast expanding plasma corona. Here, a novel integrated-phase technique, based on laser interferometry, provides the dynamic dipole polarizability of metal atoms. This data was previously unavailable for tungsten atoms. Furthermore, an extremely high melting temperature and significant pre-melt electronic emission make these measurements particularly complicated for this refractory metal.

Thin film coating process using an inductively coupled plasma

DOEpatents

Kniseley, Richard N.; Schmidt, Frederick A.; Merkle, Brian D.

1990-01-30

Thin coatings of normally solid materials are applied to target substrates using an inductively coupled plasma. Particles of the coating material are vaporized by plasma heating, and pass through an orifice to a first vacuum zone in which the particles are accelerated to a velocity greater than Mach 1. The shock wave generated in the first vacuum zone is intercepted by the tip of a skimmer cone that provides a second orifice. The particles pass through the second orifice into a second zone maintained at a higher vacuum and impinge on the target to form the coating. Ultrapure coatings can be formed.

Vacuum pull down method for an enhanced bonding process

DOEpatents

Davidson, James C.; Balch, Joseph W.

1999-01-01

A process for effectively bonding arbitrary size or shape substrates. The process incorporates vacuum pull down techniques to ensure uniform surface contact during the bonding process. The essence of the process for bonding substrates, such as glass, plastic, or alloys, etc., which have a moderate melting point with a gradual softening point curve, involves the application of an active vacuum source to evacuate interstices between the substrates while at the same time providing a positive force to hold the parts to be bonded in contact. This enables increasing the temperature of the bonding process to ensure that the softening point has been reached and small void areas are filled and come in contact with the opposing substrate. The process is most effective where at least one of the two plates or substrates contain channels or grooves that can be used to apply vacuum between the plates or substrates during the thermal bonding cycle. Also, it is beneficial to provide a vacuum groove or channel near the perimeter of the plates or substrates to ensure bonding of the perimeter of the plates or substrates and reduce the unbonded regions inside the interior region of the plates or substrates.

Formation of β-NiAl Phase During Casting of a Ni-Based Superalloy

NASA Astrophysics Data System (ADS)

Detrois, Martin; Jablonski, Paul D.

2018-04-01

A high-refractory Ni-based superalloy prototype was melted on a research scale while simulating industry practices. Ingots were vacuum induction melted and subjected to a computationally optimized homogenization heat treatment prior to fabrication which consisted of forging and hot rolling. Failure of one of the ingots at the early stage of the forging process was attributed to the precipitation of the β-NiAl phase during melting which stabilized the eutectic constituent.

Interruption Phenomenon in Intermediate-Frequency Vacuum Arc

NASA Astrophysics Data System (ADS)

Jiang, Yuan; Wu, Jianwen

2016-03-01

In the condition of the 3 mm gap, experiments for 360 Hz intermediate-frequency vacuum arc are carried out in interrupters with the diameters being 41 mm and with the contact materials being CuCr50 and Cu-W-WC alloy respectively. The results indicate that the contacts material is closely related to the breaking capacity of the vacuum interrupters and characteristics of an intermediate-frequency vacuum arc. For contacts with the same diameter, the breaking capacity of CuCr50 is better than that of Cu-W-WC. When the current fails to be interrupted, the arcs overflow the gap and present irregular performances in the first half wave. Consequently a voltage spike appears. More macroscopic metal droplets can be seen in the arc column between CuCr50 contacts because of the lower melting point. It is observed that the droplet emission is much more severe during arc reignition than that in the first half wave. It is much more conspicuous that the high frequency arc voltage noises appear in Cu-W-WC contacts when the vacuum arcs reignite, for higher temperature and stronger electronic emission ability of Cu-W-WC contacts. supported by National Natural Science Foundation of China (No. 51377007), Specialized Research Fund for the Doctoral Program of Higher Education of China (No. 20131102130006), and Fundamental Research Funds for the Central Universities of China

Linear induction accelerator and pulse forming networks therefor

DOEpatents

Buttram, Malcolm T.; Ginn, Jerry W.

1989-01-01

A linear induction accelerator includes a plurality of adder cavities arranged in a series and provided in a structure which is evacuated so that a vacuum inductance is provided between each adder cavity and the structure. An energy storage system for the adder cavities includes a pulsed current source and a respective plurality of bipolar converting networks connected thereto. The bipolar high-voltage, high-repetition-rate square pulse train sets and resets the cavities.

Optical measurement of high-temperature melt flow rate.

PubMed

Bizjan, Benjamin; Širok, Brane; Chen, Jinpeng

2018-05-20

This paper presents an optical method and system for contactless measurement of the mass flow rate of melts by digital cameras. The proposed method is based on reconstruction of melt stream geometry and flow velocity calculation by cross correlation, and is very cost-effective due its modest hardware requirements. Using a laboratory test rig with a small inductive melting pot and reference mass flow rate measurement by weighing, the proposed method was demonstrated to have an excellent dynamic response (0.1 s order of magnitude) while producing deviations from the reference of about 5% in the steady-state flow regime. Similar results were obtained in an industrial stone wool production line for two repeated measurements. Our method was tested in a wide range of melt flow rates (0.05-1.2 kg/s) and did not require very fast cameras (120 frames per second would be sufficient for most industrial applications).

Induction furnace testing of the durability of prototype crucibles in a molten metal environment

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jablonski, Paul D.

2005-09-01

Engineered ceramic crucibles are commonly used to contain molten metal. Besides high temperature stability, other desired crucible characteristics include thermal shock resistance, minimal reaction with the molten metal and resistance to attack from the base metal oxide formed during melting. When used in an induction furnace, they can be employed as a “semi-permanent” crucible incorporating a dry ram backup and a ceramic cap. This report covers several 250-lb single melt crucible tests in an air melt induction furnace. These tests consisted of melting a charge of 17-4PH stainless steel, holding the charge molten for two hours before pouring off themore » heat and then subsequently sectioning the crucible to review the extent of erosion, penetration and other physical characteristics. Selected temperature readings were made throughout each melt. Chemistry samples were also taken from each heat periodically throughout the hold. The manganese level was observed to affect the rate of chromium loss in a non-linear fashion.« less

Melt segregation during Poiseuille flow of partially molten rocks

NASA Astrophysics Data System (ADS)

Quintanilla-Terminel, A.; Dillman, A. M.; Kohlstedt, D. L.

2015-12-01

Studies of the dynamics of partially molten regions of the Earth's mantle provide the basis necessary for understanding the chemical and physical evolution of our planet. Since we cannot directly observe processes occurring at depth, we rely on models and experiments to constrain the rheological behavior of partially molten rocks. Here, we present the results of an experimental investigation of the role of viscous anisotropy on melt segregation in partially molten rocks through Poiseuille flow experiments. Partially molten rock samples with a composition of either forsterite or anorthite plus a few percent melt were prepared from vacuum sintered powders and taken to 1200ºC at 0.1 MPa. The partially molten samples were then extruded through a channel of circular cross section under a fixed pressure gradient at 1200o to 1500oC. The melt distribution in the channel was subsequently mapped through image analyses of optical and backscattered electron microscopy images. In these experiments, melt segregates from the center toward the outer radius of the channel with the melt fraction at the outer radius increasing to twice that at the center. These results are consistent with base-state melt segregation as predicted by Takei and Holtzman (JGR, 2009), Takei and Katz (JFM, 2013) and Allwright and Katz (GJI, 2014) for sheared partially molten rocks for which viscosity is anisotropic due to the stress-induced, grain-scale alignment of melt.

[A DNA study of rat liver oligonucleosomes enriched by transcriptionally active genes during induction due to the administration of an amino acid mixture].

PubMed

Vardevanian, P O; Davtian, A M; Tiratsuian, S G; Vardevanian, A O

1990-01-01

A highly active fraction of rat liver oligonucleosome DNA has been isolated and studied by means of thermal denaturation after induction by amino acid mixture or hydrocortisone. A considerable redistribution of DNA content has been shown in sucrose gradient fractions during these forms of induction. The changes are revealed in melting temperature, differential melting profile of DNA, isolated from actively transcribed chromatine fractions. Analysis of melting profiles shows changes of GC content of oligonucleosome DNA, suggesting that there are differences in activation during two studied forms of induction.

Method for treating reactive metals in a vacuum furnace

DOEpatents

Hulsey, W.J.

1975-10-28

The invention is directed to a method for reducing the contamination of reactive metal melts in vacuum furnaces due to the presence of residual gaseous contaminants in the furnace atmosphere. This reduction is achieved by injecting a stream of inert gas directly over the metal confined in a substantially closed crucible with the flow of the gas being sufficient to establish a pressure differential between the interior of the crucible and the furnace atmosphere.

X-ray and optical crystallographic parameters investigations of high frequency induction melted Al-(alpha-Al(2)O(3)) alloys.

PubMed

Bourbia, A; Draissia, M; Bedboudi, H; Boulkhessaim, S; Debili, M Y

2010-01-01

This article deals with the microstructural strengthening mechanisms of aluminium by means of hard alpha-Al(2)O(3) alumina fine particles. A broad of understanding views covering materials preparations, elaboration process, characterization techniques and associated microstructural characteristic parameters measurements is given. In order to investigate the microstructural characteristic parameters and the mechanical strengthening mechanisms of pure aluminium by hard fine particles, a set of Al-(alpha-Al(2)O(3)) alloys samples were made under vacuum by high fusion temperature melting, the high frequency (HF) process, and rapidly solidified under ambient temperature from a mixture of cold-compacted high-pure fine Al and alpha-Al(2)O(3) powders. The as-solidified Al-(alpha-Al(2)O(3)) alloys were characterized by means of X-ray diffraction (XRD) analyses, optical microscopy observations and Vickers microhardness tests in both brut and heat-treated states. It was found that the as-solidified HF Al-(alpha-Al(2)O(3)) alloys with compositions below 4 wt.% (alpha-Al(2)O(3)) are single-phase microstructures of the solid solution FCC Al phase and over two-phase microstructures of the solid solution FCC Al and the Rhombohedral alpha-Al(2)O(3) phases. The optical micrographs reveal the presence of a grain size refinement in these alloys. Vickers microhardness of the as-solidified Al-(alpha-Al(2)O(3)) is increased by means of pure fine alpha-Al(2)O(3) alumina particles. These combined effects of strengthening and grain size refinement observed in the as-solidified Al-(alpha-Al(2)O(3)) alloys are essentially due to a strengthening of Al by the alpha-Al(2)O(3) alumina particles insertion in the (HF) melted and rapidly solidified alloys.

Enhanced Magnetic Properties of Nd15Fe77B8 Alloy Powders Produced by Melt-Spinning Technique

NASA Astrophysics Data System (ADS)

Öztürk, Sultan; İcin, Kürşat; Öztürk, Bülent; Topal, Uğur; Odabaşı, Hülya Kaftelen; Göbülük, Metin; Cora, Ömer Necati

2017-10-01

Rapidly solidified Nd15Fe77B8 alloy powders were produced by means of melt-spinning method in high-vacuum atmosphere to achieve improved magnetic and thermal properties. To this goal, a vacuum milling apparatus was designed and constructed to ball-mill the melt-spun powders in a surfactant active atmosphere. Various milling times were experimented to reveal the effect of the milling time on the mean particle size and other size-dependent properties such as magnetism and Curie temperature. Grain structure, cooling rate, and phase structure of the produced powders were also investigated. The Curie points shifted to higher temperatures from the ingot condition to surfactant active ball-milling and the values for Nd15Fe77B8 ingot alloy, melt-spun powders, and surfactant active ball-milled powders were 552 K, 595 K, and 604 K (279 °C, 322 °C, and 331 °C), respectively. It was noted that the surfactant active ball-milling process improved the magnetic and thermal properties of melt-spun Nd15Fe77B8 alloy powders. Compared to relevant literature, the coercivity of powders increased significantly with increasing milling time and decreasing in powder size. The coercivity value as high as 3427 kA m-1 was obtained.

Vacuum Outgassing Behavior of Carbon Nanotube Cathode with High-Intensity Pulsed Electron Emission

NASA Astrophysics Data System (ADS)

Shen, Yi; Zhang, Huang; Xia, Liansheng; Liu, Xingguang; Pan, Haifeng; Lv, Lu; Yang, Anmin; Shi, Jinshui; Zhang, Linwen; Deng, Jianjun

2015-02-01

Experimental investigations on the vacuum outgassing of a carbon nanotube (CNT) cathode with high-intensity pulsed electron emission on a 2 MeV linear induction accelerator injector are presented. Under the 1.60 MV diode voltage, the CNT cathode could provide 1.67 kA electron beam with the amount of outgassing of about 0.51 Pa·L. It is found that the amount of outgassing, which determines the cathode emission current, depends on the diode voltage and the vacuum.

Molecular dynamics simulation of UO2 nanocrystals melting under isolated and periodic boundary conditions

NASA Astrophysics Data System (ADS)

Boyarchenkov, A. S.; Potashnikov, S. I.; Nekrasov, K. A.; Kupryazhkin, A. Ya.

2012-08-01

Melting of uranium dioxide (UO2) nanocrystals has been studied by molecular dynamics (MD) simulation. Ten recent and widely used sets of pair potentials were assessed in the rigid ion approximation. Both isolated (in vacuum) and periodic boundary conditions (PBC) were explored. Using barostat under PBC the pressure dependences of melting point were obtained. These curves intersected zero near -20 GPa, saturated near 25 GPa and increased nonlinearly in between. Using simulation of surface under isolated boundary conditions (IBC) recommended melting temperature and density jump were successfully reproduced. However, the heat of fusion is still underestimated. These melting characteristics were calculated for nanocrystals of cubic shape in the range of 768-49 152 particles (volume range of 10-1000 nm3). The obtained reciprocal size dependences decreased nonlinearly. Linear and parabolic extrapolations to macroscopic values are considered. The parabolic one is found to be better suited for analysis of the data on temperature and heat of melting.

The Influence of Vacuum Circuit Breakers and Different Motor Models on Switching Overvoltages in Motor Circuits

NASA Astrophysics Data System (ADS)

Wong, Cat S. M.; Snider, L. A.; Lo, Edward W. C.; Chung, T. S.

Switching of induction motors with vacuum circuit breakers continues to be a concern. In this paper the influence on statistical overvoltages of the stochastic characteristics of vacuum circuit breakers, high frequency models of motors and transformers, and network characteristics, including cable lengths and network topology are evaluated and a general view of the overvoltages phenomena is presented. Finally, a real case study on the statistical voltage levels and risk-of-failure resulting from switching of a vacuum circuit breaker in an industrial installation in Hong Kong is presented.

Cold crucible levitation melting of biomedical Ti-30 wt%Ta alloy.

PubMed

Fukui, H; Yang, W; Yamada, S; Fujishiro, Y; Morita, A; Niinomi, M

2001-06-01

Recently, titanium-tantalum alloys have been studied as implant materials for dental and orthopedic surgery. However, titanium and tantalum are difficult to mix by common arc melting and induction melting, because of their high melting point and the marked difference between their densities (Ti: 1,680 degrees C, 4.5 g/cm3, Ta: 2,990 degrees C, 16.6 g/cm3). Thus, the Cold Crucible Levitation Melting (CCLM) method was chosen to produce a Ti-30 wt%Ta binary alloy in the present study. The CCLM furnace, with 1 kg capacity, consisted of a water-cooled crucible comprising oxygen-free high purity copper segments and coils wrapped around the crucible and connected to a frequency inverter power supply. A qualified ingot of 1.0 kg of Ti-30 wt%Ta alloy was obtained. The ingot was characterized from the surface quality, chemical composition distribution and microstructure, and finally the melting process was discussed.

Thermocapillary convection of melts and its role in laser-plasma synthesis and laser-induced amorphism

NASA Astrophysics Data System (ADS)

Uglov, A. A.; Smurov, I. Iu.; Gus'kov, A. G.; Semakhin, S. A.

1987-06-01

The role of thermocapillary convection in mass transfer processes in melts is investigated analytically and experimentally using vacuum-arc melted Ni63-Ta37 and Cu50-Zr50 alloys. It is shown that thermocapillary convection not only leads to the transfer of alloying components to the deeper layers of the melt but also may produce, in certain cases, a significant temperature redistribution in the liquid phase. Convective transfer dominates over conduction when the product of Re and Pr is greater than 1. In the experiments, the structure of the amorphous and crystalline layers in the solidified alloys is found to be in qualitative agreement with the structure of a thermocapillary vortex.

PREFACE: International Symposium on `Vacuum Science and Technology' (IVS 2007)

NASA Astrophysics Data System (ADS)

Mittal, K. C.; Gupta, S. K.

2008-03-01

The Indian Vacuum Society (established in 1970) has organized a symposium every alternate year on various aspects of vacuum science and technology. There has been considerable participation from R & D establishments, universities and Indian industry in this event. In view of the current global scenario and emerging trends in vacuum technology, this year, the executive committee of IVS felt it appropriate to organize an international symposium at Tata Institute of Fundamental Research, Colaba, Mumbai 400 005 from 29-30 November 2007. This symposium provided a forum for exchange of information among vacuum scientists, technologists and industrialists on recent advances made in the areas of large vacuum systems, vacuum production, its measurement and applications in industry, and material processing in vacuum. Vacuum science and technology has made vital contributions in high tech areas like space, high energy particle accelerators, large plasma systems, electronics, thin films, melting and refining of metals, extraction and processing of advanced materials etc. The main areas covered in the symposium were the production and measurement of vacuums, leak detection, large vacuum systems, vacuum metallurgy, vacuum materials and processing inclusive of applications of vacuum in industry. Large vacuum systems for high energy particle accelerators, plasma devices and light sources are of special significance for this symposium. Vacuum evaporation, hard coatings, thin films, joining techniques, sintering, melting and heat treatment, furnaces and thermo dynamics are also covered in this symposium. There were eighteen invited talks from the best experts in the respective fields and more than one hundred contributed papers. This fact itself indicates the interest that has been generated amongst the scientists, technologists and industrialists in this field. In view of the industrial significance of the vacuum technology, an exhibition of vacuum and vacuum processing related

Hot melt adhesive pad surface attachment assembly concept for on-orbit operations

NASA Technical Reports Server (NTRS)

Progar, D. J.; Stein, B. A.

1984-01-01

The use of a hot melt adhesive concept to develop a Surface Attachment Assembly (SAA) for on-orbit attachment and detachment operations for the Manned Maneuvering Unit (MMU) was investigated. The concept involved impregnation of the hot melt adhesive into a fiberglass covered pad which contained electrical heating and thermoelectric cooling devices. The polyamide hot melt adhesive selected can be repeatedly heated to its melting point in a vacuum and provide good adhesion to various surfaces, i.e., reusable surface insulation tiles, metals, and composites, when cooled. After a series of adhesive screening tests, Jet-Melt 3746 was selected from a group of commercially available thermoplastic adhesive candidates which met or exceeded many of the criteria established for the SAA system. The SAA system was designed and fabricted with the goal of proving the concept with a working model rather than attempting to optimize all facets of the system. This system evolved by investigating alternate attachment concepts, designing and fabricating electronic systems to heat and cool the adhesive, and then fabricating electronic systems to heat and cool the adhesive, and then fabricating and testing two prototype full-size units.

Experimental program on nucleation and structure in undercooled melts

NASA Technical Reports Server (NTRS)

1982-01-01

Undercooling and structural refinements in droplets of molten metal levitated in an induction field and/or by dispersion in a fluid carrier were studied. Nickel base and lower melting point alloys levitated in molten carrier fluids are considered. The dispersion of molten alloy droplets in a high temperature fluid following the procedures developed by Perepezko and co-workers for lower melting point alloys; obtaining a similar dispersion by room temperature mechanical mixing of particles of the metal and solidified liquid carrier; and solidification of single relatively large droplets in a transparent fluid carrier, enabling high-speed temperature measurement of the recalescence and subsequent cooling behavior are described.

Vacuum force

NASA Astrophysics Data System (ADS)

Han, Yongquan

2015-03-01

To study on vacuum force, we must clear what is vacuum, vacuum is a space do not have any air and also ray. There is not exist an absolute the vacuum of space. The vacuum of space is relative, so that the vacuum force is relative. There is a certain that vacuum vacuum space exists. In fact, the vacuum space is relative, if the two spaces compared to the existence of relative vacuum, there must exist a vacuum force, and the direction of the vacuum force point to the vacuum region. Any object rotates and radiates. Rotate bend radiate- centripetal, gravity produced, relative gravity; non gravity is the vacuum force. Gravity is centripetal, is a trend that the objects who attracted wants to Centripetal, or have been do Centripetal movement. Any object moves, so gravity makes the object curve movement, that is to say, the radiation range curve movement must be in the gravitational objects, gravity must be existed in non vacuum region, and make the object who is in the region of do curve movement (for example: The earth moves around the sun), or final attracted in the form gravitational objects, and keep relatively static with attract object. (for example: objects on the earth moves but can't reach the first cosmic speed).

Vapor pressures and evaporation coefficients for melts of ferromagnesian chondrule-like compositions

NASA Astrophysics Data System (ADS)

Fedkin, A. V.; Grossman, L.; Ghiorso, M. S.

2006-01-01

To determine evaporation coefficients for the major gaseous species that evaporate from silicate melts, the Hertz-Knudsen equation was used to model the compositions of residues of chondrule analogs produced by evaporation in vacuum by Hashimoto [Hashimoto A. (1983) Evaporation metamorphism in the early solar nebula-evaporation experiments on the melt FeO-MgO-SiO 2-CaO-Al 2O 3 and chemical fractionations of primitive materials. Geochem. J. 17, 111-145] and Wang et al. [Wang J., Davis A. M., Clayton R. N., Mayeda T. K., Hashimoto A. (2001) Chemical and isotopic fractionation during the evaporation of the FeO-MgO-SiO 2-CaO-Al 2O 3-TiO 2 rare earth element melt system. Geochim. Cosmochim. Acta 65, 479-494], in vacuum and in H 2 by Yu et al. [Yu Y., Hewins R. H., Alexander C. M. O'D., Wang J. (2003) Experimental study of evaporation and isotopic mass fractionation of potassium in silicate melts. Geochim. Cosmochim. Acta 67, 773-786], and in H 2 by Cohen et al. [Cohen B. A., Hewins R. H., Alexander C. M. O'D. (2004) The formation of chondrules by open-system melting of nebular condensates. Geochim. Cosmochim. Acta 68, 1661-1675]. Vapor pressures were calculated using the thermodynamic model of Ghiorso and Sack [Ghiorso M. S., Sack R. O. (1995) Chemical mass transfer in magmatic processes IV. A revised and internally consistent thermodynamic model for the interpolation and extrapolation of liquid-solid equilibria in magmatic systems at elevated temperatures and pressures. Contrib. Mineral. Petrol. 119, 197-212], except for the late, FeO-free stages of the Wang et al. (2001) and Cohen et al. (2004) experiments, where the CMAS activity model of Berman [Berman R. G. (1983) A thermodynamic model for multicomponent melts, with application to the system CaO-MgO-Al 2O 3-SiO 2. Ph.D. thesis, University of British Columbia] was used. From these vapor pressures, evaporation coefficients ( α) were obtained that give the best fits to the time variation of the residue compositions

Magnetic hysterysis evolution of Ni-Al alloy with Fe and Mn substitution by vacuum arc melting to produce the room temperature magnetocaloric effect material

DOE Office of Scientific and Technical Information (OSTI.GOV)

Notonegoro, Hamdan Akbar; Mechanical Engineering Dept., FT-Universitas Sultan Ageng Tirtayasa, Cilegon 42435; Kurniawan, Budhy

The development of magnetocaloric effect (MCE) material is done in order to reduce the damage of the ozone layer caused by the chlorofluorocarbons (CFCs) emitted into the air. The research dealing with synthesis of magnetocaloric materials based of Ni-Al Heusler Alloy structure and by varying substitution some atoms of Ni with Fe and Al with Mn on Ni-Al Heusler Alloy structure to become Ni{sub 44}Fe{sub 6}Mn{sub 32}Al{sub 18}. Vacuum Arc Melting (VAM) equipment is used to form the alloys on vacuum condition and by flowing argon gas atmosphere and then followed by annealing process for 72 hours. X-Ray Diffraction (XRD)more » reveals that crystallite structure of material is observed. We define that Ni{sub 44}Fe{sub 6} as X{sub 2}, Mn{sub 25} as Y, and Al{sub 18}Mn{sub 7} as Z. Based on the XRD result, we observed that the general formula X{sub 2}YZ is not changed. The PERMAGRAF measurement revealed that there exists of magnetic hysterysis. The hysterysis show that the magnetic structures of the system undego evolution from diamagnetic to soft ferromagnetic material which all of the compound have the same crystallite structure. This evolution indicated that the change in the composition has led to changes the magnetic composition. Mn is the major element that gives strong magnetic properties to the sample. When Mn partially replaced position of Al, the sample became dominant to be influenced to improve their magnetic properties. In addition, substitution a part of Ni by Fe in the composition reveals a pinning of the domain walls in the sample.« less

High-Temperature Wettability and Interactions between Y-Containing Ni-Based Alloys and Various Oxide Ceramics.

PubMed

Li, Jinpeng; Zhang, Huarui; Gao, Ming; Li, Qingling; Bian, Weidong; Tao, Tongxiang; Zhang, Hu

2018-05-07

To obtain appropriate crucible materials for vacuum induction melting of MCrAlY alloys, four different oxide ceramics, including MgO, Y₂O₃, Al₂O₃, and ZrO₂, with various microstructures were designed and characterized. The high-temperature wettability and interactions between Ni-20Co-20Cr-10Al-1.5Y alloys and oxide ceramics were studied by sessile drop experiments under vacuum. The results showed that all the systems exhibited non-wetting behavior. The contact angles were stable during the melting process of alloys and the equilibrium contact angles were 140° (MgO), 148° (Y₂O₃), 154° (Al₂O₃), and 157° (ZrO₂), respectively. The interfacial reaction between the ceramic substrates and alloys occurred at high temperature. Though the ceramics had different microstructures, similar continuous Y₂O₃ reaction layer with thicknesses of about 25 μm at the alloy-ceramic interface in MgO, Al₂O₃, and ZrO₂ systems formed. The average area percentage of oxides in the alloy matrices were 0.59% (MgO), 0.11% (Al₂O₃), 0.09% (ZrO₂), and 0.02% (Y₂O₃), respectively. The alloys, after reacting with MgO ceramic, had the highest inclusion content, while those with the lowest content were in the Y₂O₃ system. Y₂O₃ ceramic was the most beneficial for vacuum induction melting of high-purity Y-containing Ni-based alloys.

Solvent Free Low-Melt Viscosity Imide Oligomers And Thermosetting Polyimide Composites

NASA Technical Reports Server (NTRS)

Chuang, CHun-Hua (Inventor)

2006-01-01

This invention relates to the composition and a solvent-free process for preparing novel imide oligomers and polymers specifically formulated with effective amounts of a dianhydride such as 2,3,3',4-biphenyltetra carboxylic dianydride (a-BPDA), at least one aromatic diamine' and an endcapped of 4-phenylethynylphthalic anhydride (PEPA) or nadic anhydride to produce imide oligomers that possess a low-melt viscosity of 1-60 poise at 260-280" C. When the imide oligomer melt is cured at about 371 C. in a press or autoclave under 100-500 psi, the melt resulted in a thermoset polyimide having a glass transition temperature (T(sub g)) equal to and above 310 C. A novel feature of this process is that the monomers; namely the dianhydrides, diamines and the endcaps, are melt processable to form imide oligomers at temperatures ranging between 232-280 C. (450-535 F) without any solvent. These low-melt imide oligomers can be easily processed by resin transfer molding (RTM), vacuum-assisted resin transfer molding (VARTM) or the resin infusion process with fiber preforms e.g. carbon, glass or quartz preforms to produce polyimide matrix composites with 288-343C (550-650 F) high temperature performance capability.

Surface Fatigue Tests Of M50NiL Gears And Bars

NASA Technical Reports Server (NTRS)

Townsend, Dennis P.; Bamberger, Eric N.

1994-01-01

Report presents results of tests of steels for use in gears and bearings of advanced aircraft. Spur-gear endurance tests and rolling-element surface fatigue tests performed on gear and bar specimens of M50NiL steel processed by vacuum induction melting and vacuum arc remelting (VIM-VAR). Compares results of tests with similar tests of specimens of VIM-VAR AISI 9310 steel and of AISI 9310 steel subjected to VAR only.

Automatic thermocouple positioner for use in vacuum furnaces

DOEpatents

Mee, D.K.; Stephens, A.E.

1980-06-06

The invention is a simple and reliable mechanical arrangement for automatically positioning a thermocouple-carrying rod in a vacuum-furnace assembly of the kind including a casing, a furnace mounted in the casing, and a charge-containing crucible mounted in the furnace for vertical movement between a lower (loading) position and a raised (charge-melting) position. In a preferred embodiment, a welded-diaphragm metal bellows is mounted above the furnace, the upper end of the bellows being fixed against movement and the lower end of the bellows being affixed to support means for a thermocouple-carrying rod which is vertically oriented and extends freely through the furnace lid toward the mouth of the crucible. The support means and rod are mounted for relative vertical movement. Before pumpdown of the furnace, the differential pressure acting on the bellows causes it to contract and lift the thermocouple rod to a position where it will not be contacted by the crucible charge when the crucible is elevated to its raised position. During pumpdown, the bellows expands downward, lowering the thermocouple rod and its support. The bellows expands downward beyond a point where downward movement of the thermocouple rod is arrested by contact with the crucible charge and to a point where the upper end of the thermocouple extends well above the thermocouple support. During subsequent melting of the charge, the thermocouple sinks into the melt to provide an accurate measurement of melt temperatures.

Automatic thermocouple positioner for use in vacuum furnaces

DOEpatents

Mee, David K.; Stephens, Albert E.

1981-01-01

The invention is a simple and reliable mechanical arrangement for automatically positioning a thermocouple-carrying rod in a vacuum-furnace assembly of the kind including a casing, a furnace mounted in the casing, and a charge-containing crucible mounted in the furnace for vertical movement between a lower (loading) position and a raised (charge-melting) position. In a preferred embodiment, a welded-diaphragm metal bellows is mounted above the furnace, the upper end of the bellows being fixed against movement and the lower end of the bellows being affixed to support means for a thermocouple-carrying rod which is vertically oriented and extends freely through the furnace lid toward the mouth of the crucible. The support means and rod are mounted for relative vertical movement. Before pumpdown of the furnace, the differential pressure acting on the bellows causes it to contract and lift the thermocouple rod to a position where it will not be contacted by the crucible charge when the crucible is elevated to its raised position. During pumpdown, the bellows expands downward, lowering the thermocouple rod and its support. The bellows expands downward beyond a point where downward movement of the thermocouple rod is arrested by contact with the crucible charge and to a point where the upper end of the thermocouple extends well above the thermocouple support. During subsequent melting of the charge, the thermocouple sinks into the melt to provide an accurate measurement of melt temperatures.

Structural Characteristics and In Vitro Biodegradation of a Novel Zn-Li Alloy Prepared by Induction Melting and Hot Rolling

NASA Astrophysics Data System (ADS)

Zhao, Shan; McNamara, Cameron T.; Bowen, Patrick K.; Verhun, Nicholas; Braykovich, Jacob P.; Goldman, Jeremy; Drelich, Jaroslaw W.

2017-03-01

Zinc shows great promise as a bioabsorbable metal; however, the low tensile strength of pure zinc limits its application for endovascular stent purposes. In this study, a new Zn- xLi alloy (with x = 2, 4, 6 at. pct) was prepared by induction melting in an argon atmosphere and processed through hot rolling. Structures of the formulated binary alloys were characterized by X-ray diffraction and optical microscopy. Mechanical testing showed that the incorporation of Li into Zn increased ultimate tensile strength from <120 MPa (pure Zn) to >560 MPa ( x = 6 at. pct). In vitro corrosion behavior was evaluated by immersion tests in simulated body fluid. The Zn-2Li and Zn-4Li corrosion study demonstrated that corrosion rates and products resemble those observed for pure Zn in vivo, and in addition, the Zn-4Li alloy exhibits higher resistance to corrosion as compared to Zn-2Li. The findings herein encourage further exploration of Zn-Li systems for structural use in biomedical vascular support applications with the ultimate goal of simplifying stent procedures, thereby reducing stent-related complications.

Evaluation of the physicochemical properties and compaction behavior of melt granules produced in microwave-induced and conventional melt granulation in a single pot high shear processor.

PubMed

Loh, Z H; Sia, B Y; Heng, Paul W S; Lee, C C; Liew, Celine V

2011-12-01

Recently, microwave-induced melt granulation was shown to be a promising alternative to conventional melt granulation with improved process monitoring capabilities. This study aimed to compare the physicochemical and compaction properties of granules produced from microwave-induced and conventional melt granulation. Powder admixtures comprising equivalent proportions by weight of lactose 200 M and anhydrous dicalcium phosphate were granulated with polyethylene glycol 3350 under the influence of microwave-induced and conventional heating in a 10-L single pot high shear processor. The properties of the granules and compacts produced from the two processes were compared. Relative to conventional melt granulation, the rates at which the irradiated powders heated up in microwave-induced melt granulation were lower. Agglomerate growth proceeded at a slower rate, and this necessitated longer massing durations for growth induction. These factors prompted greater evaporative moisture losses from the melt granules. Additionally, nonuniform heating of the powders under the influence of microwaves led to increased inter-batch variations in the binder contents of resultant melt granules and a reliance of content homogeneity on massing duration. Agglomerate growth proceeded more rapidly under the influence of conventional heating due to the enhanced heating capabilities of the powders. Melt granules produced using the conventional method possessed higher moisture contents and improved content homogeneity. The compaction behavior of melt granules were affected by their mean sizes, porosities, flow properties, binder, and moisture contents. The last two factors were responsible for the disparities in compaction behavior of melt granules produced from microwave-induced and conventional melt granulation.

Ion sampling and transport in Inductively Coupled Plasma Mass Spectrometry

NASA Astrophysics Data System (ADS)

Farnsworth, Paul B.; Spencer, Ross L.

2017-08-01

Quantitative accuracy and high sensitivity in inductively coupled plasma mass spectrometry (ICP-MS) depend on consistent and efficient extraction and transport of analyte ions from an inductively coupled plasma to a mass analyzer, where they are sorted and detected. In this review we examine the fundamental physical processes that control ion sampling and transport in ICP-MS and compare the results of theory and computerized models with experimental efforts to characterize the flow of ions through plasma mass spectrometers' vacuum interfaces. We trace the flow of ions from their generation in the plasma, into the sampling cone, through the supersonic expansion in the first vacuum stage, through the skimmer, and into the ion optics that deliver the ions to the mass analyzer. At each stage we consider idealized behavior and departures from ideal behavior that affect the performance of ICP-MS as an analytical tool.

Control of electromagnetic stirring by power focusing in large induction crucible furnaces

NASA Astrophysics Data System (ADS)

Frizen, V. E.; Sarapulov, F. N.

2011-12-01

An approach is proposed for the calculation of the operating conditions of an induction crucible furnace at the final stage of melting with the power focused in various regions of melted metal. The calculation is performed using a model based on the method of detailed magnetic equivalent circuits. The combination of the furnace and a thyristor frequency converter is taken into account in modeling.

Dehydration and melting experiments constrain the fate of subducted sediments

NASA Astrophysics Data System (ADS)

Johnson, Marie C.; Plank, Terry

1999-12-01

Geochemical tracers demonstrate that elements are cycled from subducted sediments into the arc melting regime at subduction zones, although the transfer mechanism is poorly understood. Are key elements (Th, Be, Rb) lost during sediment dehydration or is sediment melting required? To investigate this question, we conducted phase equilibria and trace element partitioning experiments on a pelagic red clay for conditions appropriate to the slab beneath arc volcanoes (2-4 GPa, 600°-1000°C). Using both piston cylinders and multianvils, we determined the solidus, phase stabilities, and major element compositions of coexisting phases. The solidus (H2O + Cl fluid-saturated) was located at 775 +/- 25°C at 2 GPa, 810 +/- 15°C at 3 GPa, and 1025 +/- 25°C at 4 GPa with noevidence for complete miscibility between melt and fluid. This sediment composition produces a profusion of phases both above and below the solidus: garnet, jadeitic pyroxene, alkali-rich amphibole, phengite, biotite, magnetite, coesite, kyanite, apatite, zircon, Cl-rich fluids, and peraluminous to peralkaline granitic melts. At 2 GPa the phengite dehydration solidus is at 800°-825°C, while biotite breaks down between 850° and 900°C. To explore trace element partitioning across the solidus at 2 GPa, we used diamonds to trap fluids and melts. Both the bulk sediment residues and diamond traps were analyzed postexperiment by inductively coupled plasma-mass spectrometry (ICP-MS) and inductively coupled plasma-atomic emission spectrometry (ICP-AES) for 40 elements for which we calculated bulk partition coefficients (D = Csolid/Cfluid). Below the solidus, Rb, Sr, Ba, and Pb showed the greatest mobility (D ~ 0.5-1.0), while at the solidus, Th and Be became notably partitioned into the melt (D values changing from >2.0 to <1.0). K and Rb D values fall below 1.0 when the micas breakdown. Only at the solidus do Th and Rb attain similar partition coefficients, a condition required by arc data. Taken together, the

Dehydration and melting experiments constrain the fate of subducted sediments

NASA Astrophysics Data System (ADS)

Johnson, Marie C.; Plank, Terry

2000-12-01

Geochemical tracers demonstrate that elements are cycled from subducted sediments into the arc melting regime at subduction zones, although the transfer mechanism is poorly understood. Are key elements (Th, Be, Rb) lost during sediment dehydration or is sediment melting required? To investigate this question, we conducted phase equilibria and trace element partitioning experiments on a pelagic red clay for conditions appropriate to the slab beneath arc volcanoes (2-4 GPa, 600°-1000°C). Using both piston cylinders and multianvils, we determined the solidus, phase stabilities, and major element compositions of coexisting phases. The solidus (H2O + Cl fluid-saturated) was located at 775 ± 25°C at 2 GPa, 810 ± 15°C at 3 GPa, and 1025 ± 25°C at 4 GPa with noevidence for complete miscibility between melt and fluid. This sediment composition produces a profusion of phases both above and below the solidus: garnet, jadeitic pyroxene, alkali-rich amphibole, phengite, biotite, magnetite, coesite, kyanite, apatite, zircon, Cl-rich fluids, and peraluminous to peralkaline granitic melts. At 2 GPa the phengite dehydration solidus is at 800°-825°C, while biotite breaks down between 850° and 900°C. To explore trace element partitioning across the solidus at 2 GPa, we used diamonds to trap fluids and melts. Both the bulk sediment residues and diamond traps were analyzed postexperiment by inductively coupled plasma-mass spectrometry (ICP-MS) and inductively coupled plasma-atomic emission spectrometry (ICP-AES) for 40 elements for which we calculated bulk partition coefficients (D = Csolid/Cfluid). Below the solidus, Rb, Sr, Ba, and Pb showed the greatest mobility (D ˜ 0.5-1.0), while at the solidus, Th and Be became notably partitioned into the melt (D values changing from >2.0 to <1.0). K and Rb D values fall below 1.0 when the micas breakdown. Only at the solidus do Th and Rb attain similar partition coefficients, a condition required by arc data. Taken together, the

Metals purification by improved vacuum arc remelting

DOEpatents

Zanner, Frank J.; Williamson, Rodney L.; Smith, Mark F.

1994-12-13

The invention relates to improved apparatuses and methods for remelting metal alloys in furnaces, particularly consumable electrode vacuum arc furnaces. Excited reactive gas is injected into a stationary furnace arc zone, thus accelerating the reduction reactions which purify the metal being melted. Additionally, a cooled condensation surface is disposed within the furnace to reduce the partial pressure of water in the furnace, which also fosters the reduction reactions which result in a purer produced ingot. Methods and means are provided for maintaining the stationary arc zone, thereby reducing the opportunity for contaminants evaporated from the arc zone to be reintroduced into the produced ingot.

Process for alloying uranium and niobium

DOEpatents

Holcombe, Cressie E.; Northcutt, Jr., Walter G.; Masters, David R.; Chapman, Lloyd R.

1991-01-01

Alloys such as U-6Nb are prepared by forming a stacked sandwich array of uraniun sheets and niobium powder disposed in layers between the sheets, heating the array in a vacuum induction melting furnace to a temperature such as to melt the uranium, holding the resulting mixture at a temperature above the melting point of uranium until the niobium dissolves in the uranium, and casting the uranium-niobium solution. Compositional uniformity in the alloy product is enabled by use of the sandwich structure of uranium sheets and niobium powder.

The influence of melt composition on the partitioning of REEs, Y, Sc, Zr and Al between forsterite and melt in the system CMAS

NASA Astrophysics Data System (ADS)

Evans, Thomas M.; O'Neill, Hugh St. C.; Tuff, James

2008-12-01

Partition coefficients for a range of Rare Earth Elements (REEs), Y, Sc, Al and Zr were determined between forsteritic olivine (nearly end-member Mg 2SiO 4) and ten melt compositions in the system CaO-MgO-Al 2O 3-SiO 2 (CMAS) at 1 bar and 1400 °C, with concentrations of the trace elements in the olivine and the melt measured by laser-ablation inductively coupled plasma mass spectrometry (LA-ICP-MS). The REEs and Sc were added at levels sufficient to ensure that concentrations in the olivine were well above the detection limits. The REE partition coefficients (DREEol/melt) decrease with increasing silica in the melt, indicating strong bonding between REEO 1.5 and SiO 2 in the melt. The variation of DREEol/melt as a function of ionic radius is well described by the Brice equation for each composition, although a small proportion of this variation is due to the increase in the strength of the REEO 1.5-SiO 2 interactions in the melt with ionic radius. Scandium behaves very similarly to the REEs, but a global fit of the data from all ten melt compositions suggests that DScol/melt deviates somewhat from the parabolas established by the REE and Y, implying that Sc may substitute into olivine differently to that of the REEs. In contrast to the behaviour of the large trivalent cations, the concentration of Al in olivine is proportional to the square root of its concentration in the melt, indicating a coupled substitution in olivine with a high degree of short-range order. The lack of any correlation of REE partition coefficients with Al in olivine or melt suggests that the REE substitution in olivine is charge-balanced by cation vacancies. The partition coefficient of the tetravalent trace element Zr, which is highly incompatible in olivine, depends on the CaO content of the melt.

Experimental Determination of Spinel/Melt, Olivine/Melt, and Pyroxene/Melt Partition Coefficients for Re, Ru, Pd, Au, and Pt

NASA Technical Reports Server (NTRS)

Righter, K.; Campbell, A. J.; Humayun, M.

2003-01-01

Experimental studies have identified spinels as important hosts phases for many of the highly siderophile elements (HSE). Yet experimental studies involving chromite or Cr-rich spinel have been lacking. Experimental studies of partitioning of HSEs between silicate, oxides and silicate melt are plagued by low solubilities and the presence of small metallic nuggets at oxygen fugacities relevant to magmas, which interfere with analysis of the phases of interest. We have circumvented these problems in two ways: 1) performing experiments at oxidized conditions, which are still relevant to natural systems but in which nuggets are not observed, and 2) analysis of run products with laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS), allowing a combination of high sensitivity and good spatial resolution.

Preparation of Aluminum-Zirconium Master Alloy by Aluminothermic Reduction in Cryolite Melt

NASA Astrophysics Data System (ADS)

Liu, Fengguo; Ding, Chenliang; Tao, Wenju; Hu, Xianwei; Gao, Bingliang; Shi, Zhongning; Wang, Zhaowen

2017-12-01

Al-Zr master alloy was prepared by aluminothermic reduction in cryolite melt without alumina impurity. The Al-Zr master alloy was characterized by x-ray diffraction, scanning electron microscopy, and energy-dispersive spectroscopy. The composition of the master alloy was analyzed by inductively coupled plasma optical emission spectrometry. The results indicated that Al-Zr master alloy with high purity could be obtained when byproduct Al2O3 was dissolved in the cryolite melt. The Al-Zr alloy was embedded in the Al matrix in the form of Al3Zr phase with long rod or tetragonal morphology due to temperature variation. Finally, we obtained Al-Zr alloy with 7 wt.% Zr by aluminothermic reduction for 90 min in cryolite melt at 980°C.

11. VIEW OF DEPLETED URANIUM INGOT. THE METALS WERE PLACED ...

Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

11. VIEW OF DEPLETED URANIUM INGOT. THE METALS WERE PLACED IN CRUCIBLES, LOADED INTO ONE OF EIGHT INDUCTION FURNACES AND MELTED IN A VACUUM ATMOSPHERE. (11/11/57) - Rocky Flats Plant, Non-Nuclear Production Facility, South of Cottonwood Avenue, west of Seventh Avenue & east of Building 460, Golden, Jefferson County, CO

Technology and equipment based on induction melters with ``cold'' crucible for reprocessing active metal waste

NASA Astrophysics Data System (ADS)

Pastushkov, V. G.; Molchanov, A. V.; Serebryakov, V. P.; Smelova, T. V.; Shestoperov, I. N.

2000-07-01

The paper discusses specific features of technology, equipment and control of a single stage RAMW decontamination and melting process in an induction furnace equipped with a "cold" crucible. The calculated and experimental data are given on melting high activity level stainless steel and Zr simulating high activity level metal waste. The work is under way in SSC RF VNIINM.

Inductive detection of the free surface of liquid metals

NASA Astrophysics Data System (ADS)

Zürner, Till; Ratajczak, Matthias; Wondrak, Thomas; Eckert, Sven

2017-11-01

A novel measurement system to determine the surface position and topology of liquid metals is presented. It is based on the induction of eddy currents by a time-harmonic magnetic field and the subsequent measurement of the resulting secondary magnetic field using gradiometric induction coils. The system is validated experimentally for static and dynamic surfaces of the low-melting liquid metal alloy gallium-indium-tin in a narrow vessel. It is shown that a precision below 1 mm and a time resolution of at least 20 Hz can be achieved.

Induction heating of planetary interiors

NASA Astrophysics Data System (ADS)

Kislyakova, K.; Noack, L.; Johnstone, C. P.; Zaitsev, V. V.; Fossati, L.; Lammer, H.; Khodachenko, M. L.; Odert, P.; Güdel, M.

2017-09-01

We present a calculation of the energy release in planetary interiors caused by induction heating. If an exoplanet orbits a host star with a strong magnetic field, it will be embedded in periodically varying magnetic environment. In our work, we consider only a dipole field of the host star and assume the dipole axis to be inclined with respect to the stellar rotational axis, which causes the magnetic field to vary. In this case, the varying magnetic field surrounding the planet will generate induction currents inside the planetary mantle, which will dissipate in the planetary interiors. We show that this energy release can be very substantial and in some cases even lead to complete melting of the planetary mantle over geological timescales, accompanied by the enhanced magnetic activity.

Xenon Release by the In-Vacuum Etching of Aerogel: Implications for the Study of Noble Gases in Comet Wild 2 Stardust

NASA Astrophysics Data System (ADS)

O'Mara, A.; Busemann, H.; Clay, P. L.; Crowther, S. A.; Gilmour, J. D.; Wieler, R.

2014-09-01

Xenon detection in comet Wild 2 stardust is hampered by the large adsorption of Xe on aerogel. In-vacuum etching presented here may enable the stepwise separation of terrestrial Xe, cometary Xe trapped in melted aerogel and Xe in cometary silicates.

Incorporation and distribution of rhenium in a borosilicate glass melt heat treated in a sealed ampoule

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kim, Dong-Sang; Schweiger, Michael J.

2013-07-25

We investigated a mass balance of rhenium (used as a surrogate for technetium-99) in a borosilicate glass that was mixed with excess Re source (KReO4) beyond its solubility and heat treated in a vacuum-sealed fused silica ampoule. Distribution of Re in the bulk of the glass, in a salt phase formed on the melt surface, and in condensate material deposited on the ampoule wall was evaluated to understand the Re migration into different phases during the reaction between the molten glass and KReO4. The information gained from this study will contribute to an effort to understand the mechanism of technetiummore » retention in or escape from glass melt during early stages of glass batch melting, which is a goal of the present series of studies.« less

Indian Vacuum Society: The Indian Vacuum Society

NASA Astrophysics Data System (ADS)

Saha, T. K.

2008-03-01

The Indian Vacuum Society (IVS) was established in 1970. It has over 800 members including many from Industry and R & D Institutions spread throughout India. The society has an active chapter at Kolkata. The society was formed with the main aim to promote, encourage and develop the growth of Vacuum Science, Techniques and Applications in India. In order to achieve this aim it has conducted a number of short term courses at graduate and technician levels on vacuum science and technology on topics ranging from low vacuum to ultrahigh vacuum So far it has conducted 39 such courses at different parts of the country and imparted training to more than 1200 persons in the field. Some of these courses were in-plant training courses conducted on the premises of the establishment and designed to take care of the special needs of the establishment. IVS also regularly conducts national and international seminars and symposia on vacuum science and technology with special emphasis on some theme related to applications of vacuum. A large number of delegates from all over India take part in the deliberations of such seminars and symposia and present their work. IVS also arranges technical visits to different industries and research institutes. The society also helped in the UNESCO sponsored post-graduate level courses in vacuum science, technology and applications conducted by Mumbai University. The society has also designed a certificate and diploma course for graduate level students studying vacuum science and technology and has submitted a syllabus to the academic council of the University of Mumbai for their approval, we hope that some colleges affiliated to the university will start this course from the coming academic year. IVS extended its support in standardizing many of the vacuum instruments and played a vital role in helping to set up a Regional Testing Centre along with BARC. As part of the development of vacuum education, the society arranges the participation of

Characterization of hydrotreated Mayan and Wilmington vacuum tower bottoms

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pearson, C.D.; Green, J.B.; Bhan, O.K.

1989-04-01

Mayan and Wilmington vacuum tower bottoms were hydrotreated at various severity levels in a batch autoclave with and without catalyst. Each of the feeds and the hydrotreated products was separated into acid-base (ABN) fraction using a unique non-aqueous ion exchange technique. The feeds, hydrotreated whole products, and the ABN fractions were characterized by determining their elemental and metal content. Selected samples were analyzed by size exclusion chromatography/inductively coupled plasma technique to determine molecular size distribution of various species.

The Generating Mechanism of Non-Sustained Disruptive Discharges in Vacuum Interrupters

NASA Astrophysics Data System (ADS)

Hara, Daisuke; Taki, Masayuki; Tanaka, Hitoshi; Okawa, Mikio; Yanabu, Satoru

To develop vacuum circuit breaker (VCB) for higher voltage application, it may be important to understand generating mechanism and its influence of non-sustained disruptive discharges (NSDD) to the systems. So, we carried out the tests using equivalent testing circuit and observed the contacts after testing, For the test, by using commercial vacuum circuit interrupters, AC voltages of 50Hz was applied between contacts for 4 seconds after current interruption, and measured generating frequencies of NSDD vs. the voltages and vs. currents. Typical contact material used in the commercial switching equipment, such as AgWC, CuW, CuCr were tested and compared. Then CuCr's of different composition and manufacturing process are investigated. And CuCr-50 (manufactured by melting process) showed the best performance in all tests. We point out that surface condition may affect the generation of NSDD and also conditioning effect is very important.

Controlling superconductivity in La 2-xSr xCuO 4+δ by ozone and vacuum annealing

DOE PAGES

Leng, Xiang; Bozovic, Ivan

2014-11-21

In this study we performed a series of ozone and vacuum annealing experiments on epitaxial La 2-xSr xCuO 4+δ thin films. The transition temperature after each annealing step has been measured by the mutual inductance technique. The relationship between the effective doping and the vacuum annealing time has been studied. Short-time ozone annealing at 470 °C oxidizes an underdoped film all the way to the overdoped regime. The subsequent vacuum annealing at 350 °C to 380 °C slowly brings the sample across the optimal doping point back to the undoped, non-superconducting state. Several ozone and vacuum annealing cycles have beenmore » done on the same sample and the effects were found to be repeatable and reversible Vacuum annealing of ozone-loaded LSCO films is a very controllable process, allowing one to tune the doping level of LSCO in small steps across the superconducting dome, which can be used for fundamental physics studies.« less

Controlling superconductivity in La 2-xSr xCuO 4+δ by ozone and vacuum annealing

DOE Office of Scientific and Technical Information (OSTI.GOV)

Leng, Xiang; Bozovic, Ivan

In this study we performed a series of ozone and vacuum annealing experiments on epitaxial La 2-xSr xCuO 4+δ thin films. The transition temperature after each annealing step has been measured by the mutual inductance technique. The relationship between the effective doping and the vacuum annealing time has been studied. Short-time ozone annealing at 470 °C oxidizes an underdoped film all the way to the overdoped regime. The subsequent vacuum annealing at 350 °C to 380 °C slowly brings the sample across the optimal doping point back to the undoped, non-superconducting state. Several ozone and vacuum annealing cycles have beenmore » done on the same sample and the effects were found to be repeatable and reversible Vacuum annealing of ozone-loaded LSCO films is a very controllable process, allowing one to tune the doping level of LSCO in small steps across the superconducting dome, which can be used for fundamental physics studies.« less

Petrological Geodynamics of Mantle Melting II. AlphaMELTS + Multiphase Flow: Dynamic Fractional Melting

NASA Astrophysics Data System (ADS)

Tirone, Massimiliano

2018-03-01

In this second installment of a series that aims to investigate the dynamic interaction between the composition and abundance of the solid mantle and its melt products, the classic interpretation of fractional melting is extended to account for the dynamic nature of the process. A multiphase numerical flow model is coupled with the program AlphaMELTS, which provides at the moment possibly the most accurate petrological description of melting based on thermodynamic principles. The conceptual idea of this study is based on a description of the melting process taking place along a 1-D vertical ideal column where chemical equilibrium is assumed to apply in two local sub-systems separately on some spatial and temporal scale. The solid mantle belongs to a local sub-system (ss1) that does not interact chemically with the melt reservoir which forms a second sub-system (ss2). The local melt products are transferred in the melt sub-system ss2 where the melt phase eventually can also crystallize into a different solid assemblage and will evolve dynamically. The main difference with the usual interpretation of fractional melting is that melt is not arbitrarily and instantaneously extracted from the mantle, but instead remains a dynamic component of the model, hence the process is named dynamic fractional melting (DFM). Some of the conditions that may affect the DFM model are investigated in this study, in particular the effect of temperature, mantle velocity at the boundary of the mantle column. A comparison is made with the dynamic equilibrium melting (DEM) model discussed in the first installment. The implications of assuming passive flow or active flow are also considered to some extent. Complete data files of most of the DFM simulations, four animations and two new DEM simulations (passive/active flow) are available following the instructions in the supplementary material.

Effect of sugar additives on stability of human serum albumin during vacuum foam drying and storage.

PubMed

Hajare, A A; More, H N; Pisal, S S

2011-11-01

No literature on the protein stabilization of human serum albumin (HSA) by vacuum foam drying (VFD) has been reported. The purpose of this study was to investigate the effect of sugar-additive systems on the stability of HSA by VFD. For the assessment, HSA was formulated with sucrose and mannitol, respectively, alone or in combination with stabilizers, which were vacuum foam dried and stored at 25C. Protein content of the resulting dried formulations was analyzed by Lowry method. Fourier-transform infrared spectroscopy (FT-IR) analysis of the HSA secondary structure showed apparent protein structure-stabilizing effects of the amorphous sugar and phosphate combination during the VFD. In particular, sucrose-sodium phosphate monobasic mixture provide an interesting alternative to pure saccharide formulations due to their high glass transition temperatures and their increased ability to maintain a low melting transition temperature in the presence of small amounts of water. Inhibition of the sucrose crystallization in solutions under vacuum resulted in highly amorphous sucrose. Changes in the endothermic melting transition suggested reduced sucrose molecular mobility with increase in the sodium phosphate ratio. The addition of phosphate salts to sugar systems has several interesting features that merit its consideration in formulations to protect dehydrated labile biomaterials. In conclusion, our data suggest that sucrose and phosphate as additives seem to protect HSA during VFD better than lyophilized products and also maintain its stability in the VFD state during storage.

Shock melting and vaporization of metals.

NASA Technical Reports Server (NTRS)

Ahrens, T. J.

1972-01-01

The effect of initial porosity on shock induction of melting and vaporization is investigated for Ba, Sr, Li, Fe, Al, U, and Th. For the less compressible of these metals, it is found that for a given strong shock-generation system (explosive in contact, or flyer-plate impact) an optimum initial specific volume exists such that the total entropy production, and hence the amount of metal liquid or vapor, is a maximum. Initial volumes from 1.4 to 2.0 times crystal volumes, depending on the metal sample and shock-inducing system, will result in optimum post-shock entropies.

Melt-Vapor Phase Diagram of the Te-S System

NASA Astrophysics Data System (ADS)

Volodin, V. N.; Trebukhov, S. A.; Kenzhaliyev, B. K.; Nitsenko, A. V.; Burabaeva, N. M.

2018-03-01

The values of partial pressure of saturated vapor of the constituents of the Te-S system are determined from boiling points. The boundaries of the melt-vapor phase transition at atmospheric pressure and in vacuum of 2000 and 100 Pa are calculated on the basis of partial pressures. A phase diagram that includes vapor-liquid equilibrium fields whose boundaries allow us to assess the behavior of elements upon distillation fractioning is plotted. It is established that the separation of elements is possible at the first evaporation-condensation cycle. Complications can be caused by crystallization of a sulfur solid solution in tellurium.

Crystallization of rhenium salts in a simulated low-activity waste borosilicate glass

DOE Office of Scientific and Technical Information (OSTI.GOV)

Riley, Brian J.; McCloy, John S.; Goel, Ashutosh

2013-04-01

This study presents a new method for looking at the solubility of volatile species in simulated low-activity waste glass. The present study looking at rhenium salts is also applicable to real applications involving radioactive technetium salts. In this synthesis method, oxide glass powder is mixed with the volatiles species, vacuum-sealed in a fused quartz ampoule, and then heat-treated under vacuum in a furnace. This technique restricts the volatile species to the headspace above the melt but still within the sealed ampoule, thus maximizing the volatile concentration in contact with the glass. Various techniques were used to measure the solubility ofmore » rhenium in glass and include energy dispersive spectroscopy, wavelength dispersive spectroscopy, laser ablation inductively-coupled plasma mass spectroscopy, and inductively-coupled plasma optical emission spectroscopy. The Re-solubility in this glass was determined to be ~3004 parts per million Re atoms. Above this concentration, the salts separated out of the melt as inclusions and as a low viscosity molten salt phase on top of the melt observed during and after cooling. This salt phase was analyzed with X-ray diffraction, scanning electron microscopy as well as some of the other aforementioned techniques and identified to be composed of alkali perrhenate and alkali sulfate.« less

Melting Processes at the Base of the Mantle Wedge: Melt Compositions and Melting Reactions for the First Melts of Vapor-Saturated Lherzolite

NASA Astrophysics Data System (ADS)

Grove, T. L.; Till, C. B.

2014-12-01

Vapor-saturated melting experiments have been performed at pressures near the base of the mantle wedge (3.2 GPa). The starting composition is a metasomatized lherzolite containing 3 wt. % H2O. Near-solidus melts and coexisting mineral phases have been characterized in experiments that span 925 to 1100 oC with melt % varying from 6 to 9 wt. %. Olivine, orthopyroxene, clinopyroxene and garnet coexist with melt over the entire interval and rutile is also present at < 1000 oC. Melt is andesitic in composition and varies from 60 wt. % SiO2 at 950 oC to 52 wt. % at 1075 oC. The Al2O3 contents of the melt are 13 to 14 wt. %, and CaO contents range from 1 and 4 wt. %. Melting is peritectic with orthopyroxene + liquid produced by melting of garnet + olivine + high-Ca pyroxene. In addition to quenched melt, we observe a quenched silicate component that is rhyolitic (>72 % SiO2) that we interpret as a precipitate from the coexisting supercritical H2O-rich vapor. Extrapolation of the measured compositional variation toward the solidus suggests that the first melt may be very SiO2 rich (i.e., granitic). We suggest that these granitic melts are the first melts of the mantle near the slab-wedge interface. As these SiO2-rich melts ascend into shallower, hotter overlying mantle, they continue to interact with the surrounding mantle and evolve in composition. These first melts may elucidate the geochemical and physical processes that accompany the beginnings of H2O flux melting.

Evaluation of the Mechanical Properties of Electroslag Refined Fe-12Ni Alloys

NASA Technical Reports Server (NTRS)

Bhat, G. K.

1978-01-01

Three Fe-12Ni alloys, individually alloyed with small amounts of V, Ti, and Al, were manufactured through different melting techniques, with special emphasis on electroslag remelting, in order to achieve different levels of metal purity and associated costs. The relative effectiveness of these melting techniques was evaluated from tensile and slow bend fracture toughness behavior at 25 C and -196 C after tempering the test specimens at various temperatures. The best melting procedure was vacuum induction melting (VIM) with or without electroslag remelting (ESR). VIM+ESR is the recommended procedure since ESR provides increased yield of plate product, a reduction of overall manufacturing costs and, depending on the alloy composition, improved tensile and fracture toughness properties.

Boron and Zirconium from Crucible Refractories in a Complex Heat-Resistant Alloy

NASA Technical Reports Server (NTRS)

Decker, R F; Rowe, John P; Freeman, J W

1958-01-01

In a laboratory study of the factors involved in the influence of induction vacuum melting on 55ni-20cr-15co-4mo-3ti-3al heat resistant alloy, it was found that the major factor was the type of ceramic used as the crucible. The study concluded that trace amounts of boron or zirconium derived from reaction of the melt with the crucible refactories improved creep-rupture properties at 1,600 degrees F. Boron was most effective and, in addition, markedly improved hot-workability.

Vacuum mechatronics

NASA Technical Reports Server (NTRS)

Hackwood, Susan; Belinski, Steven E.; Beni, Gerardo

1989-01-01

The discipline of vacuum mechatronics is defined as the design and development of vacuum-compatible computer-controlled mechanisms for manipulating, sensing and testing in a vacuum environment. The importance of vacuum mechatronics is growing with an increased application of vacuum in space studies and in manufacturing for material processing, medicine, microelectronics, emission studies, lyophylisation, freeze drying and packaging. The quickly developing field of vacuum mechatronics will also be the driving force for the realization of an advanced era of totally enclosed clean manufacturing cells. High technology manufacturing has increasingly demanding requirements for precision manipulation, in situ process monitoring and contamination-free environments. To remove the contamination problems associated with human workers, the tendency in many manufacturing processes is to move towards total automation. This will become a requirement in the near future for e.g., microelectronics manufacturing. Automation in ultra-clean manufacturing environments is evolving into the concept of self-contained and fully enclosed manufacturing. A Self Contained Automated Robotic Factory (SCARF) is being developed as a flexible research facility for totally enclosed manufacturing. The construction and successful operation of a SCARF will provide a novel, flexible, self-contained, clean, vacuum manufacturing environment. SCARF also requires very high reliability and intelligent control. The trends in vacuum mechatronics and some of the key research issues are reviewed.

Preparation of low strategic metal content superalloys

NASA Technical Reports Server (NTRS)

Sczerzenie, F. E.; Maurer, G. E.

1982-01-01

The properties of modified NIMONIC 115 and UDIMET 720 with reduced levels of cobalt were evaluated. Vacuum induction melted and vacuum arc remelted ingots were hot rolled to 3/4 inch diameter bar. Hot workability was evaluated in terms of the ingot rolling behavior and the hot ductility of the as-rolled bar. Variations in workability and bar ductility were correlated to variations in incipient melting temperature and gamma prime solvus, both of which varied with cobalt content. Heat treatments were defined to yield, as far as possible, similar structures from alloy to alloy. At the lowest cobalt levels N-115 workability was severely limited and the alloys could not be worked to bar. It is suggested that incipient melting in combination with heavy grain boundary carbide precipitation reduced ingot workability. Final heat treatment of modified alloys was difficult in the situation where the gamma prime solvus temperature was close to the incipient melting point, indicating that it may not be feasible to fully solution low cobalt alloys to obtain the large grain size required for optimum creep resistance.

Scale up of NiTi shape memory alloy production by EBM

NASA Astrophysics Data System (ADS)

Otubo, J.; Rigo, O. D.; Moura Neto, C.; Kaufman, M. J.; Mei, P. R.

2003-10-01

The usual process to produce NiTi shape memory alloy is by vacuum induction melting (VIM) using a graphite crucible, which causes contamination of the melt with carbon. Contamination with oxygen originates from the residual oxygen inside the melting chamber. An alternative process to produce NiTi alloys is by electron beam melting (EBM) using a water-cooled copper crucible that eliminates carbon contamination, and the oxygen contamination would be minimal due to operation in a vacuum of better than 10^{-2} Pa. In a previous work, it was demonstrated that the technique is feasible for button shaped samples weighing around 30g. The present work presents the results on the scale up program that enables the production of larger samples/ingots. The results are very promising in terms of chemical composition homogeneity as well as in terms of carbon contamination, the latter being four to ten times lower than the commercially-produced VIM products, and in terms of final oxygen content which is shown to depend primarily on the starting raw materials.

Natural vacuum electronics

NASA Technical Reports Server (NTRS)

Leggett, Nickolaus

1990-01-01

The ambient natural vacuum of space is proposed as a basis for electron valves. Each valve is an electron controlling structure similiar to a vacuum tube that is operated without a vacuum sustaining envelope. The natural vacuum electron valves discussed offer a viable substitute for solid state devices. The natural vacuum valve is highly resistant to ionizing radiation, system generated electromagnetic pulse, current transients, and direct exposure to space conditions.

Development of high purity large forgings for nuclear power plants

NASA Astrophysics Data System (ADS)

Tanaka, Yasuhiko; Sato, Ikuo

2011-10-01

The recent increase in the size of energy plants has been supported by the development of manufacturing technology for high purity large forgings for the key components of the plant. To assure the reliability and performance of the large forgings, refining technology to make high purity steels, casting technology for gigantic ingots, forging technology to homogenize the material and consolidate porosity are essential, together with the required heat treatment and machining technologies. To meet these needs, the double degassing method to reduce impurities, multi-pouring methods to cast the gigantic ingots, vacuum carbon deoxidization, the warm forging process and related technologies have been developed and further improved. Furthermore, melting facilities including vacuum induction melting and electro slag re-melting furnaces have been installed. By using these technologies and equipment, large forgings have been manufactured and shipped to customers. These technologies have also been applied to the manufacture of austenitic steel vessel components of the fast breeder reactors and components for fusion experiments.

High-Temperature Wettability and Interactions between Y-Containing Ni-Based Alloys and Various Oxide Ceramics

PubMed Central

Li, Jinpeng; Gao, Ming; Li, Qingling; Bian, Weidong; Tao, Tongxiang; Zhang, Hu

2018-01-01

To obtain appropriate crucible materials for vacuum induction melting of MCrAlY alloys, four different oxide ceramics, including MgO, Y2O3, Al2O3, and ZrO2, with various microstructures were designed and characterized. The high-temperature wettability and interactions between Ni-20Co-20Cr-10Al-1.5Y alloys and oxide ceramics were studied by sessile drop experiments under vacuum. The results showed that all the systems exhibited non-wetting behavior. The contact angles were stable during the melting process of alloys and the equilibrium contact angles were 140° (MgO), 148° (Y2O3), 154° (Al2O3), and 157° (ZrO2), respectively. The interfacial reaction between the ceramic substrates and alloys occurred at high temperature. Though the ceramics had different microstructures, similar continuous Y2O3 reaction layer with thicknesses of about 25 μm at the alloy-ceramic interface in MgO, Al2O3, and ZrO2 systems formed. The average area percentage of oxides in the alloy matrices were 0.59% (MgO), 0.11% (Al2O3), 0.09% (ZrO2), and 0.02% (Y2O3), respectively. The alloys, after reacting with MgO ceramic, had the highest inclusion content, while those with the lowest content were in the Y2O3 system. Y2O3 ceramic was the most beneficial for vacuum induction melting of high-purity Y-containing Ni-based alloys. PMID:29735958

VACUUM TRAP

DOEpatents

Gordon, H.S.

1959-09-15

An improved adsorption vacuum trap for use in vacuum systems was designed. The distinguishing feature is the placement of a plurality of torsionally deformed metallic fins within a vacuum jacket extending from the walls to the central axis so that substantially all gas molecules pass through the jacket will impinge upon the fin surfaces. T fins are heated by direct metallic conduction, thereby ol taining a uniform temperature at the adeorbing surfaces so that essentially all of the condensible impurities from the evacuating gas are removed from the vacuum system.

Solid sulfur in vacuum: Sublimation effects on surface microtexture, color and spectral reflectance, and applications to planetary surfaces

NASA Technical Reports Server (NTRS)

Nash, D. B.

1987-01-01

A form of sulfur that is white at room temperature and very fluffy in texture has been found in laboratory experiments on the effects of vacuum sublimation (evaporation) on solid sulfur. This work is an outgrowth of proton sputtering experiments on sulfur directed toward understanding Jovian magnetospheric effects on the surface of Io. Fluffy white sulfur is formed on the surface of solid yellow, tan, or brown sulfur melt freezes in vacuum by differential (fractional) evaporation of two or more sulfur molecular species present in the original sulfur; S(8) ring sulfur is thought to be the dominant sublimination phase lost to the vacuum sink, and polymeric chain sulfur S(u) the dominant residual phase that remains in place, forming the residual fluffy surface layer. The reflectance spectrum of the original sulfur surface is greaty modified by formation of the fluffy layer: the blue absorption band-edge and shoulder move 0.05 to 0.06 microns toward shorter wavelengths resulting in a permanent increase in reflectivity near 0.42 to 0.46 microns; the UV reflectivity below 0.40 microns is reduced. This form of sulfur should exist in large quantity on the surface of Io, especially in hotspot regions if there is solid free sulfur there that has solidified from a melt. Its color and spectra will indicate relative crystallization age on a scale of days to months and/or surface temperature distribution history.

Solvent free low-melt viscosity imide oligomers and thermosetting polymide composites

NASA Technical Reports Server (NTRS)

Chuang, Chun-Hua (Inventor)

2012-01-01

.[.This invention relates to the composition and a solvent-free process for preparing novel imide oligomers and polymers specifically formulated with effective amounts of a dianhydride such as 2,3,3',4-biphenyltetra carboxylic dianydride (a-BPDA), at least one aromatic diamine and an endcapped of 4-phenylethynylphthalic anhydride (PEPA) or nadic anhydride to produce imide oligomers that possess a low-melt viscosity of 1-60 poise at 260-280.degree. C. When the imide oligomer melt is cured at about 371.degree. C. in a press or autoclave under 100-500 psi, the melt resulted in a thermoset polyimide having a glass transition temperature (T.sub.g) equal to and above 310.degree. C. A novel feature of this process is that the monomers; namely the dianhydrides, diamines and the endcaps, are melt processable to form imide oligomers at temperatures ranging between 232-280.degree. C. (450-535.degree. F.) without any solvent. These low-melt imide oligomers can be easily processed by resin transfer molding (RTM), vacuum-assisted resin transfer molding (VARTM) or the resin infusion process with fiber preforms e.g. carbon, glass or quartz preforms to produce polyimide matrix composites with 288-343.degree. C. (550-650.degree. F.) high temperature performance capability..]. .Iadd.This invention relates to compositions and a solvent-free reaction process for preparing imide oligomers and polymers specifically derived from effective amounts of dianhydrides such as 2,3,3',4'-biphenyltetracarboxylic dianhydride (a-BPDA), at least one aromatic polyamine and an end-cap such as 4-phenylethynyphthalic anhydride (PEPA) or nadic anhydride to produce imide oligomers that possess a low-melt viscosity of 1-60 poise at 260.degree. C.-280.degree. C..Iaddend.

Study of formation mechanism of incipient melting in thixo-cast Al–Si–Cu–Mg alloys

DOE Office of Scientific and Technical Information (OSTI.GOV)

Du, Kang, E-mail: du126kang@126.com; Zhu, Qiang, E-mail: zhu.qiang@grinm.com; Li, Daquan, E-mail: lidaquan@grinm.com

Mechanical properties of thixo-cast Al–Si–Cu–Mg alloys can be enhanced by T61 heat treatment. Copper and magnesium atoms in aluminum matrix can form homogeneously distributed precipitations after solution and aging treatment which harden the alloys. However, microsegregation of these alloying elements could form numerous tiny multi-compound phases during solidification. These phases could cause incipient melting defects in subsequent heat treatment process and degrade the macro-mechanical properties of productions. This study is to present heterogeneous distribution of Cu, Si, and Mg elements and formation of incipient melting defects (pores). In this study, incipient melting pores that occurred during solution treatment at variousmore » temperatures, even lower than common melting points of various intermetallic phases, were identified, in terms of a method of investigating the same surface area in the samples before and after solution treatment in a vacuum environment. The results also show that the incipient melting mostly originates at the clusters with fine intermetallic particles while also some at the edge of block-like Al{sub 2}Cu. The fine particles were determined being Al{sub 2}Cu, Al{sub 5}Cu{sub 2}Mg{sub 8}Si{sub 6} and Al{sub 8}Mg{sub 3}FeSi{sub 2}. Tendency of the incipient melting decreases with decreases of the width of the clusters. The formation mechanism of incipient melting pores in solution treatment process was discussed using both the Fick law and the LSW theory. Finally, a criterion of solution treatment to avoid incipient melting pores for the thixo-cast alloys is proposed. - Highlights: • In-situ comparison technique was used to analysis the change of eutectic phases. • The ralationship between eutectic phase size and incipient melting was studied. • Teat treatment criterion for higher incipient melting resistance was proposed.« less

Numerical simulation and experimental investigation of Ti-6Al-4V melted by CW fiber laser at different pressures

NASA Astrophysics Data System (ADS)

Tabassum, Aasma; Zhou, Jie; Han, Bing; Ni, Xiao-wu; Sardar, Maryam

2017-07-01

The interaction of continuous wave (CW) fiber laser with Ti-6Al-4V alloy is investigated numerically and experimentally at different laser fluence values and ambient pressures of N2 atmosphere to determine the melting time threshold of Ti-6Al-4V alloy. A 2D-axisymmetric numerical model considering heat transfer and laminar flow is established to describe the melting process. The simulation results indicate that material melts earlier at lower pressure (8.0 Pa) than at higher pressure (8.8×104 Pa) in several milliseconds with the same laser fluence. The experimental results demonstrate that the melting time threshold at high laser fluence (above 1.89×108 W/m2) is shorter for lower pressure (vacuum), which is consistent with the simulation. While the melting time threshold at low laser fluence (below 1.89×108 W/m2) is shorter for higher pressure. The possible aspects which can affect the melting process include the increased heat loss induced by the heat conduction between the metal surface and the ambient gas with the increased pressure, and the absorption variation of the coarse surface resulted from the chemical reaction.

METAL SPRAYER FOR USE IN VACUUM OR INERT ATMOSPHERE

DOEpatents

Monroe, R.E.

1958-10-14

A metal sprayer is described for use in a vacuum or inert atmosphere with a straight line wire feed and variable electrode contact angle. This apparatus comprises two wires which are fed through straight tubes of two mechanisms positioned on opposite sides of a central tube to which an inert gas is fed. The two mechanisms and the wires being fed constitute electrodes to which electrical current is supplied so that the wires are melted by the electric are formed at their contacting region and sprayed by the gas supplied by the central tube. This apparatus is designed specifically to apply a zirconium coating to uranium in an inert atmosphere and without the use of an oxidizing flame.

Vacuum characteristics of the sucking cycle and relationships with milk removal from the breast in term infants.

PubMed

Cannon, Anna Maria; Sakalidis, Vanessa Susanna; Lai, Ching Tat; Perrella, Sharon Lisa; Geddes, Donna Tracy

2016-05-01

The importance of an infant's intra-oral vacuum in milk removal from the breast has been established. However, the relationship between the vacuum curve and milk transfer is not well understood. To investigate the parameters of the infant suck cycle in relation to the volume of milk removed from the breast. Cross-sectional study to elucidate the role of infant intra-oral vacuum in efficient milk removal from the breast. Nineteen fully breastfed term infants. Intra-oral vacuum was recorded during monitored breastfeeds using a pressure transducer. Ultrasound imaging (milk flow) and respiratory inductive plethysmography (swallowing) were used to determine the nutritive sucking (NS) portion of the feed. Milk intake was determined by weighing infants before and after feeds. Vacuum traces of the first and next 2min of NS from the first breast were analysed. The volumes of milk removed during both NS periods were negatively associated with peak vacuum (p<0.001) and rate of vacuum application (p<0.001), and positively related to area under first half of the suck cycle (p<0.001). Most parameters changed significantly from the first 2min of NS to the next 2min including significant reduction in peak vacuum and area under first half of the suck cycle. These results further support the role of intra-oral vacuum, specifically optimal peak vacuum, in effective and efficient milk removal during breastfeeding. It also appears that infants modify their sucking dynamics to adapt to changes in milk flow during milk ejection as the breast empties. Copyright © 2016 Elsevier Ireland Ltd. All rights reserved.

High Vacuum Creep Facility in the Materials Processing Laboratory

NASA Image and Video Library

1973-01-21

Technicians at work in the Materials Processing Laboratory’s Creep Facility at the National Aeronautics and Space Administration (NASA) Lewis Research Center. The technicians supported the engineers’ studies of refractory materials, metals, and advanced superalloys. The Materials Processing Laboratory contained laboratories and test areas equipped to prepare and develop these metals and materials. The ultra-high vacuum lab, seen in this photograph, contained creep and tensile test equipment. Creep testing is used to study a material’s ability to withstand long durations under constant pressure and temperatures. The equipment measured the strain over a long period of time. Tensile test equipment subjects the test material to strain until the material fails. The two tests were used to determine the strength and durability of different materials. The Materials Processing Laboratory also housed arc and electron beam melting furnaces, a hydraulic vertical extrusion press, compaction and forging equipment, and rolling mills and swagers. There were cryogenic and gas storage facilities and mechanical and oil diffusion vacuum pumps. The facility contained both instrumental and analytical chemistry laboratories for work on radioactive or toxic materials and the only shop to machine toxic materials in the Midwest.

Numerical Simulation of Induction Channel Furnace to Investigate Efficiency for low Frequencies

NASA Astrophysics Data System (ADS)

Hang, N. Tran Thi; Lüdtke, U.

2018-05-01

The foundry industry worldwide commonly uses induction channel furnaces to heat and melt alloys. The operating frequency is one of the main issues when constructing an efficient channel furnace. It is possible to choose operating frequencies lower than 50 Hz using a modern IGBT power converter. This work shows the simulation results using ANSYS with the goal of finding the best electrical frequency necessary to operate the induction furnace. First, a two-dimensional model is used to calculate the efficiency depending on frequency. Then, the channel model is extended to a more realistic three-dimensional model. Finally, the influence of frequency, inductor profile, and several components of the induction channel furnace are discussed.

Polyimide Composites Properties of RTM370 Fabricated by Vacuum Assisted Resins Transfer Molding (VARTM)

NASA Technical Reports Server (NTRS)

Chuang, Kathy C.; Criss, Jim M.; Mintz, Eric A.

2011-01-01

RTM370 imide resin based on 2,3,3 ,4 -biphenyl dianhydride ( a-BPDA), 3,4 -oxydianinline (3,4 -ODA) with 4-phenylethynylphthalic (PEPA) endcap has shown to exhibit high Tg (370 C) and low melt viscosity (10-30 poise) at 280 C with a pot-life of 1-2 h. Previously, RTM370 resin has been fabricated into composites with T650-35 carbon fabrics by resin transfer molding (RTM) successfully. RTM370 composites exhibit excellent mechanical properties up to 327 C (620 F), and outstanding property retention after aging at 288 C (550 F) for 1000 hrs. In this presentation, RTM 370 composites will be fabricated by vacuum assisted resins transfer molding (VARTM), using vacuum bags without mold. The mechanical properties of RTM370 composites fabricated by VARTM will be compared to those of RTM370 made by RTM.

Comparison of vacuum and non-vacuum urine tubes for urinary sediment analysis.

PubMed

Topcuoglu, Canan; Sezer, Sevilay; Kosem, Arzu; Ercan, Mujgan; Turhan, Turan

2017-12-01

Urine collection systems with aspiration system for vacuum tubes are becoming increasingly common for urinalysis, especially for microscopic examination of the urine. In this study, we aimed to examine whether vacuum aspiration of the urine sample has any adverse effect on sediment analysis by comparing results from vacuum and non-vacuum urine tubes. The study included totally 213 urine samples obtained from inpatients and outpatients in our hospital. Urine samples were collected to containers with aspiration system for vacuum tubes. Each sample was aliquoted to both vacuum and non-vacuum urine tubes. Urinary sediment analysis was performed using manual microscope. Results were evaluated using chi-square test. Comparison of the sediment analysis results from vacuum and non-vacuum urine tubes showed that results were highly concordant for erythrocyte, leukocyte and epithelial cells (gamma values 1, 0.997, and 0.994, respectively; p < .001). Results were also concordant for urinary casts, crystals and yeast (kappa values 0.815, 0.945 and 1, respectively; p < .001). The results show that in urinary sediment analysis, vacuum aspiration has no adverse effect on the cellular components except on casts.

100-kA vacuum current breaker of a modular design

NASA Astrophysics Data System (ADS)

Ivanov, V. P.; Vozdvijenskii, V. A.; Jagnov, V. A.; Solodovnikov, S. G.; Mazulin, A. V.; Ryjkov, V. M.

1994-05-01

Direct current breaker of a modular design is developed for the strong field tokamak power supply system. The power supply system comprises four 800 MW alternative current generators with 4 GJ flywheels, thyristor rectifiers providing inductive stores pumping by a current up to 100 kA for 1 - 4 sec. To form current pulses of various shapes in the tokamak windings current breakers are used with either pneumatic or explosive drive, at a current switching synchronously of not worse than 100 mks. Current breakers of these types require that the current conducting elements be replaced after each shot. For recent years vacuum arc quenching chambers with an axial magnetic field are successfully employed as repetitive performance current breakers, basically for currents up to 40 kA. In the report some results of researches of a vacuum switch modular are presented which we used as prototype switch for currents of the order of 100 kA.

Noncontact technique for measuring the electrical resistivity and magnetic susceptibility of electrostatically levitated melts

NASA Astrophysics Data System (ADS)

Rustan, G. E.; Spyrison, N. S.; Kreyssig, A.; Prozorov, R.; Goldman, A. I.

2012-02-01

Over the last two decades the popularity of levitation methods for studying equilibrium and supercooled melts has increased steadily. Measurements of density, viscosity, surface tension, and atomic structure have become well established. In contrast, measurements of electrical resistivity and magnetic susceptibility of levitated melts have been very limited. To fill this void, we have combined the tunnel diode oscillator (TDO) technique with electrostatic levitation (ESL) to perform inductively coupled measurements on levitated melts. A description of the basic operating principles of the TDO and ESL will be given, as well as a description of the implementation and performance characteristics of this technique. Preliminary measurements of electrical resistivity in the solid and liquid state will be presented for samples of Zr, Si, and Ge, as well as the measurements of ferromagnetic transitions in Fe and Co based alloys.

Development of a low-permeability glass--ceramic to seal to molybdenum. [For long-life vacuum tubes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Eagan, R. J.

1975-03-01

This report describes the development of low-permeability glass-ceramics which can be sealed directly to molybdenum for the purpose of producing long-life vacuum tubes. Low permeability to helium and thermal expansion match to molybdenum are the bases upon which particular glass-ceramic compositions were selected and developed. The fabrication of tube envelopes using glass-ceramics is simplified when compared to conventional ceramic/metal tubes and these melting and sealing techniques are presented.

Use of vacuum tubes in test instrumentation for measuring characteristics of fast high-voltage semiconductor devices

NASA Technical Reports Server (NTRS)

Berning, D.

1981-01-01

Circuits are described that permit measurement of fast events occurring in power semiconductors. These circuits were developed for the dynamic characterization of transistors used in inductive-load switching applications. Fast voltage clamping using vacuum diodes is discussed, and reference is made to a unique circuit that was built for performing nondestructive, reverse-bias, second-breakdown tests on transistors.

49 CFR 570.56 - Vacuum brake assist unit and vacuum brake system.

Code of Federal Regulations, 2010 CFR

2010-10-01

.... The following requirements apply to vehicles with vacuum brake assist units and vacuum brake systems. (a) Vacuum brake assist unit integrity. The vacuum brake assist unit shall demonstrate integrity as... maintained on the pedal. (1) Inspection procedure. Stop the engine and apply service brake several times to...

Demonstrations with a Vacuum: Old Demonstrations for New Vacuum Pumps.

ERIC Educational Resources Information Center

Greenslade, Thomas B., Jr.

1989-01-01

Explains mechanisms of 19th-century vacuum pumps. Describes demonstrations using the pump including guinea and feather tube, aurora tube, electric egg, Gassiots cascade, air mill, bell in vacuum, density and buoyancy of air, fountain in vacuum, mercury shower, palm and bladder glasses, Bacchus demonstration, pneumatic man-lifter, and Magdeburg…

Method for reproducibly preparing a low-melting high-carbon yield precursor

DOEpatents

Smith, Wesley E.; Napier, Jr., Bradley

1978-01-01

The present invention is directed to a method for preparing a reproducible synthetic carbon precursor by the autoclave polymerization of indene (C.sub.9 H.sub.8) at a temperature in the range of 470.degree.-485.degree. C, and at a pressure in the range of about 1000 to about 4300 psi. Volatiles in the resulting liquid indene polymer are removed by vacuum outgassing to form a solid carbon precursor characterized by having a relatively low melting temperature, high-carbon yield, and high reproducibility which provide for the fabrication of carbon and graphite composites having strict requirements for reproducible properties.

Improved Vacuum Bazooka

NASA Astrophysics Data System (ADS)

Cockman, John

2003-04-01

This apparatus is a modification to the well-known "vacuum bazooka" (PIRA 2B30.70). My vacuum bazooka is easy to construct and demonstrate, requires no precise fittings, foil, or vacuum grease, and propels ping-pong balls at a tremendous velocity!

Composite Properties of RTM370 Polyimide Fabricated by Vacuum Assisted Resin Transfer Molding (VARTM)

NASA Technical Reports Server (NTRS)

Chuang, Kathy C.; Criss, James M.; Mintz, Eric A.; Shonkwiler, Brian; McCorkle, Linda S.

2011-01-01

RTM370 imide resin based on 2,3,3?,4?-biphenyl dianhydride (a-BPDA), 3,4'-oxydianinline (3,4'-ODA) with the 4-phenylethynylphthalic (PEPA) endcap has been shown to exhibit a high cured T(sub g) (370 C) and low melt viscosity (10-30 poise) at 280 C with a pot-life of 1-2 h. Previously, RTM370 resin has been successfully fabricated into composites reinforced with T650-35 carbon fabrics by resin transfer molding (RTM). RTM370 composites exhibit excellent mechanical properties up to 327?C (620?F), and outstanding property retention after aging at 288?C (550?F) for 1000 h. In this work, RTM370 composites were fabricated by vacuum assisted resin transfer molding (VARTM), using vacuum bags on a steel plate. The mechanical properties of RTM370 composites fabricated by VARTM are compared to those prepared by RTM.

The Classical Vacuum.

ERIC Educational Resources Information Center

Boyer, Timothy H.

1985-01-01

The classical vacuum of physics is not empty, but contains a distinctive pattern of electromagnetic fields. Discovery of the vacuum, thermal spectrum, classical electron theory, zero-point spectrum, and effects of acceleration are discussed. Connection between thermal radiation and the classical vacuum reveals unexpected unity in the laws of…

Electroweak vacuum instability and renormalized Higgs field vacuum fluctuations in the inflationary universe

NASA Astrophysics Data System (ADS)

Kohri, Kazunori; Matsui, Hiroki

2017-08-01

In this work, we investigated the electroweak vacuum instability during or after inflation. In the inflationary Universe, i.e., de Sitter space, the vacuum field fluctuations < δ phi 2 > enlarge in proportion to the Hubble scale H2. Therefore, the large inflationary vacuum fluctuations of the Higgs field < δ phi 2 > are potentially catastrophic to trigger the vacuum transition to the negative-energy Planck-scale vacuum state and cause an immediate collapse of the Universe. However, the vacuum field fluctuations < δ phi 2 >, i.e., the vacuum expectation values have an ultraviolet divergence, and therefore a renormalization is necessary to estimate the physical effects of the vacuum transition. Thus, in this paper, we revisit the electroweak vacuum instability from the perspective of quantum field theory (QFT) in curved space-time, and discuss the dynamical behavior of the homogeneous Higgs field phi determined by the effective potential V eff( phi ) in curved space-time and the renormalized vacuum fluctuations < δ phi 2 >ren via adiabatic regularization and point-splitting regularization. We simply suppose that the Higgs field only couples the gravity via the non-minimal Higgs-gravity coupling ξ(μ). In this scenario, the electroweak vacuum stability is inevitably threatened by the dynamical behavior of the homogeneous Higgs field phi, or the formations of AdS domains or bubbles unless the Hubble scale is small enough H< ΛI .

Partial Melting of the Indarch (EH4) Meteorite : A Textural, Chemical and Phase Relations View of Melting and Melt Migration

NASA Technical Reports Server (NTRS)

McCoy, Timothy J.; Dickinson, Tamara L.; Lofgren, Gary E.

2000-01-01

To Test whether Aubrites can be formed by melting of enstatite Chondrites and to understand igneous processes at very low oxygen fugacities, we have conducted partial melting experiments on the Indarch (EH4) chondrite at 1000-1500 C. Silicate melting begins at 1000 C. Substantial melt migration occurs at 1300-1400 C and metal migrates out of the silicate change at 1450 C and approx. 50% silicate partial melting. As a group, our experiments contain three immiscible metallic melts 9Si-, and C-rich), two immiscible sulfide melts(Fe-and FeMgMnCa-rich) and Silicate melt. Our partial melting experiments on the Indarch (EH4) enstatite Chondrite suggest that igneous processes at low fO2 exhibit serveral unique features. The complete melting of sulfides at 1000 C suggest that aubritic sulfides are not relicts. Aubritic oldhamite may have crystallized from Ca and S complexed in the silicate melt. Significant metal-sulfide melt migration might occur at relatively low degrees of silicate partial melting. Substantial elemental exchange occurred between different melts (e.g., between sulfide and silicate, Si between silicate and metal), a feature not observed during experiments at higher fO2. This exchange may help explain the formation of aubrites from known enstatite chondrites.

Germanium detector vacuum encapsulation

NASA Technical Reports Server (NTRS)

Madden, N. W.; Malone, D. F.; Pehl, R. H.; Cork, C. P.; Luke, P. N.; Landis, D. A.; Pollard, M. J.

1991-01-01

This paper describes an encapsulation technology that should significantly improve the viability of germanium gamma-ray detectors for a number of important applications. A specialized vacuum chamber has been constructed in which the detector and the encapsulating module are processed in high vacuum. Very high vacuum conductance is achieved within the valveless encapsulating module. The detector module is then sealed without breaking the chamber vacuum. The details of the vacuum chamber, valveless module, processing, and sealing method are presented.

A Plasma Window for Transmission of Radiation and Particle Beams from Vacuum to Atmosphere for Various Applications

NASA Astrophysics Data System (ADS)

Hershcovitch, Ady

1997-11-01

Many industrial and scientific processes like electron beam melting and welding, material modification by ion implantation, dry etching, and micro-fabrication, as well as generation of synchrotron radiation are performed almost exclusively in vacuum nowadays, since the electron and ion guns and their extractors must be kept at a reasonably high vacuum. Consequently, there are numerous drawbacks, among which are low production rates due to required pumping time, limits the vacuum volume sets on the size of target objects. In a small number of applications like non-vacuum electron beam welding, and various processes involving UV and x-ray radiation, thin vacuum walls or long stages of differential pumping are used. But, the resultant degradations of particle and radiation beams severely limit those applications. A novel apparatus, which utilized a short plasma arc, was successfully used to maintain a pressure of 7.6 x exp(-6) Torr in a vacuum chamber with a 2.36mm aperture to atmosphere, i.e., a plasma was successfully used to "plug" a hole to atmosphere while maintaining a reasonably high vacuum in the chamber. Successful transmission of charged particle beams from a vacuum through the plasma to atmosphere was accomplished. More details can be found in A. Hershcovitch, J. Appl. Physics 78, p. 5283 (1995). In addition to sustaining a vacuum atmosphere interface, the plasma has very strong lensing effect on charged particles. The plasma current generates an azimuthal magnetic field which exerts a radial Lorentz on charged particles moving parallel to the current channel. With proper orientation of the current direction, the Lorentz force is radially inward. This feature can be used to focus in beams to a very small spot size, and to overcome beam dispersion due to scattering by atmospheric atoms and molecules. Relatively hot plasma at the atmosphere boundary rarefies the atmospheric gases to further enhance particle beam propagation to the materials to target. Recent

A Life Study of Ausforged, Standard Forged and Standard Machined AISI M-50 Spur Gears

NASA Technical Reports Server (NTRS)

Townsend, D. P.; Bamberger, E. N.; Zaretsky, E. V.

1975-01-01

Tests were conducted at 350 K (170 F) with three groups of 8.9 cm (3.5 in.) pitch diameter spur gears made of vacuum induction melted (VIM) consumable-electrode vacuum-arc melted (VAR), AISI M-50 steel and one group of vacuum-arc remelted (VAR) AISI 9310 steel. The pitting fatigue life of the standard forged and ausforged gears was approximately five times that of the VAR AISI 9310 gears and ten times that of the bending fatigue life of the standard machined VIM-VAR AISI M-50 gears run under identical conditions. There was a slight decrease in the 10-percent life of the ausforged gears from that for the standard forged gears, but the difference is not statistically significant. The standard machined gears failed primarily by gear tooth fracture while the forged and ausforged VIM-VAR AISI M-50 and the VAR AISI 9310 gears failed primarily by surface pitting fatigue. The ausforged gears had a slightly greater tendency to fail by tooth fracture than the standard forged gears.

Development of High Interruption Capability Vacuum Circuit Breaker -Technology of Vacuum Arc Control-

NASA Astrophysics Data System (ADS)

Niwa, Yoshimitsu; Kaneko, Eiji

Vacuum circuit breakers (VCB) have been widely used for power distribution systems. Vacuum Interrupters, which are the current interruption unit, have been increased its interruption capability with the development of vacuum arc control technology by magnetic field. There are three major type electrodes: disk shaped electrodes, radial magnetic field electrodes, axial magnetic field (AMF) electrodes. In the disk shaped electrode, the vacuum arc between the electrodes is not controlled. In the AMF electrode, the vacuum arc is diffused and stabilized by an axial magnetic field, which is parallel to the arc current. In the last type of electrodes, the vacuum arc column is rotated by magnetic force generated by the current flowing in the electrodes. The interruption current and the voltage of one break VCB is increased to 100 kA, 144 kV respectively. This paper describes basic configurations and functions of VCB, vacuum arc control technology in vacuum interrupters, recent researches and applications of VCB.

Electroweak vacuum instability and renormalized Higgs field vacuum fluctuations in the inflationary universe

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kohri, Kazunori; Matsui, Hiroki, E-mail: kohri@post.kek.jp, E-mail: matshiro@post.kek.jp

In this work, we investigated the electroweak vacuum instability during or after inflation. In the inflationary Universe, i.e., de Sitter space, the vacuum field fluctuations < δ φ {sup 2} > enlarge in proportion to the Hubble scale H {sup 2}. Therefore, the large inflationary vacuum fluctuations of the Higgs field < δ φ {sup 2} > are potentially catastrophic to trigger the vacuum transition to the negative-energy Planck-scale vacuum state and cause an immediate collapse of the Universe. However, the vacuum field fluctuations < δ φ {sup 2} >, i.e., the vacuum expectation values have an ultraviolet divergence, andmore » therefore a renormalization is necessary to estimate the physical effects of the vacuum transition. Thus, in this paper, we revisit the electroweak vacuum instability from the perspective of quantum field theory (QFT) in curved space-time, and discuss the dynamical behavior of the homogeneous Higgs field φ determined by the effective potential V {sub eff}( φ ) in curved space-time and the renormalized vacuum fluctuations < δ φ {sup 2} >{sub ren} via adiabatic regularization and point-splitting regularization. We simply suppose that the Higgs field only couples the gravity via the non-minimal Higgs-gravity coupling ξ(μ). In this scenario, the electroweak vacuum stability is inevitably threatened by the dynamical behavior of the homogeneous Higgs field φ, or the formations of AdS domains or bubbles unless the Hubble scale is small enough H < Λ {sub I} .« less

Formation and characterization of mullite fibers produced by inviscid melt-spinning

NASA Astrophysics Data System (ADS)

Xiao, Zhijun

IMS is a technique used to form fibers from low viscosity melts by means of stream stabilization in a reactant gas, in this case propane. Mullite (3Alsb2Osb3*2SiOsb2) was selected as the material to be fiberized. A stable mullite melt was obtained at 2000sp°C. Some short fibers and shot were formed in the fiber forming experiments. Crucible material selection is a prerequisite for proper application of the IMS technique. The effect of two crucible materials-graphite and boron nitride were studied. A carbothermal reaction occurred between the mullite melt and the graphite crucible. Boron nitride was selected as the crucible material because a relatively stable melt could be obtained. Operating environment is another factor that affects IMS mullite fiber formation. The effects of vacuum, nitrogen and argon on mullite melting behavior were studied. Argon gas was selected as the operating environment. A 2sp3 factorial design was developed to study the effect of such variables as temperature, holding time at the temperature, and heating rate on mullite melting behavior. The effects of the variables and interactions were calculated. Temperature has the biggest positive effect, holding time is the second, heating rate just has a very small negative effect. A detailed investigation of the mullite decomposition mechanism and kinetics was conducted in this work. A solid reaction mechanism was proposed. The kinetic results and IR analysis support the proposed mechanism. The carbon source inside the furnace led to the decomposition of mullite. A feasible experimental technique was developed to prevent the decomposition of mullite. The experiments with this design completely controlled the mullite decomposition. The short fibers, shot and some side products formed in the fiber forming experiments were characterized using XRD, XRF and SEM-EDS. The composition of the short fiber and shot was in the range of mullite composition. XRD showed that the diffraction pattern of shot is

Melt Heterogeneity and Degassing at MT Etna from Melt Inclusions

NASA Astrophysics Data System (ADS)

Salem, L. C.; Edmonds, M.; Maclennan, J.; Corsaro, R. A.

2014-12-01

The melts feeding Mt Etna, Italy, are rich in volatiles and drive long-lasting powerful eruptions of basaltic magma in both effusive and explosive styles of activity. The volatile systematics of the volcanic system are well understood through melt inclusion and volcanic gas studies. Etna's melts are generated from a complex mantle setting, with subduction-related chemical modifications as well as OIB-type features, and then the melts must travel through thick carbonate-rich crust. The continual influx of mantle-derived volatile-rich magma controls the major compositional and eruptive features of Mount Etna and magma mixing has been recognized as an important process driving large eruptions [Kamenetsky, 2007]. Our study focusses on the 1669 eruption, the largest in historical times. Olivine-hosted melt inclusions were analyzed for volatile, trace and major elements using electron microprobe and ion probe (SIMS). We use volatile systematics and geochemical data to deconvolve mantle-derived heterogeneity from melt mixing and crystal fractionation. Our data are well described by a mixing trend between two distinct melts: a CO2-rich (CO2~1000ppm), incompatible trace element depleted melt (La/Yb~16), and a CO2-poor, enriched melt. The mixing also generates a strong correlation between Sr and CO2 in the melt inclusions dataset, reflecting the presence of a strong Sr anomaly in one of the end-member melts. We investigate the origin of this Sr anomaly by considering plagioclase dissolution and crustal assimilation. We also investigate degassing processes in the crust and plumbing system of the volcano. We compare our results with similar studies of OIB and arc-related basalts elsewhere and assess the implications for linking eruption size and style with the nature of the mantle-derived melts. Kamenetsky et al. (2007) Geology 35, 255-258.

Modelling of crater formation on anode surface by high-current vacuum arcs

NASA Astrophysics Data System (ADS)

Tian, Yunbo; Wang, Zhenxing; Jiang, Yanjun; Ma, Hui; Liu, Zhiyuan; Geng, Yingsan; Wang, Jianhua; Nordlund, Kai; Djurabekova, Flyura

2016-11-01

Anode melting and crater formation significantly affect interruption of high-current vacuum arcs. The primary objective of this paper is to theoretically investigate the mechanism of anode surface crater formation, caused by the combined effect of surface heating during the vacuum arc and pressure exerted on the molten surface by ions and electrons from the arc plasma. A model of fluid flow and heat transfer in the arc anode is developed and combined with a magnetohydrodynamics model of the vacuum arc plasma. Crater formation is observed in simulation for a peak arcing current higher than 15 kA on 40 mm diam. Cu electrodes spaced 10 mm apart. The flow of liquid metal starts after 4 or 5 ms of arcing, and the maximum velocities are 0.95 m/s and 1.39 m/s for 20 kA and 25 kA arcs, respectively. This flow redistributes thermal energy, and the maximum temperature of the anode surface does not remain in the center. Moreover, the condition for the liquid droplet formation on the anode surfaces is developed. The solidification process after current zero is also analyzed. The solidification time has been found to be more than 3 ms after 25 kA arcing. The long solidification time and sharp features on crater rims induce Taylor cone formation.

A benchmark initiative on mantle convection with melting and melt segregation

NASA Astrophysics Data System (ADS)

Schmeling, Harro; Dannberg, Juliane; Dohmen, Janik; Kalousova, Klara; Maurice, Maxim; Noack, Lena; Plesa, Ana; Soucek, Ondrej; Spiegelman, Marc; Thieulot, Cedric; Tosi, Nicola; Wallner, Herbert

2016-04-01

In recent years a number of mantle convection models have been developed which include partial melting within the asthenosphere, estimation of melt volumes, as well as melt extraction with and without redistribution at the surface or within the lithosphere. All these approaches use various simplifying modelling assumptions whose effects on the dynamics of convection including the feedback on melting have not been explored in sufficient detail. To better assess the significance of such assumptions and to provide test cases for the modelling community we carry out a benchmark comparison. The reference model is taken from the mantle convection benchmark, cases 1a to 1c (Blankenbach et al., 1989), assuming a square box with free slip boundary conditions, the Boussinesq approximation, constant viscosity and Rayleigh numbers of 104 to 10^6. Melting is modelled using a simplified binary solid solution with linearly depth dependent solidus and liquidus temperatures, as well as a solidus temperature depending linearly on depletion. Starting from a plume free initial temperature condition (to avoid melting at the onset time) five cases are investigated: Case 1 includes melting, but without thermal or dynamic feedback on the convection flow. This case provides a total melt generation rate (qm) in a steady state. Case 2 is identical to case 1 except that latent heat is switched on. Case 3 includes batch melting, melt buoyancy (melt Rayleigh number Rm) and depletion buoyancy, but no melt percolation. Output quantities are the Nusselt number (Nu), root mean square velocity (vrms), the maximum and the total melt volume and qm approaching a statistical steady state. Case 4 includes two-phase flow, i.e. melt percolation, assuming a constant shear and bulk viscosity of the matrix and various melt retention numbers (Rt). These cases are carried out using the Compaction Boussinseq Approximation (Schmeling, 2000) or the full compaction formulation. For cases 1 - 3 very good agreement

Tin in granitic melts: The role of melting temperature and protolith composition

NASA Astrophysics Data System (ADS)

Wolf, Mathias; Romer, Rolf L.; Franz, Leander; López-Moro, Francisco Javier

2018-06-01

Granite bound tin mineralization typically is seen as the result of extreme magmatic fractionation and late exsolution of magmatic fluids. Mineralization, however, also could be obtained at considerably less fractionation if initial melts already had enhanced Sn contents. We present chemical data and results from phase diagram modeling that illustrate the dominant roles of protolith composition, melting conditions, and melt extraction/evolution for the distribution of Sn between melt and restite and, thus, the Sn content of melts. We compare the element partitioning between leucosome and restite of low-temperature and high-temperature migmatites. During low-temperature melting, trace elements partition preferentially into the restite with the possible exception of Sr, Cd, Bi, and Pb, that may be enriched in the melt. In high-temperature melts, Ga, Y, Cd, Sn, REE, Pb, Bi, and U partition preferentially into the melt whereas Sc, V, Cr, Co, Ni, Mo, and Ba stay in the restite. This contrasting behavior is attributed to the stability of trace element sequestering minerals during melt generation. In particular muscovite, biotite, titanite, and rutile act as host phases for Sn and, therefore prevent Sn enrichment in the melt as long as they are stable phases in the restite. As protolith composition controls both the mineral assemblage and modal contents of the various minerals, protolith composition eventually also controls the fertility of a rock during anatexis, restite mineralogy, and partitioning behavior of trace metals. If a particular trace element is sequestered in a phase that is stable during partial melting, the resulting melt is depleted in this element whereas the restite becomes enriched. Melt generation at high temperature may release Sn when Sn-hosts become unstable. If melt has not been lost before the breakdown of Sn-hosts, Sn contents in the melt will increase but never will be high. In contrast, if melt has been lost before the decomposition of Sn

Measurement of the thermal expansion of melt-textured YBCO using optical fibre grating sensors

NASA Astrophysics Data System (ADS)

Zeisberger, M.; Latka, I.; Ecke, W.; Habisreuther, T.; Litzkendorf, D.; Gawalek, W.

2005-02-01

In this paper we present measurements of the thermal expansion of melt-textured YBaCuO in the temperature range 30-300 K by means of optical fibre sensors. The sample, which had a size of 38 × 38 × 18 mm3, was prepared by our standard melt-texturing process using SmBaCuO seeds. One fibre containing three Bragg gratings which act as strain sensors was glued to the sample surface with two sensors parallel to the ab-plane and one sensor parallel to the c-axis. The sample was cooled down to a minimum temperature of 30 K in a vacuum chamber using a closed cycle refrigerator. In the temperature range we used, the thermal expansion coefficients are in the range of (3-9) × 10-6 K-1 (ab-direction) and (5-13) × 10-6 K-1 (c-direction).

Metal Solidification Imaging Process by Magnetic Induction Tomography.

PubMed

Ma, Lu; Spagnul, Stefano; Soleimani, Manuchehr

2017-11-06

There are growing number of important applications that require a contactless method for monitoring an object surrounded inside a metallic enclosure. Imaging metal solidification is a great example for which there is no real time monitoring technique at present. This paper introduces a technique - magnetic induction tomography - for the real time in-situ imaging of the metal solidification process. Rigorous experimental verifications are presented. Firstly, a single inductive coil is placed on the top of a melting wood alloy to examine the changes of its inductance during solidification process. Secondly, an array of magnetic induction coils are designed to investigate the feasibility of a tomographic approach, i.e., when one coil is driven by an alternating current as a transmitter and a vector of phase changes are measured from the remaining of the coils as receivers. Phase changes are observed when the wood alloy state changes from liquid to solid. Thirdly, a series of static cold phantoms are created to represent various liquid/solid interfaces to verify the system performance. Finally, a powerful temporal reconstruction method is applied to realise real time in-situ visualisation of the solidification and the measurement of solidified shell thickness, a first report of its kind.

Melt containment member

DOEpatents

Rieken, Joel R.; Heidloff, Andrew J.

2014-09-09

A tubular melt containment member for transient containment of molten metals and alloys, especially reactive metals and alloys, includes a melt-contacting layer or region that comprises an oxygen-deficient rare earth oxide material that is less reactive as compared to the counterpart stoichiometric rare earth oxide. The oxygen-deficient (sub-stoichiometric) rare earth oxide can comprise oxygen-deficient yttria represented by Y.sub.2O.sub.3-x wherein x is from 0.01 to 0.1. Use of the oxygen-deficient rare earth oxide as the melt-contacting layer or region material reduces reaction with the melt for a given melt temperature and melt contact time.

A preliminary mechanical property and stress corrosion evaluation of VIM-VAR work strengthened and direct aged Inconel 718 bar material

NASA Technical Reports Server (NTRS)

Montano, J. W.

1987-01-01

This report presents a preliminary mechanical property and stress corrosion evaluation of double melted (vacuum induction melted (VIM), and vacuum arc remelted (VAR)), solution treated, work strengthened and direct aged Inconel 718 alloy bar (5.50 in. (13.97 cm) diameter). Two sets of tensile specimens, one direct single aged and the other direct double aged, were tested at ambient temperature in both the longitudinal and transverse directions. Longitudinal tensile and yield strengths in excess of 200 ksi (1378.96 MPa) and 168 ksi (1158.33 MPa), respectively, were realized at ambient temperature, for the direct double aged specimen. No failures occurred in the single or double edged longitudinal and transverse tensile specimens stressed to 75 and 100 percent of their respective yield strengths and exposed to a salt fog environment for 180 days. Tensile tests performed after the stress corrosion test showed no mechanical property degradation.

Evolution of gettering technologies for vacuum tubes to getters for MEMS

NASA Astrophysics Data System (ADS)

Amiotti, M.

2008-05-01

Getter materials are technically proven and industrially accepted practical ways to maintain vacuum inside hermetically sealed tubes or devices to assure high reliability and long lifetime of the operating devices. The most industrially proven vacuum tube is the cathode rays tubes (CRTs), where large surfaces are available for the deposition of an evaporated barium film by a radio frequency inductive heating of a stainless steel container filled with a BaAl4 powder mixed to Ni powder. The evolution of the CRTs manufacturing technologies required also new types of barium getters able to withstand some thermal process in air without any deterioration of the evaporation characteristics. In other vacuum tubes such as traveling waves tubes, the space available for the evaporation of a barium film and the sorption capacity required to assure the vacuum for the lifetime of the devices did not allow the use of the barium film, prompting the development of sintered non evaporable getter pills that can be activated during the manufacturing process or by flowing current through an embedded resistance. The same sintered non evaporable getter pills could find usage also in evacuated parts to thermally isolate the infrared sensors for different final applications. In high energy physics particle accelerators, the getter technology moved from localized vacuum getter pumps or getter strips to a getter coating over the surface of vacuum chambers in order to guarantee a more uniform pumping speed. With the advent of solid state electronics, new challenges faced the getter technology to assure long life to vacuum or inert gas filled hermetical packages containing microelectronic devices, especially in the telecommunication and military applications. A well known problem of GaAs devices with Pd or Pt metalization is the H2 poisoning of the metal gate: to prevent this degradation a two layer getter film has been develop to absorb a large quantity of H2 per unit of getter surface. The

Vacuum powder injector and method of impregnating fiber with powder

NASA Astrophysics Data System (ADS)

Working, Dennis C.

1993-05-01

A method and apparatus uniformly impregnate stranded material with dry powder such as low solubility, high melt flow polymer powder to produce, for example, composite prepregs. The stranded material is expanded in an impregnation chamber by an influx of air so that the powder, which may enter through the same inlet as the air, penetrates to the center of the stranded material. The stranded material then is contracted for holding the powder therein. The stranded material and powder may be pulled through the impregnation chamber in the same direction by vacuum. Larger particles of powder which do not fully penetrate the stranded material may be combed into the stranded material and powder which does not impregnate the stranded material may be collected and reused.

Vacuum powder injector and method of impregnating fiber with powder

NASA Technical Reports Server (NTRS)

Working, Dennis C. (Inventor)

1993-01-01

A method and apparatus uniformly impregnate stranded material with dry powder such as low solubility, high melt flow polymer powder to produce, for example, composite prepregs. The stranded material is expanded in an impregnation chamber by an influx of air so that the powder, which may enter through the same inlet as the air, penetrates to the center of the stranded material. The stranded material then is contracted for holding the powder therein. The stranded material and powder may be pulled through the impregnation chamber in the same direction by vacuum. Larger particles of powder which do not fully penetrate the stranded material may be combed into the stranded material and powder which does not impregnate the stranded material may be collected and reused.

Radiation hard vacuum switch

DOEpatents

Boettcher, Gordon E.

1990-01-01

A vacuum switch with an isolated trigger probe which is not directly connected to the switching electrodes. The vacuum switch within the plasmatron is triggered by plasma expansion initiated by the trigger probe which travels through an opening to reach the vacuum switch elements. The plasma arc created is directed by the opening to the space between the anode and cathode of the vacuum switch to cause conduction.

Radiation hard vacuum switch

DOEpatents

Boettcher, Gordon E.

1990-03-06

A vacuum switch with an isolated trigger probe which is not directly connected to the switching electrodes. The vacuum switch within the plasmatron is triggered by plasma expansion initiated by the trigger probe which travels through an opening to reach the vacuum switch elements. The plasma arc created is directed by the opening to the space between the anode and cathode of the vacuum switch to cause conduction.

A benchmark initiative on mantle convection with melting and melt segregation

NASA Astrophysics Data System (ADS)

Schmeling, Harro; Dohmen, Janik; Wallner, Herbert; Noack, Lena; Tosi, Nicola; Plesa, Ana-Catalina; Maurice, Maxime

2015-04-01

In recent years a number of mantle convection models have been developed which include partial melting within the asthenosphere, estimation of melt volumes, as well as melt extraction with and without redistribution at the surface or within the lithosphere. All these approaches use various simplifying modelling assumptions whose effects on the dynamics of convection including the feedback on melting have not been explored in sufficient detail. To better assess the significance of such assumptions and to provide test cases for the modelling community we initiate a benchmark comparison. In the initial phase of this endeavor we focus on the usefulness of the definitions of the test cases keeping the physics as sound as possible. The reference model is taken from the mantle convection benchmark, case 1b (Blanckenbach et al., 1989), assuming a square box with free slip boundary conditions, the Boussinesq approximation, constant viscosity and a Rayleigh number of 1e5. Melting is modelled assuming a simplified binary solid solution with linearly depth dependent solidus and liquidus temperatures, as well as a solidus temperature depending linearly on depletion. Starting from a plume free initial temperature condition (to avoid melting at the onset time) three cases are investigated: Case 1 includes melting, but without thermal or dynamic feedback on the convection flow. This case provides a total melt generation rate (qm) in a steady state. Case 2 includes batch melting, melt buoyancy (melt Rayleigh number Rm), depletion buoyancy and latent heat, but no melt percolation. Output quantities are the Nusselt number (Nu), root mean square velocity (vrms) and qm approaching a statistical steady state. Case 3 includes two-phase flow, i.e. melt percolation, assuming a constant shear and bulk viscosity of the matrix and various melt retention numbers (Rt). These cases should be carried out using the Compaction Boussinseq Approximation (Schmeling, 2000) or the full compaction

Additive Manufacturing of NiTiHf High Temperature Shape Memory Alloy

NASA Technical Reports Server (NTRS)

Benafan, Othmane; Bigelow, Glen S.; Elahinia, Mohammad; Moghaddam, Narges Shayesteh; Amerinatanzi, Amirhesam; Saedi, Soheil; Toker, Guher Pelin; Karaca, Haluk

2017-01-01

Additive manufacturing of a NiTi-20Hf high temperature shape memory alloy (HTSMA) was investigated. A selective laser melting (SLM) process by Phenix3D Systems was used to develop components from NiTiHf powder (of approximately 25-75 m particle fractions), and the thermomechanical response was compared to the conventionally vacuum induction skull melted counterpart. Transformation temperatures of the SLM material were found to be slightly lower due to the additional oxygen pick up from the gas atomization and melting process. The shape memory response in compression was measured for stresses up to 500 MPa, and transformation strains were found to be very comparable (Up to 1.26 for the as-extruded; up to 1.52 for SLM).

Vacuum fluctuations in an ancestor vacuum: A possible dark energy candidate

NASA Astrophysics Data System (ADS)

Aoki, Hajime; Iso, Satoshi; Lee, Da-Shin; Sekino, Yasuhiro; Yeh, Chen-Pin

2018-02-01

We consider an open universe created by bubble nucleation, and study possible effects of our "ancestor vacuum," a de Sitter space in which bubble nucleation occurred, on the present universe. We compute vacuum expectation values of the energy-momentum tensor for a minimally coupled scalar field, carefully taking into account the effect of the ancestor vacuum by the Euclidean prescription. We pay particular attention to the so-called supercurvature mode, a non-normalizable mode on a spatial slice of the open universe, which has been known to exist for sufficiently light fields. This mode decays in time most slowly, and may leave residual effects of the ancestor vacuum, potentially observable in the present universe. We point out that the vacuum energy of the quantum field can be regarded as dark energy if mass of the field is of order the present Hubble parameter or smaller. We obtain preliminary results for the dark energy equation of state w (z ) as a function of the redshift.

Synthesis of Lithium Metal Oxide Nanoparticles by Induction Thermal Plasmas.

PubMed

Tanaka, Manabu; Kageyama, Takuya; Sone, Hirotaka; Yoshida, Shuhei; Okamoto, Daisuke; Watanabe, Takayuki

2016-04-06

Lithium metal oxide nanoparticles were synthesized by induction thermal plasma. Four different systems-Li-Mn, Li-Cr, Li-Co, and Li-Ni-were compared to understand formation mechanism of Li-Me oxide nanoparticles in thermal plasma process. Analyses of X-ray diffractometry and electron microscopy showed that Li-Me oxide nanoparticles were successfully synthesized in Li-Mn, Li-Cr, and Li-Co systems. Spinel structured LiMn₂O₄ with truncated octahedral shape was formed. Layer structured LiCrO₂ or LiCoO₂ nanoparticles with polyhedral shapes were also synthesized in Li-Cr or Li-Co systems. By contrast, Li-Ni oxide nanoparticles were not synthesized in the Li-Ni system. Nucleation temperatures of each metal in the considered system were evaluated. The relationship between the nucleation temperature and melting and boiling points suggests that the melting points of metal oxides have a strong influence on the formation of lithium metal oxide nanoparticles. A lower melting temperature leads to a longer reaction time, resulting in a higher fraction of the lithium metal oxide nanoparticles in the prepared nanoparticles.

The 3-D numerical simulation research of vacuum injector for linear induction accelerator

NASA Astrophysics Data System (ADS)

Liu, Dagang; Xie, Mengjun; Tang, Xinbing; Liao, Shuqing

2017-01-01

Simulation method for voltage in-feed and electron injection of vacuum injector is given, and verification of the simulated voltage and current is carried out. The numerical simulation for the magnetic field of solenoid is implemented, and a comparative analysis is conducted between the simulation results and experimental results. A semi-implicit difference algorithm is adopted to suppress the numerical noise, and a parallel acceleration algorithm is used for increasing the computation speed. The RMS emittance calculation method of the beam envelope equations is analyzed. In addition, the simulated results of RMS emittance are compared with the experimental data. Finally, influences of the ferromagnetic rings on the radial and axial magnetic fields of solenoid as well as the emittance of beam are studied.

Vacuum Virtues

ERIC Educational Resources Information Center

Rathey, Allen

2007-01-01

Upright vacuums, like cars, vary in quality, features and performance. Like automobiles, some uprights are reliable, others may be problematic, and some become a problem as a result of neglect or improper use. So, how do education institutions make an informed choice and, having done so, ensure that an upright vacuum goes the distance? In this…

Microfabricated triggered vacuum switch

DOEpatents

Roesler, Alexander W [Tijeras, NM; Schare, Joshua M [Albuquerque, NM; Bunch, Kyle [Albuquerque, NM

2010-05-11

A microfabricated vacuum switch is disclosed which includes a substrate upon which an anode, cathode and trigger electrode are located. A cover is sealed over the substrate under vacuum to complete the vacuum switch. In some embodiments of the present invention, a metal cover can be used in place of the trigger electrode on the substrate. Materials used for the vacuum switch are compatible with high vacuum, relatively high temperature processing. These materials include molybdenum, niobium, copper, tungsten, aluminum and alloys thereof for the anode and cathode. Carbon in the form of graphitic carbon, a diamond-like material, or carbon nanotubes can be used in the trigger electrode. Channels can be optionally formed in the substrate to mitigate against surface breakdown.

Compositions of Magmatic and Impact Melt Sulfides in Tissint And EETA79001: Precursors of Immiscible Sulfide Melt Blebs in Shergottite Impact Melts

NASA Technical Reports Server (NTRS)

Ross, D. K.; Rao, M. N.; Nyquist, L.; Agee, C.; Sutton, S.

2013-01-01

Immiscible sulfide melt spherules are locally very abundant in shergottite impact melts. These melts can also contain samples of Martian atmospheric gases [1], and cosmogenic nuclides [2] that are present in impact melt, but not in the host shergottite, indicating some components in the melt resided at the Martian surface. These observations show that some regolith components are, at least locally, present in the impact melts. This view also suggests that one source of the over-abundant sulfur in these impact melts could be sulfates that are major constituents of Martian regolith, and that the sulfates were reduced during shock heating to sulfide. An alternative view is that sulfide spherules in impact melts are produced solely by melting the crystalline sulfide minerals (dominantly pyrrhotite, Fe(1-x)S) that are present in shergottites [3]. In this abstract we report new analyses of the compositions of sulfide immiscible melt spherules and pyrrhotite in the shergottites Tissint, and EETA79001,507, and we use these data to investigate the possible origins of the immiscible sulfide melt spherules. In particular, we use the metal/S ratios determined in these blebs as potential diagnostic criteria for tracking the source material from which the numerous sulfide blebs were generated by shock in these melts.

Influence of Gap Distance on Vacuum Arc Characteristics of Cup Type AMF Electrode in Vacuum Interrupters

NASA Astrophysics Data System (ADS)

Cheng, Shaoyong; Xiu, Shixin; Wang, Jimei; Shen, Zhengchao

2006-11-01

The greenhouse effect of SF6 is a great concern today. The development of high voltage vacuum circuit breakers becomes more important. The vacuum circuit breaker has minimum pollution to the environment. The vacuum interrupter is the key part of a vacuum circuit breaker. The interrupting characteristics in vacuum and arc-controlling technique are the main problems to be solved for a longer gap distance in developing high voltage vacuum interrupters. To understand the vacuum arc characteristics and provide effective technique to control vacuum arc in a long gap distance, the arc mode transition of a cup-type axial magnetic field electrode is observed by a high-speed charge coupled device (CCD) video camera under different gap distances while the arc voltage and arc current are recorded. The controlling ability of the axial magnetic field on vacuum arc obviously decreases when the gap distance is longer than 40 mm. The noise components and mean value of the arc voltage significantly increase. The effective method for controlling the vacuum arc characteristics is provided by long gap distances based on the test results. The test results can be used as a reference to develop high voltage and large capacity vacuum interrupters.

Controlling hollow relativistic electron beam orbits with an inductive current divider

DOE PAGES

Swanekamp, S. B.; Richardson, A. S.; Angus, J. R.; ...

2015-02-06

A passive method for controlling the trajectory of an intense, hollow electron beam is proposed using a vacuum structure that inductively splits the beam's return current. A central post carries a portion of the return current (I 1), while the outer conductor carries the remainder (I 2). An envelope equation appropriate for a hollow electron beam is derived and applied to the current divider. The force on the beam trajectory is shown to be proportional to (I 2-I 1), while the average force on the envelope (the beam width) is proportional to the beam current I b = (I 2more » + I 1). The values of I 1 and I 2 depend on the inductances in the return-current path geometries. Proper choice of the return-current geometries determines these inductances and offers control over the beam trajectory. As a result, solutions using realistic beam parameters show that, for appropriate choices of the return-current-path geometry, the inductive current divider can produce a beam that is both pinched and straightened so that it approaches a target at near-normal incidence with a beam diameter that is on the order of a few mm.« less

Melting Inside the Tibetan Crust? Constraint From Electrical Conductivity of Peraluminous Granitic Melt

NASA Astrophysics Data System (ADS)

Guo, Xuan; Zhang, Li; Su, Xue; Mao, Zhu; Gao, Xiao-Ying; Yang, Xiaozhi; Ni, Huaiwei

2018-05-01

Magnetotelluric and seismological studies suggested the presence of partial melts in the middle to lower Himalaya-Tibetan crust. However, the melt fractions inferred by previous work were based on presumed electrical conductivity of melts. We performed measurements on the electrical conductivity of peraluminous granitic melts with 0.16-8.4 wt % H2O (the expected compositions in the Tibetan crust) at 600-1,300°C and 0.5-1.0 GPa. Peraluminous melt exhibits lower electrical conductivity than peralkaline melt at dry condition, but this difference diminishes at H2O > 2 wt %. With our data, the observed electrical anomalies in the Tibetan crust could be explained by 2-33 vol % of peraluminous granitic melts with H2O > 6 wt %. Possible reasons for our inferred melt fractions being higher than seismological constraints include the following: (1) The real melts are more Na and H2O rich, (2) the effect of melt reducing seismic velocities was overestimated, and (3) the anomalies at some locations are due to fluids.

The Effect of Oxygen Partial Pressure on Microstructure and Properties of Fe40Al Alloy Sintered under Vacuum

PubMed Central

Siemiaszko, Dariusz; Kowalska, Beata; Jóźwik, Paweł; Kwiatkowska, Monika

2015-01-01

This paper presents the results of studies on the influence of oxygen partial pressure (vacuum level in the chamber) on the properties of FeAl intermetallics. One of the problems in the application of classical methods of prepared Fe-Al intermetallic is the occurrence of oxides. Applying a vacuum during sintering should reduce this effect. In order to analyze the effect of oxygen partial pressure on sample properties, five samples were processed (by a pressure-assisted induction sintering—PAIS method) under the following pressures: 3, 8, 30, 80, and 300 mbar (corresponding to oxygen partial pressures of 0.63, 1.68, 6.3, 16.8, and 63 mbar, respectively). The chemical and phase composition, hardness, density, and microstructure observations indicate that applying a vacuum significantly impacts intermetallic samples. The compact sintered at pressure 3 mbar is characterized by the most homogeneous microstructure, the highest density, high hardness, and nearly homogeneous chemical composition. PMID:28788015

Rapakivi texture formation via disequilibrium melting in a contact partial melt zone, Antarctica

NASA Astrophysics Data System (ADS)

Currier, R. M.

2017-12-01

In the McMurdo Dry Valleys of Antarctica, a Jurassic aged dolerite sill induced partial melting of granite in the shallow crust. The melt zone can be traced in full, from high degrees of melting (>60%) along the dolerite contact, to no apparent signs of melting, 10s of meters above the contact. Within this melt zone, the well-known rapakivi texture is found, arrested in various stages of development. High above the contact, and at low degrees of melting, K-feldspar crystals are slightly rounded and unmantled. In the lower half of the melt zone, mantles of cellular textured plagioclase appear on K-feldspar, and thicken towards the contact heat source. At the highest degrees of melting, cellular-textured plagioclase completely replaces restitic K-feldspar. Because of the complete exposure and intact context, the leading models of rapakivi texture formation can be tested against this system. The previously proposed mechanisms of subisothermal decompression, magma-mixing, and hydrothermal exsolution all fail to adequately describe rapakivi generation in this melt zone. Preferred here is a closed system model that invokes the production of a heterogeneous, disequilibrium melt through rapid heating, followed by calcium and sodium rich melt reacting in a peritectic fashion with restitic K-feldspar crystals. This peritectic reaction results in the production of plagioclase of andesine-oligoclase composition—which is consistent with not just mantles in the melt zone, but globally as well. The thickness of the mantle is diffusion limited, and thus a measure of the diffusive length scale of sodium and calcium over the time scale of melting. Thermal modeling provides a time scale of melting that is consistent with the thickness of observed mantles. Lastly, the distribution of mantled feldspars is highly ordered in this melt zone, but if it were mobilized and homogenized—mixing together cellular plagioclase, mantled feldspars, and unmantled feldspars—the result would be

Understanding the High Temperature Behavior of Niobium Aluminides; First Year Summary Report

DTIC Science & Technology

1990-11-08

characterization to follow. Near-net shape processing may be used to form test specimens. A transmission elec- tron microscopy effort will be used ...to identify deformation mechanisms. ,, 20 DISTRIBUTION/AVAII ABILITY OF ABSTRACT SK’NCI ASSIFIFD’UNL MITED • SAME AS R"T • DTC USEDS J...ingots have been processed for us (gratis) by Nippon Mining Corporation by vacuum induction melted from a stock of niobium oxide and elemental aluminum

Electrical conductivity of basaltic and carbonatite melt-bearing peridotites at high pressures: Implications for melt distribution and melt fraction in the upper mantle

NASA Astrophysics Data System (ADS)

Yoshino, Takashi; Laumonier, Mickael; McIsaac, Elizabeth; Katsura, Tomoo

2010-07-01

Electrical impedance measurements were performed on two types of partial molten samples with basaltic and carbonatitic melts in a Kawai-type multi-anvil apparatus in order to investigate melt fraction-conductivity relationships and melt distribution of the partial molten mantle peridotite under high pressure. The silicate samples were composed of San Carlos olivine with various amounts of mid-ocean ridge basalt (MORB), and the carbonate samples were a mixture of San Carlos olivine with various amounts of carbonatite. High-pressure experiments on the silicate and carbonate systems were performed up to 1600 K at 1.5 GPa and up to at least 1650 K at 3 GPa, respectively. The sample conductivity increased with increasing melt fraction. Carbonatite-bearing samples show approximately one order of magnitude higher conductivity than basalt-bearing ones at the similar melt fraction. A linear relationship between log conductivity ( σbulk) and log melt fraction ( ϕ) can be expressed well by the Archie's law (Archie, 1942) ( σbulk/ σmelt = Cϕn) with parameters C = 0.68 and 0.97, n = 0.87 and 1.13 for silicate and carbonate systems, respectively. Comparison of the electrical conductivity data with theoretical predictions for melt distribution indicates that the model assuming that the grain boundary is completely wetted by melt is the most preferable melt geometry. The gradual change of conductivity with melt fraction suggests no permeability jump due to melt percolation at a certain melt fraction. The melt fraction of the partial molten region in the upper mantle can be estimated to be 1-3% and ˜ 0.3% for basaltic melt and carbonatite melt, respectively.

Evaluation of Titanium Alloys Fabricated Using Rapid Prototyping Technologies—Electron Beam Melting and Laser Beam Melting

PubMed Central

Koike, Mari; Greer, Preston; Owen, Kelly; Lilly, Guo; Murr, Lawrence E.; Gaytan, Sara M.; Martinez, Edwin; Okabe, Toru

2011-01-01

This study characterized properties of Ti-6Al-4V ELI (extra low interstitial, ASTM grade 23) specimens fabricated by a laser beam melting (LBM) and an electron beam melting (EBM) system for dental applications. Titanium alloy specimens were made into required size and shape for each standard test using fabrication methods. The LBM specimens were made by an LBM machine utilizing 20 µm of Ti-6Al-4V ELI powder. Ti-6Al-4V ELI specimens were also fabricated by an EBM using 40 µm of Ti-6Al-4V ELI powder (average diameter, 40 µm: Arcam AB®) in a vacuum. As a control, cast Ti-6Al-4V ELI specimens (Cast) were made using a centrifugal casting machine in an MgO-based mold. Also, a wrought form of Ti-6Al-4V ELI (Wrought) was used as a control. The mechanical properties, corrosion properties and grindability (wear properties) were evaluated and data was analyzed using ANOVA and a non-parametric method (α = 0.05). The strength of the LBM and wrought specimens were similar, whereas the EBM specimens were slightly lower than those two specimens. The hardness of both the LBM and EBM specimens was similar and slightly higher than that of the cast and wrought alloys. For the higher grindability speed at 1,250 m/min, the volume loss of Ti64 LBM and EBM showed no significant differences among all the fabrication methods. LBM and EBM exhibited favorable results in fabricating dental appliances with excellent properties as found for specimens made by other fabricating methods. PMID:28824107

Evaluation of Titanium Alloys Fabricated Using Rapid Prototyping Technologies-Electron Beam Melting and Laser Beam Melting.

PubMed

Koike, Mari; Greer, Preston; Owen, Kelly; Lilly, Guo; Murr, Lawrence E; Gaytan, Sara M; Martinez, Edwin; Okabe, Toru

2011-10-10

This study characterized properties of Ti-6Al-4V ELI (extra low interstitial, ASTM grade 23) specimens fabricated by a laser beam melting (LBM) and an electron beam melting (EBM) system for dental applications. Titanium alloy specimens were made into required size and shape for each standard test using fabrication methods. The LBM specimens were made by an LBM machine utilizing 20 µm of Ti-6Al-4V ELI powder. Ti-6Al-4V ELI specimens were also fabricated by an EBM using 40 µm of Ti-6Al-4V ELI powder (average diameter, 40 µm: Arcam AB Ò ) in a vacuum. As a control, cast Ti-6Al-4V ELI specimens (Cast) were made using a centrifugal casting machine in an MgO-based mold. Also, a wrought form of Ti-6Al-4V ELI (Wrought) was used as a control. The mechanical properties, corrosion properties and grindability (wear properties) were evaluated and data was analyzed using ANOVA and a non-parametric method (α = 0.05). The strength of the LBM and wrought specimens were similar, whereas the EBM specimens were slightly lower than those two specimens. The hardness of both the LBM and EBM specimens was similar and slightly higher than that of the cast and wrought alloys. For the higher grindability speed at 1,250 m/min, the volume loss of Ti64 LBM and EBM showed no significant differences among all the fabrication methods. LBM and EBM exhibited favorable results in fabricating dental appliances with excellent properties as found for specimens made by other fabricating methods.

Internal stress-induced melting below melting temperature at high-rate laser heating

NASA Astrophysics Data System (ADS)

Hwang, Yong Seok; Levitas, Valery I.

2014-06-01

In this Letter, continuum thermodynamic and phase field approaches (PFAs) predicted internal stress-induced reduction in melting temperature for laser-irradiated heating of a nanolayer. Internal stresses appear due to thermal strain under constrained conditions and completely relax during melting, producing an additional thermodynamic driving force for melting. Thermodynamic melting temperature for Al reduces from 933.67 K for a stress-free condition down to 898.1 K for uniaxial strain and to 920.8 K for plane strain. Our PFA simulations demonstrated barrierless surface-induced melt nucleation below these temperatures and propagation of two solid-melt interfaces toward each other at the temperatures very close to the corresponding predicted thermodynamic equilibrium temperatures for the heating rate Q ≤1.51×1010K/s. At higher heating rates, kinetic superheating competes with a reduction in melting temperature and melting under uniaxial strain occurs at 902.1 K for Q = 1.51 × 1011 K/s and 936.9 K for Q = 1.46 × 1012 K/s.

Transient current interruption mechanism in a magnetically delayed vacuum switch

NASA Technical Reports Server (NTRS)

Morris, Gibson, Jr.; Dougal, Roger A.

1993-01-01

The capacity of a magnetically delayed vacuum switch to conduct current depends on the density of plasma injected into the switch. Exceeding the current capacity results in the switch entering a lossy mode of operation characterized by a transient interruption of the main current (opening behavior) and a rapid increase of voltage across the vacuum gap. Streak and framing photographs of the discharge indicate that a decrease of luminosity near the middle of the gap preceeds the transition to the opening phase. The zone of low luminosity propagates toward the cathode. This evidence suggests that the mechanism causing the opening phase is erosion of the background plasma in a manner similar to that in a plasma-opening switch. The resulting ion depletion forces a space-charge-limited conduction mode. The switch inductance maintains a high discharge current even during the space-charge-limited conduction phase, thus producing high internal fields. The high accelerating voltage, in turn, produces electron and ion beams that heat the electrode surfaces. As a result of the heating, jets of electrode vapor issue from the electrodes, either cathode or anode, depending on the selection of electrode materials.

Model 'zero-age' lunar thermal profiles resulting from electrical induction

NASA Technical Reports Server (NTRS)

Herbert, F.; Sonett, C. P.; Wiskerchen, M. J.

1977-01-01

Thermal profiles for the moon are calculated under the assumption that a pre-main-sequence T-Tauri-like solar wind excites both transverse magnetic and transverse electric induction while the moon is accreting. A substantial initial temperature rise occurs, possibly of sufficient magnitude to cause subsequent early extensive melting throughout the moon in conjunction with nominal long-lived radioactives. In these models, accretion is an unimportant direct source of thermal energy but is important because even small temperature rises from accretion cause significant changes in bulk electrical conductivity. Induction depends upon the radius of the moon, which we take to be accumulating while it is being heated electrically. The 'zero-age' profiles calculated in this paper are proposed as initial conditions for long-term thermal evolution of the moon.

X-ray fluorescence analysis of K, Al and trace elements in chloroaluminate melts

NASA Astrophysics Data System (ADS)

Shibitko, A. O.; Abramov, A. V.; Denisov, E. I.; Lisienko, D. G.; Rebrin, O. I.; Bunkov, G. M.; Rychkov, V. N.

2017-09-01

Energy dispersive x-ray fluorescence spectrometry was applied to quantitative determination of K, Al, Cr, Fe and Ni in chloroaluminate melts. To implement the external standard calibration method, an unconventional way of samples preparation was suggested. A mixture of metal chlorides was melted in a quartz cell at 350-450 °C under a slightly excessive pressure of purified argon (99.999 %). The composition of the calibration samples (CSs) prepared was controlled by means of the inductively coupled plasma atomic emission spectrometry (ICP-AES). The optimal conditions for analytical lines excitation were determined, the analytes calibration curves were obtained. There was some influence of matrix effects in synthesized samples on the analytical signal of some elements. The CSs are to be stored in inert gas atmosphere. The precision, accuracy, and reproducibility factors of the quantitative chemical analysis were computed.

Multicharged iron ions produced by using induction heating vapor source.

PubMed

Kato, Yushi; Kubo, Takashi; Muramatsu, Masayuki; Tanaka, Kiyokatsu; Kitagawa, Atsushi; Yoshida, Yoshikazu; Asaji, Toyohisa; Sato, Fuminobu; Iida, Toshiyuki

2008-02-01

Multiply charged Fe ions are produced from solid pure material in an electron cyclotron resonance (ECR) ion source. We develop an evaporator by using induction heating with an induction coil which is made of bare molybdenum wire partially covered by ceramic beads in vacuum and surrounding and heating directly the pure Fe rod. Heated material has no contact with insulators, so that outgas is minimized. The evaporator is installed around the mirror end plate outside of the ECR plasma with its hole grazing the ECR zone. Helium or argon gas is usually chosen for supporting gas. The multicharged Fe ions up to Fe(13+) are extracted from the opposite side of mirror and against the evaporator, and then multicharged Fe ion beam is formed. We compare production of multicharged iron ions by using this new source with our previous methods.

Magma oceans and enhanced volcanism on TRAPPIST-1 planets due to induction heating

NASA Astrophysics Data System (ADS)

Kislyakova, K. G.; Noack, L.; Johnstone, C. P.; Zaitsev, V. V.; Fossati, L.; Lammer, H.; Khodachenko, M. L.; Odert, P.; Guedel, M.

2017-10-01

Low-mass M stars are plentiful in the Universe and often host small, rocky planets detectable with the current instrumentation. Recently, seven small planets have been discovered orbiting the ultracool dwarf TRAPPIST-1 te{Gillon16,Gillon17}. We examine the role of electromagnetic induction heating of these planets, caused by the star's rotation and the planet's orbital motion. If the stellar rotation and magnetic dipole axes are inclined with respect to each other, induction heating can melt the upper mantle and enormously increase volcanic activity, sometimes producing a magma ocean below the planetary surface. We show that induction heating leads the three innermost planets, one of which is in the habitable zone, to either evolve towards a molten mantle planet, or to experience increased outgassing and volcanic activity, while the four outermost planets remain mostly unaffected.

Vacuum probe surface sampler

NASA Technical Reports Server (NTRS)

Zahlava, B. A. (Inventor)

1973-01-01

A vacuum probe surface sampler is described for rapidly sampling relatively large surface areas which possess relatively light loading densities of micro-organism, drug particles or the like. A vacuum head with a hollow handle connected to a suitable vacuum source is frictionally attached to a cone assembly terminating in a flared tip adapted to be passed over the surface to be sampled. A fine mesh screen carried by the vacuum head provides support for a membrane filter which collects the microorganisms or other particles. The head assembly is easily removed from the cone assembly without contacting the cone assembly with human hands.

MgO melting curve constraints from shock temperature and rarefaction overtake measurements in samples preheated to 2300 K

NASA Astrophysics Data System (ADS)

Fat'yanov, O.; Asimow, P.

2013-06-01

In a continuous effort to determine experimentally the melting curve of MgO at 100-200 GPa, we extended our target preheating capability to 2300 K. The limit was primarily caused by intense sublimation of pure MgO in vacuum above ~2050 K. Completely redesigned Mo capsules holding ~20 mm long MgO crystals with controlled thermal gradients were impacted by thin Ta flyers launched at 6.5 to 7.5 km/s on the Caltech two-stage light-gas gun. Radiative shock temperatures and rarefaction overtake times were measured simultaneously by a 6-channel pyrometer with 3 ns time resolution, over 440-750 nm spectral range. All our experiments showed smooth pressure dependence of MgO sound speed consistent with the solid phase at 204-239 GPa. Observed temperatures are ~1000 K lower than those predicted by the solid phase model, but the plot of measured shock temperature versus pressure exhibits a pattern typical of shock melting at the highest pressure investigated. This may suggest that the Hugoniot of MgO preheated to 2300 K crosses its melting line at 220-240 GPa. Sound speed data indistinguishable from the solid phase model do not exclude the possibility of melting there.

Comparison of work rates, energy expenditure, and perceived exertion during a 1-h vacuuming task with a backpack vacuum cleaner and an upright vacuum cleaner.

PubMed

Mengelkoch, Larry J; Clark, Kirby

2006-03-01

The purpose of this study was to evaluate two types of industrial vacuum cleaners, in terms of cleaning rates, energy expenditure, and perceived exertion. Twelve industrial cleaners (six males and six females, age 28-39 yr) performed two 1-h vacuuming tasks with an upright vacuum cleaner (UVC) and a backpack vacuum cleaner (BPVC). Measures for oxygen uptake (VO2) and ratings of perceived exertion (RPE) were collected continuously during the 1-h vacuuming tasks. Cleaning rates for the UVC and BPVC were 7.23 and 14.98 m2min(-1), respectively. On a separate day subjects performed a maximal treadmill exercise test to determine their maximal aerobic capacity (peak VO2). Average absolute energy costs (in Metabolic equivalents), relative energy costs of the vacuum task compared to the subjects' maximal aerobic capacity (% peak VO2), and RPE responses for the 1-h vacuuming tasks were similar between vacuum cleaners, but % peak VO2 and RPE values differed between genders. These results indicate that the BPVC was more efficient than the UVC. With the BPVC, experienced workers vacuumed at a cleaning rate 2.07 times greater than the UVC and had similar levels of energy expenditure and perceived effort, compared to the slower cleaning rate with the UVC.

Cloud screening and melt water detection over melting sea ice using AATSR/SLSTR

NASA Astrophysics Data System (ADS)

Istomina, Larysa; Heygster, Georg

2014-05-01

With the onset of melt in the Arctic Ocean, the fraction of melt water on sea ice, the melt pond fraction, increases. The consequences are: the reduced albedo of sea ice, increased transmittance of sea ice and affected heat balance of the system with more heat passing through the ice into the ocean, which facilitates further melting. The onset of melt, duration of melt season and melt pond fraction are good indicators of the climate state of the Arctic and its change. In the absence of reliable sea ice thickness retrievals in summer, melt pond fraction retrieval from satellite is in demand as input for GCM as an indicator of melt state of the sea ice. The retrieval of melt pond fraction with a moderate resolution radiometer as AATSR is, however, a non-trivial task due to a variety of subpixel surface types with very different optical properties, which give non-unique combinations if mixed. In this work this has been solved by employing additional information on the surface and air temperature of the pixel. In the current work, a concept of melt pond detection on sea ice is presented. The basis of the retrieval is the sensitivity of AATSR reflectance channels 550nm and 860nm to the amount of melt water on sea ice. The retrieval features extensive usage of a database of in situ surface albedo spectra. A tree of decisions is employed to select the feasible family of in situ spectra for the retrieval, depending on the melt stage of the surface. Reanalysis air temperature at the surface and brightness temperature measured by the satellite sensor are analyzed in order to evaluate the melting status of the surface. Case studies for FYI and MYI show plausible retrieved melt pond fractions, characteristic for both of the ice types. The developed retrieval can be used to process the historical AATSR (2002-2012) dataset, as well as for the SLSTR sensor onboard the future Sentinel-3 mission (scheduled for launch in 2015), to keep the continuity and obtain longer time sequence

Internal stress-induced melting below melting temperature at high-rate laser heating

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hwang, Yong Seok, E-mail: yshwang@iastate.edu; Levitas, Valery I., E-mail: vlevitas@iastate.edu

In this Letter, continuum thermodynamic and phase field approaches (PFAs) predicted internal stress-induced reduction in melting temperature for laser-irradiated heating of a nanolayer. Internal stresses appear due to thermal strain under constrained conditions and completely relax during melting, producing an additional thermodynamic driving force for melting. Thermodynamic melting temperature for Al reduces from 933.67 K for a stress-free condition down to 898.1 K for uniaxial strain and to 920.8 K for plane strain. Our PFA simulations demonstrated barrierless surface-induced melt nucleation below these temperatures and propagation of two solid-melt interfaces toward each other at the temperatures very close to the corresponding predicted thermodynamicmore » equilibrium temperatures for the heating rate Q≤1.51×10{sup 10}K/s. At higher heating rates, kinetic superheating competes with a reduction in melting temperature and melting under uniaxial strain occurs at 902.1 K for Q = 1.51 × 10{sup 11 }K/s and 936.9 K for Q = 1.46 × 10{sup 12 }K/s.« less

Investigating evaporation of melting ice particles within a bin melting layer model

NASA Astrophysics Data System (ADS)

Neumann, Andrea J.

Single column models have been used to help develop algorithms for remote sensing retrievals. Assumptions in the single-column models may affect the assumptions of the remote sensing retrievals. Studies of the melting layer that use single column models often assume environments that are near or at water saturation. This study investigates the effects of evaporation upon melting particles to determine whether the assumption of negligible mass loss still holds within subsaturated melting layers. A single column, melting layer model is modified to include the effects of sublimation and evaporation upon the particles. Other changes to the model include switching the order in which the model loops over particle sizes and model layers; including a particle sedimentation scheme; adding aggregation, accretion, and collision and coalescence processes; allowing environmental variables such as the water vapor diffusivity and the Schmidt number to vary with the changes in the environment; adding explicitly calculated particle temperature, changing the particle terminal velocity parameterization; and using a newly-derived effective density-dimensional relationship for use in particle mass calculations. Simulations of idealized melting layer environments show that significant mass loss due to evaporation during melting is possible within subsaturated environments. Short melting distances, accelerating particle fall speeds, and short melting times help constrain the amount of mass lost due to evaporation while melting is occurring, even in subsaturated profiles. Sublimation prior to melting can also be a significant source of mass loss. The trends shown on the particle scale also appear in the bulk distribution parameters such as rainfall rate and ice water content. Simulations incorporating observed melting layer environments show that significant mass loss due to evaporation during the melting process is possible under certain environmental conditions. A profile such as the

A radiation hard vacuum switch

DOEpatents

Boettcher, G.E.

1988-07-19

A vacuum switch with an isolated trigger probe which is not directly connected to the switching electrodes. The vacuum switch within the plasmatron is triggered by plasma expansion initiated by the trigger probe which travels through an opening to reach the vacuum switch elements. The plasma arc created is directed by the opening to the space between the anode and cathode of the vacuum switch to cause conduction. 3 figs.

Comparison of vacuum rise time, vacuum limit accuracy, and occlusion break surge of 3 new phacoemulsification systems.

PubMed

Han, Young Keun; Miller, Kevin M

2009-08-01

To compare vacuum rise time, vacuum limit accuracy, and occlusion break surge of 3 new phacoemulsification machines. Jules Stein Eye Institute and Department of Ophthalmology, David Geffen School of Medicine at UCLA, Los Angeles, California, USA. The vacuum rise time under normal and enhanced aspiration modes, vacuum limit accuracy, and occlusion break surge of the Infiniti Vision System, Stellaris Vision Enhancement System, and WhiteStar Signature Phacoemulsification System were tested. Vacuum rise time and limit accuracy were measured at limit settings of 400 mm Hg and 600 mm Hg. Surge area was recorded at vacuum limit settings of 200 mm Hg, 300 mm Hg, 400 mm Hg, and 500 mm Hg. The Infiniti had the fastest vacuum rise times under normal and enhanced aspiration modes. At 4 seconds, the vacuum limit accuracy was greatest with the Infiniti at the 400 mm Hg limit and the Signature at the 600 mm Hg limit. The Stellaris did not reach either vacuum target. The Infiniti performed better than the other 2 machines during testing of occlusion break surge at all vacuum limit settings above 200 mm Hg. Under controlled laboratory test conditions, the Infiniti had the fastest vacuum rise time, greatest vacuum limit accuracy at 400 mm Hg, and least occlusion break surge. These results can be explained by the lower compliance of the Infiniti system.

Paradise Lost: Uncertainties in melting and melt extraction processes beneath oceanic spreading ridges

NASA Astrophysics Data System (ADS)

Kelemen, P. B.

2014-12-01

In many ways, decompression melting and focused melt transport beneath oceanic spreading ridges is the best understood igneous process on Earth. However, there are remaining - increasing - uncertainties in interpreting residual mantle peridotites. Indicators of degree of melting in residual peridotite are questionable. Yb concentration and spinel Cr# are affected by (a) small scale variations in reactive melt transport, (b) variable extents of melt extraction, and (c) "impregnation", i.e. partial crystallization of cooling melt in pore space. Roughly 75% of abyssal peridotites have undergone major element refertilization. Many may have undergone several melting events. The following three statements are inconsistent: (1) Peridotite melt productivity beyond cpx exhaustion is > 0.1%/GPa. (2) Crustal thickness is independent of spreading rate at rates > 2 cm/yr full rate (excluding ultra-slow spreading ridges). (3) Thermal models predict, and observations confirm, thick thermal boundary layers beneath slow spreading ridges. If (a) melt productivity is << 0.1%/GPa beyond cpx-out, and (b) cpx-out occurs > 15 km below the seafloor beneath most ridges, then the independence of crustal thickness with spreading rate can be understood. Most sampled peridotites from ridges melted beyond cpx-out. Cpx in these rocks formed via impregnation and/or exsolution during cooling. Most peridotites beneath ridges may undergo cpx exhaustion during decompression melting. This would entail an upward modification of potential temperature estimates. Alternatively, perhaps oceanic crustal thickness does vary with spreading rate but this is masked by complicated tectonics and serpentinization at slow-spreading ridges. Dissolution channels (dunites) are predicted to coalesce downstream, but numerical models of these have not shown why > 95% of oceanic crust forms in a zone < 5 km wide. There may be permeability barriers guiding deeper melt toward the ridge, but field studies have not identified

Melt fracture revisited

DOE Office of Scientific and Technical Information (OSTI.GOV)

Greenberg, J. M.

2003-07-16

In a previous paper the author and Demay advanced a model to explain the melt fracture instability observed when molten linear polymer melts are extruded in a capillary rheometer operating under the controlled condition that the inlet flow rate was held constant. The model postulated that the melts were a slightly compressible viscous fluid and allowed for slipping of the melt at the wall. The novel feature of that model was the use of an empirical switch law which governed the amount of wall slip. The model successfully accounted for the oscillatory behavior of the exit flow rate, typically referredmore » to as the melt fracture instability, but did not simultaneously yield the fine scale spatial oscillations in the melt typically referred to as shark skin. In this note a new model is advanced which simultaneously explains the melt fracture instability and shark skin phenomena. The model postulates that the polymer is a slightly compressible linearly viscous fluid but assumes no slip boundary conditions at the capillary wall. In simple shear the shear stress {tau}and strain rate d are assumed to be related by d = F{tau} where F ranges between F{sub 2} and F{sub 1} > F{sub 2}. A strain rate dependent yield function is introduced and this function governs whether F evolves towards F{sub 2} or F{sub 1}. This model accounts for the empirical observation that at high shears polymers align and slide more easily than at low shears and explains both the melt fracture and shark skin phenomena.« less

Air bearing vacuum seal assembly

DOEpatents

Booth, Rex

1978-01-01

An air bearing vacuum seal assembly capable of rotating at the speed of several thousand revolutions per minute using an air cushion to prevent the rotating and stationary parts from touching, and a two stage differential pumping arrangement to maintain the pressure gradient between the air cushion and the vacuum so that the leak rate into the vacuum is, for example, less than 1 .times. 10.sup.-4 Pa m.sup.3 /s. The air bearing vacuum seal has particular application for mounting rotating targets to an evacuated accelerator beam tube for bombardment of the targets with high-power charged particle beams in vacuum.

Vacuum-Gauge Connection For Shipping Container

NASA Technical Reports Server (NTRS)

Henry, Robert H.

1990-01-01

External connector enables measurement of vacuum in stored part. Remote-readout connector added to shipping container and connected to thermo-couple vacuum gauge in vacuum-insulated cryogenic line packed in container. Enables monitoring of condition of vacuum without opening container.

Burning and graphitization of optically levitated nanodiamonds in vacuum

NASA Astrophysics Data System (ADS)

Rahman, A. T. M. A.; Frangeskou, A. C.; Kim, M. S.; Bose, S.; Morley, G. W.; Barker, P. F.

2016-02-01

A nitrogen-vacancy (NV-) centre in a nanodiamond, levitated in high vacuum, has recently been proposed as a probe for demonstrating mesoscopic centre-of-mass superpositions and for testing quantum gravity. Here, we study the behaviour of optically levitated nanodiamonds containing NV- centres at sub-atmospheric pressures and show that while they burn in air, this can be prevented by replacing the air with nitrogen. However, in nitrogen the nanodiamonds graphitize below ≈10 mB. Exploiting the Brownian motion of a levitated nanodiamond, we extract its internal temperature (Ti) and find that it would be detrimental to the NV- centre’s spin coherence time. These values of Ti make it clear that the diamond is not melting, contradicting a recent suggestion. Additionally, using the measured damping rate of a levitated nanoparticle at a given pressure, we propose a new way of determining its size.

Partial melting of TTG gneisses: crustal contamination and the production of granitic melts

NASA Astrophysics Data System (ADS)

Meade, F. C.; Masotta, M.; Troll, V. R.; Freda, C.; Johnson, T. E.; Dahren, B.

2011-12-01

Understanding partial melting of ancient TTG gneiss terranes is crucial when considering crustal contamination in volcanic systems, as these rocks are unlikely to melt completely at magmatic temperatures (1000-1200 °C) and crustal pressures (<500 MPa). Variations in the bulk composition of the gneiss, magma temperature, pressure (depth) and the composition and abundance of any fluids present will produce a variety of melt compositions, from partial melts enriched in incompatible elements to more complete melts, nearing the bulk chemistry of the parent gneiss. We have used piston cylinder experiments to simulate partial melting in a suite of 12 gneisses from NW Scotland (Lewisian) and Eastern Greenland (Ammassalik, Liverpool Land) under magma chamber temperature and pressure conditions (P=200 MPa, T=975 °C). These gneisses form the basement to much of the North Atlantic Igneous Province, where crustal contamination of magmas was commonplace but the composition of the crustal partial melts are poorly constrained [1]. The experiments produced partial melts in all samples (e.g. Fig 1). Electron microprobe analyses of glasses indicate they are compositionally heterogeneous and are significantly different from the whole rock chemistry of the parent gneisses. The melts have variably evolved compositions but are typically trachy-dacitic to rhyolitic (granitic). This integrated petrological, experimental and in-situ geochemical approach allows quantification of the processes of partial melting of TTG gneiss in a volcanic context, providing accurate major/trace element and isotopic (Sr, Pb) end-members for modeling crustal contamination. The experimental melts and restites will be compared geochemically with a suite of natural TTG gneisses, providing constraints on the extent to which the gneisses have produced and subsequently lost melt. [1] Geldmacher et al. (2002) Scottish Journal of Geology, v.38, p.55-61.

NSLS II Vacuum System

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ferreira, M.; Doom, L.; Hseuh, H.

2009-09-13

National Synchrotron Light Source II, being constructed at Brookhaven, is a 3-GeV, 500 mA, 3rd generation synchrotron radiation facility with ultra low emittance electron beams. The storage ring vacuum system has a circumference of 792 m and consists of over 250 vacuum chambers with a simulated average operating pressure of less than 1 x 10{sup -9} mbar. A summary of the update design of the vacuum system including girder supports of the chambers, gauges, vacuum pumps, bellows, beam position monitors and simulation of the average pressure will be shown. A brief description of the techniques and procedures for cleaning andmore » mounting the chambers are given.« less

Study on the plasma generation characteristics of an induction-triggered coaxial pulsed plasma thruster

NASA Astrophysics Data System (ADS)

Weisheng, CUI; Wenzheng, LIU; Jia, TIAN; Xiuyang, CHEN

2018-02-01

At present, spark plugs are used to trigger discharge in pulsed plasma thrusters (PPT), which are known to be life-limiting components due to plasma corrosion and carbon deposition. A strong electric field could be formed in a cathode triple junction (CTJ) to achieve a trigger function under vacuum conditions. We propose an induction-triggered electrode structure on the basis of the CTJ trigger principle. The induction-triggered electrode structure could increase the electric field strength of the CTJ without changing the voltage between electrodes, contributing to a reduction in the electrode breakdown voltage. Additionally, it can maintain the plasma generation effect when the breakdown voltage is reduced in the discharge experiments. The induction-triggered electrode structure could ensure an effective trigger when the ablation distance of Teflon increases, and the magnetic field produced by the discharge current could further improve the plasma density and propagation velocity. The induction-triggered coaxial PPT we propose has a simplified trigger structure, and it is an effective attempt to optimize the micro-satellite thruster.

Effective Porosity Measurements by Wet- and Dry-type Vacuum Saturations using Process-Programmable Vacuum Saturation System

NASA Astrophysics Data System (ADS)

Lee, T. J.; Lee, K. S., , Dr; Lee, S. K.

2017-12-01

One of the most important factors in measuring effective porosity by vacuum saturation method is that the air in the pore space can be fully substituted by water during the vacuum saturation process. International Society of Rock Mechanics (ISRM) suggests vacuuming a rock sample submerged in the water, while American Society of Test and Materials (ASTM) vacuuming the sample and water separately and then pour the water to the sample. In this study, we call the former wet-type vacuum saturation (WVS) method and the latter dry-type vacuum saturation (DVS) method, and compare the effective porosity measured by the two different vacuum saturation processes. For that purpose, a vacuum saturation system has been developed, which can support both WVS and DVS by only changing the process by programming. Comparison of effective porosity has been made for a cement mortar and rock samples. As a result, DVS can substitute more void volume to water than WVS, which in turn insists that DVS can provide more exact value of effective porosity than WVS.

Controlling hollow relativistic electron beam orbits with an inductive current divider

DOE Office of Scientific and Technical Information (OSTI.GOV)

Swanekamp, S. B.; Richardson, A. S.; Angus, J. R.

2015-02-15

A passive method for controlling the trajectory of an intense, hollow electron beam is proposed using a vacuum structure that inductively splits the beam's return current. A central post carries a portion of the return current (I{sub 1}), while the outer conductor carries the remainder (I{sub 2}). An envelope equation appropriate for a hollow electron beam is derived and applied to the current divider. The force on the beam trajectory is shown to be proportional to (I{sub 2}-I{sub 1}), while the average force on the envelope (the beam width) is proportional to the beam current I{sub b} = (I{sub 2} + I{sub 1}). Themore » values of I{sub 1} and I{sub 2} depend on the inductances in the return-current path geometries. Proper choice of the return-current geometries determines these inductances and offers control over the beam trajectory. Solutions using realistic beam parameters show that, for appropriate choices of the return-current-path geometry, the inductive current divider can produce a beam that is both pinched and straightened so that it approaches a target at near-normal incidence with a beam diameter that is on the order of a few mm.« less

Energy Efficiency Model for Induction Furnace

NASA Astrophysics Data System (ADS)

Dey, Asit Kr

2018-01-01

In this paper, a system of a solar induction furnace unit was design to find out a new solution for the existing AC power consuming heating process through Supervisory control and data acquisition system. This unit can be connected directly to the DC system without any internal conversion inside the device. The performance of the new system solution is compared with the existing one in terms of power consumption and losses. This work also investigated energy save, system improvement, process control model in a foundry induction furnace heating framework corresponding to PV solar power supply. The results are analysed for long run in terms of saving energy and integrated process system. The data acquisition system base solar foundry plant is an extremely multifaceted system that can be run over an almost innumerable range of operating conditions, each characterized by specific energy consumption. Determining ideal operating conditions is a key challenge that requires the involvement of the latest automation technologies, each one contributing to allow not only the acquisition, processing, storage, retrieval and visualization of data, but also the implementation of automatic control strategies that can expand the achievement envelope in terms of melting process, safety and energy efficiency.

Translational induction of heat shock transcription factor σ32: evidence for a built-in RNA thermosensor

PubMed Central

Morita, Miyo Terao; Tanaka, Yoshiyuki; Kodama, Takashi S.; Kyogoku, Yoshimasa; Yanagi, Hideki; Yura, Takashi

1999-01-01

Induction of heat shock proteins in Escherichia coli is primarily caused by increased cellular levels of the heat shock σ-factor σ32 encoded by the rpoH gene. Increased σ32 levels result from both enhanced synthesis and stabilization. Previous work indicated that σ32 synthesis is induced at the translational level and is mediated by the mRNA secondary structure formed within the 5′-coding sequence of rpoH, including the translation initiation region. To understand the mechanism of heat induction of σ32 synthesis further, we analyzed expression of rpoH–lacZ gene fusions with altered stability of mRNA structure before and after heat shock. A clear correlation was found between the stability and expression or the extent of heat induction. Temperature-melting profiles of mRNAs with or without mutations correlated well with the expression patterns of fusion genes carrying the corresponding mutations in vivo. Furthermore, temperature dependence of mRNA–30S ribosome–tRNAfMet complex formation with wild-type or mutant mRNAs in vitro agreed well with that of the expression of gene fusions in vivo. Our results support a novel mechanism in which partial melting of mRNA secondary structure at high temperature enhances ribosome entry and translational initiation without involvement of other cellular components, that is, intrinsic mRNA stability controls synthesis of a transcriptional regulator. PMID:10090722

Energy Saving Melting and Revert Reduction Technology: Melting Efficiency in Die Casting Operations

DOE Office of Scientific and Technical Information (OSTI.GOV)

David Schwam

2012-12-15

This project addressed multiple aspects of the aluminum melting and handling in die casting operations, with the objective of increasing the energy efficiency while improving the quality of the molten metal. The efficiency of melting has always played an important role in the profitability of aluminum die casting operations. Consequently, die casters need to make careful choices in selecting and operating melting equipment and procedures. The capital cost of new melting equipment with higher efficiency can sometimes be recovered relatively fast when it replaces old melting equipment with lower efficiency. Upgrades designed to improve energy efficiency of existing equipment maymore » be well justified. Energy efficiency is however not the only factor in optimizing melting operations. Melt losses and metal quality are also very important. Selection of melting equipment has to take into consideration the specific conditions at the die casting shop such as availability of floor space, average quantity of metal used as well as the ability to supply more metal during peaks in demand. In all these cases, it is essential to make informed decisions based on the best available data.« less

Shock melting method to determine melting curve by molecular dynamics: Cu, Pd, and Al.

PubMed

Liu, Zhong-Li; Zhang, Xiu-Lu; Cai, Ling-Cang

2015-09-21

A melting simulation method, the shock melting (SM) method, is proposed and proved to be able to determine the melting curves of materials accurately and efficiently. The SM method, which is based on the multi-scale shock technique, determines melting curves by preheating and/or prepressurizing materials before shock. This strategy was extensively verified using both classical and ab initio molecular dynamics (MD). First, the SM method yielded the same satisfactory melting curve of Cu with only 360 atoms using classical MD, compared to the results from the Z-method and the two-phase coexistence method. Then, it also produced a satisfactory melting curve of Pd with only 756 atoms. Finally, the SM method combined with ab initio MD cheaply achieved a good melting curve of Al with only 180 atoms, which agrees well with the experimental data and the calculated results from other methods. It turned out that the SM method is an alternative efficient method for calculating the melting curves of materials.

New Approach in Filling of Fixed-Point Cells: Case Study of the Melting Point of Gallium

NASA Astrophysics Data System (ADS)

Bojkovski, J.; Hiti, M.; Batagelj, V.; Drnovšek, J.

2008-02-01

The typical way of constructing fixed-point cells is very well described in the literature. The crucible is loaded with shot, or any other shape of pure metal, inside an argon-filled glove box. Then, the crucible is carefully slid into a fused-silica tube that is closed at the top with an appropriate cap. After that, the cell is removed from the argon glove box and melted inside a furnace while under vacuum or filled with an inert gas like argon. Since the metal comes as shot, or in some other shape such as rods of various sizes, and takes more volume than the melted material, it is necessary to repeat the procedure until a sufficient amount of material is introduced into the crucible. With such a procedure, there is the possibility of introducing additional impurities into the pure metal with each cycle of melting the material and putting it back into the glove box to fill the cell. Our new approach includes the use of a special, so-called dry-box system, which is well known in chemistry. The atmosphere inside the dry box contains less than 20 ppm of water and less than 3 ppm of oxygen. Also, the size of the dry box allows it to contain a furnace for melting materials, not only for gallium but for higher-temperature materials as well. With such an approach, the cell and all its parts (pure metal, graphite, fused-silica tube, and cap) are constantly inside the controlled atmosphere, even while melting the material and filling the crucible. With such a method, the possibility of contaminating the cell during the filling process is minimized.

Stretching and smearing of chemical heterogeneity by melting and melt migration beneath mid-ocean ridges

NASA Astrophysics Data System (ADS)

Liu, B.; Liang, Y.

2017-12-01

The size of mantle source heterogeneity is important to the interpretation of isotopic signals observed in residual peridotites and basalts. During concurrent melting and melt migration beneath a mid-ocean ridge, both porosity and melt velocity increase upward, resulting in an upward increase in the effective transport velocity for a trace element. Hence a chemical heterogeneity of finite size will be stretched during its transport in the upwelling mantle. This melt migration induced chemical deformation can be quantified by a simple stretching factor. During equilibrium melting, the isotope signals of Sr, Nd and Hf in a 1 km size enriched mantle will be stretched to 2 6 km at the top of the melting column, depending on the style of melt migration. A finite rate of diffusive exchange between residual minerals and partial melt will result in smearing of chemical heterogeneity during its transport in the upwelling melting column. A Gaussian-shaped enriched source in depleted background mantle would be gradually deformed its transit through the melting column. The width of the enriched signal spreads out between the fronts of melt and solid while its amplitude decreases. This melt migration induced smearing also cause mixing of nearby heterogeneities or absorption of enriched heterogeneity by the ambient mantle. Smaller heterogeneities in the solid is more efficiently mixed or aborted by the background mantle than larger ones. Mixing of heterogeneities in the melt depends on the size in the same sense although the erupted melt is more homogenized due to melt accumulation and magma chamber process. The mapping of chemical heterogeneities observed in residual peridotites and basalts into their source region is therefore highly nonlinear. We will show that the observed variations in Nd and Hf isotopes in the global MORB and abyssal peridotites are consistent with kilometer-scale enriched heterogeneities embedded in depleted MORB mantle.

Vacuum leak detector and method

DOEpatents

Edwards, Jr., David

1983-01-01

Apparatus and method for detecting leakage in a vacuum system involves a moisture trap chamber connected to the vacuum system and to a pressure gauge. Moisture in the trap chamber is captured by freezing or by a moisture adsorbent to reduce the residual water vapor pressure therein to a negligible amount. The pressure gauge is then read to determine whether the vacuum system is leaky. By directing a stream of carbon dioxide or helium at potentially leaky parts of the vacuum system, the apparatus can be used with supplemental means to locate leaks.

Robot design for a vacuum environment

NASA Technical Reports Server (NTRS)

Belinski, S.; Trento, W.; Imani-Shikhabadi, R.; Hackwood, S.

1987-01-01

The cleanliness requirements for many processing and manufacturing tasks are becoming ever stricter, resulting in a greater interest in the vacuum environment. Researchers discuss the importance of this special environment, and the development of robots which are physically and functionally suited to vacuum processing tasks. Work is in progress at the Center for robotic Systems in Microelectronics (CRSM) to provide a robot for the manufacture of a revolutionary new gyroscope in high vacuum. The need for vacuum in this and other processes is discussed as well as the requirements for a vacuum-compatible robot. Finally, researchers present details on work done at the CRSM to modify an existing clean-room compatible robot for use at high vacuum.

The Microwave Properties of Simulated Melting Precipitation Particles: Sensitivity to Initial Melting

NASA Technical Reports Server (NTRS)

Johnson, B. T.; Olson, W. S.; Skofronick-Jackson, G.

2016-01-01

A simplified approach is presented for assessing the microwave response to the initial melting of realistically shaped ice particles. This paper is divided into two parts: (1) a description of the Single Particle Melting Model (SPMM), a heuristic melting simulation for ice-phase precipitation particles of any shape or size (SPMM is applied to two simulated aggregate snow particles, simulating melting up to 0.15 melt fraction by mass), and (2) the computation of the single-particle microwave scattering and extinction properties of these hydrometeors, using the discrete dipole approximation (via DDSCAT), at the following selected frequencies: 13.4, 35.6, and 94.0GHz for radar applications and 89, 165.0, and 183.31GHz for radiometer applications. These selected frequencies are consistent with current microwave remote-sensing platforms, such as CloudSat and the Global Precipitation Measurement (GPM) mission. Comparisons with calculations using variable-density spheres indicate significant deviations in scattering and extinction properties throughout the initial range of melting (liquid volume fractions less than 0.15). Integration of the single-particle properties over an exponential particle size distribution provides additional insight into idealized radar reflectivity and passive microwave brightness temperature sensitivity to variations in size/mass, shape, melt fraction, and particle orientation.

Experimental correlation of melt structures, nucleation rates, and thermal histories of silicate melts

NASA Technical Reports Server (NTRS)

Boynton, W. V.; DRAKE; HILDEBRAND; JONES; LEWIS; TREIMAN; WARK

1987-01-01

The theory and measurement of the structure of liquids is an important aspect of modern metallurgy and igneous petrology. Liquid structure exerts strong controls on both the types of crystals that may precipitate from melts and on the chemical composition of those crystals. An interesting aspect of melt structure studies is the problem of melt memories; that is, a melt can retain a memory of previous thermal history. This memory can influence both nucleation behavior and crystal composition. This melt memory may be characterized quantitatively with techniques such as Raman, infrared and NMR spectroscopy to provide information on short-range structure. Melt structure studies at high temperature will take advantage of the microgravity conditions of the Space Station to perform containerless experiments. Melt structure determinations at high temperature (experiments that are greatly facilitated by containerless technology) will provide invaluable information for materials science, glass technology, and geochemistry. In conjunction with studies of nucleation behavior and nucleation rates, information relevant to nucleation in magma chambers in terrestrial planets will be acquired.

Tensile Properties and Structure of Several Superalloys after Long- Term Exposure to LiF and Vacuum at 1173 K

NASA Astrophysics Data System (ADS)

Whittenberger, J. D.

1995-12-01

The use of the solid- to- liquid phase transformation of LiF to store thermal energy is under consideration for a space- based solar dynamic system. Although advantageous in terms of its energy density, the melting point of this salt (1121K) is beyond the commonly accepted upper- use temperature of 1100 K for chromium- bearing superalloys in vacuum. However, one commercially available nickel- base superalloy (Hastelloy B- 2) is chromium free; unfortunately, because of its high molybdenum content, this alloy can form phases that cause high- temperature embrittlement. To test the suitability of Hastelloy B- 2, it has been exposed to molten LiF, its vapor and vacuum at 1173 K for 2500, 5000, and 10 h. For control, the chromium- containing cobalt- base Haynes alloy 188 and nickel- base Haynes alloy 230 were also exposed to LiF and vacuum at 1173 K for 5000 h. Neither LiF nor vacuum exposures had any significant effect on Hastelloy B- 2 in terms of microstructural surface damage or weight change. Measurement of the post exposure tensile properties of Hastelloy B- 2, nevertheless, revealed low tensile ductility at 1050 K. Such embrittlement and low strength at elevated temperatures appear to preclude the use of Hastelloy B- 2 as a containment material for LiF. Little evidence of significant attack by LiF was seen in either of the chromium- containing superalloys; however, considerable weight loss and near- surface microstructural damage occurred in both alloys exposed to vacuum. Although measurement of the post exposure room-temperature tensile properties of Haynes alloys 188 and 230 revealed no significant loss of strength or ductility, the severe degree of microstructural damage found in unshielded alloys exposed to vacuum indicates that chromium-bearing superalloys might also be unsuitable for prolonged containment of LiF in space above 1100 K. Keywords

Technical specification for vacuum systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Khaw, J.

The vacuum systems at the Stanford Linear Accelerator Center (SLAC) are primarily of all-metal construction and operate at pressures from 10/sup -5/ to 10/sup -11/ Torr. The primary gas loads during operation result from thermal desorption and beam-induced desorption from the vacuum chamber walls. These desorption rates can be extremely high in the case of hydrocarbons and other contaminants. These specifications place a major emphasis on eliminating contamination sources. The specifications and procedures have been written to insure the cleanliness and vacuum integrity of all SLAC vacuum systems, and to assist personnel involved with SLAC vacuum systems in choosing andmore » designing components that are compatible with existing systems and meet the quality and reliability of SLAC vacuum standards. The specification includes requirements on design, procurement, fabrication, chemical cleaning, clean room practices, welding and brazing, helium leak testing, residual gas analyzer testing, bakeout, venting, and pumpdown. Also appended are specifications regarding acceptable vendors, isopropyl alcohol, bakeable valve cleaning procedure, mechanical engineering safety inspection, notes on synchrotron radiation, and specifications of numerous individual components. (LEW)« less

Shock melting method to determine melting curve by molecular dynamics: Cu, Pd, and Al

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liu, Zhong-Li, E-mail: zl.liu@163.com; Zhang, Xiu-Lu; Cai, Ling-Cang

A melting simulation method, the shock melting (SM) method, is proposed and proved to be able to determine the melting curves of materials accurately and efficiently. The SM method, which is based on the multi-scale shock technique, determines melting curves by preheating and/or prepressurizing materials before shock. This strategy was extensively verified using both classical and ab initio molecular dynamics (MD). First, the SM method yielded the same satisfactory melting curve of Cu with only 360 atoms using classical MD, compared to the results from the Z-method and the two-phase coexistence method. Then, it also produced a satisfactory melting curvemore » of Pd with only 756 atoms. Finally, the SM method combined with ab initio MD cheaply achieved a good melting curve of Al with only 180 atoms, which agrees well with the experimental data and the calculated results from other methods. It turned out that the SM method is an alternative efficient method for calculating the melting curves of materials.« less

Cold crucible induction melter test for crystalline ceramic waste form fabrication: A feasibility assessment

DOE PAGES

Amoroso, Jake W.; Marra, James; Dandeneau, Christopher S.; ...

2017-01-18

The first scaled proof-of-principle cold crucible induction melter (CCIM) test to process a multiphase ceramic waste form from a simulated combined (Cs/Sr, lanthanide and transition metal fission products) commercial used nuclear fuel waste stream was recently conducted in the United States. X-ray diffraction, 2-D X-ray absorption near edge structure (XANES), electron microscopy, inductively coupled plasma-atomic emission spectroscopy (and inductively coupled plasma-mass spectroscopy for Cs), and product consistency tests were used to characterize the fabricated CCIM material. Characterization analyses confirmed that a crystalline ceramic with a desirable phase assemblage was produced from a melt using a CCIM. We identified primary hollandite,more » pyrochlore/zirconolite, and perovskite phases in addition to minor phases rich in Fe, Al, or Cs. The material produced in the CCIM was chemically homogeneous and displayed a uniform phase assemblage with acceptable aqueous chemical durability.« less

Partial melting and melt percolation in the mantle: The message from Fe isotopes

NASA Astrophysics Data System (ADS)

Weyer, Stefan; Ionov, Dmitri A.

2007-07-01

High precision Fe isotope measurements have been performed on various mantle peridotites (fertile lherzolites, harzburgites, metasomatised Fe-enriched peridotites) and volcanic rocks (mainly oceanic basalts) from different localities and tectonic settings. The peridotites yield an average δ 56Fe = 0.01‰ and are significantly lighter than the basalts (average δ 56Fe = 0.11‰). Furthermore, the peridotites display a negative correlation of δ 56Fe with Mg# indicating a link between δ 56Fe and degrees of melt extraction. Taken together, these findings imply that Fe isotopes fractionate during partial melting, with heavy isotopes preferentially entering the melt. The slope of depletion trends (δ 56Fe versus Mg#) of the peridotites was used to model Fe isotope fractionation during partial melting, resulting in αmantle-melt ≈ 1.0001-1.0003 or ln αmantle-melt ≈ 0.1-0.3‰. In contrast to most other peridotites investigated in this study, spinel lherzolites and harzburgites from three localities (Horoman, Kamchatka and Lherz) are virtually unaffected by metasomatism. These three sites display a particularly good correlation and define an isotope fractionation factor of ln αmantle-melt ≈ 0.3‰. This modelled value implies Fe isotope fractionation between residual mantle and mantle-derived melts corresponding to Δ56Fe mantle-basalt ≈ 0.2-0.3‰, i.e. significantly higher than the observed difference between averages for all the peridotites and the basalts in this study (corresponding to Δ56Fe mantle-basalt ≈ 0.1‰). Either disequilibrium melting increased the modelled αmantle-melt for these particular sites or the difference between average peridotite and basalt may be reduced by partial re-equilibration between the isotopically heavy basalts and the isotopically light depleted lithospheric mantle during melt ascent. The slope of the weaker δ 56Fe-Mg# trend defined by the combined set of all mantle peridotites from this study is more consistent with

Bakeout Chamber Within Vacuum Chamber

NASA Technical Reports Server (NTRS)

Taylor, Daniel M.; Soules, David M.; Barengoltz, Jack B.

1995-01-01

Vacuum-bakeout apparatus for decontaminating and measuring outgassing from pieces of equipment constructed by mounting bakeout chamber within conventional vacuum chamber. Upgrade cost effective: fabrication and installation of bakeout chamber simple, installation performed quickly and without major changes in older vacuum chamber, and provides quantitative data on outgassing from pieces of equipment placed in bakeout chamber.

Power Quality Improvement in Induction Furnace by Harmonic Reduction Using Dynamic Voltage Restorer

NASA Astrophysics Data System (ADS)

Saggu, Tejinder Singh; Singh, Lakhwinder

2016-06-01

Induction furnaces are used in wide quantity under different capacities for annual production of around 25 million tons of iron and steel in India. It plays a vital role in various manufacturing processes around the world for melting different types of metal scraps i. e. Copper, Cast Iron, Aluminium, Steel, Brass, Bronze, Silicon, Gold, Silver etc. which are further used in many other industrial applications. The induction furnace causes a huge disturbance to the utility and nearby consumers during its operation due to its non-linear characteristics. This is a serious phenomenon responsible for power quality degradation in the power system. This paper presents methodology to improve the power quality degradation caused by induction furnace using Dynamic Voltage Restorer (DVR) which is a type of custom power device. The real time data has been taken from an industry employing induction furnace for production of ingots from scrap material. The experimental readings are measured using power quality analyser equipment. The simulation of whole plant is done by analysing this same data and the simulation results are compared with actual onsite results. Then, solution methodology using DVR is presented which revealed that the implementation of DVR is an effective solution for voltage sag mitigation and harmonics improvement in induction furnace.

On the phase evolution of AlCoCrCuFeMnSix high entropy alloys prepared by mechanical alloying and arc melting route

NASA Astrophysics Data System (ADS)

Kumar, Anil; Chopkar, Manoj

2018-05-01

Effect of Si addition on phase formation of AlCoCrCuFeMnSix (x=0, 0.3, 0.6 and 0.9) high entropy alloy have been investigated in this work. The alloys are prepared by mechanical alloying and vacuum arc melting technique. The X-ray diffraction results reveals the formation of mixture of face centered and body centered cubic solid solution phases in milled powders. The addition of Si favours body centered cubic structure formation during milling process. Whereas, after melting the milled powders, body centered phases formed during milling is partial transformed into sigma phases. XRD results were also correlated with the SEM elemental mapping of as casted samples. Addition of Si favours σ phase formation in the as cast samples.

Experimental Phase Relations of Hydrous, Primitive Melts: Implications for variably depleted mantle melting in arcs and the generation of primitive high-SiO2 melts

NASA Astrophysics Data System (ADS)

Weaver, S.; Wallace, P. J.; Johnston, A.

2010-12-01

There has been considerable experimental and theoretical work on how the introduction of H2O-rich fluids into the mantle wedge affects partial melting in arcs and chemical evolution of mantle melts as they migrate through the mantle. Studies aimed at describing these processes have become largely quantitative, with an emphasis on creating models that suitably predict the production and evolution of melts and describe the thermal state of arcs worldwide. A complete experimental data set that explores the P-T conditions of melt generation and subsequent melt extraction is crucial to the development, calibration, and testing of these models. This work adds to that data set by constraining the P-T-H2O conditions of primary melt extraction from two end-member subduction zones, a continental arc (Mexico) and an intraoceanic arc (Aleutians). We present our data in context with primitive melts found worldwide and with other experimental studies of melts produced from fertile and variably depleted mantle sources. Additionally, we compare our experimental results to melt compositions predicted by empirical and thermodynamic models. We used a piston-cylinder apparatus and employed an inverse approach in our experiments, constraining the permissible mantle residues with which our melts could be in equilibrium. We confirmed our inverse approach with forced saturation experiments at the P-T-H2O conditions of melt-mantle equilibration. Our experimental results show that a primitive, basaltic andesite melt (JR-28) from monogenetic cinder cone Volcan Jorullo (Central Mexico) last equilibrated with a harzburgite mantle residue at 1.2-1.4 GPa and 1150-1175°C with H2O contents in the range of 5.5-7 wt% H2O prior to ascent and eruption. Phase relations of a tholeiitic high-MgO basaltic melt (ID-16) from the Central Aleutians (Okmok) show the conditions of last equilibration with a fertile lherzolite mantle residue at shallower (1.2 GPa) but hotter (1275°C) conditions with

Viscosity Measurement for Tellurium Melt

NASA Technical Reports Server (NTRS)

Lin, Bochuan; Li, Chao; Ban, Heng; Scripa, Rosalia N.; Su, Ching-Hua; Lehoczky, Sandor L.

2006-01-01

The viscosity of high temperature Te melt was measured using a new technique in which a rotating magnetic field was applied to the melt sealed in a suspended ampoule, and the torque exerted by rotating melt flow on the ampoule wall was measured. Governing equations for the coupled melt flow and ampoule torsional oscillation were solved, and the viscosity was extracted from the experimental data by numerical fitting. The computational result showed good agreement with experimental data. The melt velocity transient initiated by the rotating magnetic field reached a stable condition quickly, allowing the viscosity and electrical conductivity of the melt to be determined in a short period.

Improving Vacuum Cleaners

NASA Technical Reports Server (NTRS)

1997-01-01

Under a Space Act Agreement between the Kirby company and Lewis Research Center, NASA technology was applied to a commercial vacuum cleaner product line. Kirby engineers were interested in advanced operational concepts, such as particle flow behavior and vibration, critical factors to improve vacuum cleaner performance. An evaluation of the company 1994 home care system, the Kirby G4, led to the refinement of the new G5 and future models. Under the cooperative agreement, Kirby had access to Lewis' holography equipment, which added insight into how long a vacuum cleaner fan would perform, as well as advanced computer software that can simulate the flow of air through fans. The collaboration resulted in several successes including fan blade redesign and continuing dialogue on how to improve air-flow traits in various nozzle designs.

Pure Material Vapor Source by Induction Heating Evaporator for an Electron Cyclotron Resonance Ion Source

NASA Astrophysics Data System (ADS)

Matsui, Y.; Watanabe, T.; Satani, T.; Muramatsu, M.; Tanaka, K.; Kitagawa, A.; Yoshida, Y.; Sato, F.; Kato, Y.; Iida, T.

2008-11-01

Multiply charged iron ions are produced from solid pure material in an electron cyclotron resonance (ECR) ion source. We develop an evaporator by using induction heating with the induction coil which is made from bare molybdenum wire and surrounding the pure iron rod. We optimize the shape of induction heating coil and operation of rf power supply. We conduct experiment to investigate reproducibility and stability in the operation and heating efficiency. Induction heating evaporator produces pure material vapor, because materials directly heated by eddy currents have non-contact with insulated materials which are impurity gas sources. The power and the frequency of the induction currents range from 100 to 900 W and from 48 to 23 kHz, respectively. The working pressure is about 10-4 to 10-3 Pa. We measure temperature of iron rod and film deposition rate by depositing iron vapor to crystal oscillator. We confirm stability and reproducibility of evaporator enough to conduct experiment in ECR ion source. We can obtain required temperature of iron under maximum power of power supply. We are aiming the evaporator higher melting point material than iron.

Investigation of Slag Compositions and Pressure Ranges Suitable for Electroslag Remelting under Vacuum Conditions

NASA Astrophysics Data System (ADS)

Radwitz, S.; Scholz, H.; Friedrich, B.

It is well known that high contents of oxygen and hydrogen in creep resistant structural steels like 21CrMoV5-7 have negative influence on a variety of material properties. To investigate the refining ability of various slag compositions under reduced pressure multiple experiments were performed in a 40 kW vacuum-induction furnace with the aim to ensure minimal oxygen and hydrogen contents. With regard to slag evaporation, different mixtures of fluorides and oxides as well as pure oxide systems were utilized. The pressure was varied in the range of 5 and 700 mbar.

Olivine-hosted melt inclusions record efficient mixing of mantle melts in continental flood basalt provinces

NASA Astrophysics Data System (ADS)

Jennings, E. S.; Gibson, S. A.; Maclennan, J.; Heinonen, J. S.

2017-12-01

Primitive melt inclusions trapped in various minerals found in global ridge settings have been shown to record highly variable magmatic compositions. Mantle melting is expected to be near-fractional, producing a wide range of melt compositions that must accumulate and mix in crustal magma chambers. In primitive rocks, the melt inclusion variability observed in major, trace and isotope geochemistry is consistent to the first order with partial melting of variably depleted mantle, and indicate that the host phases began to crystallise prior to the completion of melt aggregation and mixing. We present new major and trace element data from a large number of rehomogenised olivine-hosted melt inclusions from the Cretaceous Paraná-Etendeka and Jurassic Karoo continental flood basalt (CFB) provinces [1]. We show that the major element chemistry of the melt inclusions can be severely disrupted by the rehomogenisation process and, as a consequence, their initial compositions cannot easily be back-calculated. However, despite the age of the samples, the trace element geochemistry of the melt inclusions is well-preserved. Despite coming from near-liquidus olivines from primitive picrites and ferropicrites, the inclusions are remarkably homogeneous; none of the anticipated variability in incompatible trace element compositions is observed. When considered alongside literature data, it appears that variability in primitive melts - as recorded by melt inclusions - is low in CFBs and OIBs relative to ridge settings, e.g. Iceland. We suggest that the tectonic setting imposes a control on the mixing of mantle melts: hot, plume-derived melts generated beneath relatively thick lithosphere may be prone to efficient mixing, perhaps due to their low viscosity, long transport pathways, and/or a superliquidus emplacement temperature [1]. This interpretation is supported by the almost non-existent variability of olivine-hosted inclusions from ferropicrite samples: these magmas represents

Switching Circuit for Shop Vacuum System

NASA Technical Reports Server (NTRS)

Burley, R. K.

1987-01-01

No internal connections to machine tools required. Switching circuit controls vacuum system draws debris from grinders and sanders in machine shop. Circuit automatically turns on vacuum system whenever at least one sander or grinder operating. Debris safely removed, even when operator neglects to turn on vacuum system manually. Pickup coils sense alternating magnetic fields just outside operating machines. Signal from any coil or combination of coils causes vacuum system to be turned on.

Vacuum Brazing of Accelerator Components

NASA Astrophysics Data System (ADS)

Singh, Rajvir; Pant, K. K.; Lal, Shankar; Yadav, D. P.; Garg, S. R.; Raghuvanshi, V. K.; Mundra, G.

2012-11-01

Commonly used materials for accelerator components are those which are vacuum compatible and thermally conductive. Stainless steel, aluminum and copper are common among them. Stainless steel is a poor heat conductor and not very common in use where good thermal conductivity is required. Aluminum and copper and their alloys meet the above requirements and are frequently used for the above purpose. The accelerator components made of aluminum and its alloys using welding process have become a common practice now a days. It is mandatory to use copper and its other grades in RF devices required for accelerators. Beam line and Front End components of the accelerators are fabricated from stainless steel and OFHC copper. Fabrication of components made of copper using welding process is very difficult and in most of the cases it is impossible. Fabrication and joining in such cases is possible using brazing process especially under vacuum and inert gas atmosphere. Several accelerator components have been vacuum brazed for Indus projects at Raja Ramanna Centre for Advanced Technology (RRCAT), Indore using vacuum brazing facility available at RRCAT, Indore. This paper presents details regarding development of the above mentioned high value and strategic components/assemblies. It will include basics required for vacuum brazing, details of vacuum brazing facility, joint design, fixturing of the jobs, selection of filler alloys, optimization of brazing parameters so as to obtain high quality brazed joints, brief description of vacuum brazed accelerator components etc.

Recent Changes in Arctic Sea Ice Melt Onset, Freeze-Up, and Melt Season Length

NASA Technical Reports Server (NTRS)

Markus, Thorsten; Stroeve, Julienne C.; Miller, Jeffrey

2010-01-01

In order to explore changes and trends in the timing of Arctic sea ice melt onset and freeze-up and therefore melt season length, we developed a method that obtains this information directly from satellite passive microwave data, creating a consistent data set from 1979 through present. We furthermore distinguish between early melt (the first day of the year when melt is detected) and the first day of continuous melt. A similar distinction is made for the freeze-up. Using this method we analyze trends in melt onset and freeze-up for 10 different Arctic regions. In all regions except for the Sea of Okhotsk, which shows a very slight and statistically insignificant positive trend (O.4 days/decade), trends in melt onset are negative, i.e. towards earlier melt. The trends range from -1.0day/decade for the Bering Sea to -7.3 days/decade for the East Greenland Sea. Except for the Sea of Okhotsk all areas also show a trend towards later autumn freeze onset. The Chukchi/Beaufort Seas and Laptev/East Siberian Seas observe the strongest trends with 7 days/decade. For the entire Arctic, the melt season length has increased by about 20 days over the last 30 years. Largest trends of over 1O days/decade are seen for Hudson Bay, the East Greenland Sea the Laptev/East Siberian Seas, and the Chukchi/Beaufort Seas. Those trends are statistically significant a1 the 99% level.

On high-pressure melting of tantalum

NASA Astrophysics Data System (ADS)

Luo, Sheng-Nian; Swift, Damian C.

2007-01-01

The issues related to high-pressure melting of Ta are discussed within the context of diamond-anvil cell (DAC) and shock wave experiments, theoretical calculations and common melting models. The discrepancies between the extrapolations of the DAC melting curve and the melting point inferred from shock wave experiments, cannot be reconciled either by superheating or solid-solid phase transition. The failure to reproduce low-pressure DAC melting curve by melting models such as dislocation-mediated melting and the Lindemann law, and molecular dynamics and quantum mechanics-based calculations, undermines their predictions at moderate and high pressures. Despite claims to the contrary, the melting curve of Ta (as well as Mo and W) remains inconclusive at high pressures.

Investigation of Dielectric Breakdown Characteristics for Double-break Vacuum Interrupter and Dielectric Breakdown Probability Distribution in Vacuum Interrupter

NASA Astrophysics Data System (ADS)

Shioiri, Tetsu; Asari, Naoki; Sato, Junichi; Sasage, Kosuke; Yokokura, Kunio; Homma, Mitsutaka; Suzuki, Katsumi

To investigate the reliability of equipment of vacuum insulation, a study was carried out to clarify breakdown probability distributions in vacuum gap. Further, a double-break vacuum circuit breaker was investigated for breakdown probability distribution. The test results show that the breakdown probability distribution of the vacuum gap can be represented by a Weibull distribution using a location parameter, which shows the voltage that permits a zero breakdown probability. The location parameter obtained from Weibull plot depends on electrode area. The shape parameter obtained from Weibull plot of vacuum gap was 10∼14, and is constant irrespective non-uniform field factor. The breakdown probability distribution after no-load switching can be represented by Weibull distribution using a location parameter. The shape parameter after no-load switching was 6∼8.5, and is constant, irrespective of gap length. This indicates that the scatter of breakdown voltage was increased by no-load switching. If the vacuum circuit breaker uses a double break, breakdown probability at low voltage becomes lower than single-break probability. Although potential distribution is a concern in the double-break vacuum cuicuit breaker, its insulation reliability is better than that of the single-break vacuum interrupter even if the bias of the vacuum interrupter's sharing voltage is taken into account.

Vacuum-insulated catalytic converter

DOEpatents

Benson, David K.

2001-01-01

A catalytic converter has an inner canister that contains catalyst-coated substrates and an outer canister that encloses an annular, variable vacuum insulation chamber surrounding the inner canister. An annular tank containing phase-change material for heat storage and release is positioned in the variable vacuum insulation chamber a distance spaced part from the inner canister. A reversible hydrogen getter in the variable vacuum insulation chamber, preferably on a surface of the heat storage tank, releases hydrogen into the variable vacuum insulation chamber to conduct heat when the phase-change material is hot and absorbs the hydrogen to limit heat transfer to radiation when the phase-change material is cool. A porous zeolite trap in the inner canister absorbs and retains hydrocarbons from the exhaust gases when the catalyst-coated substrates and zeolite trap are cold and releases the hydrocarbons for reaction on the catalyst-coated substrate when the zeolite trap and catalyst-coated substrate get hot.

Partial melting of metagreywackes, Part II. Compositions of minerals and melts

NASA Astrophysics Data System (ADS)

Montel, Jean-Marc; Vielzeuf, Daniel

A series of experiments on the fluid-absent melting of a quartz-rich aluminous metagreywacke has been carried out. In this paper, we report the chemical composition of the phases present in the experimental charges as determined by electron microprobe. This analytical work includes biotite, plagioclase, orthopyroxene, garnet, cordierite, hercynite, staurolite, gedrite, oxide, and glass, over the range 100-1000MPa, 780-1025°C. Biotites are Na- and Mg-rich, with Ti contents increasing with temperature. The compositions of plagioclase range from An17 to An35, with a significant orthoclase component, and are always different from the starting minerals. At high temperature, plagioclase crystals correspond to ternary feldspars with Or contents in the range 11-20 mol%. Garnets are almandine pyrope grossular spessartine solid solutions, with a regular and significant increase of the grossular content with pressure. All glasses are silicic (SiO2=67.6-74.4 wt%), peraluminous, and leucocratic (FeO+MgO=0.9-2.9 wt%), with a bulk composition close to that of peraluminous leucogranites, even for degrees of melting as high as 60 vol.%. With increasing pressure, SiO2 contents decrease while K2O increases. At any pressure, the melt compositions are more potassic than the water-saturated granitic minima. The H2O contents estimated by mass balance are in the range 2.5-5.6 wt%. These values are higher than those predicted by thermodynamic models. Modal compositions were estimated by mass balance calculations and by image processing of the SEM photographs. The positions of the 20 to 70% isotects (curves of equal proportion of melt) have been located in the pressure-temperature space between 100MPa and 1000MPa. With increasing pressure, the isotects shift toward lower temperature between 100 and 200MPa, then bend back toward higher temperature. The melting interval increases with pressure; the difference in temperature between the 20% and the 70% isotects is 40°C at 100MPa, and 150�

Channelized Melting Drives Thinning Under a Rapidly Melting Antarctic Ice Shelf

NASA Astrophysics Data System (ADS)

Gourmelen, Noel; Goldberg, Dan N.; Snow, Kate; Henley, Sian F.; Bingham, Robert G.; Kimura, Satoshi; Hogg, Anna E.; Shepherd, Andrew; Mouginot, Jeremie; Lenaerts, Jan T. M.; Ligtenberg, Stefan R. M.; van de Berg, Willem Jan

2017-10-01

Ice shelves play a vital role in regulating loss of grounded ice and in supplying freshwater to coastal seas. However, melt variability within ice shelves is poorly constrained and may be instrumental in driving ice shelf imbalance and collapse. High-resolution altimetry measurements from 2010 to 2016 show that Dotson Ice Shelf (DIS), West Antarctica, thins in response to basal melting focused along a single 5 km-wide and 60 km-long channel extending from the ice shelf's grounding zone to its calving front. If focused thinning continues at present rates, the channel will melt through, and the ice shelf collapse, within 40-50 years, almost two centuries before collapse is projected from the average thinning rate. Our findings provide evidence of basal melt-driven sub-ice shelf channel formation and its potential for accelerating the weakening of ice shelves.

Diffusive loss of argon in response to melt vein formation in polygenetic impact melt breccias

NASA Astrophysics Data System (ADS)

Mercer, Cameron M.; Hodges, Kip V.

2017-08-01

Many planetary surfaces in the solar system have experienced prolonged bombardment. With each impact, new rocks can be assembled that incorporate freshly generated impact melts with fragments of older rocks. Some breccias can become polygenetic, containing multiple generations of impact melt products, and can potentially provide important insights into the extensive bombardment history of a region. However, the amount of chronological information that can be extracted from such samples depends on how well the mineral isotopic systems of geochronometers can preserve the ages of individual melt generations without being disturbed by younger events. We model the thermal evolution of impact melt veins and the resulting loss of Ar from K-bearing phases common in impact melt breccias to assess the potential for preserving the 40Ar/39Ar ages of individual melt generations. Our model results demonstrate that millimeter-scale, clast-free melt veins cause significant heating of adjacent host rock minerals and can cause detectable Ar loss in contact zones that are generally thinner than, and at most about the same thickness as, the vein width. The incorporation of cold clasts in melt veins reduces the magnitudes of heating and Ar loss in the host rocks, and Ar loss can be virtually undetectable for sufficiently clast-rich veins. Quantitative evidence of the timing of impacts, as measured with the 40Ar/39Ar method, can be preserved in polygenetic impact melt breccias, particularly for those containing millimeter-scale bodies of clast-bearing melt products.

Wireless Integrated Microelectronic Vacuum Sensor System

NASA Technical Reports Server (NTRS)

Krug, Eric; Philpot, Brian; Trott, Aaron; Lawrence, Shaun

2013-01-01

NASA Stennis Space Center's (SSC's) large rocket engine test facility requires the use of liquid propellants, including the use of cryogenic fluids like liquid hydrogen as fuel, and liquid oxygen as an oxidizer (gases which have been liquefied at very low temperatures). These fluids require special handling, storage, and transfer technology. The biggest problem associated with transferring cryogenic liquids is product loss due to heat transfer. Vacuum jacketed piping is specifically designed to maintain high thermal efficiency so that cryogenic liquids can be transferred with minimal heat transfer. A vacuum jacketed pipe is essentially two pipes in one. There is an inner carrier pipe, in which the cryogenic liquid is actually transferred, and an outer jacket pipe that supports and seals the vacuum insulation, forming the "vacuum jacket." The integrity of the vacuum jacketed transmission lines that transfer the cryogenic fluid from delivery barges to the test stand must be maintained prior to and during engine testing. To monitor the vacuum in these vacuum jacketed transmission lines, vacuum gauge readings are used. At SSC, vacuum gauge measurements are done on a manual rotation basis with two technicians, each using a handheld instrument. Manual collection of vacuum data is labor intensive and uses valuable personnel time. Additionally, there are times when personnel cannot collect the data in a timely fashion (i.e., when a leak is detected, measurements must be taken more often). Additionally, distribution of this data to all interested parties can be cumbersome. To simplify the vacuum-gauge data collection process, automate the data collection, and decrease the labor costs associated with acquiring these measurements, an automated system that monitors the existing gauges was developed by Invocon, Inc. For this project, Invocon developed a Wireless Integrated Microelectronic Vacuum Sensor System (WIMVSS) that provides the ability to gather vacuum

Global simulation of the induction heating TSSG process of SiC for the effects of Marangoni convection, free surface deformation and seed rotation

NASA Astrophysics Data System (ADS)

Yamamoto, Takuya; Okano, Yasunori; Ujihara, Toru; Dost, Sadik

2017-07-01

A global numerical simulation was performed for the induction heating Top-Seeded Solution Growth (TSSG) process of SiC. Analysis included the furnace and growth melt. The effects of interfacial force due to free surface tension gradient, the RF coil-induced electromagnetic body force, buoyancy, melt free surface deformation, and seed rotation were examined. The simulation results showed that the contributions of free surface tension gradient and the electromagnetic body force to the melt flow are significant. Marangoni convection affects the growth process adversely by making the melt flow downward in the region under the seed crystal. This downward flow reduces carbon flux into the seed and consequently lowers growth rate. The effects of free surface deformation and seed rotation, although positive, are not so significant compared with those of free surface tension gradient and the electromagnetic body force. Due to the small size of the melt the contribution of buoyancy is also small.

Processing and Properties of Vacuum Assisted Resin Transfer Molded Phenylethynyl Terminated Imide Composites

NASA Technical Reports Server (NTRS)

Cano, Roberto J.; Ghose, Sayata; Watson, Kent A.; Chunchu, Prasad B.; Jensen, Brian J.; Connell, John W.

2012-01-01

Polyimide composites are very attractive for applications that require a high strength to weight ratio and thermal stability. Recent work at NASA Langley Research Center (LaRC) has concentrated on developing new polyimide resin systems that can be processed without the use of an autoclave for advanced aerospace applications. Due to their low melt viscosities and long melt stability, certain phenylethynyl terminated imides (PETI) can be processed into composites using high temperature vacuum assisted resin transfer molding (HT-VARTM). VARTM has shown the potential to reduce the manufacturing cost of composite structures. In the current study, two PETI resins, LARC(Trademark) PETI-330 and LARC(Trademark) PETI-9, were infused into carbon fiber preforms at 260 C and cured at temperatures up to 371 C. Photomicrographs of polished cross sections were taken and void contents, determined by acid digestion, were below 4.5%. Mechanical properties including short block compression (SBC), compression after impact (CAI), and open hole compression (OHC) were determined at room temperature, 177 C, and 288 C. Both PETI-9 and PETI-330 composites demonstrated very good retention of mechanical properties at elevated temperatures. SBC and OHC properties after aging for 1000 hours at temperatures up to 288 C were also determined.

Fault rheology beyond frictional melting.

PubMed

Lavallée, Yan; Hirose, Takehiro; Kendrick, Jackie E; Hess, Kai-Uwe; Dingwell, Donald B

2015-07-28

During earthquakes, comminution and frictional heating both contribute to the dissipation of stored energy. With sufficient dissipative heating, melting processes can ensue, yielding the production of frictional melts or "pseudotachylytes." It is commonly assumed that the Newtonian viscosities of such melts control subsequent fault slip resistance. Rock melts, however, are viscoelastic bodies, and, at high strain rates, they exhibit evidence of a glass transition. Here, we present the results of high-velocity friction experiments on a well-characterized melt that demonstrate how slip in melt-bearing faults can be governed by brittle fragmentation phenomena encountered at the glass transition. Slip analysis using models that incorporate viscoelastic responses indicates that even in the presence of melt, slip persists in the solid state until sufficient heat is generated to reduce the viscosity and allow remobilization in the liquid state. Where a rock is present next to the melt, we note that wear of the crystalline wall rock by liquid fragmentation and agglutination also contributes to the brittle component of these experimentally generated pseudotachylytes. We conclude that in the case of pseudotachylyte generation during an earthquake, slip even beyond the onset of frictional melting is not controlled merely by viscosity but rather by an interplay of viscoelastic forces around the glass transition, which involves a response in the brittle/solid regime of these rock melts. We warn of the inadequacy of simple Newtonian viscous analyses and call for the application of more realistic rheological interpretation of pseudotachylyte-bearing fault systems in the evaluation and prediction of their slip dynamics.

Additive Manufacturing of Patient-Customizable Scaffolds for Tubular Tissues Using the Melt-Drawing Method.

PubMed

Tan, Yu Jun; Tan, Xipeng; Yeong, Wai Yee; Tor, Shu Beng

2016-11-03

Polymeric fibrous scaffolds for guiding cell growth are designed to be potentially used for the tissue engineering (TE) of tubular organs including esophagi, blood vessels, tracheas, etc. Tubular scaffolds were fabricated via melt-drawing of highly elastic poly(l-lactide-co-ε-caprolactone) (PLC) fibers layer-by-layer on a cylindrical mandrel. The diameter and length of the scaffolds are customizable via 3D printing of the mandrel. Thickness of the scaffolds was varied by changing the number of layers of the melt-drawing process. The morphology and tensile properties of the PLC fibers were investigated. The fibers were highly aligned with a uniform diameter. Their diameters and tensile properties were tunable by varying the melt-drawing speeds. These tailorable topographies and tensile properties show that the additive-based scaffold fabrication technique is customizable at the micro- and macro-scale for different tubular tissues. The merits of these scaffolds in TE were further shown by the finding that myoblast and fibroblast cells seeded onto the scaffolds in vitro showed appropriate cell proliferation and distribution. Human mesenchymal stem cells (hMSCs) differentiated to smooth muscle lineage on the microfibrous scaffolds in the absence of soluble induction factors, showing cellular shape modulation and scaffold elasticity may encourage the myogenic differentiation of stem cells.

Running vacuum cosmological models: linear scalar perturbations

NASA Astrophysics Data System (ADS)

Perico, E. L. D.; Tamayo, D. A.

2017-08-01

In cosmology, phenomenologically motivated expressions for running vacuum are commonly parameterized as linear functions typically denoted by Λ(H2) or Λ(R). Such models assume an equation of state for the vacuum given by bar PΛ = - bar rhoΛ, relating its background pressure bar PΛ with its mean energy density bar rhoΛ ≡ Λ/8πG. This equation of state suggests that the vacuum dynamics is due to an interaction with the matter content of the universe. Most of the approaches studying the observational impact of these models only consider the interaction between the vacuum and the transient dominant matter component of the universe. We extend such models by assuming that the running vacuum is the sum of independent contributions, namely bar rhoΛ = Σibar rhoΛi. Each Λ i vacuum component is associated and interacting with one of the i matter components in both the background and perturbation levels. We derive the evolution equations for the linear scalar vacuum and matter perturbations in those two scenarios, and identify the running vacuum imprints on the cosmic microwave background anisotropies as well as on the matter power spectrum. In the Λ(H2) scenario the vacuum is coupled with every matter component, whereas the Λ(R) description only leads to a coupling between vacuum and non-relativistic matter, producing different effects on the matter power spectrum.

Particle-in-cell simulations of electron beam control using an inductive current divider

DOE PAGES

Swanekamp, S. B.; Angus, J. R.; Cooperstein, G.; ...

2015-11-18

Kinetic, time-dependent, electromagnetic, particle-in-cell simulations of the inductive current divider are presented. The inductive current divider is a passive method for controlling the trajectory of an intense, hollow electron beam using a vacuum structure that inductively splits the beam’s return current. The current divider concept was proposed and studied theoretically in a previous publication [Phys. Plasmas 22, 023107 (2015)] A central post carries a portion of the return current (I 1) while the outer conductor carries the remainder (I 2) with the injected beam current given by I b=I 1+I 2. The simulations are in agreement with the theory whichmore » predicts that the total force on the beam trajectory is proportional to (I 2-I 1) and the force on the beam envelope is proportional to I b. For a fixed central post, the beam trajectory is controlled by varying the outer conductor radius which changes the inductance in the return-current path. The simulations show that the beam emittance is approximately constant as the beam propagates through the current divider to the target. As a result, independent control over both the current density and the beam angle at the target is possible by choosing the appropriate return-current geometry.« less

Size effects on melting and wetting in the Ga-Pb nano-alloy

NASA Astrophysics Data System (ADS)

Allione, M.; Kofman, R.; Celestini, F.; Lereah, Y.

2009-04-01

Ga-Pb alloys with 15 at% Pb mean concentration have been prepared at the nanoscale by means of evaporation-condensation technique in ultra high vacuum conditions. Transmission electron microscope images indicate that at room temperature, the system is a two-components breath figure composed of liquid Ga nanodrops containing Pb nanocrystals. Some thermodynamic properties of this nano-alloy are investigated for different temperatures and particle sizes. The results obtained put in evidence a large modification of the Ga-Pb bulk phase diagram: a decrease of the melting temperatures of the two components as well as the ones of the miscibility gap. Changes in the microscopic structure of the system as a function of temperature have been investigated and a full wetting transition from a dry to a completely wet state has been put in evidence.

Melt inclusions: Chapter 6

USGS Publications Warehouse

,; Lowenstern, J. B.

2014-01-01

Melt inclusions are small droplets of silicate melt that are trapped in minerals during their growth in a magma. Once formed, they commonly retain much of their initial composition (with some exceptions) unless they are re-opened at some later stage. Melt inclusions thus offer several key advantages over whole rock samples: (i) they record pristine concentrations of volatiles and metals that are usually lost during magma solidification and degassing, (ii) they are snapshots in time whereas whole rocks are the time-integrated end products, thus allowing a more detailed, time-resolved view into magmatic processes (iii) they are largely unaffected by subsolidus alteration. Due to these characteristics, melt inclusions are an ideal tool to study the evolution of mineralized magma systems. This chapter first discusses general aspects of melt inclusions formation and methods for their investigation, before reviewing studies performed on mineralized magma systems.

14 CFR 29.1433 - Vacuum systems.

Code of Federal Regulations, 2010 CFR

2010-01-01

... STANDARDS: TRANSPORT CATEGORY ROTORCRAFT Equipment Miscellaneous Equipment § 29.1433 Vacuum systems. (a... the discharge lines from the vacuum air pump when the delivery temperature of the air becomes unsafe. (b) Each vacuum air system line and fitting on the discharge side of the pump that might contain...

Vacuum Technology Considerations For Mass Metrology

PubMed Central

Abbott, Patrick J.; Jabour, Zeina J.

2011-01-01

Vacuum weighing of mass artifacts eliminates the necessity of air buoyancy correction and its contribution to the measurement uncertainty. Vacuum weighing is also an important process in the experiments currently underway for the redefinition of the SI mass unit, the kilogram. Creating the optimum vacuum environment for mass metrology requires careful design and selection of construction materials, plumbing components, pumping, and pressure gauging technologies. We review the vacuum technology1 required for mass metrology and suggest procedures and hardware for successful and reproducible operation. PMID:26989593

Gas propagation in a liquid helium cooled vacuum tube following a sudden vacuum loss

NASA Astrophysics Data System (ADS)

Dhuley, Ram C.

This dissertation describes the propagation of near atmospheric nitrogen gas that rushes into a liquid helium cooled vacuum tube after the tube suddenly loses vacuum. The loss-of-vacuum scenario resembles accidental venting of atmospheric air to the beam-line of a superconducting radio frequency particle accelerator and is investigated to understand how in the presence of condensation, the in-flowing air will propagate in such geometry. In a series of controlled experiments, room temperature nitrogen gas (a substitute for air) at a variety of mass flow rates was vented to a high vacuum tube immersed in a bath of liquid helium. Pressure probes and thermometers installed on the tube along its length measured respectively the tube pressure and tube wall temperature rise due to gas flooding and condensation. At high mass in-flow rates a gas front propagated down the vacuum tube but with a continuously decreasing speed. Regression analysis of the measured front arrival times indicates that the speed decreases nearly exponentially with the travel length. At low enough mass in-flow rates, no front propagated in the vacuum tube. Instead, the in-flowing gas steadily condensed over a short section of the tube near its entrance and the front appeared to `freeze-out'. An analytical expression is derived for gas front propagation speed in a vacuum tube in the presence of condensation. The analytical model qualitatively explains the front deceleration and flow freeze-out. The model is then simplified and supplemented with condensation heat/mass transfer data to again find the front to decelerate exponentially while going away from the tube entrance. Within the experimental and procedural uncertainty, the exponential decay length-scales obtained from the front arrival time regression and from the simplified model agree.

Developing a vacuum cooking equipment prototype to produce strawberry jam and optimization of vacuum cooking conditions.

PubMed

Okut, Dilara; Devseren, Esra; Koç, Mehmet; Ocak, Özgül Özdestan; Karataş, Haluk; Kaymak-Ertekin, Figen

2018-01-01

Purpose of this study was to develop prototype cooking equipment that can work at reduced pressure and to evaluate its performance for production of strawberry jam. The effect of vacuum cooking conditions on color soluble solid content, reducing sugars total sugars HMF and sensory properties were investigated. Also, the optimum vacuum cooking conditions for strawberry jam were optimized for Composite Rotatable Design. The optimum cooking temperature and time were determined targeting maximum soluble solid content and sensory attributes (consistency) and minimum Hue value and HMF content. The optimum vacuum cooking conditions determined were 74.4 °C temperature and 19.8 time. The soluble solid content strawberry jam made by vacuum process were similar to those prepared by traditional method. HMF contents of jams produced with vacuum cooking method were well within limit of standards.

Greater-than-bulk melting temperatures explained: Gallium melts Gangnam style

NASA Astrophysics Data System (ADS)

Gaston, Nicola; Steenbergen, Krista

2014-03-01

The experimental discovery of superheating in gallium clusters contradicted the clear and well-demonstrated paradigm that the melting temperature of a particle should decrease with its size. However the extremely sensitive dependence of melting temperature on size also goes to the heart of cluster science, and the interplay between the effects of electronic and geometric structure. We have performed extensive first-principles molecular dynamics calculations, incorporating parallel tempering for an efficient exploration of configurational phase space. This is necessary, due to the complicated energy landscape of gallium. In the nanoparticles, melting is preceded by a transitions between phases. A structural feature, referred to here as the Gangnam motif, is found to increase with the latent heat and appears throughout the observed phase changes of this curious metal. We will present our detailed analysis of the solid-state isomers, performed using extensive statistical sampling of the trajectory data for the assignment of cluster structures to known phases of gallium. Finally, we explain the greater-than-bulk melting through analysis of the factors that stabilise the liquid structures.

Plastic welder

NASA Technical Reports Server (NTRS)

Buckley, J. D.; Fox, R. L.; Swain, R. J.

1980-01-01

Low-cost, self-contained, portable welder joins plastic parts by induction heating. Welder is useable in any atmosphere or in vacuum and with most types of thermoplastic; plastic components can be joined in situ. Device is applicable to aerospace industry and in automobile, furniture, and construction industries. Power requirements are easily met by battery or solar energy. In welder, toroidal inductor transfers magnetic flux through thermoplastic to screen. Heated screen causes plastic surface on either side to melt and flow into it to form joint.

Seedless Growth of Bismuth Nanowire Array via Vacuum Thermal Evaporation

PubMed Central

Liu, Mingzhao; Nam, Chang-Yong; Zhang, Lihua

2015-01-01

Here a seedless and template-free technique is demonstrated to scalably grow bismuth nanowires, through thermal evaporation in high vacuum at RT. Conventionally reserved for the fabrication of metal thin films, thermal evaporation deposits bismuth into an array of vertical single crystalline nanowires over a flat thin film of vanadium held at RT, which is freshly deposited by magnetron sputtering or thermal evaporation. By controlling the temperature of the growth substrate the length and width of the nanowires can be tuned over a wide range. Responsible for this novel technique is a previously unknown nanowire growth mechanism that roots in the mild porosity of the vanadium thin film. Infiltrated into the vanadium pores, the bismuth domains (~ 1 nm) carry excessive surface energy that suppresses their melting point and continuously expels them out of the vanadium matrix to form nanowires. This discovery demonstrates the feasibility of scalable vapor phase synthesis of high purity nanomaterials without using any catalysts. PMID:26709727

14 CFR 29.1433 - Vacuum systems.

Code of Federal Regulations, 2014 CFR

2014-01-01

... 14 Aeronautics and Space 1 2014-01-01 2014-01-01 false Vacuum systems. 29.1433 Section 29.1433... STANDARDS: TRANSPORT CATEGORY ROTORCRAFT Equipment Miscellaneous Equipment § 29.1433 Vacuum systems. (a.... (b) Each vacuum air system line and fitting on the discharge side of the pump that might contain...

Detailed numerical simulation of cathode spots in vacuum arcs: Interplay of different mechanisms and ejection of droplets

NASA Astrophysics Data System (ADS)

Kaufmann, H. T. C.; Cunha, M. D.; Benilov, M. S.; Hartmann, W.; Wenzel, N.

2017-10-01

A model of cathode spots in high-current vacuum arcs is developed with account of all the potentially relevant mechanisms: the bombardment of the cathode surface by ions coming from a pre-existing plasma cloud; vaporization of the cathode material in the spot, its ionization, and the interaction of the produced plasma with the cathode; the Joule heat generation in the cathode body; melting of the cathode material and motion of the melt under the effect of the plasma pressure and the Lorentz force and related phenomena. After the spot has been ignited by the action of the cloud (which takes a few nanoseconds), the metal in the spot is melted and accelerated toward the periphery of the spot, with the main driving force being the pressure due to incident ions. Electron emission cooling and convective heat transfer are dominant mechanisms of cooling in the spot, limiting the maximum temperature of the cathode to approximately 4700-4800 K. A crater is formed on the cathode surface in this way. After the plasma cloud has been extinguished, a liquid-metal jet is formed and a droplet is ejected. No explosions have been observed. The modeling results conform to estimates of different mechanisms of cathode erosion derived from the experimental data on the net and ion erosion of copper cathodes.

The Extra Flask

NASA Astrophysics Data System (ADS)

Thielemann, R.

1981-05-01

It seemed quite natural and logical for me to want to address such an informed group about some of the many superalloys developed over the past forty years-but then I realized that most, if not all of them are listed with their compositions and properties in the ASM Metals Handbook, so this subject did not seem promising. At this point I started to think about the many new and important developments in processing techniques that made the melting, casting, and forming of the alloys possible. It seemed to me that the new procedures were, in most every instance, just as important as the new compositions themselves. Without the new techniques, many of the higher strength compositions were difficult, if not impossible to produce by existing procedures. Certainly, vacuum induction melting allowed us to melt and cast the titanium-and aluminum-bearing compositions without incurring the usual oxide and nitride inclusions.

Vacuum status-display and sector-conditioning programs

NASA Astrophysics Data System (ADS)

Skelly, J.; Yen, S.

1990-08-01

Two programs have been developed for observation and control of the AGS vacuum system, which include the following notable features: (1) they incorporate a graphical user interface and (2) they are driven by a relational database which describes the vacuum system. The vacuum system comprises some 440 devices organized into 28 vacuum sectors. The status-display program invites menu selection of a sector, interrogates the relational database for relevant vacuum devices, acquires live readbacks and posts a graphical display of their status. The sector-conditioning program likewise invites sector selection, produces the same status display and also implements process control logic on the sector devices to pump the sector down from atmospheric pressure to high vacuum over a period extending several hours. As additional devices are installed in the vacuum system, the devices are added to the relational database; these programs then automatically include the new devices.

Hypoeutectic melting in the UO2-x-Gd2O3 system

NASA Astrophysics Data System (ADS)

Journeau, Christophe; Fouquart, Pascal; Domenger, Renaud; Allegri, Patrick

2017-05-01

Gadolinium is one of the best neutron absorber materials and its use can be considered as a sacrificial material in a Sodium Fast Reactor core catcher in view of preventing recriticallity. A series of experiments have been conducted in the VITI induction-heated facility to study the melting in the UO2-x-Gd2O3 system with 60-87 mol% gadolinia. These experiments have indicated that the eutectic composition is around 92 mol% Gd2O3 - 8 mol% UO2-x and that the liquidus line is close to that of Popov et al. [Atom. Energ. 110 (2011) pp. 221-229] phase diagram.

Working in a Vacuum

ERIC Educational Resources Information Center

Rathey, Allen

2005-01-01

In this article, the author discusses several myths about vacuum cleaners and offers tips on evaluating and purchasing this essential maintenance tool. These myths are: (1) Amps mean performance; (2) Everyone needs high-efficiency particulate air (HEPA): (3) Picking up a "bowling ball" shows cleaning power; (4) All vacuum bags are the same; (5)…

Effect of Feed Forms on the Results of Melting of Fly Ash by a DC Plasma Arc Furnace

NASA Astrophysics Data System (ADS)

Chen, Mingzhou; Meng, Yuedong; Shi, Jiabiao; Ni, Guohua; Jiang, Yiman; Yu, Xinyao; ZHAO, Peng

2009-10-01

Fly ash from a municipal solid waste incinerator (MSWI) without preprocessing (original fly ash, OFA) was melted by a direct current (DC) plasma arc furnace to investigate how the feed forms governed the results. Dioxins in flue gas from stack and bag-filter ash (BFA) were detected. The distribution of heavy metals of Pb, Cd, As, and Cr along the flue gas process system was analyzed. Through a comparison of the results for dioxins and heavy metals in this study and previous work, carrying-over of fly ash particles with the flue gas stream can be deduced. Based on the magnetic induction equation and Navier-Stokes equations, a magnetohydrodynamic (MHD) model for the plasma arc was developed to describe the particle-carrying effect. The results indicate that, a. when melted, the feed forms of MSWI fly ash affect the results significantly; b. it is not preferable to melt MSWI fly ash directly, and efforts should be made to limit the mass transfer of OFA from the plasma furnace.

Some physical aspects of fluid-fluxed melting

NASA Astrophysics Data System (ADS)

Patiño Douce, A.

2012-04-01

Fluid-fluxed melting is thought to play a crucial role in the origin of many terrestrial magmas. We can visualize the fundamental physics of the process as follows. An infinitesimal amount of fluid infiltrates dry rock at the temperature of its dry solidus. In order to restore equilibrium the temperature must drop, so that enthalpy is released and immediately reabsorbed as enthalpy of melting. The amount of melt produced must be such that the energy balance and thermodynamic equilibrium conditions are simultaneously satisfied. We wish to understand how an initially dry rock melts in response to progressive fluid infiltration, under both batch and fractional melting constraints. The simplest physical model for this process is a binary system in which one of the components makes up a pure solid phase and the other component a pure fluid phase, and in which a binary melt phase exists over certain temperature range. Melting point depression is calculated under the assumption of ideal mixing. The equations of energy balance and thermodynamic equilibrium are solved simultaneously for temperature and melt fraction, using an iterative procedure that allows addition of fluid in infinitesimal increments. Batch melting and fractional melting are simulated by allowing successive melt increments to remain in the system (batch) or not (fractional). Despite their simplified nature, these calculations reveal some important aspects of fluid-fluxed melting. The model confirms that, if the solubility of the fluid in the melt is sufficiently high, fluid fluxed melting is an efficient mechanism of magma generation. One might expect that the temperature of the infiltrating fluid would have a significant effect on melt productivity, but the results of the calculations show this not to be the case, because a relatively small mass of low molecular weight fluid has a strong effect on the melting point of minerals with much higher molecular weights. The calculations reveal the somewhat

Nonperturbative vacuum polarization effects in two-dimensional supercritical Dirac-Coulomb system I. Vacuum charge density

NASA Astrophysics Data System (ADS)

Davydov, A.; Sveshnikov, K.; Voronina, Yu.

2018-01-01

Based on the original combination of analytical methods, computer algebra tools and numerical calculations, proposed recently in Refs. 1-3, the nonperturbative vacuum polarization effects in the 2+1D supercritical Dirac-Coulomb system with Z > Zcr,1 are explored. Both the vacuum charge density ρV P(r→) and vacuum energy ℰV P are considered. The main result of the work is that in the overcritical region ℰV P turns out to be a rapidly decreasing function ˜-ηeffZ3/R with ηeff > 0 and R being the size of the external Coulomb source. Due to a lot of details of calculation the whole work is divided into two parts I and II. In the present part I, we consider the evaluation and behavior of the vacuum density ρV P, which further is used in part II for evaluation of the vacuum energy, with emphasis on the renormalization, convergence of the partial expansion for ρV P and behavior of the integral induced charge QV P in the overcritical region.

Demonstration of a non-contact x-ray source using an inductively heated pyroelectric accelerator

NASA Astrophysics Data System (ADS)

Klopfer, Michael; Satchouk, Vladimir; Cao, Anh; Wolowiec, Thomas; Alivov, Yahya; Molloi, Sabee

2015-04-01

X-ray emission from pyroelectric sources can be produced through non-contact thermal cycling using induction heating. In this study, we demonstrated a proof of concept non-contact x-ray source powered via induction heating. An induction heater operating at 62.5 kHz provided a total of 6.5 W of delivered peak thermal power with 140 V DC of driving voltage. The heat was applied to a ferrous substrate mechanically coupled to a cubic 1 cm3 Lithium Niobate (LiNbO3) pyroelectric crystal maintained in a 3-12 mTorr vacuum. The maximum temperature reached was 175 °C in 86 s of heating. The cooling cycle began immediately after heating and was provided by passive radiative cooling. The total combined cycle time was 250 s. x-ray photons were produced and analyzed in both heating and cooling phases. Maximum photon energies of 59 keV and 55 keV were observed during heating and cooling, respectively. Non-contact devices such as this, may find applications in cancer therapy (brachytherapy), non-destructive testing, medical imaging, and physics education fields.

Evolution of melt-vapor surface tension in silicic volcanic systems: Experiments with hydrous melts

USGS Publications Warehouse

Mangan, M.; Sisson, T.

2005-01-01

We evaluate the melt-vapor surface tension (??) of natural, water-saturated dacite melt at 200 MPa, 950-1055??C, and 4.8-5.7 wt % H2O. We experimentally determine the critical supersaturation pressure for bubble nucleation as a function of dissolved water and then solve for ?? at those conditions using classical nucleation theory. The solutions obtained give dacite melt-vapor surface tensions that vary inversely with dissolved water from 0.042 (??0.003) J m-2 at 5.7 wt% H2O to 0.060 (??0.007) J m-2 at 5.2 wt% H2O to 0.073 (??0.003) J m-2 at 4.8 wt% H2O. Combining our dacite results with data from published hydrous haplogranite and high-silica rhyolite experiments reveals that melt-vapor surface tension also varies inversely with the concentration of mafic melt components (e.g., CaO, FeOtotal, MgO). We develop a thermodynamic context for these observations in which melt-vapor surface tension is represented by a balance of work terms controlled by melt structure. Overall, our results suggest that cooling, crystallization, and vapor exsolution cause systematic changes in ?? that should be considered in dynamic modeling of magmatic processes.

Temperature and composition dependencies of trace element partitioning - Olivine/melt and low-Ca pyroxene/melt

NASA Technical Reports Server (NTRS)

Colson, R. O.; Mckay, G. A.; Taylor, L. A.

1988-01-01

This paper presents a systematic thermodynamic analysis of the effects of temperature and composition on olivine/melt and low-Ca pyroxene/melt partitioning. Experiments were conducted in several synthetic basalts with a wide range of Fe/Mg, determining partition coefficients for Eu, Ca, Mn, Fe, Ni, Sm, Cd, Y, Yb, Sc, Al, Zr, and Ti and modeling accurately the changes in free energy for trace element exchange between crystal and melt as functions of the trace element size and charge. On the basis of this model, partition coefficients for olivine/melt and low-Ca pyroxene/melt can be predicted for a wide range of elements over a variety of basaltic bulk compositions and temperatures. Moreover, variations in partition coeffeicients during crystallization or melting can be modeled on the basis of changes in temperature and major element chemistry.

Microhardness variation and related microstructure in Al-Cu alloys prepared by HF induction melting and RF sputtering

NASA Astrophysics Data System (ADS)

Boukhris, N.; Lallouche, S.; Debili, M. Y.; Draissia, M.

2009-03-01

The materials under consideration are binary aluminium-copper alloys (10 at% to 90.3 at%Cu) produced by HF melting and RF magnetron sputtering. The resulting micro structures have been observed by standard metallographic techniques, X-ray powder diffraction, scanning electron microscopy and transmission electron microscopy. Vickers microhardness of bulk Al-Cu alloys reaches a maximum of 1800 MPa at 70.16 at%Cu. An unexpected metastable θ ' phase has been observed within aluminium grain in Al-37 at%Cu. The mechanical properties of a family of homogeneous Al{1-x}Cu{x} (0 < x < 0.92) thin films made by radiofrequency (13.56 MHz) cathodic magnetron sputtering from composite Al-Cu targets have been investigated. The as-deposited microstructures for all film compositions consisted of a mixture of the two expected face-centred-cubic (fcc) Al solid solution and tetragonal θ (Al{2}Cu) phases. The microhardness regularly increases and the grain size decreases both with copper concentration. This phenomenon of significant mechanical strengthening of aluminium by means of copper is essentially due to a combination between solid solution effects and grain size refinement. This paper reports some structural features of different Al-Cu alloys prepared by HF melting and RF magnetron on glass substrate sputtering.

Nonperturbative vacuum polarization effects in two-dimensional supercritical Dirac-Coulomb system II. Vacuum energy

NASA Astrophysics Data System (ADS)

Davydov, A.; Sveshnikov, K.; Voronina, Yu.

2018-01-01

Nonperturbative vacuum polarization effects are explored for a supercritical Dirac-Coulomb system with Z > Zcr,1 in 2+1D, based on the original combination of analytical methods, computer algebra and numerical calculations, proposed recently in Refs. 1-3. Both the vacuum charge density ρV P(r→) and vacuum energy ℰV P are considered. Due to a lot of details of calculation the whole work is divided into two parts I and II. Taking account of results, obtained in the part I4 for ρV P, in the present part II, the evaluation of the vacuum energy ℰV P is investigated with emphasis on the renormalization and convergence of the partial expansion for ℰV P. It is shown that the renormalization via fermionic loop turns out to be the universal tool, which removes the divergence of the theory both in the purely perturbative and essentially nonperturbative regimes of the vacuum polarization. The main result of calculation is that for a wide range of the system parameters in the overcritical region ℰV P turns out to be a rapidly decreasing function ˜-ηeffZ3/R with ηeff > 0 and R being the size of the external Coulomb source. To the end the similarity in calculations of ℰV P in 2+1 and 3+1D is discussed, and qualitative arguments are presented in favor of the possibility for complete screening of the classical electrostatic energy of the Coulomb source by the vacuum polarization effects for Z ≫ Zcr,1 in 3+1D.

Quantum vacuum noise in physics and cosmology.

PubMed

Davies, P. C. W.

2001-09-01

The concept of the vacuum in quantum field theory is a subtle one. Vacuum states have a rich and complex set of properties that produce distinctive, though usually exceedingly small, physical effects. Quantum vacuum noise is familiar in optical and electronic devices, but in this paper I wish to consider extending the discussion to systems in which gravitation, or large accelerations, are important. This leads to the prediction of vacuum friction: The quantum vacuum can act in a manner reminiscent of a viscous fluid. One result is that rapidly changing gravitational fields can create particles from the vacuum, and in turn the backreaction on the gravitational dynamics operates like a damping force. I consider such effects in early universe cosmology and the theory of quantum black holes, including the possibility that the large-scale structure of the universe might be produced by quantum vacuum noise in an early inflationary phase. I also discuss the curious phenomenon that an observer who accelerates through a quantum vacuum perceives a bath of thermal radiation closely analogous to Hawking radiation from black holes, even though an inertial observer registers no particles. The effects predicted raise very deep and unresolved issues about the nature of quantum particles, the role of the observer, and the relationship between the quantum vacuum and the concepts of information and entropy. (c) 2001 American Institute of Physics.

Running vacuum cosmological models: linear scalar perturbations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Perico, E.L.D.; Tamayo, D.A., E-mail: elduartep@usp.br, E-mail: tamayo@if.usp.br

In cosmology, phenomenologically motivated expressions for running vacuum are commonly parameterized as linear functions typically denoted by Λ( H {sup 2}) or Λ( R ). Such models assume an equation of state for the vacuum given by P-bar {sub Λ} = - ρ-bar {sub Λ}, relating its background pressure P-bar {sub Λ} with its mean energy density ρ-bar {sub Λ} ≡ Λ/8π G . This equation of state suggests that the vacuum dynamics is due to an interaction with the matter content of the universe. Most of the approaches studying the observational impact of these models only consider the interactionmore » between the vacuum and the transient dominant matter component of the universe. We extend such models by assuming that the running vacuum is the sum of independent contributions, namely ρ-bar {sub Λ} = Σ {sub i} ρ-bar {sub Λ} {sub i} . Each Λ i vacuum component is associated and interacting with one of the i matter components in both the background and perturbation levels. We derive the evolution equations for the linear scalar vacuum and matter perturbations in those two scenarios, and identify the running vacuum imprints on the cosmic microwave background anisotropies as well as on the matter power spectrum. In the Λ( H {sup 2}) scenario the vacuum is coupled with every matter component, whereas the Λ( R ) description only leads to a coupling between vacuum and non-relativistic matter, producing different effects on the matter power spectrum.« less

The Role of CO2 on Silica Undersaturated Melt Structure: Implication for Melt Physical Properties

NASA Astrophysics Data System (ADS)

Scaillet, B.; Morizet, Y.; Paris, M.; Gaillard, F.

2012-12-01

Silica undersaturated melts such as nephelinite and melilitite are very peculiar magmatic materials. Their occurrence on the Earth surface is often associated with carbonatites melts. These low-silica melts can dissolve a large quantity of CO2 issued from mantle fluid metasomatism. However, the melt structure, the way CO2 dissolves into these melts and the effect of different alkalis element are poorly constrained. We present preliminary experimental results on the melt structure of synthetic nephelinite (NBO/T = 1.25) and Ca-melilitite (NBO/T = 2.50) synthesized in the NKCMAS system and equilibrated at high-pressure (200-300 MPa), high-temperature (1250°C) with an excess C-O-H fluid phase. The nephelinite glasses were synthesized with varying K2O / K2O+Na2O (0-10 mol.% K2O) ratio so as to investigate the differential effect of those two cations. All experiments were conducted under oxidizing conditions (ΔNNO+5) resulting in binary fluid phase composition with CO2 and H2O species. The silicate melt structure, CO2 solubility and speciation were investigated using Micro-Raman and Solid State NMR spectroscopies for 13C, 1H, 29Si, 27Al and 23Na nuclei. The replacement of Na by K does not change the nephelinite melt structure for volatile-free sample suggesting that the basicity of these glasses is not dramatically affected by the presence of mixed alkali. Within 5 mol.% K2O, the CO2 solubility (measured in relative to Raman signature of the melt structure) is only slightly affected with an increasing CO2 solubility with increasing K2O content. As a function of pressure, we observe an increase in CO2 solubility consistent with previous studies. The 13C NMR investigation of the CO2 speciation show three different carbonates environments for CO2 in nephelinite melts attributed to non-network carbonates: 1) 170 ppm shift assigned to NBO-carb. Na or K; 2) 169 ppm assigned to NBO-carb. Ca; and 3) 165 ppm assigned to isolated Na+..CO32- carbonates. As K2O is increased into

Thermodynamics of Oligonucleotide Duplex Melting

ERIC Educational Resources Information Center

Schreiber-Gosche, Sherrie; Edwards, Robert A.

2009-01-01

Melting temperatures of oligonucleotides are useful for a number of molecular biology applications, such as the polymerase chain reaction (PCR). Although melting temperatures are often calculated with simplistic empirical equations, application of thermodynamics provides more accurate melting temperatures and an opportunity for students to apply…

First-principles melting of gallium clusters down to nine atoms: structural and electronic contributions to melting.

PubMed

Steenbergen, Krista G; Gaston, Nicola

2013-10-07

First-principles Born-Oppenheimer molecular dynamics simulations of small gallium clusters, including parallel tempering, probe the distinction between cluster and molecule in the size range of 7-12 atoms. In contrast to the larger sizes, dynamic measures of structural change at finite temperature demonstrate that Ga7 and Ga8 do not melt, suggesting a size limit to melting in gallium exists at 9 atoms. Analysis of electronic structure further supports this size limit, additionally demonstrating that a covalent nature cannot be identified for clusters larger than the gallium dimer. Ga9, Ga10 and Ga11 melt at greater-than-bulk temperatures, with no evident covalent character. As Ga12 represents the first small gallium cluster to melt at a lower-than-bulk temperature, we examine the structural properties of each cluster at finite temperature in order to probe both the origins of greater-than-bulk melting, as well as the significant differences in melting temperatures induced by a single atom addition. Size-sensitive melting temperatures can be explained by both energetic and entropic differences between the solid and liquid phases for each cluster. We show that the lower-than-bulk melting temperature of the 12-atom cluster can be attributed to persistent pair bonding, reminiscent of the pairing observed in α-gallium. This result supports the attribution of greater-than-bulk melting in gallium clusters to the anomalously low melting temperature of the bulk, due to its dimeric structure.

Automatic Control of Silicon Melt Level

NASA Technical Reports Server (NTRS)

Duncan, C. S.; Stickel, W. B.

1982-01-01

A new circuit, when combined with melt-replenishment system and melt level sensor, offers continuous closed-loop automatic control of melt-level during web growth. Installed on silicon-web furnace, circuit controls melt-level to within 0.1 mm for as long as 8 hours. Circuit affords greater area growth rate and higher web quality, automatic melt-level control also allows semiautomatic growth of web over long periods which can greatly reduce costs.

Vacuum phonon tunneling.

PubMed

Altfeder, Igor; Voevodin, Andrey A; Roy, Ajit K

2010-10-15

Field-induced phonon tunneling, a previously unknown mechanism of interfacial thermal transport, has been revealed by ultrahigh vacuum inelastic scanning tunneling microscopy (STM). Using thermally broadened Fermi-Dirac distribution in the STM tip as in situ atomic-scale thermometer we found that thermal vibrations of the last tip atom are effectively transmitted to sample surface despite few angstroms wide vacuum gap. We show that phonon tunneling is driven by interfacial electric field and thermally vibrating image charges, and its rate is enhanced by surface electron-phonon interaction.

21 CFR 884.4340 - Fetal vacuum extractor.

Code of Federal Regulations, 2011 CFR

2011-04-01

... means of a suction cup attached to the scalp and is powered by an external vacuum source. This generic type of device may include the cup, hosing, vacuum source, and vacuum control. (b) Classification...

21 CFR 884.4340 - Fetal vacuum extractor.

Code of Federal Regulations, 2010 CFR

2010-04-01

... means of a suction cup attached to the scalp and is powered by an external vacuum source. This generic type of device may include the cup, hosing, vacuum source, and vacuum control. (b) Classification...

Dynamic melting of metals in the diamond cell: Clues for melt viscosity?

NASA Astrophysics Data System (ADS)

Boehler, R.; Karandikar, A.; Yang, L.

2011-12-01

From the observed decreasing mobility of liquid iron at high pressure in the laser-heated diamond cell and the gradual decrease in the shear modulus in shock experiments, one may derive high viscosity in the liquid outer core of the Earth. A possible explanation could be the presence of local structures in the liquid as has been observed for several transition metals. In order to bridge the large gap in the timescales between static and dynamic melting experiments, we have developed new experimental techniques to solve the large discrepancies in the melting curves of transition metals (Fe, W, Ta, Mo) measured statically in the laser-heated diamond cell and in shock experiments. The new methods employ "single-shot" laser heating in order to reduce problems associated with mechanical instabilities and chemical reactions of the samples subjected to several thousand degrees at megabar pressures. For melt detection, both synchrotron X-ray diffraction and Scanning Electron Microscopy (SEM) on recovered samples are used. A third approach is the measurement of latent heat effects associated with melting or freezing. This method employs simultaneous CW and pulse laser heating and monitoring the temperature-time history with fast photomultipliers. Using the SEM recovery method, we measured first melting temperatures of rhenium, which at high pressure may be one of the most refractory materials. From the melt textures of Re, we did not observe a significant pressure dependence of viscosity.

Understanding Melt-Memory of Commercial Polyolefins

NASA Astrophysics Data System (ADS)

Alamo, Rufina

Self-nucleation (SN) or controlling self-generated seeds in a polymer melt is an avenue to increase the rate of solidification of semicrystalline polymers of commercial relevance. Self-nuclei are remains in the melt of the segmental self-assembly to form polymer crystallites providing a path to enhance primary crystal nucleation. SN has been extensively studied in homopolymers such as iPP. Recently, a strong memory effect of crystallization has been observed in melts of random ethylene copolymers well above the equilibrium melting temperature. The melt memory is associated with clusters or seeds that remain in the melt from the copolymer's sequence length partitioning. Cooling from progressively lower self-seeded melt temperatures, ethylene copolymers with a broad inter-chain comonomer composition (1 - 15 mol%) display first the expected accelerated crystallization, followed by a decrease in the rate in a range of melt temperatures where narrow copolymers show a continuous acceleration of the rate. This unusual inversion of the crystallization rate was postulated to arise from the onset of liquid-liquid phase separation (LLPS) between comonomer-rich and comonomer-poor components of the broad copolymer. The UCST type phase diagram of these commercial copolymers has been documented via SANS using a blend of components, some deuterated, to reproduce the broad distribution. Furthermore, the components that contribute to LLPS have been identified by the crystallization behavior of molar mass fractions. The influence of long chain branching on the topology of copolymer melts has been analyzed using model 3-arm stars hydrogenated polybutadienes. The effect of melt viscosity on strength of melt memory is also evident when SN data of random ethylene copolymers are compared with those of propylene-ethylene copolymers. The strong dependence of melt viscosity on melt memory, and a critical threshold crystallinity level to observe the effect of melt memory on crystallization

Cooling and stabilization of graphene nanoplatelets in high vacuum

NASA Astrophysics Data System (ADS)

Nagornykh, Pavel

The study of 2D materials is a rapidly growing area of research, where the ability to isolate and probe an individual single-layer specimen is of high importance. The levitation approach serves as a natural solution for this problem and can be used in ways complementary to the standard techniques. Experiments, including study of properties at high or close to melting temperatures, stretching, folding, vibration and functionalization, can be conducted on levitated 2D materials. As a first step towards realization of all these ideas, one needs to develop and test a system allowing for control over the thermal state and orientation of mono-layer flakes. In this thesis, I present the results of implementation of the parametric feedback cooling scheme in a quadrupole ion trap for stabilization and cooling of graphene nanopletelets. I have tested and showed that the feedback allows to stabilize levitated graphene nanoplatelets in high vacuum conditions (<1 microTorr) to have trapped life times longer than a week. Cooling of the center of mass motion to temperatures below 20 K for all translational degrees of freedom was observed. I have also studied the coupling of DC patch potentials, which were found to be present in the high vacuum chamber. Their effect on cooling was studied and the protocol for minimizing the noise coupling created by the DC fields was designed. We have shown that by varying DC voltages on a set of auxiliary DC electrodes, placed near the trap, one can balance out the DC fields and achieve the lowest cooling temperature. The settings corresponding to this temperature were measured to have a slow drift in time. Ability to tune the settings to balance this drift without breaking the vacuum was studied and found to be a viable solution for the drift cancellation. In addition, our effort in characterization of the flakes is presented. It was shown that the flake discharge quantization observed during the initial pumping down of the high vacuum chamber

The influence of partial melting and melt migration on the rheology of the continental crust

NASA Astrophysics Data System (ADS)

Cavalcante, Geane Carolina G.; Viegas, Gustavo; Archanjo, Carlos José; da Silva, Marcos Egydio

2016-11-01

The presence of melt during deformation produces a drastic change in the rheological behavior of the continental crust; rock strength is decreased even for melt fractions as low as ∼7%. At pressure/temperature conditions typical of the middle to lower crust, melt-bearing systems may play a critical role in the process of strain localization and in the overall strength of the continental lithosphere. In this contribution we focus on the role and dynamics of melt flow in two different mid-crustal settings formed during the Brasiliano orogeny: (i) a large-scale anatectic layer in an orthogonal collision belt, represented by the Carlos Chagas anatexite in southeastern Brazil, and (ii) a strike-slip setting, in which the Espinho Branco anatexite in the Patos shear zone (northeast Brazil) serves as an analogue. Both settings, located in eastern Brazil, are part of the Neoproterozoic tectonics that resulted in widespread partial melting, shear zone development and the exhumation of middle to lower crustal layers. These layers consist of compositionally heterogeneous anatexites, with variable former melt fractions and leucosome structures. The leucosomes usually form thick interconnected networks of magma that reflect a high melt content (>30%) during deformation. From a comparison of previous work based on detailed petrostructural and AMS studies of the anatexites exposed in these areas, we discuss the rheological implications caused by the accumulation of a large volume of melt ;trapped; in mid-crustal levels, and by the efficient melt extraction along steep shear zones. Our analyses suggest that rocks undergoing partial melting along shear settings exhibit layers with contrasting competence, implying successive periods of weakening and strengthening. In contrast, regions where a large amount of magma accumulates lack clear evidence of competence contrast between layers, indicating that they experienced only one major stage of dramatic strength drop. This comparative

Cold cathode vacuum gauging system

DOEpatents

Denny, Edward C.

2004-03-09

A vacuum gauging system of the cold cathode type is provided for measuring the pressure of a plurality of separate vacuum systems, such as in a gas centrifuge cascade. Each casing is fitted with a gauge tube assembly which communicates with the vacuum system in the centrifuge casing. Each gauge tube contains an anode which may be in the form of a slender rod or wire hoop and a cathode which may be formed by the wall of the gauge tube. The tube is provided with an insulated high voltage connector to the anode which has a terminal for external connection outside the vacuum casing. The tube extends from the casing so that a portable magnet assembly may be inserted about the tube to provide a magnetic field in the area between the anode and cathode necessary for pressure measurements in a cold cathode-type vacuum gauge arrangement. The portable magnetic assembly is provided with a connector which engages the external high voltage terminal for providing power to the anode within in the gauge tube. Measurement is made in the same manner as the prior cold cathode gauges in that the current through the anode to the cathode is measured as an indication of the pressure. By providing the portable magnetic assembly, a considerable savings in cost, installation, and maintenance of vacuum gauges for pressure measurement in a gas centrifuge cascade is realizable.

Measurement of partial pressures in vacuum technology and vacuum physics

NASA Technical Reports Server (NTRS)

Huber, W. K.

1986-01-01

It is pointed out that the measurement of gaseous pressures of less than 0.0001 torr is based on the ionization of gas atoms and molecules due to collisions with electrons. The particle density is determined in place of the pressure. The ionization cross sections for molecules of various gases are discussed. It is found that the true pressure in a vacuum system cannot be determined with certainty if it is unknown which gas is present. Effects of partial pressure determination on the condition of the vacuum system are discussed together with ion sources, systems of separation, and ion detection.

VACUUM TRAP AND VALVE COMBINATION

DOEpatents

Milleron, N.; Levenson, L.

1963-02-19

This patent relates to a vacuum trap and valve combination suitable for use in large ultra-high vacuum systems. The vacuum trap is a chamber having an inlet and outlet opening which may be made to communicate with a chamber to be evacuated and a diffusion pump, respectively. A valve is designed to hermeticaliy seal with inlet opening and, when opened, block the line-of- sight'' between the inlet and outlet openings, while allowing a large flow path between the opened vaive and the side walls of the trap. The interior of the trap and the side of the valve facing the inlet opening are covered with an impurity absorbent, such as Zeolite or activated aluminum. Besides the advantage of combining two components of a vacuum system into one, the present invention removes the need for a baffle between the pump and the chamber to be evacuated. In one use of a specific embodiment of this invention, the transmission probability was 45 and the partial pressure of the pump fluid vapor in the vacuum chamber was at least 100 times lower than its vapor pressure. (AEC)

Partial Melting in the Inner Core

NASA Astrophysics Data System (ADS)

Hernlund, J. W.

2014-12-01

The inner core boundary (ICB) is often considered to be permeable to flow, because solid iron could melt as it upwells across the ICB. Such a mechanism has been proposed to accompany inner core convective processes (including translation from a freezing to melting hemisphere), and has also been invoked to explain the formation of a dense Fe-rich liquid F-layer above the ICB. However, the conceptions of ICB melting invoked thus far are extremely simplistic, and neglect the many lessons learned from melting in other geological contexts. Owing to some degree of solid solution in relatively incompatible light alloys in solid iron, the onset of melting in the inner core will likely occur as a partial melt, with the liquid being enriched in these light alloys relative to the co-existing solid. Such a partial melt is then subject to upward migration/percolation out of the solid matrix owing to the buoyancy of melt relative to solid. Removal of melt and viscous compaction of the pore space results in an iron-enriched dense solid, whose negative buoyancy will oppose whatever buoyancy forces initially gave rise to upwelling. Either the negative buoyancy will balance these other forces and cause upwelling to cease, or else the solid will become so depleted in light alloys that it is unable to undergo further melting. Thus a proper accounting of partial melting results in a very different melting regime in the inner core, and suppression of upwelling across the ICB. Any fluid that is able to escape into the outer core from inner core partial melting will likely be buoyant because in order to be a melt it should be enriched in incompatiable alloys relative to whatever is freezing at the ICB. Therefore inner core melting is unlikely to contribute to the formation of an F-layer, but instead will tend to de-stabilize it. I will present models that illustrate these processes, and propose that the F-layer is a relic of incomplete mixing of the core during Earth's final stages of

Human Mitochondrial Transcription Factor B2 Is Required for Promoter Melting during Initiation of Transcription.

PubMed

Posse, Viktor; Gustafsson, Claes M

2017-02-17

The mitochondrial transcription initiation machinery in humans consists of three proteins: the RNA polymerase (POLRMT) and two accessory factors, transcription factors A and B2 (TFAM and TFB2M, respectively). This machinery is required for the expression of mitochondrial DNA and the biogenesis of the oxidative phosphorylation system. Previous experiments suggested that TFB2M is required for promoter melting, but conclusive experimental proof for this effect has not been presented. Moreover, the role of TFB2M in promoter unwinding has not been discriminated from that of TFAM. Here we used potassium permanganate footprinting, DNase I footprinting, and in vitro transcription from the mitochondrial light-strand promoter to study the role of TFB2M in transcription initiation. We demonstrate that a complex composed of TFAM and POLRMT was readily formed at the promoter but alone was insufficient for promoter melting, which only occurred when TFB2M joined the complex. We also show that mismatch bubble templates could circumvent the requirement of TFB2M, but TFAM was still required for efficient initiation. Our findings support a model in which TFAM first recruits POLRMT to the promoter, followed by TFB2M binding and induction of promoter melting. © 2017 by The American Society for Biochemistry and Molecular Biology, Inc.

Melt segregation from partially molten source regions - The importance of melt density and source region size

NASA Technical Reports Server (NTRS)

Stolper, E.; Hager, B. H.; Walker, D.; Hays, J. F.

1981-01-01

An investigation is conducted regarding the changes expected in the density contrast between basic melts and peridotites with increasing pressure using the limited data available on the compressibilities of silicate melts and data on the densities of mantle minerals. It is concluded that since compressibilities of silicate melts are about an order of magnitude greater than those of mantle minerals, the density contrast between basic melts and mantle minerals must diminish significantly with increasing pressure. An earlier analysis regarding the migration of liquid in partially molten source regions conducted by Walker et al. (1978) is extended, giving particular attention to the influence of the diminished density contrast between melt and residual crystals with increasing source region depth and to the influence of source region size. This analysis leads to several generalizations concerning the factors influencing the depths at which magmas will segregate from their source regions and the degrees of partial melting that can be achieved in these source regions before melt segregation occurs.

Partial melting kinetics of plagioclase-diopside pairs

NASA Astrophysics Data System (ADS)

Tsuchiyama, Akira

1985-09-01

Partial melting experiments on plagioclase (An60) and diopside have been carried out using pairs of large crystals to investigate textures and kinetics of melting. The experiments were done at one atmosphere pressure as a function of temperature (1,190 1,307° C) and time (1.5 192 h). Melting took place mainly at the plagioclase-diopside contact planes. Reaction zones composed of fine mixtures of calcic plagioclase and melt were developed from the surface of the plagioclase crystal inward. There exists a critical temperature, below which only a few % melting can occur over the duration of the experiments. This sluggish melting is caused by slow NaSi-CaAl diffusion in plagioclase, because the plagioclase crystal must change its composition to produce albite-rich cotectic melts. Diffusion in the solid also affects the chemical composition of the melts. During initial melting, potassium is preferentially extracted from plagioclase because K-Na diffusion in plagioclase is faster than that of NaSi-CaAl. This also causes a shift in the cotectic compositions. Above the “critical temperature”, on the other hand, melting is promoted by a metastable reaction in which the plagioclase composition does not change, and which produces melts with compositional gradients along the original An60-diopside tie line. The critical temperature is determined by the intersection of the cotectic and the An60-diopside tie line. Interdiffusion coefficients of plagioclase-diopside components in the melt are estimated from melting rates above the critical temperature by using a simplified steady-state diffusion model (e.g., 10-8 cm2/sec at 1,300° C). Many examples of reaction zones due to partial melting have been described as spongy or fingerprint-like textures in xenoliths. Metastable melting above the critical temperature is considered to take place in natural melting where there is a high degree of melting. However, we cannot exclude the possibility of disequilibrium created by

Melt volume flow rate and melt flow rate of kenaf fibre reinforced Floreon/magnesium hydroxide biocomposites.

PubMed

Lee, C H; Sapuan, S M; Lee, J H; Hassan, M R

2016-01-01

A study of the melt volume flow rate (MVR) and the melt flow rate (MFR) of kenaf fibre (KF) reinforced Floreon (FLO) and magnesium hydroxide (MH) biocomposites under different temperatures (160-180 °C) and weight loadings (2.16, 5, 10 kg) is presented in this paper. FLO has the lowest values of MFR and MVR. The increment of the melt flow properties (MVR and MFR) has been found for KF or MH insertion due to the hydrolytic degradation of the polylactic acid in FLO. Deterioration of the entanglement density at high temperature, shear thinning and wall slip velocity were the possible causes for the higher melt flow properties. Increasing the KF loadings caused the higher melt flow properties while the higher MH contents created stronger bonding for higher macromolecular chain flow resistance, hence lower melt flow properties were recorded. However, the complicated melt flow behaviour of the KF reinforced FLO/MH biocomposites was found in this study. The high probability of KF-KF and KF-MH collisions was expected and there were more collisions for higher fibre and filler loading causing lower melt flow properties.

Promoted-Combustion Chamber with Induction Heating Coil

NASA Technical Reports Server (NTRS)

Richardson, Erin; Hagood, Richard; Lowery, Freida; Herald, Stephen

2006-01-01

An improved promoted-combustion system has been developed for studying the effects of elevated temperatures on the flammability of metals in pure oxygen. In prior promoted-combustion chambers, initial temperatures of metal specimens in experiments have been limited to the temperatures of gas supplies, usually near room temperature. Although limited elevated temperature promoted-combustion chambers have been developed using water-cooled induction coils for preheating specimens, these designs have been limited to low-pressure operation due to the hollow induction coil. In contrast, the improved promoted-combustion chamber can sustain a pressure up to 10 kpsi (69 MPa) and, through utilization of a solid induction coil, is capable of preheating a metal specimen up to its melting point [potentially in excess of 2,000 F (approximately equal to 1,100 C)]. Hence, the improved promoted combustion chamber makes a greater range of physical conditions and material properties accessible for experimentation. The chamber consists of a vertical cylindrical housing with an inner diameter of 8 in. (20.32 cm) and an inner height of 20.4 in. (51.81 cm). A threaded, sealing cover at one end of the housing can be unscrewed to gain access for installing a specimen. Inlet and outlet ports for gases are provided. Six openings arranged in a helical pattern in the chamber wall contain sealed sapphire windows for viewing an experiment in progress. The base of the chamber contains pressure-sealed electrical connectors for supplying power to the induction coil. The connectors feature a unique design that prevents induction heating of the housing and the pressure sealing surfaces; this is important because if such spurious induction heating were allowed to occur, chamber pressure could be lost. The induction coil is 10 in. (25.4 cm) long and is fitted with a specimen holder at its upper end. At its lower end, the induction coil is mounted on a ceramic base, which affords thermal insulation to

Vacuum enhanced cutaneous biopsy instrument

DOEpatents

Collins, Joseph

2000-01-01

A syringe-like disposable cutaneous biopsy instrument equipped with a tubular blade at its lower end, and designed so that a vacuum is created during use, said vacuum serving to retain undeformed a plug of tissue cut from a patient's skin.

Troubleshooting crude vacuum tower overhead ejector systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lines, J.R.; Frens, L.L.

1995-03-01

Routinely surveying tower overhead vacuum systems can improve performance and product quality. These vacuum systems normally provide reliable and consistent operation. However, process conditions, supplied utilities, corrosion, erosion and fouling all have an impact on ejector system performance. Refinery vacuum distillation towers use ejector systems to maintain tower top pressure and remove overhead gases. However, as with virtually all refinery equipment, performance may be affected by a number of variables. These variables may act independently or concurrently. It is important to understand basic operating principles of vacuum systems and how performance is affected by: utilities, corrosion and erosion, fouling, andmore » process conditions. Reputable vacuum-system suppliers have service engineers that will come to a refinery to survey the system and troubleshoot performance or offer suggestions for improvement. A skilled vacuum-system engineer may be needed to diagnose and remedy system problems. The affect of these variables on performance is discussed. A case history is described of a vacuum system on a crude tower in a South American refinery.« less

Melt migration modeling in partially molten upper mantle

NASA Astrophysics Data System (ADS)

Ghods, Abdolreza

The objective of this thesis is to investigate the importance of melt migration in shaping major characteristics of geological features associated with the partial melting of the upper mantle, such as sea-floor spreading, continental flood basalts and rifting. The partial melting produces permeable partially molten rocks and a buoyant low viscosity melt. Melt migrates through the partially molten rocks, and transfers mass and heat. Due to its much faster velocity and appreciable buoyancy, melt migration has the potential to modify dynamics of the upwelling partially molten plumes. I develop a 2-D, two-phase flow model and apply it to investigate effects of melt migration on the dynamics and melt generation of upwelling mantle plumes and focusing of melt migration beneath mid-ocean ridges. Melt migration changes distribution of the melt-retention buoyancy force and therefore affects the dynamics of the upwelling plume. This is investigated by modeling a plume with a constant initial melt of 10% where no further melting is considered. Melt migration polarizes melt-retention buoyancy force into high and low melt fraction regions at the top and bottom portions of the plume and therefore results in formation of a more slender and faster upwelling plume. Allowing the plume to melt as it ascends through the upper mantle also produces a slender and faster plume. It is shown that melt produced by decompressional melting of the plume migrates to the upper horizons of the plume, increases the upwelling velocity and thus, the volume of melt generated by the plume. Melt migration produces a plume which lacks the mushroom shape observed for the plume models without melt migration. Melt migration forms a high melt fraction layer beneath the sloping base of the impermeable oceanic lithosphere. Using realistic conditions of melting, freezing and melt extraction, I examine whether the high melt fraction layer is able to focus melt from a wide partial melting zone to a narrow region

Melting line of polymeric nitrogen

NASA Astrophysics Data System (ADS)

Yakub, L. N.

2013-05-01

We made an attempt to predict location of the melting line of polymeric nitrogen using two equations for Helmholtz free energy: proposed earlier for cubic gauche-structure and developed recently for liquid polymerized nitrogen. The P-T relation, orthobaric densities and latent heat of melting were determined using a standard double tangent construction. The estimated melting temperature decreases with increasing pressure, alike the temperature of molecular-nonmolecular transition in solid. We discuss the possibility of a triple point (solid-molecular fluid-polymeric fluid) at ˜80 GPa and observed maximum of melting temperature of nitrogen.

Oceanic slab melting and mantle metasomatism.

PubMed

Scaillet, B; Prouteau, G

2001-01-01

Modern plate tectonic brings down oceanic crust along subduction zones where it either dehydrates or melts. Those hydrous fluids or melts migrate into the overlying mantle wedge trigerring its melting which produces arc magmas and thus additional continental crust. Nowadays, melting seems to be restricted to cases of young (< 50 Ma) subducted plates. Slab melts are silicic and strongly sodic (trondhjemitic). They are produced at low temperatures (< 1000 degrees C) and under water excess conditions. Their interaction with mantle peridotite produces hydrous metasomatic phases such as amphibole and phlogopite that can be more or less sodium rich. Upon interaction the slab melt becomes less silicic (dacitic to andesitic), and Mg, Ni and Cr richer. Virtually all exposed slab melts display geochemical evidence of ingestion of mantle material. Modern slab melts are thus unlike Archean Trondhjemite-Tonalite-Granodiorite rocks (TTG), which suggests that both types of magmas were generated via different petrogenetic pathways which may imply an Archean tectonic model of crust production different from that of the present-day, subduction-related, one.

Welding wire selection critical to jet engine repair work

NASA Astrophysics Data System (ADS)

1992-11-01

A review is provided of issues related to the selection of welding wire for aircraft gas-turbine engines emphasizing the importance of cleanliness in the welding wire product. A three-step metallurgical control process is described for the production of welding wire that is clean and suitable for turbine repair. The process is based on: (1) vacuum induction melting; (2) contamination-free processing of the wire; and (3) environmentally controlled packaging. Weld work on aerospace casting is shown to be useful and suitable for many alloy and superalloy materials with various filler materials.

Vapor-barrier Vacuum Isolation System

NASA Technical Reports Server (NTRS)

Weinstein, Leonard M. (Inventor); Taminger, Karen M. (Inventor)

2014-01-01

A system includes a collimated beam source within a vacuum chamber, a condensable barrier gas, cooling material, a pump, and isolation chambers cooled by the cooling material to condense the barrier gas. Pressure levels of each isolation chamber are substantially greater than in the vacuum chamber. Coaxially-aligned orifices connect a working chamber, the isolation chambers, and the vacuum chamber. The pump evacuates uncondensed barrier gas. The barrier gas blocks entry of atmospheric vapor from the working chamber into the isolation chambers, and undergoes supersonic flow expansion upon entering each isolation chamber. A method includes connecting the isolation chambers to the vacuum chamber, directing vapor to a boundary with the working chamber, and supersonically expanding the vapor as it enters the isolation chambers via the orifices. The vapor condenses in each isolation chamber using the cooling material, and uncondensed vapor is pumped out of the isolation chambers via the pump.

Ice-Shelf Melting Around Antarctica

NASA Astrophysics Data System (ADS)

Rignot, E.; Jacobs, S.; Mouginot, J.; Scheuchl, B.

2013-07-01

We compare the volume flux divergence of Antarctic ice shelves in 2007 and 2008 with 1979 to 2010 surface accumulation and 2003 to 2008 thinning to determine their rates of melting and mass balance. Basal melt of 1325 ± 235 gigatons per year (Gt/year) exceeds a calving flux of 1089 ± 139 Gt/year, making ice-shelf melting the largest ablation process in Antarctica. The giant cold-cavity Ross, Filchner, and Ronne ice shelves covering two-thirds of the total ice-shelf area account for only 15% of net melting. Half of the meltwater comes from 10 small, warm-cavity Southeast Pacific ice shelves occupying 8% of the area. A similar high melt/area ratio is found for six East Antarctic ice shelves, implying undocumented strong ocean thermal forcing on their deep grounding lines.

7 CFR 58.423 - Cheese vacuumizing chamber.

Code of Federal Regulations, 2010 CFR

2010-01-01

... 7 Agriculture 3 2010-01-01 2010-01-01 false Cheese vacuumizing chamber. 58.423 Section 58.423 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards....423 Cheese vacuumizing chamber. The vacuum chamber shall be satisfactorily constructed and maintained...

7 CFR 58.423 - Cheese vacuumizing chamber.

Code of Federal Regulations, 2011 CFR

2011-01-01

... 7 Agriculture 3 2011-01-01 2011-01-01 false Cheese vacuumizing chamber. 58.423 Section 58.423 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards....423 Cheese vacuumizing chamber. The vacuum chamber shall be satisfactorily constructed and maintained...

Critical porosity of melt segregation during crustal melting: Constraints from zonation of peritectic garnets in a dacite volcano

NASA Astrophysics Data System (ADS)

Yu, Xun; Lee, Cin-Ty A.

2016-09-01

The presence of leucogranitic dikes in orogenic belts suggests that partial melting may be an important process in the lower crust of active orogenies. Low seismic velocity and low electrical resistivity zones have been observed in the lower crust of active mountain belts and have been argued to reflect the presence of partial melt in the deep crust, but volcanoes are rare or absent above many of these inferred melt zones. Understanding whether these low velocity zones are melt-bearing, and if so, why they do not commonly erupt, is essential for understanding the thermal and rheologic structure of the crust and its dynamic evolution. Central to this problem is an understanding of how much melt can be stored before it can escape from the crust via compaction and eventually erupt. Experimental and theoretical studies predict trapped melt fractions anywhere from <5% to >30%. Here, we examine Mn growth-zoning in peritectic garnets in a Miocene dacite volcano from the ongoing Betic-Rif orogeny in southern Spain to estimate the melt fraction at the time of large-scale melt extraction that subsequently led to eruption. We show that the melt fraction at segregation, corresponding approximately to the critical melt porosity, was ∼30%, implying significant amounts of melt can be stored in the lower crust without draining or erupting. However, seismic velocities in the lower crust beneath active orogenic belts (southern Spain and Tibet) as well as beneath active magmatic zones (e.g., Yellowstone hotspot) correspond to average melt porosities of <10%, suggesting that melt porosities approaching critical values are short-lived or that high melt porosity regions are localized into heterogeneously distributed sills or dikes, which individually cannot be resolved by seismic studies.

Induction technique in manufacturing preforms

NASA Astrophysics Data System (ADS)

Frauenhofer, M.; Ströhlein, T.; Fabig, S.; Böhm, S.; Herbeck, L.; Dilger, K.

2008-09-01

The prepreg technology is a state-of-the-art method to produce high-performance CFRP parts. Due to the high material prices, the restricted process rate, and limitations to the component complexity, in future, more and more parts will be assembled by using liquid composite moulding. Especially in the case of series larger than 100 parts per year, the LCM technology offers the best cost-effectiveness. This technology is based on resin injection into dry multilayer fibre textiles (preforms). The Institute of Joining and Welding (TU, Braunschweig), together with the Institute of Composite Structures and Adaptive Systems (DLR), has elaborated a new technology to speed up the preform process, which is the most labour-intensive step within the LCM process chain. A novel concept to consolidate binder-coated fabrics is under development. By applying the high energy transfer rate of induction technology, it is possible to heat up a preform with rates up to 50 K/s to melt the binder and consolidate the preform.

Lithospheric processes that enhance melting at rifts

NASA Astrophysics Data System (ADS)

Elkins-Tanton, L. T.; Furman, T.

2008-12-01

Continental rifts are commonly sites for mantle melting, whether in the form of ridge melting to create new oceanic crust, or as the locus of flood basalt activity, or in the long initial period of rifting before lavas evolve fully into MORBs. The high topography in the lithosphere-asthenosphere boundary under a rift creates mantle upwelling and adiabatic melting even in the absence of a plume. This geometry itself, however, is conducive to lithospheric instability on the sides of the rifts. Unstable lithosphere may founder into the mantle, producing more complex aesthenospheric convective patterns and additional opportunities to produce melt. Lithospheric instabilities can produce additional adiabatic melting in convection produced as they sink, and they may also devolatilize as they sink, introducing the possibility of flux melting to the rift environment. We call this process upside-down melting, since devolatilization and melting proceed as the foundering lithosphere sinks, rather than while rising, as in the more familiar adiabatic decompression melting. Both adiabatic melting and flux melting would take place along the edges of the rift and may even move magmatism outside the rift, as has been seen in Ethiopia. In volcanism postdating the flood basalts on and adjacent to the Ethiopian Plateau there is evidence for both lithospheric thinning and volatile enrichment in the magmas, potentially consistent with the upside-down melting model. Here we present a physical model for the conjunction of adiabatic decompression melting to produce new oceanic crust in the rift, while lithospheric gravitational instabilities drive both adiabatic and flux melting at its margins.

Engineering Matter Interactions Using Squeezed Vacuum

NASA Astrophysics Data System (ADS)

Zeytinoǧlu, Sina; Imamoǧlu, Ataç; Huber, Sebastian

2017-04-01

Virtually all interactions that are relevant for atomic and condensed matter physics are mediated by quantum fluctuations of the electromagnetic field vacuum. Consequently, controlling the vacuum fluctuations can be used to engineer the strength and the range of interactions. Recent experiments have used this premise to demonstrate novel quantum phases or entangling gates by embedding electric dipoles in photonic cavities or wave guides, which modify the electromagnetic fluctuations. Here, we show theoretically that the enhanced fluctuations in the antisqueezed quadrature of a squeezed vacuum state allow for engineering interactions between electric dipoles without the need for a photonic structure. Thus, the strength and range of the interactions can be engineered in a time-dependent way by changing the spatial profile of the squeezed vacuum in a traveling-wave geometry, which also allows the implementation of chiral dissipative interactions. Using experimentally realized squeezing parameters and including realistic losses, we predict single-atom cooperativities C of up to 10 for the squeezed-vacuum-enhanced interactions.

Partitioning of Mg, Ca, and Na between carbonatite melt and hydrous fluid at 0.1-0.2 GPa

NASA Astrophysics Data System (ADS)

Veksler, Ilya V.; Keppler, Hans

Experimental studies of the element distribution between carbonatite melts and hydrous fluids are hampered by the fact that neither the fluid nor the melt can be isochemically quenched in conventional high-pressure vessels. In order to overcome this problem, we used a double-capsule technique to separate immiscible fluid and melt phases during and after the runs. The inner platinum capsules were charged with carbonate mixtures (CaCO3, MgCO3 and Na2CO3) and placed inside the outer capsules charged with distilled water and diamond powder. The latter was used as an inert trap for solids precipitating from the fluid on quenching. Carbonate melt and hydrous fluid equilibrated through a small hole left in the upper end of the inner capsule. The runs were performed in rapid-quench cold-seal pressure vessels at 0.1-0.2 GPa and 700-900°C in the two-phase (fluid+melt) stability region. Both quenched melt and quenched fluid were dissolved in dilute HCl and analysed by inductively coupled plasma atomic emission spectroscopy. The results show that under all conditions investigated, fluid/melt partition coefficients for Ca and Mg are similar and several times smaller than those for Na. At 0.1 GPa and a water/carbonatite ratio of 1 (by weight), the partition coefficients are DNa= 0.35+/- 0.02, DCa=0.09+/-0.02, and DMg=0.13+/- 0.01. Between 700 and 900°C, the effect of temperature on partitioning is negligible. However, DNa increases significantly with decreasing water/carbonatite ratio in the system. Our data show that the release of a hydrous fluid enriched in sodium and simultaneous crystallisation of calcite can transform an alkaline, vapour-saturated carbonatite melt into a body of pure calcite surrounded by zones of sodium metasomatism. Thus, it is quite possible that carbonate magmas with substantial amounts of alkalies were common parental liquids of plutonic carbonatites.

Lightweight Vacuum Jacket for Cryogenic Insulation. Volume 1

NASA Technical Reports Server (NTRS)

Barclay, D. L.; Bell, J. E.; Brogren, E. W.; Straayer, J. W.

1975-01-01

The feasibility of producing a lightweight vacuum jacket using state-of-the-art technology and materials was examined. Design and analytical studies were made on a full-scale, orbital maneuvering system fuel tank. Preliminary design details were made for the tank assembly, including an optimized vacuum jacket and multilayer insulation system. A half-scale LH2 test model was designed and fabricated, and a force/stiffness proof test was conducted on the vacuum jacket. A vacuum leak rate of .000001 atmosphere ml of helium per second was measured, approximately 1500 hours of vacuum pressure were sustained, and 29 vacuum-pressure cycles were experienced prior to failure.

Dissolution Mechanism for High Melting Point Transition Elements in Aluminum Melt

NASA Astrophysics Data System (ADS)

Lee, Young E.; Houser, Stephen L.

When added cold in aluminum melt, the alloying process for compacts of transition metal elements such as Mn, Fe, Cr, Ni, Ti, Cu, and Zn takes a sequence of incubation, exothermic reactions to form intermetallic compounds, and dispersion of the alloying elements into aluminum melt. The experiments with Cr compacts show that the incubation period is affected by the content of ingredient Al and size of compacts and by size of Cr particles. Incubation period becomes longer as the content of ingredient aluminum in compact decreases, and this prolonged incubation period negatively impacts the dissolution of the alloying elements in aluminum. Once liquid aluminum forms at reaction sites, the exothermic reaction takes place quickly and significantly raises the temperature of the compacts. As the result of it, the compacts swell in volume with a sponge like structure. Such porous structure encourages the penetration of liquid aluminum from the melt. The compacts become weak mechanically, and the alloying elements are dispersed and entrained in aluminum melt as discrete and small sized units. When Cr compacts are deficient in aluminum, the unreacted Cr particles are encased by the intermetallic compounds in the dispersed particles. They are carried in the melt flow and continue the dissolution reaction in aluminum. The entire dissolution process of Cr compacts completes within 10 to 15 minutes with a full recovery when the aluminum content is 10 to 20% in compacts.

Induction of stromule formation by extracellular sucrose and glucose in epidermal leaf tissue of Arabidopsis thaliana

PubMed Central

2011-01-01

Background Stromules are dynamic tubular structures emerging from the surface of plastids that are filled with stroma. Despite considerable progress in understanding the importance of certain cytoskeleton elements and motor proteins for stromule maintenance, their function within the plant cell is still unknown. It has been suggested that stromules facilitate the exchange of metabolites and/or signals between plastids and other cell compartments by increasing the cytosolically exposed plastid surface area but experimental evidence for the involvement of stromules in metabolic processes is not available. The frequent occurrence of stromules in both sink tissues and heterotrophic cell cultures suggests that the presence of carbohydrates in the extracellular space is a possible trigger of stromule formation. We have examined this hypothesis with induction experiments using the upper epidermis from rosette leaves of Arabidopsis thaliana as a model system. Results We found that the stromule frequency rises significantly if either sucrose or glucose is applied to the apoplast by vacuum infiltration. In contrast, neither fructose nor sorbitol or mannitol are capable of inducing stromule formation which rules out the hypothesis that stromule induction is merely the result of changes in the osmotic conditions. Stromule formation depends on translational activity in the cytosol, whereas protein synthesis within the plastids is not required. Lastly, stromule induction is not restricted to the plastids of the upper epidermis but is similarly observed also with chloroplasts of the palisade parenchyma. Conclusions The establishment of an experimental system allowing the reproducible induction of stromules by vacuum infiltration of leaf tissue provides a suitable tool for the systematic analysis of conditions and requirements leading to the formation of these dynamic organelle structures. The applicability of the approach is demonstrated here by analyzing the influence of

7 CFR 305.29 - Vacuum heat treatment schedule.

Code of Federal Regulations, 2010 CFR

2010-01-01

... 7 Agriculture 5 2010-01-01 2010-01-01 false Vacuum heat treatment schedule. 305.29 Section 305.29... SERVICE, DEPARTMENT OF AGRICULTURE PHYTOSANITARY TREATMENTS Heat Treatments § 305.29 Vacuum heat treatment... vacuum at 8 hours. Maintain the vacuum until the end of the treatment. Gradually increase the temperature...

[The evolution of vacuum extraction in obstetrics].

PubMed

Nikolov, A

2010-01-01

Vacuum extraction is one of the methods for assisted vaginal delivery. In this article the evolution of vacuum extraction in obstetrics is been discussed. Historical facts and data from the invention up to state-of-the-art vacuum systems in modern obstetrics are presented.

Evaluation of a Prototype Hybrid Vacuum Pump to Provide Vacuum-Assisted Suspension for Above-Knee Prostheses

PubMed Central

Major, Matthew J.; Caldwell, Ryan; Fatone, Stefania

2015-01-01

Vacuum-assisted suspension (VAS) of prosthetic sockets utilizes a pump to evacuate air from between the prosthetic liner and socket, and are available as mechanical or electric systems. This technical note describes a hybrid pump that benefits from the advantages of mechanical and electric systems, and evaluates a prototype as proof-of-concept. Cyclical bench testing of the hybrid pump mechanical system was performed using a materials testing system to assess the relationship between compression cycles and vacuum pressure. Phase 1 in vivo testing of the hybrid pump was performed by an able-bodied individual using prosthesis simulator boots walking on a treadmill, and phase 2 involved an above-knee prosthesis user walking with the hybrid pump and a commercial electric pump for comparison. Bench testing of 300 compression cycles produced a maximum vacuum of 24 in-Hg. In vivo testing demonstrated that the hybrid pump continued to pull vacuum during walking, and as opposed to the commercial electric pump, did not require reactivation of the electric system during phase 2 testing. The novelty of the hybrid pump is that while the electric system provides rapid, initial vacuum suspension, the mechanical system provides continuous air evacuation while walking to maintain suspension without reactivation of the electric system, thereby allowing battery power to be reserved for monitoring vacuum levels. PMID:27462383

The Gao-Guenie impact melt breccia—Sampling a rapidly cooled impact melt dike on an H chondrite asteroid?

NASA Astrophysics Data System (ADS)

Schmieder, Martin; Kring, David A.; Swindle, Timothy D.; Bond, Jade C.; Moore, Carleton B.

2016-06-01

The Gao-Guenie H5 chondrite that fell on Burkina Faso (March 1960) has portions that were impact-melted on an H chondrite asteroid at ~300 Ma and, through later impact events in space, sent into an Earth-crossing orbit. This article presents a petrographic and electron microprobe analysis of a representative sample of the Gao-Guenie impact melt breccia consisting of a chondritic clast domain, quenched melt in contact with chondritic clasts, and an igneous-textured impact melt domain. Olivine is predominantly Fo80-82. The clast domain contains low-Ca pyroxene. Impact melt-grown pyroxene is commonly zoned from low-Ca pyroxene in cores to pigeonite and augite in rims. Metal-troilite orbs in the impact melt domain measure up to ~2 mm across. The cores of metal orbs in the impact melt domain contain ~7.9 wt% of Ni and are typically surrounded by taenite and Ni-rich troilite. The metallography of metal-troilite droplets suggest a stage I cooling rate of order 10 °C s-1 for the superheated impact melt. The subsolidus stage II cooling rate for the impact melt breccia could not be determined directly, but was presumably fast. An analogy between the Ni rim gradients in metal of the Gao-Guenie impact melt breccia and the impact-melted H6 chondrite Orvinio suggests similar cooling rates, probably on the order of ~5000-40,000 °C yr-1. A simple model of conductive heat transfer shows that the Gao-Guenie impact melt breccia may have formed in a melt injection dike ~0.5-5 m in width, generated during a sizeable impact event on the H chondrite parent asteroid.

Ice-shelf melting around Antarctica

NASA Astrophysics Data System (ADS)

Rignot, E.; Jacobs, S.

2008-12-01

The traditional view on the mass balance of Antarctic ice shelves is that they loose mass principally from iceberg calving with bottom melting a much lower contributing factor. Because ice shelves are now known to play a fundamental role in ice sheet evolution, it is important to re-evaluate their wastage processes from a circumpolar perspective using a combination of remote sensing techniques. We present area average rates deduced from grounding line discharge, snow accumulation, firn depth correction and ice shelf topography. We find that ice shelf melting accounts for roughly half of ice-shelf ablation, with a total melt water production of 1027 Gt/yr. The attrition fraction due to in-situ melting varies from 9 to 90 percent around Antarctica. High melt producers include the Ronne, Ross, Getz, Totten, Amery, George VI, Pine Island, Abbot, Dotson/Crosson, Shackleton, Thwaites and Moscow University Ice Shelves. Low producers include the Larsen C, Princess Astrid and Ragnhild coast, Fimbul, Brunt and Filchner. Correlation between melt water production and grounding line discharge is low (R2 = 0.65). Correlation with thermal ocean forcing from the ocean are highest in the northern parts of West Antarctica where regressions yield R2 of 0.93-0.97. Melt rates in the Amundsen Sea exhibit a quadratic sensitivity to thermal ocean forcing. We conclude that ice shelf melting plays a dominant role in ice shelf mass balance, with a potential to change rapidly in response to altered ocean heat transport onto the Antarctic continental shelf.

Gravitational collapse and the vacuum energy

NASA Astrophysics Data System (ADS)

Campos, M.

2014-03-01

To explain the accelerated expansion of the universe, models with interacting dark components (dark energy and dark matter) have been considered recently in the literature. Generally, the dark energy component is physically interpreted as the vacuum energy of the all fields that fill the universe. As the other side of the same coin, the influence of the vacuum energy on the gravitational collapse is of great interest. We study such collapse adopting different parameterizations for the evolution of the vacuum energy. We discuss the homogeneous collapsing star fluid, that interacts with a vacuum energy component, using the stiff matter case as example. We conclude this work with a discussion of the Cahill-McVittie mass for the collapsed object.

Gravitational baryogenesis in running vacuum models

NASA Astrophysics Data System (ADS)

Oikonomou, V. K.; Pan, Supriya; Nunes, Rafael C.

2017-08-01

We study the gravitational baryogenesis mechanism for generating baryon asymmetry in the context of running vacuum models. Regardless of whether these models can produce a viable cosmological evolution, we demonstrate that they produce a nonzero baryon-to-entropy ratio even if the universe is filled with conformal matter. This is a sound difference between the running vacuum gravitational baryogenesis and the Einstein-Hilbert one, since in the latter case, the predicted baryon-to-entropy ratio is zero. We consider two well known and most used running vacuum models and show that the resulting baryon-to-entropy ratio is compatible with the observational data. Moreover, we also show that the mechanism of gravitational baryogenesis may constrain the running vacuum models.

Melting in super-earths.

PubMed

Stixrude, Lars

2014-04-28

We examine the possible extent of melting in rock-iron super-earths, focusing on those in the habitable zone. We consider the energetics of accretion and core formation, the timescale of cooling and its dependence on viscosity and partial melting, thermal regulation via the temperature dependence of viscosity, and the melting curves of rock and iron components at the ultra-high pressures characteristic of super-earths. We find that the efficiency of kinetic energy deposition during accretion increases with planetary mass; considering the likely role of giant impacts and core formation, we find that super-earths probably complete their accretionary phase in an entirely molten state. Considerations of thermal regulation lead us to propose model temperature profiles of super-earths that are controlled by silicate melting. We estimate melting curves of iron and rock components up to the extreme pressures characteristic of super-earth interiors based on existing experimental and ab initio results and scaling laws. We construct super-earth thermal models by solving the equations of mass conservation and hydrostatic equilibrium, together with equations of state of rock and iron components. We set the potential temperature at the core-mantle boundary and at the surface to the local silicate melting temperature. We find that ancient (∼4 Gyr) super-earths may be partially molten at the top and bottom of their mantles, and that mantle convection is sufficiently vigorous to sustain dynamo action over the whole range of super-earth masses.

Preliminary results of sulfide melt/silicate wetting experiments in a partially melted ordinary chondrite

NASA Technical Reports Server (NTRS)

Jurewicz, Stephen R.; Jones, John H.

1994-01-01

Recently, mechanisms for core formation in planetary bodies have received considerable attention. Most current theories emphasize the need for large degrees of silicate partial melting to facilitate the coalescence and sinking of sulfide-metal liquid blebs through a low strength semi-crystalline silicate mush. This scenario is based upon observations that sulfide-metal liquid tends to form circular blebs in partially molten meteorites during laboratory experiments. However, recent experimental work by Herpfer and Larimer indicates that some sulfide-Fe liquids have wetting angles at and slightly below 60 deg in an olivine aggregate, implying an interconnected melt structure at any melt fraction. Such melt interconnectivity provides a means for gravitational compaction and extraction of the majority of a sulfide liquid phase in small planetary bodies without invoking large degrees of silicate partial melting. Because of the important ramifications of these results, we conducted a series of experiments using H-chondrite starting material in order to evaluate sulfide-liquid/silicate wetting behavior in a more complex natural system.

High-pressure melting of molybdenum.

PubMed

Belonoshko, A B; Simak, S I; Kochetov, A E; Johansson, B; Burakovsky, L; Preston, D L

2004-05-14

The melting curve of the body-centered cubic (bcc) phase of Mo has been determined for a wide pressure range using both direct ab initio molecular dynamics simulations of melting as well as a phenomenological theory of melting. These two methods show very good agreement. The simulations are based on density functional theory within the generalized gradient approximation. Our calculated equation of state of bcc Mo is in excellent agreement with experimental data. However, our melting curve is substantially higher than the one determined in diamond anvil cell experiments up to a pressure of 100 GPa. An explanation is suggested for this discrepancy.

Diffraction-limited storage-ring vacuum technology

PubMed Central

Al-Dmour, Eshraq; Ahlback, Jonny; Einfeld, Dieter; Tavares, Pedro Fernandes; Grabski, Marek

2014-01-01

Some of the characteristics of recent ultralow-emittance storage-ring designs and possibly future diffraction-limited storage rings are a compact lattice combined with small magnet apertures. Such requirements present a challenge for the design and performance of the vacuum system. The vacuum system should provide the required vacuum pressure for machine operation and be able to handle the heat load from synchrotron radiation. Small magnet apertures result in the conductance of the chamber being low, and lumped pumps are ineffective. One way to provide the required vacuum level is by distributed pumping, which can be realised by the use of a non-evaporable getter (NEG) coating of the chamber walls. It may not be possible to use crotch absorbers to absorb the heat from the synchrotron radiation because an antechamber is difficult to realise with such a compact lattice. To solve this, the chamber walls can work as distributed absorbers if they are made of a material with good thermal conductivity, and distributed cooling is used at the location where the synchrotron radiation hits the wall. The vacuum system of the 3 GeV storage ring of MAX IV is used as an example of possible solutions for vacuum technologies for diffraction-limited storage rings. PMID:25177979

Electric Propulsion Laboratory Vacuum Chamber

NASA Image and Video Library

1964-06-21

Engineer Paul Reader and his colleagues take environmental measurements during testing of a 20-inch diameter ion engine in a vacuum tank at the Electric Propulsion Laboratory (EPL). Researchers at the Lewis Research Center were investigating the use of a permanent-magnet circuit to create the magnetic field required power electron bombardment ion engines. Typical ion engines use a solenoid coil to create this magnetic field. It was thought that the substitution of a permanent magnet would create a comparable magnetic field with a lower weight. Testing of the magnet system in the EPL vacuum tanks revealed no significant operational problems. Reader found the weight of the two systems was similar, but that the thruster’s efficiency increased with the magnet. The EPL contained a series of large vacuum tanks that could be used to simulate conditions in space. Large vacuum pumps reduced the internal air pressure, and a refrigeration system created the cryogenic temperatures found in space.

High-Voltage Characterization for the Prototype Induction Cells

NASA Astrophysics Data System (ADS)

Huacen, Wang; Kaizhi, Zhang; Long, Wen; Qinggui, Lai; Linwen, Zhang; Jianjun, Deng

2002-12-01

Two linear induction prototype cells expected to work at 250kV, 3kA,with accelerating voltage flattop (±1%) ⩾ 70ns, have been tested to determine their high-voltage characteristics. Each cell is composed of a ferrite core immersed in oil, a gap with curved stainless steel electrodes, a solenoid magnet, and a insulator. The experiments were carried out with full-scale cells. The high voltage pulses were applied to two cells using a 100ns, 12Ω pulse Blumlein. The tests were performed at various high-voltage levels ranging from -250kV to -350kV. No breakdown was observed during the test at vacuum level (7-10) ṡ10-4 Pa. The cell schematic, the experimental set up, and the measured voltage waveforms are presented in this paper.

Impact melting early in lunar history

NASA Technical Reports Server (NTRS)

Lange, M. A.; Ahrens, T. J.

1979-01-01

The total amount of impact melt produced during early lunar history is examined in light of theoretically and experimentally determined relations between crater diameter (D) and impact melt volume. The time dependence of the melt production is given by the time dependent impact rate as derived from cratering statistics for two different crater-size classes. Results show that small scale cratering (D less than or equal to 30 km) leads to melt volumes which fit selected observations specifying the amount of impact melt contained in the lunar regolith and in craters with diameters less than 10 km. Larger craters (D greater than 30 km) are capable of forming the abundant impact melt breccias found on the lunar surface. The group of large craters (D greater than 30 km) produces nearly 10 times as much impact melt as all the smaller craters, and thus, the large impacts dominate the modification of the lunar surface. A contradiction between the distribution of radiometric rock ages and a model of exponentially decreasing cratering rate going back to 4.5 b.y. is reflected in uncertainty in the distribution of impact melt as a function of time on the moon.

Vacuum brazing of 316L stainless steel based on additively manufactured and conventional material grades

NASA Astrophysics Data System (ADS)

Tillmann, W.; Henning, T.; Wojarski, L.

2018-06-01

Many industrial applications require components with an increasing geometric complexity and specific material properties. Furthermore, the production costs and the affordable production time have to be minimized in order to ensure competitiveness. These divergent objectives are difficult to achieve with a single manufacturing technology. Therefore, joining of selective laser melted (SLM) complex shaped parts to conventionally produced high-volume components provides a high potential. The current investigation focuses on vacuum brazing conventionally manufactured to non-hipped SLM generated AISI 316L stainless steel. Cylindrical samples (Ø 14 mm) were brazed using a B-Ni2 foil (50 µm) at 1050 °C for 30 minutes in vacuum (< 4.5·10-5 mbar) and directly cooled down to room temperature with 4 bar overpressure to prevent the formation of chromium carbides within the base material. It could be proven that the brazing quality is extremely sensitive to even marginal porosities (< 0.2 %) and/or oxide inclusions of the SLM microstructure. Therefore, the fracture mirror in SLM/conventional steel brazements was at the joint braze/SLM steel interface, leading to a joint strength of 317.4 MPa. This corresponds to only 67.4 % of the joint strength obtained with conventional steel, where the fracture propagated through the diffusion area.

Melting ice

NASA Astrophysics Data System (ADS)

Benedetto, Elmo

2018-01-01

In this brief frontline, we want to describe the well-known fact that, when freshwater ice melts, the freshwater liquid level does not change. In the Italian Ministerial programs, fluid statics is introduced in the three years of middle school (students of 11-13 years) and during the first two years of high school (14-15 years). The Italian textbooks do not clearly explain why the abovementioned phenomenon occurs. The explanations are qualitative and they may lead to misinterpretation. I have noted that the students are very curious about this phenomenon. They sought a demonstration from books and from the web; and when they do not find it they asked me. Moreover, they have allowed me to observe that there are contradictory statements about the melting of icebergs. Some authors claim that they would not raise the sea-level, others say the opposite. Honestly speaking, I had never thought about this phenomenon and in classroom I tried to give them proof, expressing my opinion about the melting of icebergs.

Melting behavior of nanometer sized gold isomers

NASA Astrophysics Data System (ADS)

Liu, H. B.; Ascencio, J. A.; Perez-Alvarez, M.; Yacaman, M. J.

2001-09-01

In the present work, the melting behavior of nanometer sized gold isomers was studied using a tight-binding potential with a second momentum approximation. The cases of cuboctahedra, icosahedra, Bagley decahedra, Marks decahedra and star-like decahedra were considered. We calculated the temperature dependence of the total energy and volume during melting and the melting point for different types and sizes of clusters. In addition, the structural evolutions of the nanosized clusters during the melting transition were monitored and revealed. It is found that the melting process has three characteristic time periods for the intermediate nanosized clusters. The whole process includes surface disordering and reordering, followed by surface melting and a final rapid overall melting. This is a new observation, which it is in contrast with previous reports where surface melting is the dominant step.

Toroid Joining Gun. [thermoplastic welding system using induction heating

NASA Technical Reports Server (NTRS)

Buckley, J. D.; Fox, R. L.; Swaim, R J.

1985-01-01

The Toroid Joining Gun is a low cost, self-contained, portable low powered (100-400 watts) thermoplastic welding system developed at Langley Research Center for joining plastic and composite parts using an induction heating technique. The device developed for use in the fabrication of large space sructures (LSST Program) can be used in any atmosphere or in a vacuum. Components can be joined in situ, whether on earth or on a space platform. The expanded application of this welding gun is in the joining of thermoplastic composites, thermosetting composites, metals, and combinations of these materials. Its low-power requirements, light weight, rapid response, low cost, portability, and effective joining make it a candidate for solving many varied and unique bonding tasks.

Trace element control in binary Ni-25Cr and ternary Ni-30Co-30Cr master alloy castings

DOE Office of Scientific and Technical Information (OSTI.GOV)

Detrois, Martin; Jablonski, Paul D.

Electro-slag remelting (ESR) is used for control of unwanted elements in commercial alloys. This study focuses on master alloys of Ni-25Cr and Ni-30Co-30Cr, processed through a combination of vacuum induction melting (VIM) and electro-slag remelting (ESR). Minor additions were made to control tramp element levels and modify the melting characteristics. Nitrogen and sulfur levels below 10 ppm and oxygen levels below 100 ppm were obtained in the final products. The role of the alloy additions in lowering the tramp element content, the resulting residual inclusions and the melting characteristics were determined computationally and confirmed experimentally. Additions of titanium were beneficialmore » to the control of oxygen levels during VIM and nitrogen levels during ESR. Aluminum additions helped to control oxygen levels during remelting, however, aluminum pickup occurred when excess titanium was present during ESR. The usefulness of these master alloys for use as experimental remelt stock will also be discussed.« less

A Reevaluation of Impact Melt Production

NASA Astrophysics Data System (ADS)

Pierazzo, E.; Vickery, A. M.; Melosh, H. J.

1997-06-01

The production of melt and vapor is an important process in impact cratering events. Because significant melting and vaporization do not occur in impacts at velocities currently achievable in the laboratory, a detailed study of the production of melt and vapor in planetary impact events is carried out with hydrocode simulations. Sandia's two-dimensional axisymmetric hydrocode CSQ was used to estimate the amount of melt and vapor produced for widely varying initial conditions: 10 to 80 km/sec for impact velocity, 0.2 to 10 km for the projectile radius. Runs with different materials demonstrate the material dependency of the final result. These results should apply to any size projectile (for given impact velocity and material), since the results can be dynamically scaled so long as gravity is unimportant in affecting the early-time flow. In contrast with the assumptions of previous analytical models, a clear difference in shape, impact-size dependence, and depth of burial has been found between the melt regions and the isobaric core. In particular, the depth of the isobaric core is not a good representation of the depth of the melt regions, which form deeper in the target. While near-surface effects cause the computed melt region shapes to look like “squashed spheres” the spherical shape is still a good analytical analog. One of the goals of melt production studies is to find proper scaling laws to infer melt production for any impact event of interest. We tested the point source limit scaling law for melt volumes (μ = 0.55-0.6) proposed by M. D. Bjorkman and K. A. Holsapple (1987,Int. J. Impact Eng.5, 155-163). Our results indicate that the point source limit concept does not apply to melt and vapor production. Rather, melt and vapor production follows an energy scaling law (μ = 0.67), in good agreement with previous results of T. J. Ahrens and J. D. O'Keefe [1977, inImpact and Explosion Cratering(D. J. Roddy, R. O. Pepin, and R. B. Merrill, Eds.), pp. 639

Do Melt Inclusions Answer Big Questions?

NASA Astrophysics Data System (ADS)

Hofmann, A. W.; Sobolev, A. V.

2009-12-01

In a pioneering paper, Sobolev and Shimizu (1993) demonstrated the existence of ultra-depleted melt inclusions in olivine phenocrysts in MORB. They interpreted these as evidence for the preservation of parental melts formed by progressive near-fractional melting. Subsequently many cases have been described where melt inclusions from single basalt samples display enormous chemical and isotopic heterogeneity. The interpretation of these observations hinges critically on whether such melt inclusions can faithfully preserve primary or parental melt composition. If they do, melt inclusion data can truly answer big questions from small-scale observations. If they do not, they answer rather small questions. Favoring the second possibility, Danyushevsky et al. (2004) have suggested that much of the observed variability of highly incompatible trace elements in melt inclusions “may not represent geologically significant melts, but instead reflect localized, grain-scale reaction processes within the magmatic plumbing system.” We disagree and show that this mechanism cannot, for example, explain isotopic heterogeneity measured in several suites of melt inclusions, nor does it not account for the presence of ultra-depleted melts and "ghost" plagioclase signatures in other inclusions. More recently, Spandler et al. (2007) have suggested on the basis of experimental evidence that diffusion rates for REE in olivine are so rapid that parental melt compositions in melt inclusions are rapidly falsified by diffusional exchange with (evolved) host lava. We show that the very fact that extreme chemical and isotopic heterogeneities are routinely preserved in melt inclusions demonstrates that this conclusion is unwarranted, either because residence times of the olivine phenocrysts are much shorter than assumed by Spandler et al. or because the high experimental diffusion rates are caused by an unknown experimental artifact. Although there is no obvious flaw in design and execution of

Vacuum Energy and Inflation: 4. An Inflationary Universe

ERIC Educational Resources Information Center

Huggins, Elisha

2013-01-01

This is the fourth paper in a series of four. The first paper in the series, "Vacuum Energy and Inflation: 1. A Liter of Vacuum Energy" [EJ1024183] discusses an example of vacuum energy. Vacuum energy is explained as an energy with a negative pressure whose energy density remains constant in an expanding space. Paper 2, "Vacuum…

Engineering and Design of the Steady Inductive Helicity Injected Torus (HIT--SI)

NASA Astrophysics Data System (ADS)

Sieck, P. E.; Jarboe, T. R.; Nelson, B. A.; Rogers, J. A.; Shumlak, U.

1999-11-01

Steady Inductive Helicity Injection (SIHI) is an inductive helicity injection method that injects helicity at a nearly constant rate, without open field lines, and without removing any helicity or magnetic energy from the plasma.(T.R. Jarboe, Fusion Technology, 36) (1), p. 85, 1999 SIHI directly produces a rotating magnetic field structure, and in the frame of the rotating field the current profile is nearly time independent. The Steady Inductive Helicity Injected Torus (HIT--SI) is a spheromak designed to implement SIHI so that the current profile in the rotating frame is optimized. The geometry of HIT--SI will be presented, including the manufacturing techniques and metallurgical processes planned for construction of the close-fitting flux conserver. The flux conserver is made of aged chromium copper with 80% the conductivity of pure copper. The detailed electrical insulation requirements in the helicity injector design lead to a complex o-ring seal and a plasma-sprayed alumina insulation coating. This has prompted the construction of an o-ring prototype test fixture having the main features of the o-ring design and the alumina coating. The design and evaluation of this fixture will also be presented with vacuum and voltage test results.

Structure, thermodynamics, and properties of hydrous aluminosilicate melt in the deep Earth

NASA Astrophysics Data System (ADS)

Bajgain, S. K.; Mookherjee, M.

2017-12-01

In this study, we use first-principles molecular dynamics (FPMD) simulations to explore the structure, thermodynamics, and transport properties of alkali bearing aluminosliciate melt (NaAlSi2O6) with 4 wt.% H2O. We explored physical properties of the hydrous jadeite melt at temperatures and pressures relevant for the Earth's mantle, i.e., 2500- 4000 K and up to 50 GPa. Our results indicate that the fundamental structural units of jadeite, i.e., one dimensional (1-D) chain with a repeat of [Si2O6]4- is well preserved in anhydrous jadeite melt at low pressures. However, the 1-D chains are nonlinear and the silicate tetrahedral units are very distorted. We also note that in the hydrous jadeite melt, the dominant hydrogen bearing species are hydroxyl (OH) and water molecules (H2O). We do not find any evidence of OH attached to the bridging oxygen atoms. However, we do find OH groups attached to the non-bridging oxygen atoms at the terminal sites of the tetrahedral units associated with the distorted 1-D chains. It is possible that these terminal OH groups were former bridging oxygen atoms. Pressure-volume-temperature results of hydrous jadeite melt could be adequately described with a finite-strain equation of state with ρ0, K0, and K'0 being 2.0 g/cm3, 13.0 GPa, and 4.0, respectively. Our FPMD results also indicate that the diffusivity of alkali (Na) ions is comparable to the hydrogen atoms at lower pressures ( 90 ×10-10 m2/s at 6 GPa and 2500 K). The self diffusion of aluminum (6.5 ×10-10 m2/s) and silicon (4.5 ×10-10 m2/s) ions are significantly lower compared to the alkali ions and proton at the similar P-T condition. At higher pressures i.e., P> 20 GPa, the diffusivity of Na reduces significantly. At P> 20 GPa, the proton diffusivity remains higher than the other cation species. Therefore, a small fraction of hydrous melt at mantle transition zone conditions may explain the observed elevated electrical conductivity in specific regions such as in Japan and in

21 CFR 884.5070 - Vacuum abortion system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Vacuum abortion system. 884.5070 Section 884.5070 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... § 884.5070 Vacuum abortion system. (a) Identification. A vacuum abortion system is a device designed to...

46 CFR 153.368 - Pressure-vacuum valves.

Code of Federal Regulations, 2014 CFR

2014-10-01

... 46 Shipping 5 2014-10-01 2014-10-01 false Pressure-vacuum valves. 153.368 Section 153.368 Shipping... BULK LIQUID, LIQUEFIED GAS, OR COMPRESSED GAS HAZARDOUS MATERIALS Design and Equipment Cargo Venting Systems § 153.368 Pressure-vacuum valves. (a) The pressure side of a required pressure-vacuum relief valve...

46 CFR 153.368 - Pressure-vacuum valves.

Code of Federal Regulations, 2011 CFR

2011-10-01

... 46 Shipping 5 2011-10-01 2011-10-01 false Pressure-vacuum valves. 153.368 Section 153.368 Shipping... BULK LIQUID, LIQUEFIED GAS, OR COMPRESSED GAS HAZARDOUS MATERIALS Design and Equipment Cargo Venting Systems § 153.368 Pressure-vacuum valves. (a) The pressure side of a required pressure-vacuum relief valve...

46 CFR 153.368 - Pressure-vacuum valves.

Code of Federal Regulations, 2012 CFR

2012-10-01

... 46 Shipping 5 2012-10-01 2012-10-01 false Pressure-vacuum valves. 153.368 Section 153.368 Shipping... BULK LIQUID, LIQUEFIED GAS, OR COMPRESSED GAS HAZARDOUS MATERIALS Design and Equipment Cargo Venting Systems § 153.368 Pressure-vacuum valves. (a) The pressure side of a required pressure-vacuum relief valve...

46 CFR 153.368 - Pressure-vacuum valves.

Code of Federal Regulations, 2013 CFR

2013-10-01

... 46 Shipping 5 2013-10-01 2013-10-01 false Pressure-vacuum valves. 153.368 Section 153.368 Shipping... BULK LIQUID, LIQUEFIED GAS, OR COMPRESSED GAS HAZARDOUS MATERIALS Design and Equipment Cargo Venting Systems § 153.368 Pressure-vacuum valves. (a) The pressure side of a required pressure-vacuum relief valve...

46 CFR 153.368 - Pressure-vacuum valves.

Code of Federal Regulations, 2010 CFR

2010-10-01

... 46 Shipping 5 2010-10-01 2010-10-01 false Pressure-vacuum valves. 153.368 Section 153.368 Shipping... BULK LIQUID, LIQUEFIED GAS, OR COMPRESSED GAS HAZARDOUS MATERIALS Design and Equipment Cargo Venting Systems § 153.368 Pressure-vacuum valves. (a) The pressure side of a required pressure-vacuum relief valve...

21 CFR 884.5070 - Vacuum abortion system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Vacuum abortion system. 884.5070 Section 884.5070 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... § 884.5070 Vacuum abortion system. (a) Identification. A vacuum abortion system is a device designed to...

21 CFR 884.5070 - Vacuum abortion system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Vacuum abortion system. 884.5070 Section 884.5070 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... § 884.5070 Vacuum abortion system. (a) Identification. A vacuum abortion system is a device designed to...

21 CFR 884.5070 - Vacuum abortion system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Vacuum abortion system. 884.5070 Section 884.5070 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... § 884.5070 Vacuum abortion system. (a) Identification. A vacuum abortion system is a device designed to...

21 CFR 884.5070 - Vacuum abortion system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Vacuum abortion system. 884.5070 Section 884.5070 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... § 884.5070 Vacuum abortion system. (a) Identification. A vacuum abortion system is a device designed to...

The localized quantum vacuum field

NASA Astrophysics Data System (ADS)

Dragoman, D.

2008-03-01

A model for the localized quantum vacuum is proposed in which the zero-point energy (ZPE) of the quantum electromagnetic field originates in energy- and momentum-conserving transitions of material systems from their ground state to an unstable state with negative energy. These transitions are accompanied by emissions and re-absorptions of real photons, which generate a localized quantum vacuum in the neighborhood of material systems. The model could help resolve the cosmological paradox associated with the ZPE of electromagnetic fields, while reclaiming quantum effects associated with quantum vacuum such as the Casimir effect and the Lamb shift. It also offers a new insight into the Zitterbewegung of material particles.

Vacuum casting of thick polymeric films

NASA Technical Reports Server (NTRS)

Cuddihy, E. F.; Moacanin, J.

1979-01-01

Bubble formation and layering, which often plague vacuum-evaporated films, are prevented by properly regulating process parameters. Vacuum casting may be applicable to forming thick films of other polymer/solvent solutions.

14 CFR 25.1433 - Vacuum systems.

Code of Federal Regulations, 2010 CFR

2010-01-01

... STANDARDS: TRANSPORT CATEGORY AIRPLANES Equipment Miscellaneous Equipment § 25.1433 Vacuum systems. There... discharge lines from the vacuum air pump when the delivery temperature of the air becomes unsafe. [Doc. No...

Ceramic vacuum tubes for geothermal well logging

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kelly, R.D.

1977-01-12

The results of investigations carried out into the availability and suitability of ceramic vacuum tubes for the development of logging tools for geothermal wells are summarized. Design data acquired in the evaluation of ceramic vacuum tubes for the development of a 500/sup 0/C instrumentation amplifier are presented. The general requirements for ceramic vacuum tubes for application to the development of high temperature well logs are discussed. Commercially available tubes are described and future contract activities that specifically relate to ceramic vacuum tubes are detailed. Supplemental data is presented in the appendix. (MHR)

Optimizing the vacuum plasma spray deposition of metal, ceramic, and cermet coatings using designed experiments

NASA Astrophysics Data System (ADS)

Kingswell, R.; Scott, K. T.; Wassell, L. L.

1993-06-01

The vacuum plasma spray (VPS) deposition of metal, ceramic, and cermet coatings has been investigated using designed statistical experiments. Processing conditions that were considered likely to have a significant influence on the melting characteristics of the precursor powders and hence deposition efficiency were incorporated into full and fractional factorial experimental designs. The processing of an alumina powder was very sensitive to variations in the deposition conditions, particularly the injection velocity of the powder into the plasma flame, the plasma gas composition, and the power supplied to the gun. Using a combination of full and fractional factorial experimental designs, it was possible to rapidly identify the important spraying variables and adjust these to produce a deposition efficiency approaching 80 percent. The deposition of a nickel-base alloy metal powder was less sensitive to processing conditions. Generally, however, a high degree of particle melting was achieved for a wide range of spray conditions. Preliminary experiments performed using a tungsten carbide/cobalt cermet powder indicated that spray efficiency was not sensitive to deposition conditions. However, microstructural analysis revealed considerable variations in the degree of tungsten carbide dissolution. The structure and properties of the optimized coatings produced in the factorial experiments are also discussed.

Volatiles in melt inclusions from Icelandic magmas

NASA Astrophysics Data System (ADS)

Nichols, A. R.; Wysoczanski, R. J.; Carroll, M. R.

2006-12-01

Melt inclusions hosted in olivine crystals from the glassy rims of subglacially erupted pillow basalts on Iceland have been analysed for volatiles, major elements and trace elements. Volatile measurements were undertaken using Fourier-Transform InfraRed spectroscopy utilising a novel technique which enables unexposed and much smaller inclusions than were previously possible to be analysed. Major elements were measured using electron microprobe and trace elements by laser ablation-inductively coupled plasma-mass spectrometry. Comparison between initial results from the inclusions and the compositions of the bulk glasses show that the inclusions are less evolved and contain more H2O at the same MgO content. In addition many of the inclusions have higher H2O/K2O than their bulk glasses and some even contain CO2 (up to 629 ppm), which is below detection limits in the bulk glasses. This indicates that these inclusions are less affected by degassing. Two inclusions have extreme H2O/K2O (> 10), possibly suggesting that they have assimilated hydrous crustal material. The volatile and major element compositions of the bulk glasses have been used to suggest that the Iceland mantle plume is wet. However, trace element measurements show that enriched Iceland magmas have lower H2O/Ce than the adjacent Reykjanes Ridge. This could reflect syn-eruptive degassing or mixing between undegassed and recycled degassed magmas. Alternatively Iceland magmas could be derived from the EM (enriched mantle) component, which is believed to represent recycled oceanic crust. It is suggested that this material is efficiently dehydrated during the subduction process, so even though it has an enriched character, H2O is relatively depleted. As a result, EM melts have higher absolute H2O contents than mid- ocean ridge basalts (MORB), but lower H2O/Ce (or other H2O-incompatible element ratios), which has led to EM plumes being termed `dampspots'. The inclusion data will be presented in this context

Compressed Air/Vacuum Transportation Techniques

NASA Astrophysics Data System (ADS)

Guha, Shyamal

2011-03-01

General theory of compressed air/vacuum transportation will be presented. In this transportation, a vehicle (such as an automobile or a rail car) is powered either by compressed air or by air at near vacuum pressure. Four version of such transportation is feasible. In all versions, a ``c-shaped'' plastic or ceramic pipe lies buried a few inches under the ground surface. This pipe carries compressed air or air at near vacuum pressure. In type I transportation, a vehicle draws compressed air (or vacuum) from this buried pipe. Using turbine or reciprocating air cylinder, mechanical power is generated from compressed air (or from vacuum). This mechanical power transferred to the wheels of an automobile (or a rail car) drives the vehicle. In type II-IV transportation techniques, a horizontal force is generated inside the plastic (or ceramic) pipe. A set of vertical and horizontal steel bars is used to transmit this force to the automobile on the road (or to a rail car on rail track). The proposed transportation system has following merits: virtually accident free; highly energy efficient; pollution free and it will not contribute to carbon dioxide emission. Some developmental work on this transportation will be needed before it can be used by the traveling public. The entire transportation system could be computer controlled.

Failure modes of vacuum plasma spray tungsten coating created on carbon fibre composites under thermal loads

NASA Astrophysics Data System (ADS)

Hirai, T.; Bekris, N.; Coad, J. P.; Grisolia, C.; Linke, J.; Maier, H.; Matthews, G. F.; Philipps, V.; Wessel, E.

2009-07-01

Vacuum plasma spray tungsten (VPS-W) coating created on a carbon fibre reinforced composite (CFC) was tested under two thermal load schemes in the electron beam facility to examine the operation limits and failure modes. In cyclic ELM-like short transient thermal loads, the VPS-W coating was destroyed sub-layer by sub-layer at 0.33 GW/m 2 for 1 ms pulse duration. At longer single pulses, simulating steady-state thermal loads, the coating was destroyed at surface temperatures above 2700 °C by melting of the rhenium containing multilayer at the interface between VPS-W and CFC. The operation limits and failure modes of the VPS-W coating in the thermal load schemes are discussed in detail.

Stress-Driven Melt Segregation and Organization in Partially Molten Rocks III: Annealing Experiments and Surface Tension-Driven Redistribution of Melt

NASA Astrophysics Data System (ADS)

Parsons, R.; Hustoft, J. W.; Holtzman, B. K.; Kohlstedt, D. L.; Phipps Morgan, J.

2004-12-01

As discussed in the two previous abstracts in this series, simple shear experiments on synthetic upper mantle-type rock samples reveal the segregation of melt into melt-rich bands separated by melt-depleted lenses. Here, we present new results from experiments designed to understand the driving forces working for and against melt segregation. To better understand the kinetics of surface tension-driven melt redistribution, we first deform samples at similar conditions (starting material, sample size, stress and strain) to produce melt-rich band networks that are statistically similar. Then the load is removed and the samples are statically annealed to allow surface tension to redistribute the melt-rich networks. Three samples of olivine + 20 vol% chromite + 4 vol% MORB were deformed at a confining pressure of 300 MPa and a temperature of 1523 K in simple shear at shear stresses of 20 - 55 MPa to shear strains of 3.5 and then statically annealed for 0, 10, or 100 h at the same P-T conditions. Melt-rich bands are fewer in number and appear more diffuse when compared to the deformed but not annealed samples. Bands with less melt tend to disappear more rapidly than more melt-rich ones. The melt fraction in the melt-rich bands decreased from 0.2 in the quenched sample to 0.1 in the sample annealed for 100 h. After deformation, the melt fraction in the melt-depleted regions are ~0.006; after static annealing for 100 h, this value increases to 0.02. These experiments provide new quantitative constraints on the kinetics of melt migration driven by surface tension. By quantifying this driving force in the same samples in which stress-driven distribution occurred, we learn about the relative kinetics of stress-driven melt segregation. The kinetics of both of these processes must be scaled together to mantle conditions to understand the importance of stress-driven melt segregation in the Earth, and to understand the interaction of this process with melt-rock reaction

Growth of early continental crust by water-present eclogite melting in subduction zones

NASA Astrophysics Data System (ADS)

Laurie, A.; Stevens, G.

2011-12-01

The geochemistry of well preserved Paleo- to Meso-Archaean Tonalite-Trondhjemite-Granodiorite (TTG) suite rocks, such as the ca 3.45 Ga trondhjemites from the Barberton greenstone belt in South Africa, provides insight into the origins of Earth's early felsic continental crust. This is particularly well demonstrated by the high-Al2O3 variety of these magmas, such as the Barberton rocks, where the geochemistry requires that they are formed by high pressure (HP) melting of a garnet-rich metamafic source. This has been interpreted as evidence for the formation of these magmas by anatexis of the upper portions of slabs within Archaean subduction zones. Most of the experimental data relevant to Archaean TTG genesis has been generated by studies of fluid-absent melting of metabasaltic sources. However, water drives arc magmatism within Phanerozoic subduction zones and thus, understanding the behaviour of water in Archaean subduction zones, may have considerable value for understanding the genesis of these TTG magmas. Consequently, this study investigates the role of HP water-present melting of an eclogite-facies starting material, in the production of high-Al2O3 type TTG melts. Water-saturated partial melting experiments were conducted between 1.9 and 3.0GPa; and, 870°C and 900°C. The melting reaction is characterized by the breakdown of sodic Cpx, together with Qtz and H2O, to form melt in conjunction with a less sodic Cpx: Qtz + Cpx1 + Grt1 + H2O = Melt + Cpx2 + Grt2. In many of the experimental run products, melt segregated efficiently from residual crystals, allowing for the measurement of a full range of trace elements via Laser Ablation Inductively Coupled Plasma Mass Spectroscopy. The experimental glasses produced by this study have the compositions of peraluminous trondhjemites; and they are light rare earth element, Zr and Sr enriched; and heavy rare earth element, Y and Nb depleted. The compositions of the experimental glasses are similar to high-Al2O3 type

Vacuum chamber-free centrifuge with magnetic bearings.

PubMed

Park, Cheol Hoon; Kim, Soohyun; Kim, Kyung-Soo

2013-09-01

Centrifuges are devices that separate particles of different densities and sizes through the application of a centrifugal force. If a centrifuge could be operated under atmospheric conditions, all vacuum-related components such as the vacuum chamber, vacuum pump, diffusion pump, and sealing could be removed from a conventional centrifuge system. The design and manufacturing procedure for centrifuges could then be greatly simplified to facilitate the production of lightweight centrifuge systems of smaller volume. Furthermore, the maintenance costs incurred owing to wear and tear due to conventional ball bearings would be eliminated. In this study, we describe a novel vacuum chamber-free centrifuge supported by magnetic bearings. We demonstrate the feasibility of the vacuum chamber-free centrifuge by presenting experimental results that verify its high-speed support capability and motoring power capacity.

Vacuum deposition and curing of liquid monomers

DOEpatents

Affinito, J.D.

1993-11-09

The present invention is the formation of solid polymer layers under vacuum. More specifically, the present invention is the use of standard polymer layer-making equipment that is generally used in an atmospheric environment in a vacuum, and degassing the monomer material prior to injection into the vacuum. Additional layers of polymer or metal may be vacuum deposited onto solid polymer layers. Formation of polymer layers under a vacuum improves material and surface characteristics, and subsequent quality of bonding to additional layers. Further advantages include use of less to no photoinitiator for curing, faster curing, fewer impurities in the polymer electrolyte, as well as improvement in material properties including no trapped gas resulting in greater density, and reduced monomer wetting angle that facilitates spreading of the monomer and provides a smoother finished surface.

Vacuum deposition and curing of liquid monomers

DOEpatents

Affinito, J.D.

1995-03-07

The present invention is the formation of solid polymer layers under vacuum. More specifically, the present invention is the use of ``standard`` polymer layer-making equipment that is generally used in an atmospheric environment in a vacuum, and degassing the monomer material prior to injection into the vacuum. Additional layers of polymer or metal or oxide may be vacuum deposited onto solid polymer layers. Formation of polymer layers under a vacuum improves material and surface characteristics, and subsequent quality of bonding to additional layers. Further advantages include use of less to no photoinitiator for curing, faster curing, fewer impurities in the polymer electrolyte, as well as improvement in material properties including no trapped gas resulting in greater density, and reduced monomer wetting angle that facilitates spreading of the monomer and provides a smoother finished surface.

Vacuum deposition and curing of liquid monomers

DOEpatents

Affinito, John D.

1993-01-01

The present invention is the formation of solid polymer layers under vacuum. More specifically, the present invention is the use of "standard" polymer layer-making equipment that is generally used in an atmospheric environment in a vacuum, and degassing the monomer material prior to injection into the vacuum. Additional layers of polymer or metal may be vacuum deposited onto solid polymer layers. Formation of polymer layers under a vacuum improves material and surface characteristics, and subsequent quality of bonding to additional layers. Further advantages include use of less to no photoinitiator for curing, faster curing, fewer impurities in the polymer electrolyte, as well as improvement in material properties including no trapped gas resulting in greater density, and reduced monomer wetting angle that facilitates spreading of the monomer and provides a smoother finished surface.

Vacuum deposition and curing of liquid monomers

DOEpatents

Affinito, John D.

1995-01-01

The present invention is the formation of solid polymer layers under vacuum. More specifically, the present invention is the use of "standard" polymer layer-making equipment that is generally used in an atmospheric environment in a vacuum, and degassing the monomer material prior to injection into the vacuum. Additional layers of polymer or metal or oxide may be vacuum deposited onto solid polymer layers. Formation of polymer layers under a vacuum improves material and surface characteristics, and subsequent quality of bonding to additional layers. Further advantages include use of less to no photoinitiator for curing, faster curing, fewer impurities in the polymer electrolyte, as well as improvement in material properties including no trapped gas resulting in greater density, and reduced monomer wetting angle that facilitates spreading of the monomer and provides a smoother finished surface.

Low inductance diode design of the Proto 2 accelerator for imploding plasma loads

NASA Astrophysics Data System (ADS)

Hsing, W. W.; Coats, R.; McDaniel, D. H.; Spielman, R. B.

A new water transmission line convolute, single piece insulator, and double accelerator. The water transmission lines have a 5 cm gap to eliminate any water arcing. A two-dimensional magnetic field code was used to calculate the convolute inductance. An acrylic insulator was used as well as a single piece, laminated polycarbonate insulator. They have been successfully tested at over 90% of the Shipman criteria for classical insulator breakdown, although the laminations in the polycarbonate insulator failed after a few shots. The anode and cathode each have two pieces and are held together mechanically. The vacuum MITL tapers to a 3 mm minimum gap. The total inductance is 8.4 nH for gas puff loads and 7.8 nH for imploding foil loads. Out of a forward-going energy of 290 kJ, 175 kJ has been delivered past the insulator, and 100 kJ has been successfully delivered to the load.

Cryogenic Insulation System for Soft Vacuum

NASA Technical Reports Server (NTRS)

Augustynowicz, S. D.; Fesmire, J. E.

1999-01-01

The development of a cryogenic insulation system for operation under soft vacuum is presented in this paper. Conventional insulation materials for cryogenic applications can be divided into three levels of thermal performance, in terms of apparent thermal conductivity [k-value in milliwatt per meter-kelvin (mW/m-K)]. System k-values below 0.1 can be achieved for multilayer insulation operating at a vacuum level below 1 x 10(exp -4) torr. For fiberglass or powder operating below 1 x 10(exp -3) torr, k-values of about 2 are obtained. For foam and other materials at ambient pressure, k-values around 30 are typical. New industry and aerospace applications require a versatile, robust, low-cost thermal insulation with performance in the intermediate range. The target for the new composite insulation system is a k-value below 4.8 mW/m-K (R-30) at a soft vacuum level (from 1 to 10 torr) and boundary temperatures of approximately 77 and 293 kelvin (K). Many combinations of radiation shields, spacers, and composite materials were tested from high vacuum to ambient pressure using cryostat boiloff methods. Significant improvement over conventional systems in the soft vacuum range was demonstrated. The new layered composite insulation system was also shown to provide key benefits for high vacuum applications as well.

Vacuum-assisted venous return reduces blood usage.

PubMed

Banbury, Michael K; White, Jennifer A; Blackstone, Eugene H; Cosgrove, Delos M

2003-09-01

To determine whether vacuum-assisted venous return has clinical advantages over conventional gravity drainage apart from allowing the use of smaller cannulas and shorter tubing. A total of 150 valve operations were performed at our institution between February and July 1999 using vacuum-assisted venous return with small venous cannulas connected to short tubing. These were compared with (1) 83 valve operations performed between April 1997 and January 1998 using the initial version of vacuum-assisted venous return, and (2) 124 valve operations performed between January and April of 1997 using conventional gravity drainage. Priming volume, hematocrit value, red blood cell usage, and total blood product usage were compared multivariably. These comparisons were covariate and propensity adjusted for dissimilarities between the groups and confirmed by propensity-matched pairs analysis. Priming volume was 1.4 +/- 0.4 L for small-cannula vacuum-assisted venous return, 1.7 +/- 0.4 L for initial vacuum-assisted venous return, and 2.0 +/- 0.4 L for gravity drainage (P <.0001). Smaller priming resulted in higher hematocrit values both at the beginning of cardiopulmonary bypass (27% +/- 5% compared with 26% +/- 4% and 25% +/- 4%, respectively, P <.0001) and at the end (30% +/- 4% compared with 28% +/- 4% and 27% +/- 4%, respectively, P <.0001). Red cell transfusions were used in 17% of the patients having small-cannula vacuum-assisted venous return, 27% of the initial patients having vacuum-assisted venous return, and 37% of the patients having gravity drainage (P =.001); total blood product usage was 19%, 27%, and 39%, respectively (P =.002). Although ministernotomy also was associated with reduced blood product usage (P <.004), propensity matching on type of sternotomy confirmed the association of vacuum-assisted venous return with lowered blood product usage. Vacuum-assisted venous return results in (1) higher hematocrit values during cardiopulmonary bypass and (2) decreased

Effects of water, depth and temperature on partial melting of mantle-wedge fluxed by hydrous sediment-melt in subduction zones

NASA Astrophysics Data System (ADS)

Mallik, Ananya; Dasgupta, Rajdeep; Tsuno, Kyusei; Nelson, Jared

2016-12-01

This study investigates the partial melting of variable bulk H2O-bearing parcels of mantle-wedge hybridized by partial melt derived from subducted metapelites, at pressure-temperature (P-T) conditions applicable to the hotter core of the mantle beneath volcanic arcs. Experiments are performed on mixtures of 25% sediment-melt and 75% fertile peridotite, from 1200 to 1300 °C, at 2 and 3 GPa, with bulk H2O concentrations of 4 and 6 wt.%. Combining the results from these experiments with previous experiments containing 2 wt.% bulk H2O (Mallik et al., 2015), it is observed that all melt compositions, except those produced in the lowest bulk H2O experiments at 3 GPa, are saturated with olivine and orthopyroxene. Also, higher bulk H2O concentration increases melt fraction at the same P-T condition, and causes exhaustion of garnet, phlogopite and clinopyroxene at lower temperatures, for a given pressure. The activity coefficient of silica (ϒSiO2) for olivine-orthopyroxene saturated melt compositions (where the activity of silica, aSiO2 , is buffered by the reaction olivine + SiO2 = orthopyroxene) from this study and from mantle melting studies in the literature are calculated. In melt compositions generated at 2 GPa or shallower, with increasing H2O concentration, ϒSiO2 increases from <1 to ∼1, indicating a transition from non-ideal mixing as OH- in the melt (ϒSiO2 <1) to ideal mixing as molecular H2O (ϒSiO2 ∼1). At pressures >2 GPa, ϒSiO2 >1 at higher H2O concentrations in the melt, indicate requirement of excess energy to incorporate molecular H2O in the silicate melt structure, along with a preference for bridging species and polyhedral edge decorations. With vapor saturation in the presence of melt, ϒSiO2 decreases indicating approach towards ideal mixing of H2O in silicate melt. For similar H2O concentrations in the melt, ϒSiO2 for olivine-orthopyroxene saturated melts at 3 GPa is higher than melts at 2 GPa or shallower. This results in melts generated at

Vacuum Plasma Spray Forming of Tungsten Lorentz Force Accelerator Components

NASA Technical Reports Server (NTRS)

Zimmerman, Frank R.

2001-01-01

The Vacuum Plasma Spray (VPS) Laboratory at NASA's Marshall Space Flight Center has developed and demonstrated a fabrication technique using the VPS process to form anode sections for a Lorentz force accelerator from tungsten. Lorentz force accelerators are an attractive form of electric propulsion that provides continuous, high-efficiency propulsion at useful power levels for such applications as orbit transfers or deep space missions. The VPS process is used to deposit refractory metals such as tungsten onto a graphite mandrel of the desired shape. Because tungsten is reactive at high temperatures, it is thermally sprayed in an inert environment where the plasma gun melts and accelerates the metal powder onto the mandrel. A three-axis robot inside the chamber controls the motion of the plasma spray torch. A graphite mandrel acts as a male mold, forming the required contour and dimensions of the inside surface of the anode. This paper describes the processing techniques, design considerations, and process development associated with the VPS forming of the Lorentz force accelerator.

Melting of superheated molecular crystals

NASA Astrophysics Data System (ADS)

Cubeta, Ulyana; Bhattacharya, Deepanjan; Sadtchenko, Vlad

2017-07-01

Melting dynamics of micrometer scale, polycrystalline samples of isobutane, dimethyl ether, methyl benzene, and 2-propanol were investigated by fast scanning calorimetry. When films are superheated with rates in excess of 105 K s-1, the melting process follows zero-order, Arrhenius-like kinetics until approximately half of the sample has transformed. Such kinetics strongly imply that melting progresses into the bulk via a rapidly moving solid-liquid interface that is likely to originate at the sample's surface. Remarkably, the apparent activation energies for the phase transformation are large; all exceed the enthalpy of vaporization of each compound and some exceed it by an order of magnitude. In fact, we find that the crystalline melting kinetics are comparable to the kinetics of dielectric α-relaxation in deeply supercooled liquids. Based on these observations, we conclude that the rate of non-isothermal melting for superheated, low-molecular-weight crystals is limited by constituent diffusion into an abnormally dense, glass-like, non-crystalline phase.

Nanorheology of Entangled Polymer Melts

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ge, Ting; Grest, Gary S.; Rubinstein, Michael

In this study, we use molecular simulations to probe the local viscoelasticity of an entangled polymer melt by tracking the motion of embedded nonsticky nanoparticles (NPs). As in conventional microrheology, the generalized Stokes-Einstein relation is employed to extract an effective stress relaxation function G GSE(t) from the mean square displacement of NPs. G GSE(t) for different NP diameters d are compared with the stress relaxation function G(t) of a pure polymer melt. The deviation of G GSE(t) from G(t) reflects the incomplete coupling between NPs and the dynamic modes of the melt. For linear polymers, a plateau in G GSE(t)more » emerges as d exceeds the entanglement mesh size a and approaches the entanglement plateau in G(t) for a pure melt with increasing d. For ring polymers, as d increases towards the spanning size R of ring polymers, G GSE(t) approaches G(t) of the ring melt with no entanglement plateau.« less

Nanorheology of Entangled Polymer Melts

DOE PAGES

Ge, Ting; Grest, Gary S.; Rubinstein, Michael

2018-02-01

In this study, we use molecular simulations to probe the local viscoelasticity of an entangled polymer melt by tracking the motion of embedded nonsticky nanoparticles (NPs). As in conventional microrheology, the generalized Stokes-Einstein relation is employed to extract an effective stress relaxation function G GSE(t) from the mean square displacement of NPs. G GSE(t) for different NP diameters d are compared with the stress relaxation function G(t) of a pure polymer melt. The deviation of G GSE(t) from G(t) reflects the incomplete coupling between NPs and the dynamic modes of the melt. For linear polymers, a plateau in G GSE(t)more » emerges as d exceeds the entanglement mesh size a and approaches the entanglement plateau in G(t) for a pure melt with increasing d. For ring polymers, as d increases towards the spanning size R of ring polymers, G GSE(t) approaches G(t) of the ring melt with no entanglement plateau.« less

Breakdown-Resistant RF Connectors for Vacuum

NASA Technical Reports Server (NTRS)

Caro, Edward R.; Bonazza, Walter J.

1987-01-01

Resilient inserts compensate for insulation shrinkage. Coaxial-cable connector for radio-frequency (RF) energy resists electrical breakdown in vacuum. Used on RF equipment in vacuum chambers as well as in spaceborne radar and communication gear.

Pressure melting and ice skating

NASA Astrophysics Data System (ADS)

Colbeck, S. C.

1995-10-01

Pressure melting cannot be responsible for the low friction of ice. The pressure needed to reach the melting temperature is above the compressive failure stress and, if it did occur, high squeeze losses would result in very thin films. Pure liquid water cannot coexist with ice much below -20 °C at any pressure and friction does not increase suddenly in that range. If frictional heating and pressure melting contribute equally, the length of the wetted contact could not exceed 15 μm at a speed of 5 m/s, which seems much too short. If pressure melting is the dominant process, the water films are less than 0.08 μm thick because of the high pressures.

Quasi-equilibrium melting of quartzite upon extreme friction

NASA Astrophysics Data System (ADS)

Lee, Sung Keun; Han, Raehee; Kim, Eun Jeong; Jeong, Gi Young; Khim, Hoon; Hirose, Takehiro

2017-06-01

The friction on fault planes that controls how rocks slide during earthquakes decreases significantly as a result of complex fault-lubrication processes involving frictional melting. Fault friction has been characterized in terms of the preferential melting of minerals with low melting points--so-called disequilibrium melting. Quartz, which has a high melting temperature of about 1,726 °C and is a major component of crustal rocks, is not expected to melt often during seismic slip. Here we use high-velocity friction experiments on quartzite to show that quartz can melt at temperatures of 1,350 to 1,500 °C. This implies that quartz within a fault plane undergoing rapid friction sliding could melt at substantially lower temperatures than expected. We suggest that depression of the melting temperature is caused by the preferential melting of ultra-fine particles and metastable melting of β-quartz at about 1,400 °C during extreme frictional slip. The results for quartzite are applicable to complex rocks because of the observed prevalence of dynamic grain fragmentation, the preferential melting of smaller grains and the kinetic preference of β-quartz formation during frictional sliding. We postulate that frictional melting of quartz on a fault plane at temperatures substantially below the melting temperature could facilitate slip-weakening and lead to large earthquakes.

Heterozygote PCR product melting curve prediction.

PubMed

Dwight, Zachary L; Palais, Robert; Kent, Jana; Wittwer, Carl T

2014-03-01

Melting curve prediction of PCR products is limited to perfectly complementary strands. Multiple domains are calculated by recursive nearest neighbor thermodynamics. However, the melting curve of an amplicon containing a heterozygous single-nucleotide variant (SNV) after PCR is the composite of four duplexes: two matched homoduplexes and two mismatched heteroduplexes. To better predict the shape of composite heterozygote melting curves, 52 experimental curves were compared with brute force in silico predictions varying two parameters simultaneously: the relative contribution of heteroduplex products and an ionic scaling factor for mismatched tetrads. Heteroduplex products contributed 25.7 ± 6.7% to the composite melting curve, varying from 23%-28% for different SNV classes. The effect of ions on mismatch tetrads scaled to 76%-96% of normal (depending on SNV class) and averaged 88 ± 16.4%. Based on uMelt (www.dna.utah.edu/umelt/umelt.html) with an expanded nearest neighbor thermodynamic set that includes mismatched base pairs, uMelt HETS calculates helicity as a function of temperature for homoduplex and heteroduplex products, as well as the composite curve expected from heterozygotes. It is an interactive Web tool for efficient genotyping design, heterozygote melting curve prediction, and quality control of melting curve experiments. The application was developed in Actionscript and can be found online at http://www.dna.utah.edu/hets/. © 2013 WILEY PERIODICALS, INC.

Estimation of Melting Points of Organics.

PubMed

Yalkowsky, Samuel H; Alantary, Doaa

2018-05-01

Unified physicochemical property estimation relationships is a system of empirical and theoretical relationships that relate 20 physicochemical properties of organic molecules to each other and to chemical structure. Melting point is a key parameter in the unified physicochemical property estimation relationships scheme because it is a determinant of several other properties including vapor pressure, and solubility. This review describes the first-principals calculation of the melting points of organic compounds from structure. The calculation is based on the fact that the melting point, T m , is equal to the ratio of the heat of melting, ΔH m , to the entropy of melting, ΔS m . The heat of melting is shown to be an additive constitutive property. However, the entropy of melting is not entirely group additive. It is primarily dependent on molecular geometry, including parameters which reflect the degree of restriction of molecular motion in the crystal to that of the liquid. Symmetry, eccentricity, chirality, flexibility, and hydrogen bonding, each affect molecular freedom in different ways and thus make different contributions to the total entropy of fusion. The relationships of these entropy determining parameters to chemical structure are used to develop a reasonably accurate means of predicting the melting points over 2000 compounds. Copyright © 2018 American Pharmacists Association®. Published by Elsevier Inc. All rights reserved.

Breather cloth for vacuum curing

NASA Technical Reports Server (NTRS)

Reed, M. W.

1979-01-01

Finely-woven nylon cloth that has been treated with Teflon improves vacuum adhesive bonding of coatings to substrates. Cloth is placed over coating; entire assembly, including substrate, coating, and cloth, is placed in plastic vacuum bag for curing. Cloth allows coating to "breathe" when bag is evacuated. Applications include bonding film coatings to solar concentrators and collectors.

Vacuum Gas Tungsten Arc Welding

NASA Technical Reports Server (NTRS)

Weeks, J. L.; Todd, D. T.; Wooten, J. R.

1997-01-01

A two-year program investigated vacuum gas tungsten arc welding (VGTAW) as a method to modify or improve the weldability of normally difficult-to-weld materials. After a vacuum chamber and GTAW power supply were modified, several difficult-to-weld materials were studied and key parameters developed. Finally, Incoloy 903 weld overlays were produced without microfissures.

Pyroxene-melt equilibria. [for lunar maria basalts

NASA Technical Reports Server (NTRS)

Nielsen, R. L.; Drake, M. J.

1979-01-01

A thermodynamic analysis of pyroxene-melt equilibria is performed through use of a literature survey of analyses of high-Ca pyroxene and coexisting silicate melt pairs and analyses of low-Ca pyroxene silicate melt pairs. Reference is made to a modified version of a model developed by Bottinga and Weill (1972) which more successfully accounts for variations in melt composition than does a model which considers the melt to be composed of simple oxides which mix ideally. By using a variety of pyroxene melt relations, several pyroxene-melt and low-Ca pyroxene-high-Ca pyroxene geothermometers are developed which have internally consistant precisions of approximately + or - 20 C. Finally, it is noted that these equations may have application in modeling the evolution of mineral compositions during differentiation of basaltic magmas.

Improved efficiency and precise temperature control of low-frequency induction-heating pure iron vapor source on ECR ion source

NASA Astrophysics Data System (ADS)

Kato, Y.; Takenaka, T.; Yano, K.; Kiriyama, R.; Kurisu, Y.; Nozaki, D.; Muramatsu, M.; Kitagawa, A.; Uchida, T.; Yoshida, Y.; Sato, F.; Iida, T.

2012-11-01

Multiply charged ions to be used prospectively are produced from solid pure material in an electron cyclotron resonance ion source (ECRIS). Recently a pure iron source is also required for the production of caged iron ions in the fullerene in order to control cells in vivo in bio-nano science and technology. We adopt directly heating iron rod by induction heating (IH) because it has non-contact with insulated materials which are impurity gas sources. We choose molybdenum wire for the IH coils because it doesn't need water cooling. To improve power efficiency and temperature control, we propose to the new circuit without previously using the serial and parallel dummy coils (SPD) for matching and safety. We made the circuit consisted of inductively coupled coils which are thin-flat and helix shape, and which insulates the IH power source from the evaporator. This coupling coils circuit, i.e. insulated induction heating coil transformer (IHCT), can be move mechanically. The secondary current can be adjusted precisely and continuously. Heating efficiency by using the IHCT is much higher than those of previous experiments by using the SPD, because leakage flux is decreased and matching is improved simultaneously. We are able to adjust the temperature in heating the vapor source around melting point. And then the vapor pressure can be controlled precisely by using the IHCT. We can control ±10K around 1500°C by this method, and also recognize to controlling iron vapor flux experimentally in the extreme low pressures. Now we come into next stage of developing induction heating vapor source for materials with furthermore high temperature melting points above 2000K with the IHCT, and then apply it in our ECRIS.

Apparatus For Metal/Inert-Gas Welding In Vacuum

NASA Technical Reports Server (NTRS)

Stocks, C. O.

1994-01-01

Metal/inert-gas welding-torch assembly operates in vacuum. Plasma generated in interior chamber and focused onto workpiece in vacuum. Pinch rollers feed wire to weld puddle. Controlled flow of plasma reduces dispersal in vacuum, preventing extinction.

Submarine melt rates under Greenland's ice tongues

NASA Astrophysics Data System (ADS)

Wilson, Nat; Straneo, Fiametta; Heimbach, Patrick; Cenedese, Claudia

2017-04-01

The few remaining ice tongues (ice-shelf like extensions) of Greenland's glaciers are undergoing rapid changes with potential implications for the stability of the ice sheet. Submarine melting is recognized as a major contributor to mass loss, yet the magnitude and spatial distribution of melt are poorly known or understood. Here, we use high resolution satellite imagery to infer the magnitude and spatial variability of melt rates under Greenland's largest remaining ice tongues: Ryder Glacier, Petermann Glacier and Nioghalvfjerdsbræ (79 North Glacier). We find that submarine plus aerial melt approximately balance the ice flux from the grounded ice sheet for the first two while at Nioghalvfjerdsbræ the total melt flux exceeds the inflow of ice indicating thinning of the ice tongue. We also show that melt rates under the ice tongues vary considerably, exceeding 60 m yr-1 near the grounding zone and decaying rapidly downstream. Channels, likely originating from upstream subglacial channels, give rise to large melt variations across the ice tongues. Using derived melt rates, we test simplified melt parameterizations appropriate for ice sheet models and find the best agreement with those that incorporate ice tongue geometry in the form of depth and slope.

TFTR diagnostic vacuum controller

DOE Office of Scientific and Technical Information (OSTI.GOV)

Olsen, D.; Persons, R.

1981-01-01

The TFTR diagnostic vacuum controller (DVC) provides in conjunction with the Central Instrumentation Control and Data Acquisition System (CICADA), control and monitoring for the pumps, valves and gauges associated with each individual diagnostic vacuum system. There will be approximately 50 systems on TFTR. Two standard versions of the controller (A and B) wil be provided in order to meet the requirements of two diagnostic manifold arrangements. All pump and valve sequencing, as well as protection features, will be implemented by the controller.

Pulsed Inductive Thruster (PIT): Modeling and Validation Using the MACH2 Code

NASA Technical Reports Server (NTRS)

Schneider, Steven (Technical Monitor); Mikellides, Pavlos G.

2003-01-01

Numerical modeling of the Pulsed Inductive Thruster exercising the magnetohydrodynamics code, MACH2 aims to provide bilateral validation of the thruster's measured performance and the code's capability of capturing the pertinent physical processes. Computed impulse values for helium and argon propellants demonstrate excellent correlation to the experimental data for a range of energy levels and propellant-mass values. The effects of the vacuum tank wall and massinjection scheme were investigated to show trivial changes in the overall performance. An idealized model for these energy levels and propellants deduces that the energy expended to the internal energy modes and plasma dissipation processes is independent of the propellant type, mass, and energy level.

The geometry and volume of melt beneath Ethiopia

NASA Astrophysics Data System (ADS)

Kendall, J. M.; Hammond, J. O. S.

2016-12-01

A range of seismic measurements can be used to map melt distribution in the crust and uppermost mantle. These include seismic P- and S-wave velocities derived from surface- and body-wave tomography, Vp/Vs ratios obtained from receiver functions, and estimates of seismic anisotropy and attenuation. The most obvious melt parameter that seismic data might be sensitive to is volume fraction. However, such data are more sensitive to the aspect ratio of melt inclusions, which is controlled by the melt wetting angle or in other words the shape of the melt inclusion. To better understand this we perform numerical modelling, varying the shape and amount of melt, to show how various seismic phases are effected by melt. To consider the effects on seismic anisotropy we assume that the melt can be stored in pockets of melt that are either horizontally or vertically aligned (e.g., sills versus dykes). We then consider a range of seismic observations from the rifting environment of Ethiopia. Recent studies of P- and S-wave tomography, Rayleigh and Love waves, and Pn or wide angle P-wave refractions provide provide complimentary constraints on melt volume, orientation and inclusion aspect ratio. Furthermore, receiver functions and shear-wave splitting in body waves show strong anisotropy in this region and can be used to constrain the strike of vertically-aligned partial melt. We show that melt in the mantle beneath Ethiopia is likely stored in low aspect ratio disk-like inclusions, suggesting melt is not in textural equilibrium. We estimate that 2-7% vertically aligned melt is stored beneath the Main Ethiopian Rift, >6% horizontally and vertically aligned melt is stored beneath the Afar-region of the Red Sea Rift and 1-6% horizontally aligned melt is stored beneath the Danakil microplate. This supports ideas of strong shear-derived segregation of melt in narrow parts of the rift and large volumes of melt beneath Afar.

Fate of electroweak vacuum during preheating

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ema, Yohei; Mukaida, Kyohei; Nakayama, Kazunori

2016-10-28

Our electroweak vacuum may be metastable in light of the current experimental data of the Higgs/top quark mass. If this is really the case, high-scale inflation models require a stabilization mechanism of our vacuum during inflation. A possible candidate is the Higgs-inflaton/-curvature coupling because it induces an additional mass term to the Higgs during the slow roll regime. However, after inflation, the additional mass term oscillates, and it can destabilize our electroweak vacuum via production of large Higgs fluctuations during the inflaton oscillation era. In this paper, we study whether or not the Higgs-inflaton/-curvature coupling can save our vacuum bymore » properly taking account of Higgs production during the preheating stage. We put upper bounds on the Higgs-inflaton and -curvature couplings, and discuss possible dynamics that might relax them.« less

Influence of Melting and Hydrothermal Alteration on Lead in Abyssal Peridotites

NASA Astrophysics Data System (ADS)

Warren, J. M.; D'Errico, M. E.; Godard, M.; Coble, M. A.; Horan, M.

2017-12-01

The lead isotopic system is a key tracer of mantle convection, yet the abundance and mineralogical hosts of Pb in the upper mantle are poorly constrained. To address this, we analyzed the concentration of Pb in minerals and bulk rock powders of abyssal peridotites. These samples represent the oceanic upper mantle following melt extraction. They can be used to explore the mantle Pb budget, assuming that the amount of Pb lost during mantle melting and gained during seafloor alteration can be determined. We performed in situ analysis of the three main silicate phases (olivine, orthopyroxene, and clinopyroxene), which yield Pb concentrations of 2-30 ppb. Olivine is the main mineralogical host of Pb, unlike other trace elements, which are predominantly hosted in clinopyroxene. Sulfide contains an average of 3 ppm Pb, but these high concentrations are offset by low modal abundances (<0.01%), making this mineral a minor source of peridotite Pb. Whole rock Pb concentrations of abyssal peridotites measured by thermal ionization mass spectrometry range from 3 to 38 ppb. These values are close to the reconstructed whole rock values of 2 to 14 ppb, calculated from the mineral concentrations of Pb multiplied by their modes. In contrast, the average value among literature data for whole rock abyssal peridotites is >100 ppb [1, 2], measured by inductively-coupled plasma mass spectrometry. The higher values among literature data may reflect a combination of lower analytical sensitivity and effects of alteration. Samples in this study include an unaltered peridotite from the Gakkel Ridge, which shows the closest agreement between reconstructed and measured whole rock values. We estimate that our peridotites have undergone 5 to 9% melting [3], based on non-modal fractional melt modeling of rare earth element abundances. Assuming 18 to 23 ppb Pb in the depleted source mantle [4, 5], expected concentrations in abyssal peridotites after melting are <1 ppb. However, as suggested by [5

Occurrence of silicate melt, carbonate-rich melt and fluid during medium pressure anatexis of metapelitic gneisses (Oberpfalz, Bavaria) revealed by melt and fluid inclusions study

NASA Astrophysics Data System (ADS)

Ferrero, Silvio; O'Brien, Patrick; Hecht, Lutz; Wunder, Bernd

2014-05-01

In the last decades our understanding of partial melting processes in the lower crust profited from the investigation of fluid inclusions (Touret et al., 2009) and more recently of anatectic melt inclusions (Cesare et al., 2011) within enclaves and high-grade terranes. The latter finding allowed us to directly analyse the original anatectic melt (Ferrero et al., 2012; Bartoli et al., 2013) preserved within peritectic phases, i.e. mainly garnet, but also ilmenite and spinel, before fractionation, mixing and contamination processes took place. Furthermore, the occurrence of primary fluid inclusions (FI) and anatectic melt inclusions (MI) within enclaves allowed the characterization of the COH fluid present during anatexis under fluid+melt immiscibility conditions (Ferrero et al., 2014). Primary crystallized MI, or "nanogranites", and FI have been identified to occur as clusters in garnet from stromatic migmatites (Zeilengneise) from Oberpfalz, Eastern Bavaria (Moldanubian Zone). During the late Carboniferous, these Grt+Bt+Sill+Crd+Spl metapelitic gneisses underwent HT/MP metamorphism, followed by a HT/LP event (Tanner & Behrmann, 1995). Nanogranites, ≤20 µm in size, consist of Qtz+Bt+Wm+Ab±Ap, and show abundant nanoporosity, localized in the quartz. Fluid inclusions are smaller, generally ≤10 µm, and contain CO2+N2+CH4 plus siderite, pyrophillite and cristobalite, mineral phases not observed in the surrounding rock or as mineral inclusion in garnet. Polycrystalline inclusions containing Cc+Wm+Opx±Qz, commonly ≤10 µm in diameter, occur in the same cluster with MI and FI. Microstructural features, negative-crystal shape and the well-developed crystalline faces of calcite within inclusions suggest that they may result from the crystallization of a carbonate-rich melt. The lack of arrays of carbonate-bearing MI, verified by cathodoluminiscence investigation, supports their primary nature, i.e. they formed during garnet growth. This would suggest the occurrence

Simulation of the synergistic low Earth orbit effects of vacuum thermal cycling, vacuum UV radiation, and atomic oxygen

NASA Technical Reports Server (NTRS)

Dever, Joyce A.; Degroh, Kim K.; Stidham, Curtis R.; Stueber, Thomas J.; Dever, Therese M.; Rodriguez, Elvin; Terlep, Judith A.

1992-01-01

In order to assess the low Earth orbit (LEO) durability of candidate space materials, it is necessary to use ground laboratory facilities which provide LEO environmental effects. A facility combining vacuum thermal cycling and vacuum ultraviolet (VUV) radiation has been designed and constructed at NASA Lewis Research Center for this purpose. This facility can also be operated without the VUV lamps. An additional facility can be used to provide VUV exposure only. By utilizing these facilities, followed by atomic oxygen exposure in an RF plasma asher, the effects of the individual vacuum thermal cycling and VUV environments can be compared to the effect of the combined vacuum thermal cycling/VUV environment on the atomic oxygen durability of materials. The synergistic effects of simulated LEO environmental conditions on materials were evaluated by first exposing materials to vacuum thermal cycling, VUV, and vacuum thermal cycling/VUV environments followed by exposure to atomic oxygen in an RP plasma asher. Candidate space power materials such as atomic oxygen protected polyimides and solar concentrator mirrors were evaluated using these facilities. Characteristics of the Vacuum Thermal Cycling/VUV Exposure Facility which simulates the temperature sequences and solar ultraviolet radiation exposure that would be experienced by a spacecraft surface in LEO are discussed. Results of durability evaluations of some candidate space power materials to the simulated LEO environmental conditions will also be discussed. Such results have indicated that for some materials, atomic oxygen durability is affected by previous exposure to thermal cycling and/or VUV exposure.

Nearly Seamless Vacuum-Insulated Boxes

NASA Technical Reports Server (NTRS)

Stepanian, Christopher J.; Ou, Danny; Hu, Xiangjun

2010-01-01

A design concept, and a fabrication process that would implement the design concept, have been proposed for nearly seamless vacuum-insulated boxes that could be the main structural components of a variety of controlled-temperature containers, including common household refrigerators and insulating containers for shipping foods. In a typical case, a vacuum-insulated box would be shaped like a rectangular parallelepiped conventional refrigerator box having five fully closed sides and a hinged door on the sixth side. Although it is possible to construct the five-closed-side portion of the box as an assembly of five unitary vacuum-insulated panels, it is not desirable to do so because the relatively high thermal conductances of the seams between the panels would contribute significant amounts of heat leakage, relative to the leakage through the panels themselves. In contrast, the proposal would make it possible to reduce heat leakage by constructing the five-closed-side portion of the box plus the stationary portion (if any) of the sixth side as a single, seamless unit; the only remaining seam would be the edge seal around the door. The basic cross-sectional configuration of each side of a vacuum-insulated box according to the proposal would be that of a conventional vacuum-insulated panel: a low-density, porous core material filling a partially evacuated space between face sheets. However, neither the face sheets nor the core would be conventional. The face sheets would be opposite sides of a vacuum bag. The core material would be a flexible polymer-modified silica aerogel of the type described in Silica/Polymer and Silica/Polymer/Fiber Composite Aero - gels (MSC-23736) in this issue of NASA Tech Briefs. As noted in that article, the stiffness of this core material against compression is greater than that of prior aerogels. This is an important advantage because it translates to greater retention of thickness and, hence, of insulation performance when pressure is

Melts of garnet lherzolite: experiments, models and comparison to melts of pyroxenite and carbonated lherzolite

USGS Publications Warehouse

Grove, Timothy L.; Holbig, Eva S.; Barr, Jay A.; Till, Christy B.; Krawczynski, Michael J.

2013-01-01

Phase equilibrium experiments on a compositionally modified olivine leucitite from the Tibetan plateau have been carried out from 2.2 to 2.8 GPa and 1,380–1,480 °C. The experiments-produced liquids multiply saturated with spinel and garnet lherzolite phase assemblages (olivine, orthopyroxene, clinopyroxene and spinel ± garnet) under nominally anhydrous conditions. These SiO2-undersaturated liquids and published experimental data are utilized to develop a predictive model for garnet lherzolite melting of compositionally variable mantle under anhydrous conditions over the pressure range of 1.9–6 GPa. The model estimates the major element compositions of garnet-saturated melts for a range of mantle lherzolite compositions and predicts the conditions of the spinel to garnet lherzolite phase transition for natural peridotite compositions at above-solidus temperatures and pressures. We compare our predicted garnet lherzolite melts to those of pyroxenite and carbonated lherzolite and develop criteria for distinguishing among melts of these different source types. We also use the model in conjunction with a published predictive model for plagioclase and spinel lherzolite to characterize the differences in major element composition for melts in the plagioclase, spinel and garnet facies and develop tests to distinguish between melts of these three lherzolite facies based on major elements. The model is applied to understand the source materials and conditions of melting for high-K lavas erupted in the Tibetan plateau, basanite–nephelinite lavas erupted early in the evolution of Kilauea volcano, Hawaii, as well as younger tholeiitic to alkali lavas from Kilauea.

Design of the Helicity Injected Torus with Steady Inductive Helicity Injection (HIT-SI)

NASA Astrophysics Data System (ADS)

Sieck, P. E.; Gu, P.; Hamp, W. T.; Izzo, V. A.; McCollam, K. J.; Jarboe, T. R.; Nelson, B. A.; Redd, A. J.; Rogers, J. A.; Shumlak, U.

2000-10-01

Steady Inductive Helicity Injection (SIHI) is an inductive current drive method that injects helicity at a nearly constant rate, without open field lines, and without removing any helicity or magnetic energy from the plasma(T.R. Jarboe, Fusion Technology 36), p. 85, 1999. SIHI directly produces a rotating magnetic field structure, and the current profile is nearly time independent in the frame of the rotating field. The Helicity Injected Torus with SIHI (HIT-SI) is a ``bow tie'' spheromak designed to implement SIHI so that the current profile in the rotating frame is optimized. SIHI is accomplished using two inductive helicity injectors that operate 90^o out of phase with each other. Each helicity injector is a 180^o segment of a ZT-P size (a ≈ 8cm, R ≈ 32cm) RFP. The presence of a spheromak equilibrium will be readily apparent on several diagnostics, including the surface magnetic probes. The design of HIT-SI is presented, including the manufacturing techniques and metallurgical processes being used in the construction of the one-meter diameter close-fitting flux conserver. Several small prototype tests have been performed to prove the vacuum seal and electrical insulation capabilities of the design, and a finite element stress analysis of the flux conserver will be presented.

The role of subgrain boundaries in partial melting

NASA Astrophysics Data System (ADS)

Levine, Jamie S. F.; Mosher, Sharon; Rahl, Jeffrey M.

2016-08-01

Evidence for partial melting along subgrain boundaries in quartz and plagioclase is documented for rocks from the Lost Creek Gneiss of the Llano Uplift, central Texas, the Wet Mountains of central Colorado, and the Albany-Fraser Orogen, southwestern Australia. Domains of quartz or plagioclase crystals along subgrain boundaries are preferentially involved in partial melting over unstrained domains of these minerals. Material along subgrain boundaries in quartz and plagioclase has the same morphology as melt pseudomorphs present along grain boundaries and is commonly laterally continuous with this former grain boundary melt, indicating the material along subgrain boundaries can also be categorized as a melt pseudomorph. Subgrain boundaries consist of arrays of dislocations within a crystal lattice, and unlike fractures would not act as conduits for melt migration. Instead, the presence of former melt along subgrain boundaries requires that partial melting occurred in these locations because it is kinetically more favorable for melting reactions to occur there. Preferential melting in high strain locations may be attributed to strain energy, which provides a minor energetic contribution to the reaction and leads to preferential melting in locations with weakened bonds, and/or the presence of small quantities of water associated with dislocations, which may enhance diffusion rates or locally lower the temperature needed for partial melting.

Compact vacuum insulation

DOEpatents

Benson, D.K.; Potter, T.F.

1993-01-05

An ultra-thin compact vacuum insulation panel is comprised of two hard, but bendable metal wall sheets closely spaced apart from each other and welded around the edges to enclose a vacuum chamber. Glass or ceramic spacers hold the wall sheets apart. The spacers can be discrete spherical beads or monolithic sheets of glass or ceramic webs with nodules protruding therefrom to form essentially point'' or line'' contacts with the metal wall sheets. In the case of monolithic spacers that form line'' contacts, two such spacers with the line contacts running perpendicular to each other form effectively point'' contacts at the intersections. Corrugations accommodate bending and expansion, tubular insulated pipes and conduits, and preferred applications are also included.

Compact vacuum insulation

DOEpatents

Benson, David K.; Potter, Thomas F.

1993-01-01

An ultra-thin compact vacuum insulation panel is comprised of two hard, but bendable metal wall sheets closely spaced apart from each other and welded around the edges to enclose a vacuum chamber. Glass or ceramic spacers hold the wall sheets apart. The spacers can be discrete spherical beads or monolithic sheets of glass or ceramic webs with nodules protruding therefrom to form essentially "point" or "line" contacts with the metal wall sheets. In the case of monolithic spacers that form "line" contacts, two such spacers with the line contacts running perpendicular to each other form effectively "point" contacts at the intersections. Corrugations accommodate bending and expansion, tubular insulated pipes and conduits, and preferred applications are also included.

Investigating steam penetration using thermometric methods in dental handpieces with narrow internal lumens during sterilizing processes with non-vacuum or vacuum processes.

PubMed

Winter, S; Smith, A; Lappin, D; McDonagh, G; Kirk, B

2017-12-01

Dental handpieces are required to be sterilized between patient use. Vacuum steam sterilization processes with fractionated pre/post-vacuum phases or unique cycles for specified medical devices are required for hollow instruments with internal lumens to assure successful air removal. Entrapped air will compromise achievement of required sterilization conditions. Many countries and professional organizations still advocate non-vacuum sterilization processes for these devices. To investigate non-vacuum downward/gravity displacement, type-N steam sterilization of dental handpieces, using thermometric methods to measure time to achieve sterilization temperature at different handpiece locations. Measurements at different positions within air turbines were undertaken with thermocouples and data loggers. Two examples of widely used UK benchtop steam sterilizers were tested: a non-vacuum benchtop sterilizer (Little Sister 3; Eschmann, Lancing, UK) and a vacuum benchtop sterilizer (Lisa; W&H, Bürmoos, Austria). Each sterilizer cycle was completed with three handpieces and each cycle in triplicate. A total of 140 measurements inside dental handpiece lumens were recorded. The non-vacuum process failed (time range: 0-150 s) to reliably achieve sterilization temperatures within the time limit specified by the international standard (15 s equilibration time). The measurement point at the base of the handpiece failed in all test runs (N = 9) to meet the standard. No failures were detected with the vacuum steam sterilization type B process with fractionated pre-vacuum and post-vacuum phases. Non-vacuum downward/gravity displacement, type-N steam sterilization processes are unreliable in achieving sterilization conditions inside dental handpieces, and the base of the handpiece is the site most likely to fail. Copyright © 2017 The Healthcare Infection Society. Published by Elsevier Ltd. All rights reserved.

Impact Melt Emplacement on Mercury

NASA Astrophysics Data System (ADS)

Daniels, J. W.; Neish, C. D.

2018-05-01

This work proposes that fresh craters on rocky bodies may deposit impact melt externally ultimately according to the strength of its surface gravity, regardless of the body's surface topography and melt abundance.

Study on convection improvement of standard vacuum tube

NASA Astrophysics Data System (ADS)

He, J. H.; Du, W. P.; Qi, R. R.; He, J. X.

2017-11-01

For the standard all-glass vacuum tube collector, enhancing the vacuum tube axial natural convection can improve its thermal efficiency. According to the study of the standard all-glass vacuum tube, three kinds of guide plates which can inhibit the radial convection and increase axial natural convection are designed, and theory model is established. Experiments were carried out on vacuum tubes with three types of baffles and standard vacuum tubes without the improvement. The results show that T-type guide plate is better than that of Y-type guide plate on restraining convection and increasing axial radial convection effect, Y type is better than that of flat plate type, all guide plates are better than no change; the thermal efficiency of the tube was 2.6% higher than that of the unmodified standard vacuum tube. The efficiency of the system in the experiment can be increased by 3.1%.

21 CFR 864.9125 - Vacuum-assisted blood collection system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Vacuum-assisted blood collection system. 864.9125... Blood and Blood Products § 864.9125 Vacuum-assisted blood collection system. (a) Identification. A vacuum-assisted blood collection system is a device intended for medical purposes that uses a vacuum to...

21 CFR 864.9125 - Vacuum-assisted blood collection system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Vacuum-assisted blood collection system. 864.9125... Blood and Blood Products § 864.9125 Vacuum-assisted blood collection system. (a) Identification. A vacuum-assisted blood collection system is a device intended for medical purposes that uses a vacuum to...

21 CFR 864.9125 - Vacuum-assisted blood collection system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Vacuum-assisted blood collection system. 864.9125... Blood and Blood Products § 864.9125 Vacuum-assisted blood collection system. (a) Identification. A vacuum-assisted blood collection system is a device intended for medical purposes that uses a vacuum to...

21 CFR 864.9125 - Vacuum-assisted blood collection system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Vacuum-assisted blood collection system. 864.9125... Blood and Blood Products § 864.9125 Vacuum-assisted blood collection system. (a) Identification. A vacuum-assisted blood collection system is a device intended for medical purposes that uses a vacuum to...

21 CFR 864.9125 - Vacuum-assisted blood collection system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Vacuum-assisted blood collection system. 864.9125... Blood and Blood Products § 864.9125 Vacuum-assisted blood collection system. (a) Identification. A vacuum-assisted blood collection system is a device intended for medical purposes that uses a vacuum to...

Electrochemical studies in aluminum chloride melts

NASA Technical Reports Server (NTRS)

Osteryoung, R. A.

1971-01-01

A melt purification system was developed which produces a final melt far superior electrochemically than those previously reported. A residual current of less than 2 microamps/sq mn at a sweep rate of 0.5 V/sec was used as the criteria for a pure melt. The use of a second purified bulk melt and a heated pipette permitted the rapid exchange of working electrode compartments while retaining the same reference electrode system. The major portion of the work was carried out in the 1:1 AlCl3:NaCl melt at 175 and 200 C. Several measurements were made in the 2:1 melt and a few on the silver systems in intermediate compositions. Programs for PDP-8I and PDP-12 digital computers and the required electronic circuitry systems were developed to carry out various electrochemical measurements in the melt. A pair of 50 yard transmission lines were used to connect the computer to the experiment. Ensemble averaging and digital, least squares smoothing are used within the programs to improve the signal-to-noise ratio by at least an order of magnitude. Some of the computerized electrochemcial techniques used to examine the different systems were pulse polarography, double pulse polarography, staircase voltammetry, kinetic double potential step chronoamperometry and double potential step chronocoulometry.

14 CFR 25.1433 - Vacuum systems.

Code of Federal Regulations, 2014 CFR

2014-01-01

... 14 Aeronautics and Space 1 2014-01-01 2014-01-01 false Vacuum systems. 25.1433 Section 25.1433 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: TRANSPORT CATEGORY AIRPLANES Equipment Miscellaneous Equipment § 25.1433 Vacuum systems. There...

Icebergs Melting in Uniform and Vertically Sheared Flows

NASA Astrophysics Data System (ADS)

Cenedese, Claudia; Fitzmaurice, Anna; Straneo, Fiammetta

2017-11-01

Icebergs calving into Greenlandic Fjords frequently experience strongly sheared flows over their draft, but the impact of this flow past the iceberg on the melt plumes generated along the iceberg sides is not fully captured by existing melt parameterizations. A series of novel laboratory experiments showed that side melting of icebergs subject to relative velocities is controlled by two distinct regimes, which depend on the melt plume behavior (side-attached or side-detached). These two regimes produce a nonlinear dependence of melt rate on velocity, and different distributions of meltwater in the water column. Iceberg meltwater may either be confined to a thin surface layer, when the melt plumes are side-attached, or mixed down to the iceberg draft, when the melt plumes are side-detached. In a two-layer vertically sheared flow, the average flow speed in existing melt parameterizations gives an underestimate of the submarine melt rate, in part due to the nonlinearity of the dependence of melt rate on flow speed, but also because vertical shear in the velocity profile fundamentally changes the flow splitting around the ice block and consequently the velocity felt by the ice surface. Including this nonlinear velocity dependence in melting parameterizations applied to observed icebergs increases iceberg side melt in the side-attached regime, improving agreement with observations of iceberg submarine melt rates. AF was supported by NA14OAR4320106, CC by NSF OCE-1434041 and OCE-1658079, and FS by NSF PLR-1332911 and OCE-1434041.

Numerical simulation of hot-melt extrusion processes for amorphous solid dispersions using model-based melt viscosity.

PubMed

Bochmann, Esther S; Steffens, Kristina E; Gryczke, Andreas; Wagner, Karl G

2018-03-01

Simulation of HME processes is a valuable tool for increased process understanding and ease of scale-up. However, the experimental determination of all required input parameters is tedious, namely the melt rheology of the amorphous solid dispersion (ASD) in question. Hence, a procedure to simplify the application of hot-melt extrusion (HME) simulation for forming amorphous solid dispersions (ASD) is presented. The commercial 1D simulation software Ludovic ® was used to conduct (i) simulations using a full experimental data set of all input variables including melt rheology and (ii) simulations using model-based melt viscosity data based on the ASDs glass transition and the physical properties of polymeric matrix only. Both types of HME computation were further compared to experimental HME results. Variation in physical properties (e.g. heat capacity, density) and several process characteristics of HME (residence time distribution, energy consumption) among the simulations and experiments were evaluated. The model-based melt viscosity was calculated by using the glass transition temperature (T g ) of the investigated blend and the melt viscosity of the polymeric matrix by means of a T g -viscosity correlation. The results of measured melt viscosity and model-based melt viscosity were similar with only few exceptions, leading to similar HME simulation outcomes. At the end, the experimental effort prior to HME simulation could be minimized and the procedure enables a good starting point for rational development of ASDs by means of HME. As model excipients, Vinylpyrrolidone-vinyl acetate copolymer (COP) in combination with various APIs (carbamazepine, dipyridamole, indomethacin, and ibuprofen) or polyethylene glycol (PEG 1500) as plasticizer were used to form the ASDs. Copyright © 2017 Elsevier B.V. All rights reserved.

Researches on Position Detection for Vacuum Switch Electrode

NASA Astrophysics Data System (ADS)

Dong, Huajun; Guo, Yingjie; Li, Jie; Kong, Yihan

2018-03-01

Form and transformation character of vacuum arc is important influencing factor on the vacuum switch performance, and the dynamic separations of electrode is the chief effecting factor on the transformation of vacuum arcs forms. Consequently, how to detect the position of electrode to calculate the separations in the arcs image is of great significance. However, gray level distribution of vacuum arcs image isn’t even, the gray level of burning arcs is high, but the gray level of electrode is low, meanwhile, the forms of vacuum arcs changes sharply, the problems above restrict electrode position detection precisely. In this paper, algorithm of detecting electrode position base on vacuum arcs image was proposed. The digital image processing technology was used in vacuum switch arcs image analysis, the upper edge and lower edge were detected respectively, then linear fitting was done using the result of edge detection, the fitting result was the position of electrode, thus, accurate position detection of electrode was realized. From the experimental results, we can see that: algorithm described in this paper detected upper and lower edge of arcs successfully and the position of electrode was obtained through calculation.

Advanced Photon Source accelerator ultrahigh vacuum guide