Design of a normal incidence multilayer imaging X-ray microscope

NASA Astrophysics Data System (ADS)

Shealy, David L.; Gabardi, David R.; Hoover, Richard B.; Walker, Arthur B. C., Jr.; Lindblom, Joakim F.

Normal incidence multilayer Cassegrain X-ray telescopes were flown on the Stanford/MSFC Rocket X-ray Spectroheliograph. These instruments produced high spatial resolution images of the sun and conclusively demonstrated that doubly reflecting multilayer X-ray optical systems are feasible. The images indicated that aplanatic imaging soft X-ray/EUV microscopes should be achievable using multilayer optics technology. A doubly reflecting normal incidence multilayer imaging X-ray microscope based on the Schwarzschild configuration has been designed. The design of the microscope and the results of the optical system ray trace analysis are discussed. High resolution aplanatic imaging X-ray microscopes using normal incidence multilayer X-ray mirrors should have many important applications in advanced X-ray astronomical instrumentation, X-ray lithography, biological, biomedical, metallurgical, and laser fusion research.

Continuing data analysis of the AS/E grazing incidence X-ray telescope experiment on the OSO-4 satellite

NASA Technical Reports Server (NTRS)

Vaiana, G.; Haggerty, R.; Kahler, S.; Krieger, A.; Landini, M.; Timothy, A.; Webb, D.

1973-01-01

The work to correct and extend the calculation of the theoretical solar X-ray spectrum produced during earlier OSO-4 data analysis is reported along with the work to formulate models of active regions, and compare these models with the experimental values. An atlas of solar X-ray photographs is included, and solar X-ray observations are correlated with the solar wind.

[Study on spectrum analysis of X-ray based on rotational mass effect in special relativity].

PubMed

Yu, Zhi-Qiang; Xie, Quan; Xiao, Qing-Quan

2010-04-01

Based on special relativity, the formation mechanism of characteristic X-ray has been studied, and the influence of rotational mass effect on X-ray spectrum has been given. A calculation formula of the X-ray wavelength based upon special relativity was derived. Error analysis was carried out systematically for the calculation values of characteristic wavelength, and the rules of relative error were obtained. It is shown that the values of the calculation are very close to the experimental values, and the effect of rotational mass effect on the characteristic wavelength becomes more evident as the atomic number increases. The result of the study has some reference meaning for the spectrum analysis of characteristic X-ray in application.

The BL LAC phenomenon: X-ray observations of transition objects and determination of the x-ray spectrum of a complete sample of flat-spectrum radio sources

NASA Technical Reports Server (NTRS)

Worrall, Diana M.

1994-01-01

This report summarizes the activities related to two ROSAT investigations: (1) x-ray properties of radio galaxies thought to contain BL Lac type nuclei; and (2) x-ray spectra of a complete sample of flat-spectrum radio sources. The following papers describing the research are provided as attachments: Multiple X-ray Emission Components in Low Power Radio Galaxies; New X-ray Results on Radio Galaxies; Analysis Techniques for a Multiwavelength Study of Radio Galaxies; Separation of X-ray Emission Components in Radio Galaxies; X-ray Emission in Powerful Radio Galaxies and Quasars; Extended and Compact X-ray Emission in Powerful Radio Galaxies; and X-ray Spectra of a Complete Sample of Extragalactic Core-dominated Radio Sources.

The Chandra Source Catalog

NASA Astrophysics Data System (ADS)

Evans, Ian; Primini, Francis A.; Glotfelty, Kenny J.; Anderson, Craig S.; Bonaventura, Nina R.; Chen, Judy C.; Davis, John E.; Doe, Stephen M.; Evans, Janet D.; Fabbiano, Giuseppina; Galle, Elizabeth C.; Gibbs, Danny G., II; Grier, John D.; Hain, Roger; Hall, Diane M.; Harbo, Peter N.; He, Xiang Qun (Helen); Houck, John C.; Karovska, Margarita; Kashyap, Vinay L.; Lauer, Jennifer; McCollough, Michael L.; McDowell, Jonathan C.; Miller, Joseph B.; Mitschang, Arik W.; Morgan, Douglas L.; Mossman, Amy E.; Nichols, Joy S.; Nowak, Michael A.; Plummer, David A.; Refsdal, Brian L.; Rots, Arnold H.; Siemiginowska, Aneta L.; Sundheim, Beth A.; Tibbetts, Michael S.; van Stone, David W.; Winkelman, Sherry L.; Zografou, Panagoula

2009-09-01

The first release of the Chandra Source Catalog (CSC) was published in 2009 March, and includes information about 94,676 X-ray sources detected in a subset of public ACIS imaging observations from roughly the first eight years of the Chandra mission. This release of the catalog includes point and compact sources with observed spatial extents <˜30''.The CSC is a general purpose virtual X-ray astrophysics facility that provides access to a carefully selected set of generally useful quantities for individual X-ray sources, and is designed to satisfy the needs of a broad-based group of scientists, including those who may be less familiar with astronomical data analysis in the X-ray regime.The catalog (1) provides access to the best estimates of the X-ray source properties for detected sources, with good scientific fidelity, and directly supports medium sophistication scientific analysis on using the individual source data; (2) facilitates analysis of a wide range of statistical properties for classes of X-ray sources; (3) provides efficient access to calibrated observational data and ancillary data products for individual X-ray sources, so that users can perform detailed further analysis using existing tools; and (4) includes real X-ray sources detected with flux significance greater than a predefined threshold, while maintaining the number of spurious sources at an acceptable level. For each detected X-ray source, the CSC provides commonly tabulated quantities, including source position, extent, multi-band fluxes, hardness ratios, and variability statistics, derived from the observations in which the source is detected. In addition to these traditional catalog elements, for each X-ray source the CSC includes an extensive set of file-based data products that can be manipulated interactively, including source images, event lists, light curves, and spectra from each observation in which a source is detected.

Investigating the galactic Supernova Remnant Kes 78 with XMM-Newton

NASA Astrophysics Data System (ADS)

Miceli, M.; Bamba, A.; Orlando, S.; Bocchino, F.

2016-06-01

The galactic supernova remnant Kes 78 is associated with a HESS gamma-ray source and its X-ray emission has been recently revealed by Suzaku observations which have found indications for a hard X-ray component in the spectra. We analyzed an XMM-Newton EPIC observation of Kes 78 and studied the spatial distribution of the physical and chemical properties of the X-ray emitting plasma. The EPIC data unveiled a very complex morphology for the soft X-ray emission. We performed image analysis and spatially resolved spectral analysis finding indications for the interaction of the remnant with a local molecular cloud. Finally, we investigated the origin of the hard X-ray emitting component.

Investigating the Galactic supernova remnant Kes 78 with XMM-Newton

NASA Astrophysics Data System (ADS)

Miceli, Marco; Bamba, Aya; Orlando, Salvatore; Bocchino, Fabrizio

2016-06-01

The galactic supernova remnant Kes 78 is associated with a HESS gamma-ray source and its X-ray emission has been recently revealed by Suzaku observations which have found indications for a hard X-ray component in the spectra. We analyzed an XMM-Newton EPIC observation of Kes 78 and studied the spatial distribution of the physical and chemical properties of the X-ray emitting plasma. The EPIC data unveiled a very complex morphology for the soft X-ray emission. We performed image analysis and spatially resolved spectral analysis finding indications for the interaction of the remnant with a local molecular cloud. Finally, we investigated the origin of the hard X-ray emitting component.

Microanalysis of iron oxidation state in iron oxides using X Ray Absorption Near Edge Structure (XANES)

NASA Technical Reports Server (NTRS)

Sutton, S. R.; Delaney, J.; Bajt, S.; Rivers, M. L.; Smith, J. V.

1993-01-01

An exploratory application of x ray absorption near edge structure (XANES) analysis using the synchrotron x ray microprobe was undertaken to obtain Fe XANES spectra on individual sub-millimeter grains in conventional polished sections. The experiments concentrated on determinations of Fe valence in a suite of iron oxide minerals for which independent estimates of the iron speciation could be made by electron microprobe analysis and x ray diffraction.

Simulating x-ray telescopes with McXtrace: a case study of ATHENA's optics

NASA Astrophysics Data System (ADS)

Ferreira, Desiree D. M.; Knudsen, Erik B.; Westergaard, Niels J.; Christensen, Finn E.; Massahi, Sonny; Shortt, Brian; Spiga, Daniele; Solstad, Mathias; Lefmann, Kim

2016-07-01

We use the X-ray ray-tracing package McXtrace to simulate the performance of X-ray telescopes based on Silicon Pore Optics (SPO) technologies. We use as reference the design of the optics of the planned X-ray mission Advanced Telescope for High ENergy Astrophysics (ATHENA) which is designed as a single X-ray telescope populated with stacked SPO substrates forming mirror modules to focus X-ray photons. We show that is possible to simulate in detail the SPO pores and qualify the use of McXtrace for in-depth analysis of in-orbit performance and laboratory X-ray test results.

21 CFR 892.1660 - Non-image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Non-image-intensified fluoroscopic x-ray system... fluoroscopic x-ray system. (a) Identification. A non-image-intensified fluoroscopic x-ray system is a device... of x-radiation into a visible image. This generic type of device may include signal analysis and...

21 CFR 892.1660 - Non-image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Non-image-intensified fluoroscopic x-ray system... fluoroscopic x-ray system. (a) Identification. A non-image-intensified fluoroscopic x-ray system is a device... of x-radiation into a visible image. This generic type of device may include signal analysis and...

Empirical studies of solar flares: Comparison of X-ray and H alpha filtergrams and analysis of the energy balance of the X-ray plasma

NASA Technical Reports Server (NTRS)

Moore, R. L.

1979-01-01

The physics of solar flares was investigated through a combined analysis of X-ray filtergrams of the high temperature coronal component of flares and H alpha filtergrams of the low temperature chromospheric component. The data were used to study the magnetic field configuration and its changes in solar flares, and to examine the chromospheric location and structure of X-ray bright points (XPB) and XPB flares. Each topic and the germane data are discussed. The energy balance of the thermal X-ray plasma in flares, while not studied, is addressed.

VETA-I x ray test analysis

NASA Technical Reports Server (NTRS)

Brissenden, R. J. V.; Chartas, G.; Freeman, M. D.; Hughes, J. P.; Kellogg, E. M.; Podgorski, W. A.; Schwartz, D. A.; Zhao, P.

1992-01-01

This interim report presents some definitive results from our analysis of the VETA-I x-ray testing data. It also provides a description of the hardware and software used in the conduct of the VETA-I x-ray test program performed at the MSFC x-ray Calibration Facility (XRCF). These test results also serve to supply data and information to include in the TRW final report required by DPD 692, DR XC04. To provide an authoritative compendium of results, we have taken nine papers as published in the SPIE Symposium, 'Grazing Incidence X-ray/EUV Optics for Astronomy and Projection Lithography' and have reproduced them as the content of this report.

Advances toward submicron resolution optics for x-ray instrumentation and applications

NASA Astrophysics Data System (ADS)

Cordier, Mark; Stripe, Benjamin; Yun, Wenbing; Lau, S. H.; Lyon, Alan; Reynolds, David; Lewis, Sylvia J. Y.; Chen, Sharon; Semenov, Vladimir A.; Spink, Richard I.; Seshadri, Srivatsan

2017-08-01

Sigray's axially symmetric x-ray optics enable advanced microanalytical capabilities for focusing x-rays to microns-scale to submicron spot sizes, which can potentially unlock many avenues for laboratory micro-analysis. The design of these optics allows submicron spot sizes even at low x-ray energies, enabling research into low atomic number elements and allows increased sensitivity of grazing incidence measurements and surface analysis. We will discuss advances made in the fabrication of these double paraboloidal mirror lenses designed for use in laboratory x-ray applications. We will additionally present results from as-built paraboloids, including surface figure error and focal spot size achieved to-date.

Local x-ray structure analysis of optically manipulated biological micro-objects

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cojoc, Dan; Ferrari, Enrico; Santucci, Silvia C.

2010-12-13

X-ray diffraction using micro- and nanofocused beams is well suited for nanostructure analysis at different sites of a biological micro-object. To conduct in vitro studies without mechanical contact, we developed object manipulation by optical tweezers in a microfluidic cell. Here we report x-ray microdiffraction analysis of a micro-object optically trapped in three dimensions. We revealed the nanostructure of a single starch granule at different points and investigated local radiation damage induced by repeated x-ray exposures at the same position, demonstrating high stability and full control of the granule orientation by multiple optical traps.

X-ray elemental mapping techniques for elucidating the ecophysiology of hyperaccumulator plants.

PubMed

van der Ent, Antony; Przybyłowicz, Wojciech J; de Jonge, Martin D; Harris, Hugh H; Ryan, Chris G; Tylko, Grzegorz; Paterson, David J; Barnabas, Alban D; Kopittke, Peter M; Mesjasz-Przybyłowicz, Jolanta

2018-04-01

Contents Summary 432 I. Introduction 433 II. Preparation of plant samples for X-ray micro-analysis 433 III. X-ray elemental mapping techniques 438 IV. X-ray data analysis 442 V. Case studies 443 VI. Conclusions 446 Acknowledgements 449 Author contributions 449 References 449 SUMMARY: Hyperaccumulators are attractive models for studying metal(loid) homeostasis, and probing the spatial distribution and coordination chemistry of metal(loid)s in their tissues is important for advancing our understanding of their ecophysiology. X-ray elemental mapping techniques are unique in providing in situ information, and with appropriate sample preparation offer results true to biological conditions of the living plant. The common platform of these techniques is a reliance on characteristic X-rays of elements present in a sample, excited either by electrons (scanning/transmission electron microscopy), protons (proton-induced X-ray emission) or X-rays (X-ray fluorescence microscopy). Elucidating the cellular and tissue-level distribution of metal(loid)s is inherently challenging and accurate X-ray analysis places strict demands on sample collection, preparation and analytical conditions, to avoid elemental redistribution, chemical modification or ultrastructural alterations. We compare the merits and limitations of the individual techniques, and focus on the optimal field of applications for inferring ecophysiological processes in hyperaccumulator plants. X-ray elemental mapping techniques can play a key role in answering questions at every level of metal(loid) homeostasis in plants, from the rhizosphere interface, to uptake pathways in the roots and shoots. Further improvements in technological capabilities offer exciting perspectives for the study of hyperaccumulator plants into the future. © 2017 University of Queensland. New Phytologist © 2017 New Phytologist Trust.

Chemical speciation using high energy resolution PIXE spectroscopy in the tender X-ray range

NASA Astrophysics Data System (ADS)

Kavčič, Matjaž; Petric, Marko; Vogel-Mikuš, Katarina

2018-02-01

High energy resolution X-ray emission spectroscopy employing wavelength dispersive (WDS) crystal spectrometers can provide energy resolution on the level of core-hole lifetime broadening of the characteristic emission lines. While crystal spectrometers have been traditionally used in combination with electron excitation for major and minor element analysis, they have been rarely considered in proton induced X-ray emission (PIXE) trace element analysis mainly due to low detection efficiency. Compared to the simplest flat crystal WDS spectrometer the efficiency can be improved by employing cylindrically or even spherically curved crystals in combination with position sensitive X-ray detectors. When such spectrometer is coupled to MeV proton excitation, chemical bonding effects are revealed in the high energy resolution spectra yielding opportunity to extend the analytical capabilities of PIXE technique also towards chemical state analysis. In this contribution we will focus on the high energy resolution PIXE (HR-PIXE) spectroscopy in the tender X-ray range performed in our laboratory with our home-built tender X-ray emission spectrometer. Some general properties of high energy resolution PIXE spectroscopy in the tender X-ray range are presented followed by an example of sulfur speciation in biological tissue illustrating the capabilities as well as limitations of HR-PIXE method used for chemical speciation in the tender X-ray range.

Analysis of solar X-ray data

NASA Technical Reports Server (NTRS)

Teske, R. G.

1972-01-01

Type III solar bursts occurring in the absence of solar flares were observed to be accompanied by weak X-radiation. The energy scale of an OSO-3 soft X-ray ion chamber was assessed using realistic theoretical X-ray spectra. Relationships between soft solar X-rays and solar activity were investigated. These included optical studies, the role of the Type III acceleration mechanism in establishing the soft X-ray source volume, H alpha flare intensity variations, and gross magnetic field structure.

ID16B: a hard X-ray nanoprobe beamline at the ESRF for nano-analysis

PubMed Central

Martínez-Criado, Gema; Villanova, Julie; Tucoulou, Rémi; Salomon, Damien; Suuronen, Jussi-Petteri; Labouré, Sylvain; Guilloud, Cyril; Valls, Valentin; Barrett, Raymond; Gagliardini, Eric; Dabin, Yves; Baker, Robert; Bohic, Sylvain; Cohen, Cédric; Morse, John

2016-01-01

Within the framework of the ESRF Phase I Upgrade Programme, a new state-of-the-art synchrotron beamline ID16B has been recently developed for hard X-ray nano-analysis. The construction of ID16B was driven by research areas with major scientific and societal impact such as nanotechnology, earth and environmental sciences, and bio-medical research. Based on a canted undulator source, this long beamline provides hard X-ray nanobeams optimized mainly for spectroscopic applications, including the combination of X-ray fluorescence, X-ray diffraction, X-ray excited optical luminescence, X-ray absorption spectroscopy and 2D/3D X-ray imaging techniques. Its end-station re-uses part of the apparatus of the earlier ID22 beamline, while improving and enlarging the spectroscopic capabilities: for example, the experimental arrangement offers improved lateral spatial resolution (∼50 nm), a larger and more flexible capability for in situ experiments, and monochromatic nanobeams tunable over a wider energy range which now includes the hard X-ray regime (5–70 keV). This paper describes the characteristics of this new facility, short-term technical developments and the first scientific results. PMID:26698084

X-Ray Processing of ChaMPlane Fields: Methods and Initial Results for Selected Anti-Galactic Center Fields

NASA Astrophysics Data System (ADS)

Hong, JaeSub; van den Berg, Maureen; Schlegel, Eric M.; Grindlay, Jonathan E.; Koenig, Xavier; Laycock, Silas; Zhao, Ping

2005-12-01

We describe the X-ray analysis procedure of the ongoing Chandra Multiwavelength Plane (ChaMPlane) Survey and report the initial results from the analysis of 15 selected anti-Galactic center observations (90deg

Long-term variability in bright hard X-ray sources: 5+ years of BATSE data

NASA Technical Reports Server (NTRS)

Robinson, C. R.; Harmon, B. A.; McCollough, M. L.; Paciesas, W. S.; Sahi, M.; Scott, D. M.; Wilson, C. A.; Zhang, S. N.; Deal, K. J.

1997-01-01

The operation of the Compton Gamma Ray Observatory (CGRO)/burst and transient source experiment (BATSE) continues to provide data for inclusion into a data base for the analysis of long term variability in bright, hard X-ray sources. The all-sky capability of BATSE provides up to 30 flux measurements/day for each source. The long baseline and the various rising and setting occultation flux measurements allow searches for periodic and quasi-periodic signals with periods of between several hours to hundreds of days to be conducted. The preliminary results from an analysis of the hard X-ray variability in 24 of the brightest BATSE sources are presented. Power density spectra are computed for each source and profiles are presented of the hard X-ray orbital modulations in some X-ray binaries, together with amplitude modulations and variations in outburst durations and intensities in recurrent X-ray transients.

Research in Solar Physics: Analysis of Skylab/ATM S-056 X-Ray Data

NASA Technical Reports Server (NTRS)

Henze, W., Jr.

1977-01-01

Data obtained by the X-ray event analyzer are described as well as methods used for film calibration. Topics discussed include analyses of the 15 June 1973 flare, oscillations in the solar soft X-ray flux, and deconvolution of X-ray images of the 5 September 1973 flare.

Extracting chemical information from high-resolution Kβ X-ray emission spectroscopy

NASA Astrophysics Data System (ADS)

Limandri, S.; Robledo, J.; Tirao, G.

2018-06-01

High-resolution X-ray emission spectroscopy allows studying the chemical environment of a wide variety of materials. Chemical information can be obtained by fitting the X-ray spectra and observing the behavior of some spectral features. Spectral changes can also be quantified by means of statistical parameters calculated by considering the spectrum as a probability distribution. Another possibility is to perform statistical multivariate analysis, such as principal component analysis. In this work the performance of these procedures for extracting chemical information in X-ray emission spectroscopy spectra for mixtures of Mn2+ and Mn4+ oxides are studied. A detail analysis of the parameters obtained, as well as the associated uncertainties is shown. The methodologies are also applied for Mn oxidation state characterization of double perovskite oxides Ba1+xLa1-xMnSbO6 (with 0 ≤ x ≤ 0.7). The results show that statistical parameters and multivariate analysis are the most suitable for the analysis of this kind of spectra.

Non-destructive elemental analysis of a carbonaceous chondrite with direct current Muon beam at MuSIC.

PubMed

Terada, K; Sato, A; Ninomiya, K; Kawashima, Y; Shimomura, K; Yoshida, G; Kawai, Y; Osawa, T; Tachibana, S

2017-11-13

Electron- or X-ray-induced characteristic X-ray analysis has been widely used to determine chemical compositions of materials in vast research fields. In recent years, analysis of characteristic X-rays from muonic atoms, in which a muon is captured, has attracted attention because both a muon beam and a muon-induced characteristic X-ray have high transmission abilities. Here we report the first non-destructive elemental analysis of a carbonaceous chondrite using one of the world-leading intense direct current muon beam source (MuSIC; MUon Science Innovative Channel). We successfully detected characteristic muonic X-rays of Mg, Si, Fe, O, S and C from Jbilet Winselwan CM chondrite, of which carbon content is about 2 wt%, and the obtained elemental abundance pattern was consistent with that of CM chondrites. Because of its high sensitivity to carbon, non-destructive elemental analysis with a muon beam can be a novel powerful tool to characterize future retuned samples from carbonaceous asteroids.

Fixture for supporting and aligning a sample to be analyzed in an x-ray diffraction apparatus

DOEpatents

Green, L.A.; Heck, J.L. Jr.

1985-04-23

A fixture is provided for supporting and aligning small samples of material on a goniometer for x-ray diffraction analysis. A sample-containing capillary is accurately positioned for rotation in the x-ray beam by selectively adjusting the fixture to position the capillary relative to the x and y axes thereof to prevent wobble and position the sample along the z axis or the axis of rotation. By employing the subject fixture relatively small samples of materials can be analyzed in an x-ray diffraction apparatus previously limited to the analysis of much larger samples.

Fixture for supporting and aligning a sample to be analyzed in an X-ray diffraction apparatus

DOEpatents

Green, Lanny A.; Heck, Jr., Joaquim L.

1987-01-01

A fixture is provided for supporting and aligning small samples of material on a goniometer for X-ray diffraction analysis. A sample-containing capillary is accurately positioned for rotation in the X-ray beam by selectively adjusting the fixture to position the capillary relative to the x and y axes thereof to prevent wobble and position the sample along the z axis or the axis of rotation. By employing the subject fixture relatively small samples of materials can be analyzed in an X-ray diffraction apparatus previously limited to the analysis of much larger samples.

Application of an X-ray Fluorescence Instrument to Helicopter Wear Debris Analysis

DTIC Science & Technology

2008-04-01

from magnesium (Mg) to uranium (U) using two X-ray detection sensors: a FOCUS 5+ detector AlX-ray tube X-ray Detector 1. Incident X-ray...zinc (Zn), whilst the PIN detector is used to detect elements from calcium (Ca) to uranium (U) [4]. Elements between calcium (Ca) to zinc (Zn) can be... carbide paper, however polishing is not a normal sample preparation requirement for the Twin-X (see Figure 16). The samples were placed polished side

Lead foil in dental X-ray film: Backscattering rejection or image intensifier?

NASA Astrophysics Data System (ADS)

Hönnicke, M. G.; Delben, G. J.; Godoi, W. C.; Swinka-Filho, V.

2014-11-01

Dental X-ray films are still largely used due to sterilization issues, simplicity and, mainly, economic reasons. These films almost always are double coated (double emulsion) and have a lead foil in contact with the film for X-ray backscattering rejection. Herein we explore the use of the lead foil as an image intensifier. In these studies, spatial resolution was investigated when images were acquired on the dental X-ray films with and without the lead foil. Also, the lead foil was subjected to atomic analysis (fluorescent measurements) and structure analysis (X-ray diffraction). We determined that the use of the lead foil reduces the exposure time, however, does not affect the spatial resolution on the acquired images. This suggests that the fluorescent radiation spread is smaller than the grain sizes of the dental X-ray films.

X-ray observations of LMC X-3 with the monitor proportional counter aboard the HEAO 2 Einstein observatory - A comparison with Cygnus X-1

NASA Technical Reports Server (NTRS)

Weisskopf, M. C.; Darbro, W. A.; Elsner, R. F.; Williams, A. C.; Kahn, S. M.; Grindlay, J. E.; Naranan, S.; Sutherland, P. G.

1983-01-01

A comparison is presented of the black hole candidates LMC X-3 and Cygnus X-1 based on Einstein observations of LMC X-3 with the monitor proportional counter. A spectral analysis shows LMC X-3 to be more like the typical bright galactic X-ray source than Cygnus X-1. A search for periodic pulsations over a period range from 0.2 ms to over 1000 s set upper limits at the 90 percent confidence level of the order of 10 percent. An analysis of the aperiodic variability of LMC X-3 shows none of the shot noise behavior characteristic of Cygnus X-1. The absence of distinctive X-ray properties common to both sources suggests that the identification of black hole candidates on the basis of X-ray properties similar to Cygnus X-1 (or LMC X-3) is not reliable.

Characterization of ceramic powders by an X-ray measuring method

NASA Technical Reports Server (NTRS)

Ziegler, B.

1983-01-01

X-ray line broadening analysis gives quantitative data on structural changes of ceramic powders after different processing steps. Various Al2O3 powders were investigated and the following points are discussed on the basis of these results: X-ray line broadening analysis, structural changes during grinding, structural changes during annealing, influence of structural properties on sintering behavior and application of line broadening analysis to quality control of powders.

Reconstitution of SNARE proteins into solid-supported lipid bilayer stacks and X-ray structure analysis.

PubMed

Xu, Yihui; Kuhlmann, Jan; Brennich, Martha; Komorowski, Karlo; Jahn, Reinhard; Steinem, Claudia; Salditt, Tim

2018-02-01

SNAREs are known as an important family of proteins mediating vesicle fusion. For various biophysical studies, they have been reconstituted into supported single bilayers via proteoliposome adsorption and rupture. In this study we extended this method to the reconstitution of SNAREs into supported multilamellar lipid membranes, i.e. oriented multibilayer stacks, as an ideal model system for X-ray structure analysis (X-ray reflectivity and diffraction). The reconstitution was implemented through a pathway of proteomicelle, proteoliposome and multibilayer. To monitor the structural evolution in each step, we used small-angle X-ray scattering for the proteomicelles and proteoliposomes, followed by X-ray reflectivity and grazing-incidence small-angle scattering for the multibilayers. Results show that SNAREs can be successfully reconstituted into supported multibilayers, with high enough orientational alignment for the application of surface sensitive X-ray characterizations. Based on this protocol, we then investigated the effect of SNAREs on the structure and phase diagram of the lipid membranes. Beyond this application, this reconstitution protocol could also be useful for X-ray analysis of many further membrane proteins. Copyright © 2017 Elsevier B.V. All rights reserved.

Skylab ATM/S-056 X-ray event analyzer: Instrument description, parameter determination, and analysis example (15 June 1973 1B/M3 flare)

NASA Technical Reports Server (NTRS)

Wilson, R. M.

1976-01-01

The Skylab ATM/S-056 X-Ray Event Analyzer, part of an X-ray telescope experiment, is described. The techniques employed in the analysis of its data to determine electron temperatures and emission measures are reviewed. The analysis of a sample event - the 15 June 1973 1B/M3 flare - is performed. Comparison of the X-Ray Event Analyzer data with that of the SolRad 9 observations indicates that the X-Ray Event Analyzer accurately monitored the sun's 2.5 to 7.25 A X-ray emission and to a lesser extent the 6.1 to 20 A emission. A mean average peak temperature of 15 million K at 1,412 UT and a mean average peak electron density (assuming a flare volume of 10 to the 13 power cu km) of 27 million/cu mm at 1,416 to 1,417 UT are deduced for the event. The X-Ray Event Analyzer data, having a 2.5 s time resolution, should be invaluable in comparisons with other high-time resolution data (e.g., radio bursts).

Data reduction and analysis for the graphite crystal X-ray spectrometer and polarimeter experiment flown aboard OSO-8 spacecraft

NASA Technical Reports Server (NTRS)

Novick, R.

1980-01-01

The documentation and software programs developed for the reception, initial processing (quickbook), and production analysis of data obtained by solar X-ray spectroscopy, stellar spectroscopy, and X-ray polarimetry experiments on OSO-8 are listed. The effectiveness and sensitivity of the Bragg crystal scattering instruments used are assessed. The polarization data polarimetric data obtained shows that some X-ray sources are polarized and that a larger polarimeter of this type is required to perform the measurements necessary to fully understand the physics of X-ray sources. The scanning Bragg crystal spectrometer was ideally suited for studying rapidly changing solar conditions. Observations of the Crab Nebula and pulsar, Cyg X-1, Cyg X-2, Cyg X-3, Sco X-1, Cen X-3, and Her X-1 are discussed as well as of 4U1656-53 and 4U1820-30. Evidence was obtained for iron line emission from Cyg X-3.

Portable total reflection x-ray fluorescence analysis in the identification of unknown laboratory hazards

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liu, Ying, E-mail: liu.ying.48r@st.kyoto-u.ac.jp; Imashuku, Susumu; Sasaki, Nobuharu

In this study, a portable total reflection x-ray fluorescence (TXRF) spectrometer was used to analyze unknown laboratory hazards that precipitated on exterior surfaces of cooling pipes and fume hood pipes in chemical laboratories. With the aim to examine the accuracy of TXRF analysis for the determination of elemental composition, analytical results were compared with those of wavelength-dispersive x-ray fluorescence spectrometry, scanning electron microscope and energy-dispersive x-ray spectrometry, energy-dispersive x-ray fluorescence spectrometry, inductively coupled plasma atomic emission spectrometry, x-ray diffraction spectrometry (XRD), and x-ray photoelectron spectroscopy (XPS). Detailed comparison of data confirmed that the TXRF method itself was not sufficient tomore » determine all the elements (Z > 11) contained in the samples. In addition, results suggest that XRD should be combined with XPS in order to accurately determine compound composition. This study demonstrates that at least two analytical methods should be used in order to analyze the composition of unknown real samples.« less

Effects of X-ray irradiation on the Eu3+ → Eu2+ conversion in CaAl2O4 phosphors

NASA Astrophysics Data System (ADS)

Gomes, Manassés A.; Carvalho, Jéssica C.; Andrade, Adriano B.; Rezende, Marcos V.; Macedo, Zélia S.; Valerio, Mário E. G.

2018-01-01

This paper reports structural and luminescence properties of Eu-doped CaAl2O4 produced by an alternative sol-gel method using coconut water. Results of differential thermal analysis (DTA), thermogravimetric analysis (TGA), and X-ray diffraction (XRD) allowed us to identify the best synthesis conditions for sample preparation. Simultaneous measurements of X-ray absorption spectroscopy (XAS) and X-ray excited optical luminescence (XEOL) were also performed in the X-ray energy range of the Eu LIII edge. Results from photoluminescence (PL) showed only the characteristic Eu3+ emission. However, radioluminescence emission spectra from Eu-doped CaAl2O4 shows a process of conversion of Eu3+ to Eu2+, which is induced by X-ray irradiation and is dependent on the radiation dose energy. X-ray absorption near edge structure (XANES) measurements corroborate Eu reduction due to irradiation, showing that only the Eu3+ ion is present in stable form in the CaAl2O4.

HEAO-1 analysis of Low Energy Detectors (LED)

NASA Technical Reports Server (NTRS)

Nousek, John A.

1992-01-01

The activities at Penn State University are described. During the period Oct. 1990 to Dec. 1991 work on HEAO-1 analysis of the Low Energy Detectors (LED) concentrated on using the improved detector spectral simulation model and fitting diffuse x-ray background spectral data. Spectral fitting results, x-ray point sources, and diffuse x-ray sources are described.

Imaging local electric fields produced upon synchrotron X-ray exposure

DOE PAGES

Dettmar, Christopher M.; Newman, Justin A.; Toth, Scott J.; ...

2014-12-31

Electron–hole separation following hard X-ray absorption during diffraction analysis of soft materials under cryogenic conditions produces substantial local electric fields visualizable by second harmonic generation (SHG) microscopy. Monte Carlo simulations of X-ray photoelectron trajectories suggest the formation of substantial local electric fields in the regions adjacent to those exposed to X-rays, indicating a possible electric-field–induced SHG (EFISH) mechanism for generating the observed signal. In studies of amorphous vitreous solvents, analysis of the SHG spatial profiles following X-ray microbeam exposure was consistent with an EFISH mechanism. Within protein crystals, exposure to 12-keV (1.033-Å) X-rays resulted in increased SHG in the regionmore » extending ~3 μm beyond the borders of the X-ray beam. Moderate X-ray exposures typical of those used for crystal centering by raster scanning through an X-ray beam were sufficient to produce static electric fields easily detectable by SHG. The X-ray–induced SHG activity was observed with no measurable loss for longer than 2 wk while maintained under cryogenic conditions, but disappeared if annealed to room temperature for a few seconds. In conclusion, these results provide direct experimental observables capable of validating simulations of X-ray–induced damage within soft materials. Additionally, X-ray–induced local fields may potentially impact diffraction resolution through localized piezoelectric distortions of the lattice.« less

Chemical imaging analysis of the brain with X-ray methods

NASA Astrophysics Data System (ADS)

Collingwood, Joanna F.; Adams, Freddy

2017-04-01

Cells employ various metal and metalloid ions to augment the structure and the function of proteins and to assist with vital biological processes. In the brain they mediate biochemical processes, and disrupted metabolism of metals may be a contributing factor in neurodegenerative disorders. In this tutorial review we will discuss the particular role of X-ray methods for elemental imaging analysis of accumulated metal species and metal-containing compounds in biological materials, in the context of post-mortem brain tissue. X-rays have the advantage that they have a short wavelength and can penetrate through a thick biological sample. Many of the X-ray microscopy techniques that provide the greatest sensitivity and specificity for trace metal concentrations in biological materials are emerging at synchrotron X-ray facilities. Here, the extremely high flux available across a wide range of soft and hard X-rays, combined with state-of-the-art focusing techniques and ultra-sensitive detectors, makes it viable to undertake direct imaging of a number of elements in brain tissue. The different methods for synchrotron imaging of metals in brain tissues at regional, cellular, and sub-cellular spatial resolution are discussed. Methods covered include X-ray fluorescence for elemental imaging, X-ray absorption spectrometry for speciation imaging, X-ray diffraction for structural imaging, phase contrast for enhanced contrast imaging and scanning transmission X-ray microscopy for spectromicroscopy. Two- and three-dimensional (confocal and tomographic) imaging methods are considered as well as the correlation of X-ray microscopy with other imaging tools.

Development of a mercuric iodide solid state spectrometer for X-ray astronomy

NASA Technical Reports Server (NTRS)

Vallerga, J.

1983-01-01

Mercuric iodide detectors, experimental development for astronomical use, X ray observations of the 1980 Cygnus X-1 High State, astronomical had X ray detectors in current use, detector development, balloon flight of large area (1500 sq cm) Phoswich detectors, had X ray telescope design, shielded mercuric iodide background measurement, Monte Carlo analysis, measurements with a shielded mercuric iodide detector are discussed.

Sealed-tube synthesis and phase diagram of Li{sub x}TiS{sub 2} (0 ≤ x ≤1)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Ziping; National Laboratory for Superconductivity, Institute of Physics, Chinese Academy of Science, Beijing 100190; Dong, Cheng, E-mail: chengdon@aphy.iphy.ac.cn

2015-01-15

Graphical abstract: We reported a new method to prepare Li{sub x}TiS{sub 2} (0 ≤ x ≤ 1) at 600 °C in sealed tube using Li{sub 2}S aslithium source. A schematic phase diagram of the Li{sub x}TiS{sub 2} system has been constructed based on the DTA and XRD data. - Abstract: We reported a new method to prepare Li{sub x}TiS{sub 2} (0 ≤ x ≤ 1) at 600 °C in sealed tube using Li{sub 2}S as lithium source. The Li{sub x}TiS{sub 2} samples were characterized by powder X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectroscopy, and differential thermal analysis. Themore » variations of the lattice parameters with lithium content x in Li{sub x}TiS{sub 2} were determined by X-ray powder diffraction analysis for both 1T and 3R phases. The phase transition between low-temperature 1T phase and high-temperature 3R phase was confirmed by the powder X-ray diffraction analysis. Based on the differential thermal analysis and X-ray diffraction results, a schematic phase diagram of the Li{sub x}TiS{sub 2} system has been constructed, providing a guideline to synthesize Li{sub x}TiS{sub 2} in 1T structure or 3R structure.« less

X-ray Crystallography Facility

NASA Technical Reports Server (NTRS)

2000-01-01

Edward Snell, a National Research Council research fellow at NASA's Marshall Space Flight Center (MSFC), prepares a protein crystal for analysis by x-ray crystallography as part of NASA's structural biology program. The small, individual crystals are bombarded with x-rays to produce diffraction patterns, a map of the intensity of the x-rays as they reflect through the crystal.

The Prompt-afterglow Connection in Gamma-ray Bursts: a Comprehensive Statistical Analysis of Swift X-ray Light-curves

NASA Technical Reports Server (NTRS)

Margutti, R.; Zaninoni, E.; Bernardini, M. G.; Chincarini, G.; Pasotti, F.; Guidorzi, C.; Angelini, Lorella; Burrows, D. N.; Capalbi, M.; Evans, P. A.;

Exposure to ionizing radiation during dental X-rays is not associated with risk of developing meningioma: a meta-analysis based on seven case-control studies.

PubMed

Xu, Ping; Luo, Hong; Huang, Guang-Lei; Yin, Xin-Hai; Luo, Si-Yang; Song, Ju-Kun

2015-01-01

Many observational studies have found that exposure to dental X-rays is associated with the risk of development of meningioma. However, these findings are inconsistent. We conducted a meta-analysis to assess the relationship between exposure to dental X-rays and the risk of development of meningioma. The PubMed and EMBASE databases were searched to identify eligible studies. Summary odds ratio (OR) estimates and 95% confidence intervals (95% CIs) were used to compute the risk of meningioma development according to heterogeneity. Subgroup and sensitivity analyses were performed to further explore the potential heterogeneity. Finally, publication bias was assessed. Seven case-control studies involving 6,174 patients and 19,459 controls were included in the meta-analysis. Neither exposure to dental X-rays nor performance of full-mouth panorex X-rays was associated with an increased risk of development of meningioma (overall: OR, 0.97; 95% CI, 0.70-1.32; dental X-rays: OR, 1.05; 95% CI, 0.89-1.25; panorex X-rays: OR, 1.01; 95% CI, 0.76-1.34). However, exposure to bitewing X-rays was associated with a slightly increased risk of development of meningioma (OR, 1.73; 95% CI, 1.28-2.34). Similar results were obtained in the subgroup and sensitivity analyses. Little evidence of publication bias was observed. Based on the currently limited data, there is no association between exposure to dental X-rays and the risk of development of meningioma. However, these results should be cautiously interpreted because of the heterogeneity among studies. Additional large, high-quality clinical trials are needed to evaluate the association between exposure to dental X-rays and the risk of development of meningioma.

Confocal total reflection X-ray fluorescence technology based on an elliptical monocapillary and a parallel polycapillary X-ray optics.

PubMed

Zhu, Yu; Wang, Yabing; Sun, Tianxi; Sun, Xuepeng; Zhang, Xiaoyun; Liu, Zhiguo; Li, Yufei; Zhang, Fengshou

2018-07-01

A total reflection X-ray fluorescence (TXRF) spectrometer based on an elliptical monocapillary X-ray lens (MXRL) and a parallel polycapillary X-ray lens (PPXRL) was designed. This TXRF instrument has micro focal spot, low divergence and high intensity of incident X-ray beam. The diameter of the focal spot of MXRL was 16.5 µm, and the divergence of the incident X-ray beam was 3.4 mrad. We applied this TXRF instrument to the micro analysis of a single-layer film containing Ni deposited on a Si substrate by metal vapor vacuum arc ion source. Copyright © 2018 Elsevier Ltd. All rights reserved.

An Investigation of the Effects of Deposit Feeding Invertebrates on the Structural Properties of Clay Minerals.

DTIC Science & Technology

1981-07-01

Dennis M. Lavoie of NORDA for chemical analysis of clay minerals with the x-ray energy dispersive spectrometer. We thank Fred Bowles, Peter Fleischer...diffractograi of Nuculana acuta fecal pellet 11 residue (illite experiment). TABLES TABLE 1. X-ray energy dispersive spectrometer chemical 8 analysis for...inontmorillonite experiments. Counts for elements after background counts removed. TABLE 2. X-ray energy dispersive spectroneter chemical analysis 12 for

Atmospheric electron x-ray spectrometer

NASA Technical Reports Server (NTRS)

Feldman, Jason E. (Inventor); George, Thomas (Inventor); Wilcox, Jaroslava Z. (Inventor)

2002-01-01

The present invention comprises an apparatus for performing in-situ elemental analyses of surfaces. The invention comprises an atmospheric electron x-ray spectrometer with an electron column which generates, accelerates, and focuses electrons in a column which is isolated from ambient pressure by a:thin, electron transparent membrane. After passing through the membrane, the electrons impinge on the sample in atmosphere to generate characteristic x-rays. An x-ray detector, shaping amplifier, and multi-channel analyzer are used for x-ray detection and signal analysis. By comparing the resultant data to known x-ray spectral signatures, the elemental composition of the surface can be determined.

The superconducting high-resolution soft X-ray spectrometer at the advanced biological and environmental X-ray facility

NASA Astrophysics Data System (ADS)

Friedrich, S.; Drury, O. B.; George, S. J.; Cramer, S. P.

2007-11-01

We have built a 36-pixel superconducting tunnel junction X-ray spectrometer for chemical analysis of dilute samples in the soft X-ray band. It offers an energy resolution of ˜10-20 eV FWHM below 1 keV, a solid angle coverage of ˜10 -3, and can be operated at total rates of up to ˜10 6 counts/s. Here, we describe the spectrometer performance in speciation measurements by fluorescence-detected X-ray absorption spectroscopy at the Advanced Biological and Environmental X-ray facility at the ALS synchrotron.

X-ray Fluorescence Holography: Principles, Apparatus, and Applications

NASA Astrophysics Data System (ADS)

Hayashi, Kouichi; Korecki, Pawel

2018-06-01

X-ray fluorescence holography (XFH) is an atomic structure determination technique that combines the capabilities of X-ray diffraction and X-ray fluorescence spectroscopy. It provides a unique means of gaining fully three-dimensional information about the local atomic structure and lattice site positions of selected elements inside compound samples. In this work, we discuss experimental and theoretical aspects that are essential for the efficient recording and analysis of X-ray fluorescence holograms and review the most recent advances in XFH. We describe experiments performed with brilliant synchrotron radiation as well as with tabletop setups that employ conventional X-ray tubes.

New developments of X-ray fluorescence imaging techniques in laboratory

NASA Astrophysics Data System (ADS)

Tsuji, Kouichi; Matsuno, Tsuyoshi; Takimoto, Yuki; Yamanashi, Masaki; Kometani, Noritsugu; Sasaki, Yuji C.; Hasegawa, Takeshi; Kato, Shuichi; Yamada, Takashi; Shoji, Takashi; Kawahara, Naoki

2015-11-01

X-ray fluorescence (XRF) analysis is a well-established analytical technique with a long research history. Many applications have been reported in various fields, such as in the environmental, archeological, biological, and forensic sciences as well as in industry. This is because XRF has a unique advantage of being a nondestructive analytical tool with good precision for quantitative analysis. Recent advances in XRF analysis have been realized by the development of new x-ray optics and x-ray detectors. Advanced x-ray focusing optics enables the making of a micro x-ray beam, leading to micro-XRF analysis and XRF imaging. A confocal micro-XRF technique has been applied for the visualization of elemental distributions inside the samples. This technique was applied for liquid samples and for monitoring chemical reactions such as the metal corrosion of steel samples in the NaCl solutions. In addition, a principal component analysis was applied for reducing the background intensity in XRF spectra obtained during XRF mapping, leading to improved spatial resolution of confocal micro-XRF images. In parallel, the authors have proposed a wavelength dispersive XRF (WD-XRF) imaging spectrometer for a fast elemental imaging. A new two dimensional x-ray detector, the Pilatus detector was applied for WD-XRF imaging. Fast XRF imaging in 1 s or even less was demonstrated for Euro coins and industrial samples. In this review paper, these recent advances in laboratory-based XRF imaging, especially in a laboratory setting, will be introduced.

Continuously variable focal length lens

DOE Office of Scientific and Technical Information (OSTI.GOV)

Adams, Bernhard W; Chollet, Matthieu C

2013-12-17

A material preferably in crystal form having a low atomic number such as beryllium (Z=4) provides for the focusing of x-rays in a continuously variable manner. The material is provided with plural spaced curvilinear, optically matched slots and/or recesses through which an x-ray beam is directed. The focal length of the material may be decreased or increased by increasing or decreasing, respectively, the number of slots (or recesses) through which the x-ray beam is directed, while fine tuning of the focal length is accomplished by rotation of the material so as to change the path length of the x-ray beammore » through the aligned cylindrical slows. X-ray analysis of a fixed point in a solid material may be performed by scanning the energy of the x-ray beam while rotating the material to maintain the beam's focal point at a fixed point in the specimen undergoing analysis.« less

X-ray fluorescence analysis of low concentrations metals in geological samples and technological products

NASA Astrophysics Data System (ADS)

Lagoida, I. A.; Trushin, A. V.

2016-02-01

For the past several years many nuclear physics methods of quantitative elemental analysis have been designed. Many of these methods have applied in different devices which have become useful and effective instrument in many industrial laboratories. Methods of a matter structure analysis are based on the intensity detection of the X-ray radiation from the nuclei of elements which are excited by external X-ray source. The production of characteristic X-rays involves transitions of the orbital electrons of atoms in the target material between allowed orbits, or energy states, associated with ionization of the inner atomic shells. One of these methods is X-ray fluorescence analysis, which is widespread in metallurgical and processing industries and is used to identify and measure the concentration of the elements in ores and minerals on a conveyor belt. Samples of copper ore with known concentrations of elements, were taken from the Ural deposit. To excite the characteristic X-rays radionuclide sources 109Cd, with half-life 461.4 days were used. After finding the calibration coefficients, control measurements of samples and averaging of overall samples were made. The measurement error did not exceed 3%.

Remote X-Ray Diffraction and X-Ray Fluorescence Analysis on Planetary Surfaces

NASA Technical Reports Server (NTRS)

Blake, David F.; DeVincenzi, D. (Technical Monitor)

1999-01-01

The legacy of planetary X-ray Diffraction (XRD) and X-ray Fluorescence (XRF) began in 1960 when W. Parish proposed an XRD instrument for deployment on the moon. The instrument was built and flight qualified, but the Lunar XRD program was cancelled shortly before the first human landing in 1969. XRF chemical data have been collected in situ by surface landers on Mars (Viking 1 & 2, Pathfinder) and Venus (Venera 13 & 14). These highly successful experiments provide critical constraints on our current understanding of surface processes and planetary evolution. However, the mineralogy, which is more critical to planetary surface science than simple chemical analysis, will remain unknown or will at best be imprecisely constrained until X-ray diffraction (XRD) data are collected. Recent progress in X-ray detector technology allows the consideration of simultaneous XRD (mineralogic analysis) and high-precision XRF (elemental analysis) in systems miniaturized to the point where they can be mounted on fixed landers or small robotic rovers. There is a variety of potential targets for XRD/XRF equipped landers within the solar system, the most compelling of which are the poles of the moon, the southern highlands of Mars and Europa.

Application of a Self-Similar Pressure Profile to Sunyaev-Zeldovich Effect Data from Galaxy Clusters

NASA Technical Reports Server (NTRS)

Mroczkowski, Tony; Bonamente, Max; Carlstrom, John E.; Culverhouse, Thomas L.; Greer, Christopher; Hawkins, David; Hennessy, Ryan; Joy, Marshall; Lamb, James W.; Leitch, Erik M.;

Analytical characterization of a new mobile X-ray fluorescence and X-ray diffraction instrument combined with a pigment identification case study

NASA Astrophysics Data System (ADS)

Van de Voorde, Lien; Vekemans, Bart; Verhaeven, Eddy; Tack, Pieter; De Wolf, Robin; Garrevoet, Jan; Vandenabeele, Peter; Vincze, Laszlo

2015-08-01

A new, commercially available, mobile system combining X-ray diffraction and X-ray fluorescence has been evaluated which enables both elemental analysis and phase identification simultaneously. The instrument makes use of a copper or molybdenum based miniature X-ray tube and a silicon-Pin diode energy-dispersive detector to count the photons originating from the samples. The X-ray tube and detector are both mounted on an X-ray diffraction protractor in a Bragg-Brentano θ:θ geometry. The mobile instrument is one of the lightest and most compact instruments of its kind (3.5 kg) and it is thus very useful for in situ purposes such as the direct (non-destructive) analysis of cultural heritage objects which need to be analyzed on site without any displacement. The supplied software allows both the operation of the instrument for data collection and in-depth data analysis using the International Centre for Diffraction Data database. This paper focuses on the characterization of the instrument, combined with a case study on pigment identification and an illustrative example for the analysis of lead alloyed printing letters. The results show that this commercially available light-weight instrument is able to identify the main crystalline phases non-destructively, present in a variety of samples, with a high degree of flexibility regarding sample size and position.

Impact of imaging guidelines on X-ray use among American provider network chiropractors: interrupted time series analysis.

PubMed

Bussières, André E; Sales, Anne E; Ramsay, Timothy; Hilles, Steven M; Grimshaw, Jeremy M

2014-08-01

Overuse and misuse of spine X-ray imaging for nonspecific back and neck pain persists among chiropractors. Distribution of educational materials among physicians results in small-to-modest improvements in appropriate care, such as ordering spine X-ray studies, but little is known about its impact among North American chiropractors. To evaluate the impact of web-based dissemination of a diagnostic imaging guideline on the use of spine X-ray images among chiropractors. Quasi-experimental design that used interrupted time series to evaluate the effect of guidelines dissemination on spine X-ray imaging claims by chiropractors enlisted in managed care network in the United States. Consecutive adult patients consulting for complaints of spine disorders. A change in level (the mean number of spine X-ray imaging claims per month immediately after the introduction of the guidelines), change in trend (any differences between preintervention and postintervention slopes), estimation of monthly average intervention effect after the intervention. The imaging guideline was disseminated online in April 2008. Administrative claims data were extracted between January 2006 and December 2010. Segmented regression analysis with autoregressive error was used to estimate the impact of guideline recommendations on the rate of spine X-ray studies. Sensitivity analysis considered the effect of two additional quality improvement strategies, a policy change and an education intervention. Time series analysis revealed a significant change in the level of spine X-ray study ordering weeks after introduction of the guidelines (-0.01; 95% confidence interval=-0.01, -0.002; p=.01), but no change in trend of the regression lines. The monthly mean rate of spine X-ray studies within 5 days of initial visit per new patient exams decreased by 10 per 1000, a 5.26% relative decrease after guideline dissemination. Controlling for two quality improvement strategies did not change the results. Web-based guideline dissemination was associated with an immediate reduction in spine X-ray imaging claims. Sensitivity analysis suggests our results are robust. This passive strategy is likely cost-effective in a chiropractic network setting. Copyright © 2014 Elsevier Inc. All rights reserved.

The Mapping X-ray Fluorescence Spectrometer (MapX)

NASA Astrophysics Data System (ADS)

Sarrazin, P.; Blake, D. F.; Marchis, F.; Bristow, T.; Thompson, K.

2017-12-01

Many planetary surface processes leave traces of their actions as features in the size range 10s to 100s of microns. The Mapping X-ray Fluorescence Spectrometer (MapX) will provide elemental imaging at 100 micron spatial resolution, yielding elemental chemistry at a scale where many relict physical, chemical, or biological features can be imaged and interpreted in ancient rocks on planetary bodies and planetesimals. MapX is an arm-based instrument positioned on a rock or regolith with touch sensors. During an analysis, an X-ray source (tube or radioisotope) bombards the sample with X-rays or alpha-particles / gamma-rays, resulting in sample X-ray Fluorescence (XRF). X-rays emitted in the direction of an X-ray sensitive CCD imager pass through a 1:1 focusing lens (X-ray micro-pore Optic (MPO)) that projects a spatially resolved image of the X-rays onto the CCD. The CCD is operated in single photon counting mode so that the energies and positions of individual X-ray photons are recorded. In a single analysis, several thousand frames are both stored and processed in real-time. Higher level data products include single-element maps with a lateral spatial resolution of 100 microns and quantitative XRF spectra from ground- or instrument- selected Regions of Interest (ROI). XRF spectra from ROI are compared with known rock and mineral compositions to extrapolate the data to rock types and putative mineralogies. When applied to airless bodies and implemented with an appropriate radioisotope source for alpha-particle excitation, MapX will be able to analyze biogenic elements C, N, O, P, S, in addition to the cations of the rock-forming elements >Na, accessible with either X-ray or gamma-ray excitation. The MapX concept has been demonstrated with a series of lab-based prototypes and is currently under refinement and TRL maturation.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shin, Jaejin; Woo, Jong-Hak; Mulchaey, John S.

We perform a comprehensive study of X-ray cavities using a large sample of X-ray targets selected from the Chandra archive. The sample is selected to cover a large dynamic range including galaxy clusters, groups, and individual galaxies. Using β -modeling and unsharp masking techniques, we investigate the presence of X-ray cavities for 133 targets that have sufficient X-ray photons for analysis. We detect 148 X-ray cavities from 69 targets and measure their properties, including cavity size, angle, and distance from the center of the diffuse X-ray gas. We confirm the strong correlation between cavity size and distance from the X-raymore » center similar to previous studies. We find that the detection rates of X-ray cavities are similar among galaxy clusters, groups and individual galaxies, suggesting that the formation mechanism of X-ray cavities is independent of environment.« less

Towards shot-noise limited diffraction experiments with table-top femtosecond hard x-ray sources.

PubMed

Holtz, Marcel; Hauf, Christoph; Weisshaupt, Jannick; Salvador, Antonio-Andres Hernandez; Woerner, Michael; Elsaesser, Thomas

2017-09-01

Table-top laser-driven hard x-ray sources with kilohertz repetition rates are an attractive alternative to large-scale accelerator-based systems and have found widespread applications in x-ray studies of ultrafast structural dynamics. Hard x-ray pulses of 100 fs duration have been generated at the Cu K α wavelength with a photon flux of up to 10 9 photons per pulse into the full solid angle, perfectly synchronized to the sub-100-fs optical pulses from the driving laser system. Based on spontaneous x-ray emission, such sources display a particular noise behavior which impacts the sensitivity of x-ray diffraction experiments. We present a detailed analysis of the photon statistics and temporal fluctuations of the x-ray flux, together with experimental strategies to optimize the sensitivity of optical pump/x-ray probe experiments. We demonstrate measurements close to the shot-noise limit of the x-ray source.

Towards shot-noise limited diffraction experiments with table-top femtosecond hard x-ray sources

PubMed Central

Holtz, Marcel; Hauf, Christoph; Weisshaupt, Jannick; Salvador, Antonio-Andres Hernandez; Woerner, Michael; Elsaesser, Thomas

2017-01-01

Table-top laser-driven hard x-ray sources with kilohertz repetition rates are an attractive alternative to large-scale accelerator-based systems and have found widespread applications in x-ray studies of ultrafast structural dynamics. Hard x-ray pulses of 100 fs duration have been generated at the Cu Kα wavelength with a photon flux of up to 109 photons per pulse into the full solid angle, perfectly synchronized to the sub-100-fs optical pulses from the driving laser system. Based on spontaneous x-ray emission, such sources display a particular noise behavior which impacts the sensitivity of x-ray diffraction experiments. We present a detailed analysis of the photon statistics and temporal fluctuations of the x-ray flux, together with experimental strategies to optimize the sensitivity of optical pump/x-ray probe experiments. We demonstrate measurements close to the shot-noise limit of the x-ray source. PMID:28795079

High-energy transients. [from weakly and strongly magnetic neutron stars

NASA Technical Reports Server (NTRS)

Lamb, D. Q.

1991-01-01

The observational characteristics of X-ray bursts are reviewed and the thermonuclear-flash model is examined to assess the suitability of the model and the sources of X- and gamma-ray bursts. The profiles of X-ray bursts from five different sources are delineated, and the global analysis of nuclear burning is discussed to review th range possible X-ray burst behavior. The analysis by Fushiki and Lamb (1987) is noted for the description of regions which lie away from the steady-state cut. The discussion of cyclotron lines in gamma-ray bursts emphasizes the source GB880205, and it is shown that Raman and cyclotron resonant scattering can explain the observed positions, strengths, and widths of the dips in the spectrum. X-ray bursts are theorized to emanate from weakly magnetic neutron stars, and gamma-ray bursts are shown to be the products of strongly magnetic neutron stars.

X-ray and synchrotron methods in studies of cultural heritage sites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Koval’chuk, M. V.; Yatsishina, E. B.; Blagov, A. E.

2016-09-15

X-ray and synchrotron methods that are most widely used in studies of cultural heritage objects (including archaeological sites)—X-ray diffraction analysis, X-ray spectroscopy, and visualization techniques— have been considered. The reported examples show high efficiency and informativeness of natural science studies when solving most diverse problems of archaeology, history, the study of art, museology, etc.

Crystal and Vibrational Structure of Energetic 3,5-dinitro 1,3,5-oxadiazinane (DOD) by Single Crystal X-ray Diffractometry and Raman Spectroscopy

DTIC Science & Technology

2018-03-19

calculations using a temperature of 298 K. 15. SUBJECT TERMS 3,5-dinitro-1,3,5-oxadiazinane (DOD), X-ray crystallography , Raman, energetic material...X-ray analysis. 2.2 Characterization X-ray Crystallography . DOD crystals were characterized with a SuperNova, Dualflex, EosS2 diffractometer using

X- And γ-Ray Pulsations Of The Nearby Radio-Faint PSR J1741–2054

DOE PAGES

Marelli, M.; Belfiore, A.; Saz Parkinson, P.; ...

2014-07-02

The results of a deep XMM-Newton observation of the radio-faint γ-ray pulsar J1741–2054 and its nebula together with the analysis of five years of Fermi Large Area Telescope (LAT) data are reported. The X-ray spectrum of the pulsar is consistent with an absorbed power law plus a blackbody, originating at least partly from the neutron star cooling. The nebular emission is consistent with that of a synchrotron pulsar wind nebula, with hints of spatial spectral variation. We extended the available Fermi LAT ephemeris and folded the γ-ray and X-ray data. We detected X-ray pulsations from the neutron star: both themore » thermal and non-thermal components are ~35%-40% pulsed, with phase-aligned maxima. A sinusoid fits the thermal-folded profile well. A 10 bin phase-resolved analysis of the X-ray emission shows softening of the non-thermal spectrum during the on-pulse phases. The radio, X-ray, and γ-ray light curves are single-peaked, not phase-aligned, with the X-ray peak trailing the γ-ray peak by more than half a rotation. Spectral considerations suggest that the most probable pulsar distance is in the 0.3-1.0 kpc range, in agreement with the radio dispersion measure.« less

XAP, a program for deconvolution and analysis of complex X-ray spectra

USGS Publications Warehouse

Quick, James E.; Haleby, Abdul Malik

1989-01-01

The X-ray analysis program (XAP) is a spectral-deconvolution program written in BASIC and specifically designed to analyze complex spectra produced by energy-dispersive X-ray analytical systems (EDS). XAP compensates for spectrometer drift, utilizes digital filtering to remove background from spectra, and solves for element abundances by least-squares, multiple-regression analysis. Rather than base analyses on only a few channels, broad spectral regions of a sample are reconstructed from standard reference spectra. The effects of this approach are (1) elimination of tedious spectrometer adjustments, (2) removal of background independent of sample composition, and (3) automatic correction for peak overlaps. Although the program was written specifically to operate a KEVEX 7000 X-ray fluorescence analytical system, it could be adapted (with minor modifications) to analyze spectra produced by scanning electron microscopes, electron microprobes, and probes, and X-ray defractometer patterns obtained from whole-rock powders.

[Characteristics of specifications of transportable inverter-type X-ray equipment].

PubMed

Yamamoto, Keiichi; Miyazaki, Shigeru; Asano, Hiroshi; Shinohara, Fuminori; Ishikawa, Mitsuo; Ide, Toshinori; Abe, Shinji; Negishi, Toru; Miyake, Hiroyuki; Imai, Yoshio; Okuaki, Tomoyuki

2003-07-01

Our X-ray systems study group measured and examined the characteristics of four transportable inverter-type X-ray equipments. X-ray tube voltage and X-ray tube current were measured with the X-ray tube voltage and the X-ray tube current measurement terminals provided with the equipment. X-ray tube voltage, irradiation time, and dose were measured with a non-invasive X-ray tube voltage-measuring device, and X-ray output was measured by fluorescence meter. The items investigated were the reproducibility and linearity of X-ray output, error of pre-set X-ray tube voltage and X-ray tube current, and X-ray tube voltage ripple percentage. The waveforms of X-ray tube voltage, the X-ray tube current, and fluorescence intensity draw were analyzed using the oscilloscope gram and a personal computer. All of the equipment had a preset error of X-ray tube voltage and X-ray tube current that met JIS standards. The X-ray tube voltage ripple percentage of each equipment conformed to the tendency to decrease when X-ray tube voltage increased. Although the X-ray output reproducibility of system A exceeded the JIS standard, the other systems were within the JIS standard. Equipment A required 40 ms for X-ray tube current to reach the target value, and there was some X-ray output loss because of a trough in X-ray tube current. Owing to the influence of the ripple in X-ray tube current, the strength of the fluorescence waveform rippled in equipments B and C. Waveform analysis could not be done by aliasing of the recording device in equipment D. The maximum X-ray tube current of transportable inverter-type X-ray equipment is as low as 10-20 mA, and the irradiation time of chest X-ray photography exceeds 0.1 sec. However, improvement of the radiophotographic technique is required for patients who cannot move their bodies or halt respiration. It is necessary to make the irradiation time of the equipments shorter for remote medical treatment.

Use of different spectroscopic techniques in the analysis of Roman age wall paintings.

PubMed

Agnoli, Francesca; Calliari, Irene; Mazzocchin, Gian-Antonio

2007-01-01

In this paper the analysis of samples of Roman age wall paintings coming from: Pordenone, Vicenza and Verona is carried out by using three different techniques: energy dispersive x-rays spectroscopy (EDS), x-rays fluorescence (XRF) and proton induced x-rays emission (PIXE). The features of the three spectroscopic techniques in the analysis of samples of archaeological interest are discussed. The studied pigments were: cinnabar, yellow ochre, green earth, Egyptian blue and carbon black.

The prompt-afterglow connection in gamma-ray bursts: a comprehensive statistical analysis of Swift X-ray light curves

NASA Astrophysics Data System (ADS)

Margutti, R.; Zaninoni, E.; Bernardini, M. G.; Chincarini, G.; Pasotti, F.; Guidorzi, C.; Angelini, L.; Burrows, D. N.; Capalbi, M.; Evans, P. A.; Gehrels, N.; Kennea, J.; Mangano, V.; Moretti, A.; Nousek, J.; Osborne, J. P.; Page, K. L.; Perri, M.; Racusin, J.; Romano, P.; Sbarufatti, B.; Stafford, S.; Stamatikos, M.

2013-01-01

We present a comprehensive statistical analysis of Swift X-ray light curves of gamma-ray bursts (GRBs) collecting data from more than 650 GRBs discovered by Swift and other facilities. The unprecedented sample size allows us to constrain the rest-frame X-ray properties of GRBs from a statistical perspective, with particular reference to intrinsic time-scales and the energetics of the different light-curve phases in a common rest-frame 0.3-30 keV energy band. Temporal variability episodes are also studied and their properties constrained. Two fundamental questions drive this effort: (i) Does the X-ray emission retain any kind of `memory' of the prompt γ-ray phase? (ii) Where is the dividing line between long and short GRB X-ray properties? We show that short GRBs decay faster, are less luminous and less energetic than long GRBs in the X-rays, but are interestingly characterized by similar intrinsic absorption. We furthermore reveal the existence of a number of statistically significant relations that link the X-ray to prompt γ-ray parameters in long GRBs; short GRBs are outliers of the majority of these two-parameter relations. However and more importantly, we report on the existence of a universal three-parameter scaling that links the X-ray and the γ-ray energy to the prompt spectral peak energy of both long and short GRBs: EX, iso∝E1.00 ± 0.06γ, iso/E0.60 ± 0.10pk.

The Mapping X-Ray Fluorescence Spectrometer (MAPX)

NASA Technical Reports Server (NTRS)

Blake, David; Sarrazin, Philippe; Bristow, Thomas; Downs, Robert; Gailhanou, Marc; Marchis, Franck; Ming, Douglas; Morris, Richard; Sole, Vincente Armando; Thompson, Kathleen;

Statistical analysis of tiny SXR flares observed by SphinX

NASA Astrophysics Data System (ADS)

Gryciuk, Magdalena; Siarkowski, Marek; Sylwester, Janusz; Kepa, Anna; Gburek, Szymon; Mrozek, Tomasz; Podgórski, Piotr

2015-08-01

The Solar Photometer in X-rays (SphinX) was designed to observe soft X-ray solar emission in the energy range between ~1 keV and 15 keV with the resolution better than 0.5 keV. The instrument operated from February until November 2009 aboard CORONAS-Photon satellite, during the phase of exceptionally low minimum of solar activity. Here we use SphinX data for analysis of micro-flares and brightenings. Despite a very low activity more than a thousand small X-ray events have been recognized by semi-automatic inspection of SphinX light curves. A catalogue of temporal and physical characteristics of these events is shown and discussed and results of the statistical analysis of the catalogue data are presented.

Analyzing the Spectra of Accreting X-Ray Pulsars

NASA Astrophysics Data System (ADS)

Wolff, Michael

This proposal seeks funding for the analysis of accretion-powered X-ray pulsar spectra from NASA/ HEASARC archived X-ray data. Spectral modeling of accreting X-ray pulsars can tell us a great deal about the physical conditions in and near high mass X-ray binary systems. Such systems have accretion flows where plasma is initially channeled from an accretion disk by the strong neutron star magnetic field, eventually falling onto the magnetic polar cap of the neutron star compact object. Many of these accreting X-ray pulsars have X-ray spectra that consist of broad power-law continua with superposed cyclotron resonant scattering features indicating magnetic field strengths above 10^12 G. The energies of these cyclotron line features have recently been shown to vary with X-ray luminosity in a number of sources such as Her X-1 and V 0332+53, a phenomenon not well understood. Another recent development is the relatively new analytic model for the spectral continuum formation in accretion-powered pulsar systems developed by Becker & Wolff. In their formalism the accretion flows are assumed to go through radiation- dominated radiative shocks and settle onto the neutron star surface. The radiation field consists of strongly Comptonized bremsstrahlung emission from the entire plasma, Comptonized cyclotron emission from the de-excitations of Landau-excited electrons in the neutron star magnetic field, and Comptonized black-body emission from a thermal mound near the neutron star surface. We seek to develop the data analysis tools to apply this model framework to the X-ray data from a wide set of sources to make progress characterizing the basic accretion properties (e.g., magnetic field strength, plasma temperatures, polar cap size, accretion rate per unit area, dominance of bulk vs. thermal Comptonization) as well as understanding the variations of the cyclotron line energies with X-ray luminosity. The three major goals of our proposed work are as follows: In the first year, we will develop the new software module (essentially a computer code representing the theoretical model) necessary to perform the analysis of accretion-powered pulsar X-ray spectra in the XSPEC spectral analysis environment. Also in this first year we will analyze new Suzaku Cycle 6 Target of Opportunity observations of GX 304-1 and 4U 0115+63, two known cyclotron line sources, that we have recently carried out. In the second year of this study we will apply our new XSPEC spectral continuum module to the archival X-ray observational data from a number of accreting X-ray pulsars from the RXTE/PCA/HEXTE and Suzaku/XIS/HXD instruments to extract basic accretion parameters. Our source list contains eight pulsars, seven of which have observed cyclotron scattering lines. These pulsars span a range in magnetic field strength, luminosity, expected accretion rate, expected polar cap size, and Comptonizing temperature. In the second year of this work we also plan to make our new fully tested XSPEC continuum analysis module available to the Goddard Space Flight Center HEASARC for distribution to the astrophysical research community. The development and analysis tasks proposed here will provide for the first time a physical basis for the analysis and interpretation of data on accreting X-ray pulsar spectra.

Discovery of Spatial and Spectral Structure in the X-Ray Emission from the Crab Nebula

NASA Technical Reports Server (NTRS)

Weisskopf, Martin C.; Hester, J. Jeff; Tennant, Allyn F.; Elsner, Ronald F.; Schulz, Norbert S.; Marshall, Herman L.; Karovska, Margarita; Nichols, Joy S.; Swartz, Douglas A.; Kolodziejczak, Jeffery J.

2000-01-01

The Chandra X-Ray Observatory observed the Crab Nebula and pulsar during orbital calibration. Zeroth-order images with the High-Energy Transmission Grating (HETG) readout by the Advanced Charge Coupled Devices (CCD) Imaging Spectrometer spectroscopy array (ACIS-S) show a striking richness of X-ray structure at a resolution comparable to that of the best ground-based visible-light observations. The HETG-ACIS-S images reveal, for the first time, an X-ray inner ring within the X-ray torus, the suggestion of a hollow-tube structure for the torus, and X-ray knots along the inner ring and (perhaps) along the inward extension of the X-ray jet. Although complicated by instrumental effects and the brightness of the Crab Nebula, the spectrometric analysis shows systematic variations of the X-ray spectrum throughout the nebula.

Discovery of Spatial and Spectral Structure in the X-Ray Emission from the Crab Nebula.

PubMed

Weisskopf; Hester; Tennant; Elsner; Schulz; Marshall; Karovska; Nichols; Swartz; Kolodziejczak; O'Dell

2000-06-20

The Chandra X-Ray Observatory observed the Crab Nebula and pulsar during orbital calibration. Zeroth-order images with the High-Energy Transmission Grating (HETG) readout by the Advanced CCD Imaging Spectrometer spectroscopy array (ACIS-S) show a striking richness of X-ray structure at a resolution comparable to that of the best ground-based visible-light observations. The HETG-ACIS-S images reveal, for the first time, an X-ray inner ring within the X-ray torus, the suggestion of a hollow-tube structure for the torus, and X-ray knots along the inner ring and (perhaps) along the inward extension of the X-ray jet. Although complicated by instrumental effects and the brightness of the Crab Nebula, the spectrometric analysis shows systematic variations of the X-ray spectrum throughout the nebula.

NuSTAR Hard X-Ray Survey of the Galactic Center Region I: Hard X-Ray Morphology and Spectroscopy of the Diffuse Emission

NASA Astrophysics Data System (ADS)

Mori, Kaya; Hailey, Charles J.; Krivonos, Roman; Hong, Jaesub; Ponti, Gabriele; Bauer, Franz; Perez, Kerstin; Nynka, Melania; Zhang, Shuo; Tomsick, John A.; Alexander, David M.; Baganoff, Frederick K.; Barret, Didier; Barrière, Nicolas; Boggs, Steven E.; Canipe, Alicia M.; Christensen, Finn E.; Craig, William W.; Forster, Karl; Giommi, Paolo; Grefenstette, Brian W.; Grindlay, Jonathan E.; Harrison, Fiona A.; Hornstrup, Allan; Kitaguchi, Takao; Koglin, Jason E.; Luu, Vy; Madsen, Kristen K.; Mao, Peter H.; Miyasaka, Hiromasa; Perri, Matteo; Pivovaroff, Michael J.; Puccetti, Simonetta; Rana, Vikram; Stern, Daniel; Westergaard, Niels J.; Zhang, William W.; Zoglauer, Andreas

2015-12-01

We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456-2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). NuSTAR detects four non-thermal X-ray filaments, extending the detection of their power-law spectra with Γ ˜ 1.3-2.3 up to ˜50 keV. A morphological and spectral study of the filaments suggests that their origin may be heterogeneous, where previous studies suggested a common origin in young pulsar wind nebulae (PWNe). NuSTAR detects non-thermal X-ray continuum emission spatially correlated with the 6.4 keV Fe Kα fluorescence line emission associated with two Sgr A molecular clouds: MC1 and the Bridge. Broadband X-ray spectral analysis with a Monte-Carlo based X-ray reflection model self-consistently determined their intrinsic column density (˜1023 cm-2), primary X-ray spectra (power-laws with Γ ˜ 2) and set a lower limit of the X-ray luminosity of Sgr A* flare illuminating the Sgr A clouds to LX ≳ 1038 erg s-1. Above ˜20 keV, hard X-ray emission in the central 10 pc region around Sgr A* consists of the candidate PWN G359.95-0.04 and the CHXE, possibly resulting from an unresolved population of massive CVs with white dwarf masses MWD ˜ 0.9 M⊙. Spectral energy distribution analysis suggests that G359.95-0.04 is likely the hard X-ray counterpart of the ultra-high gamma-ray source HESS J1745-290, strongly favoring a leptonic origin of the GC TeV emission.

Study of mass flow distribution and chemical composition of comets from solar induced X-ray fluorescence

NASA Technical Reports Server (NTRS)

Gorenstein, P.

1979-01-01

The expected performance of an X-ray detector as an instrument aboard a mission to a comet was evaluated. The functions of the detector are both nondispersive analysis of chemical composition and measurement of mass flow from the comet nucleus. Measurements are to be carried out at a distance from the comet. The approach distances considered are of the order of 1000 km and 100 km. A new type of X-ray detector, a proportional scintillation detector, is considered as an X-ray counter for nondispersive elemental analysis.

Contamination of X-ray Cassettes with Methicillin-resistant Staphylococcus aureus and Methicillin-resistant Staphylococcus haemolyticus in a Radiology Department

PubMed Central

Kim, Han-Sung; Park, Ji-Young; Koo, Hyun-Sook; Choi, Chul-Sun; Song, Wonkeun; Cho, Hyoun Chan; Lee, Kyu Man

2012-01-01

Background We performed surveillance cultures of the surfaces of X-ray cassettes to assess contamination with methicillin-resistant Staphylococcus aureus (MRSA). Methods The surfaces of 37 X-ray cassettes stored in a radiology department were cultured using mannitol salt agar containing 6 µg/mL oxacillin. Suspected methicillin-resistant staphylococcal colonies were isolated and identified by biochemical testing. Pulsed-field gel electrophoresis (PFGE) analysis was performed to determine the clonal relationships of the contaminants. Results Six X-ray cassettes (16.2%) were contaminated with MRSA. During the isolation procedure, we also detected 19 X-ray cassettes (51.4%) contaminated with methicillin-resistant Staphylococcus haemolyticus (MRSH), identified as yellow colonies resembling MRSA on mannitol salt agar. PFGE analysis of the MRSA and MRSH isolates revealed that most isolates of each organism were identical or closely related to each other, suggesting a common source of contamination. Conclusions X-ray cassettes, which are commonly in direct contact with patients, were contaminated with MRSA and MRSH. In hospital environments, contaminated X-ray cassettes may serve as fomites for methicillin-resistant staphylococci. PMID:22563556

Contamination of X-ray cassettes with methicillin-resistant Staphylococcus aureus and methicillin-resistant Staphylococcus haemolyticus in a radiology department.

PubMed

Kim, Jae-Seok; Kim, Han-Sung; Park, Ji-Young; Koo, Hyun-Sook; Choi, Chul-Sun; Song, Wonkeun; Cho, Hyoun Chan; Lee, Kyu Man

2012-05-01

We performed surveillance cultures of the surfaces of X-ray cassettes to assess contamination with methicillin-resistant Staphylococcus aureus (MRSA). The surfaces of 37 X-ray cassettes stored in a radiology department were cultured using mannitol salt agar containing 6 µg/mL oxacillin. Suspected methicillin-resistant staphylococcal colonies were isolated and identified by biochemical testing. Pulsed-field gel electrophoresis (PFGE) analysis was performed to determine the clonal relationships of the contaminants. Six X-ray cassettes (16.2%) were contaminated with MRSA. During the isolation procedure, we also detected 19 X-ray cassettes (51.4%) contaminated with methicillin-resistant Staphylococcus haemolyticus (MRSH), identified as yellow colonies resembling MRSA on mannitol salt agar. PFGE analysis of the MRSA and MRSH isolates revealed that most isolates of each organism were identical or closely related to each other, suggesting a common source of contamination. X-ray cassettes, which are commonly in direct contact with patients, were contaminated with MRSA and MRSH. In hospital environments, contaminated X-ray cassettes may serve as fomites for methicillin-resistant staphylococci.

13.1 micrometers hard X-ray focusing by a new type monocapillary X-ray optic designed for common laboratory X-ray source

NASA Astrophysics Data System (ADS)

Sun, Xuepeng; zhang, Xiaoyun; Zhu, Yu; Wang, Yabing; Shang, Hongzhong; Zhang, Fengshou; Liu, Zhiguo; Sun, Tianxi

2018-04-01

A new type of monocapillary X-ray optic, called 'two bounces monocapillary X-ray optics' (TBMXO), is proposed for generating a small focal spot with high power-density gain for micro X-ray analysis, using a common laboratory X-ray source. TBMXO is consists of two parts: an ellipsoidal part and a tapered part. Before experimental testing, the TBMXO was simulated by the ray tracing method in MATLAB. The simulated results predicted that the proposed TBMXO would produce a smaller focal spot with higher power-density gain than the ellipsoidal monocapillary X-ray optic (EMXO). In the experiment, the TBMXO performance was tested by both an optical device and a Cu target X-ray tube with focal spot of 100 μm. The results indicated that the TBMXO had a slope error of 57.6 μrad and a 13.1 μm focal spot and a 1360 gain in power density were obtained.

Temporal characteristic analysis of laser-modulated pulsed X-ray source for space X-ray communication

NASA Astrophysics Data System (ADS)

Hang, Shuang; Liu, Yunpeng; Li, Huan; Tang, Xiaobin; Chen, Da

2018-04-01

X-ray communication (XCOM) is a new communication type and is expected to realize high-speed data transmission in some special communication scenarios, such as deep space communication and blackout communication. This study proposes a high-speed modulated X-ray source scheme based on the laser-to-X-ray conversion. The temporal characteristics of the essential components of the proposed laser-modulated pulsed X-ray source (LMPXS) were analyzed to evaluate its pulse emission performance. Results show that the LMPXS can provide a maximum modulation rate up to 100 Mbps which is expected to significantly improve the data rate of XCOM.

An X-ray image of the violent interstellar medium in 30 Doradus

NASA Technical Reports Server (NTRS)

Wang, Q.; Helfand, D. J.

1991-01-01

A detailed analysis of the X-ray emission from the largest H II region complex in the Local Group, 30 Dor, is presented. Applying a new maximum entropy deconvolution algorithm to the Einstein Observatory data, reveals striking correlations among the X-ray, radio, and optical morphologies of the region, with X-ray-emitting bubbles filling cavities surrounded by H-alpha shells and coextensive diffuse X-ray and radio continuum emission from throughout the region. The total X-ray luminosity in the 0.16-3.5 keV band from an area within 160 pc of the central cluster R136 is about 2 x 10 to the 37th ergs/sec.

NuSTAR hard X-ray observations of the Jovian magnetosphere during Juno perijove and apojove intervals

NASA Astrophysics Data System (ADS)

Dunn, W.; Mori, K.; Hailey, C. J.; Branduardi-Raymont, G.; Grefenstette, B.; Jackman, C. M.; Hord, B. J.; Ray, L. C.

2017-12-01

The Nuclear Spectroscopic Telescope Array (NuSTAR) is the first focusing hard X-ray telescope operating in the 3-79 keV band with sub-arcminute angular resolution (18" FWHM). For the first time, NuSTAR provides sufficient sensitivity to detect/resolve hard X-ray emission from Jupiter above 10 keV, since the in-situ Ulysses observation failed to detect X-ray emission in the 27-48 keV band [Hurley et al. 1993]. The initial, exploratory NuSTAR observation of Jupiter was performed in February 2015 with 100 ksec exposure. NuSTAR detected hard X-ray emission (E > 10 keV) from the south polar region at a marginally significance of 3 sigma level [Mori et al. 2016, AAS meeting poster]. This hard X-ray emission is likely an extension of the non-thermal bremsstrahlung component detected up to 7 keV by XMM-Newton [Branduardi-Raymont et al. 2007]. The Ulysses non-detection suggests there should be a spectral cutoff between 7 and 27 keV. Most intriguingly, the NuSTAR detection of hard X-ray emission from the south aurora is in contrast to the 2003 XMM-Newton observations where soft X-ray emission below 8 keV was seen from both the north and south poles [Gladstone et al. 2002]. Given the marginal, but tantalizing, hard X-ray detection of the southern Jovian aurora, a series of NuSTAR observations with total exposure of nearly half a million seconds were approved in the NuSTAR GO and DDT program. These NuSTAR observations coincided with one Juno apojove (in June 2017) and three perijoves (in May, July and September 2017), also joining the multi-wavelength campaigns of observing Jupiter coordinating with Chandra and XMM-Newton X-ray telescope (below 10 keV) and HST. We will present NuSTAR imaging, spectral and timing analysis of Jupiter. NuSTAR imaging analysis will map hard X-ray emission in comparison with soft X-ray and UV images. In addition to investigating any distinctions between the soft and hard X-ray morphology of the Jovian aurorae, we will probe whether hard X-ray emission is spatially associated with the FUV auroral oval. NuSTAR spectral analysis will measure to how high an energy the non-thermal bremsstrahlung component extends, and detect an expected spectral cutoff between 7 and 27 keV. Since NuSTAR operates in the hard X-ray energy band, it probes the maximum energy of accelerating electrons in the Jovian magnetosphere.

VizieR Online Data Catalog: GRB Swift X-ray light curves analysis (Margutti+, 2013)

NASA Astrophysics Data System (ADS)

Margutti, R.; Zaninoni, E.; Bernardini, M. G.; Chincarini, G.; Pasotti, F.; Guidorzi, C.; Angelini, L.; Burrows, D. N.; Capalbi, M.; Evans, P. A.; Gehrels, N.; Kennea, J.; Mangano, V.; Moretti, A.; Nousek, J.; Osborne, J. P.; Page, K. L.; Perri, M.; Racusin, J.; Romano, P.; Sbarufatti, B.; Stafford, S.; Stamatikos, M.

2013-11-01

We present a comprehensive statistical analysis of Swift X-ray light curves of gamma-ray bursts (GRBs) collecting data from more than 650 GRBs discovered by Swift and other facilities. The unprecedented sample size allows us to constrain the rest-frame X-ray properties of GRBs from a statistical perspective, with particular reference to intrinsic time-scales and the energetics of the different light-curve phases in a common rest-frame 0.3-30keV energy band. Temporal variability episodes are also studied and their properties constrained. Two fundamental questions drive this effort: (i) Does the X-ray emission retain any kind of 'memory' of the prompt γ-ray phase? (ii) Where is the dividing line between long and short GRB X-ray properties? We show that short GRBs decay faster, are less luminous and less energetic than long GRBs in the X-rays, but are interestingly characterized by similar intrinsic absorption. We furthermore reveal the existence of a number of statistically significant relations that link the X-ray to prompt γ-ray parameters in long GRBs; short GRBs are outliers of the majority of these two-parameter relations. However and more importantly, we report on the existence of a universal three-parameter scaling that links the X-ray and the γ-ray energy to the prompt spectral peak energy of both long and short GRBs: EX,iso{prop.to}E1.00+/-0.06γ,iso/E0.60+/-0.10pk. (3 data files).

Searching for X-ray emission from AGB stars

NASA Astrophysics Data System (ADS)

Ramstedt, S.; Montez, R.; Kastner, J.; Vlemmings, W. H. T.

2012-07-01

Context. Magnetic fields have been measured around asymptotic giant branch (AGB) stars of all chemical types using maser polarization observations. If present, a large-scale magnetic field would lead to X-ray emission, which should be observable using current X-ray observatories. Aims: The aim is to search the archival data for AGB stars that are intrinsic X-ray emitters. Methods: We have searched the ROSAT, CXO, and XMM-Newton archives for serendipitous X-ray observations of a sample of ~500 AGB stars. We specifically searched for the AGB stars detected with GALEX. The data is calibrated, analyzed and the X-ray luminosities and temperatures are estimated as functions of the circumstellar absorption. Results: We identify 13 AGB stars as having either serendipitous or targeted observations in the X-ray data archives, however for a majority of the sources the detailed analysis show that the detections are questionable. Two new sources are detected by ROSAT: T Dra and R UMa. The spectral analysis suggests that the emission associated with these sources could be due to coronal activity or interaction across a binary system. Conclusions: Further observations of the detected sources are necessary to clearly determine the origin of the X-ray emission. Moreover, additional objects should be subject to targeted X-ray observations in order to achieve better constraints for the magnetic fields around AGB stars. Appendices are available in electronic form at http://www.aanda.org

Surface modification of platinum by laser-produced X-rays

NASA Astrophysics Data System (ADS)

Latif, Hamid; Shahid Rafique, M.; Khaleeq-ur-Rahaman, M.; Sattar, Abdul; Anjum, S.; Usman, A.; Zaheer, S.; Rawat, R. S.

2014-11-01

Laser-induced plasma is used as an X-ray source for the growth of hillocks like nanostructures on platinum surface. To generate X-rays, plasma is produced by Nd:YAG laser, which is operated at second harmonics (λ = 532 nm, E = 400 mJ). Analytical grade 5 N pure Al, Cu and W are used as laser targets for X-rays production. X-rays produced from Al, Cu and W plasmas are used to irradiate three analytical grade (5 N pure) platinum substrates, respectively, under the vacuum ∼10-4 torr. XRD analysis shows considerable structural changes in the exposed platinum. The decrement in reflection intensities, increment in dislocation line density, change in d-spacing and disturbance in the periodicity of planes evidently prove these structural changes. Atomic force microscope AFM topographic analysis of the platinum exposed to X-rays emitted from Al, Cu and W targets showed that nanometer-size hillocks are produced on the platinum surface irrespective of the source. It has also been observed that due to these hillocks, the roughness of the surface has increased. Conductivity of hillocks produced from X-rays produced by Al, Cu and W targets is compared and it is shown that the hillocks produced by Al target X-rays have better conductivity compared to the hillocks produced by X-rays from Cu and W targets.

Determination of the atmospheric structure of the BO star companion of SMC X-1 by analysis of Ginga observations

NASA Technical Reports Server (NTRS)

Clark, George W.

1994-01-01

The x-ray phenomena of the binary system SMC X-1/Sk 160, observed with the Ginga and ROSAT x-ray observatories, are compared with computed phenomena derived from a three dimensional hydrodynamical model of the stellar wind perturbed by x-ray heating and ionization which is described in the accompanying paper. In the model the BOI primary star has a line-driven stellar wind in the region of the x-ray shadow and a thermal wind in the region heated by x-rays. We find general agreement between the observed and predicted x-ray spectra throughout the binary orbit cycle, including the extended, variable, and asymmetric eclipse transitions and the period of deep eclipse.

Bayesian analysis of X-ray jet features of the high redshift quasar jets observed with Chandra

NASA Astrophysics Data System (ADS)

McKeough, Kathryn; Siemiginowska, Aneta; Kashyap, Vinay; Stein, Nathan; Cheung, Chi C.

2015-01-01

X-ray emission of powerful quasar jets may be a result of the inverse Compton (IC) process in which the Cosmic Microwave Background (CMB) photons gain energy by interactions with the jet's relativistic electrons. However, there is no definite evidence that IC/CMB process is responsible for the observed X-ray emission of large scale jets. A step toward understanding the X-ray emission process is to study the Radio and X-ray morphologies of the jet. Results from Chandra X-ray and multi-frequency VLA imaging observations of a sample of 11 high- redshift (z > 2) quasars with kilo-parsec scale radio jets are reported. The sample consists of a set of four z ≥ 3.6 flat-spectrum radio quasars, and seven intermediate redshift (z = 2.1 - 2.9) quasars comprised of four sources with integrated steep radio spectra and three with flat radio spectra.We implement a Bayesian image analysis program, Low-count Image Reconstruction and Analysis (LIRA) , to analyze jet features in the X-ray images of the high redshift quasars. Out of the 36 regions where knots are visible in the radio jets, nine showed detectable X-ray emission. Significant detections are based on the upper bound p-value test based on LIRA simulations. The X-ray and radio properties of this sample combined are examined and compared to lower-redshift samples.This work is supported in part by the National Science Foundation REU and the Department of Defense ASSURE programs under NSF Grant no.1262851 and by the Smithsonian Institution, and by NASA Contract NAS8-39073 to the Chandra X-ray Center (CXC). This research has made use of data obtained from the Chandra Data Archive and Chandra Source Catalog, and software provided by the CXC in the application packages CIAO, ChIPS, and Sherpa. Work is also supported by the Chandra grant GO4-15099X.

Optical Density Analysis of X-Rays Utilizing Calibration Tooling to Estimate Thickness of Parts

NASA Technical Reports Server (NTRS)

Grau, David

2012-01-01

This process is designed to estimate the thickness change of a material through data analysis of a digitized version of an x-ray (or a digital x-ray) containing the material (with the thickness in question) and various tooling. Using this process, it is possible to estimate a material's thickness change in a region of the material or part that is thinner than the rest of the reference thickness. However, that same principle process can be used to determine the thickness change of material using a thinner region to determine thickening, or it can be used to develop contour plots of an entire part. Proper tooling must be used. An x-ray film with an S-shaped characteristic curve or a digital x-ray device with a product resulting in like characteristics is necessary. If a film exists with linear characteristics, this type of film would be ideal; however, at the time of this reporting, no such film has been known. Machined components (with known fractional thicknesses) of a like material (similar density) to that of the material to be measured are necessary. The machined components should have machined through-holes. For ease of use and better accuracy, the throughholes should be a size larger than 0.125 in. (.3 mm). Standard components for this use are known as penetrameters or image quality indicators. Also needed is standard x-ray equipment, if film is used in place of digital equipment, or x-ray digitization equipment with proven conversion properties. Typical x-ray digitization equipment is commonly used in the medical industry, and creates digital images of x-rays in DICOM format. It is recommended to scan the image in a 16-bit format. However, 12-bit and 8-bit resolutions are acceptable. Finally, x-ray analysis software that allows accurate digital image density calculations, such as Image-J freeware, is needed. The actual procedure requires the test article to be placed on the raw x-ray, ensuring the region of interest is aligned for perpendicular x-ray exposure capture. One or multiple machined components of like material/ density with known thicknesses are placed atop the part (preferably in a region of nominal and non-varying thickness) such that exposure of the combined part and machined component lay-up is captured on the x-ray. Depending on the accuracy required, the machined component fs thickness must be carefully chosen. Similarly, depending on the accuracy required, the lay-up must be exposed such that the regions of the x-ray to be analyzed have a density range between 1 and 4.5. After the exposure, the image is digitized, and the digital image can then be analyzed using the image analysis software.

The Born-again Planetary Nebula A78: An X-Ray Twin of A30

NASA Astrophysics Data System (ADS)

Toalá, J. A.; Guerrero, M. A.; Todt, H.; Hamann, W.-R.; Chu, Y.-H.; Gruendl, R. A.; Schönberner, D.; Oskinova, L. M.; Marquez-Lugo, R. A.; Fang, X.; Ramos-Larios, G.

2015-01-01

We present the XMM-Newton discovery of X-ray emission from the planetary nebula (PN) A78, the second born-again PN detected in X-rays apart from A30. These two PNe share similar spectral and morphological characteristics: they harbor diffuse soft X-ray emission associated with the interaction between the H-poor ejecta and the current fast stellar wind and a point-like source at the position of the central star (CSPN). We present the spectral analysis of the CSPN, using for the first time an NLTE code for expanding atmospheres that takes line blanketing into account for the UV and optical spectra. The wind abundances are used for the X-ray spectral analysis of the CSPN and the diffuse emission. The X-ray emission from the CSPN in A78 can be modeled by a single C VI emission line, while the X-ray emission from its diffuse component is better described by an optically thin plasma emission model with a temperature of kT = 0.088 keV (T ≈ 1.0 × 106 K). We estimate X-ray luminosities in the 0.2-2.0 keV energy band of L X, CSPN = (1.2 ± 0.3) × 1031 erg s-1 and L X, DIFF = (9.2 ± 2.3) × 1030 erg s-1 for the CSPN and diffuse components, respectively.

The Chandra Source Catalog

NASA Astrophysics Data System (ADS)

Evans, Ian N.; Primini, Francis A.; Glotfelty, Kenny J.; Anderson, Craig S.; Bonaventura, Nina R.; Chen, Judy C.; Davis, John E.; Doe, Stephen M.; Evans, Janet D.; Fabbiano, Giuseppina; Galle, Elizabeth C.; Gibbs, Danny G., II; Grier, John D.; Hain, Roger M.; Hall, Diane M.; Harbo, Peter N.; He, Xiangqun Helen; Houck, John C.; Karovska, Margarita; Kashyap, Vinay L.; Lauer, Jennifer; McCollough, Michael L.; McDowell, Jonathan C.; Miller, Joseph B.; Mitschang, Arik W.; Morgan, Douglas L.; Mossman, Amy E.; Nichols, Joy S.; Nowak, Michael A.; Plummer, David A.; Refsdal, Brian L.; Rots, Arnold H.; Siemiginowska, Aneta; Sundheim, Beth A.; Tibbetts, Michael S.; Van Stone, David W.; Winkelman, Sherry L.; Zografou, Panagoula

2010-07-01

The Chandra Source Catalog (CSC) is a general purpose virtual X-ray astrophysics facility that provides access to a carefully selected set of generally useful quantities for individual X-ray sources, and is designed to satisfy the needs of a broad-based group of scientists, including those who may be less familiar with astronomical data analysis in the X-ray regime. The first release of the CSC includes information about 94,676 distinct X-ray sources detected in a subset of public Advanced CCD Imaging Spectrometer imaging observations from roughly the first eight years of the Chandra mission. This release of the catalog includes point and compact sources with observed spatial extents lsim30''. The catalog (1) provides access to the best estimates of the X-ray source properties for detected sources, with good scientific fidelity, and directly supports scientific analysis using the individual source data; (2) facilitates analysis of a wide range of statistical properties for classes of X-ray sources; and (3) provides efficient access to calibrated observational data and ancillary data products for individual X-ray sources, so that users can perform detailed further analysis using existing tools. The catalog includes real X-ray sources detected with flux estimates that are at least 3 times their estimated 1σ uncertainties in at least one energy band, while maintaining the number of spurious sources at a level of lsim1 false source per field for a 100 ks observation. For each detected source, the CSC provides commonly tabulated quantities, including source position, extent, multi-band fluxes, hardness ratios, and variability statistics, derived from the observations in which the source is detected. In addition to these traditional catalog elements, for each X-ray source the CSC includes an extensive set of file-based data products that can be manipulated interactively, including source images, event lists, light curves, and spectra from each observation in which a source is detected.

X-ray Emission Line Spectroscopy of Nearby Galaxies

NASA Astrophysics Data System (ADS)

Wang, Daniel

What are the origins of the diffuse soft X-ray emission from non-AGN galaxies? Preliminary analysis of XMM-Newton RGS spectra shows that a substantial fraction of the emission cannot arise from optically-thin thermal plasma, as commonly assumed, and may originate in charge exchange at the interface with neutral gas. We request the support for a comprehensive observing, data analysis, and modeling program to spectroscopically determine the origins of the emission. First, we will use our scheduled XMM-Newton AO-10 368 ks observations of the nearest compact elliptical galaxy M32 to obtain the first spectroscopic calibration of the cumulative soft X-ray emission from the old stellar population and will develop a spectral model for the charge exchange, as well as analysis tools to measure the spatial and kinematic properties of the X-ray line- emitting plasma. Second, we will characterize the truly diffuse emission from the hot plasma and/or its interplay with the neutral gas in a sample of galactic spheroids and active star forming/starburst regions in nearby galaxies observed by XMM-Newton. In particular, we will map out the spatial distributions of key emission lines and measure (or tightly constrain) the kinematics of hot plasma outflows for a few X-ray-emitting regions with high-quality RGS data. For galaxies with insufficient counting statistics in individual emission lines, we will conduct a spectral stacking analysis to constrain the average properties of the X-ray-emitting plasma. We will use the results of these X-ray spectroscopic analyses, together with complementary X-ray CCD imaging/spectral data and observations in other wavelength bands, to test the models of the emission. In addition to the charge exchange, alternative scenarios such as resonance scattering and relic AGN photo-ionization will also be examined for suitable regions. These studies are important to the understanding of the relationship between the diffuse soft X-ray emission and various high-energy feedback processes of the galaxies.

Using X-Ray Image Analysis to Assess the Viability of Northern Red Oak Acorns: Implications for Seed Handlers

Treesearch

Rosa C. Goodman; Douglass F. Jacobs; Robert P. Karrfalt

2006-01-01

This paper discusses the potential to use X-ray image analysis as a rapid and nondestructive test of viability of northern red oak (Quercus rubra L.) acorns and the methodology to do so. Acorns are sensitive to desiccation and lose viability as moisture content (MC) decreases, so we examined X-ray images for cotyledon damage in dried acorns to...

Design of a normal incidence multilayer imaging x-ray microscope.

PubMed

Shealy, D L; Gabardi, D R; Hoover, R B; Walker, A B; Lindblom, J F; Barbee, T W

1989-01-01

Normal incidence multilayer Cassegrain x-ray telescopes were flown on the Stanford/MSFC Rocket X-Ray Spectroheliograph. These instruments produced high spatial resolution images of the Sun and conclusively demonstrated that doubly reflecting multilayer x-ray optical systems are feasible. The images indicated that aplanatic imaging soft x-ray /EUV microscopes should be achievable using multilayer optics technology. We have designed a doubly reflecting normal incidence multilayer imaging x-ray microscope based on the Schwarzschild configuration. The Schwarzschild microscope utilizes two spherical mirrors with concentric radii of curvature which are chosen such that the third-order spherical aberration and coma are minimized. We discuss the design of the microscope and the results of the optical system ray trace analysis which indicates that diffraction-limited performance with 600 Å spatial resolution should be obtainable over a 1 mm field of view at a wavelength of 100 Å. Fabrication of several imaging soft x-ray microscopes based upon these designs, for use in conjunction with x-ray telescopes and laser fusion research, is now in progress. High resolution aplanatic imaging x-ray microscopes using normal incidence multilayer x-ray mirrors should have many important applications in advanced x-ray astronomical instrumentation, x-ray lithography, biological, biomedical, metallurgical, and laser fusion research.

Laser power meters as an X-ray power diagnostic for LCLS-II

DOE Office of Scientific and Technical Information (OSTI.GOV)

Heimann, Philip; Moeller, Stefan; Carbajo, Sergio

For the LCLS-II X-ray instruments, laser power meters are being developed as compact X-ray power diagnostics to operate at soft and tender X-ray photon energies. These diagnostics can be installed at various locations along an X-ray free-electron laser (FEL) beamline in order to monitor the transmission of X-ray optics along the beam path. In addition, the power meters will be used to determine the absolute X-ray power at the endstations. Here, thermopile power meters, which measure average power, and have been chosen primarily for their compatibility with the high repetition rates at LCLS-II, are evaluated. Here, a number of characteristicsmore » in the soft X-ray range are presented including linearity, calibrations conducted with a photodiode and a gas monitor detector as well as ultra-high-vacuum compatibility tests using residual gas analysis. The application of these power meters for LCLS-II and other X-ray FEL sources is discussed.« less

Evaluation of the sensitivity and fading characteristics of an image plate system for x-ray diagnostics

NASA Astrophysics Data System (ADS)

Meadowcroft, A. L.; Bentley, C. D.; Stott, E. N.

2008-11-01

Image plates (IPs) are a reusable recording media capable of detecting ionizing radiation, used to diagnose x-ray emission from laser-plasma experiments. Due to their superior performance characteristics in x-ray applications [C. C. Bradford, W. W. Peppler, and J. T. Dobbins III, Med. Phys. 26, 27 (1999) and J. Digit. Imaging. 12, 54 (1999)], the Fuji Biological Analysis System (BAS) IPs are fielded on x-ray diagnostics for the HELEN laser by the Plasma Physics Department at AWE. The sensitivities of the Fuji BAS IPs have been absolutely calibrated for absolute measurements of x-ray intensity in the energy range of 0-100 keV. In addition, the Fuji BAS IP fading as a function of time was investigated. We report on the characterization of three Fuji BAS IP responses to x-rays using a radioactive source, and discrete x-ray line energies generated by the Excalibur soft x-ray facility and the Defense Radiological Standards Centre filter-fluorescer hard x-ray system at AWE.

Laser power meters as an X-ray power diagnostic for LCLS-II.

PubMed

Heimann, Philip; Moeller, Stefan; Carbajo, Sergio; Song, Sanghoon; Dakovski, Georgi; Nordlund, Dennis; Fritz, David

2018-01-01

For the LCLS-II X-ray instruments, laser power meters are being developed as compact X-ray power diagnostics to operate at soft and tender X-ray photon energies. These diagnostics can be installed at various locations along an X-ray free-electron laser (FEL) beamline in order to monitor the transmission of X-ray optics along the beam path. In addition, the power meters will be used to determine the absolute X-ray power at the endstations. Here, thermopile power meters, which measure average power, and have been chosen primarily for their compatibility with the high repetition rates at LCLS-II, are evaluated. A number of characteristics in the soft X-ray range are presented including linearity, calibrations conducted with a photodiode and a gas monitor detector as well as ultra-high-vacuum compatibility tests using residual gas analysis. The application of these power meters for LCLS-II and other X-ray FEL sources is discussed.

Laser power meters as an X-ray power diagnostic for LCLS-II

DOE PAGES

Heimann, Philip; Moeller, Stefan; Carbajo, Sergio; ...

2018-01-01

For the LCLS-II X-ray instruments, laser power meters are being developed as compact X-ray power diagnostics to operate at soft and tender X-ray photon energies. These diagnostics can be installed at various locations along an X-ray free-electron laser (FEL) beamline in order to monitor the transmission of X-ray optics along the beam path. In addition, the power meters will be used to determine the absolute X-ray power at the endstations. Here, thermopile power meters, which measure average power, and have been chosen primarily for their compatibility with the high repetition rates at LCLS-II, are evaluated. Here, a number of characteristicsmore » in the soft X-ray range are presented including linearity, calibrations conducted with a photodiode and a gas monitor detector as well as ultra-high-vacuum compatibility tests using residual gas analysis. The application of these power meters for LCLS-II and other X-ray FEL sources is discussed.« less

Chandra stacking analysis of CANDELS galaxies at z>1.5

NASA Astrophysics Data System (ADS)

Civano, Francesca

2016-09-01

The goal of this proposal is to study the X-ray emission of non-X-ray detected galaxies at z>1.5, beyond the peak of stellar and nuclear activity, in combination with galaxy global properties, such as stellar mass and star formation activity and their morphological classification. To achieve this goal, we will select galaxies in CANDELS. Making use of the 5 X-ray surveys with different depths (160 ks for COSMOS, 800 ks for AEGIS-XD and X-UDS, 2 Ms for GOODS-N and 4 (8) Ms GOODS-S) available in these famous fields, we will be able to reach X-ray luminosities where stellar emission dominate the nuclear one. This analysis will extend to z>1.5, the results obtained performing stacking analysis solely using the Chandra COSMOS Legacy Survey at lower redshift.

Estimation of identification limit for a small-type OSL dosimeter on the medical images by measurement of X-ray spectra.

PubMed

Takegami, Kazuki; Hayashi, Hiroaki; Okino, Hiroki; Kimoto, Natsumi; Maehata, Itsumi; Kanazawa, Yuki; Okazaki, Tohru; Hashizume, Takuya; Kobayashi, Ikuo

2016-07-01

Our aim in this study is to derive an identification limit on a dosimeter for not disturbing a medical image when patients wear a small-type optically stimulated luminescence (OSL) dosimeter on their bodies during X-ray diagnostic imaging. For evaluation of the detection limit based on an analysis of X-ray spectra, we propose a new quantitative identification method. We performed experiments for which we used diagnostic X-ray equipment, a soft-tissue-equivalent phantom (1-20 cm), and a CdTe X-ray spectrometer assuming one pixel of the X-ray imaging detector. Then, with the following two experimental settings, corresponding X-ray spectra were measured with 40-120 kVp and 0.5-1000 mAs at a source-to-detector distance of 100 cm: (1) X-rays penetrating a soft-tissue-equivalent phantom with the OSL dosimeter attached directly on the phantom, and (2) X-rays penetrating only the soft-tissue-equivalent phantom. Next, the energy fluence and errors in the fluence were calculated from the spectra. When the energy fluence with errors concerning these two experimental conditions was estimated to be indistinctive, we defined the condition as the OSL dosimeter not being identified on the X-ray image. Based on our analysis, we determined the identification limit of the dosimeter. We then compared our results with those for the general irradiation conditions used in clinics. We found that the OSL dosimeter could not be identified under the irradiation conditions of abdominal and chest radiography, namely, one can apply the OSL dosimeter to measurement of the exposure dose in the irradiation field of X-rays without disturbing medical images.

Phase-contrast x-ray computed tomography for biological imaging

NASA Astrophysics Data System (ADS)

Momose, Atsushi; Takeda, Tohoru; Itai, Yuji

1997-10-01

We have shown so far that 3D structures in biological sot tissues such as cancer can be revealed by phase-contrast x- ray computed tomography using an x-ray interferometer. As a next step, we aim at applications of this technique to in vivo observation, including radiographic applications. For this purpose, the size of view field is desired to be more than a few centimeters. Therefore, a larger x-ray interferometer should be used with x-rays of higher energy. We have evaluated the optimal x-ray energy from an aspect of does as a function of sample size. Moreover, desired spatial resolution to an image sensor is discussed as functions of x-ray energy and sample size, basing on a requirement in the analysis of interference fringes.

Charged particle induced delayed X-rays (DEX) for the analysis of intermediate and heavy elements

NASA Astrophysics Data System (ADS)

Pillay, A. E.; Erasmus, C. S.; Andeweg, A. H.; Sellschop, J. P. F.; Annegarn, H. J.; Dunn, J.

1988-12-01

The emission of K X-rays from proton-rich and metastable radionuclides, following proton activation of the stable isotopes of the elements of interest, has not been widely used as a means of analysis. The thrust of this paper proposes a nuclear technique using delayed X-rays for the analysis of low concentrations of intermediate and heavy elements. The method is similar to the delayed gamma-ray technique. Proton bombardment induces mainly (p, n) reactions whereas the delayed X-rays originate largely from e --capture and isomeric transition. Samples of rare earth and platinum group elements (PGE), in the form of compacted powders, were irradiated with an 11 MeV proton beam and delayed X-rays detected with a 100 mm 2 Ge detector. Single element spectra for a range of rare earths and PGEs are presented. Analytical conditions are demonstrated for Pd in the range 0.1-5%. Spectra from actual geological samples of a PGE ore, preconcentrated by fire-assay, and monazite are presented. All six platinum group elements are visible and interference-free in a single spectrum, a marked advance on other nuclear techniques for these elements, including PIXE and neutron activation analysis (NAA).

X-ray standing wave analysis of nanostructures using partially coherent radiation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tiwari, M. K., E-mail: mktiwari@rrcat.gov.in; Das, Gangadhar; Bedzyk, M. J.

2015-09-07

The effect of longitudinal (or temporal) coherence on total reflection assisted x-ray standing wave (TR-XSW) analysis of nanoscale materials is quantitatively demonstrated by showing how the XSW fringe visibility can be strongly damped by decreasing the spectral resolution of the incident x-ray beam. The correction for nonzero wavelength dispersion (δλ ≠ 0) of the incident x-ray wave field is accounted for in the model computations of TR-XSW assisted angle dependent fluorescence yields of the nanostructure coatings on x-ray mirror surfaces. Given examples include 90 nm diameter Au nanospheres deposited on a Si(100) surface and a 3 nm thick Zn layer trapped on top amore » 100 nm Langmuir-Blodgett film coating on a Au mirror surface. Present method opens up important applications, such as enabling XSW studies of large dimensioned nanostructures using conventional laboratory based partially coherent x-ray sources.« less

Portable TXRF Spectrometer with 10{sup -11}g Detection Limit and Portable XRF Spectromicroscope with Sub-mm Spatial Resolution

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kunimura, Shinsuke; Hatakeyama, So; Sasaki, Nobuharu

A portable total reflection X-ray fluorescence (TXRF) spectrometer that we have developed is applied to trace elemental analysis of water solutions. Although a 5 W X-ray tube is used in the portable TXRF spectrometer, detection limits of several ppb are achieved for 3d transition metal elements and trace elements in a leaching solution of soils, a leaching solution of solder, and alcoholic beverages are detected. Portable X-ray fluorescence (XRF) spectromicroscopes with a 1 W X-ray tube and an 8 W X-ray tube are also presented. Using the portable XRF spectromicroscope with the 1 W X-ray tube, 93 ppm of Crmore » is detected with an about 700 {mu}m spatial resolution. Spatially resolved elemental analysis of a mug painted with blue, red, green, and white is performed using the two portable spectromicroscopes, and the difference in elemental composition at each paint is detected.« less

THE IDENTIFICATION OF THE X-RAY COUNTERPART TO PSR J2021+4026

DOE Office of Scientific and Technical Information (OSTI.GOV)

Weisskopf, Martin C.; Elsner, Ronald F.; O'Dell, Stephen L.

2011-12-10

We report the probable identification of the X-ray counterpart to the {gamma}-ray pulsar PSR J2021+4026 using imaging with the Chandra X-ray Observatory Advanced CCD Imaging Spectrometer and timing analysis with the Fermi satellite. Given the statistical and systematic errors, the positions determined by both satellites are coincident. The X-ray source position is R.A. 20{sup h}21{sup m}30.{sup s}733, decl. +40 Degree-Sign 26'46.''04 (J2000) with an estimated uncertainty of 1.''3 combined statistical and systematic error. Moreover, both the X-ray to {gamma}-ray and the X-ray to optical flux ratios are sensible assuming a neutron star origin for the X-ray flux. The X-ray sourcemore » has no cataloged infrared-to-visible counterpart and, through new observations, we set upper limits to its optical emission of i' > 23.0 mag and r' > 25.2 mag. The source exhibits an X-ray spectrum with most likely both a power law and a thermal component. We also report on the X-ray and visible light properties of the 43 other sources detected in our Chandra observation.« less

The Identification Of The X-Ray Counterpart To PSR J2021+4026

DOE PAGES

Weisskopf, Martin C.; Romani, Roger W.; Razzano, Massimiliano; ...

2011-11-23

We report the probable identification of the X-ray counterpart to the γ-ray pulsar PSR J2021+4026 using imaging with the Chandra X-ray Observatory ACIS and timing analysis with the Fermi satellite. Given the statistical and systematic errors, the positions determined by both satellites are coincident. The X-ray source position is R.A. 20h21m30s.733, Decl. +40°26'46.04" (J2000) with an estimated uncertainty of 1."3 combined statistical and systematic error. Moreover, both the X-ray to γ-ray and the X-ray to optical flux ratios are sensible assuming a neutron star origin for the X-ray flux. The X-ray source has no cataloged infrared-to-visible counterpart and, through newmore » observations, we set upper limits to its optical emission of i' > 23.0 mag and r' > 25.2 mag. The source exhibits an X-ray spectrum with most likely both a powerlaw and a thermal component. We also report on the X-ray and visible light properties of the 43 other sources detected in our Chandra observation.« less

Structural analysis of polymer thin films using GISAXS in the tender X-ray region: Concept and design of GISAXS experiments using the tender X-ray energy at BL-15A2 at the Photon Factory

DOE Office of Scientific and Technical Information (OSTI.GOV)

Takagi, H., E-mail: takagih@post.kek.jp; Igarashi, N.; Mori, T.

If small angle X-ray scattering (SAXS) utilizing the soft X-ray region is available, advanced and unique experiments, which differ from traditional SAXS methods, can be realized. For example, grazing-incidence small angle X-ray scattering (GISAXS) using hard X-ray is a powerful tool for understanding the nanostructure in both vertical and lateral directions of thin films, while GISAXS utilizing the tender X-ray region (SX-GISAXS) enables depth-resolved analysis as well as a standard GISAXS analysis in thin films. Thus, at BL-15A2 at the Photon Factory, a dedicated diffractometer for SX-GISAXS (above 2.1 keV) was constructed. This diffractometer is composed of four vacuum chambers andmore » can be converted into the vacuum state from the sample chamber in front of the detector surface. Diffractions are clearly observed until 12th peak when measuring collagen by SAXS with an X-ray energy of 2.40 keV and a camera length of 825 mm. Additionally, we conducted the model experiment using SX-GISAXS with an X-ray energy of 2.40 keV to confirm that a poly(methyl methacrylate)-poly(n-butyl acrylate) block copolymer thin film has a microphase-separated structure in the thin film, which is composed of lamellae aligned both parallel and perpendicular to the substrate surface. Similarly, in a polystyrene-poly(methyl methacrylate) block copolymer thin film, SX-GISAXS with 3.60 keV and 5.73 keV revealed that hexagonally packed cylinders are aligned parallel to the substrate surface. The incident angle dependence of the first order peak position of the q{sub z} direction obtained from experiments at various incident X-ray energies agrees very well with the theoretical one calculated from the distorted wave Born approximation.« less

A high-transparency, micro-patternable chip for X-ray diffraction analysis of microcrystals under native growth conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Murray, Thomas D.; Johns Hopkins University School of Medicine, Baltimore, MD 21205; Lyubimov, Artem Y.

A highly X-ray-transparent, silicon nitride-based device has been designed and fabricated to harvest protein microcrystals for high-resolution X-ray diffraction data collection using microfocus beamlines and XFELs. Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common laboratory formats and delivering them to an X-ray beam source under native growth conditions. One approach that shows promise in overcoming themore » challenges intrinsic to microcrystal analysis is to pair so-called ‘fixed-target’ sample-delivery devices with microbeam-based X-ray diffraction methods. However, to record weak diffraction patterns it is necessary to fabricate devices from X-ray-transparent materials that minimize background scattering. Presented here is the design of a new micro-diffraction device consisting of three layers fabricated from silicon nitride, photoresist and polyimide film. The chip features low X-ray scattering and X-ray absorption properties, and uses a customizable blend of hydrophobic and hydrophilic surface patterns to help localize microcrystals to defined regions. Microcrystals in their native growth conditions can be loaded into the chips with a standard pipette, allowing data collection at room temperature. Diffraction data collected from hen egg-white lysozyme microcrystals (10–15 µm) loaded into the chips yielded a complete, high-resolution (<1.6 Å) data set sufficient to determine a high-quality structure by molecular replacement. The features of the chip allow the rapid and user-friendly analysis of microcrystals grown under virtually any laboratory format at microfocus synchrotron beamlines and XFELs.« less

The hoard of Beçin—non-destructive analysis of the silver coins

NASA Astrophysics Data System (ADS)

Rodrigues, M.; Schreiner, M.; Mäder, M.; Melcher, M.; Guerra, M.; Salomon, J.; Radtke, M.; Alram, M.; Schindel, N.

2010-05-01

We report the results of an analytical investigation on 416 silver-copper coins stemming from the Ottoman Empire (end of 16th and beginning of 17th centuries), using synchrotron micro X-ray fluorescence analysis (SRXRF). In the past, analyses had already been conducted with energy dispersive X-ray fluorescence analysis (EDXRF), scanning electron microscopy with energy dispersive X-ray spectrometry (SEM/EDX) and proton induced X-ray emission spectroscopy (PIXE). With this combination of techniques it was possible to confirm the fineness of the coinage as well as to study the provenance of the alloy used for the coins. For the interpretation of the data statistical analysis (principal component analysis—PCA) has been performed. A definite local assignment was explored and significant clustering was obtained regarding the minor and trace elements composing the coin alloys.

Measuring silicon pore optics

NASA Astrophysics Data System (ADS)

Vacanti, Giuseppe; Barrière, Nicolas; Bavdaz, Marcos; Chatbi, Abdelhakim; Collon, Maximilien; Dekker, Daniëlle; Girou, David; Günther, Ramses; van der Hoeven, Roy; Krumrey, Michael; Landgraf, Boris; Müller, Peter; Schreiber, Swenja; Vervest, Mark; Wille, Eric

2017-09-01

While predictions based on the metrology (local slope errors and detailed geometrical details) play an essential role in controlling the development of the manufacturing processes, X-ray characterization remains the ultimate indication of the actual performance of Silicon Pore Optics (SPO). For this reason SPO stacks and mirror modules are routinely characterized at PTB's X-ray Pencil Beam Facility at BESSY II. Obtaining standard X-ray results quickly, right after the production of X-ray optics is essential to making sure that X-ray results can inform decisions taken in the lab. We describe the data analysis pipeline in operations at cosine, and how it allows us to go from stack production to full X-ray characterization in 24 hours.

Final Report - X-ray Studies of Highly Correlated Systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Burns, Clement

2017-11-27

The overall goal of the research was to improve the capabilities of x-ray synchrotron instrumentation to enable cutting-edge research in condensed matter physics. The main goal of the current grant cycle was to find a method to measure the polarization of the scattered x-ray in resonant inelastic x-ray scattering. To do this, we developed a polarization analysis apparatus using a thin, toroidally bent single crystal, which could be set to reflect one or the other of the two polarization components in the scattered x-ray beam. Resonant x-ray scattering measurements were also carried out on interfaces and the charge density wavemore » in high temperature superconducting materials.« less

Automated analysis of hot spot X-ray images at the National Ignition Facility

NASA Astrophysics Data System (ADS)

Khan, S. F.; Izumi, N.; Glenn, S.; Tommasini, R.; Benedetti, L. R.; Ma, T.; Pak, A.; Kyrala, G. A.; Springer, P.; Bradley, D. K.; Town, R. P. J.

2016-11-01

At the National Ignition Facility, the symmetry of the hot spot of imploding capsules is diagnosed by imaging the emitted x-rays using gated cameras and image plates. The symmetry of an implosion is an important factor in the yield generated from the resulting fusion process. The x-ray images are analyzed by decomposing the image intensity contours into Fourier and Legendre modes. This paper focuses on the additional protocols for the time-integrated shape analysis from image plates. For implosions with temperatures above ˜4 keV, the hard x-ray background can be utilized to infer the temperature of the hot spot.

Analysis of photographic X-ray images. [S-054 telescope on Skylab

NASA Technical Reports Server (NTRS)

Krieger, A. S.

1977-01-01

Some techniques used to extract quantitative data from the information contained in photographic images produced by grazing incidence soft X-ray optical systems are described. The discussion is focussed on the analysis of the data returned by the S-054 X-Ray Spectrographic Telescope Experiment on Skylab. The parameters of the instrument and the procedures used for its calibration are described. The technique used to convert photographic density to focal plane X-ray irradiance is outlined. The deconvolution of the telescope point response function from the image data is discussed. Methods of estimating the temperature, pressure, and number density of coronal plasmas are outlined.

Automated analysis of hot spot X-ray images at the National Ignition Facility

DOE PAGES

Khan, S. F.; Izumi, N.; Glenn, S.; ...

2016-09-02

At the National Ignition Facility, the symmetry of the hot spot of imploding capsules is diagnosed by imaging the emitted x-rays using gated cameras and image plates. The symmetry of an implosion is an important factor in the yield generated from the resulting fusion process. The x-ray images are analyzed by decomposing the image intensity contours into Fourier and Legendre modes. This paper focuses on the additional protocols for the time-integrated shape analysis from image plates. Here, for implosions with temperatures above ~4keV, the hard x-ray background can be utilized to infer the temperature of the hot spot.

Uncooled spectrometer for x-ray astrophysics

NASA Astrophysics Data System (ADS)

Urban, Martin; Nentvich, Ondrej; Stehlikova, Veronika; Sieger, Ladislav

2017-05-01

In the field of X-ray detection for Astrophysics there are mainly two objectives; first is to create 2D images as a result of sensing radiation by detectors consisting of a pixels matrix and the second is a spectral analysis of the incident radiation. For spectral analysis, the basis is usually the principle of diffraction. This paper describes the new design of X-ray spectrometer based on Timepix detector with optics positioned in front of it. The advantage of this setup is the ability to get the image and spectrum from the same devices. With other modifications is possible to shift detection threshold into areas of soft X-ray radiation.

Automated analysis of hot spot X-ray images at the National Ignition Facility

DOE Office of Scientific and Technical Information (OSTI.GOV)

Khan, S. F., E-mail: khan9@llnl.gov; Izumi, N.; Glenn, S.

At the National Ignition Facility, the symmetry of the hot spot of imploding capsules is diagnosed by imaging the emitted x-rays using gated cameras and image plates. The symmetry of an implosion is an important factor in the yield generated from the resulting fusion process. The x-ray images are analyzed by decomposing the image intensity contours into Fourier and Legendre modes. This paper focuses on the additional protocols for the time-integrated shape analysis from image plates. For implosions with temperatures above ∼4 keV, the hard x-ray background can be utilized to infer the temperature of the hot spot.

Automated analysis of hot spot X-ray images at the National Ignition Facility.

PubMed

Khan, S F; Izumi, N; Glenn, S; Tommasini, R; Benedetti, L R; Ma, T; Pak, A; Kyrala, G A; Springer, P; Bradley, D K; Town, R P J

2016-11-01

At the National Ignition Facility, the symmetry of the hot spot of imploding capsules is diagnosed by imaging the emitted x-rays using gated cameras and image plates. The symmetry of an implosion is an important factor in the yield generated from the resulting fusion process. The x-ray images are analyzed by decomposing the image intensity contours into Fourier and Legendre modes. This paper focuses on the additional protocols for the time-integrated shape analysis from image plates. For implosions with temperatures above ∼4 keV, the hard x-ray background can be utilized to infer the temperature of the hot spot.

Alternative difference analysis scheme combining R -space EXAFS fit with global optimization XANES fit for X-ray transient absorption spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhan, Fei; Tao, Ye; Zhao, Haifeng

Time-resolved X-ray absorption spectroscopy (TR-XAS), based on the laser-pump/X-ray-probe method, is powerful in capturing the change of the geometrical and electronic structure of the absorbing atom upon excitation. TR-XAS data analysis is generally performed on the laser-on minus laser-off difference spectrum. Here, a new analysis scheme is presented for the TR-XAS difference fitting in both the extended X-ray absorption fine-structure (EXAFS) and the X-ray absorption near-edge structure (XANES) regions.R-space EXAFS difference fitting could quickly provide the main quantitative structure change of the first shell. The XANES fitting part introduces a global non-derivative optimization algorithm and optimizes the local structure changemore » in a flexible way where both the core XAS calculation package and the search method in the fitting shell are changeable. The scheme was applied to the TR-XAS difference analysis of Fe(phen) 3spin crossover complex and yielded reliable distance change and excitation population.« less

Alternative difference analysis scheme combining R-space EXAFS fit with global optimization XANES fit for X-ray transient absorption spectroscopy.

PubMed

Zhan, Fei; Tao, Ye; Zhao, Haifeng

2017-07-01

Time-resolved X-ray absorption spectroscopy (TR-XAS), based on the laser-pump/X-ray-probe method, is powerful in capturing the change of the geometrical and electronic structure of the absorbing atom upon excitation. TR-XAS data analysis is generally performed on the laser-on minus laser-off difference spectrum. Here, a new analysis scheme is presented for the TR-XAS difference fitting in both the extended X-ray absorption fine-structure (EXAFS) and the X-ray absorption near-edge structure (XANES) regions. R-space EXAFS difference fitting could quickly provide the main quantitative structure change of the first shell. The XANES fitting part introduces a global non-derivative optimization algorithm and optimizes the local structure change in a flexible way where both the core XAS calculation package and the search method in the fitting shell are changeable. The scheme was applied to the TR-XAS difference analysis of Fe(phen) 3 spin crossover complex and yielded reliable distance change and excitation population.

Bio-metals imaging and speciation in cells using proton and synchrotron radiation X-ray microspectroscopy

PubMed Central

Ortega, Richard; Devès, Guillaume; Carmona, Asunción

2009-01-01

The direct detection of biologically relevant metals in single cells and of their speciation is a challenging task that requires sophisticated analytical developments. The aim of this article is to present the recent achievements in the field of cellular chemical element imaging, and direct speciation analysis, using proton and synchrotron radiation X-ray micro- and nano-analysis. The recent improvements in focusing optics for MeV-accelerated particles and keV X-rays allow application to chemical element analysis in subcellular compartments. The imaging and quantification of trace elements in single cells can be obtained using particle-induced X-ray emission (PIXE). The combination of PIXE with backscattering spectrometry and scanning transmission ion microscopy provides a high accuracy in elemental quantification of cellular organelles. On the other hand, synchrotron radiation X-ray fluorescence provides chemical element imaging with less than 100 nm spatial resolution. Moreover, synchrotron radiation offers the unique capability of spatially resolved chemical speciation using micro-X-ray absorption spectroscopy. The potential of these methods in biomedical investigations will be illustrated with examples of application in the fields of cellular toxicology, and pharmacology, bio-metals and metal-based nano-particles. PMID:19605403

Constraining MHD Disk-Winds with X-ray Absorbers

NASA Astrophysics Data System (ADS)

Fukumura, Keigo; Tombesi, F.; Shrader, C. R.; Kazanas, D.; Contopoulos, J.; Behar, E.

2014-01-01

From the state-of-the-art spectroscopic observations of active galactic nuclei (AGNs) the robust features of absorption lines (e.g. most notably by H/He-like ions), called warm absorbers (WAs), have been often detected in soft X-rays (< 2 keV). While the identified WAs are often mildly blueshifted to yield line-of-sight velocities up to ~100-3,000 km/sec in typical X-ray-bright Seyfert 1 AGNs, a fraction of Seyfert galaxies such as PG 1211+143 exhibits even faster absorbers (v/ 0.1-0.2) called ultra-fast outflows (UFOs) whose physical condition is much more extreme compared with the WAs. Motivated by these recent X-ray data we show that the magnetically- driven accretion-disk wind model is a plausible scenario to explain the characteristic property of these X-ray absorbers. As a preliminary case study we demonstrate that the wind model parameters (e.g. viewing angle and wind density) can be constrained by data from PG 1211+143 at a statistically significant level with chi-squared spectral analysis. Our wind models can thus be implemented into the standard analysis package, XSPEC, as a table spectrum model for general analysis of X-ray absorbers.

The X-CLASS-redMaPPer galaxy cluster comparison. I. Identification procedures

NASA Astrophysics Data System (ADS)

Sadibekova, T.; Pierre, M.; Clerc, N.; Faccioli, L.; Gastaud, R.; Le Fevre, J.-P.; Rozo, E.; Rykoff, E.

2014-11-01

Context. This paper is the first in a series undertaking a comprehensive correlation analysis between optically selected and X-ray-selected cluster catalogues. The rationale of the project is to develop a holistic picture of galaxy clusters utilising optical and X-ray-cluster-selected catalogues with well-understood selection functions. Aims: Unlike most of the X-ray/optical cluster correlations to date, the present paper focuses on the non-matching objects in either waveband. We investigate how the differences observed between the optical and X-ray catalogues may stem from (1) a shortcoming of the detection algorithms; (2) dispersion in the X-ray/optical scaling relations; or (3) substantial intrinsic differences between the cluster populations probed in the X-ray and optical bands. The aim is to inventory and elucidate these effects in order to account for selection biases in the further determination of X-ray/optical cluster scaling relations. Methods: We correlated the X-CLASS serendipitous cluster catalogue extracted from the XMM archive with the redMaPPer optical cluster catalogue derived from the Sloan Digital Sky Survey (DR8). We performed a detailed and, in large part, interactive analysis of the matching output from the correlation. The overlap between the two catalogues has been accurately determined and possible cluster positional errors were manually recovered. The final samples comprise 270 and 355 redMaPPer and X-CLASS clusters, respectively. X-ray cluster matching rates were analysed as a function of optical richness. In the second step, the redMaPPer clusters were correlated with the entire X-ray catalogue, containing point and uncharacterised sources (down to a few 10-15 erg s-1 cm-2 in the [0.5-2] keV band). A stacking analysis was performed for the remaining undetected optical clusters. Results: We find that all rich (λ ≥ 80) clusters are detected in X-rays out to z = 0.6. Below this redshift, the richness threshold for X-ray detection steadily decreases with redshift. Likewise, all X-ray bright clusters are detected by redMaPPer. After correcting for obvious pipeline shortcomings (about 10% of the cases both in optical and X-ray), ~50% of the redMaPPer (down to a richness of 20) are found to coincide with an X-CLASS cluster; when considering X-ray sources of any type, this fraction increases to ~80%; for the remaining objects, the stacking analysis finds a weak signal within 0.5 Mpc around the cluster optical centres. The fraction of clusters totally dominated by AGN-type emission appears to be a few percent. Conversely, ~40% of the X-CLASS clusters are identified with a redMaPPer (down to a richness of 20) - part of the non-matches being due to the X-CLASS sample extending further out than redMaPPer (z< 1.5 vs. z< 0.6), but extending the correlation down to a richness of 5 raises the matching rate to ~65%. Conclusions: This state-of-the-art study involving two well-validated cluster catalogues has shown itself to be complex, and it points to a number of issues inherent to blind cross-matching, owing both to pipeline shortcomings and cluster peculiar properties. These can only been accounted for after a manual check. The combined X-ray and optical scaling relations will be presented in a subsequent article.

Demonstration of imaging X-ray Thomson scattering on OMEGA EP.

PubMed

Belancourt, Patrick X; Theobald, Wolfgang; Keiter, Paul A; Collins, Tim J B; Bonino, Mark J; Kozlowski, Pawel M; Regan, Sean P; Drake, R Paul

2016-11-01

Foams are a common material for high-energy-density physics experiments because of low, tunable densities, and being machinable. Simulating these experiments can be difficult because the equation of state is largely unknown for shocked foams. The focus of this experiment was to develop an x-ray scattering platform for measuring the equation of state of shocked foams on OMEGA EP. The foam used in this experiment is resorcinol formaldehyde with an initial density of 0.34 g/cm 3 . One long-pulse (10 ns) beam drives a shock into the foam, while the remaining three UV beams with a 2 ns square pulse irradiate a nickel foil to create the x-ray backlighter. The primary diagnostic for this platform, the imaging x-ray Thomson spectrometer, spectrally resolves the scattered x-ray beam while imaging in one spatial dimension. Ray tracing analysis of the density profile gives a compression of 3 ± 1 with a shock speed of 39 ± 6 km/s. Analysis of the scattered x-ray spectra gives an upper bound temperature of 20 eV.

Hartman Testing of X-Ray Telescopes

NASA Technical Reports Server (NTRS)

Saha, Timo T.; Biskasch, Michael; Zhang, William W.

2013-01-01

Hartmann testing of x-ray telescopes is a simple test method to retrieve and analyze alignment errors and low-order circumferential errors of x-ray telescopes and their components. A narrow slit is scanned along the circumference of the telescope in front of the mirror and the centroids of the images are calculated. From the centroid data, alignment errors, radius variation errors, and cone-angle variation errors can be calculated. Mean cone angle, mean radial height (average radius), and the focal length of the telescope can also be estimated if the centroid data is measured at multiple focal plane locations. In this paper we present the basic equations that are used in the analysis process. These equations can be applied to full circumference or segmented x-ray telescopes. We use the Optical Surface Analysis Code (OSAC) to model a segmented x-ray telescope and show that the derived equations and accompanying analysis retrieves the alignment errors and low order circumferential errors accurately.

NBSGSC - a FORTRAN program for quantitative x-ray fluorescence analysis. Technical note (final)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tao, G.Y.; Pella, P.A.; Rousseau, R.M.

1985-04-01

A FORTRAN program (NBSGSC) was developed for performing quantitative analysis of bulk specimens by x-ray fluorescence spectrometry. This program corrects for x-ray absorption/enhancement phenomena using the comprehensive alpha coefficient algorithm proposed by Lachance (COLA). NBSGSC is a revision of the program ALPHA and CARECAL originally developed by R.M. Rousseau of the Geological Survey of Canada. Part one of the program (CALCO) performs the calculation of theoretical alpha coefficients, and part two (CALCOMP) computes the composition of the analyte specimens. The analysis of alloys, pressed minerals, and fused specimens can currently be treated by the program. In addition to using measuredmore » x-ray tube spectral distributions, spectra from seven commonly used x-ray tube targets could also be calculated with an NBS algorithm included in the program. NBSGSC is written in FORTRAN IV for a Digital Equipment Corporation (DEC PDP-11/23) minicomputer using RLO2 firm disks and an RSX 11M operating system.« less

An x ray scatter approach for non-destructive chemical analysis of low atomic numbered elements

NASA Technical Reports Server (NTRS)

Ross, H. Richard

1993-01-01

A non-destructive x-ray scatter (XRS) approach has been developed, along with a rapid atomic scatter algorithm for the detection and analysis of low atomic-numbered elements in solids, powders, and liquids. The present method of energy dispersive x-ray fluorescence spectroscopy (EDXRF) makes the analysis of light elements (i.e., less than sodium; less than 11) extremely difficult. Detection and measurement become progressively worse as atomic numbers become smaller, due to a competing process called 'Auger Emission', which reduces fluorescent intensity, coupled with the high mass absorption coefficients exhibited by low energy x-rays, the detection and determination of low atomic-numbered elements by x-ray spectrometry is limited. However, an indirect approach based on the intensity ratio of Compton and Rayleigh scattered has been used to define light element components in alloys, plastics and other materials. This XRS technique provides qualitative and quantitative information about the overall constituents of a variety of samples.

Searching for Intermediate Mass Black Holes in Ultraluminous X-ray Binaries

NASA Astrophysics Data System (ADS)

Fritze, Hannah; Wright, Simon; Kilgard, Roy

2018-01-01

X-ray observations of nearby galaxies provide one of the best laboratories in the universe for studying two exotic classes of object: black holes and neutron stars. These observations allow us to study the dramatic effect such objects have on their surroundings, as well as the high-energy physics involved in their emission. We conduct a volume-limited archival survey of X-ray sources in all galaxies observed with the Chandra X-ray observatory within 15 Mpc, and identify a set of ultraluminous X-ray sources for detailed spectral analysis. We perform this analysis with the aim of searching for signatures of spectral state transitions and super-Eddington accretion that could indicate the presence of an Intermediate Mass Black Hole (IMBH) binary system. Here, we identify 43 potential IMBH sources that have signatures of super-Eddington accretion. We plan to follow up this initial selection with a multiwavelength analysis of these sources, in order to place further constraints on their nature and surrounding environment.

X-ray and optical substructures of the DAFT/FADA survey clusters

NASA Astrophysics Data System (ADS)

Guennou, L.; Durret, F.; Adami, C.; Lima Neto, G. B.

2013-04-01

We have undertaken the DAFT/FADA survey with the double aim of setting constraints on dark energy based on weak lensing tomography and of obtaining homogeneous and high quality data for a sample of 91 massive clusters in the redshift range 0.4-0.9 for which there were HST archive data. We have analysed the XMM-Newton data available for 42 of these clusters to derive their X-ray temperatures and luminosities and search for substructures. Out of these, a spatial analysis was possible for 30 clusters, but only 23 had deep enough X-ray data for a really robust analysis. This study was coupled with a dynamical analysis for the 26 clusters having at least 30 spectroscopic galaxy redshifts in the cluster range. Altogether, the X-ray sample of 23 clusters and the optical sample of 26 clusters have 14 clusters in common. We present preliminary results on the coupled X-ray and dynamical analyses of these 14 clusters.

NuSTAR HARD X-RAY SURVEY OF THE GALACTIC CENTER REGION. I. HARD X-RAY MORPHOLOGY AND SPECTROSCOPY OF THE DIFFUSE EMISSION

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mori, Kaya; Hailey, Charles J.; Perez, Kerstin

2015-12-01

We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456–2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). NuSTAR detects four non-thermal X-ray filaments, extending the detection of their power-law spectra with Γ ∼ 1.3–2.3 up to ∼50 keV. A morphological and spectral study of the filaments suggests that their origin may be heterogeneous, where previous studies suggested a common origin in young pulsar wind nebulae (PWNe). NuSTAR detects non-thermal X-ray continuum emission spatially correlated with the 6.4more » keV Fe Kα fluorescence line emission associated with two Sgr A molecular clouds: MC1 and the Bridge. Broadband X-ray spectral analysis with a Monte-Carlo based X-ray reflection model self-consistently determined their intrinsic column density (∼10{sup 23} cm{sup −2}), primary X-ray spectra (power-laws with Γ ∼ 2) and set a lower limit of the X-ray luminosity of Sgr A* flare illuminating the Sgr A clouds to L{sub X} ≳ 10{sup 38} erg s{sup −1}. Above ∼20 keV, hard X-ray emission in the central 10 pc region around Sgr A* consists of the candidate PWN G359.95–0.04 and the CHXE, possibly resulting from an unresolved population of massive CVs with white dwarf masses M{sub WD} ∼ 0.9 M{sub ⊙}. Spectral energy distribution analysis suggests that G359.95–0.04 is likely the hard X-ray counterpart of the ultra-high gamma-ray source HESS J1745–290, strongly favoring a leptonic origin of the GC TeV emission.« less

Deep Chandra Survey of the Small Magellanic Cloud. II. Timing Analysis of X-Ray Pulsars

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hong, JaeSub; Antoniou, Vallia; Zezas, Andreas

We report the timing analysis results of X-ray pulsars from a recent deep Chandra survey of the Small Magellanic Cloud (SMC). We analyzed a total exposure of 1.4 Ms from 31 observations over a 1.2 deg{sup 2} region in the SMC under a Chandra X-ray Visionary Program. Using the Lomb–Scargle and epoch-folding techniques, we detected periodic modulations from 20 pulsars and a new candidate pulsar. The survey also covered 11 other pulsars with no clear sign of periodic modulation. The 0.5–8 keV X-ray luminosity ( L {sub X} ) of the pulsars ranges from 10{sup 34} to 10{sup 37} ergmore » s{sup −1} at 60 kpc. All of the Chandra sources with L {sub X} ≳ 4 × 10{sup 35} erg s{sup −1} exhibit X-ray pulsations. The X-ray spectra of the SMC pulsars (and high-mass X-ray binaries) are in general harder than those of the SMC field population. All but SXP 8.02 can be fitted by an absorbed power-law model with a photon index of Γ ≲ 1.5. The X-ray spectrum of the known magnetar SXP 8.02 is better fitted with a two-temperature blackbody model. Newly measured pulsation periods of SXP 51.0, SXP 214, and SXP 701, are significantly different from the previous XMM-Newton and RXTE measurements. This survey provides a rich data set for energy-dependent pulse profile modeling. Six pulsars show an almost eclipse-like dip in the pulse profile. Phase-resolved spectral analysis reveals diverse spectral variations during pulsation cycles: e.g., for an absorbed power-law model, some exhibit an (anti)-correlation between absorption and X-ray flux, while others show more intrinsic spectral variation (i.e., changes in photon indices).« less

ESTIMATE OF SOLAR MAXIMUM USING THE 1-8 Å GEOSTATIONARY OPERATIONAL ENVIRONMENTAL SATELLITES X-RAY MEASUREMENTS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Winter, L. M.; Balasubramaniam, K. S., E-mail: lwinter@aer.com

We present an alternate method of determining the progression of the solar cycle through an analysis of the solar X-ray background. Our results are based on the NOAA Geostationary Operational Environmental Satellites (GOES) X-ray data in the 1-8 Å band from 1986 to the present, covering solar cycles 22, 23, and 24. The X-ray background level tracks the progression of the solar cycle through its maximum and minimum. Using the X-ray data, we can therefore make estimates of the solar cycle progression and the date of solar maximum. Based upon our analysis, we conclude that the Sun reached its hemisphere-averagedmore » maximum in solar cycle 24 in late 2013. This is within six months of the NOAA prediction of a maximum in spring 2013.« less

X-ray spectral signatures of photoionized plasmas. [astrophysics

NASA Technical Reports Server (NTRS)

Liedahl, Duane A.; Kahn, Steven M.; Osterheld, Albert L.; Goldstein, William H.

1990-01-01

Plasma emission codes have become a standard tool for the analysis of spectroscopic data from cosmic X-ray sources. However, the assumption of collisional equilibrium, typically invoked in these codes, renders them inapplicable to many important astrophysical situations, particularly those involving X-ray photoionized nebulae. This point is illustrated by comparing model spectra which have been calculated under conditions appropriate to both coronal plasmas and X-ray photoionized plasmas. It is shown that the (3s-2p)/(3d-2p) line ratios in the Fe L-shell spectrum can be used to effectively discriminate between these two cases. This diagnostic will be especially useful for data analysis associated with AXAF and XMM, which will carry spectroscopic instrumentation with sufficient sensitivity and resolution to identify X-ray photoionized nebulae in a wide range of astrophysical environments.

Lunar elemental analysis obtained from the Apollo gamma-ray and X-ray remote sensing experiment

NASA Technical Reports Server (NTRS)

Trombka, J. I.; Arnold, J. R.; Adler, I.; Metzger, A. E.; Reedy, R. C.

1974-01-01

Gamma ray and X-ray spectrometers carried in the service module of the Apollo 15 and 16 spacecraft were employed for compositional mapping of the lunar surface. The measurements involved the observation of the intensity and characteristics energy distribution of gamma rays and X-rays emitted from the lunar surface. A large scale compositional map of over 10 percent of the lunar surface was obtained from an analysis of the observed spectra. The objective of the X-ray experiment was to measure the K spectral lines from Mg, Al, and Si. Spectra were obtained and the data were reduced to Al/Si and Mg/Si intensity ratios and ultimately to chemical ratios. The objective of the gamma-ray experiment was to measure the natural and cosmic ray induced activity emission spectrum. At this time, the elemental abundances for Th, U, K, Fe, Ti, Si, and O have been determined over a number of major lunar regions.

Applications of Coherent Radiation from Electrons traversing Crystals

NASA Astrophysics Data System (ADS)

Überall, H.

2000-04-01

Historically, the first types of coherent radiation from electrons traversing crystals studied were coherent bremsstrahlung (CB: Dyson and Überall 1955; Überall 1956, 1962) and channeling radiation (CR: Kumakhov, 1976) which produce quasimonochromatic X-rays and γ-rays, as well as parametric X-rays (Baryshevsky and Feranchuk, 1983). Related non-crystal sources are transition radiation and synchrotron radiation. We here present a comparison of radiation types from these sources, and we discuss a series of their possible applications, namely (a) CR: X-ray lithography, angiography, structure analysis of macromolecules, and trace element analysis, and (b) for CB: Radiography, use as a neutron source, elemental analysis, radiation therapy, and radioisotope production for commercial or medical use. CR and CB are very intense sources, needing only low-energy, moderately-priced electron linacs for their generation, hence competing with (or surpassing) more conventional X-ray sources intensity-wise and from a cost standpoint.

Improving material identification by combining x-ray and neutron tomography

NASA Astrophysics Data System (ADS)

LaManna, Jacob M.; Hussey, Daniel S.; Baltic, Eli; Jacobson, David L.

2017-09-01

X-rays and neutrons provide complementary non-destructive probes for the analysis of structure and chemical composition of materials. Contrast differences between the modes arise due to the differences in interaction with matter. Due to the high sensitivity to hydrogen, neutrons excel at separating liquid water or hydrogenous phases from the underlying structure while X-rays resolve the solid structure. Many samples of interest, such as fluid flow in porous materials or curing concrete, are stochastic or slowly changing with time which makes analysis of sequential imaging with X-rays and neutrons difficult as the sample may change between scans. To alleviate this issue, NIST has developed a system for simultaneous X-ray and neutron tomography by orienting a 90 keVpeak micro-focus X-ray tube orthogonally to a thermal neutron beam. This system allows for non-destructive, multimodal tomography of dynamic or stochastic samples while penetrating through sample environment equipment such as pressure and flow vessels. Current efforts are underway to develop methods for 2D histogram based segmentation of reconstructed volumes. By leveraging the contrast differences between X-rays and neutrons, greater histogram peak separation can occur in 2D vs 1D enabling improved material identification.

Simultaneous small- and wide-angle scattering at high X-ray energies.

PubMed

Daniels, J E; Pontoni, D; Hoo, Rui Ping; Honkimäki, V

2010-07-01

Combined small- and wide-angle X-ray scattering (SAXS/WAXS) is a powerful technique for the study of materials at length scales ranging from atomic/molecular sizes (a few angstroms) to the mesoscopic regime ( approximately 1 nm to approximately 1 microm). A set-up to apply this technique at high X-ray energies (E > 50 keV) has been developed. Hard X-rays permit the execution of at least three classes of investigations that are significantly more difficult to perform at standard X-ray energies (8-20 keV): (i) in situ strain analysis revealing anisotropic strain behaviour both at the atomic (WAXS) as well as at the mesoscopic (SAXS) length scales, (ii) acquisition of WAXS patterns to very large q (>20 A(-1)) thus allowing atomic pair distribution function analysis (SAXS/PDF) of micro- and nano-structured materials, and (iii) utilization of complex sample environments involving thick X-ray windows and/or samples that can be penetrated only by high-energy X-rays. Using the reported set-up a time resolution of approximately two seconds was demonstrated. It is planned to further improve this time resolution in the near future.

When will Low-Contrast Features be Visible in a STEM X-Ray Spectrum Image?

PubMed

Parish, Chad M

2015-06-01

When will a small or low-contrast feature, such as an embedded second-phase particle, be visible in a scanning transmission electron microscopy (STEM) X-ray map? This work illustrates a computationally inexpensive method to simulate X-ray maps and spectrum images (SIs), based upon the equations of X-ray generation and detection. To particularize the general procedure, an example of nanostructured ferritic alloy (NFA) containing nm-sized Y2Ti2O7 embedded precipitates in ferritic stainless steel matrix is chosen. The proposed model produces physically appearing simulated SI data sets, which can either be reduced to X-ray dot maps or analyzed via multivariate statistical analysis. Comparison to NFA X-ray maps acquired using three different STEM instruments match the generated simulations quite well, despite the large number of simplifying assumptions used. A figure of merit of electron dose multiplied by X-ray collection solid angle is proposed to compare feature detectability from one data set (simulated or experimental) to another. The proposed method can scope experiments that are feasible under specific analysis conditions on a given microscope. Future applications, such as spallation proton-neutron irradiations, core-shell nanoparticles, or dopants in polycrystalline photovoltaic solar cells, are proposed.

Analysis of the Relationship Between the Solar X-Ray Radiation Intensity and the D-Region Electron Density Using Satellite and Ground-Based Radio Data

NASA Astrophysics Data System (ADS)

Nina, Aleksandra; Čadež, Vladimir M.; Bajčetić, Jovan; Mitrović, Srdjan T.; Popović, Luka Č.

2018-04-01

Increases in the X-ray radiation that is emitted during a solar X-ray flare induce significant changes in the ionospheric D region. Because of the numerous complex processes in the ionosphere and the characteristics of the radiation and plasma, the causal-consequential relationship between the X-ray radiation and ionospheric parameters is not easily determined. In addition, modeling the ionospheric D-region plasma parameters is very difficult because of the lack of data for numerous time- and space-dependent physical quantities. In this article we first give a qualitative analysis of the relationship between the electron density and the recorded solar X-ray intensity. After this, we analyze the differences in the relationships between the D-region response and various X-ray radiation properties. The quantitative study is performed for data observed on 5 May 2010 in the time period between 11:40 UT - 12:40 UT when the GOES 14 satellite detected a considerable X-ray intensity increase. Modeling the electron density is based on characteristics of the 23.4 kHz signal emitted in Germany and recorded by the receiver in Serbia.

Combined analysis of 1,3-benzodioxoles by crystalline sponge X-ray crystallography and laser desorption ionization mass spectrometry.

PubMed

Hayashi, Yukako; Ohara, Kazuaki; Taki, Rika; Saeki, Tomomi; Yamaguchi, Kentaro

2018-03-12

The crystalline sponge (CS) method, which employs single-crystal X-ray diffraction to determine the structure of an analyte present as a liquid or an oil and having a low melting point, was used in combination with laser desorption ionization mass spectrometry (LDI-MS). 1,3-Benzodioxole derivatives were encapsulated in CS and their structures were determined by combining X-ray crystallography and MS. After the X-ray analysis, the CS was subjected to imaging mass spectrometry (IMS) with an LDI spiral-time-of-flight mass spectrometer (TOF-MS). The ion detection area matched the microscopic image of the encapsulated CS. In addition, the accumulated 1D mass spectra showed that fragmentation of the guest molecule (hereafter, guest) can be easily visualized without any interference from the fragment ions of CS except for two strong ion peaks derived from the tridentate ligand TPT (2,4,6-tris(4-pyridyl)-1,3,5-triazine) of the CS and its fragment. X-ray analysis clearly showed the presence of the guest as well as the π-π, CH-halogen, and CH-O interactions between the guest and the CS framework. However, some guests remained randomly diffused in the nanopores of CS. In addition, the detection limit was less than sub-pmol order based on the weight and density of CS determined by X-ray analysis. Spectroscopic data, such as UV-vis and NMR, also supported the encapsulation of the guest through the interaction between the guest and CS components. The results denote that the CS-LDI-MS method, which combines CS, X-ray analysis and LDI-MS, is effective for structure determination.

CHANDRA Detects Relativistic Broad Absorption Lines from APM 08279+5255

NASA Astrophysics Data System (ADS)

Chartas, G.; Brandt, W. N.; Gallagher, S. C.; Garmire, G. P.

2002-11-01

We report the discovery of X-ray broad absorption lines (BALs) from the BAL quasar APM 08279+5255 originating from material moving at relativistic velocities with respect to the central source. The large flux magnification by a factor of ~100 provided by the gravitational lens effect combined with the large redshift (z=3.91) of the quasar have facilitated the acquisition of the first high signal-to-noise X-ray spectrum of a quasar containing X-ray BALs. Our analysis of the X-ray spectrum of APM 08279+5255 places the rest-frame energies of the two observed absorption lines at 8.1 and 9.8 keV. The detection of each of these lines is significant at a greater than 99.9% confidence level based on the F-test. Assuming that the absorption lines are from Fe XXV Kα, the implied bulk velocities of the X-ray BALs are ~0.2c and ~0.4c, respectively. The observed high bulk velocities of the X-ray BALs combined with the relatively short recombination timescales of the X-ray-absorbing gas imply that the absorbers responsible for the X-ray BALs are located at radii of <~2×1017 cm, within the expected location of the UV absorber. With this implied geometry, the X-ray gas could provide the necessary shielding to prevent the UV absorber from being completely ionized by the central X-ray source, consistent with hydrodynamical simulations of line-driven disk winds. Estimated mass-outflow rates for the gas creating the X-ray BALs are typically less than a solar mass per year. Our spectral analysis also indicates that the continuum X-ray emission of APM 08279+5255 is consistent with that of a typical radio-quiet quasar with a spectral slope of Γ=1.72+0.06-0.05.

Miniature x-ray source

DOEpatents

Trebes, James E.; Stone, Gary F.; Bell, Perry M.; Robinson, Ronald B.; Chornenky, Victor I.

2002-01-01

A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

TRANSIENT X-RAY SOURCE POPULATION IN THE MAGELLANIC-TYPE GALAXY NGC 55

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jithesh, V.; Wang, Zhongxiang, E-mail: jithesh@shao.ac.cn

2016-04-10

We present the spectral and temporal properties of 15 candidate transient X-ray sources detected in archival XMM-Newton and Chandra observations of the nearby Magellanic-type, SB(s)m galaxy NGC 55. Based on an X-ray color classification scheme, the majority of the sources may be identified as X-ray binaries (XRBs), and six sources are soft, including a likely supernova remnant. We perform a detailed spectral and variability analysis of the data for two bright candidate XRBs. Both sources displayed strong short-term X-ray variability, and their X-ray spectra and hardness ratios are consistent with those of XRBs. These results, combined with their high X-raymore » luminosities (∼10{sup 38} erg s{sup −1}), strongly suggest that they are black hole (BH) binaries. Seven less luminous sources have spectral properties consistent with those of neutron star or BH XRBs in both normal and high-rate accretion modes, but one of them is the likely counterpart to a background galaxy (because of positional coincidence). From our spectral analysis, we find that the six soft sources are candidate super soft sources (SSSs) with dominant emission in the soft (0.3–2 keV) X-ray band. Archival Hubble Space Telescope optical images for seven sources are available, and the data suggest that most of them are likely to be high-mass XRBs. Our analysis has revealed the heterogeneous nature of the transient population in NGC 55 (six high-mass XRBs, one low-mass XRBs, six SSSs, one active galactic nucleus), helping establish the similarity of the X-ray properties of this galaxy to those of other Magellanic-type galaxies.« less

HEAO Science Symposium

NASA Technical Reports Server (NTRS)

Dailey, C. (Editor); Johnson, W. (Editor)

1979-01-01

Scientific results from the early analysis of data from the HEAO 1 mission are presented. Development of astronomical catalogs and maps, X-ray variability, extragalactic astronomy, X-ray iron line emission, and optical identification and spectroscopy of X-ray sources are among the topics discussed. Results from HEAO 2 imaging and nonimaging instruments are included.

THE EFFECT OF SATELLITE LINES FROM THE X-RAY SOURCE ON X-RAY DIFFRACTION PEAKS

EPA Science Inventory

The article discusses the development of a method for relating reactivity to crystallite size and strain parameters obtained by the Warren-Averbach technique. EPA has been using crystallite size and strain data obtained from x-ray diffraction (XRD) peak profile analysis to predic...

X-ray stars observed in LAMOST spectral survey

NASA Astrophysics Data System (ADS)

Lu, Hong-peng; Zhang, Li-yun; Han, Xianming L.; Shi, Jianrong

2018-05-01

X-ray stars have been studied since the beginning of X-ray astronomy. Investigating and studying the chromospheric activity from X-ray stellar optical spectra is highly significant in providing insights into stellar magnetic activity. The big data of LAMOST survey provides an opportunity for researching stellar optical spectroscopic properties of X-ray stars. We inferred the physical properties of X-ray stellar sources from the analysis of LAMOST spectra. First, we cross-matched the X-ray stellar catalogue (12254 X-ray stars) from ARXA with LAMOST data release 3 (DR3), and obtained 984 good spectra from 713 X-ray sources. We then visually inspected and assigned spectral type to each spectrum and calculated the equivalent width (EW) of Hα line using the Hammer spectral typing facility. Based on the EW of Hα line, we found 203 spectra of 145 X-ray sources with Hα emission above the continuum. For these spectra we also measured the EWs of Hβ, Hγ, Hδ and Ca ii IRT lines of these spectra. After removing novae, planetary nebulae and OB-type stars, we found there are 127 X-ray late-type stars with Hα line emission. By using our spectra and results from the literature, we found 53 X-ray stars showing Hα variability; these objects are Classical T Tauri stars (CTTs), cataclysmic variables (CVs) or chromospheric activity stars. We also found 18 X-ray stars showing obvious emissions in the Ca ii IRT lines. Of the 18 X-ray stars, 16 are CTTs and 2 are CVs. Finally, we discussed the relationships between the EW of Hα line and X-ray flux.

Recent results of synchrotron radiation induced total reflection X-ray fluorescence analysis at HASYLAB, beamline L

NASA Astrophysics Data System (ADS)

Streli, C.; Pepponi, G.; Wobrauschek, P.; Jokubonis, C.; Falkenberg, G.; Záray, G.; Broekaert, J.; Fittschen, U.; Peschel, B.

2006-11-01

At the Hamburger Synchrotronstrahlungslabor (HASYLAB), Beamline L, a vacuum chamber for synchrotron radiation-induced total reflection X-ray fluorescence analysis, is now available which can easily be installed using the adjustment components for microanalysis present at this beamline. The detector is now in the final version of a Vortex silicon drift detector with 50-mm 2 active area from Radiant Detector Technologies. With the Ni/C multilayer monochromator set to 17 keV extrapolated detection limits of 8 fg were obtained using the 50-mm 2 silicon drift detector with 1000 s live time on a sample containing 100 pg of Ni. Various applications are presented, especially of samples which are available in very small amounts: As synchrotron radiation-induced total reflection X-ray fluorescence analysis is much more sensitive than tube-excited total reflection X-ray fluorescence analysis, the sampling time of aerosol samples can be diminished, resulting in a more precise time resolution of atmospheric events. Aerosols, directly sampled on Si reflectors in an impactor were investigated. A further application was the determination of contamination elements in a slurry of high-purity Al 2O 3. No digestion is required; the sample is pipetted and dried before analysis. A comparison with laboratory total reflection X-ray fluorescence analysis showed the higher sensitivity of synchrotron radiation-induced total reflection X-ray fluorescence analysis, more contamination elements could be detected. Using the Si-111 crystal monochromator also available at beamline L, XANES measurements to determine the chemical state were performed. This is only possible with lower sensitivity as the flux transmitted by the crystal monochromator is about a factor of 100 lower than that transmitted by the multilayer monochromator. Preliminary results of X-ray absorption near-edge structure measurements for As in xylem sap from cucumber plants fed with As(III) and As(V) are reported. Detection limits of 170 ng/l of As in xylem sap were achieved.

Theoretical detection limit of PIXE analysis using 20 MeV proton beams

NASA Astrophysics Data System (ADS)

Ishii, Keizo; Hitomi, Keitaro

2018-02-01

Particle-induced X-ray emission (PIXE) analysis is usually performed using proton beams with energies in the range 2∼3 MeV because at these energies, the detection limit is low. The detection limit of PIXE analysis depends on the X-ray production cross-section, the continuous background of the PIXE spectrum and the experimental parameters such as the beam currents and the solid angle and detector efficiency of X-ray detector. Though the continuous background increases as the projectile energy increases, the cross-section of the X-ray increases as well. Therefore, the detection limit of high energy proton PIXE is not expected to increase significantly. We calculated the cross sections of continuous X-rays produced in several bremsstrahlung processes and estimated the detection limit of a 20 MeV proton PIXE analysis by modelling the Compton tail of the γ-rays produced in the nuclear reactions, and the escape effect on the secondary electron bremsstrahlung. We found that the Compton tail does not affect the detection limit when a thin X-ray detector is used, but the secondary electron bremsstrahlung escape effect does have an impact. We also confirmed that the detection limit of the PIXE analysis, when used with 4 μm polyethylene backing film and an integrated beam current of 1 μC, is 0.4∼2.0 ppm for proton energies in the range 10∼30 MeV and elements with Z = 16-90. This result demonstrates the usefulness of several 10 MeV cyclotrons for performing PIXE analysis. Cyclotrons with these properties are currently installed in positron emission tomography (PET) centers.

SEARCHES FOR MILLISECOND PULSAR CANDIDATES AMONG THE UNIDENTIFIED FERMI OBJECTS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hui, C. Y.; Park, S. M.; Hu, C. P.

2015-08-10

Here we report the results of searching millisecond pulsar (MSP) candidates from the Fermi LAT second source catalog (2FGL). Seven unassociated γ-ray sources in this catalog are identified as promising MSP candidates based on their γ-ray properties. Through the X-ray analysis, we have detected possible X-ray counterparts, localized to an arcsecond accuracy. We have systematically estimated their X-ray fluxes and compared them with the corresponding γ-ray fluxes. The X-ray to γ-ray flux ratios for 2FGL J1653.6-0159 and 2FGL J1946.4-5402 are comparable with the typical value for pulsars. For 2FGL J1625.2-0020, 2FGL J1653.6-0159, and 2FGL J1946.4-5402, their candidate X-ray counterparts aremore » bright enough to perform a detailed spectral and temporal analysis to discriminate their thermal/non-thermal nature and search for the periodic signal. We have also searched for possible optical/IR counterparts at the X-ray positions. For the optical/IR source coincident with the brightest X-ray object associated with 2FGL J1120.0-2204, its spectral energy distribution is comparable with a late-type star. Evidence for the variability has also been found by examining its optical light curve. All the aforementioned 2FGL sources resemble a pulsar in one or more aspects, making them promising targets for follow-up investigations.« less

Spectroscopic analysis of solar and cosmic X-ray spectra. 1: The nature of cosmic X-ray spectra and proposed analytical techniques

NASA Technical Reports Server (NTRS)

Walker, A. B. C., Jr.

1975-01-01

Techniques for the study of the solar corona are reviewed as an introduction to a discussion of modifications required for the study of cosmic sources. Spectroscopic analysis of individual sources and the interstellar medium is considered. The latter was studied via analysis of its effect on the spectra of selected individual sources. The effects of various characteristics of the ISM, including the presence of grains, molecules, and ionization, are first discussed, and the development of ISM models is described. The expected spectral structure of individual cosmic sources is then reviewed with emphasis on supernovae remnants and binary X-ray sources. The observational and analytical requirements imposed by the characteristics of these sources are identified, and prospects for the analysis of abundances and the study of physical parameters within them are assessed. Prospects for the spectroscopic study of other classes of X-ray sources are also discussed.

Discovery of Spatial and Spectral Structure in the X-Ray Emission from the Crab Nebula

NASA Technical Reports Server (NTRS)

Weisskopf, M.; Hester, J. J.; Tennant, A. F.; Elsner, R. F.; Schulz, N. S.; Marshall, H. L.; Karovska, M.; Nichols, J. S.; Swartz, D. A.; Kolodziejczak, J. J.

2000-01-01

The Chandra X-ray Observatory observed the Crab Nebula and Pulsar During orbital calibration. Zeroth-order images with the High-Energy Transmission Grating (HETG) read-out by the Advanced CCD Imaging Spectrometer spectroscopy array (ACIS-S) show a striking richness of X-ray structure, at a resolution comparable to that of the best ground-based visible-light observations. The HETG-ACIS-S images reveal, for the first time, an X-ray knots along the inner ring and (perhaps) along the inward extension of the X-ray jet. Although complicated by instrumental effects and the brightness of the Crab Nebula, the spectrometric analysis shows systematic variations of the X-ray spectrum throughout the Nebula.

X-Ray Emission from Ultraviolet Luminous Galaxies and Lyman Break Galaxies

NASA Technical Reports Server (NTRS)

Hornschemeier, Ann; Ptak, A. F.; Salim, S.; Heckman, T. P.; Overzier, R.; Mallery, R.; Rich, M.; Strickland, D.; Grimes, J.

2009-01-01

We present results from an XMM mini-survey of GALEX-selected Ultraviolet-Luminous Galaxies (UVLGs) that appear to include an interesting subset that are analogs to the distant (3

Symposium U: Thermoelectric Power Generation. Held in Boston, Massachusetts on November 26-29, 2007

DTIC Science & Technology

2008-04-01

including X - ray /electron diffraction, TGA analysis, Raman / Fourier Transform Infrared Spectroscopy, electron microscopy, Rutherford back-scattering and...Energy dispersive X - ray analysis were performed on the treated sample. The results revealed that a surface layer (from 10 nm to up to micron in...nanoparticles into a matrix of bulk Bi2Te 3 material via a hot pressing process. These nanocomposites have been examined by SEM and X - ray powder

Three-dimensional x-ray diffraction nanoscopy

NASA Astrophysics Data System (ADS)

Nikulin, Andrei Y.; Dilanian, Ruben A.; Zatsepin, Nadia A.; Muddle, Barry C.

2008-08-01

A novel approach to x-ray diffraction data analysis for non-destructive determination of the shape of nanoscale particles and clusters in three-dimensions is illustrated with representative examples of composite nanostructures. The technique is insensitive to the x-rays coherence, which allows 3D reconstruction of a modal image without tomographic synthesis and in-situ analysis of large (over a several cubic millimeters) volume of material with a spatial resolution of few nanometers, rendering the approach suitable for laboratory facilities.

Evidence for magnetic energy storage in coronal active regions

NASA Technical Reports Server (NTRS)

Krieger, A. S.; De Feiter, L. D.; Vaiana, G. S.

1976-01-01

Examination of X-ray images obtained by the S-054 X-ray spectrographic telescope on Skylab shows the presence of some atypical X-ray-emitting coronal structures in active regions which are not consistent with potential extrapolations of photospheric magnetic fields. Analysis of the observed temporal changes in the X-ray-emitting active-region structures demonstrates that the majority of these consist of brightness changes representing temperature (and perhaps density) variations of the material in the loops.

Hard state neutron star and black hole X-ray binaries in the radio:X-ray luminosity plane

NASA Astrophysics Data System (ADS)

Gallo, Elena; Degenaar, Nathalie; van den Eijnden, Jakob

2018-07-01

Motivated by the large body of literature around the phenomenological properties of accreting black hole (BH) and neutron star (NS) X-ray binaries in the radio:X-ray luminosity plane, we carry out a comparative regression analysis on 36 BHs and 41 NSs in hard X-ray states, with data over 7 dex in X-ray luminosity for both. The BHs follow a radio to X-ray (logarithmic) luminosity relation with slope β = 0.59 ± 0.02, consistent with the NSs' slope (β =0.44^{+0.05}_{-0.04}) within 2.5σ. The best-fitting intercept for the BHs significantly exceeds that for the NSs, cementing BHs as more radio loud, by a factor ˜22. This discrepancy cannot be fully accounted for by the mass or bolometric correction gap, or by the NS boundary layer contribution to the X-rays, and is likely to reflect physical differences in the accretion flow efficiency, or the jet powering mechanism. Once importance sampling is implemented to account for the different luminosity distributions, the slopes of the non-pulsating and pulsating NS subsamples are formally inconsistent (>3σ), unless the transitional millisecond pulsars (whose incoherent radio emission mechanism is not firmly established) are excluded from the analysis. We confirm the lack of a robust partitioning of the BH data set into separate luminosity tracks.

Hard state neutron star and black hole X-ray binaries in the radio:X-ray luminosity plane

NASA Astrophysics Data System (ADS)

Gallo, Elena; Degenaar, Nathalie; van den Eijnden, Jakob

2018-05-01

Motivated by the large body of literature around the phenomenological properties of accreting black hole (BH) and neutron star (NS) X-ray binaries in the radio:X-ray luminosity plane, we carry out a comparative regression analysis on 36 BHs and 41 NSs in hard X-ray states, with data over 7 dex in X-ray luminosity for both. The BHs follow a radio to X-ray (logarithmic) luminosity relation with slope β = 0.59 ± 0.02, consistent with the NSs' slope (β =0.44^{+0.05}_{-0.04}) within 2.5σ. The best-fitting intercept for the BHs significantly exceeds that for the NSs, cementing BHs as more radio loud, by a factor ˜22. This discrepancy can not be fully accounted for by the mass or bolometric correction gap, nor by the NS boundary layer contribution to the X-rays, and is likely to reflect physical differences in the accretion flow efficiency, or the jet powering mechanism. Once importance sampling is implemented to account for the different luminosity distributions, the slopes of the non-pulsating and pulsating NS subsamples are formally inconsistent (>3σ), unless the transitional millisecond pulsars (whose incoherent radio emission mechanism is not firmly established) are excluded from the analysis. We confirm the lack of a robust partitioning of the BH data set into separate luminosity tracks.

Depth resolved compositional analysis of aluminium oxide thin film using non-destructive soft x-ray reflectivity technique

NASA Astrophysics Data System (ADS)

Sinha, Mangalika; Modi, Mohammed H.

2017-10-01

In-depth compositional analysis of 240 Å thick aluminium oxide thin film has been carried out using soft x-ray reflectivity (SXR) and x-ray photoelectron spectroscopy technique (XPS). The compositional details of the film is estimated by modelling the optical index profile obtained from the SXR measurements over 60-200 Å wavelength region. The SXR measurements are carried out at Indus-1 reflectivity beamline. The method suggests that the principal film region is comprised of Al2O3 and AlOx (x = 1.6) phases whereas the interface region comprised of SiO2 and AlOx (x = 1.6) mixture. The soft x-ray reflectivity technique combined with XPS measurements explains the compositional details of principal layer. Since the interface region cannot be analyzed with the XPS technique in a non-destructive manner in such a case the SXR technique is a powerful tool for nondestructive compositional analysis of interface region.

Three Bright X-ray Sources in NGC 1313

NASA Astrophysics Data System (ADS)

Colbert, E.; Petre, R.; Schlegel, E.

1992-12-01

Three bright X-ray sources were detected in a recent (April/May 1991) ROSAT PSPC observation of the nearby (D ~ 4.5 Mpc) face--on barred spiral galaxy NGC 1313. Two of the sources were at positions coincident with X-ray sources detected by Fabbiano & Trinchieri (ApJ 315, 1987) in a previous (Jan 1980) Einstein IPC observation. The position of the brightest Einstein source is near the center of NGC 1313, and the second Einstein source is ~ 7' south of the ``nuclear'' source, in the outskirts of the spiral arms. A third bright X-ray source was detected in the ROSAT observation ~ 7' southwest of the ``nuclear'' source. We present X-ray spectra and X-ray images for the three bright sources found in the ROSAT observation of NGC 1313, and compare with previous Einstein results. Spectral analysis of these sources require them to have very large soft X-ray luminosities ( ~ 10(40) erg s(-1) ) when compared with typical X-ray sources in our Galaxy. Feasible explanations for the X-ray emission are presented. The third X-ray source is positively identified with the recently discovered (Ryder et. al., ApJ 1992) peculiar type-II supernova 1978K.

Analysis of field of view limited by a multi-line X-ray source and its improvement for grating interferometry.

PubMed

Du, Yang; Huang, Jianheng; Lin, Danying; Niu, Hanben

2012-08-01

X-ray phase-contrast imaging based on grating interferometry is a technique with the potential to provide absorption, differential phase contrast, and dark-field signals simultaneously. The multi-line X-ray source used recently in grating interferometry has the advantage of high-energy X-rays for imaging of thick samples for most clinical and industrial investigations. However, it has a drawback of limited field of view (FOV), because of the axial extension of the X-ray emission area. In this paper, we analyze the effects of axial extension of the multi-line X-ray source on the FOV and its improvement in terms of Fresnel diffraction theory. Computer simulation results show that the FOV limitation can be overcome by use of an alternative X-ray tube with a specially designed multi-step anode. The FOV of this newly designed X-ray source can be approximately four times larger than that of the multi-line X-ray source in the same emission area. This might be beneficial for the applications of X-ray phase contrast imaging in materials science, biology, medicine, and industry.

Energy spectrum of multi-radiation of X-rays in a low energy Mather-type plasma focus device

NASA Astrophysics Data System (ADS)

Farzin, M. Aghamir; Reza, A. Behbahani

2014-06-01

The multi-radiation of X-rays was investigated with special attention to their energy spectrum in a Mather-type plasma focus device (operated with argon gas). The analysis is based on the effect of anomalous resistances. To study the energy spectrum, a four-channel diode X-ray spectrometer was used along with a special set of filters. The filters were suitable for detection of medium range X-rays as well as hard X-rays with energy exceeding 30 keV. The results indicate that the anomalous resistivity effect during the post pinch phase may cause multi-radiation of X-rays with a total duration of 300 ± 50 ns. The significant contribution of Cu—Kα was due to the medium range X-rays, nonetheless, hard X-rays with energies greater than 15 keV also participate in the process. The total emitted X-ray energy in the forms of Cu—Kα and Cu—Kβ was around 0.14 ± 0.02 (J/Sr) and 0.04 ± 0.01 (J/Sr), respectively. The total energy of the emitted hard X-ray (> 15 keV) was around 0.12 ± 0.02 (J/Sr).

Evaluation of the sensitivity and fading characteristics of an image plate system for x-ray diagnostics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Meadowcroft, A. L.; Bentley, C. D.; Stott, E. N.

2008-11-15

Image plates (IPs) are a reusable recording media capable of detecting ionizing radiation, used to diagnose x-ray emission from laser-plasma experiments. Due to their superior performance characteristics in x-ray applications [C. C. Bradford, W. W. Peppler, and J. T. Dobbins III, Med. Phys. 26, 27 (1999) and J. Digit. Imaging. 12, 54 (1999)], the Fuji Biological Analysis System (BAS) IPs are fielded on x-ray diagnostics for the HELEN laser by the Plasma Physics Department at AWE. The sensitivities of the Fuji BAS IPs have been absolutely calibrated for absolute measurements of x-ray intensity in the energy range of 0-100 keV.more » In addition, the Fuji BAS IP fading as a function of time was investigated. We report on the characterization of three Fuji BAS IP responses to x-rays using a radioactive source, and discrete x-ray line energies generated by the Excalibur soft x-ray facility and the Defense Radiological Standards Centre filter-fluorescer hard x-ray system at AWE.« less

Generation Mechanisms UV and X-ray Emissions During SL9 Impact

NASA Technical Reports Server (NTRS)

Waite, J. Hunter, Jr.

1997-01-01

The purpose of this grant was to study the ultraviolet and X-ray emissions associated with the impact of comet Shoemaker-Levy 9 with Jupiter. The University of Michigan task was primarily focused on theoretical calculations. The NAGW-4788 subtask was to be largely devoted to determining the constraints placed by the X-ray observations on the physical mechanisms responsible for the generation of the X-rays. Author summarized below the ROSAT observations and suggest a physical mechanism that can plausibly account for the observed emissions. It is hoped that the full set of activities can be completed at a later date. Further analysis of the ROSAT data acquired at the time of the impact was necessary to define the observational constraints on the magnetospheric-ionospheric processes involved in the excitation of the X-ray emissions associated with the fragment impacts. This analysis centered around improvements in the pointing accuracy and improvements in the timing information. Additional pointing information was made possible by the identification of the optical counterparts to the X-ray sources in the ROSAT field-of-view. Due to the large number of worldwide observers of the impacts, a serendipitous visible plate image from an observer in Venezuela provided a very accurate location of the present position of the X-ray source, virtually eliminating pointing errors in the data. Once refined, the pointing indicated that the two observed X-ray brightenings that were highly correlated in time with the K and P2 events were brightenings of the X-ray aurora (as identified in images prior to the impact).Appendix A "ROSAT observations of X-ray emissions from Jupiter during the impact of comet Shoemaker-Levy 9' also included.

NuSTAR Hard X-Ray Survey of the Galactic Center Region. II. X-Ray Point Sources

NASA Technical Reports Server (NTRS)

Hong, Jaesub; Mori, Kaya; Hailey, Charles J.; Nynka, Melania; Zhang, Shou; Gotthelf, Eric; Fornasini, Francesca M.; Krivonos, Roman; Bauer, Franz; Perez, Kerstin;

3D X-ray ultra-microscopy of bone tissue.

PubMed

Langer, M; Peyrin, F

2016-02-01

We review the current X-ray techniques with 3D imaging capability at the nano-scale: transmission X-ray microscopy, ptychography and in-line phase nano-tomography. We further review the different ultra-structural features that have so far been resolved: the lacuno-canalicular network, collagen orientation, nano-scale mineralization and their use as basis for mechanical simulations. X-ray computed tomography at the micro-metric scale is increasingly considered as the reference technique in imaging of bone micro-structure. The trend has been to push towards increasingly higher resolution. Due to the difficulty of realizing optics in the hard X-ray regime, the magnification has mainly been due to the use of visible light optics and indirect detection of the X-rays, which limits the attainable resolution with respect to the wavelength of the visible light used in detection. Recent developments in X-ray optics and instrumentation have allowed to implement several types of methods that achieve imaging that is limited in resolution by the X-ray wavelength, thus enabling computed tomography at the nano-scale. We review here the X-ray techniques with 3D imaging capability at the nano-scale: transmission X-ray microscopy, ptychography and in-line phase nano-tomography. Further, we review the different ultra-structural features that have so far been resolved and the applications that have been reported: imaging of the lacuno-canalicular network, direct analysis of collagen orientation, analysis of mineralization on the nano-scale and use of 3D images at the nano-scale to drive mechanical simulations. Finally, we discuss the issue of going beyond qualitative description to quantification of ultra-structural features.

Analysis of eight argonne premium coal samples by X-ray fluorescence spectrometry

USGS Publications Warehouse

Evans, J.R.; Sellers, G.A.; Johnson, R.G.; Vivit, D.V.; Kent, J.

1990-01-01

X-ray fluorescence spectrometric methods were used in the analysis of eight Argonne Premium Coal Samples. Trace elements (Cr, Ni, Cu, Zn, Rb, Sr, Y, Zr, Nb, Ba, La, and Ce) in coal ash were determined by energy-dispersive X-ray fluorescence spectrometry; major elements (Na, Mg, Al, Si, P, S, K, Ca, Ti, Mn, and Fe) in coal ash and trace elements (Cl and P) in whole coal were determined by wavelength-dispersive X-ray fluorescence spectrometry. The results of this study will be used in a geochemical database compiled for these materials from various analytical techniques. The experimental XRF methods and procedures used to determine these major and trace elements are described.

Tunable X-ray speckle-based phase-contrast and dark-field imaging using the unified modulated pattern analysis approach

NASA Astrophysics Data System (ADS)

Zdora, M.-C.; Thibault, P.; Deyhle, H.; Vila-Comamala, J.; Rau, C.; Zanette, I.

2018-05-01

X-ray phase-contrast and dark-field imaging provides valuable, complementary information about the specimen under study. Among the multimodal X-ray imaging methods, X-ray grating interferometry and speckle-based imaging have drawn particular attention, which, however, in their common implementations incur certain limitations that can restrict their range of applications. Recently, the unified modulated pattern analysis (UMPA) approach was proposed to overcome these limitations and combine grating- and speckle-based imaging in a single approach. Here, we demonstrate the multimodal imaging capabilities of UMPA and highlight its tunable character regarding spatial resolution, signal sensitivity and scan time by using different reconstruction parameters.

Optical and X-ray studies of Compact X-ray Binaries in NGC 5904

NASA Astrophysics Data System (ADS)

Bhalotia, Vanshree; Beck-Winchatz, Bernhard

2018-06-01

Due to their high stellar densities, globular cluster systems trigger various dynamical interactions, such as the formation of compact X-ray binaries. Stellar collisional frequencies have been correlated to the number of X-ray sources detected in various clusters and we hope to measure this correlation for NGC 5904. Optical fluxes of sources from archival HST images of NGC 5904 have been measured using a DOLPHOT PSF photometry in the UV, optical and near-infrared. We developed a data analysis pipeline to process the fluxes of tens of thousands of objects using awk, python and DOLPHOT. We plot color magnitude diagrams in different photometric bands in order to identify outliers that could be X-ray binaries, since they do not evolve the same way as singular stars. Aligning previously measured astrometric data for X-ray sources in NGC 5904 from Chandra with archival astrometric data from HST will filter out the outlier objects that are not X-ray producing, and provide a sample of compact binary systems that are responsible for X-ray emission in NGC 5904. Furthermore, previously measured X-ray fluxes of NGC 5904 from Chandra have also been used to measure the X-ray to optical flux ratio and identify the types of compact X-ray binaries responsible for the X-ray emissions in NGC 5904. We gratefully acknowledge the support from the Illinois Space Grant Consortium.

X-ray microscopy of live biological micro-organisms

NASA Astrophysics Data System (ADS)

Raja Al-Ani, Ma'an Nassar

Real-time, compact x-ray microscopy has the potential to benefit many scientific fields, including microbiology, pharmacology, organic chemistry, and physics. Single frame x-ray micro-radiography, produced by a compact, solid-state laser plasma source, allows scientists to use x-ray emission for elemental analysis, and to observe biological specimens in their natural state. In this study, x-ray images of mouse kidney tissue, live bacteria, Pseudomonas aeruginosa and Burkholderia cepacia, and the bacteria's interaction with the antibiotic gentamicin, are examined using x-ray microscopy. For the purposes of comparing between confocal microscopy and x-ray microscopy, we introduced to our work the technique of gold labeling. Indirect immunofluorescence staining and immuno-gold labeling were applied on human lymphocytes and human tumor cells. Differential interference contrast microscopy (DIC) showed the lymphocyte body and nucleus, as did x-ray microscopy. However, the high resolution of x-ray microscopy allows us to differentiate between the gold particles bound to the antibodies and the free gold. A compact, tabletop Nd: glass laser is used in this study to produce x-rays from an Yttrium target. An atomic force microscope is used to scan the x-ray images from the developed photo-resist. The use of compact, tabletop laser plasma sources, in conjunction with x-ray microscopy, is a new technique that has great potential as a flexible, user-friendly scientific research tool.

Microstructure Analysis of Bismuth Absorbers for Transition-Edge Sensor X-ray Microcalorimeters

NASA Astrophysics Data System (ADS)

Yan, Daikang; Divan, Ralu; Gades, Lisa M.; Kenesei, Peter; Madden, Timothy J.; Miceli, Antonino; Park, Jun-Sang; Patel, Umeshkumar M.; Quaranta, Orlando; Sharma, Hemant; Bennett, Douglas A.; Doriese, William B.; Fowler, Joseph W.; Gard, Johnathon D.; Hays-Wehle, James P.; Morgan, Kelsey M.; Schmidt, Daniel R.; Swetz, Daniel S.; Ullom, Joel N.

2018-03-01

Given its large X-ray stopping power and low specific heat capacity, bismuth (Bi) is a promising absorber material for X-ray microcalorimeters and has been used with transition-edge sensors (TESs) in the past. However, distinct X-ray spectral features have been observed in TESs with Bi absorbers deposited with different techniques. Evaporated Bi absorbers are widely reported to have non-Gaussian low-energy tails, while electroplated ones do not show this feature. In this study, we fabricated Bi absorbers with these two methods and performed microstructure analysis using scanning electron microscopy and X-ray diffraction microscopy. The two types of material showed the same crystallographic structure, but the grain size of the electroplated Bi was about 40 times larger than that of the evaporated Bi. This distinction in grain size is likely to be the cause of their different spectral responses.

IUE and ROSAT monitoring of the bright QSO H1821+643

NASA Technical Reports Server (NTRS)

Halpern, Jules; Kolman, Michiel; Shrader, Chris; Filippenko, Alexei

1991-01-01

The analysis is presented of IUE observations of the bright QSO H1821+643, obtained during the ROSAT All Sky Survey (the RIASS program). The objectives were: (1) to establish whether the UV and soft X ray radiation have the same physical origin; and (2) to determine if this physical origin is an accretion disk. Supporting ground based spectrophotometry was also obtained. The analysis shows that the shape and flux level of the UV continuum did not vary among the seven IUE observation spanning one month, to an upper limit of about 8 percent. So it is of great interest to determine whether the soft X ray flux varied during this period. Since X ray variability in AGNs is often more rapid and of higher amplitude than in the UV, detection of X ray variability in the ROSAT data could severely challenge the accretion disk model for the soft X ray excess.

Thick-target bremsstrahlung interpretation of short time-scale solar hard X-ray features

NASA Technical Reports Server (NTRS)

Emslie, A. G.

1983-01-01

Steady-state analyses of bremsstrahlung hard X-ray production in solar flares are appropriate only if the lifetime of the high energy electrons in the X-ray source is much shorter than the duration of the observed X-ray burst. For a thick-target nonthermal model, this implies that a full time-dependent analysis is required when the duration of the burst is comparable to the collisional lifetime of the injected electrons, in turn set by the lengths and densities of the flaring region. In this paper we present the results of such a time-dependent analysis, and we point out that the intrinsic temporal signature of the thick-target production mechanism, caused by the finite travel time of the electrons through the target, may indeed rule out such a mechanism for extremely short duration hard X-ray events.

Dynamical effects in Bragg coherent x-ray diffraction imaging of finite crystals

NASA Astrophysics Data System (ADS)

Shabalin, A. G.; Yefanov, O. M.; Nosik, V. L.; Bushuev, V. A.; Vartanyants, I. A.

2017-08-01

We present simulations of Bragg coherent x-ray diffractive imaging (CXDI) data from finite crystals in the frame of the dynamical theory of x-ray diffraction. The developed approach is based on a numerical solution of modified Takagi-Taupin equations and can be applied for modeling of a broad range of x-ray diffraction experiments with finite three-dimensional crystals of arbitrary shape also in the presence of strain. We performed simulations for nanocrystals of a cubic and hemispherical shape of different sizes and provided a detailed analysis of artifacts in the Bragg CXDI reconstructions introduced by the dynamical diffraction. Based on our theoretical analysis we developed an analytical procedure to treat effects of refraction and absorption in the reconstruction. Our results elucidate limitations for the kinematical approach in the Bragg CXDI and suggest a natural criterion to distinguish between kinematical and dynamical cases in coherent x-ray diffraction on a finite crystal.

Rapid soft X-ray fluctuations in solar flares observed with the X-ray polychromator

NASA Technical Reports Server (NTRS)

Zarro, D. M.; Saba, J. L. R.; Strong, K. T.

1986-01-01

Three flares observed by the Soft X-Ray Polychromator on the Solar Maximum Mission were studied. Flare light curves from the Flat Crystal Spectrometer and Bent Crystal Spectrometer were examined for rapid signal variations. Each flare was characterized by an initial fast (less than 1 min) burst, observed by the Hard X-Ray Burst Spectrometer (HXRBS), followed by softer gradual X-ray emission lasting several minutes. From an autocorrelation function analysis, evidence was found for quasi-periodic fluctuations with rise and decay times of 10 s in the Ca XIX and Fe XXV light curves. These variations were of small amplitude (less than 20%), often coincided with hard X-ray emissions, and were prominent during the onset of the gradual phase after the initial hard X-ray burst. It is speculated that these fluctuations were caused by repeated energy injections in a coronal loop that had already been heated and filled with dense plasma associated with the initial hard X-ray burst.

Macromolecular structures probed by combining single-shot free-electron laser diffraction with synchrotron coherent X-ray imaging.

PubMed

Gallagher-Jones, Marcus; Bessho, Yoshitaka; Kim, Sunam; Park, Jaehyun; Kim, Sangsoo; Nam, Daewoong; Kim, Chan; Kim, Yoonhee; Noh, Do Young; Miyashita, Osamu; Tama, Florence; Joti, Yasumasa; Kameshima, Takashi; Hatsui, Takaki; Tono, Kensuke; Kohmura, Yoshiki; Yabashi, Makina; Hasnain, S Samar; Ishikawa, Tetsuya; Song, Changyong

2014-05-02

Nanostructures formed from biological macromolecular complexes utilizing the self-assembly properties of smaller building blocks such as DNA and RNA hold promise for many applications, including sensing and drug delivery. New tools are required for their structural characterization. Intense, femtosecond X-ray pulses from X-ray free-electron lasers enable single-shot imaging allowing for instantaneous views of nanostructures at ambient temperatures. When combined judiciously with synchrotron X-rays of a complimentary nature, suitable for observing steady-state features, it is possible to perform ab initio structural investigation. Here we demonstrate a successful combination of femtosecond X-ray single-shot diffraction with an X-ray free-electron laser and coherent diffraction imaging with synchrotron X-rays to provide an insight into the nanostructure formation of a biological macromolecular complex: RNA interference microsponges. This newly introduced multimodal analysis with coherent X-rays can be applied to unveil nano-scale structural motifs from functional nanomaterials or biological nanocomplexes, without requiring a priori knowledge.

PREFACE: Exploring surfaces and buried interfaces of functional materials by advanced x-ray and neutron techniques Exploring surfaces and buried interfaces of functional materials by advanced x-ray and neutron techniques

NASA Astrophysics Data System (ADS)

Sakurai, Kenji

2010-12-01

This special issue is devoted to describing recent applications of x-ray and neutron scattering techniques to the exploration of surfaces and buried interfaces of various functional materials. Unlike many other surface-sensitive methods, these techniques do not require ultra high vacuum, and therefore, a variety of real and complicated surfaces fall within the scope of analysis. It must be particularly emphasized that the techniques are capable of seeing even buried function interfaces as well as the surface. Furthermore, the information, which ranges from the atomic to mesoscopic scale, is highly quantitative and reproducible. The non-destructive nature of the techniques is another important advantage of using x-rays and neutrons, when compared with other atomic-scale analyses. This ensures that the same specimen can be measured by other techniques. Such features are fairly attractive when exploring multilayered materials with nanostructures (dots, tubes, wires, etc), which are finding applications in electronic, magnetic, optical and other devices. The Japan Applied Physics Society has established a group to develop the research field of studying buried function interfaces with x-rays and neutrons. As the methods can be applied to almost all types of materials, from semiconductor and electronic devices to soft materials, participants have fairly different backgrounds but share a common interest in state-of-the-art x-ray and neutron techniques and sophisticated applications. A series of workshops has been organized almost every year since 2001. Some international interactions have been continued intensively, although the community is part of a Japanese society. This special issue does not report the proceedings of the recent workshop, although all the authors are in some way involved in the activities of the above society. Initially, we intended to collect quite long overview papers, including the authors' latest and most important original results, as well as updates on recent progress and global trends in the field. We planned to cover quite a wide area of surface and buried interface science with x-rays and neutrons. Following a great deal of discussion during the editing process, we have decided to change direction. As we intend to publish similar special issues on a frequent basis, we will not insist on editing this issue as systematic and complete collections of research. Many authors decided to write an ordinary research paper rather than an article including systematic accounts. Due to this change in policy, some authors declined to contribute, and the number of papers is now just 12. However, readers will find that the special issue gives an interesting collection of new original research in surface and buried interface studies with x-rays and neutrons. The 12 papers cover the following research topics: (1) polymer analysis by diffuse scattering; (2) discussion of the electrochemical solid--liquid interface by synchrotron x-ray diffraction; (3) analysis of capped nanodots by grazing incidence small-angle x-ray scattering (GISAXS); (4) discussion of the strain distribution in silicon by high-resolution x-ray diffraction; (5) study of mesoporous structures by a combination of x-ray reflectivity and GISAXS; (6) discussion of energy-dispersive x-ray reflectometry and its applications; (7) neutron reflectivity studies on hydrogen terminated silicon interface; (8) the fabrication and performance of a special mirror for water windows; (9) depth selective analysis by total-reflection x-ray diffraction; (10) nanoparticle thin films prepared by a gas deposition technique; (11) discussion of crystal truncation rod (CTR) scattering of semiconductor nanostructures; (12) magnetic structure analysis of thin films by polarized neutron reflectivity. While not discussed in the present special issue, x-ray and neutron techniques have made great progress. The most important steps forward have been in 2D/3D real-space imaging, and realtime measurement. Advances in such technologies are bringing with them new opportunities in surface and buried interface science. In the not too distant future, we will publish a special issue or a book detailing such progress. Exploring surfaces and buried interfaces of functional materials by advanced x-ray and neutron techniques contents Lateral uniformity in chemical composition along a buried reaction front in polymers using off-specular reflectivity Kristopher A Lavery, Vivek M Prabhu, Sushil Satija and Wen-li Wu Orientation dependence of Pd growth on Au electrode surfaces M Takahasi, K Tamura, J Mizuki, T Kondo and K Uosaki A grazing incidence small-angle x-ray scattering analysis on capped Ge nanodots in layer structures Hiroshi Okuda, Masayuki Kato, Keiji Kuno, Shojiro Ochiai, Noritaka Usami, Kazuo Nakajima and Osami Sakata High resolution grazing-incidence in-plane x-ray diffraction for measuring the strain of a Si thin layer Kazuhiko Omote X-ray analysis of mesoporous silica thin films templated by Brij58 surfactant S Fall, M Kulij and A Gibaud Review of the applications of x-ray refraction and the x-ray waveguide phenomenon to estimation of film structures Kouichi Hayashi Epitaxial growth of largely mismatched crystals on H-terminated Si(111) surfaces Hidehito Asaoka Novel TiO2/ZnO multilayer mirrors at 'water-window' wavelengths fabricated by atomic layer epitaxy H Kumagai, Y Tanaka, M Murata, Y Masuda and T Shinagawa Depth-selective structural analysis of thin films using total-external-reflection x-ray diffraction Tomoaki Kawamura and Hiroo Omi Structures of Yb nanoparticle thin films grown by deposition in He and N2 gas atmospheres: AFM and x-ray reflectivity studies Martin Jerab and Kenji Sakurai Ga and As composition profiles in InP/GaInAs/InP heterostructures—x-ray CTR scattering and cross-sectional STM measurements Yoshikazu Takeda, Masao Tabuchi and Arao Nakamura Polarized neutron reflectivity study of a thermally treated MnIr/CoFe exchange bias system Naoki Awaji, Toyoo Miyajima, Shuuichi Doi and Kenji Nomura

The X-Ray Counterpart to LAT PSR J2021+4026 and Its Interesting Spectrum

NASA Technical Reports Server (NTRS)

Weisskopf, Martin C.; Becker, W.; Carraminana, A.; De Luca, A.; Dormandy, M.; Harding, A.; Kanbach, G.; O'Dell, S. L.; Parkinson, P. Saz; Ray, P.;

Airborne particulate matter (PM) filter analysis and modeling by total reflection X-ray fluorescence (TXRF) and X-ray standing wave (XSW).

PubMed

Borgese, L; Salmistraro, M; Gianoncelli, A; Zacco, A; Lucchini, R; Zimmerman, N; Pisani, L; Siviero, G; Depero, L E; Bontempi, E

2012-01-30

This work is presented as an improvement of a recently introduced method for airborne particulate matter (PM) filter analysis [1]. X-ray standing wave (XSW) and total reflection X-ray fluorescence (TXRF) were performed with a new dedicated laboratory instrumentation. The main advantage of performing both XSW and TXRF, is the possibility to distinguish the nature of the sample: if it is a small droplet dry residue, a thin film like or a bulk sample. Another advantage is related to the possibility to select the angle of total reflection to make TXRF measurements. Finally, the possibility to switch the X-ray source allows to measure with more accuracy lighter and heavier elements (with a change in X-ray anode, for example from Mo to Cu). The aim of the present study is to lay the theoretical foundation of the new proposed method for airborne PM filters quantitative analysis improving the accuracy and efficiency of quantification by means of an external standard. The theoretical model presented and discussed demonstrated that airborne PM filters can be considered as thin layers. A set of reference samples is prepared in laboratory and used to obtain a calibration curve. Our results demonstrate that the proposed method for quantitative analysis of air PM filters is affordable and reliable without the necessity to digest filters to obtain quantitative chemical analysis, and that the use of XSW improve the accuracy of TXRF analysis. Copyright © 2011 Elsevier B.V. All rights reserved.

Spectromicroscope for the PHotoelectron Imaging of Nanostructures with X-rays (SPHINX): performance in biology, medicine and geology.

PubMed

Frazer, Bradley H; Girasole, Marco; Wiese, Lisa M; Franz, Torsten; De Stasio, Gelsomina

2004-05-01

Several X-ray PhotoElectron Emission spectroMicroscopes (X-PEEMs) exist around the world at this time. We present recent performance and resolution tests of one of them, the Spectromicroscope for PHotoelectron Imaging of Nanostructures with X-rays (SPHINX) X-PEEM, installed at the University of Wisconsin Synchrotron Radiation Center. With this state-of-the-art instrument we demonstrate chemical analysis capabilities on conducting and insulating specimens of diverse interests, and an unprecedented lateral resolution of 10 nm with monochromatic X-rays and 7.2 nm with ultraviolet illumination.

Publications - GMC 297 | Alaska Division of Geological & Geophysical

Science.gov Websites

DGGS GMC 297 Publication Details Title: X-ray diffraction analysis of cuttings from the: Texaco Inc information. Bibliographic Reference Unknown, 2001, X-ray diffraction analysis of cuttings from the: Texaco

Publications - GMC 43 | Alaska Division of Geological & Geophysical Surveys

Science.gov Websites

DGGS GMC 43 Publication Details Title: X-ray diffraction clay mineralogy analysis of 23 North Slope more information. Bibliographic Reference Unknown, 1983, X-ray diffraction clay mineralogy analysis of

X-Ray Microanalysis and Electron Energy Loss Spectrometry in the Analytical Electron Microscope: Review and Future Directions

NASA Technical Reports Server (NTRS)

Goldstein, J. I.; Williams, D. B.

1992-01-01

This paper reviews and discusses future directions in analytical electron microscopy for microchemical analysis using X-ray and Electron Energy Loss Spectroscopy (EELS). The technique of X-ray microanalysis, using the ratio method and k(sub AB) factors, is outlined. The X-ray absorption correction is the major barrier to the objective of obtaining I% accuracy and precision in analysis. Spatial resolution and Minimum Detectability Limits (MDL) are considered with present limitations of spatial resolution in the 2 to 3 microns range and of MDL in the 0.1 to 0.2 wt. % range when a Field Emission Gun (FEG) system is used. Future directions of X-ray analysis include improvement in X-ray spatial resolution to the I to 2 microns range and MDL as low as 0.01 wt. %. With these improvements the detection of single atoms in the analysis volume will be possible. Other future improvements include the use of clean room techniques for thin specimen preparation, quantification available at the I% accuracy and precision level with light element analysis quantification available at better than the 10% accuracy and precision level, the incorporation of a compact wavelength dispersive spectrometer to improve X-ray spectral resolution, light element analysis and MDL, and instrument improvements including source stability, on-line probe current measurements, stage stability, and computerized stage control. The paper reviews the EELS technique, recognizing that it has been slow to develop and still remains firmly in research laboratories rather than in applications laboratories. Consideration of microanalysis with core-loss edges is given along with a discussion of the limitations such as specimen thickness. Spatial resolution and MDL are considered, recognizing that single atom detection is already possible. Plasmon loss analysis is discussed as well as fine structure analysis. New techniques for energy-loss imaging are also summarized. Future directions in the EELS technique will be the development of new spectrometers and improvements in thin specimen preparation. The microanalysis technique needs to be simplified and software developed so that the EELS technique approaches the relative simplicity of the X-ray technique. Finally, one can expect major improvements in EELS imaging as data storage and processing improvements occur.

Design and mathematical analysis of a three-mirror X-ray telescope based on ATM S-056 X-ray telescope hardware

NASA Technical Reports Server (NTRS)

Foreman, J. W., Jr.; Cardone, J. M.

1973-01-01

The mathematical design of the aspheric third mirror for the three-mirror X-ray telescope (TMXRT) is presented, along with the imaging characteristics of the telescope obtained by a ray trace analysis. The present design effort has been directed entirely toward obtaining an aspheric third mirror which will be compatible with existing S-056 paraboloidal-hyperboloidal mirrors. This compatability will facilitate the construction of a prototype model of the TMXRT, since it will only be necessary to fabricate one new mirror in order to obtain a working model.

Should plain X-rays be routinely performed after blunt knee trauma? A prospective analysis.

PubMed

Jenny, Jean-Yves; Boeri, Cyril; El Amrani, Hakima; Dosch, Jean-Claude; Dupuis, Michel; Moussaoui, Akli; Mairot, Fabrice

2005-06-01

We tested the hypothesis that it was possible to decrease the number of performed x-rays after a knee trauma without delayed fracture diagnosis by using the Ottawa knee rules. Patients had routine x-rays of the injured knee during the first stage of the study and selective x-rays during the second stage. All patients were followed up to 6 months after the trauma. 138 patients were included in the first stage; 57 had negative Ottawa criteria: no fracture was observed; following the Ottawa rules, 41% of the x-rays could have been avoided. 178 patients were included in the second stage; 63 patients had negative Ottawa criteria: no fracture was diagnosed during the whole follow-up; 35% of the x-rays have been avoided. Ottawa rules allowed decreasing the number of x-rays performed after a knee trauma by 35% with a sensitivity for a knee fracture detection of 100%.

Microgravity

NASA Image and Video Library

2000-04-20

Edward Snell, a National Research Council research fellow at NASA's Marshall Space Flight Center (MSFC), prepares a protein crystal for analysis by x-ray crystallography as part of NASA's structural biology program. The small, individual crystals are bombarded with x-rays to produce diffraction patterns, a map of the intensity of the x-rays as they reflect through the crystal.

The Origin of the Extra-nuclear X-ray Emission in the Seyfert Galaxy NGC 2992

NASA Astrophysics Data System (ADS)

Colbert, E. J. M.; Strickland, D. K.; Veilleux, S.; Weaver, K. A.

2004-12-01

We present an analysis of a Chandra ACIS observation of the edge-on Seyfert galaxy NGC 2992. We find extended X-ray emission with Lx(total) in excess of 10**40 erg/s. The brightest nebula is positioned a few 100 pc from the X-ray core, and is spatially coincident with optical line and radio emission. This emission nebula may be energized by the AGN, as opposed to a nuclear starburst. The expected kpc-scale X-ray emission due to a starburst-driven wind is larger than a few 10**39 erg/s, and we present large-scale X-ray emission that may be associated with such an outflow. The extra-nuclear emission has a very soft spectrum. Chandra and XMM spectra of the total nuclear region show a very prominent ``soft excess'' below 2-3 keV. We shall discuss the spectral properties of this soft excess, and will compare with the results from the spatial analysis, and with AGN and starburst models for extranuclear X-ray nebulae.

SPECTRAL ANALYSIS IN ORBITAL/SUPERORBITAL PHASE SPACE AND HINTS OF SUPERORBITAL VARIABILITY IN THE HARD X-RAYS OF LS I +61°303

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Jian; Torres, Diego F.; Zhang, Shu

2014-04-10

We present an INTEGRAL spectral analysis in the orbital/superorbital phase space of LS I +61°303. A hard X-ray spectrum with no cutoff is observed at all orbital/superorbital phases. The hard X-ray index is found to be uncorrelated with the radio index (non-simultaneously) measured at the same orbital and superorbital phases. In particular, the absence of an X-ray spectrum softening during periods of negative radio index does not favor a simple interpretation of the radio index variations in terms of a microquasar's changes of state. We uncover hints of superorbital variability in the hard X-ray flux, in phase with the superorbitalmore » modulation in soft X-rays. An orbital phase drift of the radio peak flux and index along the superorbital period is observed in the radio data. We explore its influence on a previously reported double-peak structure of a radio orbital light curve, and present it as a plausible explanation.« less

X-ray power and yield measurements at the refurbished Z machine

DOE PAGES

Jones, M. C.; Ampleford, D. J.; Cuneo, M. E.; ...

2014-08-04

Advancements have been made in the diagnostic techniques to measure accurately the total radiated x-ray yield and power from z-pinch loads at the Z Machine with high accuracy. The Z-accelerator is capable of outputting 2MJ and 330 TW of x-ray yield and power, and accurately measuring these quantities is imperative. We will describe work over the past several years which include the development of new diagnostics, improvements to existing diagnostics, and implementation of automated data analysis routines. A set of experiments were conducted on the Z machine where the load and machine configuration were held constant. During this shot series,more » it was observed that total z-pinch x-ray emission power determined from the two common techniques for inferring the x-ray power, Kimfol filtered x-ray diode diagnostic and the Total Power and Energy diagnostic gave 450 TW and 327 TW respectively. Our analysis shows the latter to be the more accurate interpretation. More broadly, the comparison demonstrates the necessity to consider spectral response and field of view when inferring xray powers from z-pinch sources.« less

The 300 Kpc Long X-Ray Jet in PKS 1127-145, Z=1.18 Quasar: Constraining X-Ray Emission Models

DOE Office of Scientific and Technical Information (OSTI.GOV)

Siemiginowska, Aneta; /Harvard-Smithsonian Ctr. Astrophys.; Stawarz, Lukasz

2006-11-20

We present a {approx} 100 ksec Chandra X-ray observation and new VLA radio data of the large scale, 300 kpc long X-ray jet in PKS 1127-145, a radio loud quasar at redshift z=1.18. With this deep X-ray observation we now clearly discern the complex X-ray jet morphology and see substructure within the knots. The X-ray and radio jet intensity profiles are seen to be strikingly different with the radio emission peaking strongly at the two outer knots while the X-ray emission is strongest in the inner jet region. The jet X-ray surface brightness gradually decreases by an order of magnitudemore » going out from the core. The new X-ray data contain sufficient counts to do spectral analysis of the key jet features. The X-ray energy index of the inner jet is relatively flat with {alpha}{sub x} = 0.66 {+-} 0.15 and steep in the outer jet with {alpha}{sub x} = 1.0 {+-} 0.2. We discuss the constraints implied by the new data on the X-ray emission models and conclude that ''one-zone'' models fail and at least a two component model is needed to explain the jet's broad-band emission. We propose that the X-ray emission originates in the jet proper while the bulk of the radio emission comes from a surrounding jet sheath. We also consider intermittent jet activity as a possible cause of the observed jet morphology.« less

Anisotropy enhanced X-ray scattering from solvated transition metal complexes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Biasin, Elisa; van Driel, Tim B.; Levi, Gianluca

Time-resolved X-ray scattering patterns from photoexcited molecules in solution are in many cases anisotropic at the ultrafast time scales accessible at X-ray free-electron lasers (XFELs). This anisotropy arises from the interaction of a linearly polarized UV–Vis pump laser pulse with the sample, which induces anisotropic structural changes that can be captured by femtosecond X-ray pulses. In this work, a method for quantitative analysis of the anisotropic scattering signal arising from an ensemble of molecules is described, and it is demonstrated how its use can enhance the structural sensitivity of the time-resolved X-ray scattering experiment. This method is applied on time-resolvedmore » X-ray scattering patterns measured upon photoexcitation of a solvated di-platinum complex at an XFEL, and the key parameters involved are explored. Here it is shown that a combined analysis of the anisotropic and isotropic difference scattering signals in this experiment allows a more precise determination of the main photoinduced structural change in the solute,i.e.the change in Pt—Pt bond length, and yields more information on the excitation channels than the analysis of the isotropic scattering only. Finally, it is discussed how the anisotropic transient response of the solvent can enable the determination of key experimental parameters such as the instrument response function.« less

Anisotropy enhanced X-ray scattering from solvated transition metal complexes

DOE PAGES

Biasin, Elisa; van Driel, Tim B.; Levi, Gianluca; ...

2018-02-13

Time-resolved X-ray scattering patterns from photoexcited molecules in solution are in many cases anisotropic at the ultrafast time scales accessible at X-ray free-electron lasers (XFELs). This anisotropy arises from the interaction of a linearly polarized UV–Vis pump laser pulse with the sample, which induces anisotropic structural changes that can be captured by femtosecond X-ray pulses. In this work, a method for quantitative analysis of the anisotropic scattering signal arising from an ensemble of molecules is described, and it is demonstrated how its use can enhance the structural sensitivity of the time-resolved X-ray scattering experiment. This method is applied on time-resolvedmore » X-ray scattering patterns measured upon photoexcitation of a solvated di-platinum complex at an XFEL, and the key parameters involved are explored. Here it is shown that a combined analysis of the anisotropic and isotropic difference scattering signals in this experiment allows a more precise determination of the main photoinduced structural change in the solute,i.e.the change in Pt—Pt bond length, and yields more information on the excitation channels than the analysis of the isotropic scattering only. Finally, it is discussed how the anisotropic transient response of the solvent can enable the determination of key experimental parameters such as the instrument response function.« less

Correlative analysis of hard and soft x ray observations of solar flares

NASA Technical Reports Server (NTRS)

Zarro, Dominic M.

1994-01-01

We have developed a promising new technique for jointly analyzing BATSE hard X-ray observations of solar flares with simultaneous soft X-ray observations. The technique is based upon a model in which electric currents and associated electric fields are responsible for the respective heating and particle acceleration that occur in solar flares. A useful by-product of this technique is the strength and evolution of the coronal electric field. The latter permits one to derive important flare parameters such as the current density, the number of current filaments composing the loop, and ultimately the hard X-ray spectrum produced by the runaway electrons. We are continuing to explore the technique by applying it to additional flares for which we have joint BATSE/Yohkoh observations. A central assumption of our analysis is the constant of proportionality alpha relating the hard X-ray flux above 50 keV and the rate of electron acceleration. For a thick-target model of hard X-ray production, it can be shown that cv is in fact related to the spectral index and low-energy cutoff of precipitating electrons. The next step in our analysis is to place observational constraints on the latter parameters using the joint BATSE/Yohkoh data.

X-RAY SOURCES IN THE DWARF SPHEROIDAL GALAXY DRACO

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sonbas, E.; Rangelov, B.; Kargaltsev, O.

2016-04-10

We present the spectral analysis of an 87 ks XMM-Newton observation of Draco, a nearby dwarf spheroidal galaxy. Of the approximately 35 robust X-ray source detections, we focus our attention on the brightest of these sources, for which we report X-ray and multiwavelength parameters. While most of the sources exhibit properties consistent with active galactic nuclei, few of them possess the characteristics of low-mass X-ray binaries (LMXBs) and cataclysmic variable (CVs). Our analysis places constraints on the population of X-ray sources with L{sub X} > 3 × 10{sup 33} erg s{sup −1} in Draco, suggesting that there are no actively accreting black hole andmore » neutron star binaries. However, we find four sources that could be quiescent state LMXBs/CVs associated with Draco. We also place constraints on the central black hole luminosity and on a dark matter decay signal around 3.5 keV.« less

A high-transparency, micro-patternable chip for X-ray diffraction analysis of microcrystals under native growth conditions

DOE PAGES

Murray, Thomas D.; Lyubimov, Artem Y.; Ogata, Craig M.; ...

2015-08-11

Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common laboratory formats and delivering them to an X-ray beam source under native growth conditions. One approach that shows promise in overcoming the challenges intrinsic to microcrystal analysis is to pair so-called `fixed-target' sample-delivery devices with microbeam-based X-ray diffraction methods. However, to record weak diffraction patterns it is necessarymore » to fabricate devices from X-ray-transparent materials that minimize background scattering. Presented here is the design of a new micro-diffraction device consisting of three layers fabricated from silicon nitride, photoresist and polyimide film. The chip features low X-ray scattering and X-ray absorption properties, and uses a customizable blend of hydrophobic and hydrophilic surface patterns to help localize microcrystals to defined regions. Microcrystals in their native growth conditions can be loaded into the chips with a standard pipette, allowing data collection at room temperature. Diffraction data collected from hen egg-white lysozyme microcrystals (10–15 µm) loaded into the chips yielded a complete, high-resolution (<1.6 Å) data set sufficient to determine a high-quality structure by molecular replacement. In addition, the features of the chip allow the rapid and user-friendly analysis of microcrystals grown under virtually any laboratory format at microfocus synchrotron beamlines and XFELs.« less

A high-transparency, micro-patternable chip for X-ray diffraction analysis of microcrystals under native growth conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Murray, Thomas D.; Lyubimov, Artem Y.; Ogata, Craig M.

Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common laboratory formats and delivering them to an X-ray beam source under native growth conditions. One approach that shows promise in overcoming the challenges intrinsic to microcrystal analysis is to pair so-called `fixed-target' sample-delivery devices with microbeam-based X-ray diffraction methods. However, to record weak diffraction patterns it is necessarymore » to fabricate devices from X-ray-transparent materials that minimize background scattering. Presented here is the design of a new micro-diffraction device consisting of three layers fabricated from silicon nitride, photoresist and polyimide film. The chip features low X-ray scattering and X-ray absorption properties, and uses a customizable blend of hydrophobic and hydrophilic surface patterns to help localize microcrystals to defined regions. Microcrystals in their native growth conditions can be loaded into the chips with a standard pipette, allowing data collection at room temperature. Diffraction data collected from hen egg-white lysozyme microcrystals (10–15 µm) loaded into the chips yielded a complete, high-resolution (<1.6 Å) data set sufficient to determine a high-quality structure by molecular replacement. In addition, the features of the chip allow the rapid and user-friendly analysis of microcrystals grown under virtually any laboratory format at microfocus synchrotron beamlines and XFELs.« less

A high-transparency, micro-patternable chip for X-ray diffraction analysis of microcrystals under native growth conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Murray, Thomas D.; Lyubimov, Artem Y.; Ogata, Craig M.

Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2µl) of microcrystals grown under common laboratory formats and delivering them to an X-ray beam source under native growth conditions. One approach that shows promise in overcoming the challenges intrinsic to microcrystal analysis is to pair so-called `fixed-target' sample-delivery devices with microbeam-based X-ray diffraction methods. However, to record weak diffraction patterns it is necessary tomore » fabricate devices from X-ray-transparent materials that minimize background scattering. Presented here is the design of a new micro-diffraction device consisting of three layers fabricated from silicon nitride, photoresist and polyimide film. The chip features low X-ray scattering and X-ray absorption properties, and uses a customizable blend of hydrophobic and hydrophilic surface patterns to help localize microcrystals to defined regions. Microcrystals in their native growth conditions can be loaded into the chips with a standard pipette, allowing data collection at room temperature. Diffraction data collected from hen egg-white lysozyme microcrystals (10–15µm) loaded into the chips yielded a complete, high-resolution (<1.6Å) data set sufficient to determine a high-quality structure by molecular replacement. The features of the chip allow the rapid and user-friendly analysis of microcrystals grown under virtually any laboratory format at microfocus synchrotron beamlines and XFELs.« less

A high-transparency, micro-patternable chip for X-ray diffraction analysis of microcrystals under native growth conditions

PubMed Central

Murray, Thomas D.; Lyubimov, Artem Y.; Ogata, Craig M.; Vo, Huy; Uervirojnangkoorn, Monarin; Brunger, Axel T.; Berger, James M.

2015-01-01

Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common laboratory formats and delivering them to an X-ray beam source under native growth conditions. One approach that shows promise in overcoming the challenges intrinsic to microcrystal analysis is to pair so-called ‘fixed-target’ sample-delivery devices with microbeam-based X-ray diffraction methods. However, to record weak diffraction patterns it is necessary to fabricate devices from X-ray-transparent materials that minimize background scattering. Presented here is the design of a new micro-diffraction device consisting of three layers fabricated from silicon nitride, photoresist and polyimide film. The chip features low X-ray scattering and X-ray absorption properties, and uses a customizable blend of hydrophobic and hydrophilic surface patterns to help localize microcrystals to defined regions. Microcrystals in their native growth conditions can be loaded into the chips with a standard pipette, allowing data collection at room temperature. Diffraction data collected from hen egg-white lysozyme microcrystals (10–15 µm) loaded into the chips yielded a complete, high-resolution (<1.6 Å) data set sufficient to determine a high-quality structure by molecular replacement. The features of the chip allow the rapid and user-friendly analysis of microcrystals grown under virtually any laboratory format at microfocus synchrotron beamlines and XFELs. PMID:26457423

Probing the extent of the non-thermal emission from the Vela X region at TeV energies with H.E.S.S.

NASA Astrophysics Data System (ADS)

Abramowski, A.; Acero, F.; Aharonian, F.; Akhperjanian, A. G.; Anton, G.; Balenderan, S.; Balzer, A.; Barnacka, A.; Becherini, Y.; Becker Tjus, J.; Bernlöhr, K.; Birsin, E.; Biteau, J.; Bochow, A.; Boisson, C.; Bolmont, J.; Bordas, P.; Brucker, J.; Brun, F.; Brun, P.; Bulik, T.; Carrigan, S.; Casanova, S.; Cerruti, M.; Chadwick, P. M.; Charbonnier, A.; Chaves, R. C. G.; Cheesebrough, A.; Cologna, G.; Conrad, J.; Couturier, C.; Dalton, M.; Daniel, M. K.; Davids, I. D.; Degrange, B.; Deil, C.; deWilt, P.; Dickinson, H. J.; Djannati-Ataï, A.; Domainko, W.; Drury, L. O.' C.; Dubois, F.; Dubus, G.; Dutson, K.; Dyks, J.; Dyrda, M.; Egberts, K.; Eger, P.; Espigat, P.; Fallon, L.; Farnier, C.; Fegan, S.; Feinstein, F.; Fernandes, M. V.; Fernandez, D.; Fiasson, A.; Fontaine, G.; Förster, A.; Füßling, M.; Gajdus, M.; Gallant, Y. A.; Garrigoux, T.; Gast, H.; Giebels, B.; Glicenstein, J. F.; Glück, B.; Göring, D.; Grondin, M.-H.; Häffner, S.; Hague, J. D.; Hahn, J.; Hampf, D.; Harris, J.; Heinz, S.; Heinzelmann, G.; Henri, G.; Hermann, G.; Hillert, A.; Hinton, J. A.; Hofmann, W.; Hofverberg, P.; Holler, M.; Horns, D.; Jacholkowska, A.; Jahn, C.; Jamrozy, M.; Jung, I.; Kastendieck, M. A.; Katarzyński, K.; Katz, U.; Kaufmann, S.; Khélifi, B.; Klochkov, D.; Kluźniak, W.; Kneiske, T.; Komin, Nu.; Kosack, K.; Kossakowski, R.; Krayzel, F.; Krüger, P. P.; Laffon, H.; Lamanna, G.; Lenain, J.-P.; Lennarz, D.; Lohse, T.; Lopatin, A.; Lu, C.-C.; Marandon, V.; Marcowith, A.; Masbou, J.; Maurin, G.; Maxted, N.; Mayer, M.; McComb, T. J. L.; Medina, M. C.; Méhault, J.; Menzler, U.; Moderski, R.; Mohamed, M.; Moulin, E.; Naumann, C. L.; Naumann-Godo, M.; de Naurois, M.; Nedbal, D.; Nguyen, N.; Niemiec, J.; Nolan, S. J.; Ohm, S.; de Oña Wilhelmi, E.; Opitz, B.; Ostrowski, M.; Oya, I.; Panter, M.; Parsons, D.; Paz Arribas, M.; Pekeur, N. W.; Pelletier, G.; Perez, J.; Petrucci, P.-O.; Peyaud, B.; Pita, S.; Pühlhofer, G.; Punch, M.; Quirrenbach, A.; Raue, M.; Reimer, A.; Reimer, O.; Renaud, M.; de los Reyes, R.; Rieger, F.; Ripken, J.; Rob, L.; Rosier-Lees, S.; Rowell, G.; Rudak, B.; Rulten, C. B.; Sahakian, V.; Sanchez, D. A.; Santangelo, A.; Schlickeiser, R.; Schulz, A.; Schwanke, U.; Schwarzburg, S.; Schwemmer, S.; Sheidaei, F.; Skilton, J. L.; Sol, H.; Spengler, G.; Stawarz, Ł.; Steenkamp, R.; Stegmann, C.; Stinzing, F.; Stycz, K.; Sushch, I.; Szostek, A.; Tavernet, J.-P.; Terrier, R.; Tluczykont, M.; Trichard, C.; Valerius, K.; van Eldik, C.; Vasileiadis, G.; Venter, C.; Viana, A.; Vincent, P.; Völk, H. J.; Volpe, F.; Vorobiov, S.; Vorster, M.; Wagner, S. J.; Ward, M.; White, R.; Wierzcholska, A.; Wouters, D.; Zacharias, M.; Zajczyk, A.; Zdziarski, A. A.; Zech, A.; Zechlin, H.-S.

2012-12-01

Context. Vela X is a region of extended radio emission in the western part of the Vela constellation: one of the nearest pulsar wind nebulae, and associated with the energetic Vela pulsar (PSR B0833-45). Extended very-high-energy (VHE) γ-ray emission (HESS J0835-455) was discovered using the H.E.S.S. experiment in 2004. The VHE γ-ray emission was found to be coincident with a region of X-ray emission discovered with ROSAT above 1.5 keV (the so-called Vela X cocoon): a filamentary structure extending southwest from the pulsar to the centre of Vela X. Aims: A deeper observation of the entire Vela X nebula region, also including larger offsets from the cocoon, has been performed with H.E.S.S. This re-observation was carried out in order to probe the extent of the non-thermal emission from the Vela X region at TeV energies and to investigate its spectral properties. Methods: To increase the sensitivity to the faint γ-ray emission from the very extended Vela X region, a multivariate analysis method combining three complementary reconstruction techniques of Cherenkov-shower images is applied for the selection of γ-ray events. The analysis is performed with the On/Off background method, which estimates the background from separate observations pointing away from Vela X; towards regions free of γ-ray sources but with comparable observation conditions. Results: The γ-ray surface brightness over the large Vela X region reveals that the detection of non-thermal VHE γ-ray emission from the PWN HESS J0835-455 is statistically significant over a region of radius 1.2° around the position α = 08h35m00s, δ = -45°36'00'' (J2000). The Vela X region exhibits almost uniform γ-ray spectra over its full extent: the differential energy spectrum can be described by a power-law function with a hard spectral index Γ = 1.32 ± 0.06stat ± 0.12sys and an exponential cutoff at an energy of (14.0 ± 1.6stat ± 2.6sys) TeV. Compared to the previous H.E.S.S. observations of Vela X the new analysis confirms the general spatial overlap of the bulk of the VHE γ-ray emission with the X-ray cocoon, while its extent and morphology appear more consistent with the (more extended) radio emission, contradicting the simple correspondence between VHE γ-ray and X-ray emissions. Morphological and spectral results challenge the interpretation of the origin of γ-ray emission in the GeV and TeV ranges in the framework of current models.

Comet composition and density analyzer

NASA Technical Reports Server (NTRS)

Clark, B. C.

1982-01-01

Distinctions between cometary material and other extraterrestrial materials (meteorite suites and stratospherically-captured cosmic dust) are addressed. The technique of X-ray fluorescence (XRF) for analysis of elemental composition is involved. Concomitant with these investigations, the problem of collecting representative samples of comet dust (for rendezvous missions) was solved, and several related techniques such as mineralogic analysis (X-ray diffraction), direct analysis of the nucleus without docking (electron macroprobe), dust flux rate measurement, and test sample preparation were evaluated. An explicit experiment concept based upon X-ray fluorescence analysis of biased and unbiased sample collections was scoped and proposed for a future rendezvous mission with a short-period comet.

SAVLOC, computer program for automatic control and analysis of X-ray fluorescence experiments

NASA Technical Reports Server (NTRS)

Leonard, R. F.

1977-01-01

A program for a PDP-15 computer is presented which provides for control and analysis of trace element determinations by using X-ray fluorescence. The program simultaneously handles data accumulation for one sample and analysis of data from previous samples. Data accumulation consists of sample changing, timing, and data storage. Analysis requires the locating of peaks in X-ray spectra, determination of intensities of peaks, identification of origins of peaks, and determination of a real density of the element responsible for each peak. The program may be run in either a manual (supervised) mode or an automatic (unsupervised) mode.

Application of relativistic electrons for the quantitative analysis of trace elements

NASA Astrophysics Data System (ADS)

Hoffmann, D. H. H.; Brendel, C.; Genz, H.; Löw, W.; Richter, A.

1984-04-01

Particle induced X-ray emission methods (PIXE) have been extended to relativistic electrons to induce X-ray emission (REIXE) for quantitative trace-element analysis. The electron beam (20 ≤ E0≤ 70 MeV) was supplied by the Darmstadt electron linear accelerator DALINAC. Systematic measurements of absolute K-, L- and M-shell ionization cross sections revealed a scaling behaviour of inner-shell ionization cross sections from which X-ray production cross sections can be deduced for any element of interest for a quantitative sample investigation. Using a multielemental mineral monazite sample from Malaysia the sensitivity of REIXE is compared to well established methods of trace-element analysis like proton- and X-ray-induced X-ray fluorescence analysis. The achievable detection limit for very heavy elements amounts to about 100 ppm for the REIXE method. As an example of an application the investigation of a sample prepared from manganese nodules — picked up from the Pacific deep sea — is discussed, which showed the expected high mineral content of Fe, Ni, Cu and Ti, although the search for aliquots of Pt did not show any measurable content within an upper limit of 250 ppm.

Composition analysis of a polymer electrolyte membrane fuel cell microporous layer using scanning transmission X-ray microscopy and near edge X-ray absorption fine structure analysis

NASA Astrophysics Data System (ADS)

George, Michael G.; Wang, Jian; Banerjee, Rupak; Bazylak, Aimy

2016-03-01

The novel application of scanning transmission X-ray microscopy (STXM) to the microporous layer (MPL) of a polymer electrolyte membrane fuel cell is investigated. A spatially resolved chemical component distribution map is obtained for the MPL of a commercially available SGL 25 BC sample. This is achieved with near edge X-ray absorption fine structure spectroscopic analysis. Prior to analysis the sample is embedded in non-reactive epoxy and ultra-microtomed to a thickness of 100 nm. Polytetrafluoroethylene (PTFE), carbon particle agglomerates, and supporting epoxy resin distributions are identified and reconstructed for a scanning area of 6 μm × 6 μm. It is observed that the spatial distribution of PTFE is strongly correlated to the carbon particle agglomerations. Additionally, agglomerate structures of PTFE are identified, possibly indicating the presence of a unique mesostructure in the MPL. STXM analysis is presented as a useful technique for the investigation of chemical species distributions in the MPL.

The Chandra X-ray Observatory: An Astronomical Facility Available to the World

NASA Technical Reports Server (NTRS)

Smith, Randall K.

2006-01-01

The Chandra X-ray observatory, one of NASA's "Great Observatories," provides high angular and spectral resolution X-ray data which is freely available to all. In this review I describe the instruments on chandra along with their current calibration, as well as the chandra proposal system, the freely-available Chandra analysis software package CIAO, and the Chandra archive. As Chandra is in its 6th year of operation, the archive already contains calibrated observations of a large range of X-ray sources. The Chandra X-ray Center is committed to assisting astronomers from any country who wish to use data from the archive or propose for observations

Synchrotron X-Ray Diffraction Analysis of Meteorites in Thin Section: Preliminary Results

NASA Technical Reports Server (NTRS)

Treiman, A. H.; Lanzirotti, A.; Xirouchakis, D.

2004-01-01

X-ray diffraction is the pre-eminent technique for mineral identification and structure determination, but is difficult to apply to grains in thin section, the standard meteorite preparation. Bright focused X-ray beams from synchrotrons have been used extensively in mineralogy and have been applied to extraterrestrial particles. The intensity and small spot size achievable in synchrotron X-ray beams makes them useful for study of materials in thin sections. Here, we describe Synchrotron X-ray Diffraction (SXRD) in thin section as done at the National Synchrotron Light Source, and cite examples of its value for studies of meteorites in thin section.

Industrial applications of automated X-ray inspection

NASA Astrophysics Data System (ADS)

Shashishekhar, N.

2015-03-01

Many industries require that 100% of manufactured parts be X-ray inspected. Factors such as high production rates, focus on inspection quality, operator fatigue and inspection cost reduction translate to an increasing need for automating the inspection process. Automated X-ray inspection involves the use of image processing algorithms and computer software for analysis and interpretation of X-ray images. This paper presents industrial applications and illustrative case studies of automated X-ray inspection in areas such as automotive castings, fuel plates, air-bag inflators and tires. It is usually necessary to employ application-specific automated inspection strategies and techniques, since each application has unique characteristics and interpretation requirements.

BL-Lacs in X-Ray Outburst

NASA Technical Reports Server (NTRS)

Remillard, Ronald A.; Urry, C. Megan; Aharonian, Felix; Pian, Elena; Sambruna, Rita; Coppi, Paolo

2000-01-01

We conducted a multifrequency campaign for the TeV blazar Markarian 421 in 1998 April. The campaign started from a pronounced high-amplitude flare recorded by BeppoSAX and Whipple; the Advanced Satellite for Cosmology and Astrophysics (ASCA) observation started three days later. In the X-ray data, we detected multiple flares, occurring on timescales of about one day. ASCA data clearly reveal spectral variability. The comparison of the data from ASCA, the Extreme Ultraviolet Explorer, and the Rossi X-Ray Timing Explorer indicates that the variability amplitudes in the low-energy synchrotron component are larger at higher photon energies. In TeV and gamma-rays, large intraday variations-which were correlated with the X-ray flux-were observed when results from three Cerenkov telescopes were combined. The rms variability of TeV and gamma-rays was similar to that observed in hard X-rays, above ten keV. The X-ray light curve reveals flares that are almost symmetric for most cases, implying that the dominant timescale is the light crossing time through the emitting region. The structure function analysis based on the continuous X-ray light curve of seven days indicates that the characteristic timescale is approx. 0.5 days. The analysis of ASCA light curves in various energy bands appears to show both soft (positive) and hard (negative) lags. These may not be real, as systematic effects could also produce these lags, which are all much smaller than an orbit. If the lags of both signs are real, these imply that the particle acceleration and X-ray cooling timescales are similar.

Analysis and interpretation of diffuse x-ray emission using data from the Einstein satellite

NASA Technical Reports Server (NTRS)

Helfand, David J.

1991-01-01

An ambitious program to create a powerful and accessible archive of the HEAO-2 Imaging Proportional Counter (IPC) database was outlined. The scientific utility of that database for studies of diffuse x ray emissions was explored. Technical and scientific accomplishments are reviewed. Three papers were presented which have major new scientific findings relevant to the global structure of the interstellar medium and the origin of the cosmic x ray background. An all-sky map of diffuse x ray emission was constructed.

X-ray and optical observations of 2 new cataclysmic variables

NASA Technical Reports Server (NTRS)

Singh, K. P.; Szkody, P.; Barrett, P.; Schlegel, E.; White, N. E.; Silber, A.; Fierce, E.; Hoard, D.; Hakala, P. J.; Piirola, V.;

Quality assessment of digital X-ray chest images using an anthropomorphic chest phantom

NASA Astrophysics Data System (ADS)

Vodovatov, A. V.; Kamishanskaya, I. G.; Drozdov, A. A.; Bernhardsson, C.

2017-02-01

The current study is focused on determining the optimal tube voltage for the conventional X-ray digital chest screening examinations, using a visual grading analysis method. Chest images of an anthropomorphic phantom were acquired in posterior-anterior projection on four digital X-ray units with different detector types. X-ray images obtained with an anthropomorphic phantom were accepted by the radiologists as corresponding to a normal human anatomy, hence allowing using phantoms in image quality trials without limitations.

Applications of High Throughput (Combinatorial) Methodologies to Electronic, Magnetic, Optical, and Energy-Related Materials

DTIC Science & Technology

2013-06-17

of the films without having to fabricate capacitors. In addition, the use of X - ray diffraction (XRD) analysis enabled Chikyow et al.40 to identify an...effects of Al doping and annealing on the thermal stabil- ity of the Y2O3/Si gate stack were studied by X - ray photoemission spectroscopy (XPS) and X - ray ...the major diffraction features in the phase distribution. For a given structural phase, the X - ray peak intensity allows one to track the compositional

Structural studies of liquid Co–Sn alloys

PubMed Central

Yakymovych, A.; Shtablavyi, I.; Mudry, S.

2014-01-01

An analysis of the structure features of liquid Co–Sn alloys has been performed by means of X-ray diffraction method, viscosity coefficient analysis and computer simulation method. The X-ray diffraction investigations were carried out over a wide concentration range at the temperature 1473 K. It was found that the structure of these alloys can be described in the frame of independent X-ray scattering model. The viscosity coefficient was calculated by an excess entropy scaling and compared with experimental data. PMID:25328282

Synthesis of samarium doped gadolinium oxide nanorods, its spectroscopic and physical properties

NASA Astrophysics Data System (ADS)

Boopathi, G.; Gokul Raj, S.; Ramesh Kumar, G.; Mohan, R.; Mohan, S.

2018-06-01

One-dimensional samarium doped gadolinium oxide [Sm:Gd2O3] nanorods have been synthesized successfully through co-precipitation technique in aqueous solution. The as-synthesized and calcined products were characterized by using powder X-ray diffraction pattern, Fourier transform Raman spectroscopy, thermogravimetric/differential thermal analysis, scanning electron microscopy with energy-dispersive X-ray analysis, transmission electron microscopy, Fourier transform infrared spectroscopy, Ultraviolet-Visible spectrometry, photoluminescence spectrophotometer and X-ray photoelectron spectroscopy techniques. The obtained results are discussed in detailed manner.

Weak hard X-ray emission from broad absorption line quasars: evidence for intrinsic X-ray weakness

DOE Office of Scientific and Technical Information (OSTI.GOV)

Luo, B.; Brandt, W. N.; Scott, A. E.

We report NuSTAR observations of a sample of six X-ray weak broad absorption line (BAL) quasars. These targets, at z = 0.148-1.223, are among the optically brightest and most luminous BAL quasars known at z < 1.3. However, their rest-frame ≈2 keV luminosities are 14 to >330 times weaker than expected for typical quasars. Our results from a pilot NuSTAR study of two low-redshift BAL quasars, a Chandra stacking analysis of a sample of high-redshift BAL quasars, and a NuSTAR spectral analysis of the local BAL quasar Mrk 231 have already suggested the existence of intrinsically X-ray weak BAL quasars,more » i.e., quasars not emitting X-rays at the level expected from their optical/UV emission. The aim of the current program is to extend the search for such extraordinary objects. Three of the six new targets are weakly detected by NuSTAR with ≲ 45 counts in the 3-24 keV band, and the other three are not detected. The hard X-ray (8-24 keV) weakness observed by NuSTAR requires Compton-thick absorption if these objects have nominal underlying X-ray emission. However, a soft stacked effective photon index (Γ{sub eff} ≈ 1.8) for this sample disfavors Compton-thick absorption in general. The uniform hard X-ray weakness observed by NuSTAR for this and the pilot samples selected with <10 keV weakness also suggests that the X-ray weakness is intrinsic in at least some of the targets. We conclude that the NuSTAR observations have likely discovered a significant population (≳ 33%) of intrinsically X-ray weak objects among the BAL quasars with significantly weak <10 keV emission. We suggest that intrinsically X-ray weak quasars might be preferentially observed as BAL quasars.« less

Multiscale tomographic analysis of heterogeneous cast Al-Si-X alloys.

PubMed

Asghar, Z; Requena, G; Sket, F

2015-07-01

The three-dimensional microstructure of cast AlSi12Ni and AlSi10Cu5Ni2 alloys is investigated by laboratory X-ray computed tomography, synchrotron X-ray computed microtomography, light optical tomography and synchrotron X-ray computed microtomography with submicrometre resolution. The results obtained with each technique are correlated with the size of the scanned volumes and resolved microstructural features. Laboratory X-ray computed tomography is sufficient to resolve highly absorbing aluminides but eutectic and primary Si remain unrevealed. Synchrotron X-ray computed microtomography at ID15/ESRF gives better spatial resolution and reveals primary Si in addition to aluminides. Synchrotron X-ray computed microtomography at ID19/ESRF reveals all the phases ≥ ∼1 μm in volumes about 80 times smaller than laboratory X-ray computed tomography. The volumes investigated by light optical tomography and submicrometre synchrotron X-ray computed microtomography are much smaller than laboratory X-ray computed tomography but both techniques provide local chemical information on the types of aluminides. The complementary techniques applied enable a full three-dimensional characterization of the microstructure of the alloys at length scales ranging over six orders of magnitude. © 2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.

Electronic and atomic structures of Ti{sub 1-x}Al{sub x}N thin films related to their damage behavior

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tuilier, M.-H.; Pac, M.-J.; Girleanu, M.

2008-04-15

Ti and Al K-edge x-ray absorption spectroscopy is used to investigate the electronic structure of Ti{sub 1-x}Al{sub x}N thin films deposited by reactive magnetron sputtering. The experimental near edge spectra of TiN and AlN are interpreted in the light of unoccupied density of state band structure calculations. The comparison of the structural parameters derived from x-ray absorption fine structure and x-ray diffraction reveals segregation between Al-rich and Ti-rich domains within the Ti{sub 1-x}Al{sub x}N films. Whereas x-ray diffraction probes only the crystallized domains, the structural information derived from extended x-ray absorption fine structure analysis turns on both crystalline and grainmore » boundaries. The results are discussed by considering the damage behavior of the films depending on the composition.« less

Formation and Evolution of X-ray Binaries

NASA Astrophysics Data System (ADS)

Fragkos, Anastasios

X-ray binaries - mass-transferring binary stellar systems with compact object accretors - are unique astrophysical laboratories. They carry information about many complex physical processes such as star formation, compact object formation, and evolution of interacting binaries. My thesis work involves the study of the formation and evolution of Galactic and extra-galacticX-ray binaries using both detailed and realistic simulation tools, and population synthesis techniques. I applied an innovative analysis method that allows the reconstruction of the full evolutionary history of known black hole X-ray binaries back to the time of compact object formation. This analysis takes into account all the available observationally determined properties of a system, and models in detail four of its evolutionary evolutionary phases: mass transfer through the ongoing X-ray phase, tidal evolution before the onset of Roche-lobe overflow, motion through the Galactic potential after the formation of the black hole, and binary orbital dynamics at the time of core collapse. Motivated by deep extra-galactic Chandra survey observations, I worked on population synthesis models of low-mass X-ray binaries in the two elliptical galaxies NGC3379 and NGC4278. These simulations were targeted at understanding the origin of the shape and normalization of the observed X-ray luminosity functions. In a follow up study, I proposed a physically motivated prescription for the modeling of transient neutron star low-mass X-ray binary properties, such as duty cycle, outburst duration and recurrence time. This prescription enabled the direct comparison of transient low-mass X-ray binary population synthesis models to the Chandra X-ray survey of the two ellipticals NGC3379 and NGC4278. Finally, I worked on population synthesismodels of black holeX-ray binaries in the MilkyWay. This work was motivated by recent developments in observational techniques for the measurement of black hole spin magnitudes in black hole X-ray binaries. The accuracy of these techniques depend on misalignment of the black hole spin with respect to the orbital angular momentum. In black hole X-ray binaries, this misalignment can occur during the supernova explosion that forms the compact object. In this study, I presented population synthesis models of Galactic black hole X-ray binaries, and examined the distribution of misalignment angles, and its dependence on the model parameters.

A catalogue of optical to X-ray spectral energy distributions of z ≈ 2 quasars observed with Swift - I. First results

NASA Astrophysics Data System (ADS)

Lawther, D.; Vestergaard, M.; Raimundo, S.; Grupe, D.

2017-06-01

We present the Swift optical to X-ray spectral energy distributions (SEDs) of 44 quasars at redshifts z ≈ 2 observed by Swift, part of a larger program to establish and characterize the optical through X-ray SEDs of moderate-redshift quasars. Here, we outline our analysis approach and present preliminary analysis and results for the first third of the full quasar sample. Not all quasars in the sample are detected in X-rays; all of the X-ray-detected objects so far are radio loud. As expected for radio-loud objects, they are X-ray bright relative to radio-quiet quasars of comparable optical luminosities, with an average αox =1.39 ± 0.03 (where αox is the power-law slope connecting the monochromatic flux at 2500 Å and at 2 keV), and display hard X-ray spectra. We find integrated 3000 Å-25 keV accretion luminosities of between 0.7 × 1046 erg s-1 and 5.2 × 1047 erg s-1. Based on single-epoch spectroscopic virial black hole mass estimates, we find that these quasars are accreting at substantial Eddington fractions, 0.1 ≲ L/LEdd ≲ 1.

When will low-contrast features be visible in a STEM X-ray spectrum image?

DOE PAGES

Parish, Chad M.

2015-04-01

When will a small or low-contrast feature, such as an embedded second-phase particle, be visible in a scanning transmission electron microscopy (STEM) X-ray map? This work illustrates a computationally inexpensive method to simulate X-ray maps and spectrum images (SIs), based upon the equations of X-ray generation and detection. To particularize the general procedure, an example of nanostructured ferritic alloy (NFA) containing nm-sized Y 2Ti 2O 7 embedded precipitates in ferritic stainless steel matrix is chosen. The proposed model produces physically appearing simulated SI data sets, which can either be reduced to X-ray dot maps or analyzed via multivariate statistical analysis.more » Comparison to NFA X-ray maps acquired using three different STEM instruments match the generated simulations quite well, despite the large number of simplifying assumptions used. A figure of merit of electron dose multiplied by X-ray collection solid angle is proposed to compare feature detectability from one data set (simulated or experimental) to another. The proposed method can scope experiments that are feasible under specific analysis conditions on a given microscope. As a result, future applications, such as spallation proton–neutron irradiations, core-shell nanoparticles, or dopants in polycrystalline photovoltaic solar cells, are proposed.« less

Publications - GMC 95 | Alaska Division of Geological & Geophysical Surveys

Science.gov Websites

DGGS GMC 95 Publication Details Title: X-ray diffraction analysis of seven core samples from the information. Bibliographic Reference Bergman, S.C., and Stuart, C.J., 1988, X-ray diffraction analysis of

CONTIN XPCS: Software for Inverse Transform Analysis of X-Ray Photon Correlation Spectroscopy Dynamics

PubMed Central

Narayanan, Suresh; Zhang, Fan; Kuzmenko, Ivan; Ilavsky, Jan

2018-01-01

X-ray photon correlation spectroscopy (XPCS) and dynamic light scattering (DLS) both reveal dynamics using coherent scattering, but X-rays permit investigating of dynamics in a much more diverse array of materials. Heterogeneous dynamics occur in many such materials, and we showed how classic tools employed in analysis of heterogeneous DLS dynamics extend to XPCS, revealing additional information that conventional Kohlrausch exponential fitting obscures. This work presents the software implementation of inverse transform analysis of XPCS data called CONTIN XPCS, an extension of traditional CONTIN that accommodates dynamics encountered in equilibrium XPCS measurements. PMID:29875507

CONTIN XPCS: Software for Inverse Transform Analysis of X-Ray Photon Correlation Spectroscopy Dynamics.

PubMed

Andrews, Ross N; Narayanan, Suresh; Zhang, Fan; Kuzmenko, Ivan; Ilavsky, Jan

2018-02-01

X-ray photon correlation spectroscopy (XPCS) and dynamic light scattering (DLS) both reveal dynamics using coherent scattering, but X-rays permit investigating of dynamics in a much more diverse array of materials. Heterogeneous dynamics occur in many such materials, and we showed how classic tools employed in analysis of heterogeneous DLS dynamics extend to XPCS, revealing additional information that conventional Kohlrausch exponential fitting obscures. This work presents the software implementation of inverse transform analysis of XPCS data called CONTIN XPCS, an extension of traditional CONTIN that accommodates dynamics encountered in equilibrium XPCS measurements.

Luminosity correlations in quasars

NASA Technical Reports Server (NTRS)

Chanan, G. A.

1983-01-01

Simulations are conducted with and without flux thresholds in an investigation of quasar luminosity correlations by means of a Monte Carlo analysis, for various model distributions of quasars in X-rays and optical luminosity. For the case where the X-ray photons are primary, an anticorrelation between X-ray-to-optical luminosity ratio and optical luminosity arises as a natural consequence which resembles observations. The low optical luminosities of X-ray selected quasars can be understood as a consequence of the same effect, and similar conclusions may hold if the X-ray and optical luminosities are determined independently by a third parameter, although they do not hold if the optical photons are primary. The importance of such considerations is demonstrated through a reanalysis of the published X-ray-to-optical flux ratios for the 3CR sample.

X-ray studies of quasars with the Einstein Observatory. IV - X-ray dependence on radio emission

NASA Technical Reports Server (NTRS)

Worrall, D. M.; Tananbaum, H.; Giommi, P.; Zamorani, G.

1987-01-01

The X-ray properties of a sample of 114 radio-loud quasars observed with the Einstein Observatory are examined, and the results are compared with those obtained from a large sample of radio-quiet quasars. The results of statistical analysis of the dependence of X-ray luminosity on combined functions of optical and radio luminosity show that the dependence on both luminosities is important. However, statistically significant differences are found between subsamples of flat radio spectra quasars and steep radio spectra quasars with regard to dependence of X-ray luminosity on only radio luminosity. The data are consistent with radio-loud quasars having a physical component, not directly related to the optical luminosity, which produces the core radio luminosity plus 'extra' X-ray emission.

First centenary of Röntgen's discovery of X-rays

NASA Astrophysics Data System (ADS)

Valkovic, V.

1996-04-01

Usually it takes a decade or even several decades, from a discovery to its practical applications. This was not the case with X-rays; they were widely applied in medical and industrial radiography within a year of their discovery in 1895 by W.C. Röntgen. Today, X-ray analysis covers a wide range of techniques and fields of applications: from deduction of atomic arrangements by observation of diffraction phenomena to measurements of trace element concentration levels, distributions and maps by measuring fluorescence, X-ray attenuation or scattering. Although the contribution of analytical applications of X-rays to the present knowledge is difficult to surpass, modern application cover a wide range of activities from three-dimensional microfabrication using synchroton radiation to collecting information from the deep space by X-ray astronomy.

THE BORN-AGAIN PLANETARY NEBULA A78: AN X-RAY TWIN OF A30

DOE Office of Scientific and Technical Information (OSTI.GOV)

Toalá, J. A.; Guerrero, M. A.; Marquez-Lugo, R. A.

We present the XMM-Newton discovery of X-ray emission from the planetary nebula (PN) A78, the second born-again PN detected in X-rays apart from A30. These two PNe share similar spectral and morphological characteristics: they harbor diffuse soft X-ray emission associated with the interaction between the H-poor ejecta and the current fast stellar wind and a point-like source at the position of the central star (CSPN). We present the spectral analysis of the CSPN, using for the first time an NLTE code for expanding atmospheres that takes line blanketing into account for the UV and optical spectra. The wind abundances aremore » used for the X-ray spectral analysis of the CSPN and the diffuse emission. The X-ray emission from the CSPN in A78 can be modeled by a single C VI emission line, while the X-ray emission from its diffuse component is better described by an optically thin plasma emission model with a temperature of kT = 0.088 keV (T ≈ 1.0 × 10{sup 6} K). We estimate X-ray luminosities in the 0.2-2.0 keV energy band of L {sub X,} {sub CSPN} = (1.2 ± 0.3) × 10{sup 31} erg s{sup –1} and L {sub X,} {sub DIFF} = (9.2 ± 2.3) × 10{sup 30} erg s{sup –1} for the CSPN and diffuse components, respectively.« less

HEAO 1 high-energy X-ray observations of Centaurus X-3

NASA Technical Reports Server (NTRS)

Howe, S. K.; Primini, F. A.; Bautz, M. W.; Lang, F. L.; Levine, A. M.; Lewin, W. H. G.

1983-01-01

Pulsations of 4.8 sec were detected up to energies above 38 keV by the present High Energy X-ray and Low Energy Gamma-Ray HEAO 1 satellite experiment observations of Cen X-3, and an analysis of the X-ray spectrum as a function of pulse phase indicates that the spectrum hardens during an interval of about 1.2 sec which lags the pulse peak by about 0.6 sec. The results of correlated observations of pulse period and X-ray intensity include (1) the detection of a high intensity state during which the pulse period is on the average increasing, (2) the measurement of comparable high intensities during episodes of both period increase and decrease, (3) the detection of X-ray pulsations at a much reduced level during a period of low intensity, and (4) the detection of a transition between spin-down, and spin-up episodes that coincides with a rapid decrease in X-ray intensity.

Laboratory-based micro-X-ray fluorescence setup using a von Hamos crystal spectrometer and a focused beam X-ray tube

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kayser, Y., E-mail: yves.kayser@psi.ch; Paul Scherrer Institut, 5232 Villigen-PSI; Błachucki, W.

2014-04-15

The high-resolution von Hamos bent crystal spectrometer of the University of Fribourg was upgraded with a focused X-ray beam source with the aim of performing micro-sized X-ray fluorescence (XRF) measurements in the laboratory. The focused X-ray beam source integrates a collimating optics mounted on a low-power micro-spot X-ray tube and a focusing polycapillary half-lens placed in front of the sample. The performances of the setup were probed in terms of spatial and energy resolution. In particular, the fluorescence intensity and energy resolution of the von Hamos spectrometer equipped with the novel micro-focused X-ray source and a standard high-power water-cooled X-raymore » tube were compared. The XRF analysis capability of the new setup was assessed by measuring the dopant distribution within the core of Er-doped SiO{sub 2} optical fibers.« less

X-Ray Measurements Of A Thermo Scientific P385 DD Neutron Generator

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wharton, C. J.; Seabury, E. H.; Chichester, D. L.

2011-06-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X rays are a normal byproduct from neutron generators, but depending on their intensity and energy, x rays can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum wasmore » measured with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60 deg. between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and its x-ray emission appears to be axially symmetric. A thin lead shield, 3.2 mm (1/8 inch) thick, reduced the 70-keV generator x rays to negligible levels.« less

X-Ray Measurements Of A Thermo Scientific P385 DD Neutron Generator

NASA Astrophysics Data System (ADS)

Wharton, C. J.; Seabury, E. H.; Chichester, D. L.; Caffrey, A. J.; Simpson, J.; Lemchak, M.

2011-06-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X rays are a normal byproduct from neutron generators, but depending on their intensity and energy, x rays can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum was measured with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60° between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and its x-ray emission appears to be axially symmetric. A thin lead shield, 3.2 mm (1/8 inch) thick, reduced the 70-keV generator x rays to negligible levels.

Dual-energy x-ray image decomposition by independent component analysis

NASA Astrophysics Data System (ADS)

Jiang, Yifeng; Jiang, Dazong; Zhang, Feng; Zhang, Dengfu; Lin, Gang

2001-09-01

The spatial distributions of bone and soft tissue in human body are separated by independent component analysis (ICA) of dual-energy x-ray images. It is because of the dual energy imaging modelí-s conformity to the ICA model that we can apply this method: (1) the absorption in body is mainly caused by photoelectric absorption and Compton scattering; (2) they take place simultaneously but are mutually independent; and (3) for monochromatic x-ray sources the total attenuation is achieved by linear combination of these two absorption. Compared with the conventional method, the proposed one needs no priori information about the accurate x-ray energy magnitude for imaging, while the results of the separation agree well with the conventional one.

Some radiation effects on organic binders in X-ray fluorescence spectrometry

NASA Astrophysics Data System (ADS)

Novosel-Radović, Vj.; MaljkoviĆ, Da.; NenadiĆ, N.

The paper deals with diminished wear resistance of standard samples in X-ray fluorescence spectrometry. The effect of X-ray irradiation on pellet samples, pressed with starch as organic binder, was investigated by sieve analysis and scanning electron microscopy. A change in the starch grain size was found as a result of swelling and cracking.

X-ray chemical analyzer for field applications

DOEpatents

Gamba, Otto O. M.

1977-01-01

A self-supporting portable field multichannel X-ray chemical analyzer system comprising a lightweight, flexibly connected, remotely locatable, radioisotope-excited sensing probe utilizing a cryogenically-cooled solid state semi-conductor crystal detector for fast in situ non-destructive, qualitative and quantitative analysis of elements in solid, powder, liquid or slurried form, utilizing an X-ray energy dispersive spectrometry technique.

Surface degradation of uranium tetrafluoride

DOE PAGES

Tobin, J. G.; Duffin, A. M.; Yu, S. -W.; ...

2017-05-01

A detailed analysis of a single crystal of uranium tetrafluoride has been carried out. The techniques include x-ray absorption spectroscopy, as well as x-ray photoelectron spectroscopy and x-ray emission spectroscopy. Evidence will be presented for the presence of a uranyl species, possibly UO 2F 2, as a product of, or participant in the surface degradation.

Nanoscience

DTIC Science & Technology

2011-07-22

L., Upgrading of Existing X - Ray Photoelectron Spectrometer Capabilities for Development and Analysis of Novel Energetic NanoCluster materials (DURIP...References From the Technical Reports database Allara, David L., Pennsylvania State University, Upgrading of Existing X - Ray Photoelectron...Scanning probe  X - ray Of these techniques, the most popularly used is the scanning probe, also known as the Dip-Pen Nanolithography (DPN) technique

Status and expected perfomance of the MAXI mission for the JEM/ISS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kataoka, J.; Kawai, N.

2008-12-24

MAXI (Monitor of All-sky X-ray Image) is the first payload to be attached on JEM-EF (Kibo exposed facility) of ISS. It provides an all sky X-ray image every ISS orbit. Only with a few weeks scan, MAXI is expected to make a milli-Crab X-ray all sky map excluding bright region around the sun. Thus, MAXI does not only inform X-ray novae and transients rapidly to world astronomers if once they occur, but also observes long-term variability of Galact ic and extra-Galactic X-ray sources. MAXI also provides an X-ray source catalogue at that time with diffuse cosmic X-ray background. MAXI consistsmore » of two kinds of detectors, position sensitive gas-proportional counters for 2-30 keV X-rays and CCD cameras for 0.5-10 keV X-rays. All instruments of MAXI are now in final phase of pre-launching tests of their flight modules. We are also carrying out performance tests for X-ray detectors and collimators. Data processing and analysis software including alert system on ground are being developed by mission team. In this paper we report an overview of final instruments of MAXI and capability of MAXI.« less

X-rays from the Solar System

NASA Astrophysics Data System (ADS)

Dennerl, K.

2017-10-01

While the beginning of X-ray astronomy was motivated by solar system studies (Sun and Moon), the main research interest soon shifted outwards to much more distant and exotic objects. However, the ROSAT discovery of X-rays from comets in 1996 and the insight that this `new' kind of X-ray emission, charge exchange, was underestimated for a long time, has demonstrated that solar system studies are still important for X-ray astrophysics in general. While comets provide the best case for studying the physics of charge exchange, the X-ray signatures of this process have now also been detected at Venus, Mars, and Jupiter, thanks to Chandra and XMM-Newton. An analysis of the X-ray data of solar system objects, however, is challenging in many respects. This is particularly true for comets, which appear as moving, extended X-ray sources, emitting a line-rich spectrum at low energies. Especially for XMM-Newton, which has the unparalleled capability to observe with five highly sensitive X-ray instruments plus an optical monitor simultaneously, it is a long way towards photometrically and spectroscopically calibrated results, which are consistent between all its instruments. I will show this in my talk, where I will also summarize the current state of solar system X-ray research.

Multiwavelength study of Chandra X-ray sources in the Antennae

NASA Astrophysics Data System (ADS)

Clark, D. M.; Eikenberry, S. S.; Brandl, B. R.; Wilson, J. C.; Carson, J. C.; Henderson, C. P.; Hayward, T. L.; Barry, D. J.; Ptak, A. F.; Colbert, E. J. M.

2011-01-01

We use Wide-field InfraRed Camera (WIRC) infrared (IR) images of the Antennae (NGC 4038/4039) together with the extensive catalogue of 120 X-ray point sources to search for counterpart candidates. Using our proven frame-tie technique, we find 38 X-ray sources with IR counterparts, almost doubling the number of IR counterparts to X-ray sources that we first identified. In our photometric analysis, we consider the 35 IR counterparts that are confirmed star clusters. We show that the clusters with X-ray sources tend to be brighter, Ks≈ 16 mag, with (J-Ks) = 1.1 mag. We then use archival Hubble Space Telescope (HST) images of the Antennae to search for optical counterparts to the X-ray point sources. We employ our previous IR-to-X-ray frame-tie as an intermediary to establish a precise optical-to-X-ray frame-tie with <0.6 arcsec rms positional uncertainty. Due to the high optical source density near the X-ray sources, we determine that we cannot reliably identify counterparts. Comparing the HST positions to the 35 identified IR star cluster counterparts, we find optical matches for 27 of these sources. Using Bruzual-Charlot spectral evolutionary models, we find that most clusters associated with an X-ray source are massive, and young, ˜ 106 yr.

X-Ray Astronomy Research at the Marshall Space Flight Center

NASA Technical Reports Server (NTRS)

Austin, Robert A.

1999-01-01

For at least twenty years, NASA's Marshall Space Flight Center (MSFC) has played a major role in the development of X-ray astronomy in the United States. MSFC scientists and engineers are currently involved in a wide range of programs which will contribute to the growth of X-ray astronomy well into the next century. Areas of activity include calibration of X-ray astronomy instrumentation using Marshall's world-class X-ray Calibration Facility (XRCF), development of high-throughput, replicated X-ray optics, X-ray detector development, balloon-based X-ray astronomy, and analysis of Active Galactic Nuclei (AGNs) and clusters of galaxies. Recent milestones include the successful calibration of NASA's premier X-ray Astronomy Satellite - AXAF (recently renamed Chandra), a balloon flight of a large area (1000 sq cm) micro-strip proportional counter, and work on a hard X-ray (30-100 keV) telescope called HERO, capable of high quality spectroscopy and imaging through the use of grazing incidence optics and an Imaging Gas Scintillation Proportional Counter (IGSPC). In my presentation, I will provide a general overview of our research and facilities. I will conclude with a more detailed discussion of our High Energy Replicated Optics (HERO) program and plans for long duration (>100 days) balloon flights which will take place in the near future.

Non-destructive determination of floral staging in cereals using X-ray micro computed tomography (µCT).

PubMed

Tracy, Saoirse R; Gómez, José Fernández; Sturrock, Craig J; Wilson, Zoe A; Ferguson, Alison C

2017-01-01

Accurate floral staging is required to aid research into pollen and flower development, in particular male development. Pollen development is highly sensitive to stress and is critical for crop yields. Research into male development under environmental change is important to help target increased yields. This is hindered in monocots as the flower develops internally in the pseudostem. Floral staging studies therefore typically rely on destructive analysis, such as removal from the plant, fixation, staining and sectioning. This time-consuming analysis therefore prevents follow up studies and analysis past the point of the floral staging. This study focuses on using X-ray µCT scanning to allow quick and detailed non-destructive internal 3D phenotypic information to allow accurate staging of Arabidopsis thaliana L. and Barley ( Hordeum vulgare L.) flowers. X-ray µCT has previously relied on fixation methods for above ground tissue, therefore two contrast agents (Lugol's iodine and Bismuth) were observed in Arabidopsis and Barley in planta to circumvent this step. 3D models and 2D slices were generated from the X-ray µCT images providing insightful information normally only available through destructive time-consuming processes such as sectioning and microscopy. Barley growth and development was also monitored over three weeks by X-ray µCT to observe flower development in situ. By measuring spike size in the developing tillers accurate non-destructive staging at the flower and anther stages could be performed; this staging was confirmed using traditional destructive microscopic analysis. The use of X-ray micro computed tomography (µCT) scanning of living plant tissue offers immense benefits for plant phenotyping, for successive developmental measurements and for accurate developmental timing for scientific measurements. Nevertheless, X-ray µCT remains underused in plant sciences, especially in above-ground organs, despite its unique potential in delivering detailed non-destructive internal 3D phenotypic information. This work represents a novel application of X-ray µCT that could enhance research undertaken in monocot species to enable effective non-destructive staging and developmental analysis for molecular genetic studies and to determine effects of stresses at particular growth stages.

Thermal Stability and X-ray Attenuation Studies on α-Bi₂O₃, β-Bi₂O₃ and Bi Based Nanocomposites for Radiopaque Fabrics.

PubMed

Jayakumar, Sangeetha; Saravanan, T; Philip, John

2018-06-01

Nanocomposites containing α-Bi2O3, β-Bi2O3 and Bi nanoparticles as nanofillers in vulcanized silicone resin as a matrix are prepared and their diagnostic X-ray attenuation property is studied. The nanocomposites are prepared using a simple solution casting technique, with nanofiller concentration varying from 2-50 wt%. Thermogravimetric analysis and differential scanning calorimetry are performed to study the thermal stability of the nanocomposites. The attenuation property is studied by exposing the nanocomposites containing α-Bi2O3, β-Bi2O3 and Bi nanoparticles to X-rays of energy 30-60 keV. Nanocomposites containing β-Bi2O3 nanoparticles are found to exhibit the highest attenuation than nanocomposites of α-Bi2O3 and Bi nanoparticles of similar concentration. Nanocomposites containing 50 wt% of β-Bi2O3 nanoparticles exhibit an X-ray attenuation of 93, 86, 71, 45 and 10% at an X-ray photon energy of 40, 45, 50, 55 and 59 keV, respectively. Further increase in photon energy is found to saturate the flat panel detector owing to the lower thickness of the nanocomposites. Analysis of high resolution X-ray radiographs of the nanocomposites confirms the uniform distribution of nanofillers in the matrix. Thermal analysis confirms the structural integrity and thermal stability of the nanocomposites. Heat flow curves also confirm the interaction of nanofillers with the matrix, corroborated by a change in the peak position and its endothermic/exothermic nature, corresponding to the phase transition of the nanofillers. It is also interpreted from thermal analysis of nanocomposites that the nanofillers interact with the matrix either by intercalating in the bridging polymer chain of silicone resin network structure or by occupying the interchain space. Thermal analysis of X-ray exposed nanocomposites shows no significant change in heat flow rates, thus, confirming the stability of the nanocomposites. Our study shows that nanocomposites containing β-Bi2O3 nanofiller are potential candidates for radiopaque fabrics which can find application in diagnostic X-ray shielding in mammography, dental scan, etc.

SPITZER IRAC OBSERVATIONS OF IR EXCESS IN HOLMBERG IX X-1: A CIRCUMBINARY DISK OR A VARIABLE JET?

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dudik, R. P.; Berghea, C. T.; Roberts, T. P.

2016-11-01

We present Spitzer Infrared Array Camera photometric observations of the ultraluminous X-ray source (ULX, X-1) in Holmberg IX. We construct a spectral energy distribution (SED) for Holmberg IX X-1 based on published optical, UV, and X-ray data combined with the IR data from this analysis. We modeled the X-ray and optical data with disk and stellar models; however, we find a clear IR excess in the ULX SED that cannot be explained by fits or extrapolations of any of these models. Instead, further analysis suggests that the IR excess results from dust emission, possibly a circumbinary disk, or a variablemore » jet.« less

Publications - GMC 361 | Alaska Division of Geological & Geophysical

Science.gov Websites

DGGS GMC 361 Publication Details Title: X-ray Diffraction Analysis of: Drew Point #1, East Simpson Test , 2009, X-ray Diffraction Analysis of: Drew Point #1, East Simpson Test Well #1, East Simpson #2

Publications - GMC 41 | Alaska Division of Geological & Geophysical Surveys

Science.gov Websites

DGGS GMC 41 Publication Details Title: X-ray diffraction clay mineralogy analysis of core samples from Unknown, [n.d.], X-ray diffraction clay mineralogy analysis of core samples from Mobil West Staines State

In-Line Phase-Contrast X-ray Imaging and Tomography for Materials Science

PubMed Central

Mayo, Sheridan C.; Stevenson, Andrew W.; Wilkins, Stephen W.

2012-01-01

X-ray phase-contrast imaging and tomography make use of the refraction of X-rays by the sample in image formation. This provides considerable additional information in the image compared to conventional X-ray imaging methods, which rely solely on X-ray absorption by the sample. Phase-contrast imaging highlights edges and internal boundaries of a sample and is thus complementary to absorption contrast, which is more sensitive to the bulk of the sample. Phase-contrast can also be used to image low-density materials, which do not absorb X-rays sufficiently to form a conventional X-ray image. In the context of materials science, X-ray phase-contrast imaging and tomography have particular value in the 2D and 3D characterization of low-density materials, the detection of cracks and voids and the analysis of composites and multiphase materials where the different components have similar X-ray attenuation coefficients. Here we review the use of phase-contrast imaging and tomography for a wide variety of materials science characterization problems using both synchrotron and laboratory sources and further demonstrate the particular benefits of phase contrast in the laboratory setting with a series of case studies. PMID:28817018

In-Line Phase-Contrast X-ray Imaging and Tomography for Materials Science.

PubMed

Mayo, Sheridan C; Stevenson, Andrew W; Wilkins, Stephen W

2012-05-24

X-ray phase-contrast imaging and tomography make use of the refraction of X-rays by the sample in image formation. This provides considerable additional information in the image compared to conventional X-ray imaging methods, which rely solely on X-ray absorption by the sample. Phase-contrast imaging highlights edges and internal boundaries of a sample and is thus complementary to absorption contrast, which is more sensitive to the bulk of the sample. Phase-contrast can also be used to image low-density materials, which do not absorb X-rays sufficiently to form a conventional X-ray image. In the context of materials science, X-ray phase-contrast imaging and tomography have particular value in the 2D and 3D characterization of low-density materials, the detection of cracks and voids and the analysis of composites and multiphase materials where the different components have similar X-ray attenuation coefficients. Here we review the use of phase-contrast imaging and tomography for a wide variety of materials science characterization problems using both synchrotron and laboratory sources and further demonstrate the particular benefits of phase contrast in the laboratory setting with a series of case studies.

Common observations of solar X-rays from SPHINX/CORONAS-PHOTON and XRS/MESSENGER

NASA Astrophysics Data System (ADS)

Kepa, Anna; Sylwester, Janusz; Sylwester, Barbara; Siarkowski, Marek; Mrozek, Tomasz; Gryciuk, Magdalena; Phillips, Kenneth

SphinX was a soft X-ray spectrophotometer constructed in the Space Research Centre of Polish Academy of Sciences. The instrument was launched on 30 January 2009 aboard CORONAS-PHOTON satellite as a part of TESIS instrument package. SphinX measured total solar X-ray flux in the energy range from 1 to 15 keV during the period of very low solar activity from 20 February to 29 November 2009. For these times the solar detector (X-ray Spectrometer - XRS) onboard MESSENGER also observed the solar X-rays from a different vantage point. XRS measured the radiation in similar energy range. We present results of the comparison of observations from both instruments and show the preliminary results of physical analysis of spectra for selected flares.

The Mapping X-Ray Fluorescence Spectrometer (mapx)

NASA Astrophysics Data System (ADS)

Blake, D. F.; Sarrazin, P.; Bristow, T.; Downs, R. T.; Gailhanou, M.; Marchis, F.; Ming, D. W.; Morris, R. V.; Sole, V. A.; Thompson, K.; Walter, P.; Wilson, M.; Yen, A. S.; Webb, S.

2016-12-01

MapX will provide elemental imaging at ≤100 µm spatial resolution over 2.5 X 2.5 cm areas, yielding elemental chemistry at or below the scale length where many relict physical, chemical, and biological features can be imaged and interpreted in ancient rocks. MapX is a full-frame spectroscopic imager positioned on soil or regolith with touch sensors. During an analysis, an X-ray source (tube or radioisotope) bombards the sample surface with X-rays or α-particles / γ-rays, resulting in sample X-ray Fluorescence (XRF). Fluoresced X-rays pass through an X-ray lens (X-ray µ-Pore Optic, "MPO") that projects a spatially resolved image of the X-rays onto a CCD. The CCD is operated in single photon counting mode so that the positions and energies of individual photons are retained. In a single analysis, several thousand frames are stored and processed. A MapX experiment provides elemental maps having a spatial resolution of ≤100 µm and quantitative XRF spectra from Regions of Interest (ROI) 2 cm ≤ x ≤ 100 µm. ROI are compared with known rock and mineral compositions to extrapolate the data to rock types and putative mineralogies. The MapX geometry is being refined with ray-tracing simulations and with synchrotron experiments at SLAC. Source requirements are being determined through Monte Carlo modeling and experiment using XMIMSIM [1], GEANT4 [2] and PyMca [3] and a dedicated XRF test fixture. A flow-down of requirements for both tube and radioisotope sources is being developed from these experiments. In addition to Mars lander and rover missions, MapX could be used for landed science on other airless bodies (Phobos/Deimos, Comet nucleus, asteroids, the Earth's moon, and the icy satellites of the outer planets, including Europa. [1] Schoonjans, T. et al.(2012). Spectrachim. Acta Part B, 70, 10-23. [2] Agostinelli, S. et al. (2003). Nucl. Instr. and Methods in Phys. Research A, 506, 250-303. [3] V.A. Solé et al. (2007). Spectrochim. Acta Part B, 62, 63-68.

TH-AB-209-07: High Resolution X-Ray-Induced Acoustic Computed Tomography

DOE Office of Scientific and Technical Information (OSTI.GOV)

Xiang, L; Tang, S; Ahmad, M

Purpose: X-ray radiographic absorption imaging is an invaluable tool in medical diagnostics, biology and materials science. However, the use of conventional CT is limited by two factors: the detection sensitivity to weak absorption material and the radiation dose from CT scanning. The purpose of this study is to explore X-ray induced acoustic computed tomography (XACT), a new imaging modality, which combines X-ray absorption contrast and high ultrasonic resolution to address these challenges. Methods: First, theoretical models was built to analyze the XACT sensitivity to X-ray absorption and calculate the minimal radiation dose in XACT imaging. Then, an XACT system comprisedmore » of an ultrashort X-ray pulse, a low noise ultrasound detector and a signal acquisition system was built to evaluate the X-ray induced acoustic signal generation. A piece of chicken bone and a phantom with two golden fiducial markers were exposed to 270 kVp X-ray source with 60 ns exposure time, and the X-ray induced acoustic signal was received by a 2.25MHz ultrasound transducer in 200 positions. XACT images were reconstructed by a filtered back-projection algorithm. Results: The theoretical analysis shows that X-ray induced acoustic signals have 100% relative sensitivity to X-ray absorption, but not to X-ray scattering. Applying this innovative technology to breast imaging, we can reduce radiation dose by a factor of 50 compared with newly FDA approved breast CT. The reconstructed images of chicken bone and golden fiducial marker phantom reveal that the spatial resolution of the built XACT system is 350µm. Conclusion: In XACT, the imaging sensitivity to X-ray absorption is improved and the imaging dose is dramatically reduced by using ultrashort pulsed X-ray. Taking advantage of the high ultrasonic resolution, we can also perform 3D imaging with a single X-ray pulse. This new modality has the potential to revolutionize x-ray imaging applications in medicine and biology.« less

Use of polarized radiation for increasing the sensitivity of multielement x-ray fluorescence analysis

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ter-Saakov, A.A.; Glebov, M.V.

1985-10-01

An experimental x-ray fluorescence analysis facility has been developed using polarized radiation. A modernized small-sized REIS-I emitter is used as the x-ray genertor. Its characteristics are: a straight-through drift tube with a copper, molybdenum, or silver anode; and a controlled working voltage from 0 to 45 kV. The thickness of the inlet beryllium window is 100 um. Experiments were carried out on the facility on the optimization of fluorescence excitation conditions of biological samples. The investigations conducted of the dosimetric and spectral characteristics of the BS-1, BS-3, and BKh-7 x-ray tubes with copper, silver, and molybdenum anodes have shown thatmore » for the analysis in samples of biogenic elements, it is most efficient to use the BKh-7 and BS-1 tubes with a copper anode.« less

Proton-Induced X-Ray Emission Analysis of Crematorium Emissions

NASA Astrophysics Data System (ADS)

Ali, Salina; Nadareski, Benjamin; Safiq, Alexandrea; Smith, Jeremy; Yoskowitz, Josh; Labrake, Scott; Vineyard, Michael

2013-10-01

There has been considerable concern in recent years about possible mercury emissions from crematoria. We have performed a particle-induced X-ray emission (PIXE) analysis of atmospheric aerosol samples collected on the roof of the crematorium at Vale Cemetery in Schenectady, NY, to address this concern. The samples were collected with a nine-stage cascade impactor that separates the particulate matter according to particle size. The aerosol samples were bombarded with 2.2-MeV protons from the Union College 1.1-MV Pelletron Accelerator. The emitted X-rays were detected with a silicon drift detector and the X-ray energy spectra were analyzed using GUPIX software to determine the elemental concentrations. We measured significant concentrations of sulfur, phosphorus, potassium, calcium, and iron, but essentially no mercury. The lower limit of detection for mercury in this experiment was approximately 0.2 ng/m3. We will describe the experimental procedure, discuss the PIXE analysis, and present preliminary results.

Electron microprobe mineral analysis guide

NASA Technical Reports Server (NTRS)

Brown, R. W.

1980-01-01

Electron microprobe mineral analysis guide is a compilation of X-ray tables and spectra recorded from various mineral matrices. Spectra were obtained using electron microprobe, equipped with LiF geared, curved crystal X-ray spectrometers, utilizing typical analytical operating conditions: 15 Kv acceleration potential, 0.02 microampere sample current as measured on a clinopyroxene standard (CP19). Tables and spectra are presented for the majority of elements, fluorine through uranium, occurring in mineral samples from lunar, meteoritic and terrestrial sources. Tables for each element contain relevant analytical information, i.e., analyzing crystal, X-ray peak, background and relative intensity information, X-ray interferences and a section containing notes on the measurement. Originally intended to cover silicates and oxide minerals the tables and spectra have been expanded to cover other mineral phases. Electron microprobe mineral analysis guide is intended as a spectral base to which additional spectra can be added as the analyst encounters new mineral matrices.

Automated X-ray image analysis for cargo security: Critical review and future promise.

PubMed

Rogers, Thomas W; Jaccard, Nicolas; Morton, Edward J; Griffin, Lewis D

2017-01-01

We review the relatively immature field of automated image analysis for X-ray cargo imagery. There is increasing demand for automated analysis methods that can assist in the inspection and selection of containers, due to the ever-growing volumes of traded cargo and the increasing concerns that customs- and security-related threats are being smuggled across borders by organised crime and terrorist networks. We split the field into the classical pipeline of image preprocessing and image understanding. Preprocessing includes: image manipulation; quality improvement; Threat Image Projection (TIP); and material discrimination and segmentation. Image understanding includes: Automated Threat Detection (ATD); and Automated Contents Verification (ACV). We identify several gaps in the literature that need to be addressed and propose ideas for future research. Where the current literature is sparse we borrow from the single-view, multi-view, and CT X-ray baggage domains, which have some characteristics in common with X-ray cargo.

Einstein Observatory survey of X-ray emission from solar-type stars - The late F and G dwarf stars

NASA Technical Reports Server (NTRS)

Maggio, A.; Sciortino, S.; Vaiana, G. S.; Majer, P.; Bookbinder, J.

1987-01-01

Results of a volume-limited X-ray survey of stars of luminosity classes IV and V in the spectral range F7-G9 observed with the Einstein Observatory are presented. Using survival analysis techniques, the stellar X-ray luminosity function in the 0.15-4.0 keV energy band for both single and multiple sources. It is shown that the difference in X-ray luminosity between these two classes of sources is consistent with the superposition of individual components in multiple-component systems, whose X-ray properties are similar to those of the single-component sources. The X-ray emission of the stars in our sample is well correlated with their chromospheric CA II H-K line emission and with their projected equatorial rotational velocity. Comparison of the X-ray luminosity function constructed for the sample of the dG stars of the local population with the corresponding functions derived elsewhere for the Hyades, the Pleiades, and the Orion Ic open cluster confirms that the level of X-ray emission decreases with stellar age.

X-Ray Spectroscopy of the Nearby, Classical T Tauri Star TW Hydrae

NASA Astrophysics Data System (ADS)

Kastner, Joel H.; Huenemoerder, David P.; Schulz, Norbert S.; Weintraub, David A.

1999-11-01

We present ASCA and ROSAT X-ray observations of the classical T Tauri star TW Hya, the namesake of a small association that, at a distance of ~50 pc, represents the nearest known region of recent star formation. Analysis of ASCA and ROSAT spectra indicates characteristic temperatures of ~1.7 and ~9.7 MK for the X-ray-emitting region(s) of TW Hya, with emission lines of highly ionized Fe dominating the spectrum at energies of ~1 keV. The X-ray data show variations in X-ray flux on timescales of <~1 hr as well as indications of changes in the X-ray-absorbing column on timescales of several years, suggesting that flares and variable obscuration are responsible for the large-amplitude optical variability of TW Hya on short and long timescales, respectively. Comparison with model calculations suggests that TW Hya produces sufficient hard X-ray flux to produce significant ionization of molecular gas within its circumstellar disk; such X-ray ionization may regulate both protoplanetary accretion and protoplanetary chemistry.

X-Ray Emissions from Accreting White Dwarfs: A Review

NASA Technical Reports Server (NTRS)

Mukai, K.

2017-01-01

Interacting binaries in which a white dwarf accretes material from a companion-cataclysmic variables (CVs) in which the mass donor is a Roche-lobe filling star on or near the main sequence, and symbiotic stars in which the mass donor is a late type giant-are relatively commonplace. They display a wide range of behaviors in the optical, X-rays, and other wavelengths, which still often baffle observers and theorists alike. Here I review the existing body of research on X-ray emissions from these objects for the benefits of both experts and newcomers to the field. I provide introductions to the past and current X-ray observatories, the types of known X-ray emissions from these objects, and the data analysis techniques relevant to this field. I then summarize of our knowledge regarding the X-ray emissions from magnetic CVs, non-magnetic CVs and symbiotic stars, and novae in eruption. I also discuss space density and the X-ray luminosity functions of these binaries and their contribution to the integrated X-ray emission from the Galaxy. I then discuss open questions and future prospects.

Silicon Drift Detector response function for PIXE spectra fitting

NASA Astrophysics Data System (ADS)

Calzolai, G.; Tapinassi, S.; Chiari, M.; Giannoni, M.; Nava, S.; Pazzi, G.; Lucarelli, F.

2018-02-01

The correct determination of the X-ray peak areas in PIXE spectra by fitting with a computer program depends crucially on accurate parameterization of the detector peak response function. In the Guelph PIXE software package, GUPIXWin, one of the most used PIXE spectra analysis code, the response of a semiconductor detector to monochromatic X-ray radiation is described by a linear combination of several analytical functions: a Gaussian profile for the X-ray line itself, and additional tail contributions (exponential tails and step functions) on the low-energy side of the X-ray line to describe incomplete charge collection effects. The literature on the spectral response of silicon X-ray detectors for PIXE applications is rather scarce, in particular data for Silicon Drift Detectors (SDD) and for a large range of X-ray energies are missing. Using a set of analytical functions, the SDD response functions were satisfactorily reproduced for the X-ray energy range 1-15 keV. The behaviour of the parameters involved in the SDD tailing functions with X-ray energy is described by simple polynomial functions, which permit an easy implementation in PIXE spectra fitting codes.

The soft x ray halo of the spiral galaxy NGC4631

NASA Technical Reports Server (NTRS)

Walterbos, Rene A. M.; Steakley, Michael F.; Wang, Q. Daniel; Norman, Colin A.; Braun, Robert

1994-01-01

ROSAT PSPC observations of the close to edge-on spiral galaxy NGC4631 are presented. This vigorously star forming galaxy shows extented x ray emission perpendicular to the plane, out to about 6 to 8 kpc. The spatial extent is largest at soft x ray energies. The total x ray luminosity of hot gas can be easily supplied by star formation in the disk, and it is likely that the halo is due to outflow of hot gas from the inner disk. Spectral analysis of the x ray data shows that part of the halo emission may be quite cool, well below 10(exp 6)K. Implications of these results are briefly discussed.

High resolution projection X-ray microscope equipped with fluorescent X-ray analyzer and its applications

NASA Astrophysics Data System (ADS)

Minami, K.; Saito, Y.; Kai, H.; Shirota, K.; Yada, K.

2009-09-01

We have newly developed an open type fine-focus X-ray tube "TX-510" to realize a spatial resolution of 50nm and to radiate low energy characteristic X-rays for giving high absorption contrast to images of microscopic organisms. The "TX-510" employs a ZrO/W(100) Schottky emitter and an "In-Lens Field Emission Gun". The key points of the improvements are (1) reduced spherical aberration coefficient of magnetic objective lens, (2) easy and accurate focusing, (3) newly designed astigmatism compensator, (4) segmented thin film target for interchanging the target materials by electron beam shift and (5) fluorescent X-ray analysis system.

A first evaluation of the analytical capabilities of the new X-ray fluorescence facility at International Atomic Energy Agency-Elettra Sincrotrone Trieste for multipurpose total reflection X-ray fluorescence analysis

NASA Astrophysics Data System (ADS)

Marguí, Eva; Hidalgo, Manuela; Migliori, Alessandro; Leani, Juan José; Queralt, Ignasi; Kallithrakas-Kontos, Nikolaos; Streli, Christina; Prost, Josef; Karydas, Andreas Germanos

2018-07-01

The aim of the work is to present a systematic evaluation of the analytical capabilities of the new X-ray fluorescence facility jointly operated between the International Atomic Energy Agency and the Elettra Sincrotrone Trieste for multipurpose total reflection X-ray fluorescence analysis. The analytical performance of the XRF beamline end-station (IAEAXspe) was systematically evaluated under TXRF excitation geometry by analyzing different types of aqueous (lake, waste and fresh water) and solid (soil, vegetal, biological) certified reference materials using an excitation energy of 13.0 keV (for the purpose of multielemental analysis). The results obtained for both types of samples in terms of limits of detection and accuracy were also compared with those obtained using laboratory X-ray tube based TXRF systems with different features (including Mo and W X-ray tube systems). Taking advantage of the possibility to work under high vacuum, the IAEAXspe set-up instrumental sensitivity was also determined using an excitation energy of 6.2 keV to explore the possibilities for light elements determination. A clear improvement of the element detection limits is achieved when comparing this facility to conventional X-ray tube based TXRF systems highlighting the benefits of using the monoenergetic synchrotron exciting radiation and the ultra-high vacuum chamber in comparison with conventional laboratory systems. The results of the present work are discussed in view of further exploitation of the facility for different environmental and biological related applications.

The Nature of the UV/X-ray Absorber In PG 2302+029

NASA Technical Reports Server (NTRS)

Sabra, Bassem M.; Hamann, Fred; Jannuzi, Buell T.; George, Ian M.; Shields, Joseph C.

2003-01-01

We present Chandra X-ray observations of the radio-quiet QSO PG 2302+029. This quasar has a rare system of ultra-high velocity (-56,000 km s(exp -1) UV absorption lines that form in an outflow from the active nucleus. The Chandra data indicate that soft X-ray absorption is also present. We perform a joint UV and X-ray analysis, using photoionization calculations, to determine the nature of the absorbing gas. The UV and X-ray datasets were not obtained simultaneously. Nonetheless, our analysis suggests that the X-ray absorption occurs at high velocities in the same general region as the UV absorber. There are not enough constraints to rule out multi-zone models. In fact, the distinct broad and narrow UV line profiles clearly indicate that multiple zones are present. Our preferred estimates of the ionization and total column density in the X-ray absorber (logU = 1.6, N(sub eta) = 10(exp 22.4) cm (exp -2) over predict the O VI lambda lambda1032,1038 absorption unless the X-ray absorber is also outflowing at approximately 56,000 km s(exp-l), but they over predict the Ne VIII lambda lambda 770,780 absorption at all velocities. If we assume that the X-ray absorbing gas is outflowing at the same velocity of the UV-absorbing wind and that the wind is radiatively accelerated, then the outflow must be launched at a radius of less than or equal to 10(exp 15) cm from the central continuum source. The smallness of this radius casts doubts on the assumption of radiative acceleration.

A Deep Chandra ACIS Survey of M83

NASA Astrophysics Data System (ADS)

Long, Knox S.; Kuntz, Kip D.; Blair, William P.; Godfrey, Leith; Plucinsky, Paul P.; Soria, Roberto; Stockdale, Christopher; Winkler, P. Frank

2014-06-01

We have obtained a series of deep X-ray images of the nearby galaxy M83 using Chandra, with a total exposure of 729 ks. Combining the new data with earlier archival observations totaling 61 ks, we find 378 point sources within the D25 contour of the galaxy. We find 80 more sources, mostly background active galactic nuclei (AGNs), outside of the D25 contour. Of the X-ray sources, 47 have been detected in a new radio survey of M83 obtained using the Australia Telescope Compact Array. Of the X-ray sources, at least 87 seem likely to be supernova remnants (SNRs), based on a combination of their properties in X-rays and at other wavelengths. We attempt to classify the point source population of M83 through a combination of spectral and temporal analysis. As part of this effort, we carry out an initial spectral analysis of the 29 brightest X-ray sources. The soft X-ray sources in the disk, many of which are SNRs, are associated with the spiral arms, while the harder X-ray sources, mostly X-ray binaries (XRBs), do not appear to be. After eliminating AGNs, foreground stars, and identified SNRs from the sample, we construct the cumulative luminosity function (CLF) of XRBs brighter than 8 × 1035 erg s-1. Despite M83's relatively high star formation rate, the CLF indicates that most of the XRBs in the disk are low mass XRBs. Based on observations made with NASA's Chandra X-Ray Observatory. NASA's Chandra Observatory is operated by Smithsonian Astrophysical Observatory under contract NAS83060 and the data were obtained through program GO1-12115.

The 3CR Chandra Snapshot Survey: Extragalactic Radio Sources with Redshifts between 1 and 1.5

NASA Astrophysics Data System (ADS)

Stuardi, C.; Missaglia, V.; Massaro, F.; Ricci, F.; Liuzzo, E.; Paggi, A.; Kraft, R. P.; Tremblay, G. R.; Baum, S. A.; O’Dea, C. P.; Wilkes, B. J.; Kuraszkiewicz, J.; Forman, W. R.; Harris, D. E.

2018-04-01

The aim of this paper is to present an analysis of newly acquired X-ray observations of 16 extragalactic radio sources listed in the Third Cambridge Revised (3CR) catalog and not previously observed by Chandra. Observations were performed during Chandra Cycle 17, extending X-ray coverage for the 3CR extragalactic catalog up to z = 1.5. Among the 16 targets, two lie at z < 0.5 (3CR 27 at z = 0.184 and 3CR 69 at z = 0.458) all of the remaining 14 have redshifts between 1.0 and 1.5. In the current sample, there are three compact steep spectrum (CSS) sources, three quasars, and an FR I radio galaxy, while the other nine are FR II radio galaxies. All radio sources have an X-ray counterpart. We measured nuclear X-ray fluxes as well as X-ray emission associated with radio jet knots, hotspots, or lobes in three energy bands: soft (0.5–1 keV), medium (1–2 keV), and hard (2–7 keV). We also performed standard X-ray spectral analysis for the four brightest nuclei. We discovered X-ray emission associated with the radio lobe of 3CR 124, a hotspot of the quasar 3CR 220.2, another hotspot of the radio galaxy 3CR 238, and the jet knot of 3CR 297. We also detected extended X-ray emission around the nuclear region of 3CR 124 and 3CR 297 on scales of several tens of kiloparsecs. Finally, we present an update on the X-ray observations performed with Chandra and XMM-Newton on the entire 3CR extragalactic catalog.

BROADBAND JET EMISSION IN YOUNG AND POWERFUL RADIO SOURCES: THE CASE OF THE COMPACT STEEP SPECTRUM QUASAR 3C 186

DOE Office of Scientific and Technical Information (OSTI.GOV)

Migliori, Giulia; Siemiginowska, Aneta; Celotti, Annalisa, E-mail: migliori@cfa.harvard.edu

2012-04-20

We present the X-ray analysis of a deep ({approx}200 ks) Chandra observation of the compact steep spectrum radio-loud quasar 3C 186 (z = 1.06) and investigate the contribution of the unresolved radio jet to the total X-ray emission. The spectral analysis is not conclusive on the origin of the bulk of the X-ray emission. In order to examine the jet contribution to the X-ray flux, we model the quasar spectral energy distribution, adopting several scenarios for the jet emission. For the values of the main physical parameters favored by the observables, a dominant role of the jet emission in themore » X-ray band is ruled out when a single-zone (leptonic) scenario is adopted, even including the contribution of the external photon fields as seed photons for inverse Compton emission. We then consider a structured jet, with the blazar component that-although not directly visible in the X-ray band-provides an intense field of seed synchrotron photons Compton-scattered by electrons in a mildly relativistic knot. In this case, the whole X-ray emission can be accounted for if we assume a blazar luminosity within the range observed from flat spectrum radio quasars. The X-ray radiative efficiency of such a (structured) jet is intimately related to the presence of a complex velocity structure. The jet emission can provide a significant contribution in X-rays if it decelerates within the host galaxy on kiloparsec scales. We discuss the implications of this model in terms of jet dynamics and interaction with the ambient medium.« less

Digital Dental X-ray Database for Caries Screening

NASA Astrophysics Data System (ADS)

Rad, Abdolvahab Ehsani; Rahim, Mohd Shafry Mohd; Rehman, Amjad; Saba, Tanzila

2016-06-01

Standard database is the essential requirement to compare the performance of image analysis techniques. Hence the main issue in dental image analysis is the lack of available image database which is provided in this paper. Periapical dental X-ray images which are suitable for any analysis and approved by many dental experts are collected. This type of dental radiograph imaging is common and inexpensive, which is normally used for dental disease diagnosis and abnormalities detection. Database contains 120 various Periapical X-ray images from top to bottom jaw. Dental digital database is constructed to provide the source for researchers to use and compare the image analysis techniques and improve or manipulate the performance of each technique.

X-ray fractography on fatigue fractured surface of austenitic stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yajima, Zenjiro; Tokuyama, Hideki; Kibayashi, Yasuo

1995-12-31

X-ray diffraction observation of the material internal structure beneath fracture surfaces provide fracture analysis with useful information to investigate the conditions and mechanisms of fracture. X-ray fractography is a generic name given to this technique. In the present study, X-ray fractography was applied to fatigue fracture surfaces of austenitic stainless steel (AISI 304) which consisted of solution treatment. The fatigue tests were carried out on compact tension (CT) specimens. The plastic strain on the fracture surface was estimated from measuring the line broadening of X-ray diffraction profiles. The line broadening of X-ray diffraction profiles was measured on and beneath fatiguemore » fracture surfaces. The depth of the plastic zone left on fracture surfaces was evaluated from the line broadening. The results are discussed on the basis of fracture mechanics.« less

Characterization results from several commercial soft X-ray streak cameras

NASA Astrophysics Data System (ADS)

Stradling, G. L.; Studebaker, J. K.; Cavailler, C.; Launspach, J.; Planes, J.

The spatio-temporal performance of four soft X-ray streak cameras has been characterized. The objective in evaluating the performance capability of these instruments is to enable us to optimize experiment designs, to encourage quantitative analysis of streak data and to educate the ultra high speed photography and photonics community about the X-ray detector performance which is available. These measurements have been made collaboratively over the space of two years at the Forge pulsed X-ray source at Los Alamos and at the Ketjak laser facility an CEA Limeil-Valenton. The X-ray pulse lengths used for these measurements at these facilities were 150 psec and 50 psec respectively. The results are presented as dynamically-measured modulation transfer functions. Limiting temporal resolution values were also calculated. Emphasis is placed upon shot noise statistical limitations in the analysis of the data. Space charge repulsion in the streak tube limits the peak flux at ultra short experiments duration times. This limit results in a reduction of total signal and a decrease in signal to no ise ratio in the streak image. The four cameras perform well with 20 1p/mm resolution discernable in data from the French C650X, the Hadland X-Chron 540 and the Hamamatsu C1936X streak cameras. The Kentech X-ray streak camera has lower modulation and does not resolve below 10 1p/mm but has a longer photocathode.

X-Ray Properties of Lensing-Selected Clusters

NASA Astrophysics Data System (ADS)

Paterno-Mahler, Rachel; Sharon, Keren; Bayliss, Matthew; McDonald, Michael; Gladders, Michael; Johnson, Traci; Dahle, Hakon; Rigby, Jane R.; Whitaker, Katherine E.; Florian, Michael; Wuyts, Eva

2017-08-01

I will present preliminary results from the Michigan Swift X-ray observations of clusters from the Sloan Giant Arcs Survey (SGAS). These clusters were lensing selected based on the presence of a giant arc visible from SDSS. I will characterize the morphology of the intracluster medium (ICM) of the clusters in the sample, and discuss the offset between the X-ray centroid, the mass centroid as determined by strong lensing analysis, and the BCG position. I will also present early-stage work on the scaling relation between the lensing mass and the X-ray luminosity.

REVIEWS OF TOPICAL PROBLEMS: Recent advances in X-ray refractive optics

NASA Astrophysics Data System (ADS)

Aristov, V. V.; Shabel'nikov, L. G.

2008-01-01

X-ray refractive optics has made rapid strides to a large degree due to the work of Russian scientists, and has now become one of the most rapidly advancing areas in modern physical optics. This review outlines the results of investigation of refractive devices and analysis of their properties. The conception of planar lenses made of silicon and other materials is set forth. We discuss the applications of refractive lenses to the transformation of X-ray images, photonic crystal research, and the development of focusing devices in high-energy X-ray telescopes.

Solar flares observed simultaneously with SphinX, GOES and RHESSI

NASA Astrophysics Data System (ADS)

Mrozek, Tomasz; Gburek, Szymon; Siarkowski, Marek; Sylwester, Barbara; Sylwester, Janusz; Kępa, Anna; Gryciuk, Magdalena

2013-07-01

In February 2009, during recent deepest solar minimum, Polish Solar Photometer in X-rays (SphinX) begun observations of the Sun in the energy range of 1.2-15 keV. SphinX was almost 100 times more sensitive than GOES X-ray Sensors. The silicon PIN diode detectors used in the experiment were carefully calibrated on the ground using Synchrotron Radiation Source BESSY II. The SphinX energy range overlaps with the Ramaty High Energy Solar Spectroscopic Imager (RHESSI) energy range. The instrument provided us with observations of hundreds of very small flares and X-ray brightenings. We have chosen a group of solar flares observed simultaneously with GOES, SphinX and RHESSI and performed spectroscopic analysis of observations wherever possible. The analysis of thermal part of the spectra showed that SphinX is a very sensitive complementary observatory for RHESSI and GOES.

Long-Term X-Ray Variability of Circinus X-1

NASA Technical Reports Server (NTRS)

Saz Parkinson, P. M.; Tournear, D. M.; Bloom, E. D.; Focke, W. B.; Reilly, K. T.

2003-01-01

We present an analysis of long term X-ray monitoring observations of Circinus X-1 (Cir X-1) made with four different instruments: Vela 5B, Ariel V ASM, Ginga ASM, and RXTE ASM, over the course of more than 30 years. We use Lomb-Scargle periodograms to search for the approx. 16.5 day orbital period of Cir X-1 in each of these data sets and from this derive a new orbital ephemeris based solely on X-ray measurements, which we compare to the previous ephemerides obtained from radio observations. We also use the Phase Dispersion Minimization (PDM) technique, as well as FFT analysis, to verify the periods obtained from periodograms. We obtain dynamic periodograms (both Lomb-Scargle and PDM) of Cir X-1 during the RXTE era, showing the period evolution of Cir X-1, and also displaying some unexplained discrete jumps in the location of the peak power.

Correlation between Wavelength Dispersive X-ray Fluorescence (WDXRF) analysis of hardened concrete for chlorides vs. Atomic Absorption (AA) analysis in accordance with AASHTO T- 260; sampling and testing for chloride ion in concrete and concrete raw mater

DOT National Transportation Integrated Search

2014-04-01

A correlation between Wavelength Dispersive X-ray Fluorescence(WDXRF) analysis of Hardened : Concrete for Chlorides and Atomic Absorption (AA) analysis (current method AASHTO T-260, procedure B) has been : found and a new method of analysis has been ...

Tritium analysis of divertor tiles used in JET ITER-like wall campaigns by means of β-ray induced x-ray spectrometry

NASA Astrophysics Data System (ADS)

Hatano, Y.; Yumizuru, K.; Koivuranta, S.; Likonen, J.; Hara, M.; Matsuyama, M.; Masuzaki, S.; Tokitani, M.; Asakura, N.; Isobe, K.; Hayashi, T.; Baron-Wiechec, A.; Widdowson, A.; contributors, JET

2017-12-01

Energy spectra of β-ray induced x-rays from divertor tiles used in ITER-like wall campaigns of the Joint European Torus were measured to examine tritium (T) penetration into tungsten (W) layers. The penetration depth of T evaluated from the intensity ratio of W(Lα) x-rays to W(Mα) x-rays showed clear correlation with poloidal position; the penetration depth at the upper divertor region reached several micrometers, while that at the lower divertor region was less than 500 nm. The deep penetration at the upper part was ascribed to the implantation of high energy T produced by DD fusion reactions. The poloidal distribution of total x-ray intensity indicated higher T retention in the inboard side than the outboard side of the divertor region.

Methods of chemical and phase composition analysis of gallstones

NASA Astrophysics Data System (ADS)

Suvorova, E. I.; Pantushev, V. V.; Voloshin, A. E.

2017-11-01

This review presents the instrumental methods used for chemical and phase composition investigation of gallstones. A great body of data has been collected in the literature on the presence of elements and their concentrations, obtained by fluorescence microscopy, X-ray fluorescence spectroscopy, neutron activation analysis, proton (particle) induced X-ray emission, atomic absorption spectroscopy, high-resolution gamma-ray spectrometry, electron paramagnetic resonance. Structural methods—powder X-ray diffraction, infrared spectroscopy, Raman spectroscopy—provide information about organic and inorganic phases in gallstones. Stone morphology was studied at the macrolevel with optical microscopy. Results obtained by analytical scanning and transmission electron microscopy with X-ray energy dispersive spectrometry are discussed. The chemical composition and structure of gallstones determine the strategy of removing stone from the body and treatment of patients: surgery or dissolution in the body. Therefore one chapter of the review describes the potential of dissolution methods. Early diagnosis and appropriate treatment of the disease depend on the development of clinical methods for in vivo investigation, which gave grounds to present the main characteristics and potential of ultrasonography (ultrasound scanning), magnetic resonance imaging, and X-ray computed tomography.

XAssist: A System for the Automation of X-ray Astrophysics Analysis

NASA Astrophysics Data System (ADS)

Ptak, A.

2004-08-01

XAssist is a NASA AISR-funded project for the automation of X-ray astrophysics. It is capable of data reprocessing, source detection, and preliminary spatial, temporal and spectral analysis for each source with sufficient counts. The bulk of the system is written in Python, which in turn drives underlying software (CIAO for Chandra data, etc.). Future work will include a GUI (mainly for beginners and status monitoring) and the exposure of at least some functionality as web services. The latter will help XAssist to eventually become part of the VO, making advanced queries possible, such as determining the X-ray fluxes of counterparts to HST or SDSS sources (including the use of unpublished X-ray data), and add the ability of ``on-the-fly'' X-ray processing. Pipelines are running on Chandra and XMM-Newton observations of galaxies to demonstrate XAssist's capabilities, and the results are available online (in real time) at http://www.xassist.org. XAssist itself as well as various associated projects are available for download.

Variable spectra of active galaxies

NASA Technical Reports Server (NTRS)

Halpern, Jules P.

1988-01-01

The analysis of EXOSAT spectra of active galaxies are presented. The objects examined for X-ray spectral variability were MR 2251-178 and 3C 120. The results of these investigations are described, as well as additional results on X-ray spectral variability related to EXOSAT observations of active galaxies. Additionally, the dipping X-ray source 4U1624-49 was also investigated.

Synchrotron x-ray modification of nanoparticle superlattice formation

NASA Astrophysics Data System (ADS)

Lu, Chenguang; Akey, Austin J.; Herman, Irving P.

2012-09-01

The synchrotron x-ray radiation used to perform small angle x-ray scattering (SAXS) during the formation of three-dimensional nanoparticle superlattices by drop casting nanoparticle solutions affects the structure and the local crystalline order of the resulting films. The domain size decreases due to the real-time SAXS analysis during drying and more macroscopic changes are visible to the eye.

Thin Film Research. Volume 1

DTIC Science & Technology

1985-05-30

Order (FECO) ......... 23 3. X -Ray Diffraction ............................... 26 4. Transmission Electron Microscopy (TEM) ............... 26 5...remained amorphous after bombardment, as evidenced by X - ray diffraction, and showed no other changes. 0 (2) For Sb203, the crystallite size was reduced...main effect on MgF2 was the reduction in crystallite size. The films were too thir. for meaningful x - ray diffraction analysis. Durability and

X-Ray Diffraction and the Discovery of the Structure of DNA

ERIC Educational Resources Information Center

Crouse, David T.

2007-01-01

A method is described for teaching the analysis of X-ray diffraction of DNA through a series of steps utilizing the original methods used by James Watson, Francis Crick, Maurice Wilkins and Rosalind Franklin. The X-ray diffraction pattern led to the conclusion of the basic helical structure of DNA and its dimensions while basic chemical principles…

Analysis of a measurement scheme for ultrafast hole dynamics by few femtosecond resolution X-ray pump-probe Auger spectroscopy.

PubMed

Cooper, Bridgette; Kolorenč, Přemysl; Frasinski, Leszek J; Averbukh, Vitali; Marangos, Jon P

2014-01-01

Ultrafast hole dynamics created in molecular systems as a result of sudden ionisation is the focus of much attention in the field of attosecond science. Using the molecule glycine we show through ab initio simulations that the dynamics of a hole, arising from ionisation in the inner valence region, evolves with a timescale appropriate to be measured using X-ray pulses from the current generation of SASE free electron lasers. The examined pump-probe scheme uses X-rays with photon energy below the K edge of carbon (275-280 eV) that will ionise from the inner valence region. A second probe X-ray at the same energy can excite an electron from the core to fill the vacancy in the inner-valence region. The dynamics of the inner valence hole can be tracked by measuring the Auger electrons produced by the subsequent refilling of the core hole as a function of pump-probe delay. We consider the feasibility of the experiment and include numerical simulation to support this analysis. We discuss the potential for all X-ray pump-X-ray probe Auger spectroscopy measurements for tracking hole migration.

Knee X-ray image analysis method for automated detection of Osteoarthritis

PubMed Central

Shamir, Lior; Ling, Shari M.; Scott, William W.; Bos, Angelo; Orlov, Nikita; Macura, Tomasz; Eckley, D. Mark; Ferrucci, Luigi; Goldberg, Ilya G.

2008-01-01

We describe a method for automated detection of radiographic Osteoarthritis (OA) in knee X-ray images. The detection is based on the Kellgren-Lawrence classification grades, which correspond to the different stages of OA severity. The classifier was built using manually classified X-rays, representing the first four KL grades (normal, doubtful, minimal and moderate). Image analysis is performed by first identifying a set of image content descriptors and image transforms that are informative for the detection of OA in the X-rays, and assigning weights to these image features using Fisher scores. Then, a simple weighted nearest neighbor rule is used in order to predict the KL grade to which a given test X-ray sample belongs. The dataset used in the experiment contained 350 X-ray images classified manually by their KL grades. Experimental results show that moderate OA (KL grade 3) and minimal OA (KL grade 2) can be differentiated from normal cases with accuracy of 91.5% and 80.4%, respectively. Doubtful OA (KL grade 1) was detected automatically with a much lower accuracy of 57%. The source code developed and used in this study is available for free download at www.openmicroscopy.org. PMID:19342330

Detailed Calibration of SphinX instrument at the Palermo XACT facility of INAF-OAPA

NASA Astrophysics Data System (ADS)

Szymon, Gburek; Collura, Alfonso; Barbera, Marco; Reale, Fabio; Sylwester, Janusz; Kowalinski, Miroslaw; Bakala, Jaroslaw; Kordylewski, Zbigniew; Plocieniak, Stefan; Podgorski, Piotr; Trzebinski, Witold; Varisco, Salvatore

The Solar photometer in X-rays (SphinX) experiment is scheduled for launch late summer 2008 on-board the Russian CORONAS-Photon satellite. SphinX will use three silicon PIN diode detectors with selected effective areas in order to record solar spectra in the X-ray energy range 0.3-15 keV with unprecedented temporal and medium energy resolution. High sensitivity and large dynamic range of the SphinX instrument will give for the first time possibility of observing solar soft X-ray variability from the weakest levels, ten times below present thresholds, to the largest X20+ flares. We present the results of the ground X-ray calibrations of the SphinX instrument performed at the X-ray Astronomy Calibration and Testing (XACT) facility of INAF-OAPA. The calibrations were essential for determination of SphinX detector energy resolution and efficiency. We describe the ground tests instrumental set-up, adopted measurement techniques and present results of the calibration data analysis.

Identification of two new HMXBs in the LMC: an ˜2013 s pulsar and a probable SFXT

NASA Astrophysics Data System (ADS)

Vasilopoulos, G.; Maitra, C.; Haberl, F.; Hatzidimitriou, D.; Petropoulou, M.

2018-03-01

We report on the X-ray and optical properties of two high-mass X-ray binary systems located in the Large Magellanic Cloud (LMC). Based on the obtained optical spectra, we classify the massive companion as a supergiant star in both systems. Timing analysis of the X-ray events collected by XMM-Newton revealed the presence of coherent pulsations (spin period ˜2013 s) for XMMU J053108.3-690923 and fast flaring behaviour for XMMU J053320.8-684122. The X-ray spectra of both systems can be modelled sufficiently well by an absorbed power law, yielding hard spectra and high intrinsic absorption from the environment of the systems. Due to their combined X-ray and optical properties, we classify both systems as SgXRBs: the 19th confirmed X-ray pulsar and a probable supergiant fast X-ray transient in the LMC, the second such candidate outside our Galaxy.

X-ray illumination of globular cluster puzzles. [globular cluster X ray sources as clues to Milky Way Galaxy age and evolution

NASA Technical Reports Server (NTRS)

Lightman, A. P.; Grindlay, J. E.

1982-01-01

Globular clusters are thought to be among the oldest objects in the Galaxy, and provide, in this connection, important clues for determining the age and process of formation of the Galaxy. The present investigation is concerned with puzzles relating to the X-ray emission of globular clusters, taking into account questions regarding the location of X-ray emitting clusters (XEGC) unusually near the galactic plane and/or galactic center. An adopted model is discussed for the nature, formation, and lifetime of X-ray sources in globular clusters. An analysis of the available data is conducted in connection with a search for correlations between binary formation time scales, central relaxation times, galactic locations, and X-ray emission. The positive correlation found between distance from galactic center and two-body binary formation time for globular clusters, explanations for this correlation, and the hypothesis that X-ray sources in globular clusters require binary star systems provide a possible explanation of the considered puzzles.

Identification of high-mass X-ray binaries selected from XMM-Newton observations of the LMC★

NASA Astrophysics Data System (ADS)

van Jaarsveld, N.; Buckley, D. A. H.; McBride, V. A.; Haberl, F.; Vasilopoulos, G.; Maitra, C.; Udalski, A.; Miszalski, B.

2018-04-01

The Large Magellanic Cloud (LMC) currently hosts around 23 high-mass X-ray binaries (HMXBs) of which most are Be/X-ray binaries. The LMC XMM-Newton survey provided follow-up observations of previously known X-ray sources that were likely HMXBs, as well as identifying new HMXB candidates. In total, 19 candidate HMXBs were selected based on their X-ray hardness ratios. In this paper we present red and blue optical spectroscopy, obtained with Southern African Large Telescope and the South African Astronomical Observatory 1.9-m telescope, plus a timing analysis of the long-term optical light curves from OGLE to confirm the nature of these candidates. We find that nine of the candidates are new Be/X-ray binaries, substantially increasing the LMC Be/X-ray binary population. Furthermore, we present the optical properties of these new systems, both individually and as a group of all the BeXBs identified by the XMM-Newton survey of the LMC.

Density of bunched threading dislocations in epitaxial GaN layers as determined using X-ray diffraction

NASA Astrophysics Data System (ADS)

Barchuk, M.; Holý, V.; Rafaja, D.

2018-04-01

X-ray diffraction is one of the most popular experimental methods employed for determination of dislocation densities, as it can recognize both the strain fields and the local lattice rotations produced by dislocations. The main challenge of the quantitative analysis of the dislocation density is the formulation of a suitable microstructure model, which describes the dislocation arrangement and the effect of the interactions between the strain fields from neighboring dislocations reliably in order to be able to determine the dislocation densities precisely. The aim of this study is to prove the capability of X-ray diffraction and two computational methods, which are frequently used for quantification of the threading dislocation densities from X-ray diffraction measurements, in the special case of partially bunched threading dislocations. The first method is based on the analysis of the dislocation-controlled crystal mosaicity, and the other one on the analysis of diffuse X-ray scattering from threading dislocations. The complementarity of both methods is discussed. Furthermore, it is shown how the complementarity of these methods can be used to improve the results of the quantitative analysis of bunched and thus inhomogeneously distributed threading dislocations and to get a better insight into the dislocation arrangement.

VizieR Online Data Catalog: Unidentified gamma-ray sources. IV. X-ray (Paggi+, 2013)

NASA Astrophysics Data System (ADS)

Paggi, A.; Massaro, F.; D'Abrusco, R.; Smith, H. A.; Masetti, N.; Giroletti, M.; Tosti, G.; Funk, S.

2013-11-01

The initial sample considered in our analysis is constituted by the 299 unidentified gamma-ray sources (UGSs) in the 2FGL catalog that do not present any γ-ray analysis flag (Nolan et al. 2012, Cat. J/ApJS/199/31). After Fermi was launched, the Swift XRT Survey of Fermi Unassociated Sources was started in order to perform follow-up observations of the unidentified gamma-ray sources (UGSs) in an attempt to find their potential X-ray counterparts (PI: A. Falcone). We analyze all data collected between the beginning of the follow-up program until 2013 March 31. We note that 203 of the 205 UGSs that constitute our sample have been also observed in the optical and UV by UVOT. We then produced for each X-ray observation the corresponding merged UVOT event files, adopting standard procedures. (6 data files).

The Chandra Source Catalog

NASA Astrophysics Data System (ADS)

Evans, Ian N.; Primini, F. A.; Glotfelty, K. J.; Anderson, C. S.; Bonaventura, N. R.; Chen, J. C.; Davis, J. E.; Doe, S. M.; Evans, J. D.; Fabbiano, G.; Galle, E. C.; Gibbs, D. G., II; Grier, J. D.; Hain, R. M.; Hall, D. M.; Harbo, P. N.; He, X.; Houck, J. C.; Karovska, M.; Kashyap, V. L.; Lauer, J.; McCollough, M. L.; McDowell, J. C.; Miller, J. B.; Mitschang, A. W.; Morgan, D. L.; Mossman, A. E.; Nichols, J. S.; Nowak, M. A.; Plummer, D. A.; Refsdal, B. L.; Rots, A. H.; Siemiginowska, A.; Sundheim, B. A.; Tibbetts, M. S.; Van Stone, D. W.; Winkelman, S. L.; Zografou, P.

2010-03-01

The Chandra Source Catalog (CSC) is a general purpose virtual X-ray astrophysics facility that provides access to a carefully selected set of generally useful quantities for individual X-ray sources, and is designed to satisfy the needs of a broad-based group of scientists, including those who may be less familiar with astronomical data analysis in the X-ray regime. The first release of the CSC includes information about 94,676 distinct X-ray sources detected in a subset of public ACIS imaging observations from roughly the first eight years of the Chandra mission. This release of the catalog includes point and compact sources with observed spatial extents < 30". The catalog (1) provides access to estimates of the X-ray source properties for detected sources with good scientific fidelity; (2) facilitates analysis of a wide range of statistical properties for classes of X-ray sources; and (3) provides efficient access to calibrated observational data and ancillary data products for individual X-ray sources. The catalog includes real X-ray sources detected with flux estimates that are at least 3 times their estimated 1σ uncertainties in at least one energy band, while maintaining the number of spurious sources at a level of < 1 false source per field for a 100 ks observation. For each detected source, the CSC provides commonly tabulated quantities, including source position, extent, multi-band fluxes, hardness ratios, and variability statistics. In addition, for each X-ray source the CSC includes an extensive set of file-based data products that can be manipulated interactively, including source images, event lists, light curves, and spectra. Support for development of the CSC is provided by the National Aeronautics and Space Administration through the Chandra X-ray Center, which is operated by the Smithsonian Astrophysical Observatory for and on behalf of the National Aeronautics and Space Administration under contract NAS 8-03060.

Identification of differentially expressed genes associated with the enhancement of X-ray susceptibility by RITA in a hypopharyngeal squamous cell carcinoma cell line (FaDu).

PubMed

Luan, Jinwei; Li, Xianglan; Guo, Rutao; Liu, Shanshan; Luo, Hongyu; You, Qingshan

2016-06-01

Next generation sequencing and bio-informatic analyses were conducted to investigate the mechanism of reactivation of p53 and induction of tumor cell apoptosis (RITA)-enhancing X-ray susceptibility in FaDu cells. The cDNA was isolated from FaDu cells treated with 0 X-ray, 8 Gy X-ray, or 8 Gy X-ray + RITA. Then, cDNA libraries were created and sequenced using next generation sequencing, and each assay was repeated twice. Subsequently, differentially expressed genes (DEGs) were identified using Cuffdiff in Cufflinks and their functions were predicted by pathway enrichment analyses. Genes that were constantly up- or down-regulated in 8 Gy X-ray-treated FaDu cells and 8 Gy X-ray + RITA-treated FaDu cells were obtained as RITA genes. Afterward, the protein-protein interaction (PPI) relationships were obtained from the STRING database and a PPI network was constructed using Cytoscape. Furthermore, ClueGO was used for pathway enrichment analysis of genes in the PPI network. Total 2,040 and 297 DEGs were identified in FaDu cells treated with 8 Gy X-ray or 8 Gy X-ray + RITA, respectively. PARP3 and NEIL1 were enriched in base excision repair, and CDK1 was enriched in p53 signaling pathway. RFC2 and EZH2 were identified as RITA genes. In the PPI network, many interaction relationships were identified (e.g., RFC2-CDK1, EZH2-CDK1 and PARP3-EZH2). ClueGO analysis showed that RFC2 and EZH2 were related to cell cycle. RFC2, EZH2, CDK1, PARP3 and NEIL1 may be associated, and together enhance the susceptibility of FaDu cells treated with RITA to the deleterious effects of X-ray.

Gold nanoparticle contrast agents in advanced X-ray imaging technologies.

PubMed

Ahn, Sungsook; Jung, Sung Yong; Lee, Sang Joon

2013-05-17

Recently, there has been significant progress in the field of soft- and hard-X-ray imaging for a wide range of applications, both technically and scientifically, via developments in sources, optics and imaging methodologies. While one community is pursuing extensive applications of available X-ray tools, others are investigating improvements in techniques, including new optics, higher spatial resolutions and brighter compact sources. For increased image quality and more exquisite investigation on characteristic biological phenomena, contrast agents have been employed extensively in imaging technologies. Heavy metal nanoparticles are excellent absorbers of X-rays and can offer excellent improvements in medical diagnosis and X-ray imaging. In this context, the role of gold (Au) is important for advanced X-ray imaging applications. Au has a long-history in a wide range of medical applications and exhibits characteristic interactions with X-rays. Therefore, Au can offer a particular advantage as a tracer and a contrast enhancer in X-ray imaging technologies by sensing the variation in X-ray attenuation in a given sample volume. This review summarizes basic understanding on X-ray imaging from device set-up to technologies. Then this review covers recent studies in the development of X-ray imaging techniques utilizing gold nanoparticles (AuNPs) and their relevant applications, including two- and three-dimensional biological imaging, dynamical processes in a living system, single cell-based imaging and quantitative analysis of circulatory systems and so on. In addition to conventional medical applications, various novel research areas have been developed and are expected to be further developed through AuNP-based X-ray imaging technologies.

Small-angle X-ray scattering (SAXS) studies of the structure of mesoporous silicas

NASA Astrophysics Data System (ADS)

Zienkiewicz-Strzałka, M.; Skibińska, M.; Pikus, S.

2017-11-01

Mesoporous ordered silica nanostructures show strong interaction with X-ray radiation in the range of small-angles. Small-angle X-ray scattering (SAXS) measurements based on the elastically scattered X-rays are important in analysis of condensed matter. In the case of mesoporous silica materials SAXS technique provides information on the distribution of electron density in the mesoporous material, in particular describing their structure and size of the unit cell as well as type of ordered structure and finally their parameters. The characterization of nanopowder materials, nanocomposites and porous materials by Small-Angle X-ray Scattering seems to be valuable and useful. In presented work, the SAXS investigation of structures from the group of mesoporous ordered silicates was performed. This work has an objective to prepare functional materials modified by noble metal ions and nanoparticles and using the small-angle X-ray scattering to illustrate their properties. We report the new procedure for describing mesoporous materials belonging to SBA-15 and MCM-41 family modified by platinum, palladium and silver nanoparticles, based on detailed analysis of characteristic peaks in the small-angle range of X-ray scattering. This procedure allows to obtained the most useful parameters for mesoporous materials characterization and their successfully compare with experimental measurements reducing the time and material consumption with good precision for particles and pores with a size below 10 nm.

Evaluation of partial coherence correction in X-ray ptychography

DOE PAGES

Burdet, Nicolas; Shi, Xiaowen; Parks, Daniel; ...

2015-02-23

Coherent X-ray Diffraction Imaging (CDI) and X-ray ptychography both heavily rely on the high degree of spatial coherence of the X-ray illumination for sufficient experimental data quality for reconstruction convergence. Nevertheless, the majority of the available synchrotron undulator sources have a limited degree of partial coherence, leading to reduced data quality and a lower speckle contrast in the coherent diffraction patterns. It is still an open question whether experimentalists should compromise the coherence properties of an X-ray source in exchange for a higher flux density at a sample, especially when some materials of scientific interest are relatively weak scatterers. Amore » previous study has suggested that in CDI, the best strategy for the study of strong phase objects is to maintain a high degree of coherence of the illuminating X-rays because of the broadening of solution space resulting from the strong phase structures. In this article, we demonstrate the first systematic analysis of the effectiveness of partial coherence correction in ptychography as a function of the coherence properties, degree of complexity of illumination (degree of phase diversity of the probe) and sample phase complexity. We have also performed analysis of how well ptychographic algorithms refine X-ray probe and complex coherence functions when those variables are unknown at the start of reconstructions, for noise-free simulated data, in the case of both real-valued and highly-complex objects.« less

Revisiting Weak Emission-line Quasars with a Simple Approach to Deduce their Nature and the Tracers of X-ray Weakness

NASA Astrophysics Data System (ADS)

Ni, Qingling

2018-01-01

We present an X-ray and multi-wavelength study of 17 “bridge” weak emission-line quasars (WLQs) and 16 “extreme” WLQs naturally divided by their C IV rest equivalent widths (REWs), which constitute our clean WLQ sample together. New Chandra 3.1-4.8 ks observations were obtained for 14 objects while the other 19 have archival X-ray observations. 4 of the 17 bridge WLQs appear to be X-ray weak, while 9 of the 16 extreme WLQs appear to be X-ray weak. The X-ray weak fraction in the bridge sample (23.5%) is lower than in the extreme sample(56.3%), indicating the fraction of X-ray weak objects along with rising C IV REWs.X-ray stacking analysis is performed for the X-ray weak WLQs in the clean sample. We measured a relatively hard (Γeff=1.37) effective power-law photon index for a stack of the X-ray weak subsample, suggesting X-ray absorption due to shielding material inside the broad emission-line region (BELR). We proposed a geometrically and optically thick inner accretion disk as the natural shield, which could also explain the behavior of the X-ray weak fraction along with C IV REW.Futhermore, we ran Peto-Prentice tests to assess if the distributions of optical-UV spectral properties are different between X-ray weak WLQs and X-ray normal WLQs. We also examined correlations between △αOX and optical-UV spectral properties. The C IV REW, C IV blueshift, C IV FWHM, REWs of the Si IV, λ1900, Fe II, and Mg II emission features, and the relative SDSS color △(g - i) are examined in our study. △(g - i) turned out to be the most effective tracer of X-ray weakness.

Nuclear Forensics Applications of Principal Component Analysis on Micro X-ray Fluorescence Images

DTIC Science & Technology

analysis on quantified micro x-ray fluorescence intensity values. This method is then applied to address goals of nuclear forensics . Thefirst...researchers in the development and validation of nuclear forensics methods. A method for determining material homogeneity is developed and demonstrated

THE MULTIELEMENTAL ANALYSIS OF DRINKING WATER USING PROTON-INDUCED X-RAY EMISSION (PIXE)

EPA Science Inventory

A new, rapid, and economical method for the multielemental analysis of drinking water samples is described. The concentrations of 76 elements heavier than aluminum are determined using proton-induced x-ray emission (PIXE) technology. The concentration of sodium is evaluated using...

Crystallization and preliminary X-ray diffraction analysis of a chitin-binding domain of hyperthermophilic chitinase from Pyrococcus furiosus

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nakamura, Tsutomu; Ishikawa, Kazuhiko; Hagihara, Yoshihisa

The expression, purification and preliminary X-ray diffraction studies of a chitin-binding domain of the chitinase from P. furiosus are reported. The crystallization and preliminary X-ray diffraction analysis of the chitin-binding domain of chitinase from a hyperthermophilic archaeon, Pyrococcus furiosus, are reported. The recombinant protein was prepared using an Escherichia coli overexpression system and was crystallized by the hanging-drop vapour-diffusion method. An X-ray diffraction data set was collected to 1.70 Å resolution. The crystal belonged to space group P4{sub 3}2{sub 1}2 or P4{sub 1}2{sub 1}2. The unit-cell parameters were determined to be a = b = 48.8, c = 85.0 Å.

Combined FDTD-Monte Carlo analysis and a novel design for ZnO scintillator rods in polycarbonate membrane for X-ray imaging

NASA Astrophysics Data System (ADS)

Mohammadian-Behbahani, Mohammad-Reza; Saramad, Shahyar; Mohammadi, Mohammad

2017-05-01

A combination of Finite Difference Time Domain (FDTD) and Monte Carlo (MC) methods is proposed for simulation and analysis of ZnO microscintillators grown in polycarbonate membrane. A planar 10 keV X-ray source irradiating the detector is simulated by MC method, which provides the amount of absorbed X-ray energy in the assembly. The transport of generated UV scintillation light and its propagation in the detector was studied by the FDTD method. Detector responses to different probable scintillation sites and under different energies of X-ray source from 10 to 25 keV are reported. Finally, the tapered geometry for the scintillators is proposed, which shows enhanced spatial resolution in comparison to cylindrical geometry for imaging applications.

QUASI-PERIODIC PULSATIONS IN THE GAMMA-RAY EMISSION OF A SOLAR FLARE

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nakariakov, V. M.; Foullon, C.; Inglis, A. R.

2010-01-01

Quasi-periodic pulsations (QPPs) of gamma-ray emission with a period of about 40 s are found in a single loop X-class solar flare on 2005 January 1 at photon energies up to 2-6 MeV with the SOlar Neutrons and Gamma-rays (SONG) experiment aboard the CORONAS-F mission. The oscillations are also found to be present in the microwave emission detected with the Nobeyama Radioheliograph, and in the hard X-ray and low energy gamma-ray channels of RHESSI. Periodogram and correlation analysis shows that the 40 s QPPs of microwave, hard X-ray, and gamma-ray emission are almost synchronous in all observation bands. Analysis ofmore » the spatial structure of hard X-ray and low energy (80-225 keV) gamma-ray QPP with RHESSI reveals synchronous while asymmetric QPP at both footpoints of the flaring loop. The difference between the averaged hard X-ray fluxes coming from the two footpoint sources is found to oscillate with a period of about 13 s for five cycles in the highest emission stage of the flare. The proposed mechanism generating the 40 s QPP is a triggering of magnetic reconnection by a kink oscillation in a nearby loop. The 13 s periodicity could be produced by the second harmonics of the sausage mode of the flaring loop.« less

Nonlinear X-Ray and Auger Spectroscopy at X-Ray Free-Electron Laser Sources

NASA Astrophysics Data System (ADS)

Rohringer, Nina

2015-05-01

X-ray free-electron lasers (XFELs) open the pathway to transfer non-linear spectroscopic techniques to the x-ray domain. A promising all x-ray pump probe technique is based on coherent stimulated electronic x-ray Raman scattering, which was recently demonstrated in atomic neon. By tuning the XFEL pulse to core-excited resonances, a few seed photons in the spectral tail of the XFEL pulse drive an avalanche of resonant inelastic x-ray scattering events, resulting in exponential amplification of the scattering signal by of 6-7 orders of magnitude. Analysis of the line profile of the emitted radiation permits to demonstrate the cross over from amplified spontaneous emission to coherent stimulated resonance scattering. In combination with statistical covariance mapping, a high-resolution spectrum of the resonant inelastic scattering process can be obtained, opening the path to coherent stimulated x-ray Raman spectroscopy. An extension of these ideas to molecules and a realistic feasibility study of stimulated electronic x-ray Raman scattering in CO will be presented. Challenges to realizing stimulated electronic x-ray Raman scattering at present-day XFEL sources will be discussed, corroborated by results of a recent experiment at the LCLS XFEL. Due to the small gain cross section in molecular targets, other nonlinear spectroscopic techniques such as nonlinear Auger spectroscopy could become a powerful alternative. Theory predictions of a novel pump probe technique based on resonant nonlinear Auger spectroscopic will be discussed and the method will be compared to stimulated x-ray Raman spectroscopy.

Low-temperature synthesis of homogeneous solid solutions of scheelite-structured Ca 1-xSr xWO 4 and Sr 1-xBa xWO 4 nanocrystals

DOE PAGES

Culver, Sean P.; Greaney, Matthew J.; Tinoco, Antonio; ...

2015-07-24

Here, a series of compositionally complex scheelite-structured nanocrystals of the formula A 1-xA’ xWO 4 (A = Ca, Sr, Ba) have been prepared under benign synthesis conditions using the vapor diffusion sol–gel method. Discrete nanocrystals with sub-20 nm mean diameters were obtained after kinetically controlled hydro- lysis and polycondensation at room temperature, followed by composition-dependent thermal aging at or below 60 °C. Rietveld analysis of X-ray diffraction data and Raman spectroscopy verified the synthesis of continuous and phase-pure nanocrystal solid solutions across the entire composition space for A 1-xA’ xWO 4, where 0 ≤ x ≤ 1. Elemental analysis bymore » X-ray photoelectron and inductively coupled plasma- atomic emission spectroscopies demonstrated excellent agreement between the nominal and experi- mentally determined elemental stoichiometries, while energy dispersive X-ray spectroscopy illustrated good spatial elemental homogeneity within these nanocrystals synthesized under benign conditions.« less

Energy-Dispersive X-Ray Fluorescence Spectrometry: A Long Overdue Addition to the Chemistry Curriculum

ERIC Educational Resources Information Center

Palmer, Peter T.

2011-01-01

Portable Energy-Dispersive X-Ray Fluorescence (XRF) analyzers have undergone significant improvements over the past decade. Salient advantages of XRF for elemental analysis include minimal sample preparation, multielement analysis capabilities, detection limits in the low parts per million (ppm) range, and analysis times on the order of 1 min.…

CIAO: A Modern Data Analysis System for X-Ray Astronomy

NASA Astrophysics Data System (ADS)

Fruscione, Antonella

2017-08-01

It is now eighteen years after launch and Chandra continues to produce spectacular results!A portion of the success is to be attributed to the data analysis software CIAO (Chandra Interactive Analysis of Observations) that the Chandra X-Ray Center (CXC) continues to improve and release year after year.CIAO is downloaded more than 1200 times a year and it is used by a wide variety of users around the world: from novice to experienced X-ray astronomers, high school, undergraduate and graduate students, archival users (many new to X-ray or Chandra data), users with extensive resources and others from smaller countries and institutions.The scientific goals and kinds of datasets and analysis cover a wide range: observations spanning from days to years, different instrument configurations and different kinds of targets, from pointlike stars and quasars, to fuzzy galaxies and clusters, to moving solar objects. These different needs and goals require a variety of specialized software and careful and detailed documentation which is what the CIAO software provides. In general, we strive to build a software system which is easy for beginners, yet powerful for advanced users.The complexity of the Chandra data require a flexible data analysis system which provides an environment where the users can apply our tools, but can also explore and construct their own applications. The main purpose of this talk is to present CIAO as a modern data analysis system for X-ray data analysis.CIAO has grown tremendously over the years and we will highlight (a) the most recent advancements with a particular emphasis on the newly developed high-level scripts which simplify the analysis steps for the most common cases making CIAO more accessible to all users - including beginners and users who are not X-ray astronomy specialists, (b) the python-based Sherpa modelling and fitting application and the new stand-alone version openly developed and distributed on Github and (c) progress on methods to characterize the Chandra PSF.

Identification of Hard X-ray Sources in Galactic Globular Clusters: Simbol-X Simulations

NASA Astrophysics Data System (ADS)

Servillat, M.

2009-05-01

Globular clusters harbour an excess of X-ray sources compared to the number of X-ray sources in the Galactic plane. It has been proposed that many of these X-ray sources are cataclysmic variables that have an intermediate magnetic field, i.e. intermediate polars, which remains to be confirmed and understood. We present here several methods to identify intermediate polars in globular clusters from multiwavelength analysis. First, we report on XMM-Newton, Chandra and HST observations of the very dense Galactic globular cluster NGC 2808. By comparing UV and X-ray properties of the cataclysmic variable candidates, the fraction of intermediate polars in this cluster can be estimated. We also present the optical spectra of two cataclysmic variables in the globular cluster M 22. The HeII (4868 Å) emission line in these spectra could be related to the presence of a magnetic field in these objects. Simulations of Simbol-X observations indicate that the angular resolution is sufficient to study X-ray sources in the core of close, less dense globular clusters, such as M 22. The sensitivity of Simbol-X in an extended energy band up to 80 keV will allow us to discriminate between hard X-ray sources (such as magnetic cataclysmic variables) and soft X-ray sources (such as chromospherically active binaries).

UNCERTAINTY IN SCALING NUTRIENT EXPORT COEFFICIENTS

EPA Science Inventory

The Innov-X XT400 portable XRF analyzer features a miniature, rugged x-ray tube excitation source for analyzing a wide variety of elements and sample materials, including alloys, environmental solids, and other analytical samples. The x-ray tube source and Light Element Analysis...

"X-Ray Transients in Star-Forming Regions" and "Hard X-Ray Emission from X-Ray Bursters"

NASA Technical Reports Server (NTRS)

Halpern, Jules P.; Kaaret, Philip

1999-01-01

This grant funded work on the analysis of data obtained with the Burst and Transient Experiment (BATSE) on the Compton Gamma-Ray Observatory. The goal of the work was to search for hard x-ray transients in star forming regions using the all-sky hard x-ray monitoring capability of BATSE. Our initial work lead to the discovery of a hard x-ray transient, GRO J1849-03. Follow-up observations of this source made with the Wide Field Camera on BeppoSAX showed that the source should be identified with the previously known x-ray pulsar GS 1843-02 which itself is identified with the x-ray source X1845-024 originally discovered with the SAS-3 satellite. Our identification of the source and measurement of the outburst recurrence time, lead to the identification of the source as a Be/X-ray binary with a spin period of 94.8 s and an orbital period of 241 days. The funding was used primarily for partial salary and travel support for John Tomsick, then a graduate student at Columbia University. John Tomsick, now Dr. Tomsick, received his Ph.D. from Columbia University in July 1999, based partially on results obtained under this investigation. He is now a postdoctoral research scientist at the University of California, San Diego.

X-ray Measurements of a Thermo Scientific P385 DD Neutron Generator

DOE Office of Scientific and Technical Information (OSTI.GOV)

E.H. Seabury; D.L. Chichester; A.J. Caffrey

2001-08-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X-rays are a normal byproduct from a neutron generator and depending on their intensity and energy they can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum was measuredmore » with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x-rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60° between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and the x-ray emission appears to be axially symmetric within the neutron generator.« less

Improving packaged food quality and safety. Part 1: synchrotron X-ray analysis.

PubMed

López-Rubio, A; Hernandez-Muñoz, P; Catala, R; Gavara, R; Lagarón, J M

2005-10-01

The objective was to demonstrate, as an example of an application, the potential of synchrotron X-ray analysis to detect morphological alterations that can occur in barrier packaging materials and structures. These changes can affect the packaging barrier characteristics when conventional food preservation treatments are applied to packaged food. The paper presents the results of a number of experiments where time-resolved combined wide-angle X-ray scattering and small-angle X-ray scattering analysis as a function of temperature and humidity were applied to ethylene-vinyl alcohol co-polymers (EVOH), polypropylene (PP)/EVOH/PP structures, aliphatic polyketone terpolymer (PK) and amorphous polyamide (aPA) materials. A comparison between conventional retorting and high-pressure processing treatments in terms of morphologic alterations are also presented for EVOH. The impact of retorting on the EVOH structure contrasts with the good behaviour of the PK during this treatment and with that of aPA. However, no significant structural changes were observed by wide-angle X-ray scattering in the EVOH structures after high-pressure processing treatment. These structural observations have also been correlated with oxygen permeability measurements that are of importance when guaranteeing the intended levels of safety and quality of packaged food.

Analysis of Microflares from the Second Sounding Rocket Flight of the Focusing Optics X-ray Solar Imager (FOXSI-2)

NASA Astrophysics Data System (ADS)

Vievering, J. T.; Glesener, L.; Krucker, S.; Christe, S.; Buitrago-Casas, J. C.; Ishikawa, S. N.; Ramsey, B.; Takahashi, T.; Watanabe, S.

2016-12-01

Observations of the sun in hard x-rays can provide insight into many solar phenomena which are not currently well-understood, including the mechanisms behind particle acceleration in flares. Currently, RHESSI is the only solar-dedicated spacecraft observing in the hard x-ray regime. Though RHESSI has greatly added to our knowledge of flare particle acceleration, the method of rotation modulation collimators is limited in sensitivity and dynamic range. By instead using a direct imaging technique, the structure and evolution of even small flares and active regions can be investigated in greater depth. FOXSI (Focusing Optics X-ray Solar Imager), a hard x-ray instrument flown on two sounding rocket campaigns, seeks to achieve these improved capabilities by using focusing optics for solar observations in the 4-20 keV range. During the second of the FOXSI flights, flown on December 11, 2014, two microflares were observed, estimated as GOES class A0.5 and A2.5 (upper limits). Preliminary analysis of these two flares will be presented, including imaging spectroscopy, light curves, and photon spectra. Through this analysis, we investigate the capabilities of FOXSI in enhancing our knowledge of smaller-scale solar events.

TES X-ray microcalorimeters for X-ray astronomy and material analysis

NASA Astrophysics Data System (ADS)

Mitsuda, Kazuhisa

2016-11-01

TES X-ray microcalorimeter arrays provide not only high-energy resolution (FWHM < 10eV) in X-ray spectroscopy but also imaging and high-counting-rate capabilities. They are very promising spectrometer for X-ray astronomy and material analysis. In this paper, we report our recent progress. For material analysis, we have fabricated 8 × 8 format array with a fast signal response ( 40 μs) and proved the energy resolution of 5.8 eV FWHM at 5.9 keV. We developed common biasing scheme to reduce number of wirings from room temperature to the cryogenic stage. From measurements using the newly-designed common-bias SQUID array amplifier chips, and from numerical simulations, we demonstrated that signal cross talks due to the common bias is enough small. For space applications, we are developing frequency-division signal multiplexing system. We have fabricated a baseband feedback system and demonstrated that the noise added by the feedback system is about 4 eV FWHM equivalent for 16 ch multiplexing system. The digital to analog converter (DAC) dominates the noise, and needs be reduced by a factor of four for future astronomy missions.

INTEGRAL results on supergiant fast X-ray transients and accretion mechanism interpretation: ionization effect and formation of transient accretion discs

NASA Astrophysics Data System (ADS)

Ducci, L.; Sidoli, L.; Paizis, A.

2010-11-01

We performed a systematic analysis of all INTEGRAL observations from 2003 to 2009 of 14 supergiant fast X-ray transients (SFXTs), implying a net exposure time of about 30 Ms. For each source we obtained light curves and spectra (3-100 keV), discovering several new outbursts. We discuss the X-ray behaviour of SFXTs emerging from our analysis in the framework of the clumpy wind accretion mechanism we proposed. We discuss the effect of X-ray photoionization on accretion in close binary systems such as IGR J16479-4514 and IGR J17544-2619. We show that, because of X-ray photoionization, there is a high probability of an accretion disc forming from the capture of angular momentum in IGR J16479-4514, and we suggest that the formation of transient accretion discs could be partly responsible for the flaring activity in SFXTs with narrow orbits. We also propose an alternative way to explain the origin of flares with peculiar shapes observed in our analysis applying the model of Lamb et al., which is based on accretion via the Rayleigh-Taylor instability and was originally proposed to explain Type II bursts.

REVIEWS OF TOPICAL PROBLEMS: Cygnus X-3: a powerful galactic source of hard radiation

NASA Astrophysics Data System (ADS)

Vladimirskiĭ, B. M.; Gal'per, A. M.; Luchkov, B. I.; Stepanyan, A. A.

1985-02-01

A review is given of experimental and theoretical research on the galactic source Cyg X-3, whose electromagnetic spectrum extends from radio frequencies to ultrahigh-energy (Eγ ~ 1016 eV) γ-rays. Cyg X-3 also has a high x-ray luminosity (1038 erg/sec) and exhibits diversified sporadic and periodic variations, most notably occasional radio outbursts and a 4h.8 infrared, x-ray, and γ-ray cycle. Analysis of the observations indicates that Cyg X-3 is a close binary system comprising a compact relativistic object (neutron star, black hole) and a dwarf companion losing mass. Particles are accelerated to 1016 eV within the system.

The Origin of the UCSD X-ray Astronomy Program - A Personal Perspective

NASA Astrophysics Data System (ADS)

Peterson, Laurence E.

2013-01-01

I was a graduate student in the late 1950’s at the University of Minnesota in the Cosmic Ray Group under Prof. John R. Winckler. He had a project monitoring Cosmic ray time variations from an extensive series of balloon flights using simple detectors during the International Geophysical Year 1957-58. During the 20 March 1958 flight, a short 18 sec. burst of high energy radiation was observed simultaneously with a class II Solar flare. From the ratio of the Geiger counter rate to the energy loss in the ionization chamber, it was determined this radiation was likely hard X-rays or low-energy gamma rays and not energetic particles. Further analysis using information from other concurrent observations indicated the X-rays were likely due to Bremsstrahlung from energetic electrons accelerated in the solar flare magnetic field; these same electrons produced radio emissions. This first detection of extra-terrestrial X- or gamma rays showed the importance of non-thermal processes in Astrophysical phenomena. Winckler and I were interested by the possibility of non-solar hard X-rays. While completing my thesis on a Cosmic ray topic, I initiated a balloon program to develop more sensitive collimated low-background scintillation counters. This led to a proposal to the newly formed NASA to place an exploratory instrument on the 1st Orbiting Solar Observatory launched 7 March 1962. In August that year, I assumed a tenure-track position at UCSD; the data analysis of OSO-1 and the balloon program were transferred to UCSD to initiate the X-ray Astronomy program. The discovery of Cosmic X-ray sources in the 1-10 Kev range on a rocket flight in June 1962 by Giacconi and colleagues gave impetus to the UCSD activities. It seemed evident cosmic X-ray sources could be detected above 20 Kev using high-flying balloons. Early results included measurements of the 50 million K gas in SCO X-1, and the X-ray continuum from the Crab Nebula characterized by a power-law dN/dE ~ E-2.2. The instrument developments resulted in ever more sophisticated and sensitive counter systems. Follow-on instruments were flown on OSO-III and OSO-VII by the early 70’s, the HEAO-1 in 1976, and the RXTE in 1995. These provided many new results on Cosmic X-rays.

Using acoustic levitation in synchrotron based laser pump hard x-ray probe experiments

NASA Astrophysics Data System (ADS)

Hu, Bin; Lerch, Jason; Suthar, Kamlesh; Dichiara, Anthony

Acoustic levitation provides a platform to trap and hold a small amount of material by using standing pressure waves without a container. The technique has a potential to be used for laser pump x-ray probe experiments; x-ray scattering and laser distortion from the container can be avoided, sample consumption can be minimized, and unwanted chemistry that may occur at the container interface can be avoided. The method has been used at synchrotron sources for studying protein and pharmaceutical solutions using x-ray diffraction (XRD) and small angle x-ray scattering (SAXS). However, pump-probe experiments require homogeneously excited samples, smaller than the absorption depth of the material that must be held stably at the intersection of both the laser and x-ray beams. We discuss 1) the role of oscillations in acoustic levitation and the optimal acoustic trapping conditions for x-ray/laser experiments, 2) opportunities to automate acoustic levitation for fast sample loading and manipulation, and 3) our experimental results using SAXS to monitor laser induced thermal expansion in gold nanoparticles solution. We also performed Finite Element Analysis to optimize the trapping performance and stability of droplets ranging from 0.4 mm to 2 mm. Our early x-ray/laser demonstrated the potential of the technique for time-resolved X-ray science.

Gamma-ray emission from globular clusters. Shock high energy emission from the Be-Star/Pulsar System PSR 1259-63. Echoes in x-ray novae

NASA Technical Reports Server (NTRS)

Kaaret, Philip

1995-01-01

This grant covers work on the Compton phase 3 investigation, 'Shock High Energy Emission from the Be- Star/Pulsar System PSR 1259-63' and cycle 4 investigations 'Diffuse Gamma-Ray Emission at High Latitudes' and 'Echoes in X-Ray Novae'. Work under the investigation 'Diffuse Gamma-Ray Emission at High Latitudes' has lead to the publication of a paper (attached), describing gamma-ray emissivity variations in the northern galactic hemisphere. Using archival EGRET data, we have found a large irregular region of enhanced gamma-ray emissivity at energies greater 100 MeV. This is the first observation of local structure in the gamma-ray emissivity. Work under the investigation 'Echoes in X-Ray Novae' is proceeding with analysis of data from OSSE from the transient source GRO J1655-40. The outburst of this source last fall triggered this Target of Opportunity investigation. Preliminary spectral analysis shows emission out to 600 keV and a pure power low spectrum with no evidence of an exponential cutoff. Work is complete on the analysis of BATSE data from the Be-Star/Pulsar Sustem PSR 1259-63.

The x ray properties of a large, uniform QSO sample: Einstein observations of the LBQS

NASA Technical Reports Server (NTRS)

Margon, B.; Anderson, S. F.; Xu, X.; Green, P. J.; Foltz, C. B.

1992-01-01

Although there are large numbers of Quasi Stellar Objects (QSO's) now observed in X rays, extensive X-ray observations of uniformly selected, 'complete' QSO samples are more rare. The Large Bright QSO Survey (LBQS) consists of about 1000 objects with well understood properties, most brighter than B = 18.8 and thus amenable to X-ray detections in relatively brief exposures. The sample is thought to be highly complete in the range 0.2 less than z less than 3.3, a significantly broader interval than many other surveys. The Einstein IPC observed 150 of these objects, mostly serendipitously, during its lifetime. We report the results of an analysis of these IPC data, considering not only the 20 percent of the objects we find to have positive X-ray detections, but also the ensemble X-ray properties derived by 'image stacking'.

X-ray modeling for SMILE

NASA Astrophysics Data System (ADS)

Sun, T.; Wang, C.; Wei, F.; Liu, Z. Q.; Zheng, J.; Yu, X. Z.; Sembay, S.; Branduardi-Raymont, G.

2016-12-01

SMILE (Solar wind Magnetosphere Ionosphere Link Explorer) is a novel mission to explore the coupling of the solar wind-magnetosphere-ionosphere system via providing global images of the magnetosphere and aurora. As the X-ray imaging is a brand new technique applied to study the large scale magnetopause, modeling of the solar wind charge exchange (SWCX) X-ray emissions in the magnetosheath and cusps is vital in various aspects: it helps the design of the Soft X-ray Imager (SXI) on SMILE, selection of satellite orbits, as well as the analysis of expected scientific outcomes. Based on the PPMLR-MHD code, we present the simulation results of the X-ray emissions in geospace during storm time. Both the polar orbit and the Molniya orbit are used. From the X-ray images of the magnetosheath and cusps, the magnetospheric responses to an interplanetary shock and IMF southward turning are analyzed.

Quantum theory for 1D X-ray free electron laser

DOE PAGES

Anisimov, Petr Mikhaylovich

2017-09-19

Classical 1D X-ray Free Electron Laser (X-ray FEL) theory has stood the test of time by guiding FEL design and development prior to any full-scale analysis. Future X-ray FELs and inverse-Compton sources, where photon recoil approaches an electron energy spread value, push the classical theory to its limits of applicability. After substantial efforts by the community to find what those limits are, there is no universally agreed upon quantum approach to design and development of future X-ray sources. We offer a new approach to formulate the quantum theory for 1D X-ray FELs that has an obvious connection to the classicalmore » theory, which allows for immediate transfer of knowledge between the two regimes. In conclusion, we exploit this connection in order to draw quantum mechanical conclusions about the quantum nature of electrons and generated radiation in terms of FEL variables.« less

Design and analysis of x-ray vision systems for high-speed detection of foreign body contamination in food

NASA Astrophysics Data System (ADS)

Graves, Mark; Smith, Alexander; Batchelor, Bruce G.; Palmer, Stephen C.

1994-10-01

In the food industry there is an ever increasing need to control and monitor food quality. In recent years fully automated x-ray inspection systems have been used to detect food on-line for foreign body contamination. These systems involve a complex integration of x- ray imaging components with state of the art high speed image processing. The quality of the x-ray image obtained by such systems is very poor compared with images obtained from other inspection processes, this makes reliable detection of very small, low contrast defects extremely difficult. It is therefore extremely important to optimize the x-ray imaging components to give the very best image possible. In this paper we present a method of analyzing the x-ray imaging system in order to consider the contrast obtained when viewing small defects.

Quantum theory for 1D X-ray free electron laser

NASA Astrophysics Data System (ADS)

Anisimov, Petr M.

2018-06-01

Classical 1D X-ray Free Electron Laser (X-ray FEL) theory has stood the test of time by guiding FEL design and development prior to any full-scale analysis. Future X-ray FELs and inverse-Compton sources, where photon recoil approaches an electron energy spread value, push the classical theory to its limits of applicability. After substantial efforts by the community to find what those limits are, there is no universally agreed upon quantum approach to design and development of future X-ray sources. We offer a new approach to formulate the quantum theory for 1D X-ray FELs that has an obvious connection to the classical theory, which allows for immediate transfer of knowledge between the two regimes. We exploit this connection in order to draw quantum mechanical conclusions about the quantum nature of electrons and generated radiation in terms of FEL variables.

Photochemically Generated Thiyl Free Radicals Observed by X-ray Absorption Spectroscopy

DOE PAGES

Sneeden, Eileen Y.; Hackett, Mark J.; Cotelesage, Julien J. H.; ...

2017-07-27

Sulfur-based thiyl radicals are known to be involved in a wide range of chemical and biological processes, but they are often highly reactive, which makes them difficult to observe directly. We report herein X-ray absorption spectra and analysis that support the direct observation of two different thiyl species generated photochemically by X-ray irradiation. The thiyl radical sulfur K-edge X-ray absorption spectra of both species are characterized by a uniquely low energy transition at about 2465 eV, which occurs at a lower energy than any previously observed feature at the sulfur K-edge and corresponds to a 1s → 3p transition tomore » the singly occupied molecular orbital of the free radical. In conclusion, our results constitute the first observation of substantial levels of thiyl radicals generated by X-ray irradiation and detected by sulfur K-edge X-ray absorption spectroscopy.« less

Normal incidence X-ray telescope power spectra of X-ray emission from solar active regions. I - Observations. II - Theory

NASA Technical Reports Server (NTRS)

Gomez, Daniel O.; Martens, Petrus C. H.; Golub, Leon

1993-01-01

Fourier analysis is applied to very high resolution image of coronal active regions obtained by the Normal Incidence X-Ray Telescope is used to find a broad isotropic power-law spectrum of the spatial distribution of soft X-ray intensities. Magnetic structures of all sizes are present down to the resolution limit of the instrument. Power spectra for the X-ray intensities of a sample of topologically different active regions are found which fall off with increasing wavenumber as 1/k-cubed. A model is presented that relates the basic features of coronal magnetic fluctuations to the subphotospheric hydrodynamic turbulence that generates them. The model is used to find a theoretical power spectrum for the X-ray intensity which falls off with increasing wavenumber as 1/k-cubed. The implications of a turbulent regime in active regions are discussed.

Deviation Value for Conventional X-ray in Hospitals in South Sulawesi Province from 2014 to 2016

NASA Astrophysics Data System (ADS)

Bachtiar, Ilham; Abdullah, Bualkar; Tahir, Dahlan

2018-03-01

This paper describes the conventional X-ray machine parameters tested in the region of South Sulawesi from 2014 to 2016. The objective of this research is to know deviation of every parameter of conventional X-ray machine. The testing parameters were analyzed by using quantitative methods with participatory observational approach. Data collection was performed by testing the output of conventional X-ray plane using non-invasive x-ray multimeter. The test parameters include tube voltage (kV) accuracy, radiation output linearity, reproducibility and radiation beam value (HVL) quality. The results of the analysis show four conventional X-ray test parameters have varying deviation spans, where the tube voltage (kV) accuracy has an average value of 4.12%, the average radiation output linearity is 4.47% of the average reproducibility of 0.62% and the averaged of the radiation beam (HVL) is 3.00 mm.

Low Energy Accelerators for Cargo Inspection

NASA Astrophysics Data System (ADS)

Tang, Chuanxiang

Cargo inspection by X-rays has become essential for seaports and airports. With the emphasis on homeland security issues, the identification of dangerous things, such as explosive items and nuclear materials, is the key feature of a cargo inspection system. And new technologies based on dual energy X-rays, neutrons and monoenergetic X-rays have been studied to achieve sufficiently good material identification. An interpretation of the principle of X-ray cargo inspection technology and the features of X-ray sources are presented in this article. As most of the X-ray sources are based on RF electron linear accelerators (linacs), we give a relatively detailed description of the principle and characteristics of linacs. Cargo inspection technologies based on neutron imaging, neutron analysis, nuclear resonance fluorescence and computer tomography are also mentioned here. The main vendors and their products are summarized at the end of the article.

The intermediate polar GK Persei: An unstable relation of the X-ray and the optical intensities in a series of outbursts

NASA Astrophysics Data System (ADS)

Šimon, V.

2015-03-01

Context. GK Per is an intermediate polar that has been displaying dwarf nova outbursts since the middle of the twentieth century. Aims: I analyzed a series of such outbursts in the optical and X-ray bands. I pay attention to the relation of intensities of the optical and X-ray emissions, and its reproducibility in a series of these consecutive outbursts. Methods: This analysis uses the data from the BAT/Swift, ASM/RXTE, AAVSO, and AFOEV databases. It investigates the relation of the time evolution of the profiles of outbursts in the individual bands (hard X-ray, medium/hard X-ray, and optical). Results: This analysis shows that the X-ray intensity steeply rises only in the start of the optical outburst and steeply declines only when the optical outburst comes to its end. However, the 1.5-50 keV band intensity saturates and balances on a plateau during the outburst. (The longer the outburst, the longer its plateau.) The peak X-ray intensities of this series display a significantly narrower range than the optical ones (a factor of about two versus a factor of about eight). This implies a discrepancy between the mass flow through the disk and the production of the X-ray emission via bremsstrahlung at the polar caps of the white dwarf. This discrepancy is the largest in the time of the peak optical intensity when the whole disk (or at least its inner part) is in the hot state and the flow of matter through the disk is the greatest. This study shows that a series of outbursts constitutes more general properties of this discrepancy. I argue that the saturation of the X-ray luminosity in outburst cannot be caused by a dominant increase in X-ray absorption. In the interpretation, large structural changes of the accreting regions at the magnetic poles of the white dwarf occur during the outburst. A buried shock proposed by some authors for polars is also promising for explaining the X-ray light curves of outbursts of GK Per. This research made use of the BAT/Swift, ASM/RXTE, AAVSO, and AFOEV databases.

Publications - GMC 40 | Alaska Division of Geological & Geophysical Surveys

Science.gov Websites

DGGS GMC 40 Publication Details Title: X-ray diffraction analysis of the Pan Am Hoodoo Lake #2; Pan Am , X-ray diffraction analysis of the Pan Am Hoodoo Lake #2; Pan Am David River #1-A; and the AMOCO

X-Tip: a New Tool for Nanoscience or How to Combine X-Ray Spectroscopies to Local Probe Analysis

NASA Astrophysics Data System (ADS)

Olivier, Dhez; Mario, Rodrigues; Fabio, Comin; Roberto, Felici; Joel, Chevrier

2007-01-01

With the advent of nanoscale science, the need of tools able to image samples and bring the region of interest to the X-ray beam is essential. We show the possibility of using the high resolution imaging capability of a scanning probe microscope to image and align a sample relative to the X-ray beam, as well as the possibility to record the photoelectrons emitted by the sample.

Implications of cost-effectiveness analysis of medical technology. background paper number 5. four common x-ray procedures: problems and prospects for economic evaluation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wagner, J.L.; Krieger, M.J.

This paper is about the economic evaluation of diagnostic procedures. The issue of economic evaluation is explored in the context of four common diagnostic X-ray procedures: the chest X-ray, the skull X-ray, the barium enema study, and the excretory urogram. The paper is divided into two parts. The first part summarizes the different evaluative models underlying studies of the four diagnostic X-ray procedures and to lay out the strengths and weaknesses of each method. The second part contains four separate chapters summarizing what is known about the utilization, costs, risks, and benefits of each procedure, with particular emphasis on themore » evaluative methods employed.« less

Finite element Compton tomography

NASA Astrophysics Data System (ADS)

Jannson, Tomasz; Amouzou, Pauline; Menon, Naresh; Gertsenshteyn, Michael

2007-09-01

In this paper a new approach to 3D Compton imaging is presented, based on a kind of finite element (FE) analysis. A window for X-ray incoherent scattering (or Compton scattering) attenuation coefficients is identified for breast cancer diagnosis, for hard X-ray photon energy of 100-300 keV. The point-by-point power/energy budget is computed, based on a 2D array of X-ray pencil beams, scanned vertically. The acceptable medical doses are also computed. The proposed finite element tomography (FET) can be an alternative to X-ray mammography, tomography, and tomosynthesis. In experiments, 100 keV (on average) X-ray photons are applied, and a new type of pencil beam collimation, based on a Lobster-Eye Lens (LEL), is proposed.

A statistical analysis of the Einstein normal galaxy sample. III - Radio and X-ray properties of elliptical and S0 galaxies

NASA Technical Reports Server (NTRS)

Fabbiano, G.; Klein, U.; Trinchieri, G.; Wielebinski, R.

1987-01-01

Radioastronomy, optical and X-ray data were used to probe the cause of high X-ray luminosities of 28 radio-quiet elliptical galaxies (RQE) and S0 galaxies previously scanned by the Einstein Observatory. Comparisons were made with similar data on double-lobed 3CR galaxies. Radio luminosities were highly correlated with the X-ray luminosities, agreeing with models of radio nuclear sources in early-type galaxies as accreting compact objects. Additionally, 3CR galaxies seemed to be large-scale versions of normal RQE. The significance of interstellar medium/intracluster medium interactions for high correlations between the core and total radio power from X-ray emitting galaxies is discussed.

Synchrotron X-ray microscopy and spectroscopy analysis of iron in hemochromatosis liver and intestines

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ko, J .Y. Peter; Sham, Tsun-Kong; Chakrabarti, Subrata

2009-12-01

Hemochromatosis is a genetic disorder that causes body to store excess iron in organs such as heart or liver. Distribution of iron, as well as copper, zinc and calcium, and chemical identity of iron in hemochromatosis liver and intestine were investigated by X-ray microprobe experiments, which consist of X-ray microscopy and micro-X-ray absorption fine structure. Our results show that iron concentration in hemochromatosis liver tissue is high, while much less Fe is found in intestinal tissue. Moreover, chemical identity of Fe in hemochromatosis liver can be identified. X-ray microprobe experiments allows for examining elemental distribution at an excellent spatial resolution.more » Moreover, chemical identity of element of interest can be obtained.« less

Analysis of ultraviolet and X-ray observations of three homologous solar flares from SMM

NASA Technical Reports Server (NTRS)

Cheng, Chung-Chieh; Pallavicini, Roberto

1987-01-01

Three homologous flares observed in the UV lines of Fe XXI and O V and in X-rays from the SMM were studied. It was found that: (1) the homology of the flares was most noticeable in Fe XXI and soft X-ray emissions; (2) the three flares shared many of the same loop footprints which were located in O V bright kernals associated with hard X-ray bursts; and (3) in spite of the strong spatial homology, the temporal evolution in UV and X-ray emissions varied from flare to flare. A comparison between the UV observations and photospheric magnetograms revealed that the basic flare configuration was a complex loop system consisting of many loops or bundles of loops.

X-ray astronomical spectroscopy

NASA Technical Reports Server (NTRS)

Holt, S. S.

1980-01-01

The current status of the X-ray spectroscopy of celestial X-ray sources, ranging from nearby stars to distant quasars, is reviewed. Particular emphasis is placed on the role of such spectroscopy as a useful and unique tool in the elucidation of the physical parameters of the sources. The spectroscopic analysis of degenerate and nondegenerate stellar systems, galactic clusters and active galactic nuclei, and supernova remnants is discussed.

Time development of a small solar X-ray burst

NASA Technical Reports Server (NTRS)

Cohen, G. G.; Kestenbaum, H. L.; Long, K. S.; Novick, R.; Weisskopf, M. C.; Wolff, R. S.

1976-01-01

The 5.1-7.2 A X-ray emission from the sun was studied via OSO-8 with a high-resolution PET crystal spectrometer during the week of 17 November 1975, when the sun was active. The combination of good temporal and spectral resolution permitted the analysis of the data with multithermal coronal models over the course of a small X-ray burst.

Overview of machine vision methods in x-ray imaging and microtomography

NASA Astrophysics Data System (ADS)

Buzmakov, Alexey; Zolotov, Denis; Chukalina, Marina; Nikolaev, Dmitry; Gladkov, Andrey; Ingacheva, Anastasia; Yakimchuk, Ivan; Asadchikov, Victor

2018-04-01

Digital X-ray imaging became widely used in science, medicine, non-destructive testing. This allows using modern digital images analysis for automatic information extraction and interpretation. We give short review of scientific applications of machine vision in scientific X-ray imaging and microtomography, including image processing, feature detection and extraction, images compression to increase camera throughput, microtomography reconstruction, visualization and setup adjustment.

Bayesian Multiscale Analysis of X-Ray Jet Features in High Redshift Quasars

NASA Astrophysics Data System (ADS)

McKeough, Kathryn; Siemiginowska, A.; Kashyap, V.; Stein, N.

2014-01-01

X-ray emission of powerful quasar jets may be a result of the inverse Compton (IC) process in which the Cosmic Microwave Background (CMB) photons gain energy by interactions with the jet’s relativistic electrons. However, there is no definite evidence that IC/CMB process is responsible for the observed X-ray emission of large scale jets. A step toward understanding the X-ray emission process is to study the Radio and X-ray morphologies of the jet. We implement a sophisticated Bayesian image analysis program, Low-count Image Reconstruction and Analysis (LIRA) (Esch et al. 2004; Conners & van Dyk 2007), to analyze jet features in 11 Chandra images of high redshift quasars (z ~ 2 - 4.8). Out of the 36 regions where knots are visible in the radio jets, nine showed detectable X-ray emission. We measured the ratios of the X-ray and radio luminosities of the detected features and found that they are consistent with the CMB radiation relationship. We derived a range of the bulk lorentz factor (Γ) for detected jet features under the CMB jet emission model. There is no discernible trend of Γ with redshift within the sample. The efficiency of the X-ray emission between the detected jet feature and the corresponding quasar also shows no correlation with redshift. This work is supported in part by the National Science Foundation REU and the Department of Defense ASSURE programs under NSF Grant no.1262851 and by the Smithsonian Institution, and by NASA Contract NAS8-39073 to the Chandra X-ray Center (CXC). This research has made use of data obtained from the Chandra Data Archive and Chandra Source Catalog, and software provided by the CXC in the application packages CIAO, ChIPS, and Sherpa. We thank Teddy Cheung for providing the VLA radio images. Connors, A., & van Dyk, D. A. 2007, Statistical Challenges in Modern Astronomy IV, 371, 101 Esch, D. N., Connors, A., Karovska, M., & van Dyk, D. A. 2004, ApJ, 610, 1213

Determination of carrier yields for neutron activation analysis using energy dispersive X-ray spectrometry

USGS Publications Warehouse

Johnson, R.G.; Wandless, G.A.

1984-01-01

A new method is described for determining carrier yield in the radiochemical neutron activation analysis of rare-earth elements in silicate rocks by group separation. The method involves the determination of the rare-earth elements present in the carrier by means of energy-dispersive X-ray fluorescence analysis, eliminating the need to re-irradiate samples in a nuclear reactor after the gamma ray analysis is complete. Results from the analysis of USGS standards AGV-1 and BCR-1 compare favorably with those obtained using the conventional method. ?? 1984 Akade??miai Kiado??.

Optimization of propagation-based x-ray phase-contrast tomography for breast cancer imaging

NASA Astrophysics Data System (ADS)

Baran, P.; Pacile, S.; Nesterets, Y. I.; Mayo, S. C.; Dullin, C.; Dreossi, D.; Arfelli, F.; Thompson, D.; Lockie, D.; McCormack, M.; Taba, S. T.; Brun, F.; Pinamonti, M.; Nickson, C.; Hall, C.; Dimmock, M.; Zanconati, F.; Cholewa, M.; Quiney, H.; Brennan, P. C.; Tromba, G.; Gureyev, T. E.

2017-03-01

The aim of this study was to optimise the experimental protocol and data analysis for in-vivo breast cancer x-ray imaging. Results are presented of the experiment at the SYRMEP beamline of Elettra Synchrotron using the propagation-based phase-contrast mammographic tomography method, which incorporates not only absorption, but also x-ray phase information. In this study the images of breast tissue samples, of a size corresponding to a full human breast, with radiologically acceptable x-ray doses were obtained, and the degree of improvement of the image quality (from the diagnostic point of view) achievable using propagation-based phase-contrast image acquisition protocols with proper incorporation of x-ray phase retrieval into the reconstruction pipeline was investigated. Parameters such as the x-ray energy, sample-to-detector distance and data processing methods were tested, evaluated and optimized with respect to the estimated diagnostic value using a mastectomy sample with a malignant lesion. The results of quantitative evaluation of images were obtained by means of radiological assessment carried out by 13 experienced specialists. A comparative analysis was performed between the x-ray and the histological images of the specimen. The results of the analysis indicate that, within the investigated range of parameters, both the objective image quality characteristics and the subjective radiological scores of propagation-based phase-contrast images of breast tissues monotonically increase with the strength of phase contrast which in turn is directly proportional to the product of the radiation wavelength and the sample-to-detector distance. The outcomes of this study serve to define the practical imaging conditions and the CT reconstruction procedures appropriate for low-dose phase-contrast mammographic imaging of live patients at specially designed synchrotron beamlines.

Comparison of adverse effects of proton and X-ray chemoradiotherapy for esophageal cancer using an adaptive dose–volume histogram analysis

PubMed Central

Makishima, Hirokazu; Ishikawa, Hitoshi; Terunuma, Toshiyuki; Hashimoto, Takayuki; Yamanashi, Koichi; Sekiguchi, Takao; Mizumoto, Masashi; Okumura, Toshiyuki; Sakae, Takeji; Sakurai, Hideyuki

2015-01-01

Cardiopulmonary late toxicity is of concern in concurrent chemoradiotherapy (CCRT) for esophageal cancer. The aim of this study was to examine the benefit of proton beam therapy (PBT) using clinical data and adaptive dose–volume histogram (DVH) analysis. The subjects were 44 patients with esophageal cancer who underwent definitive CCRT using X-rays (n = 19) or protons (n = 25). Experimental recalculation using protons was performed for the patient actually treated with X-rays, and vice versa. Target coverage and dose constraints of normal tissues were conserved. Lung V5–V20, mean lung dose (MLD), and heart V30–V50 were compared for risk organ doses between experimental plans and actual treatment plans. Potential toxicity was estimated using protons in patients actually treated with X-rays, and vice versa. Pulmonary events of Grade ≥2 occurred in 8/44 cases (18%), and cardiac events were seen in 11 cases (25%). Risk organ doses in patients with events of Grade ≥2 were significantly higher than for those with events of Grade ≤1. Risk organ doses were lower in proton plans compared with X-ray plans. All patients suffering toxicity who were treated with X-rays (n = 13) had reduced predicted doses in lung and heart using protons, while doses in all patients treated with protons (n = 24) with toxicity of Grade ≤1 had worsened predicted toxicity with X-rays. Analysis of normal tissue complication probability showed a potential reduction in toxicity by using proton beams. Irradiation dose, volume and adverse effects on the heart and lung can be reduced using protons. Thus, PBT is a promising treatment modality for the management of esophageal cancer. PMID:25755255

Joint Analysis of X-Ray and Sunyaev-Zel'Dovich Observations of Galaxy Clusters Using an Analytic Model of the Intracluster Medium

NASA Technical Reports Server (NTRS)

Hasler, Nicole; Bulbul, Esra; Bonamente, Massimiliano; Carlstrom, John E.; Culverhouse, Thomas L.; Gralla, Megan; Greer, Christopher; Lamb, James W.; Hawkins, David; Hennessy, Ryan;

Experimental results of use of triple-energy X-ray beam with K-edge filter in multi-energy imaging

NASA Astrophysics Data System (ADS)

Kim, D.; Lee, S.; Jeon, P.-H.

2016-04-01

Multi-energy imaging is useful for contrast enhancement of lesions, quantitative analysis of specific materials and material separation in the human body. Generally, dual-energy methods are applied to discriminating two materials, but this method cannot discriminate more than two materials. Photon-counting detectors provide spectral information from polyenergetic X-rays using multiple energy bins. In this work, we developed triple-energy X-ray beams using a filter with K-edge energy and applied them experimentally. The energy spectra of triple-energy X-ray beams were assessed by using a spectrometer. The designed triple-energy X-ray beams were validated by measuring quantitative evaluations with mean energy ratio (MER), contrast variation ratio (CVR) and exposure efficiency (EE). Then, triple-energy X-ray beams were used to extract density map of three materials, iodine (I), aluminum (Al) and polymethyl methacrylate (PMMA). The results of the thickness density maps obtained with the developed triple-energy X-ray beams were compared to those acquired using the photon-counting method. As a result, it was found experimentally that the proposed triple-energy X-ray beam technique can separate the three materials as well as the photon-counting method.

Impact of intense x-ray pulses on a NaI(Tl)-based gamma camera

NASA Astrophysics Data System (ADS)

Koppert, W. J. C.; van der Velden, S.; Steenbergen, J. H. L.; de Jong, H. W. A. M.

2018-03-01

In SPECT/CT systems x-ray and γ-ray imaging is performed sequentially. Simultaneous acquisition may have advantages, for instance in interventional settings. However, this may expose a gamma camera to relatively high x-ray doses and deteriorate its functioning. We studied the NaI(Tl) response to x-ray pulses with a photodiode, PMT and gamma camera, respectively. First, we exposed a NaI(Tl)-photodiode assembly to x-ray pulses to investigate potential crystal afterglow. Next, we exposed a NaI(Tl)-PMT assembly to 10 ms LED pulses (mimicking x-ray pulses) and measured the response to flashing LED probe-pulses (mimicking γ-pulses). We then exposed the assembly to x-ray pulses, with detector entrance doses of up to 9 nGy/pulse, and analysed the response for γ-pulse variations. Finally, we studied the response of a Siemens Diacam gamma camera to γ-rays while exposed to x-ray pulses. X-ray exposure of the crystal, read out with a photodiode, revealed 15% afterglow fraction after 3 ms. The NaI(Tl)-PMT assembly showed disturbances up to 10 ms after 10 ms LED exposure. After x-ray exposure however, responses showed elevated baselines, with 60 ms decay-time. Both for x-ray and LED exposure and after baseline subtraction, probe-pulse analysis revealed disturbed pulse height measurements shortly after exposure. X-ray exposure of the Diacam corroborated the elementary experiments. Up to 50 ms after an x-ray pulse, no events are registered, followed by apparent energy elevations up to 100 ms after exposure. Limiting the dose to 0.02 nGy/pulse prevents detrimental effects. Conventional gamma cameras exhibit substantial dead-time and mis-registration of photon energies up to 100 ms after intense x-ray pulses. This is due PMT limitations and due to afterglow in the crystal. Using PMTs with modified circuitry, we show that deteriorative afterglow effects can be reduced without noticeable effects on the PMT performance, up to x-ray pulse doses of 1 nGy.

Software to model AXAF-I image quality

NASA Technical Reports Server (NTRS)

Ahmad, Anees; Feng, Chen

1995-01-01

A modular user-friendly computer program for the modeling of grazing-incidence type x-ray optical systems has been developed. This comprehensive computer software GRAZTRACE covers the manipulation of input data, ray tracing with reflectivity and surface deformation effects, convolution with x-ray source shape, and x-ray scattering. The program also includes the capabilities for image analysis, detector scan modeling, and graphical presentation of the results. A number of utilities have been developed to interface the predicted Advanced X-ray Astrophysics Facility-Imaging (AXAF-I) mirror structural and thermal distortions with the ray-trace. This software is written in FORTRAN 77 and runs on a SUN/SPARC station. An interactive command mode version and a batch mode version of the software have been developed.

Multilayer X-ray imaging systems

NASA Astrophysics Data System (ADS)

Shealy, D. L.; Hoover, R. B.; Gabardi, D. R.

1986-01-01

An assessment of the imaging properties of multilayer X-ray imaging systems with spherical surfaces has been made. A ray trace analysis was performed to investigate the effects of using spherical substrates (rather than the conventional paraboloidal/hyperboloidal contours) for doubly reflecting Cassegrain telescopes. These investigations were carried out for mirrors designed to operate at selected soft X-ray/XUV wavelengths that are of significance for studies of the solar corona/transition region from the Stanford/MSFC Rocket X-Ray Telescope. The effects of changes in separation of the primary and secondary elements were also investigated. These theoretical results are presented as well as the results of ray trace studies to establish the resolution and vignetting effects as a function of field angle and system parameters.

Evolution of the X-ray luminosity in young HII galaxies

NASA Astrophysics Data System (ADS)

Rosa González, D.; Terlevich, E.; Jiménez Bailón, E.; Terlevich, R.; Ranalli, P.; Comastri, A.; Laird, E.; Nandra, K.

2009-10-01

In an effort to understand the correlation between X-ray emission and present star formation rate, we obtained XMM-Newton data to estimate the X-ray luminosities of a sample of actively star-forming HII galaxies. The obtained X-ray luminosities are compared to other well-known tracers of star formation activity such as the far-infrared and the ultraviolet luminosities. We also compare the obtained results with empirical laws from the literature and with recently published analysis applying synthesis models. We use the time delay between the formation of the stellar cluster and that of the first X-ray binaries, in order to put limits on the age of a given stellar burst. We conclude that the generation of soft X-rays, as well as the Hα or infrared luminosities is instantaneous. The relation between the observed radio and hard X-ray luminosities, on the other hand, points to the existence of a time delay between the formation of the stellar cluster and the explosion of the first massive stars and the consequent formation of supernova (SN) remnants and high-mass X-ray binaries, which originate the radio and hard X-ray fluxes, respectively. When comparing hard X-rays with a star formation indicator that traces the first million years of evolution (e.g. Hα luminosities), we found a deficit in the expected X-ray luminosity. This deficit is not found when the X-ray luminosities are compared with infrared luminosities, a star formation tracer that represents an average over the last 108yr. The results support the hypothesis that hard X-rays are originated in X-ray binaries which, as SN remnants, have a formation time delay of a few mega years after the star-forming burst. Partially based on observations obtained with XMM-Newton, an ESA science mission with instruments and contributions directly funded by ESA Member States and NASA. E-mail: danrosa@inaoep.mx ‡ Visiting Fellow, IoA, Cambridge, UK.

SU-F-T-128: Dose-Volume Constraints for Particle Therapy Treatment Planning

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stewart, R; Smith, W; Hendrickson, K

2016-06-15

Purpose: Determine equivalent Organ at Risk (OAR) tolerance dose (TD) constraints for MV x-rays and particle therapy. Methods: Equivalent TD estimates for MV x-rays are determined from an isoeffect, regression-analysis of published and in-house constraints for various fractionation schedules (n fractions). The analysis yields an estimate of (α/β) for an OAR. To determine equivalent particle therapy constraints, the MV x-ray TD(n) values are divided by the RBE for DSB induction (RBE{sub DSB}) or cell survival (RBE{sub S}). Estimates of (RBE{sub DSB}) are computed using the Monte Carlo Damage Simulation, and estimates of RBES are computed using the Repair-Misrepair-Fixation (RMF) model.more » A research build of the RayStation™ treatment planning system implementing the above model is used to estimate (RBE{sub DSB}) for OARs of interest in 16 proton therapy patient plans (head and neck, thorax, prostate and brain). Results: The analysis gives an (α/β) estimate of about 20 Gy for the trachea and heart and 2–4 Gy for the esophagus, spine, and brachial plexus. Extrapolation of MV x-ray constraints (n = 1) to fast neutrons using RBE{sub DSB} = 2.7 are in excellent agreement with clinical experience (n = 10 to 20). When conventional (n > 30) x-ray treatments are used as the reference radiation, fast neutron RBE increased to a maximum of 6. For comparison to a constant RBE of 1.1, the RayStation™ analysis gave estimates of proton RBE{sub DSB} from 1.03 to 1.33 for OARs of interest. Conclusion: The presented system of models is a convenient formalism to synthesize from multiple sources of information a set of self-consistent plan constraints for MV x-ray and hadron therapy treatments. Estimates of RBE{sub DSB} from the RayStation™ analysis differ substantially from 1.1 and vary among patients and treatment sites. A treatment planning system that incorporates patient and anatomy-specific corrections in proton RBE would create opportunities to increase the therapeutic ratio. The research build of the RayStation used in the study was made available to the University of Washington free of charge. RaySearch Laboratories did not provide any monetary support for the reported studies.« less

Early Detection of Amyloid Plaque in Alzheimer’s Disease via X-Ray Phase CT

DTIC Science & Technology

2014-06-01

normal, pathologic and Alzheimer’s brains, in which the amyloid precursor protein (APP) will be included as a reference. Toward this goal, we have made...in x-ray flat panel imagers and the artifact removal using a wavelet -analysis-based algorithm” Med. Phys., 28(3): 812-25, 2001. 4. X Wu and H Liu...panel imagers and the artifact removal using a wavelet -analysis-based algorithm” Med. Phys., 28(3): 812-25, 2001 12. Tang X, Hsieh J, Nilsen RA

Early Detection of Amyloid Plaque in Alzheimer’s Disease via X-Ray Phase CT

DTIC Science & Technology

2013-06-01

fibrils in the x-ray phase contrast CT imaging, as a function over the molar concentrations corresponding to normal, pathologic and Alzheimer’s...panel imagers and the artifact removal using a wavelet -analysis-based algorithm” Med. Phys., 28(3): 812-25, 2001. 4. X Wu and H Liu, “Clinical...and the artifact removal using a wavelet -analysis-based algorithm” Med. Phys., 28(3): 812-25, 2001 12. Tang X, Hsieh J, Nilsen RA, Hagiwara A

PROS: An IRAF based system for analysis of x ray data

NASA Technical Reports Server (NTRS)

Conroy, M. A.; Deponte, J.; Moran, J. F.; Orszak, J. S.; Roberts, W. P.; Schmidt, D.

1992-01-01

PROS is an IRAF based software package for the reduction and analysis of x-ray data. The use of a standard, portable, integrated environment provides for both multi-frequency and multi-mission analysis. The analysis of x-ray data differs from optical analysis due to the nature of the x-ray data and its acquisition during constantly varying conditions. The scarcity of data, the low signal-to-noise ratio and the large gaps in exposure time make data screening and masking an important part of the analysis. PROS was developed to support the analysis of data from the ROSAT and Einstein missions but many of the tasks have been used on data from other missions. IRAF/PROS provides a complete end-to-end system for x-ray data analysis: (1) a set of tools for importing and exporting data via FITS format -- in particular, IRAF provides a specialized event-list format, QPOE, that is compatible with its IMAGE (2-D array) format; (2) a powerful set of IRAF system capabilities for both temporal and spatial event filtering; (3) full set of imaging and graphics tasks; (4) specialized packages for scientific analysis such as spatial, spectral and timing analysis -- these consist of both general and mission specific tasks; and (5) complete system support including ftp and magnetic tape releases, electronic and conventional mail hotline support, electronic mail distribution of solutions to frequently asked questions and current known bugs. We will discuss the philosophy, architecture and development environment used by PROS to generate a portable, multimission software environment. PROS is available on all platforms that support IRAF, including Sun/Unix, VAX/VMS, HP, and Decstations. It is available on request at no charge.

Data processing and analysis for 2D imaging GEM detector system

NASA Astrophysics Data System (ADS)

Czarski, T.; Chernyshova, M.; Pozniak, K. T.; Kasprowicz, G.; Byszuk, A.; Juszczyk, B.; Kolasinski, P.; Linczuk, M.; Wojenski, A.; Zabolotny, W.; Zienkiewicz, P.

2014-11-01

The Triple Gas Electron Multiplier (T-GEM) is presented as soft X-ray (SXR) energy and position sensitive detector for high-resolution X-ray diagnostics of magnetic confinement fusion plasmas [1]. Multi-channel measurement system and essential data processing for X-ray energy and position recognition is consider. Several modes of data acquisition are introduced depending on processing division for hardware and software components. Typical measuring issues aredeliberated for enhancement of data quality. Fundamental output characteristics are presented for one and two dimensional detector structure. Representative results for reference X-ray source and tokamak plasma are demonstrated.

Start of Eta Car's X-ray Minimum

NASA Technical Reports Server (NTRS)

Corcoran, Michael F.; Liburd, Jamar; Hamaguchi, Kenji; Gull, Theodore; Madura, Thomas; Teodoro, Mairan; Moffat, Anthony; Richardson, Noel; Russell, Chris; Pollock, Andrew;

Observation of the X-Ray Magneto-Optical Voigt Effect

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mertins, H.-Ch.; Oppeneer, P. M.; Kunes, J.

2001-07-23

The existence of the x-ray magneto-optical Voigt effect is demonstrated. By means of polarization analysis the Voigt rotation and ellipticity of linearly polarized synchrotron radiation are measured at the Co L{sub 3} edge upon transmission through an amorphous Co film. The observed x-ray Voigt rotation is about 7.5{sup o}/{mu}m . On the basis of ab initio calculations it is shown that the x-ray Voigt effect follows sensitively the amount of spin polarization of the 2p core states. Therefore it provides a unique measure of the spin splitting of the core states.

The HEAO-A Scanning Modulation Collimator instrument

NASA Technical Reports Server (NTRS)

Roy, A.; Ballas, J.; Jagoda, N.; Mckinnon, P.; Ramsey, A.; Wester, E.

1977-01-01

The Scanning Modulation Collimator X-ray instrument for the HEAO-A satellite was designed to measure celestial radiation in the range between 1 and 15 KeV and to resolve, and correlate, the position of X-ray sources with visible light sources on the celestial sphere to within 5 arc seconds. The positional accuracy is made possible by mechanical collimation of the X-ray sources viewed by the instrument. High sensitivity is provided from two systems each containing four gas filled proportional counters followed by preamplification, signal summing, pulse height analysis, pulse shape discrimination, X-ray event accumulators and telemetry processing electronics.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sokaras, D.; Andrianis, M.; Lagoyannis, A.

The cascade L-shell x-ray emission as an incident polarized and unpolarized monochromatic radiation overpass the 1s ionization threshold is investigated for the metallic Fe by means of moderate resolution, quantitative x-ray spectrometry. A full ab initio theoretical investigation of the L-shell x-ray emission processes is performed based on a detailed straightforward construction of the cascade decay trees within the Pauli-Fock approximation. The agreement obtained between experiments and the presented theory is indicated and discussed with respect to the accuracy of advanced atomic models as well as its significance for the characterization capabilities of x-ray fluorescence (XRF) analysis.

Modeling Contamination Migration on the Chandra X-Ray Observatory - III

NASA Technical Reports Server (NTRS)

O'Dell, Stephen L.; Swartz, Douglas A.; Tice, Neil W.; Plucinsky, Paul P.; Grant, Catherine E.; Marshall, Herman L.; Vikhlinin, Alexy A.; Tennant, Allyn F.; Dahmer, Matthew T.

2015-01-01

During its first 16 years of operation, the cold (about -60 C) optical blocking filter of the Advanced CCD Imaging Spectrometer (ACIS), aboard the Chandra X-ray Observatory, has accumulated a growing layer of molecular contamination that attenuates low-energy x rays. Over the past few years, the accumulation rate, spatial distribution, and composition have changed. This evolution has motivated further analysis of contamination migration within and near the ACIS cavity, in part to evaluate potential bake-out scenarios intended to reduce the level of contamination. Keywords: X-ray astronomy, CCDs, contamination, modeling and simulation, spacecraft operations

Day-Scale Variability of 3C 279 and Searches for Correlations in Gamma-Ray, X-Ray and Optical Bands

NASA Technical Reports Server (NTRS)

Hartman, R. C.; Villata, M.; Balonek, T. J.; Bertsch, D. L.; Bock, H.; Boettcher, M.; Carini, M. T.; Collmar, W.; DeFrancesco, G.; Ferrera, E. C.;

[Contrast of Z-Pinch X-Ray Yield Measure Technique].

PubMed

Li, Mo; Wang, Liang-ping; Sheng, Liang; Lu, Yi

2015-03-01

Resistive bolometer and scintillant detection system are two mainly Z-pinch X-ray yield measure techniques which are based on different diagnostic principles. Contrasting the results from two methods can help with increasing precision of X-ray yield measurement. Experiments with different load material and shape were carried out on the "QiangGuang-I" facility. For Al wire arrays, X-ray yields measured by the two techniques were largely consistent. However, for insulating coating W wire arrays, X-ray yields taken from bolometer changed with load parameters while data from scintillant detection system hardly changed. Simulation and analysis draw conclusions as follows: (1) Scintillant detection system is much more sensitive to X-ray photons with low energy and its spectral response is wider than the resistive bolometer. Thus, results from the former method are always larger than the latter. (2) The responses of the two systems are both flat to Al plasma radiation. Thus, their results are consistent for Al wire array loads. (3) Radiation form planar W wire arrays is mainly composed of sub-keV soft X-ray. X-ray yields measured by the bolometer is supposed to be accurate because of the nickel foil can absorb almost all the soft X-ray. (4) By contrast, using planar W wire arrays, data from scintillant detection system hardly change with load parameters. A possible explanation is that while the distance between wires increases, plasma temperature at stagnation reduces and spectra moves toward the soft X-ray region. Scintillator is much more sensitive to the soft X-ray below 200 eV. Thus, although the total X-ray yield reduces with large diameter load, signal from the scintillant detection system is almost the same. (5) Both Techniques affected by electron beams produced by the loads.

Chandra X-ray Observations of Jovian Low-latitude Emissions: Morphological, Temporal, and Spectral Characteristics

NASA Technical Reports Server (NTRS)

Bhardwaj, Anil; Elsner, Ronald F.; Gladstone, G. Randall; Cravens, Thomas E.; Waiate J. Hunter, Jr.; Branduardi-Raymont, Graziella; Ford, Peter

2004-01-01

Chandra observed X-rays from Jupiter during 24-26 February 2003 for about 40 hours with the ACIS-S and HRC-I instruments. The analysis of Jovian low-latitude "disk" Xray emissions are presented and compared with the high-latitude "auroral" emissions. We report the first Chandra ACIS-S measured X-ray spectrum (0.3-2 keV) of Jupiter's low-latitude disk The disk X-ray emission is harder and extends to higher energies than the auroral spectrum. The temporal variation in the Jovian disk X-rays is on an average consistent with those in the solar X-rays observed by GOES, and TIMED/SSE. Contrary to the auroral X-rays, the disk emissions are uniformly distributed over Jupiter; no indication of longitudinal dependence or correlation with surface magneh field strength is visible. Also, unlike the approx. 40 +/- 20 min periodic oscillations seen in the auroral X-ray emissions, the disk emissions do not show any periodic oscillations. The disk spectrum seems to be consistent with resonant and fluorescent scattering of solar X-rays by the Jovian upper atmosphere. Jupiter's disk is found to be about 50% dimmer in soft X-rays in February 2003 compared that in December 2000, which is consistent with the decrease in solar activity. No evidence of lightning-induced X-rays is seen in the Chandra X-ray data. The Jovian disk spectra observed with Chandra-ACIS is stronger than that observed with XMM-Newton two months later during April 28-29, 2003. The XMM-Newton Xray image of Jupiter shows evidence of limb darkening on the anti-sunward side as seen from Earth, as well as an asymmetry with respect to the subsolar point: suggesting a solar driven process.

DynamiX, numerical tool for design of next-generation x-ray telescopes.

PubMed

Chauvin, Maxime; Roques, Jean-Pierre

2010-07-20

We present a new code aimed at the simulation of grazing-incidence x-ray telescopes subject to deformations and demonstrate its ability with two test cases: the Simbol-X and the International X-ray Observatory (IXO) missions. The code, based on Monte Carlo ray tracing, computes the full photon trajectories up to the detector plane, accounting for the x-ray interactions and for the telescope motion and deformation. The simulation produces images and spectra for any telescope configuration using Wolter I mirrors and semiconductor detectors. This numerical tool allows us to study the telescope performance in terms of angular resolution, effective area, and detector efficiency, accounting for the telescope behavior. We have implemented an image reconstruction method based on the measurement of the detector drifts by an optical sensor metrology. Using an accurate metrology, this method allows us to recover the loss of angular resolution induced by the telescope instability. In the framework of the Simbol-X mission, this code was used to study the impacts of the parameters on the telescope performance. In this paper we present detailed performance analysis of Simbol-X, taking into account the satellite motions and the image reconstruction. To illustrate the versatility of the code, we present an additional performance analysis with a particular configuration of IXO.

Analysis of Truss Frames by Method of the Stiffness Matrix

DTIC Science & Technology

1990-12-01

of the web members of the truss. There also are variations in the truss frame given by the geometric shape of the frame, also referred to in some...at the elastic center, 0 (Figure .3.2), are: R AX = Wix - Hot RBX W2x -Ho, RAY =WIY + Vo, (1) RBy WLy - Vo, MAB =- Mo + CH. + aVo + CMA, MBA =M - CH...o Co Ce Substituting the results of Equation (7) into Equations (1), x c D x RAY = Wix + + -- (eA - GO - D (8)C x C x C cx x cx AY a D RAY

In situ X-ray measurements of MOVPE growth of InxGa1-xN single quantum wells

NASA Astrophysics Data System (ADS)

Ju, Guangxu; Fuchi, Shingo; Tabuchi, Masao; Takeda, Yoshikazu

2013-05-01

GaN/InxGa1-xN/GaN single quantum wells (SQWs) have been grown on c-plane GaN/sapphire substrates using MOVPE system. PL (photoluminescence) and AFM (atomic force microscope) measurements demonstrate good quality of after-growth thermal-annealed SQWs. In situ XRD (X-ray diffraction), XRR (X-ray reflectivity), and X-ray CTR (crystal truncation rod) scattering measurements were successfully conducted on the SQWs under the NH3+N2 ambient at 1103 K. The analysis results of the XRR and the X-ray CTR spectra at 1103 K and at 300 K on the same sample matched well. It demonstrated that In0.09Ga0.91N SQW structure with several ML (monolayer) InGaN thicknesses was successfully investigated using the XRR and CTR scattering measurements at 1103 K.

Grazing Incidence Optics for X-rays Interferometry

NASA Technical Reports Server (NTRS)

Shipley, Ann; Zissa, David; Cash, Webster; Joy, Marshall

1999-01-01

Grazing incidence mirror parameters and constraints for x-ray interferometry are described. We present interferometer system tolerances and ray trace results used to define mirror surface accuracy requirements. Mirror material, surface figure, roughness, and geometry are evaluated based on analysis results. We also discuss mirror mount design constraints, finite element analysis, environmental issues, and solutions. Challenges associated with quantifying high accuracy mirror surface quality are addressed and test results are compared with theoretical predictions.

Accretion Disks and Coronae in the X-Ray Flashlight

NASA Astrophysics Data System (ADS)

Degenaar, Nathalie; Ballantyne, David R.; Belloni, Tomaso; Chakraborty, Manoneeta; Chen, Yu-Peng; Ji, Long; Kretschmar, Peter; Kuulkers, Erik; Li, Jian; Maccarone, Thomas J.; Malzac, Julien; Zhang, Shu; Zhang, Shuang-Nan

2018-02-01

Plasma accreted onto the surface of a neutron star can ignite due to unstable thermonuclear burning and produce a bright flash of X-ray emission called a Type-I X-ray burst. Such events are very common; thousands have been observed to date from over a hundred accreting neutron stars. The intense, often Eddington-limited, radiation generated in these thermonuclear explosions can have a discernible effect on the surrounding accretion flow that consists of an accretion disk and a hot electron corona. Type-I X-ray bursts can therefore serve as direct, repeating probes of the internal dynamics of the accretion process. In this work we review and interpret the observational evidence for the impact that Type-I X-ray bursts have on accretion disks and coronae. We also provide an outlook of how to make further progress in this research field with prospective experiments and analysis techniques, and by exploiting the technical capabilities of the new and concept X-ray missions ASTROSAT, NICER, Insight-HXMT, eXTP, and STROBE-X.

Cancer diagnosis using a conventional x-ray fluorescence camera with a cadmium-telluride detector

NASA Astrophysics Data System (ADS)

Sato, Eiichi; Enomoto, Toshiyuki; Hagiwara, Osahiko; Abudurexiti, Abulajiang; Sato, Koetsu; Sato, Shigehiro; Ogawa, Akira; Onagawa, Jun

2011-10-01

X-ray fluorescence (XRF) analysis is useful for mapping various atoms in objects. Bremsstrahlung X-rays are selected using a 3.0 mm-thick aluminum filter, and these rays are absorbed by indium, cerium and gadolinium atoms in objects. Then XRF is produced from the objects, and photons are detected by a cadmium-telluride detector. The Kα photons are discriminated using a multichannel analyzer, and the number of photons is counted by a counter card. The objects are moved and scanned by an x-y stage in conjunction with a two-stage controller, and X-ray images obtained by atomic mapping are shown on a personal computer monitor. The scan steps of the x and y axes were both 2.5 mm, and the photon-counting time per mapping point was 0.5 s. We carried out atomic mapping using the X-ray camera, and Kα photons from cerium and gadolinium atoms were produced from cancerous regions in nude mice.

Conventional X-ray fluorescence camera with a cadmium-telluride detector and its application to cancer diagnosis

NASA Astrophysics Data System (ADS)

Enomoto, Toshiyuki; Sato, Eiichi; Abderyim, Purkhet; Abudurexiti, Abulajiang; Hagiwara, Osahiko; Matsukiyo, Hiroshi; Osawa, Akihiro; Watanabe, Manabu; Nagao, Jiro; Sato, Shigehiro; Ogawa, Akira; Onagawa, Jun

2011-04-01

X-ray fluorescence (XRF) analysis is useful for mapping various molecules in objects. Bremsstrahlung X-rays are selected using a 3.0-mm-thick aluminum filter, and these rays are absorbed by iodine, cerium, and gadolinium molecules in objects. Next, XRF is produced from the objects, and photons are detected by a cadmium-telluride detector. The Kα photons are discriminated using a multichannel analyzer, and the number of photons is counted by a counter card. The objects are moved and scanned by an x- y stage in conjunction with a two-stage controller, and X-ray images obtained by molecular mapping are shown on a personal computer monitor. The scan steps of x and y axes were both 2.5 mm, and the photon-counting time per mapping point was 0.5 s. We carried out molecular mapping using the X-ray camera, and Kα photons from cerium and gadolinium molecules were produced from cancerous regions in nude mice.

MgO-Al2O3-ZrO2 Amorphous Ternary Composite: A Dense and Stable Optical Coating

NASA Technical Reports Server (NTRS)

Shaoo, Naba K.; Shapiro, Alan P.

1998-01-01

The process-parameter-dependent optical and structural properties of MgO-Al2O3-ZrO2 ternary mixed-composite material were investigated. Optical properties were derived from spectrophotometric measurements. The surface morphology, grain size distributions, crystallographic phases, and process- dependent material composition of films were investigated through the use of atomic force microscopy, x-ray diffraction analysis, and energy-dispersive x-ray analysis. Energy-dispersive x-ray analysis made evident the correlation between the optical constants and the process-dependent compositions in the films. It is possible to achieve environmentally stable amorphous films with high packing density under certain optimized process conditions.

A convenient method for X-ray analysis in TEM that measures mass thickness and composition

NASA Astrophysics Data System (ADS)

Statham, P.; Sagar, J.; Holland, J.; Pinard, P.; Lozano-Perez, S.

2018-01-01

We consider a new approach for quantitative analysis in transmission electron microscopy (TEM) that offers the same convenience as single-standard quantitative analysis in scanning electron microscopy (SEM). Instead of a bulk standard, a thin film with known mass thickness is used as a reference. The procedure involves recording an X-ray spectrum from the reference film for each session of acquisitions on real specimens. There is no need to measure the beam current; the current only needs to be stable for the duration of the session. A new reference standard with a large (1 mm x 1 mm) area of uniform thickness of 100 nm silicon nitride is used to reveal regions of X-ray detector occlusion that would give misleading results for any X-ray method that measures thickness. Unlike previous methods, the new X-ray method does not require an accurate beam current monitor but delivers equivalent accuracy in mass thickness measurement. Quantitative compositional results are also automatically corrected for specimen self-absorption. The new method is tested using a wedge specimen of Inconel 600 that is used to calibrate the high angle angular dark field (HAADF) signal to provide a thickness reference and results are compared with electron energy-loss spectrometry (EELS) measurements. For the new X-ray method, element composition results are consistent with the expected composition for the alloy and the mass thickness measurement is shown to provide an accurate alternative to EELS for thickness determination in TEM without the uncertainty associated with mean free path estimates.

Automated X-ray and Optical Analysis of the Virtual Observatory and Grid Computing

NASA Technical Reports Server (NTRS)

Ptak, A.; Krughoff, S.; Connolly, A.

2011-01-01

We are developing a system to combine the Web Enabled Source Identification with X-Matching (WESIX) web service, which emphasizes source detection on optical images,with the XAssist program that automates the analysis of X-ray data. XAssist is continuously processing archival X-ray data in several pipelines. We have established a workflow in which FITS images and/or (in the case of X ray data) an X-ray field can be input to WESIX. Intelligent services return available data (if requested fields have been processed) or submit job requests to a queue to be performed asynchronously. These services will be available via web services (for non-interactive use by Virtual Observatory portals and applications) and through web applications (written in the Django web application framework). We are adding web services for specific XAssist functionality such as determining .the exposure and limiting flux for a given position on the sky and extracting spectra and images for a given region. We are improving the queuing system in XAssist to allow for "watch lists" to be specified by users, and when X-ray fields in a user's watch list become publicly available they will be automatically added to the queue. XAssist is being expanded to be used as a survey planning 1001 when coupled with simulation software, including functionality for NuStar, eRosita, IXO, and the Wide Field Xray Telescope (WFXT), as part of an end to end simulation/analysis system. We are also investigating the possibility of a dedicated iPhone/iPad app for querying pipeline data, requesting processing, and administrative job control.

Bragg x-ray survey spectrometer for ITER.

PubMed

Varshney, S K; Barnsley, R; O'Mullane, M G; Jakhar, S

2012-10-01

Several potential impurity ions in the ITER plasmas will lead to loss of confined energy through line and continuum emission. For real time monitoring of impurities, a seven channel Bragg x-ray spectrometer (XRCS survey) is considered. This paper presents design and analysis of the spectrometer, including x-ray tracing by the Shadow-XOP code, sensitivity calculations for reference H-mode plasma and neutronics assessment. The XRCS survey performance analysis shows that the ITER measurement requirements of impurity monitoring in 10 ms integration time at the minimum levels for low-Z to high-Z impurity ions can largely be met.

Quantitative analysis of thoria phase in Th-U alloys using diffraction studies

NASA Astrophysics Data System (ADS)

Thakur, Shital; Krishna, P. S. R.; Shinde, A. B.; Kumar, Raj; Roy, S. B.

2017-05-01

In the present study the quantitative phase analysis of Th-U alloys in bulk form namely Th-52 wt% U and Th-3wt%U has been performed over the data obtained from both X ray diffraction and neutron diffraction technique using Rietveld method of FULLPROF software. Quantifying thoria (ThO2) phase present in bulk of the sample is limited due to surface oxidation and low penetration of x rays in high Z material. Neutron diffraction study probing bulk of the samples has been presented in comparison with x-ray diffraction study.

Ionic liquid-templated preparation of mesoporous silica embedded with nanocrystalline sulfated zirconia

NASA Astrophysics Data System (ADS)

Ward, Antony J.; Pujari, Ajit A.; Costanzo, Lorenzo; Masters, Anthony F.; Maschmeyer, Thomas

2011-12-01

A series of mesoporous silicas impregnated with nanocrystalline sulphated zirconia was prepared by a sol-gel process using an ionic liquid-templated route. The physicochemical properties of the mesoporous sulphated zirconia materials were studied using characterisation techniques such as inductively coupled optical emission spectroscopy, X-ray diffraction, transmission electron microscopy, energy-dispersive X-ray microanalysis, elemental analysis and X-ray photoelectron spectroscopy. Analysis of the new silicas indicates isomorphous substitution of silicon with zirconium and reveals the presence of extremely small (< 10 nm) polydispersed zirconia nanoparticles in the materials with zirconium loadings from 27.77 to 41.4 wt.%.

Crystallization and X-ray diffraction analysis of a catalytic domain of hyperthermophilic chitinase from Pyrococcus furiosus

PubMed Central

Mine, Shouhei; Nakamura, Tsutomu; Hirata, Kunio; Ishikawa, Kazuhiko; Hagihara, Yoshihisa; Uegaki, Koichi

2006-01-01

The crystallization and preliminary X-ray diffraction analysis of a catalytic domain of chitinase (PF1233 gene) from the hyperthermophilic archaeon Pyrococcus furiosus is reported. The recombinant protein, prepared using an Escherichia coli expression system, was crystallized by the hanging-drop vapour-diffusion method. An X-ray diffraction data set was collected at the undulator beamline BL44XU at SPring-8 to a resolution of 1.50 Å. The crystals belong to space group P212121, with unit-cell parameters a = 90.0, b = 92.8, c = 107.2 Å. PMID:16880559

Discovery of X-Ray Emission from the Crab Pulsar at Pulse Minimum

NASA Technical Reports Server (NTRS)

Tennant, Allyn F.; Becker, Werner; Juda, Michael X.; Elsner, Ronald F.; Kolodziejczak, Jeffery J.; Murray, Stephen S.; ODell, Stephen L.; Paerels, Frits; Swartz, Douglas A.; Shibazaki, Noriaki;

Discovery of X-Ray Emission from the Crab Pulsar at Pulse Minimum

NASA Technical Reports Server (NTRS)

Tennant, Allyn F.; Becker, Werner; Juda, Michael; Elsner, Ronald F.; Kolodziejczak, Jeffery J.; Murray, Stephen S.; ODell, Stephen L.; Paerels, Frits; Swartz, Douglas A.

2001-01-01

The Chandra X-Ray Observatory observed the Crab pulsar using the Low-Energy Transmission Grating with the High-Resolution Camera. Time-resolved zeroth-order images reveal that the pulsar emits X-rays at all pulse phases. Analysis of the flux at minimum - most likely non-thermal in origin - places an upper limit (T(sub infinity) < 2.1 MK) on the surface temperature of the underlying neutron star. In addition, analysis of the pulse profile establishes that the error in the Chandra-determined absolute time is quite small, -0.2 +/- 0.1 ms.

X-ray source assembly having enhanced output stability, and fluid stream analysis applications thereof

DOEpatents

Radley, Ian [Glenmont, NY; Bievenue, Thomas J [Delmar, NY; Burdett, John H [Charlton, NY; Gallagher, Brian W [Guilderland, NY; Shakshober, Stuart M [Hudson, NY; Chen, Zewu [Schenectady, NY; Moore, Michael D [Alplaus, NY

2008-06-08

An x-ray source assembly and method of operation are provided having enhanced output stability. The assembly includes an anode having a source spot upon which electrons impinge and a control system for controlling position of the anode source spot relative to an output structure. The control system can maintain the anode source spot location relative to the output structure notwithstanding a change in one or more operating conditions of the x-ray source assembly. One aspect of the disclosed invention is most amenable to the analysis of sulfur in petroleum-based fuels.

Inorganic chemical investigation by X-ray fluorescence analysis - The Viking Mars Lander

NASA Technical Reports Server (NTRS)

Toulmin, P., III; Rose, H. J., Jr.; Baird, A. K.; Clark, B. C.; Keil, K.

1973-01-01

The inorganic chemical investigation experiment added in August 1972 to the Viking Lander scientific package uses an energy-dispersive X-ray fluorescence spectrometer in which four sealed, gas-filled proportional counters detect X-rays emitted from samples of the Martian surface materials irradiated by X-rays from radioisotope sources (Fe-55 and Cd-109). The instrument is inside the Lander body, and samples are to be delivered to it by the Viking Lander Surface Sampler. Instrument design is described along with details of the data processing and analysis procedures. The results of the investigation will characterize the surface materials of Mars as to elemental composition with accuracies ranging from a few tens of parts per million (at the trace-element level) to a few per cent (for major elements) depending on the element in question.

On the X-Ray Variability of Magnetar 1RXS J170849.0-400910

NASA Technical Reports Server (NTRS)

Scholz, P.; Archibald, R. F.; Kaspi, V. M.; Ng, C.-Y.; Beardmore, A. P.; Gehrels, C.; Kennea, J. A.

2014-01-01

We present a long-term X-ray flux and spectral analysis for 1RXS J170849.0-400910 using Swift/XRT spanning over 8 years from 2005-2013. We also analyze two observations from Chandra and XMM in the period from 2003-2004. In this 10-yr period, 1RXS J170849.0-400910 displayed several rotational glitches. Previous studies have claimed variations in the X-ray emission associated with some of the glitches. From our analysis we find no evidence for significant X-ray flux variations and evidence for only low-level spectral variations. We also present an updated timing solution for 1RXS J170849.0-400910, from RXTE and Swift observations, which includes a previously unreported glitch at MJD 56019. We discuss the frequency and implications of radiatively quiet glitches in magnetars.

Crystallization and preliminary X-ray analysis of copper amine oxidase from Escherichia coli K-12.

PubMed

Roh, J H; Suzuki, H; Kumagai, H; Yamashita, M; Azakami, H; Murooka, Y; Mikami, B

1994-05-13

Copper-containing monoamine oxidase (MAO) from Escherichia coli was overproduced in the periplasmic space by expression of the cloned gene. The purified MAO has been crystallized by means of the hanging drop technique using sodium citrate as a precipitant. The crystals belong to the orthorhombic system, space group P2(1)2(1)2(1), with unit cell dimensions of a = 136.1 A, b = 168.4 A and c = 81.6 A. The asymmetric unit contains one molecule of MAO, with a crystal volume per protein mass (Vm) of 2.88 A3/Da and a solvent content of 58% by volume. The crystals diffract X-rays to a resolution limit of at least 2.7 A and are resistant to X-ray radiation damage. They appear to be suitable for X-ray structure analysis.

Use of capillary optics as a beam intensifier for a Compton x-ray source.

PubMed

Tompkins, P A; Abreu, C C; Carroll, F E; Xiao, Q F; MacDonald, C A

1994-11-01

The use of Kumakhov capillary optics will significantly enhance the performance of near-monochromatic, Compton backscattered x-ray programs. The Vanderbilt University Medical Free-Electron Laser Center is developing the capability to create these tunable x rays for medical imaging. The present transport has only reflection optics, and the beam is quite large in diameter at the laboratory. Low loss collimation of this beam would allow higher x-ray intensities after transport. This article describes experimental and computer simulation results which predict the expected performance for a multifiber Kumakhov collimator for use in the x-ray beam transport. Estimates from our research are that a multifiber optic formed of individual polycapillary fibers could be used to capture the full 7 mrad of the Vanderbilt x-ray beam and collimate it to a 1-2 mrad divergence with approximately 40%-50% transmission efficiency. This optic should increase the x-ray intensity at the laboratory level by a factor of > or = 5 by decreasing the beam divergence and subsequent spot size. Additionally, analysis of monolithic optics of fused multicapillary fibers predicts an increase in the intensity of the x rays at the laboratory by a factor of 55. These optics can have tapered channels that greatly decrease their exit divergence. This will greatly enhance the capabilities of this unique x-ray source. This article reports the initial results from a collaboration between Vanderbilt, The Center for X-Ray Optics at University at Albany, SUNY, and X-Ray Optical Systems in Albany, NY.

Chandra Observations of M31 and their Implications for its ISM

NASA Technical Reports Server (NTRS)

Primini, F.; Garcia, M.; Murray, S.; Forman, W.; Jones, C.; McClintock, J.

2000-01-01

As part of the Chandra X-ray Observatory's Survey/Monitoring Program of M31, we have been regularly observing the bulge amd inner disk of M31 for nearly 1 year, using both the HRC and ACIS Instruments. We present results from our program th it are of interest to the study of the ISM in M31. In particular, spectral analysis of bright, unresolved x-ray sources in the bulge reveals the presence of significant local x-ray extinction (N(sub H) is about 2 x 10(exp 21)/square cm), and we will attempt to map out this extinction, Further, we find that diffuse emission accounts for a significant fraction of the overall x-ray flux from the bulge. Finally, our search for x-ray counterparts to supernova remnants in M31 yields surprisingly few candidates.

Some Like it Hot: Linking Diffuse X-Ray Luminosity, Baryonic Mass, and Star Formation Rate in Compact Groups of Galaxies

NASA Technical Reports Server (NTRS)

Desjardins, Tyler D.; Gallagher, Sarah C.; Hornschemeier, Ann E.; Mulchaey, John S.; Walker, Lisa May; Brandt, Willian N.; Charlton, Jane C.; Johnson, Kelsey E.; Tzanavaris, Panayiotis

2014-01-01

We present an analysis of the diffuse X-ray emission in 19 compact groups (CGs) of galaxies observed with Chandra. The hottest, most X-ray luminous CGs agree well with the galaxy cluster X-ray scaling relations in L(x-T) and (L(x-sigma), even in CGs where the hot gas is associated with only the brightest galaxy. Using Spitzer photometry, we compute stellar masses and classify Hickson CGs 19, 22, 40, and 42, and RSCGs 32, 44, and 86 as fossil groups using a new definition for fossil systems that includes a broader range of masses. We find that CGs with total stellar and Hi masses are great than or equal to 10(sup (11.3) solar mass are often X-ray luminous, while lower-mass CGs only sometimes exhibit faint, localized X-ray emission. Additionally, we compare the diffuse X-ray luminosity against both the total UV and 24 micron star formation rates of each CG and optical colors of the most massive galaxy in each of the CGs. The most X-ray luminous CGs have the lowest star formation rates, likely because there is no cold gas available for star formation, either because the majority of the baryons in these CGs are in stars or the X-ray halo, or due togas stripping from the galaxies in CGs with hot halos. Finally, the optical colors that trace recent star formation histories of the most massive group galaxies do not correlate with the X-ray luminosities of the CGs, indicating that perhaps the current state of the X-ray halos is independent of the recent history of stellar mass assembly in the most massive galaxies.

THE CHANDRA COSMOS LEGACY SURVEY: OPTICAL/IR IDENTIFICATIONS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Marchesi, S.; Civano, F.; Urry, C. M.

2016-01-20

We present the catalog of optical and infrared counterparts of the Chandra  COSMOS-Legacy  Survey, a 4.6 Ms Chandra  program on the 2.2 deg{sup 2} of the COSMOS field, combination of 56 new overlapping observations obtained in Cycle 14 with the previous C-COSMOS survey. In this Paper we report the i, K, and 3.6 μm identifications of the 2273 X-ray point sources detected in the new Cycle 14 observations. We use the likelihood ratio technique to derive the association of optical/infrared (IR) counterparts for 97% of the X-ray sources. We also update the information for the 1743 sources detected in C-COSMOS,more » using new K and 3.6 μm information not available when the C-COSMOS analysis was performed. The final catalog contains 4016 X-ray sources, 97% of which have an optical/IR counterpart and a photometric redshift, while ≃54% of the sources have a spectroscopic redshift. The full catalog, including spectroscopic and photometric redshifts and optical and X-ray properties described here in detail, is available online. We study several X-ray to optical (X/O) properties: with our large statistics we put better constraints on the X/O flux ratio locus, finding a shift toward faint optical magnitudes in both soft and hard X-ray band. We confirm the existence of a correlation between X/O and the the 2–10 keV luminosity for Type 2 sources. We extend to low luminosities the analysis of the correlation between the fraction of obscured AGNs and the hard band luminosity, finding a different behavior between the optically and X-ray classified obscured fraction.« less

Estimate of Solar Maximum Using the 1-8 Angstrom Geostationary Operational Environmental Satellites X-Ray Measurements

DTIC Science & Technology

2014-12-12

AFRL-RV-PS- AFRL-RV-PS- TR-2015-0005 TR-2015-0005 ESTIMATE OF SOLAR MAXIMUM USING THE 1–8 Å GEOSTATIONARY OPERATIONAL ENVIRONMENTAL SATELLITES X... Geostationary Operational Environmental Satellites X-Ray Measurements (Postprint) 5a. CONTRACT NUMBER 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 61102F 6...of the solar cycle through an analysis of the solar X-ray background. Our results are based on the NOAA Geostationary Operational Environmental

Observation of X-ray eclipses from LMC X-4

NASA Technical Reports Server (NTRS)

Li, F.; Rappaport, S.; Epstein, A.

1978-01-01

Observations made with the Rotation Modulation Collimator system (RMC) have revealed that X-ray source X-4 in the Large Magellanic Cloud (LMC X-4) is most likely part of a binary system. An analysis of the star's coordinates is presented, with attention given to orbital period and flux intensity variations. Stellar mass and orbital inclination angle are estimated for both X-4 and its companion star.

An airport cargo inspection system based on X-ray and thermal neutron analysis (TNA).

PubMed

Ipe, Nisy E; Akery, A; Ryge, P; Brown, D; Liu, F; Thieu, J; James, B

2005-01-01

A cargo inspection system incorporating a high-resolution X-ray imaging system with a material-specific detection system based on Ancore Corporation's patented thermal neutron analysis (TNA) technology can detect bulk quantities of explosives and drugs concealed in trucks or cargo containers. The TNA process utilises a 252Cf neutron source surrounded by a moderator. The neutron interactions with the inspected object result in strong and unique gamma-ray signals from nitrogen, which is a key ingredient in modern high explosives, and from chlorinated drugs. The TNA computer analyses the gamma-ray signals and automatically determines the presence of explosives or drugs. The radiation source terms and shielding design of the facility are described. For the X-ray generator, the primary beam, leakage radiation, and scattered primary and leakage radiation were considered. For the TNA, the primary neutrons and tunnel scattered neutrons as well as the neutron-capture gamma rays were considered.

Design and modeling of an additive manufactured thin shell for x-ray astronomy

NASA Astrophysics Data System (ADS)

Feldman, Charlotte; Atkins, Carolyn; Brooks, David; Watson, Stephen; Cochrane, William; Roulet, Melanie; Willingale, Richard; Doel, Peter

2017-09-01

Future X-ray astronomy missions require light-weight thin shells to provide large collecting areas within the weight limits of launch vehicles, whilst still delivering angular resolutions close to that of Chandra (0.5 arc seconds). Additive manufacturing (AM), also known as 3D printing, is a well-established technology with the ability to construct or `print' intricate support structures, which can be both integral and light-weight, and is therefore a candidate technique for producing shells for space-based X-ray telescopes. The work described here is a feasibility study into this technology for precision X-ray optics for astronomy and has been sponsored by the UK Space Agency's National Space Technology Programme. The goal of the project is to use a series of test samples to trial different materials and processes with the aim of developing a viable path for the production of an X-ray reflecting prototype for astronomical applications. The initial design of an AM prototype X-ray shell is presented with ray-trace modelling and analysis of the X-ray performance. The polishing process may cause print-through from the light-weight support structure on to the reflecting surface. Investigations in to the effect of the print-through on the X-ray performance of the shell are also presented.

Deciphering a removed text on a 16th c. centrepiece: The benefits of using AGLAEMap and AXSIA to process PIXE maps.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lemasson, Quentin; Kotula, Paul; Pichon, Laurent

2015-09-01

In the field of archaeometry, it is not uncommon to be presented with art objects that contain inscriptions, signatures and other writings that are nearly impossible to read. Scanned microbeam PIXE offers an attractive approach to attack this problem, but even then the distribution of characteristic X-rays of the element(s) used in these writings can remain illegible. We show in this paper that two methods were used to reveal the inscription: first the use of a GUPIXWin, TRAUPIXE and AGLAEMap software suite enables to make quantitative analysis of each pixel, to visualize the results and to select X-ray peaks thatmore » could enable to distinguish letters. Then, the Automated eXpert Spectral Image Analysis (AXSIA) program developed at Sandia, which analyzes the x-ray intensity vs. Energy and (X, Y) position “datacubes”, was used to factor the datacube into 1) principle component spectral shapes and 2) the weighting images of these components. The specimen selected for this study was a silver plaque representing a scroll from the so-called “MerkelscheTafelaufsatz,” a centrepiece made by the Nuremberg goldsmith Wenzel Jamnitzer in 1549. X-ray radiography of the plaque shows lines of different silver thicknesses, meaning that a text has been removed. The PIXE analysis used a 3-MeV proton beam focused to 50μm and scanned across the sample on different areas of interest of several cm². This analysis showed major elements of Cu and Ag, and minor elements such as Pb, Au, Hg. X-ray intensity maps were then made by setting windows on the various x-ray peaks but the writing on the centrepiece was not revealed even if the map of Cu after data treatment at AGLAE enabled to distinguish some letters. The AXSIA program enabled to factor two main spectral shapes from the datacube that were quite similar and involved virtually all of the X-rays being generated. Nevertheless, small differences between these factors were observed for the Cu K X-rays, Pb, Bi and Au L X-rays. The plot of the factor with the highest Au signal gave also information on the shape of some letters. The comparison of the results obtained by the two methods shows that they both drastically improve the resolution and contrast of such writings and that each of the method can also bring different information on the composition and thus the techniques used for the writing.« less

Production, purification, crystallization and preliminary X-ray analysis of adeno-associated virus serotype 8

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lane, Michael Douglas; Nam, Hyun-Joo; Padron, Eric

2005-06-01

The production, purification, crystallization and preliminary X-ray crystallographic analysis of adeno-associated virus serotype 8 is reported. Adeno-associated viruses (AAVs) are actively being developed for clinical gene-therapy applications and the efficiencies of the vectors could be significantly improved by a detailed understanding of their viral capsid structures and the structural determinants of their tissue-transduction interactions. AAV8 is ∼80% identical to the more widely studied AAV2, but its liver-transduction efficiency is significantly greater than that of AAV2 and other serotypes. The production, purification, crystallization and preliminary X-ray crystallographic analysis of AAV8 viral capsids are reported. The crystals diffract X-rays to 3.0 Åmore » resolution using synchrotron radiation and belong to the hexagonal space group P6{sub 3}22, with unit-cell parameters a = 257.5, c = 443.5 Å. The unit cell contains two viral particles, with ten capsid viral protein monomers per crystallographic asymmetric unit.« less

AUSPEX: a graphical tool for X-ray diffraction data analysis.

PubMed

Thorn, Andrea; Parkhurst, James; Emsley, Paul; Nicholls, Robert A; Vollmar, Melanie; Evans, Gwyndaf; Murshudov, Garib N

2017-09-01

In this paper, AUSPEX, a new software tool for experimental X-ray data analysis, is presented. Exploring the behaviour of diffraction intensities and the associated estimated uncertainties facilitates the discovery of underlying problems and can help users to improve their data acquisition and processing in order to obtain better structural models. The program enables users to inspect the distribution of observed intensities (or amplitudes) against resolution as well as the associated estimated uncertainties (sigmas). It is demonstrated how AUSPEX can be used to visually and automatically detect ice-ring artefacts in integrated X-ray diffraction data. Such artefacts can hamper structure determination, but may be difficult to identify from the raw diffraction images produced by modern pixel detectors. The analysis suggests that a significant portion of the data sets deposited in the PDB contain ice-ring artefacts. Furthermore, it is demonstrated how other problems in experimental X-ray data caused, for example, by scaling and data-conversion procedures can be detected by AUSPEX.

Trace element abundance determinations by Synchrotron X Ray Fluorescence (SXRF) on returned comet nucleus mineral grains

NASA Technical Reports Server (NTRS)

Flynn, G. J.; Sutton, S. R.

1989-01-01

Trace element analyses were performed on bulk cosmic dust particles by Proton Induced X Ray Emission (PIXE) and Synchrotron X Ray Fluorescence (SXRF). When present at or near chondritic abundances the trace elements K, Ti, Cr, Mn, Cu, Zn, Ga, Ge, Se, and Br are presently detectable by SXRF in particles of 20 micron diameter. Improvements to the SXRF analysis facility at the National Synchrotron Light Source presently underway should increase the range of detectable elements and permit the analysis of smaller samples. In addition the Advanced Photon Source will be commissioned at Argonne National Laboratory in 1995. This 7 to 8 GeV positron storage ring, specifically designed for high-energy undulator and wiggler insertion devices, will be an ideal source for an x ray microprobe with one micron spatial resolution and better than 100 ppb elemental sensitivity for most elements. Thus trace element analysis of individual micron-sized grains should be possible by the time of the comet nucleus sample return mission.

Analysis and implementation of a space resolving spherical crystal spectrometer for x-ray Thomson scattering experiments.

PubMed

Harding, E C; Ao, T; Bailey, J E; Loisel, G; Sinars, D B; Geissel, M; Rochau, G A; Smith, I C

2015-04-01

The application of a space-resolving spectrometer to X-ray Thomson Scattering (XRTS) experiments has the potential to advance the study of warm dense matter. This has motivated the design of a spherical crystal spectrometer, which is a doubly focusing geometry with an overall high sensitivity and the capability of providing high-resolution, space-resolved spectra. A detailed analysis of the image fluence and crystal throughput in this geometry is carried out and analytical estimates of these quantities are presented. This analysis informed the design of a new spectrometer intended for future XRTS experiments on the Z-machine. The new spectrometer collects 6 keV x-rays with a spherically bent Ge (422) crystal and focuses the collected x-rays onto the Rowland circle. The spectrometer was built and then tested with a foam target. The resulting high-quality spectra prove that a spherical spectrometer is a viable diagnostic for XRTS experiments.

Influence of solar flares on the X-ray corona

NASA Technical Reports Server (NTRS)

Rust, D. M.; Batchelor, D. A.

1986-01-01

Sequences of X-ray images of solar flares, obtained with the Hard X-ray Imaging Spectrometer on the SMM spacecraft, reveal many dynamical phenomena. Movies of 20 flares recorded with 6-sec time resolution were examined. A preliminary analysis of the events as a group are presented, and some new aspects of the well-studied May 21, 1980 flare and a November 6, 1980 flare are discussed.

Development of a Grazing Incidence X-Ray Interferometer

NASA Technical Reports Server (NTRS)

Shipley, Ann; Cash, Webster; Osterman, Steve; Joy, Marshall; Carter, James

1999-01-01

A grazing incidence x-ray interferometer design capable of micro-arcsecond level resolution is discussed. This practical design employs a Michelson Stellar interferometer approach to create x-ray interference fringes without the use of Wolter style optics or diffraction crystals. Design solutions accommodating alignment, vibration, and thermal constraints are reviewed. We present the development and demonstration of a working experiment along with tolerance studies, data analysis, and results.

A deep X-ray view of the bare AGN Ark 120. IV. XMM-Newton and NuSTAR spectra dominated by two temperature (warm, hot) Comptonization processes

NASA Astrophysics Data System (ADS)

Porquet, D.; Reeves, J. N.; Matt, G.; Marinucci, A.; Nardini, E.; Braito, V.; Lobban, A.; Ballantyne, D. R.; Boggs, S. E.; Christensen, F. E.; Dauser, T.; Farrah, D.; Garcia, J.; Hailey, C. J.; Harrison, F.; Stern, D.; Tortosa, A.; Ursini, F.; Zhang, W. W.

2018-01-01

Context. The physical characteristics of the material closest to supermassive black holes (SMBHs) are primarily studied through X-ray observations. However, the origins of the main X-ray components such as the soft X-ray excess, the Fe Kα line complex, and the hard X-ray excess are still hotly debated. This is particularly problematic for active galactic nuclei (AGN) showing a significant intrinsic absorption, either warm or neutral, which can severely distort the observed continuum. Therefore, AGN with no (or very weak) intrinsic absorption along the line of sight, so-called "bare AGN", are the best targets to directly probe matter very close to the SMBH. Aims: We perform an X-ray spectral analysis of the brightest and cleanest bare AGN known so far, Ark 120, in order to determine the process(es) at work in the vicinity of the SMBH. Methods: We present spectral analyses of data from an extensive campaign observing Ark 120 in X-rays with XMM-Newton (4 × 120 ks, 2014 March 18-24), and NuSTAR (65.5 ks, 2014 March 22). Results: During this very deep X-ray campaign, the source was caught in a high-flux state similar to the earlier 2003 XMM-Newton observation, and about twice as bright as the lower-flux observation in 2013. The spectral analysis confirms the "softer when brighter" behavior of Ark 120. The four XMM-Newton/pn spectra are characterized by the presence of a prominent soft X-ray excess and a significant Fe Kα complex. The continuum is very similar above about 3 keV, while significant variability is present for the soft X-ray excess. We find that relativistic reflection from a constant-density, flat accretion disk cannot simultaneously produce the soft excess, broad Fe Kα complex, and hard X-ray excess. Instead, Comptonization reproduces the broadband (0.3-79 keV) continuum well, together with a contribution from a mildly relativistic disk reflection spectrum. Conclusions: During this 2014 observational campaign, the soft X-ray spectrum of Ark 120 below 0.5 keV was found to be dominated by Comptonization of seed photons from the disk by a warm (kTe 0.5 keV), optically-thick corona (τ 9). Above this energy, the X-ray spectrum becomes dominated by Comptonization from electrons in a hot optically thin corona, while the broad Fe Kα line and the mild Compton hump result from reflection off the disk at several tens of gravitational radii.

Studying Dust Scattering Halos with Galactic X-ray Binaries

NASA Astrophysics Data System (ADS)

Beeler, Doreen; Corrales, Lia; Heinz, Sebastian

2018-01-01

Dust is an important part of the interstellar medium (ISM) and contributes to the formation of stars and planets. Since the advent of modern X-ray telescopes, Galactic X-ray point sources have permitted a closer look at all phases of the ISM. Interstellar metals from oxygen to iron — in both gas and dust form — are responsible for absorption and scattering of X-ray light. Dust scatters the light in a forward direction and creates a diffuse halo image surrounding many bright Galactic X-ray binaries. We use all the bright X-ray point sources available in the Chandra HETG archive to study dust scattering halos from the local ISM. We have described a data analysis pipeline using a combination of the data reduction software CIAO and Python. We compare our results from Chandra HETG and ACIS-I observations of a well studied dust scattering halo around GX 13+1, in order to characterize any systematic errors associated with the HETG data set. We describe how our data products will be used to measure ISM scaling relations for X-ray extinction, dust abundance, and dust-to-metal ratios.

Statistical study of the correlation of hard X-ray and type 3 radio bursts in solar flares

NASA Technical Reports Server (NTRS)

Hamilton, Russell J.; Petrosian, Vahe

1989-01-01

A large number of hard X-ray events which were recorded by the Hard X-Ray Burst Spectrometer (HXRBS) on the Solar Maximum Mission (SMM) during the maximum of the 21st solar cycle (circa 1980) are analyzed in order to study their statistical correlation with type 3 bursts. The earlier finding by Kane (1981) are confirmed qualitatively that flares with stronger hard X-ray emission, especially those with harder spectra, are more likely to produce a type 3 burst. The observed distribution of hard X-ray and type 3 events and their correlations are shown to be satisfactorily described by a bivariate distribution consistent with the assumption of statistical linear dependence of X-ray and radio burst intensities. From this analysis it was determined that the distribution of the ratio of X-ray intensity (in counts/s) to type 3 intensity (in solar flux units) which has a wide range and a typical value for this ratio of about 10. The implications of the results for impulsive phase models are discussed.

Spectrally resolving and scattering-compensated x-ray luminescence/fluorescence computed tomography

PubMed Central

Cong, Wenxiang; Shen, Haiou; Wang, Ge

2011-01-01

The nanophosphors, or other similar materials, emit near-infrared (NIR) light upon x-ray excitation. They were designed as optical probes for in vivo visualization and analysis of molecular and cellular targets, pathways, and responses. Based on the previous work on x-ray fluorescence computed tomography (XFCT) and x-ray luminescence computed tomography (XLCT), here we propose a spectrally-resolving and scattering-compensated x-ray luminescence/fluorescence computed tomography (SXLCT or SXFCT) approach to quantify a spatial distribution of nanophosphors (other similar materials or chemical elements) within a biological object. In this paper, the x-ray scattering is taken into account in the reconstruction algorithm. The NIR scattering is described in the diffusion approximation model. Then, x-ray excitations are applied with different spectra, and NIR signals are measured in a spectrally resolving fashion. Finally, a linear relationship is established between the nanophosphor distribution and measured NIR data using the finite element method and inverted using the compressive sensing technique. The numerical simulation results demonstrate the feasibility and merits of the proposed approach. PMID:21721815

A Comparison of the Variability of the Symbiotic X-ray Binaries GX 1+4, 4U 1954+31, and 4U 1700+24 from Swift/BAT and RXTE/ASM Observations

NASA Technical Reports Server (NTRS)

Corbet, R. H. D.; Sokoloski, J. L.; Mukai, K.; Markwardt, C. B.; Tueller, J.

2007-01-01

We present an analysis of the X-ray variability of three symbiotic X-ray binaries, GX 1+4, 4U 1700+24, and 4U 1954+31, using observations made with the Swift Burst Alert Telescope (BAT) and the Rossi X-ray Timing Explorer (RXTE) All-Sky Monitor (ASM). Observations of 4U 1954+31 with the Swift BAT show modulation at a period near 5 hours. Models to explain this modulation are discussed including the presence of an exceptionally slow X-ray pulsar in the system and accretion instabilities. We conclude that the most likely interpretation is that 4U 1954+31 contains one of the slowest known X-ray pulsars. Unlike 4U 1954+31, neither GX 1+4 nor 4U 1700+24 show any evidence for modulation on a timescale of hours. An analysis of the RXTE ASM light curves of GX l+4, 4U 1700+24, and 4U 1954+31 does not show the presence of periodic modulation in any source, although there is considerable variability on long timescales for all three sources. There is no modulation in GX 1+4 on either the optical 1161 day orbital period or a previously reported 304 day X-ray period. For 4U 1700+24 we do not confirm the 404 day period previously proposed for this source from a shorter duration ASM light curve.

Experimental research on the feature of an x-ray Talbot-Lau interferometer versus tube accelerating voltage

NASA Astrophysics Data System (ADS)

Wang, Sheng-Hao; Margie, P. Olbinado; Atsushi, Momose; Hua-Jie, Han; Hu, Ren-Fang; Wang, Zhi-Li; Gao, Kun; Zhang, Kai; Zhu, Pei-Ping; Wu, Zi-Yu

2015-06-01

X-ray Talbot-Lau interferometer has been used most widely to perform x-ray phase-contrast imaging with a conventional low-brilliance x-ray source, and it yields high-sensitivity phase and dark-field images of samples producing low absorption contrast, thus bearing tremendous potential for future clinical diagnosis. In this work, by changing the accelerating voltage of the x-ray tube from 35 kV to 45 kV, x-ray phase-contrast imaging of a test sample is performed at each integer value of the accelerating voltage to investigate the characteristic of an x-ray Talbot-Lau interferometer (located in the Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Japan) versus tube voltage. Experimental results and data analysis show that within a range this x-ray Talbot-Lau interferometer is not sensitive to the accelerating voltage of the tube with a constant fringe visibility of ˜ 44%. This x-ray Talbot-Lau interferometer research demonstrates the feasibility of a new dual energy phase-contrast x-ray imaging strategy and the possibility to collect a refraction spectrum. Project supported by the Major State Basic Research Development Program of China (Grant No. 2012CB825800), the Science Fund for Creative Research Groups, China (Grant No. 11321503), the National Natural Science Foundation of China (Grant Nos. 11179004, 10979055, 11205189, and 11205157), and the Japan-Asia Youth Exchange Program in Science (SAKURA Exchange Program in Science) Administered by the Japan Science and Technology Agency.

Cloudy Skies over AGN: Observations with Simbol-X

NASA Astrophysics Data System (ADS)

Salvati, M.; Risaliti, G.

2009-05-01

Recent time-resolved spectroscopic X-ray studies of bright obscured AGN show that column density variability on time scales of hours/days may be common, at least for sources with NH>1023 cm-2. This opens new oppurtunities in the analysis of the structure of the circumnuclear medium and of the X-ray source: resolving the variations due to single clouds covering/uncovering the X-ray source provides tight constraints on the source size, the clouds' size and distance, and their average number, density and column density. We show how Simbol-X will provide a breakthrough in this field, thanks to its broad band coverage, allowing (a) to precisely disentangle the continuum and NH variations, and (2) to extend the NH variability analysis to column densities >1023 cm-2.

IPC two-color analysis of x ray galaxy clusters

NASA Technical Reports Server (NTRS)

White, Raymond E., III

1990-01-01

The mass distributions were determined of several clusters of galaxies by using X ray surface brightness data from the Einstein Observatory Imaging Proportional Counter (IPC). Determining cluster mass distributions is important for constraining the nature of the dark matter which dominates the mass of galaxies, galaxy clusters, and the Universe. Galaxy clusters are permeated with hot gas in hydrostatic equilibrium with the gravitational potentials of the clusters. Cluster mass distributions can be determined from x ray observations of cluster gas by using the equation of hydrostatic equilibrium and knowledge of the density and temperature structure of the gas. The x ray surface brightness at some distance from the cluster is the result of the volume x ray emissivity being integrated along the line of sight in the cluster.

Multislice does it all—calculating the performance of nanofocusing X-ray optics

DOE PAGES

Li, Kenan; Wojcik, Michael; Jacobsen, Chris

2017-01-23

Here, we describe an approach to calculating the optical performance of a wide range of nanofocusing X-ray optics using multislice scalar wave propagation with a complex X-ray refractive index. This approach produces results indistinguishable from methods such as coupled wave theory, and it allows one to reproduce other X-ray optical phenomena such as grazing incidence reflectivity where the direction of energy flow is changed significantly. Just as finite element analysis methods allow engineers to compute the thermal and mechanical responses of arbitrary structures too complex to model by analytical approaches, multislice propagation can be used to understand the properties ofmore » the real-world optics of finite extent and with local imperfections, allowing one to better understand the limits to nanoscale X-ray imaging.« less

A Compressed Sensing-based Image Reconstruction Algorithm for Solar Flare X-Ray Observations

NASA Astrophysics Data System (ADS)

Felix, Simon; Bolzern, Roman; Battaglia, Marina

2017-11-01

One way of imaging X-ray emission from solar flares is to measure Fourier components of the spatial X-ray source distribution. We present a new compressed sensing-based algorithm named VIS_CS, which reconstructs the spatial distribution from such Fourier components. We demonstrate the application of the algorithm on synthetic and observed solar flare X-ray data from the Reuven Ramaty High Energy Solar Spectroscopic Imager satellite and compare its performance with existing algorithms. VIS_CS produces competitive results with accurate photometry and morphology, without requiring any algorithm- and X-ray-source-specific parameter tuning. Its robustness and performance make this algorithm ideally suited for the generation of quicklook images or large image cubes without user intervention, such as for imaging spectroscopy analysis.

A Compressed Sensing-based Image Reconstruction Algorithm for Solar Flare X-Ray Observations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Felix, Simon; Bolzern, Roman; Battaglia, Marina, E-mail: simon.felix@fhnw.ch, E-mail: roman.bolzern@fhnw.ch, E-mail: marina.battaglia@fhnw.ch

One way of imaging X-ray emission from solar flares is to measure Fourier components of the spatial X-ray source distribution. We present a new compressed sensing-based algorithm named VIS-CS, which reconstructs the spatial distribution from such Fourier components. We demonstrate the application of the algorithm on synthetic and observed solar flare X-ray data from the Reuven Ramaty High Energy Solar Spectroscopic Imager satellite and compare its performance with existing algorithms. VIS-CS produces competitive results with accurate photometry and morphology, without requiring any algorithm- and X-ray-source-specific parameter tuning. Its robustness and performance make this algorithm ideally suited for the generation ofmore » quicklook images or large image cubes without user intervention, such as for imaging spectroscopy analysis.« less

Systematic design and three-dimensional simulation of X-ray FEL oscillator for Shanghai Coherent Light Facility

NASA Astrophysics Data System (ADS)

Li, Kai; Deng, Haixiao

2018-07-01

The Shanghai Coherent Light Facility (SCLF) is a quasi-continuous wave hard X-ray free electron laser facility, which is currently under construction. Due to the high repetition rate and high-quality electron beams, it is straightforward to consider X-ray free electron laser oscillator (XFELO) operation for the SCLF. In this paper, the main processes for XFELO design, and parameter optimization of the undulator, X-ray cavity, and electron beam are described. A three-dimensional X-ray crystal Bragg diffraction code, named BRIGHT, was introduced for the first time, which can be combined with the GENESIS and OPC codes for the numerical simulations of the XFELO. The performance of the XFELO of the SCLF is investigated and optimized by theoretical analysis and numerical simulation.

Statistical and operational considerations for designs for x-ray tomographic spectrophotometry to detect, localize, and classify foreign objects in various systems

NASA Astrophysics Data System (ADS)

Fennelly, Alphonsus J.; Fry, Edward L.; Zukic, Muamer; Wilson, Michele M.; Janik, Tadeusz J.; Torr, Douglas G.

1994-11-01

In six companion papers we discuss a capability for x-ray tomographic spectrophotometry at three energy ranges to observe foreign objects in various systems using a novel x-ray optical and photometric approach. We describe new types of thin-film x-ray reflecting filters to provide energy-specific optical trains, inserted into existing x-ray interrogation systems. That is complemented by performing topographic imaging at a few, to several, energies in each case. That provides a full topographic and spectrophotometric analysis. Foreign objects can then be detected, localized, discriminated, and classified, so that they may be dealt with by excision, and replacement with benign system elements. We analyze statistical and operational concerns leading to the design of three systems: The first operates at x-ray energies of 1 - 10 keV; it deals with defects in microelectronic integrated circuits. The second operates at x-ray energies of 10 - 30 keV; it deals with the defects in human tissue. The chemical specificity and image resolution of the system will allow identification, localization, and mensuration of tumors without the need of biopsy. The system which we concentrate this discussion on, the third, operates at x- ray energies of 30 - 70 keV; it deals with the presence in transportation systems of explosive devices, and contraband materials and objects in luggage and cargo. We present the analysis of the statistical features of the detection problem in these types of systems, discussing the operational constraints which limits system performance. After considering the multivariate, multisignature, approach to the problem, we discuss the tomographic and spectrophotometric approach to the problem which yields a better solution to the detection problem within the operational constraints.

Changes in bone tissue under conditions of hypokinesia and in connection with age

NASA Technical Reports Server (NTRS)

Podrushnyak, E. P.; Suslov, E. I.

1980-01-01

X-ray micrography was used to study the optical density of the blackening of X-ray photographs made of five bones in 9 young people (ages 24 to 29) before and after strict bed rest for 16 to 37 days. Photometric studies of the X-ray film determined the relative concentration of bone structure before and after hypokinesia. In addition, the bone tissues of 25 cadavers of practically healthy individuals (aged 18 to 70) who died from injuries were investigated using X-ray structural analysis. Results show that the reaction to the state of hypokinesia is not uniform in different individuals and is quite often directly reversed. It was established that pronounced osteoporosis can be found in a relatively short time after conditions of hypokinesia in healthy young individuals. Results show that the stabilization of the crystalline structure of hydroxyapatite, especially its crystal formation, is finished by the age of 20 to 25. From 25 to 60, the crystal lattice remains in stable condition but X-ray analysis shows a reduction in the hydroxyapatite density.

XMM-Newton Observations of Four Millisecond Pulsars

NASA Technical Reports Server (NTRS)

Zavlin, Vyacheslav E.

2005-01-01

I present an analysis of the XMM-Newton observations of four millisecond pulsars, J0437-4715, J2124-3358, J1024-0719, and J0034-0534. The new data provide strong evidence of thermal emission in the X-ray flux detected from the first three objects. This thermal component is best interpreted as radiation from pulsar polar caps covered with a nonmagnetic hydrogen atmosphere. A nonthermal power-law component, dominating at energies E greater than or equal to 3 keV, can also be present in the detected X-ray emission. For PSR J0437-4715, the timing analysis reveals that the shape and pulsed fraction of the pulsar light curves are energy dependent. This, together with the results obtained from the phase-resolved spectroscopy, supports the two-component (thermal plus nonthermal) interpretation of the pulsar's X-ray radiation. Highly significant pulsations have been found in the X-ray flux of PSRs 52124-3358 and 51024-0719. For PSR 50034-0534, a possible X-ray counterpart of the radio pulsar has been suggested. The inferred properties of the detected thermal emission are compared with predictions of radio pulsar models.

Analysis of Ablative Performance of C/C Composite Throat Containing Defects Based on X-ray 3D Reconstruction in a Solid Rocket Motor

NASA Astrophysics Data System (ADS)

Hui, Wei-Hua; Bao, Fu-Ting; Wei, Xiang-Geng; Liu, Yang

2015-12-01

In this paper, a new measuring method of ablation rate was proposed based on X-ray three-dimensional (3D) reconstruction. The ablation of 4-direction carbon/carbon composite nozzles was investigated in the combustion environment of a solid rocket motor, and the macroscopic ablation and linear recession rate were studied through the X-ray 3D reconstruction method. The results showed that the maximum relative error of the X-ray 3D reconstruction was 0.0576%, which met the minimum accuracy of the ablation analysis; along the nozzle axial direction, from convergence segment, throat to expansion segment, the ablation gradually weakened; in terms of defect ablation, the middle ablation was weak, while the ablation in both sides was more serious. In a word, the proposed reconstruction method based on X-ray about C/C nozzle ablation can construct a clear model of ablative nozzle which characterizes the details about micro-cracks, deposition, pores and surface to analyze ablation, so that this method can create the ablation curve in any surface clearly.

Pt and Ru X-ray absorption spectroscopy of PtRu anode catalysts in operating direct methanol fuel cells.

PubMed

Stoupin, Stanislav; Chung, Eun-Hyuk; Chattopadhyay, Soma; Segre, Carlo U; Smotkin, Eugene S

2006-05-25

In situ X-ray absorption spectroscopy, ex situ X-ray fluorescence, and X-ray powder diffraction enabled detailed core analysis of phase segregated nanostructured PtRu anode catalysts in an operating direct methanol fuel cell (DMFC). No change in the core structures of the phase segregated catalyst was observed as the potential traversed the current onset potential of the DMFC. The methodology was exemplified using a Johnson Matthey unsupported PtRu (1:1) anode catalyst incorporated into a DMFC membrane electrode assembly. During DMFC operation the catalyst is essentially metallic with half of the Ru incorporated into a face-centered cubic (FCC) Pt alloy lattice and the remaining half in an amorphous phase. The extended X-ray absorption fine structure (EXAFS) analysis suggests that the FCC lattice is not fully disordered. The EXAFS indicates that the Ru-O bond lengths were significantly shorter than those reported for Ru-O of ruthenium oxides, suggesting that the phases in which the Ru resides in the catalysts are not similar to oxides.

Study of multilayered SiGe semiconductor structures by X-ray diffractometry, grazing-incidence X-ray reflectometry, and secondary-ion mass spectrometry

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yunin, P. A., E-mail: yunin@ipmras.ru; Drozdov, Yu. N.; Drozdov, M. N.

2013-12-15

In this publication, we report the results of studying a multilayerd nonperiodic SiGe/Si structure by the methods of X-ray diffractometry, grazing-angle X-ray reflectometry, and secondary-ion mass spectrometry (SIMS). Special attention is paid to the processing of the component distribution profile using the SIMS method and to consideration of the most significant experimental distortions introduced by this method. A method for processing the measured composition distribution profile with subsequent consideration of the influence of matrix effects, variation in the etching rate, and remnants of ion sputtering is suggested. The results of such processing are compared with a structure model obtained uponmore » combined analysis of X-ray diffractometry and grazing-angle reflectometry data. Good agreement between the results is established. It is shown that the combined use of independent techniques makes it possible to improve the methods of secondary-ion mass spectrometry and grazing-incidence reflectometry as applied to an analysis of multilayered heteroepitaxial structures (to increase the accuracy and informativity of these methods)« less

Current Technology Development Efforts on the International X-Ray Observatory

NASA Technical Reports Server (NTRS)

Robinson, David

2011-01-01

The International X-ray Observatory (IXO) is a collaboration between NASA, ESA, and JAXA which is under study for launch in 2021. IXO will be a large 6600 kilogram Great Observatory-class mission which will build upon the legacies of the Chandra and XMM-Newton X-ray observatories. There is an extensive ongoing effort to raise the technology readiness level of the X-ray mirror from TRL 3 to TRL 6 in the next decade. Improvements have recently been made in the area of positioning and bonding mirrors on the nanometer scale and developing metals and composites with a matching coefficient of thermal expansion to the glass X-ray mirrors. On the mission systems side, the NASA reference design has been through a preliminary coupled loads analysis and a STOP analysis of the flight mirror assembly has been initiated. An impact study was performed comparing launching IXO on an Ariane 5 or a U.S. EELV. This paper will provide a snapshot of NASA's current observatory configuration and summarize the progress of these various technology and design efforts.

Markov Chain Monte Carlo Joint Analysis of Chandra X-Ray Imaging Spectroscopy and Sunyaev-Zel'dovich Effect Data

NASA Technical Reports Server (NTRS)

Bonamente, Massimillano; Joy, Marshall K.; Carlstrom, John E.; Reese, Erik D.; LaRoque, Samuel J.

2004-01-01

X-ray and Sunyaev-Zel'dovich effect data can be combined to determine the distance to galaxy clusters. High-resolution X-ray data are now available from Chandra, which provides both spatial and spectral information, and Sunyaev-Zel'dovich effect data were obtained from the BIMA and Owens Valley Radio Observatory (OVRO) arrays. We introduce a Markov Chain Monte Carlo procedure for the joint analysis of X-ray and Sunyaev- Zel'dovich effect data. The advantages of this method are the high computational efficiency and the ability to measure simultaneously the probability distribution of all parameters of interest, such as the spatial and spectral properties of the cluster gas and also for derivative quantities such as the distance to the cluster. We demonstrate this technique by applying it to the Chandra X-ray data and the OVRO radio data for the galaxy cluster A611. Comparisons with traditional likelihood ratio methods reveal the robustness of the method. This method will be used in follow-up paper to determine the distances to a large sample of galaxy cluster.

Substructures in DAFT/FADA survey clusters based on XMM and optical data

NASA Astrophysics Data System (ADS)

Durret, F.; DAFT/FADA Team

2014-07-01

The DAFT/FADA survey was initiated to perform weak lensing tomography on a sample of 90 massive clusters in the redshift range [0.4,0.9] with HST imaging available. The complementary deep multiband imaging constitutes a high quality imaging data base for these clusters. In X-rays, we have analysed the XMM-Newton and/or Chandra data available for 32 clusters, and for 23 clusters we fit the X-ray emissivity with a beta-model and subtract it to search for substructures in the X-ray gas. This study was coupled with a dynamical analysis for the 18 clusters with at least 15 spectroscopic galaxy redshifts in the cluster range, based on a Serna & Gerbal (SG) analysis. We detected ten substructures in eight clusters by both methods (X-rays and SG). The percentage of mass included in substructures is found to be roughly constant with redshift, with values of 5-15%. Most of the substructures detected both in X-rays and with the SG method are found to be relatively recent infalls, probably at their first cluster pericenter approach.

Proton Induced X-Ray Emission (PIXE): Determining the Concentration of Samples

NASA Astrophysics Data System (ADS)

McCarthy, Mallory; Rodriguez Manso, Alis; Pajouhafsar, Yasmin; J Yennello, Sherry

2017-09-01

We used Proton Induced X-ray Emission (PIXE) as an analysis technique to determine the composition of samples, in particular, the elemental constituents and the concentrations. Each of the samples are bombarded with protons, which in result displaces a lower level electron and causes a higher level electron to fall into its place. This displacement produces characteristic x-rays that are `fingerprints' for each element. The protons supplied for the bombardment are produced and accelerated by the K150 proton beam in the Cyclotron Institute at Texas A&M University. The products are detected by three x-ray detectors: XR-100CR Si-PIN, XR-100SDD, and XR-100T CdTe. The peaks of the spectrum are analyzed using a software analysis tool, GUPIXWIN, to determine the concentration of the known elements of each particular sample. The goals of this work are to test run the Proton Induced X-Ray Emission experimental set up at Texas A&M University (TAMU) and to determine the concentration of thin films containing KBr given by the TAMU Chemical Engineering Department.

The evolving corona and evidence for jet launching from the supermassive black hole in Markarian 335

NASA Astrophysics Data System (ADS)

Wilkins, Daniel; Gallo, Luigi C.

2015-01-01

Through detailed analysis of the X-rays that are reflected from the accretion disc, it is possible to probe structures right down to the innermost stable circular orbit and event horizon around the supermassive black holes in AGN. By measuring the illumination pattern of the accretion disc, along with reverberation time lags between variability in the X-ray continuum and reflection, unprecedented detail of the geometry and spatial extent of the corona that produces the X-ray continuum has emerged when the observed data are combined with insight gained from general relativistic ray tracing simulations.We conducted detailed analysis of both the X-ray continuum and its reflection from the accretion disc in the narrow line Seyfert 1 galaxy Markarian 335, over observations spanning nearly a decade to measure the underlying changes in the structure of the X-ray emitting corona that gave rise to more than an order of magnitude variation in luminosity.Underlying this long timescale variability lies much more complex patterns of behaviour on short timescales. We are, for the first time, able to observe and measure the changes in the structure of the corona that give rise to transient phenomena including a flare in the X-ray emission seen during a low flux state by Suzaku in July 2013. This flaring event was found to mark a reconfiguration of the corona while there is evidence that the flare itself was cased by an aborted jet-launching event. More recently, detailed analysis of a NuSTAR target of opportunity observation is letting us understand the sudden increase in X-ray flux by a factor of 15 in Markarian 335 seen in September 2014.These observations allow us to trace, from observations, the evolution of the X-ray emitting corona that gives rise to not only the extreme variability seen in the X-ray emission from AGN, but also the processes by which jets and other outflow are launched from the extreme environments around black holes. This gives us important insight into the physical processes by which energy is liberated from black hole accretion flows and allows observational constraints to be placed upon theoretical models of how these extreme objects are powered.

A whole-system approach to x-ray spectroscopy in cargo inspection systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Langeveld, Willem G. J.; Gozani, Tsahi; Ryge, Peter

The bremsstrahlung x-ray spectrum used in high-energy, high-intensity x-ray cargo inspection systems is attenuated and modified by the materials in the cargo in a Z-dependent way. Therefore, spectroscopy of the detected x rays yields information about the Z of the x-rayed cargo material. It has previously been shown that such ZSpectroscopy (Z-SPEC) is possible under certain circumstances. A statistical approach, Z-SCAN (Z-determination by Statistical Count-rate ANalysis), has also been shown to be effective, and it can be used either by itself or in conjunction with Z-SPEC when the x-ray count rate is too high for individual x-ray spectroscopy. Both techniquesmore » require fast x-ray detectors and fast digitization electronics. It is desirable (and possible) to combine all techniques, including x-ray imaging of the cargo, in a single detector array, to reduce costs, weight, and overall complexity. In this paper, we take a whole-system approach to x-ray spectroscopy in x-ray cargo inspection systems, and show how the various parts interact with one another. Faster detectors and read-out electronics are beneficial for both techniques. A higher duty-factor x-ray source allows lower instantaneous count rates at the same overall x-ray intensity, improving the range of applicability of Z-SPEC in particular. Using an intensity-modulated advanced x-ray source (IMAXS) allows reducing the x-ray count rate for cargoes with higher transmission, and a stacked-detector approach may help material discrimination for the lowest attenuations. Image processing and segmentation allow derivation of results for entire objects, and subtraction of backgrounds. We discuss R and D performed under a number of different programs, showing progress made in each of the interacting subsystems. We discuss results of studies into faster scintillation detectors, including ZnO, BaF{sub 2} and PbWO{sub 4}, as well as suitable photo-detectors, read-out and digitization electronics. We discuss high-duty-factor linear-accelerator x-ray sources and their associated requirements, and how such sources improve spectroscopic techniques. We further discuss how image processing techniques help in correcting for backgrounds and overlapping materials. In sum, we present an integrated picture of how to optimize a cargo inspection system for x-ray spectroscopy.« less

Quantitative analysis of crystalline pharmaceuticals in tablets by pattern-fitting procedure using X-ray diffraction pattern.

PubMed

Takehira, Rieko; Momose, Yasunori; Yamamura, Shigeo

2010-10-15

A pattern-fitting procedure using an X-ray diffraction pattern was applied to the quantitative analysis of binary system of crystalline pharmaceuticals in tablets. Orthorhombic crystals of isoniazid (INH) and mannitol (MAN) were used for the analysis. Tablets were prepared under various compression pressures using a direct compression method with various compositions of INH and MAN. Assuming that X-ray diffraction pattern of INH-MAN system consists of diffraction intensities from respective crystals, observed diffraction intensities were fitted to analytic expression based on X-ray diffraction theory and separated into two intensities from INH and MAN crystals by a nonlinear least-squares procedure. After separation, the contents of INH were determined by using the optimized normalization constants for INH and MAN. The correction parameter including all the factors that are beyond experimental control was required for quantitative analysis without calibration curve. The pattern-fitting procedure made it possible to determine crystalline phases in the range of 10-90% (w/w) of the INH contents. Further, certain characteristics of the crystals in the tablets, such as the preferred orientation, size of crystallite, and lattice disorder were determined simultaneously. This method can be adopted to analyze compounds whose crystal structures are known. It is a potentially powerful tool for the quantitative phase analysis and characterization of crystals in tablets and powders using X-ray diffraction patterns. Copyright 2010 Elsevier B.V. All rights reserved.

Cascaded analysis of signal and noise propagation through a heterogeneous breast model.

PubMed

Mainprize, James G; Yaffe, Martin J

2010-10-01

The detectability of lesions in radiographic images can be impaired by patterns caused by the surrounding anatomic structures. The presence of such patterns is often referred to as anatomic noise. Others have previously extended signal and noise propagation theory to include variable background structure as an additional noise term and used in simulations for analysis by human and ideal observers. Here, the analytic forms of the signal and noise transfer are derived to obtain an exact expression for any input random distribution and the "power law" filter used to generate the texture of the tissue distribution. A cascaded analysis of propagation through a heterogeneous model is derived for x-ray projection through simulated heterogeneous backgrounds. This is achieved by considering transmission through the breast as a correlated amplification point process. The analytic forms of the cascaded analysis were compared to monoenergetic Monte Carlo simulations of x-ray propagation through power law structured backgrounds. As expected, it was found that although the quantum noise power component scales linearly with the x-ray signal, the anatomic noise will scale with the square of the x-ray signal. There was a good agreement between results obtained using analytic expressions for the noise power and those from Monte Carlo simulations for different background textures, random input functions, and x-ray fluence. Analytic equations for the signal and noise properties of heterogeneous backgrounds were derived. These may be used in direct analysis or as a tool to validate simulations in evaluating detectability.

Quantitative X-ray diffraction and fluorescence analysis of paint pigment systems : final report.

DOT National Transportation Integrated Search

1978-01-01

This study attempted to correlate measured X-ray intensities with concentrations of each member of paint pigment systems, thereby establishing calibration curves for the quantitative analyses of such systems.

Influence of gamma ray irradiation on stoichiometry of hydrothermally synthesized bismuth telluride nanoparticles

NASA Astrophysics Data System (ADS)

Abishek, N. S.; Naik, K. Gopalakrishna

2018-05-01

Bismuth telluride (Bi2Te3) nanoparticles were synthesized by the hydrothermal method at 200 °C for 24 h. The synthesized Bi2Te3 nanoparticles were irradiated with gamma rays at doses of 50 kGy and 100 kGy. The structural characterization of the pre-irradiated and post-irradiated samples was carried out by X-ray diffraction technique and was found to have rhombohedral phase having R3 ¯m (166) space group. The X-ray diffraction peaks were found to shift towards lower diffraction angle with gamma ray irradiation. The morphologies and compositions of the grown Bi2Te3 nanoparticles were studied using Field Emission Scanning Electron Microscope and X-ray energy dispersive analysis, respectively. The possible cause for the shift in the X-ray diffraction peaks with gamma ray irradiation has been discussed in the present work.

Infrared and X-Ray Spectroscopy of the KES 75 Supernova Remnant Shell: Characterizing the Dust and Gas Properties

NASA Technical Reports Server (NTRS)

Temim, Tea; Dwek, Eli; Slane, Patrick; Arendt, Richard G.

2009-01-01

We present deep Chandra observations and Spitzer Space Telescope infrared (IR) spectroscopy of the shell in the composite supernova remnant (SNR) Kes 75 (G29.7-0.3). The remnant is composed of a central pulsar wind nebula and a bright partial shell in the south that is visible at radio, IR, and X-ray wavelengths. The X-ray emission can be modeled by either a single thermal component with a temperature of 1.5 keV, or with two thermal components with temperatures of 1.5 and 0.2 keV. Previous studies suggest that the hot component may originate from reverse-shocked SN ejecta. However, our new analysis shows no definitive evidence for enhanced abundances of Si, S, Ar, Mg, and Fe, as expected from supernova (SN) ejecta, or for the IR spectral signatures characteristic of confirmed SN condensed dust, thus favoring a circumstellar or interstellar origin for the X-ray and IR emission. The X-ray and ill emission in the shell are spatially correlated, suggesting that the dust particles are collisionally heated by the X-ray emitting gas. The IR spectrum of the shell is dominated by continuum emission from dust with little, or no line emission. Modeling the IR spectrum shows that the dust is heated to a temperature of 140 K by a relatively dense, hot plasma, that also gives rise to the hot X-ray emission component. The density inferred from the IR emission is significantly higher than the density inferred from the X-ray models, suggesting a low filling factor for this X-ray emitting gas. The total mass of the warm dust component is at least 1.3 x 10(exp -2) solar mass, assuming no significant dust destruction has occurred in the shell. The IR data also reveal the presence of an additional plasma component with a cooler temperature, consistent with the 0.2 keV gas component. Our IR analysis therefore provides an independent verification of the cooler component of the X-ray emission. The complementary analyses of the X-ray and IR emission provide quantitative estimates of density and filling factors of the clumpy medium swept up by the SNR.

Infrared and X-Ray Spectroscopy of the Kes 75 Supernova Shell Characterizing the Dust and Gas Properties

NASA Technical Reports Server (NTRS)

Temim, Tea; Arendt, Richard G.; Dwek, Eli; Slane, Patrick

2012-01-01

We present deep Chandra observations and Spitzer Space Telescope infrared (IR) spectroscopy of the shell in the composite supernova remnant (SNR) Kes 75 (G29.7-0.3). The remnant is composed of a central pulsar wind nebula and a bright partial shell in the south that is visible at radio, IR, and X-ray wavelengths. The X-ray emission can be modeled by either a single thermal component with a temperature of approx 1.5 keV, or with two thermal components with temperatures of 1.5 and 0.2 keY. Previous studies suggest that the hot component may originate from reverse-shocked SN ejecta. However, our new analysis shows no definitive evidence for enhanced abundances of Si, S, Ar, Mg, and Fe, as expected from supernova (SN) ejecta, or for the IR spectral signatures characteristic of confirmed SN condensed dust, thus favoring a circumstellar or interstellar origin for the X-ray and IR emission. The X-ray and IR emission in the shell are spatially correlated, suggesting that the dust particles are collisionally heated by the X-ray emitting gas. The IR spectrum of the shell is dominated by continuum emission from dust with little, or no line emission. Modeling the IR spectrum shows that the dust is heated to a temperature of approx 140 K by a relatively dense, hot plasma, that also gives rise to the hot X-ray emission component. The density inferred from the IR emission is significantly higher than the density inferred from the X-ray models, suggesting a low filling factor for this X-ray emitting gas. The total mass of the warm dust component is at least 1.3 x 10(exp -2) Solar Mass, assuming no significant dust destruction has occurred in the shell. The IR data also reveal the presence of an additional plasma component with a cooler temperature, consistent with the 0.2 keV gas component. Our IR analysis therefore provides an independent verification of the cooler component of the X-ray emission. The complementary analyses of the X-ray and IR emission provide quantitative estimates of density and filling factors of the clumpy medium swept up by the SNR.

HIGH-RESOLUTION X-RAY SPECTROSCOPY REVEALS THE SPECIAL NATURE OF WOLF-RAYET STAR WINDS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Oskinova, L. M.; Hamann, W.-R.; Gayley, K. G.

We present the first high-resolution X-ray spectrum of a putatively single Wolf-Rayet (WR) star. 400 ks observations of WR 6 by the XMM-Newton telescope resulted in a superb quality high-resolution X-ray spectrum. Spectral analysis reveals that the X-rays originate far out in the stellar wind, more than 30 stellar radii from the photosphere, and thus outside the wind acceleration zone where the line-driving instability (LDI) could create shocks. The X-ray emitting plasma reaches temperatures up to 50 MK and is embedded within the unshocked, 'cool' stellar wind as revealed by characteristic spectral signatures. We detect a fluorescent Fe line atmore » Almost-Equal-To 6.4 keV. The presence of fluorescence is consistent with a two-component medium, where the cool wind is permeated with the hot X-ray emitting plasma. The wind must have a very porous structure to allow the observed amount of X-rays to escape. We find that neither the LDI nor any alternative binary scenario can explain the data. We suggest a scenario where X-rays are produced when the fast wind rams into slow 'sticky clumps' that resist acceleration. Our new data show that the X-rays in single WR star are generated by some special mechanism different from the one operating in the O-star winds.« less

Quantitative X-ray mapping, scatter diagrams and the generation of correction maps to obtain more information about your material

NASA Astrophysics Data System (ADS)

Wuhrer, R.; Moran, K.

2014-03-01

Quantitative X-ray mapping with silicon drift detectors and multi-EDS detector systems have become an invaluable analysis technique and one of the most useful methods of X-ray microanalysis today. The time to perform an X-ray map has reduced considerably with the ability to map minor and trace elements very accurately due to the larger detector area and higher count rate detectors. Live X-ray imaging can now be performed with a significant amount of data collected in a matter of minutes. A great deal of information can be obtained from X-ray maps. This includes; elemental relationship or scatter diagram creation, elemental ratio mapping, chemical phase mapping (CPM) and quantitative X-ray maps. In obtaining quantitative x-ray maps, we are able to easily generate atomic number (Z), absorption (A), fluorescence (F), theoretical back scatter coefficient (η), and quantitative total maps from each pixel in the image. This allows us to generate an image corresponding to each factor (for each element present). These images allow the user to predict and verify where they are likely to have problems in our images, and are especially helpful to look at possible interface artefacts. The post-processing techniques to improve the quantitation of X-ray map data and the development of post processing techniques for improved characterisation are covered in this paper.

Lunar elemental analysis obtained from the Apollo gamma-ray and X-ray remote sensing experiment

NASA Technical Reports Server (NTRS)

Trombka, J. I.; Arnold, J. R.; Adler, I.; Metzger, A. E.; Reedy, R. C.

1977-01-01

Gamma-ray and X-ray spectrometers carried in the service modules of the Apollo 15 and Apollo 16 spacecraft were employed for compositional mapping of the lunar surface. The measurements involved the observation of the intensity and characteristic energy distribution of gamma rays and X-rays emitted from the lunar surface. A large-scale compositional map of over 10 percent of the lunar surface was obtained from an analysis of the observed spectra. The objective of the X-ray experiment was to measure the K spectral lines from Mg, Al, and Si. Spectra were obtained and the data were reduced to Al/Si and Mg/Si intensity ratios and ultimately to chemical ratios. Analyses of the results have indicated (1) that the Al/Si ratios are highest in the lunar highlands and considerably lower in the maria, and (2) that the Mg/Si concentrations generally show the opposite relationship. The objective of the gamma-ray experiment was to measure the natural and cosmic-ray-induced activity emission spectrum. At this time, the elemental abundances for Th, U, K, Fe, Ti, Si, and O have been determined over a number of major lunar regions. Regions of relatively high natural radioactivity were found in the Mare Imbrium and Oceanus Procellarum regions.

Investigation of the nanoscale two-component ZnS-ZnO heterostructures by means of HR-TEM and X-ray based analysis

NASA Astrophysics Data System (ADS)

Pankin, I. A.; Polozhentsev, O. E.; Soldatov, M. A.; Bugaev, A. L.; Tsaturyan, A.; Lomachenko, K. A.; Guda, A. A.; Budnyk, A. P.; Lamberti, C.; Soldatov, A. V.

2018-06-01

This article is devoted to the spectroscopic characterization of ZnS-ZnO nanoscale heterostructures synthesized by the microwave-assisted solvothermal method. The synthesized samples were investigated by means of X-ray powder diffraction (XRPD), high energy resolution fluorescence detected X-ray absorption near-edge-structure (HERFD-XANES) spectroscopy, valence-to-core X-ray emission spectroscopy (VtC-XES) and high resolution transmission electron microscopy (HR-TEM) as well as energy dispersive X-ray spectroscopy (EDX). The average crystallite size estimated by the broadening of XRPD peaks increases from 2.7 nm to 3.7 nm in the temperature range from 100 °C to 150 °C. HR-TEM images show that nanoparticles are arranged in aggregates with the 60-200 nm size. Theoretical estimation shows that the systems synthesized at higher temperatures more prone to the agglomeration. The full profile Reitveld analysis of XRPD data reveals the formation of hexagonal zinc sulfide structure, whereas electron diffraction data reveal also the formation of cubic zinc sulfide and claim the polymorphous character of the system. High energy resolution Zn K-edge XANES data unambiguously demonstrate the presence of a certain amount of the zinc oxide which is likely to have an amorphous structure and could not be detected by XRPD. Qualitative analysis of XANES data allows deriving ZnS/ZnO ratio as a function of synthesis temperature. EDX analysis depicts homogeneous distribution of ZnS and amorphous ZnO phases across the conglomerates. A complementary element-selective valence to core X-ray emission spectroscopy evidences formation of two-component system and confirms estimations of ZnS/ZnO fractions obtained by linear combination fit of XANES data.

Infrared Counterparts to Chandra X-Ray Sources in the Antennae

NASA Astrophysics Data System (ADS)

Clark, D. M.; Eikenberry, S. S.; Brandl, B. R.; Wilson, J. C.; Carson, J. C.; Henderson, C. P.; Hayward, T. L.; Barry, D. J.; Ptak, A. F.; Colbert, E. J. M.

2007-03-01

We use deep J (1.25 μm) and Ks (2.15 μm) images of the Antennae (NGC 4038/4039) obtained with the Wide-field InfraRed Camera on the Palomar 200 inch (5 m) telescope, together with the Chandra X-ray source list of Zezas and coworkers to search for infrared counterparts to X-ray point sources. We establish an X-ray/IR astrometric frame tie with ~0.5" rms residuals over a ~4.3' field. We find 13 ``strong'' IR counterparts brighter than Ks=17.8 mag and <1.0" from X-ray sources, and an additional 6 ``possible'' IR counterparts between 1.0'' and 1.5'' from X-ray sources. Based on a detailed study of the surface density of IR sources near the X-ray sources, we expect only ~2 of the ``strong'' counterparts and ~3 of the ``possible'' counterparts to be chance superpositions of unrelated objects. Comparing both strong and possible IR counterparts to our photometric study of ~220 IR clusters in the Antennae, we find with a >99.9% confidence level that IR counterparts to X-ray sources are ΔMKs~1.2 mag more luminous than average non-X-ray clusters. We also note that the X-ray/IR matches are concentrated in the spiral arms and ``overlap'' regions of the Antennae. This implies that these X-ray sources lie in the most ``super'' of the Antennae's super star clusters, and thus trace the recent massive star formation history here. Based on the NH inferred from the X-ray sources without IR counterparts, we determine that the absence of most of the ``missing'' IR counterparts is not due to extinction, but that these sources are intrinsically less luminous in the IR, implying that they trace a different (possibly older) stellar population. We find no clear correlation between X-ray luminosity classes and IR properties of the sources, although small-number statistics hamper this analysis.

Comparison of the X-Ray and Radio Light Curves of Quasar PKS 1510--089

NASA Technical Reports Server (NTRS)

Aller, M. F.; Marscher, A. P.; Marchenko-Jorstad, S. G.; McHardy, I. M.; Aller, H. D.

1998-01-01

We present results for the X-ray-bright superluminal AGN PKS 1510-089 (z=0.36) monitored weekly with the Rossi X-Ray Timing Explorer for the past four years in order to study the origin of X-ray emission from this extremely variable blazer. These RXTE data are compared with weekly cm-band flux and polarization observations from the Michigan Diameter telescope, to identify correlated activity and associated frequency-dependent time delays for constraining X-ray emission models; and bimonthly 7mm VLBA total and linearly polarized intensity imaging to identify temporal associations between X-ray events and the ejection of superluminal components and disturbances in the magnetic field, to test if the X-ray energy release is related to changes in the inner jet flow. Both the X-ray (2-20 keV) and radio flux are highly variable on timescales of weeks. The VLBA mas structure is dominated by a bright core with a weak jet; both the ejection of very fast superluminal knots and changes in the fractional polarization and EVPA of the core on timescales of one to four months are identified. Two outbursts in 1997 are well-resolved in both the centimeter and X-ray bands. Both the strong temporal association and the similar outburst shape support a causal relation, and a discrete cross-correlation analysis identifies that the X-ray lags the radio by 16 days during the bursts. Starting in 1998 the behavior changes: the correlation is weaker with the X-ray possibly leading the radio by six days. During the full time window there is a correlation between bands as expected if the radio photons are upscattered to X-ray energies. The time correlations and difference between the flat X-ray spectral index (0.0 <= alpha <= 0.5 where F(sub v) is proportional to v(exp -alpha)), and the mm-wave synchrotron spectrum (alpha = 0.8) are discussed within the framework of viable SSC models.

A year-long AGILE observation of Cygnus X-1 in hard spectral state

NASA Astrophysics Data System (ADS)

Del Monte, E.; Feroci, M.; Evangelista, Y.; Costa, E.; Donnarumma, I.; Lapshov, I.; Lazzarotto, F.; Pacciani, L.; Rapisarda, M.; Soffitta, P.; Argan, A.; Barbiellini, G.; Boffelli, F.; Bulgarelli, A.; Caraveo, P.; Cattaneo, P. W.; Chen, A.; D'Ammando, F.; Di Cocco, G.; Fuschino, F.; Galli, M.; Gianotti, F.; Giuliani, A.; Labanti, C.; Lipari, P.; Longo, F.; Marisaldi, M.; Mereghetti, S.; Moretti, E.; Morselli, A.; Pellizzoni, A.; Perotti, F.; Piano, G.; Picozza, P.; Pilia, M.; Prest, M.; Pucella, G.; Rappoldi, A.; Sabatini, S.; Striani, E.; Tavani, M.; Trifoglio, M.; Trois, A.; Vallazza, E.; Vercellone, S.; Vittorini, V.; Zambra, A.; Antonelli, L. A.; Cutini, S.; Pittori, C.; Preger, B.; Santolamazza, P.; Verrecchia, F.; Giommi, P.; Salotti, L.

2010-09-01

Context. Cygnus X-1 (Cyg X-1) is a high mass X-ray binary system, known to be a black hole candidate and one of the brightest sources in the X-ray sky, which shows both variability on all timescales and frequent flares. The source spends most of the time in a hard spectral state, dominated by a power-law emission, with occasional transitions to the soft and intermediate states, where a strong blackbody component emerges. Aims: We present the observation of Cyg X-1 in a hard spectral state performed during the AGILE science verification phase and observing cycle 1 in hard X-rays (with SuperAGILE) and gamma rays (with the gamma ray imaging detector) and lasting for about 160 days with a live time of ~6 Ms. Methods: We investigated the variability of Cyg X-1 in hard X-rays on different timescales, from ~300 s up to one day, and we applied different tools of timing analysis, such as the autocorrelation function, the first-order structure function, and the Lomb-Scargle periodogram, to our data (from SuperAGILE) and to the simultaneous data in soft X-rays (from RXTE/ASM). We concluded our investigation with a search for emission in the energy range above 100 MeV with the maximum likelihood technique. Results: In the hard X-ray band, the flux of Cyg X-1 shows its typical erratic fluctuations on all timescales with variations of about a factor of two that do not significantly affect the shape of the energy spectrum. From the first-order structure function, we find that the X-ray emission of Cyg X-1 is characterized by antipersistence (anticorrelation in the time series, with an increase in the emission likely followed by a decrease), indicative of a negative feedback mechanism at work. In the gamma ray data a statistically significant point-like source at the position of Cyg X-1 is not found, and the upper limit on the flux is 5 × 10-8 ph cm-2 s-1 over the whole observation (160 days). Finally we compared our upper limit in gamma rays with the expectation of various models of the Cyg X-1 emission, both of hadronic and leptonic origin, in the GeV-TeV band. Conclusions: The time history of Cyg X-1 in the hard X-ray band over 13 months (not continuous) is shown. Different analysis tools do not provide fully converging results of the characteristic timescales in the system, suggesting that the timescales found in the structure function are not intrinsic to the physics of the source. While Cyg X-1 is not detected in gamma rays, our upper limit is a factor of two lower than the EGRET one and is compatible with the extrapolation of the flux measured by COMPTEL in the same spectral state.

The physical origin of the X-ray emission from SN 1987A

NASA Astrophysics Data System (ADS)

Miceli, M.; Orlando, S.; Petruk, O.

2017-10-01

We revisit the spectral analysis of the set of archive XMM-Newton observations of SN 1987A through our 3-D hydrodynamic model describing the whole evolution from the onset of the supernova to the full remnant development. For the first time the spectral analysis accounts for the single observations and for the evolution of the system self-consistently. We adopt a forward modeling approach which allows us to directly synthesize, from the model, X-ray spectra and images in different energy bands. We fold the synthetic observables through the XMM-Newton instrumental response and directly compare models and actual data. We find that our simulation provides an excellent fit to the data, by reproducing simultaneously X-ray fluxes, spectral features, and morphology of SN 1987A at all evolutionary stages. Our analysis enables us to obtain a deep insight on the physical origin of the observed multi-thermal emission, by revealing the contribution of shocked surrounding medium, dense clumps of the circumstellar ring, and ejecta to the total emission. We finally provide predictions for future observations (to be performed with XMM-Newton in the next future and with the forthcoming Athena X-ray telescope in approximately 10 years), showing the growing contribution of the ejecta X-ray emission.

Progress Towards Improved Analysis of TES X-ray Data Using Principal Component Analysis

NASA Technical Reports Server (NTRS)

Busch, S. E.; Adams, J. S.; Bandler, S. R.; Chervenak, J. A.; Eckart, M. E.; Finkbeiner, F. M.; Fixsen, D. J.; Kelley, R. L.; Kilbourne, C. A.; Lee, S.-J.;

Unified Theory for Decoding the Signals from X-Ray Florescence and X-Ray Diffraction of Mixtures.

PubMed

Chung, Frank H

2017-05-01

For research and development or for solving technical problems, we often need to know the chemical composition of an unknown mixture, which is coded and stored in the signals of its X-ray fluorescence (XRF) and X-ray diffraction (XRD). X-ray fluorescence gives chemical elements, whereas XRD gives chemical compounds. The major problem in XRF and XRD analyses is the complex matrix effect. The conventional technique to deal with the matrix effect is to construct empirical calibration lines with standards for each element or compound sought, which is tedious and time-consuming. A unified theory of quantitative XRF analysis is presented here. The idea is to cancel the matrix effect mathematically. It turns out that the decoding equation for quantitative XRF analysis is identical to that for quantitative XRD analysis although the physics of XRD and XRF are fundamentally different. The XRD work has been published and practiced worldwide. The unified theory derives a new intensity-concentration equation of XRF, which is free from the matrix effect and valid for a wide range of concentrations. The linear decoding equation establishes a constant slope for each element sought, hence eliminating the work on calibration lines. The simple linear decoding equation has been verified by 18 experiments.

The Determination of Metals in Welding Fume by X-RaySpectrometry

NASA Astrophysics Data System (ADS)

Kuznetsova, O. V.; Begunova, L. A.; Romanenko, S. V.; Solodsky, S. A.

2018-01-01

Analysis of the current hygienic situation in the welding production showed that the intensification of welding processes involves the deterioration of air quality, which negatively affects the welders health. Respiratory effects seen in full-time welders have included bronchitis, airway irritation, lung function changes, and a possible increase in the incidence of lung cancer. The metal concentration in the air of the working area have been determined using the photometric method of analysis, which involves the stage of decomposition of the sample material before analysis. However, losses of the analyzed elements are possible when the sample is decomposed. The X-ray fluorescence method of analysis has the advantage of being nondestructive. The investigations shown the data of photometric determination of metals in welding aerosols is 1.5÷2 times lower than the results of X-ray fluorescence analysis.

Syntheses, structures and luminescent properties of two novel Zn (II) coordination polymers

NASA Astrophysics Data System (ADS)

Huang, Ya-Ru; Gao, Ling-Ling; Wang, Xiao-Qing; Fan, Li-Ming; Hu, Tuo-Ping

2018-02-01

Two new coordination polymers, namely [Zn(TZMB)]n (1) and {[Zn(TZMB)](H2TZMB)]·(C2H5OH)0.5(H2O)2.5}n (2), (H2TZMB = 4,4‧-(1H-1,2,4-triazol-1-yl)methylene-bis(benzonic acid), have been synthesized under hydrothermal conditions and characterized by single-crystal X-ray diffraction analysis, elemental analysis (EA), IR spectrum analysis (IR), powder X-ray diffraction (PXRD), and thermogravimetric (TG) analysis. Single X-ray diffraction analysis reveals that complex 1 is a 3D 3,6-connected net with the point symbol of (6110.84)(63)2 and complex 2 is a 2D 3-connected net with the point symbol of (63). Furthermore, luminescent properties of complexes 1 and 2 were also investigated in detail.

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

How little data is enough? Phase-diagram analysis of sparsity-regularized X-ray computed tomography

PubMed Central

Jørgensen, J. S.; Sidky, E. Y.

2015-01-01

We introduce phase-diagram analysis, a standard tool in compressed sensing (CS), to the X-ray computed tomography (CT) community as a systematic method for determining how few projections suffice for accurate sparsity-regularized reconstruction. In CS, a phase diagram is a convenient way to study and express certain theoretical relations between sparsity and sufficient sampling. We adapt phase-diagram analysis for empirical use in X-ray CT for which the same theoretical results do not hold. We demonstrate in three case studies the potential of phase-diagram analysis for providing quantitative answers to questions of undersampling. First, we demonstrate that there are cases where X-ray CT empirically performs comparably with a near-optimal CS strategy, namely taking measurements with Gaussian sensing matrices. Second, we show that, in contrast to what might have been anticipated, taking randomized CT measurements does not lead to improved performance compared with standard structured sampling patterns. Finally, we show preliminary results of how well phase-diagram analysis can predict the sufficient number of projections for accurately reconstructing a large-scale image of a given sparsity by means of total-variation regularization. PMID:25939620

How little data is enough? Phase-diagram analysis of sparsity-regularized X-ray computed tomography.

PubMed

Jørgensen, J S; Sidky, E Y

2015-06-13

We introduce phase-diagram analysis, a standard tool in compressed sensing (CS), to the X-ray computed tomography (CT) community as a systematic method for determining how few projections suffice for accurate sparsity-regularized reconstruction. In CS, a phase diagram is a convenient way to study and express certain theoretical relations between sparsity and sufficient sampling. We adapt phase-diagram analysis for empirical use in X-ray CT for which the same theoretical results do not hold. We demonstrate in three case studies the potential of phase-diagram analysis for providing quantitative answers to questions of undersampling. First, we demonstrate that there are cases where X-ray CT empirically performs comparably with a near-optimal CS strategy, namely taking measurements with Gaussian sensing matrices. Second, we show that, in contrast to what might have been anticipated, taking randomized CT measurements does not lead to improved performance compared with standard structured sampling patterns. Finally, we show preliminary results of how well phase-diagram analysis can predict the sufficient number of projections for accurately reconstructing a large-scale image of a given sparsity by means of total-variation regularization.

CHANDRA AND SWIFT X-RAY OBSERVATIONS OF THE X-RAY PULSAR SMC X-2 DURING THE OUTBURST OF 2015

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, K. L.; Hu, C.-P; Lin, L. C. C.

2016-09-10

We report the Chandra /HRC-S and Swift /XRT observations for the 2015 outburst of the high-mass X-ray binary pulsar in the Small Magellanic Cloud, SMC X-2. While previous studies suggested that either an O star or a Be star in the field is the high-mass companion of SMC X-2, our Chandra /HRC-S image unambiguously confirms the O-type star as the true optical counterpart. Using the Swift /XRT observations, we extracted accurate orbital parameters of the pulsar binary through a time of arrivals analysis. In addition, there were two X-ray dips near the inferior conjunction, which are possibly caused by eclipsesmore » or an ionized high-density shadow wind near the companion’s surface. Finally, we propose that an outflow driven by the radiation pressure from day ∼10 played an important role in the X-ray/optical evolution of the outburst.« less

X-Ray Emission from the Soft X-Ray Transient Aquila X-1

NASA Technical Reports Server (NTRS)

Tavani, Marco

1998-01-01

Aquila X-1 is the most prolific of soft X-ray transients. It is believed to contain a rapidly spinning neutron star sporadically accreting near the Eddington limit from a low-mass companion star. The interest in studying the repeated X-ray outbursts from Aquila X-1 is twofold: (1) studying the relation between optical, soft and hard X-ray emission during the outburst onset, development and decay; (2) relating the spectral component to thermal and non-thermal processes occurring near the magnetosphere and in the boundary layer of a time-variable accretion disk. Our investigation is based on the BATSE monitoring of Aquila X-1 performed by our group. We observed Aquila X-1 in 1997 and re-analyzed archival information obtained in April 1994 during a period of extraordinary outbursting activity of the source in the hard X-ray range. Our results allow, for the first time for this important source, to obtain simultaneous spectral information from 2 keV to 200 keV. A black body (T = 0.8 keV) plus a broken power-law spectrum describe accurately the 1994 spectrum. Substantial hard X-ray emission is evident in the data, confirming that the accretion phase during sub-Eddington limit episodes is capable of producing energetic hard emission near 5 x 10(exp 35) ergs(exp -1). A preliminary paper summarizes our results, and a more comprehensive account is being written. We performed a theoretical analysis of possible emission mechanisms, and confirmed that a non-thermal emission mechanism triggered in a highly sheared magnetosphere at the accretion disk inner boundary can explain the hard X-ray emission. An anticorrelation between soft and hard X-ray emission is indeed prominently observed as predicted by this model.

The XMM-Newton Extended Survey of the Taurus Molecular Cloud (XEST)

NASA Technical Reports Server (NTRS)

Guedel, M.; Briggs, K. R.; Arzner, K.; Audard, M.; Bouvier, J.; Feigelson, E. D.; Franciosini, E.; Glauser, A.; Grosso, N.; Micela, G.;

A normal incidence X-ray telescope

NASA Technical Reports Server (NTRS)

Golub, Leon

1987-01-01

The postflight performance evaluation of the X-ray telescope was summarized. All payload systems and subsystems performed well within acceptable limits, with the sole exception of the light-blocking prefilters. Launch, flight and recovery were performed in a fully satisfactory manner. The payload was recovered in a timely manner and in excellent condition. The prefilter performance analysis showed that no X-ray images were detected on the processed flight film. Recommendations for improved performance are listed.

Small astronomy satellite-A, Uhuru data analysis

NASA Technical Reports Server (NTRS)

Koch, D.

1974-01-01

Objectives were to conduct observations with the first satellite entirely devoted to X-ray astronomy and to analyze the results obtained. A catalog of X-ray sources was generated, and results of discoveries and further detailed observations of sources were presented in scientific journals and meetings. A list of how objectives were met, a brief description of the instrument, significant results, the X-ray catalog, and a complete bibliography of results are included.

Topological Insulators and Superconductors for Innovative Devices

DTIC Science & Technology

2015-03-20

bulk-sensitive experiment with hard x ray or low-energy photons.) This demon- strates that the bulk band gap can be enhanced by taking advantage of the...crystallinity in X - ray Laue analysis, and their detailed transport properties are described in the Supplementary Information. ARPES measurements were...high quality of our fi lms grown at high temperatures, including ultrathin ones, is evident from the X - ray diffraction patterns shown in Figure 2 d

Measurement of X-ray mass attenuation coefficients in biological and geological samples in the energy range of 7-12keV.

PubMed

Trunova, Valentina; Sidorina, Anna; Kriventsov, Vladimir

2015-01-01

Information about X-ray mass attenuation coefficients in different materials is necessary for accurate X-ray fluorescent analysis. The X-ray mass attenuation coefficients for energy of 7-12keV were measured in biological (Mussel and Oyster tissues, blood, hair, liver, and Cabbage leaves) and geological (Baikal sludge, soil, and Alaskite granite) samples. The measurements were carried out at the EXAFS Station of Siberian Synchrotron Radiation Center (VEPP-3). Obtained experimental mass attenuation coefficients were compared with theoretical values calculated for some samples. Copyright © 2014 Elsevier Ltd. All rights reserved.

Discovery of a 50 millisecond pulsar in the Large Magellanic Cloud

NASA Technical Reports Server (NTRS)

Seward, F. D.; Harnden, F. R., Jr.; Helfand, D. J.

1984-01-01

The present investigation is concerned with the discovery of a new pulsed X-ray source in the Large Magellanic Cloud (LMC) supernova remnant 0540 - 693. The SNR 0540 - 693 is one of three suspected Crab-like remnants in the LMC. The existing X-ray, optical, and radio observations of the remnant itself are discussed, and an analysis is conducted of the implications of the period, period derivative, and X-ray pulse shape of the new source. It is concluded that the pulsed X-ray source is almost certainly a young, isolated pulsar. Many of its properties are very similar to those of the Crab pulsar.

X-ray texture analysis of paper coating pigments and the correlation with chemical composition analysis

NASA Astrophysics Data System (ADS)

Roine, J.; Tenho, M.; Murtomaa, M.; Lehto, V.-P.; Kansanaho, R.

2007-10-01

The present research experiments the applicability of x-ray texture analysis in investigating the properties of paper coatings. The preferred orientations of kaolin, talc, ground calcium carbonate, and precipitated calcium carbonate particles used in four different paper coatings were determined qualitatively based on the measured crystal orientation data. The extent of the orientation, namely, the degree of the texture of each pigment, was characterized quantitatively using a single parameter. As a result, the effect of paper calendering is clearly seen as an increase on the degree of texture of the coating pigments. The effect of calendering on the preferred orientation of kaolin was also evident in an independent energy dispersive spectrometer analysis on micrometer scale and an electron spectroscopy for chemical analysis on nanometer scale. Thus, the present work proves x-ray texture analysis to be a potential research tool for characterizing the properties of paper coating layers.

Design of an imaging microscope for soft X-ray applications

NASA Astrophysics Data System (ADS)

Hoover, Richard B.; Shealy, David L.; Gabardi, David R.; Walker, Arthur B. C., Jr.; Lindblom, Joakim F.

1988-01-01

An imaging soft X-ray microscope with a spatial resolution of 0.1 micron and normal incidence multilayer optics is discussed. The microscope has a Schwarzschild configuration, which consists of two concentric spherical mirrors with radii of curvature which minimize third-order spherical aberration, coma, and astigmatism. The performance of the Stanford/MSFC Cassegrain X-ray telescope and its relevance to the present microscope are addressed. A ray tracing analysis of the optical system indicates that diffraction-limited performance can be expected for an object height of 0.2 mm.

Spread spectrum phase modulation for coherent X-ray diffraction imaging.

PubMed

Zhang, Xuesong; Jiang, Jing; Xiangli, Bin; Arce, Gonzalo R

2015-09-21

High dynamic range, phase ambiguity and radiation limited resolution are three challenging issues in coherent X-ray diffraction imaging (CXDI), which limit the achievable imaging resolution. This paper proposes a spread spectrum phase modulation (SSPM) method to address the aforementioned problems in a single strobe. The requirements on phase modulator parameters are presented, and a practical implementation of SSPM is discussed via ray optics analysis. Numerical experiments demonstrate the performance of SSPM under the constraint of available X-ray optics fabrication accuracy, showing its potential to real CXDI applications.

Publications - GMC 419 | Alaska Division of Geological & Geophysical

Science.gov Websites

DGGS GMC 419 Publication Details Title: X-Ray diffraction analysis of cuttings samples from the Trading for more information. Quadrangle(s): Kenai Bibliographic Reference TIORCO Inc., 2013, X-Ray

Publications - GMC 332 | Alaska Division of Geological & Geophysical

Science.gov Websites

DGGS GMC 332 Publication Details Title: X-Ray Diffraction analysis and flow testing of Hemlock information. Quadrangle(s): Alaska Statewide Bibliographic Reference BJ Services Company , 2006, X-Ray

New X-Ray Technique to Characterize Nanoscale Precipitates in Aged Aluminum Alloys

NASA Astrophysics Data System (ADS)

Sitdikov, V. D.; Murashkin, M. Yu.; Valiev, R. Z.

2017-10-01

This paper puts forward a new technique for measurement of x-ray patterns, which enables to solve the problem of identification and determination of precipitates (nanoscale phases) in metallic alloys of the matrix type. The minimum detection limit of precipitates in the matrix of the base material provided by this technique constitutes as little as 1%. The identification of precipitates in x-ray patterns and their analysis are implemented through a transmission mode with a larger radiation area, longer holding time and higher diffractometer resolution as compared to the conventional reflection mode. The presented technique has been successfully employed to identify and quantitatively describe precipitates formed in the Al alloy of the Al-Mg-Si system as a result of artificial aging. For the first time, the x-ray phase analysis has been used to identify and measure precipitates formed during the alloy artificial aging.

About microcracking due to leaching in cementitious composites: X-ray microtomography description and numerical approach

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rougelot, Thomas; Burlion, Nicolas, E-mail: nicolas.burlion@polytech-lille.f; Bernard, Dominique

2010-02-15

Chemical shock of cement based materials leads to significant degradation of their physical properties. A typical scenario is a calcium leaching due to water (water with very low pH compared with that of pore fluid). The main objective of this paper is to evaluate the evolution of microstructure induced by leaching of a cementitious composite using synchrotron X-ray micro tomography, mainly from an experimental point of view. In this particular case, it was possible to identify cracking induced by leaching. After a description of the degradation mechanism and the X-ray synchrotron microtomographic analysis, numerical simulations are performed in order tomore » show that cracking is induced by an initial pre-stressing of the composite, coupled with decalcification shrinkage and dramatic decrease in tensile strength during leaching. X-ray microtomography analysis allowed to make evidence of an induced microcracking in cementitious material submitted to leaching.« less

X ray microscope assembly and alignment support and advanced x ray microscope design and analysis

NASA Technical Reports Server (NTRS)

Shealy, David L.

1991-01-01

Considerable efforts have been devoted recently to the design, analysis, fabrication, and testing of spherical Schwarzschild microscopes for soft x ray application in microscopy and projection lithography. The spherical Schwarzschild microscope consists of two concentric spherical mirrors configured such that the third order spherical aberration and coma are zero. Since multilayers are used on the mirror substrates for x ray applications, it is desirable to have only two reflecting surfaces in a microscope. In order to reduce microscope aberrations and increase the field of view, generalized mirror surface profiles have been considered in this investigation. Based on incoherent and sine wave modulation transfer function (MTF) calculations, the object plane resolution of a microscope has been analyzed as a function of the object height and numerical aperture (NA) of the primary for several spherical Schwarzschild, conic, and aspherical head reflecting two mirror microscope configurations.

Identification and analysis of structures in the corona from X-ray photography

NASA Technical Reports Server (NTRS)

Vaiana, G. S.; Krieger, A. S.; Timothy, A. F.

1973-01-01

This paper summarizes the results of a program of rocket observations of the solar corona with grazing incidence X-ray telescopes. A series of five flights of a Kanigen-surfaced telescope with a few arc seconds resolution, together with the first flight of a newer telescope have resulted in the identification of six classes of coronal structures observable in the X-ray photographs. These are: active regions, active region interconnections, large loop structures associated with unipolar magnetic regions, coronal holes, coronal bright points, and the structures surrounding filament cavities. Two solar flares have been observed. The methods involved in deriving coronal temperature and density information from X-ray photographs are described and the analysis of a bright active region (McMath plage 11035) observed at the west limb on November 24, 1970 is presented as an example of these techniques.

XMM-Newton confirmation of a new intermediate polar: XMMU J185330.7-012815

NASA Astrophysics Data System (ADS)

Hui, C. Y.; Sriram, K.; Choi, C.-S.

2012-01-01

We report on the results of a detailed spectro-imaging and temporal analysis of an archival XMM-Newton observation of a new intermediate polar XMMU J185330.7-012815. Its X-ray spectrum can be well described by a multitemperature thermal plasma model with the K lines of heavy elements clearly detected. Possible counterparts of XMMU J185330.7-012815 have been identified in optical and ultraviolet (UV) bands. The low values of the inferred X-ray-to-UV and X-ray-to-optical flux ratios safely rule out the possibility of its being an isolated neutron star. We confirm the X-ray periodicity of ˜238 s but, differently from the previous preliminary results, we do not find any convincing evidence of phase shift in this observation. We further investigate its properties through an energy-resolved temporal analysis and find that the pulsed fraction monotonically increases with energy.

Thermal analysis, X-ray powder diffraction and electron microscopy data related with the production of 1:1 Caffeine:Glutaric Acid cocrystals.

PubMed

Duarte, Íris; Andrade, Rita; Pinto, João F; Temtem, Márcio

2016-09-01

The data presented in this article are related to the production of 1:1 Caffeine:Glutaric Acid cocrystals as part of the research article entitled "Green production of cocrystals using a new solvent-free approach by spray congealing" (Duarte et al., 2016) [1]. More specifically, here we present the thermal analysis and the X-ray powder diffraction data for pure Glutaric Acid, used as a raw material in [1]. We also include the X-ray powder diffraction and electron microscopy data obtained for the 1:1 Caffeine:Glutaric Acid cocrystal (form II) produced using the cooling crystallization method reported in "Operating Regions in Cooling Cocrystallization of Caffeine and Glutaric Acid in Acetonitrile" (Yu et al., 2010) [2]. Lastly, we show the X-ray powder diffraction data obtained for assessing the purity of the 1:1 Caffeine:Glutaric cocrystals produced in [1].

Plasma properties of hot coronal loops utilizing coordinated SMM and solar research rocket observations

NASA Technical Reports Server (NTRS)

Moses, J. Daniel

1989-01-01

Three improvements in photographic x-ray imaging techniques for solar astronomy are presented. The testing and calibration of a new film processor was conducted; the resulting product will allow photometric development of sounding rocket flight film immediately upon recovery at the missile range. Two fine grained photographic films were calibrated and flight tested to provide alternative detector choices when the need for high resolution is greater than the need for high sensitivity. An analysis technique used to obtain the characteristic curve directly from photographs of UV solar spectra were applied to the analysis of soft x-ray photographic images. The resulting procedure provides a more complete and straightforward determination of the parameters describing the x-ray characteristic curve than previous techniques. These improvements fall into the category of refinements instead of revolutions, indicating the fundamental suitability of the photographic process for x-ray imaging in solar astronomy.

An XMM-Newton spectral survey of 12 μm selected galaxies - II. Implications for AGN selection and unification

NASA Astrophysics Data System (ADS)

Brightman, Murray; Nandra, Kirpal

2011-07-01

We present a multi-waveband analysis of a 126-galaxy sub-sample of the 12 μm galaxy sample (12MGS), for which we have carried out a detailed X-ray spectral analysis in a previous paper. We determine the activity class of the galaxies by way of optical-line ratio diagnostics and characterize the optical classes by their X-ray, 12 μm and [O III] luminosities and X-ray spectral properties. Our most interesting results from this investigation are as follows. (i) Seyfert (Sy) 1s and Sy2s show a significantly different X-ray luminosity distributions from each other. (ii) Sy2 galaxies with a detection of a hidden broad-line region show a significantly higher X-ray luminosity than those without a detection, supporting the findings of Tran. (iii) Sy1s also present a significantly different 12 μm luminosity distribution from both intermediate Sy types and Sy2s. (iv) The Sy2 fraction decreases towards high X-ray luminosities. (v) X-ray indications of active galactic nuclei (AGN) power agree well with the optical classifications. (vi) There is X-ray evidence for the presence of an AGN in 17 per cent of H II/AGN composite galaxies and 40 per cent of LINERs. (vii) We advocate the use of a 2-10 keV X-ray luminosity of 1041 erg s-1 in the X-ray selection of AGN, rather than 1042 erg s-1, which we find gives a contamination rate of only 3 per cent from star-forming galaxies. (viii) From an analysis of the X-ray power-law index, Γ, we find that Sy1s and Sy2 have the same intrinsic distributions, implying that the central engines are the same, in support of AGN unification schemes. (ix) In 24 per cent of cases the absorption measured in the X-ray spectra does not correspond directly to that implied in the optical band from the visibility of the broad-line regions (BLRs), which is in conflict with AGN unification schemes. (x) We confirm the previous work showing that the obscured fraction in AGN declines at high X-ray luminosity, but also find a decrease at low luminosity having peaked at LX˜ 1042 erg s-1, suggesting that source luminosity has a large effect on the obscuring material, therefore also calling for a modification to unified schemes. (xi) The average obscured and Compton-thick fractions for this sample are 62 ± 5 per cent and 20 ± 4 per cent, respectively, which are higher than hard X-ray and optically selected samples, therefore supporting mid-infrared (MIR) selection as a relatively unbiased method of selecting AGN. (xii) We assess the use of the 'T' ratio (?) for selecting Compton-thick candidates. We conclude here that this quantity can often be unreliable due to uncertainties in the extinction corrections to the [O III] flux. These results have important impacts on AGN selection and unification, and the results from the 12MGS are particularly useful as a local analogue to Spitzer/MIPS 24 μm samples selected at z= 1, as observed 24 μm emission originates at rest-frame 12 μm in sources at this redshift.

Discovery of Oxygen Kalpha X-ray Emission from the Rings of Saturn

NASA Technical Reports Server (NTRS)

Bhardwaj, Anil; Elsner, Ronald F.; Waite, J. Hunter, Jr.; Gladstone, G Randall; Cravens, Thomas E.; Ford, Peter G.

2005-01-01

Using the Advanced CCD Imaging Spectrometer (ACIS), the Chandra X-ray Observatory (CXO) observed the Saturnian system for one rotation of the planet (approx.37 ks) on 20 January, 2004, and again on 26-27 January, 2004. In this letter we report the detection of X-ray emission from the rings of Saturn. The X-ray spectrum from the rings is dominated by emission in a narrow (approx.130 eV wide) energy band centered on the atomic oxygen Ka fluorescence line at 0.53 keV. The X-ray power emitted from the rings in the 0.49-0.62 keV band is about one-third of that emitted from Saturn disk in the photon energy range 0.24-2.0 keV. Our analysis also finds a clear detection of X-ray emission from the rings in the 0.49-0.62 keV band in an earlier (14-15 April, 2003) Chandra ACIS observation of Saturn. Fluorescent scattering of solar X-rays from oxygen atoms in the H20 icy ring material is the likely source mechanism for ring X-rays, consistent with the scenario of solar photo-production of a tenuous ring oxygen atmosphere and ionosphere recently discovered by Cassini.

Winds in collision. II - An analysis of the X-ray emission from the eruptive symbiotic HM Sge

NASA Technical Reports Server (NTRS)

Willson, L. A.; Wallerstein, G.; Brugel, E. W.; Stencel, R. E.

1984-01-01

X-ray emissions from HM Sge obtained in 1981 from the HEAO-2 satellite are analyzed and compared quantitatively with observations of HM Sge made in 1980 and of HM Sge, V 1016 Cyg, and RR Tel made in 1979. The change in the X-ray emission from HM Sge between 1979 and 1981 is found to be consistent with the X-ray luminosity and/or temperature of the emitting region declining with an e-folding timescale of the order of one to several decades. Comparison with X-ray data from V 1016 Cyg and RR Tel gives a composite X-ray light curve that is also consistent with such a decline. A comparison of the X-ray observation with spectroscopic information makes it possible to constrain the properties of the X-ray emitting region: the result is consistent with emission from an optically thin region between the two stars in the system where their winds collide head on. It is also shown that the observations are inconsistent with a stellar (blackbody) source, with emission from an accretion disk around a white dwarf or a neutron star, and with emission from a single star wind from either a white dwarf or a neutron star.

X-Ray Properties of K-Selected Galaxies at 0.5 Less than z Less than 2.0: Investigating Trends with Stellar Mass, Redshift and Spectral Type

NASA Technical Reports Server (NTRS)

Jones, Therese M.; Kriek, Mariska; vanDokkum, Peter G.; Brammer, Gabriel; Franx, Marijn; Greene, Jenny E.; Labbe, Ivo; Whitaker, Katherine E.

2014-01-01

We examine how the total X-ray luminosity correlates with stellar mass, stellar population, and redshift for a K-band limited sample of approximately 3500 galaxies at 0.5 < z < 2.0 from the NEWFIRM Medium Band Survey in the COSMOS field. The galaxy sample is divided into 32 different galaxy types, based on similarities between the spectral energy distributions. For each galaxy type, we further divide the sample into bins of redshift and stellar mass, and perform an X-ray stacking analysis using the Chandra COSMOS data. We find that full band X-ray luminosity is primarily increasing with stellar mass, and at similar mass and spectral type is higher at larger redshifts. When comparing at the same stellar mass, we find that the X-ray luminosity is slightly higher for younger galaxies (i.e., weaker 4000 angstrom breaks), but the scatter in this relation is large. We compare the observed X-ray luminosities to those expected from low- and high-mass X-ray binaries (XRBs). For blue galaxies, XRBs can almost fully account for the observed emission, while for older galaxies with larger 4000 angstrom breaks, active galactic nuclei (AGN) or hot gas dominate the measured X-ray flux. After correcting for XRBs, the X-ray luminosity is still slightly higher in younger galaxies, although this correlation is not significant. AGN appear to be a larger component of galaxy X-ray luminosity at earlier times, as the hardness ratio increases with redshift. Together with the slight increase in X-ray luminosity this may indicate more obscured AGNs or higher accretion rates at earlier times.

Pixel detectors for x-ray imaging spectroscopy in space

NASA Astrophysics Data System (ADS)

Treis, J.; Andritschke, R.; Hartmann, R.; Herrmann, S.; Holl, P.; Lauf, T.; Lechner, P.; Lutz, G.; Meidinger, N.; Porro, M.; Richter, R. H.; Schopper, F.; Soltau, H.; Strüder, L.

2009-03-01

Pixelated semiconductor detectors for X-ray imaging spectroscopy are foreseen as key components of the payload of various future space missions exploring the x-ray sky. Located on the platform of the new Spectrum-Roentgen-Gamma satellite, the eROSITA (extended Roentgen Survey with an Imaging Telescope Array) instrument will perform an imaging all-sky survey up to an X-ray energy of 10 keV with unprecedented spectral and angular resolution. The instrument will consist of seven parallel oriented mirror modules each having its own pnCCD camera in the focus. The satellite born X-ray observatory SIMBOL-X will be the first mission to use formation-flying techniques to implement an X-ray telescope with an unprecedented focal length of around 20 m. The detector instrumentation consists of separate high- and low energy detectors, a monolithic 128 × 128 DEPFET macropixel array and a pixellated CdZTe detector respectively, making energy band between 0.5 to 80 keV accessible. A similar concept is proposed for the next generation X-ray observatory IXO. Finally, the MIXS (Mercury Imaging X-ray Spectrometer) instrument on the European Mercury exploration mission BepiColombo will use DEPFET macropixel arrays together with a small X-ray telescope to perform a spatially resolved planetary XRF analysis of Mercury's crust. Here, the mission concepts and their scientific targets are briefly discussed, and the resulting requirements on the detector devices together with the implementation strategies are shown.

Accurate Modeling of X-ray Extinction by Interstellar Grains

NASA Astrophysics Data System (ADS)

Hoffman, John; Draine, B. T.

2016-02-01

Interstellar abundance determinations from fits to X-ray absorption edges often rely on the incorrect assumption that scattering is insignificant and can be ignored. We show instead that scattering contributes significantly to the attenuation of X-rays for realistic dust grain size distributions and substantially modifies the spectrum near absorption edges of elements present in grains. The dust attenuation modules used in major X-ray spectral fitting programs do not take this into account. We show that the consequences of neglecting scattering on the determination of interstellar elemental abundances are modest; however, scattering (along with uncertainties in the grain size distribution) must be taken into account when near-edge extinction fine structure is used to infer dust mineralogy. We advertise the benefits and accuracy of anomalous diffraction theory for both X-ray halo analysis and near edge absorption studies. We present an open source Fortran suite, General Geometry Anomalous Diffraction Theory (GGADT), that calculates X-ray absorption, scattering, and differential scattering cross sections for grains of arbitrary geometry and composition.

OSO 8 X-ray spectra of clusters of galaxies. II - Discussion

NASA Technical Reports Server (NTRS)

Smith, B. W.; Mushotzky, R. F.; Serlemitsos, P. J.

1979-01-01

An observational description of X-ray clusters of galaxies is given based on OSO 8 X-ray results for spatially integrated spectra of 20 such clusters and various correlations obtained from these results. It is found from a correlation between temperature and velocity dispersion that the X-ray core radius should be less than the galaxy core radius or, alternatively, that the polytropic index is about 1.1 for most of the 20 clusters. Analysis of a correlation between temperature and emission integral yields evidence that more massive clusters accumulate a larger fraction of their mass as intracluster gas. Galaxy densities and optical morphology, as they correlate with X-ray properties, are reexamined for indications as to how mass injection by galaxies affects the density structure of the gas. The physical arguments used to derive iron abundances from observed equivalent widths of iron line features in X-ray spectra are critically evaluated, and the associated uncertainties in abundances derived in this manner are estimated to be quite large.

Infrastructure development for radioactive materials at the NSLS-II

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sprouster, D. J.; Weidner, R.; Ghose, S. K.

2018-02-01

The X-ray Powder Diffraction (XPD) Beamline at the National Synchrotron Light Source-II is a multipurpose instrument designed for high-resolution, high-energy X-ray scattering techniques. In this article, the capabilities, opportunities and recent developments in the characterization of radioactive materials at XPD are described. The overarching goal of this work is to provide researchers access to advanced synchrotron techniques suited to the structural characterization of materials for advanced nuclear energy systems. XPD is a new beamline providing high photon flux for X-ray Diffraction, Pair Distribution Function analysis and Small Angle X-ray Scattering. The infrastructure and software described here extend the existing capabilitiesmore » at XPD to accommodate radioactive materials. Such techniques will contribute crucial information to the characterization and quantification of advanced materials for nuclear energy applications. We describe the automated radioactive sample collection capabilities and recent X-ray Diffraction and Small Angle X-ray Scattering results from neutron irradiated reactor pressure vessel steels and oxide dispersion strengthened steels.« less

Results from OSO-IV - The long term behavior of X-ray emitting regions.

NASA Technical Reports Server (NTRS)

Krieger, A.; Paolini, F.; Vaiana, G. S.; Webb, D.

1972-01-01

Analysis of images of the sun obtained with the aid of a grazing incidence X-ray telescope on board the OSO IV spacecraft in the 2.5 to 12-A waveband nearly continuously from Oct. 27, 1967, to May 12, 1968. The instrument had sufficient spatial resolution (one and four arc minutes) and temporal resolution (5 to 20 min) to estimate the spatial characteristics of X-ray emitting regions and to monitor the temporal behavior of individual active regions. Variations in the absence of flares of as much as a factor of 10 in the X-ray output of individual regions were observed, with typical durations ranging from several hours to several days. The X-ray time variations are related to observations at optical and radio wavelengths. The results are interpreted under the assumption that the X-ray time variations are caused by temperature changes in the coronal portions of active regions. The contribution of radiative losses to the energy budget of the coronal active region is estimated.

Laboratory Measurements of X-Ray Emissions From Centimeter-Long Streamer Corona Discharges

NASA Astrophysics Data System (ADS)

da Silva, C. L.; Millan, R. M.; McGaw, D. G.; Yu, C. T.; Putter, A. S.; LaBelle, J.; Dwyer, J.

2017-11-01

We provide extensive evidence that runaway electron acceleration and subsequent bremsstrahlung X-ray emission are a common feature in negative electrical discharges with voltages as low as 100 kV, indicating that all negative lightning could potentially produce runaway electrons. Centimeter long streamer corona discharges produce bursts of X-ray radiation, emitted by a source highly compact in space and time, leading to photon pileup. Median photon burst energies vary between 33 and 96 keV in 100 kV discharges. Statistical analysis of 5,000+ discharges shows that X-rays are observed in as many as 60% of the triggers, depending on the configuration. X-ray detection is more frequent when streamers are not followed by a spark, the detector is oriented perpendicular to the gap, and a thicker anode is used. In an 8-cm-long gap, X-rays are produced when runaway electrons hit the anode, and the electron acceleration is not necessarily correlated with streamer collisions.

Optics for coherent X-ray applications.

PubMed

Yabashi, Makina; Tono, Kensuke; Mimura, Hidekazu; Matsuyama, Satoshi; Yamauchi, Kazuto; Tanaka, Takashi; Tanaka, Hitoshi; Tamasaku, Kenji; Ohashi, Haruhiko; Goto, Shunji; Ishikawa, Tetsuya

2014-09-01

Developments of X-ray optics for full utilization of diffraction-limited storage rings (DLSRs) are presented. The expected performance of DLSRs is introduced using the design parameters of SPring-8 II. To develop optical elements applicable to manipulation of coherent X-rays, advanced technologies on precise processing and metrology were invented. With propagation-based coherent X-rays at the 1 km beamline of SPring-8, a beryllium window fabricated with the physical-vapour-deposition method was found to have ideal speckle-free properties. The elastic emission machining method was utilized for developing reflective mirrors without distortion of the wavefronts. The method was further applied to production of diffraction-limited focusing mirrors generating the smallest spot size in the sub-10 nm regime. To enable production of ultra-intense nanobeams at DLSRs, a low-vibration cooling system for a high-heat-load monochromator and advanced diagnostic systems to characterize X-ray beam properties precisely were developed. Finally, new experimental schemes for combinative nano-analysis and spectroscopy realised with novel X-ray optics are discussed.

Spectral structure of a polycapillary lens shaped X-ray beam

NASA Astrophysics Data System (ADS)

Gogolev, A. S.; Filatov, N. A.; Uglov, S. R.; Hampai, D.; Dabagov, S. B.

2018-04-01

Polycapillary X-ray optics is widely used in X-ray analysis techniques to create a small secondary source, for instance, or to deliver X-rays to the point of interest with minimum intensity losses [1]. The main characteristics of the analytical devices on its base are the size and divergence of the focused or translated beam. In this work, we used the photon-counting pixel detector ModuPIX to study the parameters for polycapillary focused X-ray tube radiation as well as the energy and spatial dependences of radiation at the focus. We have characterized the high-speed spectral camera ModuPIX, which is a single Timepix device with a fast parallel readout allowing up to 850 frames per second with 256 × 256 pixels and a 55 μm pitch defined by the frame frequency. By means of the silicon monochromator the energy response function is measured in clustering mode by the energy scan over total X-ray tube spectrum.

Infrastructure development for radioactive materials at the NSLS-II

DOE PAGES

Sprouster, David J.; Weidner, R.; Ghose, S. K.; ...

2017-11-04

The X-ray Powder Diffraction (XPD) Beamline at the National Synchrotron Light Source-II is a multipurpose instrument designed for high-resolution, high-energy X-ray scattering techniques. In this paper, the capabilities, opportunities and recent developments in the characterization of radioactive materials at XPD are described. The overarching goal of this work is to provide researchers access to advanced synchrotron techniques suited to the structural characterization of materials for advanced nuclear energy systems. XPD is a new beamline providing high photon flux for X-ray Diffraction, Pair Distribution Function analysis and Small Angle X-ray Scattering. The infrastructure and software described here extend the existing capabilitiesmore » at XPD to accommodate radioactive materials. Such techniques will contribute crucial information to the characterization and quantification of advanced materials for nuclear energy applications. Finally, we describe the automated radioactive sample collection capabilities and recent X-ray Diffraction and Small Angle X-ray Scattering results from neutron irradiated reactor pressure vessel steels and oxide dispersion strengthened steels.« less

Luminosity function and cosmological evolution of X-ray selected quasars

NASA Technical Reports Server (NTRS)

Maccacaro, T.; Gioia, I. M.

1983-01-01

The preliminary analysis of a complete sample of 55 X-ray sources is presented as part of the Medium Sensitivity Survey of the Einstein Observatory. A pure luminosity evolutionary law is derived in order to determine the uniform distribution of the sources and the rates of evolution for Active Galactic Nuclei (AGNs) observed by X-ray and optical techniques are compared. A nonparametric representation of the luminosity function is fitted to the observational data. On the basis of the reduced data, it is determined that: (1) AGNs evolve cosmologically; (2) less evolution is required to explain the X-ray data than the optical data; (3) the high-luminosity portion of the X-ray luminosity can be described by a power-law with a slope of gamma = 3.6; and (4) the X-ray luminosity function flattens at low luminosities. Some of the implications of the results for conventional theoretical models of the evolution of quasars and Seyfert galaxies are discussed.

An Inquiry-Based Project Focused on the X-Ray Powder Diffraction Analysis of Common Household Solids

ERIC Educational Resources Information Center

Hulien, Molly L.; Lekse, Jonathan W.; Rosmus, Kimberly A.; Devlin, Kasey P.; Glenn, Jennifer R.; Wisneski, Stephen D.; Wildfong, Peter; Lake, Charles H.; MacNeil, Joseph H.; Aitken, Jennifer A.

2015-01-01

While X-ray powder diffraction (XRPD) is a fundamental analytical technique used by solid-state laboratories across a breadth of disciplines, it is still underrepresented in most undergraduate curricula. In this work, we incorporate XRPD analysis into an inquiry-based project that requires students to identify the crystalline component(s) of…

Aerogel as a Sample Collector and Sample Mount for Transmission XRD Analysis

NASA Technical Reports Server (NTRS)

Bish, D. L.; Vaniman, D. T.; Chipera, S. J.; Yen, A. S.; Jones, S. M.

2001-01-01

Silica aerogel can be used for dust collection and in situ X-ray analysis. Aerogels can be less absorbing than Be, and it is feasible to obtain X-ray transmission factors >50% using typical aerogels together with a 100-micrometer Be backing foil. Additional information is contained in the original extended abstract.

Soft X-ray astronomy using grazing incidence optics

NASA Technical Reports Server (NTRS)

Davis, John M.

1989-01-01

The instrumental background of X-ray astronomy with an emphasis on high resolution imagery is outlined. Optical and system performance, in terms of resolution, are compared and methods for improving the latter in finite length instruments described. The method of analysis of broadband images to obtain diagnostic information is described and is applied to the analysis of coronal structures.

X-ray peak profile analysis of zinc oxide nanoparticles formed by simple precipitation method

NASA Astrophysics Data System (ADS)

Pelicano, Christian Mark; Rapadas, Nick Joaquin; Magdaluyo, Eduardo

2017-12-01

Zinc oxide (ZnO) nanoparticles were successfully synthesized by a simple precipitation method using zinc acetate and tetramethylammonium hydroxide. The synthesized ZnO nanoparticles were characterized by X-ray Diffraction analysis (XRD) and Transmission Electron Microscopy (TEM). The XRD result revealed a hexagonal wurtzite structure for the ZnO nanoparticles. The TEM image showed spherical nanoparticles with an average crystallite size of 6.70 nm. For x-ray peak analysis, Williamson-Hall (W-H) and Size-Strain Plot (SSP) methods were applied to examine the effects of crystallite size and lattice strain on the peak broadening of the ZnO nanoparticles. Based on the calculations, the estimated crystallite sizes and lattice strains obtained are in good agreement with each other.

Argon content of the Martian atmosphere at the Viking 1 landing site - Analysis by X-ray fluorescence spectroscopy

NASA Technical Reports Server (NTRS)

Clark, B. C.; Toulmin, P., III; Rose, H. J., Jr.; Baird, A. K.; Keil, K.

1976-01-01

Spectra provided by the Viking 1 X-ray fluorescence spectrometer operating in the calibration mode (without a soil sample in the analysis chamber) were analyzed to determine the argon content of the Martian atmosphere at the landing site. This was found to be less than or equal to 0.15 millibar, or not more than 2% by volume, consistent with data obtained by the entry mass spectrometer and by the mass spectrometer on the lander. It is anticipated that analysis of the K content of surface samples using X-ray fluorescence data will provide information on the evolution of the atmosphere, since most atmospheric argon is apparently produced by decay of K-40.

Fluorescence imaging of reactive oxygen species by confocal laser scanning microscopy for track analysis of synchrotron X-ray photoelectric nanoradiator dose: X-ray pump-optical probe.

PubMed

Jeon, Jae Kun; Han, Sung Mi; Kim, Jong Ki

2016-09-01

Bursts of emissions of low-energy electrons, including interatomic Coulomb decay electrons and Auger electrons (0-1000 eV), as well as X-ray fluorescence produced by irradiation of large-Z element nanoparticles by either X-ray photons or high-energy ion beams, is referred to as the nanoradiator effect. In therapeutic applications, this effect can damage pathological tissues that selectively take up the nanoparticles. Herein, a new nanoradiator dosimetry method is presented that uses probes for reactive oxygen species (ROS) incorporated into three-dimensional gels, on which macrophages containing iron oxide nanoparticles (IONs) are attached. This method, together with site-specific irradiation of the intracellular nanoparticles from a microbeam of polychromatic synchrotron X-rays (5-14 keV), measures the range and distribution of OH radicals produced by X-ray emission or superoxide anions ({\\rm{O}}_2^-) produced by low-energy electrons. The measurements are based on confocal laser scanning of the fluorescence of the hydroxyl radical probe 2-[6-(4'-amino)phenoxy-3H-xanthen-3-on-9-yl] benzoic acid (APF) or the superoxide probe hydroethidine-dihydroethidium (DHE) that was oxidized by each ROS, enabling tracking of the radiation dose emitted by the nanoradiator. In the range 70 µm below the irradiated cell, ^\\bullet{\\rm{OH}} radicals derived mostly from either incident X-ray or X-ray fluorescence of ION nanoradiators are distributed along the line of depth direction in ROS gel. In contrast, {\\rm{O}}_2^- derived from secondary electron or low-energy electron emission by ION nanoradiators are scattered over the ROS gel. ROS fluorescence due to the ION nanoradiators was observed continuously to a depth of 1.5 mm for both oxidized APF and oxidized DHE with relatively large intensity compared with the fluorescence caused by the ROS produced solely by incident primary X-rays, which was limited to a depth of 600 µm, suggesting dose enhancement as well as more penetration by nanoradiators. In conclusion, the combined use of a synchrotron X-ray microbeam-irradiated three-dimensional ROS gel and confocal laser scanning fluorescence microscopy provides a simple dosimetry method for track analysis of X-ray photoelectric nanoradiator radiation, suggesting extensive cellular damage with dose-enhancement beyond a single cell containing IONs.

Infrared and X-Ray Spectroscopy of the Kes 75 Supernova Remnant Shell: Characterizing the Dust and Gas Properties

NASA Astrophysics Data System (ADS)

Temim, Tea; Slane, Patrick; Arendt, Richard G.; Dwek, Eli

2012-01-01

We present deep Chandra observations and Spitzer Space Telescope infrared (IR) spectroscopy of the shell in the composite supernova remnant (SNR) Kes 75 (G29.7-0.3). The remnant is composed of a central pulsar wind nebula and a bright partial shell in the south that is visible at radio, IR, and X-ray wavelengths. The X-ray emission can be modeled by either a single thermal component with a temperature of ~1.5 keV, or with two thermal components with temperatures of 1.5 and 0.2 keV. Previous studies suggest that the hot component may originate from reverse-shocked supernova (SN) ejecta. However, our new analysis shows no definitive evidence for enhanced abundances of Si, S, Ar, Mg, and Fe, as expected from SN ejecta, or for the IR spectral signatures characteristic of confirmed SN condensed dust, thus favoring a circumstellar or interstellar origin for the X-ray and IR emission. The X-ray and IR emission in the shell are spatially correlated, suggesting that the dust particles are collisionally heated by the X-ray emitting gas. The IR spectrum of the shell is dominated by continuum emission from dust with little, or no line emission. Modeling the IR spectrum shows that the dust is heated to a temperature of ~140 K by a relatively dense, hot plasma that also gives rise to the hot X-ray emission component. The density inferred from the IR emission is significantly higher than the density inferred from the X-ray models, suggesting a low filling factor for this X-ray emitting gas. The total mass of the warm dust component is at least 1.3 × 10-2 M ⊙, assuming no significant dust destruction has occurred in the shell. The IR data also reveal the presence of an additional plasma component with a cooler temperature, consistent with the 0.2 keV gas component. Our IR analysis therefore provides an independent verification of the cooler component of the X-ray emission. The complementary analyses of the X-ray and IR emission provide quantitative estimates of density and filling factors of the clumpy medium swept up by the SNR.

High resolution energy-angle correlation measurement of hard x rays from laser-Thomson backscattering.

PubMed

Jochmann, A; Irman, A; Bussmann, M; Couperus, J P; Cowan, T E; Debus, A D; Kuntzsch, M; Ledingham, K W D; Lehnert, U; Sauerbrey, R; Schlenvoigt, H P; Seipt, D; Stöhlker, Th; Thorn, D B; Trotsenko, S; Wagner, A; Schramm, U

2013-09-13

Thomson backscattering of intense laser pulses from relativistic electrons not only allows for the generation of bright x-ray pulses but also for the investigation of the complex particle dynamics at the interaction point. For this purpose a complete spectral characterization of a Thomson source powered by a compact linear electron accelerator is performed with unprecedented angular and energy resolution. A rigorous statistical analysis comparing experimental data to 3D simulations enables, e.g., the extraction of the angular distribution of electrons with 1.5% accuracy and, in total, provides predictive capability for the future high brightness hard x-ray source PHOENIX (photon electron collider for narrow bandwidth intense x rays) and potential gamma-ray sources.

The Ultraluminous X-Ray Source X-37 Is a Background Quasar in the Antennae Galaxies

NASA Astrophysics Data System (ADS)

Clark, D. M.; Christopher, M. H.; Eikenberry, S. S.; Brandl, B. R.; Wilson, J. C.; Carson, J. C.; Henderson, C. P.; Hayward, T. L.; Barry, D. J.; Ptak, A. F.; Colbert, E. J. M.

2005-10-01

In this Letter we report that a bright, X-ray source in the Antennae galaxies (NGC 4038/9), previously identified as an ultraluminous X-ray source (ULX), is in fact a background quasar. We identify an isolated infrared and optical counterpart within 0.3" +/- 0.5" of the X-ray source X-37. After acquiring an optical spectrum of its counterpart, we use the narrow [O III] and broad Hα emission lines to identify X-37 as a quasar at a redshift of z=0.26. Through a U, V, and Ks photometric analysis, we demonstrate that most of the observable light along this line of sight is from the quasar. We discuss the implications of this discovery and the importance of acquiring spectra for optical and IR counterparts to ULXs.

Analysis of X-ray and EUV spectra of solar active regions

NASA Technical Reports Server (NTRS)

Strong, K. T.; Acton, L. W.

1979-01-01

Data acquired by two flights of an array of six Bragg crystal spectrometers on an Aerobee rocket to obtain high spatial and spectral resolution observations of various coronal features at soft X-ray wavelengths (9-23A) were analyzed. The various aspects of the analysis of the X-ray data are described. These observations were coordinated with observations from the experiments on the Apollo Telescope Mount and the various data sets were related to one another. The Appendices contain the published results, abstracts of papers, computer code descriptions and preprints of papers, all produced as a result of this research project.