Evaluation of the sensitivity and fading characteristics of an image plate system for x-ray diagnostics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Meadowcroft, A. L.; Bentley, C. D.; Stott, E. N.

2008-11-15

Image plates (IPs) are a reusable recording media capable of detecting ionizing radiation, used to diagnose x-ray emission from laser-plasma experiments. Due to their superior performance characteristics in x-ray applications [C. C. Bradford, W. W. Peppler, and J. T. Dobbins III, Med. Phys. 26, 27 (1999) and J. Digit. Imaging. 12, 54 (1999)], the Fuji Biological Analysis System (BAS) IPs are fielded on x-ray diagnostics for the HELEN laser by the Plasma Physics Department at AWE. The sensitivities of the Fuji BAS IPs have been absolutely calibrated for absolute measurements of x-ray intensity in the energy range of 0-100 keV.more » In addition, the Fuji BAS IP fading as a function of time was investigated. We report on the characterization of three Fuji BAS IP responses to x-rays using a radioactive source, and discrete x-ray line energies generated by the Excalibur soft x-ray facility and the Defense Radiological Standards Centre filter-fluorescer hard x-ray system at AWE.« less

Control Scheme for Quickly Starting X-ray Tube

NASA Astrophysics Data System (ADS)

Nakahama, Masayuki; Nakanishi, Toshiki; Ishitobi, Manabu; Ito, Tuyoshi; Hosoda, Kenichi

A control scheme for quickly starting a portable X-ray generator used in the livestock industry is proposed in this paper. A portable X-ray generator used to take X-ray images of animals such as horses, sheep and dogs should be capable of starting quickly because it is difficult for veterinarians to take X-ray images of animals at their timing. In order to develop a scheme for starting the X-ray tube quickly, it is necessary to analysis the X-ray tube. However, such an analysis has not been discussed until now. First, the states of an X-ray tube are classified into the temperature-limited state and the space-charge-limited state. Furthermore, existence of “mixed state” that comprises both is newly proposed in this paper. From these analyses, a novel scheme for quickly starting an X-ray generator is proposed; this scheme is considered with the characteristics of the X-ray tube. The proposed X-ray system that is capable of starting quickly is evaluated on the basis of experimental results.

Remote X-Ray Diffraction and X-Ray Fluorescence Analysis on Planetary Surfaces

NASA Technical Reports Server (NTRS)

Blake, David F.; DeVincenzi, D. (Technical Monitor)

1999-01-01

The legacy of planetary X-ray Diffraction (XRD) and X-ray Fluorescence (XRF) began in 1960 when W. Parish proposed an XRD instrument for deployment on the moon. The instrument was built and flight qualified, but the Lunar XRD program was cancelled shortly before the first human landing in 1969. XRF chemical data have been collected in situ by surface landers on Mars (Viking 1 & 2, Pathfinder) and Venus (Venera 13 & 14). These highly successful experiments provide critical constraints on our current understanding of surface processes and planetary evolution. However, the mineralogy, which is more critical to planetary surface science than simple chemical analysis, will remain unknown or will at best be imprecisely constrained until X-ray diffraction (XRD) data are collected. Recent progress in X-ray detector technology allows the consideration of simultaneous XRD (mineralogic analysis) and high-precision XRF (elemental analysis) in systems miniaturized to the point where they can be mounted on fixed landers or small robotic rovers. There is a variety of potential targets for XRD/XRF equipped landers within the solar system, the most compelling of which are the poles of the moon, the southern highlands of Mars and Europa.

An airport cargo inspection system based on X-ray and thermal neutron analysis (TNA).

PubMed

Ipe, Nisy E; Akery, A; Ryge, P; Brown, D; Liu, F; Thieu, J; James, B

2005-01-01

A cargo inspection system incorporating a high-resolution X-ray imaging system with a material-specific detection system based on Ancore Corporation's patented thermal neutron analysis (TNA) technology can detect bulk quantities of explosives and drugs concealed in trucks or cargo containers. The TNA process utilises a 252Cf neutron source surrounded by a moderator. The neutron interactions with the inspected object result in strong and unique gamma-ray signals from nitrogen, which is a key ingredient in modern high explosives, and from chlorinated drugs. The TNA computer analyses the gamma-ray signals and automatically determines the presence of explosives or drugs. The radiation source terms and shielding design of the facility are described. For the X-ray generator, the primary beam, leakage radiation, and scattered primary and leakage radiation were considered. For the TNA, the primary neutrons and tunnel scattered neutrons as well as the neutron-capture gamma rays were considered.

[Contrast of Z-Pinch X-Ray Yield Measure Technique].

PubMed

Li, Mo; Wang, Liang-ping; Sheng, Liang; Lu, Yi

2015-03-01

Resistive bolometer and scintillant detection system are two mainly Z-pinch X-ray yield measure techniques which are based on different diagnostic principles. Contrasting the results from two methods can help with increasing precision of X-ray yield measurement. Experiments with different load material and shape were carried out on the "QiangGuang-I" facility. For Al wire arrays, X-ray yields measured by the two techniques were largely consistent. However, for insulating coating W wire arrays, X-ray yields taken from bolometer changed with load parameters while data from scintillant detection system hardly changed. Simulation and analysis draw conclusions as follows: (1) Scintillant detection system is much more sensitive to X-ray photons with low energy and its spectral response is wider than the resistive bolometer. Thus, results from the former method are always larger than the latter. (2) The responses of the two systems are both flat to Al plasma radiation. Thus, their results are consistent for Al wire array loads. (3) Radiation form planar W wire arrays is mainly composed of sub-keV soft X-ray. X-ray yields measured by the bolometer is supposed to be accurate because of the nickel foil can absorb almost all the soft X-ray. (4) By contrast, using planar W wire arrays, data from scintillant detection system hardly change with load parameters. A possible explanation is that while the distance between wires increases, plasma temperature at stagnation reduces and spectra moves toward the soft X-ray region. Scintillator is much more sensitive to the soft X-ray below 200 eV. Thus, although the total X-ray yield reduces with large diameter load, signal from the scintillant detection system is almost the same. (5) Both Techniques affected by electron beams produced by the loads.

Sealed-tube synthesis and phase diagram of Li{sub x}TiS{sub 2} (0 ≤ x ≤1)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Ziping; National Laboratory for Superconductivity, Institute of Physics, Chinese Academy of Science, Beijing 100190; Dong, Cheng, E-mail: chengdon@aphy.iphy.ac.cn

2015-01-15

Graphical abstract: We reported a new method to prepare Li{sub x}TiS{sub 2} (0 ≤ x ≤ 1) at 600 °C in sealed tube using Li{sub 2}S aslithium source. A schematic phase diagram of the Li{sub x}TiS{sub 2} system has been constructed based on the DTA and XRD data. - Abstract: We reported a new method to prepare Li{sub x}TiS{sub 2} (0 ≤ x ≤ 1) at 600 °C in sealed tube using Li{sub 2}S as lithium source. The Li{sub x}TiS{sub 2} samples were characterized by powder X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectroscopy, and differential thermal analysis. Themore » variations of the lattice parameters with lithium content x in Li{sub x}TiS{sub 2} were determined by X-ray powder diffraction analysis for both 1T and 3R phases. The phase transition between low-temperature 1T phase and high-temperature 3R phase was confirmed by the powder X-ray diffraction analysis. Based on the differential thermal analysis and X-ray diffraction results, a schematic phase diagram of the Li{sub x}TiS{sub 2} system has been constructed, providing a guideline to synthesize Li{sub x}TiS{sub 2} in 1T structure or 3R structure.« less

TES X-ray microcalorimeters for X-ray astronomy and material analysis

NASA Astrophysics Data System (ADS)

Mitsuda, Kazuhisa

2016-11-01

TES X-ray microcalorimeter arrays provide not only high-energy resolution (FWHM < 10eV) in X-ray spectroscopy but also imaging and high-counting-rate capabilities. They are very promising spectrometer for X-ray astronomy and material analysis. In this paper, we report our recent progress. For material analysis, we have fabricated 8 × 8 format array with a fast signal response ( 40 μs) and proved the energy resolution of 5.8 eV FWHM at 5.9 keV. We developed common biasing scheme to reduce number of wirings from room temperature to the cryogenic stage. From measurements using the newly-designed common-bias SQUID array amplifier chips, and from numerical simulations, we demonstrated that signal cross talks due to the common bias is enough small. For space applications, we are developing frequency-division signal multiplexing system. We have fabricated a baseband feedback system and demonstrated that the noise added by the feedback system is about 4 eV FWHM equivalent for 16 ch multiplexing system. The digital to analog converter (DAC) dominates the noise, and needs be reduced by a factor of four for future astronomy missions.

[Characteristics of specifications of transportable inverter-type X-ray equipment].

PubMed

Yamamoto, Keiichi; Miyazaki, Shigeru; Asano, Hiroshi; Shinohara, Fuminori; Ishikawa, Mitsuo; Ide, Toshinori; Abe, Shinji; Negishi, Toru; Miyake, Hiroyuki; Imai, Yoshio; Okuaki, Tomoyuki

2003-07-01

Our X-ray systems study group measured and examined the characteristics of four transportable inverter-type X-ray equipments. X-ray tube voltage and X-ray tube current were measured with the X-ray tube voltage and the X-ray tube current measurement terminals provided with the equipment. X-ray tube voltage, irradiation time, and dose were measured with a non-invasive X-ray tube voltage-measuring device, and X-ray output was measured by fluorescence meter. The items investigated were the reproducibility and linearity of X-ray output, error of pre-set X-ray tube voltage and X-ray tube current, and X-ray tube voltage ripple percentage. The waveforms of X-ray tube voltage, the X-ray tube current, and fluorescence intensity draw were analyzed using the oscilloscope gram and a personal computer. All of the equipment had a preset error of X-ray tube voltage and X-ray tube current that met JIS standards. The X-ray tube voltage ripple percentage of each equipment conformed to the tendency to decrease when X-ray tube voltage increased. Although the X-ray output reproducibility of system A exceeded the JIS standard, the other systems were within the JIS standard. Equipment A required 40 ms for X-ray tube current to reach the target value, and there was some X-ray output loss because of a trough in X-ray tube current. Owing to the influence of the ripple in X-ray tube current, the strength of the fluorescence waveform rippled in equipments B and C. Waveform analysis could not be done by aliasing of the recording device in equipment D. The maximum X-ray tube current of transportable inverter-type X-ray equipment is as low as 10-20 mA, and the irradiation time of chest X-ray photography exceeds 0.1 sec. However, improvement of the radiophotographic technique is required for patients who cannot move their bodies or halt respiration. It is necessary to make the irradiation time of the equipments shorter for remote medical treatment.

A nearly on-axis spectroscopic system for simultaneously measuring UV-visible absorption and X-ray diffraction in the SPring-8 structural genomics beamline.

PubMed

Sakaguchi, Miyuki; Kimura, Tetsunari; Nishida, Takuma; Tosha, Takehiko; Sugimoto, Hiroshi; Yamaguchi, Yoshihiro; Yanagisawa, Sachiko; Ueno, Go; Murakami, Hironori; Ago, Hideo; Yamamoto, Masaki; Ogura, Takashi; Shiro, Yoshitsugu; Kubo, Minoru

2016-01-01

UV-visible absorption spectroscopy is useful for probing the electronic and structural changes of protein active sites, and thus the on-line combination of X-ray diffraction and spectroscopic analysis is increasingly being applied. Herein, a novel absorption spectrometer was developed at SPring-8 BL26B2 with a nearly on-axis geometry between the X-ray and optical axes. A small prism mirror was placed near the X-ray beamstop to pass the light only 2° off the X-ray beam, enabling spectroscopic analysis of the X-ray-exposed volume of a crystal during X-ray diffraction data collection. The spectrometer was applied to NO reductase, a heme enzyme that catalyzes NO reduction to N2O. Radiation damage to the heme was monitored in real time during X-ray irradiation by evaluating the absorption spectral changes. Moreover, NO binding to the heme was probed via caged NO photolysis with UV light, demonstrating the extended capability of the spectrometer for intermediate analysis.

Multilayer X-ray imaging systems

NASA Astrophysics Data System (ADS)

Shealy, D. L.; Hoover, R. B.; Gabardi, D. R.

1986-01-01

An assessment of the imaging properties of multilayer X-ray imaging systems with spherical surfaces has been made. A ray trace analysis was performed to investigate the effects of using spherical substrates (rather than the conventional paraboloidal/hyperboloidal contours) for doubly reflecting Cassegrain telescopes. These investigations were carried out for mirrors designed to operate at selected soft X-ray/XUV wavelengths that are of significance for studies of the solar corona/transition region from the Stanford/MSFC Rocket X-Ray Telescope. The effects of changes in separation of the primary and secondary elements were also investigated. These theoretical results are presented as well as the results of ray trace studies to establish the resolution and vignetting effects as a function of field angle and system parameters.

A first evaluation of the analytical capabilities of the new X-ray fluorescence facility at International Atomic Energy Agency-Elettra Sincrotrone Trieste for multipurpose total reflection X-ray fluorescence analysis

NASA Astrophysics Data System (ADS)

Marguí, Eva; Hidalgo, Manuela; Migliori, Alessandro; Leani, Juan José; Queralt, Ignasi; Kallithrakas-Kontos, Nikolaos; Streli, Christina; Prost, Josef; Karydas, Andreas Germanos

2018-07-01

The aim of the work is to present a systematic evaluation of the analytical capabilities of the new X-ray fluorescence facility jointly operated between the International Atomic Energy Agency and the Elettra Sincrotrone Trieste for multipurpose total reflection X-ray fluorescence analysis. The analytical performance of the XRF beamline end-station (IAEAXspe) was systematically evaluated under TXRF excitation geometry by analyzing different types of aqueous (lake, waste and fresh water) and solid (soil, vegetal, biological) certified reference materials using an excitation energy of 13.0 keV (for the purpose of multielemental analysis). The results obtained for both types of samples in terms of limits of detection and accuracy were also compared with those obtained using laboratory X-ray tube based TXRF systems with different features (including Mo and W X-ray tube systems). Taking advantage of the possibility to work under high vacuum, the IAEAXspe set-up instrumental sensitivity was also determined using an excitation energy of 6.2 keV to explore the possibilities for light elements determination. A clear improvement of the element detection limits is achieved when comparing this facility to conventional X-ray tube based TXRF systems highlighting the benefits of using the monoenergetic synchrotron exciting radiation and the ultra-high vacuum chamber in comparison with conventional laboratory systems. The results of the present work are discussed in view of further exploitation of the facility for different environmental and biological related applications.

Design of a normal incidence multilayer imaging x-ray microscope.

PubMed

Shealy, D L; Gabardi, D R; Hoover, R B; Walker, A B; Lindblom, J F; Barbee, T W

1989-01-01

Normal incidence multilayer Cassegrain x-ray telescopes were flown on the Stanford/MSFC Rocket X-Ray Spectroheliograph. These instruments produced high spatial resolution images of the Sun and conclusively demonstrated that doubly reflecting multilayer x-ray optical systems are feasible. The images indicated that aplanatic imaging soft x-ray /EUV microscopes should be achievable using multilayer optics technology. We have designed a doubly reflecting normal incidence multilayer imaging x-ray microscope based on the Schwarzschild configuration. The Schwarzschild microscope utilizes two spherical mirrors with concentric radii of curvature which are chosen such that the third-order spherical aberration and coma are minimized. We discuss the design of the microscope and the results of the optical system ray trace analysis which indicates that diffraction-limited performance with 600 Å spatial resolution should be obtainable over a 1 mm field of view at a wavelength of 100 Å. Fabrication of several imaging soft x-ray microscopes based upon these designs, for use in conjunction with x-ray telescopes and laser fusion research, is now in progress. High resolution aplanatic imaging x-ray microscopes using normal incidence multilayer x-ray mirrors should have many important applications in advanced x-ray astronomical instrumentation, x-ray lithography, biological, biomedical, metallurgical, and laser fusion research.

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

21 CFR 892.5900 - X-ray radiation therapy system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false X-ray radiation therapy system. 892.5900 Section 892.5900 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES...-rays used for radiation therapy. This generic type of device may include signal analysis and display...

Observation of X-ray eclipses from LMC X-4

NASA Technical Reports Server (NTRS)

Li, F.; Rappaport, S.; Epstein, A.

1978-01-01

Observations made with the Rotation Modulation Collimator system (RMC) have revealed that X-ray source X-4 in the Large Magellanic Cloud (LMC X-4) is most likely part of a binary system. An analysis of the star's coordinates is presented, with attention given to orbital period and flux intensity variations. Stellar mass and orbital inclination angle are estimated for both X-4 and its companion star.

Improving material identification by combining x-ray and neutron tomography

NASA Astrophysics Data System (ADS)

LaManna, Jacob M.; Hussey, Daniel S.; Baltic, Eli; Jacobson, David L.

2017-09-01

X-rays and neutrons provide complementary non-destructive probes for the analysis of structure and chemical composition of materials. Contrast differences between the modes arise due to the differences in interaction with matter. Due to the high sensitivity to hydrogen, neutrons excel at separating liquid water or hydrogenous phases from the underlying structure while X-rays resolve the solid structure. Many samples of interest, such as fluid flow in porous materials or curing concrete, are stochastic or slowly changing with time which makes analysis of sequential imaging with X-rays and neutrons difficult as the sample may change between scans. To alleviate this issue, NIST has developed a system for simultaneous X-ray and neutron tomography by orienting a 90 keVpeak micro-focus X-ray tube orthogonally to a thermal neutron beam. This system allows for non-destructive, multimodal tomography of dynamic or stochastic samples while penetrating through sample environment equipment such as pressure and flow vessels. Current efforts are underway to develop methods for 2D histogram based segmentation of reconstructed volumes. By leveraging the contrast differences between X-rays and neutrons, greater histogram peak separation can occur in 2D vs 1D enabling improved material identification.

A whole-system approach to x-ray spectroscopy in cargo inspection systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Langeveld, Willem G. J.; Gozani, Tsahi; Ryge, Peter

The bremsstrahlung x-ray spectrum used in high-energy, high-intensity x-ray cargo inspection systems is attenuated and modified by the materials in the cargo in a Z-dependent way. Therefore, spectroscopy of the detected x rays yields information about the Z of the x-rayed cargo material. It has previously been shown that such ZSpectroscopy (Z-SPEC) is possible under certain circumstances. A statistical approach, Z-SCAN (Z-determination by Statistical Count-rate ANalysis), has also been shown to be effective, and it can be used either by itself or in conjunction with Z-SPEC when the x-ray count rate is too high for individual x-ray spectroscopy. Both techniquesmore » require fast x-ray detectors and fast digitization electronics. It is desirable (and possible) to combine all techniques, including x-ray imaging of the cargo, in a single detector array, to reduce costs, weight, and overall complexity. In this paper, we take a whole-system approach to x-ray spectroscopy in x-ray cargo inspection systems, and show how the various parts interact with one another. Faster detectors and read-out electronics are beneficial for both techniques. A higher duty-factor x-ray source allows lower instantaneous count rates at the same overall x-ray intensity, improving the range of applicability of Z-SPEC in particular. Using an intensity-modulated advanced x-ray source (IMAXS) allows reducing the x-ray count rate for cargoes with higher transmission, and a stacked-detector approach may help material discrimination for the lowest attenuations. Image processing and segmentation allow derivation of results for entire objects, and subtraction of backgrounds. We discuss R and D performed under a number of different programs, showing progress made in each of the interacting subsystems. We discuss results of studies into faster scintillation detectors, including ZnO, BaF{sub 2} and PbWO{sub 4}, as well as suitable photo-detectors, read-out and digitization electronics. We discuss high-duty-factor linear-accelerator x-ray sources and their associated requirements, and how such sources improve spectroscopic techniques. We further discuss how image processing techniques help in correcting for backgrounds and overlapping materials. In sum, we present an integrated picture of how to optimize a cargo inspection system for x-ray spectroscopy.« less

REVIEWS OF TOPICAL PROBLEMS: Cygnus X-3: a powerful galactic source of hard radiation

NASA Astrophysics Data System (ADS)

Vladimirskiĭ, B. M.; Gal'per, A. M.; Luchkov, B. I.; Stepanyan, A. A.

1985-02-01

A review is given of experimental and theoretical research on the galactic source Cyg X-3, whose electromagnetic spectrum extends from radio frequencies to ultrahigh-energy (Eγ ~ 1016 eV) γ-rays. Cyg X-3 also has a high x-ray luminosity (1038 erg/sec) and exhibits diversified sporadic and periodic variations, most notably occasional radio outbursts and a 4h.8 infrared, x-ray, and γ-ray cycle. Analysis of the observations indicates that Cyg X-3 is a close binary system comprising a compact relativistic object (neutron star, black hole) and a dwarf companion losing mass. Particles are accelerated to 1016 eV within the system.

CIAO: A Modern Data Analysis System for X-Ray Astronomy

NASA Astrophysics Data System (ADS)

Fruscione, Antonella

2017-08-01

It is now eighteen years after launch and Chandra continues to produce spectacular results!A portion of the success is to be attributed to the data analysis software CIAO (Chandra Interactive Analysis of Observations) that the Chandra X-Ray Center (CXC) continues to improve and release year after year.CIAO is downloaded more than 1200 times a year and it is used by a wide variety of users around the world: from novice to experienced X-ray astronomers, high school, undergraduate and graduate students, archival users (many new to X-ray or Chandra data), users with extensive resources and others from smaller countries and institutions.The scientific goals and kinds of datasets and analysis cover a wide range: observations spanning from days to years, different instrument configurations and different kinds of targets, from pointlike stars and quasars, to fuzzy galaxies and clusters, to moving solar objects. These different needs and goals require a variety of specialized software and careful and detailed documentation which is what the CIAO software provides. In general, we strive to build a software system which is easy for beginners, yet powerful for advanced users.The complexity of the Chandra data require a flexible data analysis system which provides an environment where the users can apply our tools, but can also explore and construct their own applications. The main purpose of this talk is to present CIAO as a modern data analysis system for X-ray data analysis.CIAO has grown tremendously over the years and we will highlight (a) the most recent advancements with a particular emphasis on the newly developed high-level scripts which simplify the analysis steps for the most common cases making CIAO more accessible to all users - including beginners and users who are not X-ray astronomy specialists, (b) the python-based Sherpa modelling and fitting application and the new stand-alone version openly developed and distributed on Github and (c) progress on methods to characterize the Chandra PSF.

Data processing and analysis for 2D imaging GEM detector system

NASA Astrophysics Data System (ADS)

Czarski, T.; Chernyshova, M.; Pozniak, K. T.; Kasprowicz, G.; Byszuk, A.; Juszczyk, B.; Kolasinski, P.; Linczuk, M.; Wojenski, A.; Zabolotny, W.; Zienkiewicz, P.

2014-11-01

The Triple Gas Electron Multiplier (T-GEM) is presented as soft X-ray (SXR) energy and position sensitive detector for high-resolution X-ray diagnostics of magnetic confinement fusion plasmas [1]. Multi-channel measurement system and essential data processing for X-ray energy and position recognition is consider. Several modes of data acquisition are introduced depending on processing division for hardware and software components. Typical measuring issues aredeliberated for enhancement of data quality. Fundamental output characteristics are presented for one and two dimensional detector structure. Representative results for reference X-ray source and tokamak plasma are demonstrated.

PROS: An IRAF based system for analysis of x ray data

NASA Technical Reports Server (NTRS)

Conroy, M. A.; Deponte, J.; Moran, J. F.; Orszak, J. S.; Roberts, W. P.; Schmidt, D.

1992-01-01

PROS is an IRAF based software package for the reduction and analysis of x-ray data. The use of a standard, portable, integrated environment provides for both multi-frequency and multi-mission analysis. The analysis of x-ray data differs from optical analysis due to the nature of the x-ray data and its acquisition during constantly varying conditions. The scarcity of data, the low signal-to-noise ratio and the large gaps in exposure time make data screening and masking an important part of the analysis. PROS was developed to support the analysis of data from the ROSAT and Einstein missions but many of the tasks have been used on data from other missions. IRAF/PROS provides a complete end-to-end system for x-ray data analysis: (1) a set of tools for importing and exporting data via FITS format -- in particular, IRAF provides a specialized event-list format, QPOE, that is compatible with its IMAGE (2-D array) format; (2) a powerful set of IRAF system capabilities for both temporal and spatial event filtering; (3) full set of imaging and graphics tasks; (4) specialized packages for scientific analysis such as spatial, spectral and timing analysis -- these consist of both general and mission specific tasks; and (5) complete system support including ftp and magnetic tape releases, electronic and conventional mail hotline support, electronic mail distribution of solutions to frequently asked questions and current known bugs. We will discuss the philosophy, architecture and development environment used by PROS to generate a portable, multimission software environment. PROS is available on all platforms that support IRAF, including Sun/Unix, VAX/VMS, HP, and Decstations. It is available on request at no charge.

X-ray source assembly having enhanced output stability, and fluid stream analysis applications thereof

DOEpatents

Radley, Ian [Glenmont, NY; Bievenue, Thomas J [Delmar, NY; Burdett, John H [Charlton, NY; Gallagher, Brian W [Guilderland, NY; Shakshober, Stuart M [Hudson, NY; Chen, Zewu [Schenectady, NY; Moore, Michael D [Alplaus, NY

2008-06-08

An x-ray source assembly and method of operation are provided having enhanced output stability. The assembly includes an anode having a source spot upon which electrons impinge and a control system for controlling position of the anode source spot relative to an output structure. The control system can maintain the anode source spot location relative to the output structure notwithstanding a change in one or more operating conditions of the x-ray source assembly. One aspect of the disclosed invention is most amenable to the analysis of sulfur in petroleum-based fuels.

X-Ray Studies of Diffusion Dynamics in Nano-Confined Geometries

NASA Astrophysics Data System (ADS)

Boucheron, Leandra

Since their discovery in the late 1800s, x-rays have taken the stage as one of the most powerful research techniques for materials science. Their element-specific absorption has allowed for everyday applications in security and medical imaging, while their short wavelength has a tremendous ability to resolve materials on a molecular or even atomic level. In this dissertation, I will discuss basic properties of x-rays as well as how they are produced and detected. I will also present x-ray scattering and analysis techniques before moving onto a discussion of my research on diffusion in soft-matter systems. I provide a full alignment guide for a lab-based dynamic light scattering (DLS) goniometer system, which I used for some preliminary studies of systems. I proceed to discuss diffusion on the nanoscale in quasi-1D (nanopores) and quasi-2D (liquid surface) systems. The latter of these systems was the main focus of my dissertation research. I utilized x-ray photon correlation spectroscopy (XPCS) to study the diffusion and interparticle dynamics of iron oxide nanoparticles at the air-water interface. Autocorrelation analysis revealed that these particles show signatures of a jammed system under lateral compression. I present these results as well as a description of their interpretation and importance in the main text.

21 CFR 892.1660 - Non-image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Non-image-intensified fluoroscopic x-ray system. 892.1660 Section 892.1660 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... of x-radiation into a visible image. This generic type of device may include signal analysis and...

21 CFR 892.1660 - Non-image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Non-image-intensified fluoroscopic x-ray system. 892.1660 Section 892.1660 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... of x-radiation into a visible image. This generic type of device may include signal analysis and...

21 CFR 892.1660 - Non-image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Non-image-intensified fluoroscopic x-ray system. 892.1660 Section 892.1660 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... of x-radiation into a visible image. This generic type of device may include signal analysis and...

X-ray chemical analyzer for field applications

DOEpatents

Gamba, Otto O. M.

1977-01-01

A self-supporting portable field multichannel X-ray chemical analyzer system comprising a lightweight, flexibly connected, remotely locatable, radioisotope-excited sensing probe utilizing a cryogenically-cooled solid state semi-conductor crystal detector for fast in situ non-destructive, qualitative and quantitative analysis of elements in solid, powder, liquid or slurried form, utilizing an X-ray energy dispersive spectrometry technique.

Chandra Interactive Analysis of Observations (CIAO)

NASA Technical Reports Server (NTRS)

Dobrzycki, Adam

2000-01-01

The Chandra (formerly AXAF) telescope, launched on July 23, 1999, provides X-rays data with unprecedented spatial and spectral resolution. As part of the Chandra scientific support, the Chandra X-ray Observatory Center provides a new data analysis system, CIAO ("Chandra Interactive Analysis of Observations"). We will present the main components of the system: "First Look" analysis; SHERPA: a multi-dimensional, multi-mission modeling and fitting application; Chandra Imaging and Plotting System; Detect package-source detection algorithms; and DM package generic data manipulation tools, We will set up a demonstration of the portable version of the system and show examples of Chandra Data Analysis.

Optical and X-ray studies of Compact X-ray Binaries in NGC 5904

NASA Astrophysics Data System (ADS)

Bhalotia, Vanshree; Beck-Winchatz, Bernhard

2018-06-01

Due to their high stellar densities, globular cluster systems trigger various dynamical interactions, such as the formation of compact X-ray binaries. Stellar collisional frequencies have been correlated to the number of X-ray sources detected in various clusters and we hope to measure this correlation for NGC 5904. Optical fluxes of sources from archival HST images of NGC 5904 have been measured using a DOLPHOT PSF photometry in the UV, optical and near-infrared. We developed a data analysis pipeline to process the fluxes of tens of thousands of objects using awk, python and DOLPHOT. We plot color magnitude diagrams in different photometric bands in order to identify outliers that could be X-ray binaries, since they do not evolve the same way as singular stars. Aligning previously measured astrometric data for X-ray sources in NGC 5904 from Chandra with archival astrometric data from HST will filter out the outlier objects that are not X-ray producing, and provide a sample of compact binary systems that are responsible for X-ray emission in NGC 5904. Furthermore, previously measured X-ray fluxes of NGC 5904 from Chandra have also been used to measure the X-ray to optical flux ratio and identify the types of compact X-ray binaries responsible for the X-ray emissions in NGC 5904. We gratefully acknowledge the support from the Illinois Space Grant Consortium.

Analyzing the Spectra of Accreting X-Ray Pulsars

NASA Astrophysics Data System (ADS)

Wolff, Michael

This proposal seeks funding for the analysis of accretion-powered X-ray pulsar spectra from NASA/ HEASARC archived X-ray data. Spectral modeling of accreting X-ray pulsars can tell us a great deal about the physical conditions in and near high mass X-ray binary systems. Such systems have accretion flows where plasma is initially channeled from an accretion disk by the strong neutron star magnetic field, eventually falling onto the magnetic polar cap of the neutron star compact object. Many of these accreting X-ray pulsars have X-ray spectra that consist of broad power-law continua with superposed cyclotron resonant scattering features indicating magnetic field strengths above 10^12 G. The energies of these cyclotron line features have recently been shown to vary with X-ray luminosity in a number of sources such as Her X-1 and V 0332+53, a phenomenon not well understood. Another recent development is the relatively new analytic model for the spectral continuum formation in accretion-powered pulsar systems developed by Becker & Wolff. In their formalism the accretion flows are assumed to go through radiation- dominated radiative shocks and settle onto the neutron star surface. The radiation field consists of strongly Comptonized bremsstrahlung emission from the entire plasma, Comptonized cyclotron emission from the de-excitations of Landau-excited electrons in the neutron star magnetic field, and Comptonized black-body emission from a thermal mound near the neutron star surface. We seek to develop the data analysis tools to apply this model framework to the X-ray data from a wide set of sources to make progress characterizing the basic accretion properties (e.g., magnetic field strength, plasma temperatures, polar cap size, accretion rate per unit area, dominance of bulk vs. thermal Comptonization) as well as understanding the variations of the cyclotron line energies with X-ray luminosity. The three major goals of our proposed work are as follows: In the first year, we will develop the new software module (essentially a computer code representing the theoretical model) necessary to perform the analysis of accretion-powered pulsar X-ray spectra in the XSPEC spectral analysis environment. Also in this first year we will analyze new Suzaku Cycle 6 Target of Opportunity observations of GX 304-1 and 4U 0115+63, two known cyclotron line sources, that we have recently carried out. In the second year of this study we will apply our new XSPEC spectral continuum module to the archival X-ray observational data from a number of accreting X-ray pulsars from the RXTE/PCA/HEXTE and Suzaku/XIS/HXD instruments to extract basic accretion parameters. Our source list contains eight pulsars, seven of which have observed cyclotron scattering lines. These pulsars span a range in magnetic field strength, luminosity, expected accretion rate, expected polar cap size, and Comptonizing temperature. In the second year of this work we also plan to make our new fully tested XSPEC continuum analysis module available to the Goddard Space Flight Center HEASARC for distribution to the astrophysical research community. The development and analysis tasks proposed here will provide for the first time a physical basis for the analysis and interpretation of data on accreting X-ray pulsar spectra.

XAssist: A System for the Automation of X-ray Astrophysics Analysis

NASA Astrophysics Data System (ADS)

Ptak, A.

2004-08-01

XAssist is a NASA AISR-funded project for the automation of X-ray astrophysics. It is capable of data reprocessing, source detection, and preliminary spatial, temporal and spectral analysis for each source with sufficient counts. The bulk of the system is written in Python, which in turn drives underlying software (CIAO for Chandra data, etc.). Future work will include a GUI (mainly for beginners and status monitoring) and the exposure of at least some functionality as web services. The latter will help XAssist to eventually become part of the VO, making advanced queries possible, such as determining the X-ray fluxes of counterparts to HST or SDSS sources (including the use of unpublished X-ray data), and add the ability of ``on-the-fly'' X-ray processing. Pipelines are running on Chandra and XMM-Newton observations of galaxies to demonstrate XAssist's capabilities, and the results are available online (in real time) at http://www.xassist.org. XAssist itself as well as various associated projects are available for download.

TH-AB-209-07: High Resolution X-Ray-Induced Acoustic Computed Tomography

DOE Office of Scientific and Technical Information (OSTI.GOV)

Xiang, L; Tang, S; Ahmad, M

Purpose: X-ray radiographic absorption imaging is an invaluable tool in medical diagnostics, biology and materials science. However, the use of conventional CT is limited by two factors: the detection sensitivity to weak absorption material and the radiation dose from CT scanning. The purpose of this study is to explore X-ray induced acoustic computed tomography (XACT), a new imaging modality, which combines X-ray absorption contrast and high ultrasonic resolution to address these challenges. Methods: First, theoretical models was built to analyze the XACT sensitivity to X-ray absorption and calculate the minimal radiation dose in XACT imaging. Then, an XACT system comprisedmore » of an ultrashort X-ray pulse, a low noise ultrasound detector and a signal acquisition system was built to evaluate the X-ray induced acoustic signal generation. A piece of chicken bone and a phantom with two golden fiducial markers were exposed to 270 kVp X-ray source with 60 ns exposure time, and the X-ray induced acoustic signal was received by a 2.25MHz ultrasound transducer in 200 positions. XACT images were reconstructed by a filtered back-projection algorithm. Results: The theoretical analysis shows that X-ray induced acoustic signals have 100% relative sensitivity to X-ray absorption, but not to X-ray scattering. Applying this innovative technology to breast imaging, we can reduce radiation dose by a factor of 50 compared with newly FDA approved breast CT. The reconstructed images of chicken bone and golden fiducial marker phantom reveal that the spatial resolution of the built XACT system is 350µm. Conclusion: In XACT, the imaging sensitivity to X-ray absorption is improved and the imaging dose is dramatically reduced by using ultrashort pulsed X-ray. Taking advantage of the high ultrasonic resolution, we can also perform 3D imaging with a single X-ray pulse. This new modality has the potential to revolutionize x-ray imaging applications in medicine and biology.« less

Determination of the atmospheric structure of the BO star companion of SMC X-1 by analysis of Ginga observations

NASA Technical Reports Server (NTRS)

Clark, George W.

1994-01-01

The x-ray phenomena of the binary system SMC X-1/Sk 160, observed with the Ginga and ROSAT x-ray observatories, are compared with computed phenomena derived from a three dimensional hydrodynamical model of the stellar wind perturbed by x-ray heating and ionization which is described in the accompanying paper. In the model the BOI primary star has a line-driven stellar wind in the region of the x-ray shadow and a thermal wind in the region heated by x-rays. We find general agreement between the observed and predicted x-ray spectra throughout the binary orbit cycle, including the extended, variable, and asymmetric eclipse transitions and the period of deep eclipse.

Analysis of photographic X-ray images. [S-054 telescope on Skylab

NASA Technical Reports Server (NTRS)

Krieger, A. S.

1977-01-01

Some techniques used to extract quantitative data from the information contained in photographic images produced by grazing incidence soft X-ray optical systems are described. The discussion is focussed on the analysis of the data returned by the S-054 X-Ray Spectrographic Telescope Experiment on Skylab. The parameters of the instrument and the procedures used for its calibration are described. The technique used to convert photographic density to focal plane X-ray irradiance is outlined. The deconvolution of the telescope point response function from the image data is discussed. Methods of estimating the temperature, pressure, and number density of coronal plasmas are outlined.

High-rate x-ray spectroscopy in mammography with a CdTe detector: a digital pulse processing approach.

PubMed

Abbene, L; Gerardi, G; Principato, F; Del Sordo, S; Ienzi, R; Raso, G

2010-12-01

Direct measurement of mammographic x-ray spectra under clinical conditions is a difficult task due to the high fluence rate of the x-ray beams as well as the limits in the development of high resolution detection systems in a high counting rate environment. In this work we present a detection system, based on a CdTe detector and an innovative digital pulse processing (DPP) system, for high-rate x-ray spectroscopy in mammography. The DPP system performs a digital pile-up inspection and a digital pulse height analysis of the detector signals, digitized through a 14-bit, 100 MHz digitizer, for x-ray spectroscopy even at high photon counting rates. We investigated on the response of the digital detection system both at low (150 cps) and at high photon counting rates (up to 500 kcps) by using monoenergetic x-ray sources and a nonclinical molybdenum anode x-ray tube. Clinical molybdenum x-ray spectrum measurements were also performed by using a pinhole collimator and a custom alignment device. The detection system shows excellent performance up to 512 kcps with an energy resolution of 4.08% FWHM at 22.1 keV. Despite the high photon counting rate (up to 453 kcps), the molybdenum x-ray spectra, measured under clinical conditions, are characterized by a low number of pile-up events. The agreement between the attenuation curves and the half value layer values, obtained from the measured spectra, simulated spectra, and from the exposure values directly measured with an ionization chamber, also shows the accuracy of the measurements. These results make the proposed detection system a very attractive tool for both laboratory research and advanced quality controls in mammography.

Final Report - X-ray Studies of Highly Correlated Systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Burns, Clement

2017-11-27

The overall goal of the research was to improve the capabilities of x-ray synchrotron instrumentation to enable cutting-edge research in condensed matter physics. The main goal of the current grant cycle was to find a method to measure the polarization of the scattered x-ray in resonant inelastic x-ray scattering. To do this, we developed a polarization analysis apparatus using a thin, toroidally bent single crystal, which could be set to reflect one or the other of the two polarization components in the scattered x-ray beam. Resonant x-ray scattering measurements were also carried out on interfaces and the charge density wavemore » in high temperature superconducting materials.« less

Compact energy dispersive X-ray microdiffractometer for diagnosis of neoplastic tissues

NASA Astrophysics Data System (ADS)

Sosa, C.; Malezan, A.; Poletti, M. E.; Perez, R. D.

2017-08-01

An energy dispersive X-ray microdiffractometer with capillary optics has been developed for characterizing breast cancer. The employment of low divergence capillary optics helps to reduce the setup size to a few centimeters, while providing a lateral spatial resolution of 100 μm. The system angular calibration and momentum transfer resolution were assessed by a detailed study of a polycrystalline reference material. The performance of the system was tested by means of the analysis of tissue-equivalent samples previously characterized by conventional X-ray diffraction. In addition, a simplified correction model for an appropriate comparison of the diffraction spectra was developed and validated. Finally, the system was employed to evaluate normal and neoplastic human breast samples, in order to determine their X-ray scatter signatures. The initial results indicate that the use of this compact energy dispersive X-ray microdiffractometer combined with a simplified correction procedure is able to provide additional information to breast cancer diagnosis.

Reconstitution of SNARE proteins into solid-supported lipid bilayer stacks and X-ray structure analysis.

PubMed

Xu, Yihui; Kuhlmann, Jan; Brennich, Martha; Komorowski, Karlo; Jahn, Reinhard; Steinem, Claudia; Salditt, Tim

2018-02-01

SNAREs are known as an important family of proteins mediating vesicle fusion. For various biophysical studies, they have been reconstituted into supported single bilayers via proteoliposome adsorption and rupture. In this study we extended this method to the reconstitution of SNAREs into supported multilamellar lipid membranes, i.e. oriented multibilayer stacks, as an ideal model system for X-ray structure analysis (X-ray reflectivity and diffraction). The reconstitution was implemented through a pathway of proteomicelle, proteoliposome and multibilayer. To monitor the structural evolution in each step, we used small-angle X-ray scattering for the proteomicelles and proteoliposomes, followed by X-ray reflectivity and grazing-incidence small-angle scattering for the multibilayers. Results show that SNAREs can be successfully reconstituted into supported multibilayers, with high enough orientational alignment for the application of surface sensitive X-ray characterizations. Based on this protocol, we then investigated the effect of SNAREs on the structure and phase diagram of the lipid membranes. Beyond this application, this reconstitution protocol could also be useful for X-ray analysis of many further membrane proteins. Copyright © 2017 Elsevier B.V. All rights reserved.

Taking into Account Interelement Interference in X-Ray Fluorescence Analysis of Thin Two-Layer Ti/V Systems

NASA Astrophysics Data System (ADS)

Mashin, N. I.; Razuvaev, A. G.; Cherniaeva, E. A.; Gafarova, L. M.; Ershov, A. V.

2018-03-01

We propose a new method for determining the thickness of layers in x-ray fluorescence analysis of two-layer Ti/V systems, using easily fabricated standardized film layers obtained by sputter deposition of titanium on a polymer film substrate. We have calculated correction factors taking into account the level of attenuation for the intensity of the primary emission from the x-ray tube and the analytical line for the element of the bottom layer in the top layer, and the enhancement of the fluorescence intensity for the top layer by the emission of atoms in the bottom layer.

X-ray source assembly having enhanced output stability, and fluid stream analysis applications thereof

DOEpatents

Radley, Ian; Bievenue, Thomas J.; Burdett Jr., John H.; Gallagher, Brian W.; Shakshober, Stuart M.; Chen, Zewu; Moore, Michael D.

2007-04-24

An x-ray source assembly (2700) and method of operation are provided having enhanced output stability. The assembly includes an anode (2125) having a source spot upon which electrons (2120) impinge and a control system (2715/2720) for controlling position of the anode source spot relative to an output structure. The control system can maintain the anode source spot location relative to the output structure (2710) notwithstanding a change in one or more operating conditions of the x-ray source assembly. One aspect of the disclosed invention is most amenable to the analysis of sulfur in petroleum-based fuels.

Automated X-ray and Optical Analysis of the Virtual Observatory and Grid Computing

NASA Technical Reports Server (NTRS)

Ptak, A.; Krughoff, S.; Connolly, A.

2011-01-01

We are developing a system to combine the Web Enabled Source Identification with X-Matching (WESIX) web service, which emphasizes source detection on optical images,with the XAssist program that automates the analysis of X-ray data. XAssist is continuously processing archival X-ray data in several pipelines. We have established a workflow in which FITS images and/or (in the case of X ray data) an X-ray field can be input to WESIX. Intelligent services return available data (if requested fields have been processed) or submit job requests to a queue to be performed asynchronously. These services will be available via web services (for non-interactive use by Virtual Observatory portals and applications) and through web applications (written in the Django web application framework). We are adding web services for specific XAssist functionality such as determining .the exposure and limiting flux for a given position on the sky and extracting spectra and images for a given region. We are improving the queuing system in XAssist to allow for "watch lists" to be specified by users, and when X-ray fields in a user's watch list become publicly available they will be automatically added to the queue. XAssist is being expanded to be used as a survey planning 1001 when coupled with simulation software, including functionality for NuStar, eRosita, IXO, and the Wide Field Xray Telescope (WFXT), as part of an end to end simulation/analysis system. We are also investigating the possibility of a dedicated iPhone/iPad app for querying pipeline data, requesting processing, and administrative job control.

Cephalometric landmark detection in dental x-ray images using convolutional neural networks

NASA Astrophysics Data System (ADS)

Lee, Hansang; Park, Minseok; Kim, Junmo

2017-03-01

In dental X-ray images, an accurate detection of cephalometric landmarks plays an important role in clinical diagnosis, treatment and surgical decisions for dental problems. In this work, we propose an end-to-end deep learning system for cephalometric landmark detection in dental X-ray images, using convolutional neural networks (CNN). For detecting 19 cephalometric landmarks in dental X-ray images, we develop a detection system using CNN-based coordinate-wise regression systems. By viewing x- and y-coordinates of all landmarks as 38 independent variables, multiple CNN-based regression systems are constructed to predict the coordinate variables from input X-ray images. First, each coordinate variable is normalized by the length of either height or width of an image. For each normalized coordinate variable, a CNN-based regression system is trained on training images and corresponding coordinate variable, which is a variable to be regressed. We train 38 regression systems with the same CNN structure on coordinate variables, respectively. Finally, we compute 38 coordinate variables with these trained systems from unseen images and extract 19 landmarks by pairing the regressed coordinates. In experiments, the public database from the Grand Challenges in Dental X-ray Image Analysis in ISBI 2015 was used and the proposed system showed promising performance by successfully locating the cephalometric landmarks within considerable margins from the ground truths.

21 CFR 892.1600 - Angiographic x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Angiographic x-ray system. 892.1600 Section 892.1600 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... device may include signal analysis and display equipment, patient and equipment supports, component parts...

21 CFR 892.1680 - Stationary x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Stationary x-ray system. 892.1680 Section 892.1680 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... signal analysis and display equipment, patient and equipment supports, component parts, and accessories...

21 CFR 892.1600 - Angiographic x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Angiographic x-ray system. 892.1600 Section 892.1600 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... device may include signal analysis and display equipment, patient and equipment supports, component parts...

21 CFR 892.1710 - Mammographic x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Mammographic x-ray system. 892.1710 Section 892.1710 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1720 - Mobile x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Mobile x-ray system. 892.1720 Section 892.1720 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... for diagnostic procedures. This generic type of device may include signal analysis and display...

21 CFR 892.1720 - Mobile x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Mobile x-ray system. 892.1720 Section 892.1720 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... for diagnostic procedures. This generic type of device may include signal analysis and display...

21 CFR 892.1680 - Stationary x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Stationary x-ray system. 892.1680 Section 892.1680 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... signal analysis and display equipment, patient and equipment supports, component parts, and accessories...

21 CFR 892.1740 - Tomographic x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Tomographic x-ray system. 892.1740 Section 892.1740 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1680 - Stationary x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Stationary x-ray system. 892.1680 Section 892.1680 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... signal analysis and display equipment, patient and equipment supports, component parts, and accessories...

21 CFR 892.1730 - Photofluorographic x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Photofluorographic x-ray system. 892.1730 Section 892.1730 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1740 - Tomographic x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Tomographic x-ray system. 892.1740 Section 892.1740 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1650 - Image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Image-intensified fluoroscopic x-ray system. 892.1650 Section 892.1650 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... through electronic amplification. This generic type of device may include signal analysis and display...

21 CFR 892.1710 - Mammographic x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Mammographic x-ray system. 892.1710 Section 892.1710 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1650 - Image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Image-intensified fluoroscopic x-ray system. 892.1650 Section 892.1650 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... through electronic amplification. This generic type of device may include signal analysis and display...

21 CFR 892.1740 - Tomographic x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Tomographic x-ray system. 892.1740 Section 892.1740 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1730 - Photofluorographic x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Photofluorographic x-ray system. 892.1730 Section 892.1730 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1720 - Mobile x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Mobile x-ray system. 892.1720 Section 892.1720 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... for diagnostic procedures. This generic type of device may include signal analysis and display...

21 CFR 892.1730 - Photofluorographic x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Photofluorographic x-ray system. 892.1730 Section 892.1730 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1710 - Mammographic x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Mammographic x-ray system. 892.1710 Section 892.1710 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1740 - Tomographic x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Tomographic x-ray system. 892.1740 Section 892.1740 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1710 - Mammographic x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Mammographic x-ray system. 892.1710 Section 892.1710 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1600 - Angiographic x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Angiographic x-ray system. 892.1600 Section 892.1600 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... device may include signal analysis and display equipment, patient and equipment supports, component parts...

21 CFR 892.1740 - Tomographic x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Tomographic x-ray system. 892.1740 Section 892.1740 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1680 - Stationary x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Stationary x-ray system. 892.1680 Section 892.1680 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... signal analysis and display equipment, patient and equipment supports, component parts, and accessories...

21 CFR 892.1730 - Photofluorographic x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Photofluorographic x-ray system. 892.1730 Section 892.1730 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1720 - Mobile x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Mobile x-ray system. 892.1720 Section 892.1720 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... for diagnostic procedures. This generic type of device may include signal analysis and display...

21 CFR 892.1650 - Image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Image-intensified fluoroscopic x-ray system. 892.1650 Section 892.1650 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... through electronic amplification. This generic type of device may include signal analysis and display...

21 CFR 892.1600 - Angiographic x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Angiographic x-ray system. 892.1600 Section 892.1600 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... device may include signal analysis and display equipment, patient and equipment supports, component parts...

21 CFR 892.1720 - Mobile x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Mobile x-ray system. 892.1720 Section 892.1720 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... for diagnostic procedures. This generic type of device may include signal analysis and display...

21 CFR 892.1710 - Mammographic x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Mammographic x-ray system. 892.1710 Section 892.1710 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED.... This generic type of device may include signal analysis and display equipment, patient and equipment...

21 CFR 892.1680 - Stationary x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Stationary x-ray system. 892.1680 Section 892.1680 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... signal analysis and display equipment, patient and equipment supports, component parts, and accessories...

21 CFR 892.1600 - Angiographic x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Angiographic x-ray system. 892.1600 Section 892.1600 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED... device may include signal analysis and display equipment, patient and equipment supports, component parts...

21 CFR 892.1730 - Photofluorographic x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Photofluorographic x-ray system. 892.1730 Section 892.1730 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES.... This generic type of device may include signal analysis and display equipment, patient and equipment...

X-Ray Measurements Of A Thermo Scientific P385 DD Neutron Generator

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wharton, C. J.; Seabury, E. H.; Chichester, D. L.

2011-06-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X rays are a normal byproduct from neutron generators, but depending on their intensity and energy, x rays can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum wasmore » measured with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60 deg. between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and its x-ray emission appears to be axially symmetric. A thin lead shield, 3.2 mm (1/8 inch) thick, reduced the 70-keV generator x rays to negligible levels.« less

X-Ray Measurements Of A Thermo Scientific P385 DD Neutron Generator

NASA Astrophysics Data System (ADS)

Wharton, C. J.; Seabury, E. H.; Chichester, D. L.; Caffrey, A. J.; Simpson, J.; Lemchak, M.

2011-06-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X rays are a normal byproduct from neutron generators, but depending on their intensity and energy, x rays can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum was measured with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60° between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and its x-ray emission appears to be axially symmetric. A thin lead shield, 3.2 mm (1/8 inch) thick, reduced the 70-keV generator x rays to negligible levels.

Chandra X-ray Center Science Data Systems Regression Testing of CIAO

NASA Astrophysics Data System (ADS)

Lee, N. P.; Karovska, M.; Galle, E. C.; Bonaventura, N. R.

2011-07-01

The Chandra Interactive Analysis of Observations (CIAO) is a software system developed for the analysis of Chandra X-ray Observatory observations. An important component of a successful CIAO release is the repeated testing of the tools across various platforms to ensure consistent and scientifically valid results. We describe the procedures of the scientific regression testing of CIAO and the enhancements made to the testing system to increase the efficiency of run time and result validation.

Gamma-ray emission from globular clusters. Shock high energy emission from the Be-Star/Pulsar System PSR 1259-63. Echoes in x-ray novae

NASA Technical Reports Server (NTRS)

Kaaret, Philip

1995-01-01

This grant covers work on the Compton phase 3 investigation, 'Shock High Energy Emission from the Be- Star/Pulsar System PSR 1259-63' and cycle 4 investigations 'Diffuse Gamma-Ray Emission at High Latitudes' and 'Echoes in X-Ray Novae'. Work under the investigation 'Diffuse Gamma-Ray Emission at High Latitudes' has lead to the publication of a paper (attached), describing gamma-ray emissivity variations in the northern galactic hemisphere. Using archival EGRET data, we have found a large irregular region of enhanced gamma-ray emissivity at energies greater 100 MeV. This is the first observation of local structure in the gamma-ray emissivity. Work under the investigation 'Echoes in X-Ray Novae' is proceeding with analysis of data from OSSE from the transient source GRO J1655-40. The outburst of this source last fall triggered this Target of Opportunity investigation. Preliminary spectral analysis shows emission out to 600 keV and a pure power low spectrum with no evidence of an exponential cutoff. Work is complete on the analysis of BATSE data from the Be-Star/Pulsar Sustem PSR 1259-63.

21 CFR Appendix B to Subpart B of... - Scope of Product Coverage

Code of Federal Regulations, 2010 CFR

2010-04-01

... Transducer ITX—Transducer, Ultrasonic, Diagnostic Diagnostic X-Ray Imaging Devices (except mammographic x-ray systems): RA 892.1600 Angiographic X-Ray System IZI—System, X-Ray, Angiographic RA 892.1650 Image-Intensified Fluoroscopic X-Ray System MQB—Solid State X-Ray Imager (Flat Panel/Digital Imager) JAA—System, X...

21 CFR Appendix B to Subpart B of... - Scope of Product Coverage

Code of Federal Regulations, 2011 CFR

2011-04-01

... Transducer ITX—Transducer, Ultrasonic, Diagnostic Diagnostic X-Ray Imaging Devices (except mammographic x-ray systems): RA 892.1600 Angiographic X-Ray System IZI—System, X-Ray, Angiographic RA 892.1650 Image-Intensified Fluoroscopic X-Ray System MQB—Solid State X-Ray Imager (Flat Panel/Digital Imager) JAA—System, X...

X-ray photoemission study of NiS2-xSex (x=0.0 1.2)

NASA Astrophysics Data System (ADS)

Krishnakumar, S. R.; Sarma, D. D.

2003-10-01

Electronic structure of NiS2-xSex system has been investigated for various compositions (x) using x-ray photoemission spectroscopy. An analysis of the core-level as well as the valence-band spectra of NiS2 in conjunction with many-body cluster calculations provides a quantitative description of the electronic structure of this compound. With increasing Se content, the on-site Coulomb correlation strength (U) does not change, while the bandwidth W of the system increases, driving the system from a covalent insulating state to a pd-metallic state.

The Chandra X-ray Observatory: An Astronomical Facility Available to the World

NASA Technical Reports Server (NTRS)

Smith, Randall K.

2006-01-01

The Chandra X-ray observatory, one of NASA's "Great Observatories," provides high angular and spectral resolution X-ray data which is freely available to all. In this review I describe the instruments on chandra along with their current calibration, as well as the chandra proposal system, the freely-available Chandra analysis software package CIAO, and the Chandra archive. As Chandra is in its 6th year of operation, the archive already contains calibrated observations of a large range of X-ray sources. The Chandra X-ray Center is committed to assisting astronomers from any country who wish to use data from the archive or propose for observations

An adjustable short-focal length, high-gradient PMQ electron-beam final-focus system for the PLEIADES ultra-fast x-ray Thomson source

NASA Astrophysics Data System (ADS)

Lim, Jae-Ku

In the span of a 100 year since the discovery of first x-rays by Roentgen that won him the first Nobel prize in physics, several types of radiation sources have been developed. Currently, radiations at extremely short wavelengths have only been accessed at synchrotron radiation sources. However, the current 3rd generation synchrotron sources can only produce x-rays of energy up to 60 keV and pulse lengths of several picoseconds long. But needs for shorter wavelength and shorter pulse duration radiations demanded by scientists to understand the nature of matter at atomic/molecular scale initiated the new scientific research for the production of sub-picosecond, hard x-rays. At the Lawrence Livermore National Laboratory, a Thomson x-ray source in the backscattering mode---a head-on collision between a high intensity Ti:Sapphire Chirped Pulse Amplification laser and a relativistic electron beam---called the PLEIADES (Picosecond Laser-Electron Inter-Action for the Dynamical Evaluation of Structures) laboratory has been developed. Early works demonstrated the production of quasi-monochromatic, femto-second long, hard x-rays. Initially reported x-ray flux was in the low range of 105--10 6 photons per shot. During the early stage of PLEIADES experiments, 15 T/m electromagnet final focusing quadrupoles (in a triplet lattice configuration) were employed to focus the beam to a 40-50 mum spot-size. A larger focal spot-size beam has a low-density of electron particles available at the interaction with incident photons, which leads to a low scattering probability. The current dissertation shows that by employing a 560 T/m PMQ (Permanent-Magnet Quadrupole) final focus system, an electron beam as small as 10-20 mum can be achieved. The implementation of this final focus system demonstrated the improvement of the total x-ray flux by two orders of magnitude. The PMQ final focus system also produced small electron beams consistently over 30-100 MeV electron beam energy, which enabled the production of x-ray energy over 40-140 keV. In this dissertation, the PLEIADES Thomson x-ray facility will be described in detail includes the 100 MeV linac and the FALCON laser system. Later, we will discuss the design, construction and implementation of the PMQ final focus system in the beamline. The measurement of electron beam parameters before and after the final focus system will be presented. The beam measurements at the interaction region were accomplished with the use of both OTR (Optical Transition Radiation) imaged by a CCD camera and the fast streak camera for respective spatial and temporal alignments. The theoretical analysis in "real beam" effects and spacetime beam jitter effects will be given to help understand the observations. A 3D simulation tool developed for x-ray data analysis was used to provide direct comparisons with the x-ray flux, spectrum distribution and transverse x-ray profile.

Investigation of the nanoscale two-component ZnS-ZnO heterostructures by means of HR-TEM and X-ray based analysis

NASA Astrophysics Data System (ADS)

Pankin, I. A.; Polozhentsev, O. E.; Soldatov, M. A.; Bugaev, A. L.; Tsaturyan, A.; Lomachenko, K. A.; Guda, A. A.; Budnyk, A. P.; Lamberti, C.; Soldatov, A. V.

2018-06-01

This article is devoted to the spectroscopic characterization of ZnS-ZnO nanoscale heterostructures synthesized by the microwave-assisted solvothermal method. The synthesized samples were investigated by means of X-ray powder diffraction (XRPD), high energy resolution fluorescence detected X-ray absorption near-edge-structure (HERFD-XANES) spectroscopy, valence-to-core X-ray emission spectroscopy (VtC-XES) and high resolution transmission electron microscopy (HR-TEM) as well as energy dispersive X-ray spectroscopy (EDX). The average crystallite size estimated by the broadening of XRPD peaks increases from 2.7 nm to 3.7 nm in the temperature range from 100 °C to 150 °C. HR-TEM images show that nanoparticles are arranged in aggregates with the 60-200 nm size. Theoretical estimation shows that the systems synthesized at higher temperatures more prone to the agglomeration. The full profile Reitveld analysis of XRPD data reveals the formation of hexagonal zinc sulfide structure, whereas electron diffraction data reveal also the formation of cubic zinc sulfide and claim the polymorphous character of the system. High energy resolution Zn K-edge XANES data unambiguously demonstrate the presence of a certain amount of the zinc oxide which is likely to have an amorphous structure and could not be detected by XRPD. Qualitative analysis of XANES data allows deriving ZnS/ZnO ratio as a function of synthesis temperature. EDX analysis depicts homogeneous distribution of ZnS and amorphous ZnO phases across the conglomerates. A complementary element-selective valence to core X-ray emission spectroscopy evidences formation of two-component system and confirms estimations of ZnS/ZnO fractions obtained by linear combination fit of XANES data.

X-ray astronomical spectroscopy

NASA Technical Reports Server (NTRS)

Holt, S. S.

1980-01-01

The current status of the X-ray spectroscopy of celestial X-ray sources, ranging from nearby stars to distant quasars, is reviewed. Particular emphasis is placed on the role of such spectroscopy as a useful and unique tool in the elucidation of the physical parameters of the sources. The spectroscopic analysis of degenerate and nondegenerate stellar systems, galactic clusters and active galactic nuclei, and supernova remnants is discussed.

Elemental mapping in a contemporary miniature by full-field X-ray fluorescence imaging with gaseous detector vs. scanning X-ray fluorescence imaging with polycapillary optics

NASA Astrophysics Data System (ADS)

Silva, A. L. M.; Cirino, S.; Carvalho, M. L.; Manso, M.; Pessanha, S.; Azevedo, C. D. R.; Carramate, L. F. N. D.; Santos, J. P.; Guerra, M.; Veloso, J. F. C. A.

2017-03-01

Energy dispersive X-ray imaging can be used in several research fields and industrial applications. Elemental mapping through energy dispersive X-ray imaging technique has become a promising method to obtain positional distribution of specific elements in a non-destructive way. To obtain the elemental distribution of a sample it is necessary to use instruments capable of providing a precise positioning together with a good energy resolution. Polycapillary beams together with silicon drift chamber detectors are used in several commercial systems and are considered state-of-the-art spectrometers, however they are usually very costly. A new concept of large energy dispersive X-ray imaging systems based on gaseous radiation detectors emerged in the last years enabling a promising 2D elemental detection at a very reduced price. The main goal of this work is to analyze a contemporary Indian miniature with both X-ray fluorescence imaging systems, the one based on a gaseous detector 2D-THCOBRA and the state-of-the-art spectrometer M4 Tornado, from Bruker. The performance of both systems is compared and evaluated in the context of the sample's analysis.

X-ray Measurements of a Thermo Scientific P385 DD Neutron Generator

DOE Office of Scientific and Technical Information (OSTI.GOV)

E.H. Seabury; D.L. Chichester; A.J. Caffrey

2001-08-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X-rays are a normal byproduct from a neutron generator and depending on their intensity and energy they can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum was measuredmore » with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x-rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60° between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and the x-ray emission appears to be axially symmetric within the neutron generator.« less

21 CFR 892.1750 - Computed tomography x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Computed tomography x-ray system. 892.1750 Section 892.1750 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... same axial plane taken at different angles. This generic type of device may include signal analysis and...

21 CFR 892.1750 - Computed tomography x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Computed tomography x-ray system. 892.1750 Section 892.1750 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... same axial plane taken at different angles. This generic type of device may include signal analysis and...

21 CFR 892.1630 - Electrostatic x-ray imaging system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Electrostatic x-ray imaging system. 892.1630 Section 892.1630 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... visible image. This generic type of device may include signal analysis and display equipment, patient and...

21 CFR 892.1750 - Computed tomography x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Computed tomography x-ray system. 892.1750 Section 892.1750 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... same axial plane taken at different angles. This generic type of device may include signal analysis and...

21 CFR 892.1750 - Computed tomography x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Computed tomography x-ray system. 892.1750 Section 892.1750 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... same axial plane taken at different angles. This generic type of device may include signal analysis and...

21 CFR 892.1630 - Electrostatic x-ray imaging system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Electrostatic x-ray imaging system. 892.1630 Section 892.1630 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... visible image. This generic type of device may include signal analysis and display equipment, patient and...

21 CFR 892.1630 - Electrostatic x-ray imaging system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Electrostatic x-ray imaging system. 892.1630 Section 892.1630 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... visible image. This generic type of device may include signal analysis and display equipment, patient and...

21 CFR 892.1750 - Computed tomography x-ray system.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Computed tomography x-ray system. 892.1750 Section 892.1750 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES... same axial plane taken at different angles. This generic type of device may include signal analysis and...

Adaptive x-ray threat detection using sequential hypotheses testing with fan-beam experimental data (Conference Presentation)

NASA Astrophysics Data System (ADS)

Thamvichai, Ratchaneekorn; Huang, Liang-Chih; Ashok, Amit; Gong, Qian; Coccarelli, David; Greenberg, Joel A.; Gehm, Michael E.; Neifeld, Mark A.

2017-05-01

We employ an adaptive measurement system, based on sequential hypotheses testing (SHT) framework, for detecting material-based threats using experimental data acquired on an X-ray experimental testbed system. This testbed employs 45-degree fan-beam geometry and 15 views over a 180-degree span to generate energy sensitive X-ray projection data. Using this testbed system, we acquire multiple view projection data for 200 bags. We consider an adaptive measurement design where the X-ray projection measurements are acquired in a sequential manner and the adaptation occurs through the choice of the optimal "next" source/view system parameter. Our analysis of such an adaptive measurement design using the experimental data demonstrates a 3x-7x reduction in the probability of error relative to a static measurement design. Here the static measurement design refers to the operational system baseline that corresponds to a sequential measurement using all the available sources/views. We also show that by using adaptive measurements it is possible to reduce the number of sources/views by nearly 50% compared a system that relies on static measurements.

Analytical characterization of a new mobile X-ray fluorescence and X-ray diffraction instrument combined with a pigment identification case study

NASA Astrophysics Data System (ADS)

Van de Voorde, Lien; Vekemans, Bart; Verhaeven, Eddy; Tack, Pieter; De Wolf, Robin; Garrevoet, Jan; Vandenabeele, Peter; Vincze, Laszlo

2015-08-01

A new, commercially available, mobile system combining X-ray diffraction and X-ray fluorescence has been evaluated which enables both elemental analysis and phase identification simultaneously. The instrument makes use of a copper or molybdenum based miniature X-ray tube and a silicon-Pin diode energy-dispersive detector to count the photons originating from the samples. The X-ray tube and detector are both mounted on an X-ray diffraction protractor in a Bragg-Brentano θ:θ geometry. The mobile instrument is one of the lightest and most compact instruments of its kind (3.5 kg) and it is thus very useful for in situ purposes such as the direct (non-destructive) analysis of cultural heritage objects which need to be analyzed on site without any displacement. The supplied software allows both the operation of the instrument for data collection and in-depth data analysis using the International Centre for Diffraction Data database. This paper focuses on the characterization of the instrument, combined with a case study on pigment identification and an illustrative example for the analysis of lead alloyed printing letters. The results show that this commercially available light-weight instrument is able to identify the main crystalline phases non-destructively, present in a variety of samples, with a high degree of flexibility regarding sample size and position.

Optics for coherent X-ray applications.

PubMed

Yabashi, Makina; Tono, Kensuke; Mimura, Hidekazu; Matsuyama, Satoshi; Yamauchi, Kazuto; Tanaka, Takashi; Tanaka, Hitoshi; Tamasaku, Kenji; Ohashi, Haruhiko; Goto, Shunji; Ishikawa, Tetsuya

2014-09-01

Developments of X-ray optics for full utilization of diffraction-limited storage rings (DLSRs) are presented. The expected performance of DLSRs is introduced using the design parameters of SPring-8 II. To develop optical elements applicable to manipulation of coherent X-rays, advanced technologies on precise processing and metrology were invented. With propagation-based coherent X-rays at the 1 km beamline of SPring-8, a beryllium window fabricated with the physical-vapour-deposition method was found to have ideal speckle-free properties. The elastic emission machining method was utilized for developing reflective mirrors without distortion of the wavefronts. The method was further applied to production of diffraction-limited focusing mirrors generating the smallest spot size in the sub-10 nm regime. To enable production of ultra-intense nanobeams at DLSRs, a low-vibration cooling system for a high-heat-load monochromator and advanced diagnostic systems to characterize X-ray beam properties precisely were developed. Finally, new experimental schemes for combinative nano-analysis and spectroscopy realised with novel X-ray optics are discussed.

NBSGSC - a FORTRAN program for quantitative x-ray fluorescence analysis. Technical note (final)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tao, G.Y.; Pella, P.A.; Rousseau, R.M.

1985-04-01

A FORTRAN program (NBSGSC) was developed for performing quantitative analysis of bulk specimens by x-ray fluorescence spectrometry. This program corrects for x-ray absorption/enhancement phenomena using the comprehensive alpha coefficient algorithm proposed by Lachance (COLA). NBSGSC is a revision of the program ALPHA and CARECAL originally developed by R.M. Rousseau of the Geological Survey of Canada. Part one of the program (CALCO) performs the calculation of theoretical alpha coefficients, and part two (CALCOMP) computes the composition of the analyte specimens. The analysis of alloys, pressed minerals, and fused specimens can currently be treated by the program. In addition to using measuredmore » x-ray tube spectral distributions, spectra from seven commonly used x-ray tube targets could also be calculated with an NBS algorithm included in the program. NBSGSC is written in FORTRAN IV for a Digital Equipment Corporation (DEC PDP-11/23) minicomputer using RLO2 firm disks and an RSX 11M operating system.« less

Searching for Intermediate Mass Black Holes in Ultraluminous X-ray Binaries

NASA Astrophysics Data System (ADS)

Fritze, Hannah; Wright, Simon; Kilgard, Roy

2018-01-01

X-ray observations of nearby galaxies provide one of the best laboratories in the universe for studying two exotic classes of object: black holes and neutron stars. These observations allow us to study the dramatic effect such objects have on their surroundings, as well as the high-energy physics involved in their emission. We conduct a volume-limited archival survey of X-ray sources in all galaxies observed with the Chandra X-ray observatory within 15 Mpc, and identify a set of ultraluminous X-ray sources for detailed spectral analysis. We perform this analysis with the aim of searching for signatures of spectral state transitions and super-Eddington accretion that could indicate the presence of an Intermediate Mass Black Hole (IMBH) binary system. Here, we identify 43 potential IMBH sources that have signatures of super-Eddington accretion. We plan to follow up this initial selection with a multiwavelength analysis of these sources, in order to place further constraints on their nature and surrounding environment.

Automated X-ray and Optical Analysis of the Virtual Observatory and Grid Computing

NASA Astrophysics Data System (ADS)

Ptak, A.; Krughoff, S.; Connolly, A.

2011-07-01

We are developing a system to combine the Web Enabled Source Identification with X-Matching (WESIX) web service, which emphasizes source detection on optical images,with the XAssist program that automates the analysis of X-ray data. XAssist is continuously processing archival X-ray data in several pipelines. We have established a workflow in which FITS images and/or (in the case of X-ray data) an X-ray field can be input to WESIX. Intelligent services return available data (if requested fields have been processed) or submit job requests to a queue to be performed asynchronously. These services will be available via web services (for non-interactive use by Virtual Observatory portals and applications) and through web applications (written in the Django web application framework). We are adding web services for specific XAssist functionality such as determining the exposure and limiting flux for a given position on the sky and extracting spectra and images for a given region. We are improving the queuing system in XAssist to allow for "watch lists" to be specified by users, and when X-ray fields in a user's watch list become publicly available they will be automatically added to the queue. XAssist is being expanded to be used as a survey planning tool when coupled with simulation software, including functionality for NuStar, eRosita, IXO, and the Wide-Field Xray Telescope (WFXT), as part of an end-to-end simulation/analysis system. We are also investigating the possibility of a dedicated iPhone/iPad app for querying pipeline data, requesting processing, and administrative job control. This work was funded by AISRP grant NNG06GE59G.

Remote analysis of planetary soils: X-ray diffractometer development

NASA Technical Reports Server (NTRS)

Gregory, J. C.

1973-01-01

A system is described suitable for remote low power mineralogical analysis of lunar, planetary, or asteroid soils. It includes an X-ray diffractometer, fluorescence spectrometer, and sample preparation system. A one Curie Fe-55 source provides a monochromatic X-ray beam of 5.9 keV. Seeman-Bohlin or focusing geometry is employed in the camera, allowing peak detection to proceed simultaneously at all angles and obviating the need for moving parts. The detector system is an array of 500-600 proportional counters with a wire-spacing of 1 mm. An electronics unit comprising preamplifier, postamplifier, window discriminators, and storage flipflops requiring only 3.5 milliwatts was designed and tested. Total instrument power is less than 5 watts. Powder diffraction patterns using a flat breadboard multiwire counter were recorded.

Direct measurement of mammographic X-ray spectra with a digital CdTe detection system.

PubMed

Abbene, Leonardo; Gerardi, Gaetano; Principato, Fabio; Del Sordo, Stefano; Raso, Giuseppe

2012-01-01

In this work we present a detection system, based on a CdTe detector and an innovative digital pulse processing (DPP) system, for high-rate X-ray spectroscopy in mammography (1-30 keV). The DPP system performs a height and shape analysis of the detector pulses, sampled and digitized by a 14-bit, 100 MHz ADC. We show the results of the characterization of the detection system both at low and high photon counting rates by using monoenergetic X-ray sources and a nonclinical X-ray tube. The detection system exhibits excellent performance up to 830 kcps with an energy resolution of 4.5% FWHM at 22.1 keV. Direct measurements of clinical molybdenum X-ray spectra were carried out by using a pinhole collimator and a custom alignment device. A comparison with the attenuation curves and the half value layer values, obtained from the measured and simulated spectra, from an ionization chamber and from a solid state dosimeter, also shows the accuracy of the measurements. These results make the proposed detection system a very attractive tool for both laboratory research, calibration of dosimeters and advanced quality controls in mammography.

Gold nanoparticle contrast agents in advanced X-ray imaging technologies.

PubMed

Ahn, Sungsook; Jung, Sung Yong; Lee, Sang Joon

2013-05-17

Recently, there has been significant progress in the field of soft- and hard-X-ray imaging for a wide range of applications, both technically and scientifically, via developments in sources, optics and imaging methodologies. While one community is pursuing extensive applications of available X-ray tools, others are investigating improvements in techniques, including new optics, higher spatial resolutions and brighter compact sources. For increased image quality and more exquisite investigation on characteristic biological phenomena, contrast agents have been employed extensively in imaging technologies. Heavy metal nanoparticles are excellent absorbers of X-rays and can offer excellent improvements in medical diagnosis and X-ray imaging. In this context, the role of gold (Au) is important for advanced X-ray imaging applications. Au has a long-history in a wide range of medical applications and exhibits characteristic interactions with X-rays. Therefore, Au can offer a particular advantage as a tracer and a contrast enhancer in X-ray imaging technologies by sensing the variation in X-ray attenuation in a given sample volume. This review summarizes basic understanding on X-ray imaging from device set-up to technologies. Then this review covers recent studies in the development of X-ray imaging techniques utilizing gold nanoparticles (AuNPs) and their relevant applications, including two- and three-dimensional biological imaging, dynamical processes in a living system, single cell-based imaging and quantitative analysis of circulatory systems and so on. In addition to conventional medical applications, various novel research areas have been developed and are expected to be further developed through AuNP-based X-ray imaging technologies.

SU-F-T-128: Dose-Volume Constraints for Particle Therapy Treatment Planning

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stewart, R; Smith, W; Hendrickson, K

2016-06-15

Purpose: Determine equivalent Organ at Risk (OAR) tolerance dose (TD) constraints for MV x-rays and particle therapy. Methods: Equivalent TD estimates for MV x-rays are determined from an isoeffect, regression-analysis of published and in-house constraints for various fractionation schedules (n fractions). The analysis yields an estimate of (α/β) for an OAR. To determine equivalent particle therapy constraints, the MV x-ray TD(n) values are divided by the RBE for DSB induction (RBE{sub DSB}) or cell survival (RBE{sub S}). Estimates of (RBE{sub DSB}) are computed using the Monte Carlo Damage Simulation, and estimates of RBES are computed using the Repair-Misrepair-Fixation (RMF) model.more » A research build of the RayStation™ treatment planning system implementing the above model is used to estimate (RBE{sub DSB}) for OARs of interest in 16 proton therapy patient plans (head and neck, thorax, prostate and brain). Results: The analysis gives an (α/β) estimate of about 20 Gy for the trachea and heart and 2–4 Gy for the esophagus, spine, and brachial plexus. Extrapolation of MV x-ray constraints (n = 1) to fast neutrons using RBE{sub DSB} = 2.7 are in excellent agreement with clinical experience (n = 10 to 20). When conventional (n > 30) x-ray treatments are used as the reference radiation, fast neutron RBE increased to a maximum of 6. For comparison to a constant RBE of 1.1, the RayStation™ analysis gave estimates of proton RBE{sub DSB} from 1.03 to 1.33 for OARs of interest. Conclusion: The presented system of models is a convenient formalism to synthesize from multiple sources of information a set of self-consistent plan constraints for MV x-ray and hadron therapy treatments. Estimates of RBE{sub DSB} from the RayStation™ analysis differ substantially from 1.1 and vary among patients and treatment sites. A treatment planning system that incorporates patient and anatomy-specific corrections in proton RBE would create opportunities to increase the therapeutic ratio. The research build of the RayStation used in the study was made available to the University of Washington free of charge. RaySearch Laboratories did not provide any monetary support for the reported studies.« less

Coronal temperatures of unusually active K-dwarf binary systems

NASA Technical Reports Server (NTRS)

Stern, Robert A.

1994-01-01

We report the results of a ROSAT pointed study of 4 BY Dra systems. Good quality pulse-height spectra are available from all four systems. Except for a required interstellar absorption component in HD 319139, the four systems have remarkably similar x-ray spectra; the two systems BD +22deg.669 and BD +23deg.635 look virtually identical in x rays. Analysis of the 4 x-ray spectra reveals that, in all cases, a single-temperature hot plasma (RS or Mewe) spectra is inadequate to fit the data, and two temperatures are required. We present examples of fitted pulse-height spectra and chi squared contours in kT(sub 1)-kT(sub 2) space.

Grazing Incidence Optics for X-rays Interferometry

NASA Technical Reports Server (NTRS)

Shipley, Ann; Zissa, David; Cash, Webster; Joy, Marshall

1999-01-01

Grazing incidence mirror parameters and constraints for x-ray interferometry are described. We present interferometer system tolerances and ray trace results used to define mirror surface accuracy requirements. Mirror material, surface figure, roughness, and geometry are evaluated based on analysis results. We also discuss mirror mount design constraints, finite element analysis, environmental issues, and solutions. Challenges associated with quantifying high accuracy mirror surface quality are addressed and test results are compared with theoretical predictions.

Method and apparatus for digitally based high speed x-ray spectrometer

DOEpatents

Warburton, W.K.; Hubbard, B.

1997-11-04

A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a ``hardwired`` processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer. 19 figs.

Method and apparatus for digitally based high speed x-ray spectrometer

DOEpatents

Warburton, William K.; Hubbard, Bradley

1997-01-01

A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a "hardwired" processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer.

High resolution projection X-ray microscope equipped with fluorescent X-ray analyzer and its applications

NASA Astrophysics Data System (ADS)

Minami, K.; Saito, Y.; Kai, H.; Shirota, K.; Yada, K.

2009-09-01

We have newly developed an open type fine-focus X-ray tube "TX-510" to realize a spatial resolution of 50nm and to radiate low energy characteristic X-rays for giving high absorption contrast to images of microscopic organisms. The "TX-510" employs a ZrO/W(100) Schottky emitter and an "In-Lens Field Emission Gun". The key points of the improvements are (1) reduced spherical aberration coefficient of magnetic objective lens, (2) easy and accurate focusing, (3) newly designed astigmatism compensator, (4) segmented thin film target for interchanging the target materials by electron beam shift and (5) fluorescent X-ray analysis system.

Soft X-ray astronomy using grazing incidence optics

NASA Technical Reports Server (NTRS)

Davis, John M.

1989-01-01

The instrumental background of X-ray astronomy with an emphasis on high resolution imagery is outlined. Optical and system performance, in terms of resolution, are compared and methods for improving the latter in finite length instruments described. The method of analysis of broadband images to obtain diagnostic information is described and is applied to the analysis of coronal structures.

Searching for X-ray emission from AGB stars

NASA Astrophysics Data System (ADS)

Ramstedt, S.; Montez, R.; Kastner, J.; Vlemmings, W. H. T.

2012-07-01

Context. Magnetic fields have been measured around asymptotic giant branch (AGB) stars of all chemical types using maser polarization observations. If present, a large-scale magnetic field would lead to X-ray emission, which should be observable using current X-ray observatories. Aims: The aim is to search the archival data for AGB stars that are intrinsic X-ray emitters. Methods: We have searched the ROSAT, CXO, and XMM-Newton archives for serendipitous X-ray observations of a sample of ~500 AGB stars. We specifically searched for the AGB stars detected with GALEX. The data is calibrated, analyzed and the X-ray luminosities and temperatures are estimated as functions of the circumstellar absorption. Results: We identify 13 AGB stars as having either serendipitous or targeted observations in the X-ray data archives, however for a majority of the sources the detailed analysis show that the detections are questionable. Two new sources are detected by ROSAT: T Dra and R UMa. The spectral analysis suggests that the emission associated with these sources could be due to coronal activity or interaction across a binary system. Conclusions: Further observations of the detected sources are necessary to clearly determine the origin of the X-ray emission. Moreover, additional objects should be subject to targeted X-ray observations in order to achieve better constraints for the magnetic fields around AGB stars. Appendices are available in electronic form at http://www.aanda.org

X-ray monitoring optical elements

DOEpatents

Stoupin, Stanislav; Shvydko, Yury; Katsoudas, John; Blank, Vladimir D.; Terentyev, Sergey A.

2016-12-27

An X-ray article and method for analyzing hard X-rays which have interacted with a test system. The X-ray article is operative to diffract or otherwise process X-rays from an input X-ray beam which have interacted with the test system and at the same time provide an electrical circuit adapted to collect photoelectrons emitted from an X-ray optical element of the X-ray article to analyze features of the test system.

Some Aspects of the Wavelength Dispersive X-Ray Determination of Fluorine Content in Various Matrices

NASA Astrophysics Data System (ADS)

Boča, M.; Gurišová, V.; Šimko, F.

2017-05-01

X-ray fluorescent signals of F Kα, Na Kα, Cl Kα, K Kα, and Ta Lα were measured by WD-XRF for various fluorine-containing systems: K2TaF7, Na3AlF6, K2ZrF6, NaF, and LiF (with NaCl and wax as additional additives). The data were recorded for 41 samples (in the form of pellets prepared in the laboratory) by more than 200 scans. The analysis of the measured fluorine X-ray fluorescence intensities demonstrated that the balance between absorption and enhancement effects depends strongly on the presence and concentration of other elements in the system. The experimental intensities of X-ray fluorescent radiation of fluorine for different systems with comparable fluorine content could differ by as much as 500%.

The nature of the cataclysmic variable PT Per

NASA Astrophysics Data System (ADS)

Watson, M. G.; Bruce, A.; MacLeod, C.; Osborne, J. P.; Schwope, A. D.

2016-08-01

We present a study of the cataclysmic variable star PT Per based on archival XMM-Newton X-ray data and new optical spectroscopy from the William Herschel Telescope (WHT) with Intermediate dispersion Spectrograph and Imaging System (ISIS). The X-ray data show deep minima which recur at a period of 82 min and a hard, unabsorbed X-ray spectrum. The optical spectra of PT Per show a relatively featureless blue continuum. From an analysis of the X-ray and optical data we conclude that PT Per is likely to be a magnetic cataclysmic variable of the polar class in which the minima correspond to those phase intervals when the accretion column rotates out of the field of view of the observer. We suggest that the optical spectrum, obtained around 4 yr after the X-ray coverage, is dominated by the white dwarf in the system, implying that PT Per was in a low accretion state at the time of the observations. An analysis of the likely system parameters for PT Per suggests a distance of ≈90 pc and a very low mass secondary, consistent with the idea that PT Per is a `period-bounce' binary. Matching the observed absorption features in the optical spectrum with the expected Zeeman components constrains the white dwarf polar field to be Bp ≈ 25-27 MG.

XMM-Newton study of the supersoft symbiotic system Draco C1

NASA Astrophysics Data System (ADS)

Saeedi, Sara; Sasaki, Manami; Ducci, Lorenzo

2018-01-01

We present the results of the analysis of thirty-one XMM-Newton observations of the symbiotic star Draco C1 located in the Draco dwarf spheroidal galaxy. This object had been identified as a supersoft source based on ROSAT data. We analysed X-ray, ultraviolet (UV) and optical data taken with XMM-Newton in order to obtain the physical parameters and the geometry of the system. We have also performed the first X-ray timing analysis of Draco C1. The X-ray spectrum is well fitted with a blackbody model with a temperature of (1.8 ± 0.3) × 105 K. We obtained a bolometric luminosity of ≳1038 erg s-1 for the white dwarf. The X-ray spectrum and luminosity suggest stable nuclear burning on the surface of the white dwarf. The low column density derived from the X-ray spectrum is consistent with the lack of nebular lines found in previous UV studies. The long-term variability in the optical and the UV suggests that the system is not observed face-on and that the variability is caused by the reflection effect. For the red giant companion, we estimate a radius of ∼110 R⊙ and an upper limit ≲1.5 M⊙ for its mass assuming Roche lobe overflow.

Photometric, Spectroscopic, and X-ray Analysis of the Cool Algol BD+05 706

NASA Astrophysics Data System (ADS)

Torres, G.; Mader, J.; Marschall, L. A.; Neuhaeuser, R.; Duffy, A. S.

2000-12-01

BD+05 706 is an example of a rare class of a dozen or so interacting binaries called ``cool Algols", in which both components of the system are late-type stars. By contrast, the ``classical Algols" are systems in which the star transfering mass is of late spectral type, but the mass gainer is much hotter. BD+05 706 was shown previously to be eclipsing (Marschall, Torres & Neuhaeuser 1998, BAAS, 30, 835). In this paper we report our complete analysis of BVRI light curves for the system obtained at Gettysburg College Observatory, together with spectroscopy from the Harvard-Smithsonian Center for Astrophysics reported previously (Torres, Neuhaeuser & Wichmann 1998, AJ, 115, 2028), and X-ray observations obtained with the ROSAT satellite. Our light curve analysis indicates the presence of spots, most likely on the more massive, active component (primary), which change from season to season. Our results confirm the semi-detached nature of the system, and combined with the spectroscopy they have allowed us to obtain the most precise absolute masses and radii for any object of this class. Our X-ray light curve for BD+05 706 shows the primary eclipse clearly, but no sign of a secondary eclipse, confirming that the primary is the active star. Strong X-ray flares are also visible.

Formation and Evolution of X-ray Binaries

NASA Astrophysics Data System (ADS)

Fragkos, Anastasios

X-ray binaries - mass-transferring binary stellar systems with compact object accretors - are unique astrophysical laboratories. They carry information about many complex physical processes such as star formation, compact object formation, and evolution of interacting binaries. My thesis work involves the study of the formation and evolution of Galactic and extra-galacticX-ray binaries using both detailed and realistic simulation tools, and population synthesis techniques. I applied an innovative analysis method that allows the reconstruction of the full evolutionary history of known black hole X-ray binaries back to the time of compact object formation. This analysis takes into account all the available observationally determined properties of a system, and models in detail four of its evolutionary evolutionary phases: mass transfer through the ongoing X-ray phase, tidal evolution before the onset of Roche-lobe overflow, motion through the Galactic potential after the formation of the black hole, and binary orbital dynamics at the time of core collapse. Motivated by deep extra-galactic Chandra survey observations, I worked on population synthesis models of low-mass X-ray binaries in the two elliptical galaxies NGC3379 and NGC4278. These simulations were targeted at understanding the origin of the shape and normalization of the observed X-ray luminosity functions. In a follow up study, I proposed a physically motivated prescription for the modeling of transient neutron star low-mass X-ray binary properties, such as duty cycle, outburst duration and recurrence time. This prescription enabled the direct comparison of transient low-mass X-ray binary population synthesis models to the Chandra X-ray survey of the two ellipticals NGC3379 and NGC4278. Finally, I worked on population synthesismodels of black holeX-ray binaries in the MilkyWay. This work was motivated by recent developments in observational techniques for the measurement of black hole spin magnitudes in black hole X-ray binaries. The accuracy of these techniques depend on misalignment of the black hole spin with respect to the orbital angular momentum. In black hole X-ray binaries, this misalignment can occur during the supernova explosion that forms the compact object. In this study, I presented population synthesis models of Galactic black hole X-ray binaries, and examined the distribution of misalignment angles, and its dependence on the model parameters.

Differential phase contrast X-ray imaging system and components

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stutman, Daniel; Finkenthal, Michael

2017-11-21

A differential phase contrast X-ray imaging system includes an X-ray illumination system, a beam splitter arranged in an optical path of the X-ray illumination system, and a detection system arranged in an optical path to detect X-rays after passing through the beam splitter.

A normal incidence X-ray telescope

NASA Technical Reports Server (NTRS)

Golub, Leon

1987-01-01

The postflight performance evaluation of the X-ray telescope was summarized. All payload systems and subsystems performed well within acceptable limits, with the sole exception of the light-blocking prefilters. Launch, flight and recovery were performed in a fully satisfactory manner. The payload was recovered in a timely manner and in excellent condition. The prefilter performance analysis showed that no X-ray images were detected on the processed flight film. Recommendations for improved performance are listed.

The HEAO-A Scanning Modulation Collimator instrument

NASA Technical Reports Server (NTRS)

Roy, A.; Ballas, J.; Jagoda, N.; Mckinnon, P.; Ramsey, A.; Wester, E.

1977-01-01

The Scanning Modulation Collimator X-ray instrument for the HEAO-A satellite was designed to measure celestial radiation in the range between 1 and 15 KeV and to resolve, and correlate, the position of X-ray sources with visible light sources on the celestial sphere to within 5 arc seconds. The positional accuracy is made possible by mechanical collimation of the X-ray sources viewed by the instrument. High sensitivity is provided from two systems each containing four gas filled proportional counters followed by preamplification, signal summing, pulse height analysis, pulse shape discrimination, X-ray event accumulators and telemetry processing electronics.

Accretion disk dynamics in X-ray binaries

NASA Astrophysics Data System (ADS)

Peris, Charith Srian

Accreting X-ray binaries consist of a normal star which orbits a compact object with the former transferring matter onto the later via an accretion disk. These accretion disks emit radiation across the entire electromagnetic spectrum. This thesis exploits two regions of the spectrum, exploring the (1) inner disk regions of an accreting black hole binary, GRS1915+105, using X-ray spectral analysis and (2) the outer accretion disks of a set of neutron star and black hole binaries using Doppler Tomography applied on optical observations. X-ray spectral analysis of black hole binary GRS1915+105: GRS1915+105 stands out as an exceptional black hole primarily due to the wild variability exhibited by about half of its X-ray observations. This study focused on the steady X-ray observations of the source, which were found to exhibit significant curvature in the harder coronal component within the RXTE/PCA band-pass. The roughly constant inner-disk radius seen in a majority of the steady-soft observations is strongly reminiscent of canonical soft state black-hole binaries. Remarkably, the steady-hard observations show the presence of growing truncation in the inner-disk. A majority of the steady observations of GRS1915+105 map to the states observed in canonical black hole binaries which suggests that within the complexity of this source is a simpler underlying basis of states. Optical tomography of X-ray binary systems: Doppler tomography was applied to the strong line features present in the optical spectra of X-ray binaries in order to determine the geometric structure of the systems' emitting regions. The point where the accretion stream hits the disk, also referred to as the "hotspot'', is clearly identified in the neutron star system V691 CrA and the black hole system Nova Muscae 1991. Evidence for stream-disk overflows exist in both systems, consistent with relatively high accretion rates. In contrast, V926 Sco does not show evidence for the presence of a hotspot which is consistent with its lower accretion state. The donor stars in V691 CrA and Nova Muscae 1991 were also detected.

Quantitative analysis of crystalline pharmaceuticals in tablets by pattern-fitting procedure using X-ray diffraction pattern.

PubMed

Takehira, Rieko; Momose, Yasunori; Yamamura, Shigeo

2010-10-15

A pattern-fitting procedure using an X-ray diffraction pattern was applied to the quantitative analysis of binary system of crystalline pharmaceuticals in tablets. Orthorhombic crystals of isoniazid (INH) and mannitol (MAN) were used for the analysis. Tablets were prepared under various compression pressures using a direct compression method with various compositions of INH and MAN. Assuming that X-ray diffraction pattern of INH-MAN system consists of diffraction intensities from respective crystals, observed diffraction intensities were fitted to analytic expression based on X-ray diffraction theory and separated into two intensities from INH and MAN crystals by a nonlinear least-squares procedure. After separation, the contents of INH were determined by using the optimized normalization constants for INH and MAN. The correction parameter including all the factors that are beyond experimental control was required for quantitative analysis without calibration curve. The pattern-fitting procedure made it possible to determine crystalline phases in the range of 10-90% (w/w) of the INH contents. Further, certain characteristics of the crystals in the tablets, such as the preferred orientation, size of crystallite, and lattice disorder were determined simultaneously. This method can be adopted to analyze compounds whose crystal structures are known. It is a potentially powerful tool for the quantitative phase analysis and characterization of crystals in tablets and powders using X-ray diffraction patterns. Copyright 2010 Elsevier B.V. All rights reserved.

Performance of ASTRO-H Hard X-Ray Telescope (HXT)

NASA Technical Reports Server (NTRS)

Awaki, Hisamitsu; Kunieda, Hideyo; Ishida, Manabu; Matsumoto, Hironori; Furuzawa, Akihiro; Haba, Yohsito; Hayashi, Takayuki; Iizuka, Ryo; Ishibashi, Kazunori; Itoh, Masayuki;

Crystallization and X-ray diffraction analysis of a catalytic domain of hyperthermophilic chitinase from Pyrococcus furiosus

PubMed Central

Mine, Shouhei; Nakamura, Tsutomu; Hirata, Kunio; Ishikawa, Kazuhiko; Hagihara, Yoshihisa; Uegaki, Koichi

2006-01-01

The crystallization and preliminary X-ray diffraction analysis of a catalytic domain of chitinase (PF1233 gene) from the hyperthermophilic archaeon Pyrococcus furiosus is reported. The recombinant protein, prepared using an Escherichia coli expression system, was crystallized by the hanging-drop vapour-diffusion method. An X-ray diffraction data set was collected at the undulator beamline BL44XU at SPring-8 to a resolution of 1.50 Å. The crystals belong to space group P212121, with unit-cell parameters a = 90.0, b = 92.8, c = 107.2 Å. PMID:16880559

Materials identification using a small-scale pixellated x-ray diffraction system

NASA Astrophysics Data System (ADS)

O'Flynn, D.; Crews, C.; Drakos, I.; Christodoulou, C.; Wilson, M. D.; Veale, M. C.; Seller, P.; Speller, R. D.

2016-05-01

A transmission x-ray diffraction system has been developed using a pixellated, energy-resolving detector (HEXITEC) and a small-scale, mains operated x-ray source (Amptek Mini-X). HEXITEC enables diffraction to be measured without the requirement of incident spectrum filtration, or collimation of the scatter from the sample, preserving a large proportion of the useful signal compared with other diffraction techniques. Due to this efficiency, sufficient molecular information for material identification can be obtained within 5 s despite the relatively low x-ray source power. Diffraction data are presented from caffeine, hexamine, paracetamol, plastic explosives and narcotics. The capability to determine molecular information from aspirin tablets inside their packaging is demonstrated. Material selectivity and the potential for a sample classification model is shown with principal component analysis, through which each different material can be clearly resolved.

49 CFR 1546.209 - Use of X-ray systems.

Code of Federal Regulations, 2012 CFR

2012-10-01

... 49 Transportation 9 2012-10-01 2012-10-01 false Use of X-ray systems. 1546.209 Section 1546.209... Use of X-ray systems. (a) TSA authorization required. No foreign air carrier may use any X-ray system... security program. TSA authorizes foreign air carriers to use X-ray systems for inspecting accessible...

First use of portable system coupling X-ray diffraction and X-ray fluorescence for in-situ analysis of prehistoric rock art.

PubMed

Beck, L; Rousselière, H; Castaing, J; Duran, A; Lebon, M; Moignard, B; Plassard, F

2014-11-01

Study of prehistoric art is playing a major role in the knowledge of human evolution. Many scientific methods are involved in this investigation including chemical analysis of pigments present on artefacts or applied to cave walls. In the past decades, the characterization of coloured materials was carried on by taking small samples. This procedure had two main disadvantages: slight but existing damage of the paintings and limitation of the number of samples. Thanks to the advanced development of portable systems, in-situ analysis of pigment in cave can be now undertaken without fear for this fragile Cultural Heritage. For the first time, a portable system combining XRD and XRF was used in an underground and archaeological environment for prehistoric rock art studies. In-situ non-destructive analysis of black prehistoric drawings and determination of their composition and crystalline structure were successfully carried out. Original results on pigments used 13,000 years ago in the cave of Rouffignac (France) were obtained showing the use of two main manganese oxides: pyrolusite and romanechite. The capabilities of the portable XRD-XRF system have been demonstrated for the characterization of pigments as well as for the analysis of rock in a cave environment. This first in-situ experiment combining X-ray diffraction and X-ray fluorescence open up new horizons and can fundamentally change our approach of rock art studies. Copyright © 2014 Elsevier B.V. All rights reserved.

XAssist: A System for the Automation of X-ray Astrophysics Analysis

NASA Astrophysics Data System (ADS)

Ptak, A.; Griffiths, R.

XAssist is a NASA AISR-funded project for the automation of X-ray astrophysics, with emphasis on galaxies. It is nearing completion of its initially funded effort, and is working well for Chandra and ROSAT data. Initial support for XMM-Newton data is present as well. It is capable of data reprocessing, source detection, and preliminary spatial, temporal and spectral analysis for each source with sufficient counts. The bulk of the system is written in Python, which in turn drives underlying software (CIAO for Chandra data, etc.). Future work will include a GUI (mainly for beginners and status monitoring) and the exposure of at least some functionality as web services. The latter will help XAssist to eventually become part of the VO, making advanced queries possible, such as determining the X-ray fluxes of counterparts to HST or SDSS sources (including the use of unpublished X-ray data), and add the ability of ``on-the-fly'' X-ray processing. Pipelines are running on ROSAT, Chandra and now XMM-Newton observations of galaxies to demonstrate XAssist's capabilities, and the results are available online (in real time) at http://www.xassist.org. XAssist itself as well as various associated projects are available for download.

Lightning x-rays inside thunderclouds, in-flight measurements on-board an A350

NASA Astrophysics Data System (ADS)

van Deursen, Alexander; Kochkin, Pavlo; de Boer, Alte; Bardet, Michiel; Boissin, Jean-François

2015-04-01

Thunderstorms emit bursts of energetic radiation. Moreover, lightning stepped leader produces x-ray pulses. The phenomena, their interrelation and impact on Earth's atmosphere and near space are not fully understood yet. The In-flight Lightning Strike Damage Assessment System ILDAS was developed in an EU FP6 project ( http://ildas.nlr.nl/ ) to provide information on threat that lightning poses to aircraft. It is intended to localize the lightning attachment points in order to reduce maintenance time and to build statics on lightning current. The system consists of 2 E-field sensors and a varying number of H-field sensors. It has recently been enhanced by two LaBr3 scintillation detectors inside the aircraft. The scintillation detectors are sensitive to x- and gamma-rays above 30 keV. The entire system is installed on-board of an A-350 aircraft and digitizes data with 100Msamples/sec rate when triggered by lightning. A continuously monitoring channel counts the number of occurrences that the x-ray signal exceeds a set of trigger levels. In the beginning of 2014 the aircraft flew through thunderstorm cells collecting the data from the sensors. The x-rays generated by the lightning flash are measured in synchronization better than 40 ns with the lightning current information during a period of 1 second around the strike. The continuous channel stores x-ray information with very limited time and amplitude resolution during the whole flight. That channel would allow x-rays from cosmic ray background, TGFs and continuous gamma-ray glow of thundercloud outside the 1 s time window. In the EGU2014 we presented the ILDAS system and showed that the x-ray detection works as intended. Fast x-ray bursts have been detected during stepped/dart stepped leaders and during interception of lightning. Data analysis of continuous channel recordings will be presented as well.

Crystallization and preliminary X-ray diffraction analysis of a chitin-binding domain of hyperthermophilic chitinase from Pyrococcus furiosus

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nakamura, Tsutomu; Ishikawa, Kazuhiko; Hagihara, Yoshihisa

The expression, purification and preliminary X-ray diffraction studies of a chitin-binding domain of the chitinase from P. furiosus are reported. The crystallization and preliminary X-ray diffraction analysis of the chitin-binding domain of chitinase from a hyperthermophilic archaeon, Pyrococcus furiosus, are reported. The recombinant protein was prepared using an Escherichia coli overexpression system and was crystallized by the hanging-drop vapour-diffusion method. An X-ray diffraction data set was collected to 1.70 Å resolution. The crystal belonged to space group P4{sub 3}2{sub 1}2 or P4{sub 1}2{sub 1}2. The unit-cell parameters were determined to be a = b = 48.8, c = 85.0 Å.

A Coordinated X-Ray and Optical Campaign of the Nearest Massive Eclipsing Binary, Delta Orionis Aa. I. Overview of the X-Ray Spectrum

NASA Technical Reports Server (NTRS)

Corcoran, M. F.; Nicholas, J. S.; Pablo, H.; Shenar, T.; Pollock, A. M. T.; Waldron, W. L.; Moffat, A. F. J.; Richardson, N. D.; Russell, C. M. P.; Hamaguchi, K.;

A COORDINATED X-RAY AND OPTICAL CAMPAIGN OF THE NEAREST MASSIVE ECLIPSING BINARY, δ ORIONIS Aa. I. OVERVIEW OF THE X-RAY SPECTRUM

DOE Office of Scientific and Technical Information (OSTI.GOV)

Corcoran, M. F.; Hamaguchi, K.; Nichols, J. S.

2015-08-20

We present an overview of four deep phase-constrained Chandra HETGS X-ray observations of δ Ori A. Delta Ori A is actually a triple system that includes the nearest massive eclipsing spectroscopic binary, δ Ori Aa, the only such object that can be observed with little phase-smearing with the Chandra gratings. Since the fainter star, δ Ori Aa2, has a much lower X-ray luminosity than the brighter primary (δ Ori Aa1), δ Ori Aa provides a unique system with which to test the spatial distribution of the X-ray emitting gas around δ Ori Aa1 via occultation by the photosphere of, andmore » wind cavity around, the X-ray dark secondary. Here we discuss the X-ray spectrum and X-ray line profiles for the combined observation, having an exposure time of nearly 500 ks and covering nearly the entire binary orbit. The companion papers discuss the X-ray variability seen in the Chandra spectra, present new space-based photometry and ground-based radial velocities obtained simultaneously with the X-ray data to better constrain the system parameters, and model the effects of X-rays on the optical and UV spectra. We find that the X-ray emission is dominated by embedded wind shock emission from star Aa1, with little contribution from the tertiary star Ab or the shocked gas produced by the collision of the wind of Aa1 against the surface of Aa2. We find a similar temperature distribution to previous X-ray spectrum analyses. We also show that the line half-widths are about 0.3−0.5 times the terminal velocity of the wind of star Aa1. We find a strong anti-correlation between line widths and the line excitation energy, which suggests that longer-wavelength, lower-temperature lines form farther out in the wind. Our analysis also indicates that the ratio of the intensities of the strong and weak lines of Fe xvii and Ne x are inconsistent with model predictions, which may be an effect of resonance scattering.« less

Analysis of ultraviolet and X-ray observations of three homologous solar flares from SMM

NASA Technical Reports Server (NTRS)

Cheng, Chung-Chieh; Pallavicini, Roberto

1987-01-01

Three homologous flares observed in the UV lines of Fe XXI and O V and in X-rays from the SMM were studied. It was found that: (1) the homology of the flares was most noticeable in Fe XXI and soft X-ray emissions; (2) the three flares shared many of the same loop footprints which were located in O V bright kernals associated with hard X-ray bursts; and (3) in spite of the strong spatial homology, the temporal evolution in UV and X-ray emissions varied from flare to flare. A comparison between the UV observations and photospheric magnetograms revealed that the basic flare configuration was a complex loop system consisting of many loops or bundles of loops.

The x-ray light valve: a potentially low-cost, digital radiographic imaging system-concept and implementation considerations.

PubMed

Webster, Christie Ann; Koprinarov, Ivaylo; Germann, Stephen; Rowlands, J A

2008-03-01

New x-ray radiographic systems based on large-area flat-panel technology have revolutionized our capability to produce digital x-ray images. However, these imagers are extraordinarily expensive compared to the systems they are replacing. Hence, there is a need for a low-cost digital imaging system for general applications in radiology. A novel potentially low-cost radiographic imaging system based on established technologies is proposed-the X-Ray Light Valve (XLV). This is a potentially high-quality digital x-ray detector made of a photoconducting layer and a liquid-crystal cell, physically coupled in a sandwich structure. Upon exposure to x rays, charge is collected on the surface of the photoconductor. This causes a change in the optical properties of the liquid-crystal cell and a visible image is generated. Subsequently, it is digitized by a scanned optical imager. The image formation is based on controlled modulation of light from an external source. The operation and practical implementation of the XLV system are described. The potential performance of the complete system and issues related to sensitivity, spatial resolution, noise, and speed are discussed. The feasibility of clinical use of an XLV device based on amorphous selenium (a-Se) as the photoconductor and a reflective electrically controlled birefringence cell is analyzed. The results of our analysis indicate that the XLV can potentially be adapted to a wide variety of radiographic tasks.

Optics for coherent X-ray applications

PubMed Central

Yabashi, Makina; Tono, Kensuke; Mimura, Hidekazu; Matsuyama, Satoshi; Yamauchi, Kazuto; Tanaka, Takashi; Tanaka, Hitoshi; Tamasaku, Kenji; Ohashi, Haruhiko; Goto, Shunji; Ishikawa, Tetsuya

2014-01-01

Developments of X-ray optics for full utilization of diffraction-limited storage rings (DLSRs) are presented. The expected performance of DLSRs is introduced using the design parameters of SPring-8 II. To develop optical elements applicable to manipulation of coherent X-rays, advanced technologies on precise processing and metrology were invented. With propagation-based coherent X-rays at the 1 km beamline of SPring-8, a beryllium window fabricated with the physical-vapour-deposition method was found to have ideal speckle-free properties. The elastic emission machining method was utilized for developing reflective mirrors without distortion of the wavefronts. The method was further applied to production of diffraction-limited focusing mirrors generating the smallest spot size in the sub-10 nm regime. To enable production of ultra-intense nanobeams at DLSRs, a low-vibration cooling system for a high-heat-load monochromator and advanced diagnostic systems to characterize X-ray beam properties precisely were developed. Finally, new experimental schemes for combinative nano-analysis and spectroscopy realised with novel X-ray optics are discussed. PMID:25177986

Automatic tool alignment in a backscatter X-ray scanning system

DOEpatents

Garretson, Justin; Hobart, Clinton G.; Gladwell, Thomas S.; Monda, Mark J.

2015-11-17

Technologies pertaining to backscatter x-ray scanning systems are described herein. The backscatter x-ray scanning system includes an x-ray source, which directs collimated x-rays along a plurality of output vectors towards a target. A detector detects diffusely reflected x-rays subsequent to respective collimated x-rays impacting the target, and outputs signals indicative of parameters of the detected x-rays. An image processing system generates an x-ray image based upon parameters of the detected x-rays, wherein each pixel in the image corresponds to a respective output vector. A user selects a particular portion of the image, and a medical device is positioned such that its directional axis is coincident with the output vector corresponding to at least one pixel in the portion of the image.

Automatic tool alignment in a backscatter x-ray scanning system

DOEpatents

Garretson, Justin; Hobart, Clinton G.; Gladwell, Thomas S.; Monda, Mark J.

2015-06-16

Technologies pertaining to backscatter x-ray scanning systems are described herein. The backscatter x-ray scanning system includes an x-ray source, which directs collimated x-rays along a plurality of output vectors towards a target. A detector detects diffusely reflected x-rays subsequent to respective collimated x-rays impacting the target, and outputs signals indicative of parameters of the detected x-rays. An image processing system generates an x-ray image based upon parameters of the detected x-rays, wherein each pixel in the image corresponds to a respective output vector. A user selects a particular portion of the image, and a tool is positioned such that its directional axis is coincident with the output vector corresponding to at least one pixel in the portion of the image.

Performance of a gaseous detector based energy dispersive X-ray fluorescence imaging system: Analysis of human teeth treated with dental amalgam

NASA Astrophysics Data System (ADS)

Silva, A. L. M.; Figueroa, R.; Jaramillo, A.; Carvalho, M. L.; Veloso, J. F. C. A.

2013-08-01

Energy dispersive X-ray fluorescence (EDXRF) imaging systems are of great interest in many applications of different areas, once they allow us to get images of the spatial elemental distribution in the samples. The detector system used in this study is based on a micro patterned gas detector, named Micro-Hole and Strip Plate. The full field of view system, with an active area of 28 × 28 mm2 presents some important features for EDXRF imaging applications, such as a position resolution below 125 μm, an intrinsic energy resolution of about 14% full width at half maximum for 5.9 keV X-rays, and a counting rate capability of 0.5 MHz. In this work, analysis of human teeth treated by dental amalgam was performed by using the EDXRF imaging system mentioned above. The goal of the analysis is to evaluate the system capabilities in the biomedical field by measuring the drift of the major constituents of a dental amalgam, Zn and Hg, throughout the tooth structures. The elemental distribution pattern of these elements obtained during the analysis suggests diffusion of these elements from the amalgam to teeth tissues.

Design of an imaging microscope for soft X-ray applications

NASA Astrophysics Data System (ADS)

Hoover, Richard B.; Shealy, David L.; Gabardi, David R.; Walker, Arthur B. C., Jr.; Lindblom, Joakim F.

1988-01-01

An imaging soft X-ray microscope with a spatial resolution of 0.1 micron and normal incidence multilayer optics is discussed. The microscope has a Schwarzschild configuration, which consists of two concentric spherical mirrors with radii of curvature which minimize third-order spherical aberration, coma, and astigmatism. The performance of the Stanford/MSFC Cassegrain X-ray telescope and its relevance to the present microscope are addressed. A ray tracing analysis of the optical system indicates that diffraction-limited performance can be expected for an object height of 0.2 mm.

A microanalysis approach to investigate problems encountered in mycology.

PubMed Central

Thibaut, M.; Ansel, M.; de Azevedo Carneiro, J.

1978-01-01

X-ray microanalysis has been applied to the study of pathogenic fungi for the acquisition of chemical information. The technique of combined scanning electron microscopy and wavelength dispersive spectrometry is described. The chemical analysis depends on the characteristic x-ray spectrum excited by the electrons passing through the sample. This spectrum is analyzed by x-ray wavelength dispersion using crystal spectrometers. All the elements of the periodic system above beryllium can be detected with good sensitivity. PMID:619693

Software to model AXAF-I image quality

NASA Technical Reports Server (NTRS)

Ahmad, Anees; Feng, Chen

1995-01-01

A modular user-friendly computer program for the modeling of grazing-incidence type x-ray optical systems has been developed. This comprehensive computer software GRAZTRACE covers the manipulation of input data, ray tracing with reflectivity and surface deformation effects, convolution with x-ray source shape, and x-ray scattering. The program also includes the capabilities for image analysis, detector scan modeling, and graphical presentation of the results. A number of utilities have been developed to interface the predicted Advanced X-ray Astrophysics Facility-Imaging (AXAF-I) mirror structural and thermal distortions with the ray-trace. This software is written in FORTRAN 77 and runs on a SUN/SPARC station. An interactive command mode version and a batch mode version of the software have been developed.

Anisotropic imaging performance in indirect x-ray imaging detectors

DOE Office of Scientific and Technical Information (OSTI.GOV)

Badano, Aldo; Kyprianou, Iacovos S.; Sempau, Josep

We report on the variability in imaging system performance due to oblique x-ray incidence, and the associated transport of quanta (both x rays and optical photons) through the phosphor, in columnar indirect digital detectors. The analysis uses MANTIS, a combined x-ray, electron, and optical Monte Carlo transport code freely available. We describe the main features of the simulation method and provide some validation of the phosphor screen models considered in this work. We report x-ray and electron three-dimensional energy deposition distributions and point-response functions (PRFs), including optical spread in columnar phosphor screens of thickness 100 and 500 {mu}m, for 19,more » 39, 59, and 79 keV monoenergetic x-ray beams incident at 0 deg., 10 deg., and 15 deg. . In addition, we present pulse-height spectra for the same phosphor thickness, x-ray energies, and angles of incidence. Our results suggest that the PRF due to the phosphor blur is highly nonsymmetrical, and that the resolution properties of a columnar screen in a tomographic, or tomosynthetic imaging system varies significantly with the angle of x-ray incidence. Moreover, we find that the noise due to the variability in the number of light photons detected per primary x-ray interaction, summarized in the information or Swank factor, is somewhat independent of thickness and incidence angle of the x-ray beam. Our results also suggest that the anisotropy in the PRF is not less in screens with absorptive backings, while the noise introduced by variations in the gain and optical transport is larger. Predictions from MANTIS, after additional validation, can provide the needed understanding of the extent of such variations, and eventually, lead to the incorporation of the changes in imaging performance with incidence angle into the reconstruction algorithms for volumetric x-ray imaging systems.« less

21 CFR 872.1810 - Intraoral source x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Intraoral source x-ray system. 872.1810 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1810 Intraoral source x-ray system. (a) Identification. An intraoral source x-ray system is an electrically powered device that produces x-rays and is...

21 CFR 872.1810 - Intraoral source x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Intraoral source x-ray system. 872.1810 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1810 Intraoral source x-ray system. (a) Identification. An intraoral source x-ray system is an electrically powered device that produces x-rays and is...

21 CFR 872.1810 - Intraoral source x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Intraoral source x-ray system. 872.1810 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1810 Intraoral source x-ray system. (a) Identification. An intraoral source x-ray system is an electrically powered device that produces x-rays and is...

21 CFR 872.1810 - Intraoral source x-ray system.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Intraoral source x-ray system. 872.1810 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1810 Intraoral source x-ray system. (a) Identification. An intraoral source x-ray system is an electrically powered device that produces x-rays and is...

Characterization of X-Ray Diffraction System with a Microfocus X-Ray Source and a Polycapillary Optic

NASA Technical Reports Server (NTRS)

Gubarev, Mikhail; Marshall, Joy K.; Ciszak, Ewa; Ponomarev, Igor

2000-01-01

We present here an optimized microfocus x-ray source and polycapillary optic system designed for diffraction of small protein crystals. The x-ray beam is formed by a 5.5mm focal length capillary collimator coupled with a 40 micron x-ray source operating at 46Watts. Measurements of the x-ray flux, the divergence and the spectral characteristics of the beam are presented, This optimized system provides a seven fold greater flux than our recently reported configuration [M. Gubarev, et al., J. of Applied Crystallography (2000) 33, in press]. We now make a comparison with a 5kWatts rotating anode generator (Rigaku) coupled with confocal multilayer focusing mirrors (Osmic, CMF12- 38Cu6). The microfocus x-ray source and polycapillary collimator system delivers 60% of the x-ray flux from the rotating anode system. Additional ways to improve our microfocus x-ray system, and thus increase the x-ray flux will be discussed.

Soft x-ray scattering facility at the Advanced Light Source with real-time data processing and analysis

NASA Astrophysics Data System (ADS)

Gann, E.; Young, A. T.; Collins, B. A.; Yan, H.; Nasiatka, J.; Padmore, H. A.; Ade, H.; Hexemer, A.; Wang, C.

2012-04-01

We present the development and characterization of a dedicated resonant soft x-ray scattering facility. Capable of operation over a wide energy range, the beamline and endstation are primarily used for scattering from soft matter systems around the carbon K-edge (˜285 eV). We describe the specialized design of the instrument and characteristics of the beamline. Operational characteristics of immediate interest to users such as polarization control, degree of higher harmonic spectral contamination, and detector noise are delineated. Of special interest is the development of a higher harmonic rejection system that improves the spectral purity of the x-ray beam. Special software and a user-friendly interface have been implemented to allow real-time data processing and preliminary data analysis simultaneous with data acquisition.

X-ray illumination of globular cluster puzzles. [globular cluster X ray sources as clues to Milky Way Galaxy age and evolution

NASA Technical Reports Server (NTRS)

Lightman, A. P.; Grindlay, J. E.

1982-01-01

Globular clusters are thought to be among the oldest objects in the Galaxy, and provide, in this connection, important clues for determining the age and process of formation of the Galaxy. The present investigation is concerned with puzzles relating to the X-ray emission of globular clusters, taking into account questions regarding the location of X-ray emitting clusters (XEGC) unusually near the galactic plane and/or galactic center. An adopted model is discussed for the nature, formation, and lifetime of X-ray sources in globular clusters. An analysis of the available data is conducted in connection with a search for correlations between binary formation time scales, central relaxation times, galactic locations, and X-ray emission. The positive correlation found between distance from galactic center and two-body binary formation time for globular clusters, explanations for this correlation, and the hypothesis that X-ray sources in globular clusters require binary star systems provide a possible explanation of the considered puzzles.

Identification of high-mass X-ray binaries selected from XMM-Newton observations of the LMC★

NASA Astrophysics Data System (ADS)

van Jaarsveld, N.; Buckley, D. A. H.; McBride, V. A.; Haberl, F.; Vasilopoulos, G.; Maitra, C.; Udalski, A.; Miszalski, B.

2018-04-01

The Large Magellanic Cloud (LMC) currently hosts around 23 high-mass X-ray binaries (HMXBs) of which most are Be/X-ray binaries. The LMC XMM-Newton survey provided follow-up observations of previously known X-ray sources that were likely HMXBs, as well as identifying new HMXB candidates. In total, 19 candidate HMXBs were selected based on their X-ray hardness ratios. In this paper we present red and blue optical spectroscopy, obtained with Southern African Large Telescope and the South African Astronomical Observatory 1.9-m telescope, plus a timing analysis of the long-term optical light curves from OGLE to confirm the nature of these candidates. We find that nine of the candidates are new Be/X-ray binaries, substantially increasing the LMC Be/X-ray binary population. Furthermore, we present the optical properties of these new systems, both individually and as a group of all the BeXBs identified by the XMM-Newton survey of the LMC.

Simulation tools for analyzer-based x-ray phase contrast imaging system with a conventional x-ray source

NASA Astrophysics Data System (ADS)

Caudevilla, Oriol; Zhou, Wei; Stoupin, Stanislav; Verman, Boris; Brankov, J. G.

2016-09-01

Analyzer-based X-ray phase contrast imaging (ABI) belongs to a broader family of phase-contrast (PC) X-ray imaging modalities. Unlike the conventional X-ray radiography, which measures only X-ray absorption, in PC imaging one can also measures the X-rays deflection induced by the object refractive properties. It has been shown that refraction imaging provides better contrast when imaging the soft tissue, which is of great interest in medical imaging applications. In this paper, we introduce a simulation tool specifically designed to simulate the analyzer-based X-ray phase contrast imaging system with a conventional polychromatic X-ray source. By utilizing ray tracing and basic physical principles of diffraction theory our simulation tool can predicting the X-ray beam profile shape, the energy content, the total throughput (photon count) at the detector. In addition we can evaluate imaging system point-spread function for various system configurations.

X-ray modeling for SMILE

NASA Astrophysics Data System (ADS)

Sun, T.; Wang, C.; Wei, F.; Liu, Z. Q.; Zheng, J.; Yu, X. Z.; Sembay, S.; Branduardi-Raymont, G.

2016-12-01

SMILE (Solar wind Magnetosphere Ionosphere Link Explorer) is a novel mission to explore the coupling of the solar wind-magnetosphere-ionosphere system via providing global images of the magnetosphere and aurora. As the X-ray imaging is a brand new technique applied to study the large scale magnetopause, modeling of the solar wind charge exchange (SWCX) X-ray emissions in the magnetosheath and cusps is vital in various aspects: it helps the design of the Soft X-ray Imager (SXI) on SMILE, selection of satellite orbits, as well as the analysis of expected scientific outcomes. Based on the PPMLR-MHD code, we present the simulation results of the X-ray emissions in geospace during storm time. Both the polar orbit and the Molniya orbit are used. From the X-ray images of the magnetosheath and cusps, the magnetospheric responses to an interplanetary shock and IMF southward turning are analyzed.

Low Energy Accelerators for Cargo Inspection

NASA Astrophysics Data System (ADS)

Tang, Chuanxiang

Cargo inspection by X-rays has become essential for seaports and airports. With the emphasis on homeland security issues, the identification of dangerous things, such as explosive items and nuclear materials, is the key feature of a cargo inspection system. And new technologies based on dual energy X-rays, neutrons and monoenergetic X-rays have been studied to achieve sufficiently good material identification. An interpretation of the principle of X-ray cargo inspection technology and the features of X-ray sources are presented in this article. As most of the X-ray sources are based on RF electron linear accelerators (linacs), we give a relatively detailed description of the principle and characteristics of linacs. Cargo inspection technologies based on neutron imaging, neutron analysis, nuclear resonance fluorescence and computer tomography are also mentioned here. The main vendors and their products are summarized at the end of the article.

Einstein Observatory survey of X-ray emission from solar-type stars - The late F and G dwarf stars

NASA Technical Reports Server (NTRS)

Maggio, A.; Sciortino, S.; Vaiana, G. S.; Majer, P.; Bookbinder, J.

1987-01-01

Results of a volume-limited X-ray survey of stars of luminosity classes IV and V in the spectral range F7-G9 observed with the Einstein Observatory are presented. Using survival analysis techniques, the stellar X-ray luminosity function in the 0.15-4.0 keV energy band for both single and multiple sources. It is shown that the difference in X-ray luminosity between these two classes of sources is consistent with the superposition of individual components in multiple-component systems, whose X-ray properties are similar to those of the single-component sources. The X-ray emission of the stars in our sample is well correlated with their chromospheric CA II H-K line emission and with their projected equatorial rotational velocity. Comparison of the X-ray luminosity function constructed for the sample of the dG stars of the local population with the corresponding functions derived elsewhere for the Hyades, the Pleiades, and the Orion Ic open cluster confirms that the level of X-ray emission decreases with stellar age.

A laboratory based system for laue micro x-ray diffraction.

PubMed

Lynch, P A; Stevenson, A W; Liang, D; Parry, D; Wilkins, S; Tamura, N

2007-02-01

A laboratory diffraction system capable of illuminating individual grains in a polycrystalline matrix is described. Using a microfocus x-ray source equipped with a tungsten anode and prefigured monocapillary optic, a micro-x-ray diffraction system with a 10 microm beam was developed. The beam profile generated by the ellipsoidal capillary was determined using the "knife edge" approach. Measurement of the capillary performance, indicated a beam divergence of 14 mrad and a useable energy bandpass from 5.5 to 19 keV. Utilizing the polychromatic nature of the incident x-ray beam and application of the Laue indexing software package X-Ray Micro-Diffraction Analysis Software, the orientation and deviatoric strain of single grains in a polycrystalline material can be studied. To highlight the system potential the grain orientation and strain distribution of individual grains in a polycrystalline magnesium alloy (Mg 0.2 wt % Nd) was mapped before and after tensile loading. A basal (0002) orientation was identified in the as-rolled annealed alloy; after tensile loading some grains were observed to undergo an orientation change of 30 degrees with respect to (0002). The applied uniaxial load was measured as an increase in the deviatoric tensile strain parallel to the load axis.

The Orbital Parameters and Nature of the X-ray Pulsar IGR J16393-4643 Using Pulse Timing Analysis

NASA Astrophysics Data System (ADS)

Pearlman, Aaron B.; Corbet, R. H. D.; Pottschmidt, K.; Skinner, G. K.

2011-09-01

A 3.7 day orbital period was previously suggested for the 910 s X-ray pulsar IGR J16393-4643 from a pulse timing study of widely separated X-ray observations (Thompson et al., 2006), placing the system in the supergiant wind-fed region of the Ppulse-Porb diagram. However, orbital periods of 50.2 and 8.1 days could not be excluded. Nespoli et al. (2010) refute this wind-accreting high-mass X-ray binary classification and suggest a symbiotic X-ray binary (SyXB) designation based on infrared spectroscopy of the proposed counterpart and the potential 50.2 day orbital solution. SyXBs are low-mass X-ray binaries in which a neutron star accretes from the inhomogeneous medium around an M-type giant companion. We find that two statistically independent light curves of IGR J16393-4643, from the Swift Burst Alert Telescope (15-50 keV) and the Rossi X-ray Timing Explorer (RXTE) Proportional Counter Array (PCA) Galactic bulge scans (2-10 keV), show highly significant orbital modulation near 4.24 days. Making use of this precise orbital period, we present the results from pulse arrival time analysis on IGR J16393-4643 using RXTE PCA observations. We provide significantly improved phase-connected pulse timing results using archival observations presented in Thompson et al. (2006) and additional pulse timing data not included in their study to determine the orbital parameters of the system. The derived 7.5 M⊙ mass function is inconsistent with a SyXB identification.

21 CFR 872.1800 - Extraoral source x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Extraoral source x-ray system. 872.1800 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1800 Extraoral source x-ray system. (a) Identification. An extraoral source x-ray system is an AC-powered device that produces x-rays and is intended for...

21 CFR 872.1800 - Extraoral source x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Extraoral source x-ray system. 872.1800 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1800 Extraoral source x-ray system. (a) Identification. An extraoral source x-ray system is an AC-powered device that produces x-rays and is intended for...

21 CFR 872.1800 - Extraoral source x-ray system.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Extraoral source x-ray system. 872.1800 Section... (CONTINUED) MEDICAL DEVICES DENTAL DEVICES Diagnostic Devices § 872.1800 Extraoral source x-ray system. (a) Identification. An extraoral source x-ray system is an AC-powered device that produces x-rays and is intended for...

CIAO: CHANDRA/X-RAY DATA ANALYSIS FOR EVERYONE

NASA Astrophysics Data System (ADS)

McDowell, Jonathan; CIAO Team

2018-01-01

Eighteen years after the launch of Chandra, the archive is full of scientifically rich data and new observations continue. Improvements in recent years to the data analysis package CIAO (Chandra Interactive Analysis of Observations) and its extensive accompanying documentation make it easier for astronomers without a specialist background in high energy astrophysics to take advantage of this resource.The CXC supports hundreds of CIAO users around the world at all levels of training from high school and undergraduate students to the most experienced X-ray astronomers. In general, we strive to provide a software system which is easy for beginners, yet powerful for advanced users.Chandra data cover a range of instrument configurations and types of target (pointlike, extended and moving), requiring a flexible data analysis system. In addition to CIAO tools using the familiar FTOOLS/IRAF-style parameter interface, CIAO includes applications such as the Sherpa fitting engine which provide access to the data via Python scripting.In this poster we point prospective (and existing!) users to the high level Python scripts now provided to reprocess Chandra or other X-ray mission data, determine source fluxes and upper limits, and estimate backgrounds; and to the latest documentation including the CIAO Gallery, a new entry point featuring the system's different capabilities.This work has been supported by NASA under contract NAS 8-03060 to the Smithsonian Astrophysical Observatory for operation of the Chandra X-ray Center.

Polarization for Background Reduction in EDXRF - The Technique That Would Not Work

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ryon, R W

2002-07-24

As with all electromagnet radiation, polarization of x-rays is a general phenomenon. Such polarization has been known since the classic experiments of Barkla in 1906. The general implementation of polarization to x-ray analysis had to await the fixed geometry of energy-dispersive systems. The means of optimizing these systems is shown in this review paper. Improved detection limits are the result.

Periodicity Analysis of X-ray Light Curves of SS 433

NASA Astrophysics Data System (ADS)

Wang, Jun-yi; Lu, Xiang-long; Zhao, Qiu-wen; Dong, Dian-qiao; Lao, Bao-qiang; Lu, Yang; Wei, Yan-heng; Wu, Xiao-cong; An, Tao

2017-01-01

SS 433 is sofar the unique X-ray binary that has the simultaneously detected orbital period, super-orbital period, and nutation period, as well as a bidirectional spiral jet. The study on its X-ray light variability is helpful for understanding the dynamic process of the system, and the correlations between the different wavebands. In this paper, two time-series analysis techniques, i.e., the Lomb-Scargle periodogram and weighted wavelet Z-transform, are employed to search for the periods in the Swift/BAT (Burst Alert Telescope) (15-50 keV) and RXTE/ASM (Rose X-ray Timing Explorer/All Sky Monitor) (1.5-3, 3- 4, and 5-12 keV) light curves of SS 433, and the Monte Carlo simulation is performed for the obtained periodical components. For the 15-50 keV energy band, five significant periodical components are detected, which are P1(∼6.29 d), P2 (∼6.54 d), P3 (∼13.08 d), P4 (∼81.50 d), and P5 (∼162.30 d). For the 3-5 and 5-12 keV energy bands, the periodical components P3 (∼13 d) and P5 (∼162 d) are detected in both energy bands. However, for the 1.5-3 keV energy band, no significant periodic signal is detected. P5 is the strongest periodic signal in the power spectrum for all the energy bands of 3-5, 5-12, and 15-50 keV, and it is consistent with the previous result obtained from the study of optical light curves. Furthermore, in combination with the radio spiral jet of SS 433, it is suggested that the X-ray and optical variability of P5 (∼162 d) is probably related to the precession of its relativistic jet. The high correlation between the X-ray and optical light curves may also imply that the X-ray and optical radiations are of the same physical origin. P3 shows a good agreement with the orbital period (∼13.07 d) obtained by the previous study, and P2 and P4 are respectively the high-frequency harmonics of P3 and P5. P1 is detected only in the power spectrum of the 15-50 keV energy band, and it is consistent with the nutation period of the system. As the energy of energy band decreases (from hard X-ray to soft X-ray), the number of detected periods becomes gradually less, this result verifies that the radiation in the high-energy band (hard X-ray) comes primarily from the jet, and the radiation in the low-energy band (soft X-ray) may be dominated by the medium around the binary system. The multiple X-ray periods obtained from the present study have provided a reliable basis for the further analysis of the multi-band data of SS 433, and the study on the dynamical mechanism of the system.

Crystallization and preliminary X-ray analysis of copper amine oxidase from Escherichia coli K-12.

PubMed

Roh, J H; Suzuki, H; Kumagai, H; Yamashita, M; Azakami, H; Murooka, Y; Mikami, B

1994-05-13

Copper-containing monoamine oxidase (MAO) from Escherichia coli was overproduced in the periplasmic space by expression of the cloned gene. The purified MAO has been crystallized by means of the hanging drop technique using sodium citrate as a precipitant. The crystals belong to the orthorhombic system, space group P2(1)2(1)2(1), with unit cell dimensions of a = 136.1 A, b = 168.4 A and c = 81.6 A. The asymmetric unit contains one molecule of MAO, with a crystal volume per protein mass (Vm) of 2.88 A3/Da and a solvent content of 58% by volume. The crystals diffract X-rays to a resolution limit of at least 2.7 A and are resistant to X-ray radiation damage. They appear to be suitable for X-ray structure analysis.

Analysis of sculptures using XRF and X-ray radiography

NASA Astrophysics Data System (ADS)

Calza, C.; Oliveira, D. F.; Freitas, R. P.; Rocha, H. S.; Nascimento, J. R.; Lopes, R. T.

2015-11-01

This work reports the analysis of two sacred images on polychrome wood using X-ray Radiography and Energy Dispersive X-Ray Fluorescence. The first case is the analysis of a sculpture portraying Saint Sebastian, the patron saint of Rio de Janeiro, which is considered the second most ancient sacred image of Brazil. This sculpture was made in Portugal and was transported to Brazil by Estácio Sá, founder of the city of Rio de Janeiro, in 1565. Nowadays, it is located on the main altar of the Church of Capuchin Friars. The second case is the analysis of a sculpture representing Our Lady of Conception, which is located in the D. João VI Museum (EBA/UFRJ, Rio de Janeiro). The objective of these analyses was to evaluate the general conditions of the sculptures, identifying possible problems and internal damages, areas that revealed signs of previous retouchings and the materials and pigments employed by the artists, in order to assist its restoration procedures. EDXRF measurements were carried out with a portable system, developed at the Nuclear Instrumentation Laboratory, consisting of a Si-PIN XR-100CR detector from Amptek and an Oxford TF3005 X-ray tube with W anode. An X-ray source, a CR System GE CR50P and IP detectors were used to perform the radiographs. The XRF analysis of the sculptures identified the original pigments in both cases and the radiographic images revealed details of the manufacture; restored regions; extensive use of lead white; presence of cracks on the wood; use of nails and spikes, etc.

Substantial superiority of Niobe ES over Niobe II system in remote-controlled magnetic pulmonary vein isolation.

PubMed

Da Costa, Antoine; Guichard, Jean Baptiste; Maillard, Nicolas; Romeyer-Bouchard, Cécile; Gerbay, Antoine; Isaaz, Karl

2017-03-01

Catheter ablation of atrial fibrillation (AFib) primarily relies upon pulmonary vein isolation (PVI), but such procedures are associated with significant X-ray exposure. The newer Epoch system has been developed so as to enable more precise magnetic navigation whilst limiting X-ray exposure. This study was aimed at quantifying both exposure time and X-ray reduction with the newer Epoch system compared to Niobe II during AFib ablation procedures. From November 2011 to November 2013, our last 92 consecutive patients treated with the Niobe ES (Epoch Solution; 4th generation magnetic navigation technology) system were compared with the first 92 consecutive patients treated using the Niobe II system (3rd generation magnetic navigation technology) for symptomatic drug-refractory AFib. Mean patient age was 59±11years (20% female), and the study population was affected by either symptomatic paroxysmal (65.2%) or persistent (34.8%) AFib. Median procedure time was 2±0.5h and median total X-ray exposure 12.3±6.4min. Procedure time (1.9±0.4 vs. 2.7±1h, p<0.0001) and X-ray duration (12±4 vs. 15±7min, p=0.001) were significantly lower with Niobe ES than with the Niobe II system. X-ray ablation exposure time was also significantly lower with the Niobe ES system than with the Niobe II system (2.9±2 vs. 4±3.5min; p=0.01). Through multivariate analysis, the only predictive factors influencing both procedure duration and X-ray exposure were found to be the Niobe ES system use and LA size. Our study was the first to demonstrate that the new Niobe ES magnetic robotic system substantially reduced overall operating, fluoroscopy, and ablation times during AFib ablation procedure. Copyright © 2016 Elsevier Ireland Ltd. All rights reserved.

In situ X-ray measurements of MOVPE growth of InxGa1-xN single quantum wells

NASA Astrophysics Data System (ADS)

Ju, Guangxu; Fuchi, Shingo; Tabuchi, Masao; Takeda, Yoshikazu

2013-05-01

GaN/InxGa1-xN/GaN single quantum wells (SQWs) have been grown on c-plane GaN/sapphire substrates using MOVPE system. PL (photoluminescence) and AFM (atomic force microscope) measurements demonstrate good quality of after-growth thermal-annealed SQWs. In situ XRD (X-ray diffraction), XRR (X-ray reflectivity), and X-ray CTR (crystal truncation rod) scattering measurements were successfully conducted on the SQWs under the NH3+N2 ambient at 1103 K. The analysis results of the XRR and the X-ray CTR spectra at 1103 K and at 300 K on the same sample matched well. It demonstrated that In0.09Ga0.91N SQW structure with several ML (monolayer) InGaN thicknesses was successfully investigated using the XRR and CTR scattering measurements at 1103 K.

Analysis of Patients' X-ray Exposure in 146 Percutaneous Radiologic Gastrostomies.

PubMed

Petersen, Tim-Ole; Reinhardt, Martin; Fuchs, Jochen; Gosch, Dieter; Surov, Alexey; Stumpp, Patrick; Kahn, Thomas; Moche, Michael

2017-09-01

Purpose  Analysis of patient´s X-ray exposure during percutaneous radiologic gastrostomies (PRG) in a larger population. Materials and Methods  Data of primary successful PRG-procedures, performed between 2004 and 2015 in 146 patients, were analyzed regarding the exposition to X-ray. Dose-area-product (DAP), dose-length-product (DLP) respectively, and fluoroscopy time (FT) were correlated with the used x-ray systems (Flatpanel Detector (FD) vs. Image Itensifier (BV)) and the necessity for periprocedural placement of a nasogastric tube. Additionally, the effective X-ray dose for PRG placement using fluoroscopy (DL), computed tomography (CT), and cone beam CT (CBCT) was estimated using a conversion factor. Results  The median DFP of PRG-placements under fluoroscopy was 163 cGy*cm 2 (flat panel detector systems: 155 cGy*cm 2 ; X-ray image intensifier: 175 cGy*cm 2 ). The median DLZ was 2.2 min. Intraprocedural placement of a naso- or orogastric probe (n = 68) resulted in a significant prolongation of the median DLZ to 2.5 min versus 2 min in patients with an already existing probe. In addition, dose values were analyzed in smaller samples of patients in which the PRG was placed under CBCT (n = 7, median DFP = 2635 cGy*cm 2 ), or using CT (n = 4, median DLP = 657 mGy*cm). Estimates of the median DFP and DLP showed effective doses of 0.3 mSv for DL-assisted placements (flat panel detector 0.3 mSv, X-ray image converter 0.4 mSv), 7.9 mSv using a CBCT - flat detector, and 9.9 mSv using CT. This corresponds to a factor 26 of DL versus CBCT, or a factor 33 of DL versus CT. Conclusion  In order to minimize X-ray exposure during PRG-procedures for patients and staff, fluoroscopically-guided interventions should employ flat detector systems with short transmittance sequences in low dose mode and with slow image frequency. Series recordings can be dispensed with. The intraprocedural placement of a naso- or orogastric probe significantly extends FT, but has little effect on the overall dose of the intervention. Due to the significantly higher X-ray exposure, the use of a CBCT as well as PRG-placements using CT should be limited to clinically absolutely necessary exceptions with strict indication. Key Points   · Fluoroscopically-guided PRG placements are interventions with low X-ray exposure.. · X-ray exposure from fluoroscopy is lower using flat panel detector systems as compared to image intensifier systems.. · The concomitant placement of an oro- or nasogastric probe extends the fluoroscopy time.. · Gastric probe placement is worthwhile to prevent the premature use of the significantly radiation-intensive CT.. · The use of the C-arm CT or the CT increases the beam exposure by 26 or 33 times, respectively.. · The PRG placement using C-arm CT and CT should only be performed in exceptional cases.. Citation Format · Petersen TO, Reinhardt M, Fuchs J et al. Analysis of Patients' X-ray Exposure in 146 Percutaneous Radiologic Gastrostomies. Fortschr Röntgenstr 2017; 189: 820 - 827. © Georg Thieme Verlag KG Stuttgart · New York.

Status and expected perfomance of the MAXI mission for the JEM/ISS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kataoka, J.; Kawai, N.

2008-12-24

MAXI (Monitor of All-sky X-ray Image) is the first payload to be attached on JEM-EF (Kibo exposed facility) of ISS. It provides an all sky X-ray image every ISS orbit. Only with a few weeks scan, MAXI is expected to make a milli-Crab X-ray all sky map excluding bright region around the sun. Thus, MAXI does not only inform X-ray novae and transients rapidly to world astronomers if once they occur, but also observes long-term variability of Galact ic and extra-Galactic X-ray sources. MAXI also provides an X-ray source catalogue at that time with diffuse cosmic X-ray background. MAXI consistsmore » of two kinds of detectors, position sensitive gas-proportional counters for 2-30 keV X-rays and CCD cameras for 0.5-10 keV X-rays. All instruments of MAXI are now in final phase of pre-launching tests of their flight modules. We are also carrying out performance tests for X-ray detectors and collimators. Data processing and analysis software including alert system on ground are being developed by mission team. In this paper we report an overview of final instruments of MAXI and capability of MAXI.« less

Systems engineering analysis of five 'as-manufactured' SXI telescopes

NASA Astrophysics Data System (ADS)

Harvey, James E.; Atanassova, Martina; Krywonos, Andrey

2005-09-01

Four flight models and a spare of the Solar X-ray Imager (SXI) telescope mirrors have been fabricated. The first of these is scheduled to be launched on the NOAA GOES- N satellite on July 29, 2005. A complete systems engineering analysis of the "as-manufactured" telescope mirrors has been performed that includes diffraction effects, residual design errors (aberrations), surface scatter effects, and all of the miscellaneous errors in the mirror manufacturer's error budget tree. Finally, a rigorous analysis of mosaic detector effects has been included. SXI is a staring telescope providing full solar disc images at X-ray wavelengths. For wide-field applications such as this, a field-weighted-average measure of resolution has been modeled. Our performance predictions have allowed us to use metrology data to model the "as-manufactured" performance of the X-ray telescopes and to adjust the final focal plane location to optimize the number of spatial resolution elements in a given operational field-of-view (OFOV) for either the aerial image or the detected image. The resulting performance predictions from five separate mirrors allow us to evaluate and quantify the optical fabrication process for producing these very challenging grazing incidence X-ray optics.

Quantitative analysis of crystalline pharmaceuticals in powders and tablets by a pattern-fitting procedure using X-ray powder diffraction data.

PubMed

Yamamura, S; Momose, Y

2001-01-16

A pattern-fitting procedure for quantitative analysis of crystalline pharmaceuticals in solid dosage forms using X-ray powder diffraction data is described. This method is based on a procedure for pattern-fitting in crystal structure refinement, and observed X-ray scattering intensities were fitted to analytical expressions including some fitting parameters, i.e. scale factor, peak positions, peak widths and degree of preferred orientation of the crystallites. All fitting parameters were optimized by the non-linear least-squares procedure. Then the weight fraction of each component was determined from the optimized scale factors. In the present study, well-crystallized binary systems, zinc oxide-zinc sulfide (ZnO-ZnS) and salicylic acid-benzoic acid (SA-BA), were used as the samples. In analysis of the ZnO-ZnS system, the weight fraction of ZnO or ZnS could be determined quantitatively in the range of 5-95% in the case of both powders and tablets. In analysis of the SA-BA systems, the weight fraction of SA or BA could be determined quantitatively in the range of 20-80% in the case of both powders and tablets. Quantitative analysis applying this pattern-fitting procedure showed better reproducibility than other X-ray methods based on the linear or integral intensities of particular diffraction peaks. Analysis using this pattern-fitting procedure also has the advantage that the preferred orientation of the crystallites in solid dosage forms can be also determined in the course of quantitative analysis.

Analysis of a measurement scheme for ultrafast hole dynamics by few femtosecond resolution X-ray pump-probe Auger spectroscopy.

PubMed

Cooper, Bridgette; Kolorenč, Přemysl; Frasinski, Leszek J; Averbukh, Vitali; Marangos, Jon P

2014-01-01

Ultrafast hole dynamics created in molecular systems as a result of sudden ionisation is the focus of much attention in the field of attosecond science. Using the molecule glycine we show through ab initio simulations that the dynamics of a hole, arising from ionisation in the inner valence region, evolves with a timescale appropriate to be measured using X-ray pulses from the current generation of SASE free electron lasers. The examined pump-probe scheme uses X-rays with photon energy below the K edge of carbon (275-280 eV) that will ionise from the inner valence region. A second probe X-ray at the same energy can excite an electron from the core to fill the vacancy in the inner-valence region. The dynamics of the inner valence hole can be tracked by measuring the Auger electrons produced by the subsequent refilling of the core hole as a function of pump-probe delay. We consider the feasibility of the experiment and include numerical simulation to support this analysis. We discuss the potential for all X-ray pump-X-ray probe Auger spectroscopy measurements for tracking hole migration.

Analysis of particulate contamination on tape lift samples from the VETA optical surfaces

NASA Technical Reports Server (NTRS)

Germani, Mark S.

1992-01-01

Particulate contamination analysis was carried out on samples taken from the Verification Engineering Test Article (VETA) x-ray detection system. A total of eighteen tape lift samples were taken from the VETA optical surfaces. Initially, the samples were tested using a scanning electron microscope. Additionally, particle composition was determined by energy dispersive x-ray spectrometry. Results are presented in terms of particle loading per sample.

The Chaotic Long-term X-ray Variability of 4U 1705-44

NASA Astrophysics Data System (ADS)

Phillipson, R. A.; Boyd, P. T.; Smale, A. P.

2018-04-01

The low-mass X-ray binary 4U1705-44 exhibits dramatic long-term X-ray time variability with a timescale of several hundred days. The All-Sky Monitor (ASM) aboard the Rossi X-ray Timing Explorer (RXTE) and the Japanese Monitor of All-sky X-ray Image (MAXI) aboard the International Space Station together have continuously observed the source from December 1995 through May 2014. The combined ASM-MAXI data provide a continuous time series over fifty times the length of the timescale of interest. Topological analysis can help us identify 'fingerprints' in the phase-space of a system unique to its equations of motion. The Birman-Williams theorem postulates that if such fingerprints are the same between two systems, then their equations of motion must be closely related. The phase-space embedding of the source light curve shows a strong resemblance to the double-welled nonlinear Duffing oscillator. We explore a range of parameters for which the Duffing oscillator closely mirrors the time evolution of 4U1705-44. We extract low period, unstable periodic orbits from the 4U1705-44 and Duffing time series and compare their topological information. The Duffing and 4U1705-44 topological properties are identical, providing strong evidence that they share the same underlying template. This suggests that we can look to the Duffing equation to help guide the development of a physical model to describe the long-term X-ray variability of this and other similarly behaved X-ray binary systems.

21 CFR 892.1650 - Image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Image-intensified fluoroscopic x-ray system. 892... fluoroscopic x-ray system. (a) Identification. An image-intensified fluoroscopic x-ray system is a device intended to visualize anatomical structures by converting a pattern of x-radiation into a visible image...

21 CFR 892.1650 - Image-intensified fluoroscopic x-ray system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Image-intensified fluoroscopic x-ray system. 892... fluoroscopic x-ray system. (a) Identification. An image-intensified fluoroscopic x-ray system is a device intended to visualize anatomical structures by converting a pattern of x-radiation into a visible image...

AN EXTENDED AND MORE SENSITIVE SEARCH FOR PERIODICITIES IN ROSSI X-RAY TIMING EXPLORER/ALL-SKY MONITOR X-RAY LIGHT CURVES

DOE Office of Scientific and Technical Information (OSTI.GOV)

Levine, Alan M.; Bradt, Hale V.; Chakrabarty, Deepto

2011-09-01

We present the results of a systematic search in {approx}14 years of Rossi X-ray Timing Explorer All-Sky Monitor (ASM) data for evidence of periodicities. Two variations of the commonly used Fourier analysis search method have been employed to significantly improve upon the sensitivity achieved by Wen et al. in 2006, who also searched for periodicities in ASM data. In addition, the present search is comprehensive in terms of sources studied and frequency range covered, and has yielded the detection of the signatures of the orbital periods of eight low-mass X-ray binary systems and of ten high-mass X-ray binaries not listedmore » in the tables of Wen et al. Orbital periods, epochs, signal amplitudes, modulation fractions, and folded light curves are given for each of these systems. Seven of the orbital periods are the most precise reported to date. In the course of this work, the 18.545 day orbital period of IGR J18483-0311 was co-discovered, and the first detections in X-rays were made of the {approx}3.9 day orbital period of LMC X-1 and the {approx}3.79 hr orbital period of 4U 1636-536. The results inform future searches for orbital and other periodicities in X-ray binaries.« less

Broad-Band Measurements of Cen X-3 With XTE and CGRO

NASA Technical Reports Server (NTRS)

Vestrand, W. Thomas

1999-01-01

Centaurus X-3 has played a key role in the development of our understanding of galactic x-ray binary sources. Timing analysis of the UHURU x-ray observations for the luminous Cen X-3 source (L approximately 10(exp 38) erg/s) revealed the first evidence for coherent x-ray pulsations from an object in a binary system (Giaconni 1971; Schreier 1972). It was quickly understood that the luminous pulsed x-ray emission could be generated by the accretion of matter from a companion star onto a rotating neutron star and led to the adoption of binary star models as the fundamental model for galactic x-ray sources (e.g. Pringle and Rees 1972; Lamb 1973). Based on modeling and refined observations since the original measurements, we now believe that Cen X-3 is a high mass x-ray binary system that contains a disk-fed pulsar with a period of 4.84 seconds that is in a 2.087 day orbit around an O-star companion. Since the pulsar discovery, its period has been intermittently monitored and those studies show a long term spin-up of the pulsar punctuated by short intervals of spin-down (e.g. Finger 1994). The implied torques are thought to originate from the interaction of an accretion disk with the magnetic field of a neutron star (Ghosh and Lamb 1979).

Experiment and application of soft x-ray grazing incidence optical scattering phenomena

NASA Astrophysics Data System (ADS)

Chen, Shuyan; Li, Cheng; Zhang, Yang; Su, Liping; Geng, Tao; Li, Kun

2017-08-01

For short wavelength imaging systems，surface scattering effects is one of important factors degrading imaging performance. Study of non-intuitive surface scatter effects resulting from practical optical fabrication tolerances is a necessary work for optical performance evaluation of high resolution short wavelength imaging systems. In this paper, Soft X-ray optical scattering distribution is measured by a soft X-ray reflectometer installed by my lab, for different sample mirrors、wavelength and grazing angle. Then aim at space solar telescope, combining these scattered light distributions, and surface scattering numerical model of grazing incidence imaging system, PSF and encircled energy of optical system of space solar telescope are computed. We can conclude that surface scattering severely degrade imaging performance of grazing incidence systems through analysis and computation.

Analysis of the Central X-ray Source in DG Tau

NASA Astrophysics Data System (ADS)

Schneider, P. Christian; Schmitt, Jürgen H. M. M.

As a stellar X-ray source DG Tau shows two rather unusual features: A resolved X-ray jet [2] and an X-ray spectrum best described by two thermal components with different absorbing column densities, a so called "two-absorber X-ray (TAX)" morphology [1, 2]. In an effort to understand the properties of the central X-ray source in DG Tau a detailed position analysis was carried out.

VETA x ray data acquisition and control system

NASA Technical Reports Server (NTRS)

Brissenden, Roger J. V.; Jones, Mark T.; Ljungberg, Malin; Nguyen, Dan T.; Roll, John B., Jr.

1992-01-01

We describe the X-ray Data Acquisition and Control System (XDACS) used together with the X-ray Detection System (XDS) to characterize the X-ray image during testing of the AXAF P1/H1 mirror pair at the MSFC X-ray Calibration Facility. A variety of X-ray data were acquired, analyzed and archived during the testing including: mirror alignment, encircled energy, effective area, point spread function, system housekeeping and proportional counter window uniformity data. The system architecture is presented with emphasis placed on key features that include a layered UNIX tool approach, dedicated subsystem controllers, real-time X-window displays, flexibility in combining tools, network connectivity and system extensibility. The VETA test data archive is also described.

Soft x-ray scattering facility at the Advanced Light Source with real-time data processing and analysis.

PubMed

Gann, E; Young, A T; Collins, B A; Yan, H; Nasiatka, J; Padmore, H A; Ade, H; Hexemer, A; Wang, C

2012-04-01

We present the development and characterization of a dedicated resonant soft x-ray scattering facility. Capable of operation over a wide energy range, the beamline and endstation are primarily used for scattering from soft matter systems around the carbon K-edge (∼285 eV). We describe the specialized design of the instrument and characteristics of the beamline. Operational characteristics of immediate interest to users such as polarization control, degree of higher harmonic spectral contamination, and detector noise are delineated. Of special interest is the development of a higher harmonic rejection system that improves the spectral purity of the x-ray beam. Special software and a user-friendly interface have been implemented to allow real-time data processing and preliminary data analysis simultaneous with data acquisition. © 2012 American Institute of Physics

INTEGRAL results on supergiant fast X-ray transients and accretion mechanism interpretation: ionization effect and formation of transient accretion discs

NASA Astrophysics Data System (ADS)

Ducci, L.; Sidoli, L.; Paizis, A.

2010-11-01

We performed a systematic analysis of all INTEGRAL observations from 2003 to 2009 of 14 supergiant fast X-ray transients (SFXTs), implying a net exposure time of about 30 Ms. For each source we obtained light curves and spectra (3-100 keV), discovering several new outbursts. We discuss the X-ray behaviour of SFXTs emerging from our analysis in the framework of the clumpy wind accretion mechanism we proposed. We discuss the effect of X-ray photoionization on accretion in close binary systems such as IGR J16479-4514 and IGR J17544-2619. We show that, because of X-ray photoionization, there is a high probability of an accretion disc forming from the capture of angular momentum in IGR J16479-4514, and we suggest that the formation of transient accretion discs could be partly responsible for the flaring activity in SFXTs with narrow orbits. We also propose an alternative way to explain the origin of flares with peculiar shapes observed in our analysis applying the model of Lamb et al., which is based on accretion via the Rayleigh-Taylor instability and was originally proposed to explain Type II bursts.

VETA-1 x ray detection system

NASA Technical Reports Server (NTRS)

Podgorski, W. A.; Flanagan, Kathy A.; Freeman, Mark D.; Goddard, R. G.; Kellogg, Edwin M.; Norton, T. J.; Ouellette, J. P.; Roy, A. G.; Schwartz, Daniel A.

1992-01-01

The alignment and X-ray imaging performance of the Advanced X-ray Astrophysics Facility (AXAF) Verification Engineering Test Article-I (VETA-I) was measured by the VETA-I X-Ray Detection System (VXDS). The VXDS was based on the X-ray detection system utilized in the AXAF Technology Mirror Assembly (TMA) program, upgraded to meet the more stringent requirements of the VETA-I test program. The VXDS includes two types of X-ray detectors: (1) a High Resolution Imager (HRI) which provides X-ray imaging capabilities, and (2) sealed and flow proportional counters which, in conjunction with apertures of various types and precision translation stages, provide the most accurate measurement of VETA-I performance. Herein we give an overview of the VXDS hardware including X-ray detectors, translation stages, apertures, proportional counters and flow counter gas supply system and associated electronics. We also describe the installation of the VXDS into the Marshall Space Flight Center (MSFC) X-Ray Calibration Facility (XRCF). We discuss in detail the design and performance of those elements of the VXDS which have not been discussed elsewhere; translation systems, flow counter gas supply system, apertures and thermal monitoring system.

Satellite services system analysis study. Volume 3A: Service equipment requirements, appendix

NASA Technical Reports Server (NTRS)

1981-01-01

Spacecraft descriptions and mission sequences, mission and servicing operations functional analyses, servicing requirements, and servicing equipment are discussed for five reference satellites: the X-ray Timing Explorer, the Upper Atmospheric Research Satellite, the Advanced X-ray Astrophysics Facility, the Earth Gravity Field Survey Mission, and the Orbiting Astronomical Observatory.

Handbook Of X-ray Astronomy

NASA Astrophysics Data System (ADS)

Arnaud, Keith A.; Smith, R. K.; Siemiginowska, A.; Edgar, R. J.; Grant, C. E.; Kuntz, K. D.; Schwartz, D. A.

2011-09-01

This poster advertises a book to be published in September 2011 by Cambridge University Press. Written for graduate students, professional astronomers and researchers who want to start working in this field, this book is a practical guide to x-ray astronomy. The handbook begins with x-ray optics, basic detector physics and CCDs, before focussing on data analysis. It introduces the reduction and calibration of x-ray data, scientific analysis, archives, statistical issues and the particular problems of highly extended sources. The book describes the main hardware used in x-ray astronomy, emphasizing the implications for data analysis. The concepts behind common x-ray astronomy data analysis software are explained. The appendices present reference material often required during data analysis.

Illicit drug detection using energy dispersive x-ray diffraction

NASA Astrophysics Data System (ADS)

Cook, E. J.; Griffiths, J. A.; Koutalonis, M.; Gent, C.; Pani, S.; Horrocks, J. A.; George, L.; Hardwick, S.; Speller, R.

2009-05-01

Illicit drugs are imported into countries in myriad ways, including via the postal system and courier services. An automated system is required to detect drugs in parcels for which X-ray diffraction is a suitable technique as it is non-destructive, material specific and uses X-rays of sufficiently high energy to penetrate parcels containing a range of attenuating materials. A database has been constructed containing the measured powder diffraction profiles of several thousand materials likely to be found in parcels. These include drugs, cutting agents, packaging and other innocuous materials. A software model has been developed using these data to predict the diffraction profiles which would be obtained by X-ray diffraction systems with a range of suggested detector (high purity germanium, CZT and scintillation), source and collimation options. The aim of the model was to identify the most promising system geometries, which was done with the aid of multivariate analysis (MVA). The most promising systems were constructed and tested. The diffraction profiles of a range of materials have been measured and used to both validate the model and to identify the presence of drugs in sample packages.

X-ray/EUV optics for astronomy, microscopy, polarimetry, and projection lithography; Proceedings of the Meeting, San Diego, CA, July 9-13, 1990

NASA Technical Reports Server (NTRS)

Hoover, Richard B. (Editor); Walker, Arthur B. C., Jr. (Editor)

1991-01-01

Topics discussed in this issue include the fabrication of multilayer X-ray/EUV coatings; the design, characterization, and test of multilayer X-ray/EUV coatings; multilayer X-ray/EUV monochromators and imaging microscopes; X-ray/EUV telescopes; the test and calibration performance of X-ray/EUV instruments; XUV/soft X-ray projection lithography; X-ray/EUV space observatories and missions; X-ray/EUV telescopes for solar research; X-ray/EUV polarimetry; X-ray/EUV spectrographs; and X-ray/EUV filters and gratings. Papers are presented on the deposition-controlled uniformity of multilayer mirrors, interfaces in Mo/Si multilayers, the design and analysis of an aspherical multilayer imaging X-ray microscope, recent developments in the production of thin X-ray reflecting foils, and the ultraprecise scanning technology. Consideration is also given to an active sun telescope array, the fabrication and performance at 1.33 nm of a 0.24-micron-period multilayer grating, a cylindrical proportional counter for X-ray polarimetry, and the design and analysis of the reflection grating arrays for the X-Ray Multi-Mirror Mission.

High-frame-rate digital radiographic videography

NASA Astrophysics Data System (ADS)

King, Nicholas S. P.; Cverna, Frank H.; Albright, Kevin L.; Jaramillo, Steven A.; Yates, George J.; McDonald, Thomas E.; Flynn, Michael J.; Tashman, Scott

1994-10-01

High speed x-ray imaging can be an important tool for observing internal processes in a wide range of applications. In this paper we describe preliminary implementation of a system having the eventual goal of observing the internal dynamics of bone and joint reactions during loading. Two Los Alamos National Laboratory (LANL) gated and image intensified camera systems were used to record images from an x-ray image convertor tube to demonstrate the potential of high frame-rate digital radiographic videography in the analysis of bone and joint dynamics of the human body. Preliminary experiments were done at LANL to test the systems. Initial high frame-rate imaging (from 500 to 1000 frames/s) of a swinging pendulum mounted to the face of an X-ray image convertor tube demonstrated high contrast response and baseline sensitivity. The systems were then evaluated at the Motion Analysis Laboratory of Henry Ford Health Systems Bone and Joint Center. Imaging of a 9 inch acrylic disk with embedded lead markers rotating at approximately 1000 RPM, demonstrated the system response to a high velocity/high contrast target. By gating the P-20 phosphor image from the X-ray image convertor with a second image intensifier (II) and using a 100 microsecond wide optical gate through the second II, enough prompt light decay from the x-ray image convertor phosphor had taken place to achieve reduction of most of the motion blurring. Measurement of the marker velocity was made by using video frames acquired at 500 frames/s. The data obtained from both experiments successfully demonstrated the feasibility of the technique. Several key areas for improvement are discussed along with salient test results and experiment details.

REVIEWS OF TOPICAL PROBLEMS: Masses of black holes in binary stellar systems

NASA Astrophysics Data System (ADS)

Cherepashchuk, Anatolii M.

1996-08-01

Mass determination methods and their results for ten black holes in X-ray binary systems are summarised. A unified interpretation of the radial velocity and optical light curves allows one to reliably justify the close binary system model and to prove the correctness of determination of the optical star mass function fv(m).The orbit plane inclination i can be estimated from an analysis of optical light curve of the system, which is due mainly to the ellipsoidal shape of the optical star (the so-called ellipticity effect). The component mass ratio q = mx/mv is obtained from information about the distance to the binary system as well as from data about rotational broadening of absorption lines in the spectrum of the optical star. These data allow one to obtain from the value of fv(m) a reliable value of the black hole mass mx or its low limit, as well as the optical star mass mv. An independent estimate of the optical star mass mv obtained from information about its spectral class and luminosity gives us test results. Additional test comes from information about the absence or presence of X-ray eclipses in the system. Effects of the non-zero dimension of the optical star, its pear-like shape, and X-ray heating on the absorption line profiles and the radial velocity curve are investigated. It is very significant that none of ten known massive (mx > 3M\\odot) X-ray sources considered as black hole candidates is an X-ray pulsar or an X-ray burster of the first kind.

Cascaded systems analysis of charge sharing in cadmium telluride photon-counting x-ray detectors.

PubMed

Tanguay, Jesse; Cunningham, Ian A

2018-05-01

Single-photon-counting (SPC) and spectroscopic x-ray detectors are under development in academic and industry laboratories for medical imaging applications. The spatial resolution of SPC and spectroscopic x-ray detectors is an important design criterion. The purpose of this article was to extend the cascaded systems approach to include a description of the spatial resolution of SPC and spectroscopic x-ray imaging detectors. A cascaded systems approach was used to model reabsorption of characteristic x rays, Coulomb repulsion, and diffusion in SPC and spectroscopic x-ray detectors. In addition to reabsorption, diffusion, and Coulomb repulsion, the model accounted for x-ray conversion to electron-hole (e-h) pairs, integration of e-h pairs in detector elements, electronic noise, and energy thresholding. The probability density function (PDF) describing the number of e-h pairs was propagated through each stage of the model and was used to derive new theoretical expressions for the large-area gain and modulation transfer function (MTF) of CdTe SPC x-ray detectors, and the energy bin sensitivity functions and MTFs of CdTe spectroscopic detectors. Theoretical predictions were compared with the results of MATLAB-based Monte Carlo (MC) simulations and published data. Comparisons were also made with the MTF of energy-integrating systems. Under general radiographic conditions, reabsorption, diffusion, and Coulomb repulsion together artificially inflate count rates by 20% to 50%. For thicker converters (e.g. 1000 μm) and larger detector elements (e.g. 500 μm pixel pitch) these processes result in modest inflation (i.e. ∼10%) in apparent count rates. Our theoretical and MC analyses predict that SPC MTFs will be degraded relative to those of energy-integrating systems for fluoroscopic, general radiographic, and CT imaging conditions. In most cases, this degradation is modest (i.e., ∼10% at the Nyquist frequency). However, for thicker converters, the SPC MTF can be degraded by up to 25% at the Nyquist frequency relative to EI systems. Additionally, unlike EI systems, the MTF of spectroscopic systems is strongly dependent on photon energy, which results in energy-bin-dependent spatial resolution in spectroscopic systems. The PDF-transfer approach to modeling signal transfer through SPC and spectroscopic x-ray imaging systems provides a framework for understanding system performance. Application of this approach demonstrated that charge sharing artificially inflates the SPC image signal and degrades the MTF of SPC and spectroscopic systems relative to energy-integrating systems. These results further motivate the need for anticharge-sharing circuits to mitigate the effects of charge sharing on SPC and spectroscopic x-ray image quality. © 2018 American Association of Physicists in Medicine.

Variable mid-latitude X-ray source 3U 0042+32

NASA Technical Reports Server (NTRS)

Rappaport, S.; Clark, G. W.; Dower, R.; Doxsey, R.; Jernigan, G.; Li, F.

1977-01-01

A celestial location with an error circle of radius one minute is reported for the mid-latitude X-ray source 3U 0042+32; comparison of observations from the Ariel-5 and Uhuru satellites with data obtained from two independent rotation modulation collimators yields the precise position. Studies to detect regular pulsations and energy spectra of the X-ray source are also discussed. Analysis of the peak X-ray flux in the error circle, as well as certain distance constraints, suggests that the source of the flux may be a neutron star in a distant galactic binary system having a companion that undergoes episodes of mass transfer due to eruption or orbital eccentricity.

New X-Ray Technique to Characterize Nanoscale Precipitates in Aged Aluminum Alloys

NASA Astrophysics Data System (ADS)

Sitdikov, V. D.; Murashkin, M. Yu.; Valiev, R. Z.

2017-10-01

This paper puts forward a new technique for measurement of x-ray patterns, which enables to solve the problem of identification and determination of precipitates (nanoscale phases) in metallic alloys of the matrix type. The minimum detection limit of precipitates in the matrix of the base material provided by this technique constitutes as little as 1%. The identification of precipitates in x-ray patterns and their analysis are implemented through a transmission mode with a larger radiation area, longer holding time and higher diffractometer resolution as compared to the conventional reflection mode. The presented technique has been successfully employed to identify and quantitatively describe precipitates formed in the Al alloy of the Al-Mg-Si system as a result of artificial aging. For the first time, the x-ray phase analysis has been used to identify and measure precipitates formed during the alloy artificial aging.

A laboratory demonstration of high-resolution hard X-ray and gamma-ray imaging using Fourier-transform techniques

NASA Technical Reports Server (NTRS)

Palmer, David; Prince, Thomas A.

1987-01-01

A laboratory imaging system has been developed to study the use of Fourier-transform techniques in high-resolution hard X-ray and gamma-ray imaging, with particular emphasis on possible applications to high-energy astronomy. Considerations for the design of a Fourier-transform imager and the instrumentation used in the laboratory studies is described. Several analysis methods for image reconstruction are discussed including the CLEAN algorithm and maximum entropy methods. Images obtained using these methods are presented.

Orbital Parameters for the X-Ray Pulsar IGR J16393-4643

NASA Astrophysics Data System (ADS)

Thompson, Thomas W. J.; Tomsick, John A.; Rothschild, Richard E.; in't Zand, J. J. M.; Walter, Roland

2006-09-01

With recent and archival Rossi X-Ray Timing Explorer (RXTE) X-ray measurements of the heavily obscured X-ray pulsar IGR J16393-4643, we carried out a pulse timing analysis to determine the orbital parameters. Assuming a circular orbit, we phase-connected data spanning over 1.5 yr. The most likely orbital solution has a projected semimajor axis of 43+/-2 lt-s and an orbital period of 3.6875+/-0.0006 days. This implies a mass function of 6.5+/-1.1 Msolar and confirms that this INTEGRAL source is a high-mass X-ray binary (HMXB) system. By including eccentricity in the orbital model, we find e<0.25 at the 2 σ level. The 3.7 day orbital period and the previously known ~910 s pulse period place the system in the region of the Corbet diagram populated by supergiant wind accretors, and the low eccentricity is also consistent with this type of system. Finally, it should be noted that although the 3.7 day solution is the most likely one, we cannot completely rule out two other solutions with orbital periods of 50.2 and 8.1 days.

Two new intermediate polars with a soft X-ray component

NASA Astrophysics Data System (ADS)

Anzolin, G.; de Martino, D.; Bonnet-Bidaud, J.-M.; Mouchet, M.; Gänsicke, B. T.; Matt, G.; Mukai, K.

2008-10-01

Aims: We analyze the first X-ray observations with XMM-Newton of 1RXS J070407.9+262501 and 1RXS 180340.0+401214, in order to characterize their broad-band temporal and spectral properties, also in the UV/optical domain, and to confirm them as intermediate polars. Methods: For both objects, we performed a timing analysis of the X-ray and UV/optical light curves to detect the white dwarf spin pulsations and study their energy dependence. For 1RXS 180340.0+401214 we also analyzed optical spectroscopic data to determine the orbital period. X-ray spectra were analyzed in the 0.2-10.0 keV range to characterize the emission properties of both sources. Results: We find that the X-ray light curves of both systems are energy dependent and are dominated, below 3-5 keV, by strong pulsations at the white dwarf rotational periods (480 s for 1RXS J070407.9+262501 and 1520.5 s for 1RXS 180340.0+401214). In 1RXS 180340.0+401214 we also detect an X-ray beat variability at 1697 s which, together with our new optical spectroscopy, favours an orbital period of 4.4 h that is longer than previously estimated. Both systems show complex spectra with a hard (temperature up to 40 keV) optically thin and a soft (kT ~ 85-100 eV) optically thick components heavily absorbed by material partially covering the X-ray sources. Conclusions: Our observations confirm the two systems as intermediate polars and also add them as new members of the growing group of “soft” systems which show the presence of a soft X-ray blackbody component. Differences in the temperatures of the blackbodies are qualitatively explained in terms of reprocessing over different sizes of the white dwarf spot. We suggest that systems showing cooler soft X-ray blackbody components also possess white dwarfs irradiated by cyclotron radiation. Based on observations obtained with XMM-Newton, an ESA science mission with instruments and contributions directly funded by ESA Member States and NASA, and with the Observatoire de Haute Provence (CNRS), France.

21 CFR 1020.40 - Cabinet x-ray systems.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Cabinet x-ray systems. 1020.40 Section 1020.40...) RADIOLOGICAL HEALTH PERFORMANCE STANDARDS FOR IONIZING RADIATION EMITTING PRODUCTS § 1020.40 Cabinet x-ray systems. (a) Applicability. The provisions of this section are applicable to cabinet x-ray systems...

21 CFR 1020.40 - Cabinet x-ray systems.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Cabinet x-ray systems. 1020.40 Section 1020.40...) RADIOLOGICAL HEALTH PERFORMANCE STANDARDS FOR IONIZING RADIATION EMITTING PRODUCTS § 1020.40 Cabinet x-ray systems. (a) Applicability. The provisions of this section are applicable to cabinet x-ray systems...

21 CFR 892.1630 - Electrostatic x-ray imaging system.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Electrostatic x-ray imaging system. 892.1630... (CONTINUED) MEDICAL DEVICES RADIOLOGY DEVICES Diagnostic Devices § 892.1630 Electrostatic x-ray imaging system. (a) Identification. An electrostatic x-ray imaging system is a device intended for medical...

21 CFR 892.1630 - Electrostatic x-ray imaging system.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Electrostatic x-ray imaging system. 892.1630... (CONTINUED) MEDICAL DEVICES RADIOLOGY DEVICES Diagnostic Devices § 892.1630 Electrostatic x-ray imaging system. (a) Identification. An electrostatic x-ray imaging system is a device intended for medical...

21 CFR 1020.40 - Cabinet x-ray systems.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Cabinet x-ray systems. 1020.40 Section 1020.40...) RADIOLOGICAL HEALTH PERFORMANCE STANDARDS FOR IONIZING RADIATION EMITTING PRODUCTS § 1020.40 Cabinet x-ray systems. (a) Applicability. The provisions of this section are applicable to cabinet x-ray systems...

Adaptive CT scanning system

DOEpatents

Sampayan, Stephen E.

2016-11-22

Apparatus, systems, and methods that provide an X-ray interrogation system having a plurality of stationary X-ray point sources arranged to substantially encircle an area or space to be interrogated. A plurality of stationary detectors are arranged to substantially encircle the area or space to be interrogated, A controller is adapted to control the stationary X-ray point sources to emit X-rays one at a time, and to control the stationary detectors to detect the X-rays emitted by the stationary X-ray point sources.

Measurement and simulation for a complementary imaging with the neutron and X-ray beams

NASA Astrophysics Data System (ADS)

Hara, Kaoru Y.; Sato, Hirotaka; Kamiyama, Takashi; Shinohara, Takenao

2017-09-01

By using a composite source system, we measured radiographs of the thermal neutron and keV X-ray in the 45-MeV electron linear accelerator facility at Hokkaido University. The source system provides the alternative beam of neutron and X-ray by switching the production target onto the electron beam axis. In the measurement to demonstrate a complementary imaging, the detector based on a vacuum-tube type neutron color image intensifier was applied to the both beams for dual-purpose. On the other hand, for reducing background in a neutron transmission spectrum, test measurements using a gadolinium-type neutron grid were performed with a cold neutron source at Hokkaido University. In addition, the simulations of the neutron and X-ray transmissions for various substances were performed using the PHITS code. A data analysis procedure for estimating the substance of sample was investigated through the simulations.

Novel micro-reactor flow cell for investigation of model catalysts using in situ grazing-incidence X-ray scattering

PubMed Central

Kehres, Jan; Pedersen, Thomas; Masini, Federico; Andreasen, Jens Wenzel; Nielsen, Martin Meedom; Diaz, Ana; Nielsen, Jane Hvolbæk; Hansen, Ole

2016-01-01

The design, fabrication and performance of a novel and highly sensitive micro-reactor device for performing in situ grazing-incidence X-ray scattering experiments of model catalyst systems is presented. The design of the reaction chamber, etched in silicon on insulator (SIO), permits grazing-incidence small-angle X-ray scattering (GISAXS) in transmission through 10 µm-thick entrance and exit windows by using micro-focused beams. An additional thinning of the Pyrex glass reactor lid allows simultaneous acquisition of the grazing-incidence wide-angle X-ray scattering (GIWAXS). In situ experiments at synchrotron facilities are performed utilizing the micro-reactor and a designed transportable gas feed and analysis system. The feasibility of simultaneous in situ GISAXS/GIWAXS experiments in the novel micro-reactor flow cell was confirmed with CO oxidation over mass-selected Ru nanoparticles. PMID:26917133

Current Technology Development Efforts on the International X-Ray Observatory

NASA Technical Reports Server (NTRS)

Robinson, David

2011-01-01

The International X-ray Observatory (IXO) is a collaboration between NASA, ESA, and JAXA which is under study for launch in 2021. IXO will be a large 6600 kilogram Great Observatory-class mission which will build upon the legacies of the Chandra and XMM-Newton X-ray observatories. There is an extensive ongoing effort to raise the technology readiness level of the X-ray mirror from TRL 3 to TRL 6 in the next decade. Improvements have recently been made in the area of positioning and bonding mirrors on the nanometer scale and developing metals and composites with a matching coefficient of thermal expansion to the glass X-ray mirrors. On the mission systems side, the NASA reference design has been through a preliminary coupled loads analysis and a STOP analysis of the flight mirror assembly has been initiated. An impact study was performed comparing launching IXO on an Ariane 5 or a U.S. EELV. This paper will provide a snapshot of NASA's current observatory configuration and summarize the progress of these various technology and design efforts.

Mapping the Dark Matter Distribution of the Merging Galaxy Cluster Abell 115

NASA Astrophysics Data System (ADS)

Kim, Mincheol; Jee, Myungkook James; Forman, William; Golovich, Nathan; van Weeren, Reinout

2018-01-01

The colliding galaxy cluster Abell 115 shows a number of clear merging features including radio relics, double X-ray peaks, and offsets between the cluster member galaxies and the X-ray distributions. In order to constrain the merging scenario of this complex system, it is critical to know where the dark matter is. We present a high-fidelity weak-lensing analysis of the system using a state-of-the-art method that robustly models the detailed PSF variations. Our mass reconstruction reveals two distinct mass peaks. Through a careful bootstrapping analysis, we demonstrate that the positions of these two mass peaks are highly consistent with those of the cluster galaxies, although the comparison with the X-ray emission shows that the mass peaks lead the X-ray peaks. We obtain the first weak-lensing mass of each subcluster by simultaneously fitting two NFW profiles, as well as the total mass of the system. Interestingly, the total mass is a few factors lower than the published dynamical mass based on velocity dispersion. This large mass discrepancy may be attributed to a significant disruption of the cluster galaxy orbits due to the violent merger. Our preliminary analysis indicates that the two subclusters might have experienced a first off-axis collision a few Gyrs ago and might be now returning for a second collision.

Characterization of New Hard X-ray Cataclysmic Variables

NASA Technical Reports Server (NTRS)

Bernardini, F.; deMartino, D.; Falanga, M.; Mukai, K.; Matt, G.; Bonnet-Bidaud, J.-M.; Masetti, N.; Mouchet, M.

2012-01-01

Aims. We aim at characterizing a sample of nine new hard X-ray selected Cataclysmic Variable (CVs), to unambiguously identify them as magnetic systems of the Intermediate Polar (IP) type. Methods. We performed detailed timing and spectral analysis by using X-ray, and simultaneous UV and optical data collected by XMM-Newton, complemented with hard X-ray data provided by INTEGRAL and Swift. The pulse arrival time were used to estimate the orbital periods. The broad band X-ray spectra were fitted using composite models consisting of different absorbing columns and emission components. Results. Strong X-ray pulses at the White Dwarf (WD) spin period are detected and found to decrease with energy. Most sources are spin-dominated systems in the X-rays, though four are beat dominated at optical wavelengths. We estimated the orbital period in all system (except for IGR J16500-3307), providing the first estimate for IGRJ08390-4833, IGRJ18308-1232, and IGR J18173-2509. All X-ray spectra are multi-temperature. V2069 Cyg and RX J0636+3535 poses a soft X-ray optically thick component at kT approx. 80 eV. An intense K (sub alpha) Fe line at 6.4 keV is detected in all sources. An absorption edge at 0.76 keV from OVII is detected in IGR J08390-4833. The WD masses and lower limits to the accretion rates are also estimated. Conclusions. We found all sources to be IPs. IGR J08390-4833, V2069 Cyg, and IGR J16500-3307 are pure disc accretors, while IGR J18308-1232, IGR J1509-6649, IGR J17195-4100, and RX J0636+3535 display a disc-overflow accretion mode. All sources show a temperature gradient in the post-shock regions and a highly absorbed emission from material located in the pre-shock flow which is also responsible for the X-ray pulsations. Reflection at the WD surface is likely the origin of the fluorescent iron line. There is an increasing evidence for the presence of a warm absorber in IPs, a feature that needs future exploration. The addition of two systems to the subgroup of soft X-ray IPs confirms a relatively large ( 30%) incidence.

Infrastructure development for radioactive materials at the NSLS-II

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sprouster, D. J.; Weidner, R.; Ghose, S. K.

2018-02-01

The X-ray Powder Diffraction (XPD) Beamline at the National Synchrotron Light Source-II is a multipurpose instrument designed for high-resolution, high-energy X-ray scattering techniques. In this article, the capabilities, opportunities and recent developments in the characterization of radioactive materials at XPD are described. The overarching goal of this work is to provide researchers access to advanced synchrotron techniques suited to the structural characterization of materials for advanced nuclear energy systems. XPD is a new beamline providing high photon flux for X-ray Diffraction, Pair Distribution Function analysis and Small Angle X-ray Scattering. The infrastructure and software described here extend the existing capabilitiesmore » at XPD to accommodate radioactive materials. Such techniques will contribute crucial information to the characterization and quantification of advanced materials for nuclear energy applications. We describe the automated radioactive sample collection capabilities and recent X-ray Diffraction and Small Angle X-ray Scattering results from neutron irradiated reactor pressure vessel steels and oxide dispersion strengthened steels.« less

Infrastructure development for radioactive materials at the NSLS-II

DOE PAGES

Sprouster, David J.; Weidner, R.; Ghose, S. K.; ...

2017-11-04

The X-ray Powder Diffraction (XPD) Beamline at the National Synchrotron Light Source-II is a multipurpose instrument designed for high-resolution, high-energy X-ray scattering techniques. In this paper, the capabilities, opportunities and recent developments in the characterization of radioactive materials at XPD are described. The overarching goal of this work is to provide researchers access to advanced synchrotron techniques suited to the structural characterization of materials for advanced nuclear energy systems. XPD is a new beamline providing high photon flux for X-ray Diffraction, Pair Distribution Function analysis and Small Angle X-ray Scattering. The infrastructure and software described here extend the existing capabilitiesmore » at XPD to accommodate radioactive materials. Such techniques will contribute crucial information to the characterization and quantification of advanced materials for nuclear energy applications. Finally, we describe the automated radioactive sample collection capabilities and recent X-ray Diffraction and Small Angle X-ray Scattering results from neutron irradiated reactor pressure vessel steels and oxide dispersion strengthened steels.« less

Interferometric analysis of laboratory photoionized plasmas utilizing supersonic gas jet targets.

NASA Astrophysics Data System (ADS)

Swanson, Kyle James; Ivanov, Vladimir; Mancini, Roberto; Mayes, Daniel C.

2018-06-01

Photoionized plasmas are an important component of active galactic nuclei, x-ray binary systems and other astrophysical objects. Laboratory produced photoionized plasmas have mainly been studied at large scale facilities, due to the need for high intensity broadband x-ray flux. Using supersonic gas jets as targets has allowed university scale pulsed power generators to begin similar research. The two main advantages of this approach with supersonic gas jets include: possibility of a closer location to the x-ray source and no attenuation related to material used for containment and or tamping. Due to these factors, this experimental platform creates a laboratory environment that more closely resembles astrophysical environments. This system was developed at the Nevada Terawatt Facility using the 1 MA pulsed power generator Zebra. Neon, argon, and nitrogen supersonic gas jets are produced approximately 7-8mm from the z-pinch axis. The high intensity broadband x-ray flux produced by the collapse of the z-pinch wire array implosion irradiates the gas jet. Cylindrical wire arrays are made with 4 and 8 gold 10µm thick wire. The z-pinch radiates approximately 12-16kj of x-ray energy, with x-ray photons under 1Kev in energy. The photoionized plasma is measured via x-ray absorption spectroscopy and interferometry. A Mach-Zehnder interferometer is used to the measure neutral density of the jet prior to the zebra shot at a wavelength of 266 nm. A dual channel air-wedge shearing interferometer is used to measure electron density of the ionized gas jet during the shot, at wavelengths of 532nm and 266nm. Using a newly developed interferometric analysis tool, average ionization state maps of the plasma can be calculated. Interferometry for nitrogen and argon show an average ionization state in the range of 3-8. Preliminary x-ray absorption spectroscopy collected show neon absorption lines. This work was sponsored in part by DOE Office of Science Grant DE-SC0014451.

The selection criteria elements of X-ray optics system

NASA Astrophysics Data System (ADS)

Plotnikova, I. V.; Chicherina, N. V.; Bays, S. S.; Bildanov, R. G.; Stary, O.

2018-01-01

At the design of new modifications of x-ray tomography there are difficulties in the right choice of elements of X-ray optical system. Now this problem is solved by practical consideration, selection of values of the corresponding parameters - tension on an x-ray tube taking into account the thickness and type of the studied material. For reduction of time and labor input of design it is necessary to create the criteria of the choice, to determine key parameters and characteristics of elements. In the article two main elements of X-ray optical system - an x-ray tube and the detector of x-ray radiation - are considered. Criteria of the choice of elements, their key characteristics, the main dependences of parameters, quality indicators and also recommendations according to the choice of elements of x-ray systems are received.

Disk Disruptions and X-ray Intensity Excursions in Cyg X-2, LMC X-3 and Cyg X-3

NASA Astrophysics Data System (ADS)

Boyd, P. T.; Smale, A. P.

2001-05-01

The RXTE All Sky Monitor soft X-ray light curves of many X-ray binaries show long-term intensity variations (a.k.a "superorbital periodicities") that have been ascribed to precession of a warped, tilted accretion disk around the X-ray source. We have found that the excursion times between X-ray minima in Cyg X-2 can be characterized as a series of integer multiples of the 9.8 binary orbital period, (as opposed to the previously reported stable 77.7 day single periodicity, or a single modulation whose period changes slowly with time). While the data set is too short for a proper statistical analysis, it is clear that the length of any given intensity excursion cannot be used to predict the next (integer) excursion length in the series. In the black hole candidate system LMC X-3, the excursion times are shown to be related to each other by rational fractions. We find that the long term light curve of the unusual galactic X-ray jet source Cyg X-3 can also be described as a series of intensity excursions related to each other by integer multiples of a fundamental underlying clock. In the latter cases, the clock is apparently not related to the known binary periods. A unified physical model, involving both an inclined accretion disk and a fixed-probability disk disruption mechanism is presented, and compared with three-body scattering results. Each time the disk passes through the orbital plane it experiences a fixed probability P that it will disrupt. This model has testable predictions---the distribution of integers should resemble that of an atomic process with a characteristic half life. Further analysis can support or refute the model, and shed light on what system parameters effectively set the value of P.

49 CFR 1544.211 - Use of X-ray systems.

Code of Federal Regulations, 2012 CFR

2012-10-01

... 49 Transportation 9 2012-10-01 2012-10-01 false Use of X-ray systems. 1544.211 Section 1544.211... COMMERCIAL OPERATORS Operations § 1544.211 Use of X-ray systems. (a) TSA authorization required. No aircraft operator may use any X-ray system within the United States or under the aircraft operator's operational...

On the influence of monochromator thermal deformations on X-ray focusing

DOE PAGES

Antimonov, M. A.; Khounsary, A. M.; Sandy, A. R.; ...

2016-03-02

A cooled double crystal monochromator system is used on many high heat load X-ray synchrotron radiation beamlines in order to select, by diffraction, a narrow spectrum of the beam. Thermal deformation of the first crystal monochromator – and the potential loss of beam brightness – is often a concern. However, if downstream beam focusing is planned, the lensing effect of the monochromator must be considered even if thermal deformations are small. In this paper we report on recent experiments at an Advanced Photon Source (APS) beamline that focuses the X-ray beam using compound refractive lenses downstream of an X-ray monochromatormore » system. Increasing the X-ray beam power by increasing the storage ring current from 100 mA to 130 mA resulted in an effective doubling of the focal distance. We show quantitatively that this is due to a lensing effect of the distorted monochromator that results in the creation of a virtual source downstream of the actual source. Lastly, an analysis of the defocusing and options to mitigate this effect are explored.« less

A multi-dataset data-collection strategy produces better diffraction data

PubMed Central

Liu, Zhi-Jie; Chen, Lirong; Wu, Dong; Ding, Wei; Zhang, Hua; Zhou, Weihong; Fu, Zheng-Qing; Wang, Bi-Cheng

2011-01-01

A multi-dataset (MDS) data-collection strategy is proposed and analyzed for macromolecular crystal diffraction data acquisition. The theoretical analysis indicated that the MDS strategy can reduce the standard deviation (background noise) of diffraction data compared with the commonly used single-dataset strategy for a fixed X-ray dose. In order to validate the hypothesis experimentally, a data-quality evaluation process, termed a readiness test of the X-ray data-collection system, was developed. The anomalous signals of sulfur atoms in zinc-free insulin crystals were used as the probe to differentiate the quality of data collected using different data-collection strategies. The data-collection results using home-laboratory-based rotating-anode X-ray and synchrotron X-ray systems indicate that the diffraction data collected with the MDS strategy contain more accurate anomalous signals from sulfur atoms than the data collected with a regular data-collection strategy. In addition, the MDS strategy offered more advantages with respect to radiation-damage-sensitive crystals and better usage of rotating-anode as well as synchrotron X-rays. PMID:22011470

A comparison between EGS4 and MCNP computer modeling of an in vivo X-ray fluorescence system.

PubMed

Al-Ghorabie, F H; Natto, S S; Al-Lyhiani, S H

2001-03-01

The Monte Carlo computer codes EGS4 and MCNP were used to develop a theoretical model of a 180 degrees geometry in vivo X-ray fluorescence system for the measurement of platinum concentration in head and neck tumors. The model included specification of the photon source, collimators, phantoms and detector. Theoretical results were compared and evaluated against X-ray fluorescence data obtained experimentally from an existing system developed by the Swansea In Vivo Analysis and Cancer Research Group. The EGS4 results agreed well with the MCNP results. However, agreement between the measured spectral shape obtained using the experimental X-ray fluorescence system and the simulated spectral shape obtained using the two Monte Carlo codes was relatively poor. The main reason for the disagreement between the results arises from the basic assumptions which the two codes used in their calculations. Both codes assume a "free" electron model for Compton interactions. This assumption will underestimate the results and invalidates any predicted and experimental spectra when compared with each other.

The Nature of the UV/X-ray Absorber In PG 2302+029

NASA Technical Reports Server (NTRS)

Sabra, Bassem M.; Hamann, Fred; Jannuzi, Buell T.; George, Ian M.; Shields, Joseph C.

2003-01-01

We present Chandra X-ray observations of the radio-quiet QSO PG 2302+029. This quasar has a rare system of ultra-high velocity (-56,000 km s(exp -1) UV absorption lines that form in an outflow from the active nucleus. The Chandra data indicate that soft X-ray absorption is also present. We perform a joint UV and X-ray analysis, using photoionization calculations, to determine the nature of the absorbing gas. The UV and X-ray datasets were not obtained simultaneously. Nonetheless, our analysis suggests that the X-ray absorption occurs at high velocities in the same general region as the UV absorber. There are not enough constraints to rule out multi-zone models. In fact, the distinct broad and narrow UV line profiles clearly indicate that multiple zones are present. Our preferred estimates of the ionization and total column density in the X-ray absorber (logU = 1.6, N(sub eta) = 10(exp 22.4) cm (exp -2) over predict the O VI lambda lambda1032,1038 absorption unless the X-ray absorber is also outflowing at approximately 56,000 km s(exp-l), but they over predict the Ne VIII lambda lambda 770,780 absorption at all velocities. If we assume that the X-ray absorbing gas is outflowing at the same velocity of the UV-absorbing wind and that the wind is radiatively accelerated, then the outflow must be launched at a radius of less than or equal to 10(exp 15) cm from the central continuum source. The smallness of this radius casts doubts on the assumption of radiative acceleration.

The effect of well-characterized, very low-dose x-ray radiation on fibroblasts

PubMed Central

Truong, Katelyn; Bradley, Suzanne; Baginski, Bryana; Wilson, Joseph R.; Medlin, Donald; Zheng, Leon; Wilson, R. Kevin; Rusin, Matthew; Takacs, Endre

2018-01-01

The purpose of this study is to determine the effects of low-dose radiation on fibroblast cells irradiated by spectrally and dosimetrically well-characterized soft x-rays. To achieve this, a new cell culture x-ray irradiation system was designed. This system generates characteristic fluorescent x-rays to irradiate the cell culture with x-rays of well-defined energies and doses. 3T3 fibroblast cells were cultured in cups with Mylar® surfaces and were irradiated for one hour with characteristic iron (Fe) K x-ray radiation at a dose rate of approximately 550 μGy/hr. Cell proliferation, total protein analysis, flow cytometry, and cell staining were performed on fibroblast cells to determine the various effects caused by the radiation. Irradiated cells demonstrated increased proliferation and protein production compared to control samples. Flow cytometry revealed that a higher percentage of irradiated cells were in the G0/G1 phase of the cell cycle compared to control counterparts, which is consistent with other low-dose studies. Cell staining results suggest that irradiated cells maintained normal cell functions after radiation exposure, as there were no qualitative differences between the images of the control and irradiated samples. The result of this study suggest that low-dose soft x-ray radiation might cause an initial pause, followed by a significant increase, in proliferation. An initial “pause” in cell proliferation could be a protective mechanism of the cells to minimize DNA damage caused by radiation exposure. The new cell irradiation system developed here allows for unprecedented control over the properties of the x-rays given to the cell cultures. This will allow for further studies on various cell types with known spectral distribution and carefully measured doses of radiation, which may help to elucidate the mechanisms behind varied cell responses to low-dose x-rays reported in the literature. PMID:29300773

The chaotic long-term X-ray variability of 4U 1705-44

NASA Astrophysics Data System (ADS)

Phillipson, R. A.; Boyd, P. T.; Smale, A. P.

2018-07-01

The low-mass X-ray binary 4U1705-44 exhibits dramatic long-term X-ray time variability with a time-scale of several hundred days. The All-Sky Monitor (ASM) aboard the Rossi X-ray Timing Explorer (RXTE) and the Japanese Monitor of All-sky X-ray Image (MAXI) aboard the International Space Station together have continuously observed the source from 1995 December through 2014 May. The combined ASM-MAXI data provide a continuous time series over 50 times the length of the time-scale of interest. Topological analysis can help us identify `fingerprints' in the phase space of a system unique to its equations of motion. The Birman-Williams theorem postulates that if such fingerprints are the same between two systems, then their equations of motion must be closely related. The phase-space embedding of the source light curve shows a strong resemblance to the double-welled non-linear Duffing oscillator. We explore a range of parameters for which the Duffing oscillator closely mirrors the time evolution of 4U1705-44. We extract low period, unstable periodic orbits from the 4U1705-44 and Duffing time series and compare their topological information. The Duffing and 4U1705-44 topological properties are identical, providing strong evidence that they share the same underlying template. This suggests that we can look to the Duffing equation to help guide the development of a physical model to describe the long-term X-ray variability of this and other similarly behaved X-ray binary systems.

Technique charts for Kodak EC-L film screen system for portal localization in a 6MV X-ray beam.

PubMed

Sandilos, P; Antypas, C; Paraskevopoulou, C; Kouvaris, J; Vlachos, L

2006-01-01

Port films are used in radiotherapy for visual evaluation of the radiation fields and subsequent quantitative analysis. Common port films suffer from poor image quality compared to the simulator-diagnostic films and is desirable to determine the appropriate exposure required for the best image contrast. The aim of this work is to generate technique charts for the Kodak EC-L film screen system for use in a 6MV x-ray beam. Three homogeneous water phantoms were used to simulate head-neck, thorax and abdomen dimensions of adult human, correspondingly. The film screen system was calibrated in a 6MV x-ray beam and under various irradiation conditions. The film screen system behavior was studied as a function of phantom thickness, field size and air gap between the phantom and the film screen system. In each case the optimum film exposure which produces the maximum image contrast was determined. The generated technique charts for the EC-L film screen system and for a 6 MV x-ray beam are used in our radiotherapy department for daily quality assurance of the radiotherapy procedure.

Nuclear Fuel Assay through analysis of Uranium L-shell by Hybrid L-edge/XRF Densitometer using a Surrogate Material

NASA Astrophysics Data System (ADS)

Park, Seunghoon; Joung, Sungyeop; Park, Jerry AB(; ), AC(; )

2018-01-01

Assay of L-series of nuclear material solution is useful for determination of amount of nuclear materials and ratio of minor actinide in the materials. The hybrid system of energy dispersive X-ray absorption edge spectrometry, i.e. L-edge densitometry, and X-ray fluorescence spectrometry is one of the analysis methods. The hybrid L-edge/XRF densitometer can be a promising candidate for a portable and compact equipment due to advantage of using low energy X-ray beams without heavy shielding systems and liquid nitrogen cooling compared to hybrid K-edge/XRF densitometer. A prototype of the equipment was evaluated for feasibility of the nuclear material assay using a surrogate material (lead) to avoid radiation effects from nuclear materials. The uncertainty of L-edge and XRF characteristics of the sample material and volume effects was discussed in the article.

X-ray morphological study of galaxy cluster catalogues

NASA Astrophysics Data System (ADS)

Democles, Jessica; Pierre, Marguerite; Arnaud, Monique

2016-07-01

Context : The intra-cluster medium distribution as probed by X-ray morphology based analysis gives good indication of the system dynamical state. In the race for the determination of precise scaling relations and understanding their scatter, the dynamical state offers valuable information. Method : We develop the analysis of the centroid-shift so that it can be applied to characterize galaxy cluster surveys such as the XXL survey or high redshift cluster samples. We use it together with the surface brightness concentration parameter and the offset between X-ray peak and brightest cluster galaxy in the context of the XXL bright cluster sample (Pacaud et al 2015) and a set of high redshift massive clusters detected by Planck and SPT and observed by both XMM-Newton and Chandra observatories. Results : Using the wide redshift coverage of the XXL sample, we see no trend between the dynamical state of the systems with the redshift.

Chandra X-Ray Observatory Observations of the Jovian System

NASA Technical Reports Server (NTRS)

Elsner, R. F.; Bhardwaj, A.; Gladstone, R.; Waite, J. H.; Ford, P.; Branduari-Raymont, G.

2005-01-01

Chandra X-ray Observatory (CXO) and XMM-Newton observations of x-rays from the Jovian system have answered questions that arose from early observations with the Einstein and Rosat X-ray Observatories, but in the process of vastly increasing our knowledge of x-ray emission from Jupiter and its environs they have also raised new questions and point to new opportunities for future studies. We will review recent x-ray results on the Jovian system, from the point of view of the CXO, and discuss various questions that have arisen in the course of our studies. We will discuss prospects for more observations in the immediate future, and how they might address open questions. Finally we will briefly describe ways in which an imaging x-ray spectrometer in the vicinity of the Jovian system could provide a wealth of data and results concerning Jupiter's x-ray auroral and disk emission, elemental abundance measurements for the Galilean moons, and detailed studies of x-ray emission from the Io Plasma Torus.

Structural analysis of jewelry from the Moche tomb of the `lady of Cao' by X-ray digital radiography

NASA Astrophysics Data System (ADS)

Azeredo, S. R.; Cesareo, R.; Franco, R.; Fernandez, A.; Bustamante, A.; Lopes, R. T.

2018-04-01

Nose ornaments from the tomb of the `Lady of Cao', a mummified woman representative of the Moche culture and dated to the third-or-fourth century AD, were analyzed by X-ray digital radiography. These spectacular gold and silver jewels are some of the most sophisticated metalworking ever produced in ancient America. The Mochecivilization flourished along the north coast of present-day Peru, between the Andes and the Pacific Ocean, approximately between 100 and 600 AD. The Moche were very sophisticated artisans and metal smiths, being considered the finest producers of jewels and artifacts of the region. A portable X-ray digital radiography (XDR) system consisting of a flat panel detector with high resolution image and a mini X-ray tube was used for the structural analysis of the Moche jewels aiming at inferring different joining methods of the silver-gold sheets. The radiographic analysis showed some differences in the joint of the silver-and-gold sheets. Presence of filler material and adhesive for joining the silver-and-gold sheets was visible as well as silver-gold junctions without filler material (or with a material invisible in radiography). Furthermore, the technique demonstrated the advantage of using a portable XDR micro system when the sample cannot be brought to the laboratory.

X-ray diffraction-based electronic structure calculations and experimental x-ray analysis for medical and materials applications

NASA Astrophysics Data System (ADS)

Mahato, Dip Narayan

This thesis includes x-ray experiments for medical and materials applications and the use of x-ray diffraction data in a first-principles study of electronic structures and hyperfine properties of chemical and biological systems. Polycapillary focusing lenses were used to collect divergent x rays emitted from conventional x-ray tubes and redirect them to form an intense focused beam. These lenses are routinely used in microbeam x-ray fluorescence analysis. In this thesis, their potential application to powder diffraction and focused beam orthovoltage cancer therapy has been investigated. In conventional x-ray therapy, very high energy (˜ MeV) beams are used, partly to reduce the skin dose. For any divergent beam, the dose is necessarily highest at the entry point, and decays exponentially into the tissue. To reduce the skin dose, high energy beams, which have long absorption lengths, are employed, and rotated about the patient to enter from different angles. This necessitates large expensive specialized equipment. A focused beam could concentrate the dose within the patient. Since this is inherently skin dose sparing, lower energy photons could be employed. A primary concern in applying focused beams to therapy is whether the focus would be maintained despite Compton scattering within the tissue. To investigate this, transmission and focal spot sizes as a function of photon energy of two polycapillary focusing lenses were measured. The effects of tissue-equivalent phantoms of different thicknesses on the focal spot size were studied. Scatter fraction and depth dose were calculated. For powder diffraction, the polycapillary optics provide clean Gaussian peaks, which result in angular resolution that is much smaller than the peak width due to the beam convergence. Powder diffraction (also called coherent scatter) without optics can also be used to distinguish between tissue types that, because they have different nanoscale structures, scatter at different angles. Measurements were performed on the development of coherent scatter imaging to provide tissue type information in mammography. Atomic coordinates from x-ray diffraction data were used to study the nuclear quadrupole interactions and nature of molecular binding in DNA/RNA nucleobases and molecular solid BF3 systems.

The study of chemical composition and elemental mappings of colored over-glaze porcelain fired in Qing Dynasty by micro-X-ray fluorescence

NASA Astrophysics Data System (ADS)

Lin, Cheng; Meitian, Li; Youshi, Kim; Changsheng, Fan; Shanghai, Wang; Qiuli, Pan; Zhiguo, Liu; Rongwu, Li

2011-02-01

It is very difficult to measure the chemical composition of colored pigments of over-glaze porcelain by X-ray fluorescence because it contains high concentration of Pb. One of the disadvantages of our polycapillary optics is that it has low transmission efficiency to the high energy X-ray. However, it is beneficial to measure the chemical compositions of rich Pb sample. In this paper, we reported the performances of a tabletop setup of micro-X-ray fluorescence system base on slightly focusing polycapillary and its applications for analysis of rich Pb sample. A piece of Chinese ancient over-glaze porcelain was analyzed by micro-X-ray fluorescence. The experimental results showed that the Cu, Fe and Mn are the major color elements. The possibilities of the process of decorative technology were discussed in this paper, also.

X-ray analysis of electron Bernstein wave heating in MST

DOE Office of Scientific and Technical Information (OSTI.GOV)

Seltzman, A. H., E-mail: seltzman@wisc.edu; Anderson, J. K.; DuBois, A. M.

2016-11-15

A pulse height analyzing x-ray tomography system has been developed to detect x-rays from electron Bernstein wave heated electrons in the Madison symmetric torus reversed field pinch (RFP). Cadmium zinc telluride detectors are arranged in a parallel beam array with two orthogonal multi-chord detectors that may be used for tomography. In addition a repositionable 16 channel fan beam camera with a 55° field of view is used to augment data collected with the Hard X-ray array. The chord integrated signals identify target emission from RF heated electrons striking a limiter located 12° toroidally away from the RF injection port. Thismore » provides information on heated electron spectrum, transport, and diffusion. RF induced x-ray emission from absorption on harmonic electron cyclotron resonances in low current (<250 kA) RFP discharges has been observed.« less

Large area CMOS active pixel sensor x-ray imager for digital breast tomosynthesis: Analysis, modeling, and characterization.

PubMed

Zhao, Chumin; Kanicki, Jerzy; Konstantinidis, Anastasios C; Patel, Tushita

2015-11-01

Large area x-ray imagers based on complementary metal-oxide-semiconductor (CMOS) active pixel sensor (APS) technology have been proposed for various medical imaging applications including digital breast tomosynthesis (DBT). The low electronic noise (50-300 e-) of CMOS APS x-ray imagers provides a possible route to shrink the pixel pitch to smaller than 75 μm for microcalcification detection and possible reduction of the DBT mean glandular dose (MGD). In this study, imaging performance of a large area (29×23 cm2) CMOS APS x-ray imager [Dexela 2923 MAM (PerkinElmer, London)] with a pixel pitch of 75 μm was characterized and modeled. The authors developed a cascaded system model for CMOS APS x-ray imagers using both a broadband x-ray radiation and monochromatic synchrotron radiation. The experimental data including modulation transfer function, noise power spectrum, and detective quantum efficiency (DQE) were theoretically described using the proposed cascaded system model with satisfactory consistency to experimental results. Both high full well and low full well (LFW) modes of the Dexela 2923 MAM CMOS APS x-ray imager were characterized and modeled. The cascaded system analysis results were further used to extract the contrast-to-noise ratio (CNR) for microcalcifications with sizes of 165-400 μm at various MGDs. The impact of electronic noise on CNR was also evaluated. The LFW mode shows better DQE at low air kerma (Ka<10 μGy) and should be used for DBT. At current DBT applications, air kerma (Ka∼10 μGy, broadband radiation of 28 kVp), DQE of more than 0.7 and ∼0.3 was achieved using the LFW mode at spatial frequency of 0.5 line pairs per millimeter (lp/mm) and Nyquist frequency ∼6.7 lp/mm, respectively. It is shown that microcalcifications of 165-400 μm in size can be resolved using a MGD range of 0.3-1 mGy, respectively. In comparison to a General Electric GEN2 prototype DBT system (at MGD of 2.5 mGy), an increased CNR (by ∼10) for microcalcifications was observed using the Dexela 2923 MAM CMOS APS x-ray imager at a lower MGD (2.0 mGy). The Dexela 2923 MAM CMOS APS x-ray imager is capable to achieve a high imaging performance at spatial frequencies up to 6.7 lp/mm. Microcalcifications of 165 μm are distinguishable based on reported data and their modeling results due to the small pixel pitch of 75 μm. At the same time, potential dose reduction is expected using the studied CMOS APS x-ray imager.

A novel x-ray imaging system and its imaging performance

NASA Astrophysics Data System (ADS)

Yu, Chunyu; Chang, Benkang; Wang, Shiyun; Zhang, Junju; Yao, Xiao

2006-09-01

Since x-ray was discovered and applied to the imaging technology, the x-ray imaging techniques have experienced several improvements, from film-screen, x-ray image intensifier, CR to DR. To store and transmit the image information conveniently, the digital imaging is necessary for the imaging techniques in medicine and biology. Usually as the intensifying screen technique as for concerned, to get the digital image signals, the CCD was lens coupled directly to the screen, but which suffers from a loss of x-ray signal and resulted in the poor x-ray image perfonnance. Therefore, to improve the image performance, we joined the brightness intensifier, which, was named the Low Light Level (LLL) image intensifier in military affairs, between the intensifying screen and the CCD and designed the novel x-ray imaging system. This design method improved the image performance of the whole system thus decreased the x-ray dose. Comparison between two systems with and without the brightness intensifier was given in detail in this paper. Moreover, the main noise source of the image produced by the novel system was analyzed, and in this paper, the original images produced by the novel x-ray imaging system and the processed images were given respectively. It was clear that the image performance was satisfied and the x-ray imaging system can be used in security checking and many other nondestructive checking fields.

A year-long AGILE observation of Cygnus X-1 in hard spectral state

NASA Astrophysics Data System (ADS)

Del Monte, E.; Feroci, M.; Evangelista, Y.; Costa, E.; Donnarumma, I.; Lapshov, I.; Lazzarotto, F.; Pacciani, L.; Rapisarda, M.; Soffitta, P.; Argan, A.; Barbiellini, G.; Boffelli, F.; Bulgarelli, A.; Caraveo, P.; Cattaneo, P. W.; Chen, A.; D'Ammando, F.; Di Cocco, G.; Fuschino, F.; Galli, M.; Gianotti, F.; Giuliani, A.; Labanti, C.; Lipari, P.; Longo, F.; Marisaldi, M.; Mereghetti, S.; Moretti, E.; Morselli, A.; Pellizzoni, A.; Perotti, F.; Piano, G.; Picozza, P.; Pilia, M.; Prest, M.; Pucella, G.; Rappoldi, A.; Sabatini, S.; Striani, E.; Tavani, M.; Trifoglio, M.; Trois, A.; Vallazza, E.; Vercellone, S.; Vittorini, V.; Zambra, A.; Antonelli, L. A.; Cutini, S.; Pittori, C.; Preger, B.; Santolamazza, P.; Verrecchia, F.; Giommi, P.; Salotti, L.

2010-09-01

Context. Cygnus X-1 (Cyg X-1) is a high mass X-ray binary system, known to be a black hole candidate and one of the brightest sources in the X-ray sky, which shows both variability on all timescales and frequent flares. The source spends most of the time in a hard spectral state, dominated by a power-law emission, with occasional transitions to the soft and intermediate states, where a strong blackbody component emerges. Aims: We present the observation of Cyg X-1 in a hard spectral state performed during the AGILE science verification phase and observing cycle 1 in hard X-rays (with SuperAGILE) and gamma rays (with the gamma ray imaging detector) and lasting for about 160 days with a live time of ~6 Ms. Methods: We investigated the variability of Cyg X-1 in hard X-rays on different timescales, from ~300 s up to one day, and we applied different tools of timing analysis, such as the autocorrelation function, the first-order structure function, and the Lomb-Scargle periodogram, to our data (from SuperAGILE) and to the simultaneous data in soft X-rays (from RXTE/ASM). We concluded our investigation with a search for emission in the energy range above 100 MeV with the maximum likelihood technique. Results: In the hard X-ray band, the flux of Cyg X-1 shows its typical erratic fluctuations on all timescales with variations of about a factor of two that do not significantly affect the shape of the energy spectrum. From the first-order structure function, we find that the X-ray emission of Cyg X-1 is characterized by antipersistence (anticorrelation in the time series, with an increase in the emission likely followed by a decrease), indicative of a negative feedback mechanism at work. In the gamma ray data a statistically significant point-like source at the position of Cyg X-1 is not found, and the upper limit on the flux is 5 × 10-8 ph cm-2 s-1 over the whole observation (160 days). Finally we compared our upper limit in gamma rays with the expectation of various models of the Cyg X-1 emission, both of hadronic and leptonic origin, in the GeV-TeV band. Conclusions: The time history of Cyg X-1 in the hard X-ray band over 13 months (not continuous) is shown. Different analysis tools do not provide fully converging results of the characteristic timescales in the system, suggesting that the timescales found in the structure function are not intrinsic to the physics of the source. While Cyg X-1 is not detected in gamma rays, our upper limit is a factor of two lower than the EGRET one and is compatible with the extrapolation of the flux measured by COMPTEL in the same spectral state.

X-Ray Microanalysis and Electron Energy Loss Spectrometry in the Analytical Electron Microscope: Review and Future Directions

NASA Technical Reports Server (NTRS)

Goldstein, J. I.; Williams, D. B.

1992-01-01

This paper reviews and discusses future directions in analytical electron microscopy for microchemical analysis using X-ray and Electron Energy Loss Spectroscopy (EELS). The technique of X-ray microanalysis, using the ratio method and k(sub AB) factors, is outlined. The X-ray absorption correction is the major barrier to the objective of obtaining I% accuracy and precision in analysis. Spatial resolution and Minimum Detectability Limits (MDL) are considered with present limitations of spatial resolution in the 2 to 3 microns range and of MDL in the 0.1 to 0.2 wt. % range when a Field Emission Gun (FEG) system is used. Future directions of X-ray analysis include improvement in X-ray spatial resolution to the I to 2 microns range and MDL as low as 0.01 wt. %. With these improvements the detection of single atoms in the analysis volume will be possible. Other future improvements include the use of clean room techniques for thin specimen preparation, quantification available at the I% accuracy and precision level with light element analysis quantification available at better than the 10% accuracy and precision level, the incorporation of a compact wavelength dispersive spectrometer to improve X-ray spectral resolution, light element analysis and MDL, and instrument improvements including source stability, on-line probe current measurements, stage stability, and computerized stage control. The paper reviews the EELS technique, recognizing that it has been slow to develop and still remains firmly in research laboratories rather than in applications laboratories. Consideration of microanalysis with core-loss edges is given along with a discussion of the limitations such as specimen thickness. Spatial resolution and MDL are considered, recognizing that single atom detection is already possible. Plasmon loss analysis is discussed as well as fine structure analysis. New techniques for energy-loss imaging are also summarized. Future directions in the EELS technique will be the development of new spectrometers and improvements in thin specimen preparation. The microanalysis technique needs to be simplified and software developed so that the EELS technique approaches the relative simplicity of the X-ray technique. Finally, one can expect major improvements in EELS imaging as data storage and processing improvements occur.

Continued Analysis of EUVE Solar System Observations

NASA Technical Reports Server (NTRS)

Gladstone, G. Randall

2001-01-01

This is the final report for this project. We proposed to continue our work on extracting important results from the EUVE (Extreme UltraViolet Explorer) archive of lunar and jovian system observations. In particular, we planned to: (1) produce several monochromatic images of the Moon at the wavelengths of the brightest solar EUV emission lines; (2) search for evidence of soft X-ray emissions from the Moon and/or X-ray fluorescence at specific EUV wavelengths; (3) search for localized EUV and soft X-ray emissions associated with each of the Galilean satellites; (4) search for correlations between localized Io Plasma Torus (IPT) brightness and volcanic activity on Io; (5) search for soft X-ray emissions from Jupiter; and (6) determine the long term variability of He 58.4 nm emissions from Jupiter, and relate these to solar variability. However, the ADP review panel suggested that the work concentrate on the Jupiter/IPT observations, and provided half the requested funding. Thus we have performed no work on the first two tasks, and instead concentrated on the last three. In addition we used funds from this project to support reduction and analysis of EUVE observations of Venus. While this was not part of the original statement of work, it is entirely in keeping with extracting important results from EUVE solar system observations.

Thin soil layer of green roof systems studied by X-Ray CT

NASA Astrophysics Data System (ADS)

Šácha, Jan; Jelínková, Vladimíra; Dohnal, Michal

2016-04-01

The popular non-invasive visualization technique of X-ray computed tomography (CT) has been used for 3D examination of thin soil layer of vegetated roof systems. The two categories of anthropogenic soils, usually used for green roof systems, were scanned during the first months after green roof system construction. First was represented by stripped topsoil with admixed crushed bricks and was well graded in terms of particle size distribution. The other category represented a commercial lightweight technogenic substrate. The undisturbed soil samples of total volume of 62.8 ccm were studied be means of X-ray Computed Tomography using X-ray Inspection System GE Phoenix Nanomex 180T with resulting spatial resolution about 57 μm in all directions. For both soil categories visible macroporosity, connectivity (described by the Euler characteristic), dimensionless connectivity and critical cross section of pore network were determined. Moreover, the temporal structural changes of studied soils were discussed together with heat and water regime of the green roof system. The analysis of CT images of anthropogenic soils was problematic due to the different X-ray attenuation of individual constituents. The correct determination of the threshold image intensity differentiating the soil constituents from the air phase had substantial importance for soil pore network analyses. However, X-ray CT derived macroporosity profiles reveal significant temporal changes notably in the soil comprised the stripped topsoil with admixed crushed bricks. The results implies that the technogenic substrate is structurally more stable over time compared to the stripped topsoil. The research was realized as a part of the University Centre for Energy Efficient Buildings supported by the EU and with financial support from the Czech Science Foundation under project number 14-10455P.

Analytical performance of benchtop total reflection X-ray fluorescence instrumentation for multielemental analysis of wine samples

NASA Astrophysics Data System (ADS)

Dalipi, Rogerta; Marguí, Eva; Borgese, Laura; Bilo, Fabjola; Depero, Laura E.

2016-06-01

Recent technological improvements have led to a widespread adoption of benchtop total reflection X-ray fluorescence systems (TXRF) for analysis of liquid samples. However, benchtop TXRF systems usually present limited sensitivity compared with high-scale instrumentation which can restrict its application in some fields. The aim of the present work was to evaluate and compare the analytical capabilities of two TXRF systems, equipped with low power Mo and W target X-ray tubes, for multielemental analysis of wine samples. Using the Mo-TXRF system, the detection limits for most elements were one order of magnitude lower than those attained using the W-TXRF system. For the detection of high Z elements like Cd and Ag, however, W-TXRF remains a very good option due to the possibility of K-Lines detection. Accuracy and precision of the obtained results have been evaluated analyzing spiked real wine samples and comparing the TXRF results with those obtained by inductively coupled plasma emission spectroscopy (ICP-OES). In general, good agreement was obtained between ICP-OES and TXRF results for the analysis of both red and white wine samples except for light elements (i.e., K) which TXRF concentrations were underestimated. However, a further achievement of analytical quality of TXRF results can be achieved if wine analysis is performed after dilution of the sample with de-ionized water.

Combined Photoneutron And X Ray Interrogation Of Containers For Nuclear Materials

NASA Astrophysics Data System (ADS)

Gozani, Tsahi; Shaw, Timothy; King, Michael J.; Stevenson, John; Elsalim, Mashal; Brown, Craig; Condron, Cathie

2011-06-01

Effective cargo inspection systems for nuclear material detection require good penetration by the interrogating radiation, generation of a sufficient number of fissions, and strong and penetrating detection signatures. Inspection systems need also to be sensitive over a wide range of cargo types and densities encountered in daily commerce. Thus they need to be effective with highly hydrogenous cargo, where neutron attenuation is a major limitation, as well as with dense metallic cargo, where x-ray penetration is low. A system that interrogates cargo with both neutrons and x-rays can, in principle, achieve high performance over the widest range of cargos. Moreover, utilizing strong prompt-neutron (˜3 per fission) and delayed-gamma ray (˜7 per fission) signatures further strengthens the detection sensitivity across all cargo types. The complementary nature of x-rays and neutrons, used as both probing radiation and detection signatures, alleviates the need to employ exceedingly strong sources, which would otherwise be required to achieve adequate performance across all cargo types, if only one type of radiation probe were employed. A system based on the above principles, employing a commercially-available 9 MV linac was developed and designed. Neutrons are produced simultaneously with x-rays by the photonuclear interaction of the x-ray beam with a suitable converter. A total neutron yield on the order of 1011 n/s is achieved with an average electron beam current of 100 μA. If fissionable material is present, fissions are produced both by the high-energy x-ray beam and by the photoneutrons. Photofission and neutron fission dominate in hydrogenous and metallic cargos, respectively. Neutron-capture gamma rays provide information on the cargo composition. The prompt neutrons resulting from fission are detected by two independent detector systems: by very efficient Differential Die Away Analysis (DDAA) detectors, and by direct detection of neutrons with energies higher than 3 MeV using a recently developed fluorine-based threshold activation detector (TAD). The delayed gamma-ray signals are measured with high efficiency with the same TAD and with additional lower-cost plastic scintillators.

Automatic Insall-Salvati ratio measurement on lateral knee x-ray images using model-guided landmark localization

NASA Astrophysics Data System (ADS)

Chen, Hsin-Chen; Lin, Chii-Jeng; Wu, Chia-Hsing; Wang, Chien-Kuo; Sun, Yung-Nien

2010-11-01

The Insall-Salvati ratio (ISR) is important for detecting two common clinical signs of knee disease: patella alta and patella baja. Furthermore, large inter-operator differences in ISR measurement make an objective measurement system necessary for better clinical evaluation. In this paper, we define three specific bony landmarks for determining the ISR and then propose an x-ray image analysis system to localize these landmarks and measure the ISR. Due to inherent artifacts in x-ray images, such as unevenly distributed intensities, which make landmark localization difficult, we hence propose a registration-assisted active-shape model (RAASM) to localize these landmarks. We first construct a statistical model from a set of training images based on x-ray image intensity and patella shape. Since a knee x-ray image contains specific anatomical structures, we then design an algorithm, based on edge tracing, for patella feature extraction in order to automatically align the model to the patella image. We can estimate the landmark locations as well as the ISR after registration-assisted model fitting. Our proposed method successfully overcomes drawbacks caused by x-ray image artifacts. Experimental results show great agreement between the ISRs measured by the proposed method and by orthopedic clinicians.

Sagittal focusing of synchrotron radiation X-rays using a winged crystal

PubMed Central

Nisawa, A.; Yoneda, Y.; Ueno, G.; Murakami, H.; Okajima, Y.; Yamamoto, K.; Senba, Y.; Uesugi, K.; Tanaka, Y.; Yamamoto, M.; Goto, S.; Ishikawa, T.

2013-01-01

A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the ‘golden value’. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal. PMID:23412477

Compton tomography system

DOEpatents

Grubsky, Victor; Romanoov, Volodymyr; Shoemaker, Keith; Patton, Edward Matthew; Jannson, Tomasz

2016-02-02

A Compton tomography system comprises an x-ray source configured to produce a planar x-ray beam. The beam irradiates a slice of an object to be imaged, producing Compton-scattered x-rays. The Compton-scattered x-rays are imaged by an x-ray camera. Translation of the object with respect to the source and camera or vice versa allows three-dimensional object imaging.

TEM analysis of irradiation-induced interaction layers in coated UMo/X/Al trilayer systems (X= Ti, Nb, Zr, and Mo)

NASA Astrophysics Data System (ADS)

Chiang, H.-Y.; Wiss, T.; Park, S.-H.; Dieste-Blanco, O.; Petry, W.

2018-02-01

Uranium-molybdenum (UMo) alloy powder embedded in an Al matrix is considered as a promising candidate for fuel conversion of research reactors. A modified system with a diffusion barrier X as coating, UMo/X/Al trilayer (X = Ti, Zr, Nb, and Mo), has been investigated to suppress interdiffusion between UMo and the Al matrix. The trilayer systems were tested by swift heavy ion irradiation, the thereby created interaction zone has been analyzed by scanning transmission electron microscopy (STEM) and energy-dispersive X-ray spectroscopy (EDX). Detailed structural characterization are presented and compared to earlier μ-XRD analysis.

Relationship between radiation dose reduction and image quality change in photostimulable phosphor luminescence X-ray imaging systems.

PubMed

Sakurai, T; Kawamata, R; Kozai, Y; Kaku, Y; Nakamura, K; Saito, M; Wakao, H; Kashima, I

2010-05-01

The aim of the study was to clarify the change in image quality upon X-ray dose reduction and to re-analyse the possibility of X-ray dose reduction in photostimulable phosphor luminescence (PSPL) X-ray imaging systems. In addition, the study attempted to verify the usefulness of multiobjective frequency processing (MFP) and flexible noise control (FNC) for X-ray dose reduction. Three PSPL X-ray imaging systems were used in this study. Modulation transfer function (MTF), noise equivalent number of quanta (NEQ) and detective quantum efficiency (DQE) were evaluated to compare the basic physical performance of each system. Subjective visual evaluation of diagnostic ability for normal anatomical structures was performed. The NEQ, DQE and diagnostic ability were evaluated at base X-ray dose, and 1/3, 1/10 and 1/20 of the base X-ray dose. The MTF of the systems did not differ significantly. The NEQ and DQE did not necessarily depend on the pixel size of the system. The images from all three systems had a higher diagnostic utility compared with conventional film images at the base and 1/3 X-ray doses. The subjective image quality was better at the base X-ray dose than at 1/3 of the base dose in all systems. The MFP and FNC-processed images had a higher diagnostic utility than the images without MFP and FNC. The use of PSPL imaging systems may allow a reduction in the X-ray dose to one-third of that required for conventional film. It is suggested that MFP and FNC are useful for radiation dose reduction.

1998 Technology Showcase. JOAP International Condition Monitoring Conference.

DTIC Science & Technology

1998-04-01

Systems using Automated SEM/ EDX and New Diagnostic Routines 276 N. W Farrant & T. Luckhurst ADVANCED DIAGNOSTIC SYSTEMS Model-Based Diagnostics of Gas...Microscopy with Energy Dispersive X-Ray (SEM/ EDX ) micro analysis packages and Energy Dispersive X-Ray Fluorescence (EDXRF) analytical equipment. Therqfore...wear particles separated by ferrogram method. a- I WEAR PARTICLE A SLAS 97 (HOME PAGE) Fig I Home Page NONFE;RROUS MATERIAL A wW~ a48 -1, rV fr , ý b

The physical origin of the X-ray emission from SN 1987A

NASA Astrophysics Data System (ADS)

Miceli, M.; Orlando, S.; Petruk, O.

2017-10-01

We revisit the spectral analysis of the set of archive XMM-Newton observations of SN 1987A through our 3-D hydrodynamic model describing the whole evolution from the onset of the supernova to the full remnant development. For the first time the spectral analysis accounts for the single observations and for the evolution of the system self-consistently. We adopt a forward modeling approach which allows us to directly synthesize, from the model, X-ray spectra and images in different energy bands. We fold the synthetic observables through the XMM-Newton instrumental response and directly compare models and actual data. We find that our simulation provides an excellent fit to the data, by reproducing simultaneously X-ray fluxes, spectral features, and morphology of SN 1987A at all evolutionary stages. Our analysis enables us to obtain a deep insight on the physical origin of the observed multi-thermal emission, by revealing the contribution of shocked surrounding medium, dense clumps of the circumstellar ring, and ejecta to the total emission. We finally provide predictions for future observations (to be performed with XMM-Newton in the next future and with the forthcoming Athena X-ray telescope in approximately 10 years), showing the growing contribution of the ejecta X-ray emission.

Application of x-ray absorption fine structure (XAFS) to local-order analysis in Fe-Cr maghemite-like materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Montero-Cabrera, M. E., E-mail: elena.montero@cimav.edu.mx; Fuentes-Cobas, L. E.; Macías-Ríos, E.

2015-07-23

The maghemite-like oxide system γ-Fe{sub 2-x}Cr{sub x}O{sub 3} (x=0.75, 1 and 1.25) was studied by X-ray absorption fine structure (XAFS) and by synchrotron radiation X-ray diffraction (XRD). Measurements were performed at the Stanford Synchrotron Radiation Lightsource at room temperature, at beamlines 2-1, 2-3 and 4-3. High-resolution XRD patterns were processed by means of the Rietveld method. In cases of atoms being neighbors in the Periodic Table, the order/disorder degree of the considered solutions is indiscernible by “normal” (absence of “anomalous scattering”) diffraction experiments. Thus, maghemite-like materials were investigated by XAFS in both Fe and Cr K-edges to clarify, via short-rangemore » structure characterization, the local ordering of the investigated system. Athena and Artemis graphic user interfaces for IFEFFIT and FEFF8.4 codes were employed for XAFS spectra interpretation. Pre-edge decomposition and theoretical modeling of X-ray absorption near edge structure (XANES) transitions were performed. By analysis of the Cr K-edge XANES, it has been confirmed that Cr is located in an octahedral environment. Fitting of the extended X-ray absorption fine structure (EXAFS) spectra was performed under the consideration that the central atom of Fe is allowed to occupy octa- and tetrahedral positions, while Cr occupies only octahedral ones. Coordination number of neighboring atoms, interatomic distances and their quadratic deviation average were determined for x=1, by fitting simultaneously the EXAFS spectra of both Fe and Cr K-edges. The results of fitting the experimental spectra with theoretical standards showed that the cation vacancies tend to follow a regular pattern within the structure of the iron-chromium maghemite (FeCrO{sub 3})« less

Design and analysis of multilayer x ray/XUV microscope

NASA Technical Reports Server (NTRS)

Shealy, David L.

1990-01-01

The design and analysis of a large number of normal incidence multilayer x ray microscopes based on the spherical mirror Schwarzschild configuration is examined. Design equations for the spherical mirror Schwarzschild microscopes are summarized and used to evaluate mirror parameters for microscopes with magnifications ranging from 2 to 50x. Ray tracing and diffraction analyses are carried out for many microscope configurations to determine image resolution as a function of system parameters. The results are summarized in three publication included herein. A preliminary study of advanced reflecting microscope configurations, where aspherics are used in place of the spherical microscope mirror elements, has indicated that the aspherical elements will improve off-axis image resolution and increase the effective field of view.

PIXE Analysis of Indoor Aerosols

NASA Astrophysics Data System (ADS)

Johnson, Christopher; Turley, Colin; Moore, Robert; Battaglia, Maria; Labrake, Scott; Vineyard, Michael

2011-10-01

We have performed a proton-induced X-ray emission (PIXE) analysis of aerosol samples collected in academic buildings at Union College to investigate the air quality in these buildings and the effectiveness of their air filtration systems. This is also the commissioning experiment for a new scattering chamber in the Union College Ion-Beam Analysis Laboratory. The aerosol samples were collected on Kapton foils using a nine-stage cascade impactor that separates particles according to their aerodynamic size. The foils were bombarded with beams of 2.2-MeV protons from the Union College 1.1-MV Pelletron Accelerator and the X-ray products were detected with an Amptek silicon drift detector. After subtracting the contribution from the Kapton foils, the X-ray energy spectra of the aerosol samples were analyzed using GUPIX software to determine the elemental concentrations of the samples. We will describe the collection of the aerosol samples, discuss the PIXE analysis, and present the results.

Quantitative X-ray mapping, scatter diagrams and the generation of correction maps to obtain more information about your material

NASA Astrophysics Data System (ADS)

Wuhrer, R.; Moran, K.

2014-03-01

Quantitative X-ray mapping with silicon drift detectors and multi-EDS detector systems have become an invaluable analysis technique and one of the most useful methods of X-ray microanalysis today. The time to perform an X-ray map has reduced considerably with the ability to map minor and trace elements very accurately due to the larger detector area and higher count rate detectors. Live X-ray imaging can now be performed with a significant amount of data collected in a matter of minutes. A great deal of information can be obtained from X-ray maps. This includes; elemental relationship or scatter diagram creation, elemental ratio mapping, chemical phase mapping (CPM) and quantitative X-ray maps. In obtaining quantitative x-ray maps, we are able to easily generate atomic number (Z), absorption (A), fluorescence (F), theoretical back scatter coefficient (η), and quantitative total maps from each pixel in the image. This allows us to generate an image corresponding to each factor (for each element present). These images allow the user to predict and verify where they are likely to have problems in our images, and are especially helpful to look at possible interface artefacts. The post-processing techniques to improve the quantitation of X-ray map data and the development of post processing techniques for improved characterisation are covered in this paper.

Bone cartilage imaging with x-ray interferometry using a practical x-ray tube

NASA Astrophysics Data System (ADS)

Kido, Kazuhiro; Makifuchi, Chiho; Kiyohara, Junko; Itou, Tsukasa; Honda, Chika; Momose, Atsushi

2010-04-01

The purpose of this study was to design an X-ray Talbot-Lau interferometer for the imaging of bone cartilage using a practical X-ray tube and to develop that imaging system for clinical use. Wave-optics simulation was performed to design the interferometer with a practical X-ray tube, a source grating, two X-ray gratings, and an X-ray detector. An imaging system was created based on the results of the simulation. The specifications were as follows: the focal spot size was 0.3 mm of an X-ray tube with a tungsten anode (Toshiba, Tokyo, Japan). The tube voltage was set at 40 kVp with an additive aluminum filter, and the mean energy was 31 keV. The pixel size of the X-ray detector, a Condor 486 (Fairchild Imaging, California, USA), was 15 μm. The second grating was a Ronchi-type grating whose pitch was 5.3 μm. Imaging performance of the system was examined with X-ray doses of 0.5, 3 and 9 mGy so that the bone cartilage of a chicken wing was clearly depicted with X-ray doses of 3 and 9 mGy. This was consistent with the simulation's predictions. The results suggest that X-ray Talbot-Lau interferometry would be a promising tool in detecting soft tissues in the human body such as bone cartilage for the X-ray image diagnosis of rheumatoid arthritis. Further optimization of the system will follow to reduce the X-ray dose for clinical use.

Development and tests of x-ray multifoil optical system for 1D imaging (Conference Presentation)

NASA Astrophysics Data System (ADS)

Pína, Ladislav; Hudec, René; Inneman, Adolf J.; Baca, Tomas; Blazek, M.; Platkevic, M.; Sieger, Ladislav; Doubravova, Daniela; McEntaffer, Randall L.; Schultz, Ted B.; Dániel, Vladimír.

2016-09-01

The proposed wide-field optical system has not been used yet. Described novel approach is based on the use of 1D "Lobster eye" optics in combination with Timepix X-ray detector in the energy range 3 - 40 keV. The proposed project includes theoretical study and a functional sample of the Timepix X-ray detector with multifoil wide-field X-ray "Lobster eye" optics. Using optics to focus X-rays on a detector is necessary in cases where the intensity of impinging X-ray radiation is below the sensitivity of the detector without optic. Generally this is the case of very low light phenomena, or e.g. monitoring astrophysical objects in space. Namely, such optical system could find applications in laboratory spectroscopy systems or in a rocket space experiment. Designed wide-field optical system combined with Timepix X-ray detector is described together with experimental results obtained during laboratory tests.

Discovery of Oxygen Kalpha X-ray Emission from the Rings of Saturn

NASA Technical Reports Server (NTRS)

Bhardwaj, Anil; Elsner, Ronald F.; Waite, J. Hunter, Jr.; Gladstone, G Randall; Cravens, Thomas E.; Ford, Peter G.

2005-01-01

Using the Advanced CCD Imaging Spectrometer (ACIS), the Chandra X-ray Observatory (CXO) observed the Saturnian system for one rotation of the planet (approx.37 ks) on 20 January, 2004, and again on 26-27 January, 2004. In this letter we report the detection of X-ray emission from the rings of Saturn. The X-ray spectrum from the rings is dominated by emission in a narrow (approx.130 eV wide) energy band centered on the atomic oxygen Ka fluorescence line at 0.53 keV. The X-ray power emitted from the rings in the 0.49-0.62 keV band is about one-third of that emitted from Saturn disk in the photon energy range 0.24-2.0 keV. Our analysis also finds a clear detection of X-ray emission from the rings in the 0.49-0.62 keV band in an earlier (14-15 April, 2003) Chandra ACIS observation of Saturn. Fluorescent scattering of solar X-rays from oxygen atoms in the H20 icy ring material is the likely source mechanism for ring X-rays, consistent with the scenario of solar photo-production of a tenuous ring oxygen atmosphere and ionosphere recently discovered by Cassini.

Winds in collision. II - An analysis of the X-ray emission from the eruptive symbiotic HM Sge

NASA Technical Reports Server (NTRS)

Willson, L. A.; Wallerstein, G.; Brugel, E. W.; Stencel, R. E.

1984-01-01

X-ray emissions from HM Sge obtained in 1981 from the HEAO-2 satellite are analyzed and compared quantitatively with observations of HM Sge made in 1980 and of HM Sge, V 1016 Cyg, and RR Tel made in 1979. The change in the X-ray emission from HM Sge between 1979 and 1981 is found to be consistent with the X-ray luminosity and/or temperature of the emitting region declining with an e-folding timescale of the order of one to several decades. Comparison with X-ray data from V 1016 Cyg and RR Tel gives a composite X-ray light curve that is also consistent with such a decline. A comparison of the X-ray observation with spectroscopic information makes it possible to constrain the properties of the X-ray emitting region: the result is consistent with emission from an optically thin region between the two stars in the system where their winds collide head on. It is also shown that the observations are inconsistent with a stellar (blackbody) source, with emission from an accretion disk around a white dwarf or a neutron star, and with emission from a single star wind from either a white dwarf or a neutron star.

Periodicity Analysis of X-ray Light Curves of SS 433

NASA Astrophysics Data System (ADS)

Wang, J. Y.; Lu, X. L.; Zhao, Q. W.; Dong, D. Q.; Lao, B. Q.; Lu, Y.; Wei, Y. H.; Wu, X. C.; An, T.

2016-03-01

SS 433 is the only X-ray binary to date that was detected to have a pair of well-collimated jets, and its orbital period, super orbital period, and nutation period were all detected at the same time. The study on the periodic X-ray variabilities is helpful for understanding its dynamic process of the central engine and the correlation with other bands. In the present paper, two time series analysis techniques, Lomb-Scargle periodogram and weighted wavelet Z-transform, are employed to search for the periodicities from the Swift/BAT (Burst Alert Telescope)(15--50 keV) and RXTE/ASM (Rossi X-Ray Timing Explorer/All-Sky Monitor)(1.5--3, 3--5 and 5--12 keV) light curves of SS 433, and the Monte Carlo simulation is performed. For the 15--50 keV energy band, five significant periodic signals are detected, which are P_1(˜6.29 d), P_2 (˜6.54 d), P_3 (˜13.08 d), P_4 (˜81.50 d), and P_5 (˜162.30 d). For the 3--5 and 5--12 keV energy bands, periodic signals P_3 (˜13 d) and P_5 (˜162 d) are detected in both energy bands. However, for the 1.5--3 keV energy band, no significant periodic signal is detected. P_5 has the strongest periodic signal in the power spectrum for all the energy bands of 3--5, 5--12, and 15--50 keV, and it is consistent with that obtained by previous study in optical band. Further, due to the existence of relativistic radio jets, the X-ray and optical band variability of P_5 (˜162 d) is probably related to the precession of the relativistic jets. High coherence between X-ray and optical light curves may also imply that the X-ray and optical emissions are of the same physical origin. P_3 shows a good agreement with the orbital period (˜13.07 d) first obtained by previous study, and P_2 and P_4 are the high frequency harmonic components of P_3 and P_5, respectively. P_1 is detected from the power spectrum of 15--50 keV energy band only, and it is consistent with the systematic nutation period. As the power of energy band decreases (from hard X-ray to soft X-ray), less periodicities are detected, which provides an evidence that the emission from high energy band (hard X-ray) comes primarily from jets, and the emission from low energy band (soft X-ray) may originate from the medium around binary systems. The multiple X-ray periods obtained from the present studies provide the necessary basis for the analysis of multi-wavelength data and the dynamics of the central engine system of SS 433.

A Comparison of the Variability of the Symbiotic X-ray Binaries GX 1+4, 4U 1954+31, and 4U 1700+24 from Swift/BAT and RXTE/ASM Observations

NASA Technical Reports Server (NTRS)

Corbet, R. H. D.; Sokoloski, J. L.; Mukai, K.; Markwardt, C. B.; Tueller, J.

2007-01-01

We present an analysis of the X-ray variability of three symbiotic X-ray binaries, GX 1+4, 4U 1700+24, and 4U 1954+31, using observations made with the Swift Burst Alert Telescope (BAT) and the Rossi X-ray Timing Explorer (RXTE) All-Sky Monitor (ASM). Observations of 4U 1954+31 with the Swift BAT show modulation at a period near 5 hours. Models to explain this modulation are discussed including the presence of an exceptionally slow X-ray pulsar in the system and accretion instabilities. We conclude that the most likely interpretation is that 4U 1954+31 contains one of the slowest known X-ray pulsars. Unlike 4U 1954+31, neither GX 1+4 nor 4U 1700+24 show any evidence for modulation on a timescale of hours. An analysis of the RXTE ASM light curves of GX l+4, 4U 1700+24, and 4U 1954+31 does not show the presence of periodic modulation in any source, although there is considerable variability on long timescales for all three sources. There is no modulation in GX 1+4 on either the optical 1161 day orbital period or a previously reported 304 day X-ray period. For 4U 1700+24 we do not confirm the 404 day period previously proposed for this source from a shorter duration ASM light curve.

Ground calibrations of the X-ray detector system of the Solar Intensity X-ray Spectrometer (SIXS) on board BepiColombo

NASA Astrophysics Data System (ADS)

Huovelin, Juhani; Lehtolainen, Arto; Genzer, Maria; Korpela, Seppo; Esko, Eero; Andersson, Hans

2014-05-01

SIXS includes X-ray and particle detector systems for the BepiColombo Mercury Planetary Orbiter (MPO). Its task is to monitor the direct solar X-rays and energetic particles in a wide field of view in the energy range of 1-20 keV (X-rays), 0.1-3 MeV (electrons) and 1-30 MeV (protons). The main purpose of these measurements is to provide quantitative information on the high energy radiation incident on Mercury's surface which causes the X-ray glow of the planet measured by the MIXS instrument. The X-ray and particle measurements of SIXS are also useful for investigations of the solar corona and the magnetosphere of Mercury. The ground calibrations of the X-ray detectors of the SIXS flight model were carried out in the X-ray laboratory of the Helsinki University during May and June 2012. The aim of the ground calibrations was to characterize the performance of the SIXS instrument's three High-Purity Silicon PIN X-ray detectors and verify that they fulfil their scientific performance requirements. The calibrations included the determination of the beginning of life energy resolution at different operational temperatures, determination of the detector's sensitivity within the field of view as a function of the off-axis and roll angles, pile-up tests for determining the speed of the read out electronics, measurements of the low energy threshold of the energy scale, a cross-calibration with the SMART-1 XSM flight spare detector, and the determination of the temperature dependence of the energy scale. An X-ray tube and the detectors' internal Ti coated 55Fe calibration sources were used as primary X-ray sources. In addition, two external fluorescence sources were used as secondary X-ray sources in the determination of the energy resolutions and in the comparison calibration with the SMART-1 XSM. The calibration results show that the detectors fulfill all of the scientific performance requirements. The ground calibration data combined with the instrument house-keeping data, spacecraft attitude data in relation to the Sun, and the in-flight calibration spectra measured during the operations contain all required information for the final analysis of the solar X-ray data.

A wavelet analysis for the X-ray absorption spectra of molecules

DOE Office of Scientific and Technical Information (OSTI.GOV)

Penfold, T. J.; Ecole polytechnique Federale de Lausanne, Laboratoire de chimie et biochimie computationnelles, ISIC, FSB-BCH, CH-1015 Lausanne; SwissFEL, Paul Scherrer Inst, CH-5232 Villigen

2013-01-07

We present a Wavelet transform analysis for the X-ray absorption spectra of molecules. In contrast to the traditionally used Fourier transform approach, this analysis yields a 2D correlation plot in both R- and k-space. As a consequence, it is possible to distinguish between different scattering pathways at the same distance from the absorbing atom and between the contributions of single and multiple scattering events, making an unambiguous assignment of the fine structure oscillations for complex systems possible. We apply this to two previously studied transition metal complexes, namely iron hexacyanide in both its ferric and ferrous form, and a rheniummore » diimine complex, [ReX(CO){sub 3}(bpy)], where X = Br, Cl, or ethyl pyridine (Etpy). Our results demonstrate the potential advantages of using this approach and they highlight the importance of multiple scattering, and specifically the focusing phenomenon to the extended X-ray absorption fine structure (EXAFS) spectra of these complexes. We also shed light on the low sensitivity of the EXAFS spectrum to the Re-X scattering pathway.« less

Coherent diffraction imaging analysis of shape-controlled nanoparticles with focused hard X-ray free-electron laser pulses.

PubMed

Takahashi, Yukio; Suzuki, Akihiro; Zettsu, Nobuyuki; Oroguchi, Tomotaka; Takayama, Yuki; Sekiguchi, Yuki; Kobayashi, Amane; Yamamoto, Masaki; Nakasako, Masayoshi

2013-01-01

We report the first demonstration of the coherent diffraction imaging analysis of nanoparticles using focused hard X-ray free-electron laser pulses, allowing us to analyze the size distribution of particles as well as the electron density projection of individual particles. We measured 1000 single-shot coherent X-ray diffraction patterns of shape-controlled Ag nanocubes and Au/Ag nanoboxes and estimated the edge length from the speckle size of the coherent diffraction patterns. We then reconstructed the two-dimensional electron density projection with sub-10 nm resolution from selected coherent diffraction patterns. This method enables the simultaneous analysis of the size distribution of synthesized nanoparticles and the structures of particles at nanoscale resolution to address correlations between individual structures of components and the statistical properties in heterogeneous systems such as nanoparticles and cells.

Observation and analysis of microcirculation using high-spatial-resolution image detectors and synchrotron radiation

NASA Astrophysics Data System (ADS)

Umetani, Keiji; Yagi, Naoto; Suzuki, Yoshio; Ogasawara, Yasuo; Kajiya, Fumihiko; Matsumoto, Takeshi; Tachibana, Hiroyuki; Goto, Masami; Yamashita, Takenori; Imai, Shigeki; Kajihara, Yasumasa

2000-04-01

A microangiography system using monochromatized synchrotron radiation has been investigated as a diagnostic tool for circulatory disorders and early stage malignant tumors. The monochromatized X-rays with energies just above the contrast agent K-absorption edge energy can produce the highest contrast image of the contrast agent in small blood vessels. At SPring-8, digital microradiography with 6 - 24 micrometer pixel sizes has been carried out using two types of detectors designed for X-ray indirect and direct detection. The indirect-sensing detectors are fluorescent-screen optical-lens coupling systems using a high-sensitivity pickup-tube camera and a CCD camera. An X-ray image on the fluorescent screen is focused on the photoconductive layer of the pickup tube and the photosensitive area of the CCD by a small F number lens. The direct-sensing detector consists of an X-ray direct- sensing pickup tube with a beryllium faceplate for X-ray incidence to the photoconductive layer. Absorbed X-rays in the photoconductive layer are directly converted to photoelectrons and then signal charges are readout by electron beam scanning. The direct-sensing detector was expected to have higher spatial resolution in comparison with the indict-sensing detectors. Performance of the X-ray image detectors was examined at the bending magnet beamline BL20B2 using monochromatized X-ray at SPring-8. Image signals from the camera are converted into digital format by an analog-to- digital converter and stored in a frame memory with image format of 1024 X 1024 pixels. In preliminary experiments, tumor vessel specimens using barium contrast agent were prepared for taking static images. The growth pattern of tumor-induced vessels was clearly visualized. Heart muscle specimens were prepared for imaging of 3-dimensional microtomography using the fluorescent-screen CCD camera system. The complex structure of small blood vessels with diameters of 30 - 40 micrometer was visualized as a 3- dimensional CT image.

Use of capillary optics as a beam intensifier for a Compton x-ray source.

PubMed

Tompkins, P A; Abreu, C C; Carroll, F E; Xiao, Q F; MacDonald, C A

1994-11-01

The use of Kumakhov capillary optics will significantly enhance the performance of near-monochromatic, Compton backscattered x-ray programs. The Vanderbilt University Medical Free-Electron Laser Center is developing the capability to create these tunable x rays for medical imaging. The present transport has only reflection optics, and the beam is quite large in diameter at the laboratory. Low loss collimation of this beam would allow higher x-ray intensities after transport. This article describes experimental and computer simulation results which predict the expected performance for a multifiber Kumakhov collimator for use in the x-ray beam transport. Estimates from our research are that a multifiber optic formed of individual polycapillary fibers could be used to capture the full 7 mrad of the Vanderbilt x-ray beam and collimate it to a 1-2 mrad divergence with approximately 40%-50% transmission efficiency. This optic should increase the x-ray intensity at the laboratory level by a factor of > or = 5 by decreasing the beam divergence and subsequent spot size. Additionally, analysis of monolithic optics of fused multicapillary fibers predicts an increase in the intensity of the x rays at the laboratory by a factor of 55. These optics can have tapered channels that greatly decrease their exit divergence. This will greatly enhance the capabilities of this unique x-ray source. This article reports the initial results from a collaboration between Vanderbilt, The Center for X-Ray Optics at University at Albany, SUNY, and X-Ray Optical Systems in Albany, NY.

Analysis system of submicron particle tracks in the fine-grained nuclear emulsion by a combination of hard x-ray and optical microscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Naka, T., E-mail: naka@flab.phys.nagoya-u.ac.jp; Institute for Advanced Research, Nagoya University, Aichi 464-8602; Asada, T.

Analyses of nuclear emulsion detectors that can detect and identify charged particles or radiation as tracks have typically utilized optical microscope systems because the targets have lengths from several μm to more than 1000 μm. For recent new nuclear emulsion detectors that can detect tracks of submicron length or less, the current readout systems are insufficient due to their poor resolution. In this study, we developed a new system and method using an optical microscope system for rough candidate selection and the hard X-ray microscope system at SPring-8 for high-precision analysis with a resolution of better than 70 nm resolution.more » Furthermore, we demonstrated the analysis of submicron-length tracks with a matching efficiency of more than 99% and position accuracy of better than 5 μm. This system is now running semi-automatically.« less

X-ray tomography using the full complex index of refraction.

PubMed

Nielsen, M S; Lauridsen, T; Thomsen, M; Jensen, T H; Bech, M; Christensen, L B; Olsen, E V; Hviid, M; Feidenhans'l, R; Pfeiffer, F

2012-10-07

We report on x-ray tomography using the full complex index of refraction recorded with a grating-based x-ray phase-contrast setup. Combining simultaneous absorption and phase-contrast information, the distribution of the full complex index of refraction is determined and depicted in a bivariate graph. A simple multivariable threshold segmentation can be applied offering higher accuracy than with a single-variable threshold segmentation as well as new possibilities for the partial volume analysis and edge detection. It is particularly beneficial for low-contrast systems. In this paper, this concept is demonstrated by experimental results.

Stimulated resonant x-ray Raman scattering with incoherent radiation

NASA Astrophysics Data System (ADS)

Weninger, Clemens; Rohringer, Nina

2013-11-01

We present a theoretical study on stimulated electronic Raman scattering in neon by resonant excitation with an x-ray free electron laser (XFEL). This study is in support of the recent experimental demonstration [C. Weninger , Phys. Rev. Lett. (to be published)] of stimulated x-ray Raman scattering. Focusing the broadband XFEL pulses into a cell of neon gas at atmospheric pressure a strong inelastic x-ray scattering signal in the forward direction was observed, as the x-ray energy was varied across the region of core-excited Rydberg states and the K edge. The broadband and intrinsically incoherent x-ray pulses from the XFEL lead to a rich, structured line shape of the scattered radiation. We present a generalized Maxwell-Liouville-von Neumann approach to self-consistently solve for the amplification of the scattered radiation along with the time evolution of the density matrix of the atomic and residual ionic system. An in-depth analysis of the evolution of the emission spectra as a function of the Raman gain is presented. Furthermore, we propose the use of statistical methods to obtain high-resolution scattering data beyond the lifetime broadening despite pumping with incoherent x-ray pulses.

MACS J0553.4-3342: a young merging galaxy cluster caught through the eyes of Chandra and HST

NASA Astrophysics Data System (ADS)

Pandge, M. B.; Bagchi, Joydeep; Sonkamble, S. S.; Parekh, Viral; Patil, M. K.; Dabhade, Pratik; Navale, Nilam R.; Raychaudhury, Somak; Jacob, Joe

2017-12-01

We present a detailed analysis of a young merging galaxy cluster MACS J0553.4-3342 (z=0.43) from Chandra X-ray and Hubble Space Telescope archival data. X-ray observations confirm that the X-ray emitting intra-cluster medium (ICM) in this system is among the hottest (average T = 12.1 ± 0.6 keV) and most luminous known. Comparison of X-ray and optical images confirms that this system hosts two merging subclusters SC1 and SC2, separated by a projected distance of about 650 kpc. The subcluster SC2 is newly identified in this work, while another subcluster (SC0), previously thought to be a part of this merging system, is shown to be possibly a foreground object. Apart from two subclusters, we find a tail-like structure in the X-ray image, extending to a projected distance of ∼1 Mpc, along the north-east direction of the eastern subcluster (SC1). From a surface brightness analysis, we detect two sharp surface brightness edges at ∼40 (∼320 kpc) and ∼80 arcsec (∼640 kpc) to the east of SC1. The inner edge appears to be associated with a merger-driven cold front, while the outer one is likely to be due to a shock front, the presence of which, ahead of the cold front, makes this dynamically disturbed cluster interesting. Nearly all the early-type galaxies belonging to the two subclusters, including their brightest cluster galaxies, are part of a well-defined red sequence.

Semiconductor and thermoluminescent dosimetry of pulsed soft X ray plasma sources.

PubMed

Krása, J; Cejnarová, A; Juha, L; Ryć, L; Scholz, M; Kubes, P

2002-01-01

A multichannel detection system having a dynamic range of approximately 1 x 10(-9) Gy --20 Gy was developed with the use of commercially produced Si-photodiodes and TLDs for accurate measurement of X ray energy emitted from plasma-focus facility and from laser-produced plasmas. The proof of linearity of the employed detectors accomplished by a comparison of their responses to a broad band spectrum of X rays emitted from plasmas, is reported. It is demonstrated that TLDs irradiated with no protective filter show an incorrect response due to overloading in the sub-keV range and repopulation of dosimetric peaks induced by the UV radiation. The measurement of the power of undesirable secondary X ray sources driven by the primary plasma inside the interaction chamber was performed on the basis of analysis of space dependence of X ray intensity with respect to the assumed r(-2) decrease in the intensity far away from the plasma.

Intensity correlation measurement system by picosecond single shot soft x-ray laser.

PubMed

Kishimoto, Maki; Namikawa, Kazumichi; Sukegawa, Kouta; Yamatani, Hiroshi; Hasegawa, Noboru; Tanaka, Momoko

2010-01-01

We developed a new soft x-ray speckle intensity correlation spectroscopy system by use of a single shot high brilliant plasma soft x-ray laser. The plasma soft x-ray laser is characterized by several picoseconds in pulse width, more than 90% special coherence, and 10(11) soft x-ray photons within a single pulse. We developed a Michelson type delay pulse generator using a soft x-ray beam splitter to measure the intensity correlation of x-ray speckles from materials and succeeded in generating double coherent x-ray pulses with picosecond delay times. Moreover, we employed a high-speed soft x-ray streak camera for the picosecond time-resolved measurement of x-ray speckles caused by double coherent x-ray pulse illumination. We performed the x-ray speckle intensity correlation measurements for probing the relaxation phenomena of polarizations in polarization clusters in the paraelectric phase of the ferroelectric material BaTiO(3) near its Curie temperature and verified its performance.

Very High Energy Emission from the Binary System Cyg X-3

NASA Astrophysics Data System (ADS)

Sinitsyna, V. G.; Sinitsyna, V. Yu.

2018-03-01

Cyg X-3 is actively studied in the entire range of the electromagnetic spectrum from the radio band to ultrahigh energies. Based on the detection of ultrahigh-energy gamma-ray emission, it has been suggested that Cyg X-3 could be one of the most powerful sources of charged cosmic-ray particles in the Galaxy. We present the results of long-term observations of the Cygnus X-3 region at energies 800 GeV-100 TeV by the SHALON mirror Cherenkov telescope. In 1995 the SHALON observations revealed a new Galactic source of very high energy gamma-ray emission coincident in its coordinates with the microquasar Cyg X-3. To reliably identify the detected source with Cyg X-3, an analysis has been performed and an orbital period of 4.8 h has been found, which is a signature of Cyg X-3. A series of flares in Cyg X-3 at energies >800 GeV and their correlation with the activity in the X-ray and radio bands have been observed. The results obtained in a wide energy range for Cyg X-3, including those during the periods of relativistic jet events, are needed to find the connection and to understand the different components of an accreting binary system.

X-ray Binaries in the Central Region of M31

NASA Astrophysics Data System (ADS)

Trudolyubov, Sergey P.; Priedhorsky, W. C.; Cordova, F. A.

2006-09-01

We present the results of the systematic survey of X-ray sources in the central region of M31 using the data of XMM-Newton observations. The spectral properties and variability of 124 bright X-ray sources were studied in detail. We found that more than 80% of sources observed in two or more observations show significant variability on the time scales of days to years. At least 50% of the sources in our sample are spectrally variable. The fraction of variable sources in our survey is much higher than previously reported from Chandra survey of M31, and is remarkably close to the fraction of variable sources found in M31 globular cluster X-ray source population. We present spectral distribution of M31 X-ray sources, based on the spectral fitting with a power law model. The distribution of spectral photon index has two main peaks at 1.8 and 2.3, and shows clear evolution with source luminosity. Based on the similarity of the properties of M31 X-ray sources and their Galactic counterparts, we expect most of X-ray sources in our sample to be accreting binary systems with neutron star and black hole primaries. Combining the results of X-ray analysis (X-ray spectra, hardness-luminosity diagrams and variability) with available data at other wavelengths, we explore the possibility of distinguishing between bright neutron star and black hole binary systems, and identify 7% and 25% of sources in our sample as a probable black hole and neutron star candidates. Finally, we compare the M31 X-ray source population to the source populations of normal galaxies of different morphological type. Support for this work was provided through NASA Grant NAG5-12390. Part of this work was done during a summer workshop ``Revealing Black Holes'' at the Aspen Center for Physics, S. T. is grateful to the Center for their hospitality.

TXM-Wizard: a program for advanced data collection and evaluation in full-field transmission X-ray microscopy

PubMed Central

Liu, Yijin; Meirer, Florian; Williams, Phillip A.; Wang, Junyue; Andrews, Joy C.; Pianetta, Piero

2012-01-01

Transmission X-ray microscopy (TXM) has been well recognized as a powerful tool for non-destructive investigation of the three-dimensional inner structure of a sample with spatial resolution down to a few tens of nanometers, especially when combined with synchrotron radiation sources. Recent developments of this technique have presented a need for new tools for both system control and data analysis. Here a software package developed in MATLAB for script command generation and analysis of TXM data is presented. The first toolkit, the script generator, allows automating complex experimental tasks which involve up to several thousand motor movements. The second package was designed to accomplish computationally intense tasks such as data processing of mosaic and mosaic tomography datasets; dual-energy contrast imaging, where data are recorded above and below a specific X-ray absorption edge; and TXM X-ray absorption near-edge structure imaging datasets. Furthermore, analytical and iterative tomography reconstruction algorithms were implemented. The compiled software package is freely available. PMID:22338691

Some Like it Hot: Linking Diffuse X-Ray Luminosity, Baryonic Mass, and Star Formation Rate in Compact Groups of Galaxies

NASA Technical Reports Server (NTRS)

Desjardins, Tyler D.; Gallagher, Sarah C.; Hornschemeier, Ann E.; Mulchaey, John S.; Walker, Lisa May; Brandt, Willian N.; Charlton, Jane C.; Johnson, Kelsey E.; Tzanavaris, Panayiotis

2014-01-01

We present an analysis of the diffuse X-ray emission in 19 compact groups (CGs) of galaxies observed with Chandra. The hottest, most X-ray luminous CGs agree well with the galaxy cluster X-ray scaling relations in L(x-T) and (L(x-sigma), even in CGs where the hot gas is associated with only the brightest galaxy. Using Spitzer photometry, we compute stellar masses and classify Hickson CGs 19, 22, 40, and 42, and RSCGs 32, 44, and 86 as fossil groups using a new definition for fossil systems that includes a broader range of masses. We find that CGs with total stellar and Hi masses are great than or equal to 10(sup (11.3) solar mass are often X-ray luminous, while lower-mass CGs only sometimes exhibit faint, localized X-ray emission. Additionally, we compare the diffuse X-ray luminosity against both the total UV and 24 micron star formation rates of each CG and optical colors of the most massive galaxy in each of the CGs. The most X-ray luminous CGs have the lowest star formation rates, likely because there is no cold gas available for star formation, either because the majority of the baryons in these CGs are in stars or the X-ray halo, or due togas stripping from the galaxies in CGs with hot halos. Finally, the optical colors that trace recent star formation histories of the most massive group galaxies do not correlate with the X-ray luminosities of the CGs, indicating that perhaps the current state of the X-ray halos is independent of the recent history of stellar mass assembly in the most massive galaxies.

Current developments and tests of small x-ray optical systems for space applications

NASA Astrophysics Data System (ADS)

Pina, L.; Hudec, R.; Inneman, A.; Doubravová, D.; Marsikova, V.

2017-05-01

The paper addresses the X-ray monitoring for astrophysical applications. A novel approach based on the use of 1D and 2D "Lobster eye" optics in combination with Timepix X-ray detector in the energy range 3 - 40 keV was further studied. Wide-field optical system of this type has not been used in space yet. Designed wide-field optical system combined with Timepix X-ray detector is described together with latest experimental results obtained during laboratory tests. Proposed project includes theoretical study and a functional sample of the Timepix X-ray detector with multifoil wide-field X-ray "Lobster eye" optics. Using optics to focus X-rays on a detector is the only solution in cases where intensity of impinging X-ray radiation is below the sensitivity of the detector, e.g. while monitoring astrophysical objects in space, or phenomena in the Earth's atmosphere. The optical system is considered to be used in a student rocket experiment.

Method of photon spectral analysis

DOEpatents

Gehrke, Robert J.; Putnam, Marie H.; Killian, E. Wayne; Helmer, Richard G.; Kynaston, Ronnie L.; Goodwin, Scott G.; Johnson, Larry O.

1993-01-01

A spectroscopic method to rapidly measure the presence of plutonium in soils, filters, smears, and glass waste forms by measuring the uranium L-shell x-ray emissions associated with the decay of plutonium. In addition, the technique can simultaneously acquire spectra of samples and automatically analyze them for the amount of americium and .gamma.-ray emitting activation and fission products present. The samples are counted with a large area, thin-window, n-type germanium spectrometer which is equally efficient for the detection of low-energy x-rays (10-2000 keV), as well as high-energy .gamma. rays (>1 MeV). A 8192- or 16,384 channel analyzer is used to acquire the entire photon spectrum at one time. A dual-energy, time-tagged pulser, that is injected into the test input of the preamplifier to monitor the energy scale, and detector resolution. The L x-ray portion of each spectrum is analyzed by a linear-least-squares spectral fitting technique. The .gamma.-ray portion of each spectrum is analyzed by a standard Ge .gamma.-ray analysis program. This method can be applied to any analysis involving x- and .gamma.-ray analysis in one spectrum and is especially useful when interferences in the x-ray region can be identified from the .gamma.-ray analysis and accommodated during the x-ray analysis.

Method of photon spectral analysis

DOEpatents

Gehrke, R.J.; Putnam, M.H.; Killian, E.W.; Helmer, R.G.; Kynaston, R.L.; Goodwin, S.G.; Johnson, L.O.

1993-04-27

A spectroscopic method to rapidly measure the presence of plutonium in soils, filters, smears, and glass waste forms by measuring the uranium L-shell x-ray emissions associated with the decay of plutonium. In addition, the technique can simultaneously acquire spectra of samples and automatically analyze them for the amount of americium and [gamma]-ray emitting activation and fission products present. The samples are counted with a large area, thin-window, n-type germanium spectrometer which is equally efficient for the detection of low-energy x-rays (10-2,000 keV), as well as high-energy [gamma] rays (>1 MeV). A 8,192- or 16,384 channel analyzer is used to acquire the entire photon spectrum at one time. A dual-energy, time-tagged pulser, that is injected into the test input of the preamplifier to monitor the energy scale, and detector resolution. The L x-ray portion of each spectrum is analyzed by a linear-least-squares spectral fitting technique. The [gamma]-ray portion of each spectrum is analyzed by a standard Ge [gamma]-ray analysis program. This method can be applied to any analysis involving x- and [gamma]-ray analysis in one spectrum and is especially useful when interferences in the x-ray region can be identified from the [gamma]-ray analysis and accommodated during the x-ray analysis.

Comparison of radiation dose, workflow, patient comfort and financial break-even of standard digital radiography and a novel biplanar low-dose X-ray system for upright full-length lower limb and whole spine radiography.

PubMed

Dietrich, Tobias J; Pfirrmann, Christian W A; Schwab, Alexander; Pankalla, Katja; Buck, Florian M

2013-07-01

To compare the radiation dose, workflow, patient comfort, and financial break-even of a standard digital radiography and a biplanar low-dose X-ray system. A standard digital radiography system (Ysio, Siemens Healthcare, Erlangen, Germany) was compared with a biplanar X-ray unit (EOS, EOS imaging, Paris, France) consisting of two X-ray tubes and slot-scanning detectors, arranged at an angle of 90° allowing simultaneous vertical biplanar linear scanning in the upright patient position. We compared data of standing full-length lower limb radiographs and whole spine radiographs of both X-ray systems. Dose-area product was significantly lower for radiographs of the biplanar X-ray system than for the standard digital radiography system (e.g. whole spine radiographs; standard digital radiography system: 392.2 ± 231.7 cGy*cm(2) versus biplanar X-ray system: 158.4 ± 103.8 cGy*cm(2)). The mean examination time was significantly shorter for biplanar radiographs compared with standard digital radiographs (e.g. whole spine radiographs: 449 s vs 248 s). Patients' comfort regarding noise was significantly higher for the standard digital radiography system. The financial break-even point was 2,602 radiographs/year for the standard digital radiography system compared with 4,077 radiographs/year for the biplanar X-ray unit. The biplanar X-ray unit reduces radiation exposure and increases subjective noise exposure to patients. The biplanar X-ray unit demands a higher number of examinations per year for the financial break-even point, despite the lower labour cost per examination due to the shorter examination time.

Truly hybrid interventional MR/X-ray system: investigation of in vivo applications.

PubMed

Fahrig, R; Butts, K; Wen, Z; Saunders, R; Kee, S T; Sze, D Y; Daniel, B L; Laerum, F; Pelc, N J

2001-12-01

The purpose of this study was to provide in vivo demonstrations of the functionality of a truly hybrid interventional x-ray/magnetic resonance (MR) system. A digital flat-panel x-ray system (1,024(2) array of 200 microm pixels, 30 frames per second) was integrated into an interventional 0.5-T magnet. The hybrid system is capable of MR and x-ray imaging of the same field of view without patient movement. Two intravascular procedures were performed in a 22-kg porcine model: placement of a transjugular intrahepatic portosystemic shunt (TIPS) (x-ray-guided catheterization of the hepatic vein, MR fluoroscopy-guided portal puncture, and x-ray-guided stent placement) and mock chemoembolization (x-ray-guided subselective catheterization of a renal artery branch and MR evaluation of perfused volume). The resolution and frame rate of the x-ray fluoroscopy images were sufficient to visualize and place devices, including nitinol guidewires (0.016-0.035-inch diameter) and stents and a 2.3-F catheter. Fifth-order branches of the renal artery could be seen. The quality of both real-time (3.5 frames per second) and standard MR images was not affected by the x-ray system. During MR-guided TIPS placement, the trocar and the portal vein could be easily visualized, allowing successful puncture from hepatic to portal vein. Switching back and forth between x-ray and MR imaging modalities without requiring movement of the patient was demonstrated. The integrated nature of the system could be especially beneficial when x-ray and MR image guidance are used iteratively.

Development of a 3-D X-ray system

NASA Astrophysics Data System (ADS)

Evans, James Paul Owain

The interpretation of standard two-dimensional x-ray images by humans is often very difficult. This is due to the lack of visual cues to depth in an image which has been produced by transmitted radiation. The solution put forward in this research is to introduce binocular parallax, a powerful physiological depth cue, into the resultant shadowgraph x-ray image. This has been achieved by developing a binocular stereoscopic x-ray imaging technique, which can be used for both visual inspection by human observers and also for the extraction of three-dimensional co-ordinate information. The technique is implemented in the design and development of two experimental x-ray systems and also the development of measurement algorithms. The first experimental machine is based on standard linear x-ray detector arrays and was designed as an optimum configuration for visual inspection by human observers. However, it was felt that a combination of the 3-D visual inspection capability together with a measurement facility would enhance the usefulness of the technique. Therefore, both a theoretical and an empirical analysis of the co-ordinate measurement capability of the machine has been carried out. The measurement is based on close-range photogrammetric techniques. The accuracy of the measurement has been found to be of the order of 4mm in x, 3mm in y and 6mm in z. A second experimental machine was developed and based on the same technique as that used for the first machine. However, a major departure has been the introduction of a dual energy linear x-ray detector array which will allow, in general, the discrimination between organic and inorganic substances. The second design is a compromise between ease of visual inspection for human observers and optimum three-dimensional co-ordinate measurement capability. The system is part of an on going research programme into the possibility of introducing psychological depth cues into the resultant x-ray images. The research presented in this thesis was initiated to enhance the visual interpretation of complex x-ray images, specifically in response to problems encountered in the routine screening of freight by HM. Customs and Excise. This phase of the work culminated in the development of the first experimental machine. During this work the security industry was starting to adopt a new type of x-ray detector, namely the dual energy x-ray sensor. The Department of Transport made available funding to the Police Scientific Development Branch (P.S.D.B.), part of The Home Office Science and Technology Group, to investigate the possibility of utilising the dual energy sensor in a 3-D x-ray screening system. This phase of the work culminated in the development of the second experimental machine.

Explosives detection using photoneutrons produced by X-rays

NASA Astrophysics Data System (ADS)

Yang, Yigang; Li, Yuanjing; Wang, Haidong; Li, Tiezhu; Wu, Bin

2007-08-01

The detection of explosives has become a critical issue after recent terrorist attacks. This paper describes research on explosives detection using photoneutrons from a photoneutron convertor that consists of 20 kg heavy water in an aluminum container whose shape was optimized to most effectively convert X-rays to photoneutrons. The X-rays were produced by a 9 MeV electron accelerator with an average electron current of 100 μA, resulted in a photoneutron yield of >10 11 n/s. Monte-Carlo simulations show that the radiation field is composed of X-ray pulses, fast neutron pulses and thermal neutrons. Both the X-ray and fast neutron pulses are 5 μs wide with a 300 Hz repetition frequency. The thermal neutron flux, which is higher than 10 4 n/cm 2/s, is essentially time invariant. A time shielding circuit was developed for the spectrometry system to halt the sampling process during the intense X-ray pulses. Paraffin, boron carbide and lead were used to protect the detector from interference from the X-rays, fast neutrons, thermal neutrons and background γ-rays coming from the system materials induced by photoneutrons. 5″×5″ NaI (Tl) scintillators were chosen as the detectors to detect the photoneutrons induced γ-rays from the inspected explosive simulant. Nitrogen (6.01 cps) 10.828 MeV γ-rays were detected with one detector from a 50 kg carbamide block placed 60 cm in front of the detector. A collimator was used to reduce the number of background 10.828 MeV γ-rays coming from the nitrogen in the air to improve the signal to background ratio from 0.136 to 1.81. A detector array of seven 5″×5″ NaI (Tl) detectors was used to measure the 2-D distributions of N and H in the sample. The combination of photoneutron analysis and X-ray imaging shows promise for enhancing explosives detection capabilities.

A Comparative View of X-rays from the Solar System

NASA Technical Reports Server (NTRS)

Bhardwaj, Anil; Elsner, Ron; Gladstone, Randy; Cravens, Tom; Waite, Hunter; Branduardi-Raymont, Graziella; Ostgaard, Nikolai; Dennerl, Konrad; Lisse, Carey; Kharchenko, Vasili

2005-01-01

With the advent of sophisticated X-ray observatories, viz., Chandra and XMM-Newton, the field of planetary X-ray astronomy is advancing at a faster pace. Several new solar system objects are now know to shine in X-rays at energies generally below 2 keV. Jupiter, Saturn, and Earth, all three magnetized planets, have been observed by Chandra and XMM-Newton. At Jupiter, both auroral and non-auroral disk X-ray emissions have been observed. The first soft X-ray observation of Earth's aurora by Chandra shows that it is highly variable. X-rays have been detected from Saturn's disk, but no convincing evidence of X-ray aurora has been seen. Several comets have been observed in X-rays by Chandra and XMM-Newton. Cometary X-rays are produced due to change exchange of solar wind ions with cold cometary neutrals. Soft X-rays have also been observed from Venus, Mars, Moon, Io, Europa, Io plasma torus, and heliosphere. The non-auroral X-ray emissions from Jupiter, Saturn, and Earth, and those from sunlit disk of Mars, Venus, and Moon are produced due to scattering of solar X-rays. The spectral characteristics of X-ray emission from comets, heliosphere, darkside of Moon, and Martian halo are quite similar, but they appear to be quite different from those of Jovian auroral X-rays. The X- ray aurora on Earth is generated by electron bremsstrahlung and on Jupiter by precipitation of highly-ionized energetic heavy ions. In this paper we will present a comparative overview of X-ray emission from different solar system objects and make an attempt to synthesize a coherent picture.

Systems and methods for detecting an image of an object using multi-beam imaging from an X-ray beam having a polychromatic distribution

DOEpatents

Parham, Christopher A; Zhong, Zhong; Pisano, Etta; Connor, Jr., Dean M

2015-03-03

Systems and methods for detecting an image of an object using a multi-beam imaging system from an x-ray beam having a polychromatic energy distribution are disclosed. According to one aspect, a method can include generating a first X-ray beam having a polychromatic energy distribution. Further, the method can include positioning a plurality of monochromator crystals in a predetermined position to directly intercept the first X-ray beam such that a plurality of second X-ray beams having predetermined energy levels are produced. Further, an object can be positioned in the path of the second X-ray beams for transmission of the second X-ray beams through the object and emission from the object as transmitted X-ray beams. The transmitted X-ray beams can each be directed at an angle of incidence upon one or more crystal analyzers. Further, an image of the object can be detected from the beams diffracted from the analyzer crystals.

Irreversible metal-insulator transition in thin film VO2 induced by soft X-ray irradiation

NASA Astrophysics Data System (ADS)

Singh, V. R.; Jovic, V.; Valmianski, I.; Ramirez, J. G.; Lamoureux, B.; Schuller, Ivan K.; Smith, K. E.

2017-12-01

In this study, we show the ability of soft x-ray irradiation to induce room temperature metal-insulator transitions (MITs) in VO2 thin films grown on R-plane sapphire. The ability of soft x-rays to induce MIT in VO2 thin films is confirmed by photoemission spectroscopy and soft x-ray spectroscopy measurements. When irradiation was discontinued, the systems do not return to the insulating phase. Analysis of valence band photoemission spectra revealed that the density of states (DOSs) of the V 3d band increased with irradiation time, while the DOS of the O 2p band decreased. We use these results to propose a model in which the MIT is driven by oxygen desorption from thin films during irradiation.

Study of Lead as a Source X-ray Radiation Protection with an Analysis Grey Level Image

NASA Astrophysics Data System (ADS)

Susilo; Rahma, I. N.; Mosik; Masturi

2017-04-01

X-ray utilization in the medical field still has a potential danger for the human. This occurs when exposure to x-ray radiation received exceeds the dose limit value. It required a radiation shielding to prevent the hazard, and lead is one of the metals usually used as x-ray radiation shield. This work aims to determine the metallic lead properties to find out of the step wedge lead radiograph image. The instruments used are the plane x-ray, digital radiography system and personal computer installed by MATLAB, while the material is step wedge lead. The image of radiograph was analysed using GUI applications on MATLAB software to determine the values of grey level from the image and the optical density of the radiograph image. The results showed the greater optical density, the higher the image contrast, and the value of optical density in the image is inversely proportional to the voltage x-ray since the value of grey level at high voltage is smaller than that of at low voltage.

Instrument and method for X-ray diffraction, fluorescence, and crystal texture analysis without sample preparation

NASA Technical Reports Server (NTRS)

Gendreau, Keith (Inventor); Martins, Jose Vanderlei (Inventor); Arzoumanian, Zaven (Inventor)

2010-01-01

An X-ray diffraction and X-ray fluorescence instrument for analyzing samples having no sample preparation includes a X-ray source configured to output a collimated X-ray beam comprising a continuum spectrum of X-rays to a predetermined coordinate and a photon-counting X-ray imaging spectrometer disposed to receive X-rays output from an unprepared sample disposed at the predetermined coordinate upon exposure of the unprepared sample to the collimated X-ray beam. The X-ray source and the photon-counting X-ray imaging spectrometer are arranged in a reflection geometry relative to the predetermined coordinate.

Femtosecond laser-electron x-ray source

DOEpatents

Hartemann, Frederic V.; Baldis, Hector A.; Barty, Chris P.; Gibson, David J.; Rupp, Bernhard

2004-04-20

A femtosecond laser-electron X-ray source. A high-brightness relativistic electron injector produces an electron beam pulse train. A system accelerates the electron beam pulse train. The femtosecond laser-electron X-ray source includes a high intra-cavity power, mode-locked laser and an x-ray optics system.

Micro X-ray diffraction analysis of thin films using grazing-exit conditions.

PubMed

Noma, T; Iida, A

1998-05-01

An X-ray diffraction technique using a hard X-ray microbeam for thin-film analysis has been developed. To optimize the spatial resolution and the surface sensitivity, the X-ray microbeam strikes the sample surface at a large glancing angle while the diffracted X-ray signal is detected with a small (grazing) exit angle. Kirkpatrick-Baez optics developed at the Photon Factory were used, in combination with a multilayer monochromator, for focusing X-rays. The focused beam size was about 10 x 10 micro m. X-ray diffraction patterns of Pd, Pt and their layered structure were measured. Using a small exit angle, the signal-to-background ratio was improved due to a shallow escape depth. Under the grazing-exit condition, the refraction effect of diffracted X-rays was observed, indicating the possibility of surface sensitivity.

Observations of X-ray flares in G-K dwarfs by XMM-Newton

NASA Astrophysics Data System (ADS)

Pandey, Jeewan Chandra

Eclipsing binary BD +5 706 is best investigated member of rare class of cool Algols, which differ from clasical Algol systems in that the mass gaining component is also a late-type star. The analysis of X-ray lightcurve of this system registered by ROSAT suggested the primary component to be the dominant source of activity in the system (Torres et al, AJ 125, 3237, 2003). We reconstruct the spatial structure of coronal emission within the system according to the method proposed by Siarkowski, and show that coronal emission is most likely attributed to both components.

Element sensitive reconstruction of nanostructured surfaces with finite elements and grazing incidence soft X-ray fluorescence.

PubMed

Soltwisch, Victor; Hönicke, Philipp; Kayser, Yves; Eilbracht, Janis; Probst, Jürgen; Scholze, Frank; Beckhoff, Burkhard

2018-03-29

The geometry of a Si3N4 lamellar grating was investigated experimentally with reference-free grazing-incidence X-ray fluorescence analysis. While simple layered systems are usually treated with the matrix formalism to determine the X-ray standing-wave field, this approach fails for laterally structured surfaces. Maxwell solvers based on finite elements are often used to model electrical field strengths for any 2D or 3D structures in the optical spectral range. We show that this approach can also be applied in the field of X-rays. The electrical field distribution obtained with the Maxwell solver can subsequently be used to calculate the fluorescence intensities in full analogy to the X-ray standing-wave field obtained by the matrix formalism. Only the effective 1D integration for the layer system has to be replaced by a 2D integration of the finite elements, taking into account the local excitation conditions. We will show that this approach is capable of reconstructing the geometric line shape of a structured surface with high elemental sensitivity. This combination of GIXRF and finite-element simulations paves the way for a versatile characterization of nanoscale-structured surfaces.

The Geometry of the Stellar Winds and Shock Structure in V444 Cyg

NASA Astrophysics Data System (ADS)

Hoffman, Jennifer

Given the importance of mass loss in the evolution of massive stars, it is imperative that we improve our understanding of the processes by which the outer layers of a star may be lost to its environment. The eclipsing nature of the Wolf-Rayet binary star V444 Cyg provides us with a unique opportunity to study the detailed characteristics of the radiatively driven mass loss in colliding-wind systems. Our multi-technique study combines X-ray spectroscopic and optical spectropolarimetric methods to describe the three-dimensional nature of the shock and wind structure in V444 Cyg. In support of this project, we have won new X-ray observations of V444 Cyg using the XMM-Newton telescope through the Guest Observer program in AO-11 (proposal ID #069281). We will combine these new data with six archival XMM-Newton observations and with optical spectropolarimetry obtained with the newly refurbished Half-Wave Spectropolarimeter (HPOL) at Ritter Observatory in Toledo, OH and archival data from both HPOL and the ESPaDOnS instrument at CFHT. Detailed X-ray light curve analysis and modeling of the X-ray spectra will constrain the location of the wind collision region and the mass-loss properties of the system. Polarized light curves in optical broad bands and emission lines combined with spectropolarimetric line profile analysis and radiative transfer simulations will trace the geometrical structure of various emission and scattering regions within the winds. Joint analysis of these two data sets will allow us to construct a self-consistent, physically realistic three-dimensional model of the complex winds in V444 Cyg and quantify its mass loss characteristics. We request support for data analysis and interpretation of our four new XMM-Newton observations. This will consist primarily of salaries for program personnel, who will analyze the new data in conjunction with previous X-ray results, carry out detailed radiation-hydrodynamic simulations to investigate the effect of radiative braking and other complex effects on the X-ray characteristics of V444 Cyg, and construct a new three-dimensional model of the system incorporating information from both X-ray and spectropolarimetric studies. We also request travel funding to enable collaboration among co-investigators at different institutions and to professional meetings to publicize results, as well as nominal support for the complementary ground-based spectropolarimetric observations (this amount comprises < 25% of the total, in accordance with NASA ADAP program limitations).

New developments in flash radiography

NASA Astrophysics Data System (ADS)

Mattsson, Arne

2007-01-01

The paper will review some of the latest developments in flash radiography. A series of multi anode tubes has been developed. These are tubes with several x-ray sources within the same vacuum enclosure. The x-ray sources are closely spaced, to come as close as possible to a single source. The x-ray sources are sequentially pulsed, at times that can be independently chosen. Tubes for voltages in the range 150 - 500 kV, with up to eight x-ray sources, will be described. Combining a multi anode tube with an intensified CCD camera, will make it possible to generate short "x-ray movies". A new flash x-ray control system has been developed. The system is operated from a PC or Laptop. All parameters of a multi channel flash x-ray system can be remotely set and monitored. The system will automatically store important operation parameters.

Dual energy scanning beam laminographic x-radiography

DOEpatents

Majewski, Stanislaw; Wojcik, Randolph F.

1998-01-01

A multiple x-ray energy level imaging system includes a scanning x-ray beam and two detector design having a first low x-ray energy sensitive detector and a second high x-ray energy sensitive detector. The low x-ray energy detector is placed next to or in front of the high x-ray energy detector. The low energy sensitive detector has small stopping power for x-rays. The lower energy x-rays are absorbed and converted into electrical signals while the majority of the higher energy x-rays pass through undetected. The high energy sensitive detector has a large stopping power for x-rays as well as it having a filter placed between it and the object to absorb the lower energy x-rays. In a second embodiment; a single energy sensitive detector is provided which provides an output signal proportional to the amount of energy in each individual x-ray it absorbed. It can then have an electronic threshold or thresholds set to select two or more energy ranges for the images. By having multiple detectors located at different positions, a dual energy laminography system is possible.

Dual energy scanning beam laminographic x-radiography

DOEpatents

Majewski, S.; Wojcik, R.F.

1998-04-21

A multiple x-ray energy level imaging system includes a scanning x-ray beam and two detector design having a first low x-ray energy sensitive detector and a second high x-ray energy sensitive detector. The low x-ray energy detector is placed next to or in front of the high x-ray energy detector. The low energy sensitive detector has small stopping power for x-rays. The lower energy x-rays are absorbed and converted into electrical signals while the majority of the higher energy x-rays pass through undetected. The high energy sensitive detector has a large stopping power for x-rays as well as it having a filter placed between it and the object to absorb the lower energy x-rays. In a second embodiment; a single energy sensitive detector is provided which provides an output signal proportional to the amount of energy in each individual x-ray it absorbed. It can then have an electronic threshold or thresholds set to select two or more energy ranges for the images. By having multiple detectors located at different positions, a dual energy laminography system is possible. 6 figs.

A long-term space astrophysics research program: An x-ray perspective of the components and structure of galaxies

NASA Technical Reports Server (NTRS)

Fabbiano, G.

1995-01-01

X-ray studies of galaxies by the Smithsonian Astrophysical Observatory (SAO) and MIT are described. Activities at SAO include ROSAT PSPC x-ray data reduction and analysis pipeline; x-ray sources in nearby Sc galaxies; optical, x-ray, and radio study of ongoing galactic merger; a radio, far infrared, optical, and x-ray study of the Sc galaxy NGC247; and a multiparametric analysis of the Einstein sample of early-type galaxies. Activities at MIT included continued analysis of observations with ROSAT and ASCA, and continued development of new approaches to spectral analysis with ASCA and AXAF. Also, a new method for characterizing structure in galactic clusters was developed and applied to ROSAT images of a large sample of clusters. An appendix contains preprints generated by the research.

1RXS J173021.5-055933: a cataclysmic variable with a fast-spinning magnetic white dwarf

NASA Astrophysics Data System (ADS)

de Martino, D.; Matt, G.; Mukai, K.; Bonnet-Bidaud, J.-M.; Falanga, M.; Gänsicke, B. T.; Haberl, F.; Marsh, T. R.; Mouchet, M.; Littlefair, S. P.; Dhillon, V.

2008-04-01

Aims:We present the first X-ray observations with the XMM-Newton and INTEGRAL satellites of the recently discovered cataclysmic variable 1RXS J173021.5-055933, together with simultaneous UV and coordinated optical photometry aiming at characterising its broad-band temporal and spectral properties and classifying this system as a magnetic one. Methods: We performed a timing analysis of the X-ray, UV, and optical light curves to identify and to study the energy dependence of the fast 128 s pulsation over a wide energy range. X-ray spectral analysis in the broad 0.2-100 keV X-ray range was performed to characterise the peculiar emission properties of this source. Results: We find that the X-ray light curve is dominated by the spin period of the accreting white dwarf in contrast to the far-UV range, which turns out to be unmodulated at a 3σ level. Near-UV and optical pulses are instead detected at twice the spin frequency. We identify the contributions from two accreting poles that imply a moderately inclined dipole field allowing, one pole to dominate at energies at least up to 10 keV, and a secondary that instead is negligible above 5 keV. X-ray spectral analysis reveals the presence of multiple emission components consisting of optically thin plasma with temperatures ranging from 0.17 keV to 60 keV and a hot blackbody at ~90 eV. The spectrum is also strongly affected by peculiar absorption components consisting of two high-density (~3 × 1021~cm-2 and 2 × 1023~cm-2) intervening columns, plus a warm absorber. The last is detected from an OVII absorption edge at 0.74 keV, which suggests that photoionization of pre-shock material is also occurring in this system. Conclusions: The observed properties indicate that the accretor in 1RXS J173021.5-055933 is a white dwarf with a likely weak magnetic field, thus confirming this cataclysmic variable as an intermediate polar (IP) with one of the most extreme spin-to-orbit period ratios. This system also joins the small group of IPs showing a soft X-ray reprocessed component, suggesting that this characteristics is not uncommon in these systems. Based on observations obtained with XMM-Newton and INTEGRAL, ESA science missions with instruments and contributions directly funded by ESA Member States and NASA.

MARS: a mouse atlas registration system based on a planar x-ray projector and an optical camera

NASA Astrophysics Data System (ADS)

Wang, Hongkai; Stout, David B.; Taschereau, Richard; Gu, Zheng; Vu, Nam T.; Prout, David L.; Chatziioannou, Arion F.

2012-10-01

This paper introduces a mouse atlas registration system (MARS), composed of a stationary top-view x-ray projector and a side-view optical camera, coupled to a mouse atlas registration algorithm. This system uses the x-ray and optical images to guide a fully automatic co-registration of a mouse atlas with each subject, in order to provide anatomical reference for small animal molecular imaging systems such as positron emission tomography (PET). To facilitate the registration, a statistical atlas that accounts for inter-subject anatomical variations was constructed based on 83 organ-labeled mouse micro-computed tomography (CT) images. The statistical shape model and conditional Gaussian model techniques were used to register the atlas with the x-ray image and optical photo. The accuracy of the atlas registration was evaluated by comparing the registered atlas with the organ-labeled micro-CT images of the test subjects. The results showed excellent registration accuracy of the whole-body region, and good accuracy for the brain, liver, heart, lungs and kidneys. In its implementation, the MARS was integrated with a preclinical PET scanner to deliver combined PET/MARS imaging, and to facilitate atlas-assisted analysis of the preclinical PET images.

MARS: a mouse atlas registration system based on a planar x-ray projector and an optical camera.

PubMed

Wang, Hongkai; Stout, David B; Taschereau, Richard; Gu, Zheng; Vu, Nam T; Prout, David L; Chatziioannou, Arion F

2012-10-07

This paper introduces a mouse atlas registration system (MARS), composed of a stationary top-view x-ray projector and a side-view optical camera, coupled to a mouse atlas registration algorithm. This system uses the x-ray and optical images to guide a fully automatic co-registration of a mouse atlas with each subject, in order to provide anatomical reference for small animal molecular imaging systems such as positron emission tomography (PET). To facilitate the registration, a statistical atlas that accounts for inter-subject anatomical variations was constructed based on 83 organ-labeled mouse micro-computed tomography (CT) images. The statistical shape model and conditional Gaussian model techniques were used to register the atlas with the x-ray image and optical photo. The accuracy of the atlas registration was evaluated by comparing the registered atlas with the organ-labeled micro-CT images of the test subjects. The results showed excellent registration accuracy of the whole-body region, and good accuracy for the brain, liver, heart, lungs and kidneys. In its implementation, the MARS was integrated with a preclinical PET scanner to deliver combined PET/MARS imaging, and to facilitate atlas-assisted analysis of the preclinical PET images.

Calibration of the Verification Engineering Test Article-I (VETA-I) for AXAF using the VETA-I X-ray Detection System

NASA Technical Reports Server (NTRS)

Kellogg, E.; Brissenden, R.; Flanagan, K.; Freeman, M.; Hughes, J.; Jones, M.; Ljungberg, M.; Mckinnon, P.; Podgorski, W.; Schwartz, D.

1992-01-01

Advanced X-ray Astrophysics Facility (AXAF) X-ray optics testing is conducted by VETA-I, which consists of six nested Wolter type I grazing-incidence mirrors; VETA's X-ray Detection System (VXDS) in turn measures the imaging properties of VETA-I, yielding FWHM and encircled energy of the X-ray image obtained, as well as its effective area. VXDS contains a high resolution microchannel plate imaging X-ray detector and a pinhole scanning system in front of proportional-counter detectors. VETA-I's X-ray optics departs from the AXAF flight configuration in that it uses a temporary holding fixture; its mirror elements are not cut to final length, and are not coated with the metal film used to maximize high-energy reflection.

Inter-satellites x-ray communication system

NASA Astrophysics Data System (ADS)

Mou, Huan; Li, Bao-quan

2017-02-01

An inter-satellite X-ray communication system is presented in this paper. X-ray has a strong penetrating power without almost attenuation for transmission in outer space when the energy of X-ray photons is more than 10KeV and the atmospheric pressure is lower than 10-1 Pa, so it is convincing of x-ray communication in inter-satellite communication and deep space exploration. Additionally, using X-ray photons as information carriers can be used in some communication applications that laser communication and radio frequency (RF) communication are not available, such as ionization blackout area communication. The inter-satellites X-ray communication system, including the grid modulated X-ray source, the high-sensitivity X-ray detector and the transmitting and receiving antenna, is described explicitly. As the X-ray transmitter, a vacuum-sealed miniature modulated X-ray source has been fabricated via the single-step brazing process in a vacuum furnace. Pulse modulation of X-rays, by means of controlling the voltage value of the grid electrode, is realized. Three focusing electrodes, meanwhile, are used to make the electron beam converge and finally 150μm focusing spot diameter is obtained. The X-ray detector based on silicon avalanche photodiodes (APDs) is chosen as the communication receiver on account of its high temporal resolution and non-vacuum operating environment. Furthermore, considering x-ray emission characteristic and communication distance of X-rays, the multilayer nested rotary parabolic optics is picked out as transmitting and receiving antenna. And as a new concept of the space communication, there will be more important scientific significance and application prospects, called "Next-Generation Communications".

X1908+075: An X-Ray Binary with a 4.4 Day Period

NASA Astrophysics Data System (ADS)

Wen, Linqing; Remillard, Ronald A.; Bradt, Hale V.

2000-04-01

X1908+075 is an optically unidentified and highly absorbed X-ray source that appeared in early surveys such as Uhuru, OSO 7, Ariel 5, HEAO-1, and the EXOSAT Galactic Plane Survey. These surveys measured a source intensity in the range 2-12 mcrab at 2-10 keV, and the position was localized to ~0.5d. We use the Rossi X-Ray Timing Explorer (RXTE) All-Sky Monitor (ASM) to confirm our expectation that a particular Einstein/IPC detection (1E 1908.4+0730) provides the correct position for X1908+075. The analysis of the coded mask shadows from the ASM for the position of 1E 1908.4+0730 yields a persistent intensity ~8 mcrab (1.5-12 keV) over a 3 yr interval beginning in 1996 February. Furthermore, we detect a period of 4.400+/-0.001 days with a false-alarm probability less than 10-7. The folded light curve is roughly sinusoidal, with an amplitude that is 26% of the mean flux. The X-ray period may be attributed to the scattering and absorption of X-rays through a stellar wind combined with the orbital motion in a binary system. We suggest that X1908+075 is an X-ray binary with a high-mass companion star.

The Nature of the Enigmatic 10-Minute Accreting Binary System ES CET

NASA Technical Reports Server (NTRS)

Steeghs, Daniel

2005-01-01

ES Cet is one of the most compact binary systems known with an orbital period of only 10.3 minutes. Our allocated observations with the XMM-Newton X-ray satellite were performed in January and July 2004, with the data being delivered to the PI in August 2004. Preliminary results were presented by the PI in September 2004 and January 2005. We have also secured supporting optical observations of ES Ceti using the Magellan telescopes (November 2004). The team is currently performing a thorough and final analysis of the X-ray, UV and optical data sets with the latest XMM pipeline software and our own analysis packages.

Quantitative Electron Probe Microanalysis: State of the Art

NASA Technical Reports Server (NTRS)

Carpernter, P. K.

2005-01-01

Quantitative electron-probe microanalysis (EPMA) has improved due to better instrument design and X-ray correction methods. Design improvement of the electron column and X-ray spectrometer has resulted in measurement precision that exceeds analytical accuracy. Wavelength-dispersive spectrometer (WDS) have layered-dispersive diffraction crystals with improved light-element sensitivity. Newer energy-dispersive spectrometers (EDS) have Si-drift detector elements, thin window designs, and digital processing electronics with X-ray throughput approaching that of WDS Systems. Using these systems, digital X-ray mapping coupled with spectrum imaging is a powerful compositional mapping tool. Improvements in analytical accuracy are due to better X-ray correction algorithms, mass absorption coefficient data sets,and analysis method for complex geometries. ZAF algorithms have ban superceded by Phi(pz) algorithms that better model the depth distribution of primary X-ray production. Complex thin film and particle geometries are treated using Phi(pz) algorithms, end results agree well with Monte Carlo simulations. For geological materials, X-ray absorption dominates the corretions end depends on the accuracy of mass absorption coefficient (MAC) data sets. However, few MACs have been experimentally measured, and the use of fitted coefficients continues due to general success of the analytical technique. A polynomial formulation of the Bence-Albec alpha-factor technique, calibrated using Phi(pz) algorithms, is used to critically evaluate accuracy issues and can be also be used for high 2% relative and is limited by measurement precision for ideal cases, but for many elements the analytical accuracy is unproven. The EPMA technique has improved to the point where it is frequently used instead of the petrogaphic microscope for reconnaissance work. Examples of stagnant research areas are: WDS detector design characterization of calibration standards, and the need for more complete treatment of the continuum X-ray fluorescence correction.

First Results from a Microfocus X-Ray System for Macromolecular Crystallography

NASA Technical Reports Server (NTRS)

Gubarev, Mikhail; Ciszak, Ewa; Ponomarev, Igor; Gibson, Walter; Joy, Marshall

1999-01-01

The design and performance of a 40 Watt laboratory crystallography system optimized for the structure determination of small protein crystals are described. This system combines a microfocus x-ray generator (40 microns FWHM spot size at a power level of 40 Watts) and a short focal length (F = 2.6 mm) polycapillary collimating optic, and produces a small diameter quasi-parallel x-ray beam. Measurements of x-ray flux, divergence and spectral purity of the resulting x-ray beam are presented. The x-ray flux in a 250 microns diameter aperture produced by the microfocus system is 14.7 times higher .than that from a 3.15 kW rotating anode generator equipped with graphite monochromator. Crystallography data taken with the microfocus system are presented, and indicate that the divergence and spectral purity of the x-ray are sufficient to refine the diffraction data using a standard crystallographic software. Significant additional improvements in flux and beam divergence are possible, and plans for achieving these coals are discussed.

Apparatus and method to enhance X-ray production in laser produced plasmas

DOEpatents

Augustoni, Arnold L.; Gerardo, James B.; Raymond, Thomas D.

1992-01-01

Method and apparatus for generating x-rays for use in, for instance, x-ray photolithography. The method of generating x-rays includes the steps of providing a target and irradiating the target with a laser system which produces a train of sub-pulses to generate an x-ray producing plasma. The sub-pulses are of both high intensity and short duration. The apparatus for generating x-rays from a plasma includes a vacuum chamber, a target supported within the chamber and a laser system, including a short storage time laser.

HST spectrum and timing of the ultracompact X-ray binary candidate 47 Tuc X9

NASA Astrophysics Data System (ADS)

Tudor, V.; Miller-Jones, J. C. A.; Knigge, C.; Maccarone, T. J.; Tauris, T. M.; Bahramian, A.; Chomiuk, L.; Heinke, C. O.; Sivakoff, G. R.; Strader, J.; Plotkin, R. M.; Soria, R.; Albrow, M. D.; Anderson, G. E.; van den Berg, M.; Bernardini, F.; Bogdanov, S.; Britt, C. T.; Russell, D. M.; Zurek, D. R.

2018-05-01

To confirm the nature of the donor star in the ultracompact X-ray binary candidate 47 Tuc X9, we obtained optical spectra (3000-10 000 Å) with the Hubble Space Telescope / Space Telescope Imaging Spectrograph. We find no strong emission or absorption features in the spectrum of X9. In particular, we place 3σ upper limits on the H α and He II λ4686 emission line equivalent widths - EWH α ≲ 14 Å and -EW_{He {II}} ≲ 9 Å, respectively. This is much lower than seen for typical X-ray binaries at a similar X-ray luminosity (which, for L_2-10 keV ≈ 10^{33}-10^{34} erg s-1 is typically - EWH α ˜ 50 Å). This supports our previous suggestion, by Bahramian et al., of an H-poor donor in X9. We perform timing analysis on archival far-ultraviolet, V- and I-band data to search for periodicities. In the optical bands, we recover the 7-d superorbital period initially discovered in X-rays, but we do not recover the orbital period. In the far-ultraviolet, we find evidence for a 27.2 min period (shorter than the 28.2 min period seen in X-rays). We find that either a neutron star or black hole could explain the observed properties of X9. We also perform binary evolution calculations, showing that the formation of an initial black hole/ He-star binary early in the life of a globular cluster could evolve into a present-day system such as X9 (should the compact object in this system indeed be a black hole) via mass-transfer driven by gravitational wave radiation.

Characterization and application of automated in-vacuum PIXE/EBS system for direct analysis of chloride and sulfate ions attack in cementitious materials

NASA Astrophysics Data System (ADS)

Rihawy, M. S.; Alwazzeh, M.; Abbas, K.

2018-01-01

Ion beam analysis (IBA) techniques (Particle Induced X-ray Emission, PIXE and Elastic Backscattering Spectrometry, EBS), were applied to investigate chloride and sulfate ions diffusion into laboratory prepared mortar samples. Development and characterization of an automated in-vacuum macro PIXE/EBS system is thoroughly discussed. Depth profile information of both chloride and sulfate ions in laboratory prepared mortar samples, after immersion in sea water for nine months, was rapidly and easily obtained at fairly low cost and with standardless analysis, demonstrating the value of the application of IBA to elemental depth profiling in cementitious materials. Chloride and sulfate depth profiles were obtained for two sets of mortar samples, one prepared with different water/cement (W/C) ratios and the other with different sand/cement (S/C) ratios. Results showed higher diffusion rates of both chloride and sulfate ions when both ratios are increased. Additionally, the W/C ratio has a stronger influence in both sulfate and chloride penetration than the S/C ratio, and chloride ions penetrate faster than sulfates. Advantages and limitations of applying IBA techniques in this investigation are discussed. The comparison between PIXE and other X-ray based analytical techniques, namely X-ray fluorescence (XRF) and energy and wavelength dispersive X-rays (EDX/WDX), as well as other traditional wet chemical methods is reviewed, and industrial applications are discussed.

The Einstein Observatory Extended Medium-Sensitivity Survey. I - X-ray data and analysis

NASA Technical Reports Server (NTRS)

Gioia, I. M.; Maccacaro, T.; Schild, R. E.; Wolter, A.; Stocke, J. T.

1990-01-01

This paper presents the results of the analysis of the X-ray data and the optical identification for the Einstein Observatory Extended Medium-Sensitivity Survey (EMSS). The survey consists of 835 serendipitous sources detected at or above 4 times the rms level in 1435 imaging proportional counter fields with centers located away from the Galactic plane. Their limiting sensitivities are about (5-300) x 10 to the -14th ergs/sq cm sec in the 0.3-3.5-keV energy band. A total area of 778 square deg of the high-Galactic-latitude sky has been covered. The data have been analyzed using the REV1 processing system, which takes into account the nonuniformities of the detector. The resulting EMSS catalog of X-ray sources is a flux-limited and homogeneous sample of astronomical objects that can be used for statistical studies.

XRF Experiment for Elementary Surface Analysis

NASA Astrophysics Data System (ADS)

Köhler, E.; Dreißigacker, A.; Fabel, O.; van Gasselt, S.; Meyer, M.

2014-04-01

The proposed X-Ray Fluorescence Instrument Package (XRF-X and XRF-E) is being designed to quantitatively measure the composition and map the distribution of rock-surface materials in order to support the target area selection process for exploration, sampling, and mining. While energydispersive X-Ray fluorescence (EDX) makes use of Solar X-Rays for excitation to probe materials over arbitrary distances (by XRF-X), electron-beam excitation can be used for proximity measurements (by XRF-E) over short-distance of up to about 10 - 20m. This design is targeted at observing and analyzing surface compositions from orbital platforms and it is in particular applicable to all atmosphereless solidsurface bodies. While the instrument design for observing objects in the outer solar system is challenging due to low count rates, the Moon and objects of the asteroid belt usually receive solar X-ray radiation that allows to integrate a statistically reliable data basis. Asteroids are attractive targets and have been visited using X-ray fluorescence instruments by orbiting spacecraft in the past (Itokawa, Eros). They are wellaccessible objects for determining elemental compositions and assessing potential mineral resources.

Impact of intense x-ray pulses on a NaI(Tl)-based gamma camera

NASA Astrophysics Data System (ADS)

Koppert, W. J. C.; van der Velden, S.; Steenbergen, J. H. L.; de Jong, H. W. A. M.

2018-03-01

In SPECT/CT systems x-ray and γ-ray imaging is performed sequentially. Simultaneous acquisition may have advantages, for instance in interventional settings. However, this may expose a gamma camera to relatively high x-ray doses and deteriorate its functioning. We studied the NaI(Tl) response to x-ray pulses with a photodiode, PMT and gamma camera, respectively. First, we exposed a NaI(Tl)-photodiode assembly to x-ray pulses to investigate potential crystal afterglow. Next, we exposed a NaI(Tl)-PMT assembly to 10 ms LED pulses (mimicking x-ray pulses) and measured the response to flashing LED probe-pulses (mimicking γ-pulses). We then exposed the assembly to x-ray pulses, with detector entrance doses of up to 9 nGy/pulse, and analysed the response for γ-pulse variations. Finally, we studied the response of a Siemens Diacam gamma camera to γ-rays while exposed to x-ray pulses. X-ray exposure of the crystal, read out with a photodiode, revealed 15% afterglow fraction after 3 ms. The NaI(Tl)-PMT assembly showed disturbances up to 10 ms after 10 ms LED exposure. After x-ray exposure however, responses showed elevated baselines, with 60 ms decay-time. Both for x-ray and LED exposure and after baseline subtraction, probe-pulse analysis revealed disturbed pulse height measurements shortly after exposure. X-ray exposure of the Diacam corroborated the elementary experiments. Up to 50 ms after an x-ray pulse, no events are registered, followed by apparent energy elevations up to 100 ms after exposure. Limiting the dose to 0.02 nGy/pulse prevents detrimental effects. Conventional gamma cameras exhibit substantial dead-time and mis-registration of photon energies up to 100 ms after intense x-ray pulses. This is due PMT limitations and due to afterglow in the crystal. Using PMTs with modified circuitry, we show that deteriorative afterglow effects can be reduced without noticeable effects on the PMT performance, up to x-ray pulse doses of 1 nGy.

Large area CMOS active pixel sensor x-ray imager for digital breast tomosynthesis: Analysis, modeling, and characterization

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhao, Chumin; Kanicki, Jerzy, E-mail: kanicki@eecs.umich.edu; Konstantinidis, Anastasios C.

Purpose: Large area x-ray imagers based on complementary metal-oxide-semiconductor (CMOS) active pixel sensor (APS) technology have been proposed for various medical imaging applications including digital breast tomosynthesis (DBT). The low electronic noise (50–300 e{sup −}) of CMOS APS x-ray imagers provides a possible route to shrink the pixel pitch to smaller than 75 μm for microcalcification detection and possible reduction of the DBT mean glandular dose (MGD). Methods: In this study, imaging performance of a large area (29 × 23 cm{sup 2}) CMOS APS x-ray imager [Dexela 2923 MAM (PerkinElmer, London)] with a pixel pitch of 75 μm was characterizedmore » and modeled. The authors developed a cascaded system model for CMOS APS x-ray imagers using both a broadband x-ray radiation and monochromatic synchrotron radiation. The experimental data including modulation transfer function, noise power spectrum, and detective quantum efficiency (DQE) were theoretically described using the proposed cascaded system model with satisfactory consistency to experimental results. Both high full well and low full well (LFW) modes of the Dexela 2923 MAM CMOS APS x-ray imager were characterized and modeled. The cascaded system analysis results were further used to extract the contrast-to-noise ratio (CNR) for microcalcifications with sizes of 165–400 μm at various MGDs. The impact of electronic noise on CNR was also evaluated. Results: The LFW mode shows better DQE at low air kerma (K{sub a} < 10 μGy) and should be used for DBT. At current DBT applications, air kerma (K{sub a} ∼ 10 μGy, broadband radiation of 28 kVp), DQE of more than 0.7 and ∼0.3 was achieved using the LFW mode at spatial frequency of 0.5 line pairs per millimeter (lp/mm) and Nyquist frequency ∼6.7 lp/mm, respectively. It is shown that microcalcifications of 165–400 μm in size can be resolved using a MGD range of 0.3–1 mGy, respectively. In comparison to a General Electric GEN2 prototype DBT system (at MGD of 2.5 mGy), an increased CNR (by ∼10) for microcalcifications was observed using the Dexela 2923 MAM CMOS APS x-ray imager at a lower MGD (2.0 mGy). Conclusions: The Dexela 2923 MAM CMOS APS x-ray imager is capable to achieve a high imaging performance at spatial frequencies up to 6.7 lp/mm. Microcalcifications of 165 μm are distinguishable based on reported data and their modeling results due to the small pixel pitch of 75 μm. At the same time, potential dose reduction is expected using the studied CMOS APS x-ray imager.« less

X-Ray and near-infrared imaging: similarities, differences and combinations

NASA Astrophysics Data System (ADS)

Pogue, Brian W.

2010-02-01

The integration of x-ray imaging with optical imaging is becoming routine at the pre-clinical level, as both projection and tomography systems are now commercially integrated as packaged systems. Yet, the differences between their capabilities are wide, and there is still perhaps a lack of appreciation about how difference pre-clinical x-ray systems are from clinical x-ray systems. In this survey, the key advantages of each approach, x-ray and optical, are described, and the potential synergies and deficiencies are discussed. In simple terms, the major benefit of optical imaging is in the spectroscopic capabilities, which allow the potential for imaging fluorescent agents in vivo, and the future potential for imaging multiple species at a time with spectral discrimination or spectral fitting of the data. In comparison, multienergy x-ray systems are being realized in clinical use, or automated discrimination of soft versus hard tissues, and the combination of optical imaging with this type of dual-energy x-ray imaging will significantly enhance the capabilities of the hybrid systems. Unfortunately, the power of dual energy imaging is not as possible at the pre-clinical stage, because of the limitations of contrast-resolution and x-ray dose. This is discussed and future human systems outlined.

The Origin of the UCSD X-ray Astronomy Program - A Personal Perspective

NASA Astrophysics Data System (ADS)

Peterson, Laurence E.

2013-01-01

I was a graduate student in the late 1950’s at the University of Minnesota in the Cosmic Ray Group under Prof. John R. Winckler. He had a project monitoring Cosmic ray time variations from an extensive series of balloon flights using simple detectors during the International Geophysical Year 1957-58. During the 20 March 1958 flight, a short 18 sec. burst of high energy radiation was observed simultaneously with a class II Solar flare. From the ratio of the Geiger counter rate to the energy loss in the ionization chamber, it was determined this radiation was likely hard X-rays or low-energy gamma rays and not energetic particles. Further analysis using information from other concurrent observations indicated the X-rays were likely due to Bremsstrahlung from energetic electrons accelerated in the solar flare magnetic field; these same electrons produced radio emissions. This first detection of extra-terrestrial X- or gamma rays showed the importance of non-thermal processes in Astrophysical phenomena. Winckler and I were interested by the possibility of non-solar hard X-rays. While completing my thesis on a Cosmic ray topic, I initiated a balloon program to develop more sensitive collimated low-background scintillation counters. This led to a proposal to the newly formed NASA to place an exploratory instrument on the 1st Orbiting Solar Observatory launched 7 March 1962. In August that year, I assumed a tenure-track position at UCSD; the data analysis of OSO-1 and the balloon program were transferred to UCSD to initiate the X-ray Astronomy program. The discovery of Cosmic X-ray sources in the 1-10 Kev range on a rocket flight in June 1962 by Giacconi and colleagues gave impetus to the UCSD activities. It seemed evident cosmic X-ray sources could be detected above 20 Kev using high-flying balloons. Early results included measurements of the 50 million K gas in SCO X-1, and the X-ray continuum from the Crab Nebula characterized by a power-law dN/dE ~ E-2.2. The instrument developments resulted in ever more sophisticated and sensitive counter systems. Follow-on instruments were flown on OSO-III and OSO-VII by the early 70’s, the HEAO-1 in 1976, and the RXTE in 1995. These provided many new results on Cosmic X-rays.

The High Energy Astronomy Observatory X-ray Telescope

NASA Technical Reports Server (NTRS)

Miller, R.; Austin, G.; Koch, D.; Jagoda, N.; Kirchner, T.; Dias, R.

1978-01-01

The High Energy Astronomy Observatory-Mission B (HEAO-B) is a satellite observatory for the purpose of performing a detailed X-ray survey of the celestial sphere. Measurements will be made of stellar radiation in the range 0.2 through 20 keV. The primary viewing requirement is to provide final aspect solution and internal alignment information to correlate an observed X-ray image with the celestial sphere to within one-and-one-half arc seconds. The Observatory consists of the HEAO Spacecraft together with the X-ray Telescope. The Spacecraft provides the required attitude control and determination system, data telemetry system, space solar power system, and interface with the launch vehicle. The X-ray Telescope includes a high resolution mirror assembly, optical bench metering structure, X-ray detectors, detector positioning system, detector electronics and aspect sensing system.

XIMPOL: a new x-ray polarimetry observation-simulation and analysis framework

NASA Astrophysics Data System (ADS)

Omodei, Nicola; Baldini, Luca; Pesce-Rollins, Melissa; di Lalla, Niccolò

2017-08-01

We present a new simulation framework, XIMPOL, based on the python programming language and the Scipy stack, specifically developed for X-ray polarimetric applications. XIMPOL is not tied to any specific mission or instrument design and is meant to produce fast and yet realistic observation-simulations, given as basic inputs: (i) an arbitrary source model including morphological, temporal, spectral and polarimetric information, and (ii) the response functions of the detector under study, i.e., the effective area, the energy dispersion, the point-spread function and the modulation factor. The format of the response files is OGIP compliant, and the framework has the capability of producing output files that can be directly fed into the standard visualization and analysis tools used by the X-ray community, including XSPEC which make it a useful tool not only for simulating physical systems, but also to develop and test end-to-end analysis chains.

Simultaneous Neutron and X-ray Tomography for Quantitative analysis of Geological Samples

NASA Astrophysics Data System (ADS)

LaManna, J.; Hussey, D. S.; Baltic, E.; Jacobson, D. L.

2016-12-01

Multiphase flow is a critical area of research for shale gas, oil recovery, underground CO2 sequestration, geothermal power, and aquifer management. It is critical to understand the porous structure of the geological formations in addition to the fluid/pore and fluid/fluid interactions. Difficulties for analyzing flow characteristics of rock cores are in obtaining 3D distribution information on the fluid flow and maintaining the cores in a state for other analysis methods. Two powerful non-destructive methods for obtaining 3D structural and compositional information are X-ray and neutron tomography. X-ray tomography produces information on density and structure while neutrons excel at acquiring the liquid phase and produces compositional information. These two methods can offer strong complementary information but are typically conducted at separate times and often at different facilities. This poses issues for obtaining dynamic and stochastic information as the sample will change between analysis modes. To address this, NIST has developed a system that allows for multimodal, simultaneous tomography using thermal neutrons and X-rays by placing a 90 keVp micro-focus X-ray tube 90° to the neutron beam. High pressure core holders that simulate underground conditions have been developed to facilitate simultaneous tomography. These cells allow for the control of confining pressure, axial load, temperature, and fluid flow through the core. This talk will give an overview the simultaneous neutron and x-ray tomography capabilities at NIST, the benefits of multimodal imaging, environmental equipment for geology studies, and several case studies that have been conducted at NIST.

INTEGRAL and XMM-Newton observations of the puzzling binary system LSI +61 303

NASA Astrophysics Data System (ADS)

Chernyakova, Masha; Neronov, A.; Walter, R.

LSI +61° 303 is one of the few X-ray binaries with Be star companion from which both radio and high-energy gamma-ray emission have been observed. We present XMM-Newton and INTE- GRAL observations which reveal variability of the X-ray spectral index of the system. The X-ray spectrum is hard (photon index Γ ≃ 1.5) during the orbital phases of both high and low X-ray flux. However, the spectrum softens at the moment of transition from high to low X-ray state. The spectrum of the system in the hard X-ray band does not reveal the presence of a cut-off (or, at least a spectral break) at 10-60 keV energies, expected if the compact object is an accreting neu- tron star. The observed spectrum and spectral variability can be explained if the compact object in the system is a rotation powered pulsar. In this case the recently found X-ray spectral variability of the system on the several kiloseconds time scale can be explained by the clumpy structure of the Be star disk.

Search for Hard X-Ray Emission from the Soft X-Ray Transient Aquila X-1

NASA Astrophysics Data System (ADS)

Harmon, B. A.; Zhang, S. N.; Paciesas, W. S.; Tavani, M.; Kaaret, P.; Ford, E.

1994-12-01

We are investigating the possibility of hard x-ray emission from the recurrent soft x-ray transient and x-ray burst source Aquila X-1 (Aql X-1). Outbursts of this source are relatively frequent with a spacing of ~ 4-10 months (Kitamoto, S. et al. 1993, ApJ, 403, 315). The recent detections of hard tails (\\(>\\)20 keV) in low luminosity x-ray bursters (Barret, D. & Vedrenne, G. 1994, ApJ Supp. S. 92, 505) suggest that neutron star transient systems such as Aql X-1 can produce hard x-ray emission which is detectable by BATSE. We are correlating reported optical and soft x-ray observations since 1991 of Aql X-1 with BATSE observations in order to search for hard x-ray emission episodes, and to study their temporal and spectral evolution. We will present preliminary results of this search in the 20-1000 keV band using the Earth occultation technique applied to the large area detectors. If this work is successful, we hope to alert the astronomical community for the next Aql X-1 outburst expected in 1995. Simultaneous x-ray/hard x-ray and optical observations of Aql X-1 during outburst would be of great importance for the modeling of soft x-ray transients and related systems.

Dislocation structure in textured zirconium tensile-deformed along rolling and transverse directions determined by X-ray diffraction line profile analysis

NASA Astrophysics Data System (ADS)

Fan, Zhijian; Jóni, Bertalan; Xie, Lei; Ribárik, Gábor; Ungár, Tamás

2018-04-01

Specimens of cold-rolled zirconium were tensile-deformed along the rolling (RD) and the transverse (TD) directions. The stress-strain curves revealed a strong texture dependence. High resolution X-ray line profile analysis was used to determine the prevailing active slip-systems in the specimens with different textures. The reflections in the X-ray diffraction patterns were separated into two groups. One group corresponds to the major and the other group to the random texture component, respectively. The dislocation densities, the subgrain size and the prevailing active slip-systems were evaluated by using the convolutional multiple whole profile (CMWP) procedure. These microstructure parameters were evaluated separately in the two groups of reflections corresponding to the two different texture components. Significant differences were found in both, the evolution of dislocation densities and the development of the fractions of and type slip systems in the RD and TD specimens during tensile deformation. The differences between the RD and TD stress-strain curves are discussed in terms of the differences of the microstructure evolution.

X-rays from HD 100546- A Young Herbig Star Orbited by Giant Protoplanets

NASA Astrophysics Data System (ADS)

Skinner, Stephen

A protoplanetary system consisting of at least two giant planets has beendetected orbiting the young nearby Herbig Be star HD 100546. The inner protoplanet orbits inside a gap within 14 AU of the star and is exposed to strong stellar UV and X-ray radiation. The detection of very warm disk gas provides evidence that stellar heating is affecting physical conditions in the planet-forming environment. We obtained a deep 74 ksec X-ray observation of HD 100546 in 2015 with XMM-Newton yielding an excellent-quality spectrum. We propose here to analyze the XMM-Newton data to determine the X-ray ionization and heating rates in the disk. X-ray ionization and heating affect the thermal and chemical structure of the disk and are key parameters for constructing realistic planet formation models. We are requesting ADAP funding to support the analysis and publication of this valuable XMM-Newton data set, which is now in the public archive.

Minimally invasive positioning robot system of femoral neck hollow screw implants based on x-ray error correction

NASA Astrophysics Data System (ADS)

Zou, Yunpeng; Xu, Ying; Hu, Lei; Guo, Na; Wang, Lifeng

2017-01-01

Aiming the high failure rate, the high radiation quantity and the poor positioning accuracy of femoral neck traditional surgery, this article develops a set of new positioning robot system of femoral neck hollow screw implants based on X-rays error correction, which bases on the study of x-rays perspective principle and the Motion Principle of 6 DOF(degree of freedom) series robot UR(Universal Robots). Compared with Computer Assisted Navigation System, this system owns better positioning accuracy and more simple operation. In addition, without extra Equipment of Visual Tracking, this system can reduce a lot of cost. During the surgery, Doctor can plan the operation path and the pose of mark needle according to the positive and lateral X-rays images of patients. Then they can calculate the pixel ratio according to the ratio of the actual length of mark line and the length on image. After that, they can calculate the amount of exercise of UR Robot according to the relative position between operation path and guide pin and the fixed relationship between guide pin and UR robot. Then, they can control UR to drive the positioning guide pin to the operation path. At this point, check the positioning guide pin and the planning path is coincident, if not, repeat the previous steps, until the positioning guide pin and the planning path coincide which will eventually complete the positioning operation. Moreover, to verify the positioning accuracy, this paper make an errors analysis aiming to thirty cases of the experimental model of bone. The result shows that the motion accuracy of the UR Robot is 0.15mm and the Integral error precision is within 0.8mm. To verify the clinical feasibility of this system, this article analysis on three cases of the clinical experiment. In the whole process of positioning, the X-rays irradiation time is 2-3s, the number of perspective is 3-5 and the whole positioning time is 7-10min. The result shows that this system can complete accurately femoral neck positioning surgery. Meanwhile, it can greatly reduce the X-rays radiation of medical staff and patients. To summarize, it has a significant value in clinical application.

The massive binary CPD - 41° 7742. II. Optical light curve and X-ray observations

NASA Astrophysics Data System (ADS)

Sana, H.; Antokhina, E.; Royer, P.; Manfroid, J.; Gosset, E.; Rauw, G.; Vreux, J.-M.

2005-10-01

In the first paper of this series, we presented a detailed high-resolution spectroscopic study of CPD - 41° 7742, deriving for the first time an orbital solution for both components of the system. In this second paper, we focus on the analysis of the optical light curve and on recent XMM-Newton X-ray observations. In the optical, the system presents two eclipses, yielding an inclination i˜77°. Combining the constraints from the photometry with the results of our previous work, we derive the absolute parameters of the system. We confirm that the two components of CPD - 41° 7742 are main sequence stars (O9 V + B1-1.5 V) with masses (M_1˜18 M⊙ and M_2˜10 M⊙) and respective radii (R_1˜7.5 R⊙ and R_2˜5.4 R⊙) close to the typical values expected for such stars. We also report an unprecedented set of X-ray observations that almost uniformly cover the 2.44-day orbital cycle. The X-ray emission from CPD - 41° 7742 is well described by a two-temperature thermal plasma model with energies close to 0.6 and 1.0 keV, thus slightly harder than typical early-type emission. The X-ray light curve shows clear signs of variability. The emission level is higher when the primary is in front of the secondary. During the high emission state, the system shows a drop of its X-ray emission that almost exactly matches the optical eclipse. We interpret the main features of the X-ray light curve as the signature of a wind-photosphere interaction, in which the overwhelming primary O9 star wind crashes into the secondary surface. Alternatively the light curve could result from a wind-wind interaction zone located near the secondary star surface. As a support to our interpretation, we provide a phenomenological geometric model that qualitatively reproduces the observed modulations of the X-ray emission.

Testing the Impulsiveness of Solar Flare Heating through Analysis of Dynamic Atmospheric Response

NASA Astrophysics Data System (ADS)

Newton, E. K.; Emslie, A. G.; Mariska, J. T.

1996-03-01

One crucial test of a solar flare energy transport model is its ability to reproduce the characteristics of the atmospheric motions inferred from soft X-ray line spectra. Using a recently developed diagnostic, the velocity differential emission measure (VDEM), we can obtain from observations a physical measure of the amount of soft X-ray mitting plasma flowing at each velocity, v, and hence the total momentum of the upflowing plasma, without approximation or parametric fitting. We have correlated solar hard X-ray emission profiles by the Yohkoh Hard X-ray telescope with the mass and momentum histories inferred from soft X-ray line profiles observed by the Yohkoh Bragg crystal spectrometers. For suitably impulsive hard X-ray emission, an analysis of the hydrodynamic equations predicts a proportionality between the hard X-ray intensity and the second time derivative of the soft X-ray mitting plasma's momentum. This relationship is borne out by an analysis of 18 disk-center impulsive flares of varying durations, thereby lending support to the hypothesis that a prompt energy deposition mechanism, such as an energetic electron flux, is indeed responsible for the soft X-ray response observed in the rise phase of sufficiently impulsive solar flares.

HIGH-ENERGY OBSERVATIONS OF PSR B1259–63/LS 2883 THROUGH THE 2014 PERIASTRON PASSAGE: CONNECTING X-RAYS TO THE GeV FLARE

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tam, P. H. T.; Li, K. L.; Kong, A. K. H.

2015-01-01

The binary system PSR B1259–63/LS 2883 is well sampled in radio, X-rays, and TeV γ-rays, and shows orbital-phase-dependent variability in these frequencies. The first detection of GeV γ-rays from the system was made around the 2010 periastron passage. In this Letter, we present an analysis of X-ray and γ-ray data obtained by the Swift/XRT, NuSTAR/FPM, and Fermi/LAT, through the recent periastron passage which occurred on 2014 May 4. While PSR B1259–63/LS 2883 was not detected by the Large Area Telescope before and during this passage, we show that the GeV flares occurred at a similar orbital phase as in earlymore » 2011, thus establishing the repetitive nature of the post-periastron GeV flares. Multiple flares each lasting for a few days have been observed and short-term variability is seen as well. We also found X-ray flux variation contemporaneous with the GeV flare for the first time. Strong evidence of the keV-to-GeV connection came from the broadband high-energy spectra, which we interpret as synchrotron radiation from the shocked pulsar wind.« less

Rapid simulation of X-ray transmission imaging for baggage inspection via GPU-based ray-tracing

NASA Astrophysics Data System (ADS)

Gong, Qian; Stoian, Razvan-Ionut; Coccarelli, David S.; Greenberg, Joel A.; Vera, Esteban; Gehm, Michael E.

2018-01-01

We present a pipeline that rapidly simulates X-ray transmission imaging for arbitrary system architectures using GPU-based ray-tracing techniques. The purpose of the pipeline is to enable statistical analysis of threat detection in the context of airline baggage inspection. As a faster alternative to Monte Carlo methods, we adopt a deterministic approach for simulating photoelectric absorption-based imaging. The highly-optimized NVIDIA OptiX API is used to implement ray-tracing, greatly speeding code execution. In addition, we implement the first hierarchical representation structure to determine the interaction path length of rays traversing heterogeneous media described by layered polygons. The accuracy of the pipeline has been validated by comparing simulated data with experimental data collected using a heterogenous phantom and a laboratory X-ray imaging system. On a single computer, our approach allows us to generate over 400 2D transmission projections (125 × 125 pixels per frame) per hour for a bag packed with hundreds of everyday objects. By implementing our approach on cloud-based GPU computing platforms, we find that the same 2D projections of approximately 3.9 million bags can be obtained in a single day using 400 GPU instances, at a cost of only 0.001 per bag.

Repetitive flash x-ray generator operated at low-dose rates for a medical x-ray television system

NASA Astrophysics Data System (ADS)

Sato, Eiichi; Isobe, Hiroshi; Takahashi, Kei; Tamakawa, Yoshiharu; Yanagisawa, Toru

1991-04-01

The fundamental studies for the repetitive flash x-ray generator operated at lowdose rates for a medical x-ray television system are described. This x-ray generator consisted of the following components: a high-voltage power supply, an energy storage condenser of lOOnF, a coaxial cable condenser with a capacity of l000pF, a repetitive impulse switching system, a turbo molecular pump, and an x-ray tube having a cold cathode. The condenser was charged from 40 to 70kV by a power supply, and the electric charges stored in the condenser were discharged repetitively by using a trigger electrode operated by an impulse switching system. The x-ray tube was of the triode-type which was connected to the turbo molecular pump and had a large discharge impedance in order to prevent the damped oscillations of the tube current and voltage. The maximum tube voltage was equivalent to the initial charged voltage, and the peak current was less than 70A. The durations were about 2ps, and the x-ray intensities were less than 1. OpC/kg at 0. 5m per pulse. The repetition frequency was less than 50Hz, and the effective focal spot size was equivalent to the anode diameter of 3. 0mm. For the x-ray television system used in conjunction with this repetitive pulsed x-ray generator, since the electromagnetic noise primarily caused by the high tube current was decreased, noise-free stroboscopic radiography performed by the television system could be realized.

Closed bore XMR (CBXMR) systems for aortic valve replacement: Investigation of rotating-anode x-ray tube heat loadability

PubMed Central

Bracken, John A.; Lillaney, Prasheel V.; Fahrig, Rebecca; Rowlands, J. A.

2008-01-01

In order to improve the safety and efficacy of percutaneous aortic valve replacement procedures, a closed bore hybrid x-ray∕MRI (CBXMR) system is proposed in which an x-ray C-arm will be positioned with its isocenter ≈1 m from the entrance of a clinical MRI scanner. This system will harness the complementary strengths of both modalities to improve clinical outcome. A key component of the CBXMR system will be a rotating anode x-ray tube to produce high-quality x-ray images. There are challenges in positioning an x-ray tube in the magnetic fringe field of the MRI magnet. Here, the effects of an external magnetic field on x-ray tube induction motors of radiography x-ray tubes and the corresponding reduction of x-ray tube heat loadability are investigated. Anode rotation frequency fanode was unaffected when the external magnetic field Bb was parallel to the axis of rotation of the anode but decreased when Bb was perpendicular to the axis of rotation. The experimental fanode values agreed with predicted values to within ±3% over a Bb range of 0–30 mT. The MRI fringe field at the proposed location of the x-ray tube mounted on the C-arm (≈4 mT) reduced fanode by only 1%, so x-ray tube heat loadability will not be compromised when using CBXMR systems for percutaneous aortic valve replacement procedures. Eddy current heating power in the rotor due to an MRI fringe field was found to be two orders of magnitude weaker than the heating power produced on the anode due to a fluoroscopic exposure, so eddy current heating had no effect on x-ray tube heat loadability. PMID:18841857

Method for spatially modulating X-ray pulses using MEMS-based X-ray optics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lopez, Daniel; Shenoy, Gopal; Wang, Jin

A method and apparatus are provided for spatially modulating X-rays or X-ray pulses using microelectromechanical systems (MEMS) based X-ray optics. A torsionally-oscillating MEMS micromirror and a method of leveraging the grazing-angle reflection property are provided to modulate X-ray pulses with a high-degree of controllability.

Comprehensive assessment of patient image quality and radiation dose in latest generation cardiac x-ray equipment for percutaneous coronary interventions

PubMed Central

Gislason-Lee, Amber J.; Keeble, Claire; Egleston, Daniel; Bexon, Josephine; Kengyelics, Stephen M.; Davies, Andrew G.

2017-01-01

Abstract. This study aimed to determine whether a reduction in radiation dose was found for percutaneous coronary interventional (PCI) patients using a cardiac interventional x-ray system with state-of-the-art image enhancement and x-ray optimization, compared to the current generation x-ray system, and to determine the corresponding impact on clinical image quality. Patient procedure dose area product (DAP) and fluoroscopy duration of 131 PCI patient cases from each x-ray system were compared using a Wilcoxon test on median values. Significant reductions in patient dose (p≪0.001) were found for the new system with no significant change in fluoroscopy duration (p=0.2); procedure DAP reduced by 64%, fluoroscopy DAP by 51%, and “cine” acquisition DAP by 76%. The image quality of 15 patient angiograms from each x-ray system (30 total) was scored by 75 clinical professionals on a continuous scale for the ability to determine the presence and severity of stenotic lesions; image quality scores were analyzed using a two-sample t-test. Image quality was reduced by 9% (p≪0.01) for the new x-ray system. This demonstrates a substantial reduction in patient dose, from acquisition more than fluoroscopy imaging, with slightly reduced image quality, for the new x-ray system compared to the current generation system. PMID:28491907

National Synchrotron Light Source annual report 1991

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hulbert, S.L.; Lazarz, N.M.

1992-04-01

This report discusses the following research conducted at NSLS: atomic and molecular science; energy dispersive diffraction; lithography, microscopy and tomography; nuclear physics; UV photoemission and surface science; x-ray absorption spectroscopy; x-ray scattering and crystallography; x-ray topography; workshop on surface structure; workshop on electronic and chemical phenomena at surfaces; workshop on imaging; UV FEL machine reviews; VUV machine operations; VUV beamline operations; VUV storage ring parameters; x-ray machine operations; x-ray beamline operations; x-ray storage ring parameters; superconducting x-ray lithography source; SXLS storage ring parameters; the accelerator test facility; proposed UV-FEL user facility at the NSLS; global orbit feedback systems; and NSLSmore » computer system.« less

Solid state structural investigations of the bis(chalcone) compound with single crystal X-ray crystallography, DFT, gamma-ray spectroscopy and chemical spectroscopy methods

NASA Astrophysics Data System (ADS)

Yakalı, Gül; Biçer, Abdullah; Eke, Canel; Cin, Günseli Turgut

2018-04-01

A bis(chalcone), (2E,6E)-2,6-bis((E)-3phenylallidene)cyclohexanone, was characterized by 1H NMR, 13C NMR, FTIR, UV-Vis spectroscopy, gamma-ray spectroscopy and single crystal X- ray structural analysis. The optimized molecular structure of the compound is calculated using DFT/B3LYP with 6-31G (d,p) level. The calculated geometrical parameters are in good agreement with the experimental data obtained from our reported X-ray structure. The powder and single crystal compounds were gama-irradiated using clinical electron linear accelerator and 60Co gamma-ray source, respectively. Spectral studies (1H NMR, 13C NMR, FTIR and UV-Vis) of powder chalcone compound were also investigated before and after irradiation. Depending on the irradiation notable changes were observed in spectral features powder sample. Single crystal X-ray diffraction investigation shows that both unirradiated and irradiated single crystal samples crystallizes in a orthorhombic crystal system in the centrosymmetric space group Pbcn and exhibits an C-H..O intramolecular and intermolecular hydrogen bonds. The crystal packing is stabilised by strong intermolecular bifurcate C-H..O hydrogen bonds and π…π stacking interactions. The asymmetric unit of the title compound contains one-half of a molecule. The other half of the molecule is generated with (1-x,y,-3/2-z) symmetry operator. The molecule is almost planar due to having π conjugated system of chalcones. However, irradiated single crystal compound showed significant changes lattice parameters, crystal volume and density. According to results of gamma-ray spectroscopy, radioactive elements of powder compound which are 123Sb(n,g),124Sb,57Fe(g,p),56Mn, 55Mn(g,n), and 54Mn were determined using photoactivation analysis. However, the most intensive gamma-ray energy signals are 124Sb.

Superhumps linked to X-ray emission. The superoutbursts of SSS J122221.7-311525 and GW Lib

NASA Astrophysics Data System (ADS)

Neustroev, V. V.; Page, K. L.; Kuulkers, E.; Osborne, J. P.; Beardmore, A. P.; Knigge, C.; Marsh, T.; Suleimanov, V. F.; Zharikov, S. V.

2018-03-01

Context. We present more than 4 years of Swift X-ray observations of the 2013 superoutburst, subsequent decline and quiescence of the WZ Sge-type dwarf nova SSS J122221.7-311525 (SSS J122222) from 6 days after discovery. Aims: Only a handful of WZ Sge-type dwarf novae have been observed in X-rays, and until recently GW Lib was the only binary of this type with complete coverage of an X-ray light curve throughout a superoutburst. We collected extensive X-ray data of a second such system to understand the extent to which the unexpected properties of GW Lib are common to the WZ Sge class. Methods: We collected 60 Swift-XRT observations of SSS J122222 between 2013 January 6 and 2013 July 1. Four follow-up observations were performed in 2014, 2015, 2016 and 2017. The total exposure time of our observations is 86.6 ks. We analysed the X-ray light curve and compared it with the behaviour of superhumps which were detected in the optical light curve. We also performed spectral analysis of the data. The results were compared with the properties of GW Lib, for which new X-ray observations were also obtained. Results: SSS J122222 was variable and around five times brighter in 0.3-10 keV X-rays during the superoutburst than in quiescence, mainly because of a significant strengthening of a high-energy component of the X-ray spectrum. The post-outburst decline of the X-ray flux lasted at least 500 d. The data show no evidence of the expected optically thick boundary layer in the system during the outburst. SSS J122222 also exhibited a sudden X-ray flux change in the middle of the superoutburst, which occurred exactly at the time of the superhump stage transition. A similar X-ray behaviour was also detected in GW Lib. Conclusions: We show that the X-ray flux exhibits changes at the times of changes in the superhump behaviour of both SSS J122222 and GW Lib. This result demonstrates a relationship between the outer disc and the white dwarf boundary layer for the first time, and suggests that models for accretion discs in high mass ratio accreting binaries are currently incomplete. The very long decline to X-ray quiescence is also in strong contrast to the expectation of low viscosity in the disc after outburst.

Timing Studies and QPO Detection for Transient Xray Pulsar 4u 0115+634 by RXTE.

NASA Astrophysics Data System (ADS)

Ram Dugair, Moti; Jaaffrey, S. N. A.

We present results of timing analysis of data of the transient X-ray pulsar 4U 0115+634 (Neu-tron star with fast spin entry) taken by the Rossi X-ray Timing Explorer (RXTE) space satellite. We first time observed the occurrence of 3 QPOs of 3 m Hz, 8 m Hz and 60 m Hz of the X-ray outburst of 2008. In particular the frequencies of the QPO's may be attributed to those of oscillations of disturbance occuring in the inner region of the accreted disk of the neutron star during the truncation of viscous circum stellar disc around the Be-star. The role of the interaction between the neutron star and the circumstellar is very important. Appearance of three QPOs in X-ray Binary system is a new phenomenon and difficult to understand.

Ambient x-ray pollution assessment at inspection gates of airports- a case study of Mehrabad and Imam Khomeini Airports in Iran.

PubMed

Pourtaghi, Gholamhossein; Valipour, Firouz; Nourian, Sepideh; Mofidi, Amirabbas

2014-01-01

As a well-known, physical carcinogen, ambient X-ray pollution assessment would be of great importance in today's modern world. Accordingly, the present study was done to measure the exposure level of ambient X-ray at inspection gates of two airports in Iran. According to which, the X-ray was measured at different points of the inspection gates including closed and opened Curtain, as well as seating place of operators beside the X-ray inspection systems. The recorded data were then analyzed by "sign" and t-tests. The total average exposure level of the measured x-ray was 2.68 ± 0.73 μsv.h(-1). The measured x-ray exposure level was 2.07 ± 0.61 (μsv.h(-1)) released from RAPISCAN X-ray inspection system and 3.3 ± 1.34 (μsv.h(-1)) emitted from HEIMANN X-ray inspection system. Comparison of average x-ray doses of the systems in both airports showed that the minimum and maximum exposure levels were recorded at 1(m) far from the devices and at the entrance of the devices, respectively. The exposure levels at all measurement points were lower than the occupational exposure limit. This reveals the fact that the exposed operators are not probably at risk of adverse health effects.

Advances in indirect detector systems for ultra high-speed hard X-ray imaging with synchrotron light

NASA Astrophysics Data System (ADS)

Olbinado, M. P.; Grenzer, J.; Pradel, P.; De Resseguier, T.; Vagovic, P.; Zdora, M.-C.; Guzenko, V. A.; David, C.; Rack, A.

2018-04-01

We report on indirect X-ray detector systems for various full-field, ultra high-speed X-ray imaging methodologies, such as X-ray phase-contrast radiography, diffraction topography, grating interferometry and speckle-based imaging performed at the hard X-ray imaging beamline ID19 of the European Synchrotron—ESRF. Our work highlights the versatility of indirect X-ray detectors to multiple goals such as single synchrotron pulse isolation, multiple-frame recording up to millions frames per second, high efficiency, and high spatial resolution. Besides the technical advancements, potential applications are briefly introduced and discussed.

Apparatus and method to enhance X-ray production in laser produced plasmas

DOEpatents

Augustoni, A.L.; Gerardo, J.B.; Raymond, T.D.

1992-12-29

Method and apparatus for generating x-rays for use in, for instance, x-ray photolithography is disclosed. The method of generating x-rays includes the steps of providing a target and irradiating the target with a laser system which produces a train of sub-pulses to generate an x-ray producing plasma. The sub-pulses are of both high intensity and short duration. The apparatus for generating x-rays from a plasma includes a vacuum chamber, a target supported within the chamber and a laser system, including a short storage time laser. 8 figs.

Microfocus/Polycapillary-Optic Crystallographic X-Ray System

NASA Technical Reports Server (NTRS)

Joy, Marshall; Gubarev, Mikhail; Ciszak, Ewa

2005-01-01

A system that generates an intense, nearly collimated, nearly monochromatic, small-diameter x-ray beam has been developed for use in macromolecular crystallography. A conventional x-ray system for macromolecular crystallography includes a rotating-anode x-ray source, which is massive (.500 kg), large (approximately 2 by 2 by 1 m), and power-hungry (between 2 and 18 kW). In contrast, the present system generates a beam of the required brightness from a microfocus source, which is small and light enough to be mounted on a laboratory bench, and operates at a power level of only tens of watts. The figure schematically depicts the system as configured for observing x-ray diffraction from a macromolecular crystal. In addition to the microfocus x-ray source, the system includes a polycapillary optic . a monolithic block (typically a bundle of fused glass tubes) that contains thousands of straight or gently curved capillary channels, along which x-rays propagate with multiple reflections. This particular polycapillary optic is configured to act as a collimator; the x-ray beam that emerges from its output face consists of quasi-parallel subbeams with a small angular divergence and a diameter comparable to the size of a crystal to be studied. The gap between the microfocus x-ray source and the input face of the polycapillary optic is chosen consistently with the focal length of the polycapillary optic and the need to maximize the solid angle subtended by the optic in order to maximize the collimated x-ray flux. The spectrum from the source contains a significant component of Cu K (photon energy is 8.08 keV) radiation. The beam is monochromatized (for Cu K ) by a nickel filter 10 m thick. In a test, this system was operated at a power of 40 W (current of 897 A at an accelerating potential of 45 kV), with an anode x-ray spot size of 41+/-2 microns. Also tested, in order to provide a standard for comparison, was a commercial rotating-anode x-ray crystallographic system with a pyrolytic graphite monochromator and a 250-micron pinhole collimator, operating at a power of 3.15 kW (current of 70 mA at an accelerating potential of 45 kV). The flux of collimated Cu K radiation in this system was found to be approximately 16 times that in the rotatinganode system. Data on x-ray diffraction from crystals of tetragonal form of lysozyme (protein) in this system were found to be of high quality and to be reducible by use of standard crystallographic software.

TOPICAL REVIEW: Human soft tissue analysis using x-ray or gamma-ray techniques

NASA Astrophysics Data System (ADS)

Theodorakou, C.; Farquharson, M. J.

2008-06-01

This topical review is intended to describe the x-ray techniques used for human soft tissue analysis. X-ray techniques have been applied to human soft tissue characterization and interesting results have been presented over the last few decades. The motivation behind such studies is to provide improved patient outcome by using the data obtained to better understand a disease process and improve diagnosis. An overview of theoretical background as well as a complete set of references is presented. For each study, a brief summary of the methodology and results is given. The x-ray techniques include x-ray diffraction, x-ray fluorescence, Compton scattering, Compton to coherent scattering ratio and attenuation measurements. The soft tissues that have been classified using x-rays or gamma rays include brain, breast, colon, fat, kidney, liver, lung, muscle, prostate, skin, thyroid and uterus.

The UHURU X-ray instrument.

NASA Technical Reports Server (NTRS)

Jagoda, N.; Austin, G.; Mickiewicz, S.; Goddard, R.

1972-01-01

On Dec. 12, 1970, the UHURU X-ray observatory was launched into equatorial orbit with the prime mission of conducting an all-sky survey of astronomical X-ray sources with intensities of 0.00005 Sco-X1 or greater. The X-ray detection system contains 12 gas-filled proportional counters, 6 behind each collimator. The aspect system is discussed together with the structure, the pulse height analyzer, the command system, the calibration system, and the power distribution system. Pulse shape discrimination circuits used on UHURU use the same technique that was used on the system originally developed for large area proportional counters described by Gorenstein and Mickiewicz (1968).

Analysis of XMM-Newton Data from Extended Sources and the Diffuse X-Ray Background

NASA Technical Reports Server (NTRS)

Snowden, Steven

2011-01-01

Reduction of X-ray data from extended objects and the diffuse background is a complicated process that requires attention to the details of the instrumental response as well as an understanding of the multiple background components. We present methods and software that we have developed to reduce data from XMM-Newton EPIC imaging observations for both the MOS and PN instruments. The software has now been included in the Science Analysis System (SAS) package available through the XMM-Newton Science Operations Center (SOC).

NuSTAR Hard X-Ray Observation of the Gamma-Ray Binary Candidate HESS J1832-093

NASA Astrophysics Data System (ADS)

Mori, Kaya; Gotthelf, E. V.; Hailey, Charles J.; Hord, Ben J.; de Oña Wilhelmi, Emma; Rahoui, Farid; Tomsick, John A.; Zhang, Shuo; Hong, Jaesub; Garvin, Amani M.; Boggs, Steven E.; Christensen, Finn E.; Craig, William W.; Harrison, Fiona A.; Stern, Daniel; Zhang, William W.

2017-10-01

We present a hard X-ray observation of the TeV gamma-ray binary candidate HESS J1832-093, which is coincident with the supernova remnant G22.7-0.2, using the Nuclear Spectroscopic Telescope Array. Non-thermal X-ray emission from XMMU J183245-0921539, the X-ray source associated with HESS J1832-093, is detected up to ˜30 keV and is well-described by an absorbed power-law model with a best-fit photon index {{Γ }}=1.5+/- 0.1. A re-analysis of archival Chandra and XMM-Newton data finds that the long-term X-ray flux increase of XMMU J183245-0921539 is {50}-20+40 % (90% C.L.), much less than previously reported. A search for a pulsar spin period or binary orbit modulation yields no significant signal to a pulse fraction limit of {f}p< 19 % in the range 4 ms < P< 40 ks. No red noise is detected in the FFT power spectrum to suggest active accretion from a binary system. While further evidence is required, we argue that the X-ray and gamma-ray properties of XMMU J183245-0921539 are most consistent with a non-accreting binary generating synchrotron X-rays from particle acceleration in the shock formed as a result of the pulsar and stellar wind collision. We also report on three nearby hard X-ray sources, one of which may be associated with diffuse emission from a fast-moving supernova fragment interacting with a dense molecular cloud.

Longterm lightcurves of X-ray binaries

NASA Astrophysics Data System (ADS)

Clarkson, William

The X-ray Binaries (XRB) consist of a compact object and a stellar companion, which undergoes large-scale mass-loss to the compact object by virtue of the tight ( P orb usually hours-days) orbit, producing an accretion disk surrounding the compact object. The liberation of gravitational potential energy powers exotic high-energy phenomena, indeed the resulting accretion/ outflow process is among the most efficient energy-conversion machines in the universe. The Burst And Transient Source Experiment (BATSE) and RXTE All Sky Monitor (ASM) have provided remarkable X-ray lightcurves above 1.3keV for the entire sky, at near-continuous coverage, for intervals of 9 and 7 years respectively (with ~3 years' overlap). With an order of magnitude increase in sensitivity compared to previous survey instruments, these instruments have provided new insight into the high-energy behaviour of XRBs on timescales of tens to thousands of binary orbits. This thesis describes detailed examination of the long-term X-ray lightcurves of the neutron star XRB X2127+119, SMC X-1, Her X- 1, LMC X-4, Cyg X-2 and the as yet unclassified Circinus X-1, and for Cir X-1, complementary observations in the IR band. Chapters 1 & 2 introduce X-ray Binaries in general and longterm periodicities in particular. Chapter 3 introduces the longterm datasets around which this work is based, and the chosen methods of analysis of these datasets. Chapter 4 examines the burst history of the XRB X2127+119, suggesting three possible interpretations of the apparently contradictory X-ray emission from this system, including a possible confusion of two spatially distinct sources (which was later vindicated by high-resolution imaging). Chapters 5 and 6 describe the characterisation of accretion disk warping, providing observational verification of the prevailing theoretical framework for such disk-warps. Chapters 7 & 8 examine the enigmatic XRB Circinus X-1 with high-resolution IR spectroscopy (chapter 7) and the RXTE/ASM (chapter 8), establishing an improved orbital ephemeris and suggesting the system may be in a state of rapid post- supernova evolution. In chapter 8 we follow this up with a direct search for the X-ray supernova remnant expected from such a system, concluding that with present observations the diffuse emission from Cir X-1 is indistinguishable from scattering by dust-grains in the interstellar medium.

A novel lobster-eye imaging system based on Schmidt-type objective for X-ray-backscattering inspection

DOE Office of Scientific and Technical Information (OSTI.GOV)

Xu, Jie; Wang, Xin, E-mail: wangx@tongji.edu.cn, E-mail: mubz@tongji.edu.cn; Zhan, Qi

This paper presents a novel lobster-eye imaging system for X-ray-backscattering inspection. The system was designed by modifying the Schmidt geometry into a treble-lens structure in order to reduce the resolution difference between the vertical and horizontal directions, as indicated by ray-tracing simulations. The lobster-eye X-ray imaging system is capable of operating over a wide range of photon energies up to 100 keV. In addition, the optics of the lobster-eye X-ray imaging system was tested to verify that they meet the requirements. X-ray-backscattering imaging experiments were performed in which T-shaped polymethyl-methacrylate objects were imaged by the lobster-eye X-ray imaging system basedmore » on both the double-lens and treble-lens Schmidt objectives. The results show similar resolution of the treble-lens Schmidt objective in both the vertical and horizontal directions. Moreover, imaging experiments were performed using a second treble-lens Schmidt objective with higher resolution. The results show that for a field of view of over 200 mm and with a 500 mm object distance, this lobster-eye X-ray imaging system based on a treble-lens Schmidt objective offers a spatial resolution of approximately 3 mm.« less

A novel lobster-eye imaging system based on Schmidt-type objective for X-ray-backscattering inspection

NASA Astrophysics Data System (ADS)

Xu, Jie; Wang, Xin; Zhan, Qi; Huang, Shengling; Chen, Yifan; Mu, Baozhong

2016-07-01

This paper presents a novel lobster-eye imaging system for X-ray-backscattering inspection. The system was designed by modifying the Schmidt geometry into a treble-lens structure in order to reduce the resolution difference between the vertical and horizontal directions, as indicated by ray-tracing simulations. The lobster-eye X-ray imaging system is capable of operating over a wide range of photon energies up to 100 keV. In addition, the optics of the lobster-eye X-ray imaging system was tested to verify that they meet the requirements. X-ray-backscattering imaging experiments were performed in which T-shaped polymethyl-methacrylate objects were imaged by the lobster-eye X-ray imaging system based on both the double-lens and treble-lens Schmidt objectives. The results show similar resolution of the treble-lens Schmidt objective in both the vertical and horizontal directions. Moreover, imaging experiments were performed using a second treble-lens Schmidt objective with higher resolution. The results show that for a field of view of over 200 mm and with a 500 mm object distance, this lobster-eye X-ray imaging system based on a treble-lens Schmidt objective offers a spatial resolution of approximately 3 mm.

Inverse Transformation: Unleashing Spatially Heterogeneous Dynamics with an Alternative Approach to XPCS Data Analysis.

PubMed

Andrews, Ross N; Narayanan, Suresh; Zhang, Fan; Kuzmenko, Ivan; Ilavsky, Jan

2018-02-01

X-ray photon correlation spectroscopy (XPCS), an extension of dynamic light scattering (DLS) in the X-ray regime, detects temporal intensity fluctuations of coherent speckles and provides scattering vector-dependent sample dynamics at length scales smaller than DLS. The penetrating power of X-rays enables probing dynamics in a broad array of materials with XPCS, including polymers, glasses and metal alloys, where attempts to describe the dynamics with a simple exponential fit usually fails. In these cases, the prevailing XPCS data analysis approach employs stretched or compressed exponential decay functions (Kohlrausch functions), which implicitly assume homogeneous dynamics. In this paper, we propose an alternative analysis scheme based upon inverse Laplace or Gaussian transformation for elucidating heterogeneous distributions of dynamic time scales in XPCS, an approach analogous to the CONTIN algorithm widely accepted in the analysis of DLS from polydisperse and multimodal systems. Using XPCS data measured from colloidal gels, we demonstrate the inverse transform approach reveals hidden multimodal dynamics in materials, unleashing the full potential of XPCS.

Inverse Transformation: Unleashing Spatially Heterogeneous Dynamics with an Alternative Approach to XPCS Data Analysis

PubMed Central

Andrews, Ross N.; Narayanan, Suresh; Zhang, Fan; Kuzmenko, Ivan; Ilavsky, Jan

2018-01-01

X-ray photon correlation spectroscopy (XPCS), an extension of dynamic light scattering (DLS) in the X-ray regime, detects temporal intensity fluctuations of coherent speckles and provides scattering vector-dependent sample dynamics at length scales smaller than DLS. The penetrating power of X-rays enables probing dynamics in a broad array of materials with XPCS, including polymers, glasses and metal alloys, where attempts to describe the dynamics with a simple exponential fit usually fails. In these cases, the prevailing XPCS data analysis approach employs stretched or compressed exponential decay functions (Kohlrausch functions), which implicitly assume homogeneous dynamics. In this paper, we propose an alternative analysis scheme based upon inverse Laplace or Gaussian transformation for elucidating heterogeneous distributions of dynamic time scales in XPCS, an approach analogous to the CONTIN algorithm widely accepted in the analysis of DLS from polydisperse and multimodal systems. Using XPCS data measured from colloidal gels, we demonstrate the inverse transform approach reveals hidden multimodal dynamics in materials, unleashing the full potential of XPCS. PMID:29875506

X-ray lasers: Strategic problems and potential as an in-orbit exoatmospheric ballistic missile defense system

NASA Astrophysics Data System (ADS)

Perusich, Karl Anthony

1986-12-01

The problems and potential of a single proposed ballistic missile defense system, the X-ray laser-armed satellite, are examined in this research. Specifically, the X-ray laser satellite system is examined to determine its impact on the issues of cost-effectiveness and crisis stability. To examime the cost-effectiveness and the crisis stability of the X-ray laser satellites, a simulation of a nuclear exchange was constructed. The X-ray laser satellites were assumed to be vulnerable to attack from energy satellites with limited satellite-to-satellite lethal ranges. Symmetric weapons and force postures were used. Five principal weapon classes were used in the model: ICMBs, SLBMs, X-ray laser satellites, bombers, and endo-atmospheric silo defenses. Also, the orbital dynamics of the ballistic missiles and satellites were simulated. The cost-effectiveness of the X-ray laser satellites was determined for two different operational capabilities, damage-limitation and assured destruction. The following conclusions were reached. The effects of deployment of a new weapon system on the Triad as a whole should be examined. The X-ray laser was found to have little effectiveness as a damage-limiting weapon for a defender. For an assured destruction capability, X-ray laser satellites could be part of a minimum-cost force mix with that capability.

XTE J1946+274 = GRO J1944+26: An Enigmatic Be/X-Ray Binary

NASA Technical Reports Server (NTRS)

Wilson, Colleen A.; Finger, Mark H.; Coe, M. J.; Negueruela, Ignacio

2003-01-01

XTE J1946+274 = GRO J1944+26 is a 15.8 s Be/X-ray pulsar discovered simultaneously in 1998 September with the Burst and Transient Source Experiment (BATSE) on the Compton Gamma Ray Observatory (CGRO) and the All-Sky Monitor (ASM) on the Rossi X-Ray Timing Explorer (RXTE). Here we present new results from BATSE and RXTE including a pulse timing analysis, spectral analysis, and evidence for an accretion disk. Our pulse timing analysis yielded an orbital period of 169.2 days, a moderate eccentricity 0.33, and implied a mass function of 9.7 solar masses. We observed evidence for an accretion disk, a correlation between measured spin-up rate and flux, which was fitted to obtain a distance estimate of 9.5 +/- 2.9 kpc. XTE J1946+274 remained active from 1998 September to 2001 July, undergoing 13 outbursts that were not locked in orbital phase. Comparing RXTE Proportional Counter Array observations from the initial bright outburst in 1998 and the last pair of outbursts in 2001, we found energy and intensity-dependent pulse profile variations in both outbursts and hardening spectra with increasing intensity during the fainter 2001 outbursts. In 2001 July, optical H alpha observations indicated that a density perturbation appeared in the Be disk as the X-ray outbursts ceased. We propose that the equatorial plane of the Be star is inclined with respect to the orbital plane in this system and that this inclination may be a factor in the unusual outburst behavior of the system.

X-ray Spectral Formation In High-mass X-ray Binaries: The Case Of Vela X-1

NASA Astrophysics Data System (ADS)

Akiyama, Shizuka; Mauche, C. W.; Liedahl, D. A.; Plewa, T.

2007-05-01

We are working to develop improved models of radiatively-driven mass flows in the presence of an X-ray source -- such as in X-ray binaries, cataclysmic variables, and active galactic nuclei -- in order to infer the physical properties that determine the X-ray spectra of such systems. The models integrate a three-dimensional time-dependent hydrodynamics capability (FLASH); a comprehensive and uniform set of atomic data, improved calculations of the line force multiplier that account for X-ray photoionization and non-LTE population kinetics, and X-ray emission-line models appropriate to X-ray photoionized plasmas (HULLAC); and a Monte Carlo radiation transport code that simulates Compton scattering and recombination cascades following photoionization. As a test bed, we have simulated a high-mass X-ray binary with parameters appropriate to Vela X-1. While the orbital and stellar parameters of this system are well constrained, the physics of X-ray spectral formation is less well understood because the canonical analytical wind velocity profile of OB stars does not account for the dynamical and radiative feedback effects due to the rotation of the system and to the irradiation of the stellar wind by X-rays from the neutron star. We discuss the dynamical wind structure of Vela X-1 as determined by the FLASH simulation, where in the binary the X-ray emission features originate, and how the spatial and spectral properties of the X-ray emission features are modified by Compton scattering, photoabsorption, and fluorescent emission. This work was performed under the auspices of the U.S. Department of Energy by University of California, Lawrence Livermore National Laboratory under Contract W-7405-Eng-48.

A mirror for lab-based quasi-monochromatic parallel x-rays

NASA Astrophysics Data System (ADS)

Nguyen, Thanhhai; Lu, Xun; Lee, Chang Jun; Jung, Jin-Ho; Jin, Gye-Hwan; Kim, Sung Youb; Jeon, Insu

2014-09-01

A multilayered parabolic mirror with six W/Al bilayers was designed and fabricated to generate monochromatic parallel x-rays using a lab-based x-ray source. Using this mirror, curved bright bands were obtained in x-ray images as reflected x-rays. The parallelism of the reflected x-rays was investigated using the shape of the bands. The intensity and monochromatic characteristics of the reflected x-rays were evaluated through measurements of the x-ray spectra in the band. High intensity, nearly monochromatic, and parallel x-rays, which can be used for high resolution x-ray microscopes and local radiation therapy systems, were obtained.

Development of an X-ray imaging system to prevent scintillator degradation for white synchrotron radiation.

PubMed

Zhou, Tunhe; Wang, Hongchang; Connolley, Thomas; Scott, Steward; Baker, Nick; Sawhney, Kawal

2018-05-01

The high flux of the white X-ray beams from third-generation synchrotron light sources can significantly benefit the development of high-speed X-ray imaging, but can also bring technical challenges to existing X-ray imaging systems. One prevalent problem is that the image quality deteriorates because of dust particles accumulating on the scintillator screen during exposure to intense X-ray radiation. Here, this problem has been solved by embedding the scintillator in a flowing inert-gas environment. It is also shown that the detector maintains the quality of the captured images even after days of X-ray exposure. This modification is cost-efficient and easy to implement. Representative examples of applications using the X-ray imaging system are also provided, including fast tomography and multimodal phase-contrast imaging for biomedical and geological samples. open access.

Development of an X-ray imaging system to prevent scintillator degradation for white synchrotron radiation

PubMed Central

Zhou, Tunhe; Wang, Hongchang; Scott, Steward

2018-01-01

The high flux of the white X-ray beams from third-generation synchrotron light sources can significantly benefit the development of high-speed X-ray imaging, but can also bring technical challenges to existing X-ray imaging systems. One prevalent problem is that the image quality deteriorates because of dust particles accumulating on the scintillator screen during exposure to intense X-ray radiation. Here, this problem has been solved by embedding the scintillator in a flowing inert-gas environment. It is also shown that the detector maintains the quality of the captured images even after days of X-ray exposure. This modification is cost-efficient and easy to implement. Representative examples of applications using the X-ray imaging system are also provided, including fast tomography and multimodal phase-contrast imaging for biomedical and geological samples. PMID:29714191

Image quality assessment and medical physics evaluation of different portable dental X-ray units.

PubMed

Pittayapat, Pisha; Oliveira-Santos, Christiano; Thevissen, Patrick; Michielsen, Koen; Bergans, Niki; Willems, Guy; Debruyckere, Deborah; Jacobs, Reinhilde

2010-09-10

Recently developed portable dental X-ray units increase the mobility of the forensic odontologists and allow more efficient X-ray work in a disaster field, especially when used in combination with digital sensors. This type of machines might also have potential for application in remote areas, military and humanitarian missions, dental care of patients with mobility limitation, as well as imaging in operating rooms. To evaluate radiographic image quality acquired by three portable X-ray devices in combination with four image receptors and to evaluate their medical physics parameters. Images of five samples consisting of four teeth and one formalin-fixed mandible were acquired by one conventional wall-mounted X-ray unit, MinRay 60/70 kVp, used as a clinical standard, and three portable dental X-ray devices: AnyRay 60 kVp, Nomad 60 kVp and Rextar 70 kVp, in combination with a phosphor image plate (PSP), a CCD, or a CMOS sensor. Three observers evaluated images for standard image quality besides forensic diagnostic quality on a 4-point rating scale. Furthermore, all machines underwent tests for occupational as well as patient dosimetry. Statistical analysis showed good quality imaging for all system, with the combination of Nomad and PSP yielding the best score. A significant difference in image quality between the combination of the four X-ray devices and four sensors was established (p<0.05). For patient safety, the exposure rate was determined and exit dose rates for MinRay at 60 kVp, MinRay at 70 kVp, AnyRay, Nomad and Rextar were 3.4 mGy/s, 4.5 mGy/s, 13.5 mGy/s, 3.8 mGy/s and 2.6 mGy/s respectively. The kVp of the AnyRay system was the most stable, with a ripple of 3.7%. Short-term variations in the tube output of all the devices were less than 10%. AnyRay presented higher estimated effective dose than other machines. Occupational dosimetry showed doses at the operator's hand being lowest with protective shielding (Nomad: 0.1 microGy). It was also low while using remote control (distance>1m: Rextar <0.2 microGy, MinRay <0.1 microGy). The present study demonstrated the feasibility of three portable X-ray systems to be used for specific indications, based on acceptable image quality and sufficient accuracy of the machines and following the standard guidelines for radiation hygiene. Copyright 2010 Elsevier Ireland Ltd. All rights reserved.

The XMM-Newton Extended Survey of the Taurus Molecular Cloud (XEST)

NASA Technical Reports Server (NTRS)

Guedel, M.; Briggs, K. R.; Arzner, K.; Audard, M.; Bouvier, J.; Feigelson, E. D.; Franciosini, E.; Glauser, A.; Grosso, N.; Micela, G.;

Exploring the galaxy cluster-group transition regime at high redshifts. Physical properties of two newly detected z > 1 systems

NASA Astrophysics Data System (ADS)

Šuhada, R.; Fassbender, R.; Nastasi, A.; Böhringer, H.; de Hoon, A.; Pierini, D.; Santos, J. S.; Rosati, P.; Mühlegger, M.; Quintana, H.; Schwope, A. D.; Lamer, G.; Kohnert, J.; Pratt, G. W.

2011-06-01

Context. Multi-wavelength surveys for clusters of galaxies are opening a window on the elusive high-redshift (z > 1) cluster population. Well controlled statistical samples of distant clusters will enable us to answer questions about their cosmological context, early assembly phases and the thermodynamical evolution of the intracluster medium. Aims: We report on the detection of two z > 1 systems, XMMU J0302.2-0001 and XMMU J1532.2-0836, as part of the XMM-Newton Distant Cluster Project (XDCP) sample. We investigate the nature of the sources, measure their spectroscopic redshift and determine their basic physical parameters. Methods: The results of the present paper are based on the analysis of XMM-Newton archival data, optical/near-infrared imaging and deep optical follow-up spectroscopy of the clusters. Results: We confirm the X-ray source XMMU J0302.2-0001 as a gravitationally bound, bona fide cluster of galaxies at spectroscopic redshift z = 1.185. We estimate its M500 mass to (1.6 ± 0.3) × 1014 M⊙ from its measured X-ray luminosity. This ranks the cluster among intermediate mass system. In the case of XMMU J1532.2-0836 we find the X-ray detection to be coincident with a dynamically bound system of galaxies at z = 1.358. Optical spectroscopy reveals the presence of a central active galactic nucleus, which can be a dominant source of the detected X-ray emission from this system. We provide upper limits of X-ray parameters for the system and discuss cluster identification challenges in the high-redshift low-mass cluster regime. A third, intermediate redshift (z = 0.647) cluster, XMMU J0302.1-0000, is serendipitously detected in the same field as XMMU J0302.2-0001. We provide its analysis as well. Based on observations obtained with ESO Telescopes at the Paranal Observatory under program ID 080.A-0659 and 081.A-0312, observations collected at the Centro Astrnómico Hispano Alemán (CAHA) at Calar Alto, Spain operated jointly by the Max-Planck Institut für Astronomie and the Instituto de Astrofísica de Andalucía (CSIC). X-ray observations were obtained by XMM-Newton.

A novel process control method for a TT-300 E-Beam/X-Ray system

NASA Astrophysics Data System (ADS)

Mittendorfer, Josef; Gallnböck-Wagner, Bernhard

2018-02-01

This paper presents some aspects of the process control method for a TT-300 E-Beam/X-Ray system at Mediscan, Austria. The novelty of the approach is the seamless integration of routine monitoring dosimetry with process data. This allows to calculate a parametric dose for each production unit and consequently a fine grain and holistic process performance monitoring. Process performance is documented in process control charts for the analysis of individual runs as well as historic trending of runs of specific process categories over a specified time range.

Analysis of axial spatial resolution in a variable resolution x-ray cone beam CT (VRX-CBCT) system

NASA Astrophysics Data System (ADS)

Dahi, Bahram; Keyes, Gary S.; Rendon, David A.; DiBianca, Frank A.

2008-03-01

The Variable Resolution X-ray (VRX) technique has been successfully used in a Cone-Beam CT (CBCT) system to increase the spatial resolution of CT images in the transverse plane. This was achieved by tilting the Flat Panel Detector (FPD) to smaller vrx y angles in a VRX Cone Beam CT (VRX-CBCT) system. In this paper, the effect on the axial spatial resolution of CT images created by the VRX-CBCT system is examined at different vrx x angles, where vrx x is the tilting angle of the FPD about its x-axis. An amorphous silicon FPD with a CsI scintillator is coupled with a micro-focus x-ray tube to form a CBCT. The FPD is installed on a rotating frame that allows rotation of up to 90° about x and y axes of the FPD. There is no rotation about the z-axis (i.e. normal to the imaging surface). Tilting the FPD about its x-axis (i.e. decreasing the vrx x angle) reduces both the width of the line-spread function and the sampling distance by a factor of sin vrx x, thereby increasing the theoretical detector pre-sampling spatial resolution proportionately. This results in thinner CT slices that in turn help increase the axial spatial resolution of the CT images. An in-house phantom is used to measure the MTF of the reconstructed CT images at different vrx x angles.

Simulation of a compact analyzer-based imaging system with a regular x-ray source

NASA Astrophysics Data System (ADS)

Caudevilla, Oriol; Zhou, Wei; Stoupin, Stanislav; Verman, Boris; Brankov, J. G.

2017-03-01

Analyzer-based Imaging (ABI) belongs to a broader family of phase-contrast (PC) X-ray techniques. PC measures X-ray deflection phenomena when interacting with a sample, which is known to provide higher contrast images of soft tissue than other X-ray methods. This is of high interest in the medical field, in particular for mammogram applications. This paper presents a simulation tool for table-top ABI systems using a conventional polychromatic X-ray source.

The Advanced X-Ray Astrophysics Facility. Observing the Universe in X-Rays

NASA Technical Reports Server (NTRS)

Neal, V.

1984-01-01

An overview of the Advanced X ray Astronophysics Facility (AXAF) program is presented. Beginning with a brief introduction to X ray astrophysics, the AXAF observatory is described including the onboard instrumentation and system capabilities. Possible X ray sources suitable for AXAF observation are identified and defined.

AE AURIGAE: FIRST DETECTION OF NON-THERMAL X-RAY EMISSION FROM A BOW SHOCK PRODUCED BY A RUNAWAY STAR

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lopez-Santiago, J.; Pereira, V.; De Castro, E.

2012-09-20

Runaway stars produce shocks when passing through interstellar medium at supersonic velocities. Bow shocks have been detected in the mid-infrared for several high-mass runaway stars and in radio waves for one star. Theoretical models predict the production of high-energy photons by non-thermal radiative processes in a number sufficiently large to be detected in X-rays. To date, no stellar bow shock has been detected at such energies. We present the first detection of X-ray emission from a bow shock produced by a runaway star. The star is AE Aur, which was likely expelled from its birthplace due to the encounter ofmore » two massive binary systems and now is passing through the dense nebula IC 405. The X-ray emission from the bow shock is detected at 30'' northeast of the star, coinciding with an enhancement in the density of the nebula. From the analysis of the observed X-ray spectrum of the source and our theoretical emission model, we confirm that the X-ray emission is produced mainly by inverse Compton upscattering of infrared photons from dust in the shock front.« less

Soft X-ray spectromicroscopy for speciation, quantitation and nano-eco-toxicology of nanomaterials.

PubMed

Lawrence, J R; Swerhone, G D W; Dynes, J J; Korber, D R; Hitchcock, A P

2016-02-01

There is a critical need for methods that provide simultaneous detection, identification, quantitation and visualization of nanomaterials at their interface with biological and environmental systems. The approach should allow speciation as well as elemental analysis. Using the intrinsic X-ray absorption properties, soft X-ray scanning transmission X-ray spectromicroscopy (STXM) allows characterization and imaging of a broad range of nanomaterials, including metals, oxides and organic materials, and at the same time is able to provide detailed mapping of biological components. Thus, STXM offers considerable potential for application to research on nanomaterials in biology and the environment. The potential and limitations of STXM in this context are discussed using a range of examples, focusing on the interaction of nanomaterials with microbial cells, biofilms and extracellular polymers. The studies outlined include speciation and mapping of metal-containing nanomaterials (Ti, Ni, Cu) and carbon-based nanomaterials (multiwalled carbon nanotubes, C60 fullerene). The benefits of X-ray fluorescence detection in soft X-ray STXM are illustrated with a study of low levels of Ni in a natural river biofilm. © 2014 The Authors Journal of Microscopy © 2014 Royal Microscopical Society.

Preparation and characterization of polymer layer systems for validation of 3D Micro X-ray fluorescence spectroscopy

NASA Astrophysics Data System (ADS)

Schaumann, Ina; Malzer, Wolfgang; Mantouvalou, Ioanna; Lühl, Lars; Kanngießer, Birgit; Dargel, Rainer; Giese, Ulrich; Vogt, Carla

2009-04-01

For the validation of the quantification of the newly-developed method of 3D Micro X-ray fluorescence spectroscopy (3D Micro-XRF) samples with a low average Z matrix and minor high Z elements are best suited. In a light matrix the interferences by matrix effects are minimized so that organic polymers are appropriate as basis for analytes which are more easily detected by X-ray fluorescence spectroscopy. Polymer layer systems were assembled from single layers of ethylene-propylene-diene rubber (EPDM) filled with changing concentrations of silica and zinc oxide as inorganic additives. Layer thicknesses were in the range of 30-150 μm. Before the analysis with 3D Micro-XRF all layers have been characterized by scanning micro-XRF with regard to filler dispersion, by infrared microscopy and light microscopy in order to determine the layer thicknesses and by ICP-OES to verify the concentration of the X-ray sensitive elements in the layers. With the results obtained for stacked polymer systems the validity of the analytical quantification model for the determination of stratified materials by 3D Micro-XRF could be demonstrated.

National Synchrotron Light Source annual report 1991. Volume 1, October 1, 1990--September 30, 1991

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hulbert, S.L.; Lazarz, N.M.

1992-04-01

This report discusses the following research conducted at NSLS: atomic and molecular science; energy dispersive diffraction; lithography, microscopy and tomography; nuclear physics; UV photoemission and surface science; x-ray absorption spectroscopy; x-ray scattering and crystallography; x-ray topography; workshop on surface structure; workshop on electronic and chemical phenomena at surfaces; workshop on imaging; UV FEL machine reviews; VUV machine operations; VUV beamline operations; VUV storage ring parameters; x-ray machine operations; x-ray beamline operations; x-ray storage ring parameters; superconducting x-ray lithography source; SXLS storage ring parameters; the accelerator test facility; proposed UV-FEL user facility at the NSLS; global orbit feedback systems; and NSLSmore » computer system.« less

Source Apportionment of Atmospheric Particles by Electron Probe X-Ray Microanalysis and Receptor Models.

NASA Astrophysics Data System (ADS)

van Borm, Werner August

Electron probe X-ray microanalysis (EPXMA) in combination with an automation system and an energy-dispersive X-ray detection system was used to analyse thousands of microscopical particles, originating from the ambient atmosphere. The huge amount of data was processed by a newly developed X-ray correction method and a number of data reduction procedures. A standardless ZAF procedure for EPXMA was developed for quick semi-quantitative analysis of particles starting from simple corrections, valid for bulk samples and modified taking into account the particle finit diameter, assuming a spherical shape. Tested on a limited database of bulk and particulate samples, the compromise between calculation speed and accuracy yielded for elements with Z > 14 accuracies on concentrations less than 10% while absolute deviations remained below 4 weight%, thus being only important for low concentrations. Next, the possibilities for the use of supervised and unsupervised multivariate particle classification were investigated for source apportionment of individual particles. In a detailed study of the unsupervised cluster analysis technique several aspects were considered, that have a severe influence on the final cluster analysis results, i.e. data acquisition, X-ray peak identification, data normalization, scaling, variable selection, similarity measure, cluster strategy, cluster significance and error propagation. A supervised approach was developed using an expert system-like approach in which identification rules are builded to describe the particle classes in a unique manner. Applications are presented for particles sampled (1) near a zinc smelter (Vieille-Montagne, Balen, Belgium), analyzed for heavy metals, (2) in an urban aerosol (Antwerp, Belgium), analyzed for over 20 elements and (3) in a rural aerosol originating from a swiss mountain area (Bern). Thus is was possible to pinpoint a number of known and unknown sources and characterize their emissions in terms of particles abundance and particle composition. Alternatively, the bulk analysis of filters (total, fine and coarse mode) using Particle Induced X -Ray Emission (PIXE) and the application of a receptor modeling approach provided for complementary information on a macroscopical level. A computer program was developed incorporating an absolute factor analysis based receptor modeling procedure. Source profiles and contributions are described by elemental concentrations and an atmospheric mass balance is put forward. The latter method was applied in a two year study of the Antwerp urban aerosol and for the swiss aerosol, revealing a number of previously known and unknown sources. Both methods were successfully combined to increase the source resolution.

Dual x-ray fluorescence spectrometer and method for fluid analysis

DOEpatents

Wilson, Bary W.; Shepard, Chester L.

2005-02-22

Disclosed are an X-ray fluorescence (SRF) spectrometer and method for on-site and in-line determination of contaminant elements in lubricating oils and in fuel oils on board a marine vessel. An XRF source block 13 contains two radionuclide sources 16, 17 (e.g. Cd 109 and Fe 55), each oriented 180 degrees from the other to excite separate targets. The Cd 109 source 16 excites sample lube oil flowing through a low molecular weight sample line 18. The Fe 55 source 17 excites fuel oil manually presented to the source beam inside a low molecular weight vial 26 or other container. Two separate detectors A and B are arranged to detect the fluorescent x-rays from the targets, photons from the analyte atoms in the lube oil for example, and sulfur identifying x-rays from bunker fuel oil for example. The system allows both automated in-line and manual on-site analysis using one set of signal processing and multi-channel analyzer electronics 34, 37 as well as one computer 39 and user interface 43.

Graphene-based microfluidics for serial crystallography.

PubMed

Sui, Shuo; Wang, Yuxi; Kolewe, Kristopher W; Srajer, Vukica; Henning, Robert; Schiffman, Jessica D; Dimitrakopoulos, Christos; Perry, Sarah L

2016-08-02

Microfluidic strategies to enable the growth and subsequent serial crystallographic analysis of micro-crystals have the potential to facilitate both structural characterization and dynamic structural studies of protein targets that have been resistant to single-crystal strategies. However, adapting microfluidic crystallization platforms for micro-crystallography requires a dramatic decrease in the overall device thickness. We report a robust strategy for the straightforward incorporation of single-layer graphene into ultra-thin microfluidic devices. This architecture allows for a total material thickness of only ∼1 μm, facilitating on-chip X-ray diffraction analysis while creating a sample environment that is stable against significant water loss over several weeks. We demonstrate excellent signal-to-noise in our X-ray diffraction measurements using a 1.5 μs polychromatic X-ray exposure, and validate our approach via on-chip structure determination using hen egg white lysozyme (HEWL) as a model system. Although this work is focused on the use of graphene for protein crystallography, we anticipate that this technology should find utility in a wide range of both X-ray and other lab on a chip applications.

Cardiac dimensional analysis by use of biplane cineradiography: description and validation of method.

PubMed

Lipscomb, K

1980-01-01

Biplane cineradiography is a potentially powerful tool for precise measurement of intracardiac dimensions. The most systematic approach to these measurements is the creation of a three-dimensional coordinate system within the x-ray field. Using this system, interpoint distances, such as between radiopaque clips or coronary artery bifurcations, can be calculated by use of the Pythagoras theorem. Alternatively, calibration factors can be calculated in order to determine the absolute dimensions of a structure, such as a ventricle or coronary artery. However, cineradiography has two problems that have precluded widespread use of the system. These problems are pincushion distortion and variable image magnification. In this paper, methodology to quantitate and compensate for these variables is presented. The method uses radiopaque beads permanently mounted in the x-ray field. The position of the bead images on the x-ray film determine the compensation factors. Using this system, measurements are made with a standard deviation of approximately 1% of the true value.

Connections Between Jet Formation and Multiwavelength Spectral Evolution in Black Hole Transients

NASA Technical Reports Server (NTRS)

Kakemci, Emrah; Chun, Yoon-Young; Dincer, Tolga; Buxton, Michelle; Tomsick, John A.; Corbel, Stephane; Kaaret, Philip

2011-01-01

Multiwavelength observations are the key to understand conditions of jet formation in Galactic black hole transient (GBHT) systems. By studying radio and optical-infrared evolution of such systems during outburst decays, the compact jet formation can be traced. Comparing this with X-ray spectral and timing evolution we can obtain physical and geometrical conditions for jet formation, and study the contribution of jets to X-ray emission. In this work, first X-ray evolution - jet relation for XTE J1752-223 will be discussed. This source had very good coverage in X-rays, optical, infrared and radio. A long exposure with INTEGRAL also allowed us to study gamma-ray behavior after the jet turns on. We will also show results from the analysis of data from GX 339-4 in the hard state with SUZAKU at low flux levels. The fits to iron line fluorescence emission show that the inner disk radius increases by a factor of greater than 27 with respect to radii in bright states. This result, along with other disk radius measurements in the hard state will be discussed within the context of conditions for launching and sustaining jets.

Evaluation of nondestructive testing techniques for the space shuttle nonmetallic thermal protection system

NASA Technical Reports Server (NTRS)

Tiede, D. A.

1972-01-01

A program was conducted to evaluate nondestructive analysis techniques for the detection of defects in rigidized surface insulation (a candidate material for the Space Shuttle thermal protection system). Uncoated, coated, and coated and bonded samples with internal defects (voids, cracks, delaminations, density variations, and moisture content), coating defects (holes, cracks, thickness variations, and loss of adhesion), and bondline defects (voids and unbonds) were inspected by X-ray radiography, acoustic, microwave, high-frequency ultrasonic, beta backscatter, thermal, holographic, and visual techniques. The detectability of each type of defect was determined for each technique (when applicable). A possible relationship between microwave reflection measurements (or X-ray-radiography density measurements) and the tensile strength was established. A possible approach for in-process inspection using a combination of X-ray radiography, acoustic, microwave, and holographic techniques was recommended.

A systematic search for new X-ray pulsators in ROSAT fields

NASA Astrophysics Data System (ADS)

Israel, G. L.

1996-10-01

For some 30 of the galactic X-ray sources, with a luminosity greater than 10^35 erg/s, it has been possible to detect a periodic modulation in the X-ray flux. These periodic signals often arise from the rotation of a compact magnetic star, or the orbital motion of a binary system. The accurate measurement of these periods provides a tool of paramount importance. For instance, in the early 1970s the measurement of the orbital period and the secular changes of the spin period in binary X-ray pulsars proved that the X-ray emission in these systems is powered by accretion and allowed to obtain the first measurements of neutron star masses. The study of periodicities yields also important insights into physical processes occurring close to the surface of the compact objects, such as white dwarfs and neutron stars, where strong gravitational and magnetic field effects play an important role. It is often possible to obtain fundamental additional information, such as the compact object angular momentum history, magnetic field strength and system orbital parameters (if in a binary system). Several other periodic or quasi-periodic phenomena in X-ray sources have been discovered over a variety of timescales (from milliseconds to years). Their interpretation comprises, e.g., precession, radial oscillations, accretion disc-magnetosphere interactions, motions or occultations in an accretion disc and activity of the companion star. Several populations of X-ray sources are expected to show coherent periodicities in their flux. These include X-ray binaries hosting a neutron star or even a black hole and cataclysmic variables where the accreting object is a white dwarf. It is plausible that also an isolated neutron star (not in binary systems) emits X-ray radiation as a result of material accreted from the interstellar medium or molecular cloud. Pulsations at soft (less than 2 keV) X-ray energies are expected to arise from the rotation of these isolated neutron stars. Rotation powered neutron stars, some of which were observed in the X-ray band, can show highly coherent signals as well. Photospheric oscillations due to opacity instability in a layer close to the surface of an isolated hot white dwarf or pre-white dwarf star can be also observed in the very soft X-ray band. Light curves with increased statistical quality, time resolution and duration have become available in recent years for a variety of astronomical objects and over different bands of the electromagnetic spectrum. Power spectrum analysis is probably the single most important technique that is applied to time series, in order to detect periodicities and quasi-periodicities by the presence of significant power spectrum peaks. Applications to time series of high energy astronomical data have been especially numerous and successful over the last decade, as a consequence of the pronounced variability (often both periodic and non-periodic in character) detected in many sources. ROSAT, an acronym for the German word Rontgensatellit, is an X-ray satellite launched in June 1990. Its X-ray telescope covers the soft X-ray band from 0.05 keV to 2.4 keV. The main aim of the mission was to perform the first all-sky survey (RASS) with imaging telescopes, possessing an X-ray sensitivity of about a factor 1000 higher than that of UHURU. The survey took the first 6 months of the operations of ROSAT. After that the satellite has been used to carry out pointed observations of selected targets. These observations cover a much smaller portion of the sky than the RASS, but afford a factor 10-1000 higher sensitivity. A systematic exploitation of the public domain ROSAT pointed observations with the Position Sensitive Proportional Counter (PSPC; about 10% of the sky and about 5300 fields until May 1996) was carried out by several groups. NASA-HEASARC and MPE have produced catalogues containing about 60000 serendipitous sources (WGA by White, Giommi & Angelini 1994; ROSATSRC by Zimmermann 1994). This number greatly exceeds the number of serendipitous X-ray sources previously known and catalogued in the Einstein and EXOSAT (about 6000) databases. In this thesis work, based on the results and products contained in the WGA catalogue, we have selected a sample of X-ray sources the light curves of which contained enough photons to carry out a meaningful timing analysis. These light curves were then searched for periodic modulations in a systematic way and a catalogue of candidate X-ray pulsators was created for further detailed study, including optical and X-ray observations. The definition of the sample was based on the minimum number of source photons, 200, that is required to reach a given sensitivity in a search for periodic pulsations with a specified number of trial frequencies. The WGA catalogue contains about 23000 light curves with more than 200 photons. In such a sample, a number of X-ray sources is expected to possess periodic modulation resulting in a power spectrum peak(s). A recently developed technique (Israel & Stella 1996) aimed at the detection of coherent or quasi-coherent signals in presence of additional non-Poissonian noise components in the power spectrum was used and applied to the selected sample of 23000 WGA light curves. The technique was modified and upgraded during this thesis work to take into account the timing problems specific to the ROSAT PSPC data. The ROSAT orbital period (96min) and the oscillations in the pointing direction (402s, ``wobble'') during the observations carried out with the PSPC detector were extensively investigated and, when possible, their effects on the search for periodicity minimised. The timing analysis of the 23000 light curves was performed by means of these techniques in a systematic and automated fashion. Starting from the PSPC light curves a catalogue of pulsator candidates together with the peak and power spectrum parameters was produced. Two different search approaches were adopted: one to cover the largest possible frequency interval; the other to detect periodic signals of reduced coherence. This thesis represents the first detailed timing analysis study of a very large number of X-ray sources. So far the automated search for coherent pulsations was performed twice over the whole sample: the first time by preserving the original Fourier resolution while the second extending the search to the maximum possible Nyquist frequency (depending on the total source photon). About 500 sources were found to possess power spectrum peaks above the detection threshold (besides the spurious peaks) but so far, only for about 10 of them a detailed analysis was carried out to confirm the presence of a reliable periodic signal. A search in the same light curves sample but at different energy intervals is in progress. Among the detected peaks in the database, there is a small number of especially interesting pulsator candidates, that were extensively analysed. This led to very significant results. This is the case of the strong 13s pulsations discovered (15sigma confidence level) in the X-ray flux of HD49798 / 1WGA J0648.0-4418 (Israel et al. 1995, 1996a), a 1.55 day single-component spectroscopic binary containing a hydrogen depleted subdwarf O6 star. The source X-ray spectrum is extremely soft, with an unabsorbed 0.1-2 keV luminosity of a few 10^32 erg/s (distance of 650 pc). A higher luminosity might be hidden in the EUV. These results indicate that the companion of HD49798 is a compact star: an accreting degenerate star, a white dwarf or, more likely, a neutron star. In either case HD49798 corresponds to a previously unobserved evolutionary stage of a massive binary system, after common envelope and spiral-in. If the 13s pulsations arise directly from the rotation of the degenerate star, they would be coherent enough to make HD 49798 a ``double spectroscopic" binary; in this case the system would hold a great potential for accurate mass measurement. A further important result is the discovery of 8.9 s pulsations (8sigma c.l.) in the X-ray flux of 2E0050.1-7247 / 1WGA J0051.8-7231 (Israel et al. 1995, 1996b), a variable X-ray source in the Small Magellanic Cloud (SMC). The source was detected several times within either Einstein IPC and ROSAT PSPC fields of view from 1979 and 1993 at different luminosity levels. The X-ray energy spectrum is consistent with an absorbed power law spectrum which steepens as the source luminosity decreases (photon index from 1.1 to 3). This new X-ray pulsator is associated (Bruhweiler et al. 1981) with the bright and variable B1 star AV111 in the SMC. These results together suggest that 2E0050.1-7247 is a new hard pulsating transient in a Be-type high mass X-ray binary. Photospheric oscillation modes were also detected in the ROSAT PSPC X-ray light curves of PG1159-035 / 1WGA J1201.7-0345 (Israel et al. 1996c). The most significant periodicity (6sigma confidence level) is at 490.5 s while many other modes were detected at different levels of significance in the period range 900-300 s in analogy with the oscillations found in the optical band. This is the first time that several modes are detected in the X-ray band from PG1159-035. The 490.5 s period is significantly different from the strongest periodicity detected at X-ray energies (540 s) with the EXOSAT CMA (Barstow et al. 1986). However both the pulsed fraction (about 20%) and the X-ray to optical flux ratio (20-30) of detected modes are consistent with the ones indicated by Barstow et al. (1986). There are no significant peaks corresponding to the strong optical oscillation mode at 516 s and 539s. The strong 490.5 s period pulsations might be related with the weak 495s signal observed in the optical band (Winglet et al. 1985). Preliminary results were also obtained for a sample of 8 X-ray sources with detected period in the range 1000 and 0.3s. Separate from the main thesis work but closely related to it, are the results included in the Appendix. These were obtained by the timing analysis of a sample of EXOSAT ME light curves. We present: (i) the discovery of 8.7s pulsations from 4U0142+614 which possesses an unusual ultrasoft energy spectrum, (ii) on the basis of this and similar findings by other authors the identification of a new possible class of X-ray pulsators, characterised by unusual properties, (iii) a search for orbital modulations in the X-ray flux of a sample of 25 Low Mass X-ray Binary systems, (iv) the timing analysis of a bright Seyfert 1 galaxy, NGC5548, which was performed with the main aim of confirming the previously reported quasi-periodic oscillations (Papadakis & Lawrence 1993a). Subtle effects which may yield spurious results in the analysis of EXOSAT X-ray light curves are also described in some detail.

Transforming Our Understanding of the X-ray Universe: The Imaging X-ray Polarimeter Explorer (IXPE)

NASA Technical Reports Server (NTRS)

Weisskopf, Martin C.; Bellazzini, Ronaldo; Costa, Enrico; Matt, Giorgio; Marshall, Herman; ODell, Stephen L.; Pavlov, George; Ramsey, Brian; Romani, Roger

2014-01-01

Accurate X-ray polarimetry can provide unique information on high-energy-astrophysical processes and sources. As there have been no meaningful X-ray polarization measurements of cosmic sources since our pioneering work in the 1970's, the time is ripe to explore this new parameter space in X-ray astronomy. To accomplish this requires a well-calibrated and well understood system that-particularly for an Explorer mission-has technical, cost, and schedule credibility. The system that we shall present satisfies these conditions, being based upon completely calibrated imaging- and polarization-sensitive detectors and proven X-ray-telescope technology.

Up and Down the Black Hole Radio/X-Ray Correlation: The 2017 Mini-outbursts from Swift J1753.5-0127

NASA Astrophysics Data System (ADS)

Plotkin, R. M.; Bright, J.; Miller-Jones, J. C. A.; Shaw, A. W.; Tomsick, J. A.; Russell, T. D.; Zhang, G.-B.; Russell, D. M.; Fender, R. P.; Homan, J.; Atri, P.; Bernardini, F.; Gelfand, J. D.; Lewis, F.; Cantwell, T. M.; Carey, S. H.; Grainge, K. J. B.; Hickish, J.; Perrott, Y. C.; Razavi-Ghods, N.; Scaife, A. M. M.; Scott, P. F.; Titterington, D. J.

2017-10-01

The candidate black hole X-ray binary Swift J1753.5-0127 faded to quiescence in 2016 November after a prolonged outburst that was discovered in 2005. Nearly three months later, the system displayed renewed activity that lasted through 2017 July. Here, we present radio and X-ray monitoring over ≈ 3 months of the renewed activity to study the coupling between the jet and the inner regions of the disk/jet system. Our observations cover low X-ray luminosities that have not historically been well-sampled ({L}{{X}}≈ 2× {10}33{--}{10}36 {erg} {{{s}}}-1; 1-10 keV), including time periods when the system was both brightening and fading. At these low luminosities, Swift J1753.5-0127 occupies a parameter space in the radio/X-ray luminosity plane that is comparable to “canonical” systems (e.g., GX 339-4), regardless of whether the system was brightening or fading, even though during its ≳11 year outburst, Swift J1753.5-0127 emitted less radio emission from its jet than expected. We discuss implications for the existence of a single radio/X-ray luminosity correlation for black hole X-ray binaries at the lowest luminosities ({L}{{X}}≲ {10}35 {erg} {{{s}}}-1), and we compare to supermassive black holes. Our campaign includes the lowest luminosity quasi-simultaneous radio/X-ray detection to date for a black hole X-ray binary during its rise out of quiescence, thanks to early notification from optical monitoring combined with fast responses from sensitive multiwavelength facilities.

The Chandra X-ray Center data system: supporting the mission of the Chandra X-ray Observatory

NASA Astrophysics Data System (ADS)

Evans, Janet D.; Cresitello-Dittmar, Mark; Doe, Stephen; Evans, Ian; Fabbiano, Giuseppina; Germain, Gregg; Glotfelty, Kenny; Hall, Diane; Plummer, David; Zografou, Panagoula

2006-06-01

The Chandra X-ray Center Data System provides end-to-end scientific software support for Chandra X-ray Observatory mission operations. The data system includes the following components: (1) observers' science proposal planning tools; (2) science mission planning tools; (3) science data processing, monitoring, and trending pipelines and tools; and (4) data archive and database management. A subset of the science data processing component is ported to multiple platforms and distributed to end-users as a portable data analysis package. Web-based user tools are also available for data archive search and retrieval. We describe the overall architecture of the data system and its component pieces, and consider the design choices and their impacts on maintainability. We discuss the many challenges involved in maintaining a large, mission-critical software system with limited resources. These challenges include managing continually changing software requirements and ensuring the integrity of the data system and resulting data products while being highly responsive to the needs of the project. We describe our use of COTS and OTS software at the subsystem and component levels, our methods for managing multiple release builds, and adapting a large code base to new hardware and software platforms. We review our experiences during the life of the mission so-far, and our approaches for keeping a small, but highly talented, development team engaged during the maintenance phase of a mission.

Optical design for ATHENA X-ray telescope based on slumped mirror segments

NASA Astrophysics Data System (ADS)

Proserpio, Laura; Breunig, Elias; Friedrich, Peter; Winter, Anita

2014-07-01

The Hot and Energetic Universe will be the focus of future ESA missions: in late 2013 the theme was selected for the second large-class mission in the Cosmic Vision science program. Fundamental questions on how and why ordinary matter assemble into galaxies and clusters, and how black holes grow and influence their surroundings can be addressed with an advanced X-ray observatory. The currently proposed ATHENA mission presents all the potentiality to answer the outstanding questions. It is based on the heritage of XMM-Newton and on the previous studies for IXO mission. The scientific payload will require state of the art instrumentations. In particular, the baseline for the X-ray optical system, delivering a combination of large area, high angular resolution, and large field of view, is the Silicon Pore Optics technology (SPO) developed by ESA in conjunction with the Cosine Measurement Systems. The slumping technology is also under development for the manufacturing of future X-ray telescopes: for several years the Max Planck Institute for Extraterrestrial physics (MPE) has been involved in the analysis of the indirect slumping approach, which foresees the manufacturing of segmented X-ray shells by shaping thin glass foils at high temperatures over concave moulds so to avoid any contact of the optical surface with other materials during the process, preserving in this way the original X-ray quality of the glass surface. The paper presents an alternative optical design for ATHENA based on the use of thin glass mirror segments obtained through slumping.

50 μm pixel pitch wafer-scale CMOS active pixel sensor x-ray detector for digital breast tomosynthesis.

PubMed

Zhao, C; Konstantinidis, A C; Zheng, Y; Anaxagoras, T; Speller, R D; Kanicki, J

2015-12-07

Wafer-scale CMOS active pixel sensors (APSs) have been developed recently for x-ray imaging applications. The small pixel pitch and low noise are very promising properties for medical imaging applications such as digital breast tomosynthesis (DBT). In this work, we evaluated experimentally and through modeling the imaging properties of a 50 μm pixel pitch CMOS APS x-ray detector named DynAMITe (Dynamic Range Adjustable for Medical Imaging Technology). A modified cascaded system model was developed for CMOS APS x-ray detectors by taking into account the device nonlinear signal and noise properties. The imaging properties such as modulation transfer function (MTF), noise power spectrum (NPS), and detective quantum efficiency (DQE) were extracted from both measurements and the nonlinear cascaded system analysis. The results show that the DynAMITe x-ray detector achieves a high spatial resolution of 10 mm(-1) and a DQE of around 0.5 at spatial frequencies  <1 mm(-1). In addition, the modeling results were used to calculate the image signal-to-noise ratio (SNRi) of microcalcifications at various mean glandular dose (MGD). For an average breast (5 cm thickness, 50% glandular fraction), 165 μm microcalcifications can be distinguished at a MGD of 27% lower than the clinical value (~1.3 mGy). To detect 100 μm microcalcifications, further optimizations of the CMOS APS x-ray detector, image aquisition geometry and image reconstruction techniques should be considered.

Ambient x-ray pollution assessment at inspection gates of airports- a case study of Mehrabad and Imam Khomeini Airports in Iran

PubMed Central

2014-01-01

Background As a well-known, physical carcinogen, ambient X-ray pollution assessment would be of great importance in today’s modern world. Accordingly, the present study was done to measure the exposure level of ambient X-ray at inspection gates of two airports in Iran. According to which, the X-ray was measured at different points of the inspection gates including closed and opened Curtain, as well as seating place of operators beside the X-ray inspection systems. The recorded data were then analyzed by “sign” and t-tests. Results The total average exposure level of the measured x-ray was 2.68 ± 0.73 μsv.h-1. The measured x-ray exposure level was 2.07 ± 0.61 (μsv.h-1) released from RAPISCAN X-ray inspection system and 3.3 ± 1.34 (μsv.h-1) emitted from HEIMANN X-ray inspection system. Comparison of average x-ray doses of the systems in both airports showed that the minimum and maximum exposure levels were recorded at 1(m) far from the devices and at the entrance of the devices, respectively. Conclusions The exposure levels at all measurement points were lower than the occupational exposure limit. This reveals the fact that the exposed operators are not probably at risk of adverse health effects. PMID:24955243

Einstein X-ray observations of QSO's with absorption-line systems

NASA Technical Reports Server (NTRS)

Junkkarinen, V. T.; Marscher, A. P.; Burbidge, E. M.

1982-01-01

The detection of X-ray emission from eight QSO's is reported, plus an upper limit to the X-ray flux from one QSO, using the Einstein X-ray Observatory (HEAO-2). Each object in the sample contains at least one absorption-line system that has been identified in its optical spectrum. The present results are combined with those of other investigators to form a sample of 44 absorption-line QSO's (with 2 sub e greater than 1.2) which have been observed in the X-ray. This sample cannot be distinguished, in terms of X-ray properties, from one which consists of QSO's in which no absorption systems have been identified. These results are consistent with extrinsic models for absorption-line clouds, as well as with current versions of intrinsic models.

Stochastic analysis of 1D and 2D surface topography of x-ray mirrors

NASA Astrophysics Data System (ADS)

Tyurina, Anastasia Y.; Tyurin, Yury N.; Yashchuk, Valeriy V.

2017-08-01

The design and evaluation of the expected performance of new optical systems requires sophisticated and reliable information about the surface topography for planned optical elements before they are fabricated. The problem is especially complex in the case of x-ray optics, particularly for the X-ray Surveyor under development and other missions. Modern x-ray source facilities are reliant upon the availability of optics with unprecedented quality (surface slope accuracy < 0.1μrad). The high angular resolution and throughput of future x-ray space observatories requires hundreds of square meters of high quality optics. The uniqueness of the optics and limited number of proficient vendors makes the fabrication extremely time consuming and expensive, mostly due to the limitations in accuracy and measurement rate of metrology used in fabrication. We discuss improvements in metrology efficiency via comprehensive statistical analysis of a compact volume of metrology data. The data is considered stochastic and a new statistical model called Invertible Time Invariant Linear Filter (InTILF) is developed now for 2D surface profiles to provide compact description of the 2D data additionally to 1D data treated so far. The model captures faint patterns in the data and serves as a quality metric and feedback to polishing processes, avoiding high resolution metrology measurements over the entire optical surface. The modeling, implemented in our Beatmark software, allows simulating metrology data for optics made by the same vendor and technology. The forecast data is vital for reliable specification for optical fabrication, to be exactly adequate for the required system performance.

Compact Objects In Binary Systems: Formation and Evolution of X-ray Binaries and Tides in Double White Dwarfs

NASA Astrophysics Data System (ADS)

Valsecchi, Francesca

Binary star systems hosting black holes, neutron stars, and white dwarfs are unique laboratories for investigating both extreme physical conditions, and stellar and binary evolution. Black holes and neutron stars are observed in X-ray binaries, where mass accretion from a stellar companion renders them X-ray bright. Although instruments like Chandra have revolutionized the field of X-ray binaries, our theoretical understanding of their origin and formation lags behind. Progress can be made by unravelling the evolutionary history of observed systems. As part of my thesis work, I have developed an analysis method that uses detailed stellar models and all the observational constraints of a system to reconstruct its evolutionary path. This analysis models the orbital evolution from compact-object formation to the present time, the binary orbital dynamics due to explosive mass loss and a possible kick at core collapse, and the evolution from the progenitor's Zero Age Main Sequence to compact-object formation. This method led to a theoretical model for M33 X-7, one of the most massive X-ray binaries known and originally marked as an evolutionary challenge. Compact objects are also expected gravitational wave (GW) sources. In particular, double white dwarfs are both guaranteed GW sources and observed electromagnetically. Although known systems show evidence of tidal deformation and a successful GW astronomy requires realistic models of the sources, detached double white dwarfs are generally approximated to point masses. For the first time, I used realistic models to study tidally-driven periastron precession in eccentric binaries. I demonstrated that its imprint on the GW signal yields constrains on the components' masses and that the source would be misclassified if tides are neglected. Beyond this adiabatic precession, tidal dissipation creates a sink of orbital angular momentum. Its efficiency is strongest when tides are dynamic and excite the components' free oscillation modes. Accounting for this effect will determine whether our interpretation of current and future observations will constrain the sources' true physical properties. To investigate dynamic tides I have developed CAFein, a novel code that calculates forced non-adiabatic stellar oscillations using a highly stable and efficient numerical method.

High resolution biomedical imaging system with direct detection of x-rays via a charge coupled device

DOEpatents

Atac, M.; McKay, T.A.

1998-04-21

An imaging system is provided for direct detection of x-rays from an irradiated biological tissue. The imaging system includes an energy source for emitting x-rays toward the biological tissue and a charge coupled device (CCD) located immediately adjacent the biological tissue and arranged transverse to the direction of irradiation along which the x-rays travel. The CCD directly receives and detects the x-rays after passing through the biological tissue. The CCD is divided into a matrix of cells, each of which individually stores a count of x-rays directly detected by the cell. The imaging system further includes a pattern generator electrically coupled to the CCD for reading a count from each cell. A display device is provided for displaying an image representative of the count read by the pattern generator from the cells of the CCD. 13 figs.

High resolution biomedical imaging system with direct detection of x-rays via a charge coupled device

DOEpatents

Atac, Muzaffer; McKay, Timothy A.

1998-01-01

An imaging system is provided for direct detection of x-rays from an irradiated biological tissue. The imaging system includes an energy source for emitting x-rays toward the biological tissue and a charge coupled device (CCD) located immediately adjacent the biological tissue and arranged transverse to the direction of irradiation along which the x-rays travel. The CCD directly receives and detects the x-rays after passing through the biological tissue. The CCD is divided into a matrix of cells, each of which individually stores a count of x-rays directly detected by the cell. The imaging system further includes a pattern generator electrically coupled to the CCD for reading a count from each cell. A display device is provided for displaying an image representative of the count read by the pattern generator from the cells of the CCD.

A one-parametric formula relating the frequencies of twin-peak quasi-periodic oscillations

NASA Astrophysics Data System (ADS)

Török, Gabriel; Goluchová, Kateřina; Šrámková, Eva; Horák, Jiří; Bakala, Pavel; Urbanec, Martin

2017-12-01

Timing analysis of X-ray flux in more than a dozen low-mass X-ray binary systems containing a neutron star reveals remarkable correlations between frequencies of two characteristic peaks present in the power-density spectra. We find a simple analytic relation that well reproduces all these individual correlations. We link this relation to a physical model which involves accretion rate modulation caused by an oscillating torus.

Operation of a separated-type x-ray interferometer for phase-contrast x-ray imaging

NASA Astrophysics Data System (ADS)

Yoneyama, Akio; Momose, Atsushi; Seya, Eiichi; Hirano, Keiichi; Takeda, Tohoru; Itai, Yuji

1999-12-01

Aiming at large-area phase-contrast x-ray imaging, a separated-type x-ray interferometer system was designed and developed to produce 25×20 mm interference patterns. The skew-symmetric optical system was adopted because of the feasibility of alignment. The rotation between the separated crystal blocks was controlled within a drift of 0.06 nrad using a feedback positioning system. This interferometer generated a 25×15 mm interference pattern with 0.07 nm synchrotron x-rays. A slice of a rabbit's kidney was observed, and its tubular structure could be revealed in a measured phase map.

Systems and methods for detecting an image of an object by use of an X-ray beam having a polychromatic distribution

DOEpatents

Parham, Christopher; Zhong, Zhong; Pisano, Etta; Connor, Dean; Chapman, Leroy D.

2010-06-22

Systems and methods for detecting an image of an object using an X-ray beam having a polychromatic energy distribution are disclosed. According to one aspect, a method can include detecting an image of an object. The method can include generating a first X-ray beam having a polychromatic energy distribution. Further, the method can include positioning a single monochromator crystal in a predetermined position to directly intercept the first X-ray beam such that a second X-ray beam having a predetermined energy level is produced. Further, an object can be positioned in the path of the second X-ray beam for transmission of the second X-ray beam through the object and emission from the object as a transmitted X-ray beam. The transmitted X-ray beam can be directed at an angle of incidence upon a crystal analyzer. Further, an image of the object can be detected from a beam diffracted from the analyzer crystal.

Projection x-ray topography system at 1-BM x-ray optics test beamline at the advanced photon source

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stoupin, Stanislav, E-mail: sstoupin@aps.anl.gov; Liu, Zunping; Trakhtenberg, Emil

2016-07-27

Projection X-ray topography of single crystals is a classic technique for the evaluation of intrinsic crystal quality of large crystals. In this technique a crystal sample and an area detector (e.g., X-ray film) collecting intensity of a chosen crystallographic reflection are translated simultaneously across an X-ray beam collimated in the diffraction scattering plane (e.g., [1, 2]). A bending magnet beamline of a third-generation synchrotron source delivering x-ray beam with a large horizontal divergence, and therefore, a large horizontal beam size at a crystal sample position offers an opportunity to obtain X-ray topographs of large crystalline samples (e.g., 6-inch wafers) inmore » just a few exposures. Here we report projection X-ray topography system implemented recently at 1-BM beamline of the Advanced Photon Source. A selected X-ray topograph of a 6-inch wafer of 4H-SiC illustrates capabilities and limitations of the technique.« less

HESS J1844-030: A New Gamma-Ray Binary?

NASA Astrophysics Data System (ADS)

McCall, Hannah; Errando, Manel

2018-01-01

Gamma-ray binaries are comprised of a massive, main-sequence star orbiting a neutron star or black hole that generates bright gamma-ray emission. Only six of these systems have been discovered. Here we report on a candidate stellar-binary system associated with the unidentified gamma-ray source HESS J1844-030, whose detection was revealed in the H.E.S.S. galactic plane survey. Analysis of 60 ks of archival Chandra data and over 100 ks of XMM-Newton data reveal a spatially associated X-ray counterpart to this TeV-emitting source (E>1012 eV), CXO J1845-031. The X-ray spectra derived from these exposures yields column density absorption in the range nH = (0.4 - 0.7) x 1022 cm-2, which is below the total galactic value for that part of the sky, indicating that the source is galactic. The flux from CXO J1845-031 increases with a factor of up to 2.5 in a 60 day timescale, providing solid evidence for flux variability at a confidence level exceeding 7 standard deviations. The point-like nature of the source, the flux variability of the nearby X-ray counterpart, and the low column density absorption are all indicative of a binary system. Once confirmed, HESS J1844-030 would represent only the seventh known gamma-ray binary, providing valuable data to advance our understanding of the physics of pulsars and stellar winds and testing high-energy astrophysical processes at timescales not present in other classes of objects.

Preliminary report for using X-rays as verification and authentication tool

DOE Office of Scientific and Technical Information (OSTI.GOV)

Esch, Ernst Ingo; Desimone, David J.; Lakis, Rollin Evan

2016-04-06

We examined x-rays for the use as authentication and verification tool in treaty verification. Several x-ray pictures were taken to determine the quality and feasibility of x-rays for these tasks. This document describes the capability of the used x-ray system and outlines its parameters and possible use.

Micro-System Technology for X-ray Astronomy

NASA Technical Reports Server (NTRS)

Schattenburg, Mark L.

2002-01-01

This research investigation was devoted to developing micro-system and nanotechnology for x-ray astronomy optics. The goal was to develop and demonstrate new types of lightweight, high accuracy x-ray optics for future high throughput, high resolution x-ray telescopes such as Constellation X (Con-X) and MAXIM. A number of significant accomplishments were reported under this program, which are summarized below. Most of this work has been reported in journal and conference proceedings and in presentations to NASA and at international meeting (see Bibliography).

Design and Analysis of the International X-Ray Observatory Mirror Modules

NASA Technical Reports Server (NTRS)

McClelland, Ryan S.; Carnahan, Timothy M.; Robinson, David W.; Saha, Timo T.

2009-01-01

The Soft X-Ray Telescope (SXT) modules are the fundamental focusing assemblies on NASA's next major X-ray telescope mission, the International X-Ray Observatory (IXO). The preliminary design and analysis of these assemblies has been completed, addressing the major engineering challenges and leading to an understanding of the factors effecting module performance. Each of the 60 modules in the Flight Mirror Assembly (FMA) supports 200-300 densely packed 0.4 mm thick glass mirror segments in order to meet the unprecedented effective area required to achieve the scientific objectives of the mission. Detailed Finite Element Analysis (FEA), materials testing, and environmental testing have been completed to ensure the modules can be successfully launched. Resulting stress margins are positive based on detailed FEA, a large factor of safety, and a design strength determined by robust characterization of the glass properties. FEA correlates well with the results of the successful modal, vibration, and acoustic environmental tests. Deformation of the module due to on-orbit thermal conditions is also a major design driver. A preliminary thermal control system has been designed and the sensitivity of module optical performance to various thermal loads has been determined using optomechanical analysis methods developed for this unique assembly. This design and analysis furthers the goal of building a module that demonstrates the ability to meet IXO requirements, which is the current focus of the IXO FMA technology development team.

Large area soft x-ray collimator to facilitate x-ray optics testing

NASA Technical Reports Server (NTRS)

Espy, Samuel L.

1994-01-01

The first objective of this program is to design a nested conical foil x-ray optic which will collimate x-rays diverging from a point source. The collimator could then be employed in a small, inexpensive x-ray test stand which would be used to test various x-ray optics and detector systems. The second objective is to demonstrate the fabrication of the x-ray reflectors for this optic using lacquer-smoothing and zero-stress electroforming techniques.

A Compact X-Ray System for Support of High Throughput Crystallography

NASA Technical Reports Server (NTRS)

Ciszak, Ewa; Gubarev, Mikhail; Gibson, Walter M.; Joy, Marshall K.; Whitaker, Ann F. (Technical Monitor)

2001-01-01

Standard x-ray systems for crystallography rely on massive generators coupled with optics that guide X-ray beams onto the crystal sample. Optics for single-crystal diffractometry include total reflection mirrors, polycapillary optics or graded multilayer monochromators. The benefit of using polycapillary optic is that it can collect x-rays over tile greatest solid angle, and thus most efficiently, utilize the greatest portion of X-rays emitted from the Source, The x-ray generator has to have a small anode spot, and thus its size and power requirements can be substantially reduced We present the design and results from the first high flux x-ray system for crystallography that combine's a microfocus X-ray generator (40microns FWHM Spot size at a power of 45 W) and a collimating, polycapillary optic. Diffraction data collected from small test crystals with cell dimensions up to 160A (lysozyme and thaumatin) are of high quality. For example, diffraction data collected from a lysozyme crystal at RT yielded R=5.0% for data extending to 1.70A. We compare these results with measurements taken from standard crystallographic systems. Our current microfocus X-ray diffraction system is attractive for supporting crystal growth research in the standard crystallography laboratory as well as in remote, automated crystal growth laboratory. Its small volume, light-weight, and low power requirements are sufficient to have it installed in unique environments, i.e.. on-board International Space Station.

The X-ray surface brightness distribution and spectral properties of six early-type galaxies

NASA Technical Reports Server (NTRS)

Trinchieri, G.; Fabbiano, G.; Canizares, C. R.

1986-01-01

Detailed analysis is presented of the Einstein X-ray observations of six early-type galaxies. The results show that effective cooling is probably present in these systems, at least in the innermost regions. Interaction with the surrounding medium has a major effect on the X-ray surface brightness distribution at large radii, at least for galaxies in clusters. The data do not warrant the general assumptions of isothermality and gravitational hydrostatic equilibrium at large radii. Comparison of the X-ray surface brightness profiles with model predictions indicate that 1/r-squared halos with masses of the order of 10 times the stellar masses are required to match the data. The physical model of White and Chevalier (1984) for steady cooling flows in a King law potential with no heavy halo gives a surface brightness distribution that resembles the data if supernovae heating is present.

Do Dental X-Rays Induce Genotoxicity and Cytotoxicity in Oral Mucosa Cells? A Critical Review.

PubMed

Angelieri, Fernanda; Yujra, Veronica Quispe; Oshima, Celina Tizuko Fujiyama; Ribeiro, Daniel Araki

2017-10-01

Dental X-rays are widely used in clinical practice, since the technique is an important approach for diagnosing diseases in dental and periodontal tissues. However, it is widely known that radiation is capable of causing damage to cellular systems, such as genotoxicity or cytotoxicity. Thus, the aim of this review was to present a critical analysis regarding the studies published on genotoxicity and cytotoxicity induced by dental X-rays in oral mucosa cells. Such studies have revealed that some oral cell types are more sensitive than others following exposure to dental X-rays. Certainly, this review will contribute to a better understanding of this matter as well as to highlighting perspectives for further studies. Ultimately, such data will promote better safety for both patients and dental professionals. Copyright© 2017, International Institute of Anticancer Research (Dr. George J. Delinasios), All rights reserved.

Monte Carlo analysis of megavoltage x-ray interaction-induced signal and noise in cadmium tungstate detectors for cargo container inspection

NASA Astrophysics Data System (ADS)

Kim, J.; Park, J.; Kim, J.; Kim, D. W.; Yun, S.; Lim, C. H.; Kim, H. K.

2016-11-01

For the purpose of designing an x-ray detector system for cargo container inspection, we have investigated the energy-absorption signal and noise in CdWO4 detectors for megavoltage x-ray photons. We describe the signal and noise measures, such as quantum efficiency, average energy absorption, Swank noise factor, and detective quantum efficiency (DQE), in terms of energy moments of absorbed energy distributions (AEDs) in a detector. The AED is determined by using a Monte Carlo simulation. The results show that the signal-related measures increase with detector thickness. However, the improvement of Swank noise factor with increasing thickness is weak, and this energy-absorption noise characteristic dominates the DQE performance. The energy-absorption noise mainly limits the signal-to-noise performance of CdWO4 detectors operated at megavoltage x-ray beam.

Simultaneous fits in ISIS on the example of GRO J1008-57

NASA Astrophysics Data System (ADS)

Kühnel, Matthias; Müller, Sebastian; Kreykenbohm, Ingo; Schwarm, Fritz-Walter; Grossberger, Christoph; Dauser, Thomas; Pottschmidt, Katja; Ferrigno, Carlo; Rothschild, Richard E.; Klochkov, Dmitry; Staubert, Rüdiger; Wilms, Joern

2015-04-01

Parallel computing and steadily increasing computation speed have led to a new tool for analyzing multiple datasets and datatypes: fitting several datasets simultaneously. With this technique, physically connected parameters of individual data can be treated as a single parameter by implementing this connection into the fit directly. We discuss the terminology, implementation, and possible issues of simultaneous fits based on the X-ray data analysis tool Interactive Spectral Interpretation System (ISIS). While all data modeling tools in X-ray astronomy allow in principle fitting data from multiple data sets individually, the syntax used in these tools is not often well suited for this task. Applying simultaneous fits to the transient X-ray binary GRO J1008-57, we find that the spectral shape is only dependent on X-ray flux. We determine time independent parameters such as, e.g., the folding energy E_fold, with unprecedented precision.

Description of a prototype emission-transmission computed tomography imaging system

NASA Technical Reports Server (NTRS)

Lang, T. F.; Hasegawa, B. H.; Liew, S. C.; Brown, J. K.; Blankespoor, S. C.; Reilly, S. M.; Gingold, E. L.; Cann, C. E.

1992-01-01

We have developed a prototype imaging system that can perform simultaneous x-ray transmission CT and SPECT phantom studies. This system employs a 23-element high-purity-germanium detector array. The detector array is coupled to a collimator with septa angled toward the focal spot of an x-ray tube. During image acquisition, the x-ray fan beam and the detector array move synchronously along an arc pivoted at the x-ray source. Multiple projections are obtained by rotating the object, which is mounted at the center of rotation of the system. The detector array and electronics can count up to 10(6) cps/element with sufficient energy-resolution to discriminate between x-rays at 100-120 kVp and gamma rays from 99mTc. We have used this device to acquire x-ray CT and SPECT images of a three-dimensional Hoffman brain phantom. The emission and transmission images may be superimposed in order to localize the emission image on the transmission map.

Development of cable fed flash X-ray (FXR) system

NASA Astrophysics Data System (ADS)

Menon, Rakhee; Mitra, S.; Patel, A. S.; Kumar, R.; Singh, G.; Senthil, K.; Kumar, Ranjeet; Kolge, T. S.; Roy, Amitava; Acharya, S.; Biswas, D.; Sharma, Archana

2017-08-01

Flash X-ray sources driven by pulsed power find applications in industrial radiography, and a portable X-ray source is ideal where the radiography needs to be taken at the test site. A compact and portable flash X-ray (FXR) system based on a Marx generator has been developed with the high voltage fed to the FXR tube via a cable feed-through arrangement. Hard bremsstrahlung X-rays of few tens of nanosecond duration are generated by impinging intense electron beams on an anode target of high Z material. An industrial X-ray source is developed with source size as low as 1 mm. The system can be operated from 150 kV to 450 kV peak voltages and a dose of 10 mR has been measured at 1 m distance from the source window. The modeling of the FXR source has been carried out using particle-in-cell and Monte Carlo simulations for the electron beam dynamics and X-ray generation, respectively. The angular dose profile of X-ray has been measured and compared with the simulation.

Development of X-ray CCD camera based X-ray micro-CT system

NASA Astrophysics Data System (ADS)

Sarkar, Partha S.; Ray, N. K.; Pal, Manoj K.; Baribaddala, Ravi; Agrawal, Ashish; Kashyap, Y.; Sinha, A.; Gadkari, S. C.

2017-02-01

Availability of microfocus X-ray sources and high resolution X-ray area detectors has made it possible for high resolution microtomography studies to be performed outside the purview of synchrotron. In this paper, we present the work towards the use of an external shutter on a high resolution microtomography system using X-ray CCD camera as a detector. During micro computed tomography experiments, the X-ray source is continuously ON and owing to the readout mechanism of the CCD detector electronics, the detector registers photons reaching it during the read-out period too. This introduces a shadow like pattern in the image known as smear whose direction is defined by the vertical shift register. To resolve this issue, the developed system has been incorporated with a synchronized shutter just in front of the X-ray source. This is positioned in the X-ray beam path during the image readout period and out of the beam path during the image acquisition period. This technique has resulted in improved data quality and hence the same is reflected in the reconstructed images.

Continuing data analysis of the AS/E grazing incidence X-ray telescope experiment on the OSO-4 satellite

NASA Technical Reports Server (NTRS)

Vaiana, G.; Haggerty, R.; Kahler, S.; Krieger, A.; Landini, M.; Timothy, A.; Webb, D.

1973-01-01

The work to correct and extend the calculation of the theoretical solar X-ray spectrum produced during earlier OSO-4 data analysis is reported along with the work to formulate models of active regions, and compare these models with the experimental values. An atlas of solar X-ray photographs is included, and solar X-ray observations are correlated with the solar wind.

21 CFR 1020.30 - Diagnostic x-ray systems and their major components.

Code of Federal Regulations, 2010 CFR

2010-04-01

.... Diagnostic x-ray system means an x-ray system designed for irradiation of any part of the human body for the... HUMAN SERVICES (CONTINUED) RADIOLOGICAL HEALTH PERFORMANCE STANDARDS FOR IONIZING RADIATION EMITTING... for the radiographic visualization and measurement of the dimensions of the human head. Coefficient of...

21 CFR 1020.30 - Diagnostic x-ray systems and their major components.

Code of Federal Regulations, 2011 CFR

2011-04-01

.... Diagnostic x-ray system means an x-ray system designed for irradiation of any part of the human body for the... HUMAN SERVICES (CONTINUED) RADIOLOGICAL HEALTH PERFORMANCE STANDARDS FOR IONIZING RADIATION EMITTING... for the radiographic visualization and measurement of the dimensions of the human head. Coefficient of...

X-ray and neutron interrogation of air cargo for mobile applications

NASA Astrophysics Data System (ADS)

Van Liew, Seth

2015-06-01

A system for scanning break-bulk cargo for mobile applications is presented. This combines a 140 kV multi-view, multi-energy X-ray system with 2.5 MeV neutrons. The system uses dual energy X-ray radiography with neutron radiography. The X-ray and neutron systems were designed to be collocated in a mobile environment. Various materials were interrogated with the intent of distinguishing threat materials such as explosives from similar benign materials. In particular, the identification of threats and bengins with nearly identical effective atomic numbers has been demonstrated.

X-Ray Imaging System

NASA Technical Reports Server (NTRS)

1986-01-01

The FluoroScan Imaging System is a high resolution, low radiation device for viewing stationary or moving objects. It resulted from NASA technology developed for x-ray astronomy and Goddard application to a low intensity x-ray imaging scope. FlouroScan Imaging Systems, Inc, (formerly HealthMate, Inc.), a NASA licensee, further refined the FluoroScan System. It is used for examining fractures, placement of catheters, and in veterinary medicine. Its major components include an x-ray generator, scintillator, visible light image intensifier and video display. It is small, light and maneuverable.

High precision detector robot arm system

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shu, Deming; Chu, Yong

A method and high precision robot arm system are provided, for example, for X-ray nanodiffraction with an X-ray nanoprobe. The robot arm system includes duo-vertical-stages and a kinematic linkage system. A two-dimensional (2D) vertical plane ultra-precision robot arm supporting an X-ray detector provides positioning and manipulating of the X-ray detector. A vertical support for the 2D vertical plane robot arm includes spaced apart rails respectively engaging a first bearing structure and a second bearing structure carried by the 2D vertical plane robot arm.

X-Ray Spectroscopy of Photoionized Plasmas

NASA Technical Reports Server (NTRS)

Kallman, Tim

2008-01-01

Spectroscopy allows study of sources on small spatial scales, and can provide detailed diagnostic information about elemental abundances, temperature, density and gas dynamics. For compact sources such as accreting black holes in active galactic nuclei (AGN) and X-ray binaries X-ray spectra provide truly unique insight. Observations using Chandra and XMM have revealed components of gas in these systems which were previously unknown or poorly studied. Interpretation of these data presents modeling and analysis challenges, and requires an understanding of atomic physics, ionization and spectrum formation in a radiation-dominated environment. In this talk I will discuss examples, and how they have contributed to our understanding of accreting sources and the nearby gas.

Solar X-ray Astronomy Sounding Rocket Program

NASA Technical Reports Server (NTRS)

Moses, J. Daniel

1989-01-01

Several broad objectives were pursued by the development and flight of the High Resolution Soft X-Ray Imaging Sounding Rocket Payload, followed by the analysis of the resulting data and by comparison with both ground based and space based observations from other investigators. The scientific objectives were: to study the thermal equilibrium of active region loop systems by analyzing the X-ray observations to determine electron temperatures, densities, and pressures; by recording the changes in the large scale coronal structures from the maximum and descending phases of Cycle 21 to the ascending phase of Cycle 22; and to extend the study of small scale coronal structures through the minimum of Cycle 21 with new emphasis on correlative observations.

Is scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) quantitative?

PubMed

Newbury, Dale E; Ritchie, Nicholas W M

2013-01-01

Scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) is a widely applied elemental microanalysis method capable of identifying and quantifying all elements in the periodic table except H, He, and Li. By following the "k-ratio" (unknown/standard) measurement protocol development for electron-excited wavelength dispersive spectrometry (WDS), SEM/EDS can achieve accuracy and precision equivalent to WDS and at substantially lower electron dose, even when severe X-ray peak overlaps occur, provided sufficient counts are recorded. Achieving this level of performance is now much more practical with the advent of the high-throughput silicon drift detector energy dispersive X-ray spectrometer (SDD-EDS). However, three measurement issues continue to diminish the impact of SEM/EDS: (1) In the qualitative analysis (i.e., element identification) that must precede quantitative analysis, at least some current and many legacy software systems are vulnerable to occasional misidentification of major constituent peaks, with the frequency of misidentifications rising significantly for minor and trace constituents. (2) The use of standardless analysis, which is subject to much broader systematic errors, leads to quantitative results that, while useful, do not have sufficient accuracy to solve critical problems, e.g. determining the formula of a compound. (3) EDS spectrometers have such a large volume of acceptance that apparently credible spectra can be obtained from specimens with complex topography that introduce uncontrolled geometric factors that modify X-ray generation and propagation, resulting in very large systematic errors, often a factor of ten or more. © Wiley Periodicals, Inc.

Mission planning and scheduling concept for the Advanced X-ray Astrophysics Facility (AXAF)

NASA Technical Reports Server (NTRS)

Newhouse, M.; Guffin, O. T.

1994-01-01

Projected for launch in the latter part of 1998, the Advanced X-ray Astrophysics Facility (AXAF), the third satellite in the Great Observatory series, promises to dramatically open the x-ray sky as the Hubble and Compton observatories have done in their respective realms. Unlike its companions, however, AXAF will be placed in a high altitude, highly elliptical orbit (10,000 x 100,000 km), and will therefore be subject to its own unique environment, spacecraft and science instrument constraints and communication network interactions. In support of this mission, ground operations personnel have embarked on the development of the AXAF Offline System (OFLS), a body of software divided into four basic functional elements: (1) Mission Planning and Scheduling, (2) Command Management, (3) Altitude Determination and Sensor Calibration and (4) Spacecraft Support and Engineering Analysis. This paper presents an overview concept for one of these major elements, the Mission Planning and Scheduling subsystem (MPS). The derivation of this concept is described in terms of requirements driven by spacecraft and science instrument characteristics, orbital environment and ground system capabilities. The flowdown of these requirements through the systems analysis process and the definition of MPS interfaces has resulted in the modular grouping of functional subelements depicted in the design implementation approach. The rationale for this design solution is explained and capabilities for the initial prototype system are proposed from the user perspective.

X-ray transmission movies of spontaneous dynamic events

DOE Office of Scientific and Technical Information (OSTI.GOV)

Smilowitz, L.; Henson, B. F.; Holmes, M.

2014-11-15

We describe a new x-ray radiographic imaging system which allows for continuous x-ray transmission imaging of spontaneous dynamic events. We demonstrate this method on thermal explosions in three plastic bonded formulations of the energetic material octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine. We describe the x-ray imaging system and triggering developed to enable the continuous imaging of a thermal explosion.

Study on nondestructive detection system based on x-ray for wire ropes conveyer belt

NASA Astrophysics Data System (ADS)

Miao, Changyun; Shi, Boya; Wan, Peng; Li, Jie

2008-03-01

A nondestructive detection system based on X-ray for wire ropes conveyer belt is designed by X-ray detection technology. In this paper X-ray detection principle is analyzed, a design scheme of the system is presented; image processing of conveyer belt is researched and image processing algorithms are given; X-ray acquisition receiving board is designed with the use of FPGA and DSP; the software of the system is programmed by C#.NET on WINXP/WIN2000 platform. The experiment indicates the system can implement remote real-time detection of wire ropes conveyer belt images, find faults and give an alarm in time. The system is direct perceived, strong real-time and high accurate. It can be used for fault detection of wire ropes conveyer belts in mines, ports, terminals and other fields.

Accretion Flows in Magnetic White Dwarf Systems

NASA Technical Reports Server (NTRS)

Imamura, James N.

2005-01-01

We received Type A and B funding under the NASA Astrophysics Data Program for the analysis and interpretation of hard x-ray data obtained by the Rossi X-ray Timing Explorer and other NASA sponsored missions for Intermediate Polars (IPS) and Polars. For some targets, optical data was available. We reduced and analyzed the X-ray spectra and the X-ray and optical (obtained at the Cerro Tololo Inter-American Observatory) timing data using detailed shock models (which we constructed) to place constraints on the properties of the accreting white dwarfs, the high energy emission mechanisms of white dwarfs, and the large-scale accretion flows of Polars and IPS. IPS and Polars are white dwarf mass-transfer binaries, members of the larger class of cata,clysmic variables. They differ from the bulk of the cataclysmic variables in that they contain strongly magnetic white dwarfs; the white dwarfs in Polars have B, = 7 to 230 MG and those in IPS have B, less than 10 MG. The IPS and Polars are both examples of funneled accretion flows in strong magnetic field systems. The IPS are similar to x-ray pulsars in that accretion disks form in the systems which are disrupted by the strong stellar magnetic fields of the white dwarfs near the stellar surface from where the plasma is funneled to the surface of the white dwarf. The localized hot spots formed at the footpoints of the funnels coupled with the rotation of the white dwarf leads to coherent pulsed x-ray emission. The Polars offer an example of a different accretion topology; the magnetic field of the white dwarf controls the accretion flow from near the inner Lagrangian point of the system directly to the stellar surface. Accretion disks do not form. The strong magnetic coupling generally leads to synchronous orbital/rotational motion in the Polars. The physical system in this sense resembles the Io/Jupiter system. In both IPS and Polars, pulsed emission from the infrared to x-rays is produced as the funneled flows merge onto the white dwarfs through the formation of strong radiating shock waves. A comparative study of the IPS and Polars can elucidate the primary effects of the magnetic fields on the dynamics and thermodynamics in accreting white dwarf systems.

Cadaveric and in vivo human joint imaging based on differential phase contrast by X-ray Talbot-Lau interferometry.

PubMed

Tanaka, Junji; Nagashima, Masabumi; Kido, Kazuhiro; Hoshino, Yoshihide; Kiyohara, Junko; Makifuchi, Chiho; Nishino, Satoshi; Nagatsuka, Sumiya; Momose, Atsushi

2013-09-01

We developed an X-ray phase imaging system based on Talbot-Lau interferometry and studied its feasibility for clinical diagnoses of joint diseases. The system consists of three X-ray gratings, a conventional X-ray tube, an object holder, an X-ray image sensor, and a computer for image processing. The joints of human cadavers and healthy volunteers were imaged, and the results indicated sufficient sensitivity to cartilage, suggesting medical significance. Copyright © 2012. Published by Elsevier GmbH.

A ROTSE-I/ROSAT Survey of X-ray Emission from Contact Binary Stars

NASA Astrophysics Data System (ADS)

Geske, M.; McKay, T.

2005-05-01

Using public data from the ROSAT All Sky Survey (RASS) and the ROTSE-I Sky Patrols, the incidence of strong x-ray emissions from contact binary systems was examined. The RASS data was matched to an expanded catalog of contact binary systems from the ROTSE-I data, using a 35 arc second radius. X-ray luminosities for matching objects were then determined. This information was then used to evaluate the total x-ray emissions from all such objects, in order to determine their contribution to the galactic x-ray background.

X-ray imaging using avalanche multiplication in amorphous selenium: investigation of intrinsic avalanche noise.

PubMed

Hunt, D C; Tanioka, Kenkichi; Rowlands, J A

2007-12-01

The flat-panel detector (FPD) is the state-of-the-art detector for digital radiography. The FPD can acquire images in real-time, has superior spatial resolution, and is free of the problems of x-ray image intensifiers-veiling glare, pin-cushion and magnetic distortion. However, FPDs suffer from poor signal to noise ratio performance at typical fluoroscopic exposure rates where the quantum noise is reduced to the point that it becomes comparable to the fixed electronic noise. It has been shown previously that avalanche multiplication gain in amorphous selenium (a-Se) can provide the necessary amplification to overcome the electronic noise of the FPD. Avalanche multiplication, however, comes with its own intrinsic contribution to the noise in the form of gain fluctuation noise. In this article a cascaded systems analysis is used to present a modified metric related to the detective quantum efficiency. The modified metric is used to study a diagnostic x-ray imaging system in the presence of intrinsic avalanche multiplication noise independently from other noise sources, such as electronic noise. An indirect conversion imaging system is considered to make the study independent of other avalanche multiplication related noise sources, such as the fluctuations arising from the depth of x-ray absorption. In this case all the avalanche events are initiated at the surface of the avalanche layer, and there are no fluctuations in the depth of absorption. Experiments on an indirect conversion x-ray imaging system using avalanche multiplication in a layer of a-Se are also presented. The cascaded systems analysis shows that intrinsic noise of avalanche multiplication will not have any deleterious influence on detector performance at zero spatial frequency in x-ray imaging provided the product of conversion gain, coupling efficiency, and optical quantum efficiency are much greater than a factor of 2. The experimental results show that avalanche multiplication in a-Se behaves as an intrinsic noise free avalanche multiplication, in accordance with our theory. Provided good coupling efficiency and high optical quantum efficiency are maintained, avalanche multiplication in a-Se has the potential to increase the gain and make negligible contribution to the noise, thereby improving the performance of indirect FPDs in fluoroscopy.

X-ray imaging using avalanche multiplication in amorphous selenium: Investigation of intrinsic avalanche noise

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hunt, D. C.; Tanioka, Kenkichi; Rowlands, J. A.

2007-12-15

The flat-panel detector (FPD) is the state-of-the-art detector for digital radiography. The FPD can acquire images in real-time, has superior spatial resolution, and is free of the problems of x-ray image intensifiers--veiling glare, pin-cushion and magnetic distortion. However, FPDs suffer from poor signal to noise ratio performance at typical fluoroscopic exposure rates where the quantum noise is reduced to the point that it becomes comparable to the fixed electronic noise. It has been shown previously that avalanche multiplication gain in amorphous selenium (a-Se) can provide the necessary amplification to overcome the electronic noise of the FPD. Avalanche multiplication, however, comesmore » with its own intrinsic contribution to the noise in the form of gain fluctuation noise. In this article a cascaded systems analysis is used to present a modified metric related to the detective quantum efficiency. The modified metric is used to study a diagnostic x-ray imaging system in the presence of intrinsic avalanche multiplication noise independently from other noise sources, such as electronic noise. An indirect conversion imaging system is considered to make the study independent of other avalanche multiplication related noise sources, such as the fluctuations arising from the depth of x-ray absorption. In this case all the avalanche events are initiated at the surface of the avalanche layer, and there are no fluctuations in the depth of absorption. Experiments on an indirect conversion x-ray imaging system using avalanche multiplication in a layer of a-Se are also presented. The cascaded systems analysis shows that intrinsic noise of avalanche multiplication will not have any deleterious influence on detector performance at zero spatial frequency in x-ray imaging provided the product of conversion gain, coupling efficiency, and optical quantum efficiency are much greater than a factor of 2. The experimental results show that avalanche multiplication in a-Se behaves as an intrinsic noise free avalanche multiplication, in accordance with our theory. Provided good coupling efficiency and high optical quantum efficiency are maintained, avalanche multiplication in a-Se has the potential to increase the gain and make negligible contribution to the noise, thereby improving the performance of indirect FPDs in fluoroscopy.« less

Digital X-ray camera for quality evaluation three-dimensional topographic reconstruction of single crystals of biological macromolecules

NASA Technical Reports Server (NTRS)

Borgstahl, Gloria (Inventor); Lovelace, Jeff (Inventor); Snell, Edward Holmes (Inventor); Bellamy, Henry (Inventor)

2008-01-01

The present invention provides a digital topography imaging system for determining the crystalline structure of a biological macromolecule, wherein the system employs a charge coupled device (CCD) camera with antiblooming circuitry to directly convert x-ray signals to electrical signals without the use of phosphor and measures reflection profiles from the x-ray emitting source after x-rays are passed through a sample. Methods for using said system are also provided.

PREFACE: Exploring surfaces and buried interfaces of functional materials by advanced x-ray and neutron techniques Exploring surfaces and buried interfaces of functional materials by advanced x-ray and neutron techniques

NASA Astrophysics Data System (ADS)

Sakurai, Kenji

2010-12-01

This special issue is devoted to describing recent applications of x-ray and neutron scattering techniques to the exploration of surfaces and buried interfaces of various functional materials. Unlike many other surface-sensitive methods, these techniques do not require ultra high vacuum, and therefore, a variety of real and complicated surfaces fall within the scope of analysis. It must be particularly emphasized that the techniques are capable of seeing even buried function interfaces as well as the surface. Furthermore, the information, which ranges from the atomic to mesoscopic scale, is highly quantitative and reproducible. The non-destructive nature of the techniques is another important advantage of using x-rays and neutrons, when compared with other atomic-scale analyses. This ensures that the same specimen can be measured by other techniques. Such features are fairly attractive when exploring multilayered materials with nanostructures (dots, tubes, wires, etc), which are finding applications in electronic, magnetic, optical and other devices. The Japan Applied Physics Society has established a group to develop the research field of studying buried function interfaces with x-rays and neutrons. As the methods can be applied to almost all types of materials, from semiconductor and electronic devices to soft materials, participants have fairly different backgrounds but share a common interest in state-of-the-art x-ray and neutron techniques and sophisticated applications. A series of workshops has been organized almost every year since 2001. Some international interactions have been continued intensively, although the community is part of a Japanese society. This special issue does not report the proceedings of the recent workshop, although all the authors are in some way involved in the activities of the above society. Initially, we intended to collect quite long overview papers, including the authors' latest and most important original results, as well as updates on recent progress and global trends in the field. We planned to cover quite a wide area of surface and buried interface science with x-rays and neutrons. Following a great deal of discussion during the editing process, we have decided to change direction. As we intend to publish similar special issues on a frequent basis, we will not insist on editing this issue as systematic and complete collections of research. Many authors decided to write an ordinary research paper rather than an article including systematic accounts. Due to this change in policy, some authors declined to contribute, and the number of papers is now just 12. However, readers will find that the special issue gives an interesting collection of new original research in surface and buried interface studies with x-rays and neutrons. The 12 papers cover the following research topics: (1) polymer analysis by diffuse scattering; (2) discussion of the electrochemical solid--liquid interface by synchrotron x-ray diffraction; (3) analysis of capped nanodots by grazing incidence small-angle x-ray scattering (GISAXS); (4) discussion of the strain distribution in silicon by high-resolution x-ray diffraction; (5) study of mesoporous structures by a combination of x-ray reflectivity and GISAXS; (6) discussion of energy-dispersive x-ray reflectometry and its applications; (7) neutron reflectivity studies on hydrogen terminated silicon interface; (8) the fabrication and performance of a special mirror for water windows; (9) depth selective analysis by total-reflection x-ray diffraction; (10) nanoparticle thin films prepared by a gas deposition technique; (11) discussion of crystal truncation rod (CTR) scattering of semiconductor nanostructures; (12) magnetic structure analysis of thin films by polarized neutron reflectivity. While not discussed in the present special issue, x-ray and neutron techniques have made great progress. The most important steps forward have been in 2D/3D real-space imaging, and realtime measurement. Advances in such technologies are bringing with them new opportunities in surface and buried interface science. In the not too distant future, we will publish a special issue or a book detailing such progress. Exploring surfaces and buried interfaces of functional materials by advanced x-ray and neutron techniques contents Lateral uniformity in chemical composition along a buried reaction front in polymers using off-specular reflectivity Kristopher A Lavery, Vivek M Prabhu, Sushil Satija and Wen-li Wu Orientation dependence of Pd growth on Au electrode surfaces M Takahasi, K Tamura, J Mizuki, T Kondo and K Uosaki A grazing incidence small-angle x-ray scattering analysis on capped Ge nanodots in layer structures Hiroshi Okuda, Masayuki Kato, Keiji Kuno, Shojiro Ochiai, Noritaka Usami, Kazuo Nakajima and Osami Sakata High resolution grazing-incidence in-plane x-ray diffraction for measuring the strain of a Si thin layer Kazuhiko Omote X-ray analysis of mesoporous silica thin films templated by Brij58 surfactant S Fall, M Kulij and A Gibaud Review of the applications of x-ray refraction and the x-ray waveguide phenomenon to estimation of film structures Kouichi Hayashi Epitaxial growth of largely mismatched crystals on H-terminated Si(111) surfaces Hidehito Asaoka Novel TiO2/ZnO multilayer mirrors at 'water-window' wavelengths fabricated by atomic layer epitaxy H Kumagai, Y Tanaka, M Murata, Y Masuda and T Shinagawa Depth-selective structural analysis of thin films using total-external-reflection x-ray diffraction Tomoaki Kawamura and Hiroo Omi Structures of Yb nanoparticle thin films grown by deposition in He and N2 gas atmospheres: AFM and x-ray reflectivity studies Martin Jerab and Kenji Sakurai Ga and As composition profiles in InP/GaInAs/InP heterostructures—x-ray CTR scattering and cross-sectional STM measurements Yoshikazu Takeda, Masao Tabuchi and Arao Nakamura Polarized neutron reflectivity study of a thermally treated MnIr/CoFe exchange bias system Naoki Awaji, Toyoo Miyajima, Shuuichi Doi and Kenji Nomura

[Study on spectrum analysis of X-ray based on rotational mass effect in special relativity].

PubMed

Yu, Zhi-Qiang; Xie, Quan; Xiao, Qing-Quan

2010-04-01

Based on special relativity, the formation mechanism of characteristic X-ray has been studied, and the influence of rotational mass effect on X-ray spectrum has been given. A calculation formula of the X-ray wavelength based upon special relativity was derived. Error analysis was carried out systematically for the calculation values of characteristic wavelength, and the rules of relative error were obtained. It is shown that the values of the calculation are very close to the experimental values, and the effect of rotational mass effect on the characteristic wavelength becomes more evident as the atomic number increases. The result of the study has some reference meaning for the spectrum analysis of characteristic X-ray in application.

The BL LAC phenomenon: X-ray observations of transition objects and determination of the x-ray spectrum of a complete sample of flat-spectrum radio sources

NASA Technical Reports Server (NTRS)

Worrall, Diana M.

1994-01-01

This report summarizes the activities related to two ROSAT investigations: (1) x-ray properties of radio galaxies thought to contain BL Lac type nuclei; and (2) x-ray spectra of a complete sample of flat-spectrum radio sources. The following papers describing the research are provided as attachments: Multiple X-ray Emission Components in Low Power Radio Galaxies; New X-ray Results on Radio Galaxies; Analysis Techniques for a Multiwavelength Study of Radio Galaxies; Separation of X-ray Emission Components in Radio Galaxies; X-ray Emission in Powerful Radio Galaxies and Quasars; Extended and Compact X-ray Emission in Powerful Radio Galaxies; and X-ray Spectra of a Complete Sample of Extragalactic Core-dominated Radio Sources.

In-depth study of long-term variability in the X-ray emission of the Be/X-ray binary system AX J0049.4-7323

NASA Astrophysics Data System (ADS)

Ducci, L.; Romano, P.; Malacaria, C.; Ji, L.; Bozzo, E.; Santangelo, A.

2018-06-01

AX J0049.4-7323 is a Be/X-ray binary in the Small Magellanic Cloud hosting a 750 s pulsar which has been observed over the last 17 years by several X-ray telescopes. Despite numerous observations, little is known about its X-ray behaviour. Therefore, we coherently analysed archival Swift, Chandra, XMM-Newton, RXTE, and INTEGRAL data, and we compared them with already published ASCA data, to study its X-ray long-term spectral and flux variability. AX J0049.4-7323 shows a high X-ray variability, spanning more than three orders of magnitudes, from L ≈ 1.6 × 1037 erg s-1 (0.3-8 keV, d = 62 kpc) down to L ≈ 8 × 1033 erg s-1. RXTE, Chandra, Swift, and ASCA observed, in addition to the expected enhancement of X-ray luminosity at periastron, flux variations by a factor of 270 with peak luminosities of ≈2.1 × 1036 erg s-1 far from periastron. These properties are difficult to reconcile with the typical long-term variability of Be/XRBs, traditionally interpreted in terms of type I and type II outbursts. The study of AX J0049.4-7323 is complemented with a spectral analysis of Swift, Chandra, and XMM-Newton data which showed a softening trend when the emission becomes fainter, and an analysis of optical/UV data collected by the UVOT telescope on board Swift. In addition, we measured a secular spin-up rate of Ṗ = (-3.00 ± 0.12) × 10-3 s day-1, which suggests that the pulsar has not yet achieved its equilibrium period. Assuming spherical accretion, we estimated an upper limit for the magnetic field strength of the pulsar of ≈3 × 1012 G.

Development Of A Flash X-Ray Scanner For Stereoradiography And CT

NASA Astrophysics Data System (ADS)

Endorf, Robert J.; DiBianca, Frank A.; Fritsch, Daniel S.; Liu, Wen-Ching; Burns, Charles B.

1989-05-01

We are developing a flash x-ray scanner for stereoradiography and CT which will be able to produce a stereoradiograph in 30 to 70 ns and a complete CT scan in one microsecond. This type of imaging device will be valuable in studying high speed processes, high acceleration, and traumatic events. We have built a two channel flash x-ray system capable of producing stereo radiographs with stereo angles of from 15 to 165 degrees. The dynamic and static Miff 's for the flash x-ray system were measured and compared with similar MIT's measured for a conventional medical x-ray system. We have written and tested a stereo reconstruction algorithm to determine three dimensional space points from corresponding points in the two stereo images. To demonstrate the ability of the system to image traumatic events, a radiograph was obtained of a bone undergoing a fracture. The effects of accelerations of up to 600 g were examined on radiographs taken of human kidney tissue samples in a rapidly rotating centrifuge. Feasibility studies of CT reconstruction have been performed by making simulated Cr images of various phantoms for larger flash x-ray systems of from 8 to 29 flash x-ray tubes.

A novel biometric X-ray backscatter inspection of dangerous materials based on a lobster-eye objective

NASA Astrophysics Data System (ADS)

Xu, Jie; Wang, Xin; Mu, Baozhong; Zhan, Qi; Xie, Qing; Li, Yaran; Chen, Yifan; He, Yanan

2016-10-01

In order to counter drug-related crimes effectively, and to safeguard homeland security as well as public safety, it is important to inspect drugs, explosives and other contraband quickly and accurately from the express mail system, luggage, vehicles and other objects. In this paper, we discuss X-ray backscatter inspection system based on a novel lobster-eye X-ray objective, which is an effective inspection technology for drugs, explosives and other contraband inspection. Low atomic number materials, such as drugs and explosives, leads to strong Compton scattering after irradiated by X-ray, which is much stronger than high atomic number material, such as common metals, etc. By detecting the intensity of scattering signals, it is possible to distinguish between organics and inorganics. The lobster-eye X-ray optical system imitates the reflective eyes of lobsters, which field of view can be made as large as desired and it is practical to achieve spatial resolution of several millimeters for finite distance detection. A novel lobster-eye X-ray objective is designed based on modifying Schmidt geometry by using multi-lens structure, so as to reduce the difference of resolution between the horizontal and vertical directions. The demonstration experiments of X-ray backscattering imaging were carried out. A suitcase, a wooden box and a tire with several typical samples hidden in them were imaged by the X-ray backscattering inspection system based on a lobster-eye X-ray objective. The results show that this X-ray backscattering inspection system can get a resolution of less than five millimeters under the FOV of more than two hundred millimeters with 0.5 meter object distance, which can still be improved.

Discovery of X-Ray Emission from the Galactic Supernova Remnant G32.8-0.1 with Suzaku

NASA Technical Reports Server (NTRS)

Bamba, Aya; Terada, Yukikatsu; Hewitt, John; Petre, Robert; Angelini, Lorella; Safi-Harb, Samar; Zhou, Ping; Bocchino, Fabrizio; Sawada, Makoto

2016-01-01

We present the first dedicated X-ray study of the supernova remnant (SNR) G32.8-0.1 (Kes 78) with Suzaku. X-ray emission from the whole SNR shell has been detected for the first time. The X-ray morphology is well correlated with the emission from the radio shell, while anti-correlated with the molecular cloud found in the SNR field. The X-ray spectrum shows not only conventional low-temperature (kT approximately 0.6 kiloelectronvolts) thermal emission in a nonequilibrium ionization state, but also a very high-temperature (approximately 3.4 kiloelectronvolts) component with a very low ionization timescale (approximately 2.7 times 10 (sup 9) per cubic centimeter per second), or a hard nonthermal component with a photon index Gamma approximately equal to 2.3. The average density of the low-temperature plasma is rather low, of the order of 10 (sup -3) - 10 (sup -2) per cubic centimeter, implying that this SNR is expanding into a low-density cavity. We discuss the X-ray emission of the SNR, also detected in teraelectronvolts with H.E.S.S. (High Energy Stereoscopic System), together with multi-wavelength studies of the remnant and other gamma-ray emitting SNRs, such as W28 and RCW 86. Analysis of a time-variable source, 2XMM J185114.3-000004, found in the northern part of the SNR, is also reported for the first time. Rapid time variability and a heavily absorbed hard-X-ray spectrum suggest that this source could be a new supergiant fast X-ray transient.

The Chandra Source Catalog

NASA Astrophysics Data System (ADS)

Evans, Ian; Primini, Francis A.; Glotfelty, Kenny J.; Anderson, Craig S.; Bonaventura, Nina R.; Chen, Judy C.; Davis, John E.; Doe, Stephen M.; Evans, Janet D.; Fabbiano, Giuseppina; Galle, Elizabeth C.; Gibbs, Danny G., II; Grier, John D.; Hain, Roger; Hall, Diane M.; Harbo, Peter N.; He, Xiang Qun (Helen); Houck, John C.; Karovska, Margarita; Kashyap, Vinay L.; Lauer, Jennifer; McCollough, Michael L.; McDowell, Jonathan C.; Miller, Joseph B.; Mitschang, Arik W.; Morgan, Douglas L.; Mossman, Amy E.; Nichols, Joy S.; Nowak, Michael A.; Plummer, David A.; Refsdal, Brian L.; Rots, Arnold H.; Siemiginowska, Aneta L.; Sundheim, Beth A.; Tibbetts, Michael S.; van Stone, David W.; Winkelman, Sherry L.; Zografou, Panagoula

2009-09-01

The first release of the Chandra Source Catalog (CSC) was published in 2009 March, and includes information about 94,676 X-ray sources detected in a subset of public ACIS imaging observations from roughly the first eight years of the Chandra mission. This release of the catalog includes point and compact sources with observed spatial extents <˜30''.The CSC is a general purpose virtual X-ray astrophysics facility that provides access to a carefully selected set of generally useful quantities for individual X-ray sources, and is designed to satisfy the needs of a broad-based group of scientists, including those who may be less familiar with astronomical data analysis in the X-ray regime.The catalog (1) provides access to the best estimates of the X-ray source properties for detected sources, with good scientific fidelity, and directly supports medium sophistication scientific analysis on using the individual source data; (2) facilitates analysis of a wide range of statistical properties for classes of X-ray sources; (3) provides efficient access to calibrated observational data and ancillary data products for individual X-ray sources, so that users can perform detailed further analysis using existing tools; and (4) includes real X-ray sources detected with flux significance greater than a predefined threshold, while maintaining the number of spurious sources at an acceptable level. For each detected X-ray source, the CSC provides commonly tabulated quantities, including source position, extent, multi-band fluxes, hardness ratios, and variability statistics, derived from the observations in which the source is detected. In addition to these traditional catalog elements, for each X-ray source the CSC includes an extensive set of file-based data products that can be manipulated interactively, including source images, event lists, light curves, and spectra from each observation in which a source is detected.

Radiation dose and magnification in pelvic X-ray: EOS™ imaging system versus plain radiographs.

PubMed

Chiron, P; Demoulin, L; Wytrykowski, K; Cavaignac, E; Reina, N; Murgier, J

2017-12-01

In plain pelvic X-ray, magnification makes measurement unreliable. The EOS™ (EOS Imaging, Paris France) imaging system is reputed to reproduce patient anatomy exactly, with a lower radiation dose. This, however, has not been assessed according to patient weight, although both magnification and irradiation are known to vary with weight. We therefore conducted a prospective comparative study, to compare: (1) image magnification and (2) radiation dose between the EOS imaging system and plain X-ray. The EOS imaging system reproduces patient anatomy exactly, regardless of weight, unlike plain X-ray. A single-center comparative study of plain pelvic X-ray and 2D EOS radiography was performed in 183 patients: 186 arthroplasties; 104 male, 81 female; mean age 61.3±13.7years (range, 24-87years). Magnification and radiation dose (dose-area product [DAP]) were compared between the two systems in 186 hips in patients with a mean body-mass index (BMI) of 27.1±5.3kg/m 2 (range, 17.6-42.3kg/m 2 ), including 7 with morbid obesity. Mean magnification was zero using the EOS system, regardless of patient weight, compared to 1.15±0.05 (range, 1-1.32) on plain X-ray (P<10 -5 ). In patients with BMI<25, mean magnification on plain X-ray was 1.15±0.05 (range, 1-1.25) and, in patients with morbid obesity, 1.22±0.06 (range, 1.18-1.32). The mean radiation dose was 8.19±2.63dGy/cm 2 (range, 1.77-14.24) with the EOS system, versus 19.38±12.37dGy/cm 2 (range, 4.77-81.75) with plain X-ray (P<10 -4 ). For BMI >40, mean radiation dose was 9.36±2.57dGy/cm 2 (range, 7.4-14.2) with the EOS system, versus 44.76±22.21 (range, 25.2-81.7) with plain X-ray. Radiation dose increased by 0.20dGy with each extra BMI point for the EOS system, versus 0.74dGy for plain X-ray. Magnification did not vary with patient weight using the EOS system, unlike plain X-ray, and radiation dose was 2.5-fold lower. 3, prospective case-control study. Copyright © 2017 Elsevier Masson SAS. All rights reserved.

X-Ray Variation Statistics and Wind Clumping in Vela X-1

NASA Technical Reports Server (NTRS)

Furst, Felix; Kreykenbohm, Ingo; Pottschmidt, Katja; Wilms, Joern; Hanke, Manfred; Rothschild, Richard E.; Kretschmar, Peter; Schulz, Norbert S.; Huenemoerder, David P.; Klochkov, Dmitry;

Investigating the galactic Supernova Remnant Kes 78 with XMM-Newton

NASA Astrophysics Data System (ADS)

Miceli, M.; Bamba, A.; Orlando, S.; Bocchino, F.

2016-06-01

The galactic supernova remnant Kes 78 is associated with a HESS gamma-ray source and its X-ray emission has been recently revealed by Suzaku observations which have found indications for a hard X-ray component in the spectra. We analyzed an XMM-Newton EPIC observation of Kes 78 and studied the spatial distribution of the physical and chemical properties of the X-ray emitting plasma. The EPIC data unveiled a very complex morphology for the soft X-ray emission. We performed image analysis and spatially resolved spectral analysis finding indications for the interaction of the remnant with a local molecular cloud. Finally, we investigated the origin of the hard X-ray emitting component.

Investigating the Galactic supernova remnant Kes 78 with XMM-Newton

NASA Astrophysics Data System (ADS)

Miceli, Marco; Bamba, Aya; Orlando, Salvatore; Bocchino, Fabrizio

2016-06-01

The galactic supernova remnant Kes 78 is associated with a HESS gamma-ray source and its X-ray emission has been recently revealed by Suzaku observations which have found indications for a hard X-ray component in the spectra. We analyzed an XMM-Newton EPIC observation of Kes 78 and studied the spatial distribution of the physical and chemical properties of the X-ray emitting plasma. The EPIC data unveiled a very complex morphology for the soft X-ray emission. We performed image analysis and spatially resolved spectral analysis finding indications for the interaction of the remnant with a local molecular cloud. Finally, we investigated the origin of the hard X-ray emitting component.

Long, elliptically bent, active X-ray mirrors with slope errors <200 nrad.

PubMed

Nistea, Ioana T; Alcock, Simon G; Kristiansen, Paw; Young, Adam

2017-05-01

Actively bent X-ray mirrors are important components of many synchrotron and X-ray free-electron laser beamlines. A high-quality optical surface and good bending performance are essential to ensure that the X-ray beam is accurately focused. Two elliptically bent X-ray mirror systems from FMB Oxford were characterized in the optical metrology laboratory at Diamond Light Source. A comparison of Diamond-NOM slope profilometry and finite-element analysis is presented to investigate how the 900 mm-long mirrors sag under gravity, and how this deformation can be adequately compensated using a single, spring-loaded compensator. It is shown that two independent mechanical actuators can accurately bend the trapezoidal substrates to a range of elliptical profiles. State-of-the-art residual slope errors of <200 nrad r.m.s. are achieved over the entire elliptical bending range. High levels of bending repeatability (ΔR/R = 0.085% and 0.156% r.m.s. for the two bending directions) and stability over 24 h (ΔR/R = 0.07% r.m.s.) provide reliable beamline performance.

PSPC soft x-ray observations of Seyfert 2 galaxies

NASA Technical Reports Server (NTRS)

Turner, T. J.; Urry, C. M.; Mushotzky, R. F.

1993-01-01

We present the results from ROSAT PSPC soft x-ray (0.1-2.0 keV) observations of six Seyfert 2 galaxies, chosen from the brightest Seyfert 2s detected with the Einstein Imaging Proportional Counter. All of the targets were detected with the ROSAT PSPC. Spatial analysis shows that the source density within a few arcmin of each Seyfert 2 galaxy is a factor of approximately eight higher than in the rest of the inner field of view of the PSPC images. In NGC1365 it appears that the serendipitous sources may be x-ray binary systems in the host galaxy. The proximity of the serendipitous sources, typically within a few arcmin of the target Seyfert 2, means that previous x-ray observations of the Seyfert 2 galaxies have been significantly contaminated, and that source confusion is important on a spatial scale of approximately 1 arcmin. Some spectra, most notably Mrk3 and NGC1365, indicate the presence of a high equivalent width soft x-ray line blend consistent with unresolved iron L and oxygen K emission.

X-ray fluorescence microscopy artefacts in elemental maps of topologically complex samples: Analytical observations, simulation and a map correction method

NASA Astrophysics Data System (ADS)

Billè, Fulvio; Kourousias, George; Luchinat, Enrico; Kiskinova, Maya; Gianoncelli, Alessandra

2016-08-01

XRF spectroscopy is among the most widely used non-destructive techniques for elemental analysis. Despite the known angular dependence of X-ray fluorescence (XRF), topological artefacts remain an unresolved issue when using X-ray micro- or nano-probes. In this work we investigate the origin of the artefacts in XRF imaging of topologically complex samples, which are unresolved problems in studies of organic matter due to the limited travel distances of low energy XRF emission from the light elements. In particular we mapped Human Embryonic Kidney (HEK293T) cells. The exemplary results with biological samples, obtained with a soft X-ray scanning microscope installed at a synchrotron facility were used for testing a mathematical model based on detector response simulations, and for proposing an artefact correction method based on directional derivatives. Despite the peculiar and specific application, the methodology can be easily extended to hard X-rays and to set-ups with multi-array detector systems when the dimensions of surface reliefs are in the order of the probing beam size.

Microanalysis of iron oxidation state in iron oxides using X Ray Absorption Near Edge Structure (XANES)

NASA Technical Reports Server (NTRS)

Sutton, S. R.; Delaney, J.; Bajt, S.; Rivers, M. L.; Smith, J. V.

1993-01-01

An exploratory application of x ray absorption near edge structure (XANES) analysis using the synchrotron x ray microprobe was undertaken to obtain Fe XANES spectra on individual sub-millimeter grains in conventional polished sections. The experiments concentrated on determinations of Fe valence in a suite of iron oxide minerals for which independent estimates of the iron speciation could be made by electron microprobe analysis and x ray diffraction.

Calcium measurements with electron probe X-ray and electron energy loss analysis.

PubMed

LeFurgey, A; Ingram, P

1990-03-01

This paper presents a broad survey of the rationale for electron probe X-ray microanalysis (EPXMA) and the various methods for obtaining qualitative and quantitative information on the distribution and amount of elements, particularly calcium, in cryopreserved cells and tissues. Essential in an introductory consideration of microanalysis in biological cryosections is the physical basis for the instrumentation, fundamentals of X-ray spectrometry, and various analytical modes such as static probing and X-ray imaging. Some common artifacts are beam damage and contamination. Inherent pitfalls of energy dispersive X-ray systems include Si escape peaks, doublets, background, and detector calibration shifts. Quantitative calcium analysis of thin cryosections is carried out in real time using a multiple least squares fitting program on filtered X-ray spectra and normalizing the calcium peak to a portion of the continuum. Recent work includes the development of an X-ray imaging system where quantitative data can be retrieved off-line. The minimum detectable concentration of calcium in biological cryosections is approximately 300 mumole kg dry weight with a spatial resolution of approximately 100 A. The application of electron energy loss (EELS) techniques to the detection of calcium offers the potential for greater sensitivity and spatial resolution in measurement and imaging. Determination of mass thickness with EELS can facilitate accurate calculation of wet weight concentrations from frozen hydrated and freeze-dried specimens. Calcium has multiple effects on cell metabolism, membrane transport and permeability and, thus, on overall cell physiology or pathophysiology. Cells can be rapidly frozen for EPXMA during basal or altered functional conditions to delineate the location and amount of calcium within cells and the changes in location and concentration of cations or anions accompanying calcium redistribution. Recent experiments in our laboratory document that EPXMA in combination with other biochemical and electrophysiological techniques can be used to study, for example, sodium and calcium compartmentation in cultured cardiac cells. Such analyses can also be used to clarify the role of calcium in anoxic renal cell injury and to evaluate proposed ionic defects in cells of individuals with cystic fibrosis.

A Control System and Streaming DAQ Platform with Image-Based Trigger for X-ray Imaging

NASA Astrophysics Data System (ADS)

Stevanovic, Uros; Caselle, Michele; Cecilia, Angelica; Chilingaryan, Suren; Farago, Tomas; Gasilov, Sergey; Herth, Armin; Kopmann, Andreas; Vogelgesang, Matthias; Balzer, Matthias; Baumbach, Tilo; Weber, Marc

2015-06-01

High-speed X-ray imaging applications play a crucial role for non-destructive investigations of the dynamics in material science and biology. On-line data analysis is necessary for quality assurance and data-driven feedback, leading to a more efficient use of a beam time and increased data quality. In this article we present a smart camera platform with embedded Field Programmable Gate Array (FPGA) processing that is able to stream and process data continuously in real-time. The setup consists of a Complementary Metal-Oxide-Semiconductor (CMOS) sensor, an FPGA readout card, and a readout computer. It is seamlessly integrated in a new custom experiment control system called Concert that provides a more efficient way of operating a beamline by integrating device control, experiment process control, and data analysis. The potential of the embedded processing is demonstrated by implementing an image-based trigger. It records the temporal evolution of physical events with increased speed while maintaining the full field of view. The complete data acquisition system, with Concert and the smart camera platform was successfully integrated and used for fast X-ray imaging experiments at KIT's synchrotron radiation facility ANKA.

Spherical grating based x-ray Talbot interferometry.

PubMed

Cong, Wenxiang; Xi, Yan; Wang, Ge

2015-11-01

Grating interferometry is a state-of-the-art x-ray imaging approach, which can acquire information on x-ray attenuation, phase shift, and small-angle scattering simultaneously. Phase-contrast imaging and dark-field imaging are very sensitive to microstructural variation and offers superior contrast resolution for biological soft tissues. However, a common x-ray tube is a point-like source. As a result, the popular planar grating imaging configuration seriously restricts the flux of photons and decreases the visibility of signals, yielding a limited field of view. The purpose of this study is to extend the planar x-ray grating imaging theory and methods to a spherical grating scheme for a wider range of preclinical and clinical applications. A spherical grating matches the wave front of a point x-ray source very well, allowing the perpendicular incidence of x-rays on the grating to achieve a higher visibility over a larger field of view than the planer grating counterpart. A theoretical analysis of the Talbot effect for spherical grating imaging is proposed to establish a basic foundation for x-ray spherical gratings interferometry. An efficient method of spherical grating imaging is also presented to extract attenuation, differential phase, and dark-field images in the x-ray spherical grating interferometer. Talbot self-imaging with spherical gratings is analyzed based on the Rayleigh-Sommerfeld diffraction formula, featuring a periodic angular distribution in a polar coordinate system. The Talbot distance is derived to reveal the Talbot self-imaging pattern. Numerical simulation results show the self-imaging phenomenon of a spherical grating interferometer, which is in agreement with the theoretical prediction. X-ray Talbot interferometry with spherical gratings has a significant practical promise. Relative to planar grating imaging, spherical grating based x-ray Talbot interferometry has a larger field of view and improves both signal visibility and dose utilization for pre-clinical and clinical applications.

Spherical grating based x-ray Talbot interferometry

PubMed Central

Cong, Wenxiang; Xi, Yan; Wang, Ge

2015-01-01

Purpose: Grating interferometry is a state-of-the-art x-ray imaging approach, which can acquire information on x-ray attenuation, phase shift, and small-angle scattering simultaneously. Phase-contrast imaging and dark-field imaging are very sensitive to microstructural variation and offers superior contrast resolution for biological soft tissues. However, a common x-ray tube is a point-like source. As a result, the popular planar grating imaging configuration seriously restricts the flux of photons and decreases the visibility of signals, yielding a limited field of view. The purpose of this study is to extend the planar x-ray grating imaging theory and methods to a spherical grating scheme for a wider range of preclinical and clinical applications. Methods: A spherical grating matches the wave front of a point x-ray source very well, allowing the perpendicular incidence of x-rays on the grating to achieve a higher visibility over a larger field of view than the planer grating counterpart. A theoretical analysis of the Talbot effect for spherical grating imaging is proposed to establish a basic foundation for x-ray spherical gratings interferometry. An efficient method of spherical grating imaging is also presented to extract attenuation, differential phase, and dark-field images in the x-ray spherical grating interferometer. Results: Talbot self-imaging with spherical gratings is analyzed based on the Rayleigh–Sommerfeld diffraction formula, featuring a periodic angular distribution in a polar coordinate system. The Talbot distance is derived to reveal the Talbot self-imaging pattern. Numerical simulation results show the self-imaging phenomenon of a spherical grating interferometer, which is in agreement with the theoretical prediction. Conclusions: X-ray Talbot interferometry with spherical gratings has a significant practical promise. Relative to planar grating imaging, spherical grating based x-ray Talbot interferometry has a larger field of view and improves both signal visibility and dose utilization for pre-clinical and clinical applications. PMID:26520741

Spherical grating based x-ray Talbot interferometry

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cong, Wenxiang, E-mail: congw@rpi.edu, E-mail: xiy2@rpi.edu, E-mail: wangg6@rpi.edu; Xi, Yan, E-mail: congw@rpi.edu, E-mail: xiy2@rpi.edu, E-mail: wangg6@rpi.edu; Wang, Ge, E-mail: congw@rpi.edu, E-mail: xiy2@rpi.edu, E-mail: wangg6@rpi.edu

2015-11-15

Purpose: Grating interferometry is a state-of-the-art x-ray imaging approach, which can acquire information on x-ray attenuation, phase shift, and small-angle scattering simultaneously. Phase-contrast imaging and dark-field imaging are very sensitive to microstructural variation and offers superior contrast resolution for biological soft tissues. However, a common x-ray tube is a point-like source. As a result, the popular planar grating imaging configuration seriously restricts the flux of photons and decreases the visibility of signals, yielding a limited field of view. The purpose of this study is to extend the planar x-ray grating imaging theory and methods to a spherical grating scheme formore » a wider range of preclinical and clinical applications. Methods: A spherical grating matches the wave front of a point x-ray source very well, allowing the perpendicular incidence of x-rays on the grating to achieve a higher visibility over a larger field of view than the planer grating counterpart. A theoretical analysis of the Talbot effect for spherical grating imaging is proposed to establish a basic foundation for x-ray spherical gratings interferometry. An efficient method of spherical grating imaging is also presented to extract attenuation, differential phase, and dark-field images in the x-ray spherical grating interferometer. Results: Talbot self-imaging with spherical gratings is analyzed based on the Rayleigh–Sommerfeld diffraction formula, featuring a periodic angular distribution in a polar coordinate system. The Talbot distance is derived to reveal the Talbot self-imaging pattern. Numerical simulation results show the self-imaging phenomenon of a spherical grating interferometer, which is in agreement with the theoretical prediction. Conclusions: X-ray Talbot interferometry with spherical gratings has a significant practical promise. Relative to planar grating imaging, spherical grating based x-ray Talbot interferometry has a larger field of view and improves both signal visibility and dose utilization for pre-clinical and clinical applications.« less

Comparison of two portable solid state detectors with an improved collimation and alignment device for mammographic x-ray spectroscopy.

PubMed

Bottigli, U; Golosio, B; Masala, G L; Oliva, P; Stumbo, S; Delogu, P; Fantacci, M E; Abbene, L; Fauci, F; Raso, G

2006-09-01

We describe a portable system for mammographic x-ray spectroscopy, based on a 2 X 2 X 1 mm3 cadmium telluride (CdTe) solid state detector, that is greatly improved over a similar system based on a 3 X 3 X 2 mm3 cadmium zinc telluride (CZT) solid state detector evaluated in an earlier work. The CdTe system utilized new pinhole collimators and an alignment device that facilitated measurement of mammographic x-ray spectra. Mammographic x-ray spectra acquired by each system were comparable. Half value layer measurements obtained using an ion chamber agreed closely with those derived from the x-ray spectra measured by either detector. The faster electronics and other features of the CdTe detector allowed its use with a larger pinhole collimator than could be used with the CZT detector. Additionally, the improved pinhole collimator and alignment features of the apparatus permitted much more rapid setup for acquisition of x-ray spectra than was possible on the system described in the earlier work. These improvements in detector technology, collimation and ease of alignment, as well as low cost, make this apparatus attractive as a tool for both laboratory research and advanced mammography quality control.

On the stability of the zinc x-ray laser beam quality using a half cavity

NASA Astrophysics Data System (ADS)

Prag, A. R.; Mocek, T.; Kozlova, M.; Rus, B.

2002-11-01

At the Prague Asterix Laser System Center (PALS) the Asterix laser delivering up to 700 J in 0.5 ns is used as a pump source for x-ray laser experiments and applications. The prepulse technique was applied which is known to improve the neon-like x-ray laser at the J = 0 - 1 transition dramatically. Since Zn slab targets were used the output wavelength was 21.2 nm. A prepulse having up to 20 J precedes the main pulse by 10 ns. The main beam and the prepulse beam are focussed by two different optical systems separately and their foci are superimposed at the target surface. By implementing a half-cavity for double-pass amplification using a Mo/Si multilayer mirror - which can be used for 100 shots - the x-ray laser output was more than 10 times stronger than at the single pass in a 3 cm long plasma. Double-pass amplification was observed to be most efficient when the pump pulse was at least 150 ps longer than the round trip time (approximately 260 ps) in the half-cavity. Under this fundamental condition the x-ray laser reached saturation in the double-pass regime containing approx4mJ energy which was proved to be enough for applications. In this contribution, the x-ray laser features like divergence in two dimensions, the beam quality (symmetry), and the pointing angle are investigated over 110 shots. To characterize the stability of the x-ray laser the shot distribution, the mean value and the standard deviation for these parameters are evaluated. For 18 shots of a one-day-series these values are given, and a statistical analysis carrying out a chi-squared test characterize the Zn x-ray laser as a robust tool suitable for future applications.

Optical Photometry and X-Ray Monitoring of the ``Cool Algol'' BD +05°706: Determination of the Physical Properties

NASA Astrophysics Data System (ADS)

Torres, Guillermo; Mader, Jeff A.; Marschall, Laurence A.; Neuhäuser, Ralph; Duffy, Alaine S.

2003-06-01

We present new photometric observations in the BVRI bands of the double-lined eclipsing binary BD +05°706 conducted over three observing seasons, as well as new X-ray observations obtained with ROSAT covering a full orbital cycle (P=18.9 days). A detailed light-curve analysis of the optical data shows the system to be semidetached, confirming indications from an earlier analysis by Torres et al. (published in 1998), with the less massive and cooler star filling its Roche lobe. The system is a member of the rare class of cool Algol systems, which are different from the ``classical'' Algol systems in that the mass-gaining component is also a late-type star rather than a B- or A-type star. By combining the new photometry with a reanalysis of the spectroscopic observations reported by Torres et al., we derive accurate absolute masses for the components of M1=2.633+/-0.028 Msolar and M2=0.5412+/-0.0093 Msolar, radii of R1=7.55+/-0.20 Rsolar and R2=11.02+/-0.21 Rsolar, as well as effective temperatures of 5000+/-100 and 4640+/-150 K, for the primary and secondary, respectively. There are obvious signs of activity (spottedness) in the optical light curve of the binary. Our X-ray light curve clearly shows the primary eclipse but not the secondary eclipse, suggesting that the primary star is the dominant source of the activity in the system. The depth and duration of the eclipse allow us to infer some of the properties of the X-ray-emitting region around that star.

Structural analysis of bioceramic materials for denture application

NASA Astrophysics Data System (ADS)

Rauf, Nurlaela; Tahir, Dahlang; Arbiansyah, Muhammad

2016-03-01

Structural analysis has been performed on bioceramic materials for denture application by using X-ray diffraction (XRD), X-ray fluorescence (XRF), and Scanning Electron Microscopy (SEM). XRF is using for analysis chemical composition of raw materials. XRF shows the ratio 1 : 1 : 1 : 1 between feldspar, quartz, kaolin and eggshell, respectively, resulting composition CaO content of 56.78 %, which is similar with natural tooth. Sample preparation was carried out on temperature of 800 °C, 900 °C and 1000 °C. X-ray diffraction result showed that the structure is crystalline with trigonal crystal system for SiO2 (a=b=4.9134 Å and c=5.4051 Å) and CaH2O2 (a=b=3.5925 Å and c=4.9082 Å). Based on the Scherrer's equation showed the crystallite size of the highest peak (SiO2) increase with increasing the temperature preparation. The highest hardness value (87 kg/mm2) and match with the standards of dentin hardness. The surface structure was observed by using SEM also discussed.

Structure of Nano-sized CeO 2 Materials: Combined Scattering and Spectroscopic Investigations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Marchbank, Huw R.; Clark, Adam H.; Hyde, Timothy I.

Here, the nature of nano-sized ceria, CeO 2, systems were investigated using neutron and X-ray diffraction and X-ray absorption spectroscopy. Whilst both diffraction andtotal pair distribution functions (PDFs) revealed that in all the samples the occupancy of both Ce 4+ and O 2- are very close to the ideal stoichiometry, the analysis using reverse Monte Carlo technique revealedsignificant disorder around oxygen atoms in the nano sized ceria samples in comparison to the highly crystalline NIST standard.In addition, the analysis reveal that the main differences observed in the pair correlations from various X-ray and neutron diffraction techniques were attributed to themore » particle size of the CeO 2 prepared by the reported three methods. Furthermore, detailed analysis of the Ce L 3– and K-edge EXAFS data support this finding; in particular the decrease in higher shell coordination numbers with respect to the NIST standard, are attributed to differences in particle size.« less

Structure of Nano-sized CeO 2 Materials: Combined Scattering and Spectroscopic Investigations

DOE PAGES

Marchbank, Huw R.; Clark, Adam H.; Hyde, Timothy I.; ...

2016-08-29

Here, the nature of nano-sized ceria, CeO 2, systems were investigated using neutron and X-ray diffraction and X-ray absorption spectroscopy. Whilst both diffraction andtotal pair distribution functions (PDFs) revealed that in all the samples the occupancy of both Ce 4+ and O 2- are very close to the ideal stoichiometry, the analysis using reverse Monte Carlo technique revealedsignificant disorder around oxygen atoms in the nano sized ceria samples in comparison to the highly crystalline NIST standard.In addition, the analysis reveal that the main differences observed in the pair correlations from various X-ray and neutron diffraction techniques were attributed to themore » particle size of the CeO 2 prepared by the reported three methods. Furthermore, detailed analysis of the Ce L 3– and K-edge EXAFS data support this finding; in particular the decrease in higher shell coordination numbers with respect to the NIST standard, are attributed to differences in particle size.« less

The Lixiscope: a Pocket-size X-ray Imaging System

NASA Technical Reports Server (NTRS)

Yin, L. I.; Seltzer, S. M.

1978-01-01

A Low Intensity X ray Imaging device with the acronym LIXISCOPE is described. The Lixiscope has a small format and is powered only by a 2.7V battery. The high inherent gain of the Lixiscope permits the use of radioactive sources in lieu of X-ray machines in some fluoroscopic applications. In this mode of operation the complete X ray imaging system is truly portable and pocket-sized.

Studies of electrode structures and dynamics using coherent X-ray scattering and imaging

DOE Office of Scientific and Technical Information (OSTI.GOV)

You, H.; Liu, Y.; Ulvestad, A.

2017-08-01

Electrochemical systems studied in situ with advanced surface X-ray scattering techniques are reviewed. The electrochemical systems covered include interfaces of single-crystals and nanocrystals with respect to surface modification, aqueous dissolution, surface reconstruction, and electrochemical double layers. An emphasis will be given on recent results by coherent X-ray techniques such as X-ray photon correlation spectroscopy, Bragg coherent diffraction imaging, and surface ptychography.

The Discovery of a Second Luminous Low Mass X-Ray Binary System in the Globular Cluster M15

NASA Technical Reports Server (NTRS)

White, Nicholas E.; Angelini, Lorella

2001-01-01

Using the Chandra X-ray Observatory we have discovered a second bright X-ray source in the globular cluster M15 that is 2.7" to the west of AC211, the previously known low mass X-ray binary (LMXB) in this system. Prior to the 0.5" imaging capability of Chandra this second source could not have been resolved from AC211. The luminosity and spectrum of this new source, which we call M15-X2, are consistent with it also being a LMXB system. This is the first time that two LMXBs have been seen to be simultaneously active in a globular cluster. The new source, M15-X2, is coincident with a 18th U magnitude very blue star. The discovery of a second LMXB in M15 clears up a long standing puzzle where the X-ray and optical properties of AC211 appear consistent with the central source being hidden behind an accretion disk corona, and yet also showed a luminous X-ray burst suggesting the neutron star is directly visible. This discovery suggests instead that the X-ray burst did not come from AC211, but rather from the newly discovered X-ray source. We discuss the implications of this discovery for X-ray observations of globular clusters in nearby galaxies.

49 CFR 1546.209 - Use of X-ray systems.

Code of Federal Regulations, 2013 CFR

2013-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No foreign air carrier may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1544.211 - Use of X-ray systems.

Code of Federal Regulations, 2010 CFR

2010-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No aircraft operator may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1544.211 - Use of X-ray systems.

Code of Federal Regulations, 2011 CFR

2011-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No aircraft operator may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1546.209 - Use of X-ray systems.

Code of Federal Regulations, 2011 CFR

2011-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No foreign air carrier may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1546.209 - Use of X-ray systems.

Code of Federal Regulations, 2014 CFR

2014-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No foreign air carrier may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1544.211 - Use of X-ray systems.

Code of Federal Regulations, 2013 CFR

2013-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No aircraft operator may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1546.209 - Use of X-ray systems.

Code of Federal Regulations, 2010 CFR

2010-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No foreign air carrier may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

49 CFR 1544.211 - Use of X-ray systems.

Code of Federal Regulations, 2014 CFR

2014-10-01

....40. A radiation survey is not required for an X-ray system that is designed and constructed as a... incorporated by reference in paragraph (g) of this section. (b) Annual radiation survey. No aircraft operator may use any X-ray system unless, within the preceding 12 calendar months, a radiation survey is...

21 CFR 1020.30 - Diagnostic x-ray systems and their major components.

Code of Federal Regulations, 2012 CFR

2012-04-01

... irradiation. Diagnostic source assembly means the tube housing assembly with a beam-limiting device attached. Diagnostic x-ray system means an x-ray system designed for irradiation of any part of the human body for the... diagnostic source assembly. Fluoroscopic irradiation time means the cumulative duration during an examination...

21 CFR 1020.30 - Diagnostic x-ray systems and their major components.

Code of Federal Regulations, 2013 CFR

2013-04-01

... irradiation. Diagnostic source assembly means the tube housing assembly with a beam-limiting device attached. Diagnostic x-ray system means an x-ray system designed for irradiation of any part of the human body for the... diagnostic source assembly. Fluoroscopic irradiation time means the cumulative duration during an examination...

21 CFR 1020.30 - Diagnostic x-ray systems and their major components.

Code of Federal Regulations, 2014 CFR

2014-04-01

... irradiation. Diagnostic source assembly means the tube housing assembly with a beam-limiting device attached. Diagnostic x-ray system means an x-ray system designed for irradiation of any part of the human body for the... diagnostic source assembly. Fluoroscopic irradiation time means the cumulative duration during an examination...

The Marshall Space Flight Center Development of Mirror Modules for the ART-XC Ins1rument Aboard the Spectrum-Roentgen-Gamma Mission

NASA Technical Reports Server (NTRS)

Gubarev, M.; Ramsey, B.; ODell, S. L.; Elsner, R.; Kilaru, K.; McCracken, J.; Pavlinsky, M.; Tkachenko, A.; Lapshov, I.

2012-01-01

The Spectrum-Rontgen-Gamma (SRG) mission is a Russian-German X-ray astrophysical observatory that carries two co-aligned and complementary X-ray telescope systems. The primary instrument is the German-led extended ROentgen Survey with an Imaging Telescope Array (eROSITA), a 7-module X-ray telescope system that covers the energy range from 0.2-12 keV. The complementary instrument is the Russian-led Astronomical Roentgen Telescope -- X-ray Concentrator (ART-XC or ART), a 7-module X-ray telescope system that provides higher energy coverage, up to 30 keV (with limited sensitivity above 12 keV).

Analysis of Sunyaev–Zel'dovich effect mass–observable relations using South Pole Telescope observations of an X-ray selected sample of low-mass galaxy clusters and groups

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liu, J.; Mohr, J.; Saro, A.

2015-02-26

We use microwave observations from the South Pole Telescope (SPT) to examine the Sunyaev-Zel'dovich effect (SZE) signatures of a sample of 46 X-ray selected groups and clusters drawn from similar to 6 deg(2) of the XMM-Newton Blanco Cosmology Survey. These systems extend to redshift z = 1.02 and probe the SZE signal to the lowest X-ray luminosities (>= 10(42) erg s(-1)) yet; these sample characteristics make this analysis complementary to previous studies. We develop an analysis tool, using X-ray luminosity as a mass proxy, to extract selection-bias-corrected constraints on the SZE significance and Y-500 mass relations. The former is inmore » good agreement with an extrapolation of the relation obtained from high-mass clusters. However, the latter, at low masses, while in good agreement with the extrapolation from the high-mass SPT clusters, is in tension at 2.8 sigma with the Planck constraints, indicating the low-mass systems exhibit lower SZE signatures in the SPT data. We also present an analysis of potential sources of contamination. For the radio galaxy point source population, we find 18 of our systems have 843 MHz Sydney University Molonglo Sky Survey sources within 2 arcmin of the X-ray centre, and three of these are also detected at significance >4 by SPT. Of these three, two are associated with the group brightest cluster galaxies, and the third is likely an unassociated quasar candidate. We examine the impact of these point sources on our SZE scaling relation analyses and find no evidence of biases. We also examine the impact of dusty galaxies using constraints from the 220 GHz data. The stacked sample provides 2.8 sigma significant evidence of dusty galaxy flux, which would correspond to an average underestimate of the SPT Y-500 signal that is (17 +/- 9) per cent in this sample of low-mass systems. Finally, we explore the impact of future data from SPTpol and XMM-XXL, showing that it will lead to a factor of 4 to 5 tighter constraints on these SZE mass-observable relations.« less

Analysis of Sunyaev-Zel'dovich effect mass-observable relations using South Pole Telescope observations of an X-ray selected sample of low-mass galaxy clusters and groups

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liu, J.; Mohr, J.; Saro, A.

2015-02-25

We use microwave observations from the South Pole Telescope (SPT) to examine the Sunyaev–Zel'dovich effect (SZE) signatures of a sample of 46 X-ray selected groups and clusters drawn from ~6 deg 2 of the XMM–Newton Blanco Cosmology Survey. These systems extend to redshift z = 1.02 and probe the SZE signal to the lowest X-ray luminosities (≥10 42 erg s -1) yet; these sample characteristics make this analysis complementary to previous studies. We develop an analysis tool, using X-ray luminosity as a mass proxy, to extract selection-bias-corrected constraints on the SZE significance and Y_500 mass relations. The former is in good agreement with anmore » extrapolation of the relation obtained from high-mass clusters. However, the latter, at low masses, while in good agreement with the extrapolation from the high-mass SPT clusters, is in tension at 2.8σ with the Planck constraints, indicating the low-mass systems exhibit lower SZE signatures in the SPT data. We also present an analysis of potential sources of contamination. For the radio galaxy point source population, we find 18 of our systems have 843 MHz Sydney University Molonglo Sky Survey sources within 2 arcmin of the X-ray centre, and three of these are also detected at significance >4 by SPT. Of these three, two are associated with the group brightest cluster galaxies, and the third is likely an unassociated quasar candidate. We examine the impact of these point sources on our SZE scaling relation analyses and find no evidence of biases. We also examine the impact of dusty galaxies using constraints from the 220 GHz data. The stacked sample provides 2.8σ significant evidence of dusty galaxy flux, which would correspond to an average underestimate of the SPT Y_500 signal that is (17 ± 9)per cent in this sample of low-mass systems. Finally, we explore the impact of future data from SPTpol and XMM-XXL, showing that it will lead to a factor of 4 to 5 tighter constraints on these SZE mass–observable relations.« less

Participation of the Abastumani Astrophysical Observatory in Different Programs for Coordinated Investigation of Cyg X-1

NASA Astrophysics Data System (ADS)

Kumsiashvili, M. I.; Kochiashvili, N. T.

2000-10-01

Broad-band photometric observations of the black hole candidate Cyg X-1 were carried out in 1975-1998 at the Abastumani Astrophysical Observatory in the framework of coordinated observations, at the varies observatories of the former Soviet Union. All data have been reduced to a homogeneous set.Comparison of the optical and X-ray data clearly shows the existence of several kinds of variability. Analysis of the prolonged photoelectric observations of V 1357 Cyg=Cyg X-1 confirmed long-period optical variation of this X-ray binary system with the period of 294 d revealed by Kemp et al. This periodicity is most strongly pronounced at the orbital period phase when the optical star is in front of the X-ray source. Variations of the mean level of Cyg X-1 and of the light curve form with the phase of the period 294 d agree well with the model of the precessing accretion disk which radiates in the optical range mainly by scattering and processing of the optical star radiation. The direction of the disc precession coincides with that of the orbital motion and it is hard to understand this fact in the models with the forced precession. The triple system model is less probable. There are also observations of this objects made in the Abastumani Observatory in 1982-1988 which are represented the Table and light curves. These observations have not discussed by coordinators. The observations taken in the course of the International campaign "The Optical Monitoring of the Unique Astrophysical Objects" were realized by the observatories located on the territories of Georgia, Russia, Uzbekistan and Ukraine in 1994-1998. They are united in a single set, taking into account the systemic differences between them. Number of usual observations is 2247 in 399 nights in U B V R bands. The observations were performed simultaneously in X-ray band in the energy range of 2-10 keV (ASM/RXTE), and 20-100 keV (BASTE/CGRO), and also with radio observations at the Mullard radio observatory. Our optical data overlapped well the hard band at JD 2451000-040. Both outbursts did not coincide with any optical brightening or double wave orbital light curve changes. From two independent sets strong optical flare at JD 2450988, being a possible precursor of hard X-ray flare have been detected. Intrinsic variations of the system have the chaotic character with flares and dips in time scale of a day and the amplitude of 0.10 m. Fourier spectra show predominating secondary period of 147 d at high probability level, being a half of 294 d period found by Priedhorsky et al. in X-rays, and Kemp et al. in optics. We have identified near-by period of 150 d which predominates modern X-ray light curve. The period found in optics is close to the period of 142.7 d in modern Mullard radio data by Brooksopp et al. The light curve resembles a non-stationary process by the time changes of Fourier spectra. But some spectrum peaks can be stable for several seasons. The cross-correlation analysis confirms the time delay of the trends of the X-ray light curve relative to the optical one by 11.620 days. The weak relation of the short-time variations of X-ray and optical radiation are also found at high probability level with delay 3 days.

The image enhancement and region of interest extraction of lobster-eye X-ray dangerous material inspection system

NASA Astrophysics Data System (ADS)

Zhan, Qi; Wang, Xin; Mu, Baozhong; Xu, Jie; Xie, Qing; Li, Yaran; Chen, Yifan; He, Yanan

2016-10-01

Dangerous materials inspection is an important technique to confirm dangerous materials crimes. It has significant impact on the prohibition of dangerous materials-related crimes and the spread of dangerous materials. Lobster-Eye Optical Imaging System is a kind of dangerous materials detection device which mainly takes advantage of backscatter X-ray. The strength of the system is its applicability to access only one side of an object, and to detect dangerous materials without disturbing the surroundings of the target material. The device uses Compton scattered x-rays to create computerized outlines of suspected objects during security detection process. Due to the grid structure of the bionic object glass, which imitate the eye of a lobster, grids contribute to the main image noise during the imaging process. At the same time, when used to inspect structured or dense materials, the image is plagued by superposition artifacts and limited by attenuation and noise. With the goal of achieving high quality images which could be used for dangerous materials detection and further analysis, we developed effective image process methods applied to the system. The first aspect of the image process is the denoising and enhancing edge contrast process, during the process, we apply deconvolution algorithm to remove the grids and other noises. After image processing, we achieve high signal-to-noise ratio image. The second part is to reconstruct image from low dose X-ray exposure condition. We developed a kind of interpolation method to achieve the goal. The last aspect is the region of interest (ROI) extraction process, which could be used to help identifying dangerous materials mixed with complex backgrounds. The methods demonstrated in the paper have the potential to improve the sensitivity and quality of x-ray backscatter system imaging.

Implementation of an electromagnetic imaging system to facilitate nasogastric and post-pyloric feeding tube placement in patients with and without critical illness.

PubMed

Windle, E M; Beddow, D; Hall, E; Wright, J; Sundar, N

2010-02-01

Artificial nutrition support is required to optimise nutritional status in many patients. Traditional methods of placing feeding tubes may incur clinical risk and financial costs. A technique facilitating placement of nasogastric and post-pyloric tubes via electromagnetic visual guidance may reduce the need for X-ray exposure, endoscopy time and the use of parenteral nutrition. The present study aimed to audit use of such a system at initial implementation in patients within an acute NHS Trust. A retrospective review was undertaken of dietetic and medical records for the first 14 months of using the Cortrak system. Data were collected on referral origin, preparation of the patient prior to insertion, placement success rates and need for X-ray. Cost analysis was also performed. Referrals were received from primary consultants or consultant intensivists, often on the advice of the dietitian. Fifty-nine percent of patients received prokinetic therapy at the time of placement. Thirty-nine tube placements were attempted. Sixty-nine percent of referrals for post-pyloric tube placement resulted in successful placement. X-ray films were requested for 22% of all attempted post-pyloric placements. Less than half of nasogastric tubes were successfully passed, although none of these required X-ray confirmation. The mean cost per tube insertion attempt was 111 pounds. This system confers advantages, particularly in terms of post-pyloric tube placement, even at this early stage of implementation. A reduction in clinical risk and cost avoidance related to X-ray exposure, the need for endoscopic tube placement and parenteral nutrition have been achieved. The implementation of this system should be considered in other centres.

A physical parameter method for the design of broad-band X-ray imaging systems to do coronal plasma diagnostics

NASA Technical Reports Server (NTRS)

Kahler, S.; Krieger, A. S.

1978-01-01

The technique commonly used for the analysis of data from broad-band X-ray imaging systems for plasma diagnostics is the filter ratio method. This requires the use of two or more broad-band filters to derive temperatures and line-of-sight emission integrals or emission measure distributions as a function of temperature. Here an alternative analytical approach is proposed in which the temperature response of the imaging system is matched to the physical parameter being investigated. The temperature response of a system designed to measure the total radiated power along the line of sight of any coronal structure is calculated. Other examples are discussed.

First demonstration of iodine mapping in nonliving phantoms using an X-ray fluorescence computed tomography system with a cadmium telluride detector and a tungsten-target tube

NASA Astrophysics Data System (ADS)

Sato, Eiichi; Sato, Yuichi; Ehara, Shigeru; Abudurexiti, Abulajiang; Hagiwara, Osahiko; Matsukiyo, Hiroshi; Osawa, Akihiro; Enomoto, Toshiyuki; Watanabe, Manabu; Nagao, Jiro; Sato, Shigehiro; Ogawa, Akira; Onagawa, Jun

2011-05-01

X-ray fluorescence (XRF) analysis is useful for mapping various atoms in objects, and XRF is emitted by absorbing X-ray photons with energies beyond the K-edge energy of the target atom. Narrow-energy-width bremsstrahlung X-rays are selected using a 3.0-mm-thick aluminum filter. These rays are absorbed by iodine media in objects, and iodine XRF is produced from the iodine atoms. Next, iodine Kα photons are discriminated by a multichannel analyzer and the number of photons is counted by a counter card. CT is performed by repeated linear scans and rotations of an object. The X-ray generator has a 100 μm focus tube with a 0.5-mm-thick beryllium window, and the tube voltage and the current for XRF were 80 kV and 0.50 mA, respectively. The demonstration of XRF-CT for mapping iodine atoms was carried out by selection of photons in an energy range from 27.5 to 29.5 keV with a photon-energy resolution of 1.2 keV.

Elucidating light-induced charge accumulation in an artificial analogue of methane monooxygenase enzymes using time-resolved X-ray absorption spectroscopy

DOE PAGES

Moonshiram, Dooshaye; Picon, Antonio; Vazquez-Mayagoitia, Alvaro; ...

2017-02-08

Here, we report the use of time-resolved X-ray absorption spectroscopy in the ns–μs time scale to track the light induced two electron transfer processes in a multi-component photocatalytic system, consisting of [Ru(bpy) 3] 2+/ a diiron(III,III) model/triethylamine. EXAFS analysis with DFT calculations confirms the structural configurations of the diiron(III,III) and reduced diiron(II,II) states.

Elucidating light-induced charge accumulation in an artificial analogue of methane monooxygenase enzymes using time-resolved X-ray absorption spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moonshiram, Dooshaye; Picon, Antonio; Vazquez-Mayagoitia, Alvaro

Here, we report the use of time-resolved X-ray absorption spectroscopy in the ns–μs time scale to track the light induced two electron transfer processes in a multi-component photocatalytic system, consisting of [Ru(bpy) 3] 2+/ a diiron(III,III) model/triethylamine. EXAFS analysis with DFT calculations confirms the structural configurations of the diiron(III,III) and reduced diiron(II,II) states.

X-ray and radio observations of flares from the RS Canum Venaticorum system UX ARIETIS

NASA Astrophysics Data System (ADS)

Tsuru, T.; Makishima, K.; Ohashi, T.; Inoue, H.; Koyama, K.; Turner, M. J. L.; Barstow, M. A.; McHardy, I. M.; Pye, J. P.; Tsunemi, H.; Kitamoto, S.; Taylor, A. R.; Nelson, R. F.

In July 1987 the RS CVn system UX Ari was observed in the 2-20-keV X-ray band by Ginga, immediately followed by 5-GHz radio observations. UX Ari was found to be very active at both radio and X-ray frequencies. Quiescent X-ray emission with a luminosity of 3 x 10 to the 31st erg/s (in the 2-20-keV band) was detected, together with two intense X-ray flares up to 2 x 10 to the 32nd and 6 x 10 to the 31st erg/s, respectively. Both flare and quiescent X-ray spectra are well fitted by single-temperature thermal bremsstrahlung models, with the continuum temperature and emission measure in the range 4-7 kev (in kT) and (2-10) x 10 to the 54th/cu cm, respectively.

Simulating x-ray telescopes with McXtrace: a case study of ATHENA's optics

NASA Astrophysics Data System (ADS)

Ferreira, Desiree D. M.; Knudsen, Erik B.; Westergaard, Niels J.; Christensen, Finn E.; Massahi, Sonny; Shortt, Brian; Spiga, Daniele; Solstad, Mathias; Lefmann, Kim

2016-07-01

We use the X-ray ray-tracing package McXtrace to simulate the performance of X-ray telescopes based on Silicon Pore Optics (SPO) technologies. We use as reference the design of the optics of the planned X-ray mission Advanced Telescope for High ENergy Astrophysics (ATHENA) which is designed as a single X-ray telescope populated with stacked SPO substrates forming mirror modules to focus X-ray photons. We show that is possible to simulate in detail the SPO pores and qualify the use of McXtrace for in-depth analysis of in-orbit performance and laboratory X-ray test results.

A motion detection system for AXAF X-ray ground testing

NASA Technical Reports Server (NTRS)

Arenberg, Jonathan W.; Texter, Scott C.

1993-01-01

The concept, implementation, and performance of the motion detection system (MDS) designed as a diagnostic for X-ray ground testing for AXAF are described. The purpose of the MDS is to measure the magnitude of a relative rigid body motion among the AXAF test optic, the X-ray source, and X-ray focal plane detector. The MDS consists of a point source, lens, centroid detector, transimpedance amplifier, and computer system. Measurement of the centroid position of the image of the optical point source provides a direct measure of the motions of the X-ray optical system. The outputs from the detector and filter/amplifier are digitized and processed using the calibration with a 50 Hz bandwidth to give the centroid's location on the detector. Resolution of 0.008 arcsec has been achieved by this system. Data illustrating the performance of the motion detection system are also presented.

Empirical studies of solar flares: Comparison of X-ray and H alpha filtergrams and analysis of the energy balance of the X-ray plasma

NASA Technical Reports Server (NTRS)

Moore, R. L.

1979-01-01

The physics of solar flares was investigated through a combined analysis of X-ray filtergrams of the high temperature coronal component of flares and H alpha filtergrams of the low temperature chromospheric component. The data were used to study the magnetic field configuration and its changes in solar flares, and to examine the chromospheric location and structure of X-ray bright points (XPB) and XPB flares. Each topic and the germane data are discussed. The energy balance of the thermal X-ray plasma in flares, while not studied, is addressed.

VETA-I x ray test analysis

NASA Technical Reports Server (NTRS)

Brissenden, R. J. V.; Chartas, G.; Freeman, M. D.; Hughes, J. P.; Kellogg, E. M.; Podgorski, W. A.; Schwartz, D. A.; Zhao, P.

1992-01-01

This interim report presents some definitive results from our analysis of the VETA-I x-ray testing data. It also provides a description of the hardware and software used in the conduct of the VETA-I x-ray test program performed at the MSFC x-ray Calibration Facility (XRCF). These test results also serve to supply data and information to include in the TRW final report required by DPD 692, DR XC04. To provide an authoritative compendium of results, we have taken nine papers as published in the SPIE Symposium, 'Grazing Incidence X-ray/EUV Optics for Astronomy and Projection Lithography' and have reproduced them as the content of this report.

Advances toward submicron resolution optics for x-ray instrumentation and applications

NASA Astrophysics Data System (ADS)

Cordier, Mark; Stripe, Benjamin; Yun, Wenbing; Lau, S. H.; Lyon, Alan; Reynolds, David; Lewis, Sylvia J. Y.; Chen, Sharon; Semenov, Vladimir A.; Spink, Richard I.; Seshadri, Srivatsan

2017-08-01

Sigray's axially symmetric x-ray optics enable advanced microanalytical capabilities for focusing x-rays to microns-scale to submicron spot sizes, which can potentially unlock many avenues for laboratory micro-analysis. The design of these optics allows submicron spot sizes even at low x-ray energies, enabling research into low atomic number elements and allows increased sensitivity of grazing incidence measurements and surface analysis. We will discuss advances made in the fabrication of these double paraboloidal mirror lenses designed for use in laboratory x-ray applications. We will additionally present results from as-built paraboloids, including surface figure error and focal spot size achieved to-date.

Local x-ray structure analysis of optically manipulated biological micro-objects

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cojoc, Dan; Ferrari, Enrico; Santucci, Silvia C.

2010-12-13

X-ray diffraction using micro- and nanofocused beams is well suited for nanostructure analysis at different sites of a biological micro-object. To conduct in vitro studies without mechanical contact, we developed object manipulation by optical tweezers in a microfluidic cell. Here we report x-ray microdiffraction analysis of a micro-object optically trapped in three dimensions. We revealed the nanostructure of a single starch granule at different points and investigated local radiation damage induced by repeated x-ray exposures at the same position, demonstrating high stability and full control of the granule orientation by multiple optical traps.

High speed photography, videography, and photonics III; Proceedings of the Meeting, San Diego, CA, August 22, 23, 1985

NASA Technical Reports Server (NTRS)

Ponseggi, B. G. (Editor); Johnson, H. C. (Editor)

1985-01-01

Papers are presented on the picosecond electronic framing camera, photogrammetric techniques using high-speed cineradiography, picosecond semiconductor lasers for characterizing high-speed image shutters, the measurement of dynamic strain by high-speed moire photography, the fast framing camera with independent frame adjustments, design considerations for a data recording system, and nanosecond optical shutters. Consideration is given to boundary-layer transition detectors, holographic imaging, laser holographic interferometry in wind tunnels, heterodyne holographic interferometry, a multispectral video imaging and analysis system, a gated intensified camera, a charge-injection-device profile camera, a gated silicon-intensified-target streak tube and nanosecond-gated photoemissive shutter tubes. Topics discussed include high time-space resolved photography of lasers, time-resolved X-ray spectrographic instrumentation for laser studies, a time-resolving X-ray spectrometer, a femtosecond streak camera, streak tubes and cameras, and a short pulse X-ray diagnostic development facility.

A sealable ultrathin window sample cell for the study of liquids by means of soft X-ray spectroscopy

NASA Astrophysics Data System (ADS)

Grötzsch, D.; Streeck, C.; Nietzold, C.; Malzer, W.; Mantouvalou, I.; Nutsch, A.; Dietrich, P.; Unger, W.; Beckhoff, B.; Kanngießer, B.

2017-12-01

A new sample cell concept for the analysis of liquids or solid-liquid interfaces using soft X-ray spectroscopy is presented, which enables the complete sealing of the cell as well as the transport into vacuum via, for example, a load-lock system. The cell uses pressure monitoring and active as well as passive pressure regulation systems, thereby facilitating the full control over the pressure during filling, sealing, evacuation, and measurement. The cell design and sample preparation as well as the crucial sealing procedure are explained in detail. As a first proof-of-principle experiment, successful nitrogen K-edge fluorescence yield near-edge X-ray absorption fine structure experiments of a biomolecular solution are presented. For this purpose, it is shown that the careful evaluation of all involved parameters, such as window type or photon flux, is desirable for optimizing the experimental result.

X-Ray Structure determination of the Glycine Cleavage System Protein H of Mycobacterium tuberculosis Using An Inverse Compton Synchrotron X-Ray Source

PubMed Central

Abendroth, Jan; McCormick, Michael S.; Edwards, Thomas E.; Staker, Bart; Loewen, Roderick; Gifford, Martin; Rifkin, Jeff; Mayer, Chad; Guo, Wenjin; Zhang, Yang; Myler, Peter; Kelley, Angela; Analau, Erwin; Hewitt, Stephen Nakazawa; Napuli, Alberto J.; Kuhn, Peter; Ruth, Ronald D.; Stewart, Lance J.

2010-01-01

Structural genomics discovery projects require ready access to both X-ray and NMR instrumentation which support the collection of experimental data needed to solve large numbers of novel protein structures. The most productive X-ray crystal structure determination laboratories make extensive frequent use of tunable synchrotron X-ray light to solve novel structures by anomalous diffraction methods. This requires that frozen cryo-protected crystals be shipped to large government-run synchrotron facilities for data collection. In an effort to eliminate the need to ship crystals for data collection, we have developed the first laboratory-scale synchrotron light source capable of performing many of the state-of-the-art synchrotron applications in X-ray science. This Compact Light Source is a first-in-class device that uses inverse Compton scattering to generate X-rays of sufficient flux, tunable wavelength and beam size to allow high-resolution X-ray diffraction data collection from protein crystals. We report on benchmarking tests of X-ray diffraction data collection with hen egg white lysozyme, and the successful high-resolution X-ray structure determination of the Glycine cleavage system protein H from Mycobacterium tuberculosis using diffraction data collected with the Compact Light Source X-ray beam. PMID:20364333

Luminescence properties after X-ray irradiation for dosimetry

NASA Astrophysics Data System (ADS)

Hong, Duk-Geun; Kim, Myung-Jin

2016-05-01

To investigate the luminescence characteristics after exposure to X-ray radiation, we developed an independent, small X-ray irradiation system comprising a Varian VF-50J mini X-ray generator, a Pb collimator, a delay shutter, and an Al absorber. With this system, the apparent dose rate increased linearly to 0.8 Gy/s against the emission current for a 50 kV anode potential when the shutter was delayed for an initial 4 s and the Al absorber was 300 µm thick. In addition, an approximately 20 mm diameter sample area was irradiated homogeneously with X rays. Based on three-dimensional (3D) thermoluminescence (TL) spectra, the small X-ray irradiator was considered comparable to the conventional 90Sr/90Y beta source even though the TL intensity from beta irradiation was higher than that from X-ray irradiation. The single aliquot regenerative (SAR) growth curve for the small X-ray irradiator was identical to that for the beta source. Therefore, we concluded that the characteristics of the small X-ray irradiator and the conventional 90Sr/90Y beta source were similar and that X ray irradiation had the potential for being suitable for use in luminescence dosimetry.

The x-ray light valve: a low-cost, digital radiographic imaging system-spatial resolution

NASA Astrophysics Data System (ADS)

MacDougall, Robert D.; Koprinarov, Ivaylo; Webster, Christie A.; Rowlands, J. A.

2007-03-01

In recent years, new x-ray radiographic systems based on large area flat panel technology have revolutionized our capability to produce digital x-ray radiographic images. However, these active matrix flat panel imagers (AMFPIs) are extraordinarily expensive compared to the systems they are replacing. Thus there is a need for a low cost digital imaging system for general applications in radiology. Different approaches have been considered to make lower cost, integrated x-ray imaging devices for digital radiography, including: scanned projection x-ray, an integrated approach based on computed radiography technology and optically demagnified x-ray screen/CCD systems. These approaches suffer from either high cost or high mechanical complexity and do not have the image quality of AMFPIs. We have identified a new approach - the X-ray Light Valve (XLV). The XLV has the potential to achieve the immediate readout in an integrated system with image quality comparable to AMFPIs. The XLV concept combines three well-established and hence lowcost technologies: an amorphous selenium (a-Se) layer to convert x-rays to image charge, a liquid crystal (LC) cell as an analog display, and an optical scanner for image digitization. Here we investigate the spatial resolution possible with XLV systems. Both a-Se and LC cells have both been shown separately to have inherently very high spatial resolution. Due to the close electrostatic coupling in the XLV, it can be expected that the spatial resolution of this system will also be very high. A prototype XLV was made and a typical office scanner was used for image digitization. The Modulation Transfer Function was measured and the limiting factor was seen to be the optical scanner. However, even with this limitation the XLV system is able to meet or exceed the resolution requirements for chest radiography.

Closed bore XMR (CBXMR) systems for aortic valve replacement: active magnetic shielding of x-ray tubes.

PubMed

Bracken, John A; DeCrescenzo, Giovanni; Komljenovic, Philip; Lillaney, Prasheel V; Fahrig, Rebecca; Rowlands, J A

2009-05-01

Hybrid closed bore x-ray/MRI systems are being developed to improve the safety and efficacy of percutaneous aortic valve replacement procedures by harnessing the complementary strengths of the x-ray and MRI modalities in a single interventional suite without requiring patient transfer between two rooms. These systems are composed of an x-ray C-arm in close proximity (approximately 1 m) to an MRI scanner. The MRI magnetic fringe field can cause the electron beam in the x-ray tube to deflect. The deflection causes the x-ray field of view to shift position on the detector receptacle. This could result in unnecessary radiation exposure to the patient and the staff in the cardiac catheterization laboratory. Therefore, the electron beam deflection must be corrected. The authors developed an active magnetic shielding system that can correct for electron beam deflection to within an accuracy of 5% without truncating the field of view or increasing exposure to the patient. This system was able to automatically adjust to different field strengths as the external magnetic field acting on the x-ray tube was changed. Although a small torque was observed on the shielding coils of the active shielding system when they were placed in a magnetic field, this torque will not impact their performance if they are securely mounted on the x-ray tube and the C-arm. The heating of the coils of the shielding system for use in the clinic caused by electric current was found to be slow enough not to require a dedicated cooling system for one percutaneous aortic valve replacement procedure. However, a cooling system will be required if multiple procedures are performed in one session.

Diffraction leveraged modulation of X-ray pulses using MEMS-based X-ray optics

DOEpatents

Lopez, Daniel; Shenoy, Gopal; Wang, Jin; Walko, Donald A.; Jung, Il-Woong; Mukhopadhyay, Deepkishore

2016-08-09

A method and apparatus are provided for implementing Bragg-diffraction leveraged modulation of X-ray pulses using MicroElectroMechanical systems (MEMS) based diffractive optics. An oscillating crystalline MEMS device generates a controllable time-window for diffraction of the incident X-ray radiation. The Bragg-diffraction leveraged modulation of X-ray pulses includes isolating a particular pulse, spatially separating individual pulses, and spreading a single pulse from an X-ray pulse-train.

X-ray elemental mapping techniques for elucidating the ecophysiology of hyperaccumulator plants.

PubMed

van der Ent, Antony; Przybyłowicz, Wojciech J; de Jonge, Martin D; Harris, Hugh H; Ryan, Chris G; Tylko, Grzegorz; Paterson, David J; Barnabas, Alban D; Kopittke, Peter M; Mesjasz-Przybyłowicz, Jolanta

2018-04-01

Contents Summary 432 I. Introduction 433 II. Preparation of plant samples for X-ray micro-analysis 433 III. X-ray elemental mapping techniques 438 IV. X-ray data analysis 442 V. Case studies 443 VI. Conclusions 446 Acknowledgements 449 Author contributions 449 References 449 SUMMARY: Hyperaccumulators are attractive models for studying metal(loid) homeostasis, and probing the spatial distribution and coordination chemistry of metal(loid)s in their tissues is important for advancing our understanding of their ecophysiology. X-ray elemental mapping techniques are unique in providing in situ information, and with appropriate sample preparation offer results true to biological conditions of the living plant. The common platform of these techniques is a reliance on characteristic X-rays of elements present in a sample, excited either by electrons (scanning/transmission electron microscopy), protons (proton-induced X-ray emission) or X-rays (X-ray fluorescence microscopy). Elucidating the cellular and tissue-level distribution of metal(loid)s is inherently challenging and accurate X-ray analysis places strict demands on sample collection, preparation and analytical conditions, to avoid elemental redistribution, chemical modification or ultrastructural alterations. We compare the merits and limitations of the individual techniques, and focus on the optimal field of applications for inferring ecophysiological processes in hyperaccumulator plants. X-ray elemental mapping techniques can play a key role in answering questions at every level of metal(loid) homeostasis in plants, from the rhizosphere interface, to uptake pathways in the roots and shoots. Further improvements in technological capabilities offer exciting perspectives for the study of hyperaccumulator plants into the future. © 2017 University of Queensland. New Phytologist © 2017 New Phytologist Trust.

Chandra Looks Over a Cosmic Four-Leaf Clover

NASA Astrophysics Data System (ADS)

2004-07-01

A careful analysis of observations by NASA's Chandra X-ray Observatory of a rare quadruple quasar has uncovered evidence that possibly a single star in a foreground galaxy magnified X-rays coming from the quasar. This discovery gives astronomers a new and extremely precise probe of the gas flow around the supermassive black hole that powers the quasar. "If our interpretation is correct, then we are seeing details around this black hole that are 50,000 times smaller than either the Hubble Space Telescope or Chandra could see under ordinary circumstances," said George Chartas of Penn State University in University Park, and lead author of a recent article on the Cloverleaf quasar in The Astrophysical Journal. The Cloverleaf quasar is a single object about 11 billion light years from Earth that appears as four images produced by a process known as gravitational lensing. If one or more galaxies lie along the line of sight to a more distant quasar, the gravitational field of the intervening galaxies can bend and magnify the light from the quasar and produce multiple images of it. The four images of the Cloverleaf quasar have been produced by one or more intervening galaxies. Cloverleaf Quasar Chandra X-ray Image of the Cloverleaf quasar One of the images (A), in the Cloverleaf is brighter than the others in both optical and X-ray light. Chartas and his colleagues found the relative brightness of this image was greater in X-ray than in optical light. The X-rays from iron atoms were also enhanced relative to X-rays at lower energies. Since the amount of brightening due to gravitational lensing does not vary with the wavelength, this means that an additional object has magnified the X-rays. The increased magnification of the X-ray light can be explained by gravitational microlensing, an effect which has been used to search for compact stars and planets in our galaxy. Microlensing occurs when a star or a multiple star system passes in front of light from a background object. Cloverleaf Quasar Hubble Optical Image of the Cloverleaf quasar If a single star or a multiple star system in one of the foreground galaxies passed in front of the light path for the brightest image, then that image would be selectively magnified. The X-rays would be magnified much more than the visible light, if they came from a smaller region around the black hole than the visible light. The enhancement of the X-rays from iron ions would be due to this same effect. The analysis indicates that the X-rays are coming from a very small region, about the size of the solar system, around the supermassive black hole. The visible light is coming from a region ten or more times larger. The angular size of these regions at a distance of 11 billion light years is tens of thousands times smaller than the smallest region that can be resolved by the Hubble Space Telescope. Illustration of Wind from Accretion Disk Around a Black Hole Illustration of Wind from Accretion Disk Around a Black Hole "The significance of the detection of microlensed X-rays from the Cloverleaf quasar lies in the extremely small region that is enhanced by the microlens," said Chartas. "This gives us the ability to make strong tests of models for the flow of gas around a supermassive black hole." Other team members include Michael Eracleous (Penn State), Eric Agol (University of Washington), and Sarah Gallagher (UCLA). NASA's Marshall Space Flight Center, Huntsville, Ala., manages the Chandra program for NASA's Office of Space Science, Washington. Northrop Grumman of Redondo Beach, Calif., formerly TRW, Inc., was the prime development contractor for the observatory. The Smithsonian Astrophysical Observatory controls science and flight operations from the Chandra X-ray Center in Cambridge, Mass. Additional information and images are available at: http://chandra.harvard.edu and http://chandra.nasa.gov