Single-crystal diamond refractive lens for focusing X-rays in two dimensions

PubMed Central

Antipov, S.; Baryshev, S. V.; Butler, J. E.; Antipova, O.; Liu, Z.; Stoupin, S.

2016-01-01

The fabrication and performance evaluation of single-crystal diamond refractive X-ray lenses of which the surfaces are paraboloids of revolution for focusing X-rays in two dimensions simultaneously are reported. The lenses were manufactured using a femtosecond laser micromachining process and tested using X-ray synchrotron radiation. Such lenses were stacked together to form a standard compound refractive lens (CRL). Owing to the superior physical properties of the material, diamond CRLs could become indispensable wavefront-preserving primary focusing optics for X-ray free-electron lasers and the next-generation synchrotron storage rings. They can be used for highly efficient refocusing of the extremely bright X-ray sources for secondary optical schemes with limited aperture such as nanofocusing Fresnel zone plates and multilayer Laue lenses. PMID:26698059

Refraction effects in soft x-ray multilayer blazed gratings.

PubMed

Voronov, D L; Salmassi, F; Meyer-Ilse, J; Gullikson, E M; Warwick, T; Padmore, H A

2016-05-30

A 2500 lines/mm Multilayer Blazed Grating (MBG) optimized for the soft x-ray wavelength range was fabricated and tested. The grating coated with a W/B₄C multilayer demonstrated a record diffraction efficiency in the 2nd blazed diffraction order in the energy range from 500 to 1200 eV. Detailed investigation of the diffraction properties of the grating demonstrated that the diffraction efficiency of high groove density MBGs is not limited by the normal shadowing effects that limits grazing incidence x-ray grating performance. Refraction effects inherent in asymmetrical Bragg diffraction were experimentally confirmed for MBGs. The refraction affects the blazing properties of the MBGs and results in a shift of the resonance wavelength of the gratings and broadening or narrowing of the grating bandwidth depending on diffraction geometry. The true blaze angle of the MBGs is defined by both the real structure of the multilayer stack and by asymmetrical refraction effects. Refraction effects can be used as a powerful tool in providing highly efficient suppression of high order harmonics.

Materials for x-ray refractive lenses minimizing wavefront distortions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Roth, Thomas; Alianelli, Lucia; Lengeler, Daniel

2017-06-09

Refraction through curved surfaces, reflection from curved mirrors in grazing incidence, and diffraction from Fresnel zone plates are key hard x-ray focusing mechanisms. In this article, we present materials used for refractive x-ray lenses. Important properties of such x-ray lenses include focusing strength, shape, and the material’s homogeneity and absorption coefficient. Both the properties of the initial material and the fabrication process result in a lens with imperfections, which can lead to unwanted wavefront distortions. Different fabrication methods for one-dimensional and two-dimensional focusing lenses are presented, together with the respective benefits and inconveniences that are mostly due to shape fidelity.more » Different materials and material grades have been investigated in terms of their homogeneity and the absence of inclusions. Single-crystalline materials show high homogeneity, but suffer from unwanted diffracted radiation, which can be avoided using amorphous materials. Lastly, we show that shape imperfections can be corrected using a correction lens.« less

Single-crystal diamond refractive lens for focusing X-rays in two dimensions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Antipov, S.; Baryshev, Sergey; Butler, J. E.

2016-01-01

The fabrication and performance evaluation of single-crystal diamond refractive X-ray lenses of which the surfaces are paraboloids of revolution for focusing X-rays in two dimensions simultaneously are reported. The lenses were manufactured using a femtosecond laser micromachining process and tested using X-ray synchrotron radiation. Such lenses were stacked together to form a standard compound refractive lens (CRL). Owing to the superior physical properties of the material, diamond CRLs could become indispensable wavefront-preserving primary focusing optics for X-ray free-electron lasers and the next-generation synchrotron storage rings. They can be used for highly efficient refocusing of the extremely bright X-ray sources formore » secondary optical schemes with limited aperture such as nanofocusing Fresnel zone plates and multilayer Laue lenses.« less

Study of the physical properties of a mesogenic mixture showing induced smectic A(d) phase by refractive index, density and x-ray diffraction measurements.

PubMed

Roy, P D; Prasad, A; Das, M K

2009-02-18

The binary mixture of 4-n-pentyl phenyl 4-n'-hexyloxy benzoate (ME6O.5) and p-cyanophenyl trans-4-pentyl cyclohexane carboxylate (CPPCC) shows the presence of an induced smectic A(d) phase in a certain concentration range 0.03<x(CPPCC)<0.6. The results of the differential scanning calorimetry (DSC), refractive indices, densities and x-ray diffraction measurements are reported here. In general, the change in birefringence is continuous at the smectic A(d) to nematic phase transition for mixtures with x>0.33, whereas there is a discontinuity in these values for mixtures with x<0.33, consistent with the density and transition entropy measurements done on this system. The orientational order parameter, measured from x-ray diffraction studies, are somewhat smaller than those obtained from refractive index measurement in the induced smectic phase for all the mixtures. In the smectic phase, the OOP values initially increases with molar concentration up to x = 0.24 and then decreases showing a broad minima around x = 0.4. The variation of layer thickness in the induced smectic phase with composition has been explained by assuming the formation of homo- and heterodimers. We conclude that the possible packing of molecules in the induced smectic A(d) phase stabilizes the layers but increases the orientational free volume, consistent with the lower orientational order parameter.

High resolution imaging and lithography with hard x rays using parabolic compound refractive lenses

NASA Astrophysics Data System (ADS)

Schroer, C. G.; Benner, B.; Günzler, T. F.; Kuhlmann, M.; Zimprich, C.; Lengeler, B.; Rau, C.; Weitkamp, T.; Snigirev, A.; Snigireva, I.; Appenzeller, J.

2002-03-01

Parabolic compound refractive lenses are high quality optical components for hard x rays. They are particularly suited for full field imaging, with applications in microscopy and x-ray lithography. Taking advantage of the large penetration depth of hard x rays, the interior of opaque samples can be imaged with submicrometer resolution. To obtain the three-dimensional structure of a sample, microscopy is combined with tomographic techniques. In a first hard x-ray lithography experiment, parabolic compound refractive lenses have been used to project the reduced image of a lithography mask onto a resist. Future developments are discussed.

Compound refractive lenses as prefocusing optics for X-ray FEL radiation

DOE PAGES

Heimann, Philip; MacDonald, Michael; Nagler, Bob; ...

2016-01-27

The performance of X-ray free-electron laser beamlines may be limited by the angular aperture. Compound refractive lenses (CRLs) can be employed to prefocus the X-ray beam, thereby increasing the beamline transmission. A prefocusing CRL was implemented in the X-ray transport of the Matter under Extreme Conditions Instrument at the Linac Coherent Light Source. A significant improvement in the beamline transmission was calculated over the 3–10 keV photon energy range. At 5 keV, the relative X-ray intensity was measured and a factor of four increase was seen in the beamline transmission. As a result, the X-ray focus was also determined bymore » the ablation imprint method.« less

Measuring the Index of Refraction.

ERIC Educational Resources Information Center

Phelps, F. M., III; Jacobson, B. S.

1980-01-01

Presents two methods for measuring the index of refraction of glass or lucite. These two methods, used in the freshman laboratory, are based on the fact that a ray of light inside a block will be refracted parallel to the surface. (HM)

Lithium metal for x-ray filters and refractive optics

NASA Astrophysics Data System (ADS)

Pereira, N. R.; Dufresne, Eric; Dierker, Steve

2001-04-01

Lithium is the most x-ray transparent solid element. Lithium is very stable in dry air with a dew point below -50 C or so, but as the humidity increases lithium starts to react with the air's nitrogen and oxygen. Under usual laboratory conditions a shiny piece of lithium metal becomes a white powder within the hour, preventing lithium's widespread use in x-ray work. Use of lithium as a window for pulsed x-rays demands that lithium withstands corrosion in open air for at least 15 minutes. Protection by a one micron layer of parylene turns out to be enough. Although parylene absorbs soft x-rays 12 times more than lithium, the parylene layer can remain in place for the window application. Lithium is also ideal for refractive x-ray lenses. We are evaluating the performance of such lenses with 10 keV photons from the MHATT-CAT beam line at the Advanced Photon Source. These measurements are in progress: the paper will show the results from these measurements as available.

Diffractive-refractive optics: X-ray splitter.

PubMed

Hrdý, Jaromír

2010-01-01

The possibility of splitting a thin (e.g. undulator) X-ray beam based on diffraction-refraction effects is discussed. The beam is diffracted from a crystal whose diffracting surface has the shape of a roof with the ridge lying in the plane of diffraction. The crystal is cut asymmetrically. One half of the beam impinges on the left-hand part of the roof and the other half impinges on the right-hand side of the roof. Owing to refraction the left part of the beam is deviated to the left whereas the right part is deviated to the right. The device proposed consists of two channel-cut crystals with roof-like diffraction surfaces; the crystals are set in a dispersive position. The separation of the beams after splitting is calculated at a distance of 10 m from the crystals for various asymmetry and inclination angles. It is shown that such a splitting may be utilized for long beamlines. Advantages and disadvantages of this method are discussed.

Single-shot Z(eff) dense plasma diagnostic through simultaneous refraction and attenuation measurements with a Talbot-Lau x-ray moiré deflectometer.

PubMed

Valdivia, M P; Stutman, D; Finkenthal, M

2015-04-01

The Talbot-Lau x-ray moiré deflectometer is a powerful plasma diagnostic capable of delivering simultaneous refraction and attenuation information through the accurate detection of x-ray phase shift and intensity. The diagnostic can provide the index of refraction n=1-δ+iβ of an object (dense plasma, for example) placed in the x-ray beam by independently measuring both δ and β, which are directly related to the electron density n(e) and the attenuation coefficient μ, respectively. Since δ and β depend on the effective atomic number Z(eff), a map can be obtained from the ratio between phase and absorption images acquired in a single shot. The Talbot-Lau x-ray moiré deflectometer and its corresponding data acquisition and processing are briefly described to illustrate how the above is achieved; Z(eff) values of test objects within the 4-12 range were obtained experimentally through simultaneous refraction and attenuation measurements. We show that Z(eff) mapping of objects does not require previous knowledge of sample length or shape. The determination of Z(eff) from refraction and attenuation measurements with moiré deflectometry could be of high interest to various domains of high energy density research, such as shocked materials and inertial confinement fusion experiments, as well as material science and nondestructive testing.

Single-shot Z eff dense plasma diagnostic through simultaneous refraction and attenuation measurements with a Talbot–Lau x-ray moiré deflectometer

DOE PAGES

Valdivia, M. P.; Stutman, D.; Finkenthal, M.

2015-03-23

The Talbot–Lau x-ray moiré deflectometer is a powerful plasma diagnostic capable of delivering simultaneous refraction and attenuation information through the accurate detection of x-ray phase shift and intensity. The diagnostic can provide the index of refraction n=1₋δ + iβ of an object (dense plasma, for example) placed in the x-ray beam by independently measuring both δ and β, which are directly related to the electron density n e and the attenuation coefficient μ respectively. Since δ and β depend on the effective atomic number Z eff, a map can be obtained from the ratio between phase and absorption images acquiredmore » in a single shot. The Talbot–Lau x-ray moiré deflectometer and its corresponding data acquisition and processing are briefly described to illustrate how the above is achieved; Z eff values of test objects within the 4₋12 range were obtained experimentally through simultaneous refraction and attenuation measurements. We show that Z eff mapping of objects does not require previous knowledge of sample length or shape. In conclusion, the determination of Z eff from refraction and attenuation measurements with moiré deflectometry could be of high interest to various domains of high energy density research, such as shocked materials and inertial confinement fusion experiments, as well as material science and nondestructive testing.« less

Single-shot Z eff dense plasma diagnostic through simultaneous refraction and attenuation measurements with a Talbot–Lau x-ray moiré deflectometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Valdivia, M. P.; Stutman, D.; Finkenthal, M.

The Talbot–Lau x-ray moiré deflectometer is a powerful plasma diagnostic capable of delivering simultaneous refraction and attenuation information through the accurate detection of x-ray phase shift and intensity. The diagnostic can provide the index of refraction n=1₋δ + iβ of an object (dense plasma, for example) placed in the x-ray beam by independently measuring both δ and β, which are directly related to the electron density n e and the attenuation coefficient μ respectively. Since δ and β depend on the effective atomic number Z eff, a map can be obtained from the ratio between phase and absorption images acquiredmore » in a single shot. The Talbot–Lau x-ray moiré deflectometer and its corresponding data acquisition and processing are briefly described to illustrate how the above is achieved; Z eff values of test objects within the 4₋12 range were obtained experimentally through simultaneous refraction and attenuation measurements. We show that Z eff mapping of objects does not require previous knowledge of sample length or shape. In conclusion, the determination of Z eff from refraction and attenuation measurements with moiré deflectometry could be of high interest to various domains of high energy density research, such as shocked materials and inertial confinement fusion experiments, as well as material science and nondestructive testing.« less

Diffractive-refractive optics: (+,-,-,+) X-ray crystal monochromator with harmonics separation.

PubMed

Hrdý, Jaromír; Mikulík, Petr; Oberta, Peter

2011-03-01

A new kind of two channel-cut crystals X-ray monochromator in dispersive (+,-,-,+) position which spatially separates harmonics is proposed. The diffracting surfaces are oriented so that the diffraction is inclined. Owing to refraction the diffracted beam is sagittally deviated. The deviation depends on wavelength and is much higher for the first harmonics than for higher harmonics. This leads to spatial harmonics separation. The idea is supported by ray-tracing simulation.

First refraction contrast imaging via Laser-Compton Scattering X-ray at KEK

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sakaue, Kazuyuki; Aoki, Tatsuro; Washio, Masakazu

2012-07-31

Laser-Compton Scattering (LCS) is one of the most feasible techniques for high quality, high brightness, and compact X-ray source. High energy electron beam produced by accelerators scatters off the laser photon at a small spot. As a laser target, we have been developing a pulsedlaser storage cavity for increasing an X-ray flux. The X-ray flux was still inadequate that was 2.1 Multiplication-Sign 10{sup 5}/sec, however, we performed first refraction contrast imaging in order to evaluate the quality of LCS X-ray. Edge enhanced contrast imaging was achieved by changing the distance from sample to detector. The edge enhancement indicates that themore » LCS X-ray has small source size, i.e. high brightness. We believe that the result has demonstrated good feasibility of linac-based high brightness X-ray sources via laser-electron Compton scatterings.« less

Refraction-based X-ray Computed Tomography for Biomedical Purpose Using Dark Field Imaging Method

NASA Astrophysics Data System (ADS)

Sunaguchi, Naoki; Yuasa, Tetsuya; Huo, Qingkai; Ichihara, Shu; Ando, Masami

We have proposed a tomographic x-ray imaging system using DFI (dark field imaging) optics along with a data-processing method to extract information on refraction from the measured intensities, and a reconstruction algorithm to reconstruct a refractive-index field from the projections generated from the extracted refraction information. The DFI imaging system consists of a tandem optical system of Bragg- and Laue-case crystals, a positioning device system for a sample, and two CCD (charge coupled device) cameras. Then, we developed a software code to simulate the data-acquisition, data-processing, and reconstruction methods to investigate the feasibility of the proposed methods. Finally, in order to demonstrate its efficacy, we imaged a sample with DCIS (ductal carcinoma in situ) excised from a breast cancer patient using a system constructed at the vertical wiggler beamline BL-14C in KEK-PF. Its CT images depicted a variety of fine histological structures, such as milk ducts, duct walls, secretions, adipose and fibrous tissue. They correlate well with histological sections.

Nanofocusing with aberration-corrected rotationally parabolic refractive X-ray lenses

DOE PAGES

Seiboth, Frank; Wittwer, Felix; Scholz, Maria; ...

2018-01-01

Wavefront errors of rotationally parabolic refractive X-ray lenses made of beryllium (Be CRLs) have been recovered for various lens sets and X-ray beam configurations. Due to manufacturing via an embossing process, aberrations of individual lenses within the investigated ensemble are very similar. By deriving a mean single-lens deformation for the ensemble, aberrations of any arbitrary lens stack can be predicted from the ensemble with σ¯ = 0.034λ. Using these findings the expected focusing performance of current Be CRLs are modeled for relevant X-ray energies and bandwidths and it is shown that a correction of aberrations can be realised without priormore » lens characterization but simply based on the derived lens deformation. As a result, the performance of aberration-corrected Be CRLs is discussed and the applicability of aberration-correction demonstrated over wide X-ray energy ranges.« less

Further Studies on the Effect of SiN x Refractive Index and Emitter Sheet Resistance on Potential-Induced Degradation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Oh, Jaewon; Dauksher, Bill; Bowden, Stuart

We present the impacts of silicon nitride (SiNx) antireflection coating refractive index and emitter sheet resistance on potential-induced degradation of the shunting type (PID-s). Previously, it has been shown that the cell becomes more PID-s-susceptible as the refractive index decreases or the emitter sheet resistance increases. To verify the effect of refractive index on PID-s, we fabricated cells with varying SiN x refractive index (1.87, 1.94, 2.05) on typical p-type base solar cells with ~60 Ω/sq emitters. However, none of these cells showed output power degradation, regardless of the refractive index. Further investigation of the emitter showed that the PID-smore » was suppressed at ~60 Ω/sq due to the extremely high surface phosphorus concentration (6 x 10 21 cm -3), as measured by secondary ion mass spectrometry. Furthermore, PID-s was observed on cells possessing a high emitter sheet resistance (~80 Ω/sq). In conclusion, the emitter surface phosphorus concentration plays an important role in determining PID-s susceptibility.« less

Further Studies on the Effect of SiN x Refractive Index and Emitter Sheet Resistance on Potential-Induced Degradation

DOE PAGES

Oh, Jaewon; Dauksher, Bill; Bowden, Stuart; ...

2017-01-11

We present the impacts of silicon nitride (SiNx) antireflection coating refractive index and emitter sheet resistance on potential-induced degradation of the shunting type (PID-s). Previously, it has been shown that the cell becomes more PID-s-susceptible as the refractive index decreases or the emitter sheet resistance increases. To verify the effect of refractive index on PID-s, we fabricated cells with varying SiN x refractive index (1.87, 1.94, 2.05) on typical p-type base solar cells with ~60 Ω/sq emitters. However, none of these cells showed output power degradation, regardless of the refractive index. Further investigation of the emitter showed that the PID-smore » was suppressed at ~60 Ω/sq due to the extremely high surface phosphorus concentration (6 x 10 21 cm -3), as measured by secondary ion mass spectrometry. Furthermore, PID-s was observed on cells possessing a high emitter sheet resistance (~80 Ω/sq). In conclusion, the emitter surface phosphorus concentration plays an important role in determining PID-s susceptibility.« less

Effects of refractive index mismatch in optical CT imaging of polymer gel dosimeters.

PubMed

Manjappa, Rakesh; Makki S, Sharath; Kumar, Rajesh; Kanhirodan, Rajan

2015-02-01

Proposing an image reconstruction technique, algebraic reconstruction technique-refraction correction (ART-rc). The proposed method takes care of refractive index mismatches present in gel dosimeter scanner at the boundary, and also corrects for the interior ray refraction. Polymer gel dosimeters with high dose regions have higher refractive index and optical density compared to the background medium, these changes in refractive index at high dose results in interior ray bending. The inclusion of the effects of refraction is an important step in reconstruction of optical density in gel dosimeters. The proposed ray tracing algorithm models the interior multiple refraction at the inhomogeneities. Jacob's ray tracing algorithm has been modified to calculate the pathlengths of the ray that traverses through the higher dose regions. The algorithm computes the length of the ray in each pixel along its path and is used as the weight matrix. Algebraic reconstruction technique and pixel based reconstruction algorithms are used for solving the reconstruction problem. The proposed method is tested with numerical phantoms for various noise levels. The experimental dosimetric results are also presented. The results show that the proposed scheme ART-rc is able to reconstruct optical density inside the dosimeter better than the results obtained using filtered backprojection and conventional algebraic reconstruction approaches. The quantitative improvement using ART-rc is evaluated using gamma-index. The refraction errors due to regions of different refractive indices are discussed. The effects of modeling of interior refraction in the dose region are presented. The errors propagated due to multiple refraction effects have been modeled and the improvements in reconstruction using proposed model is presented. The refractive index of the dosimeter has a mismatch with the surrounding medium (for dry air or water scanning). The algorithm reconstructs the dose profiles by estimating

Silicon saw-tooth refractive lens for high-energy x-rays made using a diamond saw.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Said, A. H.; Shastri, S. D.; X-Ray Science Division

2010-01-01

Silicon is a material well suited for refractive lenses operating at high X-ray energies (>50 keV), particularly if implemented in a single-crystal form to minimize small-angle scattering. A single-crystal silicon saw-tooth refractive lens, fabricated by a dicing process using a thin diamond wheel, was tested with 115 keV X-rays, giving an ideal 17 {mu}m line focus width in a long focal length, 2:1 ratio demagnification geometry, with a source-to-focus distance of 58.5 m. The fabrication is simple, using resources typically available at any synchrotron facility's optics shop.

Focusing properties of x-ray polymer refractive lenses from SU-8 resist layer

NASA Astrophysics Data System (ADS)

Snigirev, Anatoly A.; Snigireva, Irina; Drakopoulos, Michael; Nazmov, Vladimir; Reznikova, Elena; Kuznetsov, Sergey; Grigoriev, Maxim; Mohr, Jurgen; Saile, Volker

2003-12-01

Compound refractive lenses printed in Al and Be are becoming the key X-ray focusing and imaging components of beamline optical layouts at the 3rd generation synchrotron radiation sources. Recently proposed planar optical elements based on Si, diamond etc. may substantially broaden the spectrum of the refractive optics applicability. Planar optics has focal distances ranging from millimeters to tens of meters offering nano- and micro-focusing lenses, as well as beam condensers and collimators. Here we promote deep X-ray lithography and LIGA-type techniques to create high aspect-ratio lens structures for different optical geometries. Planar X-ray refractive lenses were manufactured in 1 mm thick SU-8 negative resist layer by means of deep synchrotron radiation lithography. The focusing properties of lenses were studied at ID18F and BM5 beamlines at the ESRF using monochromatic radiation in the energy range of 10 - 25 keV. By optimizing lens layout, mask making and resist processing, lenses of good quality were fabricated. The resolution of about 270 nm (FWHM) with gain in the order of 300 was measured at 14 keV. In-line holography of B-fiber was realized in imaging and projection mode with a magnification of 3 and 20, respectively. Submicron features of the fiber were clearly resolved. A radiation stability test proved that the fabricated lenses don't change focusing characteristics after dose of absorbed X-ray radiation of about 2 MJ/cm3. The unique radiation stability along with the high effficiency of SU8 lenses opens wide range of their synchrotron radiation applications such as microfocusing elements, condensers and collimators.

Effects of refractive index mismatch in optical CT imaging of polymer gel dosimeters

DOE Office of Scientific and Technical Information (OSTI.GOV)

Manjappa, Rakesh; Makki S, Sharath; Kanhirodan, Rajan, E-mail: rajan@physics.iisc.ernet.in

2015-02-15

Purpose: Proposing an image reconstruction technique, algebraic reconstruction technique-refraction correction (ART-rc). The proposed method takes care of refractive index mismatches present in gel dosimeter scanner at the boundary, and also corrects for the interior ray refraction. Polymer gel dosimeters with high dose regions have higher refractive index and optical density compared to the background medium, these changes in refractive index at high dose results in interior ray bending. Methods: The inclusion of the effects of refraction is an important step in reconstruction of optical density in gel dosimeters. The proposed ray tracing algorithm models the interior multiple refraction at themore » inhomogeneities. Jacob’s ray tracing algorithm has been modified to calculate the pathlengths of the ray that traverses through the higher dose regions. The algorithm computes the length of the ray in each pixel along its path and is used as the weight matrix. Algebraic reconstruction technique and pixel based reconstruction algorithms are used for solving the reconstruction problem. The proposed method is tested with numerical phantoms for various noise levels. The experimental dosimetric results are also presented. Results: The results show that the proposed scheme ART-rc is able to reconstruct optical density inside the dosimeter better than the results obtained using filtered backprojection and conventional algebraic reconstruction approaches. The quantitative improvement using ART-rc is evaluated using gamma-index. The refraction errors due to regions of different refractive indices are discussed. The effects of modeling of interior refraction in the dose region are presented. Conclusions: The errors propagated due to multiple refraction effects have been modeled and the improvements in reconstruction using proposed model is presented. The refractive index of the dosimeter has a mismatch with the surrounding medium (for dry air or water scanning). The

Fabrication process for a gradient index x-ray lens

DOEpatents

Bionta, R.M.; Makowiecki, D.M.; Skulina, K.M.

1995-01-17

A process is disclosed for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments in the soft x-ray region. 13 figures.

Fabrication process for a gradient index x-ray lens

DOEpatents

Bionta, Richard M.; Makowiecki, Daniel M.; Skulina, Kenneth M.

1995-01-01

A process for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments m the soft x-ray region.

Compensation of X-ray mirror shape-errors using refractive optics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sawhney, Kawal, E-mail: Kawal.sawhney@diamond.ac.uk; Laundy, David; Pape, Ian

2016-08-01

Focusing of X-rays to nanometre scale focal spots requires high precision X-ray optics. For nano-focusing mirrors, height errors in the mirror surface retard or advance the X-ray wavefront and after propagation to the focal plane, this distortion of the wavefront causes blurring of the focus resulting in a limit on the spatial resolution. We describe here the implementation of a method for correcting the wavefront that is applied before a focusing mirror using custom-designed refracting structures which locally cancel out the wavefront distortion from the mirror. We demonstrate in measurements on a synchrotron radiation beamline a reduction in the sizemore » of the focal spot of a characterized test mirror by a factor of greater than 10 times. This technique could be used to correct existing synchrotron beamline focusing and nanofocusing optics providing a highly stable wavefront with low distortion for obtaining smaller focus sizes. This method could also correct multilayer or focusing crystal optics allowing larger numerical apertures to be used in order to reduce the diffraction limited focal spot size.« less

Microscope using an x-ray tube and a bubble compound refractive lens

NASA Astrophysics Data System (ADS)

Piestrup, M. A.; Gary, C. K.; Park, H.; Harris, J. L.; Cremer, J. T.; Pantell, R. H.; Dudchik, Y. I.; Kolchevsky, N. N.; Komarov, F. F.

2005-03-01

We present x-ray images of grid meshes and biological material obtained using an unfiltered x-ray tube and a compound refractive lens composed of microbubbles embedded in epoxy inside a glass capillary. Images obtained using this apparatus are compared with those using a synchrotron source and the same lens. We find that the field of view is larger than that obtained using the synchrotron source, whereas the contrast and resolution are reduced. Geometrical distortion around the edges of the field of view is also reduced. The experiments demonstrate the usefulness of the apparatus in a modest laboratory setting.

Hard X-ray full field microscopy and magnifying microtomography using compound refractive lenses

NASA Astrophysics Data System (ADS)

Schroer, Christian G.; Günzler, Til Florian; Benner, Boris; Kuhlmann, Marion; Tümmler, Johannes; Lengeler, Bruno; Rau, Christoph; Weitkamp, Timm; Snigirev, Anatoly; Snigireva, Irina

2001-07-01

For hard X-rays, parabolic compound refractive lenses (PCRLs) are genuine imaging devices like glass lenses for visible light. Based on these new lenses, a hard X-ray full field microscope has been constructed that is ideally suited to image the interior of opaque samples with a minimum of sample preparation. As a result of a large depth of field, CRL micrographs are sharp projection images of most samples. To obtain 3D information about a sample, tomographic techniques are combined with magnified imaging.

Rapid assessment of mid-infrared refractive index anisotropy using a prism coupler: chemical vapor deposited ZnS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Qiao, Hong; Lipschultz, Kristen A.; Anheier, Norman C.

2012-04-01

A state-of-the-art mid-infrared prism coupler was used to study the refractive index properties of forward-looking-infrared (FLIR) grade zinc sulfide samples prepared with unique planar grain orientations and locations with respect to the CVD growth axis. This study was motivated by prior photoluminescence and x-ray diffraction measurements that suggested refractive index may vary according to grain orientation. Measurements were conducted to provide optical dispersion and thermal index (dn/dT) data at discrete laser wavelengths between 0.633 and 10.591 {mu}m at two temperature set points (30 C and 90 C). Refractive index measurements between samples exhibited an average standard deviation comparable to themore » uncertainty of the prism coupler measurement (0.0004 refractive index units), suggesting that the variation in refractive index as a function of planar grain orientation and CVD deposition time is negligible, and should have no impact on subsequent optical designs. Measured dispersion data at mid-infrared wavelengths was found to agree well with prior published measurements.« less

The eye lens: age-related trends and individual variations in refractive index and shape parameters.

PubMed

Pierscionek, Barbara; Bahrami, Mehdi; Hoshino, Masato; Uesugi, Kentaro; Regini, Justyn; Yagi, Naoto

2015-10-13

The eye lens grows throughout life by cell accrual on its surface and can change shape to adjust the focussing power of the eye. Varying concentrations of proteins in successive cell layers create a refractive index gradient. The continued growth of the lens and age-related changes in proteins render it less able to alter shape with loss of capacity by the end of the sixth decade of life. Growth and protein ageing alter the refractive index but as accurate measurement of this parameter is difficult, the nature of such alterations remains uncertain. The most accurate method to date for measuring refractive index in intact lenses has been developed at the SPring-8 synchrotron. The technique, based on Talbot interferometry, has an X-ray source and was used to measure refractive index in sixty-six human lenses, aged from 16 to 91 years. Height and width were measured for forty-five lenses. Refractive index contours show decentration in some older lenses but individual variations mask age-related trends. Refractive index profiles along the optic axis have relatively flat central sections with distinct micro-fluctuations and a steep gradient in the cortex but do not exhibit an age-related trend. The refractive index profiles in the equatorial aspect show statistical significance with age, particularly for lenses below the age of sixty that had capacity to alter shape in vivo. The maximum refractive index in the lens centre decreases slightly with age with considerable scatter in the data and there are age-related variations in sagittal thickness and equatorial height.

The eye lens: age-related trends and individual variations in refractive index and shape parameters

PubMed Central

Pierscionek, Barbara; Bahrami, Mehdi; Hoshino, Masato; Uesugi, Kentaro; Regini, Justyn; Yagi, Naoto

2015-01-01

The eye lens grows throughout life by cell accrual on its surface and can change shape to adjust the focussing power of the eye. Varying concentrations of proteins in successive cell layers create a refractive index gradient. The continued growth of the lens and age-related changes in proteins render it less able to alter shape with loss of capacity by the end of the sixth decade of life. Growth and protein ageing alter the refractive index but as accurate measurement of this parameter is difficult, the nature of such alterations remains uncertain. The most accurate method to date for measuring refractive index in intact lenses has been developed at the SPring-8 synchrotron. The technique, based on Talbot interferometry, has an X-ray source and was used to measure refractive index in sixty-six human lenses, aged from 16 to 91 years. Height and width were measured for forty-five lenses. Refractive index contours show decentration in some older lenses but individual variations mask age-related trends. Refractive index profiles along the optic axis have relatively flat central sections with distinct micro-fluctuations and a steep gradient in the cortex but do not exhibit an age-related trend. The refractive index profiles in the equatorial aspect show statistical significance with age, particularly for lenses below the age of sixty that had capacity to alter shape in vivo. The maximum refractive index in the lens centre decreases slightly with age with considerable scatter in the data and there are age-related variations in sagittal thickness and equatorial height. PMID:26416418

1D silicon refractive lenses for surface scattering with high energy x-rays

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bertram, F.; Gutowski, O.; Schroer, C.

2016-07-27

At the high energy X-ray beamline P07 at PETRA III, 1D focusing down to 4 micrometer vertical beam height while preserving a horizontal beam width of 0.5 mm was established by refractive lenses etched into a silicon wafer. A single wafer with 8 different lens structures can cover the full energy range between 50 and 120 keV. For surface diffraction on ultrathin films a factor of 4 in intensity can be achieved compared to the already established Al-compound refractive 2D-lenses.

Parabolic single-crystal diamond compound refractive lenses for coherent x-ray imaging (Conference Presentation)

NASA Astrophysics Data System (ADS)

Terentyev, Sergey; Blank, Vladimir D.; Polyakov, Sergey; Zholudev, Sergey; Snigirev, Anatoly A.; Polikarpov, Maxim; Kolodziej, Tomasz; Qian, Jun; Zhou, Hua; Shvyd'ko, Yuri V.

2016-09-01

We demonstrate parabolic single-crystal diamond compound refractive lenses [1] designed for coherent x-ray imaging resilient to extreme thermal and radiation loading expected from next generation light sources. To ensure the preservation of coherence and resilience, the lenses are manufactured from the highest-quality single-crystalline synthetic diamond material grown by a high-pressure high-temperature technique. Picosecond laser milling is applied to machine lenses to parabolic shapes with a 1-micron precision and surface roughness. A compound refractive lens comprised of six lenses with a radius of curvature R=200 microns at the vertex of the parabola and a geometrical aperture A=900 microns focuses 10 keV x-ray photons from an undulator source at the Advanced Photon Source facility to a focal spot size of 10x40 microns^2 with a gain factor of 100. [1] S. Terentyev, V. Blank, S. Polyakov, S. Zholudev, A. Snigirev, M. Polikarpov, T. Kolodziej, J. Qian, H. Zhou, and Yu. Shvyd'ko Applied Physics Letters 107, 111108 (2015); doi: 10.1063/1.4931357

FIBER OPTICS: Ray invariants and wave equations for transverse modes in three-dimensional graded-index waveguides

NASA Astrophysics Data System (ADS)

Voevodin, V. G.; Morozov, A. N.; Stepanov, V. E.

1992-09-01

A theory of the second ray invariant is proposed using the theory of plane Frenet curves. Its existence requires that the coordinate dependence of the refractive index in the waveguide cross section should satisfy the regularity condition: curves of equal refractive index differ only by an amount which can be obtained using an isotropic scaling transformation. The theoretical conclusions are illustrated using the example of waveguides having the generalized refractive index distribution n ( r ) = n [ (x/ a) + (y/ b)q].

Observation of human tissue with phase-contrast x-ray computed tomography

NASA Astrophysics Data System (ADS)

Momose, Atsushi; Takeda, Tohoru; Itai, Yuji; Tu, Jinhong; Hirano, Keiichi

1999-05-01

Human tissues obtained from cancerous kidneys fixed in formalin were observed with phase-contrast X-ray computed tomography (CT) using 17.7-keV synchrotron X-rays. By measuring the distributions of the X-ray phase shift caused by samples using an X-ray interferometer, sectional images that map the distribution of the refractive index were reconstructed. Because of the high sensitivity of phase- contrast X-ray CT, a cancerous lesion was differentiated from normal tissue and a variety of other structures were revealed without the need for staining.

Non-uniform refractive index field measurement based on light field imaging technique

NASA Astrophysics Data System (ADS)

Du, Xiaokun; Zhang, Yumin; Zhou, Mengjie; Xu, Dong

2018-02-01

In this paper, a method for measuring the non-uniform refractive index field based on the light field imaging technique is proposed. First, the light field camera is used to collect the four-dimensional light field data, and then the light field data is decoded according to the light field imaging principle to obtain image sequences with different acquisition angles of the refractive index field. Subsequently PIV (Particle Image Velocimetry) technique is used to extract ray offset of each image. Finally, the distribution of non-uniform refractive index field can be calculated by inversing the deflection of light rays. Compared with traditional optical methods which require multiple optical detectors from multiple angles to synchronously collect data, the method proposed in this paper only needs a light field camera and shoot once. The effectiveness of the method has been verified by the experiment which quantitatively measures the distribution of the refractive index field above the flame of the alcohol lamp.

Ray tracing matrix approach for refractive index mismatch aberrations in confocal microscopy.

PubMed

Nastyshyn, S Yu; Bolesta, I M; Lychkovskyy, E; Vankevych, P I; Yakovlev, M Yu; Pansu, B; Nastishin, Yu A

2017-03-20

The 2×2 ray tracing matrix (RTM) method is employed for the description of optical aberrations caused by the refractive index mismatch (RIM) in fluorescent confocal polarization microscopy. We predict and experimentally confirm that due to the RIM a liquid crystal layer with highly non-uniform director distribution appears to be imaged as a layer with non-uniform thickness, which shows up in the roughness of the rear surface. For the off-axial focusing of the probing beam in a droplet dispersed in an immiscible liquid, we have developed an extended method still keeping the 2×2 dimensionality of the RTM.

Resolution of x-ray parabolic compound refractive diamond lens defined at the home laboratory

NASA Astrophysics Data System (ADS)

Polyakov, S. N.; Zholudev, S. I.; Gasilov, S. V.; Martyushov, S. Yu.; Denisov, V. N.; Terentiev, S. A.; Blank, V. D.

2017-05-01

Here we demonstrate performance of an original lab system designed for testing of X-ray parabolic compound refractive lenses (CRL) manufactured from a high-quality single-crystalline synthetic diamond grown by the high-pressure hightemperature technique. The basic parameters of a diamond CRL comprised from 28 plano-concave lenses such as the focal length of 634 mm, transmissivity of 0.36, field of view of 1 mm and resolution of 6 µm have been determined. Usually such measurements are performed on synchrotron radiation facilities. In this work characterization of CRL was performed by means of instruments and components that are available for laboratories such as the Rigaku 9kW rotating anode X-ray generator, the PANalytical parallel beam X-ray mirror, a 6 m long optical bench, high precision multi-axis goniometers, high resolution X-ray emulsion films, and ultra-fast high-sensitive X-ray area detector PIXel3D. Developed setup was used to find differences between experimental and design parameters, which is very important for the improvement of CRLs manufacturing technology.

THz conductivities of indium-tin-oxide nanowhiskers as a graded-refractive-index structure.

PubMed

Yang, Chan-Shan; Chang, Chia-Hua; Lin, Mao-Hsiang; Yu, Peichen; Wada, Osamu; Pan, Ci-Ling

2012-07-02

Indium-tin-oxide (ITO) nanowhiskers with attractive electrical and anti-reflection properties were prepared by the glancing-angle electron-beam evaporation technique. Structural and crystalline properties of such nanostructures were examined by scanning transmission electron microscopy and X-ray diffraction. Their frequency-dependent complex conductivities, refractive indices and absorption coefficients have been characterized with terahertz time-domain spectroscopy (THz-TDS), in which the nanowhiskers were considered as a graded-refractive-index (GRIN) structure instead of the usual thin film model. The electrical properties of ITO GRIN structures are analyzed and fitted well with Drude-Smith model in the 0.2~2.0 THz band. Our results indicate that the ITO nanowhiskers and its bottom layer atop the substrate exhibit longer carrier scattering times than ITO thin films. This signifies that ITO nanowhiskers have an excellent crystallinity with large grain size, consistent with X-ray data. Besides, we show a strong backscattering effect and fully carrier localization in the ITO nanowhiskers.

Temperature-dependent Absolute Refractive Index Measurements of Synthetic Fused Silica

NASA Technical Reports Server (NTRS)

Leviton, Douglas B.; Frey, Bradley J.

2006-01-01

Using the Cryogenic, High-Accuracy Refraction Measuring System (CHARMS) at NASA's Goddard Space Flight Center, we have measured the absolute refractive index of five specimens taken from a very large boule of Corning 7980 fused silica from temperatures ranging from 30 to 310 K at wavelengths from 0.4 to 2.6 microns with an absolute uncertainty of plus or minus 1 x 10 (exp -5). Statistical variations in derived values of the thermo-optic coefficient (dn/dT) are at the plus or minus 2 x 10 (exp -8)/K level. Graphical and tabulated data for absolute refractive index, dispersion, and thermo-optic coefficient are presented for selected wavelengths and temperatures along with estimates of uncertainty in index. Coefficients for temperature-dependent Sellmeier fits of measured refractive index are also presented to allow accurate interpolation of index to other wavelengths and temperatures. We compare our results to those from an independent investigation (which used an interferometric technique for measuring index changes as a function of temperature) whose samples were prepared from the same slugs of material from which our prisms were prepared in support of the Kepler mission. We also compare our results with sparse cryogenic index data from measurements of this material from the literature.

Measurement of refractive index profile of non-symmetric, complex silica preforms with high refractive index differences

NASA Astrophysics Data System (ADS)

Probostova, Jana; Slanicka, Jiri; Mrazek, Jan; Podrazky, Ondrej; Benda, Adam; Peterka, Pavel

2016-04-01

Refractive index profile measurement is a key instrument for characterization of optical properties of preforms, which are used for drawing of high-quality optical fibers. Common industrial optical preform analyzers have been designed for measurement of simple symmetric structures such as step-index or graded-index preforms with refractive index close to the silica (n=1.457 at 633 nm). However, these conditions are usually far from more complex structures used in fiber lasers or in fiber sensor area. Preforms for the drawing of advanced optical fibers, such as Bragg, microstructure or photonic crystal fibers, are usually constituted from stacks with non-symmetric internal structure or composed of alternating layers with high refractive index contrasts. In this paper we present comparison of refractive index profile measurements of simple as well as complex structures with high refractive index differences simulating the Bragg structures. Commercial Photon Kinetics 2600 preform analyzer was used for the refractive index profile measurements. A set of concentrically arranged silica tubes was welded to form a complex preforms. Free space between the tubes was filled by immersion with varying refractive indices to simulate the Bragg structure. Up to three tubes were used for the analysis and the refractive indices of immersion were changed from 1.4 to 1.5. When refractive index of immersion was independently measured the structure of preform was defined. Profiles of these "known" structures were compared to measured data processed by originally proposed algorithm. The work provides an extension of issues of refractive index profile measurements in non-symmetric complex silica structures by a commercial preform analyzer and proposes more convenient methods of numeric data processing.

High-energy x-ray optics with silicon saw-tooth refractive lenses.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shastri, S. D.; Almer, J. A.; Ribbing, C. R.

2007-01-01

Silicon saw-tooth refractive lenses have been in successful use for vertical focusing and collimation of high-energy X-rays (50-100 keV) at the 1-ID undulator beamline of the Advanced Photon Source. In addition to presenting an effectively parabolic thickness profile, as required for aberration-free refractive optics, these devices allow high transmission and continuous tunability in photon energy and focal length. Furthermore, the use of a single-crystal material (i.e. Si) minimizes small-angle scattering background. The focusing performance of such saw-tooth lenses, used in conjunction with the 1-ID beamline's bent double-Laue monochromator, is presented for both short ({approx}1:0.02) and long ({approx}1:0.6) focal-length geometries, givingmore » line-foci in the 2 {micro}m-25 {micro}m width range with 81 keV X-rays. In addition, a compound focusing scheme was tested whereby the radiation intercepted by a distant short-focal-length lens is increased by having it receive a collimated beam from a nearer (upstream) lens. The collimation capabilities of Si saw-tooth lenses are also exploited to deliver enhanced throughput of a subsequently placed small-angular-acceptance high-energy-resolution post-monochromator in the 50-80 keV range. The successful use of such lenses in all these configurations establishes an important detail, that the pre-monochromator, despite being comprised of vertically reflecting bent Laue geometry crystals, can be brilliance-preserving to a very high degree.« less

Material Structure of a Graded Refractive Index Lens in Decapod Squid

NASA Astrophysics Data System (ADS)

Cai, Jing; Heiney, Paul; Sweeney, Alison

2013-03-01

Underwater vision with a camera-type eye that is simultaneously acute and sensitive requires a spherical lens with a graded distribution of refractive index. Squids have this type of lens, and our previous work has shown that its optical properties are likely achieved with radially variable densities of a single protein with multiple isoforms. Here we measure the spatial organization of this novel protein material in concentric layers of the lens and use these data to suggest possible mechanisms of self-assembly of the proteins into a graded refractive index structure. First, we performed small angle x-ray scattering (SAXS) to study how the protein is spatially organized. Then, molecular dynamic simulation allowed us to correlate structure to the possible dynamics of the system in different regions of the lens. The combination of simulation and SAXS data in this system revealed the likely protein-protein interactions, resulting material structure and its relationship to the observed and variable optical properties of this graded index system. We believe insights into the material properties of the squid lens system will inform the invention of self-assembling graded index devices.

Refractive index, molar refraction and comparative refractive index study of propylene carbonate binary liquid mixtures.

PubMed

Wankhede, Dnyaneshwar Shamrao

2012-06-01

Refractive indices (n) have been experimentally determined for the binary liquid-liquid mixtures of Propylene carbonate (PC) (1) with benzene, ethylbenzene, o-xylene and p-xylene (2) at 298.15, 303.15 and 308.15 K over the entire mole fraction range. The experimental values of n are utilised to calculate deviation in refractive index (Δn), molar refraction (R) and deviation in molar refraction (ΔR). A comparative study of Arago-Biot (A-B), Newton (NW), Eyring and John (E-J) equations for determining refractive index of a liquid has been carried out to test their validity for all the binary mixtures over the entire composition range at 298.15 K. Comparison of various mixing relations is represented in terms of average deviation (AVD). The Δn and ΔR values have been fitted to Redlich-Kister equation at 298.15 K and standard deviations have been calculated. The results are discussed in terms of intermolecular interactions present amongst the components.

Refractive index of erbium doped GaN thin films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Alajlouni, S.; Sun, Z. Y.; Li, J.

2014-08-25

GaN is an excellent host for erbium (Er) to provide optical emission in the technologically important as well as eye-safe 1540 nm wavelength window. Er doped GaN (GaN:Er) epilayers were synthesized on c-plane sapphire substrates using metal organic chemical vapor deposition. By employing a pulsed growth scheme, the crystalline quality of GaN:Er epilayers was significantly improved over those obtained by conventional growth method of continuous flow of reaction precursors. X-ray diffraction rocking curve linewidths of less than 300 arc sec were achieved for the GaN (0002) diffraction peak, which is comparable to the typical results of undoped high quality GaN epilayers andmore » represents a major improvement over previously reported results for GaN:Er. Spectroscopic ellipsometry was used to determine the refractive index of the GaN:Er epilayers in the 1540 nm wavelength window and a linear dependence on Er concentration was found. The observed refractive index increase with Er incorporation and the improved crystalline quality of the GaN:Er epilayers indicate that low loss GaN:Er optical waveguiding structures are feasible.« less

Refractive index degeneration in older lenses: A potential functional correlate to structural changes that underlie cataract formation.

PubMed

Bahrami, Mehdi; Hoshino, Masato; Pierscionek, Barbara; Yagi, Naoto; Regini, Justyn; Uesugi, Kentaro

2015-11-01

A major structure/function relationship in the eye lens is that between the constituent proteins, the crystallins and the optical property of refractive index. Structural breakdown that leads to cataract has been investigated in a number of studies; the concomitant changes in the optics, namely increases in light attenuation have also been well documented. Specific changes in the refractive index gradient that cause such attenuation, however, are not well studied because previous methods of measuring refractive index require transparent samples. The X-ray Talbot interferometric method using synchrotron radiation allows for measurement of fine changes in refractive index through lenses with opacities. The findings of this study on older human lenses show disruptions to the refractive index gradient and in the refractive index contours. These disruptions are linked to location in the lens and occur in polar regions, along or close to the equatorial plane or in lamellar-like formations. The disruptions that are seen in the polar regions manifest branching formations that alter with progression through the lens with some similarity to lens sutures. This study shows how the refractive index gradient, which is needed to maintain image quality of the eye, may be disturbed and that this can occur in a number of distinct ways. These findings offer insight into functional changes to a major optical parameter in older lenses. Further studies are needed to elicit how these may be related to structural degenerations reported in the literature. Copyright © 2015 The Authors. Published by Elsevier Ltd.. All rights reserved.

Saw-tooth refractive x-ray optics with sub-micron resolution

NASA Astrophysics Data System (ADS)

Cederstrom, Bjorn; Ribbing, Carolina; Lundqvist, Mats

2002-11-01

Saw-tooth refractive x-ray lenses have been used to focus a synchrotron beam to sub-μm line width. These lenses are free from spherical aberration and work in analogy with 1-D focusing parabolic compound refractive lenses. However, the focal length can be varied by a simple mechanical procedure. Silicon lenses were fabricated by wet anisotropic etching, and epoxy replicas were molded from the silicon masters. Theses lenses provided 1-D intensity gains up to a factor of 40 and the smallest focal line width was 0.74 μm, very close to the theoretical expectation. Two crossed lenses were put in series to obtain 2-D focusing and the 80 μm by 275 μm source was imaged to 1.0 μm by 5.4 μm. Beryllium lenses were fabricated using conventional computer-controlled milling. The focal line width was 1.7 μm, nearly 3 times larger than predicted by theory. This can be attributed to large surface roughness and a bent lens shape.

Refractive index and thickness determination in Langmuir monolayers of myelin lipids.

PubMed

Pusterla, Julio M; Malfatti-Gasperini, Antonio A; Puentes-Martinez, Ximena E; Cavalcanti, Leide P; Oliveira, Rafael G

2017-05-01

Langmuir monolayers at the air/water interface are widely used as biomembrane models and for amphiphilic molecules studies in general. Under controlled intermolecular organization (lateral molecular area), surface pressure, surface potential, reflectivity (R) and other magnitudes can be precisely determined on these planar monomolecular films. However, some physical parameters such as the refractive index of the monolayer (n) still remain elusive. The refractive index is very relevant because (in combination with R) it allows for the determination of the thickness of the film. The uncertainties of n determine important errors that propagate non-linearly into the calculation of monolayers thickness. Here we present an analytical method for the determination of n in monolayers based on refractive index matching. By using a Brewster angle microscopy (BAM) setup and monolayers spread over subphases with variable refractive index (n 2 ), a minimum in R is search as a function of n 2 . In these conditions, n equals n 2 . The results shown correspond to monolayers of myelin lipids. The n values remain constant at 1.46 upon compression and equals the obtained value for myelin lipid bilayers in suspension. The values for n and R allow for the determination of thickness. We establish comparisons between these thicknesses for the monolayer and those obtained from two X-ray scattering techniques: 1) GIXOS for monolayers at the air/water interface and 2) SAXS for bilayers in bulk suspension. This allows us to conclude that the thickness that we measure by BAM includes the apolar and polar headgroup regions of the monolayer. Copyright © 2017 Elsevier B.V. All rights reserved.

Effect of external index of refraction on multimode fiber couplers.

PubMed

Wang, G Z; Murphy, K A; Claus, R O

1995-12-20

The dependence of the performance of fused-taper multimode fiber couplers on the refractive index of the material surrounding the taper region has been investigated both theoretically and experimentally. It has been identified that for a 2 × 2 multimode fiber coupler there is a range of output-power-coupling ratios for which the effect of the external refractive index is negligible. When the coupler is tapered beyond this region, the performance becomes dependent on the external index of refraction and lossy. To analyze the multimode coupler-loss mechanism, we develop a two-dimensional ray-optics model that incorporates trapped cladding-mode loss and core-mode loss through frustrated total internal reflection.

Computer-simulation results support the experimental observations. Related issues such as coupler fabrication and packaging are also discussed.

Method of determining effects of heat-induced irregular refractive index on an optical system.

PubMed

Song, Xifa; Li, Lin; Huang, Yifan

2015-09-01

The effects of an irregular refractive index on optical performance are examined. A method was developed to express a lens's irregular refractive index distribution. An optical system and its mountings were modeled by a thermomechanical finite element (FE) program in the predicted operating temperature range, -45°C-50°C. FE outputs were elaborated using a MATLAB optimization routine; a nonlinear least squares algorithm was adopted to determine which gradient equation best fit each lens's refractive index distribution. The obtained gradient data were imported into Zemax for sequential ray-tracing analysis. The root mean square spot diameter, modulation transfer function, and diffraction ensquared energy were computed for an optical system under an irregular refractive index and under thermoelastic deformation. These properties are greatly reduced by the irregular refractive index effect, which is one-third to five-sevenths the size of the thermoelastic deformation effect. Thus, thermal analyses of optical systems should consider not only thermoelastic deformation but also refractive index irregularities caused by inhomogeneous temperature.

Simulation tools for analyzer-based x-ray phase contrast imaging system with a conventional x-ray source

NASA Astrophysics Data System (ADS)

Caudevilla, Oriol; Zhou, Wei; Stoupin, Stanislav; Verman, Boris; Brankov, J. G.

2016-09-01

Analyzer-based X-ray phase contrast imaging (ABI) belongs to a broader family of phase-contrast (PC) X-ray imaging modalities. Unlike the conventional X-ray radiography, which measures only X-ray absorption, in PC imaging one can also measures the X-rays deflection induced by the object refractive properties. It has been shown that refraction imaging provides better contrast when imaging the soft tissue, which is of great interest in medical imaging applications. In this paper, we introduce a simulation tool specifically designed to simulate the analyzer-based X-ray phase contrast imaging system with a conventional polychromatic X-ray source. By utilizing ray tracing and basic physical principles of diffraction theory our simulation tool can predicting the X-ray beam profile shape, the energy content, the total throughput (photon count) at the detector. In addition we can evaluate imaging system point-spread function for various system configurations.

Mean effective size and refractive index of transparent atmospheric particulates

NASA Technical Reports Server (NTRS)

Fymat, A. L.

1975-01-01

It is demonstrated that the scattering ratio-principle originally restricted to exact forward and exact backward scattering, and to values of the size parameter and of the product (refractive index x size parameter) less than 0.8 has a much wider applicability. After relaxing these stringent conditions, it is also shown that this principle can be retained as the basis of an experimental technique for retrieving the mean effective size and refractive index of transparent atmospheric particulates.

Index of refraction of GaAs-Al(x)Ga(1-x)As superlattices and multiple quantum wells

NASA Technical Reports Server (NTRS)

Kahen, K. B.; Leburton, J. P.

1987-01-01

A theoretical study of the index of refraction of superlattices and its variation as a function of frequency and the superlattice parameters, i.e., layer width and AlAs composition, is presented. Gamma-region exciton and valence-band mixing effects are included in the model. It is found that these two effects have an important influence on the value of the index of refraction and that superstructure effects rapidly decrease for energies greater than the superlattice potential barriers. Because of the quasi-two-dimensional character of the Gamma-region excitons, the results indicate that the superlattice index of refraction can vary by about two percent at the quantized, bound-exciton, transition energies. Overall, the theoretical results are in good agreement with the experimental data.

Focusing hard X-rays with old LPs

NASA Astrophysics Data System (ADS)

Cederström, Björn; Cahn, Robert N.; Danielsson, Mats; Lundqvist, Mats; Nygren, David R.

2000-04-01

We have found that two sections cut from a vinyl long-playing record can form a spherical aberration-free refractive lens for hard X-rays. Our manufactured saw-tooth refractive lens has a focal length of 22 cm for 23-keV X-rays. The low cost and short focal length of this lens make it feasible for use in small-scale experiments with conventional X-ray tubes.

Refractive Index of Sodium Iodide

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jellison Jr, Gerald Earle; Boatner, Lynn A; Ramey, Joanne Oxendine

2012-01-01

The refractive index of sodium iodide, an important scintillator material that is widely used for radiation detection, is based on a single measurement made by Spangenberg at one wavelength using the index-matching liquid immersion method (Z. Kristallogr., 57, 494-534 (1923)). In the present paper, we present new results for the refractive index of sodium iodide as measured by the minimum deviation technique at six wavelengths between 436 nm (n=1.839 0.002) and 633 nm (n=1.786 0.002). These 6 measurements can be fit to a Sellmeier model, resulting in a 2 of 1.02, indicating a good fit to the data. In addition,more » we report on ellipsometry measurements, which suggest that the near-surface region of the air sensitive NaI crystal seriously degrades, even in a moisture-free environment, resulting in a significantly lower value of the refractive index near the surface. First-principles theoretical calculations of the NaI refractive index that agree with the measured values within 0.025-0.045 are also presented and discussed.« less

Uniform refraction in negative refractive index materials.

PubMed

Gutiérrez, Cristian E; Stachura, Eric

2015-11-01

We study the problem of constructing an optical surface separating two homogeneous, isotropic media, one of which has a negative refractive index. In doing so, we develop a vector form of Snell's law, which is used to study surfaces possessing a certain uniform refraction property, in both the near- and far-field cases. In the near-field problem, unlike the case when both materials have positive refractive indices, we show that the resulting surfaces can be neither convex nor concave.

Effective aperture of X-ray compound refractive lenses.

PubMed

Kohn, V G

2017-05-01

A new definition of the effective aperture of the X-ray compound refractive lens (CRL) is proposed. Both linear (one-dimensional) and circular (two-dimensional) CRLs are considered. It is shown that for a strongly absorbing CRL the real aperture does not influence the focusing properties and the effective aperture is determined by absorption. However, there are three ways to determine the effective aperture in terms of transparent CRLs. In the papers by Kohn [(2002). JETP Lett. 76, 600-603; (2003). J. Exp. Theor. Phys. 97, 204-215; (2009). J. Surface Investig. 3, 358-364; (2012). J. Synchrotron Rad. 19, 84-92; Kohn et al. (2003). Opt. Commun. 216, 247-260; (2003). J. Phys. IV Fr, 104, 217-220], the FWHM of the X-ray beam intensity just behind the CRL was used. In the papers by Lengeler et al. [(1999). J. Synchrotron Rad. 6, 1153-1167; (1998). J. Appl. Phys. 84, 5855-5861], the maximum intensity value at the focus was used. Numerically, these two definitions differ by 50%. The new definition is based on the integral intensity of the beam behind the CRL over the real aperture. The integral intensity is the most physical value and is independent of distance. The new definition gives a value that is greater than that of the Kohn definition by 6% and less than that of the Lengeler definition by 41%. A new approximation for the aperture function of a two-dimensional CRL is proposed which allows one to calculate the two-dimensional CRL through the one-dimensional CRL and to obtain an analytical solution for a complex system of many CRLs.

Influence of stromal refractive index and hydration on corneal laser refractive surgery.

PubMed

de Ortueta, Diego; von Rüden, Dennis; Magnago, Thomas; Arba Mosquera, Samuel

2014-06-01

To evaluate the influence of the stromal refractive index and hydration on postoperative outcomes in eyes that had corneal laser refractive surgery using the Amaris laser system. Augenzentrum Recklinghausen, Recklinghausen, Germany. Comparative case series. At the 6-month follow-up, right eyes were retrospectively analyzed. The effect of the stromal refractive index and hydration on refractive outcomes was assessed using univariate linear and multilinear correlations. Sixty eyes were analyzed. Univariate linear analyses showed that the stromal refractive index and hydration were correlated with the thickness of the preoperative exposed stroma and was statistically different for laser in situ keratomileusis and laser-assisted subepithelial keratectomy treatments. Univariate multilinear analyses showed that the spherical equivalent (SE) was correlated with the attempted SE and stromal refractive index (or hydration). Analyses suggest overcorrections for higher stromal refractive index values and for lower hydration values. The stromal refractive index and hydration affected postoperative outcomes in a subtle, yet significant manner. An adjustment toward greater attempted correction in highly hydrated corneas and less intended correction in low hydrated corneas might help optimize refractive outcomes. Mr. Magnago and Dr. Arba-Mosquera are employees of and Dr. Diego de Ortueta is a consultant to Schwind eye-tech-solutions GmbH & Co. KG. Mr. Rüden has no financial or proprietary interest in any material or method mentioned. Copyright © 2014 ASCRS and ESCRS. Published by Elsevier Inc. All rights reserved.

Temperature-dependent Refractive Index of Silicon and Germanium

NASA Technical Reports Server (NTRS)

Frey, Bradley J.; Leviton, Douglas B.; Madison, Timothy J.

2006-01-01

Silicon and germanium are perhaps the two most well-understood semiconductor materials in the context of solid state device technologies and more recently micromachining and nanotechnology. Meanwhile, these two materials are also important in the field of infrared lens design. Optical instruments designed for the wavelength range where these two materials are transmissive achieve best performance when cooled to cryogenic temperatures to enhance signal from the scene over instrument background radiation. In order to enable high quality lens designs using silicon and germanium at cryogenic temperatures, we have measured the absolute refractive index of multiple prisms of these two materials using the Cryogenic, High-Accuracy Refraction Measuring System (CHARMS) at NASA's Goddard Space Flight Center, as a function of both wavelength and temperature. For silicon, we report absolute refractive index and thermo-optic coefficient (dn/dT) at temperatures ranging from 20 to 300 K at wavelengths from 1.1 to 5.6 pin, while for germanium, we cover temperatures ranging from 20 to 300 K and wavelengths from 1.9 to 5.5 microns. We compare our measurements with others in the literature and provide temperature-dependent Sellmeier coefficients based on our data to allow accurate interpolation of index to other wavelengths and temperatures. Citing the wide variety of values for the refractive indices of these two materials found in the literature, we reiterate the importance of measuring the refractive index of a sample from the same batch of raw material from which final optical components are cut when absolute accuracy greater than k5 x 10" is desired.

Initial growth, refractive index, and crystallinity of thermal and plasma-enhanced atomic layer deposition AlN films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Van Bui, Hao, E-mail: H.VanBui@utwente.nl; Wiggers, Frank B.; Gupta, Anubha

2015-01-01

The authors have studied and compared the initial growth and properties of AlN films deposited on Si(111) by thermal and plasma-enhanced atomic layer deposition (ALD) using trimethylaluminum and either ammonia or a N{sub 2}-H{sub 2} mixture as precursors. In-situ spectroscopic ellipsometry was employed to monitor the growth and measure the refractive index of the films during the deposition. The authors found that an incubation stage only occurred for thermal ALD. The linear growth for plasma-enhanced ALD (PEALD) started instantly from the beginning due to the higher nuclei density provided by the presence of plasma. The authors observed the evolution ofmore » the refractive index of AlN during the growth, which showed a rapid increase up to a thickness of about 30 nm followed by a saturation. Below this thickness, higher refractive index values were obtained for AlN films grown by PEALD, whereas above that the refractive index was slightly higher for thermal ALD films. X-ray diffraction characterization showed a wurtzite crystalline structure with a (101{sup ¯}0) preferential orientation obtained for all the layers with a slightly better crystallinity for films grown by PEALD.« less

Fabrication of high aspect grating using bonded substrate for X-ray refraction imaging by Talbot-Lau interferometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tada, Takuji; Murakoshi, Dai; Ishii, Hiroyasu

2012-07-31

In order to improve the image quality of X-ray refraction images using a Talbot-Lau interferometer, we have been attempting to fabricate gratings with high aspect ratio. In our attempt, deep grooves of grating structure were channeled on a Si substrate bonded by Au diffusion bonding method, and the grooves were filled with Au where the Au layer used for the bonding Si substrate was acting as a seed layer of Au electroplating. From the results of a visibility measurement and a cross sectional SEM image, it was confirmed that the grooves with a pitch of 5.8 {mu}m and a depthmore » of 100 {mu}m could be successfully filled with Au over a large area of 72 Multiplication-Sign 80 mm{sup 2}. Using this grating, the X-ray refraction images for the cartilage of a knee joint of a livestock pig could be obtained where SPS method was employed for the single-shot image acquisition.« less

Refractive index measurement based on confocal method

NASA Astrophysics Data System (ADS)

An, Zhe; Xu, XiPing; Yang, JinHua; Qiao, Yang; Liu, Yang

2017-10-01

The development of transparent materials is closed to optoelectronic technology. It plays an increasingly important role in various fields. It is not only widely used in optical lens, optical element, optical fiber grating, optoelectronics, but also widely used in the building material, pharmaceutical industry with vessel, aircraft windshield and daily wear glasses.Regard of solving the problem of refractive index measurement in optical transparent materials. We proposed that using the polychromatic confocal method to measuring the refractive index of transparent materials. In this article, we describes the principle of polychromatic confocal method for measuring the refractive index of glass,and sketched the optical system and its optimization. Then we establish the measurement model of the refractive index, and set up the experimental system. In this way, the refractive index of the glass has been calibrated for refractive index experiment. Due to the error in the experimental process, we manipulated the experiment data to compensate the refractive index measurement formula. The experiment taking the quartz glass for instance. The measurement accuracy of the refractive index of the glass is +/-1.8×10-5. This method is more practical and accurate, especially suitable for non-contact measurement occasions, which environmental requirements is not high. Environmental requirements are not high, the ordinary glass production line up to the ambient temperature can be fully adapted. There is no need for the color of the measured object that you can measure the white and a variety of colored glass.

Chromatic Properties of Index of Refraction Gradients in Glass.

NASA Astrophysics Data System (ADS)

Ryan-Howard, Danette Patrice

The chromatic properties of index of refraction gradients have been predicted theoretically and verified experimentally. The use of these materials in the design of color corrected optical systems has been investigated and confirmed by the evaluation of two fabricated lenses. A model for the chromatic properties of gradient index materials has been developed. The index of refraction is calculated based on the composition of the material. Since the index of refraction and the conventional Abbe number change as a function of the composition of the glass, a gradient Abbe number and a partial dispersion are defined. Analysis of combinations of ion exchange pairs and glasses result in a wide range of gradient Abbe numbers and partial dispersions. These ranges can be further extended by using glasses which contain more than one exchange ion or by using mixed salt baths. The chromatic properties were measured with a multiple wavelength A.C. interferometer. The gradient Abbe numbers and partial dispersions for a number of samples were calculated. Evaluation of the samples showed that the index and dispersion data correlated well with that predicted by the model. Thin lens formulae for the paraxial axial color and secondary spectrum of a radial gradient singlet with curves were examined. The design of a single element 10x microscope objective verified the applicability of these formulae. The design of a two element 40x microscope objective showed that a six element diffraction limited 40x objective can be replaced with a two element system composed of one homogeneous lens and one gradient lens without sacrificing either monochromatic performance or color correction. A previously fabricated axial gradient collimator and a fabricated Wood element were evaluated. Correlation of the directly measured quantities, paraxial axial color, secondary spectrum and spherochromatism with the values predicted by the model verified that the predicted superior performance of gradient-index

Formation of bulk refractive index structures

DOEpatents

Potter, Jr., Barrett George; Potter, Kelly Simmons; Wheeler, David R.; Jamison, Gregory M.

2003-07-15

A method of making a stacked three-dimensional refractive index structure in photosensitive materials using photo-patterning where first determined is the wavelength at which a photosensitive material film exhibits a change in refractive index upon exposure to optical radiation, a portion of the surfaces of the photosensitive material film is optically irradiated, the film is marked to produce a registry mark. Multiple films are produced and aligned using the registry marks to form a stacked three-dimensional refractive index structure.

Photonic crystals at visible, x-ray, and terahertz frequencies

NASA Astrophysics Data System (ADS)

Prasad, Tushar

Photonic crystals are artificial structures with a periodically varying refractive index. This property allows photonic crystals to control the propagation of photons, making them desirable components for novel photonic devices. Photonic crystals are also termed as "semiconductors of light", since they control the flow of electromagnetic radiation similar to the way electrons are excited in a semiconductor crystal. The scale of periodicity in the refractive index determines the frequency (or wavelength) of the electromagnetic waves that can be manipulated. This thesis presents a detailed analysis of photonic crystals at visible, x-ray, and terahertz frequencies. Self-assembly and spin-coating methods are used to fabricate colloidal photonic crystals at visible frequencies. Their dispersion characteristics are examined through theoretical as well as experimental studies. Based on their peculiar dispersion property called the superprism effect, a sensor that can detect small quantities of chemical substances is designed. A photonic crystal that can manipulate x-rays is fabricated by using crystals of a non-toxic plant virus as templates. Calculations show that these metallized three-dimensional crystals can find utility in x-ray optical systems. Terahertz photonic crystal slabs are fabricated by standard lithographic and etching techniques. In-plane superprism effect and out-of-plane guided resonances are studied by terahertz time-domain spectroscopy, and verified by numerical simulations.

Optofluidic two-dimensional grating volume refractive index sensor.

PubMed

Sarkar, Anirban; Shivakiran Bhaktha, B N; Khastgir, Sugata Pratik

2016-09-10

We present an optofluidic reservoir with a two-dimensional grating for a lab-on-a-chip volume refractive index sensor. The observed diffraction pattern from the device resembles the analytically obtained fringe pattern. The change in the diffraction pattern has been monitored in the far-field for fluids with different refractive indices. Reliable measurements of refractive index variations, with an accuracy of 6×10^-3 refractive index units, for different fluids establishes the optofluidic device as a potential on-chip tool for monitoring dynamic refractive index changes.

Precise determination of the refractive index of suspended particles: light transmission as a function of refractive index mismatch

NASA Astrophysics Data System (ADS)

McClymer, J. P.

2016-08-01

Many fluids appear white because refractive index differences lead to multiple scattering. In this paper, we use safe, low-cost commercial index matching fluids to quantitatively study light transmission as a function of index mismatch, reduce multiple scattering to allow single scattering probes, and to precisely determine the index of refraction of suspended material. The transmission profile is compared with Rayleigh-Gans and Mie theory predictions. The procedure is accessible as a student laboratory project, while providing advantages over other standard methods of measuring the refractive index of an unknown nanoparticle, making it valuable to researchers.

Gradient Refractive Index Lenses.

ERIC Educational Resources Information Center

Morton, N.

1984-01-01

Describes the nature of gradient refractive index (GRIN) lenses, focusing on refraction in these materials, focal length of a thin Wood lens, and on manufacturing of such lenses. Indicates that GRIN lenses of small cross section are in limited production with applications suggested for optical communication and photocopying fields. (JN)

X-ray bubble lens and x-ray hollow plastic ball lens

NASA Astrophysics Data System (ADS)

Kohmura, Yoshiki; Awaji, Mitsuhiro; Suzuki, Yoshio; Ishikawa, Tetsuya

1998-11-01

Recent development of anew refractive x-ray lens at SPring-8 is reported. This is the first refractive x-ray lens with a string of spherical lens in-spite of the string of cylindrical holes. Two types of the lends were developed which consists of a string of bubbles formed in a viscous liquid and a string of hollow plastic balls on pure water. They are sealed inside a container made from an acrylic resin. The x-ray focusing properties were investigated with the monochromated beam at an undulator beam line BL47 in SPring-8. Demagnified images of the source for these tow types of lens were observed at the energy of 19.0-24.5 keV with the focal length of approximately 5m. For the bubble lens, a gain of about 12 was observed. The observed vertical image size, 48 micrometers , was 6 times larger than the expected size. The method to improve the focusing capability is discussed.

2D and 3D X-ray phase retrieval of multi-material objects using a single defocus distance.

PubMed

Beltran, M A; Paganin, D M; Uesugi, K; Kitchen, M J

2010-03-29

A method of tomographic phase retrieval is developed for multi-material objects whose components each has a distinct complex refractive index. The phase-retrieval algorithm, based on the Transport-of-Intensity equation, utilizes propagation-based X-ray phase contrast images acquired at a single defocus distance for each tomographic projection. The method requires a priori knowledge of the complex refractive index for each material present in the sample, together with the total projected thickness of the object at each orientation. The requirement of only a single defocus distance per projection simplifies the experimental setup and imposes no additional dose compared to conventional tomography. The algorithm was implemented using phase contrast data acquired at the SPring-8 Synchrotron facility in Japan. The three-dimensional (3D) complex refractive index distribution of a multi-material test object was quantitatively reconstructed using a single X-ray phase-contrast image per projection. The technique is robust in the presence of noise, compared to conventional absorption based tomography.

X-ray irradiation of soda-lime glasses studied in situ with surface plasmon resonance spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Serrano, A.; Galvez, F.; Rodriguez de la Fuente, O.

2013-03-21

We present here a study of hard X-ray irradiation of soda-lime glasses performed in situ and in real time. For this purpose, we have used a Au thin film grown on glass and studied the excitation of its surface plasmon resonance (SPR) while irradiating the sample with X-rays, using a recently developed experimental setup at a synchrotron beamline [Serrano et al., Rev. Sci. Instrum. 83, 083101 (2012)]. The extreme sensitivity of the SPR to the features of the glass substrate allows probing the modifications caused by the X-rays. Irradiation induces color centers in the soda-lime glass, modifying its refractive index.more » Comparison of the experimental results with simulated data shows that both, the real and the imaginary parts of the refractive index of soda-lime glasses, change upon irradiation in time intervals of a few minutes. After X-ray irradiation, the effects are partially reversible. The defects responsible for these modifications are identified as non-bridging oxygen hole centers, which fade by recombination with electrons after irradiation. The kinetics of the defect formation and fading process are also studied in real time.« less

Analysis of scattering by spheres having a negative acoustical refractive index

NASA Astrophysics Data System (ADS)

Marston, Philip L.

2005-04-01

Electromagnetic waves having oppositely directed phase and group velocities propagate in metamaterials having a negative permeability and negative permittivity [J. B. Pendry and D. R. Smith, Phys. Today 57(6), 37-44 (2004)]. Such materials are predicted to have unusual electromagnetic scattering properties [R. Ruppin, Solid State Commun. 116, 411-415 (2000)]. If it is possible to fabricate acoustical materials having a simultaneously negative effective elastic modulus and density (in a dynamical sense), the mechanical energy flux will have the opposite direction as the wave-vector associated with phase evolution. Rays descriptive of the energy flux refracted by such hypothetical materials at interfaces with ordinary fluids would be characterized by a negative acoustical refractive index. Partial-wave-series calculations of high frequency scattering by fluid spheres having an acoustical refractive index at (or close to) 1 reveal backscattering enhancements associated with glory rays which, unlike ordinary spheres [P. L. Marston and D. S. Langley, J. Acoust. Soc. Am. 73, 1464-1475 (1983)], require only a single internal chord. Generalized Lamb waves on elastic shells having opposite phase and group velocities also cause enhanced backscattering associated with unusual rays [G. Kaduchak, D. H. Hughes, and P. L. Marston, J. Acoust. Soc. Am. 96, 3704-3714 (1994)].

Refractive index of liquid mixtures: theory and experiment.

PubMed

Reis, João Carlos R; Lampreia, Isabel M S; Santos, Angela F S; Moita, Maria Luísa C J; Douhéret, Gérard

2010-12-03

An innovative approach is presented to interpret the refractive index of binary liquid mixtures. The concept of refractive index "before mixing" is introduced and shown to be given by the volume-fraction mixing rule of the pure-component refractive indices (Arago-Biot formula). The refractive index of thermodynamically ideal liquid mixtures is demonstrated to be given by the volume-fraction mixing rule of the pure-component squared refractive indices (Newton formula). This theoretical formulation entails a positive change of refractive index upon ideal mixing, which is interpreted in terms of dissimilar London dispersion forces centred in the dissimilar molecules making up the mixture. For real liquid mixtures, the refractive index of mixing and the excess refractive index are introduced in a thermodynamic manner. Examples of mixtures are cited for which excess refractive indices and excess molar volumes show all of the four possible sign combinations, a fact that jeopardises the finding of a general equation linking these two excess properties. Refractive indices of 69 mixtures of water with the amphiphile (R,S)-1-propoxypropan-2-ol are reported at five temperatures in the range 283-303 K. The ideal and real refractive properties of this binary system are discussed. Pear-shaped plots of excess refractive indices against excess molar volumes show that extreme positive values of excess refractive index occur at a substantially lower mole fraction of the amphiphile than extreme negative values of excess molar volume. Analysis of these plots provides insights into the mixing schemes that occur in different composition segments. A nearly linear variation is found when Balankina's ratios between excess and ideal values of refractive indices are plotted against ratios between excess and ideal values of molar volumes. It is concluded that, when coupled with volumetric properties, the new thermodynamic functions defined for the analysis of refractive indices of liquid

Metamaterials with gradient negative index of refraction.

PubMed

Pinchuk, Anatoliy O; Schatz, George C

2007-10-01

We propose a new metamaterial with a gradient negative index of refraction, which can focus a collimated beam of light coming from a distant object. A slab of the negative refractive index metamaterial has a focal length that can be tuned by changing the gradient of the negative refractive index. A thin metal film pierced with holes of appropriate size or spacing between them can be used as a metamaterial with the gradient negative index of refraction. We use finite-difference time-domain calculations to show the focusing of a plane electromagnetic wave passing through a system of equidistantly spaced holes in a metal slab with decreasing diameters toward the edges of the slab.

Ray tracing analysis of overlapping objects in refraction contrast imaging.

PubMed

Hirano, Masatsugu; Yamasaki, Katsuhito; Okada, Hiroshi; Sakurai, Takashi; Kondoh, Takeshi; Katafuchi, Tetsuro; Sugimura, Kazuro; Kitazawa, Sohei; Kitazawa, Riko; Maeda, Sakan; Tamura, Shinichi

2005-08-01

We simulated refraction contrast imaging in overlapping objects using the ray tracing method. The easiest case, in which two columnar objects (blood vessels) with a density of 1.0 [g/cm3], run at right angles in air, was calculated. For absorption, we performed simulation using the Snell law adapted to the object's boundary. A pair of bright and dark spot results from the interference of refracted X-rays where the blood vessels crossed. This has the possibility of increasing the visibility of the image.

Electron density and effective atomic number (Zeff) determination through x-ray Moiré deflectometry

NASA Astrophysics Data System (ADS)

Valdivia Leiva, Maria Pia; Stutman, Dan; Finkenthal, Michael

2014-10-01

Talbot-Lau based Moiré deflectometry is a powerful density diagnostic capable of delivering refraction information and attenuation from a single image, through the accurate detection of X-ray phase-shift and intensity. The technique is able to accurately measure both the real part of the index of refraction δ (directly related to electron density) and the attenuation coefficient μ of an object placed in the x-ray beam. Since the atomic number Z (or Zeff for a composite sample) is proportional to these quantities, an elemental map of the effective atomic number can be obtained with the ratio of the phase and the absorption image. The determination of Zeff from refraction and attenuation measurements with Moiré deflectometry could be of high interest in various fields of HED research such as shocked materials and ICF experiments as Zeff is linked, by definition, to the x-ray absorption properties of a specific material. This work is supported by U.S. DoE/NNSA Grant No. 435 DENA0001835.

Refractive index of plant cell walls

NASA Technical Reports Server (NTRS)

Gausman, H. W.; Allen, W. A.; Escobar, D. E.

1974-01-01

Air was replaced with media of higher refractive indices by vacuum infiltration in leaves of cucumber, blackeye pea, tomato, and string bean plants, and reflectance of noninfiltrated and infiltrated leaves was spectrophotometrically measured. Infiltrated leaves reflected less light than noninfiltrated leaves over the 500-2500-nm wavelength interval because cell wall-air interfaces were partly eliminated. Minimal reflectance should occur when the average refractive index of plant cell walls was matched by the infiltrating fluid. Although refractive indices that resulted in minimal reflectance differed among the four plant genera, an average value of 1.425 approximates the refractive index of plant cell walls for the four plant genera.

Ancient administrative handwritten documents: X-ray analysis and imaging

PubMed Central

Albertin, F.; Astolfo, A.; Stampanoni, M.; Peccenini, Eva; Hwu, Y.; Kaplan, F.; Margaritondo, G.

2015-01-01

Handwritten characters in administrative antique documents from three centuries have been detected using different synchrotron X-ray imaging techniques. Heavy elements in ancient inks, present even for everyday administrative manuscripts as shown by X-ray fluorescence spectra, produce attenuation contrast. In most cases the image quality is good enough for tomography reconstruction in view of future applications to virtual page-by-page ‘reading’. When attenuation is too low, differential phase contrast imaging can reveal the characters from refractive index effects. The results are potentially important for new information harvesting strategies, for example from the huge Archivio di Stato collection, objective of the Venice Time Machine project. PMID:25723946

Ancient administrative handwritten documents: X-ray analysis and imaging.

PubMed

Albertin, F; Astolfo, A; Stampanoni, M; Peccenini, Eva; Hwu, Y; Kaplan, F; Margaritondo, G

2015-03-01

Handwritten characters in administrative antique documents from three centuries have been detected using different synchrotron X-ray imaging techniques. Heavy elements in ancient inks, present even for everyday administrative manuscripts as shown by X-ray fluorescence spectra, produce attenuation contrast. In most cases the image quality is good enough for tomography reconstruction in view of future applications to virtual page-by-page `reading'. When attenuation is too low, differential phase contrast imaging can reveal the characters from refractive index effects. The results are potentially important for new information harvesting strategies, for example from the huge Archivio di Stato collection, objective of the Venice Time Machine project.

Measurements of the hard-x-ray reflectivity of iridium

DOE Office of Scientific and Technical Information (OSTI.GOV)

Romaine, S.; Bruni, R.; Gorenstein, P.

2007-01-10

In connection with the design of a hard-x-ray telescope for the Constellation X-Ray Observatory we measured the reflectivity of an iridium-coated zerodur substrate as a function of angle at 55, 60, 70, and 80 keV at the National Synchrotron Light Source of Brookhaven National Laboratory. The optical constants were derived from the reflectivity data. The real component of the index of refraction is in excellent agreement with theoretical values at all four energies. However, the imaginary component, which is related to the mass attenuation coefficient, is 50% to 70% larger at 55, 60, and 70 keV than theoretical values.

Measurements of the hard-x-ray reflectivity of iridium.

PubMed

Romaine, S; Bruni, R; Gorenstein, P; Zhong, Z

2007-01-10

In connection with the design of a hard-x-ray telescope for the Constellation X-Ray Observatory we measured the reflectivity of an iridium-coated zerodur substrate as a function of angle at 55, 60, 70, and 80 keV at the National Synchrotron Light Source of Brookhaven National Laboratory. The optical constants were derived from the reflectivity data. The real component of the index of refraction is in excellent agreement with theoretical values at all four energies. However, the imaginary component, which is related to the mass attenuation coefficient, is 50% to 70% larger at 55, 60, and 70 keV than theoretical values.

Scalable, large area compound array refractive lens for hard X-rays

NASA Astrophysics Data System (ADS)

Reich, Stefan; dos Santos Rolo, Tomy; Letzel, Alexander; Baumbach, Tilo; Plech, Anton

2018-04-01

We demonstrate the fabrication of a 2D Compound Array Refractive Lens (CARL) for multi-contrast X-ray imaging. The CARL consists of six stacked polyimide foils with each displaying a 2D array of lenses with a 65 μm pitch aiming for a sensitivity on sub-micrometer structures with a (few-)micrometer resolution in sensing through phase and scattering contrast at multiple keV. The parabolic lenses are formed by indents in the foils by a paraboloid needle. The ability for fast single-exposure multi-contrast imaging is demonstrated by filming the kinetics of pulsed laser ablation in liquid. The three contrast channels, absorption, differential phase, and scattering, are imaged with a time resolution of 25 μs. By changing the sample-detector distance, it is possible to distinguish between nanoparticles and microbubbles.

Astigmatism of the Ex Vivo Human Lens: Surface and Gradient Refractive Index Age-Dependent Contributions.

PubMed

Birkenfeld, Judith; de Castro, Alberto; Marcos, Susana

2015-08-01

We estimated the contribution of the gradient refractive index (GRIN) and lens surfaces to lens astigmatism and lens astigmatic angle as a function of age in human donor lenses. Human lenses were imaged, ex vivo, with 3D-spectral optical coherence tomography (OCT) and their back focal length was measured using laser ray tracing. The contribution of lens surfaces and GRIN to lens astigmatism were evaluated by computational ray tracing on the GRIN lens and a homogenous equivalent index lens. Astigmatism magnitude and relative astigmatic angle of and between lens surfaces, GRIN lens, and lens with homogeneous refractive index were evaluated, and all results were correlated with age. The magnitude of astigmatism in the anterior lens surface decreased with age (slope = -0.005 diopters [D]/y; r = 0.397, P = 0.018). Posterior surface astigmatism and lens astigmatism were not age-dependent. Presence of GRIN did not alter significantly the magnitude or axis of the lens astigmatism. The astigmatism of GRIN lens and lens with homogeneous refractive index correlated with anterior lens surface astigmatism (GRIN, P = 3.9E - 6, r = 0.693; equivalent refractive index lens, P = 4.1E - 4, r = 0.565). The astigmatic angle of posterior surface, GRIN lens, and homogeneous refractive index lens did not change significantly with age. The axis of lens astigmatism is close to the astigmatic axis of the anterior lens surface. Age-related changes in lens astigmatism appear to be related to changes in the anterior lens astigmatism. The influence of the GRIN on lens astigmatism and the astigmatic axis is minor.

Concentration and temperature dependence of the refractive index of ethanol-water mixtures: influence of intermolecular interactions.

PubMed

Riobóo, R J; Philipp, M; Ramos, M A; Krüger, J K

2009-09-01

The temperature and concentration dependence of the refractive index, nD(x, T), in ethanol-water mixtures agrees with previous data in the ethanol-rich concentration range. The refractive index versus concentration x determined at 20 degrees C shows the expected maximum at about 41 mol% water (22 mass% water). The temperature derivative of the refractive index, dnD/dT, shows anomalies at lower water concentrations at about 10 mol% water but no anomaly at 41 mol% water. Both anomalies are related to intermolecular interactions, the one in nD seems to be due to molecular segregation and cluster formation while the origin of the second one in dnD/dT is still not clear.

Band gap and refractive index tunability in thallium based layered mixed crystals

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gasanly, N. M., E-mail: nizami@metu.edu.tr; Virtual International Scientific Research Centre, Baku State University, Baku 1148

2015-07-21

Compositional variation of the band gap energy and refractive index of TlMeX{sub 2}-type (Me = Ga or In and X = S or Se) layered mixed crystals have been studied by the transmission and reflection measurements in the wavelength range of 400–1100 nm. The analysis of absorption data of TlGa{sub 1-x}In{sub x}Se{sub 2}, TlGa(S{sub 1−x}Se{sub x}){sub 2}, TlGa{sub 1−x}In{sub x}S{sub 2}, and TlIn(Se{sub 1−x}S{sub x}){sub 2} mixed crystals revealed the presence of both optical indirect and direct transitions. It was found that the energy band gaps of mixed crystals decrease at the replacing of gallium atoms by indium and of sulfur atoms by selenium ones.more » Through the similar replacing of atoms (smaller atoms by larger ones) in the studied mixed crystals, the refractive index shows the quite opposite behavior.« less

Tunable two-dimensional liquid gradient refractive index (L-GRIN) lens for variable light focusing.

PubMed

Huang, Hua; Mao, Xiaole; Lin, Sz-Chin Steven; Kiraly, Brian; Huang, Yiping; Huang, Tony Jun

2010-09-21

We report a two-dimensional (2D) tunable liquid gradient refractive index (L-GRIN) lens for variable focusing of light in the out-of-plane direction. This lens focuses a light beam through a liquid medium with a 2D hyperbolic secant (HS) refractive index gradient. The refractive index gradient is established in a microfluidic chamber through the diffusion between two fluids with different refractive indices, i.e. CaCl(2) solution and deionized (DI) water. The 2D HS refractive index profile and subsequently the focal length of the L-GRIN lens can be tuned by changing the ratio of the flow rates of the CaCl(2) solution and DI water. The focusing effect is experimentally characterized through side-view and top-view image analysis, and the experimental data match well with the results from ray-tracing optical simulations. Advantages of the 2D L-GRIN lens include simple device fabrication procedure, low fluid consumption rate, convenient lens-tuning mechanism, and compatibility with existing microfluidic devices. We expect that with further optimizations, this 2D L-GRIN lens can be used in many optics-based lab-on-a-chip applications.

The refractive index of human hemoglobin in the visible range.

PubMed

Zhernovaya, O; Sydoruk, O; Tuchin, V; Douplik, A

2011-07-07

Because the refractive index of hemoglobin in the visible range is sensitive to the hemoglobin concentration, optical investigations of hemoglobin are important for medical diagnostics and treatment. Direct measurements of the refractive index are, however, challenging; few such measurements have previously been reported, especially in a wide wavelength range. We directly measured the refractive index of human deoxygenated and oxygenated hemoglobin for nine wavelengths between 400 and 700 nm for the hemoglobin concentrations up to 140 g l(-1). This paper analyzes the results and suggests a set of model functions to calculate the refractive index depending on the concentration. At all wavelengths, the measured values of the refractive index depended on the concentration linearly. Analyzing the slope of the lines, we determined the specific refraction increments, derived a set of model functions for the refractive index depending on the concentration, and compared our results with those available in the literature. Based on the model functions, we further calculated the refractive index at the physiological concentration within the erythrocytes of 320 g l(-1). The results can be used to calculate the refractive index in the visible range for arbitrary concentrations provided that the refractive indices depend on the concentration linearly.

Multislice does it all—calculating the performance of nanofocusing X-ray optics

DOE PAGES

Li, Kenan; Wojcik, Michael; Jacobsen, Chris

2017-01-23

Here, we describe an approach to calculating the optical performance of a wide range of nanofocusing X-ray optics using multislice scalar wave propagation with a complex X-ray refractive index. This approach produces results indistinguishable from methods such as coupled wave theory, and it allows one to reproduce other X-ray optical phenomena such as grazing incidence reflectivity where the direction of energy flow is changed significantly. Just as finite element analysis methods allow engineers to compute the thermal and mechanical responses of arbitrary structures too complex to model by analytical approaches, multislice propagation can be used to understand the properties ofmore » the real-world optics of finite extent and with local imperfections, allowing one to better understand the limits to nanoscale X-ray imaging.« less

High sensitivity refractive index sensor based on adiabatic tapered optical fiber deposited with nanofilm by ALD.

PubMed

Zhu, Shan; Pang, Fufei; Huang, Sujuan; Zou, Fang; Dong, Yanhua; Wang, Tingyun

2015-06-01

Atomic layer deposition (ALD) technology is introduced to fabricate a high sensitivity refractive index sensor based on an adiabatic tapered optical fiber. Different thickness of Al₂O₃ nanofilm is coated around fiber taper precisely and uniformly under different deposition cycles. Attributed to the high refractive index of the Al₂O₃ nanofilm, an asymmetry Fabry-Perot like interferometer is constructed along the fiber taper. Based on the ray-optic analysis, total internal reflection happens on the nanofilm-surrounding interface. With the ambient refractive index changing, the phase delay induced by the Goos-Hänchen shift is changed. Correspondingly, the transmission resonant spectrum shifts, which can be utilized for realizing high sensitivity sensor. The high sensitivity sensor with 6008 nm/RIU is demonstrated by depositing 3000 layers Al₂O₃ nanofilm as the ambient refractive index is close to 1.33. This high sensitivity refractive index sensor is expected to have wide applications in biochemical sensors.

Counter-propagating optical trapping system for size and refractive index measurement of microparticles.

PubMed

Flynn, Richard A; Shao, Bing; Chachisvilis, Mirianas; Ozkan, Mihrimah; Esener, Sadik C

2006-01-15

We propose and demonstrate a novel approach to measure the size and refractive index of microparticles based on two beam optical trapping, where forward scattered light is detected to give information about the particle. The counter-propagating optical trap measurement (COTM) system exploits the capability of optical traps to measure pico-Newton forces for microparticles' refractive index and size characterization. Different from the current best technique for microparticles' refractive index measurement, refractometry, a bulk technique requiring changing the fluid composition of the sample, our optical trap technique works with any transparent fluid and enables single particle analysis without the use of biological markers. A ray-optics model is used to explore the physical operation of the COTM system, predict system performance and aid system design. Experiments demonstrate the accuracy of refractive index measurement of Deltan=0.013 and size measurement of 3% of diameter with 2% standard deviation. Present performance is instrumentation limited, and a potential improvement by more than two orders of magnitude can be expected in the future. With further development in parallelism and miniaturization, the system offers advantages for cell manipulation and bioanalysis compatible with lab-on-a-chip systems.

On the effective refractive index of blood

NASA Astrophysics Data System (ADS)

Nahmad-Rohen, Alexander; Contreras-Tello, Humberto; Morales-Luna, Gesuri; García-Valenzuela, Augusto

2016-01-01

We calculated the real and imaginary parts of the effective refractive index {n}{eff} of blood as functions of wavelength from 400 to 800 nm; we employed van de Hulst’s theory, together with the anomalous diffraction approximation, for the calculation. We modelled blood as a mixture of plasma and erythrocytes. Our results indicate that erythrocyte orientation has a strong effect on {n}{eff}, making blood an optically anisotropic medium except when the erythrocytes are randomly oriented. In the case in which their symmetry axis is perpendicular to the wave vector, {n}{eff} equals the refractive index of plasma at certain wavelengths. Furthermore, the erythrocytes’ shape affects their contribution to {n}{eff} in an important way, implying that studies on the effective refractive index of blood should avoid approximating them as spheres or spheroids. Finally, the effective refractive index of blood predicted by van de Hulst’s theory is different from what would be obtained by averaging the refractive indices of its constituents weighted by volume; such a volume-weighted average is appropriate only for haemolysed blood. We then measured the real part of the refractive index of various blood solutions using two different experimental setups. One of the most important results of our expriment is that {n}{eff} is measurable to a good degree of precision even for undiluted blood, although not all measuring apparatuses are appropriate. The experimental data is self-consistent and in reasonable agreement with our theoretical calculations.

Priors for X-ray in-line phase tomography of heterogeneous objects.

PubMed

Langer, Max; Cloetens, Peter; Hesse, Bernhard; Suhonen, Heikki; Pacureanu, Alexandra; Raum, Kay; Peyrin, Françoise

2014-03-06

We present a new prior for phase retrieval from X-ray Fresnel diffraction patterns. Fresnel diffraction patterns are achieved by letting a highly coherent X-ray beam propagate in free space after interaction with an object. Previously, either homogeneous or multi-material object assumptions have been used. The advantage of the homogeneous object assumption is that the prior can be introduced in the Radon domain. Heterogeneous object priors, on the other hand, have to be applied in the object domain. Here, we let the relationship between attenuation and refractive index vary as a function of the measured attenuation index. The method is evaluated using images acquired at beamline ID19 (ESRF, Grenoble, France) of a phantom where the prior is calculated by linear interpolation and of a healing bone obtained from a rat osteotomy model. It is shown that the ratio between attenuation and refractive index in bone for different levels of mineralization follows a power law. Reconstruction was performed using the mixed approach but is compatible with other, more advanced models. We achieve more precise reconstructions than previously reported in literature. We believe that the proposed method will find application in biomedical imaging problems where the object is strongly heterogeneous, such as bone healing and biomaterials engineering.

Determination of effective complex refractive index of a turbid liquid with surface plasmon resonance phase detection.

PubMed

Yingying, Zhang; Jiancheng, Lai; Cheng, Yin; Zhenhua, Li

2009-03-01

The dependence of the surface plasmon resonance (SPR) phase difference curve on the complex refractive index of a sample in Kretschmann configuration is discussed comprehensively, based on which a new method is proposed to measure the complex refractive index of turbid liquid. A corresponding experiment setup was constructed to measure the SPR phase difference curve, and the complex refractive index of turbid liquid was determined. By using the setup, the complex refractive indices of Intralipid solutions with concentrations of 5%, 10%, 15%, and 20% are obtained to be 1.3377+0.0005 i, 1.3427+0.0028 i, 1.3476+0.0034 i, and 1.3496+0.0038 i, respectively. Furthermore, the error analysis indicates that the root-mean-square errors of both the real and the imaginary parts of the measured complex refractive index are less than 5x10(-5).

Cryogenic Refractive Index of Heraeus Homosil Glass

NASA Technical Reports Server (NTRS)

Miller, Kevin H.; Quijada, Manuel A.; Leviton, Douglas B.

2017-01-01

This paper reports measurements of the refractive index of Homosil (Heraeus) over the wavelength range of 0.343.16 m and temperature range of 120335 K. These measurements were performed by using the Cryogenic High Accuracy Refraction Measuring System (CHARMS) facility at the NASAs Goddard Space Flight Center. These measurements were in support of an integrated Structural-Thermal-Optical-Performance (STOP) model that was developed for a field-widened Michelson interferometer that is being built and tested for the High Spectral Resolution Lidar (HSRL) project at the NASA Langley Research Center (LaRC). The cryogenic refractive index measurements were required in order to account for the highly sensitivity performance of the HSRL instrument to changes in refractive index with temperature, temperature gradients, thermal expansion, and deformation due to mounting stresses. A dense coverage of the absolute refractive index over the aforementioned wavelength and temperature ranges was used to determine the thermo-optic coefficient (dndT) and dispersion relation (dnd) as a function of wavelength and temperature. Our measurements of Homosil will be compared with measurements of other glasses from the fused silica family studied in CHARMS as well as measurements reported elsewhere in literature.

Cryogenic Refractive Index of Heraeus Homosil Glass

NASA Technical Reports Server (NTRS)

Miller, Kevin H.; Quijada, Manuel A.; Leviton, Douglas B.

2017-01-01

This paper reports measurements of the refractive index of Homosil (Heraeus) over the wavelength range of 0.34-3.16 microns and temperature range of 120-335 K. These measurements were performed by using the Cryogenic High Accuracy Refraction Measuring System (CHARMS) facility at the NASAs Goddard Space Flight Center. These measurements were in support of an integrated Structural-Thermal-Optical-Performance (STOP) model that was developed for a field-widened Michelson interferometer that is being built and tested for the High Spectral Resolution Lidar (HSRL) project at the NASA Langley Research Center (LaRC). The cryogenic refractive index measurements were required in order to account for the highly sensitivity performance of the HSRL instrument to changes in refractive index with temperature, temperature gradients, thermal expansion, and deformation due to mounting stresses. A dense coverage of the absolute refractive index over the aforementioned wavelength and temperature ranges was used to determine the thermo-optic coefficient (dn/dT) and dispersion relation (dn/d(lamda)) as a function of wavelength and temperature. Our measurements of Homosil will be compared with measurements of other glasses from the fused silica family studied in CHARMS as well as measurements reported elsewhere in literature.

Refractive index inversion based on Mueller matrix method

NASA Astrophysics Data System (ADS)

Fan, Huaxi; Wu, Wenyuan; Huang, Yanhua; Li, Zhaozhao

2016-03-01

Based on Stokes vector and Jones vector, the correlation between Mueller matrix elements and refractive index was studied with the result simplified, and through Mueller matrix way, the expression of refractive index inversion was deduced. The Mueller matrix elements, under different incident angle, are simulated through the expression of specular reflection so as to analyze the influence of the angle of incidence and refractive index on it, which is verified through the measure of the Mueller matrix elements of polished metal surface. Research shows that, under the condition of specular reflection, the result of Mueller matrix inversion is consistent with the experiment and can be used as an index of refraction of inversion method, and it provides a new way for target detection and recognition technology.

Quantitative phase tomography by using x-ray microscope with Foucault knife-edge scanning filter

DOE Office of Scientific and Technical Information (OSTI.GOV)

Watanabe, Norio; Tsuburaya, Yuji; Shimada, Akihiro

2016-01-28

Quantitative phase tomography was evaluated by using a differential phase microscope with a Foucault knife-edge scanning filter. A 3D x-ray phase image of polystyrene beads was obtained at 5.4 keV. The reconstructed refractive index was fairly good agreement with the Henke’s tabulated data.

Telescope for x ray and gamma ray studies in astrophysics

NASA Technical Reports Server (NTRS)

Weaver, W. D.; Desai, Upendra D.

1993-01-01

Imaging of x-rays has been achieved by various methods in astrophysics, nuclear physics, medicine, and material science. A new method for imaging x-ray and gamma-ray sources avoids the limitations of previously used imaging devices. Images are formed in optical wavelengths by using mirrors or lenses to reflect and refract the incoming photons. High energy x-ray and gamma-ray photons cannot be reflected except at grazing angles and pass through lenses without being refracted. Therefore, different methods must be used to image x-ray and gamma-ray sources. Techniques using total absorption, or shadow casting, can provide images in x-rays and gamma-rays. This new method uses a coder made of a pair of Fresnel zone plates and a detector consisting of a matrix of CsI scintillators and photodiodes. The Fresnel zone plates produce Moire patterns when illuminated by an off-axis source. These Moire patterns are deconvolved using a stepped sine wave fitting or an inverse Fourier transform. This type of coder provides the capability of an instantaneous image with sub-arcminute resolution while using a detector with only a coarse position-sensitivity. A matrix of the CsI/photodiode detector elements provides the necessary coarse position-sensitivity. The CsI/photodiode detector also allows good energy resolution. This imaging system provides advantages over previously used imaging devices in both performance and efficiency.

Gradients of refractive index in the crystalline lens and transient changes in refraction among patients with diabetes.

PubMed

Charman, W Neil; Adnan; Atchison, David A

2012-12-01

Transient hyperopic refractive shifts occur on a timescale of weeks in some patients after initiation of therapy for hyperglycemia, and are usually followed by recovery to the original refraction. Possible lenticular origin of these changes is considered in terms of a paraxial gradient index model. Assuming that the lens thickness and curvatures remain unchanged, as observed in practice, it appears possible to account for initial hyperopic refractive shifts of up to a few diopters by reduction in refractive index near the lens center and alteration in the rate of change between center and surface, so that most of the index change occurs closer to the lens surface. Restoration of the original refraction depends on further change in the refractive index distribution with more gradual changes in refractive index from the lens center to its surface. Modeling limitations are discussed.

Gradients of refractive index in the crystalline lens and transient changes in refraction among patients with diabetes

PubMed Central

Charman, W. Neil; Adnan; Atchison, David A.

2012-01-01

Transient hyperopic refractive shifts occur on a timescale of weeks in some patients after initiation of therapy for hyperglycemia, and are usually followed by recovery to the original refraction. Possible lenticular origin of these changes is considered in terms of a paraxial gradient index model. Assuming that the lens thickness and curvatures remain unchanged, as observed in practice, it appears possible to account for initial hyperopic refractive shifts of up to a few diopters by reduction in refractive index near the lens center and alteration in the rate of change between center and surface, so that most of the index change occurs closer to the lens surface. Restoration of the original refraction depends on further change in the refractive index distribution with more gradual changes in refractive index from the lens center to its surface. Modeling limitations are discussed. PMID:23243557

On the refractive index of sodium iodide solutions for index matching in PIV

NASA Astrophysics Data System (ADS)

Bai, Kunlun; Katz, Joseph

2014-04-01

Refractive index matching has become a popular technique for facilitating applications of modern optical diagnostic techniques, such as particle image velocimetry, in complex systems. By matching the refractive index of solid boundaries with that of the liquid, unobstructed optical paths can be achieved for illumination and image acquisition. In this research note, we extend previously provided data for the refractive index of aqueous solutions of sodium iodide (NaI) for concentrations reaching the temperature-dependent solubility limit. Results are fitted onto a quadratic empirical expression relating the concentration to the refractive index. Temperature effects are also measured. The present range of indices, 1.333-1.51, covers that of typical transparent solids, from silicone elastomers to several recently introduced materials that could be manufactured using rapid prototyping. We also review briefly previous measurements of the refractive index, viscosity, and density of NaI solutions, as well as prior research that has utilized this fluid.

High transmission Ni compound refractive lens for high energy X-rays

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brancewicz, M., E-mail: brancew@spring8.or.jp; Itou, M.; Sakurai, Y.

We present a new planar Ni compound refractive lens for high energy X-rays (116 keV). The lens is composed of identical plano-concave elements with longitudinal parabolic grooves manufactured by a punch technique. In order to increase the lens transmission, the thickness of the single lens at the parabolic groove vertex was reduced to less than 5 μm and the radius of curvature was reduced to about 20 μm. The small radius of curvature allowed us to reduce the number of single elements needed to get the focal length of 3 m to 54 single lenses. The gain parameter has beenmore » significantly improved compared to the previous lenses due to higher transmission, but the focused beam size and its gain are not as good as expected, mostly due to the aberrations caused by the lens shape imperfections.« less

Refractive index sensor based on a polymer fiber directional coupler for low index sensing.

PubMed

Lee, Kwang Jo; Liu, Xiaoqi; Vuillemin, Nelly; Lwin, Richard; Leon-Saval, Sergio G; Argyros, Alexander; Kuhlmey, Boris T

2014-07-14

We propose, numerically analyze and experimentally demonstrate a novel refractive index sensor specialized for low index sensing. The device is based on a directional coupler architecture implemented in a single microstructured polymer optical fiber incorporating two waveguides within it: a single-mode core and a satellite waveguide consisting of a hollow high-index ring. This hollow channel is filled with fluid and the refractive index of the fluid is detected through changes to the wavelength at which resonant coupling occurs between the two waveguides. The sensor design was optimized for both higher sensitivity and lower detection limit, with simulations and experiments demonstrating a sensitivity exceeding 1.4 × 10(3) nm per refractive index unit. Simulations indicate a detection limit of ~2 × 10(-6) refractive index units is achievable. We also numerically investigate the performance for refractive index changes localized at the surface of the holes, a case of particular importance for biosensing.

Abdomen X-Ray (Radiography)

MedlinePlus

... News Physician Resources Professions Site Index A-Z X-ray (Radiography) - Abdomen Abdominal x-ray uses a ... of an abdominal x-ray? What is abdominal x-ray? An x-ray (radiograph) is a noninvasive ...

Fiber optic refractive index monitor

DOEpatents

Weiss, Jonathan David

2002-01-01

A sensor for measuring the change in refractive index of a liquid uses the lowest critical angle of a normal fiber optic to achieve sensitivity when the index of the liquid is significantly less than the index of the fiber core. Another embodiment uses a liquid filled core to ensure that its index is approximately the same as the liquid being measured.

X-ray phase contrast tomography by tracking near field speckle

PubMed Central

Wang, Hongchang; Berujon, Sebastien; Herzen, Julia; Atwood, Robert; Laundy, David; Hipp, Alexander; Sawhney, Kawal

2015-01-01

X-ray imaging techniques that capture variations in the x-ray phase can yield higher contrast images with lower x-ray dose than is possible with conventional absorption radiography. However, the extraction of phase information is often more difficult than the extraction of absorption information and requires a more sophisticated experimental arrangement. We here report a method for three-dimensional (3D) X-ray phase contrast computed tomography (CT) which gives quantitative volumetric information on the real part of the refractive index. The method is based on the recently developed X-ray speckle tracking technique in which the displacement of near field speckle is tracked using a digital image correlation algorithm. In addition to differential phase contrast projection images, the method allows the dark-field images to be simultaneously extracted. After reconstruction, compared to conventional absorption CT images, the 3D phase CT images show greatly enhanced contrast. This new imaging method has advantages compared to other X-ray imaging methods in simplicity of experimental arrangement, speed of measurement and relative insensitivity to beam movements. These features make the technique an attractive candidate for material imaging such as in-vivo imaging of biological systems containing soft tissue. PMID:25735237

Cryogenic refractive index of Heraeus homosil glass

NASA Astrophysics Data System (ADS)

Miller, Kevin H.; Quijada, Manuel A.; Leviton, Douglas B.

2017-08-01

This paper reports measurements of the refractive index of Homosil (Heraeus) over the wavelength range of 0.34—3.16 μm and temperature range of 120—335 K. These measurements were performed by using the Cryogenic High Accuracy Refraction Measuring System (CHARMS) facility at the NASA's Goddard Space Flight Center. These measurements were in support of an integrated Structural-Thermal-Optical-Performance (STOP) model that was developed for a fieldwidened Michelson interferometer that is being built and tested for the High Spectral Resolution Lidar (HSRL) project at the NASA Langley Research Center (LaRC). The cryogenic refractive index measurements were required in order to account for the highly sensitive performance of the HSRL instrument to changes in refractive index with temperature, temperature gradients, thermal expansion, and deformation due to mounting stresses. A dense coverage of the absolute refractive index over the aforementioned wavelength and temperature ranges was used to determine the thermo-optic coefficient (dn/dT) and dispersion relation (dn/dλ) as a function of wavelength and temperature. Our measurements of Homosil will be compared with measurements of other glasses from the fused silica family studied in CHARMS as well as measurements reported elsewhere in the literature.

Bioinspired adaptive gradient refractive index distribution lens

NASA Astrophysics Data System (ADS)

Yin, Kezhen; Lai, Chuan-Yar; Wang, Jia; Ji, Shanzuo; Aldridge, James; Feng, Jingxing; Olah, Andrew; Baer, Eric; Ponting, Michael

2018-02-01

Inspired by the soft, deformable human eye lens, a synthetic polymer gradient refractive index distribution (GRIN) lens with an adaptive geometry and focal power has been demonstrated via multilayer coextrusion and thermoforming of nanolayered elastomeric polymer films. A set of 30 polymer nanolayered films comprised of two thermoplastic polyurethanes having a refractive index difference of 0.05 were coextruded via forced-assembly technique. The set of 30 nanolayered polymer films exhibited transmission near 90% with each film varying in refractive index by 0.0017. An adaptive GRIN lens was fabricated from a laminated stack of the variable refractive index films with a 0.05 spherical GRIN. This lens was subsequently deformed by mechanical ring compression of the lens. Variation in the optical properties of the deformable GRIN lens was determined, including 20% variation in focal length and reduced spherical aberration. These properties were measured and compared to simulated results by placido-cone topography and ANSYS methods. The demonstration of a solid-state, dynamic focal length, GRIN lens with improved aberration correction was discussed relative to the potential future use in implantable devices.

Quality control analytical methods: refractive index.

PubMed

Allen, Loyd V

2015-01-01

There are numerous analytical methods that can be utilized in a compounding pharmacy for a quality-assurance program. Since the index of refraction of a liquid/solution is a physical constant, it can be used to assist in identification of a substance, establish its purity, and, in some instances, to determine the concentration of an analyte in solution. This article serves as an introduction to refractive index and some applications of its use in a compounding program.

Saw-tooth refractive lens for high energy x-ray focusing

NASA Astrophysics Data System (ADS)

Antimonov, Mikhail A.; Khounsary, Ali M.

2014-09-01

Saw-tooth refractive lens (SRL) provides a comparatively attractive option for X-ray focusing. An SRL assembly consists of two parts, each with an array of triangular structures (prisms), set tilted symmetrically with respect to the incoming beam. Its main advantage is a simple, continuous tunability in energy and focal length. SRLs can be used for both long and short focal length focusing. Long focal distance focusing of an SRL can accurately be predicted using simple analytical relations. However, the focus size at short focal distances focusing may deviate appreciably from the expected demagnified source size when: (1) the length of the SRL is comparable with the focusing distance, (2) the incident beam is not monochromatic, and (3) and the distance between adjacent prism tips, the tip step, is large . The first factor was considered in a previous work while the other two are addressed is this paper. This preliminary work is aimed at a better understanding of the SRL lenses for focusing an undulator beamline at the Advanced Photon Source (APS).

Refractive-index measurement and inverse correction using optical coherence tomography.

PubMed

Stritzel, Jenny; Rahlves, Maik; Roth, Bernhard

2015-12-01

We describe a novel technique for determination of the refractive index of hard biological tissue as well as nonopaque technical samples based on optical coherence tomography (OCT). Our method relies on an inverse refractive-index correction (I-RIC), which matches a measured feature geometry distorted due to refractive-index boundaries to its real geometry. For known feature geometry, the refractive index can be determined with high precision from the best match between the distorted and corrected images. We provide experimental data for refractive-index measurements on a polymethylmethacrylate (PMMA) and on an ex vivo porcine cranial-bone, which are compared to reference measurements and previously published data. Our method is potentially capable of in vivo measurements on rigid biological tissue such as bone as, for example, is required to improve guidance in robot-aided surgical interventions and also for retrieving complex refractive-index profiles of compound materials.

Imaging method based on attenuation, refraction and ultra-small-angle-scattering of x-rays

DOEpatents

Wernick, Miles N.; Chapman, Leroy Dean; Oltulu, Oral; Zhong, Zhong

2005-09-20

A method for detecting an image of an object by measuring the intensity at a plurality of positions of a transmitted beam of x-ray radiation emitted from the object as a function of angle within the transmitted beam. The intensity measurements of the transmitted beam are obtained by a crystal analyzer positioned at a plurality of angular positions. The plurality of intensity measurements are used to determine the angular intensity spectrum of the transmitted beam. One or more parameters, such as an attenuation property, a refraction property and a scatter property, can be obtained from the angular intensity spectrum and used to display an image of the object.

Refractive index sensor based on the leaky radiation of a microfiber.

PubMed

Gao, F; Liu, H; Sheng, C; Zhu, C; Zhu, S N

2014-05-19

In this work we present a refractive index sensor based on the leaky radiation of a microfiber. The 5.3um diameter microfiber is fabricated by drawing a commercial optical fiber. When the microfiber is immersed into a liquid with larger refractive index than the effective index of fiber mode, the light will leak out through the leaky radiation process. The variation of refractive index of liquid can be monitored by measuring radiation angle of light. The refractive index sensitivity can be over 400 degree/RIU in theory. In the experiment, the variation value 0.001 of refractive index of liquid around this microfiber can be detected through this technique. This work provides a simple and sensitive method for refractive index sensing application.

Infrared complex refractive index of astrophysical ices exposed to cosmic rays simulated in the laboratory

NASA Astrophysics Data System (ADS)

Rocha, W. R. M.; Pilling, S.; de Barros, A. L. F.; Andrade, D. P. P.; Rothard, H.; Boduch, P.

2017-01-01

In the dense and cold regions of the interstellar medium, molecules can be adsorbed on to dust grains to form ice mantles. Once formed, these can be processed by ionizing radiation coming from the stellar or interstellar medium, leading to the formation of several new molecules in the ice. Among the different types of ionizing radiation, cosmic rays play an important role in solid-phase chemistry because of the large amount of energy deposited in the ices. The physicochemical changes induced by the energetic processing of astrophysical ices are recorded in a intrinsic parameter of the matter called the complex refractive index. In this paper, for the first time, we present a catalogue containing 39 complex refractive indices (n, k) in the infrared from 5000 to 600 cm-1 (2.0-16.6 μm) for 13 different water-containing ices processed in the laboratory by cosmic ray analogues. The calculation was performed using the NKABS - an acronym of the determination of N and K from absorbance data - code,which employs the Lambert-Beer and Kramers-Kronig equations to calculate the values of n and k. The results are also available at the following web site: http://www1.univap.br/gaa/nkabs-database/data.htm. As a test case, H2O:NH3:CO2:CH4 ice was employed in a radiative transfer simulation of a protoplanetary disc to show that these data are indispensable to reproduce the spectrum of ices containing young stellar objects.

Refractive index retrieving of polarization maintaining optical fibers

NASA Astrophysics Data System (ADS)

Ramadan, W. A.; Wahba, H. H.; Shams El-Din, M. A.; Abd El-Sadek, I. G.

2018-01-01

In this paper, the cross-section images, of two different types of polarization maintaining (PM) optical fibers, are employed to estimate the optical phase variation due to transverse optical rays passing through these optical fibers. An adaptive algorithm is proposed to recognize the different areas constituting the PM optical fibers cross-sections. These areas are scanned by a transverse beam to calculate the optical paths for given values of refractive indices. Consequently, the optical phases across the PM optical fibers could be recovered. PM optical fiber is immersed in a matching fluid and set in the object arm of Mach-Zehnder interferometer. The produced interferograms are analyzed to extract the optical phases caused by the PM optical fibers. The estimated optical phases could be optimized to be in good coincidence with experimentally extracted ones. This has been achieved through changing of the PM optical fibers refractive indices to retrieve the correct values. The correct refractive indices values are confirmed by getting the best fit between the estimated and the extracted optical phases. The presented approach is a promising one because it provides a quite direct and accurate information about refractive index, birefringence and beat length of PM optical fibers comparing with different techniques handle the same task.

Refractive-index profiling of embedded microstructures in optical materials

NASA Astrophysics Data System (ADS)

Dave, Digant P.; Milner, Thomas E.

2002-04-01

We describe use of a phase-sensitive low-coherence reflectometer to measure spatial variation of refractive index in optical materials. The described interferometric technique is demonstrated to be a valuable tool to profile the refractive index of optical elements such as integrated waveguides and photowritten optical microstructures. As an example, a refractive-index profile is mapped of a microstructure written in a microscope glass slide with an ultrashort-pulse laser.

High refractive index and temperature sensitivity LPGs for high temperature operation

NASA Astrophysics Data System (ADS)

Nascimento, I. M.; Gouveia, C.; Jana, Surnimal; Bera, Susanta; Baptista, J. M.; Moreira, Paulo; Biwas, Palas; Bandyopadhyay, Somnath; Jorge, Pedro A. S.

2013-11-01

A fiber optic sensor for high sensitivity refractive index and temperature measurement able to withstand temperature up to 450 °C is reported. Two identical LPG gratings were fabricated, whereas one was coated with a high refractive index (~1.78) sol-gel thin film in order to increase its sensitivity to the external refractive index. The two sensors were characterized and compared in refractive index and temperature. Sensitivities of 1063 nm/RIU (1.338 - 1.348) and 260 pm/°C were achieved for refractive index and temperature, respectively.

Phase-contrast microtomography using an X-ray interferometer having a 40-μm analyzer

NASA Astrophysics Data System (ADS)

Momose, A.; Koyama, I.; Hamaishi, Y.; Yoshikawa, H.; Takeda, T.; Wu, J.; Itai, Y.; Takai, , K.; Uesugi, K.; Suzuki, Y.

2003-03-01

Phase-contrast X-ray tomographic experiment using a triple Laue-case (LLL) interferometer having a 40-μm lamella which was fabricated to improve spatial resolution, was carried out using undulator X-rays at SPring-8, Japan. Three-dimensional images mapping the refractive index were measured for various animal tissues. Comparing the images with those obtained in previous experiments using conventional LLL interferometers having a 1-mm lamella, improvement in the spatial resolution was demonstrated in that histological structures, such as hepatic lobules in liver and tubules in kidney, were revealed.

Equivalent refractive-index structure constant of non-Kolmogorov turbulence.

PubMed

Li, Yujie; Zhu, Wenyue; Wu, Xiaoqing; Rao, Ruizhong

2015-09-07

The relationship between the non-Kolmogorov refractive-index structure constant and the Kolmogorov refractive-index structure constant is derived by using the refractive-index structure function and the variance of refractive-index fluctuations. It shows that the non-Kolmogorov structure constant is proportional to the Kolmogorov structure constant and the scaling factor depends on the outer scale and the spectral power law. For a fixed Kolmogorov structure constant, the non-Kolmogorov structure constant increases with a increasing outer scale for the power law less than 11/3, the trend is opposite for the power law greater than 11/3. This equivalent relation provides a way of obtaining the non-Kolmogorov structure constant by using the Kolmogorov structure constant.

Refractive index dependence of L3 photonic crystal nano-cavities.

PubMed

Adawi, A M; Chalcraft, A R; Whittaker, D M; Lidzey, D G

2007-10-29

We model the optical properties of L3 photonic crystal nano-cavities as a function of the photonic crystal membrane refractive index n using a guided mode expansion method. Band structure calculations revealed that a TE-like full band-gap exists for materials of refractive index as low as 1.6. The Q-factor of such cavities showed a super-linear increase with refractive index. By adjusting the relative position of the cavity side holes, the Q-factor was optimised as a function of the photonic crystal membrane refractive index n over the range 1.6 to 3.4. Q-factors in the range 3000-8000 were predicted from absorption free materials in the visible range with refractive index between 2.45 and 2.8.

Denaturation process of laccase in various media by refractive index measurements.

PubMed

Saoudi, O; Ghaouar, N; Ben Salah, S; Othman, T

2017-09-01

In this work, we are interested in the denaturation process of a laccase from Tramates versicolor via the determination of the refractive index, the refractive index increment and the specific volume in various media. The measurements were carried out using an Abbe refractometer. We have shown that the refractive index increment values obtained from the slope of the variation of the refractive index vs. Concentration are outside the range refractive index increments of proteins. To correct the results, we have followed the theoretical predictions based on the knowledge of the protein refractive index from its amino acids composition. The denaturation process was studied by calculating the specific volume variation where its determination was related to the Gladstone-Dale and the Lorentz-Lorentz models.

Refractive index measurements in absorbing media with white light spectral interferometry.

PubMed

Arosa, Yago; Lago, Elena López; de la Fuente, Raúl

2018-03-19

White light spectral interferometry is applied to measure the refractive index in absorbing liquids in the spectral range of 400-1000 nm. We analyze the influence of absorption on the visibility of interferometric fringes and, accordingly, on the measurement of the refractive index. Further, we show that the refractive index in the absorption band can be retrieved by a two-step process. The procedure requires the use of two samples of different thickness, the thicker one to retrieve the refractive index in the transparent region and the thinnest to obtain the data in the absorption region. First, the refractive index values are retrieved with good accuracy in the transparent region of the material for 1-mm-thick samples. Second, these refractive index values serve also to precisely calculate the thickness of a thinner sample (~150 µm) since the accuracy of the methods depends strongly on the thickness of the sample. Finally, the refractive index is recovered for the entire spectral range.

INTEGRATED AND FIBER OPTICS: Investigation of the refractive index profile of inhomogeneous iron garnet films containing bismuth

NASA Astrophysics Data System (ADS)

Arzamastseva, G. V.; Kravchenko, V. B.; Filimonova, L. M.

1989-02-01

The refractive index n of quasihomogeneous iron garnet films with the composition (YGdYb)3 - xBixFe5 - yAlyO12 increased considerably as a result of reduction in the growth temperature Tg. This was attributed mainly by an increase in x and a reduction in y. The dependences n(Tg) were used to select the conditions for growth of inhomogeneous (across the thickness) films and to predict the refractive index profile n(z), where z was measured from the free surface along the normal to the film. The spectra of optical modes were analyzed in the WKB approximation and this yielded the n(z) profiles for films with a refractive index n decreasing monotonically from the free surface and for films with the symmetric profile n(z) (buried waveguides). The n(z) profiles were compared with the distributions of the compensation temperature Tc(z), and of x(z) and y(z) across the thickness.

Measurement of Refractive Index Using a Michelson Interferometer.

ERIC Educational Resources Information Center

Fendley, J. J.

1982-01-01

Describes a novel and simple method of measuring the refractive index of transparent plates using a Michelson interferometer. Since it is necessary to use a computer program when determining the refractive index, undergraduates could be given the opportunity of writing their own programs. (Author/JN)

Optofluidic refractive-index sensor in step-index fiber with parallel hollow micro-channel.

PubMed

Lee, H W; Schmidt, M A; Uebel, P; Tyagi, H; Joly, N Y; Scharrer, M; Russell, P St J

2011-04-25

We present a simple refractive index sensor based on a step-index fiber with a hollow micro-channel running parallel to its core. This channel becomes waveguiding when filled with a liquid of index greater than silica, causing sharp dips to appear in the transmission spectrum at wavelengths where the glass-core mode phase-matches to a mode of the liquid-core. The sensitivity of the dip-wavelengths to changes in liquid refractive index is quantified and the results used to study the dynamic flow characteristics of fluids in narrow channels. Potential applications of this fiber microstructure include measuring the optical properties of liquids, refractive index sensing, biophotonics and studies of fluid dynamics on the nanoscale.

Cr/B 4C multilayer mirrors: Study of interfaces and X-ray reflectance

DOE PAGES

Burcklen, C.; Soufli, R.; Gullikson, E.; ...

2016-03-24

Here, we present an experimental study of the effect of layer interfaces on the x-ray reflectance in Cr/B 4C multilayer interference coatings with layer thicknesses ranging from 0.7 nm to 5.4 nm. The multilayers were deposited by magnetron sputtering and by ion beam sputtering. Grazing incidence x-ray reflectometry, soft x-ray reflectometry, and transmission electron microscopy reveal asymmetric multilayer structures with a larger B 4C-on-Cr interface, which we modeled with a 1–1.5 nm thick interfacial layer. Reflectance measurements in the vicinity of the Cr L 2,3 absorption edge demonstrate fine structure that is not predicted by simulations using the currently tabulatedmore » refractive index (optical constants) values for Cr.« less

Manipulating Refractive Index in Organic Light-Emitting Diodes.

PubMed

Salehi, Amin; Chen, Ying; Fu, Xiangyu; Peng, Cheng; So, Franky

2018-03-21

In a conventional organic light-emitting diode (OLED), only a fraction of light can escape to the glass substrate and air. Most radiation is lost to two major channels: waveguide modes and surface plasmon polaritons. It is known that reducing the refractive indices of the constituent layers in an OLED can enhance light extraction. Among all of the layers, the refractive index of the electron transport layer (ETL) has the largest impact on light extraction because it is the layer adjacent to the metallic cathode. Oblique angle deposition (OAD) provides a way to manipulate the refractive index of a thin film by creating an ordered columnar void structure. In this work, using OAD, the refractive index of tris(8-hydroxyquinoline)aluminum (Alq3) can be tuned from 1.75 to 1.45. With this low-index ETL deposited by OAD, the resulting phosphorescent OLED shows nearly 30% increase in light extraction efficiency.

Understanding refraction contrast using a comparison of absorption and refraction computed tomographic techniques

NASA Astrophysics Data System (ADS)

Wiebe, S.; Rhoades, G.; Wei, Z.; Rosenberg, A.; Belev, G.; Chapman, D.

2013-05-01

Refraction x-ray contrast is an imaging modality used primarily in a research setting at synchrotron facilities, which have a biomedical imaging research program. The most common method for exploiting refraction contrast is by using a technique called Diffraction Enhanced Imaging (DEI). The DEI apparatus allows the detection of refraction between two materials and produces a unique ''edge enhanced'' contrast appearance, very different from the traditional absorption x-ray imaging used in clinical radiology. In this paper we aim to explain the features of x-ray refraction contrast as a typical clinical radiologist would understand. Then a discussion regarding what needs to be considered in the interpretation of the refraction image takes place. Finally we present a discussion about the limitations of planar refraction imaging and the potential of DEI Computed Tomography. This is an original work that has not been submitted to any other source for publication. The authors have no commercial interests or conflicts of interest to disclose.

Index of Refraction without Geometry

ERIC Educational Resources Information Center

Farkas, N.; Henriksen, P. N.; Ramsier, R. D.

2006-01-01

This article presents several activities that permit students to determine the index of refraction of transparent solids and liquids using simple equipment without the need for geometrical relationships, special lighting or optical instruments. Graphical analysis of the measured data is shown to be a useful method for determining the index of…

Panoramic Dental X-Ray

MedlinePlus

... Physician Resources Professions Site Index A-Z Panoramic Dental X-ray Panoramic dental x-ray uses a very small dose of ... x-ray , is a two-dimensional (2-D) dental x-ray examination that captures the entire mouth ...

Imaginary refractive index and other microphysical properties of volcanic ash, Sarahan dust, and other mineral aerosols

NASA Astrophysics Data System (ADS)

Rocha Lima, A.; Martins, J.; Krotkov, N. A.; Artaxo, P.; Todd, M.; Ben Ami, Y.; Dolgos, G.; Espinosa, R.

2013-12-01

Aerosol properties are essential to support remote sensing measurements, atmospheric circulation and climate models. This research aims to improve the understanding of the optical and microphysical properties of different types of aerosols particles. Samples of volcanic ash, Saharan dust and other mineral aerosols particles were analyzed by different techniques. Ground samples were sieved down to 45um, de-agglomerated and resuspended in the laboratory using a Fluidized Bed Aerosol Generator (FBAG). Particles were collected on Nuclepore filters into PM10, PM2.5, or PM1.0. and analyzed by different techniques, such as Scanning Electron Microscopy (SEM) for determination of size distribution and shape, spectral reflectance for determination of the optical absorption properties as a function of the wavelength, material density, and X-Ray fluorescence for the elemental composition. The spectral imaginary part of refractive index from the UV to the short wave infrared (SWIR) wavelength was derived empirically from the measurements of the spectral mass absorption coefficient, size distribution and density of the material. Some selected samples were also analyzed with the Polarized Imaging Nephelometer (PI-Neph) instrument for the characterization of the aerosol polarized phase function. This work compares results of the spectral refractive index of different materials obtained by our methodology with those available in the literature. In some cases there are significant differences both in magnitude and spectral dependence of the imaginary refractive index. These differences are evaluated and discussed in this work.

X-ray Full Field Microscopy at 30 keV

NASA Astrophysics Data System (ADS)

Marschall, F.; Last, A.; Simon, M.; Kluge, M.; Nazmov, V.; Vogt, H.; Ogurreck, M.; Greving, I.; Mohr, J.

2014-04-01

In our X-ray full field microscopy experiments, we demonstrated a resolution better than 260 nm over the entire field of view of 80 μm × 80 μm at 30 keV. Our experimental setup at PETRA III, P05, had a length of about 5 m consisting of an illumination optics, an imaging lens and a detector. For imaging, we used a compound refractive lens (CLR) consisting of mr-L negative photo resist, which was fabricated by deep X-ray lithography. As illumination optics, we choose a refractive rolled X-ray prism lens, which was adapted to the numerical aperture of the imaging lens.

Single tapered fiber tip for simultaneous measurements of thickness, refractive index and distance to a sample.

PubMed

Moreno-Hernández, Carlos; Monzón-Hernández, David; Hernández-Romano, Iván; Villatoro, Joel

2015-08-24

We demonstrate the capability of an air cavity Fabry-Perot interferometer (FPI), built with a tapered lead-in fiber tip, to measure three parameters simultaneously, distance, group refractive index and thickness of transparent samples introduced in the cavity. Tapering the lead-in fiber enhances the light coupling back efficiency, therefore is possible to enlarge the air cavity without a significant deterioration of the fringe visibility. Fourier transformation, used to analyze the reflected optical spectrum of our FPI, simplify the calculus to determine the position, thickness and refractive index. Samples made of 7 different glasses; fused silica, BK7, BalF5, SF2, BaF51, SF15, and glass slides were used to test our FPI. Each sample was measured nine times and the results for position, thickness and refractive index showed differences of ± 0.7%, ± 0.1%, and ± 0.16% respectively. The evolution of thickness and refractive index of a block of polydimethylsiloxane (PDMS) elastomer due to temperature changes in the range of 25°C to 90°C were also measured. The coefficients of the thermal expansion and thermo-optic estimated were α = 4.71x10(-4)/°C and dn/dT = -4.66 x10(-4) RIU/°C, respectively.

Refractive index of colloidal dispersions of spheroidal particles

DOE Office of Scientific and Technical Information (OSTI.GOV)

Meeten, G.H.

1980-09-01

The effect of particle shape on the refractive index of a colloidal dispersion of spheroidal particles is investigated theoretically, using the Rayleigh, Rayleigh- Gans-Debye, and the anomalous diffraction light-scattering approximations. It is shown that departure from particle sphericity modify the dispersion refractive index, both size and shape being of importance.

Spatial Frequency Multiplexing of Fiber-Optic Interferometric Refractive Index Sensors Based on Graded-Index Multimode Fibers

PubMed Central

Liu, Li; Gong, Yuan; Wu, Yu; Zhao, Tian; Wu, Hui-Juan; Rao, Yun-Jiang

2012-01-01

Fiber-optic interferometric sensors based on graded-index multimode fibers have very high refractive-index sensitivity, as we previously demonstrated. In this paper, spatial-frequency multiplexing of this type of fiber-optic refractive index sensors is investigated. It is estimated that multiplexing of more than 10 such sensors is possible. In the multiplexing scheme, one of the sensors is used to investigate the refractive index and temperature responses. The fast Fourier transform (FFT) of the combined reflective spectra is analyzed. The intensity of the FFT spectra is linearly related with the refractive index and is not sensitive to the temperature.

Fabrication of refractive index distributions in polymer using a photochemical reaction

NASA Astrophysics Data System (ADS)

Kada, Takeshi; Obara, Atsushi; Watanabe, Toshiyuki; Miyata, Seizo; Liang, Chuan Xin; Machida, Hideaki; Kiso, Koichi

2000-01-01

We demonstrate that a photochemical reaction can create various distributions of refractive index in polymer. When the polymer containing a photochemically active material is irradiated by UV light, the photochemical reaction which breaks the π-conjugated system in the material and decreases its linear polarizability can reduce refractive index of the polymer. We prepared a PMMA film added DMAPN ((4-N,N-dimethylaminophenyl)-N'-phenylnitrone) with a rate of 23 wt % by use of spin coating. Electronic structural change of DMAPN and refractive indices of the film before and after UV irradiation were evaluated by UV absorption spectra and m-line method, respectively. The UV irradiation decreased λmax at 380 nm in the absorption spectra, which is attributed to nitrone, and the refractive indices exponentially with irradiation time. The change of refractive indices reached 0.028. The refractive index profile upon depth of the film was investigated by measuring refractive indices of stacked DMAPN/PMMA films. When UV with a power of 10.7 mW/cm2 irradiated upon three stacked DMAPN/PMMA films for 35 s, variation of the refractive index change showed a quadratic profile. The refractive index profile with various irradiation time can be accounted with the combination of the chemical kinetics with the steady state approximation and Lambert-Beer's law. Thus, the photochemical reaction can be used to control the refractive index distribution in polymer.

Ultrasensitive Magnetic Field Sensing Based on Refractive-Index-Matched Coupling.

PubMed

Rao, Jie; Pu, Shengli; Yao, Tianjun; Su, Delong

2017-07-07

An ultrasensitive magnetic field sensor is proposed and investigated experimentally. The no-core fiber is fusion-spliced between two pieces of single-mode fibers and then immersed in magnetic fluid with an appropriate value of refractive index. Under the refractive-index-matched coupling condition, the guided mode becomes leaky and a coupling wavelength dip in the transmission spectrum of the structure is observed. The coupling wavelength dip is extremely sensitive to the ambient environment. The excellent sensitivity to the refractive index is measured to be 116.681 μm/RIU (refractive index unit) in the refractive index range of 1.45691-1.45926. For the as-fabricated sensors, the highest magnetic field sensing sensitivities of 6.33 and 1.83 nm/mT are achieved at low and high fields, respectively. The sensitivity is considerably enhanced compared with those of previously designed, similar structures.

Analytical transmission cross-coefficients for pink beam X-ray microscopy based on compound refractive lenses.

PubMed

Falch, Ken Vidar; Detlefs, Carsten; Snigirev, Anatoly; Mathiesen, Ragnvald H

2018-01-01

Analytical expressions for the transmission cross-coefficients for x-ray microscopes based on compound refractive lenses are derived based on Gaussian approximations of the source shape and energy spectrum. The effects of partial coherence, defocus, beam convergence, as well as lateral and longitudinal chromatic aberrations are accounted for and discussed. Taking the incoherent limit of the transmission cross-coefficients, a compact analytical expression for the modulation transfer function of the system is obtained, and the resulting point, line and edge spread functions are presented. Finally, analytical expressions for optimal numerical aperture, coherence ratio, and bandwidth are given. Copyright © 2017 Elsevier B.V. All rights reserved.

High refractive index nanocomposite fluids for immersion lithography.

PubMed

Bremer, L; Tuinier, R; Jahromi, S

2009-02-17

The concept of using dispersions of nanoparticles as high refractive index fluids in immersion lithography is examined both from a theoretical and experimental point of view. In the theoretical part we show that gelation and demixing can be controlled in high solid dispersions, needed to achieve a high (refractive) index, by using short stabilizing brushes. We considered both fluid-fluid demixing by using statistical thermodynamics and percolation, computed using liquid-state approaches. Whenever demixing or percolation takes place, the nanoparticle dispersion is unsuited for immersion lithography. The minimum thickness of the stabilizer layer of a stable suspension is estimated assuming particles plus steric stabilizer to act as hard spheres with van der Waals attraction between the cores. Since the van der Waals attraction can be related to the optical properties of the particles and dispersion medium, it is also possible to estimate the refractive index that can be attained with composite immersion fluids. Using materials that are known to be highly transparent in the bulk at a wavelength of 193 nm, indices above 1.8 can be attained. Other materials with higher indices are expected to be transparent at 193 nm due to a blue shift of the UV absorption and enable much higher indices. In the experiment, we show that it is possible to prepare suspensions with particles of about 4 nm diameter that increase the refractive index of the continuous phase with 0.2 at a wavelength of 193 nm. The refractive index and density of such dispersions are proportional to the volume fraction of the disperse phase, and it is shown that the refractive index of the composite fluid can be predicted very well from the optical properties of the components. Furthermore, successful imaging experiments were performed through a dispersion of silica nanoparticles. These findings lead to the conclusion that immersion lithography using nanoparticle dispersions is indeed possible.

Plasmonic crystal enhanced refractive index sensing

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stein, Benedikt; Devaux, Eloïse; Genet, Cyriaque, E-mail: genet@unistra.fr

2014-06-23

We demonstrate experimentally how the local anisotropy of the dispersion relation of surface plasmon modes propagating over periodic metal gratings can lead to an enhancement of the figure of merit of refractive index sensors. Exploiting the possibility to acquire defocused images of the Fourier space of a highly stable leakage radiation microscope, we report a twofold increase in sensing sensitivity close to the band gap of a one-dimensional plasmonic crystal where the anisotropy of the band structure is the most important. A practical sensing resolution of O(10{sup −6}) refractive index units is demonstrated.

Miniature interferometer for refractive index measurement in microfluidic chip

NASA Astrophysics Data System (ADS)

Chen, Minghui; Geiser, Martial; Truffer, Frederic; Song, Chengli

2012-12-01

The design and development of the miniaturized interferometer for measurement of the refractive index or concentration of sub-microliter volume aqueous solution in microfludic chip is presented. It is manifested by a successful measurement of the refractive index of sugar-water solution, by utilizing a laser diode for light source and the small robust instrumentation for practical implementation. Theoretically, the measurement principle and the feasibility of the system are analyzed. Experimental device is constructed with a diode laser, lens, two optical plate and a complementary metal oxide semiconductor (CMOS). Through measuring the positional changes of the interference fringes, the refractive index change are retrieved. A refractive index change of 10-4 is inferred from the measured image data. The entire system is approximately the size of half and a deck of cards and can operate on battery power for long time.

Biconcave micro-optofluidic lens with low-refractive-index liquids.

PubMed

Song, Chaolong; Nguyen, Nam-Trung; Asundi, Anand Krishna; Low, Cassandra Lee-Ngo

2009-12-01

One of the current problems of micro-optofluidics is the choice of a suitable liquid with a high refractive index (RI). We report the use of a low-RI liquid in a biconcave liquid-core liquid-cladding lens for focusing light. For the characterization of the lens, a telescope system was constructed from polydimethylsiloxane lenses to collimate and expand a light beam emitted from an optical fiber. The tunable optofluidic biconcave lens focuses the parallel beam. Fluorescent dye diluted in an index-matching liquid was used for the visualization of the light rays in a beam-tracing chamber. The focused beam is tuned by adjusting the flow rate ratio between core and cladding streams.

Femtosecond laser-induced refractive index modification in multicomponent glasses

NASA Astrophysics Data System (ADS)

Bhardwaj, V. R.; Simova, E.; Corkum, P. B.; Rayner, D. M.; Hnatovsky, C.; Taylor, R. S.; Schreder, B.; Kluge, M.; Zimmer, J.

2005-04-01

We present a comprehensive study on femtosecond laser-induced refractive index modification in a wide variety of multicomponent glasses grouped as borosilicate, aluminum-silicate, and heavy-metal oxide glasses along with lanthanum-borate and sodium-phosphate glasses. By using high-spatial resolution refractive index profiling techniques, we demonstrate that under a wide range of writing conditions the refractive index modification in multicomponent glasses can be positive, negative, or nonuniform, and exhibits a strong dependence on the glass composition. With the exception of some aluminum-silicate glasses all other glasses exhibited a negative/nonuniform index change. We also demonstrate direct writing of waveguides in photosensitive Foturan® glass with a femtosecond laser without initiating crystallization by thermal treatment. Upon ceramization of lithium-aluminum-silicate glasses such as Foturan®, Zerodur®, and Robax® we observe switching of laser-induced refractive index change from being positive to negative. The measured transmission losses in the waveguides at 1550nm agree with the index profile measurements in alkali-free aluminum-silicate glasses.

About complex refractive index of black Si

NASA Astrophysics Data System (ADS)

Pinčík, Emil; Brunner, Robert; Kobayashi, Hikaru; Mikula, Milan

2017-12-01

The paper deals with the complex refractive index in the IR light region of two types of samples (i) as prepared black silicon, and (ii) thermally oxidized black silicon (BSi) nano-crystalline specimens produced both by the surface structure chemical transfer method using catalytic Ag evaporated spots (as prepared sample) and by the catalytic Pt catalytic mesh (thermally oxidized sample). We present, compare, and discuss the values of the IR complex refractive index obtained by calculation using the Kramers-Krönig transformation. Results indicate that small differences between optical properties of as prepared black Si and thermally oxidized BSi are given by: (i) - oxidation procedure, (ii) - thickness of the formed black Si layer, mainly, not by utilization of different catalytic metals, and by iii) the different thickness. Contamination of the surface by different catalytic metals contributes almost equally to the calculated values of the corresponding complex refractive index.

Note: Index of refraction measurement using the Fresnel equations.

PubMed

McClymer, J P

2014-08-01

The real part of the refractive index is measured from 1.30 to above 3.00 without the use of index matching fluids. This approach expands upon the Brewster angle technique as both S and P polarized lights are used and the full Fresnel equations fitted to the data to extract the index of refraction using nonlinear curve fitting.

String and Sticky Tape Experiments: Refractive Index of Liquids.

ERIC Educational Resources Information Center

Edge, R. D., Ed.

1979-01-01

Describes a simple method of measuring the refractive index of a liquid using a paper cup, a liquid, a pencil, and a ruler. Uses the ratio between the actual depth and the apparent depth of the cup to calculate the refractive index. (GA)

Numerical simulations of negative-index refraction in wedge-shaped metamaterials.

PubMed

Dong, Z G; Zhu, S N; Liu, H; Zhu, J; Cao, W

2005-07-01

A wedge-shaped structure made of split-ring resonators (SRR) and wires is numerically simulated to evaluate its refraction behavior. Four frequency bands, namely, the stop band, left-handed band, ultralow-index band, and positive-index band, are distinguished according to the refracted field distributions. Negative phase velocity inside the wedge is demonstrated in the left-handed band and the Snell's Law is conformed in terms of its refraction behaviors in different frequency bands. Our results confirmed that negative index of refraction indeed exists in such a composite metamaterial and also provided a convincing support to the results of previous Snell's Law experiments.

Improved retroreflection method for measuring the refractive index of liquids.

PubMed

Shao, Duo; Tian, Linghao; Chen, Jingfei; Chen, Xianfeng

2010-06-01

We propose a new method for measuring the refractive index of liquids with high precision; the method is based on use of the optical fiber end face. As an example, we investigated the refractive index of sugar solution under varying conditions tens of times. The results show that this method has the advantage of higher stability and repeatability. The concentration and the temperature-dependent refractive index of the sugar solution is also experimentally studied.

From X-Ray Telescopes to Neutron Focusing

NASA Technical Reports Server (NTRS)

Gubarev, M. V.; Khaykovich, B.; Ramsey, B.; Moncton, D. E.

2011-01-01

In the case of neutrons the refractive index is slightly less than unity for most elements and their isotopes. Consequently, thermal and cold neutrons can be reflected from smooth surfaces at grazing-incidence angles. Hence, the optical technologies developed for x-ray astronomy can be applied for neutron focusing. The focusing capabilities of grazing incidence neutron imaging optics have been successfully demonstrated using nickel mirrors. The mirrors were fabricated using an electroformed nickel replication process at Marshall Space Flight Center. Results of the neutron optics experiments will be presented. Challenges of the neutron imaging optics as well as possible applications of the optics will be discussed.

Optical CT imaging of solid radiochromic dosimeters in mismatched refractive index solutions using a scanning laser and large area detector

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dekker, Kurtis H., E-mail: kdekker2@uwo.ca

Purpose: The practical use of the PRESAGE® solid plastic dosimeter is limited by the inconvenience of immersing it in high-viscosity oils to achieve refractive index matching for optical computed tomography (CT) scanning. The oils are slow to mix and difficult to clean from surfaces, and the dosimeter rotation can generate dynamic Schlieren inhomogeneity patterns in the reference liquid, limiting the rotational and overall scan speed. Therefore, it would be beneficial if lower-viscosity, water-based solutions with slightly unmatched refractive index could be used instead. The purpose of this work is to demonstrate the feasibility of allowing mismatched conditions when using amore » scanning laser system with a large acceptance angle detector. A fiducial-based ray path measurement technique is combined with an iterative CT reconstruction algorithm to reconstruct images. Methods: A water based surrounding liquid with a low viscosity was selected for imaging PRESAGE® solid dosimeters. Liquid selection was optimized to achieve as high a refractive index as possible while avoiding rotation-induced Schlieren effects. This led to a refractive index mismatch of 6% between liquid and dosimeters. Optical CT scans were performed with a fan-beam scanning-laser optical CT system with a large area detector to capture most of the refracted rays. A fiducial marker placed on the wall of a cylindrical sample occludes a given light ray twice. With knowledge of the rotation angle and the radius of the cylindrical object, the actual internal path of each ray through the dosimeter can be calculated. Scans were performed with 1024 projections of 512 data samples each, and rays were rebinned to form 512 parallel-beam projections. Reconstructions were performed on a 512 × 512 grid using 100 iterations of the SIRT iterative CT algorithm. Proof of concept was demonstrated with a uniformly attenuating solution phantom. PRESAGE® dosimeters (11 cm diameter) were irradiated with Cobalt-60

Optical CT imaging of solid radiochromic dosimeters in mismatched refractive index solutions using a scanning laser and large area detector.

PubMed

Dekker, Kurtis H; Battista, Jerry J; Jordan, Kevin J

2016-08-01

The practical use of the PRESAGE® solid plastic dosimeter is limited by the inconvenience of immersing it in high-viscosity oils to achieve refractive index matching for optical computed tomography (CT) scanning. The oils are slow to mix and difficult to clean from surfaces, and the dosimeter rotation can generate dynamic Schlieren inhomogeneity patterns in the reference liquid, limiting the rotational and overall scan speed. Therefore, it would be beneficial if lower-viscosity, water-based solutions with slightly unmatched refractive index could be used instead. The purpose of this work is to demonstrate the feasibility of allowing mismatched conditions when using a scanning laser system with a large acceptance angle detector. A fiducial-based ray path measurement technique is combined with an iterative CT reconstruction algorithm to reconstruct images. A water based surrounding liquid with a low viscosity was selected for imaging PRESAGE® solid dosimeters. Liquid selection was optimized to achieve as high a refractive index as possible while avoiding rotation-induced Schlieren effects. This led to a refractive index mismatch of 6% between liquid and dosimeters. Optical CT scans were performed with a fan-beam scanning-laser optical CT system with a large area detector to capture most of the refracted rays. A fiducial marker placed on the wall of a cylindrical sample occludes a given light ray twice. With knowledge of the rotation angle and the radius of the cylindrical object, the actual internal path of each ray through the dosimeter can be calculated. Scans were performed with 1024 projections of 512 data samples each, and rays were rebinned to form 512 parallel-beam projections. Reconstructions were performed on a 512 × 512 grid using 100 iterations of the SIRT iterative CT algorithm. Proof of concept was demonstrated with a uniformly attenuating solution phantom. PRESAGE® dosimeters (11 cm diameter) were irradiated with Cobalt-60 irradiator to achieve

Plasmonic nanoshell functionalized etched fiber Bragg gratings for highly sensitive refractive index measurements.

PubMed

Burgmeier, Jörg; Feizpour, Amin; Schade, Wolfgang; Reinhard, Björn M

2015-02-15

A novel fiber optical refractive index sensor based on gold nanoshells immobilized on the surface of an etched single-mode fiber including a Bragg grating is demonstrated. The nanoparticle coating induces refractive index dependent waveguide losses, because of the variation of the evanescently guided part of the light. Hence the amplitude of the Bragg reflection is highly sensitive to refractive index changes of the surrounding medium. The nanoshell functionalized fiber optical refractive index sensor works in reflectance mode, is suitable for chemical and biochemical sensing, and shows an intensity dependency of 4400% per refractive index unit in the refractive index range between 1.333 and 1.346. Furthermore, the physical length of the sensor is smaller than 3 mm with a diameter of 6 μm, and therefore offers the possibility of a localized refractive index measurement.

Hard x-ray phase contrastmicroscopy - techniques and applications

NASA Astrophysics Data System (ADS)

Holzner, Christian

In 1918, Einstein provided the first description of the nature of the refractive index for X-rays, showing that phase contrast effects are significant. A century later, most x-ray microscopy and nearly all medical imaging remains based on absorption contrast, even though phase contrast offers orders of magnitude improvements in contrast and reduced radiation exposure at multi-keV x-ray energies. The work presented is concerned with developing practical and quantitative methods of phase contrast for x-ray microscopy. A theoretical framework for imaging in phase contrast is put forward; this is used to obtain quantitative images in a scanning microscope using a segmented detector, and to correct for artifacts in a commercial phase contrast x-ray nano-tomography system. The principle of reciprocity between scanning and full-field microscopes is then used to arrive at a novel solution: Zernike contrast in a scanning microscope. These approaches are compared on a theoretical and experimental basis in direct connection with applications using multi-keV x-ray microscopes at the Advanced Photon Source at Argonne National Laboratory. Phase contrast provides the best means to image mass and ultrastructure of light elements that mainly constitute biological matter, while stimulated x-ray fluorescence provides high sensitivity for studies of the distribution of heavier trace elements, such as metals. These approaches are combined in a complementary way to yield quantitative maps of elemental concentration from 2D images, with elements placed in their ultrastructural context. The combination of x-ray fluorescence and phase contrast poses an ideal match for routine, high resolution tomographic imaging of biological samples in the future. The presented techniques and demonstration experiments will help pave the way for this development.

X-ray optical simulations supporting advanced commissioning of the coherent hard x-ray beamline at NSLS-II

NASA Astrophysics Data System (ADS)

Wiegart, L.; Rakitin, M.; Fluerasu, A.; Chubar, O.

2017-08-01

We present the application of fully- and partially-coherent synchrotron radiation wavefront propagation simulation functions, implemented in the "Synchrotron Radiation Workshop" computer code, to create a `virtual beamline' mimicking the Coherent Hard X-ray scattering beamline at NSLS-II. The beamline simulation includes all optical beamline components, such as the insertion device, mirror with metrology data, slits, double crystal monochromator and refractive focusing elements (compound refractive lenses and kinoform lenses). A feature of this beamline is the exploitation of X-ray beam coherence, boosted by the low-emittance NSLS-II storage-ring, for techniques such as X-ray Photon Correlation Spectroscopy or Coherent Diffraction Imaging. The key performance parameters are the degree of Xray beam coherence and photon flux, and the trade-off between them needs to guide the beamline settings for specific experimental requirements. Simulations of key performance parameters are compared to measurements obtained during beamline commissioning, and include the spectral flux of the undulator source, the degree of transverse coherence as well as focal spot sizes.

Regional variation in the refractive-index of the bovine and human cornea.

PubMed

Vasudevan, Balamurali; Simpson, Trefford L; Sivak, Jacob G

2008-10-01

Given the refractive importance of the human cornea, surprisingly little attention has been directed to the study of local variation in corneal refractive-index. This in vitro and in vivo study measures the refractive-index of different portions of the bovine and human cornea. Fifty fresh bovine corneas (obtained from an abattoir) and 10 human subjects were used for the study. The refractive-index of the central, nasal, and temporal corneal epithelium was measured with a bench-top Abbe refractometer in the case of bovine corneas and with a hand-held refractometer with humans. The mean (+/-standard deviation) refractive-indices of the central, nasal, and temporal bovine corneal epithelium were 1.3760 (+/-0.003), 1.3757 (+/-0.002), and 1.3746 (+/-0.002), respectively. Refractive-indices of the anterior and posterior bovine corneal stroma were 1.3731 (+/-0.002) and 1.3708 (+/-0.004), respectively. The mean (+/-standard deviation) refractive-index in the central, nasal, and temporal periphery of the human cornea epithelium were 1.3970 (+/-0.001), 1.3946 (+/-0.001), and 1.3940 (+/-0.001), respectively. There are small local differences in the refractive-index of the bovine and human corneal epithelium and the refractive-index of the epithelium is higher than that of the anterior and posterior stroma of the bovine cornea.

Measurement and design of refractive corrections using ultrafast laser-induced intra-tissue refractive index shaping in live cats

NASA Astrophysics Data System (ADS)

Brooks, Daniel R.; Wozniak, Kaitlin T.; Knox, Wayne; Ellis, Jonathan D.; Huxlin, Krystel R.

2018-02-01

Intra-Tissue Refractive Index Shaping (IRIS) uses a 405 nm femtosecond laser focused into the stromal region of the cornea to induce a local refractive index change through multiphoton absorption. This refractive index change can be tailored through scanning of the focal region and variations in laser power to create refractive structures, such as gradient index lenses for visual refractive correction. Previously, IRIS was used to create 2.5 mm wide, square, -1 D cylindrical refractive structures in living cats. In the present work, we first wrote 400 μm wide bars of refractive index change at varying powers in enucleated cat globes using a custom flexure-based scanning system. The cornea and surrounding sclera were then removed and mounted into a wet cell. The induced optical phase change was measured with a Mach- Zehnder Interferometer (MZI), and appeared as fringe displacement, whose magnitude was proportional to the refractive index change. The interferograms produced by the MZI were analyzed with a Fourier Transform based algorithm in order to extract the phase change. This provided a phase change versus laser power calibration, which was then used to design the scanning and laser power distribution required to create -1.5 D cylindrical Fresnel lenses in cat cornea covering an area 6 mm in diameter. This prescription was inscribed into the corneas of one eye each of two living cats, under surgical anesthesia. It was then verified in vivo by contrasting wavefront aberration measurements collected pre- IRIS with those obtained over six months post-IRIS using a Shack-Hartmann wavefront sensor.

Taheri-Saramad x-ray detector (TSXD): a novel high spatial resolution x-ray imager based on ZnO nano scintillator wires in polycarbonate membrane.

PubMed

Taheri, A; Saramad, S; Ghalenoei, S; Setayeshi, S

2014-01-01

A novel x-ray imager based on ZnO nanowires is designed and fabricated. The proposed architecture is based on scintillation properties of ZnO nanostructures in a polycarbonate track-etched membrane. Because of higher refractive index of ZnO nanowire compared to the membrane, the nanowire acts as an optical fiber that prevents the generated optical photons to spread inside the detector. This effect improves the spatial resolution of the imager. The detection quantum efficiency and spatial resolution of the fabricated imager are 11% and <6.8 μm, respectively.

Refractive index sensing by Brillouin scattering in side-polished optical fibers.

PubMed

Bernini, Romeo; Persichetti, Gianluca; Catalano, Ester; Zeni, Luigi; Minardo, Aldo

2018-05-15

In this Letter, we demonstrate the possibility to measure the refractive index of a liquid, using the stimulating Brillouin scattering in a 3-cm-long side-polished optical fiber. In addition, we show that by depositing a high-refractive index layer on the polished surface the sensitivity of the Brillouin frequency shift (BFS) can be increased due to a higher penetration of the evanescent field in the outer medium. Experiments show a maximum BFS change of about 11 MHz when varying the refractive index of the external medium from 1 (air) to 1.402, and a BFS sensitivity to refractive index of about 293 MHz/RIU around 1.40.

Highly tunable refractive index visible-light metasurface from block copolymer self-assembly.

PubMed

Kim, Ju Young; Kim, Hyowook; Kim, Bong Hoon; Chang, Taeyong; Lim, Joonwon; Jin, Hyeong Min; Mun, Jeong Ho; Choi, Young Joo; Chung, Kyungjae; Shin, Jonghwa; Fan, Shanhui; Kim, Sang Ouk

2016-09-29

The refractive index of natural transparent materials is limited to 2-3 throughout the visible wavelength range. Wider controllability of the refractive index is desired for novel optical applications such as nanoimaging and integrated photonics. We report that metamaterials consisting of period and symmetry-tunable self-assembled nanopatterns can provide a controllable refractive index medium for a broad wavelength range, including the visible region. Our approach exploits the independent control of permeability and permittivity with nanoscale objects smaller than the skin depth. The precise manipulation of the interobject distance in block copolymer nanopatterns via pattern shrinkage increased the effective refractive index up to 5.10. The effective refractive index remains above 3.0 over more than 1,000 nm wavelength bandwidth. Spatially graded and anisotropic refractive indices are also obtained with the design of transitional and rotational symmetry modification.

Highly tunable refractive index visible-light metasurface from block copolymer self-assembly

PubMed Central

Kim, Ju Young; Kim, Hyowook; Kim, Bong Hoon; Chang, Taeyong; Lim, Joonwon; Jin, Hyeong Min; Mun, Jeong Ho; Choi, Young Joo; Chung, Kyungjae; Shin, Jonghwa; Fan, Shanhui; Kim, Sang Ouk

2016-01-01

The refractive index of natural transparent materials is limited to 2–3 throughout the visible wavelength range. Wider controllability of the refractive index is desired for novel optical applications such as nanoimaging and integrated photonics. We report that metamaterials consisting of period and symmetry-tunable self-assembled nanopatterns can provide a controllable refractive index medium for a broad wavelength range, including the visible region. Our approach exploits the independent control of permeability and permittivity with nanoscale objects smaller than the skin depth. The precise manipulation of the interobject distance in block copolymer nanopatterns via pattern shrinkage increased the effective refractive index up to 5.10. The effective refractive index remains above 3.0 over more than 1,000 nm wavelength bandwidth. Spatially graded and anisotropic refractive indices are also obtained with the design of transitional and rotational symmetry modification. PMID:27683077

Interferometric atmospheric refractive-index environmental monitor

NASA Astrophysics Data System (ADS)

Ludman, Jacques E.; Ludman, Jacques J.; Callahan, Heidi; Robinson, John; Davis, Seth; Caulfield, H. John; Watt, David; Sampson, John L.; Hunt, Arlon

1995-06-01

Long, open-path, outdoor interferometric measurement of the index of refraction as a function of wavelength (spectral refractivity) requires a number of innovations. These include active compensation for vibration and turbulence. The use of electronic compensation produces an electronic signal that is ideal for extracting data. This allows the appropriate interpretation of those data and the systematic and fast scanning of the spectrum by the use of bandwidths that are intermediate between lasers (narrow bandwidth) and white light (broad bandwidth). An Environmental Interferometer that incorporates these features should be extremely valuable in both pollutant detection and pollutant identification. Spectral refractivity measurements complement the information available

Tailoring the index of refraction of nanocrystalline hafnium oxide thin films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Vargas, Mirella; Murphy, N. R.; Ramana, C. V., E-mail: rvchintalapalle@utep.edu

2014-03-10

Hafnium oxide (HfO{sub 2}) films were grown by sputter-deposition by varying the growth temperature (T{sub s} = 25–700 °C). HfO{sub 2} films grown at T{sub s} < 200 °C were amorphous, while those grown at T{sub s} ≥ 200 °C were monoclinic, nanocrystalline with (1{sup ¯}11) texturing. X-ray reflectivity (XRR) analyses indicate that the film-density (ρ) increases with increasing T{sub s}. The index of refraction (n) profiles derived from spectroscopic ellipsometry analyses follow the Cauchy dispersion relation. Lorentz-Lorenz analysis (n{sub (λ)} = 550 nm) and optical-model adopted agree well with the XRR data/analyses. A direct T{sub s}-ρ-n relationship suggests that tailoring the optical quality is possible by tuning T{sub s} and themore » microstructure of HfO{sub 2} films.« less

Demonstration of versatile whispering-gallery micro-lasers for remote refractive index sensing.

PubMed

Wan, Lei; Chandrahalim, Hengky; Zhou, Jian; Li, Zhaohui; Chen, Cong; Cho, Sangha; Zhang, Hui; Mei, Ting; Tian, Huiping; Oki, Yuji; Nishimura, Naoya; Fan, Xudong; Guo, L Jay

2018-03-05

We developed chip-scale remote refractive index sensors based on Rhodamine 6G (R6G)-doped polymer micro-ring lasers. The chemical, temperature, and mechanical sturdiness of the fused-silica host guaranteed a flexible deployment of dye-doped polymers for refractive index sensing. The introduction of the dye as gain medium demonstrated the feasibility of remote sensing based on the free-space optics measurement setup. Compared to the R6G-doped TZ-001, the lasing behavior of R6G-doped SU-8 polymer micro-ring laser under an aqueous environment had a narrower spectrum linewidth, producing the minimum detectable refractive index change of 4 × 10 -4 RIU. The maximum bulk refractive index sensitivity (BRIS) of 75 nm/RIU was obtained for SU-8 laser-based refractive index sensors. The economical, rapid, and simple realization of polymeric micro-scale whispering-gallery-mode (WGM) laser-based refractive index sensors will further expand pathways of static and dynamic remote environmental, chemical, biological, and bio-chemical sensing.

Gradient polymer network liquid crystal with a large refractive index change.

PubMed

Ren, Hongwen; Xu, Su; Wu, Shin-Tson

2012-11-19

A simple approach for preparing gradient polymer network liquid crystal (PNLC) with a large refractive index change is demonstrated. To control the effective refractive index at a given cell position, we applied a voltage to a homogeneous cell containing LC/diacrylate monomer mixture to generate the desired tilt angle and then stabilize the LC orientation with UV-induced polymer network. By varying the applied voltage along with the cells' movement, a PNLC with a gradient refractive index distribution is obtained. In comparison with conventional approaches using patterned photomask or electrode, our method offers following advantages: large refractive index change, freedom to design specific index profile, and large panel capability. Potential applications include tunable-focus lenses, prism gratings, phase modulators, and other adaptive photonic devices.

Slow-light enhanced subwavelength plasmonic waveguide refractive index sensors.

PubMed

Huang, Yin; Min, Changjun; Dastmalchi, Pouya; Veronis, Georgios

2015-06-01

We introduce slow-light enhanced subwavelength scale refractive index sensors which consist of a plasmonic metal-dielectric-metal (MDM) waveguide based slow-light system sandwiched between two conventional MDM waveguides. We first consider a MDM waveguide with small width structrue for comparison, and then consider two MDM waveguide based slow light systems: a MDM waveguide side-coupled to arrays of stub resonators system and a MDM waveguide side-coupled to arrays of double-stub resonators system. We find that, as the group velocity decreases, the sensitivity of the effective index of the waveguide mode to variations of the refractive index of the fluid filling the sensors as well as the sensitivities of the reflection and transmission coefficients of the waveguide mode increase. The sensing characteristics of the slow-light waveguide based sensor structures are systematically analyzed. We show that the slow-light enhanced sensors lead to not only 3.9 and 3.5 times enhancements in the refractive index sensitivity, and therefore in the minimum detectable refractive index change, but also to 2 and 3 times reductions in the required sensing length, respectively, compared to a sensor using a MDM waveguide with small width structure.

Refractive index dependence of Papilio Ulysses butterfly wings reflectance spectra

NASA Astrophysics Data System (ADS)

Isnaeni, Muslimin, Ahmad Novi; Birowosuto, Muhammad Danang

2016-02-01

We have observed and utilized butterfly wings of Papilio Ulysses for refractive index sensor. We noticed this butterfly wings have photonic crystal structure, which causes blue color appearance on the wings. The photonic crystal structure, which consists of cuticle and air void, is approximated as one dimensional photonic crystal structure. This photonic crystal structure opens potential to several optical devices application, such as refractive index sensor. We have utilized small piece of Papilio Ulysses butterfly wings to characterize refractive index of several liquid base on reflectance spectrum of butterfly wings in the presence of sample liquid. For comparison, we simulated reflectance spectrum of one dimensional photonic crystal structure having material parameter based on real structure of butterfly wings. We found that reflectance spectrum peaks shifted as refractive index of sample changes. Although there is a slight difference in reflectance spectrum peaks between measured spectrum and calculated spectrum, the trend of reflectance spectrum peaks as function of sample's refractive index is the similar. We assume that during the measurement, the air void that filled by sample liquid is expanded due to liquid pressure. This change of void shape causes non-similarity between measured spectrum and calculated spectrum.

Measurement of the Microwave Refractive Index of Materials Based on Parallel Plate Waveguides

NASA Astrophysics Data System (ADS)

Zhao, F.; Pei, J.; Kan, J. S.; Zhao, Q.

2017-12-01

An electrical field scanning apparatus based on a parallel plate waveguide method is constructed, which collects the amplitude and phase matrices as a function of the relative position. On the basis of such data, a method for calculating the refractive index of the measured wedge samples is proposed in this paper. The measurement and calculation results of different PTFE samples reveal that the refractive index measured by the apparatus is substantially consistent with the refractive index inferred with the permittivity of the sample. The proposed refractive index calculation method proposed in this paper is a competitive method for the characterization of the refractive index of materials with positive refractive index. Since the apparatus and method can be used to measure and calculate arbitrary direction of the microwave propagation, it is believed that both of them can be applied to the negative refractive index materials, such as metamaterials or “left-handed” materials.

Long period grating refractive-index sensor: optimal design for single wavelength interrogation.

PubMed

Kapoor, Amita; Sharma, Enakshi K

2009-11-01

We report the design criteria for the use of long period gratings (LPGs) as refractive-index sensors with output power at a single interrogating wavelength as the measurement parameter. The design gives maximum sensitivity in a given refractive-index range when the interrogating wavelength is fixed. Use of the design criteria is illustrated by the design of refractive-index sensors for specific application to refractive-index variation of a sugar solution with a concentration and detection of mole fraction of xylene in heptane (paraffin).

Predicting fiber refractive index from a measured preform index profile

NASA Astrophysics Data System (ADS)

Kiiveri, P.; Koponen, J.; Harra, J.; Novotny, S.; Husu, H.; Ihalainen, H.; Kokki, T.; Aallos, V.; Kimmelma, O.; Paul, J.

2018-02-01

When producing fiber lasers and amplifiers, silica glass compositions consisting of three to six different materials are needed. Due to the varying needs of different applications, substantial number of different glass compositions are used in the active fiber structures. Often it is not possible to find material parameters for theoretical models to estimate thermal and mechanical properties of those glass compositions. This makes it challenging to predict accurately fiber core refractive index values, even if the preform index profile is measured. Usually the desired fiber refractive index value is achieved experimentally, which is expensive. To overcome this problem, we analyzed statistically the changes between the measured preform and fiber index values. We searched for correlations that would help to predict the Δn-value change from preform to fiber in a situation where we don't know the values of the glass material parameters that define the change. Our index change models were built using the data collected from preforms and fibers made by the Direct Nanoparticle Deposition (DND) technology.

Refractive index variance of cells and tissues measured by quantitative phase imaging.

PubMed

Shan, Mingguang; Kandel, Mikhail E; Popescu, Gabriel

2017-01-23

The refractive index distribution of cells and tissues governs their interaction with light and can report on morphological modifications associated with disease. Through intensity-based measurements, refractive index information can be extracted only via scattering models that approximate light propagation. As a result, current knowledge of refractive index distributions across various tissues and cell types remains limited. Here we use quantitative phase imaging and the statistical dispersion relation (SDR) to extract information about the refractive index variance in a variety of specimens. Due to the phase-resolved measurement in three-dimensions, our approach yields refractive index results without prior knowledge about the tissue thickness. With the recent progress in quantitative phase imaging systems, we anticipate that using SDR will become routine in assessing tissue optical properties.

Reflection based Extraordinary Optical Transmission Fiber Optic Probe for Refractive Index Sensing.

PubMed

Lan, Xinwei; Cheng, Baokai; Yang, Qingbo; Huang, Jie; Wang, Hanzheng; Ma, Yinfa; Shi, Honglan; Xiao, Hai

2014-03-31

Fiber optic probes for chemical sensing based on the extraordinary optical transmission (EOT) phenomenon are designed and fabricated by perforating subwavelength hole arrays on the gold film coated optical fiber endface. The device exhibits a red shift in response to the surrounding refractive index increases with high sensitivity, enabling a reflection-based refractive index sensor with a compact and simple configuration. By choosing the period of hole arrays, the sensor can be designed to operate in the near infrared telecommunication wavelength range, where the abundant source and detectors are available for easy instrumentation. The new sensor probe is demonstrated for refractive index measurement using refractive index matching fluids. The sensitivity reaches 573 nm/RIU in the 1.333~1.430 refractive index range.

Photogeneration of refractive-index patterns in doped polyimide films.

PubMed

Chakravorty, K K

1993-05-01

A photosensitive benzophenone tetracarboxylic dianhyride-alkylated diamine polyimide formulation has been evaluated for application in an optical interconnection area. The refractive-index patterns in this material were optically recorded by UV-assisted photodoping of sensitizers. The polyimide films were selectively doped with benzoin-type photosensitizers such as benzildimethylketal and benzoin ethyl ether, which cause a decrease in the refractive index. High-dose UV irradiation that causes cross linking of the polyimide chains was also employed for augmenting the refractive-index difference to 0.017 between the doped and undoped regions. Refractive-index variations and lightguiding properties were investigated as a function of doping concentrations and other processing conditions. The author utilized this technique for the fabrication of embedded polyimide channel waveguides. The two photosensitizers have different effects on the waveguiding characteristics of the polyimide films. Losses for benzoin ethyl ether remained low whereas doping with benzildimethylketal caused significant increase in the waveguiding loss at high doping concentrations. Near-field imaging of the output from such waveguides shows good confinement of 815-nm light.

Photogeneration of refractive-index patterns in doped polyimide films

NASA Astrophysics Data System (ADS)

Chakravorty, K. K.

1993-05-01

A photosensitive benzophenone tetracarboxylic dianhyride-alkylated diamine polyimide formulation has been evaluated for application in an optical interconnection area. The refractive-index patterns in this material were optically recorded by UV-assisted photodoping of sensitizers. The polyimide films were selectively doped with benzoin-type photosensitizers such as benzildimethylketal and benzoin ethyl ether, which cause a decrease in the refractive index. High-dose UV irradiation that causes cross linking of the polyimide chains was also employed for augmenting the refractive-index difference to 0.017 between the doped and undoped regions. Refractive-index variations and lightguiding properties were investigated as a function of doping concentrations and other processing conditions. The author utilized this technique for the fabrication of embedded polyimide channel waveguides. The two photosensitizers have different effects on the waveguiding characteristics of the polyimide films. Losses for benzoin ethyl ether remained low whereas doping with benzildimethylketal caused significant increase in the waveguiding loss at high doping concentrations. Near-field imaging of the output from such waveguides shows good confinement of 815-nm light.

Measurement of refractive index of photopolymer for holographic gratings

NASA Astrophysics Data System (ADS)

Watanabe, Eriko; Mizuno, Jun; Fujikawa, Chiemi; Kodate, Kashiko

2007-02-01

We have made attempts to measure directly the small-scale variation of optical path lengths in photopolymer samples. For those with uniform thickness, the measured quantity is supposed to be proportional to the refractive index of the photopolymer. The system is based on a Mach-Zehnder interferometer using phase-locking technique and measures the change in optical path length during the sample is scanned across the optical axis. The spatial resolution is estimated to be 2μm, which is limited by the sample thickness. The path length resolution is estimated to be 6nm, which corresponds to the change in refractive index less than 10 -3 for the sample of 10μm thick. The measurement results showed clearly that the refractive index of photopolymer is not simply proportional to the exposure energy, contrary to the conventional photosensitive materials such as silver halide emulsion and dichromated gelatine. They also revealed the refractive index fluctuation in uniformly exposed photopolymer sample, which explains the milky appearance that sometimes observed in thick samples.

Surface plasmon resonance optical cavity enhanced refractive index sensing.

PubMed

Giorgini, A; Avino, S; Malara, P; Gagliardi, G; Casalino, M; Coppola, G; Iodice, M; Adam, P; Chadt, K; Homola, J; De Natale, P

2013-06-01

We report on a method for surface plasmon resonance (SPR) refractive index sensing based on direct time-domain measurements. An optical resonator is built around an SPR sensor, and its photon lifetime is measured as a function of loss induced by refractive index variations. The method does not rely on any spectroscopic analysis or direct intensity measurement. Time-domain measurements are practically immune to light intensity fluctuations and thus lead to high resolution. A proof of concept experiment is carried out in which a sensor response to liquid samples of different refractive indices is measured. A refractive index resolution of the current system, extrapolated from the reproducibility of cavity-decay time determinations over 133 s, is found to be about 10(-5) RIU. The possibility of long-term averaging suggests that measurements with a resolution better than 10(-7) RIU/√Hz are within reach.

3-D photo-patterning of refractive index structures in photosensitive thin film materials

DOEpatents

Potter, Jr., Barrett George; Potter, Kelly Simmons

2002-01-01

A method of making a three-dimensional refractive index structure in a photosensitive material using photo-patterning. The wavelengths at which a photosensitive material exhibits a change in refractive index upon exposure to optical radiation is first determined and then a portion of the surface of the photosensitive material is optically irradiated at a wavelength at which the photosensitive material exhibits a change in refractive index using a designed illumination system to produce a three-dimensional refractive index structure. The illumination system can be a micro-lenslet array, a macroscopic refractive lens array, or a binary optic phase mask. The method is a single-step, direct-write procedure to produce a designed refractive index structure.

Reflection statistics of weakly disordered optical medium when its mean refractive index is different from an outside medium

NASA Astrophysics Data System (ADS)

Pradhan, Prabhakar; John Park, Daniel; Capoglu, Ilker; Subramanian, Hariharan; Damania, Dhwanil; Cherkezyan, Lusik; Taflove, Allen; Backman, Vadim

2017-06-01

Statistical properties of light waves reflected from a one-dimensional (1D) disordered optical medium [n(x) = n0+ dn(x), x)>=0] have been well studied, however, most of the studies have focused on the situation when the mean refractive index of the optical medium matched with the outside medium, i.e., n0= nout=1. Further, considering dn(x) as a Gaussian color noise refractive index medium with exponential spatial correlation decay length lc and k as the incident wave vector, it has been shown that for smaller correlation length limit, i.e., klc <<1, both the mean reflection coefficient and std of r, σ(r), have same value, and they follow the relation = σ(r) ∝ lc. However, when the refractive index of the sample medium is different from the outside medium, the reflection statistics may have interesting features, which has not been well studied or understood. We studied the reflection statistics of a 1D weakly disordered optical medium with the mean background refractive index n0 being different from the outside medium nout (≠n0), to see the effect of mismatching (i.e., value of n0- nout) on the reflection statistics. In the mismatched case, the results show that the mean reflection coefficient follows a form similar to that of the matched refractive-index case, i.e., ∝ lc, with a linear increased shift, which is due to 1D uniform background reflection from a slab. However, σ(r) is shown to be σ(r) ∝ (lc)1/2, which is different from the matched case. This change in std of r is attributed to the interference between the mismatched-crerated edge mediated multiple scattering that are coupled with the random scattering. Applications to light scattering from random layered media and biological cells are discussed.

Propagation-based x-ray phase contrast imaging using an iterative phase diversity technique

NASA Astrophysics Data System (ADS)

Carroll, Aidan J.; van Riessen, Grant A.; Balaur, Eugeniu; Dolbnya, Igor P.; Tran, Giang N.; Peele, Andrew G.

2018-03-01

Through the use of a phase diversity technique, we demonstrate a near-field in-line x-ray phase contrast algorithm that provides improved object reconstruction when compared to our previous iterative methods for a homogeneous sample. Like our previous methods, the new technique uses the sample refractive index distribution during the reconstruction process. The technique complements existing monochromatic and polychromatic methods and is useful in situations where experimental phase contrast data is affected by noise.

Refractive index and birefringence of 2H silicon carbide.

NASA Technical Reports Server (NTRS)

Powell, J. A.

1972-01-01

Measurement of the refractive indices of 2H SiC over the wavelength range from 435.8 to 650.9 nm by the method of minimum deviation. A curve fit of the experimental data to the Cauchy dispersion equation yielded, for the ordinary index, n sub zero = 2.5513 + 25,850/lambda squared + 8.928 x 10 to the 8th power/lambda to the 4th power and, for the extraordinary index, n sub e = 2.6161 + 28,230/lambda squared + 11.490 x 10 to the 8th power/lambda to the 4th power when lambda is expressed in nm. The estimated error (standard deviation) in these values is plus or minus 0.0006 for n sub zero and plus or minus 0.0009 for n sub e. The birefringence calculated from these expressions is about 20% less than previously published values.

Engineering a Large Scale Indium Nanodot Array for Refractive Index Sensing.

PubMed

Xu, Xiaoqing; Hu, Xiaolin; Chen, Xiaoshu; Kang, Yangsen; Zhang, Zhiping; B Parizi, Kokab; Wong, H-S Philip

2016-11-23

In this work, we developed a simple method to fabricate 12 × 4 mm 2 large scale nanostructure arrays and investigated the feasibility of indium nanodot (ND) array with different diameters and periods for refractive index sensing. Absorption resonances at multiple wavelengths from the visible to the near-infrared range were observed for various incident angles in a variety of media. Engineering the ND array with a centered square lattice, we successfully enhanced the sensitivity by 60% and improved the figure of merit (FOM) by 190%. The evolution of the resonance dips in the reflection spectra, of square lattice and centered square lattice, from air to water, matches well with the results of Lumerical FDTD simulation. The improvement of sensitivity is due to the enhancement of local electromagnetic field (E-field) near the NDs with centered square lattice, as revealed by E-field simulation at resonance wavelengths. The E-field is enhanced due to coupling between the two square ND arrays with [Formula: see text]x period at phase matching. This work illustrates an effective way to engineer and fabricate a refractive index sensor at a large scale. This is the first experimental demonstration of poor-metal (indium) nanostructure array for refractive index sensing. It also demonstrates a centered square lattice for higher sensitivity and as a better basic platform for more complex sensor designs.

A new method of measuring lens refractive index.

PubMed

Buckley, John

2008-07-01

A new clinical method for determining the refractive index of a lens is described. By measuring lens power in air and then immersing the lens in a liquid of known refractive index (n), it is possible to calculate the refractive index of the lens material (micro) by using the formula: micro = (nK (v,1) - K(v,n))/(K (v,1) - K (v,n)) where K (v,1) is the lens power determined in air K (v,n) is the lens power determined in the immersion liquid. The only materials required are a digital lensmeter and a wet cell for holding the lens in a liquid. The theoretical basis of the method is explained and a description given of the limitations. The optimal method of measuring different types of lenses is discussed. Sources of error include the thin lens theory behind the method, the use of a wetcell and the digital lensmeter. The theoretical accuracy of the results is given as 0.02 but 0.01 is usually achieved. In all cases, measuring the front vertex powers (FVP) yields a more accurate estimate of refractive index of a lens than measuring back vertex power (BVP). The author found half the lenses measured attained values within 0.005 of the known material index. This method is usually sufficiently accurate to isolate which lens material has been used in manufacturing and permit manufacturing spectacles that mimic the appearance of an earlier pair. Some suggestions for further refinement are given.

Optimization of torque on an optically driven micromotor by manipulation of the index of refraction

NASA Astrophysics Data System (ADS)

Wing, Frank M., III; Mahajan, Satish; Collett, Walter

2004-12-01

Since the 1970"s, the focused laser beam has become a familiar tool to manipulate neutral, dielectric micro-objects. A number of authors, including Higurashi and Gauthier, have described the effects of radiation pressure from laser light on microrotors. Collett, et al. developed a wave, rather than a ray optic, approach in the calculation of such forces on a microrotor for the first time. This paper describes a modification to the design of a laser driven, radiation pressure microrotor, intended to improve the optically generated torque. Employing the wave approach, the electric and magnetic fields in the vicinity of the rotor are calculated using the finite difference time domain (FDTD) method, which takes into account the wave nature of the incident light. Forces are calculated from the application of Maxwell"s stress tensor over the surfaces of the rotor. Results indicate a significant increase in torque when the index of refraction of the microrotor is changed from a single value to an inhomogeneous profile. The optical fiber industry has successfully employed a variation in the index of refraction across the cross section of a fiber for the purpose of increasing the efficiency of light transmission. Therefore, it is hoped that various fabrication methods can be utilized for causing desired changes in the index of refraction of an optically driven microrotor. Various profiles of the index of refraction inside a microrotor are considered for optimization of torque. Simulation methodology and results of torque on a microrotor for various profiles of the index of refraction are presented. Guidelines for improvised fabrication of efficient microrotors may then be obtained from these profiles.

A bi-prism interferometer for hard x-ray photons

DOE Office of Scientific and Technical Information (OSTI.GOV)

Isakovic, A.F.; Siddons, D.; Stein, A.

2010-04-06

Micro-fabricated bi-prisms have been used to create an interference pattern from an incident hard X-ray beam, and the intensity of the pattern probed with fluorescence from a 30 nm-thick metal film. Maximum fringe visibility exceeded 0.9 owing to the nano-sized probe and the choice of single-crystal prism material. A full near-field analysis is necessary to describe the fringe field intensities, and the transverse coherence lengths were extracted at APS beamline 8-ID-I. It is also shown that the maximum number of fringes is dependent only on the complex refractive index of the prism material.

Nano-imprint gold grating as refractive index sensor

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kumari, Sudha; Mohapatra, Saswat; Moirangthem, Rakesh S.

Large scale of fabrication of plasmonic nanostructures has been a challenging task due to time consuming process and requirement of expensive nanofabrication tools such as electron beam lithography system, focused ion beam system, and extreme UV photolithography system. Here, we present a cost-effective fabrication technique so called soft nanoimprinting to fabricate nanostructures on the larger sample area. In our fabrication process, a commercially available optical DVD disc was used as a template which was imprinted on a polymer glass substrate to prepare 1D polymer nano-grating. A homemade nanoimprinting setup was used in this fabrication process. Further, a label-free refractive indexmore » sensor was developed by utilizing the properties of surface plasmon resonance (SPR) of a gold coated 1D polymer nano-grating. Refractive index sensing was tested by exposing different solutions of glycerol-water mixture on the surface of gold nano-grating. The calculated bulk refractive index sensitivity was found to be 751nm/RIU. We believed that our proposed SPR sensor could be a promising candidate for developing low-cost refractive index sensor with high sensitivity on a large scale.« less

Experimental determination of refractive index of condensed reflectin in squid iridocytes.

PubMed

Ghoshal, Amitabh; DeMartini, Daniel G; Eck, Elizabeth; Morse, Daniel E

2014-06-06

Loliginid squid dynamically tune the structural iridescence of cells in their skin for active camouflage and communication. Bragg reflectors in these cells consist of membrane-bound lamellae periodically alternating with low refractive index extracellular spaces; neuronal signalling induces condensation of the reflectin proteins that fill the lamellae, consequently triggering the expulsion of water. This causes an increase in refractive index within the lamellae, activating reflectance, with the change in lamellar thickness and spacing progressively shifting the wavelength of reflected light. We used micro-spectrophotometry to measure the functionally relevant refractive index of the high-index lamellae of the Bragg reflectors containing the condensed reflectins in chemically fixed dermal iridocytes of the squid, Doryteuthis opalescens. Our high-magnification imaging spectrometer allowed us to obtain normalized spectra of optically distinct sections of the individual, subcellular, multi-layer Bragg stacks. Replacement of the extracellular fluid with liquids of increasing refractive index allowed us to measure the reflectivity of the Bragg stacks as it decreased progressively to 0 when the refractive index of the extracellular medium exactly matched that of the reflectin-filled lamellae, thus allowing us to directly measure the refractive index of the reflectin-filled lamellae as ncondensed lamellae ≈ 1.44. The measured value of the physiologically relevant ncondensed lamellae from these bright iridocytes falls within the range of values that we recently determined by an independent optical method and is significantly lower than values previously reported for dehydrated and air-dried reflectin films. We propose that this directly measured value for the refractive index of the squid's Bragg lamellae containing the condensed reflectins is most appropriate for calculations of reflectivity in similar reflectin-based high-index layers in other molluscs.

Experimental determination of refractive index of condensed reflectin in squid iridocytes

PubMed Central

Ghoshal, Amitabh; DeMartini, Daniel G.; Eck, Elizabeth; Morse, Daniel E.

2014-01-01

Loliginid squid dynamically tune the structural iridescence of cells in their skin for active camouflage and communication. Bragg reflectors in these cells consist of membrane-bound lamellae periodically alternating with low refractive index extracellular spaces; neuronal signalling induces condensation of the reflectin proteins that fill the lamellae, consequently triggering the expulsion of water. This causes an increase in refractive index within the lamellae, activating reflectance, with the change in lamellar thickness and spacing progressively shifting the wavelength of reflected light. We used micro-spectrophotometry to measure the functionally relevant refractive index of the high-index lamellae of the Bragg reflectors containing the condensed reflectins in chemically fixed dermal iridocytes of the squid, Doryteuthis opalescens. Our high-magnification imaging spectrometer allowed us to obtain normalized spectra of optically distinct sections of the individual, subcellular, multi-layer Bragg stacks. Replacement of the extracellular fluid with liquids of increasing refractive index allowed us to measure the reflectivity of the Bragg stacks as it decreased progressively to 0 when the refractive index of the extracellular medium exactly matched that of the reflectin-filled lamellae, thus allowing us to directly measure the refractive index of the reflectin-filled lamellae as ncondensed lamellae ≈ 1.44. The measured value of the physiologically relevant ncondensed lamellae from these bright iridocytes falls within the range of values that we recently determined by an independent optical method and is significantly lower than values previously reported for dehydrated and air-dried reflectin films. We propose that this directly measured value for the refractive index of the squid's Bragg lamellae containing the condensed reflectins is most appropriate for calculations of reflectivity in similar reflectin-based high-index layers in other molluscs. PMID:24694894

Method of producing optical quality glass having a selected refractive index

DOEpatents

Poco, John F.; Hrubesh, Lawrence W.

2000-01-01

Optical quality glass having a selected refractive index is produced by a two stage drying process. A gel is produced using sol-gel chemistry techniques and first dried by controlled evaporation until the gel volume reaches a pre-selected value. This pre-selected volume determines the density and refractive index of the finally dried gel. The gel is refilled with solvent in a saturated vapor environment, and then dried again by supercritical extraction of the solvent to form a glass. The glass has a refractive index less than the full density of glass, and the range of achievable refractive indices depends on the composition of the glass. Glasses having different refractive indices chosen from an uninterrupted range of values can be produced from a single precursor solution.

In Vitro Validation of an Artefact Suppression Algorithm in X-Ray Phase-Contrast Computed Tomography.

PubMed

Sunaguchi, Naoki; Yuasa, Tetsuya; Hirano, Shin-Ichi; Gupta, Rajiv; Ando, Masami

2015-01-01

X-ray phase-contrast tomography can significantly increase the contrast-resolution of conventional attenuation-contrast imaging, especially for soft-tissue structures that have very similar attenuation. Just as in attenuation-based tomography, phase contrast tomography requires a linear dependence of aggregate beam direction on the incremental direction alteration caused by individual voxels along the path of the X-ray beam. Dense objects such as calcifications in biological specimens violate this condition. There are extensive beam deflection artefacts in the vicinity of such structures because they result in large distortion of wave front due to the large difference of refractive index; for such large changes in beam direction, the transmittance of the silicon analyzer crystal saturates and is no longer linearly dependent on the angle of refraction. This paper describes a method by which these effects can be overcome and excellent soft-tissue contrast of phase tomography can be preserved in the vicinity of such artefact-producing structures.

Evanescent field-based optical fiber sensing device for measuring the refractive index of liquids in microfluidic channels.

PubMed

Polynkin, PaveL; Polynkin, Alexander; Peyghambarian, N; Mansuripur, Masud

2005-06-01

We report a simple optical sensing device capable of measuring the refractive index of liquids propagating in microfluidic channels. The sensor is based on a single-mode optical fiber that is tapered to submicrometer dimensions and immersed in a transparent curable soft polymer. A channel for liquid analyte is created in the immediate vicinity of the taper waist. Light propagating through the tapered section of the fiber extends into the channel, making the optical loss in the system sensitive to the refractive-index difference between the polymer and the liquid. The fabrication process and testing of the prototype sensing devices are described. The sensor can operate both as a highly responsive on-off device and in the continuous measurement mode, with an estimated accuracy of refractive-index measurement of approximately 5 x 10(-4).

Analyzing refractive index changes and differential bending in microcantilever arrays.

PubMed

Huber, François; Lang, Hans Peter; Hegner, Martin; Despont, Michel; Drechsler, Ute; Gerber, Christoph

2008-08-01

A new microcantilever array design is investigated comprising eight flexible microcantilevers introducing two solid bars, enabling to subtract contributions from differences in refractive index in an optical laser read out system. Changes in the refractive index do not contribute undesirably to bending signals at picomolar to micromolar DNA or protein concentrations. However, measurements of samples with high salt concentrations or serum are affected, requiring corrections for refractive index artifacts. Moreover, to obtain a deeper understanding of molecular stress formation, the differential curvature of cantilevers is analyzed by positioning the laser spots along the surface of the levers during pH experiments.

Methods for prediction of refractive index in glasses for the infrared

NASA Astrophysics Data System (ADS)

McCloy, John S.

2011-06-01

It is often useful to obtain custom glasses that meet particular requirements of refractive index and dispersion for highend optical design and applications. In the case of infrared glasses, limited experimental data are available due to difficulties in processing of these glasses and also measuring refractive indices accurately. This paper proposes methods to estimate refractive index and dispersion as a function of composition for selected infrared-transmitting glasses. Methods for refractive index determination are reviewed and evaluated, including Gladstone-Dale, Wemple- DiDomenico single oscillator, Optical basicity, and Lorentz-Lorenz total polarizability. Various estimates for a set of PbO-Bi2O3-Ga2O3 (heavy metal oxide) and As-S (chalcogenide) glasses will be compared with measured values of index and dispersion.

Change in refractive index of muscle tissue during laser-induced interstitial thermotherapy.

PubMed

Chen, Na; Chen, Meimei; Liu, Shupeng; Guo, Qiang; Chen, Zhenyi; Wang, Tingyun

2014-01-01

This paper presents a long-period fiber-grating (LPG) based Michelson interferometric refractometry to monitor the change in refractive index of porcine muscle during laser-induced interstitial thermotherapy (LITT). As the wavelength of RI interferometer alters with the change in refractive index around the probe, the LPG based refractometry is combined with LITT system to measure the change in refractive index of porcine muscle when irradiated by laser. The experimental results show the denaturation of tissue alters the refractive index significantly and the LPG sensor can be applied to monitor the tissue state during the LITT.

Low-Coherence Reflectometry for Refractive Index Measurements of Cells in Micro-Capillaries.

PubMed

Carpignano, Francesca; Rigamonti, Giulia; Mazzini, Giuliano; Merlo, Sabina

2016-10-11

The refractive index of cells provides insights into their composition, organization and function. Moreover, a good knowledge of the cell refractive index would allow an improvement of optical cytometric and diagnostic systems. Although interferometric techniques undoubtedly represent a good solution for quantifying optical path variation, obtaining the refractive index of a population of cells non-invasively remains challenging because of the variability in the geometrical thickness of the sample. In this paper, we demonstrate the use of infrared low-coherence reflectometry for non-invasively quantifying the average refractive index of cell populations gently confined in rectangular glass micro-capillaries. A suspension of human red blood cells in plasma is tested as a reference. As a use example, we apply this technique to estimate the average refractive index of cell populations belonging to epithelial and hematological families.

Low-Coherence Reflectometry for Refractive Index Measurements of Cells in Micro-Capillaries

PubMed Central

Carpignano, Francesca; Rigamonti, Giulia; Mazzini, Giuliano; Merlo, Sabina

2016-01-01

The refractive index of cells provides insights into their composition, organization and function. Moreover, a good knowledge of the cell refractive index would allow an improvement of optical cytometric and diagnostic systems. Although interferometric techniques undoubtedly represent a good solution for quantifying optical path variation, obtaining the refractive index of a population of cells non-invasively remains challenging because of the variability in the geometrical thickness of the sample. In this paper, we demonstrate the use of infrared low-coherence reflectometry for non-invasively quantifying the average refractive index of cell populations gently confined in rectangular glass micro-capillaries. A suspension of human red blood cells in plasma is tested as a reference. As a use example, we apply this technique to estimate the average refractive index of cell populations belonging to epithelial and hematological families. PMID:27727172

Determination of refractive index, size, and concentration of nonabsorbing colloidal nanoparticles from measurements of the complex effective refractive index.

PubMed

Márquez-Islas, Roberto; Sánchez-Pérez, Celia; García-Valenzuela, Augusto

2014-02-01

We describe a method for obtaining the refractive index (RI), size, and concentration of nonabsorbing nanoparticles in suspension from relatively simple optical measurements. The method requires measuring the complex effective RI of two dilute suspensions of the particles in liquids of different refractive indices. We describe the theoretical basis of the proposed method and provide experimental results validating the procedure.

Correct consideration of the index of refraction using blackbody radiation.

PubMed

Hartmann, Jurgen

2006-09-04

The correct consideration of the index of refraction when using blackbody radiators as standard sources for optical radiation is derived and discussed. It is shown that simply using the index of refraction of air at laboratory conditions is not sufficient. A combination of the index of refraction of the media used inside the blackbody radiator and for the optical path between blackbody and detector has to be used instead. A worst case approximation for the introduced error when neglecting these effects is presented, showing that the error is below 0.1 % for wavelengths above 200 nm. Nevertheless, for the determination of the spectral radiance for the purpose of radiation temperature measurements the correct consideration of the refractive index is mandatory. The worst case estimation reveals that the introduced error in temperature at a blackbody temperature of 3000 degrees C can be as high as 400 mk at a wavelength of 650 nm and even higher at longer wavelengths.

Contribution of the gradient refractive index and shape to the crystalline lens spherical aberration and astigmatism.

PubMed

Birkenfeld, Judith; de Castro, Alberto; Ortiz, Sergio; Pascual, Daniel; Marcos, Susana

2013-06-28

The optical properties of the crystalline lens are determined by its shape and refractive index distribution. However, to date, those properties have not been measured together in the same lens, and therefore their relative contributions to optical aberrations are not fully understood. The shape, the optical path difference, and the focal length of ten porcine lenses (age around 6 months) were measured in vitro using Optical Coherence Tomography and laser ray tracing. The 3D Gradient Refractive Index distribution (GRIN) was reconstructed by means of an optimization method based on genetic algorithms. The optimization method searched for the parameters of a 4-variable GRIN model that best fits the distorted posterior surface of the lens in 18 different meridians. Spherical aberration and astigmatism of the lenses were estimated using computational ray tracing, with the reconstructed GRIN lens and an equivalent homogeneous refractive index. For all lenses the posterior radius of curvature was systematically steeper than the anterior one, and the conic constant of both the anterior and posterior positive surfaces was positive. In average, the measured focal length increased with increasing pupil diameter, consistent with a crystalline lens negative spherical aberration. The refractive index of nucleus and surface was reconstructed to an average value of 1.427 and 1.364, respectively, for 633 nm. The results of the GRIN reconstruction showed a wide distribution of the index in all lens samples. The GRIN shifted spherical aberration towards negative values when compared to a homogeneous index. A negative spherical aberration with GRIN was found in 8 of the 10 lenses. The presence of GRIN also produced a decrease in the total amount of lens astigmatism in most lenses, while the axis of astigmatism was only little influenced by the presence of GRIN. To our knowledge, this study is the first systematic experimental study of the relative contribution of geometry and GRIN to

Microvolume index of refraction determinations by interferometric backscatter

NASA Astrophysics Data System (ADS)

Bornhop, Darryl J.

1995-06-01

A new method has been applied to the determination of fluid bulk properties in small detection volumes. Through the use of an unfocused He-Ne laser beam and a cylindrical tube of capillary dimensions, relative refractive-index measurements are possible. The backscattered light from the illumination of a tube of capillary dimensions produces an interference pattern that is spatially defined and that contains information related to the bulk properties of the fluid contained in the tube. Positional changes in the intensity-modulated beam profile (interference fringes) are directly related to the refractive index of the fluid in the tube. The determination of dn/n at the 10-7 level is possible in probe volumes of 350 pL. The technique has been applied to tubes as small as 75 mu m inner diameter and as large as 1.0 mm inner diameter. No modification of the simple optical bench is required for facilitating the determination of refractive index for the complete range of tube diameters.

Empirical modelling to predict the refractive index of human blood.

PubMed

Yahya, M; Saghir, M Z

2016-02-21

Optical techniques used for the measurement of the optical properties of blood are of great interest in clinical diagnostics. Blood analysis is a routine procedure used in medical diagnostics to confirm a patient's condition. Measuring the optical properties of blood is difficult due to the non-homogenous nature of the blood itself. In addition, there is a lot of variation in the refractive indices reported in the literature. These are the reasons that motivated the researchers to develop a mathematical model that can be used to predict the refractive index of human blood as a function of concentration, temperature and wavelength. The experimental measurements were conducted on mimicking phantom hemoglobin samples using the Abbemat Refractometer. The results analysis revealed a linear relationship between the refractive index and concentration as well as temperature, and a non-linear relationship between refractive index and wavelength. These results are in agreement with those found in the literature. In addition, a new formula was developed based on empirical modelling which suggests that temperature and wavelength coefficients be added to the Barer formula. The verification of this correlation confirmed its ability to determine refractive index and/or blood hematocrit values with appropriate clinical accuracy.

Compact eccentric long period grating with improved sensitivity in low refractive index region.

PubMed

Shen, Fangcheng; Zhou, Kaiming; Gordon, Neil; Zhang, Lin; Shu, Xuewen

2017-07-10

We demonstrate a compact eccentric long period grating with enhanced sensitivity in low refractive index region. With a period designed at 15 µm for coupling light to high order cladding modes, the grating is more sensitive to surrounding refractive index in low refractive index region. The intrinsically low coupling coefficients for those high order cladding modes are significantly improved with the eccentric localized inscription induced by the femtosecond laser. The fabricated grating is compact with a length of 4.05 mm, and exhibits an average sensitivity of ~505 nm/RIU in low refractive index region (1.3328-1.3544). The proposed principle can also work in other refractive index region with a proper choice of the resonant cladding modes.

Low-loss negative index metamaterials for X, Ku, and K microwave bands

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lee, David A.; Vedral, L. James; Smith, David A.

2015-04-15

Low-loss, negative-index of refraction metamaterials were designed and tested for X, Ku, and K microwave frequency bands. An S-shaped, split-ring resonator was used as a unit cell to design homogeneous slabs of negative-index metamaterials. Then, the slabs of metamaterials were cut unto prisms to measure experimentally the negative index of refraction of a plane electromagnetic wave. Theoretical simulations using High-Frequency Structural Simulator, a finite element equation solver, were in good agreement with experimental measurements. The negative index of refraction was retrieved from the angle- and frequency-dependence of the transmitted intensity of the microwave beam through the metamaterial prism and comparedmore » well to simulations; in addition, near-field electromagnetic intensity mapping was conducted with an infrared camera, and there was also a good match with the simulations for expected frequency ranges for the negative index of refraction.« less

Gradient parameter and axial and field rays in the gradient-index crystalline lens model

NASA Astrophysics Data System (ADS)

Pérez, M. V.; Bao, C.; Flores-Arias, M. T.; Rama, M. A.; Gómez-Reino, C.

2003-09-01

Gradient-index models of the human lens have received wide attention in optometry and vision sciences for considering how changes in the refractive index profile with age and accommodation may affect refractive power. This paper uses the continuous asymmetric bi-elliptical model to determine gradient parameter and axial and field rays of the human lens in order to study the paraxial propagation of light through the crystalline lens of the eye.

Options for refractive index and viscosity matching to study variable density flows

NASA Astrophysics Data System (ADS)

Clément, Simon A.; Guillemain, Anaïs; McCleney, Amy B.; Bardet, Philippe M.

2018-02-01

Variable density flows are often studied by mixing two miscible aqueous solutions of different densities. To perform optical diagnostics in such environments, the refractive index of the fluids must be matched, which can be achieved by carefully choosing the two solutes and the concentration of the solutions. To separate the effects of buoyancy forces and viscosity variations, it is desirable to match the viscosity of the two solutions in addition to their refractive index. In this manuscript, several pairs of index matched fluids are compared in terms of viscosity matching, monetary cost, and practical use. Two fluid pairs are studied in detail, with two aqueous solutions (binary solutions of water and a salt or alcohol) mixed into a ternary solution. In each case: an aqueous solution of isopropanol mixed with an aqueous solution of sodium chloride (NaCl) and an aqueous solution of glycerol mixed with an aqueous solution of sodium sulfate (Na_2SO_4). The first fluid pair allows reaching high-density differences at low cost, but brings a large difference in dynamic viscosity. The second allows matching dynamic viscosity and refractive index simultaneously, at reasonable cost. For each of these four solutes, the density, kinematic viscosity, and refractive index are measured versus concentration and temperature, as well as wavelength for the refractive index. To investigate non-linear effects when two index-matched, binary solutions are mixed, the ternary solutions formed are also analyzed. Results show that density and refractive index follow a linear variation with concentration. However, the viscosity of the isopropanol and NaCl pair deviates from the linear law and has to be considered. Empirical correlations and their coefficients are given to create index-matched fluids at a chosen temperature and wavelength. Finally, the effectiveness of the refractive index matching is illustrated with particle image velocimetry measurements performed for a buoyant jet in a

Linear and nonlinear optical absorption coefficients and refractive index changes in GaN/Al{sub x}Ga{sub (1−x)}N double quantum wells operating at 1.55 μm

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dakhlaoui, Hassen

2015-04-07

In the present paper, the linear and nonlinear optical absorption coefficients and refractive index changes between the ground and the first excited states in double GaN/Al{sub x}Ga{sub (1−x)}N quantum wells are studied theoretically. The electronic energy levels and their corresponding wave functions are obtained by solving Schrödinger-Poisson equations self-consistently within the effective mass approximation. The obtained results show that the optical absorption coefficients and refractive index changes can be red- and blue-shifted through varying the left quantum well width and the aluminum concentration x{sub b2} of the central barrier, respectively. These structural parameters are found to present optimum values formore » carrying out the transition of 0.8 eV (1.55 μm). Furthermore, we show that the desired transition can also be achieved by replacing the GaN in the left quantum well with Al{sub y}Ga{sub (1−y)}N and by varying the aluminum concentration y{sub Al}. The obtained results give a new degree of freedom in optoelectronic device applications such as optical fiber telecommunications operating at (1.55 μm)« less

Effect of embedded silver nanoparticles on refractive index of soda lime glass

NASA Astrophysics Data System (ADS)

Sonal, Sharma, Annu; Aggarwal, Sanjeev

2018-05-01

Silver glass nanocomposites were prepared by exposing silver doped soda lime glass slides obtained via ion-exchange reaction to a beam of 200 keV Argon ions (Ar+) at an off normal angle of 400 with doses of 5x1015 ions cm-2 and 1x1016 ions cm-2. These nanocomposites were further characterized using UV-visible spectrophotometer so as to study their transmission and reflection behavior and compute their refractive index and real and imaginary parts of dielectric function.

Methods for Prediction of Refractive Index in Glasses for the Infrared

DOE Office of Scientific and Technical Information (OSTI.GOV)

McCloy, John S.

It is often useful to obtain custom glasses that meet particular requirements of refractive index and dispersion for high-end optical design and applications. In the case of infrared glasses, limited experimental data are available due to difficulties in processing of these glasses and also measuring refractive indices accurately. This paper proposes methods to estimate refractive index and dispersion as a function of composition for selected infrared-transmitting glasses. Methods for refractive index determination are reviewed and evaluated, including Gladstone-Dale, Wemple-DiDomenico single oscillator, Optical basicity, and Lorentz-Lorenz total polarizability. Various estimates for a set of PbO-Bi2O3-Ga2O3 (heavy metal oxide) and As-S (chalcogenide)more » glasses will be compared with measured values of index and dispersion.« less

Cell refractive index for cell biology and disease diagnosis: past, present and future.

PubMed

Liu, P Y; Chin, L K; Ser, W; Chen, H F; Hsieh, C-M; Lee, C-H; Sung, K-B; Ayi, T C; Yap, P H; Liedberg, B; Wang, K; Bourouina, T; Leprince-Wang, Y

2016-02-21

Cell refractive index is a key biophysical parameter, which has been extensively studied. It is correlated with other cell biophysical properties including mechanical, electrical and optical properties, and not only represents the intracellular mass and concentration of a cell, but also provides important insight for various biological models. Measurement techniques developed earlier only measure the effective refractive index of a cell or a cell suspension, providing only limited information on cell refractive index and hence hindering its in-depth analysis and correlation. Recently, the emergence of microfluidic, photonic and imaging technologies has enabled the manipulation of a single cell and the 3D refractive index of a single cell down to sub-micron resolution, providing powerful tools to study cells based on refractive index. In this review, we provide an overview of cell refractive index models and measurement techniques including microfluidic chip-based techniques for the last 50 years, present the applications and significance of cell refractive index in cell biology, hematology, and pathology, and discuss future research trends in the field, including 3D imaging methods, integration with microfluidics and potential applications in new and breakthrough research areas.

Iodine insertion and dispersion of refractive index in organic single crystal semiconductor.

PubMed

Kwon, Seonho; Bae, Junwan; Lee, I J

2018-02-20

Insertion of halogens such as bromine or iodine affects the electronic polarizability of ions and the local field inside the medium, and thus modifies the refractive index. Acquiring precise knowledge of the dispersion of refractive index and ultimately tailoring conventional semiconductors for wide-range refractive index control have been a vital issue to resolve before realizing advanced organic optoelectronic devices. In this report, dispersions of the refractive index of a single crystal tetramethyltetraselenafulvalene [C 10 H 12 Se 4 ] (TMTSF) are thoroughly studied from broadband interference modulations of photoluminescence (PL) spectra at various temperatures and doping levels. A large enhancement of the refractive index, more than 20% of the intrinsic value, is achieved with inclusion of a small composition of iodide ions, while the structural and optical properties remain mostly intact. Nearly temperature independent dispersion of the refractive index suggests that, unlike most polymers in which the thermal expansion coefficient dominates over the change of polarizability with temperature, the latter enhances significantly and may become more or less comparable to the thermal expansion coefficient given by 1.71 × 10 -4 /K, when single crystal TMTSF is doped by iodine.

Refraction in the lower troposphere: Higher order image distortion effects due to refractive profile curvature

NASA Astrophysics Data System (ADS)

Short, Daniel J.

the arrival angles shows the target viewed by an observer will appear stretched, or magnified (towering). Conversely, with a negative lensing action the target viewed will appear shortened or compressed (stooping). The lensing can be modeled with a parabolic refractive index profile and the curvature of the profile is characterized by the curvature parameter alpha (units: m-1). The objective of chapter 4 is to estimate the curvature parameter from an analysis of the images collected by the camera system. In effect, the camera acts as a device that measures ray angle of arrival so image changes that appear as a stretch can be related to changes in the curvature of the index profile. Time-lapse images of the F & A Dairy products building in Las Cruces, NM (15.3 km range from the camera at the NMSU campus) were analyzed using a manual cursor-marking MATLAB script developed for this project. For several different dates, we found the largest stretches occur in the morning. For example, a comparison of two morning images separated by an hour shows the apparent height of the building in a second image gained about 34 pixels compared to the first image. The refractive index curvature change for this case is calculated and found to be alpha = 6.0 x 10-5 m-1 . As the day progressed the image slowly compressed back to the early morning size. Optical measurements of the local index of refraction profile of the atmosphere have been made in the past but usually only for isolated events or time periods. There is little data to describe occurrence probabilities, spatial or temporal properties, or relative strength of effects for different seasons, or even durations of weeks. In this dissertation, time-lapse image data from two separate weeks were analyzed for daily stretching/compressing events and presented graphically. The results show a systematic trend of dramatic size changes in the morning and a slow progression to normal building size as the day continues. Using the optical

A refractive index sensor based on taper Michelson interferometer in multimode fiber

NASA Astrophysics Data System (ADS)

Fu, Xinghu; Zhang, Jiangpeng; Wang, Siwen; Fu, Guangwei; Liu, Qiang; Jin, Wa; Bi, Weihong

2016-11-01

A refractive index sensor based on taper Michelson interferometer in multimode fiber is proposed. The Hydrofluoric acid corrosion processing is studied in the preparation of single cone multimode optical fiber sensor. The taper Michelson interferometer is fabricated by changing corrosion time. The relationship between fiber sensor feature and corrosion time is analyzed. The experimental results show that the interference spectrum shift in the direction of short wave with the increase of the refractive index. The refractive index sensitivity can reach 115.8008 nm/RIU. Thereby, it can be used in detecting the refractive index in different areas including the environmental protection, health care and food production.

Experimental verification and simulation of negative index of refraction using Snell's law.

PubMed

Parazzoli, C G; Greegor, R B; Li, K; Koltenbah, B E C; Tanielian, M

2003-03-14

We report the results of a Snell's law experiment on a negative index of refraction material in free space from 12.6 to 13.2 GHz. Numerical simulations using Maxwell's equations solvers show good agreement with the experimental results, confirming the existence of negative index of refraction materials. The index of refraction is a function of frequency. At 12.6 GHz we measure and compute the real part of the index of refraction to be -1.05. The measurements and simulations of the electromagnetic field profiles were performed at distances of 14lambda and 28lambda from the sample; the fields were also computed at 100lambda.

Polymer microfiber bridging Bi-tapered refractive index sensor based on evanescent field

NASA Astrophysics Data System (ADS)

Lv, Ri-Qing; Wang, Qi; Wang, Bo-Tao; Liu, Yu; Kong, Lingxin

2018-05-01

A PDMS/graphene enhanced PMMA micro optical waveguide sensor is reported in terms of fabrication method and optical characteristics. The micro optical waveguide with a diameter of 6 μm and a length of 800 μm is used as the sensing probe to realize refractive index (RI) measurement suspended in NaCl solutions with different concentrations. Experimental results show that the refractive index sensing sensitivity can reach 2027.97 nm/RIU within the refractive index ranging from 1.3333-1.3426. Research results show that PMMA/graphene micro optical waveguide doped with PDMS is an excellent high sensitive sensing technology in refractive index detection field.

Talbot phase-contrast X-ray imaging for the small joints of the hand

PubMed Central

Stutman, Dan; Beck, Thomas J; Carrino, John A; Bingham, Clifton O

2011-01-01

A high resolution radiographic method for soft tissues in the small joints of the hand would aid in the study and treatment of Rheumatoid Arthritis (RA) and Osteoarthritis (OA), which often attacks these joints. Of particular interest would be imaging with <100 μm resolution the joint cartilage, whose integrity is a main indicator of disease. Differential phase-contrast or refraction based X-ray imaging (DPC) with Talbot grating interferometers could provide such a method, since it enhances soft tissue contrast and it can be implemented with conventional X-ray tubes. A numerical joint phantom was first developed to assess the angular sensitivity and spectrum needed for a hand DPC system. The model predicts that due to quite similar refraction indexes for joint soft tissues, the refraction effects are very small, requiring high angular resolution. To compare our model to experiment we built a high resolution bench-top interferometer using 10 μm period gratings, a W anode tube and a CCD based detector. Imaging experiments on animal cartilage and on a human finger support the model predictions. For instance, the estimated difference between the index of refraction of cartilage and water is of only several percent at ~25 keV mean energy, comparable to that between the linear attenuation coefficients. The potential advantage of DPC imaging comes thus mainly from the edge enhancement at the soft tissue interfaces. Experiments using a cadaveric human finger are also qualitatively consistent with the joint model, showing that refraction contrast is dominated by tendon embedded in muscle, with the cartilage layer difficult to observe in our conditions. Nevertheless, the model predicts that a DPC radiographic system for the small hand joints of the hand could be feasible using a low energy quasi-monochromatic source, such as a K-edge filtered Rh or Mo tube, in conjunction with a ~2 m long ‘symmetric’ interferometer operated in a high Talbot order. PMID:21841214

Talbot phase-contrast x-ray imaging for the small joints of the hand

NASA Astrophysics Data System (ADS)

Stutman, Dan; Beck, Thomas J.; Carrino, John A.; Bingham, Clifton O.

2011-09-01

A high-resolution radiographic method for soft tissues in the small joints of the hand would aid in the study and treatment of rheumatoid arthritis (RA) and osteoarthritis (OA), which often attacks these joints. Of particular interest would be imaging with <100 µm resolution the joint cartilage, whose integrity is a main indicator of disease. Differential phase-contrast (DPC) or refraction-based x-ray imaging with Talbot grating interferometers could provide such a method, since it enhances soft tissue contrast and can be implemented with conventional x-ray tubes. A numerical joint phantom was first developed to assess the angular sensitivity and spectrum needed for a hand DPC system. The model predicts that, due to quite similar refraction indexes for joint soft tissues, the refraction effects are very small, requiring high angular resolution. To compare our model to experiment we built a high-resolution bench-top interferometer using 10 µm period gratings, a W anode tube and a CCD-based detector. Imaging experiments on animal cartilage and on a human finger support the model predictions. For instance, the estimated difference between the index of refraction of cartilage and water is of only several percent at ~25 keV mean energy, comparable to that between the linear attenuation coefficients. The potential advantage of DPC imaging thus comes mainly from the edge enhancement at the soft tissue interfaces. Experiments using a cadaveric human finger are also qualitatively consistent with the joint model, showing that refraction contrast is dominated by tendon embedded in muscle, with the cartilage layer difficult to observe in our conditions. Nevertheless, the model predicts that a DPC radiographic system for the small hand joints of the hand could be feasible using a low energy quasi-monochromatic source, such as a K-edge filtered Rh or Mo tube, in conjunction with a ~2 m long 'symmetric' interferometer operated in a high Talbot order.

A three-image algorithm for hard x-ray grating interferometry.

PubMed

Pelliccia, Daniele; Rigon, Luigi; Arfelli, Fulvia; Menk, Ralf-Hendrik; Bukreeva, Inna; Cedola, Alessia

2013-08-12

A three-image method to extract absorption, refraction and scattering information for hard x-ray grating interferometry is presented. The method comprises a post-processing approach alternative to the conventional phase stepping procedure and is inspired by a similar three-image technique developed for analyzer-based x-ray imaging. Results obtained with this algorithm are quantitatively comparable with phase-stepping. This method can be further extended to samples with negligible scattering, where only two images are needed to separate absorption and refraction signal. Thanks to the limited number of images required, this technique is a viable route to bio-compatible imaging with x-ray grating interferometer. In addition our method elucidates and strengthens the formal and practical analogies between grating interferometry and the (non-interferometric) diffraction enhanced imaging technique.

Cryogenic Temperature-dependent Refractive Index Measurements of N-BK7, BaLKN3, and SF15 for NOTES PDI

NASA Technical Reports Server (NTRS)

Frey, Bradley J.; Leviton, Douglas F.; Madison, Timothy J.

2007-01-01

In order to enable high quality lens designs using N-BK7, BaLKN3, and SF15 at cryogenic temperatures, we have measured the absolute refractive index of prisms of these three materials using the Cryogenic, High-Accuracy Refraction Measuring System (CHARMS) at NASA's Goddard Space Flight Center, as a function of both wavelength and temperature. For N-BK7, we report absolute refractive index and thermo-optic coefficient (dn/dT) at temperatures ranging from 50 to 300 K at wavelengths from 0.45 to 2.7 micrometers; for BaLKN3 we cover temperatures ranging from 40 to 300 K and wavelengths from 0.4 to 2.6 micrometers; for SF15 we cover temperatures ranging from 50 to 300 K and wavelengths from 0.45 to 2.6 micrometers. We compare our measurements with others in the literature and provide temperature-dependent Sellmeier coefficients based on our data to allow accurate interpolation of index to other wavelengths and temperatures. While we generally find good agreement (plus or minus 2 x 10(exp -4) for N-BK7, less than 1 x 10(exp -4) for the other materials) at room temperature between our measured values and those provided by the vendor, there is some variation between the datasheets provided with the prisms we measured and the catalog values published by the vendor. This underlines the importance of measuring the absolute refractive index of the material when precise knowledge of the refractive index is required.

Refractive index and its impact on pseudophakic dysphotopsia.

PubMed

Radmall, Bryce R; Floyd, Anne; Oakey, Zack; Olson, Randall J

2015-01-01

It has been shown that the biggest dissatisfier for uncomplicated cataract surgery patients is pseudophakic dysphotopsia (PD). While edge design of an intraocular lens (IOL) impacts this problem, refractive index is still controversial as to its impact. This retrospective cohort study was designed to determine the role of increasing refractive index in PD. This study was conducted at the John A. Moran Eye Center, University of Utah, USA. A retrospective chart review identified patients who received one of two hydrophobic acrylic single piece IOLs (AcrySof WF SP [SN60WF] or Tecnis SP [ZCB00]), which differed mainly by refractive index (1.55 versus 1.47). Eighty-seven patients who had received implantation of a one-piece hydrophobic acrylic IOL were enrolled. Patients were included if the surgery had been uncomplicated and took place at least a year before study participation. All eligible patients had 20/20 best corrected vision, without any disease known to impact visual quality. In addition to conducting a record review, the enrolled patients were surveyed for PD, using a modified National Eye Institute Visual Function questionnaire, as well as for overall satisfaction with visual quality. Statistical analysis demonstrated no difference between the two cohorts regarding PD, general visual function, and overall visual satisfaction. The study suggests that with the two IOLs assessed, increasing the refractive index does not increase incidence of PD or decrease overall visual satisfaction.

Absence of internal conical refraction with the spatially dispersive index surface of fluorine; discussion of the orthogonality of the Poynting vector to the index surface.

PubMed

Dettwiller, Luc

2006-04-17

Since 2001 the intrinsic birefringence of fluorine has been accessible to experiment. It is known that its intrinsic anisotropy is entirely due to spatial dispersion, and that the index surface of fluorine and crystals with the same symmetry has seven optical axes, four of them intersecting this surface at pairs of conical points. I point out the fact that there is no internal conical refraction, but only simple refraction (and without walkoff), with these conical points. I also explain why the rays are not a priori normal to the index surface in the case of fluorine because of its spatial dispersion; and I discuss two particular cases of spatial dispersion where the Poynting vector remains orthogonal to the index surface.

Homodyne chiral polarimetry for measuring thermo-optic refractive index variations.

PubMed

Twu, Ruey-Ching; Wang, Jhao-Sheng

2015-10-10

Novel reflection-type homodyne chiral polarimetry is proposed for measuring the refractive index variations of a transparent plate under thermal impact. The experimental results show it is a simple and useful method for providing accurate measurements of refractive index variations. The measurement can reach a resolution of 7×10^-5.

Talbot-Lau x-ray deflectometry phase-retrieval methods for electron density diagnostics in high-energy density experiments.

PubMed

Valdivia, Maria Pia; Stutman, Dan; Stoeckl, Christian; Mileham, Chad; Begishev, Ildar A; Bromage, Jake; Regan, Sean P

2018-01-10

Talbot-Lau x-ray interferometry uses incoherent x-ray sources to measure refraction index changes in matter. These measurements can provide accurate electron density mapping through phase retrieval. An adaptation of the interferometer has been developed in order to meet the specific requirements of high-energy density experiments. This adaptation is known as a moiré deflectometer, which allows for single-shot capabilities in the form of interferometric fringe patterns. The moiré x-ray deflectometry technique requires a set of object and reference images in order to provide electron density maps, which can be costly in the high-energy density environment. In particular, synthetic reference phase images obtained ex situ through a phase-scan procedure, can provide a feasible solution. To test this procedure, an object phase map was retrieved from a single-shot moiré image obtained from a plasma-produced x-ray source. A reference phase map was then obtained from phase-stepping measurements using a continuous x-ray tube source in a small laboratory setting. The two phase maps were used to retrieve an electron density map. A comparison of the moiré and phase-stepping phase-retrieval methods was performed to evaluate single-exposure plasma electron density mapping for high-energy density and other transient plasma experiments. It was found that a combination of phase-retrieval methods can deliver accurate refraction angle mapping. Once x-ray backlighter quality is optimized, the ex situ method is expected to deliver electron density mapping with improved resolution. The steps necessary for improved diagnostic performance are discussed.

Ray tracing simulation of aero-optical effect using multiple gradient index layer

NASA Astrophysics Data System (ADS)

Yang, Seul Ki; Seong, Sehyun; Ryu, Dongok; Kim, Sug-Whan; Kwon, Hyeuknam; Jin, Sang-Hun; Jeong, Ho; Kong, Hyun Bae; Lim, Jae Wan; Choi, Jong Hwa

2016-10-01

We present a new ray tracing simulation of aero-optical effect through anisotropic inhomogeneous media as supersonic flow field surrounds a projectile. The new method uses multiple gradient-index (GRIN) layers for construction of the anisotropic inhomogeneous media and ray tracing simulation. The cone-shaped projectile studied has 19° semi-vertical angle; a sapphire window is parallel to the cone angle; and an optical system of the projectile was assumed via paraxial optics and infrared image detector. The condition for the steady-state solver conducted through computational fluid dynamics (CFD) included Mach numbers 4 and 6 in speed, 25 km altitude, and 0° angle of attack (AoA). The grid refractive index of the flow field via CFD analysis and Gladstone-Dale relation was discretized into equally spaced layers which are parallel with the projectile's window. Each layer was modeled as a form of 2D polynomial by fitting the refractive index distribution. The light source of ray set generated 3,228 rays for varying line of sight (LOS) from 10° to 40°. Ray tracing simulation adopted the Snell's law in 3D to compute the paths of skew rays in the GRIN layers. The results show that optical path difference (OPD) and boresight error (BSE) decreases exponentially as LOS increases. The variation of refractive index decreases, as the speed of flow field increases the OPD and its rate of decay at Mach number 6 in speed has somewhat larger value than at Mach number 4 in speed. Compared with the ray equation method, at Mach number 4 and 10° LOS, the new method shows good agreement, generated 0.33% of relative root-mean-square (RMS) OPD difference and 0.22% of relative BSE difference. Moreover, the simulation time of the new method was more than 20,000 times faster than the conventional ray equation method. The technical detail of the new method and simulation is presented with results and implication.

Various clinical application of phase contrast X-ray

NASA Astrophysics Data System (ADS)

Oh, Chilhwan; Park, Sangyong; Ha, Seunghan; Park, Gyuman; Lee, Gunwoo; Lee, Onseok; Je, Jungho

2008-02-01

In biomedical application study using phase contrast X-ray, both sample thickness or density and absorption difference are very important factors in aspects of contrast enhancement. We present experimental evidence that synchrotron hard X-ray are suitable for radiological imaging of biological samples down to the cellular level. We investigated the potential of refractive index radiology using un-monochromatized synchrotron hard X-rays for the imaging of cell and tissue in various diseases. Material had been adopted various medical field, such as apoE knockout mouse in cardiologic field, specimen from renal and prostatic carcinoma patient in urology, basal cell epithelioma in dermatology, brain tissue from autosy sample of pakinson's disease, artificially induced artilrtis tissue from rabbits and extracted tooth from patients of crack tooth syndrome. Formalin and paraffin fixed tissue blocks were cut in 3 mm thickness for the X-ray radiographic imaging. From adjacent areas, 4 μm thickness sections were also prepared for hematoxylin-eosin staining. Radiographic images of dissected tissues were obtained using the hard X-rays from the 7B2 beamline of the Pohang Light Source (PLS). The technique used for the study was the phase contrast images were compared with the optical microscopic images of corresponding histological slides. Radiographic images of various diseased tissues showed clear histological details of organelles in normal tissues. Most of cancerous lesions were well differentiated from adjacent normal tissues and detailed histological features of each tumor were clearly identified. Also normal microstructures were identifiable by the phase contrast imaging. Tissue in cancer or other disease showed clearly different findings from those of surrounding normal tissue. For the first time we successfully demonstrated that synchrotron hard X-rays can be used for radiological imaging of relatively thick tissue samples with great histological details.

Refractive index modulation in polymer film doped with diazo Meldrum's acid

NASA Astrophysics Data System (ADS)

Zanutta, Alessio; Villa, Filippo; Bertarelli, Chiara; Bianco, Andrea

2016-08-01

Diazo Meldrum's acid undergoes a photoreaction induced by UV light and it is used as photosensitizer in photoresists. Upon photoreaction, a change in refractive index occurs, which makes this system interesting for volume holography. We report on the sublimation effect at room temperature and the effect of photoirradiation on the refractive index in thin films of CAB (Cellulose acetate butyrate) doped with different amount of diazo Meldrum's acid. A net modulation of the refractive index of 0.01 is achieved with 40% of doping ratio together with a reduction of the film thickness.

Evidence of negative-index refraction in nonlinear chemical waves.

PubMed

Yuan, Xujin; Wang, Hongli; Ouyang, Qi

2011-05-06

The negative index of refraction of nonlinear chemical waves has become a recent focus in nonlinear dynamics researches. Theoretical analysis and computer simulations have predicted that the negative index of refraction can occur on the interface between antiwaves and normal waves in a reaction-diffusion (RD) system. However, no experimental evidence has been found so far. In this Letter, we report our experimental design in searching for such a phenomenon in a chlorite-iodide-malonic acid (CIMA) reaction. Our experimental results demonstrate that competition between waves and antiwaves at their interface determines the fate of the wave interaction. The negative index of refraction was only observed when the oscillation frequency of a normal wave is significantly smaller than that of the antiwave. All experimental results were supported by simulations using the Lengyel-Epstein RD model which describes the CIMA reaction-diffusion system.

Design and characteristics of refractive index sensor based on thinned and microstructure fiber Bragg grating.

PubMed

Huang, Xue-Feng; Chen, Zhe-Min; Shao, Li-Yang; Cen, Ke-Fa; Sheng, De-Ren; Chen, Jun; Zhou, Hao

2008-02-01

A refractive index sensor based on the thinned and microstructure fiber Bragg grating (ThMs-FBG) was proposed and realized as a chemical sensing. The numerical simulation for the reflectance spectrum of the ThMs-FBG was calculated and the phase shift down-peak could be observed from the reflectance spectrum. Many factors influencing the reflectance spectrum were considered in detail for simulation, including the etched depth, length, and position. The sandwich-solution etching method was utilized to realize the microstructure of the ThMs-FBG, and the photographs of the microstructure were obtained. Experimental results demonstrated that the reflectance spectrum, phase shift down-peak wavelength, and reflected optical intensity of the ThMs-FBG all depended on the surrounding refractive index. However, only the down-peak wavelength of the ThMs-FBG changed with the surrounding temperature. Under the condition that the length and cladding diameter of the ThMs-FBG microstructure were 800 and 14 mum, respectively, and the position of the microstructure of the ThMs-FBG is in the middle of grating region, the refractive index sensitivity of the ThMs-FBG was 0.79 nm/refractive index unit with the wide range of 1.33-1.457 and a high resolution of 1.2 x 10(-3). The temperature sensitivity was 0.0103 nm/ degrees C, which was approximately equal to that of common FBG.

Refractive index profilometry using the total internally reflected light field.

PubMed

Das, Tania; Bhattacharya, K

2017-11-20

A full-field polarization-based technique is presented for quantitative evaluation of the spatial distribution of the refractive index in macro and micro samples. The sample is mounted on a glass-air interface of a prism, illuminated by a linearly polarized collimated light beam, and two intensity frames are digitally recorded with specific orientations of an analyzer. The pair of intensity data frames captured with this simple setup is combined through an algorithm specially developed for the purpose, to yield the phase difference between the transverse electric and transverse magnetic components of the total internally reflected light field. The phase difference is then related to the refractive index of the sample. Experimental results for refractive index variations in a laser-etched glass plate and red blood corpuscles are presented. One of the salient features of the proposed technique is that the depth of measurement is dependent on the penetration depth of the sample's evanescent field, which is typically of the order of a few hundred nanometers, thereby facilitating refractive index measurements along a thin section of the sample.

Artificial dielectric stepped-refractive-index lens for the terahertz region.

PubMed

Hernandez-Serrano, A I; Mendis, Rajind; Reichel, Kimberly S; Zhang, Wei; Castro-Camus, E; Mittleman, Daniel M

2018-02-05

In this paper we theoretically and experimentally demonstrate a stepped-refractive-index convergent lens made of a parallel stack of metallic plates for terahertz frequencies based on artificial dielectrics. The lens consist of a non-uniformly spaced stack of metallic plates, forming a mirror-symmetric array of parallel-plate waveguides (PPWGs). The operation of the device is based on the TE 1 mode of the PPWG. The effective refractive index of the TE 1 mode is a function of the frequency of operation and the spacing between the plates of the PPWG. By varying the spacing between the plates, we can modify the local refractive index of the structure in every individual PPWG that constitutes the lens producing a stepped refractive index profile across the multi stack structure. The theoretical and experimental results show that this structure is capable of focusing a 1 cm diameter beam to a line focus of less than 4 mm for the design frequency of 0.18 THz. This structure shows that this artificial-dielectric concept is an important technology for the fabrication of next generation terahertz devices.

Predicting of the refractive index of haemoglobin using the Hybrid GA-SVR approach.

PubMed

Oyehan, Tajudeen A; Alade, Ibrahim O; Bagudu, Aliyu; Sulaiman, Kazeem O; Olatunji, Sunday O; Saleh, Tawfik A

2018-04-30

The optical properties of blood play crucial roles in medical diagnostics and treatment, and in the design of new medical devices. Haemoglobin is a vital constituent of the blood whose optical properties affect all of the optical properties of human blood. The refractive index of haemoglobin has been reported to strongly depend on its concentration which is a function of the physiology of biological cells. This makes the refractive index of haemoglobin an essential non-invasive bio-marker of diseases. Unfortunately, the complexity of blood tissue makes it challenging to experimentally measure the refractive index of haemoglobin. While a few studies have reported on the refractive index of haemoglobin, there is no solid consensus with the data obtained due to different measuring instruments and the conditions of the experiments. Moreover, obtaining the refractive index via an experimental approach is quite laborious. In this work, an accurate, fast and relatively convenient strategy to estimate the refractive index of haemoglobin is reported. Thus, the GA-SVR model is presented for the prediction of the refractive index of haemoglobin using wavelength, temperature, and the concentration of haemoglobin as descriptors. The model developed is characterised by an excellent accuracy and very low error estimates. The correlation coefficients obtained in these studies are 99.94% and 99.91% for the training and testing results, respectively. In addition, the result shows an almost perfect match with the experimental data and also demonstrates significant improvement over a recent mathematical model available in the literature. The GA-SVR model predictions also give insights into the influence of concentration, wavelength, and temperature on the RI measurement values. The model outcome can be used not only to accurately estimate the refractive index of haemoglobin but also could provide a reliable common ground to benchmark the experimental refractive index results

Two-dimensional interferometric characterization of laser-induced refractive index profiles in bulk Topas polymer

NASA Astrophysics Data System (ADS)

Hessler, Steffen; Rosenberger, Manuel; Schmauss, Bernhard; Hellmann, Ralf

2018-01-01

In this paper we precisely determine laser-induced refractive index profiles created in cyclic olefin copolymer Topas 6017 employing a sophisticated phase shifting Mach-Zehnder interferometry approach. Beyond the usual one-dimensional modification depth measurement we highlight that for straight waveguide structures also a two-dimensional refractive index distribution can be directly obtained providing full information of a waveguide's exact cross section and its gradient refractive index contrast. Deployed as direct data input in optical waveguide simulation, the evaluated 2D refractive index profiles permit a detailed calculation of the waveguides' actual mode profiles. Furthermore, conventional one-dimensional interferometric measurements for refractive index depth profiles with varying total imposed laser fluence of a 248 nm KrF excimer laser are included to investigate the effect on refractive index modification depth. Maximum surface refractive index increase turns out to attain up to 1.86 ·10-3 enabling laser-written optical waveguide channels. Additionally, a comprehensive optical material characterization in terms of dispersion, thermo-optic coefficient and absorption measurement of unmodified and UV-modified Topas 6017 is carried out.

In-fiber refractive index sensor based on single eccentric hole-assisted dual-core fiber.

PubMed

Yang, Jing; Guan, Chunying; Tian, Peixuan; Yuan, Tingting; Zhu, Zheng; Li, Ping; Shi, Jinhui; Yang, Jun; Yuan, Libo

2017-11-01

We propose a novel and simple in-fiber refractive index sensor based on resonant coupling, constructed by a short section of single eccentric hole-assisted dual-core fiber (SEHADCF) spliced between two single-mode fibers. The coupling characteristics of the SEHADCF are calculated numerically. The strong resonant coupling occurs when the fundamental mode of the center core phase-matches to that of the suspended core in the air hole. The effective refractive index of the fundamental mode of the suspended core can be obviously changed by injecting solution into the air hole. The responses of the proposed devices to the refractive index and temperature are experimentally measured. The refractive index sensitivity is 627.5 nm/refractive index unit in the refractive index range of 1.335-1.385. The sensor without solution filling is insensitive to temperature in the range of 30-90°C. The proposed refractive index sensor has outstanding advantages, such as simple fabrication, good mechanical strength, and excellent microfluidic channel, and will be of importance in biological detection, chemical analysis, and environment monitoring.

Refractive index measurement for biomaterial samples by total internal reflection.

PubMed

Jin, Y L; Chen, J Y; Xu, L; Wang, P N

2006-10-21

The refractive index of biological tissue is a fundamental parameter in applications of optical diagnosis and laser treatments. In the present work, the refractive indices and thermo-optic coefficients of some basic biomaterials, such as blood plasma, haemoglobin solution and lipid membrane, were studied by the method of total internal reflection at the wavelengths of 532 and 632.8 nm that are the most frequently used laser wavelengths in the biomedical field. The effects of the sample concentration and the temperature on refractive index were measured, and empirical relationships were summarized, accompanied by a theoretical explanation based on molecular polarization theory. The results provide some fundamental data for the refractive indices of these biomaterials under variant conditions, and also demonstrate that the total internal reflection method is a feasible and reliable way to measure the refractive indices of biological samples.

A software platform for phase contrast x-ray breast imaging research.

PubMed

Bliznakova, K; Russo, P; Mettivier, G; Requardt, H; Popov, P; Bravin, A; Buliev, I

2015-06-01

To present and validate a computer-based simulation platform dedicated for phase contrast x-ray breast imaging research. The software platform, developed at the Technical University of Varna on the basis of a previously validated x-ray imaging software simulator, comprises modules for object creation and for x-ray image formation. These modules were updated to take into account the refractive index for phase contrast imaging as well as implementation of the Fresnel-Kirchhoff diffraction theory of the propagating x-ray waves. Projection images are generated in an in-line acquisition geometry. To test and validate the platform, several phantoms differing in their complexity were constructed and imaged at 25 keV and 60 keV at the beamline ID17 of the European Synchrotron Radiation Facility. The software platform was used to design computational phantoms that mimic those used in the experimental study and to generate x-ray images in absorption and phase contrast modes. The visual and quantitative results of the validation process showed an overall good correlation between simulated and experimental images and show the potential of this platform for research in phase contrast x-ray imaging of the breast. The application of the platform is demonstrated in a feasibility study for phase contrast images of complex inhomogeneous and anthropomorphic breast phantoms, compared to x-ray images generated in absorption mode. The improved visibility of mammographic structures suggests further investigation and optimisation of phase contrast x-ray breast imaging, especially when abnormalities are present. The software platform can be exploited also for educational purposes. Copyright © 2015 Elsevier Ltd. All rights reserved.

Terahertz metasurfaces with a high refractive index enhanced by the strong nearest neighbor coupling.

PubMed

Tan, Siyu; Yan, Fengping; Singh, Leena; Cao, Wei; Xu, Ningning; Hu, Xiang; Singh, Ranjan; Wang, Mingwei; Zhang, Weili

2015-11-02

The realization of high refractive index is of significant interest in optical imaging with enhanced resolution. Strongly coupled subwavelength resonators were proposed and demonstrated at both optical and terahertz frequencies to enhance the refractive index due to large induced dipole moment in meta-atoms. Here, we report an alternative design for flexible free-standing terahertz metasurface in the strong coupling regime where we experimentally achieve a peak refractive index value of 14.36. We also investigate the impact of the nearest neighbor coupling in the form of frequency tuning and enhancement of the peak refractive index. We provide an analytical circuit model to explain the impact of geometrical parameters and coupling on the effective refractive index of the metasurface. The proposed meta-atom structure enables tailoring of the peak refractive index based on nearest neighbor coupling and this property offers tremendous design flexibility for transformation optics and other index-gradient devices at terahertz frequencies.

Refractive index measurements of single, spherical cells using digital holographic microscopy.

PubMed

Schürmann, Mirjam; Scholze, Jana; Müller, Paul; Chan, Chii J; Ekpenyong, Andrew E; Chalut, Kevin J; Guck, Jochen

2015-01-01

In this chapter, we introduce digital holographic microscopy (DHM) as a marker-free method to determine the refractive index of single, spherical cells in suspension. The refractive index is a conclusive measure in a biological context. Cell conditions, such as differentiation or infection, are known to yield significant changes in the refractive index. Furthermore, the refractive index of biological tissue determines the way it interacts with light. Besides the biological relevance of this interaction in the retina, a lot of methods used in biology, including microscopy, rely on light-tissue or light-cell interactions. Hence, determining the refractive index of cells using DHM is valuable in many biological applications. This chapter covers the main topics that are important for the implementation of DHM: setup, sample preparation, and analysis. First, the optical setup is described in detail including notes and suggestions for the implementation. Following that, a protocol for the sample and measurement preparation is explained. In the analysis section, an algorithm for the determination of quantitative phase maps is described. Subsequently, all intermediate steps for the calculation of the refractive index of suspended cells are presented, exploiting their spherical shape. In the last section, a discussion of possible extensions to the setup, further measurement configurations, and additional analysis methods are given. Throughout this chapter, we describe a simple, robust, and thus easily reproducible implementation of DHM. The different possibilities for extensions show the diverse fields of application for this technique. Copyright © 2015 Elsevier Inc. All rights reserved.

Analysis of interferograms of refractive index inhomogeneities produced in optical materials

NASA Astrophysics Data System (ADS)

Tarjányi, N.

2014-12-01

Optical homogeneity of materials intended for optical applications is one of the criterions which decide on an appropriate application method for the material. The existence of a refractive index inhomogeneity inside a material may disqualify it from utilization or by contrary, provide an advantage. For observation of a refractive index inhomogeneity, even a weak one, it is convenient to use any of interferometric methods. They are very sensitive and provide information on spatial distribution of the refractive index, immediately. One can use them also in case when the inhomogeneity evolves in time, usually due to action of some external fields. Then, the stream of interferograms provides a dynamic evolution of a spatial distribution of the inhomogeneity. In the contribution, there are presented results of the analysis of interferograms obtained by observing the creation of a refractive index inhomogeneity due to illumination of thin layers of a polyvinyl-alcohol/acrylamide photopolymer and a plate of photorefractive crystal, lithium niobate, by light and a refractive index inhomogeneity originated at the boundary of two layers of polydimethylsiloxane. The obtained dependences can be used for studying of the mechanisms responsible for the inhomogeneity creation, designing various technical applications or for diagnostics of fabricated components.

Modified Kramers-Kronig relations and sum rules for meromorphic total refractive index

DOE Office of Scientific and Technical Information (OSTI.GOV)

Peiponen, Kai-Erik; Saarinen, Jarkko J.; Vartiainen, Erik M.

2003-08-01

Modified Kramers-Kronig relations and corresponding sum rules are shown to hold for the total refractive index that can be presented as a sum of complex linear and nonlinear refractive indices, respectively. It is suggested that a self-action process, involving the degenerate third-order nonlinear susceptibility, can yield a negative total refractive index at some spectral range.

Refractive index measurement of the mouse crystalline lens using optical coherence tomography

PubMed Central

Chakraborty, Ranjay; Lacy, Kip D.; Tan, Christopher C.; Park, Han na; Pardue, Machelle T.

2014-01-01

In recent years, there has been a growing interest for using mouse models in refractive development and myopia research. The crystalline lens is a critical optical component of the mouse eye that occupies greater than 50% of the ocular space, and significant increases in thickness with age. However, changes in refractive index of the mouse crystalline lens are less known. In this study, we examined the changes in thickness and refractive index of the mouse crystalline lens for two different strains, wild-type (WT) and a nyx mutant (nob) over the course of normal visual development or after form deprivation. Refractive index and lens thickness measurements were made on ex vivo lens using spectral domain optical coherence tomography (SD-OCT). Comparison of refractive index measurements on 5 standard ball lenses using the SD-OCT and their known refractive indices (manufacturer provided) indicated good precision (intra-class correlation coefficient, 0.998 and Bland-Altman coefficient of repeatability, 0.116) of the SD-OCT to calculate mouse lens refractive index ex vivo. During normal visual development, lens thickness increased significantly with age for three different cohorts of mice, aged 4 (average thickness from both eyes; WT: 1.78 ± 0.03, nob: 1.79 ± 0.08 mm), 10 (WT: 2.02 ± 0.05, nob: 2.01 ± 0.04 mm) and 16 weeks (WT: 2.12 ± 0.06, nob: 2.09 ± 0.06 mm, p<0.001). Lens thickness was not significantly different between the two strains at any age (p=0.557). For mice with normal vision, refractive index for isolated crystalline lenses in nob mice was significantly greater than WT mice (mean for all ages; WT: 1.42 ± 0.01, nob: 1.44 ± 0.001, p<0.001). After 4 weeks of form deprivation to the right eye using a skull-mounted goggling apparatus, a thinning of the crystalline lens was observed in both right and left eyes of goggled animals compared to their naïve controls (average from both the right and the left eye) for both strains (p=0.052). In form deprived

Femtosecond Z-scan measurements of the nonlinear refractive index of fused silica

NASA Astrophysics Data System (ADS)

Zhang, Lin; Shi, Zhendong; Ma, Hua; Ren, Huan; Yuan, Quan; Ma, Yurong; Feng, Xiaoxuan; Chen, Bo; Yang, Yi

2018-01-01

Z-scan technology is a popular experimental technique for determining the nonlinear refractive index of the material. However, it encounters a great difficulty in measuring the weak nonlinear material like fused silica which is about two orders of magnitude below the nonlinear refractive index of most of the materials studied with the nanosecond and picosecond Z-scan methods. In this case, the change of refractive index introduced by accumulation of thermal effects cannot be neglected. In order to have a reliable measurement of the nonlinear refractive index, a metrology bench based on the femtosecond Z-scan technology is developed. The intensity modulation component and the differential measurement system are applied to guarantee the accuracy of the measuring system. Based on the femtosecond Z-scan theory, the femtosecond laser Z-scan technique is performed on fused silica, and the nonlinear refractive index of Fused silica is determined to be 9.2039×10-14esu for 800nm, 37fs pulse duration at I0=50GW/cm2 with a good repeatability of 6.7%.

Rotating of low-refractive-index microparticles with a quasi-perfect optical vortex.

PubMed

Liang, Yansheng; Lei, Ming; Yan, Shaohui; Li, Manman; Cai, Yanan; Wang, Zhaojun; Yu, Xianghua; Yao, Baoli

2018-01-01

Low-refractive-index microparticles, such as hollow microspheres, have shown great significance in some applications, such as biomedical sensing and targeted drug delivery. However, optical trapping and manipulation of low-refractive-index microparticles are challenging, owing to the repelling force exerted by typical optical traps. In this paper, we demonstrated optical trapping and rotating of large-sized low-refractive-index microparticles by using quasi-perfect optical vortex (quasi-POV) beams, which were generated by Fourier transform of high-order quasi-Bessel beams. Numerical simulation was carried out to characterize the focusing property of the quasi-POV beams. The dynamics of low-refractive-index microparticles in the quasi-POV with various topological charges was investigated in detail. To improve the trapping and rotating performances of the vortex, a point trap was introduced at the center of the ring. Experimental results showed that the quasi-POV was preferable for manipulation of large-sized low-refractive-index microparticles, with its control of the particles' rotating velocity dependent only on the topological charge due to the unchanged orbital radius.

Interferometric measurement of refractive index modification in a single mode microfiber

NASA Astrophysics Data System (ADS)

Ahmed, Farid; Ahsani, Vahid; Jun, Martin B. G.

2017-02-01

Efficient and cost effective measurement of the refractive index profile in an optical fiber is a significant technical job to design and manufacture in-fiber photonic devices and communication systems. For instance, to design fiber gratings, it is required to estimate the refractive index modulation to be inscribed by the fabrication apparatus such as ultraviolet or infrared lasers. Mach-Zehnder interferometer (MZI) based quantification of refractive index change written in single mode microfiber by femtosecond laser radiation is presented in this study. The MZI is constructed by splicing a microfiber (core diameter: 3.75 μm, cladding diameter: 40 μm) between standard single mode fibers. To measure the RI inscribed by infrared femtosecond laser, 200 μm length of the core within the MZI was scanned with laser radiation. As the higher index was written within 200 μm length of the core, the transmission spectrum of the interferometer displayed a corresponding red shift. The observed spectral shift was used to calculate the amount of refractive index change inscribed by the femtosecond irradiation. For the MZI length of 3.25 mm, and spectral shift of 0.8 nm, the calculated refractive index was found to be 0.00022. The reported results display excellent agreement between theory and experimental findings. Demonstrated method provides simple yet very effective on-site measurement of index change in optical fibers. Since the MZI can be constructed in diverse fiber types, this technique offers flexibility to quantify index change in various optical fibers.

Uncladded sensing fiber for refractive index measurement

NASA Astrophysics Data System (ADS)

Bhardwaj, V.; Gangwar, R. K.; Pathak, A. K.; Singh, V. K.

2016-05-01

The formation of chemically etched optical fiber for use in refractive index sensor is addressed. This presented design of a refractive index (RI) sensor is based on recording the power loss exhibited by radiation propagating through an etched multimode fiber (MMF) immersed in the liquid under study. The decreasing diameters of fibers are found to be strongly dependent on the temperature and etchant composition. This experiment was performed for different unclad etched fibers for same sensing length and the RI changes from 1.33 RIU to 1.38 RIU. When the multimode fiber (MMF) is etched for 12 hours the sensitivity of the sensor is approximately 204.25dBm/RIU, which is larger than without etched fiber having sensitivity 127.2dBm/RIU.

Refractive-index-sensing fiber comb using intracavity multi-mode interference fiber sensor

NASA Astrophysics Data System (ADS)

Oe, Ryo; Minamikawa, Takeo; Taue, Shuji; Fukano, Hideki; Nakajima, Yoshiaki; Minoshima, Kaoru; Yasui, Takeshi

2018-02-01

Refractive index measurement is important for evaluation of liquid materials, optical components, and bio sensing. One promising approach for such measurement is use of optical fiber sensors such as surface plasmonic resonance or multi-mode interference (MMI), which measure the change of optical spectrum resulting from the refractive index change. However, the precision of refractive index measurement is limited by the performance of optical spectrum analyzer. If such the refractive index measurement can be performed in radio frequency (RF) region in place of optical region, the measurement precision will be further improved by the frequency-standard-based RF measurement. To this end, we focus on the disturbance-to-RF conversion in a fiber optical frequency comb (OFC) cavity. Since frequency spacing frep of OFC depends on an optical cavity length nL, frep sensitively reflects the external disturbance interacted with nL. Although we previously demonstrated the precise strain measurement based on the frep measurement, the measurable physical quantity is limited to strain or temperature, which directly interacts with the fiber cavity itself. If a functional fiber sensor can be installed into the fiber OFC cavity, the measurable physical quantity will be largely expanded. In this paper, we introduce a MMI fiber sensor into a ring-type fiber OFC cavity for refractive index measurement. We confirmed the refractive-index-dependent frep shift.

Variable Refractive Index Effects on Radiation in Semitransparent Scattering Multilayered Regions

NASA Technical Reports Server (NTRS)

Siegel, R.; Spuckler, C. M.

1993-01-01

A simple set of equations is derived for predicting the temperature distribution and radiative energy flow in a semitransparent layer consisting of an arbitrary number of laminated sublayers that absorb, emit, and scatter radiation. Each sublayer can have a different refractive index and optical thickness. The plane composite region is heated on each exterior side by a different amount of incident radiation. The results are for the limiting case where heat conduction within the layers is very small relative to radiative transfer, and is neglected. The interfaces are assumed diffuse, and all interface reflections are included in the analysis. The thermal behavior is readily calculated from the analytical expressions that are obtained. By using many sublayers, expressions provide the temperature distribution and heat flow for a diffusing medium with a continually varying refractive index, including internal reflection effects caused by refractive index gradients. Temperature and heat flux results are given to show the effect of variations in refractive index and optical thickness through the multilayer laminate.

Hard x-ray nanoprobe of beamline P06 at PETRA III

DOE Office of Scientific and Technical Information (OSTI.GOV)

Schroer, C. G., E-mail: christian.schroer@desy.de; Department Physik, Universität Hamburg, Luruper Chaussee 149, D-22761 Hamburg; Baumbach, C.

2016-07-27

The hard x-ray scanning microscope at beamline P06 of PETRA III at DESY in Hamburg serves a large user community, from physics, chemistry, and nanotechnology to the bio-medical, materials, environmental, and geosciences. It has been in user operation since 2012, and is mainly based on nanofocusing refractive x-ray lenses. Using refractive optics, nearly gaussian-limited nanobeams in the range from 50 to 100 nm can be generated in the hard x-ray energy range from 8 to 30 keV. The degree of coherence can be traded off against the flux in the nanobeam by a two-stage focusing scheme. We give a briefmore » overview on published results from this instrument and describe its most important components and parameters.« less

New method to determine the refractive index and the absorption coefficient of organic nonlinear crystals in the ultra-wideband THz region.

PubMed

Ohno, Seigo; Miyamoto, Katsuhiko; Minamide, Hiroaki; Ito, Hiromasa

2010-08-02

A method for simultaneously measuring the refractive index and absorption coefficient of nonlinear optical crystals in the ultra-wideband terahertz (THz) region is described. This method is based on the analysis of a collinear difference frequency generation (DFG) process using a tunable, dual-wavelength, optical parametric oscillator. The refractive index and the absorption coefficient in the organic nonlinear crystal DAST were experimentally determined in the frequency range 2.5-26.2 THz by measuring the THz-wave output using DFG. The resultant refractive index in the x-direction was approximately 2.3, while the absorption spectrum was in good agreement with FT-IR measurements. The output of the DAST-DFG THz-wave source was optimized to the phase-matching condition using the measured refractive index spectrum in THz region, which resulted in an improvement in the output power of up to a factor of nine.

Thermally stimulated nonlinear refraction in gelatin stabilized Cu-PVP nanocomposite thin films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tamgadge, Y. S., E-mail: ystamgadge@gmail.com; Atkare, D. V.; Pahurkar, V. G.

2016-05-06

This article illustrates investigations on thermally stimulated third order nonlinear refraction of Cu-PVP nanocomposite thin films. Cu nanoparticles have been synthesized using chemical reduction method and thin films in PVP matrix have been obtained using spin coating technique. Thin films have been characterized by X-ray diffraction (XRD) and Ultraviolet-visible (UV-vis) spectroscopyfor structural and linear optical studies. Third order nonlinear refraction studies have been performed using closed aperture z-scan technique under continuous wave (CW) He-Ne laser. Cu-PVP nanocomposites are found to exhibit strong nonlinear refractive index stimulated by thermal lensing effect.

Fiber-integrated refractive index sensor based on a diced Fabry-Perot micro-resonator.

PubMed

Suntsov, Sergiy; Rüter, Christian E; Schipkowski, Tom; Kip, Detlef

2017-11-20

We report on a fiber-integrated refractive index sensor based on a Fabry-Perot micro-resonator fabricated using simple diamond blade dicing of a single-mode step-index fiber. The performance of the device has been tested for the refractive index measurements of sucrose solutions as well as in air. The device shows a sensitivity of 1160 nm/RIU (refractive index unit) at a wavelength of 1.55 μm and a temperature cross-sensitivity of less than 10 -7   RIU/°C. Based on evaluation of the broadband reflection spectra, refractive index steps of 10 -5 of the solutions were accurately measured. The conducted coating of the resonator sidewalls with layers of a high-index material with real-time reflection spectrum monitoring could help to significantly improve the sensor performance.

Simultaneous measurements of absorption spectrum and refractive index in a microfluidic system.

PubMed

Helseth, Lars Egil

2012-02-13

The characterization of dyes in various solvents requires determination of the absorption spectrum of the dye as well as the refractive index of the solvent. Typically, the refractive index of the solvent and the absorption spectrum of the solute are measured using separate experimental setups where significant liquid volumes are required. In this work the first optical measurement system that is able to do simultaneous measurements of the refractive index of the solvent and the spectral properties of the solute in a microscopic volume is presented. The laser dye Rhodamine 6G in glycerol is investigated, and the refractive index of the solution is monitored using the interference pattern of the light scattered off the channel, while its spectral properties is found by monitoring reflected light from the channel.

Quantitative measurement of binary liquid distributions using multiple-tracer x-ray fluorescence and radiography

DOE Office of Scientific and Technical Information (OSTI.GOV)

Halls, Benjamin R.; Meyer, Terrence R.; Kastengren, Alan L.

2015-01-01

The complex geometry and large index-of-refraction gradients that occur near the point of impingement of binary liquid jets present a challenging environment for optical interrogation. A simultaneous quadruple-tracer x-ray fluorescence and line-of-sight radiography technique is proposed as a means of distinguishing and quantifying individual liquid component distributions prior to, during, and after jet impact. Two different pairs of fluorescence tracers are seeded into each liquid stream to maximize their attenuation ratio for reabsorption correction and differentiation of the two fluids during mixing. This approach for instantaneous correction of x-ray fluorescence reabsorption is compared with a more time-intensive approach of usingmore » stereographic reconstruction of x-ray attenuation along multiple lines of sight. The proposed methodology addresses the need for a quantitative measurement technique capable of interrogating optically complex, near-field liquid distributions in many mixing systems of practical interest involving two or more liquid streams.« less

Imaging cells and sub-cellular structures with ultrahigh resolution full-field X-ray microscopy.

PubMed

Chien, C C; Tseng, P Y; Chen, H H; Hua, T E; Chen, S T; Chen, Y Y; Leng, W H; Wang, C H; Hwu, Y; Yin, G C; Liang, K S; Chen, F R; Chu, Y S; Yeh, H I; Yang, Y C; Yang, C S; Zhang, G L; Je, J H; Margaritondo, G

2013-01-01

Our experimental results demonstrate that full-field hard-X-ray microscopy is finally able to investigate the internal structure of cells in tissues. This result was made possible by three main factors: the use of a coherent (synchrotron) source of X-rays, the exploitation of contrast mechanisms based on the real part of the refractive index and the magnification provided by high-resolution Fresnel zone-plate objectives. We specifically obtained high-quality microradiographs of human and mouse cells with 29 nm Rayleigh spatial resolution and verified that tomographic reconstruction could be implemented with a final resolution level suitable for subcellular features. We also demonstrated that a phase retrieval method based on a wave propagation algorithm could yield good subcellular images starting from a series of defocused microradiographs. The concluding discussion compares cellular and subcellular hard-X-ray microradiology with other techniques and evaluates its potential impact on biomedical research. Copyright © 2012 Elsevier Inc. All rights reserved.

Quantitative measurement of binary liquid distributions using multiple-tracer x-ray fluorescence and radiography

DOE PAGES

Halls, Benjamin R.; Meyer, Terrence R.; Kastengren, Alan L.

2015-01-23

The complex geometry and large index-of-refraction gradients that occur near the point of impingement of binary liquid jets present a challenging environment for optical interrogation. A simultaneous quadruple-tracer x-ray fluorescence and line-of-sight radiography technique is proposed as a means of distinguishing and quantifying individual liquid component distributions prior to, during, and after jet impact. Two different pairs of fluorescence tracers are seeded into each liquid stream to maximize their attenuation ratio for reabsorption correction and differentiation of the two fluids during mixing. This approach for instantaneous correction of x-ray fluorescence reabsorption is compared with a more time-intensive approach of usingmore » stereographic reconstruction of x-ray attenuation along multiple lines of sight. The proposed methodology addresses the need for a quantitative measurement technique capable of interrogating optically complex, near-field liquid distributions in many mixing systems of practical interest involving two or more liquid streams.« less

Refractive index and viscosity: dual sensing with plastic fibre gratings

NASA Astrophysics Data System (ADS)

Ferreira, Ricardo; Bilro, Lúcia; Marques, Carlos; Oliveira, Ricardo; Nogueira, Rogério

2014-05-01

A refractive index and viscosity sensor based on FBGs in mPOF is reported for the first time. The refractive index was measured with a sensitivity of -10:98nm=RIU and a resolution of 1 - 10-4RIU. Viscosity measurements were performed with acousto-optic modulation, obtaining a sensitivity of -94:42%=mPa • s and a resolution of 0:06mPa • s.

Tapered-fiber-based refractive index sensor at an air/solution interface.

PubMed

Lu, Ping; Harris, Jeremie; Wang, Xiaozhen; Lin, Ganbin; Chen, Liang; Bao, Xiaoyi

2012-10-20

An approach to achieve refractive index sensing at an air and aqueous glycerol solution interface is proposed using a tapered-fiber-based microfiber Mach-Zehnder interferometer (MFMZI). Compared to a surrounding uniform medium of air or solutions, the spectral interference visibility of the MFMZI at the air/solution interface is significantly reduced due to a weak coupling between the fundamental cladding mode and high-order asymmetric cladding modes, which are extremely sensitive to the external refractive index. The MFMZI is experimentally demonstrated as an evanescent wave refractive index sensor to measure concentrations of glycerol solutions by monitoring average power attenuation of the tapered fiber.

Refractive index measurement of the mouse crystalline lens using optical coherence tomography.

PubMed

Chakraborty, Ranjay; Lacy, Kip D; Tan, Christopher C; Park, Han Na; Pardue, Machelle T

2014-08-01

In recent years, there has been a growing interest for using mouse models in refractive development and myopia research. The crystalline lens is a critical optical component of the mouse eye that occupies greater than 50% of the ocular space, and significant increases in thickness with age. However, changes in refractive index of the mouse crystalline lens are less known. In this study, we examined the changes in thickness and refractive index of the mouse crystalline lens for two different strains, wild-type (WT) and a nyx mutant (nob) over the course of normal visual development or after form deprivation. Refractive index and lens thickness measurements were made on ex vivo lenses using spectral domain optical coherence tomography (SD-OCT). Comparison of refractive index measurements on 5 standard ball lenses using the SD-OCT and their known refractive indices (manufacturer provided) indicated good precision (intra-class correlation coefficient, 0.998 and Bland-Altman coefficient of repeatability, 0.116) of the SD-OCT to calculate mouse lens refractive index ex vivo. During normal visual development, lens thickness increased significantly with age for three different cohorts of mice, aged 4 (average thickness from both eyes; WT: 1.78 ± 0.03, nob: 1.79 ± 0.08 mm), 10 (WT: 2.02 ± 0.05, nob: 2.01 ± 0.04 mm) and 16 weeks (WT: 2.12 ± 0.06, nob: 2.09 ± 0.06 mm, p < 0.001). Lens thickness was not significantly different between the two strains at any age (p = 0.557). For mice with normal vision, refractive index for isolated crystalline lenses in nob mice was significantly greater than WT mice (mean for all ages; WT: 1.42 ± 0.01, nob: 1.44 ± 0.001, p < 0.001). After 4 weeks of form deprivation to the right eye using a skull-mounted goggling apparatus, a thinning of the crystalline lens was observed in both right and left eyes of goggled animals compared to their naïve controls (average from both the right and the left eye) for both

IR spectroscopic determination of the refractive index of Ag1-xTlxBr1-0.54xI0.54x (0 ⩽ x ⩽ 0.05) crystals

NASA Astrophysics Data System (ADS)

Korsakov, Alexandr; Salimgareev, Dmitrii; Lvov, Alexandr; Zhukova, Liya

2017-08-01

In this paper we examined materials relevant for manufacturing various near- and mid-infrared fiber optical elements: AgBr and - presumably for the first time - AgBr - (TlBr0.46I0.54) up to 5% of TlBr0.46I0.54, produced by hot embossing. Both real and imaginary parts of refractive indices were determined within the wavelength of 3.0-14.0 μm for samples of these materials. An increase of the substituent in AgBr caused a monotonous rise of the refractive index, while for every certain composition, a shift towards longer wavelengths led to its decrease. This dependence was depicted on dispersion curves, which clearly demonstrate that optical fibers, drawn from AgBr - (TlBr0.46I0.54) crystals, can be used within the wide mid-infrared range, since the dispersion coefficient here is minimal and constant. To determine the refractive index at the absorption edge (from 0.465 to 0.484 μm), we scrutinized eleven calculation models, with preferable Moss relation.

Multimode interference tapered fiber refractive index sensors.

PubMed

Biazoli, Claudecir R; Silva, Susana; Franco, Marcos A R; Frazão, Orlando; Cordeiro, Cristiano M B

2012-08-20

Real-time monitoring of the fabrication process of tapering down a multimode-interference-based fiber structure is presented. The device is composed of a pure silica multimode fiber (MMF) with an initial 125 μm diameter spliced between two single-mode fibers. The process allows a thin MMF with adjustable parameters to obtain a high signal transmittance, arising from constructive interference among the guided modes at the output end of the MMF. Tapered structures with waist diameters as low as 55 μm were easily fabricated without the limitation of fragile splices or difficulty in controlling lateral fiber alignments. The sensing device is shown to be sensitive to the external environment, and a maximum sensitivity of 2946 nm/refractive index unit in the refractive index range of 1.42-1.43 was attained.

Uncladded sensing fiber for refractive index measurement

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bhardwaj, V., E-mail: bhardwajphyism@gmail.com; Gangwar, R. K.; Pathak, A. K.

2016-05-06

The formation of chemically etched optical fiber for use in refractive index sensor is addressed. This presented design of a refractive index (RI) sensor is based on recording the power loss exhibited by radiation propagating through an etched multimode fiber (MMF) immersed in the liquid under study. The decreasing diameters of fibers are found to be strongly dependent on the temperature and etchant composition. This experiment was performed for different unclad etched fibers for same sensing length and the RI changes from 1.33 RIU to 1.38 RIU. When the multimode fiber (MMF) is etched for 12 hours the sensitivity ofmore » the sensor is approximately 204.25dBm/RIU, which is larger than without etched fiber having sensitivity 127.2dBm/RIU.« less

Refractive index engineering of high performance coupler for compact photonic integrated circuits

NASA Astrophysics Data System (ADS)

Liu, Lu; Zhou, Zhiping

2017-04-01

High performance couplers are highly desired in many applications, but the design is limited by nearly unchangeable material refractive index. To tackle this issue, refractive index engineering method is investigated, which can be realized by subwavelength grating. Subwavelength gratings are periodical structures with pitches small enough to locally synthesize the refractive index of photonic waveguides, which allows direct control of optical profile as well as easier fabrication process. This review provides an introduction to the basics of subwavelength structures and pay special attention to the design strategies of some representative examples of subwavelength grating devices, including: edge couplers, fiber-chip grating couplers, directional couplers and multimode interference couplers. Benefited from the subwavelength grating which can engineer the refractive index as well as birefringence and dispersion, these devices show better performance when compared to their conventional counterparts.

Group refractive index quantification using a Fourier domain short coherence Sagnac interferometer.

PubMed

Montonen, Risto; Kassamakov, Ivan; Lehmann, Peter; Österberg, Kenneth; Hæggström, Edward

2018-02-15

The group refractive index is important in length calibration of Fourier domain interferometers by transparent transfer standards. We demonstrate accurate group refractive index quantification using a Fourier domain short coherence Sagnac interferometer. Because of a justified linear length calibration function, the calibration constants cancel out in the evaluation of the group refractive index, which is then obtained accurately from two uncalibrated lengths. Measurements of two standard thickness coverslips revealed group indices of 1.5426±0.0042 and 1.5434±0.0046, with accuracies quoted at the 95% confidence level. This agreed with the dispersion data of the coverslip manufacturer and therefore validates our method. Our method provides a sample specific and accurate group refractive index quantification using the same Fourier domain interferometer that is to be calibrated for the length. This reduces significantly the requirements of the calibration transfer standard.

Rapid determination of surfactant critical micelle concentration in aqueous solutions using fiber-optic refractive index sensing.

PubMed

Tan, Chun Hua; Huang, Zhen Jian; Huang, Xu Guang

2010-06-01

We describe a simple and rapid method for determining the critical micelle concentration (CMC) of surfactants from fiber-optic measurements of refractive index. The refractive index of an aqueous surfactant solution was monitored as the surfactant concentration was increased using an automated dispensing system. On reaching the surfactant's CMC value, an abrupt change was observed in the rate of increase of the refractive index with increasing concentration. The measurement system provides rapid semiautomatic data collection and analysis, increasing the precision, sensitivity, and range of applicability of the technique while substantially decreasing the amount of manual intervention required. Measurements of CMC for sodium dodecyl sulfate (8.10mM), cetyltrimethylammonium chloride (1.58mM), and Triton X-100 (0.21mM) were in excellent agreement with values previously reported in the literature. The method is applicable to cationic, anionic, and nonionic surfactants, and it offers a facile, in situ, and sensitive means of detecting micelle formation over a broad range of CMC values larger than 10(-1)mM. Copyright 2010 Elsevier Inc. All rights reserved.

Enhancing intensity and refractive index sensing capability with infrared plasmonic perfect absorbers.

PubMed

Cheng, Fei; Yang, Xiaodong; Gao, Jie

2014-06-01

An infrared refractive index sensor based on plasmonic perfect absorbers for glucose concentration sensing is experimentally demonstrated. Utilizing substantial absorption contrast between a perfect absorber (∼98% at normal incidence) and a non-perfect absorber upon the refractive index change, a maximum value of figure of merit (FOM^*) about 55 and a bulk wavelength sensitivity about 590  nm/RIU are achieved. The demonstrated sensing platform provides great potential in improving the performance of plasmonic refractive index sensors and developing future surface enhanced infrared spectroscopy.

Liquid refractive index sensing independent of opacity using an optofluidic diffraction sensor.

PubMed

Xu, Zhida; Han, Kevin; Khan, Ibrahim; Wang, Xinhao; Liu, G Logan

2014-10-15

We have implemented a multifunctional optofluidic sensor that can monitor changes in the refractive index and pressure of biofluid simultaneously and can detect free-solution molecular interaction in situ. In this Letter, we demonstrate two major improvements of this sensor proven by both simulation and experiments. One improvement is the broader measurement range of refractive index by making the diffraction grating with high-index polymer. The other improvement is the separation of refractive index sensing from opacity sensing by using the relative power ratio of diffraction orders. This simple, compact and low-cost multifunctional optofluidic sensor has the potential to be used for in situ biofluid monitoring.

Observation of acoustic Dirac-like cone and double zero refractive index

PubMed Central

Dubois, Marc; Shi, Chengzhi; Zhu, Xuefeng; Wang, Yuan; Zhang, Xiang

2017-01-01

Zero index materials where sound propagates without phase variation, holds a great potential for wavefront and dispersion engineering. Recently explored electromagnetic double zero index metamaterials consist of periodic scatterers whose refractive index is significantly larger than that of the surrounding medium. This requirement is fundamentally challenging for airborne acoustics because the sound speed (inversely proportional to the refractive index) in air is among the slowest. Here, we report the first experimental realization of an impedance matched acoustic double zero refractive index metamaterial induced by a Dirac-like cone at the Brillouin zone centre. This is achieved in a two-dimensional waveguide with periodically varying air channel that modulates the effective phase velocity of a high-order waveguide mode. Using such a zero-index medium, we demonstrated acoustic wave collimation emitted from a point source. For the first time, we experimentally confirm the existence of the Dirac-like cone at the Brillouin zone centre. PMID:28317927

Refractive index and absorption detector for liquid chromatography based on Fabry-Perot interferometry

DOEpatents

Yeung, E.S.; Woodruff, S.D.

1984-06-19

A refractive index and absorption detector are disclosed for liquid chromatography. It is based in part on a Fabry-Perot interferometer and is used for the improved detection of refractive index and absorption. It includes a Fabry-Perot interferometer having a normally fixed first partially reflecting mirror and a movable second partially reflecting mirror. A chromatographic flow-cell is positioned between the mirrors along the optical axis of a monochromatic laser beam passing through the interferometer. A means for deriving information about the interference fringes coming out of the interferometer is used with a mini-computer to compute the refractive index of the specimen injected into the flow cell. The minicomputer continuously scans the interferometer for continuous refractive index readings and outputs the continuous results of the scans on a chart recorder. The absorption of the specimen can concurrently be scanned by including a second optical path for an excitation laser which will not interfere with the first laser, but will affect the specimen so that absorption properties can be detected. By first scanning for the refractive index of the specimen, and then immediately adding the excitation laser and subsequently scanning for the refractive index again, the absorption of the specimen can be computed and recorded. 10 figs.

Refractive index and absorption detector for liquid chromatography based on Fabry-Perot interferometry

DOEpatents

Yeung, Edward S.; Woodruff, Steven D.

1984-06-19

A refractive index and absorption detector for liquid chromatography. It is based in part on a Fabry-Perot interferometer and is used for the improved detection of refractive index and absorption. It includes a Fabry-Perot interferometer having a normally fixed first partially reflecting mirror and a movable second partially reflecting mirror. A chromatographic flow-cell is positioned between the mirrors along the optical axis of a monochromatic laser beam passing through the interferometer. A means for deriving information about the interference fringes coming out of the interferometer is used with a mini-computer to compute the refractive index of the specimen injected into the flow cell. The minicomputer continuously scans the interferometer for continuous refractive index readings and outputs the continuous results of the scans on a chart recorder. The absorption of the specimen can concurrently be scanned by including a second optical path for an excitation laser which will not interfere with the first laser, but will affect the specimen so that absorption properties can be detected. By first scanning for the refractive index of the specimen, and then immediately adding the excitation laser and subsequently scanning for the refractive index again, the absorption of the specimen can be computed and recorded.

Refraction index sensor based on phase resonances in a subwavelength structure with double period.

PubMed

Skigin, Diana C; Lester, Marcelo

2016-10-01

In this paper, we numerically demonstrate a refraction index sensor based on phase resonance excitation in a subwavelength-slit structure with a double period. The sensor consists of a metal layer with subwavelength slots arranged in a bi-periodic form, separated from a high refraction index medium. Between the metallic structure and the incident medium, a dielectric waveguide is formed whose refraction index is going to be determined. Variations in the refraction index of the waveguide are detected as shifts in the peaks of transmitted intensity originated by resonant modes supported by the compound metallic structure. At normal incidence, the spectral position of these resonant peaks exhibits a linear or a quadratic dependence with the refraction index, which permits us to obtain the unknown refraction index value with a high precision for a wide range of wavelengths. Since the operating principle of the sensor is due to the morphological resonances of the slits' structure, this device can be scaled to operate in different wavelength ranges while keeping similar characteristics.

Towards a Negative Refractive Index in an Atomic System

NASA Astrophysics Data System (ADS)

Simmons, Zach; Brewer, Nick; Yavuz, Deniz

2014-05-01

The goal of our experiments is to obtain a negative index of refraction in the optical region of the spectrum using an atomic system. The concept of negative refraction, which was first predicted by Veselago more than four decades ago, has recently emerged as a very exciting field of science. Negative index materials exhibit many seemingly strange properties such as electromagnetic vectors forming a left-handed triad. A key potential application for these materials was discovered in 2000 when Pendry predicted that a slab with a negative refractive index can image objects with a resolution far better than the diffraction limit. Thus far, research in negative index materials has primarily focused on meta-materials. The fixed response and often large absorption of these engineered materials motivates our efforts to work in an atomic system. An atomic media offers the potential to be actively modified, for example by changing laser parameters, and can be tuned to cancel absorption. A doped crystal allows for high atomic densities compared to other atomic systems. So far we have identified a transition in such a material, Eu:YSO, as a candidate for these experiments and are performing spectroscopy on this material.

Evaluation of a flow cytometry method to determine size and real refractive index distributions in natural marine particle populations.

PubMed

Agagliate, Jacopo; Röttgers, Rüdiger; Twardowski, Michael S; McKee, David

2018-03-01

A flow cytometric (FC) method was developed to retrieve particle size distributions (PSDs) and real refractive index (n r ) information in natural waters. Geometry and signal response of the sensors within the flow cytometer (CytoSense, CytoBuoy b.v., Netherlands) were characterized to form a scattering inversion model based on Mie theory. The procedure produced a mesh of diameter and n r isolines where each particle is assigned the diameter and n r values of the closest node, producing PSDs and particle real refractive index distributions. The method was validated using polystyrene bead standards of known diameter and polydisperse suspensions of oil with known n r , and subsequently applied to natural samples collected across a broad range of UK shelf seas. FC PSDs were compared with independent PSDs produced from data of two LISST-100X instruments (type B and type C). PSD slopes and features were found to be consistent between the FC and the two LISST-100X instruments, but LISST concentrations were found in disagreement with FC concentrations and with each other. FC n r values were found to agree with expected refractive index values of typical marine particle components across all samples considered. The determination of particle size and refractive index distributions enabled by the FC method has potential to facilitate identification of the contribution of individual subpopulations to the bulk inherent optical properties and biogeochemical properties of the particle population.

Recovering fluorophore concentration profiles from confocal images near lateral refractive index step changes.

PubMed

Jonášová, Eleonóra Parelius; Bjørkøy, Astrid; Stokke, Bjørn Torger

2016-12-01

Optical aberrations due to refractive index mismatches occur in various types of microscopy due to refractive differences between the sample and the immersion fluid or within the sample. We study the effects of lateral refractive index differences by fluorescence confocal laser scanning microscopy due to glass or polydimethylsiloxane cuboids and glass cylinders immersed in aqueous fluorescent solution, thereby mimicking realistic imaging situations in the proximity of these materials. The reduction in fluorescence intensity near the embedded objects was found to depend on the geometry and the refractive index difference between the object and the surrounding solution. The observed fluorescence intensity gradients do not reflect the fluorophore concentration in the solution. It is suggested to apply a Gaussian fit or smoothing to the observed fluorescence intensity gradient and use this as a basis to recover the fluorophore concentration in the proximity of the refractive index step change. The method requires that the reference and sample objects have the same geometry and refractive index. The best results were obtained when the sample objects were also used for reference since small differences such as uneven surfaces will result in a different extent of aberration.

Variable Refractive Index Effects on Radiation in Semitransparent Scattering Multilayered Regions

NASA Technical Reports Server (NTRS)

Siegel, R.; Spuckler, C. M.

1993-01-01

A simple set of equations is derived for predicting the temperature distribution and radiative energy flow in a semitransparent layer consisting of an arbitrary number of laminated sublayers that absorb, emit, and scatter radiation. Each sublayer can have a different refractive index and optical thickness. The plane composite region is heated on each exterior side by a different amount of incident radiation. The results are for the limiting case where heat conduction within the layers is very small relative to radiative transfer, and is neglected. The interfaces are assumed diffuse, and all interface reflections are included in the analysis. The thermal behavior is readily calculated from the analytical expressions that are obtained. By using many sublayers, the analytical expressions provide the temperature distribution and heat flow for a diffusing medium with a continuously varying refractive index, including internal reflection effects caused by refractive index gradients. Temperature and heat flux results are given to show the effect of variations in refractive index and optical thickness through the multilayer laminate.

Refractive index sensing with Fano resonances in silicon oligomers

PubMed Central

Chong, Katie E.; Orton, Henry W.; Decker, Manuel; Miroshnichenko, Andrey E.; Brener, Igal; Kivshar, Yuri S.

2017-01-01

We demonstrate experimentally refractive index sensing with localized Fano resonances in silicon oligomers, consisting of six disks surrounding a central one of slightly different diameter. Owing to the low absorption and narrow Fano-resonant spectral features appearing as a result of the interference of the modes of the outer and the central disks, we demonstrate refractive index sensitivity of more than 150 nm RIU−1 with a figure of merit of 3.8. This article is part of the themed issue ‘New horizons for nanophotonics’. PMID:28220001

Patient age, refractive index of the corneal stroma, and outcomes of uneventful laser in situ keratomileusis.

PubMed

Patel, Sudi; Alió, Jorge L; Walewska, Anna; Amparo, Francisco; Artola, Alberto

2013-03-01

To determine the influence of age and the corneal stromal refractive index on the difference between the predicted and actual postoperative refractive error after laser in situ keratomileusis (LASIK) and whether the precision of outcomes could be improved by considering age and the refractive index. Vissum Instituto Oftalmologico de Alicante, Alicante, Spain. Case series. Flaps were created using a mechanical microkeratome. The stromal refractive index was measured using a VCH-1 refractometer after flap lifting. Refractive data were obtained 1, 3, and 6 months postoperatively. Uneventful LASIK was performed in 133 eyes. The mean age, refractive index, and applied corrections were 33.4 years ± 9.49 (SD), 1.368 ± 0.006, and -2.43 ± 3.36 diopters (D), respectively. The difference between the predicted and actual postoperative refractive error = 2.315-0.021 age-1.106 refractive index (F = 3.647, r = 0.254, P=.029; n = 109) at 1 month and = 11.820-0.023 age-7.976 refractive index (F = 3.392, r = 0.261, P=.022, n = 106) at 3 months. A correlation between the actual and calculated postoperative refraction improved from r = -0.178 (P=.064; n = 75) to r = -0.418 (P<.001) after considering the true refractive index 6 months postoperatively. The predicted outcomes of LASIK can be improved by inputting the refractive index of the individual corneal stroma. Unexpected outcomes (>0.50 D) of LASIK could be avoided by considering patient age and the refractive index and by adjusting the applied correction accordingly. Copyright © 2012 ASCRS and ESCRS. Published by Elsevier Inc. All rights reserved.

Enhancement of graphene visibility on transparent substrates by refractive index optimization.

PubMed

Gonçalves, Hugo; Alves, Luís; Moura, Cacilda; Belsley, Michael; Stauber, Tobias; Schellenberg, Peter

2013-05-20

Optical reflection microscopy is one of the main imaging tools to visualize graphene microstructures. Here is reported a novel method that employs refractive index optimization in an optical reflection microscope, which greatly improves the visibility of graphene flakes. To this end, an immersion liquid with a refractive index that is close to that of the glass support is used in-between the microscope lens and the support improving the contrast and resolution of the sample image. Results show that the contrast of single and few layer graphene crystals and structures can be enhanced by a factor of 4 compared to values commonly achieved with transparent substrates using optical reflection microscopy lacking refractive index optimization.

Determination of average refractive index of spin coated DCG films for HOE fabrication

NASA Technical Reports Server (NTRS)

Kim, T. J.; Campbell, Eugene W.; Kostuk, Raymond K.

1993-01-01

The refractive index of holographic emulsions is an important parameter needed for designing holographic optical elements (HOE's). Theoretical calculations of the accuracy required for the refractive index and thickness of emulsions needed to meet predetermined Bragg angle conditions are presented. A modified interferometric method is used to find average refractive index of the unexposed and the developed dichromated gelatin holographic films. Slanted transmission HOE's are designed considering the index and thickness variations, and used to verify the index measurement results. The Brewster angle method is used to measure surface index of the unexposed and the developed films. The differences between average index and surface index are discussed. Theoretical calculation of the effects of index variation on diffraction efficiency, and experimental results for index modulation variation caused by process changes are also presented.

Dirac directional emission in anisotropic zero refractive index photonic crystals.

PubMed

He, Xin-Tao; Zhong, Yao-Nan; Zhou, You; Zhong, Zhi-Chao; Dong, Jian-Wen

2015-08-14

A certain class of photonic crystals with conical dispersion is known to behave as isotropic zero-refractive-index medium. However, the discrete building blocks in such photonic crystals are limited to construct multidirectional devices, even for high-symmetric photonic crystals. Here, we show multidirectional emission from low-symmetric photonic crystals with semi-Dirac dispersion at the zone center. We demonstrate that such low-symmetric photonic crystal can be considered as an effective anisotropic zero-refractive-index medium, as long as there is only one propagation mode near Dirac frequency. Four kinds of Dirac multidirectional emitters are achieved with the channel numbers of five, seven, eleven, and thirteen, respectively. Spatial power combination for such kind of Dirac directional emitter is also verified even when multiple sources are randomly placed in the anisotropic zero-refractive-index photonic crystal.

Dirac directional emission in anisotropic zero refractive index photonic crystals

PubMed Central

He, Xin-Tao; Zhong, Yao-Nan; Zhou, You; Zhong, Zhi-Chao; Dong, Jian-Wen

2015-01-01

A certain class of photonic crystals with conical dispersion is known to behave as isotropic zero-refractive-index medium. However, the discrete building blocks in such photonic crystals are limited to construct multidirectional devices, even for high-symmetric photonic crystals. Here, we show multidirectional emission from low-symmetric photonic crystals with semi-Dirac dispersion at the zone center. We demonstrate that such low-symmetric photonic crystal can be considered as an effective anisotropic zero-refractive-index medium, as long as there is only one propagation mode near Dirac frequency. Four kinds of Dirac multidirectional emitters are achieved with the channel numbers of five, seven, eleven, and thirteen, respectively. Spatial power combination for such kind of Dirac directional emitter is also verified even when multiple sources are randomly placed in the anisotropic zero-refractive-index photonic crystal. PMID:26271208

Exploring vacuum birefringence based on a 100 PW laser and an x-ray free electron laser beam

NASA Astrophysics Data System (ADS)

Shen, Baifei; Bu, Zhigang; Xu, Jiancai; Xu, Tongjun; Ji, Liangliang; Li, Ruxin; Xu, Zhizhan

2018-04-01

Exploring vacuum birefringence with the station of extreme light at Shanghai Coherent Light Facility is considered. Laser pulses of intensity beyond 1023 W cm-2 are capable of polarizing the vacuum due to the ultra-strong electro-magnetic fields. The subtle difference of the vacuum refractive indexes along electric and magnetic fields leads to a birefringence effect for lights propagating through. The vacuum birefringence effect can now be captured by colliding a hard x-ray free electron laser (XFEL) beam with a high-power laser. The initial XFEL beam of pure linear polarization is predicated to gain a very small ellipticity after passing through the laser stimulated vacuum. Various interaction geometries are considered, showing that the estimated ellipticity lies between 1.8 × 10-10 and 10-9 for a 100 PW laser interacting with a 12.9 keV XFEL beam, approaching the threshold for todays’ polarity detection technique. The detailed experimental set-up is designed, including the polarimeter, the focusing compound refractive lens and the optical path. When taking into account the efficiencies of the x-ray instruments, it is found that about 10 polarization-flipped x-ray photons can be detected for a single shot for our design. Considering the background noise level, accumulating runs are necessary to obtain high confident measurement.

The refractive index in electron microscopy and the errors of its approximations.

PubMed

Lentzen, M

2017-05-01

In numerical calculations for electron diffraction often a simplified form of the electron-optical refractive index, linear in the electric potential, is used. In recent years improved calculation schemes have been proposed, aiming at higher accuracy by including higher-order terms of the electric potential. These schemes start from the relativistically corrected Schrödinger equation, and use a second simplified form, now for the refractive index squared, being linear in the electric potential. The second and higher-order corrections thus determined have, however, a large error, compared to those derived from the relativistically correct refractive index. The impact of the two simplifications on electron diffraction calculations is assessed through numerical comparison of the refractive index at high-angle Coulomb scattering and of cross-sections for a wide range of scattering angles, kinetic energies, and atomic numbers. Copyright © 2016 Elsevier B.V. All rights reserved.

Investigation of noise properties in grating-based x-ray phase tomography with reverse projection method

NASA Astrophysics Data System (ADS)

Bao, Yuan; Wang, Yan; Gao, Kun; Wang, Zhi-Li; Zhu, Pei-Ping; Wu, Zi-Yu

2015-10-01

The relationship between noise variance and spatial resolution in grating-based x-ray phase computed tomography (PCT) imaging is investigated with reverse projection extraction method, and the noise variances of the reconstructed absorption coefficient and refractive index decrement are compared. For the differential phase contrast method, the noise variance in the differential projection images follows the same inverse-square law with spatial resolution as in conventional absorption-based x-ray imaging projections. However, both theoretical analysis and simulations demonstrate that in PCT the noise variance of the reconstructed refractive index decrement scales with spatial resolution follows an inverse linear relationship at fixed slice thickness, while the noise variance of the reconstructed absorption coefficient conforms with the inverse cubic law. The results indicate that, for the same noise variance level, PCT imaging may enable higher spatial resolution than conventional absorption computed tomography (ACT), while ACT benefits more from degraded spatial resolution. This could be a useful guidance in imaging the inner structure of the sample in higher spatial resolution. Project supported by the National Basic Research Program of China (Grant No. 2012CB825800), the Science Fund for Creative Research Groups, the Knowledge Innovation Program of the Chinese Academy of Sciences (Grant Nos. KJCX2-YW-N42 and Y4545320Y2), the National Natural Science Foundation of China (Grant Nos. 11475170, 11205157, 11305173, 11205189, 11375225, 11321503, 11179004, and U1332109).

Decoupling the refractive index from the electrical properties of transparent conducting oxides via periodic superlattices.

PubMed

Caffrey, David; Norton, Emma; Coileáin, Cormac Ó; Smith, Christopher M; Bulfin, Brendan; Farrell, Leo; Shvets, Igor V; Fleischer, Karsten

2016-09-13

We demonstrate an alternative approach to tuning the refractive index of materials. Current methodologies for tuning the refractive index of a material often result in undesirable changes to the structural or optoelectronic properties. By artificially layering a transparent conducting oxide with a lower refractive index material the overall film retains a desirable conductivity and mobility while acting optically as an effective medium with a modified refractive index. Calculations indicate that, with our refractive index change of 0.2, a significant reduction of reflective losses could be obtained by the utilisation of these structures in optoelectronic devices. Beyond this, periodic superlattice structures present a solution to decouple physical properties where the underlying electronic interaction is governed by different length scales.

Effects of variability of X-ray binaries on the X-ray luminosity functions of Milky Way

NASA Astrophysics Data System (ADS)

Islam, Nazma; Paul, Biswajit

2016-08-01

The X-ray luminosity functions of galaxies have become a useful tool for population studies of X-ray binaries in them. The availability of long term light-curves of X-ray binaries with the All Sky X-ray Monitors opens up the possibility of constructing X-ray luminosity functions, by also including the intensity variation effects of the galactic X-ray binaries. We have constructed multiple realizations of the X-ray luminosity functions (XLFs) of Milky Way, using the long term light-curves of sources obtained in the 2-10 keV energy band with the RXTE-ASM. The observed spread seen in the value of slope of both HMXB and LMXB XLFs are due to inclusion of variable luminosities of X-ray binaries in construction of these XLFs as well as finite sample effects. XLFs constructed for galactic HMXBs in the luminosity range 1036-1039 erg/sec is described by a power-law model with a mean power-law index of -0.48 and a spread due to variability of HMXBs as 0.19. XLFs constructed for galactic LMXBs in the luminosity range 1036-1039 erg/sec has a shape of cut-off power-law with mean power-law index of -0.31 and a spread due to variability of LMXBs as 0.07.

Wave refraction in negative-index media: always positive and very inhomogeneous.

PubMed

Valanju, P M; Walser, R M; Valanju, A P

2002-05-06

We present the first treatment of the refraction of physical electromagnetic waves in newly developed negative index media (NIM), also known as left-handed media (LHM). The NIM dispersion relation implies that group fronts refract positively even when phase fronts refract negatively. This difference results in rapidly dispersing, very inhomogeneous waves. In fact, causality and finite signal speed always prevent negative wave signal (not phase) refraction. Earlier interpretations of phase refraction as "negative light refraction" and "light focusing by plane slabs" are therefore incorrect, and published NIM experiments can be explained without invoking negative signal refraction.

3D refractive index measurements of special optical fibers

NASA Astrophysics Data System (ADS)

Yan, Cheng; Huang, Su-Juan; Miao, Zhuang; Chang, Zheng; Zeng, Jun-Zhang; Wang, Ting-Yun

2016-09-01

A digital holographic microscopic chromatography-based approach with considerably improved accuracy, simplified configuration and performance stability is proposed to measure three dimensional refractive index of special optical fibers. Based on the approach, a measurement system is established incorporating a modified Mach-Zehnder interferometer and lab-developed supporting software for data processing. In the system, a phase projection distribution of an optical fiber is utilized to obtain an optimal digital hologram recorded by a CCD, and then an angular spectrum theory-based algorithm is adopted to extract the phase distribution information of an object wave. The rotation of the optic fiber enables the experimental measurements of multi-angle phase information. Based on the filtered back projection algorithm, a 3D refraction index of the optical fiber is thus obtained at high accuracy. To evaluate the proposed approach, both PANDA fibers and special elliptical optical fiber are considered in the system. The results measured in PANDA fibers agree well with those measured using S14 Refractive Index Profiler, which is, however, not suitable for measuring the property of a special elliptical fiber.

A Simple Method to Determine the Refractive Index of Glass.

ERIC Educational Resources Information Center

Mak, Se-yuen

1988-01-01

Describes an experiment for determining the refractive index. Discusses the experiment procedure and mathematical expression for calculating the index. Provides two geometrical diagrams and a graph for determining the index with a typical data. (YP)

Index of refraction engineering in five-level dressed interacting ground states atoms.

PubMed

Sagona-Stophel, Steven A; Weatherall, James Owen; Search, Christopher P

2011-08-15

We present a five-level atomic system in which the index of refraction of a probe laser can be enhanced or reduced below unity with vanishing absorption in the region between pairs of absorption and gain lines formed by dressing of the atoms with a control laser and rf/microwave fields. By weak incoherent pumping of the population into a single metastable state, one can create several narrow amplifying resonances. At frequencies between these gain lines and additional absorption lines, there exist regions of vanishing absorption but resonantly enhanced index of refraction. In Rb vapors with density N in units of cm(-3), we predict an index of refraction up to n≈√(1+1.2×10(-14)N) for the D1 line, which is more than an order of magnitude larger than other proposals for index of refraction enhancement. Furthermore, the index can be readily reduced below 1 by simply changing the sign of the probe or rf field detunings. This enhancement is robust with respect to homogeneous and inhomogeneous broadening. © 2011 Optical Society of America

Comparable change in stromal refractive index of cat and human corneas following blue-IRIS.

PubMed

Wozniak, Kaitlin T; Gearhart, Sara M; Savage, Daniel E; Ellis, Jonathan D; Knox, Wayne H; Huxlin, Krystel R

2017-05-01

Blue intratissue refractive index shaping (blue-IRIS) is a method with potential to correct ocular refraction noninvasively in humans. To date, blue-IRIS has only ever been applied to cat corneas and hydrogels. To test the comparability of refractive index change achievable in cat and human tissues, we used blue-IRIS to write identical phase gratings in ex vivo feline and human corneas. Femtosecond pulses (400 nm) were focused ? 300 ?? ? m below the epithelial surface of excised cat and human corneas and scanned to write phase gratings with lines ? 1 ?? ? m wide, spaced 5 ?? ? m apart, using a scan speed of 5 ?? mm / s . Additional cat corneas were used to test writing at 3 and 7 ?? mm / s in order to document speed dependence of the refractive index change magnitude. The first-order diffraction efficiency was immediately measured and used to calculate the refractive index change attained. Our data show that blue-IRIS induces comparable refractive index changes in feline and human corneas, an essential requirement for further developing its use as a clinical vision correction technique.

Comparable change in stromal refractive index of cat and human corneas following blue-IRIS

NASA Astrophysics Data System (ADS)

Wozniak, Kaitlin T.; Gearhart, Sara M.; Savage, Daniel E.; Ellis, Jonathan D.; Knox, Wayne H.; Huxlin, Krystel R.

2017-05-01

Blue intratissue refractive index shaping (blue-IRIS) is a method with potential to correct ocular refraction noninvasively in humans. To date, blue-IRIS has only ever been applied to cat corneas and hydrogels. To test the comparability of refractive index change achievable in cat and human tissues, we used blue-IRIS to write identical phase gratings in ex vivo feline and human corneas. Femtosecond pulses (400 nm) were focused ˜300 μm below the epithelial surface of excised cat and human corneas and scanned to write phase gratings with lines ˜1 μm wide, spaced 5 μm apart, using a scan speed of 5 mm/s. Additional cat corneas were used to test writing at 3 and 7 mm/s in order to document speed dependence of the refractive index change magnitude. The first-order diffraction efficiency was immediately measured and used to calculate the refractive index change attained. Our data show that blue-IRIS induces comparable refractive index changes in feline and human corneas, an essential requirement for further developing its use as a clinical vision correction technique.

Temperature independent refractive index measurement using a fiber Bragg grating on abrupt tapered tip

NASA Astrophysics Data System (ADS)

Gomes, André D.; Silveira, Beatriz; Warren-Smith, Stephen C.; Becker, Martin; Rothhardt, Manfred; Frazão, Orlando

2018-05-01

A fiber Bragg grating was inscribed in an abrupt fiber taper using a femtosecond laser and phase-mask interferometer. The abrupt taper transition allows to excite a broad range of guided modes with different effective refractive indices that are reflected at different wavelengths according to Bragg's law. The multimode-Bragg reflection expands over 30 nm in the telecom-C-band. This corresponds to a mode-field overlap of up to 30% outside of the fiber, making the device suitable for evanescent field sensing. Refractive index and temperature measurements are performed for different reflection peaks. Temperature independent refractive index measurements are achieved by considering the difference between the wavelength shifts of two measured reflection peaks. A minimum refractive index sensitivity of 16 ± 1 nm/RIU was obtained in a low refractive index regime (1.3475-1.3720) with low influence of temperature (-0.32 ± 0.06 pm/°C). The cross sensitivity for this structure is 2.0 × 10-5 RIU/°C. The potential for simultaneous measurement of refractive index and temperature is also studied.

Fiber optic refractive index sensor using optofluidic anti-resonant reflecting guidance

NASA Astrophysics Data System (ADS)

Gao, Ran; Lu, Danfeng; Cheng, Jin; Qi, Zhi-mei

2017-10-01

An optofluidic anti-resonant reflecting guidance has been proposed and experimental demonstrated for the measurement of liquid refractive index. Two micro-channels were fabricated for the delivery of the liquid sample in the hollow core photonic crystal fiber by using femtosecond laser micromachining, serving as an inlet and outlet. The refractive index can be detected by using the resonant condition of the Fabry-Perot resonator, which is interrogated through the wavelength shift and of the lossy dip in the transmission spectrum. The experimental results show that the sensitivity of up to 1328 nm/RIU is achieved for the refractive index in the range from 1.345 to 1.363 RIU, respectively. The proposed sensor appears to have potential applications of precise measurement in chemistry, medicine, and biology.

Suppression of Air Refractive Index Variations in High-Resolution Interferometry

PubMed Central

Lazar, Josef; Číp, Ondřej; Čížek, Martin; Hrabina, Jan; Buchta, Zdeněk

2011-01-01

The influence of the refractive index of air has proven to be a major problem on the road to improvement of the uncertainty in interferometric displacement measurements. We propose an approach with two counter-measuring interferometers acting as a combination of tracking refractometer and a displacement interferometer referencing the wavelength of the laser source to a mechanical standard made of a material with ultra-low thermal expansion. This technique combines length measurement within a specified range with measurement of the refractive index fluctuations in one axis. Errors caused by different position of the interferometer laser beam and air sensors are thus eliminated. The method has been experimentally tested in comparison with the indirect measurement of the refractive index of air in a thermal controlled environment. Over a 1 K temperature range an agreement on the level of 5 × 10−8 has been achieved. PMID:22164036

On-chip integrated optofluidic complex refractive index sensing using silicon photonic crystal nanobeam cavities.

PubMed

Zhang, Xingwang; Zhou, Guangya; Shi, Peng; Du, Han; Lin, Tong; Teng, Jinghua; Chau, Fook Siong

2016-03-15

Complex refractive index sensing is proposed and experimentally demonstrated in optofluidic sensors based on silicon photonic crystal nanobeam cavities. The sensitivities are 58 and 139 nm/RIU, respectively, for the real part (n) and the imaginary part (κ) of the complex refractive index, and the corresponding detection limits are 1.8×10(-5) RIU for n and 4.1×10(-6) RIU for κ. Moreover, the capability of the complex refractive index sensing method to detect the concentration composition of the ternary mixture is demonstrated without the surface immobilization of functional groups, which is impossible to realize with the conventional refractive index sensing scheme.

Decoupling the refractive index from the electrical properties of transparent conducting oxides via periodic superlattices

PubMed Central

Caffrey, David; Norton, Emma; Coileáin, Cormac Ó; Smith, Christopher M.; Bulfin, Brendan; Farrell, Leo; Shvets, Igor V.; Fleischer, Karsten

2016-01-01

We demonstrate an alternative approach to tuning the refractive index of materials. Current methodologies for tuning the refractive index of a material often result in undesirable changes to the structural or optoelectronic properties. By artificially layering a transparent conducting oxide with a lower refractive index material the overall film retains a desirable conductivity and mobility while acting optically as an effective medium with a modified refractive index. Calculations indicate that, with our refractive index change of 0.2, a significant reduction of reflective losses could be obtained by the utilisation of these structures in optoelectronic devices. Beyond this, periodic superlattice structures present a solution to decouple physical properties where the underlying electronic interaction is governed by different length scales. PMID:27623228

A Multi-D-Shaped Optical Fiber for Refractive Index Sensing

PubMed Central

Chen, Chien-Hsing; Tsao, Tzu-Chein; Tang, Jaw-Luen; Wu, Wei-Te

2010-01-01

A novel class of multi-D-shaped optical fiber suited for refractive index measurements is presented. The multi-D-shaped optical fiber was constructed by forming several D-sections in a multimode optical fiber at localized regions with femtosecond laser pulses. The total number of D-shaped zones fabricated could range from three to seven. Each D-shaped zone covered a sensor volume of 100 μm depth, 250 μm width, and 1 mm length. The mean roughness of the core surface obtained by the AFM images was 231.7 nm, which is relatively smooth. Results of the tensile test indicated that the fibers have sufficient mechanical strength to resist damage from further processing. The multi-D-shaped optical fiber as a high sensitive refractive-index sensor to detect changes in the surrounding refractive index was studied. The results for different concentrations of sucrose solution show that a resolution of 1.27 × 10−3–3.13 × 10−4 RIU is achieved for refractive indices in the range of 1.333 to 1.403, suggesting that the multi-D-shaped fibers are attractive for chemical, biological, and biochemical sensing with aqueous solutions. PMID:22399908

Refractive Index Enhancement in Gases

DTIC Science & Technology

2012-02-29

Associate Professor Deniz D. Yavuz Graduate Ph. D. Students: Nick Proite, Tyler Green, Dan Sikes, Zach Simmons, and Jared Miles Se. TASK NUMBER Sf...NUMBER OF PAGES 8 19a. NAME OF RESPONSIBLE PERSON Assoc. Prof. Deniz D. Yavuz 19b. TELEPHONE NUMBER (Include area code) Reset 608-263-9399...Refractive Index Enhancement in Gases Grant/Contract Number: FA9550-09-1-0124 Program Manager: Tatjana Curcic Principal Investigator: Deniz D. Yavuz Our

Refractive index and birefringence of 2H silicon carbide

NASA Technical Reports Server (NTRS)

Powell, J. A.

1972-01-01

The refractive indices of 2H SiC were measured over the wavelength range 435.8 to 650.9 nm by the method of minimum deviation. At the wavelength lambda = 546.1 nm, the ordinary index n sub 0 was 2.6480 and the extraordinary index n sub e was 2.7237. The estimated error (standard deviation) in the measured values is 0.0006 for n sub 0 and 0.0009 for n sub e. The experimental data were curve fitted to the Cauchy equation for the index of refraction as a function of wavelength. The birefringence of 2H SiC was found to vary from 0.0719 at lambda = 650.9 nm to 0.0846 at lambda = 435.8 nm.

Soft x-ray holographic tomography for biological specimens

NASA Astrophysics Data System (ADS)

Gao, Hongyi; Chen, Jianwen; Xie, Honglan; Li, Ruxin; Xu, Zhizhan; Jiang, Shiping; Zhang, Yuxuan

2003-10-01

In this paper, we present some experimental results on X -ray holography, holographic tomography, and a new holographic tomography method called pre-amplified holographic tomography is proposed. Due to the shorter wavelength and the larger penetration depths, X-rays provide the potential of higher resolution in imaging techniques, and have the ability to image intact, living, hydrated cells w ithout slicing, dehydration, chemical fixation or stain. Recently, using X-ray source in National Synchrotron Radiation Laboratory in Hefei, we have successfully performed some soft X-ray holography experiments on biological specimen. The specimens used in the experiments was the garlic clove epidermis, we got their X-ray hologram, and then reconstructed them by computer programs, the feature of the cell walls, the nuclei and some cytoplasm were clearly resolved. However, there still exist some problems in realization of practical 3D microscopic imaging due to the near-unity refractive index of the matter. There is no X-ray optics having a sufficient high numerical aperture to achieve a depth resolution that is comparable to the transverse resolution. On the other hand, computer tomography needs a record of hundreds of views of the test object at different angles for high resolution. This is because the number of views required for a densely packed object is equal to the object radius divided by the desired depth resolution. Clearly, it is impractical for a radiation-sensitive biological specimen. Moreover, the X-ray diffraction effect makes projection data blur, this badly degrades the resolution of the reconstructed image. In order to observe 3D structure of the biological specimens, McNulty proposed a new method for 3D imaging called "holographic tomography (HT)" in which several holograms of the specimen are recorded from various illumination directions and combined in the reconstruction step. This permits the specimens to be sampled over a wide range of spatial

High-sensitivity refractive index sensor based on large-angle tilted fiber grating with carbon nanotube deposition

NASA Astrophysics Data System (ADS)

Badmos, Abdulyezir A.; Sun, Qizhen; Yan, Zhijun; Arif, Raz N.; Zhang, Junxi; Rozhin, Alex; Zhang, Lin

2016-04-01

This paper presents a highly sensitive ambient refractive index (RI) sensor based on 81° tilted fiber grating (81°-TFG) structure UV-inscribed in standard telecom fiber (62.5μm cladding radius) with carbon nanotube (CNT) overlay deposition. The sensing mechanism is based on the ability of CNT to induce change in transmitted optical power and the high sensitivity of 81°-TFG to ambient refractive index. The thin CNT film with high refractive index enhances the cladding modes of the TFG, resulting in the significant interaction between the propagating light and the surrounding medium. Consequently, the surrounding RI change will induce not only the resonant wavelength shift but also the power intensity change of the attenuation band in the transmission spectrum. Result shows that the change in transmitted optical power produces a corresponding linear reduction in intensity with increment in RI values. The sample shows high sensitivities of 207.38nm/RIU, 241.79nm/RIU at RI range 1.344-1.374 and 113.09nm/RIU, 144.40nm/RIU at RI range 1.374-1.392 (for X-pol and Y-pol respectively). It also shows power intensity sensitivity of 65.728dBm/RIU and 45.898 (for X-pol and Y-pol respectively). The low thermal sensitivity property of the 81°-TFG offers reduction in thermal cross-sensitivity and enhances specificity of the sensor.

Validation of Ray Tracing Code Refraction Effects

NASA Technical Reports Server (NTRS)

Heath, Stephanie L.; McAninch, Gerry L.; Smith, Charles D.; Conner, David A.

2008-01-01

NASA's current predictive capabilities using the ray tracing program (RTP) are validated using helicopter noise data taken at Eglin Air Force Base in 2007. By including refractive propagation effects due to wind and temperature, the ray tracing code is able to explain large variations in the data observed during the flight test.

Frequency comb calibrated frequency-sweeping interferometry for absolute group refractive index measurement of air.

PubMed

Yang, Lijun; Wu, Xuejian; Wei, Haoyun; Li, Yan

2017-04-10

The absolute group refractive index of air at 194061.02 GHz is measured in real time using frequency-sweeping interferometry calibrated by an optical frequency comb. The group refractive index of air is calculated from the calibration peaks of the laser frequency variation and the interference signal of the two beams passing through the inner and outer regions of a vacuum cell when the frequency of a tunable external cavity diode laser is scanned. We continuously measure the refractive index of air for 2 h, which shows that the difference between measured results and Ciddor's equation is less than 9.6×10^-8, and the standard deviation of that difference is 5.9×10^-8. The relative uncertainty of the measured refractive index of air is estimated to be 8.6×10^-8. The data update rate is 0.2 Hz, making it applicable under conditions in which air refractive index fluctuates fast.

Proposal to Produce Novel, Transparent Radiation Hard Low Refractive Index

DTIC Science & Technology

1994-02-09

or ainy nht.at NX ftU 1.AECY USE a EP....3RFPfT TYP’E AND DATES~ COV-ERED-- 4. TITLE AND SUBTITLE . . FjUNDING NUMBERS PROPOSAL TO PRODUCE NOVEL...cladding use . our research resulted in identifying a radiation hard, low refractive index polymer, poly (heptafluorobutyl methacrylate), P(MFBM) as the best...candidate for a novel ~. cladding material. P(HFB) has a refractive index of 1.387. When used to clada styrene core, the theoretical light propagation

Characterization of a novel ultra low refractive index material for biosensor application

PubMed Central

Memisevic, Jasenka; Korampally, Venumadhav; Gangopadhyay, Shubhra; Grant, Sheila A.

2009-01-01

Nanoporous materials can provide significant benefits to the field of biosensors. Their size and porous structure makes them an ideal tool for improving sensor performance. This study characterized a novel ultra low index of refraction nanoporous organosilicate (NPO) material for use as an optical platform for fluorescence-based optical biosensors. While serving as the low index cladding material, the novel coating based on organosilicate nanoparticles also provides an opportunity for a high surface area coating that can be utilized for immobilizing biological probes. Biological molecules were immobilized onto NPO, which was spin-coated on silicon and glass substrates. The biological molecule was composed of Protein A conjugated to AlexaFluor 546 fluorophore and then immobilized onto the NPO substrate via silanization. Sample analysis consisted of spectrofluorometry, FT-IR spectroscopy, scanning electron microscopy, contact angle measurement and ellipsometry. The results showed the presence of emission peaks at 574 nm, indicating that the immobilization of Protein A to the NPO material is possible. When compared to Si and glass substrates not coated with NPO, the results showed a 100X and 10X increase in packing density with the NPO coated films respectively. Ellipsometric analysis, FT-IR, contact angle, and SEM imaging of the surface immobilized NPO films suggested that while the surface modifications did induce some damage, it did not incur significant changes to its unique characteristics, i.e., pore structure, wettability and index of refraction. It was concluded that NPO films would be a viable sensor substrate to enhance sensitivity and improve sensor performance. PMID:20161155

Nondestructive measurement of the refractive index distribution of a glass molded lens by two-wavelength wavefronts.

PubMed

Sugimoto, Tomohiro

2016-10-01

This paper presents a nondestructive and non-exact-index-matching method for measuring the refractive index distribution of a glass molded lens with high refractivity. The method measures two-wavelength wavefronts of a test lens immersed in a liquid with a refractive index dispersion different from that of the test lens and calculates the refractive index distribution by eliminating the refractive index distribution error caused by the shape error of the test lens. The estimated uncertainties of the refractive index distributions of test lenses with n_d≈1.77 and n_d≈1.85 were 1.9×10^-5  RMS and 2.4×10^-5  RMS, respectively. I validated the proposed method by evaluating the agreement between the estimated uncertainties and experimental values.

Determining the Thickness and Refractive Index of a Mirror

ERIC Educational Resources Information Center

Uysal, Ahmet

2010-01-01

When a laser beam reflects from a back surface glass mirror and falls on a screen, a pattern of discrete bright spots is created by partial reflection and refraction of the light at the air-glass interface and reflection at the mirror surface (Fig. 1). This paper explains how this phenomenon can be used to determine the refractive index and the…

High Sensitivity Refractive Index Sensor Based on Dual-Core Photonic Crystal Fiber with Hexagonal Lattice.

PubMed

Wang, Haiyang; Yan, Xin; Li, Shuguang; An, Guowen; Zhang, Xuenan

2016-10-08

A refractive index sensor based on dual-core photonic crystal fiber (PCF) with hexagonal lattice is proposed. The effects of geometrical parameters of the PCF on performances of the sensor are investigated by using the finite element method (FEM). Two fiber cores are separated by two air holes filled with the analyte whose refractive index is in the range of 1.33-1.41. Numerical simulation results show that the highest sensitivity can be up to 22,983 nm/RIU(refractive index unit) when the analyte refractive index is 1.41. The lowest sensitivity can reach to 21,679 nm/RIU when the analyte refractive index is 1.33. The sensor we proposed has significant advantages in the field of biomolecule detection as it provides a wide-range of detection with high sensitivity.

Development and characterization of high refractive index and high scattering acrylate polymer layers

NASA Astrophysics Data System (ADS)

Eiselt, Thomas; Gomard, Guillaume; Preinfalk, Jan; Gleißner, Uwe; Lemmer, Uli; Hanemann, Thomas

2016-11-01

In this work, we develop a wet-processable scattering layer exhibiting a high refractive index that can be used in organic light-emitting diodes for light outcoupling purposes. The composite layers contain an acrylate casting resin, benzylmethacrylate, and phenanthrene, which is employed to increase the refractive index. The mixtures are first rheologically characterized and then polymerized with heat and UV radiation. For the refractive index measurements, the polymerized samples require a planar surface without air bubbles. To produce flat samples, a special construction consisting of a glass plate, a teflon sheet, a silicone ring (PDMS mold), another teflon sheet, and another glass plate is developed. Glue clamps are used to hold the construction together. The refractive index of the samples can be increased from 1.565 to 1.585 at 20°C at a wavelength of 589 nm following the addition of 20 wt% phenanthrene. A master mixture with a high refractive index is taken for further experiments. Nanoscaled titanium dioxide is added and dispersed into the master mixture and then spin coated on a glass substrate. These layers are optically characterized. Most of the presented layers present the expected haze of over 50%.

Direct Electrospray Printing of Gradient Refractive Index Chalcogenide Glass Films.

PubMed

Novak, Spencer; Lin, Pao Tai; Li, Cheng; Lumdee, Chatdanai; Hu, Juejun; Agarwal, Anuradha; Kik, Pieter G; Deng, Weiwei; Richardson, Kathleen

2017-08-16

A spatially varying effective refractive index gradient using chalcogenide glass layers is printed on a silicon wafer using an optimized electrospray (ES) deposition process. Using solution-derived glass precursors, IR-transparent Ge 23 Sb 7 S 70 and As 40 S 60 glass films of programmed thickness are fabricated to yield a bilayer structure, resulting in an effective gradient refractive index (GRIN) film. Optical and compositional analysis tools confirm the optical and physical nature of the gradient in the resulting high-optical-quality films, demonstrating the power of direct printing of multimaterial structures compatible with planar photonic fabrication protocols. The potential application of such tailorable materials and structures as they relate to the enhancement of sensitivity in chalcogenide glass based planar chemical sensor device design is presented. This method, applicable to a broad cross section of glass compositions, shows promise in directly depositing GRIN films with tunable refractive index profiles for bulk and planar optical components and devices.

Numerical study on refractive index sensor based on hybrid-plasmonic mode

NASA Astrophysics Data System (ADS)

Yun, Jeong-Geun; Kim, Joonsoo; Lee, Kyookeun; Lee, Yohan; Lee, Byoungho

2017-04-01

We propose a highly sensitive hybrid-plasmonic sensor based on thin-gold nanoslit arrays. The transmission characteristics of gold nanoslit arrays are analyzed as changing the thickness of gold layer. The surface plasmon polariton mode excited on the sensing medium, which is sensitive to refractive index change of the sensing medium, is strengthened by reducing the thickness of the gold layer. A design rule is suggested that steeper dispersion curve of the surface plasmon polariton mode leads to higher sensitivity. For the dispersion engineering, hybrid-plasmonic structure, which consists of thin-gold nanoslit arrays, sensing region and high refractive index dielectric space is introduced. The proposed sensor structure with period of 700 nm shows the improved sensitivity up to 1080 nm/RIU (refractive index unit), and the surface sensitivity is extremely enhanced.

Broadband giant-refractive-index material based on mesoscopic space-filling curves

NASA Astrophysics Data System (ADS)

Chang, Taeyong; Kim, Jong Uk; Kang, Seung Kyu; Kim, Hyowook; Kim, Do Kyung; Lee, Yong-Hee; Shin, Jonghwa

2016-08-01

The refractive index is the fundamental property of all optical materials and dictates Snell's law, propagation speed, wavelength, diffraction, energy density, absorption and emission of light in materials. Experimentally realized broadband refractive indices remain <40, even with intricately designed artificial media. Herein, we demonstrate a measured index >1,800 resulting from a mesoscopic crystal with a dielectric constant greater than three million. This gigantic enhancement effect originates from the space-filling curve concept from mathematics. The principle is inherently very broad band, the enhancement being nearly constant from zero up to the frequency of interest. This broadband giant-refractive-index medium promises not only enhanced resolution in imaging and raised fundamental absorption limits in solar energy devices, but also compact, power-efficient components for optical communication and increased performance in many other applications.

Refractive index sensor based on plastic optical fiber with tapered structure.

PubMed

De-Jun, Feng; Guan-Xiu, Liu; Xi-Lu, Liu; Ming-Shun, Jiang; Qing-Mei, Sui

2014-04-01

This work reports a refractive index sensor made of plastic optical fiber (POF) with tapered structure. Transmission loss is measured when the external environment's refractive index changes from 1.33 to 1.41. Three wavelengths (532, 633, and 780 nm) are used to evaluate the sensitivity of the sensor, and results indicate that 633 nm is the best sensing wavelength due to the increased levels of sensitivity achieved at this wavelength. A biconical sensing structure is designed to enhance the sensitivity of the sensor. A sensitivity of 950 μW/RIU at 633 nm is obtained for a biconical sensing structure when launched power is 1 mW. Due to its sensitivity to the refractive index and simple construction, POF with tapered structure has potential applications in the biosensing field.

Photoacoustic measurement of refractive index of dye solutions and myoglobin for biosensing applications

PubMed Central

Goldschmidt, Benjamin S.; Mehta, Smit; Mosley, Jeff; Walter, Chris; Whiteside, Paul J. D.; Hunt, Heather K.; Viator, John A.

2013-01-01

Current methods of determining the refractive index of chemicals and materials, such as ellipsometry and reflectometry, are limited by their inability to analyze highly absorbing or highly transparent materials, as well as the required prior knowledge of the sample thickness and estimated refractive index. Here, we present a method of determining the refractive index of solutions using the photoacoustic effect. We show that a photoacoustic refractometer can analyze highly absorbing dye samples to within 0.006 refractive index units of a handheld optical refractometer. Further, we use myoglobin, an early non-invasive biomarker for malignant hyperthermia, as a proof of concept that this technique is applicable for use as a medical diagnostic. Comparison of the speed, cost, simplicity, and accuracy of the techniques shows that this photoacoustic method is well-suited for optically complex systems. PMID:24298407

Laser interferometry of the hydrolytic changes in protein solutions: the refractive index and hydration shells.

PubMed

Sarimov, R M; Matveyeva, T A; Binhi, V N

2018-05-11

Using an original laser interferometer of enhanced sensitivity, an increase in the refractive index of a protein solution was observed during the reaction of proteolysis catalyzed by pepsin. The increase in the refractive index of the protein solution at a concentration of 4 mg/ml was [Formula: see text] for bovine serum albumin and [Formula: see text] for lysozyme. The observed effect disproves the existing idea that the refractive index of protein solutions is determined only by their amino acid composition and concentration. It is shown that the refractive index also depends on the state of protein fragmentation. A mathematical model of proteolysis and a real-time method for estimating the state of protein hydration based on the measurement of refractive index during the reaction are proposed. A good agreement between the experimental and calculated time dependences of the refractive index shows that the growth of the surface of protein fragments and the change in the number of hydration cavities during proteolysis can be responsible for the observed effect.

Reflectivity of a disordered monolayer estimated by graded refractive index and scattering models.

PubMed

Diamant, Ruth; Garcí-Valenzuela, Augusto; Fernández-Guasti, Manuel

2012-09-01

Reflectivity of a random monolayer, consisting of transparent spherical particles, is estimated using a graded refractive index model, an effective medium approach, and two scattering models. Two cases, a self-standing film and one with a substrate, are considered. Neither the surrounding medium nor the substrate are absorbing materials. Results at normal incidence, with different particle sizes, covering ratios and refractive indexes, are compared. The purpose of this work is to find under which circumstances, for reflectivity at normal incidence, a particle monolayer behaves as a graded refractive index film.

A FORTRAN Program for Computing Refractive Index Using the Double Variation Method.

ERIC Educational Resources Information Center

Blanchard, Frank N.

1984-01-01

Describes a computer program which calculates a best estimate of refractive index and dispersion from a large number of observations using the double variation method of measuring refractive index along with Sellmeier constants of the immersion oils. Program listing with examples will be provided on written request to the author. (Author/JM)

Plasmonic Waveguide Coupled Ring Cavity for a Non-Resonant Type Refractive Index Sensor.

PubMed

Kwon, Soon-Hong

2017-11-03

Sensitive refractive index sensors with small footprints have been studied to allow the integration of a large number of sensors into a tiny chip for bio/chemical applications. In particular, resonant-type index sensors based on various micro/nanocavities, which use a resonant wavelength dependence on the refractive index of the analyte, have been developed. However, the spectral linewidth of the resonance, which becomes the resolution limit, is considerably large in plasmonic cavities due to the large absorption loss of metals. Therefore, there is demand for a new type of plasmonic refractive index sensor that is not limited by the linewidth of the cavity. We propose a new type of plasmonic index sensors consisting of a channel waveguide and a ring cavity. Two emissions from the ring cavity in both directions of the waveguide couple with a reflection phase difference depending on the length of a closed right arm with a reflecting boundary. Therefore, the output power dramatically and sensitively changes as a function of the refractive index of the analyte filling the waveguide.

Plasmonic Waveguide Coupled Ring Cavity for a Non-Resonant Type Refractive Index Sensor

PubMed Central

Kwon, Soon-Hong

2017-01-01

Sensitive refractive index sensors with small footprints have been studied to allow the integration of a large number of sensors into a tiny chip for bio/chemical applications. In particular, resonant-type index sensors based on various micro/nanocavities, which use a resonant wavelength dependence on the refractive index of the analyte, have been developed. However, the spectral linewidth of the resonance, which becomes the resolution limit, is considerably large in plasmonic cavities due to the large absorption loss of metals. Therefore, there is demand for a new type of plasmonic refractive index sensor that is not limited by the linewidth of the cavity. We propose a new type of plasmonic index sensors consisting of a channel waveguide and a ring cavity. Two emissions from the ring cavity in both directions of the waveguide couple with a reflection phase difference depending on the length of a closed right arm with a reflecting boundary. Therefore, the output power dramatically and sensitively changes as a function of the refractive index of the analyte filling the waveguide. PMID:29099740

X-ray based displacement and strain measurements for hostile environments

NASA Technical Reports Server (NTRS)

Canistraro, Howard A.; Jordan, Eric H.; Pease, Douglas M.

1993-01-01

A completely new method of non-contacting, hostile environment displacement and strain measurement based on the focus and scanning of x-rays, has been developed and demonstrated. The new technique has the ability to overcome many of the limitations associated with available methods. The system is based on the focus and scanning of low energy, hard x-rays such as those emanating from table top copper or molybdenum sources. The x-rays are focused into a narrow and intense line image which can be swept onto targets that fluoresce secondary x-ray radiation. By monitoring the secondary radiation intensity and comparing it with the focused x-ray image's position as it is swept over the target edge, the position of the target edge relative to the focused image can be determined. The present system has a resolution of 0.5 micron, which has been shown to be limited by bearing backlash (or 'yaw' error) in the linear translation table. Its use has been demonstrated in the presence of an open flame with a resultant target temperature in excess of 2000 degrees Fahrenheit (1000 degrees Celsius). Strain measurements have been conducted in a laboratory environment at both room temperature and at a specimen temperature of 1300 degrees Fahrenheit, with an accuracy of within 20 microstrain (primarily a function of the 0.5 micron resolution limit). The main advantage of the technique lies in the penetrating, non-refractive nature of x-rays, which are virtually immune to the presence of refracting gas layers, smoke, flame or intense thermal radiation.

Tunable Liquid Gradient Refractive Index (L-GRIN) lens with two degrees of freedom.

PubMed

Mao, Xiaole; Lin, Sz-Chin Steven; Lapsley, Michael Ian; Shi, Jinjie; Juluri, Bala Krishna; Huang, Tony Jun

2009-07-21

We report a tunable optofluidic microlens configuration named the Liquid Gradient Refractive Index (L-GRIN) lens for focusing light within a microfluidic device. The focusing of light was achieved through the gradient refractive index (GRIN) within the liquid medium, rather than via curved refractive lens surfaces. The diffusion of solute (CaCl(2)) between side-by-side co-injected microfluidic laminar flows was utilized to establish a hyperbolic secant (HS) refractive index profile to focus light. Tailoring the refractive index profile by adjusting the flow conditions enables not only tuning of the focal distance (translation mode), but also shifting of the output light direction (swing mode), a second degree of freedom that to our knowledge has yet to be accomplished for in-plane tunable microlenses. Advantages of the L-GRIN lens also include a low fluid consumption rate, competitive focusing performance, and high compatibility with existing microfluidic devices. This work provides a new strategy for developing integrative tunable microlenses for a variety of lab-on-a-chip applications.

Analyzing refractive index profiles of confined fluids by interferometry.

PubMed

Kienle, Daniel F; Kuhl, Tonya L

2014-12-02

This work describes an interferometry data analysis method for determining the optical thickness of thin films or any variation in the refractive index of a fluid or film near a surface. In particular, the method described is applied to the analysis of interferometry data taken with a surface force apparatus (SFA). The technique does not require contacting or confining the fluid or film. By analyzing interferometry data taken at many intersurface separation distances out to at least 300 nm, the properties of a film can be quantitatively determined. The film can consist of material deposited on the surface, like a polymer brush, or variation in a fluid's refractive index near a surface resulting from, for example, a concentration gradient, depletion in density, or surface roughness. The method is demonstrated with aqueous polyethylenimine (PEI) adsorbed onto mica substrates, which has a large concentration and therefore refractive index gradient near the mica surface. The PEI layer thickness determined by the proposed method is consistent with the thickness measured by conventional SFA methods. Additionally, a thorough investigation of the effects of random and systematic error in SFA data analysis and modeling via simulations of interferometry is described in detail.

Nanostructured crystals of fluorite phases Sr1 - x R x F2 + x ( R = Y, La-Lu) and their ordering: Part III. A study of the refractive indices

NASA Astrophysics Data System (ADS)

Glushkova, T. M.; Karimov, D. N.; Krivandina, E. A.; Zhmurova, Z. I.; Sobolev, B. P.

2009-07-01

The refractive indices n of Sr1 - x R x F2 + x crystals ( R = Y, La-Lu; 0 ≤ x ≤ 0.5) have been measured at wavelengths of 0.436, 0.546, and 0.589 μm. It is established that n increases when there is an increase in the RF3 content x according to a weakly quadratic law for each R. For the isoconcentration series of Sr0.9 R 0.1F2.1 crystals, the change in n in the series of rare earth elements has a pronounced nonlinear character, which reflects the nonmonotonous change in the properties of compounds in the R series. It is shown that the method of molecular refraction additivity can be used to calculate n for Sr1 - x R x F2 + x crystals. By varying the RF3 content in them, one can obtain optical media with a gradually varied refractive index n in the range 1.44-1.55, thus filling the gap in the n values between high ones for RF3 crystals and low ones for crystals of alkaline earth fluorides MF2.

The effect of UV irradiation on the refractive index modulation in photo-thermo-refractive glasses: Mechanisms and application

NASA Astrophysics Data System (ADS)

Chernakov, Dmitry I.; Sidorov, Alexander I.; Stolyarchuk, Maxim V.; Kozlova, Darya A.; Krykova, Victoria A.; Nikonorov, Nikolay V.

2018-02-01

It is shown experimentally that in photo-thermo-refractive glasses the transformation of charged silver subnanosized molecular clusters to neutral state by UV irradiation results in the increase of glass refractive index. The increment of the refractive index reaches Δn = 0.76·10-4. Computer simulation has shown that the polarizability of neutral molecular clusters is by 20-40% larger than of charged ones. The reason of this is the increase of electron density and volume of electron density surfaces during the transformation of molecular cluster to the neutral state. The transition molecular cluster from the ground state to the excited state also results in the increase of its polarizability.

High Sensitivity Refractive Index Sensor Based on Dual-Core Photonic Crystal Fiber with Hexagonal Lattice

PubMed Central

Wang, Haiyang; Yan, Xin; Li, Shuguang; An, Guowen; Zhang, Xuenan

2016-01-01

A refractive index sensor based on dual-core photonic crystal fiber (PCF) with hexagonal lattice is proposed. The effects of geometrical parameters of the PCF on performances of the sensor are investigated by using the finite element method (FEM). Two fiber cores are separated by two air holes filled with the analyte whose refractive index is in the range of 1.33–1.41. Numerical simulation results show that the highest sensitivity can be up to 22,983 nm/RIU(refractive index unit) when the analyte refractive index is 1.41. The lowest sensitivity can reach to 21,679 nm/RIU when the analyte refractive index is 1.33. The sensor we proposed has significant advantages in the field of biomolecule detection as it provides a wide-range of detection with high sensitivity. PMID:27740607

The Complex Refractive Index of Volcanic Ash Aerosol Retrieved From Spectral Mass Extinction

NASA Astrophysics Data System (ADS)

Reed, Benjamin E.; Peters, Daniel M.; McPheat, Robert; Grainger, R. G.

2018-01-01

The complex refractive indices of eight volcanic ash samples, chosen to have a representative range of SiO2 contents, were retrieved from simultaneous measurements of their spectral mass extinction coefficient and size distribution. The mass extinction coefficients, at 0.33-19 μm, were measured using two optical systems: a Fourier transform spectrometer in the infrared and two diffraction grating spectrometers covering visible and ultraviolet wavelengths. The particle size distribution was measured using a scanning mobility particle sizer and an optical particle counter; values for the effective radius of ash particles measured in this study varied from 0.574 to 1.16 μm. Verification retrievals on high-purity silica aerosol demonstrated that the Rayleigh continuous distribution of ellipsoids (CDEs) scattering model significantly outperformed Mie theory in retrieving the complex refractive index, when compared to literature values. Assuming the silica particles provided a good analogue of volcanic ash, the CDE scattering model was applied to retrieve the complex refractive index of the eight ash samples. The Lorentz formulation of the complex refractive index was used within the retrievals as a convenient way to ensure consistency with the Kramers-Kronig relation. The short-wavelength limit of the electric susceptibility was constrained by using independently measured reference values of the complex refractive index of the ash samples at a visible wavelength. The retrieved values of the complex refractive indices of the ash samples showed considerable variation, highlighting the importance of using accurate refractive index data in ash cloud radiative transfer models.

Photo-oxidation-modulated refractive index in Bi2Te3 thin films

NASA Astrophysics Data System (ADS)

Yue, Zengji; Chen, Qinjun; Sahu, Amit; Wang, Xiaolin; Gu, Min

2017-12-01

We report on an 800 nm femtosecond laser beam induced giant refractive index modulation and enhancement of near-infrared transparency in topological insulator material Bi2Te3 thin films. An ultrahigh refractive index of up to 5.9 was observed in the Bi2Te3 thin film in near-infrared frequency. The refractive index dramatically decreases by a factor of ~3 by an exposure to the 800 nm femtosecond laser beam. Simultaneously, the transmittance of the Bi2Te3 thin films markedly increases to ~96% in the near-infrared frequency. The Raman spectra provides strong evidences that the observed both refractive index modulation and transparency enhancement result from laser beam induced photooxidation effects in the Bi2Te3 thin films. The Bi2Te3 compound transfers into Bi2O3 and TeO2 under the laser beam illumination. These experimental results pave the way towards the design of various optical devices, such as near-infrared flat lenses, waveguide and holograms, based on topological insulator materials.

Nonscanning Moiré deflectometry for measurement of nonlinear refractive index and absorption coefficient of liquids.

PubMed

Farahani, Shahrzad Shahrabi; Madanipour, Khosro; Koohian, Ata

2017-05-01

In this work, a nonscanning measurement technique is presented for determining the nonlinear refractive index and absorption coefficient of liquid media based on Moiré deflectometry. In the proposed method two lasers are used: a low power, wide beam as probe and a high power with specific wavelength as a pump. Interaction of the pump laser beam with the nonlinear sample changes the refractive index, which leads to change in convergence/divergence of the collimated incident probe laser beam. The induced deflection is monitored by Moiré deflectometry. If the pump laser has a Gaussian intensity profile, the refractive index profile of the sample is Gaussian, too. Measuring the deflection angle of the probe beam by Moiré fringes deflection, and by using the inverse Abel transform integral, the refractive index profile and nonlinear refractive index can be determined. This method is fast, easy, and insensitive to environmental noise and allows real-time measurement. Also, the refractive index profile of the interacted medium with pump laser can be achieved by this technique. As a liquid sample, a DCJ dye in water solution was studied. The value of nonlinear refractive index, n₂, and absorption coefficient, α, were obtained -2.54×10^-4  cm² w^-1 and 1.368  cm^-1, respectively.

Method of determining dispersion dependence of refractive index of nanospheres building opals

NASA Astrophysics Data System (ADS)

Kępińska, Mirosława; Starczewska, Anna; Duka, Piotr

2017-11-01

The method of determining dispersion dependence of refractive index of nanospheres building opals is presented. In this method basing on angular dependences of the spectral positions of Bragg diffraction minima on transmission spectra for opal series of known spheres diameter, the spectrum of effective refractive index for opals and then refractive index for material building opal's spheres is determined. The described procedure is used for determination of neff(λ) for opals and nsph(λ) for material which spheres building investigated opals are made of. The obtained results are compared with literature data of nSiO2(λ) considered in the analysis and interpretation of extremes related to the light diffraction at (hkl) SiO2 opal planes.

Index of Refraction Measurements and Window Corrections for PMMA under Shock Compression

NASA Astrophysics Data System (ADS)

Chapman, David; Eakins, Daniel; Williamson, David; Proud, William

2011-06-01

Symmetric plate impact experiments were performed to investigate the change in the refractive index of PMMA under shock loading. Flyer and target geometries allowed the measurement of shock velocity, particle velocity, and refractive index in the shocked state, using the simultaneous application of VISAR (532 nm) and Het-V (1550 nm). The change in refractive index of PMMA as a function of density is generally considered to be well described by the Gladstone-Dale relationship, meaning that the ``apparent'' velocity measured by a laser velocity interferometer is the ``true'' velocity, and hence there is no window correction. The results presented characterise the accuracy of this assumption at peak stresses up to 2 GPa.

Refractive Index Dispersion in Ternary Germanate Glasses

NASA Astrophysics Data System (ADS)

Sakaguchi, Shigeki; Todoroki, Shinichi; Rigout, Nathalie

1995-10-01

The refractive index dispersion in germanate oxyfluoride glasses of GeO2-P2O5-MF2 (M=Ca, Zn), which are developed for optical fiber application, is investigated in the 0.4-4 µ m wavelength range by the minimum deviation method. The prepared glasses have a GeO2 content varying from 80 to 30 mol%. The dispersion curves for these glasses tend to shift to shorter wavelengths as the GeO2 content is decreased. Material dispersions are also derived from the refractive index measurements and the zero-material dispersion wavelengths (λ0) are found in the vicinity of 1.5 µ m. On the basis of the empirical relationship between λ0 and the minimum loss wavelength (λ0), the λ min values are located at around 1.8 µ m. A minimum loss of as low as 0.08 dB/km is expected for the present germanate glasses.

Perfect X-ray focusing via fitting corrective glasses to aberrated optics.

PubMed

Seiboth, Frank; Schropp, Andreas; Scholz, Maria; Wittwer, Felix; Rödel, Christian; Wünsche, Martin; Ullsperger, Tobias; Nolte, Stefan; Rahomäki, Jussi; Parfeniukas, Karolis; Giakoumidis, Stylianos; Vogt, Ulrich; Wagner, Ulrich; Rau, Christoph; Boesenberg, Ulrike; Garrevoet, Jan; Falkenberg, Gerald; Galtier, Eric C; Ja Lee, Hae; Nagler, Bob; Schroer, Christian G

2017-03-01

Due to their short wavelength, X-rays can in principle be focused down to a few nanometres and below. At the same time, it is this short wavelength that puts stringent requirements on X-ray optics and their metrology. Both are limited by today's technology. In this work, we present accurate at wavelength measurements of residual aberrations of a refractive X-ray lens using ptychography to manufacture a corrective phase plate. Together with the fitted phase plate the optics shows diffraction-limited performance, generating a nearly Gaussian beam profile with a Strehl ratio above 0.8. This scheme can be applied to any other focusing optics, thus solving the X-ray optical problem at synchrotron radiation sources and X-ray free-electron lasers.

Perfect X-ray focusing via fitting corrective glasses to aberrated optics

PubMed Central

Seiboth, Frank; Schropp, Andreas; Scholz, Maria; Wittwer, Felix; Rödel, Christian; Wünsche, Martin; Ullsperger, Tobias; Nolte, Stefan; Rahomäki, Jussi; Parfeniukas, Karolis; Giakoumidis, Stylianos; Vogt, Ulrich; Wagner, Ulrich; Rau, Christoph; Boesenberg, Ulrike; Garrevoet, Jan; Falkenberg, Gerald; Galtier, Eric C.; Ja Lee, Hae; Nagler, Bob; Schroer, Christian G.

2017-01-01

Due to their short wavelength, X-rays can in principle be focused down to a few nanometres and below. At the same time, it is this short wavelength that puts stringent requirements on X-ray optics and their metrology. Both are limited by today's technology. In this work, we present accurate at wavelength measurements of residual aberrations of a refractive X-ray lens using ptychography to manufacture a corrective phase plate. Together with the fitted phase plate the optics shows diffraction-limited performance, generating a nearly Gaussian beam profile with a Strehl ratio above 0.8. This scheme can be applied to any other focusing optics, thus solving the X-ray optical problem at synchrotron radiation sources and X-ray free-electron lasers. PMID:28248317

Refractive index modulation in LiNbO3: MgO slab through Lamb wave

NASA Astrophysics Data System (ADS)

Prakash, Suraj; Sharma, Gaurav; Yadav, Gulab Chand; Singh, Vivek

2018-05-01

Present theoretical analysis deals with inducing refractive index contrast in Y-Z LiNbO3:MgO plate via GHz Lamb wave perturbation for photonic applications. Dispersion curves for Lamb wave in plate are plotted by employing displacement potential technique. Selecting wave parameters from dispersion curve, fundamental symmetric Lamb mode (S0) is excited in slab for 6GHz frequency. Produced displacement field by propagating S0 mode and thus developed strain is estimated to calculate refractive index modulation by applying photo-elastic relations. Modulated refractive index is of sinusoidal nature with period of modulation dependence on Lamb's wavelength. This plate having periodically modulated refractive index can be used as photonic crystal for different applications with acoustically tunable photonic band gap.

Asymmetric nanofluidic grating detector for differential refractive index measurement and biosensing.

PubMed

Purr, F; Bassu, M; Lowe, R D; Thürmann, B; Dietzel, A; Burg, T P

2017-12-05

Measuring small changes in refractive index can provide both sensitive and contactless information on molecule concentration or process conditions for a wide range of applications. However, refractive index measurements are easily perturbed by non-specific background signals, such as temperature changes or non-specific binding. Here, we present an optofluidic device for measuring refractive index with direct background subtraction within a single measurement. The device is comprised of two interdigitated arrays of nanofluidic channels designed to form an optical grating. Optical path differences between the two sets of channels can be measured directly via an intensity ratio within the diffraction pattern that forms when the grating is illuminated by a collimated laser beam. Our results show that no calibration or biasing is required if the unit cell of the grating is designed with an appropriate built-in asymmetry. In proof-of-concept experiments we attained a noise level equivalent to ∼10 -5 refractive index units (30 Hz sampling rate, 4 min measurement interval). Furthermore, we show that the accumulation of biomolecules on the surface of the nanochannels can be measured in real-time. Because of its simplicity and robustness, we expect that this inherently differential measurement concept will find many applications in ultra-low volume analytical systems, biosensors, and portable devices.

Plasmonic refractive index sensing using strongly coupled metal nanoantennas: nonlocal limitations.

PubMed

Wang, Hancong

2018-06-25

Localized surface plasmon resonance based on coupled metallic nanoparticles has been extensively studied in the refractive index sensing and the detection of molecules. The amount of resonance peak-shift depends on the refractive index of surrounding medium and the geometry/symmetry of plasmonic oligomers. It has recently been found that as the feature size or the gap distance of plasmonic nanostructures approaches several nanometers, quantum effects can change the plasmon coupling in nanoparticles. However, most of the research on plasmonic sensing has been done based on classical local calculations even for the interparticle gap below ~3 nm, in which the nonlocal screening plays an important role. Here, we theoretically investigate the nonlocal effect on the evolution of various plasmon resonance modes in strongly coupled nanoparticle dimer and trimer antennas with the gap down to 1 nm. Then, the refractive index sensing in these nonlocal systems is evaluated and compared with the results in classical calculations. We find that in the nonlocal regime, both refractive index sensibility factor and figure of merit are actually smaller than their classical counterparts mainly due to the saturation of plasmon shifts. These results would be beneficial for the understanding of interaction between light and nonlocal plasmonic nanostructures and the development of plasmonic devices such as nanosensors and nanoantennas.

Signal Enhancement Strategies for Refractive Index-Sensitive Nanobiosensor.

PubMed

Syahir, Amir; Kajikawa, Kotaro; Mihara, Hisakazu

2018-01-01

Direct bio-monitoring essentially involves optical means since photon has insignificant effects over biomolecules. Over the years, laser induced surface Plasmon resonance method with various modifications as well as versatile localized Plasmon excited by incoherent light have facilitated in recording many nanobiological activities. Yet, monitoring interactions of small molecules including drugs requires signal amplification and improvement on signal-to-noise ratio. This paper focused on how the refractive index based nanobio-sensoring gold platform can produce more efficient, adaptable and more practical detection techniques to observe molecular interactions at high degree of sensitivity. It discusses surface chemistry approach, optimisation of the refractive index of gold platform and manipulation of gold geometry augmenting signal quality. In a normal-incidence reflectivity, r0 can be calculated using the Fresnel equation. Particularly at λ = 470 nm the ratio of r / r0 showed significant amplitude reduction mainly stemmed from the imaginary part of the Au refractive index. Hence, the fraction of reduction, Δr = 1 - r / r0. Experimentally, in a common reference frame reflectivity of a bare gold surface, R0 is compared with the reflectivity of gold surface in the presence of biolayer, R. The reduction rate (%) of reflectivity, ΔR = 1 - R / R0 is denoted as the AR signal. The method therefore enables quantitative measurement of the surface-bound protein by converting ΔR to the thickness, d, and subsequently the protein mass. We discussed four strategies to improve the AR signal by changing the effective refractive index of the biosensing platform. They are; a) Thickness optimisation of Au thin layer, b) Au / Ag bimetallic layer, c) composing alloy or Au composite, and d) Au thinlayer with nano or micro holes. As the result we successfully 'move' the refractive index, ε of the AR platform (gold only) to ε = -0.948 + 3.455i, a higher sensitivity platform. This

Cover-layer with High Refractive Index for Near-Field Recording Media

NASA Astrophysics Data System (ADS)

Kim, Jin-Hong; Lee, Jun-Seok

2007-06-01

TiO2 nanoparticles are added into UV-curable resin to increase the refractive index of the cover-layer laminated for cover-layer incident near-field recording media. A high refractive index is required for the cover-layer operating with an optical head with a high numerical aperture. The eye pattern from a cover-layer coated 20 GB read-only memory disc in which the refractive index of the cover-layer is 1.75 is achieved, but the gap servo is unstable owing to the rough surface of the cover-layer. Even though the light loss due to the nanoparticles is negligible, a rough microstructure is developed by adding the nanoparticles into an organic binder material. To achieve a smooth surface for a stable gap servo, the solubility of the nanoparticles should be enhanced by the optimization of the surface of the nanoparticles.

Cover-Layer with High Refractive Index for Near-Field Recording Media

NASA Astrophysics Data System (ADS)

Kim, Jin-Hong; Lee, Jun-Seok

2007-06-01

TiO2 nanoparticles are added into UV-curable resin to increase the refractive index of the cover-layer laminated for cover-layer incident near-field recording media. A high refractive index is required for the cover-layer operating with an optical head with a high numerical aperture. The eye pattern from a cover-layer coated 20 GB read-only memory disc in which the refractive index of the cover-layer is 1.75 is achieved, but the gap servo is unstable owing to the rough surface of the cover-layer. Even though the light loss due to the nanoparticles is negligible, a rough microstructure is developed by adding the nanoparticles into an organic binder material. To achieve a smooth surface for a stable gap servo, the solubility of the nanoparticles should be enhanced by the optimization of the surface of the nanoparticles.

Refractive Index Measurement of Fibers Through Fizeau Interferometry

DTIC Science & Technology

2013-08-01

15. SUBJECT TERMS composite, transparent, refractive index, refractometry , interferometer 16. SECURITY CLASSIFICATION OF: 17. LIMITATION OF...transparent fibers has long presented a significant challenge. Abbe refractometry , the typical measurement technique for bulk materials and liquids

Planar optical waveguides for optical panel having gradient refractive index core

DOEpatents

Veligdan, James T.

2001-01-01

An optical panel is disclosed. A plurality of stacked planar optical waveguides are used to guide light from an inlet face to an outlet face of an optical panel. Each of the optical waveguides comprises a planar sheet of core material having a central plane. The core material has an index of refraction which decreases as the distance from the central plane increases. The decrease in the index of refraction occurs gradually and continuously.

Planar optical waveguides for optical panel having gradient refractive index core

DOEpatents

Veligdan, James T.

2004-08-24

An optical panel is disclosed. A plurality of stacked planar optical waveguides are used to guide light from an inlet face to an outlet face of an optical panel. Each of the optical waveguides comprises a planar sheet of core material having a central plane. The core material has an index of refraction which decreases as the distance from the central plane increases. The decrease in the index of refraction occurs gradually and continuously.

Beam tracking approach for single–shot retrieval of absorption, refraction, and dark-field signals with laboratory  x-ray sources

DOE Office of Scientific and Technical Information (OSTI.GOV)

Vittoria, Fabio A., E-mail: fabio.vittoria.12@ucl.ac.uk; Diemoz, Paul C.; Olivo, Alessandro

We present the translation of the beam tracking approach for x-ray phase-contrast and dark-field imaging, recently demonstrated using synchrotron radiation, to a laboratory setup. A single absorbing mask is used before the sample, and a local Gaussian interpolation of the beam at the detector is used to extract absorption, refraction, and dark–field signals from a single exposure of the sample. Multiple exposures can be acquired when high resolution is needed, as shown here. A theoretical analysis of the effect of polychromaticity on the retrieved signals, and of the artifacts this might cause when existing retrieval methods are used, is alsomore » discussed.« less

Micro X-ray diffraction analysis of thin films using grazing-exit conditions.

PubMed

Noma, T; Iida, A

1998-05-01

An X-ray diffraction technique using a hard X-ray microbeam for thin-film analysis has been developed. To optimize the spatial resolution and the surface sensitivity, the X-ray microbeam strikes the sample surface at a large glancing angle while the diffracted X-ray signal is detected with a small (grazing) exit angle. Kirkpatrick-Baez optics developed at the Photon Factory were used, in combination with a multilayer monochromator, for focusing X-rays. The focused beam size was about 10 x 10 micro m. X-ray diffraction patterns of Pd, Pt and their layered structure were measured. Using a small exit angle, the signal-to-background ratio was improved due to a shallow escape depth. Under the grazing-exit condition, the refraction effect of diffracted X-rays was observed, indicating the possibility of surface sensitivity.

Development and characterization of high refractive index and high scattering acrylate polymer layers

NASA Astrophysics Data System (ADS)

Eiselt, Thomas; Gomard, Guillaume; Preinfalk, Jan; Gleissner, Uwe; Lemmer, Uli; Hanemann, Thomas

2016-04-01

The aim is to develop a polymer layer which has the ability to diffuse light homogeneously and exhibit a high refractive index. The mixtures are containing an acrylate casting resin, benzylmethacrylate, phenanthrene and other additives. Phenanthrene is employed to increase the refractive index. The mixtures are first rheologically characterized and then polymerized with heat and UV radiation. For the refractive index measurements the polymerized samples require a planar surface without air bubbles. To produce flat samples a special construction consisting of a glass plate, a teflon sheet, a silicone ring (PDMS mold), another teflon sheet and another glass plate is developed. Glue clamps are used to fix this construction together. Selected samples have a refractive index of 1.585 at 20°C at a wavelength of 589nm. A master mixture with a high refractive index is taken for further experiments. Nano scaled titanium dioxide is added and dispersed into the master mixture and then spin coated on a glass substrate. These layers are optically characterized. The specular transmission and the overall transmission are measured to investigate the degree of scattering, which is defined as the haze. Most of the presented layers express the expected haze of over 50%.

Theoretical study of polarization insensitivity of carrier-induced refractive index change of multiple quantum well.

PubMed

Miao, Qingyuan; Zhou, Qunjie; Cui, Jun; He, Ping-An; Huang, Dexiu

2014-12-29

Characteristics of polarization insensitivity of carrier-induced refractive index change of 1.55 μm tensile-strained multiple quantum well (MQW) are theoretically investigated. A comprehensive MQW model is proposed to effectively extend the application range of previous models. The model considers the temperature variation as well as the nonuniform distribution of injected carrier in MQW. Tensile-strained MQW is expected to achieve polarization insensitivity of carrier-induced refractive index change over a wide wavelength range as temperature varies from 0°C to 40°C, while the magnitude of refractive index change keeps a large value (more than 3 × 10^-3). And that the polarization insensitivity of refractive index change can maintain for a wide range of carrier concentration. Multiple quantum well with different material and structure parameters is anticipated to have the similar polarization insensitivity of refractive index change, which shows the design flexibility.

Theory and applications of refractive index-based optical microscopy to measure protein mass transfer in spherical adsorbent particles.

PubMed

Bankston, Theresa E; Stone, Melani C; Carta, Giorgio

2008-04-25

This work provides the theoretical foundation and a range of practical application examples of a recently developed method to measure protein mass transfer in adsorbent particles using refractive index-based optical microscopy. A ray-theoretic approach is first used to predict the behavior of light traveling through a particle during transient protein adsorption. When the protein concentration gradient in the particle is sharp, resulting in a steep refractive index gradient, the rays bend and intersect, thereby concentrating light in a sharp ring that marks the position of the adsorption front. This behavior is observed when mass transfer is dominated by pore diffusion and the adsorption isotherm is highly favorable. Applications to protein cation-exchange, hydrophobic interaction, and affinity adsorption are then considered using, as examples, the three commercial, agarose-based stationary phases SP-Sepharose-FF, Butyl Sepharose 4FF, and MabSelect. In all three cases, the method provides results that are consistent with measurements based on batch adsorption and previously published data confirming its utility for the determination of protein mass transfer kinetics under a broad range of practically relevant conditions.

Spatial variation of stratospheric aerosol acidity and model refractive index - Implications of recent results

NASA Technical Reports Server (NTRS)

Russell, P. B.; Hamill, P.

1984-01-01

Recent experimental results indicate that little or no solid ammonium sulfate is present in background stratospheric aerosols. Other results allow straightforward calculation of sulfuric acid/water droplet properties (acidity, specific gravity, refractive index) as functions of stratospheric temperature and humidity. These results are combined with a variety of latitudinal and seasonal temperature and humidity profiles to obtain corresponding profiles of droplet properties. These profiles are used to update a previous model of stratospheric aerosol refractive index. The new model retains the simplifying approximation of vertically constant refractive index in the inner stratosphere, but has sulfuric acid/water refractive index values that significantly exceed the previously used room temperature values. Mean conversion ratios (e.g., extinction-to-number, backscatter-to-volume) obtained using Mie scattering calculations with the new refractive indices are very similar to those obtained for the old indices, because the effects of deleting ammonium sulfate and increasing acid indices tend to cancel each other.

High-refractive index polyacrylates based on quinolinone-structures for intraocular lenses

NASA Astrophysics Data System (ADS)

Dams, Christian; Helmstetter, Simon; Hampp, Norbert

2017-02-01

Intraocular lenses (IOL) have experienced an expanding application over the last decades. Not only they can be used to cure cataract caused blindness, but they are also appointed to ease visual impairments (e.g. -18 - 10 dioptre or astigmatism).[1] These phake IOL require materials with very high refractive indices due to the limited space at the implanting position in the eye of the patient. This enables less invasive operations and such with smaller incisions.[2] Quinolinone derivates, like carbostyril, are currently known from drug design and as a main structural component of several antibiotics.[3] Although they show high refractive indices and good dispersions they have not yet been used in materials for ophthalmic applications. We synthesized and characterized novel high refractive index polymers containing quinolinones as the main refractive unit of the structure.[4] We showed that it was possible to build quinolinone polymers with high refractive indices up to 1.685 at 589 nm. Using this material it would theoretically be possible to reduce the lens thickness of an IOL to under 40 percent compared to a commercial hydrogel lens with a refractive index of 1.470. We also used the synthesized quinolinone acrylates to create hydrophobic copolymers with improved physical properties and high transmission in the visible spectral range. Besides the good lightfastness these copolymers also showed very low tendencies of glistening. In conclusion quinolinones show attractive performances for the usage as a component in acrylic copolymers. If the requirements for IOL keep rising in the coming years these monomers could be used to boost the refractive index of ophthalmic polymer compositions.

Low-refractive-index dye-aggregate films with small absorption based on anomalous dispersion.

PubMed

Wakamatsu, Takashi; Watanabe, Keita; Saito, Kazuhiro

2005-02-20

Complex-refractive-index spectra of Squarylium (SQ) dye-aggregate films deposited upon metal films have been investigated by measurements of properties of the films including absorption spectra (AS) and attenuated total reflection. Complex refractive indices are estimated by Kramers-Kronig analysis for the AS and by a theoretical curve-fitting analysis for attenuated total reflection. The dye-aggregate films exhibited an absorption that was blueshifted from that of a monomer, as a result of the H-aggregate formation of SQ molecules, and had a changing refractive index with anomalous dispersion about the H-absorption band. From both measurements of the SQ films it was found that there is a region of low absorption in the short-wavelength side of the absorption band and that the refractive index there is lower than that of glass.

Low-refractive-index dye-aggregate films with small absorption based on anomalous dispersion

NASA Astrophysics Data System (ADS)

Wakamatsu, Takashi; Watanabe, Keita; Saito, Kazuhiro

2005-02-01

Complex-refractive-index spectra of Squarylium (SQ) dye-aggregate films deposited upon metal films have been investigated by measurements of properties of the films including absorption spectra (AS) and attenuated total reflection. Complex refractive indices are estimated by Kramers-Kronig analysis for the AS and by a theoretical curve-fitting analysis for attenuated total reflection. The dye-aggregate films exhibited an absorption that was blueshifted from that of a monomer, as a result of the H-aggregate formation of SQ molecules, and had a changing refractive index with anomalous dispersion about the H-absorption band. From both measurements of the SQ films it was found that there is a region of low absorption in the short-wavelength side of the absorption band and that the refractive index there is lower than that of glass.

Elemental mapping and microimaging by x-ray capillary optics.

PubMed

Hampai, D; Dabagov, S B; Cappuccio, G; Longoni, A; Frizzi, T; Cibin, G; Guglielmotti, V; Sala, M

2008-12-01

Recently, many experiments have highlighted the advantage of using polycapillary optics for x-ray fluorescence studies. We have developed a special confocal scheme for micro x-ray fluorescence measurements that enables us to obtain not only elemental mapping of the sample but also simultaneously its own x-ray imaging. We have designed the prototype of a compact x-ray spectrometer characterized by a spatial resolution of less than 100 microm for fluorescence and less than 10 microm for imaging. A couple of polycapillary lenses in a confocal configuration together with a silicon drift detector allow elemental studies of extended samples (approximately 3 mm) to be performed, while a CCD camera makes it possible to record an image of the same samples with 6 microm spatial resolution, which is limited only by the pixel size of the camera. By inserting a compound refractive lens between the sample and the CCD camera, we hope to develop an x-ray microscope for more enlarged images of the samples under test.

Simulation of imperfections in plastic lenses - transferring local refractive index changes into surface shape modifications

NASA Astrophysics Data System (ADS)

Arasa, Josep; Pizarro, Carles; Blanco, Patricia

2016-06-01

Injection molded plastic lenses have continuously improved their performance regarding optical quality and nowadays are as usual as glass lenses in image forming devices. However, during the manufacturing process unavoidable fluctuations in material density occur, resulting in local changes in the distribution of refractive index, which degrade the imaging properties of the polymer lens. Such material density fluctuations correlate to phase delays, which opens a path for their mapping. However, it is difficult to transfer the measured variations in refractive index into conventional optical simulation tool. Thus, we propose a method to convert the local variations in refractive index into local changes of one surface of the lens, which can then be described as a free-form surface, easy to introduce in conventional simulation tools. The proposed method was tested on a commercial gradient index (GRIN) lens for a set of six different object positions, using the MTF sagittal and tangential cuts to compare the differences between the real lens and a lens with homogenous refractive index, and the last surface converted into a free-form shape containing the internal refractive index changes. The same procedure was used to reproduce the local refractive index changes of an injected plastic lens with local index changes measured using an in-house built polariscopic arrangement, showing the capability of the method to provide successful results.

Optical Enhancement in Optoelectronic Devices Using Refractive Index Grading Layers.

PubMed

Lee, Illhwan; Park, Jae Yong; Gim, Seungo; Kim, Kisoo; Cho, Sang-Hwan; Choi, Chung Sock; Song, Seung-Yong; Lee, Jong-Lam

2016-02-10

We enhanced the optical transmittance of a multilayer barrier film by inserting a refractive index grading layer (RIGL). The result indicates that the Fresnel reflection, induced by the difference of refractive indices between Si(x)N(y) and SiO2, is reduced by the RIGL. To eliminate the Fresnel reflection while maintaining high transmittance, the optimized design of grading structures with the RIGL was conducted using an optical simulator. With the RIGL, we achieved averaged transmittance in the visible wavelength region by 89.6%. It is found that the optimized grading structure inserting the multilayer barrier film has a higher optical transmittance (89.6%) in the visible region than that of a no grading sample (82.6%). Furthermore, luminance is enhanced by 14.5% (from 10,190 to 11,670 cd m(-2) at 30 mA cm(-2)) when the grading structure is applied to organic light-emitting diodes. Finally, the results offer new opportunities in development of multilayer barrier films, which assist industrialization of very cost-effective flexible organic electronic devices.

Development of optics for x-ray phase-contrast imaging of high energy density plasmas.

PubMed

Stutman, D; Finkenthal, M; Moldovan, N

2010-10-01

Phase-contrast or refraction-enhanced x-ray radiography can be useful for the diagnostic of low-Z high energy density plasmas, such as imploding inertial confinement fusion (ICF) pellets, due to its sensitivity to density gradients. To separate and quantify the absorption and refraction contributions to x-ray images, methods based on microperiodic optics, such as shearing interferometry, can be used. To enable applying such methods with the energetic x rays needed for ICF radiography, we investigate a new type of optics consisting of grazing incidence microperiodic mirrors. Using such mirrors, efficient phase-contrast imaging systems could be built for energies up to ∼100 keV. In addition, a simple lithographic method is proposed for the production of the microperiodic x-ray mirrors based on the difference in the total reflection between a low-Z substrate and a high-Z film. Prototype mirrors fabricated with this method show promising characteristics in laboratory tests.

Design of embedded system to determine liquid refractive index based on ultrasonic sensor using an ATMega328

NASA Astrophysics Data System (ADS)

Radiyonoa, Y.; Surantoro, S.; Pujayanto, P.; Budiharti, R.; Respati, Y. S.; Saputro, D. E.

2018-05-01

The occurrence of the broken pencil shadow into a glass of water becomes an interesting matter to be learned. The students of senior high school still find difficulty in determining liquid refractive index. To overcome this problem, it needs to develop an experimental tool to determine liquid refractive index by utilizing the newest technology. It is expected to be useful for students. This study is aimed to (1) make the design of physics learning experimental tool determinant of a liquid refractive index assisted by microcontroller based on ultrasonic sensors ATMega328 (2) explain the working principle and experimental result of liquid refractive indexing instrument assisted with ATMega328 microcontroller based ultrasonic sensor. This research used the experimental method. The result of the research shows design of physics learning experimental tool determinant of a liquid refractive index assisted by microcontroller based on ultrasonic sensors ATMega328 that has relative counting mistake of 0.36% on the measurement of aquades liquid refractive index, relative mistake of 0.18% on the 5% NaCl measurement, 0.24% on 5% glucose, and relative mistake of 0.50% on the measurement of 5 % fructose liquid refractive index. It has been created a proper device to be used in determining liquid refractive index.

Real refractive indices and formation yields of secondary organic aerosol generated from photooxidation of limonene and α-pinene: the effect of the HC/NO(x) ratio.

PubMed

Kim, Hwajin; Barkey, Brian; Paulson, Suzanne E

2012-06-21

The refractive index is an important property affecting aerosol optical properties, which in turn help determine the aerosol direct effect and satellite retrieval results. Here, we investigate the real refractive indices (m(r)) of secondary organic aerosols (SOA) generated from the photooxidation of limonene and α-pinene with different HC/NO(x) ratios. Refractive indices were obtained from polar nephelometer data using parallel and perpendicular polarized 532 nm light combined with measured size distributions, and retrievals were performed using a genetic algorithm and Mie-Lorenz scattering theory. The absolute error associated with the m(r) retrieval is ±0.03, and reliable retrievals are possible for mass concentrations above 5-20 μg/m(3) depending on particle size. The limonene SOA data suggest the most important factor controlling the refractive index is the HC/NO(x) ratio; the refractive index is much less sensitive to the aerosol age or mass concentration. The refractive index ranges from about 1.34 to 1.56 for limonene and from 1.36 to 1.52 for α-pinene, and generally decreases as the HC/NO(x) ratio increases. Especially for limonene, the particle diameter is also inversely related to the HC/NO(x) ratio; the final size mode increases from 220 to 330 nm as the HC/NO(x) ratio decreases from 33 to 6. In an effort to explore the ability of models from the literature to explain the observed refractive indices, a recent limonene oxidation mechanism was combined with SOA partitioning and a structure-property relationship for estimating refractive indices of condensing species. The resulting refractive indices fell in a much narrower range (1.475 ± 0.02) of m(r) than observed experimentally. We hypothesize the experimentally observed high m(r) values are due to oligomerization and the low values to water uptake, small soluble molecules such as glyoxal and other factors, each of which is not included in the oxidation mechanism. Aerosol formation yields were

Complex refractive index of starch acetate used as a biodegradable pigment and filler of paper

NASA Astrophysics Data System (ADS)

Karvinen, Petri; Oksman, Antti; Silvennoinen, Raimo; Mikkonen, Hannu

2007-05-01

Complex refractive index of strongly depolarizing starch acetate is investigated as a function of bulk package density, which is compulsory parameter in analysis of light scattering from nanoscale starch acetate pigments and fillers. The measurements were made using a laser-goniometer and spectrophotometer to gain data for refractive index analysis according to the Brewster's law and Fresnel equations. The real part of refractive index was verified by microscopic immersion method.

Refractometry studies of the optical properties of polymer films and the development of polymer coated refractive index sensors

NASA Astrophysics Data System (ADS)

Saunders, John Edward

Sensors for real-time monitoring of environmental contaminants are essential for protecting ecosystems and human health. Refractive index sensing is a non-selective technique that can be used to measure almost any analyte. Miniaturized refractive index sensors, such as silicon-on-insulator (SOI) microring resonators are one possible platform, but require coatings selective to the analytes of interest. A homemade prism refractometer is reported and used to characterize the interactions between polymer films and liquid or vapour-phase analytes. A camera was used to capture both Fresnel reflection and total internal reflection within the prism. For thin-films (d = 10 μm - 100 μm), interference fringes were also observed. Fourier analysis of the interferogram allowed for simultaneous extraction of the average refractive index and film thickness with accuracies of Δn = 1-7 x10-4 and Δd < 3-5%. The refractive indices of 29 common organic solvents as well as aqueous solutions of sodium chloride, sucrose, ethylene glycol, glycerol, and dimethylsulfoxide were measured at λ = 1550 nm. These measurements will be useful for future calibrations of near-infrared refractive index sensors. A mathematical model is presented, where the concentration of analyte adsorbed in a film can be calculated from the refractive index and thickness changes during uptake. This model can be used with Fickian diffusion models to measure the diffusion coefficients through the bulk film and at the film-substrate interface. The diffusion of water and other organic solvents into SU-8 epoxy was explored using refractometry and the diffusion coefficient of water into SU-8 is presented. Exposure of soft baked SU-8 films to acetone, acetonitrile and methanol resulted in rapid delamination. The diffusion of volatile organic compound (VOC) vapours into polydimethylsiloxane and polydimethyl-co-polydiphenylsiloxane polymers was also studied using refractometry. Diffusion and partition coefficients are

Concentration dependent refractive index of a binary mixture at high pressure.

PubMed

Croccolo, Fabrizio; Arnaud, Marc-Alexandre; Bégué, Didier; Bataller, Henri

2011-07-21

In the present work binary mixtures of varying concentrations of two miscible hydrocarbons, 1,2,3,4-tetrahydronaphtalene (THN) and n-dodecane (C12), are subjected to increasing pressure up to 50 MPa in order to investigate the dependence of the so-called concentration contrast factor (CF), i.e., (∂n/∂c)(p, T), on pressure level. The refractive index is measured by means of a Mach-Zehnder interferometer. The setup and experimental procedure are validated with different pure fluids in the same pressure range. The refractive index of the THN-C12 mixture is found to vary both over pressure and concentration, and the concentration CF is found to exponentially decrease as the pressure is increased. The measured values of the refractive index and the concentration CFs are compared with values obtained by two different theoretical predictions, the well-known Lorentz-Lorenz formula and an alternative one proposed by Looyenga. While the measured refractive indices agree very well with predictions given by Looyenga, the measured concentration CFs show deviations from the latter of the order of 6% and more than the double from the Lorentz-Lorenz predictions.

Effects of film thickness on the linear and nonlinear refractive index of p-type SnO films deposited by e-beam evaporation process

NASA Astrophysics Data System (ADS)

El-Gendy, Y. A.

2017-12-01

Tin monoxide (SnO) films of different thickness have been deposited onto glass substrates at vacuum pressure of ∼ 8 × 10-6 mbar using an e-beam evaporation system. A hot probe test revealed that the deposited films showed p-type conduction. The structure characterization and phase purity of the deposited films was confirmed using X-ray diffraction (XRD) and Raman spectroscopy. The optical transmission and reflection spectra of the deposited films recorded in the wavelength range 190-2500 nm were used to calculate the optical constants employing the Murmann's exact equations. The refractive index dispersion was adequately described by the well-known effective-single-oscillator model proposed by Wemple-DiDomenico, whereby the dispersion parameters were calculated. The nonlinear refractive index and nonlinear optical susceptibility of the deposited films were successfully evaluated using the Miller empirical relations. The lattice dielectric constant and the carrier concentration to the effective mass ratio were also calculated as a function of film thickness using the Spitzer and Fan model. The variation of the optical band gap of the deposited films as a function of film thickness was also presented.

Perfect X-ray focusing via fitting corrective glasses to aberrated optics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Seiboth, Frank; Schropp, Andreas; Scholz, Maria

2017-03-01

Due to their short wavelength, X-rays can in principle be focused down to a few nanometres and below. At the same time, it is this short wavelength that puts stringent requirements on X-ray optics and their metrology. Both are limited by today’s technology. In this work, we present accurate at wavelength measurements of residual aberrations of a refractive X-ray lens using ptychography to manufacture a corrective phase plate. Together with the fitted phase plate the optics shows diffraction-limited performance, generating a nearly Gaussian beam profile with a Strehl ratio above 0.8. As a result, this scheme can be applied tomore » any other focusing optics, thus solving the X-ray optical problem at synchrotron radiation sources and X-ray free-electron lasers.« less

Simultaneous measurement of refractive index and temperature based on all-dielectric metasurface.

PubMed

Hu, Jie; Lang, Tingting; Shi, Guo-Hua

2017-06-26

In this paper, a novel kind of sensors for simultaneous measurement of refractive index and temperature based on all-dielectric metasurfaces is proposed. The metasurfaces are constructed by an array of silicon nanoblocks on top of the bulk fused silica substrate. We used three-dimensional full wave electromagnetic field simulation by finite integral method to accurately calculate the transmission spectrum of the metasurfaces. Two transmission dips corresponding to the electric and magnetic resonances are observed. Both dips shift as the ambient refractive index or the temperature changes. Simulation results show that the sensing sensitivities of two dips to the refractive index are 243.44 nm/RIU and 159.43 nm/RIU, respectively, while the sensitivities to the temperature are 50.47 pm/°C and 75.20 pm/°C, respectively. After introducing four holes into each silicon nanoblock, the electromagnetic field overlap in the surrounding medium can be further promoted, and the sensitivities to the refractive index increase to 306.71 nm/RIU and 204.27 nm/RIU, respectively. Our proposed sensors have advantages of polarization insensitive, small size, and low loss, which offer them high potential applications in physical, biological and chemical sensing fields.

Zero refractive index in time-Floquet acoustic metamaterials

NASA Astrophysics Data System (ADS)

Koutserimpas, Theodoros T.; Fleury, Romain

2018-03-01

New scientific investigations of artificially structured materials and experiments have exhibited wave manipulation to the extreme. In particular, zero refractive index metamaterials have been on the front line of wave physics research for their unique wave manipulation properties and application potentials. Remarkably, in such exotic materials, time-harmonic fields have an infinite wavelength and do not exhibit any spatial variations in their phase distribution. This unique feature can be achieved by forcing a Dirac cone to the center of the Brillouin zone ( Γ point), as previously predicted and experimentally demonstrated in time-invariant metamaterials by means of accidental degeneracy between three different modes. In this article, we propose a different approach that enables true conical dispersion at Γ with twofold degeneracy and generates zero index properties. We break time-reversal symmetry and exploit a time-Floquet modulation scheme to demonstrate a time-Floquet acoustic metamaterial with zero refractive index. This behavior, predicted using stroboscopic analysis, is confirmed by full-wave finite element simulations. Our results establish the relevance of time-Floquet metamaterials as a novel reconfigurable platform for wave control.